Skip to main content
. 2023 Jan 13;28(2):821. doi: 10.3390/molecules28020821

Table 1.

The NMR data of compounds 13 and 6 (J in Hz).

No. 1 a 2 a 3 a 6 b
δ C δ H δ C δ H δ C δ H δ C δ H
1 166.9, C 164.5, C 164.3, C 166.1, C
2 124.2, C 120.7, C 120.3, C 121.4, C
3 126.3, CH 7.86, d (7.7) 126.6, CH 7.96, dd (7.7, 0.7) 126.3, CH 7.88, d (7.7) 126.8, CH 8.00, d (7.7)
4 124.2, CH 7.44, dd (7.7, 7.7) 124.4, CH 7.51, dd (7.7, 7.7) 124.5, CH 7.49, dd (7.7, 7.7) 123.9, CH 7.37, dd (7.7, 7.7)
5 113.7, CH 7.93, d (7.7) 115.1, CH 8.03, dd (7.7, 0.7) 114.9, CH 8.03, d (7.7) 114.6, CH 7.74, d (7.7)
6 149.2, C 149.2, C 149.4, C 150.1, C
7 140.5, C 140.8, C 140.6, C 141.8, C
8 163.7, C 164.2, C 164.3, C 165.1, C
9 105.6, C 113.3, C 105.1, C 107.1, C
10 139.7, C 139.5, C 139.9, C 140.0, C
11 146.8, C 147.0, C 146.8, C 147.2, C
12 112.5, CH 7.02, dd (7.7, 0.7) 112.4, CH 7.03, d (7.7) 112.6, CH 7.03, d (7.7) 112.1, CH 6.88, d (7.7)
13 114.9, CH 6.69, dd (7.7, 8.4) 114.9, CH 6.69, dd (7.7, 8.4) 115.1, CH 6.69, dd (7.7, 7.4) 115.4, CH 6.72, dd (7.7, 7.7)
14 119.5, CH 7.57, dd (8.4, 1.4) 119.4, CH 7.57, dd (8.4, 1.4) 119.4, CH 7.57, d (7.7) 120.3, CH 7.68, (7.7)
15 55.7, CH3 3.87, s 55.7, CH3 3.90, s 55.7, CH3 3.88, s 55.9, CH3 3.94, s
16 66.0, CH2 4.39, dd (11.2, 4.2); 4.27, dd (11.2, 5.6) 65.3, CH2 4.56, dd (14.0, 7.0) 52.4, CH3 4.03, s
17 69.2, CH 3.88, m 34.4, CH2 3.14, m
18 62.8, CH2 3.53, m 138.0, C
19 129.0, CH 7.38, d (7.7)
20 128.4, CH 7.31, dd (7.7, 7.7)
21 126.4, CH 7.22, dd (7.7, 7.7)
22 128.4, CH 7.31, dd (7.7, 7.7)
23 129.0, CH 7.38, d (7.7)

a 700 MHz for 1H, 175 MHz for 13C, DMSO-d6, b 700 MHz for 1H, 175 MHz for 13C, CDCl3, TMS as an internal standard.