| Crystal data |
| Chemical formula |
[Sn(C6H5)3Cl(C18H15O4P)] |
|
M
r
|
711.71 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
295 |
|
a, b, c (Å) |
10.0455 (4), 12.0370 (5), 13.8304 (6) |
| α, β, γ (°) |
93.552 (4), 93.469 (3), 93.128 (3) |
|
V (Å3) |
1663.21 (12) |
|
Z
|
2 |
| Radiation type |
Ag Kα, λ = 0.56083 Å |
| μ (mm−1) |
0.50 |
| Crystal size (mm) |
0.40 × 0.24 × 0.16 |
| |
| Data collection |
| Diffractometer |
Stoe Stadivari |
| Absorption correction |
Multi-scan (X-AREA; Stoe & Cie, 2018 ▸) |
|
T
min, T
max
|
0.674, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
49761, 9400, 6297 |
|
R
int
|
0.032 |
| (sin θ/λ)max (Å−1) |
0.697 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.035, 0.097, 1.00 |
| No. of reflections |
9400 |
| No. of parameters |
388 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.76, −0.71 |
