Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
Least-squares matrix: full | H-atom parameters constrained |
R[F2 > 2σ(F2)] = 0.062 | w = 1/[σ2(Fo2) + (0.0695P)2 + 1.2547P] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.186 | (Δ/σ)max < 0.001 |
S = 1.11 | Δρmax = 0.38 e Å−3 |
4026 reflections | Δρmin = −0.58 e Å−3 |
209 parameters | Extinction correction: SHELXL-2018/3 (Sheldrick 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
0 restraints | Extinction coefficient: 0.0115 (19) |