Table 6. Selected Bond Lengths and Angles from Compound 8.
| bond lengths (Å) | |||
|---|---|---|---|
| Zn(1)–O(1) | 1.976(4) | Zn(2)–O(1) | 1.970(4) |
| Zn(1)–O(4) | 1.897(4) | Zn(2)–O(5) | 1.947(4) |
| Zn(1)–O(5) | 1.954(3) | Zn(2)–O(8) | 1.867(4) |
| Zn(1)–N(3) | 2.118(6) | Zn(2)–N(4) | 2.115(5) |
| B(1)–O(1) | 1.396(9) | B(2)–O(5) | 1.405(7) |
| B(1)–O(2) | 1.457(7) | B(2)–O(6) | 1.450(8) |
| B(1)–O(3) | 1.458(7) | B(2)–O(7) | 1.474(7) |
| B(1)–N(2) | 1.662(8) | B(2)–N(2) | 1.654(7) |
| Zn(1)–Zn(2) | 2.8059(10) | ||
| bond angles (deg) | |||
|---|---|---|---|
| O(1)–Zn(1)–O(4) | 125.35(19) | O(5)–Zn(2)–O(8) | 123.61(16) |
| O(1)–Zn(1)–O(5) | 85.97(15) | O(1)–Zn(2)–O(5) | 138.9(2) |
| O(4)–Zn(1)–O(5) | 140.38(16) | O(1)–Zn(2)–O(8) | 86.34(16) |
| O(1)–Zn(1)–N(3) | 111.41(19) | O(1)–Zn(2)–N(4) | 96.76(18) |
| O(4)–Zn(1)–N(3) | 93.2(2) | O(5)–Zn(2)–N(4) | 112.6(2) |
| O(5)–Zn(1)–N(3) | 96.71(19) | O(8)–Zn(2)–N(4) | 96.0(2) |
| Zn(1)–O(1)–Zn(2) | 90.63(17) | Zn(1)–O(5)–Zn(2) | 92.01(15) |
| Zn(1)–O(1)–B(1) | 133.4(4) | Zn(2)–O(5)–B(2) | 138.4(3) |
| Zn(1)–O(5)–B(2) | 128.0(3) | Zn(2)–O(1)–B(1) | 122.4(3) |
| Zn(1)–O(4)–C(19) | 137.5(5) | Zn(2)–O(8)–C(49) | 131.6(4) |
| O(1)–B(1)–O(2) | 115.1(5) | O(5)–B(2)–O(6) | 111.8(5) |
| O(1)–B(1)–O(3) | 112.8(5) | O(5)–B(2)–O(7) | 112.9(5) |
| O(1)–B(1)–N(1) | 108.6(5) | O(5)–B(2)–N(2) | 110.2(5) |
| O(2)–B(1)–O(3) | 108.2(5) | O(6)–B(2)–O(7) | 109.4(5) |
| O(2)–B(1)–N(1) | 105.3(5) | O(6)–B(2)–N(2) | 105.1(4) |