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. 2023 Jan 28;13:1616. doi: 10.1038/s41598-023-28737-3

Table 4.

Robustness of the suggested technique using (50, 5.0, 5.0 and 10 μg/mL of PAR, LVC, PHN and AMB, respectively).

Parameter Concentration found (µg/mL) % Found
PAR LVC PHN AMB PAR LVC PHN AMB
Ethanol ratio, %
 19 49.571 4.963 4.998 10.249 99.14 99.26 99.96 102.49
 20 49.973 5.017 5.010 10.018 99.95 100.35 100.20 100.18
 21 50.561 4.900 5.055 10.220 101.12 97.99 101.10 102.20
 Mean 100.07 99.20 100.42 101.63
  ± S.D 1.00 1.18 0.60 1.26
%RSD 1.00 1.19 0.60 1.24
 %Error 0.57 0.69 0.34 0.71
Acetonitrile ratio, %
 4.5 48.953 5.081 4.926 9.903 97.91 101.61 98.52 99.03
 5.0 49.973 5.017 5.010 10.018 99.95 100.35 100.20 100.18
 5.5 50.190 5.139 5.080 10.128 100.38 102.77 101.60 101.28
 Mean 99.41 101.58 100.10 100.17
 ± S.D 1.32 1.21 1.54 1.13
 %RSD 1.33 1.19 1.54 1.12
 %Error 0.77 0.69 0.89 0.65
pH
 6.4 49.015 5.041 4.962 10.128 98.03 100.83 99.25 101.28
 6.5 49.973 5.017 5.010 10.018 99.95 100.35 100.20 100.18
 6.6 49.200 4.997 5.042 9.961 98.40 99.95 100.83 99.61
 Mean 98.79 100.38 100.09 100.36
 ± S.D 1.02 0.44 0.80 0.85
 %RSD 1.03 0.44 0.80 0.85
 %Error 0.59 0.25 0.46 0.49