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. Author manuscript; available in PMC: 2023 Feb 28.

Published in final edited form as: Biochemistry. 2009 Jan 20;48(2):492–498. doi: 10.1021/bi8016747

Table 1:

¹H Chemical Shifts for 9-, 10-, 12-, and 13-Nitro Fatty Acids

position	peak 3, 9-NO₂	peak 1, 13-NO₂	peak 3, 10-NO₂	peak 2, 12-NO₂
2	2.35, t, 7.65 Hz	2.35, t, 7.65 Hz	2.35, t, 7.43 Hz	2.37, t, 4.43
3	1.63, m	1.64, m	1.63, m	1.64, m
4	1.35, m	1.33, m	1.35, m	1.35, m
5	1.35, m	1.33, m	1.35, m	1.35, m
6	1.35, m	1.33, m	1.35, m	1.35, m
7	1.51, m	1.39, m	1.51, m	1.40, m
8	2.61, t, 7.88 Hz	2.06, q, 7.20 Hz	2.24, q, 7.65 Hz	2.13, q, 6.98 Hz
9	^a	5.53, dtt, 10.76, 7.83, 1.71 Hz	7.08, t, 7.88 Hz	5.48, dtt, 11.51, 6.94, 1.58 Hz
10	7.03, t, 8.33 Hz	5.33, dtt, 10.76, 7.58, 1.47 Hz	^a	5.26, dtt, 11.00, 7.00, 1.58 Hz
11	2.96, t, 7.65 Hz	2.96, t, 7.43 Hz	3.34, d, 7.20 Hz	3.34, d, 6.94 Hz
12	5.32, dtt, 10.51, 7.65, 1.58 Hz	7.02, t, 7.88 Hz	5.25, dtt, 11.00, 7.20, 1.58 Hz	^a
13	5.55, dtt, 10.51, 7.43, 1.58 Hz	^a	5.50, dtt, 11.00, 7.00, 1.58 Hz	7.09, t, 7.80 Hz
14	2.06, q, 7.43 Hz	2.59, t, 7.65 Hz	2.12, q, 6.98 Hz	2.25, q, 7.40 Hz
15	1.39, m	1.50, p, 7.43 Hz	1.40, m	1.51, m
16	1.39, m	1.35, m	1.40, m	1.34, m
17	1.39, m	1.35, m	1.40, m	1.34, m
18	0.904, t, 7.20 Hz	0.89, t, 6.75 Hz	0.90, t, 6.98 Hz	0.91, t, 6.98 Hz

^a

Site of nitration.