Table 1. Experimental details.
| Crystal data | |
| Chemical formula | C10H16Br2O2S |
| M r | 360.11 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 193 |
| a, b, c (Å) | 5.9685 (4), 8.9642 (6), 12.4927 (9) |
| α, β, γ (°) | 94.804 (6), 102.448 (5), 99.356 (5) |
| V (Å3) | 639.09 (8) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 6.49 |
| Crystal size (mm) | 0.67 × 0.39 × 0.08 |
| Data collection | |
| Diffractometer | Stoe IPDS 2T |
| Absorption correction | Integration (X-RED; Stoe et al., 2019 ▸) |
| T min, T max | 0.088, 0.553 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 8129, 3038, 2686 |
| R int | 0.023 |
| (sin θ/λ)max (Å−1) | 0.663 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.036, 0.089, 1.14 |
| No. of reflections | 3038 |
| No. of parameters | 140 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.28, −0.89 |