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. 2023 Jan 18;62(8):e202217809. doi: 10.1002/anie.202217809

Scheme 2.

Scheme 2

Synthesis of gluco iminosugars 24. Bn, benzyl; Tol, p‐tolyl; Trt, triphenylmethyl; DMAP, 4‐(dimethylamino)pyridine; PMB, p‐methoxybenzyl; TBAI, tetrabutylammonium iodide; DMF, N,N‐dimethylformamide; NIS, N‐iodosuccinimide; DMSO, dimethyl sulfoxide; MS, molecular sieves; DIPEA, N,N‐diisopropylethylamine; TFA, trifluoroacetic acid; Tf, trifluoromethanesulfonyl.