Table 4.
Validation parameters of the ICP-MS method aimed at determining trace element and toxic metal concentrations in whole blood.
Element | Limit of detection (ng/g) | Limits of quantification (ng/g) | Maximum linear concentrations | Recovery (%) | Precision coefficient of variation (%) |
---|---|---|---|---|---|
Fe | 40 | 130 | 250 | 99 | 5.5 |
Cu | 1.5 | 5 | 250 | 89 | 5.3 |
Mn | 0.4 | 1.3 | 250 | 97 | 5.5 |
Zn | 150 | 500 | 250 | 97 | 6.0 |
Se | 1 | 3 | 250 | 95 | 5.2 |
Cr | 1.5 | 5 | 250 | 116 | 8.8 |
Pb | 0.4 | 1.3 | 250 | 97 | 2.0 |
Hg | 0.04 | 0.13 | 10 | 93 | 5.2 |
Cd | 0.02 | 0.07 | 250 | 108 | 12 |
As | 0.2 | 0.7 | 250 | 98 | 6.1 |