Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C10H8FIN2O3S |
| M r | 382.14 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c (Å) | 5.0230 (5), 11.3241 (11), 11.5509 (11) |
| α, β, γ (°) | 103.081 (2), 96.742 (1), 97.860 (1) |
| V (Å3) | 626.43 (11) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.74 |
| Crystal size (mm) | 0.34 × 0.30 × 0.27 |
| Data collection | |
| Diffractometer | Bruker APEXII |
| Absorption correction | – |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 4073, 3207, 2315 |
| R int | 0.035 |
| (sin θ/λ)max (Å−1) | 0.673 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.055, 0.166, 1.11 |
| No. of reflections | 3207 |
| No. of parameters | 164 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.88, −1.39 |