Methods/software | Guinier (R g in ATSAS 2.1), P(r) GNOM 4.6 | |||||||
SAXS or SANS (%D2O) | SAXS | SANS (100) | SANS (90) | SANS (80) | SANS (40) | SANS (20) | SANS (10) | SANS (0) |
Guinier analysis | ||||||||
I(0) ± σ (SAXS, a.u.; SANS, cm−1) | 805 ± 5 | 0.530 ± 0.002 | 0.322 ± 0.003 | 0.1865 ± 0.0024 | 0.0677 ± 0.0015 | 0.2204 ± 0.0007 | 0.364 ± 0.005 | 0.545 ± 0.006 |
R g ± σ (Å) | 29.1 ± 0.3 | 24.7 ± 0.1 | 24.3 ± 0.3 | 22.5 ± 0.4 | 21.6 ± 0.9 | 29.1 ± 1.0 | 28.2 ± 0.5 | 28.3 ± 0.4 |
qR g range | 0.58–1.28 | 0.92–1.29 | 0.98–1.22 | 0.98–1.32 | 0.31–1.22 | 0.90–1.36 | 0.75–1.32 | 0.72–1.27 |
Pearson’s R for fit | −0.999 | −0.995 | −0.994 | −0.990 | −0.903 | −0.946 | −0.990 | −0.998 |
P(r) analysis | ||||||||
I(0) ± σ (SAXS, a.u.; SANS, cm−1) | 800 ± 2 | 0.5358 ± 0.0014 | 0.3217 ± 0.0015 | 0.1895 ± 0.0015 | 0.0703 ± 0.0014 | 0.2183 ± 0.0019 | 0.3665 ± 0.0030 | 0.5491 ± 0.0027 |
R g ± σ (Å) | 28.6 ± 0.1 | 25.1 ± 0.1 | 24.4 ± 0.1 | 23.2 ± 0.2 | 24.2 ± 0.6 | 28.9 ± 0.2 | 28.3 ± 0.2 | 28.7 ± 0.1 |
d max (Å) | 80 | 75 | 75 | 70 | 70 | 80 | 80 | 80 |
q-range (Å−1) | 0.02–0.299 | 0.024–0.479 | 0.028–0.479 | 0.032–0.479 | 0.015–0.480 | 0.0254–0.479 | 0.026–0.479 | 0.025–0.479 |
Reciprocal-space fit (χ2, CorMap P-value) | 0.95, 0.54 | 0.67, 0.48 | 0.43, 0.94 | 0.59, 0.04 | 0.55, 0.76 | 0.71, 0.47 | 0.98, 0.02 | 0.70, 0.74 |