####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_b37b _database_code_depnum_ccdc_archive 'CCDC 2127602' loop_ _audit_author_name _audit_author_address 'Cynthia S. Day' ;Wake Forest University United States of America ; _audit_update_record ; 2021-12-09 deposited with the CCDC. 2021-12-17 downloaded from the CCDC. ; _audit_creation_date 2021-12-09 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _shelx_SHELXL_version_number 2018/3 _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C12 H14 F N O2' _chemical_formula_sum 'C12 H14 F N O2' _chemical_formula_weight 223.24 _chemical_absolute_configuration ? _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 8.8761(8) _cell_length_b 12.3960(11) _cell_length_c 30.201(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3322.9(5) _cell_formula_units_Z 12 _cell_measurement_reflns_used 9733 _cell_measurement_temperature 193.65 _cell_measurement_theta_max 25.93 _cell_measurement_theta_min 3.47 _shelx_estimated_absorpt_T_max 0.986 _shelx_estimated_absorpt_T_min 0.967 _exptl_absorpt_coefficient_mu 0.102 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8963 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016) was used for absorption correction. wR2(int) was 0.0584 before and 0.0541 after correction. The Ratio of minimum to maximum transmission is 0.8963. The \l/2 correction factor is Not present. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.339 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description wedge _exptl_crystal_F_000 1416 _exptl_crystal_size_max 0.33 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.14 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0640 _diffrn_reflns_av_unetI/netI 0.0477 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 42 _diffrn_reflns_limit_l_min -42 _diffrn_reflns_number 63357 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.055 _diffrn_reflns_theta_min 3.474 _diffrn_ambient_temperature 193.65 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.793 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 7464 _reflns_number_total 9737 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.221 _refine_diff_density_min -0.179 _refine_diff_density_rms 0.038 _refine_ls_abs_structure_details ; Flack x determined using 2720 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.3(3) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.873 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 436 _refine_ls_number_reflns 9737 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0665 _refine_ls_R_factor_gt 0.0437 _refine_ls_restrained_S_all 0.873 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1176 _refine_ls_wR_factor_ref 0.1336 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All O(H) groups 2.a Ternary CH refined with riding coordinates: C00I(H00K), C00J(H00J), C00Y(H00Y) 2.b Secondary CH2 refined with riding coordinates: C00S(H00E,H00F), C00U(H00A,H00B), C00V(H00G,H00I), C00X(H00C,H00D), C00Z(H00N, H00R), C010(H01I,H01J), C012(H01E,H01F), C014(H01A,H01B), C016(H01C,H01D), C017(H01K,H01L), C019(H01G,H01H), C01B(H01N,H01O) 2.c Aromatic/amide H refined with riding coordinates: C00H(H00H), C00L(H00L), C00M(H00M), C00O(H00O), C00P(H00P), C00Q(H00Q), C00W(H00W), C011(H011), C015(H015), C018(H018), C01A(H01M), C01C(H01P) 2.d Idealised tetrahedral OH refined as rotating group: O002(H002), O003(H003), O005(H005) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F001 F 0.7383(2) 0.12501(16) 0.33375(6) 0.0541(5) Uani 1 1 d . . . . . O002 O -0.21810(19) 0.16369(14) 0.46809(5) 0.0286(4) Uani 1 1 d . . . . . H002 H -0.282019 0.158013 0.488468 0.043 Uiso 1 1 calc R U . . . O003 O -0.0865(2) 0.16797(14) 0.16040(6) 0.0333(4) Uani 1 1 d . . . . . H003 H -0.153371 0.209137 0.150303 0.050 Uiso 1 1 calc R U . . . F004 F 0.0937(3) 0.01058(16) 0.64107(6) 0.0613(6) Uani 1 1 d . . . . . O005 O 0.4110(2) 0.38283(13) 0.18583(6) 0.0301(4) Uani 1 1 d . . . . . H005 H 0.349917 0.342509 0.199149 0.045 Uiso 1 1 calc R U . . . O006 O 0.1626(2) 0.06032(15) 0.26641(6) 0.0380(4) Uani 1 1 d . . . . . O007 O 0.6846(2) 0.51513(15) 0.08958(6) 0.0391(5) Uani 1 1 d . . . . . F008 F 0.2721(3) 0.38128(18) 0.00713(6) 0.0627(6) Uani 1 1 d . . . . . O009 O 0.0588(3) 0.29855(16) 0.37323(6) 0.0406(5) Uani 1 1 d . . . . . N00A N 0.0602(2) 0.34314(16) 0.46504(6) 0.0261(4) Uani 1 1 d . . . . . N00B N 0.6981(2) 0.30286(15) 0.12379(6) 0.0250(4) Uani 1 1 d . . . . . N00C N 0.1863(2) 0.26318(16) 0.22418(6) 0.0272(4) Uani 1 1 d . . . . . C00D C 0.6001(3) 0.26748(18) 0.21760(7) 0.0234(4) Uani 1 1 d . . . . . C00E C 0.1093(3) 0.27407(19) 0.12725(8) 0.0261(5) Uani 1 1 d . . . . . C00F C -0.0363(3) 0.16762(18) 0.52680(7) 0.0233(4) Uani 1 1 d . . . . . C00G C 0.5436(3) 0.32497(17) 0.17642(7) 0.0230(4) Uani 1 1 d . . . . . C00H C 0.5921(3) 0.15644(19) 0.22289(8) 0.0302(5) Uani 1 1 d . . . . . H00H H 0.555765 0.112921 0.199308 0.036 Uiso 1 1 calc R U . . . C00I C 0.1604(3) 0.16257(18) 0.19764(7) 0.0256(4) Uani 1 1 d . . . . . H00K H 0.250835 0.139399 0.180325 0.031 Uiso 1 1 calc R U . . . C00J C 0.6657(3) 0.39642(17) 0.15365(7) 0.0243(4) Uani 1 1 d . . . . . H00J H 0.751573 0.415835 0.173535 0.029 Uiso 1 1 calc R U . . . C00K C 0.6913(3) 0.1721(2) 0.29534(9) 0.0352(6) Uani 1 1 d . . . . . C00L C 0.0038(3) 0.0587(2) 0.52610(9) 0.0304(5) Uani 1 1 d . . . . . H00L H 0.000980 0.020441 0.498863 0.036 Uiso 1 1 calc R U . . . C00M C 0.1379(3) 0.38315(19) 0.12016(9) 0.0300(5) Uani 1 1 d . . . . . H00M H 0.120027 0.433245 0.143379 0.036 Uiso 1 1 calc R U . . . C00N C -0.0898(3) 0.21852(18) 0.48415(7) 0.0228(4) Uani 1 1 d . . . . . C00O C -0.0331(3) 0.2217(2) 0.56714(8) 0.0325(5) Uani 1 1 d . . . . . H00O H -0.060561 0.295705 0.568333 0.039 Uiso 1 1 calc R U . . . C00P C 0.6547(3) 0.3299(2) 0.25247(8) 0.0284(5) Uani 1 1 d . . . . . H00P H 0.658862 0.406120 0.249451 0.034 Uiso 1 1 calc R U . . . C00Q C 0.1923(3) 0.4201(2) 0.07971(9) 0.0372(6) Uani 1 1 d . . . . . H00Q H 0.211385 0.494692 0.075060 0.045 Uiso 1 1 calc R U . . . C00R C 0.0443(3) 0.22802(18) 0.16959(8) 0.0251(4) Uani 1 1 d . . . . . C00S C 0.1006(3) 0.4255(2) 0.43203(8) 0.0333(5) Uani 1 1 d . . . . . H00E H 0.211502 0.426876 0.428723 0.040 Uiso 1 1 calc R U . . . H00F H 0.068642 0.497082 0.443155 0.040 Uiso 1 1 calc R U . . . C00T C 0.0495(3) 0.0627(2) 0.60327(9) 0.0394(6) Uani 1 1 d . . . . . C00U C 0.5990(3) 0.4928(2) 0.12877(9) 0.0318(5) Uani 1 1 d . . . . . H00A H 0.493287 0.476961 0.120579 0.038 Uiso 1 1 calc R U . . . H00B H 0.599292 0.556992 0.148272 0.038 Uiso 1 1 calc R U . . . C00V C -0.0944(3) 0.34337(19) 0.48372(7) 0.0269(5) Uani 1 1 d . . . . . H00G H -0.171373 0.373816 0.463537 0.032 Uiso 1 1 calc R U . . . H00I H -0.101472 0.376191 0.513532 0.032 Uiso 1 1 calc R U . . . C00W C 0.7030(3) 0.2824(2) 0.29142(8) 0.0338(5) Uani 1 1 d . . . . . H00W H 0.743180 0.324741 0.314822 0.041 Uiso 1 1 calc R U . . . C00X C 0.5461(3) 0.25800(19) 0.13304(8) 0.0270(5) Uani 1 1 d . . . . . H00C H 0.545185 0.179003 0.137848 0.032 Uiso 1 1 calc R U . . . H00D H 0.468462 0.279713 0.111266 0.032 Uiso 1 1 calc R U . . . C00Y C 0.0370(3) 0.23008(18) 0.44866(8) 0.0246(4) Uani 1 1 d . . . . . H00Y H 0.125286 0.181705 0.454000 0.030 Uiso 1 1 calc R U . . . C00Z C 0.0899(3) 0.0716(2) 0.22443(8) 0.0338(5) Uani 1 1 d . . . . . H00N H -0.018477 0.086795 0.229020 0.041 Uiso 1 1 calc R U . . . H00R H 0.098515 0.003116 0.207745 0.041 Uiso 1 1 calc R U . . . C010 C 0.1359(3) 0.1556(2) 0.29222(9) 0.0363(6) Uani 1 1 d . . . . . H01I H 0.171773 0.144161 0.322903 0.044 Uiso 1 1 calc R U . . . H01J H 0.026563 0.171024 0.293263 0.044 Uiso 1 1 calc R U . . . C011 C 0.0477(3) 0.0053(2) 0.56429(10) 0.0365(6) Uani 1 1 d . . . . . H011 H 0.075766 -0.068596 0.563576 0.044 Uiso 1 1 calc R U . . . C012 C -0.0223(3) 0.2254(2) 0.40141(8) 0.0338(5) Uani 1 1 d . . . . . H01E H -0.011911 0.150981 0.389888 0.041 Uiso 1 1 calc R U . . . H01F H -0.130669 0.244346 0.401198 0.041 Uiso 1 1 calc R U . . . C013 C 0.2174(4) 0.3468(3) 0.04695(9) 0.0404(6) Uani 1 1 d . . . . . C014 C 0.7433(3) 0.3270(2) 0.07803(8) 0.0338(5) Uani 1 1 d . . . . . H01A H 0.717594 0.264623 0.058998 0.041 Uiso 1 1 calc R U . . . H01B H 0.853949 0.336599 0.077029 0.041 Uiso 1 1 calc R U . . . C015 C 0.6369(3) 0.1080(2) 0.26235(9) 0.0366(6) Uani 1 1 d . . . . . H015 H 0.629640 0.032157 0.266184 0.044 Uiso 1 1 calc R U . . . C016 C 0.6685(4) 0.4273(2) 0.05943(9) 0.0378(6) Uani 1 1 d . . . . . H01C H 0.715286 0.446247 0.030709 0.045 Uiso 1 1 calc R U . . . H01D H 0.560228 0.412891 0.054246 0.045 Uiso 1 1 calc R U . . . C017 C 0.0375(3) 0.30531(19) 0.20981(8) 0.0300(5) Uani 1 1 d . . . . . H01K H 0.038583 0.382679 0.201691 0.036 Uiso 1 1 calc R U . . . H01L H -0.045432 0.289249 0.230709 0.036 Uiso 1 1 calc R U . . . C018 C 0.0099(4) 0.1689(2) 0.60577(9) 0.0421(7) Uani 1 1 d . . . . . H018 H 0.011582 0.205936 0.633295 0.051 Uiso 1 1 calc R U . . . C019 C 0.0303(3) 0.4071(2) 0.38706(9) 0.0361(6) Uani 1 1 d . . . . . H01G H -0.079629 0.419935 0.388644 0.043 Uiso 1 1 calc R U . . . H01H H 0.073742 0.458183 0.365321 0.043 Uiso 1 1 calc R U . . . C01A C 0.1372(3) 0.2025(2) 0.09251(9) 0.0356(6) Uani 1 1 d . . . . . H01M H 0.119233 0.127659 0.096753 0.043 Uiso 1 1 calc R U . . . C01B C 0.2183(3) 0.2497(2) 0.27174(8) 0.0347(6) Uani 1 1 d . . . . . H01N H 0.189373 0.316566 0.287527 0.042 Uiso 1 1 calc R U . . . H01O H 0.327989 0.239251 0.275795 0.042 Uiso 1 1 calc R U . . . C01C C 0.1904(4) 0.2380(2) 0.05220(9) 0.0435(7) Uani 1 1 d . . . . . H01P H 0.208027 0.188840 0.028638 0.052 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F001 0.0626(12) 0.0628(11) 0.0368(9) 0.0223(8) -0.0171(8) -0.0157(9) O002 0.0217(8) 0.0390(9) 0.0253(8) -0.0042(7) 0.0009(7) -0.0029(7) O003 0.0242(8) 0.0288(8) 0.0469(10) 0.0091(8) -0.0067(8) 0.0000(7) F004 0.0856(14) 0.0499(10) 0.0484(10) 0.0244(8) -0.0259(11) -0.0081(11) O005 0.0230(8) 0.0268(8) 0.0403(9) 0.0013(7) 0.0012(8) 0.0036(7) O006 0.0447(11) 0.0374(10) 0.0318(9) 0.0055(8) -0.0027(8) 0.0151(9) O007 0.0481(12) 0.0299(9) 0.0391(10) 0.0119(8) 0.0032(9) -0.0025(8) F008 0.0828(15) 0.0703(12) 0.0349(9) 0.0192(9) 0.0130(9) 0.0062(12) O009 0.0545(13) 0.0409(10) 0.0266(9) 0.0006(8) 0.0108(8) -0.0064(9) N00A 0.0291(10) 0.0247(9) 0.0246(9) 0.0014(7) -0.0041(8) -0.0004(8) N00B 0.0259(10) 0.0259(9) 0.0233(9) 0.0026(7) -0.0012(8) 0.0035(7) N00C 0.0263(10) 0.0306(10) 0.0246(9) -0.0025(8) 0.0027(8) 0.0023(8) C00D 0.0196(10) 0.0254(10) 0.0251(10) 0.0018(8) 0.0014(8) -0.0011(8) C00E 0.0257(11) 0.0265(10) 0.0260(11) 0.0027(9) -0.0051(9) 0.0016(9) C00F 0.0210(10) 0.0256(10) 0.0233(10) 0.0010(8) 0.0001(8) -0.0002(8) C00G 0.0208(10) 0.0209(9) 0.0274(10) -0.0007(8) -0.0017(8) 0.0003(8) C00H 0.0353(13) 0.0241(10) 0.0311(12) 0.0001(9) -0.0045(11) -0.0025(10) C00I 0.0234(11) 0.0278(10) 0.0255(11) -0.0010(9) 0.0015(9) 0.0078(9) C00J 0.0235(11) 0.0235(10) 0.0261(10) 0.0016(8) -0.0027(9) -0.0025(8) C00K 0.0306(13) 0.0463(14) 0.0288(12) 0.0122(11) -0.0032(10) -0.0023(11) C00L 0.0311(13) 0.0260(11) 0.0340(13) -0.0009(10) -0.0017(10) 0.0020(9) C00M 0.0308(13) 0.0259(10) 0.0332(12) 0.0021(10) -0.0027(10) 0.0014(9) C00N 0.0219(10) 0.0257(10) 0.0209(9) -0.0026(8) -0.0001(8) 0.0020(9) C00O 0.0428(14) 0.0294(11) 0.0254(11) 0.0013(9) -0.0044(11) -0.0004(11) C00P 0.0285(12) 0.0302(11) 0.0265(11) -0.0006(9) 0.0029(9) -0.0037(10) C00Q 0.0395(15) 0.0339(12) 0.0381(14) 0.0123(11) -0.0059(12) 0.0004(11) C00R 0.0230(11) 0.0222(9) 0.0299(11) 0.0027(8) -0.0006(9) 0.0042(8) C00S 0.0368(14) 0.0296(11) 0.0334(12) 0.0041(10) -0.0063(11) -0.0033(11) C00T 0.0439(16) 0.0381(13) 0.0364(14) 0.0156(11) -0.0127(12) -0.0049(12) C00U 0.0362(13) 0.0250(10) 0.0341(12) 0.0040(9) 0.0024(11) -0.0004(10) C00V 0.0292(11) 0.0277(10) 0.0237(10) -0.0004(9) -0.0027(9) 0.0080(10) C00W 0.0344(13) 0.0433(14) 0.0237(11) -0.0009(10) 0.0010(10) -0.0106(11) C00X 0.0300(12) 0.0240(10) 0.0269(11) 0.0000(8) -0.0058(9) -0.0017(9) C00Y 0.0224(11) 0.0262(10) 0.0253(10) -0.0016(9) 0.0010(9) 0.0016(9) C00Z 0.0375(14) 0.0297(11) 0.0343(13) 0.0053(10) -0.0021(11) 0.0069(10) C010 0.0379(14) 0.0445(14) 0.0266(12) 0.0043(11) 0.0046(10) 0.0095(12) C011 0.0371(14) 0.0269(11) 0.0454(15) 0.0094(11) -0.0018(12) 0.0028(11) C012 0.0426(15) 0.0356(12) 0.0231(11) -0.0030(10) 0.0050(10) -0.0058(11) C013 0.0431(16) 0.0498(16) 0.0283(12) 0.0113(12) 0.0001(11) 0.0060(13) C014 0.0366(14) 0.0390(13) 0.0259(11) 0.0052(10) 0.0024(10) 0.0082(11) C015 0.0393(15) 0.0304(12) 0.0400(14) 0.0091(11) -0.0039(11) -0.0029(10) C016 0.0445(15) 0.0387(13) 0.0302(12) 0.0106(11) -0.0015(12) 0.0054(12) C017 0.0294(12) 0.0290(11) 0.0315(12) 0.0024(9) 0.0086(10) 0.0079(9) C018 0.0594(19) 0.0397(14) 0.0272(12) 0.0020(11) -0.0130(12) -0.0053(13) C019 0.0417(15) 0.0370(13) 0.0295(12) 0.0064(10) -0.0033(11) -0.0020(11) C01A 0.0455(16) 0.0285(11) 0.0329(13) -0.0010(10) -0.0003(11) 0.0018(11) C01B 0.0326(13) 0.0454(14) 0.0262(11) -0.0052(10) 0.0004(10) 0.0035(11) C01C 0.0595(19) 0.0439(15) 0.0271(12) -0.0042(11) 0.0014(13) 0.0071(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F001 C00K 1.364(3) . ? O002 H002 0.8400 . ? O002 C00N 1.412(3) . ? O003 H003 0.8400 . ? O003 C00R 1.407(3) . ? F004 C00T 1.370(3) . ? O005 H005 0.8400 . ? O005 C00G 1.407(3) . ? O006 C00Z 1.429(3) . ? O006 C010 1.434(3) . ? O007 C00U 1.434(3) . ? O007 C016 1.427(3) . ? F008 C013 1.366(3) . ? O009 C012 1.437(3) . ? O009 C019 1.432(3) . ? N00A C00S 1.472(3) . ? N00A C00V 1.484(3) . ? N00A C00Y 1.500(3) . ? N00B C00J 1.497(3) . ? N00B C00X 1.485(3) . ? N00B C014 1.470(3) . ? N00C C00I 1.500(3) . ? N00C C017 1.485(3) . ? N00C C01B 1.474(3) . ? C00D C00G 1.518(3) . ? C00D C00H 1.388(3) . ? C00D C00P 1.394(3) . ? C00E C00M 1.392(3) . ? C00E C00R 1.514(3) . ? C00E C01A 1.397(4) . ? C00F C00L 1.396(3) . ? C00F C00N 1.511(3) . ? C00F C00O 1.391(3) . ? C00G C00J 1.559(3) . ? C00G C00X 1.551(3) . ? C00H H00H 0.9500 . ? C00H C015 1.392(4) . ? C00I H00K 1.0000 . ? C00I C00R 1.561(3) . ? C00I C00Z 1.523(3) . ? C00J H00J 1.0000 . ? C00J C00U 1.530(3) . ? C00K C00W 1.376(4) . ? C00K C015 1.363(4) . ? C00L H00L 0.9500 . ? C00L C011 1.386(4) . ? C00M H00M 0.9500 . ? C00M C00Q 1.391(4) . ? C00N C00V 1.548(3) . ? C00N C00Y 1.561(3) . ? C00O H00O 0.9500 . ? C00O C018 1.391(4) . ? C00P H00P 0.9500 . ? C00P C00W 1.384(4) . ? C00Q H00Q 0.9500 . ? C00Q C013 1.362(4) . ? C00R C017 1.548(3) . ? C00S H00E 0.9900 . ? C00S H00F 0.9900 . ? C00S C019 1.512(4) . ? C00T C011 1.376(4) . ? C00T C018 1.364(4) . ? C00U H00A 0.9900 . ? C00U H00B 0.9900 . ? C00V H00G 0.9900 . ? C00V H00I 0.9900 . ? C00W H00W 0.9500 . ? C00X H00C 0.9900 . ? C00X H00D 0.9900 . ? C00Y H00Y 1.0000 . ? C00Y C012 1.522(3) . ? C00Z H00N 0.9900 . ? C00Z H00R 0.9900 . ? C010 H01I 0.9900 . ? C010 H01J 0.9900 . ? C010 C01B 1.509(4) . ? C011 H011 0.9500 . ? C012 H01E 0.9900 . ? C012 H01F 0.9900 . ? C013 C01C 1.379(4) . ? C014 H01A 0.9900 . ? C014 H01B 0.9900 . ? C014 C016 1.517(4) . ? C015 H015 0.9500 . ? C016 H01C 0.9900 . ? C016 H01D 0.9900 . ? C017 H01K 0.9900 . ? C017 H01L 0.9900 . ? C018 H018 0.9500 . ? C019 H01G 0.9900 . ? C019 H01H 0.9900 . ? C01A H01M 0.9500 . ? C01A C01C 1.378(4) . ? C01B H01N 0.9900 . ? C01B H01O 0.9900 . ? C01C H01P 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00N O002 H002 109.5 . . ? C00R O003 H003 109.5 . . ? C00G O005 H005 109.5 . . ? C00Z O006 C010 109.10(19) . . ? C016 O007 C00U 109.04(19) . . ? C019 O009 C012 109.4(2) . . ? C00S N00A C00V 118.8(2) . . ? C00S N00A C00Y 117.27(18) . . ? C00V N00A C00Y 90.01(17) . . ? C00X N00B C00J 90.13(17) . . ? C014 N00B C00J 117.46(18) . . ? C014 N00B C00X 120.1(2) . . ? C017 N00C C00I 90.00(17) . . ? C01B N00C C00I 117.1(2) . . ? C01B N00C C017 119.72(19) . . ? C00H C00D C00G 122.9(2) . . ? C00H C00D C00P 118.8(2) . . ? C00P C00D C00G 118.2(2) . . ? C00M C00E C00R 124.4(2) . . ? C00M C00E C01A 118.0(2) . . ? C01A C00E C00R 117.6(2) . . ? C00L C00F C00N 118.1(2) . . ? C00O C00F C00L 118.3(2) . . ? C00O C00F C00N 123.5(2) . . ? O005 C00G C00D 110.48(18) . . ? O005 C00G C00J 112.38(17) . . ? O005 C00G C00X 117.10(19) . . ? C00D C00G C00J 113.48(18) . . ? C00D C00G C00X 115.83(18) . . ? C00X C00G C00J 85.49(16) . . ? C00D C00H H00H 119.6 . . ? C00D C00H C015 120.8(2) . . ? C015 C00H H00H 119.6 . . ? N00C C00I H00K 113.3 . . ? N00C C00I C00R 87.65(16) . . ? N00C C00I C00Z 113.27(19) . . ? C00R C00I H00K 113.3 . . ? C00Z C00I H00K 113.3 . . ? C00Z C00I C00R 113.7(2) . . ? N00B C00J C00G 87.66(16) . . ? N00B C00J H00J 113.7 . . ? N00B C00J C00U 112.54(18) . . ? C00G C00J H00J 113.7 . . ? C00U C00J C00G 113.0(2) . . ? C00U C00J H00J 113.7 . . ? F001 C00K C00W 118.4(2) . . ? C015 C00K F001 118.7(2) . . ? C015 C00K C00W 122.9(2) . . ? C00F C00L H00L 119.3 . . ? C011 C00L C00F 121.4(2) . . ? C011 C00L H00L 119.3 . . ? C00E C00M H00M 119.4 . . ? C00Q C00M C00E 121.2(2) . . ? C00Q C00M H00M 119.4 . . ? O002 C00N C00F 110.19(19) . . ? O002 C00N C00V 117.17(19) . . ? O002 C00N C00Y 112.94(18) . . ? C00F C00N C00V 115.66(18) . . ? C00F C00N C00Y 113.43(19) . . ? C00V C00N C00Y 85.51(17) . . ? C00F C00O H00O 119.6 . . ? C018 C00O C00F 120.9(2) . . ? C018 C00O H00O 119.6 . . ? C00D C00P H00P 119.5 . . ? C00W C00P C00D 120.9(2) . . ? C00W C00P H00P 119.5 . . ? C00M C00Q H00Q 120.8 . . ? C013 C00Q C00M 118.3(2) . . ? C013 C00Q H00Q 120.8 . . ? O003 C00R C00E 110.3(2) . . ? O003 C00R C00I 112.14(18) . . ? O003 C00R C017 116.7(2) . . ? C00E C00R C00I 113.75(19) . . ? C00E C00R C017 116.37(19) . . ? C017 C00R C00I 85.50(17) . . ? N00A C00S H00E 108.8 . . ? N00A C00S H00F 108.8 . . ? N00A C00S C019 113.8(2) . . ? H00E C00S H00F 107.7 . . ? C019 C00S H00E 108.8 . . ? C019 C00S H00F 108.8 . . ? F004 C00T C011 118.2(2) . . ? C018 C00T F004 118.9(3) . . ? C018 C00T C011 122.9(2) . . ? O007 C00U C00J 110.5(2) . . ? O007 C00U H00A 109.5 . . ? O007 C00U H00B 109.5 . . ? C00J C00U H00A 109.5 . . ? C00J C00U H00B 109.5 . . ? H00A C00U H00B 108.1 . . ? N00A C00V C00N 88.65(17) . . ? N00A C00V H00G 113.9 . . ? N00A C00V H00I 113.9 . . ? C00N C00V H00G 113.9 . . ? C00N C00V H00I 113.9 . . ? H00G C00V H00I 111.1 . . ? C00K C00W C00P 118.2(2) . . ? C00K C00W H00W 120.9 . . ? C00P C00W H00W 120.9 . . ? N00B C00X C00G 88.38(17) . . ? N00B C00X H00C 113.9 . . ? N00B C00X H00D 113.9 . . ? C00G C00X H00C 113.9 . . ? C00G C00X H00D 113.9 . . ? H00C C00X H00D 111.1 . . ? N00A C00Y C00N 87.61(16) . . ? N00A C00Y H00Y 113.5 . . ? N00A C00Y C012 113.11(19) . . ? C00N C00Y H00Y 113.5 . . ? C012 C00Y C00N 113.0(2) . . ? C012 C00Y H00Y 113.5 . . ? O006 C00Z C00I 111.0(2) . . ? O006 C00Z H00N 109.4 . . ? O006 C00Z H00R 109.4 . . ? C00I C00Z H00N 109.4 . . ? C00I C00Z H00R 109.4 . . ? H00N C00Z H00R 108.0 . . ? O006 C010 H01I 109.8 . . ? O006 C010 H01J 109.8 . . ? O006 C010 C01B 109.5(2) . . ? H01I C010 H01J 108.2 . . ? C01B C010 H01I 109.8 . . ? C01B C010 H01J 109.8 . . ? C00L C011 H011 121.0 . . ? C00T C011 C00L 117.9(2) . . ? C00T C011 H011 121.0 . . ? O009 C012 C00Y 111.0(2) . . ? O009 C012 H01E 109.4 . . ? O009 C012 H01F 109.4 . . ? C00Y C012 H01E 109.4 . . ? C00Y C012 H01F 109.4 . . ? H01E C012 H01F 108.0 . . ? F008 C013 C01C 118.0(3) . . ? C00Q C013 F008 119.3(3) . . ? C00Q C013 C01C 122.7(3) . . ? N00B C014 H01A 108.9 . . ? N00B C014 H01B 108.9 . . ? N00B C014 C016 113.3(2) . . ? H01A C014 H01B 107.7 . . ? C016 C014 H01A 108.9 . . ? C016 C014 H01B 108.9 . . ? C00H C015 H015 120.8 . . ? C00K C015 C00H 118.4(2) . . ? C00K C015 H015 120.8 . . ? O007 C016 C014 110.2(2) . . ? O007 C016 H01C 109.6 . . ? O007 C016 H01D 109.6 . . ? C014 C016 H01C 109.6 . . ? C014 C016 H01D 109.6 . . ? H01C C016 H01D 108.1 . . ? N00C C017 C00R 88.68(17) . . ? N00C C017 H01K 113.9 . . ? N00C C017 H01L 113.9 . . ? C00R C017 H01K 113.9 . . ? C00R C017 H01L 113.9 . . ? H01K C017 H01L 111.1 . . ? C00O C018 H018 120.7 . . ? C00T C018 C00O 118.6(3) . . ? C00T C018 H018 120.7 . . ? O009 C019 C00S 109.3(2) . . ? O009 C019 H01G 109.8 . . ? O009 C019 H01H 109.8 . . ? C00S C019 H01G 109.8 . . ? C00S C019 H01H 109.8 . . ? H01G C019 H01H 108.3 . . ? C00E C01A H01M 119.3 . . ? C01C C01A C00E 121.4(2) . . ? C01C C01A H01M 119.3 . . ? N00C C01B C010 113.2(2) . . ? N00C C01B H01N 108.9 . . ? N00C C01B H01O 108.9 . . ? C010 C01B H01N 108.9 . . ? C010 C01B H01O 108.9 . . ? H01N C01B H01O 107.8 . . ? C013 C01C H01P 120.9 . . ? C01A C01C C013 118.3(3) . . ? C01A C01C H01P 120.9 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F001 C00K C00W C00P -179.7(2) . . . . ? F001 C00K C015 C00H -178.7(3) . . . . ? O002 C00N C00V N00A -134.66(19) . . . . ? O002 C00N C00Y N00A 138.56(18) . . . . ? O002 C00N C00Y C012 24.4(3) . . . . ? O003 C00R C017 N00C 133.63(19) . . . . ? F004 C00T C011 C00L -179.6(3) . . . . ? F004 C00T C018 C00O 179.2(3) . . . . ? O005 C00G C00J N00B -138.58(18) . . . . ? O005 C00G C00J C00U -25.0(3) . . . . ? O005 C00G C00X N00B 134.12(19) . . . . ? O006 C010 C01B N00C 51.8(3) . . . . ? F008 C013 C01C C01A 179.1(3) . . . . ? N00A C00S C019 O009 -50.8(3) . . . . ? N00A C00Y C012 O009 45.4(3) . . . . ? N00B C00J C00U O007 -47.5(3) . . . . ? N00B C014 C016 O007 50.0(3) . . . . ? N00C C00I C00R O003 -137.95(19) . . . . ? N00C C00I C00R C00E 96.0(2) . . . . ? N00C C00I C00R C017 -20.86(16) . . . . ? N00C C00I C00Z O006 -45.3(3) . . . . ? C00D C00G C00J N00B 95.17(19) . . . . ? C00D C00G C00J C00U -151.3(2) . . . . ? C00D C00G C00X N00B -92.7(2) . . . . ? C00D C00H C015 C00K -1.2(4) . . . . ? C00D C00P C00W C00K -2.0(4) . . . . ? C00E C00M C00Q C013 -0.1(4) . . . . ? C00E C00R C017 N00C -93.3(2) . . . . ? C00E C01A C01C C013 0.7(5) . . . . ? C00F C00L C011 C00T 0.5(4) . . . . ? C00F C00N C00V N00A 92.7(2) . . . . ? C00F C00N C00Y N00A -95.15(19) . . . . ? C00F C00N C00Y C012 150.7(2) . . . . ? C00F C00O C018 C00T 0.3(5) . . . . ? C00G C00D C00H C015 -176.0(2) . . . . ? C00G C00D C00P C00W 177.8(2) . . . . ? C00G C00J C00U O007 -144.9(2) . . . . ? C00H C00D C00G O005 108.5(3) . . . . ? C00H C00D C00G C00J -124.2(2) . . . . ? C00H C00D C00G C00X -27.6(3) . . . . ? C00H C00D C00P C00W 1.2(4) . . . . ? C00I N00C C017 C00R -21.90(16) . . . . ? C00I N00C C01B C010 -34.1(3) . . . . ? C00I C00R C017 N00C 21.07(16) . . . . ? C00J N00B C00X C00G -22.10(16) . . . . ? C00J N00B C014 C016 -33.7(3) . . . . ? C00J C00G C00X N00B 21.24(15) . . . . ? C00L C00F C00N O002 58.9(3) . . . . ? C00L C00F C00N C00V -165.3(2) . . . . ? C00L C00F C00N C00Y -68.8(3) . . . . ? C00L C00F C00O C018 0.4(4) . . . . ? C00M C00E C00R O003 124.5(2) . . . . ? C00M C00E C00R C00I -108.5(3) . . . . ? C00M C00E C00R C017 -11.5(3) . . . . ? C00M C00E C01A C01C -0.5(4) . . . . ? C00M C00Q C013 F008 -179.4(3) . . . . ? C00M C00Q C013 C01C 0.4(5) . . . . ? C00N C00F C00L C011 -177.2(2) . . . . ? C00N C00F C00O C018 176.6(3) . . . . ? C00N C00Y C012 O009 143.0(2) . . . . ? C00O C00F C00L C011 -0.8(4) . . . . ? C00O C00F C00N O002 -117.3(2) . . . . ? C00O C00F C00N C00V 18.5(3) . . . . ? C00O C00F C00N C00Y 115.0(2) . . . . ? C00P C00D C00G O005 -67.9(3) . . . . ? C00P C00D C00G C00J 59.3(3) . . . . ? C00P C00D C00G C00X 155.9(2) . . . . ? C00P C00D C00H C015 0.4(4) . . . . ? C00Q C013 C01C C01A -0.6(5) . . . . ? C00R C00E C00M C00Q -177.4(2) . . . . ? C00R C00E C01A C01C 177.3(3) . . . . ? C00R C00I C00Z O006 -143.4(2) . . . . ? C00S N00A C00V C00N 143.5(2) . . . . ? C00S N00A C00Y C00N -144.6(2) . . . . ? C00S N00A C00Y C012 -30.5(3) . . . . ? C00U O007 C016 C014 -67.1(3) . . . . ? C00V N00A C00S C019 -73.0(3) . . . . ? C00V N00A C00Y C00N -21.79(16) . . . . ? C00V N00A C00Y C012 92.3(2) . . . . ? C00V C00N C00Y N00A 20.91(16) . . . . ? C00V C00N C00Y C012 -93.2(2) . . . . ? C00W C00K C015 C00H 0.4(4) . . . . ? C00X N00B C00J C00G 21.99(16) . . . . ? C00X N00B C00J C00U -92.0(2) . . . . ? C00X N00B C014 C016 74.0(3) . . . . ? C00X C00G C00J N00B -21.08(16) . . . . ? C00X C00G C00J C00U 92.5(2) . . . . ? C00Y N00A C00S C019 33.4(3) . . . . ? C00Y N00A C00V C00N 21.96(16) . . . . ? C00Y C00N C00V N00A -21.14(16) . . . . ? C00Z O006 C010 C01B -68.3(3) . . . . ? C00Z C00I C00R O003 -23.5(3) . . . . ? C00Z C00I C00R C00E -149.5(2) . . . . ? C00Z C00I C00R C017 93.6(2) . . . . ? C010 O006 C00Z C00I 65.2(3) . . . . ? C011 C00T C018 C00O -0.5(5) . . . . ? C012 O009 C019 C00S 67.5(3) . . . . ? C014 N00B C00J C00G 146.4(2) . . . . ? C014 N00B C00J C00U 32.4(3) . . . . ? C014 N00B C00X C00G -144.4(2) . . . . ? C015 C00K C00W C00P 1.2(4) . . . . ? C016 O007 C00U C00J 66.1(3) . . . . ? C017 N00C C00I C00R 21.72(16) . . . . ? C017 N00C C00I C00Z -93.1(2) . . . . ? C017 N00C C01B C010 72.9(3) . . . . ? C018 C00T C011 C00L 0.1(5) . . . . ? C019 O009 C012 C00Y -65.4(3) . . . . ? C01A C00E C00M C00Q 0.2(4) . . . . ? C01A C00E C00R O003 -53.2(3) . . . . ? C01A C00E C00R C00I 73.8(3) . . . . ? C01A C00E C00R C017 170.8(2) . . . . ? C01B N00C C00I C00R 145.6(2) . . . . ? C01B N00C C00I C00Z 30.7(3) . . . . ? C01B N00C C017 C00R -143.6(2) . . . . ? _shelx_res_file ; TITL b37b_a.res in P2(1)2(1)2(1) b37b.res created by SHELXL-2018/3 at 10:15:44 on 09-Dec-2021 REM Old TITL b37b in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.111, Rweak 0.029, Alpha 0.001 REM 0.888 for 28 systematic absences, Orientation as input REM Flack x = -0.498 ( 0.310 ) from 2344 Parsons' quotients REM Formula found by SHELXT: C36 F N3 O8 CELL 0.71073 8.8761 12.396 30.2008 90 90 90 ZERR 12 0.0008 0.0011 0.0028 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H F N O UNIT 144 168 12 12 24 L.S. 4 0 0 PLAN 1 SIZE 0.14 0.17 0.33 TEMP -79.5 CONF BOND list 4 fmap 2 53 MORE -1 BOND $H ACTA REM REM REM WGHT 0.100000 FVAR 0.40725 F001 3 0.738252 0.125012 0.333745 11.00000 0.06265 0.06283 = 0.03684 0.02233 -0.01714 -0.01565 O002 5 -0.218099 0.163687 0.468090 11.00000 0.02170 0.03896 = 0.02527 -0.00422 0.00094 -0.00293 AFIX 147 H002 2 -0.282019 0.158013 0.488468 11.00000 -1.50000 AFIX 0 O003 5 -0.086503 0.167970 0.160396 11.00000 0.02421 0.02877 = 0.04694 0.00908 -0.00674 -0.00002 AFIX 147 H003 2 -0.153371 0.209137 0.150303 11.00000 -1.50000 AFIX 0 F004 3 0.093735 0.010585 0.641068 11.00000 0.08562 0.04992 = 0.04843 0.02442 -0.02588 -0.00810 O005 5 0.411008 0.382830 0.185832 11.00000 0.02302 0.02679 = 0.04035 0.00127 0.00120 0.00358 AFIX 147 H005 2 0.349917 0.342509 0.199149 11.00000 -1.50000 AFIX 0 O006 5 0.162556 0.060319 0.266407 11.00000 0.04471 0.03740 = 0.03183 0.00549 -0.00272 0.01512 O007 5 0.684637 0.515129 0.089582 11.00000 0.04812 0.02994 = 0.03913 0.01191 0.00316 -0.00250 F008 3 0.272107 0.381279 0.007132 11.00000 0.08277 0.07029 = 0.03494 0.01918 0.01296 0.00618 O009 5 0.058796 0.298545 0.373230 11.00000 0.05449 0.04087 = 0.02658 0.00064 0.01078 -0.00639 N00A 4 0.060200 0.343137 0.465043 11.00000 0.02906 0.02471 = 0.02463 0.00138 -0.00413 -0.00037 N00B 4 0.698066 0.302859 0.123791 11.00000 0.02588 0.02588 = 0.02335 0.00257 -0.00119 0.00346 N00C 4 0.186337 0.263182 0.224179 11.00000 0.02628 0.03062 = 0.02462 -0.00247 0.00268 0.00234 C00D 1 0.600056 0.267479 0.217596 11.00000 0.01958 0.02537 = 0.02511 0.00183 0.00138 -0.00113 C00E 1 0.109256 0.274069 0.127254 11.00000 0.02574 0.02650 = 0.02598 0.00274 -0.00509 0.00164 C00F 1 -0.036320 0.167624 0.526804 11.00000 0.02099 0.02561 = 0.02329 0.00104 0.00011 -0.00020 C00G 1 0.543589 0.324975 0.176420 11.00000 0.02080 0.02087 = 0.02742 -0.00068 -0.00171 0.00031 C00H 1 0.592148 0.156436 0.222890 11.00000 0.03534 0.02411 = 0.03113 0.00015 -0.00452 -0.00248 AFIX 43 H00H 2 0.555765 0.112921 0.199308 11.00000 -1.20000 AFIX 0 C00I 1 0.160425 0.162567 0.197642 11.00000 0.02342 0.02783 = 0.02546 -0.00095 0.00148 0.00781 AFIX 13 H00K 2 0.250835 0.139399 0.180325 11.00000 -1.20000 AFIX 0 C00J 1 0.665667 0.396415 0.153650 11.00000 0.02347 0.02349 = 0.02609 0.00163 -0.00268 -0.00252 AFIX 13 H00J 2 0.751573 0.415835 0.173535 11.00000 -1.20000 AFIX 0 C00K 1 0.691349 0.172090 0.295340 11.00000 0.03056 0.04626 = 0.02876 0.01219 -0.00321 -0.00231 C00L 1 0.003826 0.058735 0.526097 11.00000 0.03107 0.02604 = 0.03398 -0.00088 -0.00168 0.00198 AFIX 43 H00L 2 0.000980 0.020441 0.498863 11.00000 -1.20000 AFIX 0 C00M 1 0.137918 0.383151 0.120161 11.00000 0.03077 0.02589 = 0.03320 0.00211 -0.00268 0.00138 AFIX 43 H00M 2 0.120027 0.433245 0.143379 11.00000 -1.20000 AFIX 0 C00N 1 -0.089778 0.218520 0.484153 11.00000 0.02195 0.02568 = 0.02091 -0.00257 -0.00008 0.00199 C00O 1 -0.033073 0.221694 0.567143 11.00000 0.04279 0.02942 = 0.02542 0.00134 -0.00442 -0.00035 AFIX 43 H00O 2 -0.060561 0.295705 0.568333 11.00000 -1.20000 AFIX 0 C00P 1 0.654719 0.329893 0.252469 11.00000 0.02847 0.03020 = 0.02652 -0.00058 0.00292 -0.00367 AFIX 43 H00P 2 0.658862 0.406120 0.249451 11.00000 -1.20000 AFIX 0 C00Q 1 0.192262 0.420145 0.079712 11.00000 0.03952 0.03395 = 0.03808 0.01230 -0.00585 0.00042 AFIX 43 H00Q 2 0.211385 0.494692 0.075060 11.00000 -1.20000 AFIX 0 C00R 1 0.044322 0.228024 0.169591 11.00000 0.02303 0.02225 = 0.02994 0.00269 -0.00058 0.00424 C00S 1 0.100550 0.425519 0.432027 11.00000 0.03683 0.02960 = 0.03345 0.00410 -0.00634 -0.00326 AFIX 23 H00E 2 0.211502 0.426876 0.428723 11.00000 -1.20000 H00F 2 0.068642 0.497082 0.443155 11.00000 -1.20000 AFIX 0 C00T 1 0.049479 0.062744 0.603268 11.00000 0.04385 0.03808 = 0.03642 0.01556 -0.01270 -0.00493 C00U 1 0.598994 0.492794 0.128772 11.00000 0.03617 0.02497 = 0.03413 0.00401 0.00242 -0.00044 AFIX 23 H00A 2 0.493287 0.476961 0.120579 11.00000 -1.20000 H00B 2 0.599292 0.556992 0.148272 11.00000 -1.20000 AFIX 0 C00V 1 -0.094447 0.343373 0.483718 11.00000 0.02922 0.02768 = 0.02371 -0.00042 -0.00270 0.00796 AFIX 23 H00G 2 -0.171373 0.373816 0.463537 11.00000 -1.20000 H00I 2 -0.101472 0.376191 0.513532 11.00000 -1.20000 AFIX 0 C00W 1 0.703027 0.282372 0.291417 11.00000 0.03442 0.04326 = 0.02375 -0.00085 0.00101 -0.01059 AFIX 43 H00W 2 0.743180 0.324741 0.314822 11.00000 -1.20000 AFIX 0 C00X 1 0.546120 0.258002 0.133042 11.00000 0.03001 0.02399 = 0.02687 0.00004 -0.00579 -0.00167 AFIX 23 H00C 2 0.545185 0.179003 0.137848 11.00000 -1.20000 H00D 2 0.468462 0.279713 0.111266 11.00000 -1.20000 AFIX 0 C00Y 1 0.036979 0.230082 0.448660 11.00000 0.02239 0.02616 = 0.02527 -0.00164 0.00102 0.00165 AFIX 13 H00Y 2 0.125286 0.181705 0.454000 11.00000 -1.20000 AFIX 0 C00Z 1 0.089897 0.071585 0.224429 11.00000 0.03751 0.02970 = 0.03428 0.00532 -0.00208 0.00689 AFIX 23 H00N 2 -0.018477 0.086795 0.229020 11.00000 -1.20000 H00R 2 0.098515 0.003116 0.207745 11.00000 -1.20000 AFIX 0 C010 1 0.135931 0.155564 0.292216 11.00000 0.03790 0.04453 = 0.02659 0.00429 0.00455 0.00951 AFIX 23 H01I 2 0.171773 0.144161 0.322903 11.00000 -1.20000 H01J 2 0.026563 0.171024 0.293263 11.00000 -1.20000 AFIX 0 C011 1 0.047737 0.005347 0.564290 11.00000 0.03706 0.02692 = 0.04540 0.00942 -0.00179 0.00275 AFIX 43 H011 2 0.075766 -0.068596 0.563576 11.00000 -1.20000 AFIX 0 C012 1 -0.022328 0.225376 0.401411 11.00000 0.04265 0.03565 = 0.02306 -0.00304 0.00498 -0.00580 AFIX 23 H01E 2 -0.011911 0.150981 0.389888 11.00000 -1.20000 H01F 2 -0.130669 0.244346 0.401198 11.00000 -1.20000 AFIX 0 C013 1 0.217362 0.346830 0.046951 11.00000 0.04313 0.04984 = 0.02831 0.01135 0.00011 0.00601 C014 1 0.743276 0.326990 0.078032 11.00000 0.03658 0.03902 = 0.02592 0.00523 0.00240 0.00819 AFIX 23 H01A 2 0.717594 0.264623 0.058998 11.00000 -1.20000 H01B 2 0.853949 0.336599 0.077029 11.00000 -1.20000 AFIX 0 C015 1 0.636895 0.108045 0.262347 11.00000 0.03928 0.03044 = 0.04005 0.00913 -0.00389 -0.00294 AFIX 43 H015 2 0.629640 0.032157 0.266184 11.00000 -1.20000 AFIX 0 C016 1 0.668514 0.427270 0.059431 11.00000 0.04445 0.03871 = 0.03016 0.01061 -0.00146 0.00542 AFIX 23 H01C 2 0.715286 0.446247 0.030709 11.00000 -1.20000 H01D 2 0.560228 0.412891 0.054246 11.00000 -1.20000 AFIX 0 C017 1 0.037531 0.305309 0.209814 11.00000 0.02941 0.02904 = 0.03151 0.00238 0.00865 0.00794 AFIX 23 H01K 2 0.038583 0.382679 0.201691 11.00000 -1.20000 H01L 2 -0.045432 0.289249 0.230709 11.00000 -1.20000 AFIX 0 C018 1 0.009873 0.168879 0.605765 11.00000 0.05941 0.03975 = 0.02720 0.00196 -0.01305 -0.00525 AFIX 43 H018 2 0.011582 0.205936 0.633295 11.00000 -1.20000 AFIX 0 C019 1 0.030330 0.407124 0.387059 11.00000 0.04173 0.03703 = 0.02955 0.00640 -0.00329 -0.00202 AFIX 23 H01G 2 -0.079629 0.419935 0.388644 11.00000 -1.20000 H01H 2 0.073742 0.458183 0.365321 11.00000 -1.20000 AFIX 0 C01A 1 0.137243 0.202492 0.092507 11.00000 0.04553 0.02849 = 0.03286 -0.00098 -0.00034 0.00175 AFIX 43 H01M 2 0.119233 0.127659 0.096753 11.00000 -1.20000 AFIX 0 C01B 1 0.218275 0.249699 0.271742 11.00000 0.03259 0.04542 = 0.02620 -0.00519 0.00042 0.00348 AFIX 23 H01N 2 0.189373 0.316566 0.287527 11.00000 -1.20000 H01O 2 0.327989 0.239251 0.275795 11.00000 -1.20000 AFIX 0 C01C 1 0.190403 0.238022 0.052200 11.00000 0.05955 0.04394 = 0.02711 -0.00422 0.00142 0.00709 AFIX 43 H01P 2 0.208027 0.188840 0.028638 11.00000 -1.20000 AFIX 0 HKLF 4 REM b37b_a.res in P2(1)2(1)2(1) REM wR2 = 0.1336, GooF = S = 0.873, Restrained GooF = 0.873 for all data REM R1 = 0.0437 for 7464 Fo > 4sig(Fo) and 0.0665 for all 9737 data REM 436 parameters refined using 0 restraints END WGHT 0.0508 0.1905 REM Highest difference peak 0.221, deepest hole -0.179, 1-sigma level 0.038 Q1 1 0.5680 0.2978 0.2001 11.00000 0.05 0.22 ; _shelx_res_checksum 9033 _shelx_hkl_file ; -2 0 0 350.36 16.50 -2 0 0 342.57 16.50 2 0 0 325.17 16.40 3 0 0 0.00 1.40 -3 0 0 -0.20 1.30 -3 0 0 0.00 1.20 3 0 0 0.80 1.10 -4 0 0 5.60 1.30 -4 0 0 6.90 1.80 4 0 0 5.80 1.80 -4 0 0 7.40 2.10 4 0 0 9.80 2.20 4 0 0 5.10 2.00 -5 0 0 -0.60 1.50 -5 0 0 0.40 1.80 -5 0 0 -0.40 1.10 5 0 0 -1.70 1.80 5 0 0 -1.50 2.00 5 0 0 -0.50 1.40 -6 0 0 76.79 6.60 6 0 0 86.79 6.00 -6 0 0 81.39 6.20 6 0 0 87.09 5.70 7 0 0 -0.10 2.30 -7 0 0 -0.80 2.70 7 0 0 -4.40 2.50 -7 0 0 -0.10 2.70 8 0 0 167.68 11.20 -8 0 0 177.58 11.10 -8 0 0 175.48 11.10 8 0 0 162.28 10.70 9 0 0 -7.30 3.60 -9 0 0 -2.00 3.40 -10 0 0 -2.40 2.50 10 0 0 7.40 4.70 -11 0 0 0.20 5.50 11 0 0 7.20 5.70 -12 0 0 7.70 5.50 12 0 0 3.40 6.20 -2 1 0 9044.70 444.16 2 -1 0 9210.28 444.06 -2 1 0 9232.38 444.16 -2 1 0 9632.24 443.96 2 -1 0 9719.73 444.16 -2 -1 0 9891.61 444.26 2 1 0 9999.00 444.26 -3 1 0 321.47 16.20 -3 -1 0 344.57 16.30 3 -1 0 311.67 16.10 3 1 0 326.57 16.00 3 1 0 340.27 15.80 3 1 0 322.47 16.20 -3 -1 0 337.07 15.80 -3 -1 0 329.07 16.00 -3 1 0 314.47 16.10 3 -1 0 317.37 16.10 -3 1 0 313.47 15.90 -4 1 0 530.75 25.10 4 1 0 522.55 25.00 4 -1 0 494.55 25.30 4 1 0 534.85 25.50 -4 -1 0 496.85 25.10 -4 1 0 502.85 25.40 -4 -1 0 516.55 25.50 4 1 0 545.75 25.20 4 -1 0 506.15 25.30 -4 -1 0 522.35 24.80 -5 1 0 415.36 22.20 5 1 0 460.05 22.40 -5 1 0 455.25 21.60 -5 -1 0 435.66 22.70 5 1 0 441.96 22.70 5 -1 0 438.26 22.60 5 1 0 466.85 22.20 -5 -1 0 484.15 21.90 -5 -1 0 484.85 22.40 -5 1 0 419.66 22.60 5 -1 0 445.96 22.40 6 -1 0 303.47 16.30 6 -1 0 303.97 16.50 6 1 0 315.67 16.70 6 1 0 317.27 16.00 -6 1 0 295.07 16.10 -6 -1 0 321.27 16.80 -6 -1 0 330.67 15.70 6 1 0 326.47 16.50 -6 -1 0 300.67 16.20 -6 1 0 287.27 16.60 7 1 0 82.49 7.30 7 1 0 88.29 6.40 -7 1 0 89.49 6.70 7 -1 0 73.49 6.50 -7 -1 0 89.89 7.10 -7 -1 0 77.19 7.30 7 -1 0 82.99 7.20 -7 1 0 84.79 6.70 8 -1 0 120.49 9.00 -8 1 0 132.09 8.80 -8 1 0 121.49 8.60 8 -1 0 118.79 8.40 -8 -1 0 115.69 8.90 8 1 0 111.49 9.50 9 -1 0 7.50 4.20 9 1 0 0.50 3.80 -9 -1 0 -1.30 3.20 -9 1 0 2.40 2.90 10 1 0 1.10 4.70 10 -1 0 5.90 4.80 -10 1 0 9.50 4.40 -10 -1 0 7.10 4.10 -11 -1 0 11.60 5.30 -11 1 0 16.30 5.60 11 1 0 19.00 6.30 11 -1 0 11.80 6.00 12 1 0 2.00 6.50 -12 1 0 2.70 5.20 -12 -1 0 2.30 5.50 12 -1 0 2.70 6.20 1 2 0 1481.55 69.29 -1 -2 0 1509.15 69.49 1 -2 0 1436.16 69.49 -1 -2 0 1495.95 69.49 1 -2 0 1452.45 69.49 -1 2 0 1509.65 69.19 2 -2 0 31.10 2.60 2 2 0 23.40 2.40 -2 2 0 33.20 2.70 -2 2 0 33.40 2.20 2 -2 0 30.30 2.40 2 2 0 32.20 2.50 -2 2 0 36.70 2.70 -2 -2 0 28.20 2.40 -2 -2 0 28.30 2.60 -3 2 0 49.90 3.80 -3 2 0 53.29 3.40 3 -2 0 46.40 3.70 -3 -2 0 54.99 3.50 3 -2 0 50.39 3.70 3 2 0 56.49 3.80 -3 2 0 47.60 3.80 -3 -2 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-0.10 3.80 -11 2 0 -5.80 4.30 11 -2 0 1.70 5.00 -11 -2 0 2.00 4.20 11 2 0 4.20 5.40 12 -2 0 40.00 8.30 -12 2 0 38.70 8.00 12 2 0 28.70 7.90 -12 -2 0 41.80 7.50 0 -3 0 1.80 1.20 0 3 0 0.70 0.70 0 3 0 0.30 1.10 0 -3 0 0.40 1.00 -1 -3 0 1862.61 86.89 1 -3 0 1876.71 86.79 1 3 0 1864.31 86.49 1 3 0 1859.71 86.79 1 -3 0 1844.82 86.89 -1 3 0 1823.02 86.39 1 3 0 1836.42 86.79 -1 3 0 1828.32 86.69 -2 -3 0 80.29 4.90 2 -3 0 75.09 4.80 -2 3 0 83.69 4.90 -2 3 0 76.79 4.40 -2 -3 0 74.19 4.70 2 3 0 71.89 4.60 2 -3 0 81.69 4.40 2 3 0 77.29 4.50 -2 3 0 80.69 4.30 -2 3 0 82.79 4.90 -3 -3 0 754.62 37.20 3 3 0 791.52 37.00 -3 3 0 774.72 37.30 -3 3 0 749.42 36.70 -3 3 0 776.72 36.60 3 3 0 780.82 37.10 3 -3 0 769.02 37.30 -3 -3 0 777.02 37.00 3 -3 0 788.52 36.90 -3 3 0 772.92 37.30 -4 3 0 1.50 1.20 -4 3 0 0.30 1.90 -4 -3 0 0.00 2.00 4 3 0 2.90 1.80 4 -3 0 0.60 1.50 -4 -3 0 -0.20 1.50 -4 -3 0 1.20 1.50 -4 -3 0 2.70 1.30 -4 3 0 2.00 1.40 4 -3 0 0.40 1.30 -4 3 0 2.10 1.90 4 3 0 1.70 1.90 5 -3 0 808.52 40.50 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12.60 -1 4 0 240.68 12.40 1 -4 0 253.77 13.00 -1 -4 0 258.97 13.10 -1 4 0 256.97 12.90 1 4 0 272.57 12.60 1 4 0 263.27 13.10 1 -4 0 252.27 13.10 2 4 0 980.60 44.30 -2 4 0 934.81 44.00 2 -4 0 903.91 44.60 -2 -4 0 917.71 44.60 2 -4 0 892.31 44.50 -2 4 0 921.71 44.20 2 4 0 931.31 44.20 2 -4 0 969.50 44.00 2 4 0 933.81 44.60 3 4 0 66.19 4.60 3 -4 0 68.19 4.30 -3 4 0 68.79 4.90 -3 -4 0 68.19 4.90 3 4 0 69.99 4.60 -3 4 0 63.69 4.80 -3 4 0 76.09 4.20 3 -4 0 64.89 4.90 -3 4 0 71.49 4.20 -4 4 0 4.40 2.30 4 -4 0 5.90 1.80 -4 4 0 2.60 1.60 -4 -4 0 9.20 2.50 -4 -4 0 9.80 1.60 -4 -4 0 6.20 2.00 4 -4 0 1.30 2.00 4 4 0 2.60 2.00 -4 4 0 6.40 1.50 4 4 0 11.20 2.30 -4 4 0 3.50 2.10 -5 4 0 72.09 5.50 5 4 0 78.79 5.90 -5 4 0 75.09 5.60 5 4 0 77.69 5.80 5 -4 0 65.59 5.90 -5 -4 0 78.39 4.80 -5 -4 0 78.19 5.90 5 -4 0 73.99 5.60 -5 4 0 76.19 5.20 6 4 0 23.60 3.90 -6 -4 0 26.30 4.00 -6 4 0 26.40 3.50 6 -4 0 21.80 3.70 -6 4 0 24.30 3.90 6 4 0 30.90 4.10 6 -4 0 29.40 3.80 -6 4 0 25.80 3.90 7 -4 0 4.50 3.00 7 4 0 2.60 3.40 -7 -4 0 5.00 3.00 7 4 0 8.20 3.10 7 4 0 9.50 4.40 -7 4 0 6.10 2.90 7 -4 0 3.90 2.90 -7 4 0 1.60 2.90 -8 4 0 61.19 6.90 8 -4 0 58.99 6.40 8 4 0 56.99 6.50 -8 -4 0 60.19 6.50 8 -4 0 64.99 6.60 -8 4 0 67.99 6.40 9 -4 0 7.90 3.70 9 4 0 4.00 3.70 -9 -4 0 8.80 4.00 -9 4 0 9.00 3.50 9 -4 0 4.60 3.90 -9 4 0 6.70 4.00 -10 4 0 19.80 5.30 -10 -4 0 7.70 4.50 10 4 0 20.50 5.30 10 -4 0 12.50 5.10 10 -4 0 14.30 5.30 -10 4 0 15.20 5.40 -11 -4 0 25.20 5.80 11 -4 0 11.80 5.80 11 4 0 13.60 5.70 -11 4 0 20.10 6.00 12 4 0 28.10 7.70 -12 -4 0 20.60 7.10 -12 4 0 22.50 7.50 12 -4 0 19.60 7.50 0 5 0 -1.20 1.50 0 -5 0 -0.40 1.20 0 5 0 -0.20 0.90 0 -5 0 -0.50 1.50 -1 5 0 1422.56 67.79 1 5 0 1450.75 67.99 1 -5 0 1422.46 67.89 -1 -5 0 1402.76 67.99 -1 -5 0 1462.05 67.49 -1 5 0 1413.66 67.29 1 -5 0 1424.46 67.99 1 5 0 1413.96 67.39 1 5 0 1487.25 67.39 -2 5 0 636.04 31.30 2 5 0 658.83 31.50 -2 -5 0 656.93 32.10 2 5 0 679.33 31.60 2 5 0 645.14 32.00 -2 5 0 664.23 31.70 -2 -5 0 696.33 31.40 2 -5 0 623.84 32.00 2 -5 0 679.03 31.20 2 -5 0 628.54 32.00 3 5 0 14.60 2.30 -3 5 0 20.40 3.00 -3 5 0 12.50 1.80 -3 5 0 16.00 2.10 -3 -5 0 14.80 2.60 -3 -5 0 14.10 1.80 3 -5 0 15.00 2.10 3 5 0 16.80 2.40 3 5 0 14.50 2.70 3 -5 0 14.90 2.40 -3 5 0 12.50 2.70 -4 -5 0 51.49 3.60 -4 5 0 53.19 4.80 4 5 0 52.59 4.70 4 5 0 53.79 4.50 4 5 0 56.69 5.00 4 -5 0 46.70 4.60 -4 -5 0 51.19 4.90 -4 5 0 50.99 4.70 -4 5 0 54.99 3.80 4 -5 0 54.99 4.30 -4 5 0 51.09 4.00 -5 5 0 2.50 2.00 -5 5 0 5.80 2.20 5 5 0 4.80 2.50 5 -5 0 1.30 2.10 -5 -5 0 6.00 2.80 5 5 0 2.50 2.30 5 -5 0 3.90 2.40 -5 5 0 3.00 2.50 5 5 0 3.50 2.40 6 5 0 62.49 6.00 6 -5 0 54.19 5.80 -6 5 0 72.29 6.60 -6 -5 0 53.39 5.90 6 5 0 65.99 5.80 -6 5 0 59.59 5.20 -6 5 0 61.29 6.20 6 -5 0 57.79 5.40 6 5 0 66.09 5.80 7 5 0 19.50 4.00 -7 5 0 18.50 4.20 7 -5 0 23.30 4.00 7 -5 0 20.90 3.90 7 5 0 12.40 4.30 7 5 0 15.60 3.90 -7 5 0 18.10 3.50 -7 5 0 18.30 4.10 -7 -5 0 14.70 3.90 8 -5 0 85.99 7.60 8 5 0 85.89 7.90 -8 5 0 77.59 7.80 8 -5 0 63.89 7.10 -8 -5 0 73.39 7.40 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1.80 -1 -7 0 181.18 8.90 1 7 0 157.88 8.50 1 -7 0 150.48 9.30 1 7 0 180.58 8.40 1 7 0 152.28 9.30 1 -7 0 150.38 9.10 -1 7 0 144.09 9.00 -1 -7 0 167.08 9.30 -1 7 0 142.19 8.30 2 -7 0 0.20 2.00 2 7 0 -0.50 1.40 2 -7 0 -1.10 1.80 -2 -7 0 2.00 2.10 2 7 0 -0.20 1.60 -2 7 0 0.90 1.20 -2 -7 0 -0.50 1.40 -2 7 0 4.40 1.80 2 7 0 2.50 2.00 3 -7 0 223.58 10.50 -3 7 0 201.18 10.60 3 7 0 200.08 11.60 -3 -7 0 188.78 11.40 -3 -7 0 208.08 10.60 3 -7 0 192.58 11.60 3 7 0 192.78 10.90 3 -7 0 195.08 11.50 -3 7 0 215.48 11.10 3 7 0 192.28 10.90 -4 7 0 39.30 4.60 -4 7 0 47.70 4.20 4 7 0 49.40 4.70 4 7 0 45.90 4.30 -4 -7 0 47.40 5.00 -4 7 0 49.00 4.90 4 7 0 41.80 4.80 4 -7 0 39.00 4.80 -4 7 0 35.50 3.60 5 7 0 18.40 3.70 5 -7 0 23.20 4.10 -5 7 0 18.80 4.10 5 7 0 28.00 4.30 -5 -7 0 21.10 3.70 -5 7 0 21.00 4.20 5 7 0 23.70 3.70 -5 7 0 20.30 3.00 -6 7 0 -1.40 3.00 6 7 0 7.00 3.60 6 7 0 -4.00 2.80 -6 -7 0 -3.60 2.50 -6 7 0 0.00 2.90 6 7 0 4.10 3.30 6 -7 0 -1.30 2.60 -6 7 0 -3.60 2.20 7 7 0 1.40 3.10 7 -7 0 4.30 3.50 -7 7 0 2.80 3.20 -7 -7 0 0.90 3.00 7 7 0 9.20 4.00 -7 7 0 8.70 3.50 7 7 0 8.50 4.10 -7 7 0 3.50 3.00 -8 7 0 -3.90 3.90 8 7 0 -6.20 3.50 -8 7 0 9.60 4.70 8 -7 0 -6.00 3.20 -8 7 0 6.10 3.60 -8 -7 0 4.40 3.60 -9 7 0 1.20 4.70 9 -7 0 6.60 4.40 -9 -7 0 3.50 3.80 -9 7 0 5.50 4.50 9 7 0 2.30 4.30 10 7 0 8.80 5.10 -10 -7 0 7.10 4.90 10 -7 0 9.70 5.60 -10 7 0 11.10 5.10 -10 7 0 17.90 6.50 11 7 0 1.30 5.70 -11 -7 0 -6.20 4.60 11 -7 0 12.10 6.90 -11 7 0 0.40 6.20 -11 7 0 -0.70 6.30 0 -8 0 2.80 2.30 0 8 0 3.90 1.60 0 -8 0 6.50 2.40 0 8 0 3.20 2.40 1 8 0 5.10 2.60 -1 8 0 2.90 1.50 1 -8 0 1.80 2.10 -1 -8 0 5.20 2.10 -1 -8 0 6.20 2.10 1 8 0 1.50 1.70 -1 8 0 0.60 2.10 1 8 0 5.50 1.90 1 -8 0 7.40 2.50 -2 8 0 69.49 4.60 -2 8 0 65.99 5.50 2 8 0 73.69 5.20 -2 -8 0 65.89 6.10 2 8 0 72.79 4.70 2 -8 0 63.89 5.60 -2 -8 0 66.89 4.80 2 -8 0 69.59 6.10 2 8 0 70.59 6.30 -3 8 0 2.40 1.70 -3 8 0 6.00 2.50 3 -8 0 7.20 2.70 3 8 0 1.10 2.80 3 -8 0 4.40 2.50 3 8 0 -3.00 1.90 -3 -8 0 3.20 2.50 3 8 0 2.80 2.10 -4 8 0 11.00 2.40 4 8 0 8.40 2.90 4 -8 0 9.30 3.30 4 8 0 11.60 3.60 -4 8 0 15.40 3.50 -4 8 0 5.50 3.20 -4 -8 0 6.50 3.10 4 8 0 7.80 2.90 -4 8 0 9.50 2.90 5 8 0 10.10 3.50 5 8 0 6.90 3.50 -5 8 0 6.10 2.30 5 8 0 12.60 3.90 -5 8 0 3.20 3.10 -5 8 0 10.40 3.60 5 -8 0 5.50 3.20 -5 -8 0 9.00 2.90 6 -8 0 71.29 7.20 -6 8 0 67.19 7.40 6 8 0 75.29 6.90 -6 8 0 71.59 7.50 6 8 0 77.89 7.50 6 8 0 67.69 7.00 -6 -8 0 69.69 7.30 -6 8 0 68.39 5.90 -7 8 0 59.39 6.00 -7 8 0 62.79 7.50 7 -8 0 65.09 7.30 7 8 0 72.09 7.50 7 8 0 69.29 7.10 7 8 0 73.99 7.20 -7 8 0 59.49 7.40 -7 -8 0 70.59 7.40 -8 -8 0 4.50 3.90 -8 8 0 3.80 3.70 -8 8 0 7.10 4.20 8 8 0 7.50 4.20 -8 8 0 1.60 3.50 8 -8 0 2.90 4.20 -9 8 0 -4.50 4.60 -9 8 0 0.20 4.00 9 -8 0 0.90 4.50 9 8 0 -4.50 4.00 -9 -8 0 6.30 4.40 -9 8 0 9.80 5.20 -10 -8 0 7.10 4.90 10 8 0 7.00 5.60 -10 8 0 5.20 5.10 10 -8 0 -0.30 4.90 -10 8 0 0.80 5.60 11 8 0 13.00 6.60 11 -8 0 7.70 7.00 -11 8 0 9.30 8.00 -11 8 0 14.40 6.70 -11 -8 0 12.80 6.70 0 9 0 0.80 2.60 0 9 0 2.40 1.70 0 -9 0 3.70 2.50 0 -9 0 -1.10 2.00 1 9 0 12.90 2.50 -1 9 0 14.10 2.30 1 -9 0 19.90 3.30 1 9 0 18.20 3.30 -1 -9 0 16.60 3.40 -1 9 0 13.30 3.20 1 -9 0 12.00 3.30 -1 -9 0 16.10 3.00 -2 -9 0 50.59 5.50 2 9 0 39.30 5.20 2 -9 0 40.60 5.00 -2 9 0 46.50 3.90 -2 -9 0 56.59 4.60 2 9 0 48.80 4.40 2 -9 0 38.50 4.80 -2 9 0 45.30 4.90 -3 9 0 -0.80 2.60 -3 9 0 -2.00 1.60 3 9 0 -2.50 3.00 3 -9 0 0.20 2.10 -3 -9 0 1.20 2.30 3 9 0 -1.20 2.30 3 9 0 4.20 2.30 3 -9 0 4.40 2.90 -4 9 0 32.80 4.50 -4 9 0 23.00 4.10 -4 9 0 27.40 3.40 4 9 0 29.60 4.10 4 9 0 29.10 4.90 -4 -9 0 23.70 4.30 4 9 0 35.40 4.40 -4 9 0 35.40 4.70 4 -9 0 26.80 4.30 -5 9 0 40.20 5.80 5 9 0 43.50 5.90 5 9 0 35.60 4.90 -5 -9 0 36.10 5.40 5 9 0 39.90 4.90 -5 9 0 44.50 4.50 -5 9 0 58.09 6.40 5 -9 0 39.50 5.70 6 9 0 16.40 4.10 -6 9 0 4.90 3.20 -6 9 0 4.20 3.70 6 9 0 1.90 4.10 6 -9 0 9.70 3.40 -6 -9 0 0.80 3.20 6 9 0 6.40 3.80 -6 9 0 7.50 3.00 -7 9 0 13.80 4.80 -7 9 0 11.70 3.90 7 9 0 10.20 4.20 7 9 0 16.10 5.00 -7 9 0 12.70 4.70 -7 -9 0 10.70 4.30 7 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6.60 2 11 0 57.29 5.30 -2 11 0 61.39 5.10 -2 11 0 56.99 6.20 2 -11 0 67.69 6.60 -2 -11 0 55.69 6.40 2 -11 0 62.59 6.60 -3 11 0 1.60 2.30 -3 -11 0 1.90 3.40 3 -11 0 2.70 2.60 3 11 0 -0.30 3.70 3 -11 0 4.00 3.60 3 11 0 -1.70 2.90 -3 11 0 3.50 3.30 4 -11 0 6.10 3.80 4 11 0 5.00 3.30 -4 11 0 -0.80 3.60 -4 -11 0 4.30 3.50 4 11 0 9.10 4.60 -4 11 0 0.90 3.80 -4 11 0 5.00 2.70 -5 11 0 6.60 2.90 -5 11 0 9.50 4.40 5 11 0 3.90 3.80 -5 11 0 9.00 4.40 5 11 0 7.10 4.60 -5 -11 0 1.70 3.60 5 -11 0 4.50 4.30 -6 11 0 16.30 5.30 6 11 0 8.50 5.00 6 11 0 15.10 4.70 -6 11 0 15.60 3.70 -6 -11 0 21.50 5.20 -6 11 0 17.20 5.50 6 -11 0 14.40 5.30 -7 11 0 8.20 5.10 7 11 0 14.80 6.00 -7 11 0 9.20 5.10 7 -11 0 24.40 5.80 -7 -11 0 12.30 4.90 -7 11 0 13.80 4.30 7 11 0 3.90 5.10 -8 11 0 -1.00 5.70 -8 11 0 -0.40 5.80 -8 -11 0 -3.80 4.30 8 -11 0 -4.60 4.20 8 11 0 3.80 6.70 -8 11 0 0.00 3.80 -9 11 0 -3.10 5.80 -9 11 0 -2.50 4.60 -9 11 0 4.00 6.10 9 -11 0 -5.80 5.40 -9 -11 0 2.10 5.20 0 12 0 324.67 18.00 0 12 0 346.57 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12 0 14.20 8.10 -9 12 0 13.40 6.60 9 -12 0 7.70 7.60 -9 -12 0 8.80 7.20 -9 12 0 3.40 7.80 -9 12 0 7.40 7.90 0 13 0 3.30 2.90 0 -13 0 2.00 3.60 0 13 0 1.70 3.70 1 13 0 11.20 4.30 1 -13 0 15.60 4.30 1 -13 0 6.60 4.30 -1 13 0 12.30 3.20 -1 -13 0 12.60 4.50 1 13 0 13.70 3.60 -1 13 0 11.10 4.10 2 13 0 7.40 3.50 -2 13 0 9.20 3.00 2 13 0 4.10 3.80 -2 13 0 7.30 3.90 2 -13 0 8.30 4.70 2 -13 0 -2.60 2.50 -2 -13 0 5.70 4.10 3 13 0 46.70 7.30 3 -13 0 58.69 7.30 3 -13 0 52.69 6.90 -3 -13 0 35.00 6.30 -3 13 0 58.59 5.70 -3 13 0 71.69 7.20 3 13 0 61.19 6.50 4 13 0 3.10 4.00 4 -13 0 1.50 4.20 4 13 0 -1.30 3.80 -4 -13 0 1.00 3.80 5 13 0 -5.50 3.90 5 13 0 1.50 5.60 5 -13 0 0.30 5.20 -5 13 0 -4.60 4.30 -5 -13 0 -7.40 3.50 -5 13 0 -9.70 4.10 -5 13 0 2.00 3.20 6 13 0 -5.40 5.10 -6 13 0 1.90 3.50 6 13 0 -1.90 6.70 -6 13 0 3.00 5.50 -6 -13 0 4.70 4.50 6 -13 0 0.90 5.50 -6 13 0 5.70 5.50 7 13 0 12.50 7.20 -7 13 0 3.70 4.10 -7 13 0 -2.20 5.40 7 13 0 -1.30 5.40 -7 -13 0 -2.00 4.90 7 -13 0 2.10 5.20 -7 13 0 0.50 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1.50 2.80 -2 10 -4 14.90 3.80 -3 10 4 -1.30 2.90 -3 -10 -4 3.30 3.30 -3 10 4 0.40 2.40 3 10 -4 1.40 3.50 3 10 -4 0.70 2.40 3 -10 4 1.80 3.10 3 -10 4 3.40 3.10 3 -10 -4 2.50 3.10 3 -10 -4 -0.10 2.70 -3 -10 4 0.40 2.50 3 10 4 3.10 3.00 -3 10 -4 2.60 3.10 3 10 4 3.30 3.40 -3 10 -4 5.60 1.80 4 10 -4 141.49 9.20 -4 10 4 149.29 10.60 -4 10 4 142.89 10.60 4 10 -4 149.88 10.80 4 -10 4 142.79 10.40 -4 -10 -4 153.18 10.40 -4 10 4 156.48 9.30 -4 10 4 152.48 10.00 4 -10 -4 157.58 10.50 -4 -10 4 150.18 10.50 -4 10 -4 148.19 10.30 -4 10 -4 141.39 8.40 -4 10 -4 140.49 10.30 4 10 4 148.59 10.60 4 10 4 151.18 9.70 5 10 -4 26.60 5.20 -5 10 4 34.20 5.60 5 -10 4 22.90 5.10 -5 10 4 29.70 5.40 5 10 -4 22.20 5.40 -5 -10 -4 39.10 5.70 -5 10 4 32.10 4.30 5 10 -4 38.10 4.90 5 -10 -4 28.00 4.90 5 10 4 33.10 5.40 -5 10 -4 38.40 3.80 -5 10 -4 28.30 5.00 -5 10 -4 19.90 4.70 5 10 4 35.30 5.80 -5 -10 4 28.60 5.40 6 10 -4 20.70 4.80 -6 10 4 25.80 5.70 6 10 -4 25.30 5.00 -6 10 4 23.60 4.20 -6 10 4 22.00 5.50 6 -10 4 26.90 5.70 -6 -10 -4 12.10 4.60 6 10 -4 24.10 5.90 -6 10 -4 25.10 3.90 6 10 4 29.10 5.70 -6 -10 4 14.60 5.00 6 10 4 17.50 4.90 6 -10 -4 24.40 5.20 -6 10 -4 20.80 5.00 -6 10 -4 25.50 5.20 -7 10 4 26.60 4.90 -7 -10 -4 38.70 6.20 7 10 -4 34.00 6.80 7 -10 4 33.00 5.70 -7 10 4 14.80 5.50 7 10 -4 35.70 6.30 -7 10 4 32.10 6.40 7 10 -4 36.20 5.90 -7 -10 4 19.40 5.00 -7 10 -4 25.20 5.60 -7 10 -4 27.20 5.90 7 10 4 35.50 6.30 -7 10 -4 34.30 4.60 7 -10 -4 36.80 6.20 8 10 -4 5.30 5.70 -8 10 4 -4.30 3.90 -8 10 4 -2.90 4.80 8 10 -4 5.80 5.50 8 10 -4 -4.00 4.30 8 -10 4 13.00 5.30 -8 10 4 5.90 5.40 -8 -10 -4 2.30 3.70 -8 10 -4 0.40 3.20 -8 -10 4 -3.40 3.80 -8 10 -4 -0.10 4.00 -8 10 -4 4.80 3.70 8 -10 -4 0.10 4.70 -9 10 4 19.20 6.60 -9 -10 -4 25.50 6.40 -9 10 4 11.20 5.10 -9 10 4 26.80 7.10 9 10 -4 18.60 6.20 9 -10 4 17.30 6.00 -9 10 -4 23.00 6.20 9 -10 -4 19.80 6.20 -9 10 -4 8.00 5.40 9 10 4 13.70 8.00 -9 10 -4 11.60 5.10 -9 -10 4 12.50 6.50 10 10 -4 12.50 6.40 -10 10 4 9.10 7.40 -10 10 4 19.50 6.60 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5.20 3 11 -4 37.80 4.40 -3 11 4 30.70 5.10 3 -11 4 33.70 5.20 3 11 4 44.80 5.20 3 -11 -4 48.20 5.90 -3 -11 4 43.50 6.20 3 -11 -4 41.30 5.80 3 11 4 46.50 6.20 -3 11 -4 34.60 3.70 -3 11 -4 39.30 5.10 4 -11 4 17.80 4.80 -4 -11 -4 26.30 5.00 -4 11 4 32.30 5.00 4 11 -4 14.90 5.00 -4 11 4 25.60 4.00 -4 11 4 20.40 4.50 -4 11 4 22.70 4.50 4 11 -4 26.10 4.40 4 11 4 25.20 4.80 -4 11 -4 22.80 4.80 -4 -11 4 19.50 4.90 4 -11 -4 39.30 5.70 -4 11 -4 20.10 4.50 4 11 4 20.30 5.20 -4 11 -4 18.60 2.90 -5 11 4 8.30 4.70 -5 11 4 17.30 3.90 5 11 -4 26.70 4.70 -5 11 4 22.60 5.30 5 11 -4 20.00 5.80 -5 -11 -4 23.60 5.30 5 -11 4 24.90 5.40 -5 11 -4 34.10 3.70 5 -11 -4 23.80 5.00 -5 11 -4 25.40 5.30 5 11 4 33.80 5.40 -5 -11 4 31.20 5.80 5 11 4 29.90 6.00 -6 11 4 12.60 4.10 -6 -11 -4 10.10 4.50 6 11 -4 6.00 5.10 -6 11 4 10.20 5.00 6 11 -4 4.80 4.00 6 -11 4 12.80 5.10 -6 11 4 10.80 5.10 -6 11 -4 11.10 4.60 6 11 4 8.60 5.00 6 -11 -4 14.80 5.50 -6 11 -4 10.80 3.20 6 11 4 7.00 5.10 -6 11 -4 6.60 4.00 -6 -11 4 12.80 4.90 -7 11 4 13.10 5.60 -7 -11 -4 8.40 5.20 7 -11 4 10.90 5.80 7 11 -4 10.70 5.10 -7 11 4 10.30 4.60 -7 11 4 2.90 4.80 7 11 -4 7.30 6.30 7 -11 -4 7.70 4.70 -7 11 -4 6.50 3.60 7 11 4 11.90 6.60 -7 -11 4 5.40 4.20 -7 11 -4 7.20 3.90 -7 11 -4 15.90 3.90 8 -11 4 5.60 5.80 -8 11 4 11.80 4.90 8 11 -4 -1.30 5.90 8 11 -4 17.60 6.20 -8 11 4 2.60 5.70 -8 11 4 8.40 6.10 -8 -11 -4 8.00 5.70 -8 11 -4 16.60 5.70 -8 11 -4 18.50 5.10 8 -11 -4 17.30 5.80 -8 -11 4 7.50 5.90 8 11 4 3.20 8.30 -8 11 -4 14.50 5.50 -9 -11 -4 10.60 6.10 -9 11 4 7.90 6.70 9 11 -4 -0.30 8.50 -9 11 4 3.00 6.50 -9 11 4 2.80 6.40 9 -11 4 2.30 5.90 -9 11 -4 10.00 5.60 -9 11 -4 4.80 5.50 -9 -11 4 11.20 7.00 -9 11 -4 6.70 5.20 9 -11 -4 8.60 6.20 0 12 4 17.60 3.50 0 -12 -4 13.80 4.20 0 -12 -4 19.20 4.10 0 12 4 9.60 4.00 0 12 -4 15.10 2.70 0 12 -4 23.10 4.50 0 -12 4 15.60 4.40 1 12 -4 6.40 3.90 1 12 -4 11.10 2.70 -1 12 4 10.90 4.10 -1 12 4 12.20 3.40 1 -12 4 13.70 3.80 1 -12 4 14.80 4.40 -1 -12 -4 12.20 4.00 -1 -12 -4 15.00 4.40 1 12 4 19.80 4.40 1 12 4 7.70 3.30 -1 12 -4 11.10 2.40 -1 -12 4 16.40 4.40 1 -12 -4 3.20 3.50 -1 12 -4 12.80 3.80 1 -12 -4 13.70 4.10 -2 -12 -4 28.40 5.20 -2 12 4 35.50 5.40 -2 12 4 28.90 4.20 2 -12 4 30.60 5.00 2 12 -4 31.60 4.00 2 12 -4 28.40 5.30 2 -12 4 37.60 5.70 -2 12 -4 32.50 5.10 2 12 4 25.30 5.20 -2 12 -4 24.50 3.20 2 12 4 36.70 5.10 2 -12 -4 28.90 5.30 -2 -12 4 37.00 5.80 2 -12 -4 38.40 5.60 3 12 -4 50.99 5.20 -3 -12 -4 32.90 5.70 3 12 -4 28.10 5.70 -3 12 4 39.60 5.70 3 -12 4 35.40 5.70 -3 12 4 41.30 4.80 3 -12 4 50.19 6.10 -3 -12 4 39.40 6.10 3 -12 -4 42.60 6.20 3 12 4 34.70 6.20 3 -12 -4 27.90 5.60 -3 12 -4 36.70 5.30 -3 12 -4 44.30 4.10 3 12 4 41.40 5.30 4 12 -4 3.80 3.50 4 -12 4 8.50 4.30 -4 12 4 4.80 4.40 -4 -12 -4 19.90 4.60 -4 12 4 5.40 3.20 -4 12 4 4.70 4.30 -4 12 4 7.00 5.30 4 12 -4 14.70 5.30 4 -12 -4 2.70 5.00 4 12 4 12.90 4.90 4 12 4 3.10 4.60 -4 -12 4 -1.60 2.90 -5 -12 -4 42.90 6.40 5 12 -4 38.80 5.50 -5 12 4 33.20 4.80 5 12 -4 41.80 7.10 -5 12 4 44.90 6.90 5 -12 4 29.60 6.20 -5 12 4 37.70 6.70 -5 12 -4 47.10 6.40 5 -12 -4 34.20 6.60 5 12 4 27.70 5.50 -5 12 -4 36.50 6.20 -5 12 -4 35.10 4.20 5 12 4 42.20 7.20 -5 -12 4 35.90 6.50 -6 12 4 25.40 6.40 -6 -12 -4 17.10 5.80 -6 12 4 19.40 4.80 6 12 -4 38.70 6.30 6 -12 4 26.90 6.70 -6 12 4 36.40 6.90 6 12 -4 29.00 7.10 -6 12 -4 21.30 4.20 6 12 4 12.90 5.80 -6 -12 4 13.00 5.60 6 12 4 16.10 6.20 -6 12 -4 23.00 5.70 6 -12 -4 37.80 7.10 -6 12 -4 38.80 6.50 -7 -12 -4 8.40 5.30 7 12 -4 9.70 5.60 7 -12 4 1.60 5.80 -7 12 4 0.70 5.30 -7 12 4 4.80 5.70 -7 12 4 1.60 4.10 7 12 -4 -0.90 6.10 -7 12 -4 -1.00 4.40 7 -12 -4 7.50 5.70 7 12 4 8.50 6.20 -7 12 -4 2.80 3.80 -7 -12 4 -2.30 5.10 -7 12 -4 2.90 4.90 8 -12 4 31.90 8.60 -8 12 4 29.60 6.20 8 12 -4 32.70 8.20 -8 12 4 22.20 7.30 8 12 -4 16.30 6.80 -8 -12 -4 32.20 7.10 -8 12 4 26.50 7.40 -8 12 -4 34.70 7.20 -8 -12 4 20.60 7.20 8 -12 -4 20.90 6.90 -8 12 -4 26.20 6.50 -8 12 -4 21.30 5.40 8 12 4 22.80 8.10 -9 12 4 8.00 8.00 -9 12 4 5.70 5.70 -9 12 4 16.80 8.50 -9 -12 -4 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10 -5 47.30 6.60 5 10 -5 44.90 5.50 5 -10 5 39.30 6.10 -5 10 5 53.09 6.60 -5 10 5 48.50 5.40 -5 10 5 57.59 6.90 -5 10 -5 55.39 6.50 5 10 5 50.89 6.60 -5 10 -5 36.20 4.00 -5 -10 5 45.10 6.20 5 -10 -5 51.89 6.50 -5 10 -5 42.40 6.00 5 10 5 51.19 6.30 6 10 -5 8.10 4.00 -6 10 5 4.10 3.20 6 10 -5 1.70 3.90 6 10 -5 10.30 4.90 -6 -10 -5 3.60 2.90 -6 10 5 -1.00 4.00 -6 10 5 6.50 4.40 6 -10 5 1.50 4.40 6 -10 -5 1.90 3.90 6 10 5 5.80 4.40 -6 -10 5 10.70 4.40 -6 10 -5 6.50 2.90 -6 10 -5 10.50 4.10 -6 10 -5 7.50 3.90 6 10 5 13.70 5.00 -7 -10 -5 72.79 8.10 7 10 -5 73.09 7.80 -7 10 5 79.39 7.20 -7 10 5 53.79 8.00 7 10 -5 58.79 7.20 7 10 -5 73.79 8.80 7 -10 5 61.89 8.30 -7 10 5 53.49 7.90 7 -10 -5 67.09 8.00 7 10 5 60.79 7.70 -7 10 -5 51.19 7.10 -7 10 -5 71.09 8.00 -7 -10 5 44.70 7.40 -7 10 -5 66.49 6.20 8 10 -5 9.70 6.30 8 10 -5 13.10 5.30 -8 -10 -5 11.70 5.40 8 -10 5 19.60 5.90 -8 10 5 14.10 5.80 8 10 -5 24.50 6.30 -8 10 5 6.80 4.40 -8 10 5 12.30 5.80 -8 10 -5 15.80 5.30 -8 10 -5 19.60 4.80 -8 -10 5 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11 5 21.60 4.90 5 11 5 23.10 6.10 -5 11 -5 19.10 4.90 -6 11 5 -2.40 4.30 -6 11 5 -2.90 4.40 -6 11 5 -0.60 3.60 6 11 -5 4.60 5.10 -6 -11 -5 2.00 3.80 6 11 -5 3.10 3.80 6 -11 5 -0.30 4.90 6 11 5 -3.20 4.60 6 -11 -5 -4.40 4.30 -6 11 -5 2.10 2.50 -6 -11 5 -0.90 4.20 -6 11 -5 3.20 4.00 6 11 5 4.80 4.90 -6 11 -5 4.80 3.80 7 -11 5 2.80 5.60 -7 11 5 -3.50 4.60 7 11 -5 1.20 5.00 7 11 -5 19.90 6.60 -7 11 5 3.50 3.80 -7 11 5 3.50 5.00 -7 -11 -5 8.30 4.70 7 -11 -5 5.70 4.60 -7 11 -5 7.30 4.50 -7 11 -5 4.00 4.20 -7 -11 5 -0.70 4.80 -7 11 -5 2.00 3.40 7 11 5 1.70 6.00 8 -11 5 18.80 6.50 8 11 -5 6.10 5.80 -8 -11 -5 20.80 6.20 -8 11 5 21.20 6.90 -8 11 5 16.80 6.50 8 11 -5 13.60 13.10 8 11 -5 5.10 7.30 -8 11 5 13.50 5.30 -8 11 -5 12.80 5.30 -8 -11 5 15.50 6.00 8 -11 -5 13.70 5.60 -8 11 -5 4.60 4.90 -8 11 -5 10.70 4.40 -9 11 5 3.10 6.70 -9 11 5 8.20 5.60 9 11 -5 -8.80 6.60 9 -11 5 -6.70 5.90 -9 11 5 5.30 6.70 -9 -11 -5 14.70 6.20 9 -11 -5 -0.30 5.90 -9 11 -5 -2.90 4.90 -9 -11 5 7.30 6.80 -9 11 -5 -0.50 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10.60 6.50 -8 12 5 5.10 6.70 -8 -12 -5 7.80 6.60 -8 12 5 1.20 6.20 -8 12 5 2.00 4.70 8 -12 5 7.30 7.10 8 12 -5 -7.00 6.80 8 12 -5 -0.90 6.20 -8 -12 5 3.10 6.10 -8 12 -5 3.70 5.00 8 -12 -5 5.80 5.40 -8 12 -5 1.20 4.90 8 12 5 -6.50 8.50 -8 12 -5 3.60 4.30 0 -13 -5 11.50 4.20 0 -13 -5 16.50 4.50 0 -13 5 15.30 4.70 0 13 -5 13.30 2.90 0 13 5 9.90 3.90 0 13 5 10.50 4.20 0 13 -5 8.20 4.00 1 13 -5 19.10 3.30 -1 -13 -5 21.40 5.00 1 -13 5 9.40 4.40 1 -13 5 15.20 4.60 -1 13 5 16.90 4.00 -1 13 5 14.80 4.60 1 13 -5 17.10 4.80 -1 13 -5 12.80 2.70 1 -13 -5 13.40 4.30 -1 -13 5 20.80 5.20 1 13 5 19.00 5.00 1 -13 -5 13.10 4.30 -1 13 -5 6.80 3.90 1 13 5 16.10 4.20 2 -13 5 3.80 3.70 2 13 -5 6.80 3.10 -2 13 5 2.10 4.20 -2 13 5 7.80 3.70 -2 -13 -5 6.60 4.10 2 -13 5 0.10 4.20 2 13 -5 14.80 4.70 2 13 5 11.90 3.80 2 -13 -5 5.80 3.80 2 -13 -5 4.60 4.20 -2 -13 5 10.30 4.00 -2 13 -5 11.90 4.00 -2 13 -5 5.80 2.40 2 13 5 10.10 4.50 -3 -13 -5 49.50 6.90 3 -13 5 46.50 6.40 3 13 -5 40.60 5.10 3 -13 5 37.90 6.50 -3 13 5 31.70 5.80 -3 13 5 49.60 5.50 3 13 -5 35.80 6.50 3 -13 -5 28.20 5.80 3 -13 -5 48.50 6.80 -3 13 -5 47.80 4.30 3 13 5 39.10 6.90 -3 -13 5 27.10 6.00 3 13 5 45.60 6.20 -4 13 5 40.00 5.20 4 -13 5 37.20 6.50 -4 13 5 56.49 7.70 -4 -13 -5 49.10 7.20 4 13 -5 35.70 5.40 4 13 -5 32.50 7.00 -4 13 5 35.90 6.80 4 13 5 41.60 6.20 -4 -13 5 45.60 7.40 4 13 5 35.10 7.20 4 -13 -5 51.59 7.50 5 -13 5 3.90 5.20 5 13 -5 14.10 6.00 5 13 -5 20.20 5.20 -5 13 5 4.60 5.10 -5 13 5 6.20 4.10 -5 -13 -5 12.00 5.30 -5 13 5 16.10 5.70 -5 13 -5 10.60 4.70 -5 13 -5 7.60 4.60 5 13 5 12.30 6.00 5 -13 -5 11.90 4.90 -5 13 -5 6.20 2.80 5 13 5 5.80 5.30 -5 -13 5 15.40 5.90 6 -13 5 24.50 7.20 -6 -13 -5 26.80 6.40 -6 13 5 16.40 6.50 -6 13 5 15.00 6.40 -6 13 5 25.40 5.40 6 13 -5 1.80 5.60 6 13 -5 22.30 7.10 -6 13 -5 31.40 6.40 6 13 5 15.70 6.60 -6 13 -5 17.70 3.90 -6 -13 5 19.90 6.40 6 13 5 22.30 6.80 -6 13 -5 14.70 5.60 6 -13 -5 18.00 6.90 -7 13 5 4.40 4.50 -7 13 5 4.30 5.80 -7 -13 -5 15.50 6.30 7 13 -5 6.40 6.10 7 -13 5 2.20 6.70 7 13 -5 7.20 7.10 -7 13 5 10.60 6.50 -7 -13 5 -1.40 6.00 -7 13 -5 10.00 5.40 7 13 5 -0.80 6.50 -7 13 -5 -0.10 4.00 7 -13 -5 6.80 7.10 -7 13 -5 1.30 4.70 8 13 -5 7.40 7.20 -8 13 5 2.70 5.20 -8 -13 -5 -2.90 6.00 -8 13 5 5.50 7.40 8 -13 5 11.30 8.70 -8 13 5 1.70 7.10 8 13 -5 5.70 8.00 -8 13 -5 -3.10 5.60 -8 13 -5 6.20 6.30 -8 13 -5 2.10 5.00 -8 -13 5 -4.50 7.30 8 13 5 2.60 8.40 8 -13 -5 1.00 7.10 0 -14 -5 8.10 5.00 0 14 5 7.00 4.40 0 14 -5 6.30 2.70 0 14 -5 8.20 4.30 0 -14 5 9.90 5.10 0 -14 -5 7.80 4.30 0 14 5 8.60 4.10 -1 14 5 25.90 4.90 1 14 -5 19.30 5.30 1 14 -5 28.80 3.80 -1 -14 -5 19.80 5.30 1 -14 5 11.20 5.10 -1 14 5 20.50 5.20 1 14 5 20.60 4.70 -1 14 -5 21.60 3.30 -1 14 -5 10.70 4.70 -1 -14 5 16.90 5.60 1 14 5 26.00 5.70 1 -14 -5 14.50 4.90 1 -14 -5 20.70 5.00 2 -14 5 2.60 4.30 2 14 -5 1.70 3.40 2 -14 5 0.50 3.50 2 14 -5 2.50 4.70 -2 14 5 9.60 5.30 -2 14 5 6.70 4.00 -2 -14 -5 1.90 4.40 2 14 5 -0.20 4.00 2 -14 -5 5.20 4.40 -2 14 -5 -1.40 4.10 2 14 5 -1.10 4.00 2 -14 -5 -1.40 3.90 -2 14 -5 7.40 2.50 -2 -14 5 5.70 4.60 3 14 -5 4.80 5.00 -3 -14 -5 12.70 5.00 3 14 -5 6.90 3.90 3 -14 5 16.80 5.60 3 -14 5 17.40 5.90 -3 14 5 11.40 4.30 -3 14 5 14.10 5.30 -3 -14 5 12.50 5.20 -3 14 -5 11.20 3.00 3 -14 -5 13.70 4.80 3 14 5 6.60 5.70 3 14 5 7.70 4.80 3 -14 -5 14.50 5.40 -4 14 5 18.80 6.20 -4 14 5 21.30 4.70 -4 14 5 29.30 6.60 -4 -14 -5 15.20 5.50 4 14 -5 16.60 6.30 4 -14 5 20.70 5.90 4 14 -5 14.50 4.90 4 14 5 24.30 6.90 -4 14 -5 24.10 3.70 4 14 5 23.70 5.60 4 -14 -5 31.80 7.00 -4 -14 5 11.00 5.80 -5 -14 -5 19.20 6.20 5 -14 5 30.10 7.30 5 14 -5 28.60 7.60 5 14 -5 23.70 5.80 -5 14 5 27.30 6.80 -5 14 5 20.80 5.20 -5 14 5 19.00 6.60 5 14 5 19.90 6.10 -5 14 -5 21.60 4.00 5 -14 -5 35.20 7.80 -5 14 -5 27.10 6.20 5 14 5 16.50 7.10 -5 14 -5 24.30 5.90 -5 -14 5 14.40 6.30 -6 14 5 -0.10 5.80 -6 14 5 3.10 6.10 6 14 -5 6.00 7.40 6 -14 5 8.80 7.00 -6 -14 -5 -3.80 4.80 6 14 -5 1.60 5.40 -6 14 5 1.00 4.50 -6 14 -5 -6.20 4.60 6 14 5 6.00 7.00 6 14 5 10.60 7.00 -6 14 -5 4.20 5.00 6 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4.50 10 -4 -10 5.40 5.40 -10 -4 10 -6.70 4.50 11 4 -10 1.20 6.30 -11 4 10 3.00 6.10 11 -4 10 -9.60 5.00 11 -4 10 5.60 6.90 -11 -4 -10 0.50 4.80 -11 4 -10 0.40 5.70 -11 -4 10 3.20 6.00 11 4 10 -1.00 4.80 -11 4 -10 -3.50 4.60 0 -5 10 357.86 17.80 0 -5 -10 349.57 17.50 0 -5 10 362.46 17.60 0 5 10 368.56 17.10 0 5 10 357.36 18.00 0 -5 -10 317.57 18.00 0 -5 10 352.46 17.70 0 5 10 344.37 17.60 0 -5 -10 359.96 17.70 0 -5 10 336.77 17.80 1 -5 10 185.18 10.30 -1 5 10 198.78 10.40 1 5 -10 186.58 9.30 1 -5 10 197.78 10.50 1 5 -10 193.28 10.50 1 -5 10 190.88 10.40 -1 5 10 184.18 10.70 1 -5 10 192.48 10.50 -1 -5 -10 200.68 10.60 1 5 -10 191.68 9.40 -1 -5 -10 203.98 10.30 -1 -5 -10 192.78 10.40 1 5 10 209.58 10.60 -1 -5 10 178.78 10.70 1 -5 -10 183.58 10.40 1 -5 -10 193.98 9.70 1 5 10 199.18 11.00 1 5 10 207.78 10.10 -1 -5 10 193.78 10.70 1 -5 -10 200.88 10.90 1 -5 -10 190.88 10.40 -1 -5 10 189.58 10.10 2 5 -10 224.58 11.00 -2 -5 -10 238.48 11.80 -2 -5 -10 230.38 11.90 2 -5 10 218.98 11.90 -2 -5 -10 213.38 12.00 2 5 -10 210.58 11.00 2 5 -10 219.08 11.90 -2 5 10 223.18 12.10 2 -5 10 219.88 11.90 2 -5 10 213.68 12.00 2 5 -10 228.28 11.20 2 -5 10 216.88 11.60 2 5 10 219.58 12.10 2 5 10 234.38 11.90 2 -5 -10 217.08 11.00 -2 -5 10 209.88 12.10 2 -5 -10 221.88 12.30 2 5 10 233.38 11.60 -2 -5 10 216.08 11.90 3 -5 10 93.49 6.80 3 5 -10 100.09 5.90 -3 5 10 100.79 6.70 -3 -5 -10 91.89 6.30 -3 -5 -10 105.09 6.60 -3 -5 -10 91.09 6.50 3 -5 10 104.49 6.60 3 -5 10 103.29 5.90 -3 5 10 98.49 6.50 3 5 -10 103.59 6.70 -3 5 10 95.39 6.40 -3 5 10 105.19 6.30 -3 5 -10 102.09 5.10 -3 -5 10 108.19 6.60 -3 -5 10 99.29 6.70 3 5 10 89.99 6.50 -3 5 -10 95.69 6.40 3 5 10 92.89 6.20 3 -5 -10 100.39 5.70 -3 5 -10 90.79 6.30 3 -5 -10 88.49 6.60 -3 5 -10 94.89 5.00 3 5 10 96.99 6.40 -4 5 10 13.90 2.90 4 -5 10 9.20 2.60 -4 -5 -10 14.30 3.00 4 5 -10 12.70 2.50 -4 5 10 12.30 2.70 -4 5 10 7.90 2.70 -4 -5 -10 11.70 2.70 -4 -5 -10 15.30 2.80 -4 5 10 10.60 2.60 4 -5 10 10.00 2.90 4 5 -10 12.50 2.90 4 5 10 11.40 2.60 -4 5 -10 7.70 2.70 4 5 10 7.40 2.50 4 5 10 12.00 2.80 -4 -5 10 12.40 2.90 4 -5 -10 9.40 2.80 -4 5 -10 5.60 1.50 -4 -5 10 9.10 2.70 -4 5 -10 9.80 2.80 4 -5 -10 14.20 2.20 5 5 -10 47.40 5.40 -5 5 10 58.69 5.70 5 5 -10 57.79 5.10 -5 -5 -10 50.99 5.30 -5 -5 -10 52.49 5.40 -5 5 10 61.29 5.30 5 -5 10 60.99 5.80 -5 5 10 61.79 5.30 -5 5 10 72.99 6.20 5 -5 10 50.89 5.50 -5 -5 10 53.09 5.50 5 -5 -10 56.69 4.90 5 -5 -10 51.59 5.50 5 5 10 48.80 5.20 -5 5 -10 52.79 5.40 5 5 10 59.09 5.40 -5 5 -10 54.69 4.20 -5 -5 10 56.99 5.60 -5 5 -10 49.70 5.30 6 -5 10 23.70 4.20 -6 5 10 11.20 3.70 -6 5 10 18.90 3.70 -6 5 10 27.70 4.10 -6 5 10 22.20 4.20 -6 -5 -10 13.20 3.90 6 5 -10 23.30 3.90 6 -5 10 22.50 4.10 6 5 -10 17.00 3.80 -6 -5 -10 12.30 3.50 6 -5 -10 27.90 4.10 6 5 10 20.10 4.30 6 -5 -10 21.70 4.10 -6 -5 10 12.30 3.70 -6 5 -10 12.80 2.80 -6 5 -10 22.40 4.10 -6 -5 10 23.20 4.00 -6 5 -10 14.80 3.70 6 5 10 22.90 4.10 -7 5 10 6.50 3.70 -7 5 10 13.70 4.30 7 5 -10 9.70 3.60 7 -5 10 8.40 3.60 7 -5 10 11.90 3.90 -7 -5 -10 16.10 3.90 7 5 -10 7.60 3.10 7 -5 -10 1.30 3.00 -7 5 -10 4.40 3.10 -7 5 -10 9.20 3.10 -7 5 -10 11.50 3.60 -7 -5 10 8.40 3.70 7 5 10 8.50 3.60 -7 -5 10 6.40 3.30 7 -5 -10 10.40 4.10 8 5 -10 28.90 5.30 8 5 -10 34.80 5.40 8 -5 10 22.40 5.30 -8 5 10 23.30 5.40 -8 -5 -10 27.80 5.30 8 -5 10 21.20 5.10 -8 5 -10 21.20 4.80 -8 -5 10 29.20 5.30 8 5 10 28.20 5.00 -8 -5 10 25.20 5.20 8 -5 -10 18.10 4.40 -8 5 -10 23.20 4.20 9 -5 10 38.90 6.60 -9 -5 -10 31.30 5.90 9 -5 10 56.49 7.60 -9 5 10 37.50 6.60 9 5 -10 38.80 6.50 -9 5 -10 41.50 6.40 -9 -5 10 29.40 6.30 9 5 10 31.70 5.90 9 -5 -10 35.90 6.40 -9 5 -10 40.90 5.70 -10 5 10 20.60 6.40 -10 -5 -10 31.30 6.00 10 -5 10 23.80 7.40 10 5 -10 24.70 6.00 10 -5 10 26.00 6.30 10 5 10 40.70 6.70 -10 5 -10 7.40 5.10 -10 -5 10 16.10 6.20 -10 5 -10 26.60 5.60 11 -5 10 15.60 6.70 11 -5 10 28.60 7.50 -11 5 10 30.10 7.80 11 5 -10 20.40 6.50 -11 -5 -10 31.80 6.90 -11 5 -10 14.70 6.20 11 5 10 32.10 7.20 -11 5 -10 21.90 6.70 -11 -5 10 19.30 7.00 0 -6 10 41.90 3.90 0 -6 -10 34.10 3.70 0 -6 10 38.70 4.10 0 -6 -10 40.90 4.20 0 -6 10 42.10 3.80 0 -6 10 38.40 4.00 0 6 10 52.19 4.70 0 6 10 49.50 4.10 1 -6 10 65.89 4.60 1 -6 10 57.59 5.00 -1 -6 -10 74.49 5.20 -1 -6 -10 69.99 5.20 -1 -6 -10 65.19 5.10 -1 6 10 70.29 4.70 1 -6 10 64.49 4.70 1 -6 10 64.79 4.70 -1 6 10 58.39 5.20 1 6 -10 61.49 4.60 1 6 -10 53.39 3.30 1 6 -10 58.29 3.40 -1 -6 10 59.89 5.10 1 6 10 69.39 4.10 1 -6 -10 62.79 4.60 1 -6 -10 63.89 5.30 -1 -6 10 55.79 5.20 1 6 10 57.79 5.40 1 6 10 59.99 4.90 -1 -6 10 60.09 4.30 2 6 -10 84.59 5.40 2 6 -10 84.69 5.80 -2 6 10 82.59 6.10 2 -6 10 80.69 5.90 2 6 -10 85.99 4.80 2 -6 10 82.19 5.80 2 -6 10 91.39 5.60 -2 6 10 78.19 5.50 -2 -6 -10 84.69 5.70 -2 -6 -10 88.39 6.20 -2 -6 -10 71.19 5.80 2 -6 10 81.59 5.60 -2 -6 10 85.09 5.80 2 -6 -10 80.29 5.50 -2 -6 10 70.99 6.10 2 -6 -10 77.99 6.00 2 6 10 80.89 5.50 2 6 10 69.99 6.10 2 6 10 75.49 5.00 -3 6 10 153.28 9.00 -3 -6 -10 157.48 9.30 -3 -6 -10 130.69 8.80 3 6 -10 142.39 9.00 3 -6 10 152.98 9.30 -3 6 10 161.08 9.10 -3 6 10 155.78 8.70 3 6 -10 145.79 8.20 -3 6 10 144.19 9.10 3 -6 10 163.88 9.10 -3 -6 10 144.69 9.30 3 6 10 152.28 9.30 -3 6 -10 155.18 7.50 -3 -6 10 148.49 9.20 3 6 10 143.79 8.90 -3 6 -10 149.39 7.60 -3 6 -10 157.48 9.20 3 6 10 156.28 8.80 -3 6 -10 146.89 9.10 3 -6 -10 151.28 9.50 -4 -6 -10 102.19 7.10 4 -6 10 102.49 7.30 -4 6 10 112.59 7.50 4 -6 10 103.79 7.70 -4 6 10 108.89 7.50 -4 6 10 101.69 7.00 4 6 -10 115.09 6.90 -4 6 10 102.09 7.20 4 6 -10 110.29 7.50 -4 -6 -10 113.09 7.50 -4 -6 10 99.29 7.20 4 -6 -10 87.49 6.90 -4 6 -10 98.09 5.60 -4 6 -10 106.39 7.30 -4 6 -10 97.19 7.20 -4 -6 10 100.19 7.30 4 6 10 112.39 7.60 4 6 10 108.29 6.80 4 6 10 93.79 7.30 -5 6 10 47.80 4.90 5 6 -10 41.10 5.10 -5 -6 -10 38.20 4.80 5 6 -10 42.70 4.60 5 -6 10 39.30 5.10 -5 6 10 40.40 5.00 -5 6 10 42.40 5.10 -5 6 10 46.70 4.70 -5 -6 -10 38.80 4.70 5 -6 10 47.00 5.50 -5 6 -10 37.50 3.50 -5 -6 10 45.60 5.20 -5 6 -10 50.79 5.30 5 6 10 41.00 5.50 -5 -6 10 42.20 5.20 5 6 10 39.30 4.80 5 6 10 40.20 4.90 -5 6 -10 40.20 4.90 5 -6 -10 37.70 5.00 -6 -6 -10 162.18 11.10 -6 6 10 162.88 11.40 6 6 -10 178.18 11.00 -6 6 10 201.28 11.20 6 6 -10 179.98 11.20 6 -6 10 186.78 11.80 -6 6 10 189.58 11.70 6 -6 10 178.78 11.30 -6 -6 10 153.38 11.00 6 6 10 173.88 11.00 6 6 10 189.48 10.90 -6 6 -10 165.18 9.80 -6 6 -10 180.08 11.20 -6 -6 10 174.38 10.90 -6 6 -10 171.78 11.10 6 -6 -10 174.48 11.20 -7 6 10 3.10 3.60 7 6 -10 3.40 3.30 7 -6 10 1.70 3.80 -7 -6 -10 6.70 3.50 7 -6 10 0.90 3.20 -7 6 10 9.40 4.00 -7 6 10 4.90 3.70 7 6 -10 -1.30 3.40 -7 -6 10 2.80 3.00 -7 6 -10 -1.00 3.00 7 6 10 4.00 3.50 7 -6 -10 -0.90 3.00 -7 -6 10 -0.10 2.70 -7 6 -10 0.10 3.10 -7 6 -10 6.50 2.90 8 6 -10 3.80 4.10 8 6 -10 4.00 3.00 -8 6 10 2.80 4.20 8 -6 10 4.60 3.90 -8 -6 -10 2.80 3.50 8 -6 10 3.50 4.10 -8 6 -10 -1.90 3.10 8 6 10 -1.40 3.80 -8 -6 10 -5.00 2.80 -8 6 -10 1.50 3.20 -8 6 -10 0.40 3.50 8 -6 -10 -2.20 3.40 -8 -6 10 4.80 4.30 -9 6 10 3.10 5.00 9 6 -10 4.50 4.70 9 -6 10 1.40 4.50 -9 -6 -10 -0.90 3.90 9 -6 10 1.20 4.60 -9 6 -10 7.50 4.40 9 -6 -10 -4.00 3.50 -9 -6 10 1.50 4.80 9 6 10 3.90 4.20 -9 6 -10 1.50 3.90 10 -6 10 -0.50 5.10 -10 -6 -10 4.20 4.80 10 6 -10 4.00 4.80 10 -6 10 3.50 6.00 -10 6 10 2.80 5.40 10 6 10 0.90 5.30 -10 -6 10 9.30 5.70 -10 6 -10 6.00 4.50 -10 6 -10 6.00 4.80 10 -6 -10 2.10 6.40 -11 -6 -10 9.70 5.80 -11 6 10 -2.20 7.20 11 6 -10 3.00 5.90 11 -6 10 7.60 5.70 11 -6 10 0.60 7.20 11 6 10 2.70 5.50 -11 6 -10 -5.10 5.00 -11 -6 10 2.40 6.10 -11 6 -10 2.40 5.60 0 -7 10 256.77 14.50 0 -7 -10 264.17 14.40 0 7 10 275.47 14.90 0 7 10 261.97 14.20 0 -7 -10 272.67 14.80 0 -7 10 291.77 14.20 0 -7 10 262.77 14.50 -1 7 10 91.79 6.70 1 7 -10 92.09 4.80 1 7 -10 89.39 6.00 -1 -7 -10 91.79 6.50 1 -7 10 80.89 6.10 1 -7 10 93.59 6.40 -1 -7 -10 91.79 6.30 -1 7 10 85.59 5.90 1 -7 10 94.89 6.30 1 -7 10 83.89 5.90 1 7 -10 87.59 4.80 -1 -7 10 91.09 6.70 1 7 10 92.89 7.00 1 -7 -10 92.99 6.30 1 -7 -10 90.79 6.50 -1 -7 10 99.09 5.90 -1 -7 10 94.99 6.60 1 7 10 94.29 6.30 2 -7 10 127.09 8.00 -2 7 10 116.29 8.00 -2 -7 -10 113.99 7.60 2 -7 10 126.99 7.60 2 7 -10 121.79 7.60 2 7 -10 116.69 6.60 2 -7 10 119.79 7.80 -2 7 10 116.99 7.50 2 -7 10 115.59 7.50 -2 -7 -10 123.69 8.00 2 -7 -10 130.09 7.70 -2 -7 10 115.59 7.80 -2 -7 10 115.59 8.00 2 7 10 122.79 8.20 2 7 10 115.49 7.50 2 -7 -10 105.59 7.90 2 7 10 123.99 7.00 -3 7 10 304.07 16.60 -3 -7 -10 319.27 16.60 3 -7 10 306.97 16.20 -3 7 10 298.07 16.50 -3 7 10 306.67 16.60 -3 7 10 312.17 16.10 3 7 -10 314.27 15.60 -3 -7 -10 321.17 16.50 3 -7 10 298.67 16.80 3 7 -10 301.77 16.40 3 7 10 349.77 17.00 -3 7 -10 312.17 15.30 3 7 10 329.07 17.30 3 7 10 318.37 16.40 -3 -7 10 323.87 17.20 -3 -7 10 312.47 17.20 -3 7 -10 316.77 16.40 3 -7 -10 292.97 17.20 4 7 -10 49.90 5.40 4 -7 10 58.79 6.00 -4 7 10 66.99 6.10 -4 7 10 61.39 5.70 -4 7 10 57.39 5.20 -4 -7 -10 52.49 5.20 4 -7 10 64.19 5.70 -4 -7 -10 45.70 5.50 -4 7 10 67.09 6.10 4 7 -10 52.99 4.70 4 7 10 44.60 4.60 4 7 10 57.49 5.80 4 7 10 45.40 5.10 -4 7 -10 45.10 5.20 4 -7 -10 60.69 5.90 -4 -7 10 49.90 5.40 -4 7 -10 46.50 3.50 -4 7 -10 44.30 5.10 -4 -7 10 57.29 5.70 5 -7 10 88.69 7.30 5 7 -10 79.59 6.60 5 7 -10 83.49 7.40 -5 7 10 90.69 7.30 -5 7 10 72.99 7.30 -5 -7 -10 95.29 7.80 -5 -7 -10 97.79 7.40 -5 7 10 75.19 6.70 5 -7 10 81.49 7.40 -5 7 10 77.19 7.40 -5 7 -10 75.99 7.30 5 7 10 90.49 7.10 -5 -7 10 82.69 7.30 -5 7 -10 83.79 7.50 -5 -7 10 97.09 7.80 -5 7 -10 69.19 5.10 5 7 10 84.19 7.30 5 -7 -10 79.89 7.40 5 7 10 75.89 7.20 -6 7 10 66.29 6.20 -6 7 10 55.69 6.40 6 -7 10 42.10 5.90 -6 -7 -10 57.09 6.50 -6 7 10 64.99 6.80 6 -7 10 60.29 6.30 6 7 -10 41.70 5.80 6 7 -10 48.20 5.60 6 -7 -10 57.09 6.40 -6 -7 10 49.70 5.90 6 7 10 49.40 5.90 -6 7 -10 55.79 6.20 6 7 10 42.20 5.70 -6 7 -10 58.79 6.30 -6 -7 10 51.89 6.10 -6 7 -10 44.70 4.30 -7 7 10 32.90 5.90 -7 -7 -10 33.40 5.40 7 7 -10 46.10 5.90 7 7 -10 39.20 5.70 -7 7 10 36.70 5.50 7 -7 10 40.30 6.10 7 -7 10 37.10 5.90 -7 7 10 43.80 6.20 -7 -7 10 39.00 5.70 7 -7 -10 31.40 5.40 -7 -7 10 32.90 5.50 -7 7 -10 30.80 4.00 -7 7 -10 38.30 5.70 -7 7 -10 32.10 5.50 7 7 10 27.20 5.10 8 7 -10 1.70 3.80 -8 -7 -10 7.90 4.00 8 -7 10 -1.50 4.80 -8 7 10 2.30 4.50 8 7 -10 6.70 4.70 -8 7 10 -0.70 4.20 8 -7 10 7.20 4.10 -8 7 10 8.30 4.90 -8 7 -10 2.30 3.40 -8 -7 10 2.20 3.90 -8 -7 10 4.90 4.40 -8 7 -10 2.20 3.70 8 -7 -10 5.90 4.50 -8 7 -10 7.50 4.10 8 7 10 6.60 4.00 -9 -7 -10 10.60 4.70 9 -7 10 4.00 7.00 9 7 -10 9.10 4.70 9 -7 10 1.20 4.70 -9 7 10 4.70 5.10 -9 7 -10 9.90 4.70 9 -7 -10 5.00 4.50 -9 7 -10 5.00 4.10 9 7 10 4.20 4.90 -9 -7 10 6.00 5.10 10 -7 10 0.10 5.00 -10 7 10 3.70 6.50 10 7 -10 -7.70 4.10 -10 -7 -10 -7.30 3.90 -10 -7 10 4.00 5.70 10 -7 -10 5.30 5.40 -10 7 -10 -4.80 4.50 -10 7 -10 -0.90 4.80 10 7 10 4.30 5.10 -11 7 10 17.70 8.90 11 -7 10 11.00 6.80 11 7 -10 15.60 7.40 -11 -7 -10 20.20 6.90 11 7 10 17.10 6.80 -11 7 -10 15.90 6.60 -11 -7 10 19.90 7.50 -11 7 -10 8.80 6.40 0 -8 -10 29.20 4.00 0 8 -10 24.00 1.70 0 8 -10 22.50 1.60 0 8 10 24.10 3.40 0 8 10 30.30 4.20 0 -8 10 22.70 3.70 0 -8 10 21.20 3.30 0 -8 -10 24.20 3.60 0 -8 10 26.20 3.90 0 8 -10 17.00 3.10 1 -8 10 2.30 2.50 1 -8 10 0.40 2.00 -1 8 10 -0.40 2.20 -1 8 10 5.00 3.00 1 8 -10 -0.50 2.10 1 -8 10 3.70 2.40 1 8 -10 3.00 1.20 -1 -8 -10 0.00 2.30 1 -8 10 2.50 2.30 -1 -8 -10 -1.60 2.00 1 -8 -10 2.50 2.20 1 8 10 2.10 2.90 1 -8 -10 1.30 2.50 -1 -8 10 1.40 2.00 -1 -8 10 -0.40 2.40 1 8 10 0.10 2.20 -1 -8 10 -0.90 2.30 2 -8 10 57.99 4.90 2 -8 10 54.69 5.30 -2 -8 -10 59.19 5.40 -2 -8 -10 56.49 5.50 2 8 -10 50.49 3.90 2 8 -10 57.59 5.20 -2 8 10 43.20 4.80 -2 8 10 51.69 5.70 2 -8 10 51.49 5.40 2 8 10 43.70 4.70 2 -8 -10 53.79 5.40 -2 8 -10 53.59 2.70 -2 -8 10 59.19 5.60 -2 8 -10 47.40 4.70 -2 8 -10 50.89 2.70 2 8 10 55.99 5.80 -2 -8 10 59.99 5.80 2 -8 -10 37.90 4.90 -3 -8 -10 77.69 6.50 3 8 -10 63.79 5.10 3 -8 10 76.99 6.80 3 -8 10 72.99 6.60 3 8 -10 78.19 6.50 -3 -8 -10 63.09 6.30 -3 8 10 75.89 6.80 3 -8 10 81.09 6.20 -3 -8 10 71.09 6.50 3 -8 -10 64.99 6.60 -3 8 -10 67.49 4.00 -3 8 -10 78.79 5.80 3 8 10 72.09 6.70 3 8 10 85.39 6.60 -3 -8 10 76.09 6.70 -4 -8 -10 36.70 4.40 -4 -8 -10 27.30 4.40 4 8 -10 27.10 4.40 -4 8 10 35.60 4.40 -4 8 10 28.20 4.60 -4 8 10 29.90 4.70 4 8 -10 25.40 3.70 -4 8 10 38.50 5.00 4 -8 10 28.70 4.80 4 -8 10 39.60 4.40 4 8 10 34.40 4.50 4 8 10 34.50 4.80 -4 8 -10 36.40 4.70 -4 -8 10 18.80 4.10 -4 8 -10 27.40 2.60 -4 8 -10 26.90 4.50 4 8 10 33.80 5.00 4 -8 -10 29.80 4.40 -4 -8 10 32.40 4.80 -5 8 10 273.27 14.90 5 -8 10 230.68 15.30 -5 -8 -10 261.57 15.10 -5 8 10 249.68 15.20 5 8 -10 248.68 14.90 -5 8 10 282.67 14.70 -5 8 10 261.27 15.30 5 -8 10 259.77 14.90 5 8 -10 267.77 14.50 -5 -8 10 230.48 14.50 -5 8 -10 234.98 14.50 -5 8 -10 246.08 12.80 5 8 10 257.47 15.00 5 -8 -10 243.88 14.80 -5 8 -10 244.08 14.50 -5 -8 10 241.68 14.70 5 8 10 272.37 15.10 5 8 10 254.37 14.30 6 8 -10 1.90 3.20 -6 8 10 7.90 3.50 6 -8 10 8.20 4.20 -6 8 10 11.00 4.10 -6 -8 -10 12.70 4.00 6 8 -10 6.70 3.60 -6 8 10 3.70 3.60 -6 8 -10 3.50 2.20 -6 -8 10 0.00 3.00 -6 8 -10 6.00 3.60 6 8 10 6.80 3.40 6 8 10 4.30 4.30 -6 8 -10 2.70 3.30 6 -8 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4 -25 13.40 4.50 4 -4 -25 13.40 4.60 -4 -4 25 21.00 4.10 4 4 25 16.80 4.10 -5 -4 -25 4.20 4.50 5 4 -25 8.60 3.70 -5 4 25 11.90 4.10 5 -4 25 5.00 4.50 5 4 -25 9.50 4.20 -5 -4 -25 8.10 4.40 5 4 25 11.50 4.00 -5 4 -25 4.00 2.40 -5 -4 25 10.30 4.00 -5 4 -25 5.90 3.50 5 -4 -25 10.60 3.90 -6 4 25 4.00 3.80 6 4 -25 4.40 4.40 6 4 -25 6.10 4.60 6 -4 25 -0.10 4.30 -6 -4 -25 -0.20 4.70 -6 -4 -25 5.30 5.30 6 4 25 -4.30 3.60 -6 -4 25 5.60 4.00 -6 4 -25 6.90 4.30 -6 4 -25 -0.20 2.90 6 -4 -25 7.50 4.10 7 -4 25 1.70 5.00 7 4 -25 10.00 5.30 -7 4 25 6.00 4.10 -7 -4 -25 3.30 5.20 7 4 -25 -4.40 4.20 -7 -4 25 -4.60 3.70 -7 4 -25 3.50 5.40 -7 4 -25 -4.80 3.40 7 4 25 -2.50 3.80 8 4 -25 -2.70 5.50 8 -4 25 -3.40 5.20 8 4 -25 10.30 5.90 -8 -4 -25 -9.50 5.30 -8 -4 25 11.30 5.00 8 4 25 9.50 5.00 -8 4 -25 8.70 5.00 -8 4 -25 7.10 5.20 9 -4 25 26.40 7.60 -9 -4 -25 11.20 7.40 9 4 -25 10.10 7.00 -9 4 -25 19.10 8.10 -9 4 -25 37.20 6.90 9 4 25 17.60 6.60 -9 -4 25 8.80 6.50 0 5 25 0.20 3.60 0 -5 25 -2.60 3.10 0 5 25 4.70 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5 25 0.40 3.80 -4 -5 25 10.30 4.30 -4 5 -25 8.70 2.30 4 5 25 9.00 3.70 5 5 -25 5.50 3.90 -5 5 25 4.70 3.80 5 -5 25 0.20 4.10 5 5 -25 -0.50 7.00 -5 -5 -25 -2.00 4.60 5 5 25 5.60 3.70 -5 -5 25 -2.00 3.40 -5 5 -25 0.80 2.20 5 -5 -25 -0.40 3.60 -5 5 -25 -0.40 3.80 -6 5 25 15.00 4.80 6 5 -25 13.50 4.60 -6 -5 -25 15.90 5.80 6 -5 25 9.80 5.20 6 5 -25 8.60 4.40 6 5 25 18.90 4.90 -6 5 -25 18.40 3.30 -6 -5 25 22.60 5.30 -6 5 -25 11.80 5.00 6 -5 -25 21.70 5.30 7 5 -25 35.10 6.40 7 -5 25 29.30 6.60 -7 5 25 32.60 6.10 -7 -5 -25 31.10 7.10 7 5 -25 23.30 6.50 7 -5 -25 35.30 7.70 7 5 25 23.00 5.80 -7 5 -25 29.00 4.90 -7 -5 25 28.70 6.10 -7 5 -25 42.30 7.30 8 -5 25 4.20 6.00 8 5 -25 -0.70 5.30 -8 -5 -25 4.20 5.80 8 5 -25 -4.00 5.10 8 5 25 -1.10 5.30 -8 -5 25 -7.30 4.40 -8 5 -25 -6.90 5.80 -8 5 -25 -0.20 4.40 9 5 -25 -3.20 6.50 9 -5 25 5.00 6.50 -9 -5 25 1.90 5.60 -9 5 -25 -2.50 5.60 -9 5 -25 4.60 7.40 9 5 25 0.30 5.70 0 -6 -25 4.10 2.80 0 6 -25 2.70 3.60 0 6 -25 0.70 1.40 0 -6 25 -1.50 3.10 0 -6 25 6.60 3.80 0 6 25 1.10 3.00 -1 6 25 6.10 4.20 1 -6 25 5.00 3.60 1 6 -25 2.00 1.70 -1 -6 -25 8.10 4.40 1 -6 25 3.10 3.70 1 -6 -25 0.30 3.40 -1 6 -25 1.70 3.10 -1 -6 25 8.70 4.00 1 6 25 7.90 4.30 -1 6 -25 5.20 1.60 2 -6 25 -0.90 3.30 -2 -6 -25 2.50 4.10 2 6 -25 1.10 3.40 -2 6 25 4.30 4.40 2 -6 25 6.90 3.90 2 6 -25 3.50 1.90 -2 6 -25 4.30 3.40 2 -6 -25 -3.60 3.30 -2 6 -25 2.70 1.60 2 6 25 6.10 4.10 -2 -6 25 3.20 3.70 3 6 -25 56.59 6.60 -3 6 25 36.10 5.80 -3 -6 -25 44.80 6.70 3 -6 25 47.50 6.60 3 6 -25 46.40 4.40 -3 6 -25 44.00 3.80 3 6 25 43.40 6.40 -3 -6 25 56.89 6.60 3 -6 -25 57.69 6.80 -3 6 -25 35.10 5.60 3 6 25 45.30 6.00 4 6 -25 16.20 3.80 4 6 -25 21.40 5.20 4 -6 25 31.30 5.80 -4 -6 -25 26.30 6.20 -4 6 25 26.70 4.90 4 6 25 15.90 4.60 4 -6 -25 35.70 5.80 -4 6 -25 34.10 3.30 -4 -6 25 26.90 5.10 -4 6 -25 17.80 5.10 4 6 25 21.40 5.60 5 6 -25 -4.10 3.20 -5 6 25 -1.30 3.70 5 6 -25 -1.70 3.30 -5 -6 -25 6.40 4.90 5 -6 25 8.30 4.90 -5 6 -25 -3.40 3.70 -5 -6 25 -4.30 3.30 5 6 25 6.40 4.20 5 -6 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5.30 4.00 2 7 -25 5.80 3.60 -2 7 25 3.60 3.90 2 -7 25 4.00 4.20 2 7 -25 -2.00 1.80 -2 -7 -25 4.80 4.60 -2 -7 25 0.30 3.90 2 -7 -25 2.40 3.80 -2 7 -25 3.60 1.50 -2 7 -25 -1.20 2.90 2 7 25 8.90 4.50 -3 -7 -25 30.20 6.00 -3 7 25 19.40 4.90 3 7 -25 31.10 3.70 3 7 -25 28.50 5.20 3 -7 25 25.30 5.40 -3 -7 25 36.30 6.10 -3 7 -25 31.30 2.90 3 7 25 32.50 6.20 -3 7 -25 21.80 4.90 3 -7 -25 25.90 4.90 -4 -7 -25 2.40 4.60 4 -7 25 2.70 4.40 -4 7 25 4.50 4.10 4 7 -25 2.60 2.90 4 7 -25 -1.50 3.40 -4 -7 25 0.10 4.30 -4 7 -25 1.20 1.80 -4 7 -25 4.40 4.10 4 7 25 0.90 4.40 4 -7 -25 2.80 4.20 5 7 -25 23.20 4.60 5 -7 25 31.40 6.30 -5 7 25 42.20 6.20 -5 -7 -25 31.80 6.70 5 7 -25 22.90 5.30 5 -7 -25 34.80 6.40 5 7 25 34.50 6.90 -5 -7 25 30.00 5.80 -5 7 -25 37.10 6.40 -5 7 -25 28.60 3.50 6 7 -25 14.20 4.40 6 -7 25 9.40 5.50 -6 -7 -25 -1.50 5.20 6 7 -25 4.80 4.20 -6 7 25 6.40 5.00 -6 -7 25 4.50 4.70 6 -7 -25 11.10 5.70 -6 7 -25 6.00 2.70 -6 7 -25 15.20 5.40 -7 -7 -25 1.20 5.80 7 7 -25 13.50 5.70 7 -7 25 9.30 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2.80 2 2 28 5.20 3.60 2 2 28 5.40 3.70 -3 2 28 0.90 3.10 -3 -2 -28 3.70 4.00 3 -2 28 3.30 3.20 3 2 -28 9.00 4.20 -3 -2 -28 -4.40 3.10 3 2 -28 2.20 3.10 -3 2 -28 -0.50 2.80 3 2 28 7.70 3.80 -3 -2 28 3.20 3.90 3 -2 -28 1.10 3.20 3 2 28 8.30 3.80 3 -2 -28 2.00 3.40 -3 2 -28 1.80 3.70 3 -2 -28 1.70 3.40 4 -2 28 51.19 6.50 4 2 -28 36.40 6.00 -4 2 28 32.70 5.60 4 2 -28 39.40 5.40 -4 -2 -28 36.20 5.70 -4 -2 -28 43.00 6.70 4 -2 -28 37.00 5.60 4 2 28 34.80 5.50 -4 2 -28 38.30 4.90 -4 -2 28 37.00 5.70 -4 2 -28 35.30 5.90 4 -2 -28 43.50 5.80 4 -2 -28 57.19 6.40 5 2 -28 -4.70 4.00 5 2 -28 -0.70 3.80 -5 -2 -28 1.60 4.00 -5 2 28 3.70 3.70 -5 -2 -28 -3.30 4.60 5 -2 28 -0.10 3.40 -5 2 -28 0.50 3.00 -5 2 -28 2.30 3.40 -5 -2 28 7.00 4.00 5 2 28 -1.50 3.40 5 -2 -28 4.80 4.10 -6 -2 -28 18.10 5.50 -6 -2 -28 12.40 5.80 6 2 -28 20.30 5.40 -6 2 28 6.80 4.50 6 -2 28 23.00 5.90 6 2 -28 20.20 5.80 -6 2 -28 22.50 4.80 -6 -2 28 14.20 4.90 6 2 28 18.60 5.40 -6 2 -28 13.30 5.90 6 -2 -28 19.80 5.30 -7 -2 -28 13.50 6.40 7 -2 28 15.90 6.00 7 2 -28 15.20 6.00 -7 -2 -28 9.80 6.10 7 2 -28 4.80 5.40 -7 2 28 10.80 4.80 7 -2 -28 1.70 5.60 -7 -2 28 6.90 4.60 -7 2 -28 8.10 5.60 7 2 28 3.60 4.60 -7 2 -28 1.20 4.80 8 -2 28 2.40 5.90 -8 -2 -28 0.90 6.20 8 2 -28 2.70 6.00 -8 -2 -28 -0.60 6.20 -8 2 28 -2.30 5.30 -8 -2 28 7.50 5.20 -8 2 -28 6.30 5.30 8 2 28 -1.90 4.90 8 -2 -28 1.20 6.60 -8 2 -28 1.90 6.30 9 -2 28 6.40 7.10 9 2 -28 8.80 7.20 -9 -2 -28 13.90 7.50 -9 2 -28 6.40 6.70 -9 -2 28 12.90 6.90 -9 2 -28 0.00 7.00 9 2 28 8.00 5.90 0 -3 -28 3.70 3.80 0 3 -28 7.00 2.50 0 -3 28 6.00 3.80 0 3 28 2.80 3.80 0 -3 28 1.20 3.10 0 -3 -28 12.10 3.80 0 3 -28 8.20 3.50 0 3 28 2.50 3.00 -1 3 28 -1.30 3.60 -1 3 28 1.80 2.60 1 3 -28 1.40 2.30 -1 -3 -28 4.20 4.00 -1 -3 -28 2.70 3.20 1 3 -28 1.00 3.40 1 -3 28 2.90 4.00 1 -3 28 7.30 3.50 1 -3 -28 0.80 3.40 1 3 28 0.60 2.90 1 -3 -28 0.30 3.20 -1 -3 28 9.70 3.60 1 3 28 8.80 4.20 -1 -3 28 0.80 3.60 -1 3 -28 4.10 2.20 -1 3 -28 4.70 3.40 2 3 -28 5.80 3.80 2 3 -28 9.80 3.10 -2 -3 -28 7.60 4.10 -2 3 28 11.30 4.40 -2 -3 -28 7.70 3.80 2 -3 28 14.00 4.20 2 -3 28 12.20 3.80 2 -3 -28 4.00 3.30 2 3 28 9.00 4.10 -2 3 -28 1.50 3.50 2 -3 -28 8.60 3.70 2 3 28 9.80 3.60 -2 -3 28 9.60 4.10 2 -3 -28 4.10 3.40 -2 3 -28 19.20 2.90 3 3 -28 21.40 4.00 -3 3 28 8.60 4.00 -3 -3 -28 10.00 5.00 3 -3 28 11.60 4.60 -3 -3 -28 15.70 4.50 3 3 -28 26.30 5.30 -3 3 -28 13.40 4.30 3 -3 -28 15.70 4.20 3 3 28 7.50 3.90 3 -3 -28 18.70 4.50 -3 3 -28 21.80 3.20 3 3 28 13.80 4.10 -3 -3 28 14.80 4.60 3 -3 -28 11.70 4.50 4 3 -28 14.20 5.10 4 3 -28 4.80 3.50 -4 -3 -28 0.50 4.80 -4 3 28 9.30 4.00 4 -3 28 6.20 4.50 -4 -3 -28 16.60 4.30 4 3 28 8.80 4.00 -4 3 -28 11.20 3.70 4 -3 -28 4.50 4.10 -4 -3 28 14.20 4.30 -4 3 -28 7.20 3.10 4 -3 -28 14.00 4.10 -5 3 28 17.60 4.60 5 3 -28 10.70 4.30 -5 -3 -28 14.80 5.80 5 -3 28 9.60 4.90 -5 -3 -28 18.40 5.00 5 3 -28 7.70 4.60 -5 3 -28 22.70 4.00 -5 -3 28 20.50 5.00 5 -3 -28 16.60 5.30 5 -3 -28 14.60 5.20 -5 3 -28 4.20 4.30 5 3 28 19.80 4.80 6 3 -28 35.30 6.80 6 3 -28 25.30 5.50 -6 -3 -28 35.30 6.10 -6 -3 -28 25.60 6.90 -6 3 28 30.70 5.80 6 -3 28 31.80 6.70 -6 -3 28 23.40 5.70 6 -3 -28 22.00 6.60 -6 3 -28 24.50 4.80 6 3 28 31.50 5.90 -6 3 -28 23.00 5.30 -7 -3 -28 18.40 7.00 7 -3 28 18.20 6.20 7 3 -28 10.60 5.50 -7 3 28 12.20 5.00 7 3 -28 2.90 5.20 -7 -3 -28 7.50 6.40 7 3 28 11.10 5.10 -7 3 -28 10.20 4.50 -7 -3 28 3.70 5.40 -7 3 -28 7.70 6.20 8 3 -28 -0.10 6.10 8 -3 28 -1.50 5.80 -8 3 28 -0.60 5.30 -8 -3 -28 5.80 6.80 -8 3 -28 4.40 6.90 -8 3 -28 1.20 5.30 -8 -3 28 1.80 4.90 8 3 28 -2.20 4.90 -9 -3 -28 -2.80 7.10 9 -3 28 -1.80 7.10 9 3 -28 4.90 7.10 -9 3 -28 8.60 8.20 -9 3 -28 6.00 6.20 -9 -3 28 -1.20 5.50 9 3 28 4.40 6.20 0 -4 28 35.70 5.90 0 -4 -28 48.20 6.00 0 -4 -28 43.30 5.60 0 4 -28 49.30 5.80 0 -4 28 43.50 5.90 0 4 28 46.90 6.30 0 4 -28 33.80 3.90 0 4 28 47.60 5.30 -1 -4 -28 17.30 4.60 -1 -4 -28 7.50 3.70 1 -4 28 7.10 4.10 -1 4 28 4.90 4.20 1 4 -28 7.80 5.00 -1 4 28 9.60 3.70 1 -4 28 6.30 3.70 1 4 -28 12.20 2.70 -1 -4 28 9.20 4.00 -1 -4 28 7.00 4.00 -1 4 -28 7.10 2.30 1 -4 -28 14.00 4.40 1 4 28 9.10 3.40 -1 4 -28 8.00 3.70 1 4 28 11.70 4.40 1 -4 -28 11.70 4.30 -2 -4 -28 2.00 3.60 2 -4 28 0.80 3.70 -2 -4 -28 2.50 4.00 2 4 -28 -1.50 2.30 -2 4 28 4.80 3.40 2 4 -28 2.90 3.80 2 -4 28 6.10 4.10 2 -4 -28 4.50 3.60 2 -4 -28 1.20 3.80 2 -4 -28 13.80 4.50 2 4 28 3.80 3.70 -2 4 -28 6.00 3.50 2 4 28 4.70 4.10 -2 -4 28 -4.10 3.70 -2 4 -28 1.40 2.10 3 4 -28 11.00 4.50 -3 -4 -28 8.10 5.00 -3 4 28 10.40 3.60 3 -4 28 6.70 4.40 -3 -4 -28 13.90 4.30 3 4 -28 6.70 3.10 -3 -4 28 -1.30 3.80 3 -4 -28 7.40 5.10 3 4 28 11.50 3.80 3 -4 -28 8.80 4.20 3 4 28 6.60 4.20 -3 4 -28 12.30 4.30 -3 4 -28 8.00 2.50 4 -4 28 8.40 4.80 4 4 -28 14.70 3.90 4 4 -28 24.90 5.00 -4 4 28 18.80 4.80 -4 -4 -28 19.60 4.90 -4 -4 -28 23.90 6.20 -4 4 -28 21.40 5.00 4 4 28 12.40 4.10 -4 -4 28 15.90 4.80 4 -4 -28 24.80 5.00 -4 4 -28 11.70 3.00 4 4 28 21.60 5.70 -5 -4 -28 12.00 5.30 -5 -4 -28 6.50 5.40 5 -4 28 -0.50 4.60 -5 4 28 8.50 4.30 5 4 -28 8.50 4.20 5 4 -28 10.60 4.90 5 -4 -28 7.40 4.20 5 4 28 12.70 4.70 -5 4 -28 3.90 2.80 -5 4 -28 6.60 4.60 -5 -4 28 4.80 4.30 -6 4 28 6.80 4.30 6 4 -28 2.70 5.00 6 -4 28 -7.50 4.60 6 4 -28 -3.80 4.30 -6 -4 -28 4.30 6.10 -6 4 -28 6.80 5.00 6 -4 -28 -4.40 6.30 -6 -4 28 2.50 4.10 6 4 28 0.90 4.20 -6 4 -28 -0.80 3.50 7 -4 28 4.00 5.70 7 4 -28 10.60 5.30 -7 4 28 6.80 4.60 7 4 -28 1.80 5.50 -7 -4 -28 3.00 6.20 -7 4 -28 4.80 4.30 7 4 28 -1.20 5.20 -7 4 -28 -2.10 4.70 -7 -4 28 10.90 5.30 8 4 -28 2.80 6.70 -8 -4 -28 4.20 6.80 8 4 -28 6.20 6.60 8 -4 28 3.20 6.40 -8 4 28 8.90 7.00 8 4 28 -0.10 4.70 -8 4 -28 2.80 5.00 -8 4 -28 10.50 7.20 -8 -4 28 13.60 5.50 0 5 -28 7.00 2.20 0 -5 28 14.60 4.60 0 -5 -28 11.90 4.50 0 5 -28 20.00 4.30 0 5 28 15.40 4.80 0 -5 28 19.30 5.10 -1 -5 -28 10.20 4.60 1 -5 28 8.20 4.10 -1 -5 -28 6.80 3.50 1 -5 28 1.20 3.60 -1 5 28 5.30 4.20 1 5 -28 7.40 2.30 1 5 28 11.30 4.60 1 5 28 4.50 4.10 -1 -5 28 4.00 4.40 1 -5 -28 1.40 4.00 -1 5 -28 2.20 1.90 -1 5 -28 9.40 3.80 2 5 -28 22.30 3.30 -2 -5 -28 21.20 4.80 2 5 -28 18.70 4.40 2 -5 28 21.10 5.10 -2 -5 -28 22.80 6.40 2 -5 28 15.90 4.90 -2 5 28 18.20 4.70 2 -5 -28 22.90 5.00 2 5 28 10.40 4.00 -2 -5 28 10.70 4.60 -2 5 -28 20.50 2.90 2 5 28 18.00 4.80 -2 5 -28 25.40 4.90 -3 5 28 35.50 5.80 -3 -5 -28 31.50 6.60 3 5 -28 40.90 6.00 3 -5 28 24.90 5.60 3 5 -28 36.60 4.60 3 5 28 43.40 5.90 3 -5 -28 27.30 5.60 -3 5 -28 34.50 5.80 -3 -5 28 32.20 5.90 -3 5 -28 34.50 3.70 3 5 28 31.30 5.60 4 5 -28 15.50 3.90 -4 -5 -28 19.50 6.20 4 5 -28 16.50 4.90 4 -5 28 19.40 5.50 -4 5 28 15.00 4.60 -4 5 -28 19.40 5.30 -4 5 -28 22.00 3.30 4 5 28 17.60 4.40 -4 -5 28 14.20 4.50 4 -5 -28 27.70 5.90 4 5 28 12.40 5.00 5 -5 28 1.10 5.00 5 5 -28 4.10 4.00 5 5 -28 9.30 4.30 -5 -5 -28 16.70 6.20 -5 5 28 -0.20 3.90 -5 5 -28 9.00 2.80 -5 5 -28 1.20 4.40 5 5 28 9.00 4.70 -5 -5 28 2.50 4.30 5 -5 -28 12.20 4.70 6 -5 28 8.10 5.70 -6 5 28 9.40 4.70 -6 -5 -28 1.10 5.80 6 5 -28 -4.10 4.80 6 5 -28 1.90 4.60 -6 5 -28 8.10 5.20 6 5 28 5.30 4.40 -6 -5 28 -1.20 4.40 6 -5 -28 5.20 4.90 -6 5 -28 3.10 2.90 7 -5 28 3.20 5.80 7 5 -28 13.00 6.40 7 5 -28 9.20 5.90 -7 -5 -28 11.20 6.60 -7 5 28 10.90 5.20 7 5 28 4.90 5.50 -7 5 -28 15.20 6.00 -7 -5 28 10.80 5.40 -7 5 -28 8.60 4.50 8 -5 28 8.60 6.70 8 5 -28 -1.90 6.40 8 5 -28 8.60 6.10 -8 -5 -28 6.90 7.40 8 5 28 2.90 5.40 -8 -5 28 11.70 5.90 -8 5 -28 5.60 5.00 -8 5 -28 6.90 7.10 0 -6 28 29.80 5.50 0 -6 28 26.20 5.40 0 -6 -28 34.80 5.50 0 6 -28 30.90 3.30 0 6 28 29.40 5.90 -1 -6 -28 18.10 5.40 -1 6 28 17.20 5.10 1 6 -28 25.20 3.20 1 6 -28 27.70 5.10 1 -6 28 35.30 5.80 1 -6 28 20.90 5.00 1 -6 -28 37.20 6.10 -1 6 -28 32.60 4.90 -1 6 -28 28.60 3.10 1 6 28 18.80 5.20 -1 -6 28 22.00 5.10 2 -6 28 12.60 5.00 2 6 -28 2.70 3.70 -2 -6 -28 0.10 4.50 2 6 -28 9.70 2.50 -2 6 28 11.50 4.40 -2 6 -28 4.20 3.70 2 6 28 6.60 4.70 -2 6 -28 6.30 2.10 2 -6 -28 16.30 4.10 -2 -6 28 4.20 4.50 3 6 -28 15.50 3.50 3 6 -28 15.10 4.50 -3 -6 -28 20.40 6.20 3 -6 28 17.60 5.20 -3 6 28 15.80 4.50 3 -6 -28 15.80 5.10 -3 -6 28 18.20 5.40 -3 6 -28 18.40 2.70 -3 6 -28 23.40 5.20 3 6 28 8.70 4.90 4 6 -28 10.30 4.60 4 6 -28 12.00 3.70 4 -6 28 13.30 5.40 -4 -6 -28 11.40 5.70 -4 6 28 11.90 4.80 -4 6 -28 3.10 4.30 -4 6 -28 8.90 2.60 4 6 28 19.00 5.30 -4 -6 28 10.00 5.40 4 -6 -28 8.10 4.70 5 6 -28 -4.50 3.50 5 6 -28 0.00 3.70 -5 -6 -28 7.50 5.90 5 -6 28 0.50 5.60 -5 6 28 0.60 3.90 -5 6 -28 2.20 4.10 -5 6 -28 -1.10 2.40 5 6 28 -0.70 4.50 5 -6 -28 6.80 5.40 -5 -6 28 -1.20 4.10 6 6 -28 12.30 5.30 6 6 -28 20.90 5.40 6 -6 28 6.80 5.90 -6 6 28 -2.20 5.00 -6 -6 -28 11.00 6.70 -6 -6 28 2.20 4.60 -6 6 -28 13.30 5.60 6 -6 -28 12.20 6.10 6 6 28 8.90 5.70 -6 6 -28 10.10 3.40 -7 -6 -28 0.10 6.30 7 -6 28 3.60 6.10 7 6 -28 6.90 5.20 -7 6 28 1.70 5.00 7 6 -28 -2.80 4.80 7 -6 -28 15.10 7.70 -7 6 -28 -4.60 4.90 7 6 28 4.80 5.20 -7 6 -28 -4.90 3.10 -7 -6 28 8.40 5.30 8 6 -28 -0.90 5.70 8 6 -28 0.60 6.70 8 -6 28 7.80 6.80 -8 -6 -28 -0.90 7.70 -8 6 -28 -0.20 4.90 8 6 28 3.50 5.70 -8 6 -28 -7.20 6.00 -8 -6 28 2.10 6.20 0 7 -28 10.70 2.20 0 -7 28 4.60 4.30 0 -7 -28 13.80 4.90 0 -7 28 11.70 4.60 0 7 28 0.30 4.50 1 -7 28 1.30 4.10 1 -7 28 -3.00 3.50 -1 7 28 12.30 5.10 -1 -7 -28 1.70 4.70 1 7 -28 0.10 2.70 1 7 -28 0.80 1.80 -1 7 -28 1.30 1.70 1 -7 -28 -0.50 3.00 -1 7 -28 -0.10 4.00 -1 -7 28 7.60 4.70 1 7 28 -5.40 4.30 -2 -7 -28 19.60 6.10 2 7 -28 32.00 3.70 -2 7 28 23.80 5.30 2 7 -28 25.30 5.40 2 -7 28 31.50 6.10 -2 -7 28 39.30 6.30 -2 7 -28 31.80 3.20 2 7 28 30.60 6.30 -2 7 -28 20.00 5.00 2 -7 -28 27.90 5.90 -3 7 28 10.30 4.40 3 7 -28 12.80 4.30 -3 -7 -28 2.30 5.00 3 -7 28 6.70 4.80 3 7 -28 11.40 2.90 -3 7 -28 4.80 4.30 3 7 28 7.70 5.20 -3 -7 28 8.80 5.30 3 -7 -28 14.80 5.30 -3 7 -28 5.70 2.20 4 -7 28 16.90 5.60 4 7 -28 13.20 4.90 4 7 -28 11.60 3.80 -4 7 28 10.80 4.70 -4 -7 -28 15.90 6.30 4 -7 -28 15.10 5.30 -4 7 -28 12.00 2.60 -4 7 -28 9.90 5.00 4 7 28 15.20 6.30 -4 -7 28 11.10 5.90 5 -7 28 5.10 5.40 -5 7 28 8.70 4.70 -5 -7 -28 -5.90 5.40 5 7 -28 6.80 4.30 5 7 -28 9.90 4.60 -5 7 -28 7.30 5.00 -5 7 -28 3.70 2.50 5 -7 -28 5.40 5.20 -5 -7 28 6.30 4.70 6 7 -28 8.80 5.00 -6 -7 -28 -0.40 6.00 -6 7 28 -2.70 4.40 6 7 -28 2.00 4.70 6 -7 28 5.50 5.70 -6 7 -28 -6.50 4.60 6 -7 -28 -3.20 5.00 -6 7 -28 7.20 3.20 -6 -7 28 2.50 4.70 7 7 -28 12.90 5.90 -7 7 28 20.70 6.70 -7 -7 -28 11.50 7.50 7 -7 28 17.90 7.20 7 7 -28 18.40 6.10 7 -7 -28 14.90 6.70 -7 -7 28 21.10 6.60 -7 7 -28 7.00 6.00 -7 7 -28 12.80 4.10 0 8 -28 8.90 2.10 0 -8 -28 12.00 5.40 0 -8 28 9.50 4.80 0 8 28 11.80 5.50 -1 -8 -28 10.20 4.50 -1 8 28 4.40 5.10 1 -8 28 7.60 4.90 1 -8 28 4.10 4.90 1 8 -28 8.30 2.20 1 8 -28 12.70 4.60 1 -8 -28 6.40 4.70 -1 -8 28 6.50 4.80 -1 8 -28 6.70 1.90 1 8 28 3.70 5.10 2 8 -28 5.10 2.30 -2 8 28 10.20 4.70 2 8 -28 9.00 4.30 -2 -8 -28 5.70 5.60 2 -8 28 12.20 4.90 -2 -8 28 -1.60 4.60 2 -8 -28 7.60 4.90 -2 8 -28 7.10 1.90 2 8 28 3.40 4.80 -2 8 -28 4.80 4.50 3 8 -28 5.90 2.60 -3 -8 -28 2.00 5.60 3 8 -28 -4.00 3.50 -3 8 28 7.50 4.60 3 -8 28 4.50 5.20 -3 -8 28 1.70 5.00 3 -8 -28 -1.80 4.30 -3 8 -28 11.60 4.70 -3 8 -28 5.00 2.10 3 8 28 1.80 5.00 -4 8 28 29.20 5.80 4 -8 28 16.10 6.30 4 8 -28 7.90 3.40 -4 -8 -28 15.20 6.30 4 8 -28 8.70 4.80 -4 8 -28 9.30 2.50 4 8 28 5.40 5.60 -4 -8 28 4.40 5.50 -4 8 -28 9.00 5.20 4 -8 -28 7.80 5.30 5 8 -28 14.30 4.80 5 -8 28 14.20 6.10 5 8 -28 11.60 5.10 -5 -8 -28 15.30 6.50 -5 8 28 17.70 5.80 -5 8 -28 18.40 3.50 -5 -8 28 18.10 6.50 -5 8 -28 17.40 5.80 5 -8 -28 28.10 6.60 -6 -8 -28 -7.00 6.60 6 8 -28 5.60 5.10 -6 8 28 7.40 5.80 6 8 -28 2.20 4.50 6 -8 28 -1.70 5.80 6 -8 -28 6.30 5.40 -6 -8 28 0.10 5.10 -6 8 -28 -1.10 5.10 -6 8 -28 2.30 2.90 -7 8 28 9.80 7.60 7 8 -28 -3.90 5.70 -7 -8 -28 0.00 7.50 7 -8 28 0.70 7.40 7 8 -28 -3.30 5.60 -7 8 -28 -2.90 3.40 -7 8 -28 10.50 6.10 -7 -8 28 3.90 5.60 7 -8 -28 -10.40 5.30 0 -9 28 31.50 6.20 0 9 -28 33.60 6.10 0 -9 -28 36.90 7.20 0 9 -28 34.30 3.30 0 9 28 38.30 7.40 1 9 -28 3.60 4.10 -1 9 28 7.00 5.30 1 -9 28 14.00 5.80 1 -9 28 11.00 5.00 1 9 -28 10.40 2.30 -1 -9 -28 5.10 5.90 -1 -9 28 6.20 5.20 -1 9 -28 6.90 1.80 1 -9 -28 9.20 5.70 1 9 28 2.80 5.30 2 -9 28 7.50 5.80 2 9 -28 7.80 4.70 -2 9 28 7.20 4.70 -2 -9 -28 10.40 6.50 2 9 -28 8.80 2.60 -2 9 -28 12.40 2.00 2 -9 -28 4.70 4.90 2 9 28 16.20 5.90 -2 -9 28 10.40 5.30 -3 9 28 4.90 4.70 -3 -9 -28 0.60 5.80 3 9 -28 0.20 4.10 3 9 -28 5.60 2.80 3 -9 28 4.50 5.10 -3 9 -28 10.20 4.90 3 9 28 12.80 5.90 -3 -9 28 5.10 5.30 3 -9 -28 5.90 3.80 -3 9 -28 4.00 1.90 4 -9 28 32.50 6.90 4 9 -28 32.30 4.50 -4 -9 -28 32.80 7.60 -4 9 28 36.70 6.90 4 9 -28 16.80 5.70 -4 9 -28 18.50 3.20 4 9 28 28.60 7.20 -4 -9 28 19.10 6.90 -4 9 -28 23.50 6.20 4 -9 -28 34.10 7.20 5 -9 28 10.70 7.00 -5 9 28 16.20 5.80 5 9 -28 5.70 4.50 -5 -9 -28 9.10 6.60 5 9 -28 10.50 5.20 5 -9 -28 19.00 6.50 -5 -9 28 6.40 5.30 -5 9 -28 16.50 6.40 -5 9 -28 9.90 2.90 -6 -9 -28 11.70 7.00 -6 9 28 -1.80 5.90 6 9 -28 3.50 5.20 6 9 -28 0.70 5.50 6 -9 28 4.50 6.50 -6 -9 28 4.10 5.20 -6 9 -28 1.90 2.70 -6 9 -28 -1.20 5.40 6 -9 -28 -0.90 5.70 0 -10 28 8.20 6.10 0 10 -28 1.00 4.80 0 10 -28 1.10 1.70 0 10 28 8.30 5.90 0 -10 -28 12.50 6.40 1 10 -28 16.70 2.70 1 10 -28 20.30 5.50 -1 -10 -28 14.90 6.50 -1 10 28 10.10 5.00 1 -10 28 15.50 5.60 1 -10 -28 20.80 6.90 -1 -10 28 10.80 5.90 -1 10 -28 19.50 2.20 1 10 28 13.20 6.20 -2 -10 -28 4.10 6.10 2 -10 28 2.30 4.90 2 10 -28 -0.30 2.30 -2 10 28 10.30 4.90 2 10 -28 5.30 5.20 -2 -10 28 7.60 5.80 2 -10 -28 9.20 5.30 -2 10 -28 2.30 1.60 2 10 28 10.00 6.40 3 -10 28 22.90 6.80 3 10 -28 10.20 3.10 -3 10 28 16.80 5.90 3 10 -28 13.00 5.70 -3 -10 -28 20.60 7.40 -3 10 -28 20.80 2.60 -3 10 -28 13.20 8.50 -3 -10 28 28.40 7.20 3 10 28 17.70 6.90 3 -10 -28 14.90 6.20 4 10 -28 6.10 3.30 -4 10 28 -6.10 4.50 -4 -10 -28 6.40 7.60 4 -10 28 3.70 6.10 4 10 -28 5.60 5.10 4 10 28 -3.10 6.60 -4 10 -28 4.10 2.00 4 -10 -28 5.80 5.50 -4 10 -28 -3.30 4.90 -4 -10 28 3.60 6.70 -5 -10 -28 21.10 8.10 -5 10 28 7.90 5.00 5 -10 28 15.60 8.70 5 10 -28 7.10 5.40 5 10 -28 9.20 4.80 -5 -10 28 14.50 7.60 -5 10 -28 15.90 6.30 -5 10 -28 12.40 2.90 5 10 28 9.20 8.60 5 -10 -28 11.50 6.30 6 10 -28 -8.70 5.10 -6 10 28 4.10 6.20 6 10 -28 11.50 6.20 -6 10 -28 4.10 6.10 -6 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3 -29 46.70 5.00 -2 -3 -29 47.20 5.80 2 -3 29 55.29 6.30 -2 -3 -29 45.90 6.80 2 -3 -29 59.69 6.80 -2 3 -29 49.10 4.70 2 -3 -29 43.50 6.00 -2 -3 29 40.00 6.20 -2 3 -29 40.50 6.10 2 3 29 44.30 5.90 2 -3 -29 52.99 6.20 2 3 29 57.79 6.70 3 -3 29 -0.70 3.90 3 3 -29 -3.20 3.90 -3 -3 -29 8.60 5.00 3 3 -29 6.50 3.30 -3 -3 -29 -4.60 3.50 -3 3 29 7.40 3.90 3 3 29 0.20 3.40 3 -3 -29 1.90 3.50 -3 3 -29 3.60 3.70 3 -3 -29 3.30 3.60 3 3 29 -2.60 3.50 -3 -3 29 1.10 4.10 -3 3 -29 -3.00 2.20 3 -3 -29 1.80 3.90 4 3 -29 18.30 5.30 -4 -3 -29 20.00 5.10 -4 3 29 7.40 4.10 -4 -3 -29 19.20 6.10 4 3 -29 16.30 4.00 4 -3 29 18.50 4.70 4 3 29 15.40 4.40 -4 -3 29 21.50 5.20 -4 3 -29 11.90 3.60 4 -3 -29 23.30 5.00 4 -3 -29 15.00 4.70 -4 3 -29 13.00 4.60 -5 3 29 12.40 4.40 5 -3 29 4.10 4.90 5 3 -29 10.70 5.20 -5 -3 -29 6.20 5.60 5 3 -29 12.40 4.30 -5 -3 -29 15.00 4.90 -5 3 -29 15.90 5.10 -5 3 -29 15.70 4.00 -5 -3 29 4.90 4.30 5 -3 -29 15.70 5.10 5 3 29 14.50 4.50 5 -3 -29 6.40 4.60 6 3 -29 27.50 5.80 -6 -3 -29 18.70 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5.50 -8 -2 30 -3.70 5.00 0 -3 -30 112.19 8.80 0 3 -30 110.69 7.30 0 -3 -30 87.59 9.20 0 -3 30 112.99 9.50 0 3 30 110.89 8.30 0 3 -30 114.19 9.60 0 3 30 100.69 9.30 0 -3 30 100.39 9.40 -1 -3 -30 58.29 7.40 1 3 -30 63.59 6.90 -1 3 30 55.09 6.50 -1 3 30 60.09 7.30 -1 -3 -30 62.39 6.50 1 -3 30 78.69 7.80 1 3 -30 57.69 5.60 1 -3 30 62.59 6.90 -1 3 -30 62.39 7.30 -1 -3 30 74.89 7.60 1 3 30 58.19 7.20 1 3 30 65.19 7.10 1 -3 -30 52.49 7.10 -1 3 -30 65.79 5.60 -1 -3 30 59.19 7.00 1 -3 -30 76.99 7.00 2 3 -30 10.40 3.30 2 -3 30 21.30 4.90 2 3 -30 16.70 5.00 -2 3 30 11.90 4.60 -2 -3 -30 14.80 4.40 -2 -3 -30 20.20 5.40 2 -3 30 14.40 4.60 -2 -3 30 16.50 4.20 2 3 30 11.30 3.90 -2 3 -30 11.80 3.00 2 -3 -30 18.50 4.50 2 -3 -30 9.00 4.20 -2 3 -30 16.80 4.40 2 3 30 18.70 4.90 2 -3 -30 20.40 4.60 3 -3 30 23.50 5.70 3 3 -30 34.80 6.20 -3 -3 -30 36.30 6.40 3 3 -30 33.90 4.90 -3 -3 -30 24.40 5.20 -3 3 30 34.50 5.80 -3 3 -30 23.20 5.40 3 -3 -30 33.40 5.60 3 -3 -30 26.70 5.70 3 3 30 26.00 5.20 3 -3 -30 18.30 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4.70 3 6 -30 28.40 4.50 3 6 -30 45.90 6.80 -3 6 30 34.20 6.20 -3 -6 -30 33.70 7.30 3 -6 30 36.10 6.90 3 -6 -30 38.70 6.70 -3 6 -30 44.70 7.00 -3 -6 30 35.10 6.90 -3 6 -30 35.70 4.00 3 6 30 40.10 6.60 4 -6 30 6.20 5.20 -4 6 30 5.30 4.30 4 6 -30 -1.00 4.20 4 6 -30 3.10 3.80 -4 -6 -30 6.60 6.10 -4 -6 30 3.70 4.20 -4 6 -30 2.50 2.60 4 6 30 2.10 5.10 -4 6 -30 1.90 4.60 4 -6 -30 0.90 4.70 5 6 -30 6.30 4.60 5 6 -30 12.20 5.10 -5 6 30 7.20 5.10 -5 -6 -30 10.40 6.90 5 -6 30 16.50 6.20 5 -6 -30 4.60 5.40 -5 -6 30 11.50 5.10 -5 6 -30 11.60 3.20 -5 6 -30 10.20 5.40 6 -6 30 11.80 7.00 6 6 -30 0.70 4.60 -6 -6 -30 -11.50 5.90 -6 6 30 -0.80 4.60 6 6 -30 -3.90 4.60 6 -6 -30 -4.70 5.10 -6 6 -30 1.20 3.00 6 6 30 -0.30 7.50 -6 6 -30 4.40 5.60 -6 -6 30 -3.00 4.30 -7 -6 -30 7.90 7.80 7 -6 30 8.70 6.90 7 6 -30 -4.80 4.70 7 6 -30 6.20 5.80 -7 6 30 7.90 5.50 -7 6 -30 8.90 3.60 -7 -6 30 -0.40 5.10 7 6 30 5.80 6.90 -7 6 -30 1.90 5.80 0 7 30 14.70 5.50 0 -7 30 -0.30 4.70 0 -7 -30 12.50 5.40 0 7 -30 6.70 2.30 0 -7 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1.20 6.20 6 7 -30 0.90 5.40 6 -7 -30 7.10 5.70 -6 -7 30 15.70 5.80 -6 7 -30 -6.70 5.00 -6 7 -30 1.70 2.90 7 7 -30 5.70 5.80 -7 -7 -30 -2.80 7.50 -7 7 30 3.90 5.50 7 7 -30 -0.40 5.90 7 -7 30 8.50 7.00 -7 7 -30 -1.20 4.00 7 -7 -30 3.40 7.90 -7 7 -30 7.60 6.90 -7 -7 30 -0.80 5.90 0 8 30 -3.80 5.00 0 -8 -30 8.90 5.80 0 -8 30 4.70 5.10 0 8 -30 5.30 2.20 1 -8 30 3.10 4.60 -1 -8 -30 2.40 5.40 -1 8 30 4.50 5.30 1 -8 30 1.90 5.10 1 8 -30 7.70 2.40 1 8 -30 0.90 4.10 1 8 30 4.10 5.50 -1 -8 30 1.70 4.70 1 -8 -30 1.20 4.60 -1 8 -30 4.50 1.90 -2 8 30 12.80 5.00 -2 -8 -30 14.80 6.40 2 8 -30 8.50 2.80 2 -8 30 23.00 6.00 2 8 -30 11.10 4.70 -2 -8 30 13.90 5.40 2 -8 -30 17.70 6.00 2 8 30 12.50 6.00 -2 8 -30 6.60 5.80 -2 8 -30 15.40 2.60 3 8 -30 33.00 4.20 -3 -8 -30 34.60 7.90 3 -8 30 42.10 7.50 -3 8 30 22.20 5.90 3 8 -30 23.40 5.90 3 8 30 29.60 7.40 -3 -8 30 48.90 7.80 3 -8 -30 51.49 7.40 -3 8 -30 39.20 3.90 -3 8 -30 38.70 7.10 4 -8 30 36.10 7.50 4 8 -30 48.20 7.50 -4 -8 -30 40.70 8.40 4 8 -30 48.00 5.80 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20.70 7.40 0 -2 41 7.10 6.00 0 2 41 20.10 7.50 0 -2 -41 13.30 6.70 0 2 -41 20.30 6.40 0 -2 -41 9.00 6.60 -1 -2 -41 7.70 7.20 1 2 -41 6.90 6.90 1 2 -41 5.50 5.40 1 -2 41 8.10 6.30 -1 2 41 3.10 6.70 -1 -2 -41 4.40 6.80 1 -2 41 -1.50 7.20 1 -2 -41 -1.60 6.80 1 -2 -41 4.60 6.90 -1 -2 41 4.20 7.00 -1 2 -41 0.10 7.80 1 2 41 4.30 6.40 1 -2 -41 5.20 6.50 -1 2 -41 -4.50 5.30 1 2 41 2.90 6.50 -2 -2 -41 7.20 7.30 2 2 -41 12.90 6.80 2 -2 41 5.30 6.50 -2 -2 -41 9.00 6.60 -2 2 41 17.00 7.80 2 2 -41 11.80 7.40 2 2 41 17.30 7.10 -2 -2 41 10.30 7.50 2 -2 -41 3.70 9.20 2 -2 -41 9.20 8.70 -2 2 -41 1.50 6.70 -2 2 -41 21.40 6.60 -3 -2 -41 -0.80 7.60 -3 -2 -41 12.20 10.10 3 2 -41 4.10 6.70 -3 2 41 0.20 9.10 -3 2 -41 -2.30 6.10 -3 2 -41 6.00 7.50 -3 -2 41 -1.50 7.70 0 3 41 8.30 6.80 0 -3 -41 -8.90 5.70 0 -3 41 2.60 6.10 0 3 -41 0.30 5.30 -1 3 41 10.50 7.20 1 3 -41 3.00 5.90 1 -3 41 19.20 7.40 1 3 -41 13.70 7.40 -1 -3 -41 -4.30 6.50 1 3 41 2.30 7.40 -1 -3 41 8.30 7.00 -1 3 -41 -1.10 5.40 -1 3 -41 9.10 10.20 1 -3 -41 10.30 6.60 2 -3 41 22.90 8.20 2 3 -41 10.30 7.70 -2 -3 -41 23.10 9.20 2 3 -41 15.20 6.60 -2 -3 -41 38.70 14.40 -2 3 41 19.20 8.30 -2 3 -41 21.20 8.70 2 3 41 9.40 7.70 2 -3 -41 32.70 9.00 2 3 41 21.00 8.50 -2 -3 41 36.90 9.00 -2 3 -41 25.50 6.70 0 -4 41 -0.30 6.60 0 -4 -41 -6.30 6.70 0 4 -41 -0.40 5.30 0 4 41 7.10 7.10 1 4 -41 28.40 9.00 1 4 -41 34.50 6.90 -1 4 41 19.10 8.00 1 -4 41 5.80 7.30 -1 -4 -41 27.50 9.00 -1 -4 41 27.20 8.50 -1 4 -41 22.30 6.30 1 4 41 16.40 7.50 1 -4 -41 13.90 7.40 0 0 42 5.50 6.00 0 0 42 13.30 7.70 0 0 -42 7.80 7.50 0 0 -42 18.50 6.80 1 0 42 2.20 6.10 1 0 -42 -2.30 6.10 1 0 -42 13.40 7.50 -1 0 42 1.50 7.40 -1 0 -42 -5.30 6.40 -1 0 -42 -6.50 5.90 1 0 42 1.70 6.90 0 -1 -42 -0.10 6.40 0 -1 42 5.90 7.20 0 1 -42 7.40 6.20 0 1 42 2.50 7.20 0 -1 42 4.10 6.20 0 1 42 5.20 5.80 0 -1 -42 -1.00 6.60 0 1 -42 -5.10 8.40 -1 -1 -42 7.50 7.50 1 1 -42 4.10 7.30 1 -1 42 8.90 7.10 1 1 -42 16.20 6.90 1 -1 42 7.50 8.80 -1 1 42 9.60 8.90 -1 -1 -42 -0.10 6.10 1 -1 -42 16.60 7.70 -1 1 -42 4.80 7.00 -1 -1 42 -5.10 6.90 1 1 42 4.90 6.00 1 1 42 7.50 7.40 -1 1 -42 16.00 6.70 1 -1 -42 4.10 7.20 1 -1 -42 9.60 7.80 0 2 42 -0.80 6.60 0 2 -42 -7.80 5.70 0 -2 -42 0.10 6.60 0 -2 42 2.20 8.20 0 -2 -42 -4.70 6.40 -1 -2 -42 -3.10 7.10 -1 2 42 2.40 7.30 1 2 -42 -0.50 6.00 -1 -2 -42 5.10 7.30 1 2 -42 5.70 8.60 1 -2 42 7.10 7.30 -1 2 -42 -1.50 6.30 1 2 42 -0.60 7.10 1 -2 -42 2.70 7.10 1 -2 -42 8.50 8.50 1 -2 -42 10.70 7.60 -1 2 -42 18.30 9.80 -1 -2 42 10.30 7.60 1 2 42 6.50 7.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 26654 _olex2_submission_special_instructions 'No special instructions were received'