Table 3.
Characterization of foaming process, foam properties, and summary of TGA results of foams
| x | Stirring time (sec) | Cream time (sec) | Gel time (sec) | Rise time (sec) | Apparent densitya (g/cm3) |
T5%, (°C) |
T50%, (°C) | Tmax1, (°C) | Tmax2, (°C) | Tmax3, (°C) | Residue (%) | |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| PU_x-20 | B | 6 | 11 | 22 | 35 | 0.094 | 236 | 441 | – | 357 | 571 | 0 |
| PET | 6 | 11 | 24 | 38 | 0.042 | 219 | 483 | – | 354 | 585 | 0 | |
| PU | 6 | 11 | 24 | 38 | 0.040 | 275 | 514 | – | 356 | 600 | 0 | |
| BPA | 6 | 12 | 30 | 60 | 0.061 | 265 | 449 | – | 373 | 577 | 0 | |
| PU_x–40 | B | 6 | 10 | 23 | 36 | 0.095 | 229 | 507 | – | 436 | 598 | 0 |
| PET | 6 | 11 | 23 | 38 | 0.050 | 227 | 501 | – | 353 | 584 | 0 | |
| PU | 6 | 11 | 24 | 38 | 0.065 | 237 | 469 | – | 345 | 585 | 0 | |
| BPA | 6 | 12 | 30 | 61 | 0.066 | 90 | 465 | 125 | 337 | 603 | 0 | |
| PU_x–60 | B | 6 | 12 | 24 | 35 | 0.096 | 98 | 482 | 110 | 356 | 581 | 0 |
| PET | 6 | 12 | 24 | 40 | 0.064 | 172 | 494 | 190 | 346 | 586 | 0 | |
| PU | 6 | 11 | 24 | 38 | 0.068 | 94 | 322 | 122 | 317 | 583 | 0 | |
| BPA | 6 | 12 | 31 | 64 | 0.075 | 58 | 547 | 89 | 286 | 610 | 0 | |
| PU_com | 5 | 10 | 23 | 37 | 0.047 | 238 | 501 | – | 354 | 584 | 0 |
aThe densities of foams were calculated by using the formula described in DIN 53479[50]