Skip to main content
. 2023 Feb 8;9(2):e13522. doi: 10.1016/j.heliyon.2023.e13522

Table 4.

A comparison of the previously reported procedures for the synthesis of chemicals 5a, 6f, and 8a.

Entry Product Catalyst Catalyst loading Solvent Temp. (°C) Time (min) Yield (%) Ref.
1 5a Cu2(NH2-BDC)2(DABCO) 40 mg Solvent-free r.t 5 96 This work
2 5a Cu2(BDC)2(DABCO) 40 mg Solvent-free r.t 20 78 This work
3 5a NH4Al(SO4)2.12H2O (Alum) 20 mg EtOH 80 120 94 [62]
4 5a PhB(OH)2 5 mol% H2O/EtOH Reflux 30 84 [63]
5 5a SiO2-Pr-SO3H 30 mg H2O/EtOH Reflux 15 97 [17]
6 5a KF/Al2O3 250 mg DMF r.t 60–180 48 [60]
7 5a MPA-MDAZYb 140 mg EtOH 80 70 90 [64]
8 5a ChCl/Urea DESc 1 mL ChCl/Urea DESc 80 60–240 92 [65]
9 5a Amberlyst A21 30 mg EtOH r.t 60 84 [66]
10 6f Sodium Alginate 10 mol% EtOH Reflux 52 93 [67]
11 6f MPA-MDAZYb 140 mg EtOH 80 40 75 [64]
12 6f Lipase from Porcine pancreas (PPL) 30 mg H2O/EtOH 35 60 96 [68]
13 8a ChCl/Urea DESc 1 mL ChCl/Urea DESc 80 210 82 [65]
14 8a Sodium Alginate 10 mol% EtOH Reflux 150 90 [67]
15 8a nanocrystalline ZnO 10 mol% H2O/EtOH r.t 150 96 [61]

a Entries 1–8: Obtained outcomes for the synthesis of molecule5a, Entries 9–11: Obtained outcomes for the synthesis of molecule6f, Entries 12–14: Obtained findings for 8a compound synthesis.

b

12-Molybdophosphoric acid (MPA), modified dealuminated zeolite Y (MDAZY).

c

Deep eutectic solvent (DES).