Conventional solvent extraction |
Solid/solvent ratio: 1:6 g/g for 12 and 24 h at 50°C |
69.1% |
(31) |
Soxhlet extraction |
Sample amount: 15 g in acetone at 60°C for 8 h |
6.9 g curcumin/100 g sample |
(30, 32) |
|
10 g sample in 250 mL of ethanol for 8 h |
1.3 g curcumin/100 g sample |
|
Ultrasound- assisted extraction |
Solid/solvent ratio: 1:20 g/mL; solvent: acetone for 40 min at 40°C |
3.9 g curcumin/100 g sample |
(30, 32) |
|
Solid/solvent ratio: 1:3 g/L in acetone for 5 min |
71.4% |
|
|
Solid/solvent ratio 1:15–1:55; time: up to 1 h; solvent: ethanol, methanol, acetone, and ethyl acetate at 25–55°C |
72% |
|
Microwave- assisted extraction |
Solid/solvent ratio: 1:20 g/mL; in acetone for 0.5–3 min |
2.4 g curcumin/100 g sample |
(30, 34) |
|
Solid/solvent ratio: 1:3 g/L; in ethanol, acetone, water for 1–7 |
90% |
|
Subcritical water extraction |
Sample amount: 0.1 g; flow rate: 0.5 mL/min; 5.0 MPa; temperature: 180, 200, and 220°C; and pH: 1, 1.5, and 2 |
1.35 g curcumin/100 g |
(33, 35) |
|
Flow rate: 1, 2.5, and 4 mL/min; temperature: 90, 120, and 150°C; and particle size: 0.5, 1, and 1.5 mm |
90% |
|
|
Particle size: 0.6,0.71, 1, and 2 mm; temperature: 120–160°C; time: 6, 10, 14, 18, and 22 min |
76% |
|
Supercritical carbon dioxide |
10 g sample in ethanol, time: 240 min; pressure: 30 MPa; temperature: 50°C; flow rate 5 mL/min |
|
(34) |