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. 2023 Jan 18;23(3):1120. doi: 10.3390/s23031120

Table 4.

Experimental data for the determination of spectra reported in Figure 6. The V1b and VDQ volumes refer to an initial 1b solution with a concentration of 50.7 μg L−1 and diquat, DQ, solution with a concentration of 1650 μg L−1, respectively. The final volume of each solution was made up to a total volume of 4000 μL by fixing with the solvent mixture.

Entry V1b, μL VDQ, μL VTOT, μL [1b], μg L−1 [DQ], μg L−1 DQ/1b, mol/mol
1 2000 0 4000 25.4 0.0 0.0
2 2000 2 4000 25.4 0.8 0.1
3 2000 5 4000 25.4 2.1 0.3
4 2000 9 4000 25.4 3.7 0.5
5 2000 14 4000 25.4 5.8 0.8
6 2000 20 4000 25.4 8.3 1.2
7 2000 28 4000 25.4 11.6 1.6
8 2000 39 4000 25.4 16.1 2.3
9 2000 54 4000 25.4 22.3 3.1
10 2000 74 4000 25.4 30.5 4.3
11 2000 104 4000 25.4 42.9 6.1
12 2000 144 4000 25.4 59.4 8.4
13 2000 204 4000 25.4 84.2 11.9
14 2000 284 4000 25.4 117.2 16.6
15 2000 384 4000 25.4 158.4 22.4
16 2000 504 4000 25.4 207.9 29.4
17 2000 654 4000 25.4 269.8 38.1
18 2000 854 4000 25.4 352.3 49.8
19 2000 1254 4000 25.4 517.3 73.1
20 2000 1574 4000 25.4 649.3 91.8