Table 4.
Robustness of the suggested technique using (50, 5.0, 5.0 and 10 μg/mL of PAR, LVC, PHN and AMB, respectively).
Parameter | Concentration found (µg/mL) | % Found | ||||||
---|---|---|---|---|---|---|---|---|
PAR | LVC | PHN | AMB | PAR | LVC | PHN | AMB | |
Ethanol ratio, % | ||||||||
19 | 49.571 | 4.963 | 4.998 | 10.249 | 99.14 | 99.26 | 99.96 | 102.49 |
20 | 49.973 | 5.017 | 5.010 | 10.018 | 99.95 | 100.35 | 100.20 | 100.18 |
21 | 50.561 | 4.900 | 5.055 | 10.220 | 101.12 | 97.99 | 101.10 | 102.20 |
Mean | 100.07 | 99.20 | 100.42 | 101.63 | ||||
± S.D | 1.00 | 1.18 | 0.60 | 1.26 | ||||
%RSD | 1.00 | 1.19 | 0.60 | 1.24 | ||||
%Error | 0.57 | 0.69 | 0.34 | 0.71 | ||||
Acetonitrile ratio, % | ||||||||
4.5 | 48.953 | 5.081 | 4.926 | 9.903 | 97.91 | 101.61 | 98.52 | 99.03 |
5.0 | 49.973 | 5.017 | 5.010 | 10.018 | 99.95 | 100.35 | 100.20 | 100.18 |
5.5 | 50.190 | 5.139 | 5.080 | 10.128 | 100.38 | 102.77 | 101.60 | 101.28 |
Mean | 99.41 | 101.58 | 100.10 | 100.17 | ||||
± S.D | 1.32 | 1.21 | 1.54 | 1.13 | ||||
%RSD | 1.33 | 1.19 | 1.54 | 1.12 | ||||
%Error | 0.77 | 0.69 | 0.89 | 0.65 | ||||
pH | ||||||||
6.4 | 49.015 | 5.041 | 4.962 | 10.128 | 98.03 | 100.83 | 99.25 | 101.28 |
6.5 | 49.973 | 5.017 | 5.010 | 10.018 | 99.95 | 100.35 | 100.20 | 100.18 |
6.6 | 49.200 | 4.997 | 5.042 | 9.961 | 98.40 | 99.95 | 100.83 | 99.61 |
Mean | 98.79 | 100.38 | 100.09 | 100.36 | ||||
± S.D | 1.02 | 0.44 | 0.80 | 0.85 | ||||
%RSD | 1.03 | 0.44 | 0.80 | 0.85 | ||||
%Error | 0.59 | 0.25 | 0.46 | 0.49 |