| Xcalibur, Sapphire3 diffractometer | 3169 reflections with I > 2σ(I) |
| Detector resolution: 16.1827 pixels mm-1 | Rint = 0.032 |
| ω scans | θmax = 30.0°, θmin = 3.3° |
| Absorption correction: multi-scan (CrysAlisPro; Agilent, 2014) | h = −19→20 |
| Tmin = 0.505, Tmax = 1.000 | k = −9→9 |
| 13393 measured reflections | l = −18→19 |
| 3918 independent reflections |
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