Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Cs(C9H11NO4P)(H2O)] |
| M r | 379.08 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 294 |
| a, b, c (Å) | 14.3676 (4), 6.8089 (2), 13.7336 (3) |
| β (°) | 90.549 (2) |
| V (Å3) | 1343.46 (6) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.88 |
| Crystal size (mm) | 0.5 × 0.3 × 0.2 |
| Data collection | |
| Diffractometer | Xcalibur, Sapphire3 |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
| T min, T max | 0.505, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 13393, 3918, 3169 |
| R int | 0.032 |
| (sin θ/λ)max (Å−1) | 0.703 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.033, 0.076, 1.03 |
| No. of reflections | 3918 |
| No. of parameters | 162 |
| No. of restraints | 3 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.52, −0.79 |