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. 2023 Jan 31;8(Pt 1):x230042. doi: 10.1107/S2414314623000421
Stoe IPDS 2T diffractometer 3038 independent reflections
Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus 2686 reflections with I > 2σ(I)
Detector resolution: 6.67 pixels mm-1 Rint = 0.023
rotation method, ω scans θmax = 28.1°, θmin = 2.7°
Absorption correction: integration (XRED; Stoe et al., 2019) h = −7→7
Tmin = 0.088, Tmax = 0.553 k = −11→11
8129 measured reflections l = −16→16