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. 2023 Mar 1;10(Pt 2):233–245. doi: 10.1107/S2052252523001501

Table 4. The datasets for analyzing the anomalous signals at the peak or remote positions of the Zn K-edge.

The datasets were collected at peak [EFhd2Zn(P)] or remote [EFhd2Zn(R)] positions of the Zn K-edge using a single EFhd2Zn crystal, and were used to analyze the anomalous signals described in Fig. 1.

Dataset EFhd2Zn(P) EFhd2Zn(R)
Space group I23 I23
X-ray source PAL-7A PAL-7A
Detector ADSC Q270 ADSC Q270
Wavelength (Å) 1.2823 (peak) 1.2917 (remote)
Unit cell parameters
   a, b, c (Å) 92.5, 92.5, 92.5 92.8, 92.8, 92.8
  α, β, γ (°) 90.0, 90.0, 90.0 90.0, 90.0, 90.0
Resolution range (Å) 50–3.45 (3.51–3.45) 50–3.94 (4.01–3.94)
R merge 26.0 (192.8) 23.2 (184.7)
CC1/2 0.979 (0.898) 0.990 (0.939)
I/σ(I)〉 49.0 (5.0) 52.8 (6.9)
Completeness (%) 99.9 (100.0) 100.0 (100.0)
Redundancy 41.7 (43.5) 40.9 (42.8)