data_global _audit_creation_method 'APEX3 v2018.1-0' _publ_requested_journal ? _publ_contact_author_name ? _publ_contact_author_address ; ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_section_title ; ; _publ_section_abstract ; ; _publ_section_references ; ; _publ_section_comment ; ; data_AD838 _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_sum 'C19 H17 N O2' _chemical_formula_iupac ? _chemical_formula_weight 291.33 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 6.1270(2) _cell_length_b 22.8523(7) _cell_length_c 10.9205(3) _cell_angle_alpha 90 _cell_angle_beta 106.0910(10) _cell_angle_gamma 90 _cell_volume 1469.14(8) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9905 _cell_measurement_theta_min 3.3050 _cell_measurement_theta_max 27.4507 _cell_measurement_temperature 100.(2) _exptl_crystal_description prism _exptl_crystal_colour colourless _exptl_crystal_size_max 0.800 _exptl_crystal_size_mid 0.260 _exptl_crystal_size_min 0.140 _exptl_crystal_density_diffrn 1.317 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 616 _exptl_absorpt_coefficient_mu 0.085 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction ; _exptl_absorpt_correction_T_min 0.89 _exptl_absorpt_correction_T_max 0.99 _exptl_special_details ; ; _diffrn_ambient_temperature 100.(2) _diffrn_source ? _diffrn_source_type 'Ceramic x-ray tube' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'doubly curved silicon crystal Bruker Triumph' _diffrn_measurement_device_type 'D8 QUEST ECO' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean 7.3910 _diffrn_detector 'CPAD' _diffrn_detector_type 'PHOTON II' _diffrn_reflns_number 56871 _diffrn_reflns_av_R_equivalents 0.0432 _diffrn_reflns_av_unetI/netI 0.0153 _diffrn_reflns_theta_min 3.31 _diffrn_reflns_theta_max 27.52 _diffrn_reflns_theta_full 27.52 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 14 _refine_special_details ; ; _reflns_number_total 3353 _reflns_number_gt 3135 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0574 _refine_ls_R_factor_gt 0.0540 _refine_ls_wR_factor_gt 0.1145 _refine_ls_wR_factor_ref 0.1158 _refine_ls_goodness_of_fit_ref 1.261 _refine_ls_restrained_S_all 1.261 _refine_ls_number_reflns 3353 _refine_ls_number_parameters 267 _refine_ls_number_restraints 0 _refine_ls_number_constraints ? _refine_ls_hydrogen_treatment refall _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0148P)^2^+1.6317P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.416 _refine_diff_density_min -0.231 _refine_ls_extinction_method none _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection 'Bruker Instrument Service vV6.2.9' _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 882)' _computing_publication_material ? loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O O1 0.3528(2) 0.31854(6) -0.00905(12) 0.0188(3) Uani d . . . 1 . . O O3 0.0529(2) 0.36260(6) 0.02741(13) 0.0212(3) Uani d . . . 1 . . C C2 0.2524(3) 0.35138(7) 0.06265(17) 0.0155(3) Uani d . . . 1 . . C C4 0.4232(3) 0.37001(7) 0.18736(16) 0.0138(3) Uani d . . . 1 . . C C5 0.3256(3) 0.35748(8) 0.30101(17) 0.0162(3) Uani d . . . 1 . . H H5A 0.174(4) 0.3750(9) 0.282(2) 0.018(5) Uiso d . . . 1 . . H H5B 0.311(3) 0.3151(9) 0.3099(19) 0.013(5) Uiso d . . . 1 . . N N6 0.4652(3) 0.38190(7) 0.41873(14) 0.0174(3) Uani d . . . 1 . . C C7 0.6650(3) 0.35509(7) 0.48705(17) 0.0167(3) Uani d . . . 1 . . C C9 0.9395(3) 0.33919(9) 0.69437(19) 0.0252(4) Uani d . . . 1 . . H H9 0.982(4) 0.3459(10) 0.782(2) 0.021(6) Uiso d . . . 1 . . C C8 0.7394(3) 0.36320(8) 0.62008(18) 0.0221(4) Uani d . . . 1 . . H H8 0.646(4) 0.3862(11) 0.661(2) 0.030(6) Uiso d . . . 1 . . C C10 1.0736(3) 0.30502(9) 0.6390(2) 0.0254(4) Uani d . . . 1 . . H H10 1.218(4) 0.2883(10) 0.691(2) 0.030(6) Uiso d . . . 1 . . C C11 1.0022(3) 0.29559(8) 0.50957(19) 0.0205(4) Uani d . . . 1 . . H H11 1.091(4) 0.2708(9) 0.468(2) 0.019(5) Uiso d . . . 1 . . C C12 0.8020(3) 0.32004(7) 0.42956(17) 0.0166(4) Uani d . . . 1 . . C C13 0.7629(3) 0.30694(7) 0.29358(18) 0.0168(4) Uani d . . . 1 . . H H13 0.866(3) 0.2775(9) 0.2779(19) 0.016(5) Uiso d . . . 1 . . C C14 0.6163(3) 0.32934(7) 0.19098(17) 0.0154(3) Uani d . . . 1 . . C C15 0.5935(3) 0.30988(9) 0.05696(18) 0.0196(4) Uani d . . . 1 . . H H15A 0.677(4) 0.3341(10) 0.013(2) 0.023(6) Uiso d . . . 1 . . H H15B 0.627(4) 0.2685(10) 0.050(2) 0.024(6) Uiso d . . . 1 . . C C16 0.4784(3) 0.43520(7) 0.18104(16) 0.0141(3) Uani d . . . 1 . . C C17 0.3069(3) 0.47596(8) 0.13305(18) 0.0201(4) Uani d . . . 1 . . H H17 0.151(4) 0.4634(10) 0.099(2) 0.028(6) Uiso d . . . 1 . . C C18 0.3585(4) 0.53502(9) 0.13035(19) 0.0232(4) Uani d . . . 1 . . H H18 0.242(4) 0.5623(11) 0.096(2) 0.036(7) Uiso d . . . 1 . . C C19 0.5810(3) 0.55414(8) 0.17660(18) 0.0218(4) Uani d . . . 1 . . H H19 0.615(4) 0.5945(10) 0.175(2) 0.023(6) Uiso d . . . 1 . . C C20 0.7514(3) 0.51402(8) 0.2254(2) 0.0239(4) Uani d . . . 1 . . H H20 0.908(4) 0.5273(11) 0.260(2) 0.034(7) Uiso d . . . 1 . . C C21 0.7002(3) 0.45483(8) 0.22770(19) 0.0202(4) Uani d . . . 1 . . H H21 0.817(4) 0.4269(10) 0.262(2) 0.026(6) Uiso d . . . 1 . . C C22 0.3553(3) 0.42485(9) 0.48026(19) 0.0221(4) Uani d . . . 1 . . H H22A 0.256(4) 0.4488(10) 0.414(2) 0.023(6) Uiso d . . . 1 . . H H22B 0.266(4) 0.4064(10) 0.536(2) 0.030(6) Uiso d . . . 1 . . H H22C 0.470(4) 0.4509(11) 0.534(2) 0.029(6) Uiso d . . . 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0159(6) 0.0222(7) 0.0188(6) -0.0028(5) 0.0056(5) -0.0046(5) O3 0.0134(6) 0.0257(7) 0.0232(7) -0.0010(5) 0.0027(5) -0.0009(5) C2 0.0152(8) 0.0149(8) 0.0169(8) -0.0027(6) 0.0055(7) 0.0004(6) C4 0.0110(7) 0.0162(8) 0.0147(8) 0.0001(6) 0.0044(6) -0.0007(6) C5 0.0131(8) 0.0186(9) 0.0186(9) -0.0002(6) 0.0072(7) 0.0006(7) N6 0.0169(7) 0.0195(7) 0.0171(7) 0.0018(6) 0.0070(6) -0.0010(6) C7 0.0167(8) 0.0140(8) 0.0199(9) -0.0025(6) 0.0058(7) 0.0025(7) C9 0.0279(10) 0.0271(10) 0.0168(9) -0.0084(8) -0.0003(8) 0.0051(8) C8 0.0267(10) 0.0196(9) 0.0208(9) -0.0031(7) 0.0077(8) 0.0006(7) C10 0.0178(9) 0.0256(10) 0.0290(10) -0.0029(7) -0.0001(8) 0.0116(8) C11 0.0163(8) 0.0182(8) 0.0275(10) -0.0001(7) 0.0068(7) 0.0068(7) C12 0.0156(8) 0.0143(8) 0.0205(9) -0.0015(6) 0.0062(7) 0.0034(7) C13 0.0140(8) 0.0133(8) 0.0255(9) 0.0006(6) 0.0094(7) -0.0004(7) C14 0.0119(8) 0.0144(8) 0.0218(9) -0.0024(6) 0.0077(7) -0.0021(6) C15 0.0142(8) 0.0248(9) 0.0208(9) -0.0005(7) 0.0064(7) -0.0046(7) C16 0.0162(8) 0.0153(8) 0.0119(8) -0.0001(6) 0.0060(6) -0.0012(6) C17 0.0165(8) 0.0214(9) 0.0204(9) 0.0022(7) 0.0018(7) -0.0015(7) C18 0.0285(10) 0.0194(9) 0.0202(9) 0.0064(8) 0.0042(8) -0.0002(7) C19 0.0319(10) 0.0156(9) 0.0210(9) -0.0023(7) 0.0123(8) -0.0010(7) C20 0.0195(9) 0.0208(9) 0.0331(11) -0.0044(7) 0.0104(8) -0.0027(8) C21 0.0150(8) 0.0175(9) 0.0286(10) 0.0005(7) 0.0066(7) -0.0009(7) C22 0.0252(10) 0.0200(9) 0.0230(10) 0.0024(8) 0.0100(8) -0.0032(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag O1 C2 . 1.350(2) ? O1 C15 . 1.464(2) ? O3 C2 . 1.203(2) ? C2 C4 . 1.530(2) ? C4 C14 . 1.497(2) ? C4 C16 . 1.534(2) ? C4 C5 . 1.546(2) ? C5 N6 . 1.445(2) ? C5 H5A . 0.98(2) ? C5 H5B . 0.98(2) ? N6 C7 . 1.387(2) ? N6 C22 . 1.456(2) ? C7 C8 . 1.409(3) ? C7 C12 . 1.426(2) ? C9 C8 . 1.382(3) ? C9 C10 . 1.388(3) ? C9 H9 . 0.94(2) ? C8 H8 . 0.97(2) ? C10 C11 . 1.376(3) ? C10 H10 . 0.98(2) ? C11 C12 . 1.409(2) ? C11 H11 . 0.98(2) ? C12 C13 . 1.468(3) ? C13 C14 . 1.329(3) ? C13 H13 . 0.97(2) ? C14 C15 . 1.499(2) ? C15 H15A . 0.97(2) ? C15 H15B . 0.97(2) ? C16 C21 . 1.387(2) ? C16 C17 . 1.393(2) ? C17 C18 . 1.388(3) ? C17 H17 . 0.97(2) ? C18 C19 . 1.387(3) ? C18 H18 . 0.94(3) ? C19 C20 . 1.381(3) ? C19 H19 . 0.95(2) ? C20 C21 . 1.390(3) ? C20 H20 . 0.98(3) ? C21 H21 . 0.95(2) ? C22 H22A . 0.98(2) ? C22 H22B . 1.02(2) ? C22 H22C . 0.98(2) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C2 O1 C15 . . 110.38(13) ? O3 C2 O1 . . 121.27(16) ? O3 C2 C4 . . 127.52(16) ? O1 C2 C4 . . 111.21(14) ? C14 C4 C2 . . 101.04(13) ? C14 C4 C16 . . 114.93(14) ? C2 C4 C16 . . 109.59(14) ? C14 C4 C5 . . 110.04(14) ? C2 C4 C5 . . 109.98(14) ? C16 C4 C5 . . 110.82(14) ? N6 C5 C4 . . 112.16(14) ? N6 C5 H5A . . 108.7(12) ? C4 C5 H5A . . 108.2(12) ? N6 C5 H5B . . 109.9(12) ? C4 C5 H5B . . 109.1(12) ? H5A C5 H5B . . 108.6(17) ? C7 N6 C5 . . 121.66(15) ? C7 N6 C22 . . 120.11(15) ? C5 N6 C22 . . 115.81(15) ? N6 C7 C8 . . 118.80(16) ? N6 C7 C12 . . 123.42(16) ? C8 C7 C12 . . 117.77(17) ? C8 C9 C10 . . 120.22(19) ? C8 C9 H9 . . 119.3(14) ? C10 C9 H9 . . 120.5(14) ? C9 C8 C7 . . 122.27(19) ? C9 C8 H8 . . 118.8(14) ? C7 C8 H8 . . 119.0(14) ? C11 C10 C9 . . 118.55(18) ? C11 C10 H10 . . 120.5(14) ? C9 C10 H10 . . 120.9(14) ? C10 C11 C12 . . 123.31(18) ? C10 C11 H11 . . 120.3(13) ? C12 C11 H11 . . 116.4(13) ? C11 C12 C7 . . 117.86(17) ? C11 C12 C13 . . 114.61(16) ? C7 C12 C13 . . 127.52(16) ? C14 C13 C12 . . 131.07(16) ? C14 C13 H13 . . 116.0(12) ? C12 C13 H13 . . 112.9(12) ? C13 C14 C4 . . 127.31(16) ? C13 C14 C15 . . 124.58(16) ? C4 C14 C15 . . 107.41(15) ? O1 C15 C14 . . 104.46(14) ? O1 C15 H15A . . 105.9(13) ? C14 C15 H15A . . 113.5(13) ? O1 C15 H15B . . 107.2(13) ? C14 C15 H15B . . 113.5(13) ? H15A C15 H15B . . 111.5(18) ? C21 C16 C17 . . 118.83(16) ? C21 C16 C4 . . 120.23(15) ? C17 C16 C4 . . 120.89(15) ? C18 C17 C16 . . 120.36(17) ? C18 C17 H17 . . 119.0(14) ? C16 C17 H17 . . 120.6(14) ? C19 C18 C17 . . 120.34(18) ? C19 C18 H18 . . 119.7(16) ? C17 C18 H18 . . 119.9(16) ? C20 C19 C18 . . 119.56(18) ? C20 C19 H19 . . 120.5(14) ? C18 C19 H19 . . 119.9(14) ? C19 C20 C21 . . 120.19(18) ? C19 C20 H20 . . 119.9(15) ? C21 C20 H20 . . 119.9(15) ? C16 C21 C20 . . 120.71(17) ? C16 C21 H21 . . 118.7(14) ? C20 C21 H21 . . 120.6(14) ? N6 C22 H22A . . 108.0(13) ? N6 C22 H22B . . 113.1(13) ? H22A C22 H22B . . 110.5(19) ? N6 C22 H22C . . 109.8(14) ? H22A C22 H22C . . 107.5(19) ? H22B C22 H22C . . 107.8(19) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C15 O1 C2 O3 . . . . -178.22(16) ? C15 O1 C2 C4 . . . . 1.42(19) ? O3 C2 C4 C14 . . . . 164.51(18) ? O1 C2 C4 C14 . . . . -15.10(18) ? O3 C2 C4 C16 . . . . -73.8(2) ? O1 C2 C4 C16 . . . . 106.59(15) ? O3 C2 C4 C5 . . . . 48.3(2) ? O1 C2 C4 C5 . . . . -131.36(15) ? C14 C4 C5 N6 . . . . 77.93(18) ? C2 C4 C5 N6 . . . . -171.62(14) ? C16 C4 C5 N6 . . . . -50.30(19) ? C4 C5 N6 C7 . . . . -78.0(2) ? C4 C5 N6 C22 . . . . 119.67(17) ? C5 N6 C7 C8 . . . . -151.91(16) ? C22 N6 C7 C8 . . . . 9.7(2) ? C5 N6 C7 C12 . . . . 28.9(2) ? C22 N6 C7 C12 . . . . -169.49(16) ? C10 C9 C8 C7 . . . . -1.0(3) ? N6 C7 C8 C9 . . . . -178.31(17) ? C12 C7 C8 C9 . . . . 0.9(3) ? C8 C9 C10 C11 . . . . -0.3(3) ? C9 C10 C11 C12 . . . . 1.6(3) ? C10 C11 C12 C7 . . . . -1.6(3) ? C10 C11 C12 C13 . . . . 177.03(17) ? N6 C7 C12 C11 . . . . 179.52(16) ? C8 C7 C12 C11 . . . . 0.3(2) ? N6 C7 C12 C13 . . . . 1.1(3) ? C8 C7 C12 C13 . . . . -178.11(17) ? C11 C12 C13 C14 . . . . -168.04(18) ? C7 C12 C13 C14 . . . . 10.4(3) ? C12 C13 C14 C4 . . . . -9.2(3) ? C12 C13 C14 C15 . . . . -178.36(17) ? C2 C4 C14 C13 . . . . -148.10(17) ? C16 C4 C14 C13 . . . . 94.0(2) ? C5 C4 C14 C13 . . . . -31.9(2) ? C2 C4 C14 C15 . . . . 22.54(17) ? C16 C4 C14 C15 . . . . -95.32(17) ? C5 C4 C14 C15 . . . . 138.75(15) ? C2 O1 C15 C14 . . . . 13.07(19) ? C13 C14 C15 O1 . . . . 148.32(17) ? C4 C14 C15 O1 . . . . -22.65(18) ? C14 C4 C16 C21 . . . . -25.3(2) ? C2 C4 C16 C21 . . . . -138.20(17) ? C5 C4 C16 C21 . . . . 100.24(18) ? C14 C4 C16 C17 . . . . 157.15(16) ? C2 C4 C16 C17 . . . . 44.2(2) ? C5 C4 C16 C17 . . . . -77.3(2) ? C21 C16 C17 C18 . . . . 1.0(3) ? C4 C16 C17 C18 . . . . 178.61(17) ? C16 C17 C18 C19 . . . . -0.7(3) ? C17 C18 C19 C20 . . . . 0.0(3) ? C18 C19 C20 C21 . . . . 0.3(3) ? C17 C16 C21 C20 . . . . -0.7(3) ? C4 C16 C21 C20 . . . . -178.33(17) ? C19 C20 C21 C16 . . . . 0.1(3) ? _shelx_res_file ; TITL AD838_a.res in P2(1)/c AD838_a.res created by SHELXL-2017/1 at 11:26:01 on 05-May-2021 REM Old TITL AD838 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.130, Rweak 0.012, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C19 N O2 CELL 0.71073 6.1270 22.8523 10.9205 90.000 106.091 90.000 ZERR 4.000 0.0002 0.0007 0.0003 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 76 68 4 8 TEMP -173.190 SIZE 0.14 0.26 0.80 L.S. 10 BOND $H conf acta LIST 6 FMAP 2 PLAN 20 OMIT -1 2 1 OMIT 0 2 1 WGHT 0.014800 1.631700 FVAR 0.69434 O1 4 0.352839 0.318539 -0.009055 11.00000 0.01585 0.02224 = 0.01882 -0.00461 0.00556 -0.00283 O3 4 0.052927 0.362604 0.027411 11.00000 0.01340 0.02568 = 0.02319 -0.00087 0.00273 -0.00098 C2 1 0.252389 0.351377 0.062653 11.00000 0.01517 0.01494 = 0.01689 0.00040 0.00552 -0.00269 C4 1 0.423162 0.370011 0.187359 11.00000 0.01102 0.01622 = 0.01471 -0.00073 0.00436 0.00012 C5 1 0.325562 0.357478 0.301006 11.00000 0.01306 0.01863 = 0.01855 0.00060 0.00717 -0.00017 H5A 2 0.173785 0.374983 0.282340 11.00000 0.01803 H5B 2 0.311319 0.315077 0.309940 11.00000 0.01342 N6 3 0.465240 0.381900 0.418725 11.00000 0.01688 0.01951 = 0.01707 -0.00099 0.00696 0.00177 C7 1 0.664972 0.355090 0.487046 11.00000 0.01671 0.01402 = 0.01987 0.00246 0.00581 -0.00248 C9 1 0.939479 0.339193 0.694373 11.00000 0.02789 0.02710 = 0.01680 0.00509 -0.00030 -0.00839 H9 2 0.982429 0.345911 0.782430 11.00000 0.02145 C8 1 0.739399 0.363195 0.620082 11.00000 0.02665 0.01965 = 0.02079 0.00061 0.00771 -0.00315 H8 2 0.646173 0.386211 0.661344 11.00000 0.02973 C10 1 1.073566 0.305020 0.638971 11.00000 0.01781 0.02560 = 0.02896 0.01163 -0.00010 -0.00291 H10 2 1.217747 0.288298 0.690673 11.00000 0.02973 C11 1 1.002165 0.295588 0.509571 11.00000 0.01633 0.01824 = 0.02748 0.00681 0.00679 -0.00011 H11 2 1.091000 0.270776 0.468454 11.00000 0.01865 C12 1 0.802031 0.320044 0.429564 11.00000 0.01563 0.01427 = 0.02053 0.00338 0.00623 -0.00149 C13 1 0.762905 0.306937 0.293584 11.00000 0.01398 0.01332 = 0.02548 -0.00040 0.00935 0.00064 H13 2 0.865623 0.277480 0.277883 11.00000 0.01598 C14 1 0.616341 0.329343 0.190983 11.00000 0.01195 0.01441 = 0.02179 -0.00210 0.00772 -0.00242 C15 1 0.593450 0.309880 0.056960 11.00000 0.01423 0.02475 = 0.02076 -0.00462 0.00638 -0.00046 H15A 2 0.676538 0.334134 0.012660 11.00000 0.02280 H15B 2 0.626626 0.268493 0.049965 11.00000 0.02429 C16 1 0.478420 0.435205 0.181037 11.00000 0.01620 0.01534 = 0.01193 -0.00119 0.00596 -0.00015 C17 1 0.306911 0.475963 0.133054 11.00000 0.01655 0.02137 = 0.02041 -0.00154 0.00184 0.00221 H17 2 0.150539 0.463442 0.098951 11.00000 0.02800 C18 1 0.358484 0.535016 0.130352 11.00000 0.02845 0.01938 = 0.02022 -0.00024 0.00422 0.00636 H18 2 0.241927 0.562293 0.095899 11.00000 0.03626 C19 1 0.580992 0.554136 0.176600 11.00000 0.03192 0.01556 = 0.02100 -0.00100 0.01229 -0.00235 H19 2 0.614724 0.594475 0.175498 11.00000 0.02280 C20 1 0.751387 0.514020 0.225437 11.00000 0.01951 0.02084 = 0.03308 -0.00267 0.01037 -0.00440 H20 2 0.908120 0.527325 0.259881 11.00000 0.03384 C21 1 0.700247 0.454825 0.227699 11.00000 0.01498 0.01746 = 0.02856 -0.00085 0.00658 0.00045 H21 2 0.816919 0.426911 0.262040 11.00000 0.02553 C22 1 0.355310 0.424846 0.480255 11.00000 0.02525 0.01995 = 0.02301 -0.00316 0.01000 0.00238 H22A 2 0.255689 0.448811 0.413791 11.00000 0.02343 H22B 2 0.266286 0.406432 0.536129 11.00000 0.02958 H22C 2 0.469883 0.450861 0.533979 11.00000 0.02858 HKLF 4 REM AD838_a.res in P2(1)/c REM R1 = 0.0540 for 3135 Fo > 4sig(Fo) and 0.0574 for all 3353 data REM 267 parameters refined using 0 restraints END WGHT 0.0150 1.6299 REM Highest difference peak 0.416, deepest hole -0.231, 1-sigma level 0.049 Q1 1 0.3376 0.3645 0.1290 11.00000 0.05 0.42 Q2 1 0.4502 0.4019 0.1821 11.00000 0.05 0.39 Q3 1 0.7550 0.3116 0.3626 11.00000 0.05 0.32 Q4 1 0.7430 0.3384 0.2486 11.00000 0.05 0.30 Q5 1 0.5310 0.3511 0.1935 11.00000 0.05 0.28 Q6 1 0.3841 0.3645 0.2438 11.00000 0.05 0.26 Q7 1 0.6203 0.2996 0.2296 11.00000 0.05 0.26 Q8 1 0.5967 0.4449 0.1626 11.00000 0.05 0.25 Q9 1 1.0020 0.2908 0.5786 11.00000 0.05 0.25 Q10 1 0.8798 0.3019 0.4748 11.00000 0.05 0.25 Q11 1 0.5848 0.3184 0.1250 11.00000 0.05 0.24 Q12 1 0.7440 0.3683 0.5561 11.00000 0.05 0.23 Q13 1 0.7412 0.3414 0.4534 11.00000 0.05 0.23 Q14 1 0.5721 0.4459 0.2369 11.00000 0.05 0.22 Q15 1 0.7150 0.4843 0.1887 11.00000 0.05 0.22 Q16 1 0.3994 0.3730 0.3649 11.00000 0.05 0.21 Q17 1 0.3879 0.4609 0.1926 11.00000 0.05 0.21 Q18 1 0.8889 0.3686 0.6526 11.00000 0.05 0.21 Q19 1 0.4051 0.4513 0.1302 11.00000 0.05 0.21 Q20 1 0.2726 0.5101 0.1612 11.00000 0.05 0.20 ; _shelx_res_checksum 22757 _shelx_hkl_file ; -2 0 0 329.67 11.80 -2 0 0 330.87 11.40 2 0 0 334.07 11.70 2 0 0 331.37 11.70 2 0 0 341.47 11.40 2 0 0 328.27 11.40 2 0 0 322.77 11.60 2 0 0 327.47 11.80 2 0 0 321.87 11.40 -2 0 0 322.87 11.40 -2 0 0 333.47 11.70 -2 0 0 322.27 11.70 -2 0 0 341.77 11.70 3 0 0 3057.29 99.39 -3 0 0 3013.30 99.09 -3 0 0 3007.30 99.19 3 0 0 2941.31 98.99 3 0 0 2923.51 98.69 -3 0 0 3036.10 98.69 3 0 0 3024.80 99.09 3 0 0 2966.40 99.19 3 0 0 3055.09 98.69 -3 0 0 3050.39 99.29 -3 0 0 3066.89 99.09 4 0 0 15.40 2.90 -4 0 0 17.60 2.50 -4 0 0 14.20 2.60 4 0 0 17.40 2.40 4 0 0 15.20 2.20 -4 0 0 21.10 2.70 -4 0 0 13.60 2.50 -4 0 0 18.70 2.20 4 0 0 14.20 2.50 4 0 0 17.30 2.70 4 0 0 17.20 2.30 5 0 0 2.80 2.60 -5 0 0 7.90 2.80 -5 0 0 6.50 2.60 -5 0 0 5.30 2.00 5 0 0 8.90 2.20 5 0 0 5.10 2.60 -5 0 0 2.00 2.30 5 0 0 4.50 2.60 5 0 0 4.20 2.10 6 0 0 20.60 4.10 -6 0 0 18.60 3.80 6 0 0 26.10 4.50 -6 0 0 27.40 4.50 -6 0 0 23.10 3.10 -6 0 0 20.00 3.60 6 0 0 22.40 4.10 6 0 0 22.70 3.20 6 0 0 25.80 3.40 -7 0 0 74.39 5.20 7 0 0 69.79 5.20 -7 0 0 71.99 6.30 7 0 0 72.39 6.70 -7 0 0 82.89 7.40 7 0 0 83.69 7.10 7 0 0 69.59 5.20 7 0 0 85.69 7.30 -7 0 0 67.39 6.90 1 -1 0 25.80 1.50 -1 -1 0 26.00 1.50 -1 -1 0 24.50 1.50 1 -1 0 26.10 1.70 -1 -1 0 23.90 1.50 -1 -1 0 26.10 1.60 1 -1 0 25.10 1.50 -1 -1 0 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0 2511.95 81.99 -1 -2 0 2503.25 82.29 1 -2 0 2494.55 82.19 -1 -2 0 2540.25 82.39 1 -2 0 2535.65 82.19 1 -2 0 2437.36 82.19 -1 -2 0 2564.44 82.19 1 -2 0 2421.56 81.89 -1 2 0 2453.25 82.19 -1 2 0 2537.15 82.19 -1 2 0 2573.74 82.29 1 2 0 2651.83 82.29 1 2 0 2489.95 82.29 1 2 0 2517.05 82.19 -1 2 0 2559.54 82.19 -1 2 0 2532.85 81.89 -1 2 0 2618.14 82.39 1 2 0 2505.55 82.19 1 2 0 2503.55 82.29 1 2 0 2584.14 82.09 1 2 0 2518.35 81.89 -1 2 0 2602.94 82.29 -1 2 0 2452.75 82.29 -1 2 0 2501.75 82.19 -2 -2 0 276.57 10.20 2 -2 0 280.87 10.40 -2 -2 0 297.17 10.10 2 -2 0 294.07 10.50 2 -2 0 279.67 10.30 2 -2 0 288.27 10.40 2 -2 0 285.47 9.80 -2 -2 0 278.47 10.30 -2 -2 0 291.17 9.80 2 -2 0 280.67 10.20 -2 -2 0 293.27 10.50 2 2 0 280.57 10.20 2 2 0 280.07 10.00 -2 2 0 287.37 10.30 2 2 0 277.57 9.70 2 2 0 279.07 9.70 2 2 0 283.67 10.40 2 2 0 283.57 10.30 -2 2 0 280.57 9.70 -2 2 0 287.07 10.30 -2 2 0 285.17 10.20 -2 2 0 281.57 10.10 2 2 0 286.77 9.70 2 2 0 296.67 10.20 -2 2 0 298.27 10.40 -2 2 0 278.97 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723.03 23.60 1 -3 0 707.33 23.70 -1 -3 0 711.93 23.80 -1 -3 0 703.93 23.50 1 -3 0 679.53 23.30 -1 -3 0 720.73 23.90 -1 -3 0 732.03 23.80 -1 -3 0 706.23 23.80 1 -3 0 727.13 23.90 1 -3 0 690.73 23.80 1 -3 0 705.53 23.90 -1 -3 0 682.33 23.40 -1 -3 0 696.73 23.70 1 3 0 722.63 23.80 -1 3 0 663.73 23.90 -1 3 0 739.43 23.90 -1 3 0 716.23 23.70 -1 3 0 746.43 23.80 -1 3 0 739.93 23.70 1 3 0 740.73 23.80 -1 3 0 704.43 23.60 1 3 0 710.83 23.30 -1 3 0 731.93 23.80 1 3 0 727.93 23.80 1 3 0 729.83 23.90 1 3 0 710.53 23.60 1 3 0 705.73 23.50 1 3 0 722.43 23.70 -1 3 0 721.83 23.40 -2 -3 0 450.05 14.90 2 -3 0 437.66 15.70 2 -3 0 441.16 15.60 -2 -3 0 454.25 15.40 -2 -3 0 463.65 15.30 2 -3 0 440.06 15.50 -2 -3 0 462.85 15.80 2 -3 0 437.16 14.90 2 -3 0 457.95 15.40 -2 -3 0 449.86 15.60 -2 3 0 447.46 15.60 2 3 0 461.25 15.50 2 3 0 441.06 14.90 -2 3 0 453.75 15.50 -2 3 0 422.36 14.90 -2 3 0 459.45 15.60 2 3 0 441.36 15.60 2 3 0 444.66 15.20 -2 3 0 461.95 15.70 -2 3 0 428.76 15.40 -2 3 0 452.15 15.40 2 3 0 403.96 14.90 2 3 0 460.25 15.80 2 3 0 464.65 15.60 -3 -3 0 429.76 15.20 3 -3 0 399.56 15.00 3 -3 0 400.26 15.00 3 -3 0 412.06 14.20 3 -3 0 409.66 14.80 -3 -3 0 426.26 15.30 3 -3 0 417.16 15.20 -3 -3 0 425.66 14.90 -3 -3 0 430.56 14.20 -3 -3 0 431.36 14.70 -3 3 0 430.96 15.10 -3 3 0 394.36 14.10 3 3 0 426.86 14.90 -3 3 0 424.66 15.00 3 3 0 415.76 15.00 3 3 0 387.66 14.10 3 3 0 407.66 14.60 -3 3 0 405.86 14.90 -3 3 0 422.66 15.10 3 3 0 417.06 15.20 3 3 0 407.96 14.20 3 3 0 410.96 15.00 3 3 0 401.96 14.10 -3 3 0 422.46 15.00 -3 3 0 428.46 14.80 4 -3 0 334.97 13.00 4 -3 0 341.07 12.20 -4 -3 0 353.06 13.40 -4 -3 0 326.57 13.00 -4 -3 0 344.97 12.20 4 -3 0 355.56 13.40 4 -3 0 344.37 13.40 -4 -3 0 362.56 12.90 4 3 0 340.17 13.20 4 3 0 340.67 12.90 4 3 0 340.47 12.10 -4 3 0 342.97 13.20 4 3 0 348.57 13.60 4 3 0 343.67 12.80 -4 3 0 349.07 12.90 -4 3 0 332.87 13.20 4 3 0 353.36 13.30 -4 3 0 333.17 13.10 -4 3 0 342.37 13.30 5 -3 0 161.48 7.80 5 -3 0 161.98 8.20 5 -3 0 159.78 7.90 5 -3 0 142.89 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333.27 11.70 2 4 0 327.27 11.80 2 4 0 324.07 11.50 -2 4 0 309.37 10.80 -2 4 0 329.27 11.70 2 4 0 327.87 11.20 -2 4 0 324.77 11.70 -2 4 0 329.37 11.60 3 -4 0 35.40 2.10 3 -4 0 28.60 2.70 -3 -4 0 28.00 3.10 -3 -4 0 30.80 3.00 -3 -4 0 32.80 2.80 -3 -4 0 32.80 2.00 3 -4 0 32.20 2.90 3 -4 0 33.30 3.10 3 -4 0 34.10 3.00 -3 -4 0 33.40 2.60 -3 4 0 30.50 3.00 -3 4 0 34.50 3.10 3 4 0 29.80 1.90 3 4 0 29.80 3.00 3 4 0 29.60 1.90 3 4 0 34.00 1.90 -3 4 0 33.60 2.90 -3 4 0 34.50 2.00 -3 4 0 34.50 3.10 3 4 0 32.80 2.90 3 4 0 32.00 3.10 3 4 0 31.00 2.50 -3 4 0 38.90 3.10 3 4 0 31.10 3.00 -3 4 0 33.80 2.80 4 -4 0 1.70 1.80 -4 -4 0 4.20 2.00 4 -4 0 3.00 1.40 4 -4 0 5.50 2.10 4 -4 0 7.50 2.30 -4 -4 0 1.60 1.80 -4 -4 0 3.50 1.70 -4 -4 0 4.50 1.30 -4 4 0 4.00 2.00 4 4 0 4.40 1.60 4 4 0 5.00 2.20 -4 4 0 5.40 2.00 -4 4 0 9.70 2.40 -4 4 0 5.40 2.10 4 4 0 3.50 1.10 4 4 0 4.90 2.00 4 4 0 1.40 2.10 4 4 0 4.40 1.20 4 4 0 6.30 2.10 -4 4 0 3.80 1.90 -4 4 0 5.90 2.10 5 -4 0 1.00 2.50 -5 -4 0 2.20 2.40 5 -4 0 0.70 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0 -5 0 1.90 1.10 0 -5 0 1.60 0.90 0 5 0 0.70 1.00 0 5 0 0.10 1.00 0 5 0 0.60 0.70 0 5 0 1.00 0.90 0 5 0 0.40 0.90 0 5 0 1.60 0.80 0 5 0 0.30 1.10 0 5 0 2.10 1.10 1 -5 0 96.09 3.70 -1 -5 0 86.99 3.60 -1 -5 0 94.19 3.70 1 -5 0 92.89 4.00 -1 -5 0 94.19 4.00 1 -5 0 96.29 3.90 1 -5 0 95.49 4.20 1 -5 0 93.89 4.10 1 -5 0 98.89 3.50 -1 -5 0 94.29 4.00 -1 -5 0 94.49 3.60 -1 -5 0 93.29 3.40 -1 -5 0 98.79 4.30 -1 5 0 97.99 4.00 -1 5 0 83.69 4.20 -1 5 0 96.79 3.80 1 5 0 98.29 4.10 1 5 0 95.49 4.00 -1 5 0 100.19 4.00 1 5 0 102.09 4.30 1 5 0 94.59 3.50 -1 5 0 90.49 3.50 1 5 0 95.69 3.70 1 5 0 93.49 4.00 -1 5 0 98.19 4.10 1 5 0 100.79 4.10 -1 5 0 98.69 4.20 -1 5 0 84.19 4.10 1 5 0 95.59 3.70 -1 5 0 97.89 3.90 2 -5 0 3.10 1.60 -2 -5 0 1.80 1.20 -2 -5 0 -0.90 1.30 -2 -5 0 0.50 0.60 -2 -5 0 0.40 0.80 2 -5 0 3.00 1.50 -2 -5 0 6.50 1.70 2 -5 0 2.00 1.40 -2 -5 0 1.50 1.00 2 -5 0 0.70 1.20 2 -5 0 1.30 0.70 -2 5 0 2.40 1.60 -2 5 0 3.30 1.40 2 5 0 1.50 1.60 -2 5 0 2.80 1.70 2 5 0 2.70 1.60 -2 5 0 0.80 1.30 2 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1.20 5 -5 0 -1.30 2.30 5 -5 0 -0.20 2.50 -5 -5 0 0.60 2.20 5 -5 0 -1.30 1.50 -5 -5 0 2.50 2.60 -5 5 0 -0.60 2.50 5 5 0 0.00 1.10 5 5 0 -1.90 2.30 -5 5 0 2.10 2.60 -5 5 0 4.10 2.80 5 5 0 4.50 2.80 5 5 0 -0.20 2.10 -5 5 0 0.60 2.20 5 5 0 4.70 1.90 5 5 0 0.00 2.40 6 -5 0 6.60 3.60 6 -5 0 7.50 2.00 6 -5 0 13.40 3.60 -6 -5 0 12.90 3.10 -6 -5 0 7.60 1.80 -6 -5 0 5.40 2.90 6 -5 0 6.10 3.10 -6 -5 0 11.50 3.70 6 -5 0 6.40 3.00 6 5 0 5.30 3.10 -6 5 0 9.50 3.70 -6 5 0 6.00 3.20 6 5 0 4.30 3.50 6 5 0 8.70 3.50 -6 5 0 4.10 3.40 6 5 0 8.80 1.50 6 5 0 12.40 3.40 -6 5 0 9.80 2.90 7 -5 0 22.30 5.00 -7 -5 0 21.60 2.60 -7 -5 0 16.60 4.60 7 -5 0 17.50 4.50 7 -5 0 29.40 4.70 7 -5 0 31.80 4.90 -7 -5 0 25.30 4.70 -7 -5 0 22.60 3.80 7 5 0 19.90 4.10 -7 5 0 22.00 4.90 -7 5 0 12.90 4.00 7 5 0 21.90 4.70 7 5 0 22.70 5.00 7 5 0 19.20 4.30 -7 5 0 20.70 3.90 -7 5 0 26.80 5.20 0 -6 0 9155.68 288.97 0 -6 0 8731.53 289.07 0 -6 0 8782.02 288.87 -1 -6 0 278.17 10.20 -1 -6 0 285.67 9.40 1 -6 0 270.97 9.80 1 -6 0 281.77 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944.11 34.60 3 -6 0 978.80 34.80 -3 -6 0 1053.59 34.80 3 -6 0 1005.30 34.60 -3 -6 0 1049.70 34.00 -3 -6 0 1023.20 33.40 -3 -6 0 1003.00 34.90 -3 -6 0 1007.50 34.30 -3 6 0 1070.59 34.90 3 6 0 1006.10 33.50 3 6 0 978.00 33.30 3 6 0 1008.80 33.90 -3 6 0 1011.80 34.30 -3 6 0 969.60 33.40 -3 6 0 1047.50 34.80 3 6 0 1039.80 34.80 3 6 0 1043.90 35.00 -3 6 0 1038.00 34.60 3 6 0 1059.89 34.70 -3 6 0 1034.10 34.70 -3 6 0 1001.10 34.40 3 6 0 1042.50 34.50 4 -6 0 3.10 2.20 4 -6 0 1.50 2.10 4 -6 0 0.80 1.10 -4 -6 0 1.40 1.60 -4 -6 0 0.70 1.50 4 -6 0 -0.60 1.80 -4 -6 0 2.40 2.00 -4 -6 0 1.30 1.00 4 6 0 1.50 0.90 4 6 0 4.80 2.40 -4 6 0 3.30 2.10 -4 6 0 0.40 2.00 4 6 0 0.60 2.10 4 6 0 1.60 1.40 4 6 0 -2.30 1.90 -4 6 0 1.20 2.10 -4 6 0 -2.30 1.60 -4 6 0 2.70 2.10 4 6 0 -1.20 1.90 4 6 0 1.10 0.90 -4 6 0 2.80 2.00 4 6 0 3.20 0.90 5 -6 0 23.50 3.40 -5 -6 0 17.80 1.90 5 -6 0 24.00 2.20 5 -6 0 22.40 3.70 5 -6 0 17.70 3.50 -5 -6 0 21.30 3.20 -5 -6 0 17.60 3.50 -5 -6 0 18.40 2.70 -5 6 0 22.00 3.60 5 6 0 22.40 4.10 5 6 0 21.40 3.50 5 6 0 20.40 3.70 5 6 0 19.80 2.50 5 6 0 22.00 3.30 5 6 0 17.70 1.70 -5 6 0 15.90 3.40 5 6 0 17.50 1.70 -5 6 0 16.60 3.10 -5 6 0 19.00 3.50 6 -6 0 57.09 5.10 6 -6 0 54.19 5.90 -6 -6 0 51.69 4.70 6 -6 0 53.49 5.20 -6 -6 0 46.10 3.10 6 -6 0 58.69 5.20 -6 -6 0 43.70 4.80 6 -6 0 50.89 3.20 -6 -6 0 49.80 5.50 -6 6 0 41.50 5.10 6 6 0 51.69 5.10 6 6 0 54.09 5.60 6 6 0 55.09 5.90 6 6 0 48.50 5.20 -6 6 0 57.79 5.80 -6 6 0 51.99 5.00 -6 6 0 52.49 5.70 -7 -6 0 52.09 5.90 7 -6 0 44.70 5.20 7 -6 0 46.50 5.60 7 -6 0 51.39 6.10 7 -6 0 53.59 6.80 -7 -6 0 45.10 4.90 -7 -6 0 43.40 3.20 -7 -6 0 41.30 5.90 -7 6 0 37.10 5.40 7 6 0 54.69 6.00 -7 6 0 45.40 6.00 7 6 0 51.49 6.70 7 6 0 56.49 6.40 -7 6 0 51.19 6.30 -7 6 0 43.00 5.10 7 6 0 43.50 5.30 0 7 0 2.90 1.30 1 -7 0 274.47 9.90 -1 -7 0 297.27 9.90 -1 -7 0 268.87 10.10 -1 -7 0 288.67 10.00 1 -7 0 303.07 10.40 -1 -7 0 295.17 10.00 -1 -7 0 281.67 10.30 1 -7 0 278.17 10.00 -1 -7 0 292.97 10.00 1 -7 0 294.47 10.00 1 -7 0 288.37 10.50 -1 -7 0 282.77 9.80 -1 -7 0 297.97 10.70 1 -7 0 291.77 10.30 -1 7 0 295.97 10.10 -1 7 0 303.97 10.40 -1 7 0 285.47 10.50 1 7 0 282.27 10.20 -1 7 0 289.27 10.60 1 7 0 290.17 10.40 1 7 0 298.57 10.50 1 7 0 287.87 9.80 -1 7 0 285.07 10.80 1 7 0 294.47 10.50 -1 7 0 300.57 10.40 -1 7 0 296.17 10.50 1 7 0 294.27 10.60 2 -7 0 48.10 3.50 -2 -7 0 51.09 2.50 2 -7 0 51.19 3.50 2 -7 0 51.79 3.20 -2 -7 0 49.80 3.40 -2 -7 0 48.30 2.40 2 -7 0 49.00 3.10 -2 -7 0 51.79 3.40 2 -7 0 49.60 2.20 -2 -7 0 49.40 2.90 2 7 0 49.80 2.50 2 7 0 49.40 3.10 -2 7 0 56.39 3.20 -2 7 0 55.79 3.60 -2 7 0 49.40 3.50 2 7 0 53.79 3.60 2 7 0 53.69 2.50 2 7 0 53.49 3.40 -2 7 0 49.20 3.70 -2 7 0 45.20 3.20 -2 7 0 49.20 2.30 2 7 0 61.19 3.70 -2 7 0 56.69 3.40 3 -7 0 93.69 3.80 3 -7 0 92.09 5.30 3 -7 0 100.59 5.00 -3 -7 0 97.39 3.90 3 -7 0 99.29 5.00 -3 -7 0 99.89 4.80 3 -7 0 94.19 5.10 -3 -7 0 96.49 5.40 -3 -7 0 101.89 5.30 -3 -7 0 103.69 4.40 -3 7 0 98.49 5.40 -3 7 0 99.89 3.70 -3 7 0 106.29 5.00 -3 7 0 101.79 5.30 -3 7 0 99.09 4.90 3 7 0 103.69 5.10 3 7 0 99.39 3.90 3 7 0 110.29 5.20 3 7 0 99.49 4.30 -3 7 0 97.69 5.20 -3 7 0 103.59 5.20 3 7 0 107.29 5.40 3 7 0 108.79 5.70 -4 -7 0 203.98 8.90 -4 -7 0 198.48 7.80 4 -7 0 200.28 8.50 4 -7 0 190.48 7.00 -4 -7 0 193.58 6.90 -4 -7 0 197.58 8.30 4 -7 0 197.18 9.00 4 -7 0 186.88 8.50 4 7 0 187.58 7.70 4 7 0 193.38 6.90 4 7 0 202.28 8.90 -4 7 0 200.08 8.60 -4 7 0 191.88 8.30 4 7 0 203.28 8.80 4 7 0 201.08 8.50 -4 7 0 197.68 8.80 4 7 0 198.68 9.10 -4 7 0 189.78 8.40 -4 7 0 204.58 8.90 -4 7 0 189.38 6.90 4 7 0 182.88 6.90 4 7 0 182.18 6.80 -4 7 0 199.38 8.90 -5 -7 0 24.90 2.00 -5 -7 0 30.00 3.50 5 -7 0 28.40 4.00 -5 -7 0 28.50 4.00 5 -7 0 33.80 4.50 5 -7 0 31.50 3.80 5 -7 0 21.60 2.10 -5 -7 0 31.20 3.20 5 7 0 25.00 3.70 -5 7 0 25.30 3.80 -5 7 0 32.00 3.80 5 7 0 26.80 4.30 5 7 0 31.70 3.00 -5 7 0 23.30 3.80 5 7 0 34.00 4.10 -5 7 0 23.40 3.80 5 7 0 31.80 4.20 -5 7 0 31.00 4.20 6 -7 0 57.19 5.20 6 -7 0 59.29 5.80 6 -7 0 48.00 5.10 -6 -7 0 49.60 5.40 -6 -7 0 43.60 2.80 -6 -7 0 46.50 4.40 -6 -7 0 50.29 5.10 6 -7 0 47.60 5.10 6 7 0 42.70 5.60 -6 7 0 52.39 5.60 -6 7 0 53.89 5.80 6 7 0 47.30 5.50 -6 7 0 51.59 5.20 6 7 0 49.20 5.30 -6 7 0 45.30 5.30 6 7 0 47.40 5.10 -7 -7 0 4.20 3.50 7 -7 0 4.70 4.20 -7 -7 0 0.20 2.50 7 -7 0 2.70 3.20 7 -7 0 2.40 3.40 7 -7 0 5.10 3.60 -7 -7 0 1.10 3.80 7 7 0 1.10 4.00 -7 7 0 2.80 3.80 -7 7 0 -0.40 2.80 7 7 0 4.10 4.20 -7 7 0 -1.00 3.40 7 7 0 3.20 3.80 -7 7 0 0.20 3.70 7 7 0 2.60 3.30 0 -8 0 1571.34 51.79 0 -8 0 1578.84 51.89 0 -8 0 1595.34 52.19 0 -8 0 1579.54 52.19 0 -8 0 1525.25 51.69 0 8 0 1555.94 52.19 0 8 0 1611.04 51.99 0 8 0 1555.24 51.89 0 8 0 1647.44 51.89 0 8 0 1556.44 51.89 0 8 0 1706.23 52.19 0 8 0 1517.85 52.29 0 8 0 1515.65 51.79 1 -8 0 165.48 6.30 -1 -8 0 151.18 5.60 -1 -8 0 167.88 5.80 -1 -8 0 145.19 6.00 1 -8 0 156.68 5.80 1 -8 0 156.88 6.30 1 -8 0 158.98 6.10 -1 -8 0 155.18 6.20 -1 -8 0 161.58 5.80 -1 -8 0 154.18 6.50 1 -8 0 157.18 5.80 -1 -8 0 158.98 5.80 -1 -8 0 165.88 5.90 1 -8 0 155.78 5.80 -1 8 0 154.28 5.80 -1 8 0 157.48 6.20 -1 8 0 167.98 6.40 1 8 0 159.98 6.50 1 8 0 159.08 6.40 1 8 0 153.98 6.30 1 8 0 154.28 6.10 1 8 0 159.78 6.60 1 8 0 149.59 5.70 -1 8 0 159.28 6.30 -1 8 0 157.78 6.40 -1 8 0 150.98 6.50 -1 8 0 152.48 6.70 2 -8 0 2.40 1.60 -2 -8 0 3.40 1.70 -2 -8 0 4.10 1.30 -2 -8 0 6.00 2.20 2 -8 0 5.00 2.00 2 -8 0 3.80 1.50 -2 -8 0 4.40 1.10 2 -8 0 4.80 1.80 2 -8 0 4.30 0.90 -2 -8 0 3.40 1.00 2 8 0 1.10 1.60 -2 8 0 5.00 1.80 2 8 0 3.20 2.10 -2 8 0 4.10 1.50 -2 8 0 7.50 1.90 -2 8 0 3.70 2.00 -2 8 0 6.40 1.70 2 8 0 2.80 1.90 2 8 0 4.50 1.20 -2 8 0 3.30 1.60 2 8 0 3.90 1.10 2 8 0 2.20 2.00 3 -8 0 39.30 3.60 -3 -8 0 35.20 3.20 -3 -8 0 32.10 1.90 3 -8 0 30.60 1.70 -3 -8 0 35.20 2.80 -3 -8 0 36.70 2.40 3 -8 0 30.20 2.80 -3 -8 0 39.10 3.30 3 -8 0 34.00 3.10 3 -8 0 30.90 3.40 -3 8 0 33.00 3.10 3 8 0 35.60 3.70 3 8 0 30.80 3.10 -3 8 0 33.40 3.40 -3 8 0 35.20 3.00 3 8 0 30.30 1.90 3 8 0 35.60 2.30 -3 8 0 31.00 3.10 -3 8 0 31.20 3.40 3 8 0 34.70 3.40 -3 8 0 31.10 1.70 3 8 0 32.40 3.50 -3 8 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6 8 0 16.00 4.10 7 -8 0 61.49 6.40 7 -8 0 62.79 7.20 -7 -8 0 53.09 6.80 7 -8 0 74.59 6.50 -7 -8 0 57.99 6.00 -7 -8 0 52.19 5.10 7 -8 0 66.19 6.30 7 8 0 58.49 6.60 7 8 0 73.39 8.10 7 8 0 72.79 7.30 -7 8 0 53.49 6.40 7 8 0 53.09 5.90 -7 8 0 72.49 7.50 -7 8 0 57.49 6.00 -7 8 0 71.79 7.10 0 -9 0 7.60 1.60 0 -9 0 7.40 1.80 0 9 0 2.80 1.10 0 9 0 2.60 1.10 0 9 0 5.60 1.40 -1 -9 0 182.38 7.10 -1 -9 0 175.98 6.60 1 -9 0 182.78 7.10 -1 -9 0 195.48 6.80 -1 -9 0 184.58 6.70 -1 -9 0 190.68 6.70 -1 -9 0 193.48 6.80 1 -9 0 189.48 7.30 -1 -9 0 187.38 7.60 1 -9 0 180.18 6.80 1 -9 0 176.98 6.80 1 -9 0 178.88 7.30 1 -9 0 174.18 6.80 1 9 0 189.38 7.40 -1 9 0 194.88 7.40 -1 9 0 169.28 7.40 -1 9 0 178.88 6.80 -1 9 0 189.28 7.40 1 9 0 184.88 7.50 1 9 0 187.78 6.70 -1 9 0 183.38 7.80 1 9 0 197.68 7.50 1 9 0 183.08 7.30 1 9 0 180.78 7.10 -1 9 0 177.98 7.30 -1 9 0 189.88 7.20 -2 -9 0 173.38 6.80 -2 -9 0 183.28 6.80 2 -9 0 189.58 7.60 2 -9 0 182.38 6.60 -2 -9 0 188.28 7.60 -2 -9 0 182.28 6.40 2 -9 0 175.98 7.60 -2 -9 0 188.18 7.10 -2 -9 0 185.48 6.40 -2 -9 0 185.38 8.00 2 -9 0 185.58 7.30 2 -9 0 174.98 6.60 2 9 0 181.68 7.80 -2 9 0 189.88 7.70 -2 9 0 199.38 7.90 2 9 0 197.48 8.10 2 9 0 183.88 6.90 -2 9 0 182.78 8.10 2 9 0 190.68 7.70 -2 9 0 191.78 7.20 -2 9 0 183.68 7.50 -2 9 0 185.98 7.70 2 9 0 194.08 7.60 3 -9 0 33.60 3.00 3 -9 0 30.00 1.60 -3 -9 0 34.50 2.30 -3 -9 0 29.90 2.60 -3 -9 0 28.40 1.90 3 -9 0 28.90 3.00 -3 -9 0 28.70 3.10 3 -9 0 31.30 3.50 -3 9 0 32.70 3.30 3 9 0 33.00 3.50 -3 9 0 34.10 3.10 -3 9 0 35.50 3.50 -3 9 0 34.20 3.70 -3 9 0 34.00 3.00 -3 9 0 33.40 3.50 3 9 0 26.20 3.00 -3 9 0 28.80 1.60 3 9 0 31.40 2.20 3 9 0 28.10 1.90 3 9 0 32.60 3.50 3 9 0 32.70 3.80 -4 -9 0 267.67 9.80 4 -9 0 251.67 10.70 4 -9 0 260.17 11.20 4 -9 0 248.98 10.50 -4 -9 0 253.57 10.90 -4 -9 0 274.67 10.40 -4 9 0 260.17 10.50 4 9 0 260.57 11.00 -4 9 0 271.17 11.00 4 9 0 235.88 8.80 4 9 0 248.58 8.90 4 9 0 254.57 10.60 4 9 0 249.08 9.60 -4 9 0 262.27 11.10 4 9 0 260.77 10.90 -4 9 0 275.27 11.00 -4 9 0 275.37 11.40 4 9 0 266.37 11.30 -4 9 0 253.27 10.50 -5 -9 0 363.06 14.60 -5 -9 0 353.76 13.70 5 -9 0 339.97 14.10 -5 -9 0 349.07 13.00 5 -9 0 345.57 14.70 5 -9 0 343.17 13.80 -5 9 0 359.06 14.60 -5 9 0 327.87 13.90 5 9 0 362.96 14.10 5 9 0 338.07 14.20 5 9 0 351.66 14.60 -5 9 0 351.26 14.20 -5 9 0 336.27 14.50 -5 9 0 344.87 14.40 5 9 0 348.17 14.90 5 9 0 336.77 12.80 6 -9 0 1.10 3.10 -6 -9 0 -2.10 2.40 -6 -9 0 -0.30 3.10 6 -9 0 -4.50 3.10 -6 -9 0 4.50 2.30 6 -9 0 -3.00 2.70 6 9 0 2.50 3.80 6 9 0 2.70 3.20 -6 9 0 -0.70 3.20 -6 9 0 0.40 2.80 6 9 0 0.20 2.70 6 9 0 -4.40 3.10 -6 9 0 0.50 3.10 -6 9 0 -4.60 3.00 7 -9 0 11.30 4.00 -7 -9 0 10.40 4.70 -7 -9 0 10.50 3.80 7 -9 0 8.20 3.70 -7 -9 0 14.30 3.00 7 -9 0 19.40 4.40 7 -9 0 8.70 4.40 -7 9 0 13.10 4.00 7 9 0 13.40 4.60 -7 9 0 10.70 4.40 -7 9 0 20.10 4.80 -7 9 0 11.40 4.50 7 9 0 17.10 4.20 7 9 0 6.10 4.00 7 9 0 11.60 5.00 0 -10 0 988.80 33.20 0 -10 0 982.20 33.60 0 -10 0 1025.30 33.70 0 10 0 970.70 33.80 0 10 0 990.10 33.30 0 10 0 1020.10 33.20 0 10 0 977.60 33.10 0 10 0 980.90 33.40 0 10 0 1020.60 33.50 0 10 0 1008.10 33.30 0 10 0 998.40 33.70 1 -10 0 272.97 10.00 1 -10 0 292.77 10.40 -1 -10 0 286.37 9.90 -1 -10 0 279.37 10.70 1 -10 0 266.17 10.50 -1 -10 0 274.97 10.30 1 -10 0 275.37 10.40 -1 -10 0 294.07 9.90 -1 -10 0 269.47 9.80 -1 10 0 275.67 10.50 1 10 0 291.37 10.80 1 10 0 287.97 10.60 -1 10 0 273.97 9.90 1 10 0 282.97 10.40 -1 10 0 281.87 10.30 1 10 0 276.37 9.80 -1 10 0 285.37 10.80 -1 10 0 279.07 11.00 -1 10 0 289.37 10.60 1 10 0 283.47 10.60 -1 10 0 284.67 10.50 1 10 0 285.57 10.60 2 -10 0 34.80 3.30 -2 -10 0 30.90 2.20 2 -10 0 37.70 2.10 -2 -10 0 36.00 1.80 -2 -10 0 36.80 3.00 -2 -10 0 35.80 2.50 2 -10 0 38.40 2.90 -2 -10 0 35.90 2.20 -2 -10 0 37.40 1.80 2 -10 0 37.30 3.10 2 -10 0 35.30 2.10 -2 -10 0 33.30 3.20 -2 10 0 38.40 3.10 -2 10 0 35.20 3.50 2 10 0 36.00 3.40 2 10 0 37.50 3.40 -2 10 0 37.10 3.40 -2 10 0 36.70 3.40 -2 10 0 34.70 3.50 2 10 0 37.10 3.00 -2 10 0 41.60 3.30 2 10 0 36.70 2.50 -2 10 0 38.10 2.70 2 10 0 38.70 3.70 3 -10 0 177.58 7.40 -3 -10 0 174.18 6.70 3 -10 0 176.08 6.20 3 -10 0 173.28 8.20 -3 -10 0 177.88 7.20 3 -10 0 171.88 7.60 -3 -10 0 187.08 8.00 -3 -10 0 177.38 6.60 3 10 0 178.18 8.30 -3 10 0 178.78 7.90 -3 10 0 173.38 8.30 3 10 0 173.48 6.70 -3 10 0 185.98 8.00 3 10 0 180.48 8.10 3 10 0 188.98 8.00 3 10 0 180.68 7.70 -3 10 0 170.38 7.60 -3 10 0 186.08 8.10 -3 10 0 179.68 7.40 3 10 0 176.38 6.60 -4 -10 0 13.60 2.40 -4 -10 0 13.20 3.00 4 -10 0 7.70 2.90 4 -10 0 13.70 3.00 4 -10 0 11.60 2.70 -4 -10 0 12.90 2.00 -4 10 0 12.60 3.00 -4 10 0 14.70 3.00 4 10 0 14.10 1.90 4 10 0 14.30 3.20 4 10 0 13.70 2.80 -4 10 0 17.40 3.10 4 10 0 14.20 3.30 4 10 0 20.80 3.90 -4 10 0 13.20 2.70 -4 10 0 7.60 2.90 -5 -10 0 146.59 8.40 5 -10 0 160.18 8.00 5 -10 0 144.69 8.00 -5 -10 0 156.98 7.60 -5 -10 0 149.59 6.80 5 -10 0 156.08 8.70 5 10 0 158.68 8.60 -5 10 0 163.58 8.80 -5 10 0 155.48 8.00 5 10 0 152.18 8.80 -5 10 0 166.28 8.90 5 10 0 157.18 7.90 5 10 0 152.98 6.60 -5 10 0 145.29 8.00 5 10 0 151.28 8.20 -5 10 0 145.99 8.40 -6 -10 0 -0.10 2.60 -6 -10 0 5.50 3.50 6 -10 0 7.60 3.90 6 -10 0 4.90 3.00 -6 -10 0 2.00 2.30 6 -10 0 2.20 3.00 -6 10 0 2.00 3.40 6 10 0 3.50 2.80 6 10 0 5.90 3.60 6 10 0 -0.20 3.30 6 10 0 2.00 3.80 -6 10 0 2.60 3.10 -6 10 0 5.20 3.60 -6 10 0 4.80 3.30 -7 -10 0 3.50 2.30 7 -10 0 2.70 3.60 -7 -10 0 -0.60 3.80 7 -10 0 -3.30 3.40 7 -10 0 -6.40 3.30 -7 -10 0 1.10 3.20 7 -10 0 5.90 3.70 7 10 0 1.40 4.00 7 10 0 3.30 3.80 7 10 0 6.20 4.50 -7 10 0 -2.70 3.60 -7 10 0 4.90 3.60 -7 10 0 -0.90 3.70 7 10 0 10.00 4.20 -7 10 0 3.10 3.80 0 -11 0 7.80 2.20 0 -11 0 7.10 1.50 0 11 0 7.90 1.40 0 11 0 9.80 1.80 0 11 0 7.50 1.60 0 11 0 8.80 2.00 0 11 0 10.00 2.00 0 11 0 8.80 2.10 0 11 0 5.80 1.40 0 11 0 9.50 1.60 1 -11 0 41.70 2.80 -1 -11 0 47.30 2.60 1 -11 0 42.20 3.10 -1 -11 0 43.60 3.00 1 -11 0 47.90 3.30 -1 -11 0 46.40 3.60 -1 -11 0 47.90 2.70 1 -11 0 47.20 3.30 1 11 0 41.60 3.40 1 11 0 45.30 3.20 1 11 0 48.60 3.20 -1 11 0 40.00 3.30 -1 11 0 42.00 3.30 1 11 0 50.29 3.50 -1 11 0 45.50 3.60 -1 11 0 42.30 3.20 -1 11 0 38.10 3.40 -1 11 0 41.30 2.70 1 11 0 50.69 2.60 -1 11 0 44.30 3.40 1 11 0 46.00 3.30 2 -11 0 131.59 6.20 -2 -11 0 137.39 5.00 -2 -11 0 137.39 5.30 -2 -11 0 136.59 5.30 2 -11 0 137.29 5.90 -2 -11 0 133.69 6.10 2 -11 0 138.19 5.20 -2 -11 0 135.99 5.60 -2 -11 0 130.89 6.40 2 -11 0 129.89 5.10 -2 -11 0 130.59 4.90 2 -11 0 139.79 6.10 -2 11 0 133.69 6.80 2 11 0 135.09 5.60 2 11 0 134.59 6.20 -2 11 0 141.79 6.20 -2 11 0 137.99 6.50 -2 11 0 136.59 6.10 2 11 0 136.39 6.40 2 11 0 137.89 6.40 -2 11 0 137.19 6.30 -2 11 0 135.69 6.60 2 11 0 132.09 6.60 -2 11 0 134.49 5.60 3 -11 0 46.70 3.80 3 -11 0 43.80 2.10 3 -11 0 42.80 2.10 -3 -11 0 39.10 3.70 -3 -11 0 46.00 3.20 3 -11 0 49.99 4.20 -3 -11 0 47.70 2.50 3 -11 0 46.20 3.60 -3 -11 0 49.30 2.70 3 11 0 46.20 4.20 3 11 0 47.60 3.90 -3 11 0 49.30 4.40 3 11 0 45.90 2.60 -3 11 0 49.00 3.50 -3 11 0 42.20 3.50 -3 11 0 47.50 4.00 -3 11 0 41.20 3.80 3 11 0 48.10 2.60 3 11 0 46.60 3.70 3 11 0 48.40 4.20 -3 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31.30 5.70 7 11 0 25.90 6.10 7 11 0 27.90 5.50 -7 11 0 19.80 5.30 -7 11 0 14.40 4.20 -7 11 0 15.40 4.90 7 11 0 28.50 5.90 7 11 0 21.10 4.70 -7 11 0 16.50 4.70 0 -12 0 911.41 31.50 0 -12 0 964.80 32.10 0 -12 0 922.41 31.90 0 12 0 932.11 31.60 0 12 0 947.91 31.40 0 12 0 982.80 31.60 0 12 0 904.41 31.30 0 12 0 945.31 31.80 0 12 0 927.81 32.20 0 12 0 927.21 32.00 0 12 0 938.31 31.70 1 -12 0 15.40 2.50 -1 -12 0 11.90 2.30 -1 -12 0 11.50 1.90 1 -12 0 16.50 2.00 1 -12 0 15.70 2.20 1 -12 0 14.50 2.20 1 -12 0 13.40 2.10 -1 -12 0 14.50 1.70 1 12 0 12.40 2.30 -1 12 0 12.40 2.00 1 12 0 19.40 2.30 1 12 0 14.30 1.60 1 12 0 13.00 2.30 -1 12 0 14.00 2.20 -1 12 0 15.00 1.70 1 12 0 15.50 2.60 -1 12 0 14.90 2.60 -1 12 0 14.10 2.20 1 12 0 16.10 2.30 -1 12 0 14.80 2.70 -2 -12 0 171.58 6.40 -2 -12 0 191.58 6.80 2 -12 0 187.28 7.70 -2 -12 0 185.78 6.50 -2 -12 0 182.88 7.60 2 -12 0 158.28 7.60 2 -12 0 183.98 7.40 -2 -12 0 183.68 6.80 -2 -12 0 182.28 7.10 2 -12 0 171.78 6.70 -2 12 0 171.88 7.90 2 12 0 184.58 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70.29 7.80 0 -24 0 152.18 7.20 0 -24 0 144.59 8.80 0 -24 0 143.09 8.60 0 -24 0 153.28 8.30 0 24 0 147.49 8.90 0 24 0 130.19 7.70 0 24 0 142.29 7.70 0 24 0 146.19 7.30 0 24 0 160.48 9.10 -1 -24 0 14.50 4.20 1 -24 0 19.70 3.70 -1 -24 0 18.50 2.80 1 -24 0 18.10 4.30 -1 -24 0 15.40 4.60 -1 -24 0 15.20 3.00 1 -24 0 20.20 4.00 -1 -24 0 14.90 3.10 -1 24 0 10.10 3.90 1 24 0 19.30 3.40 -1 24 0 21.00 3.90 1 24 0 22.80 4.30 1 24 0 20.20 4.20 -1 24 0 18.70 4.80 -1 24 0 16.90 3.70 -1 24 0 15.80 2.90 1 24 0 24.50 4.60 -1 24 0 17.50 3.40 -2 -24 0 122.49 9.10 -2 -24 0 134.59 7.50 2 -24 0 128.29 8.10 2 -24 0 131.89 7.90 -2 -24 0 131.89 6.40 -2 -24 0 138.19 6.30 -2 -24 0 128.49 8.90 2 -24 0 120.39 6.90 -2 -24 0 127.59 6.20 -2 24 0 142.89 9.60 -2 24 0 124.89 7.90 -2 24 0 135.19 8.60 2 24 0 124.69 8.50 2 24 0 122.59 6.30 -2 24 0 130.29 6.70 2 24 0 125.89 8.40 2 24 0 134.79 7.80 -2 24 0 138.89 8.90 -2 24 0 135.79 8.40 -3 -24 0 7.30 1.40 -3 -24 0 5.60 3.00 3 -24 0 -2.60 3.80 -3 -24 0 3.10 2.00 3 -24 0 6.30 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141.39 6.40 2 -9 -3 147.39 6.70 -2 -9 3 130.19 5.50 -2 -9 3 143.59 5.60 -2 -9 3 142.09 5.90 -2 -9 3 130.59 5.30 -2 -9 3 152.08 6.40 2 -9 -3 140.89 6.30 -2 9 3 135.59 6.40 -2 9 3 129.69 6.30 -2 9 3 149.09 6.50 -2 9 3 136.09 5.90 2 9 -3 141.29 6.40 2 9 -3 139.39 5.40 2 9 -3 132.69 6.20 2 9 -3 143.39 6.10 2 9 -3 145.39 6.50 2 9 -3 144.69 6.50 -2 9 3 142.29 6.40 -2 9 3 133.49 6.70 -1 -9 3 484.05 17.40 -1 -9 3 485.95 17.50 -1 -9 3 500.75 17.60 1 -9 -3 502.45 17.50 1 -9 -3 507.15 17.80 1 -9 -3 510.65 17.70 -1 -9 3 478.85 17.40 1 -9 -3 479.65 17.20 1 -9 -3 469.45 16.80 -1 9 3 490.15 17.40 -1 9 3 511.95 17.30 1 9 -3 498.45 17.60 1 9 -3 506.15 17.60 1 9 -3 485.05 17.50 -1 9 3 493.15 18.00 -1 9 3 496.65 17.70 1 9 -3 507.25 17.10 1 9 -3 504.95 17.30 -1 9 3 510.85 16.80 1 9 -3 506.65 17.40 -1 9 3 505.15 17.80 0 -9 3 39.70 2.50 0 -9 3 38.50 3.10 0 -9 3 36.80 2.90 0 -9 -3 40.50 3.60 0 -9 -3 44.10 2.10 0 -9 -3 38.40 2.30 0 -9 -3 42.40 3.40 0 -9 -3 43.20 3.60 0 9 3 35.70 2.10 0 9 -3 40.90 2.50 0 9 -3 38.90 2.70 0 9 3 36.40 2.50 0 9 3 39.80 2.30 0 9 -3 35.40 3.10 0 9 3 38.40 3.40 0 9 -3 41.90 2.60 0 9 -3 35.90 3.00 0 9 -3 40.80 3.30 0 9 -3 39.70 3.30 0 9 -3 40.00 3.20 0 9 3 35.90 3.00 1 -9 3 446.86 14.60 -1 -9 -3 450.05 15.90 1 -9 3 414.46 15.80 1 -9 3 422.66 14.60 -1 -9 -3 438.86 15.10 -1 -9 -3 416.86 14.60 1 -9 3 411.56 14.60 1 -9 3 429.56 14.70 -1 -9 -3 442.66 15.70 1 -9 3 421.76 15.70 1 -9 3 436.66 14.70 -1 9 -3 430.66 15.60 1 9 3 425.26 15.90 -1 9 -3 412.26 14.70 -1 9 -3 440.66 16.10 -1 9 -3 469.25 15.80 1 9 3 418.06 14.70 1 9 3 471.25 15.80 -1 9 -3 438.46 15.70 1 9 3 409.96 15.70 -1 9 -3 454.25 15.80 -2 -9 -3 17.40 2.80 2 -9 3 16.60 2.70 2 -9 3 15.40 1.60 -2 -9 -3 16.70 2.30 2 -9 3 16.20 1.80 -2 -9 -3 17.80 1.60 2 -9 3 14.70 1.60 -2 -9 -3 20.00 2.70 -2 9 -3 16.60 1.70 2 9 3 16.20 2.60 -2 9 -3 18.70 2.60 2 9 3 20.30 3.00 2 9 3 19.00 1.50 -2 9 -3 14.90 2.40 2 9 3 17.60 2.90 -2 9 -3 14.80 2.50 2 9 3 15.50 2.40 -2 9 -3 19.20 2.70 3 -9 3 91.39 6.10 3 -9 3 96.59 6.10 -3 -9 -3 95.79 4.40 -3 -9 -3 99.89 5.60 -3 -9 -3 92.09 5.70 3 -9 3 92.69 4.40 3 -9 3 89.59 4.20 -3 9 -3 93.69 4.40 3 9 3 101.09 5.80 -3 9 -3 97.69 5.80 3 9 3 87.39 5.40 3 9 3 97.19 5.10 -3 9 -3 88.39 5.40 3 9 3 89.39 5.40 -3 9 -3 87.69 5.60 -3 9 -3 101.69 5.70 4 -9 3 4.20 2.10 -4 -9 -3 5.00 2.90 4 -9 3 5.10 3.20 -4 -9 -3 6.10 3.10 4 -9 3 1.00 1.80 -4 -9 -3 2.00 1.20 -4 -9 -3 2.70 1.90 4 -9 3 4.80 3.00 -4 9 -3 1.70 2.70 4 9 3 -0.10 2.60 -4 9 -3 2.50 2.60 4 9 3 5.20 2.20 -4 9 -3 -0.30 2.40 -4 9 -3 6.50 1.90 4 9 3 5.20 1.20 4 9 3 4.90 2.90 4 9 3 5.10 2.80 -4 9 -3 1.80 2.60 5 -9 3 14.50 4.20 -5 -9 -3 24.40 4.60 -5 -9 -3 23.80 2.40 5 -9 3 15.60 3.10 -5 -9 -3 17.20 3.20 5 -9 3 20.90 2.90 -5 -9 -3 22.30 4.30 5 -9 3 21.00 4.60 5 9 3 23.30 4.30 -5 9 -3 36.80 3.80 -5 9 -3 21.60 4.10 5 9 3 27.50 4.70 -5 9 -3 17.50 4.10 -5 9 -3 19.20 3.70 5 9 3 28.90 4.50 5 9 3 28.80 3.30 -5 9 -3 24.40 4.30 6 -9 3 -0.10 4.10 -6 -9 -3 3.40 3.80 6 -9 3 -1.00 3.60 -6 -9 -3 1.00 2.00 6 -9 3 -0.20 2.60 6 -9 3 1.00 2.70 -6 -9 -3 -5.20 3.50 -6 -9 -3 -1.50 2.60 -6 9 -3 1.50 3.60 6 9 3 1.30 3.30 -6 9 -3 0.70 3.80 -6 9 -3 -6.60 2.70 -6 9 -3 5.40 3.80 6 9 3 1.40 3.60 6 9 3 -0.60 3.80 6 9 3 2.70 2.40 7 -10 -3 61.19 4.10 -7 -10 3 64.49 5.60 -7 -10 3 62.39 6.50 -7 -10 3 77.59 7.80 7 -10 -3 62.09 6.90 7 -10 -3 60.99 6.40 -7 -10 3 55.99 3.70 7 -10 -3 61.99 6.80 -7 10 3 63.59 6.50 -7 10 3 55.49 6.40 -7 10 3 66.19 6.50 -7 10 3 65.79 7.30 7 10 -3 66.79 7.10 -7 10 3 53.29 6.60 7 10 -3 55.29 5.30 7 10 -3 66.29 7.40 7 10 -3 58.89 6.40 6 -10 -3 7.80 2.30 -6 -10 3 13.20 3.40 6 -10 -3 5.90 3.60 6 -10 -3 16.00 4.30 -6 -10 3 7.10 3.60 6 -10 -3 8.90 3.50 -6 -10 3 9.10 2.80 -6 -10 3 13.60 2.00 -6 10 3 0.60 2.80 -6 10 3 5.70 3.60 -6 10 3 6.30 3.80 6 10 -3 5.40 3.50 6 10 -3 6.70 4.20 6 10 -3 12.20 4.20 -6 10 3 8.70 3.50 -6 10 3 8.00 3.50 6 10 -3 8.60 2.50 5 -10 -3 100.19 6.60 -5 -10 3 110.29 6.60 5 -10 -3 106.59 7.20 -5 -10 3 116.79 7.20 -5 -10 3 112.19 6.10 5 -10 -3 110.09 5.50 -5 -10 3 104.39 5.00 5 -10 -3 114.89 7.00 5 10 -3 101.69 6.90 5 10 -3 105.09 5.40 5 10 -3 109.79 7.40 -5 10 3 109.09 6.90 5 10 -3 107.49 7.10 -5 10 3 112.99 6.80 -5 10 3 106.89 6.90 -5 10 3 116.29 7.20 -5 10 3 102.79 5.80 4 -10 -3 10.00 3.20 -4 -10 3 15.60 3.00 -4 -10 3 13.70 2.70 4 -10 -3 14.20 3.10 4 -10 -3 15.70 2.40 -4 -10 3 13.10 2.60 4 -10 -3 13.50 2.90 -4 -10 3 17.80 2.10 4 10 -3 15.00 3.30 -4 10 3 13.70 3.10 4 10 -3 12.60 3.10 -4 10 3 18.50 3.30 4 10 -3 10.30 2.10 4 10 -3 16.40 2.10 -4 10 3 15.00 2.90 -4 10 3 11.10 2.10 -4 10 3 13.40 2.90 4 10 -3 11.20 3.40 3 -10 -3 51.59 4.10 -3 -10 3 60.49 3.80 3 -10 -3 53.79 4.40 -3 -10 3 60.19 4.00 -3 -10 3 50.99 2.30 -3 -10 3 55.69 3.30 -3 -10 3 53.79 4.10 3 -10 -3 50.29 3.40 3 10 -3 56.59 4.20 3 10 -3 53.19 3.50 -3 10 3 49.30 2.90 -3 10 3 55.99 4.20 3 10 -3 55.69 3.00 -3 10 3 44.50 4.20 -3 10 3 52.89 3.80 3 10 -3 47.30 4.30 -3 10 3 49.90 4.00 3 10 -3 51.19 4.00 -3 10 3 41.90 3.90 2 -10 -3 1.80 2.10 -2 -10 3 1.40 1.30 -2 -10 3 0.20 1.60 2 -10 -3 2.70 1.90 -2 -10 3 3.90 1.80 -2 -10 3 2.30 1.50 2 -10 -3 1.00 1.70 2 -10 -3 1.70 1.70 -2 -10 3 2.00 1.60 -2 10 3 0.90 1.80 -2 10 3 2.10 1.80 2 10 -3 0.70 1.80 -2 10 3 2.00 1.50 -2 10 3 1.20 1.90 2 10 -3 0.00 1.90 2 10 -3 1.70 2.10 2 10 -3 1.40 1.20 2 10 -3 1.30 1.90 -2 10 3 2.60 2.10 -2 10 3 1.60 1.90 1 -10 -3 15.90 2.50 1 -10 -3 16.00 2.50 1 -10 -3 15.50 2.00 1 -10 -3 15.10 2.30 -1 -10 3 18.70 2.30 -1 -10 3 16.50 2.30 1 -10 -3 19.50 2.90 -1 -10 3 15.90 2.20 1 10 -3 17.10 2.50 -1 10 3 15.70 2.50 -1 10 3 19.50 2.30 -1 10 3 14.90 2.40 -1 10 3 18.40 1.70 -1 10 3 21.90 2.70 -1 10 3 18.30 2.10 1 10 -3 17.40 2.30 1 10 -3 20.50 2.20 1 10 -3 18.70 2.20 1 10 -3 21.20 2.50 1 10 -3 14.90 2.20 1 10 -3 19.80 2.20 0 -10 -3 32.50 3.40 0 -10 -3 31.70 1.90 0 -10 3 30.50 2.70 0 -10 -3 31.80 3.40 0 -10 -3 28.30 2.10 0 -10 3 28.10 2.90 0 -10 -3 26.30 2.90 0 -10 3 29.30 2.40 0 10 3 27.80 2.10 0 10 -3 33.60 2.60 0 10 -3 28.20 2.50 0 10 3 28.50 3.10 0 10 -3 26.40 3.00 0 10 3 28.70 3.20 0 10 -3 31.00 3.00 0 10 -3 32.00 3.10 0 10 -3 28.60 2.30 0 10 -3 33.40 2.90 0 10 -3 27.00 2.90 0 10 3 35.70 2.50 1 -10 3 85.09 3.50 -1 -10 -3 85.29 3.90 -1 -10 -3 78.49 4.50 1 -10 3 70.89 3.30 -1 -10 -3 88.69 4.90 -1 -10 -3 72.69 3.30 1 -10 3 79.99 3.60 1 -10 3 76.69 4.70 1 -10 3 70.99 3.30 1 -10 3 78.19 4.50 1 -10 3 80.19 3.60 -1 -10 -3 89.19 4.80 1 10 3 80.19 4.80 -1 10 -3 81.99 4.50 -1 10 -3 81.59 4.60 -1 10 -3 80.49 4.50 -1 10 -3 77.09 4.70 -1 10 -3 70.79 3.40 1 10 3 77.99 4.50 1 10 3 92.29 4.80 -1 10 -3 75.39 4.40 1 10 3 74.69 3.40 2 -10 3 232.58 8.50 -2 -10 -3 249.88 9.50 2 -10 3 230.48 8.60 2 -10 3 245.18 10.20 -2 -10 -3 243.38 9.90 -2 -10 -3 237.78 8.20 -2 10 -3 213.08 9.50 2 10 3 233.08 8.30 -2 10 -3 252.37 9.90 2 10 3 237.48 9.80 -2 10 -3 236.58 9.80 2 10 3 241.88 10.00 2 10 3 242.58 10.10 -2 10 -3 245.98 10.00 -2 10 -3 234.58 8.70 2 10 3 226.58 9.50 -3 -10 -3 3.00 1.40 -3 -10 -3 -0.30 2.40 3 -10 3 -0.70 1.50 3 -10 3 2.50 1.40 3 -10 3 5.00 2.90 3 -10 3 -0.60 2.60 -3 -10 -3 1.10 2.30 -3 10 -3 1.40 2.10 3 10 3 -0.30 2.40 -3 10 -3 1.20 2.20 -3 10 -3 2.40 1.60 3 10 3 3.40 1.90 -3 10 -3 1.30 2.20 3 10 3 2.90 2.40 -3 10 -3 4.40 2.40 3 10 3 2.40 2.50 -4 -10 -3 94.69 6.40 4 -10 3 92.29 4.80 4 -10 3 99.59 6.90 4 -10 3 92.69 5.00 4 -10 3 87.39 6.70 -4 -10 -3 80.89 6.10 -4 -10 -3 90.49 5.00 4 10 3 86.89 6.00 -4 10 -3 81.49 6.10 -4 10 -3 92.79 6.50 -4 10 -3 90.99 6.20 4 10 3 91.89 5.20 -4 10 -3 94.99 4.90 -4 10 -3 95.49 6.30 4 10 3 89.79 6.30 4 10 3 94.99 6.40 -5 -10 -3 12.50 3.90 5 -10 3 13.70 4.40 -5 -10 -3 5.00 3.70 5 -10 3 14.30 4.40 5 -10 3 17.50 3.00 5 -10 3 10.10 2.50 -5 -10 -3 13.50 3.00 -5 10 -3 7.00 3.30 5 10 3 12.50 3.80 5 10 3 14.00 2.70 -5 10 -3 21.60 4.40 -5 10 -3 10.60 3.60 -5 10 -3 13.80 4.00 5 10 3 17.70 4.30 5 10 3 12.70 1.70 5 10 3 15.90 3.90 -6 -10 -3 -7.10 3.40 6 -10 3 4.40 3.00 6 -10 3 2.60 4.40 6 -10 3 0.40 3.90 6 -10 3 -0.60 2.50 -6 -10 -3 -0.20 3.90 -6 -10 -3 -2.90 2.60 -6 -10 -3 4.00 1.90 -6 10 -3 0.40 3.70 -6 10 -3 1.80 3.00 6 10 3 2.20 3.80 -6 10 -3 0.70 3.80 6 10 3 5.20 3.80 6 10 3 -1.50 3.90 -6 10 -3 5.00 3.90 6 10 3 -0.70 2.30 7 -11 -3 3.40 1.90 7 -11 -3 1.50 4.00 -7 -11 3 1.00 1.40 -7 -11 3 3.00 3.20 7 -11 -3 0.50 3.20 -7 -11 3 1.40 3.70 7 -11 -3 -1.10 3.90 -7 -11 3 3.00 2.70 7 11 -3 -2.60 4.00 -7 11 3 0.00 3.70 7 11 -3 -5.20 3.50 -7 11 3 -0.90 3.40 -7 11 3 4.60 3.70 -7 11 3 -0.60 3.40 7 11 -3 5.00 4.20 -7 11 3 -4.50 3.50 7 11 -3 1.80 2.70 -6 -11 3 -3.20 2.50 6 -11 -3 -0.50 3.50 -6 -11 3 0.70 3.10 6 -11 -3 0.00 3.10 6 -11 -3 2.30 3.50 6 -11 -3 6.50 2.20 -6 -11 3 4.00 1.60 -6 -11 3 1.00 2.30 -6 11 3 -3.10 3.00 6 11 -3 0.10 3.80 -6 11 3 0.90 3.30 6 11 -3 1.20 2.20 -6 11 3 0.70 2.80 -6 11 3 2.60 3.00 6 11 -3 -4.30 3.00 6 11 -3 2.40 3.50 -6 11 3 -1.10 3.10 -5 -11 3 13.40 3.70 5 -11 -3 21.10 4.40 -5 -11 3 18.10 2.20 5 -11 -3 20.10 2.80 5 -11 -3 18.30 4.00 -5 -11 3 19.40 3.40 5 -11 -3 14.10 3.50 -5 -11 3 20.40 3.10 5 11 -3 17.40 3.90 -5 11 3 14.60 3.50 5 11 -3 18.20 3.70 -5 11 3 18.90 3.90 -5 11 3 14.90 3.40 5 11 -3 14.20 3.60 -5 11 3 18.50 3.10 5 11 -3 16.60 2.50 -5 11 3 18.00 3.80 -4 -11 3 137.99 7.40 -4 -11 3 137.89 6.00 -4 -11 3 138.69 7.10 4 -11 -3 155.08 7.90 4 -11 -3 143.89 6.30 4 -11 -3 143.39 7.50 -4 -11 3 136.79 6.70 4 -11 -3 141.79 7.40 4 11 -3 139.69 6.50 -4 11 3 154.98 7.80 4 11 -3 141.09 7.60 -4 11 3 150.88 7.60 4 11 -3 139.29 7.60 4 11 -3 135.89 7.80 -4 11 3 143.19 7.30 -4 11 3 134.59 6.20 -4 11 3 145.59 7.70 4 11 -3 140.09 6.10 3 -11 -3 16.20 2.40 -3 -11 3 11.30 1.20 -3 -11 3 13.30 1.40 -3 -11 3 13.90 1.90 -3 -11 3 10.60 2.50 -3 -11 3 14.90 2.50 -3 -11 3 16.20 2.40 3 -11 -3 12.20 2.80 3 -11 -3 11.90 2.90 -3 11 3 17.60 2.50 -3 11 3 9.10 2.70 -3 11 3 11.30 2.60 3 11 -3 17.10 1.90 -3 11 3 13.70 1.70 3 11 -3 14.50 3.00 3 11 -3 13.20 2.70 -3 11 3 12.40 2.50 3 11 -3 15.00 2.90 3 11 -3 9.80 1.90 -3 11 3 14.10 2.90 2 -11 -3 3.90 2.00 -2 -11 3 6.40 1.90 -2 -11 3 5.50 1.50 2 -11 -3 2.60 1.70 -2 -11 3 4.30 2.10 2 -11 -3 5.00 2.20 -2 -11 3 1.90 1.50 -2 -11 3 4.30 1.70 -2 -11 3 6.90 1.80 2 -11 -3 2.70 1.80 -2 11 3 4.00 2.30 2 11 -3 7.30 2.10 -2 11 3 7.50 2.10 -2 11 3 5.70 2.00 2 11 -3 8.70 2.40 2 11 -3 1.60 2.00 -2 11 3 5.20 2.00 -2 11 3 4.70 1.60 2 11 -3 5.10 2.20 -2 11 3 7.20 2.20 2 11 -3 6.60 1.40 1 -11 -3 1915.71 63.19 1 -11 -3 1948.01 62.79 -1 -11 3 1878.51 62.79 -1 -11 3 1876.71 62.69 1 -11 -3 1814.82 62.49 -1 -11 3 1943.41 62.79 1 -11 -3 1882.21 62.89 1 11 -3 1857.91 62.39 -1 11 3 1838.02 62.99 1 11 -3 1899.81 62.69 -1 11 3 1926.81 61.99 1 11 -3 1874.71 62.79 1 11 -3 1836.92 62.69 -1 11 3 1898.21 63.39 1 11 -3 1933.51 62.59 -1 11 3 1928.91 62.49 1 11 -3 1878.41 62.59 -1 11 3 1871.11 63.09 -1 11 3 1907.71 62.69 1 11 -3 1907.71 62.89 1 11 -3 1851.31 62.79 0 -11 -3 263.77 10.30 0 -11 3 271.17 9.80 0 -11 -3 263.17 10.50 0 -11 -3 254.87 9.30 0 -11 -3 266.37 9.10 0 -11 -3 253.57 9.10 0 -11 -3 274.37 10.70 0 -11 3 251.67 10.10 0 -11 3 263.27 10.10 0 11 3 248.78 10.40 0 11 -3 262.87 10.50 0 11 -3 269.27 10.30 0 11 -3 270.67 10.10 0 11 -3 268.27 10.20 0 11 3 261.97 9.70 0 11 -3 263.07 10.20 0 11 3 258.97 9.30 0 11 -3 267.67 9.60 0 11 3 257.17 10.40 0 11 -3 257.17 9.70 1 -11 3 12.80 2.10 -1 -11 -3 16.30 2.70 -1 -11 -3 10.10 1.50 -1 -11 -3 16.20 2.90 1 -11 3 15.90 1.80 -1 -11 -3 15.20 2.50 1 -11 3 18.40 1.70 1 -11 3 15.80 2.50 1 -11 3 17.40 2.50 1 -11 3 15.90 1.80 -1 -11 -3 14.10 1.80 -1 11 -3 16.30 2.90 1 11 3 17.10 2.70 1 11 3 11.40 2.50 -1 11 -3 17.00 2.40 1 11 3 13.50 1.50 1 11 3 16.30 2.60 -1 11 -3 16.10 1.70 -1 11 -3 12.90 2.30 -1 11 -3 16.00 2.50 -1 11 -3 12.00 2.20 -2 -11 -3 45.60 4.20 -2 -11 -3 44.80 3.40 2 -11 3 42.50 2.70 2 -11 3 48.70 4.30 2 -11 3 43.20 2.60 -2 11 -3 47.90 4.20 -2 11 -3 48.80 4.00 2 11 3 49.50 4.00 -2 11 -3 44.80 3.90 2 11 3 49.80 4.00 2 11 3 46.20 3.50 -2 11 -3 48.60 3.80 -2 11 -3 48.30 4.50 2 11 3 46.50 4.20 3 -11 3 14.80 2.00 -3 -11 -3 9.40 3.10 -3 -11 -3 16.20 1.90 3 -11 3 17.00 2.20 3 -11 3 17.30 3.50 -3 -11 -3 14.50 2.90 3 -11 3 16.10 3.50 -3 11 -3 10.40 2.90 3 11 3 15.90 2.60 -3 11 -3 13.40 2.90 -3 11 -3 15.80 3.00 -3 11 -3 14.30 3.00 -3 11 -3 15.90 2.20 3 11 3 12.60 3.30 3 11 3 15.10 3.10 3 11 3 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0.90 0 -5 -4 6.00 1.60 0 -5 -4 7.60 1.40 0 -5 -4 7.00 2.10 0 -5 -4 5.80 1.80 0 -5 -4 6.50 1.20 0 -5 4 8.10 1.90 0 -5 4 7.10 1.60 0 5 -4 5.00 0.80 0 5 4 9.60 1.60 0 5 4 6.10 1.00 0 5 4 8.10 1.80 0 5 -4 4.60 0.70 0 5 4 5.50 1.30 0 5 -4 5.70 1.70 0 5 -4 6.50 1.60 0 5 -4 6.20 1.60 0 5 4 8.30 1.30 0 5 4 6.00 0.90 0 5 4 7.50 2.20 0 5 4 7.70 1.90 1 -5 4 329.37 13.10 -1 -5 -4 370.56 12.90 -1 -5 -4 347.27 12.90 -1 -5 -4 372.96 13.20 1 -5 4 346.37 12.30 -1 -5 -4 371.56 12.80 -1 -5 -4 378.86 12.20 1 -5 4 377.66 13.70 1 -5 4 334.67 13.00 1 5 4 371.06 12.80 1 5 4 356.26 13.30 1 5 4 353.76 12.40 1 5 4 321.17 13.20 -1 5 -4 369.86 13.20 -1 5 -4 346.27 13.10 1 5 4 361.16 12.20 -1 5 -4 359.86 13.10 -1 5 -4 367.56 13.10 1 5 4 361.26 12.20 1 5 4 349.07 12.10 -1 5 -4 333.07 12.30 -2 -5 -4 81.89 4.30 2 -5 4 79.69 3.10 2 -5 4 76.49 3.00 -2 -5 -4 90.09 4.70 2 -5 4 75.99 4.90 2 -5 4 83.69 5.30 2 -5 4 72.89 3.30 2 -5 4 73.09 4.50 -2 -5 -4 84.79 3.80 -2 -5 -4 84.99 4.60 2 5 4 68.79 4.60 2 5 4 81.29 4.30 2 5 4 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14 -4 18.90 4.60 5 -14 -4 50.79 5.40 -5 -14 4 40.30 3.40 5 -14 -4 41.10 5.30 -5 -14 4 42.50 4.50 -5 -14 4 49.00 5.60 -5 -14 4 46.20 4.80 5 -14 -4 40.10 4.00 5 -14 -4 49.30 5.40 -5 14 4 37.70 4.90 5 14 -4 42.60 5.50 -5 14 4 48.30 5.60 -5 14 4 44.00 5.10 5 14 -4 41.40 3.40 5 14 -4 40.30 5.50 5 14 -4 38.10 5.20 -5 14 4 38.10 3.60 -5 14 4 45.90 5.50 -4 -14 4 66.29 4.20 -4 -14 4 65.39 4.80 -4 -14 4 67.09 5.50 4 -14 -4 67.99 6.00 4 -14 -4 63.09 5.60 -4 -14 4 59.59 5.50 4 -14 -4 61.59 4.70 -4 14 4 62.39 3.60 4 14 -4 62.49 5.70 -4 14 4 65.69 5.60 4 14 -4 74.09 5.80 -4 14 4 74.59 6.10 -4 14 4 61.69 5.20 4 14 -4 68.99 3.80 -4 14 4 60.79 5.80 4 14 -4 61.09 5.50 -4 14 4 61.09 5.40 -3 -14 4 38.40 3.60 -3 -14 4 48.70 4.40 -3 -14 4 51.09 4.20 -3 -14 4 42.50 3.10 3 -14 -4 44.80 4.10 3 -14 -4 43.70 4.60 3 -14 -4 50.49 5.00 -3 -14 4 46.00 4.70 -3 14 4 46.50 4.50 3 14 -4 43.40 4.30 -3 14 4 46.20 4.50 -3 14 4 46.50 4.60 3 14 -4 54.79 4.90 -3 14 4 43.20 5.00 3 14 -4 45.50 3.10 -3 14 4 45.80 4.10 3 14 -4 47.30 4.50 2 -14 -4 41.00 4.20 -2 -14 4 46.00 4.00 -2 -14 4 38.00 3.50 -2 -14 4 42.40 3.90 -2 -14 4 44.30 3.70 2 -14 -4 45.80 3.90 2 -14 -4 39.00 4.10 2 -14 -4 40.90 3.90 2 14 -4 43.70 3.10 2 14 -4 43.30 4.30 -2 14 4 41.70 3.90 -2 14 4 41.30 3.30 2 14 -4 43.60 4.20 2 14 -4 46.30 4.10 -2 14 4 45.00 4.40 2 14 -4 45.50 4.10 -2 14 4 43.60 4.20 -2 14 4 37.00 3.80 -1 -14 4 73.39 4.90 1 -14 -4 71.09 5.30 -1 -14 4 78.19 4.50 1 -14 -4 72.29 5.00 -1 -14 4 72.99 4.90 1 -14 -4 70.59 4.10 1 -14 -4 67.09 4.90 -1 14 4 67.39 4.40 1 14 -4 71.39 4.70 1 14 -4 79.49 4.60 -1 14 4 71.39 5.40 1 14 -4 74.19 4.90 -1 14 4 72.79 3.50 1 14 -4 75.99 4.50 1 14 -4 71.19 4.60 -1 14 4 73.19 5.10 1 14 -4 82.19 4.40 1 14 -4 75.99 4.30 -1 14 4 79.99 4.30 0 -14 -4 219.48 9.40 0 -14 4 205.58 8.50 0 -14 -4 207.08 7.60 0 -14 -4 206.18 7.90 0 -14 -4 200.08 9.10 0 -14 -4 209.48 7.60 0 -14 4 230.88 9.20 0 -14 -4 218.18 9.60 0 -14 4 211.48 8.40 0 14 4 211.68 8.00 0 14 -4 215.88 9.20 0 14 -4 213.78 8.60 0 14 4 215.78 9.60 0 14 4 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22 4 7.50 4.00 2 22 4 2.10 3.30 -2 22 -4 2.20 3.60 -2 22 -4 2.00 3.20 2 22 4 6.00 3.60 -2 22 -4 -2.60 3.90 3 -22 4 36.90 6.10 -3 -22 -4 27.80 4.40 3 -22 4 40.10 3.90 3 -22 4 45.10 3.90 -3 -22 -4 29.00 6.00 -3 -22 -4 34.70 6.50 3 22 4 34.90 6.20 3 22 4 35.20 5.80 -3 22 -4 41.20 5.60 -3 22 -4 39.50 5.90 3 22 4 45.30 5.60 -3 22 -4 40.20 5.50 -3 22 -4 31.50 5.40 4 -22 4 19.70 3.00 -4 -22 -4 17.50 6.30 4 -22 4 24.30 6.20 -4 -22 -4 13.30 5.90 4 -22 4 13.90 2.50 4 -22 4 14.00 5.40 4 22 4 12.70 4.70 -4 22 -4 21.70 4.60 4 22 4 17.40 4.20 4 22 4 16.10 5.20 -4 22 -4 11.40 4.50 -4 22 -4 12.70 4.50 -4 22 -4 6.00 4.60 -4 -23 4 3.40 2.60 -4 -23 4 1.40 3.60 -4 -23 4 -1.80 1.90 -4 -23 4 0.50 2.10 4 -23 -4 0.40 2.70 4 -23 -4 -0.10 3.90 -4 -23 4 5.60 3.10 4 -23 -4 0.20 3.70 -4 23 4 -0.70 3.70 -4 23 4 -5.80 4.00 4 23 -4 -2.30 4.00 4 23 -4 5.10 2.80 4 23 -4 4.70 4.00 -4 23 4 0.50 3.80 -4 23 4 4.10 3.40 4 23 -4 4.40 4.30 -4 23 4 -0.60 3.60 -3 -23 4 55.49 4.90 3 -23 -4 63.19 7.00 -3 -23 4 52.19 4.70 3 -23 -4 59.49 6.50 3 -23 -4 57.69 5.60 -3 -23 4 54.79 6.30 -3 -23 4 52.99 5.20 -3 -23 4 66.29 6.00 -3 23 4 59.59 7.70 -3 23 4 67.29 6.90 3 23 -4 54.09 6.50 3 23 -4 51.89 5.10 3 23 -4 48.80 6.00 3 23 -4 46.30 5.90 -3 23 4 58.89 6.90 -3 23 4 54.29 6.00 -3 23 4 53.29 5.20 -2 -23 4 6.10 3.00 2 -23 -4 -0.40 3.60 2 -23 -4 9.00 3.60 -2 -23 4 0.40 2.60 -2 -23 4 0.30 2.80 2 -23 -4 2.30 4.20 2 23 -4 13.40 3.80 -2 23 4 5.80 2.30 -2 23 4 7.00 3.50 -2 23 4 1.50 3.50 -2 23 4 1.00 2.70 2 23 -4 5.00 3.10 2 23 -4 9.00 3.80 2 23 -4 0.10 3.40 -2 23 4 -0.30 3.80 -1 -23 4 77.89 6.30 1 -23 -4 73.99 7.30 1 -23 -4 90.39 6.90 -1 -23 4 79.29 6.20 1 -23 -4 73.99 6.90 1 23 -4 86.09 6.90 1 23 -4 91.29 6.30 -1 23 4 87.69 7.20 1 23 -4 86.79 6.40 -1 23 4 74.19 6.90 1 23 -4 85.59 6.30 -1 23 4 83.79 5.60 1 23 -4 77.59 6.30 -1 23 4 82.09 4.30 1 23 -4 73.39 6.30 1 23 -4 82.99 6.10 -1 23 4 90.19 6.60 0 -23 -4 243.08 10.00 0 -23 -4 258.07 12.50 0 -23 4 273.27 11.40 0 -23 4 305.07 12.70 0 -23 -4 255.37 12.70 0 -23 -4 259.27 13.10 0 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4.10 4.70 4 3 9 7.50 3.10 -7 -4 9 6.30 4.40 -7 -4 9 10.60 4.10 -7 -4 9 8.20 3.70 7 -4 -9 6.80 4.20 7 -4 -9 6.30 2.30 7 -4 -9 6.70 5.00 -7 -4 9 5.60 3.90 7 -4 -9 4.40 4.80 -7 4 9 10.10 3.90 7 4 -9 -2.30 4.10 7 4 -9 6.00 4.70 7 4 -9 10.00 5.10 -7 4 9 1.40 3.60 -7 4 9 9.60 4.20 -7 4 9 13.10 3.50 -6 -4 9 8.60 3.60 -6 -4 9 -0.50 3.40 6 -4 -9 5.60 4.00 -6 -4 9 3.90 2.00 6 -4 -9 6.10 2.10 -6 -4 9 3.80 3.40 -6 -4 9 2.00 3.70 6 -4 -9 9.10 4.40 6 -4 -9 6.40 4.20 -6 4 9 9.40 4.00 6 4 -9 8.90 4.40 6 4 -9 1.30 4.00 -6 4 9 6.30 3.70 -6 4 9 5.40 3.20 -6 4 9 3.00 3.10 6 4 -9 10.30 4.50 -6 4 9 0.50 3.20 -5 -4 9 20.40 4.10 5 -4 -9 23.90 4.90 5 -4 -9 24.70 2.60 -5 -4 9 25.70 4.70 5 -4 -9 21.10 4.60 -5 -4 9 20.00 4.00 -5 -4 9 24.50 3.30 5 -4 -9 18.80 4.50 -5 -4 9 28.00 4.70 5 4 -9 21.30 4.90 -5 4 9 22.40 4.20 -5 4 9 21.50 4.10 5 4 -9 28.20 4.60 -5 4 9 26.50 3.70 5 4 -9 21.50 4.80 -5 4 9 20.60 4.10 -5 4 9 24.40 4.50 -4 -4 9 28.10 3.80 4 -4 -9 16.40 4.10 -4 -4 9 25.00 4.10 4 -4 -9 31.60 5.00 4 -4 -9 26.40 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-1 -4 9 81.69 5.90 1 -4 -9 73.19 5.50 1 -4 -9 74.39 5.00 -1 -4 9 79.19 5.60 1 -4 -9 69.89 4.80 1 -4 -9 76.69 5.30 1 4 -9 76.89 5.50 -1 4 9 74.59 4.80 1 4 -9 74.29 4.10 1 4 -9 81.79 5.60 1 4 -9 71.09 4.20 -1 4 9 81.69 5.30 -1 4 9 70.89 5.40 -1 4 9 80.89 5.60 -1 4 9 87.39 6.50 0 -4 9 219.08 10.10 0 -4 9 199.98 9.10 0 -4 -9 184.88 8.30 0 -4 -9 190.18 8.40 0 -4 9 179.28 9.00 0 -4 -9 180.58 9.20 0 -4 9 198.88 8.70 0 -4 -9 200.78 8.20 0 -4 -9 168.88 7.90 0 4 -9 157.88 6.60 0 4 -9 177.58 8.80 0 4 9 199.98 9.90 0 4 -9 191.58 8.70 0 4 -9 182.98 6.70 0 4 9 185.28 8.00 0 4 9 189.18 8.60 0 4 -9 184.98 6.90 0 4 -9 173.68 8.90 0 4 9 187.88 8.90 0 4 -9 176.08 6.80 0 4 9 207.78 8.70 -1 -4 -9 140.99 6.80 -1 -4 -9 134.09 6.60 -1 -4 -9 127.99 7.30 -1 -4 -9 138.79 6.80 1 -4 9 136.89 7.80 -1 -4 -9 147.59 7.90 1 -4 9 136.99 7.90 -1 -4 -9 137.49 6.90 1 -4 9 146.69 8.60 1 -4 9 147.39 8.10 -1 4 -9 135.89 7.60 -1 4 -9 141.39 8.00 -1 4 -9 145.59 7.30 1 4 9 153.98 8.10 1 4 9 151.58 7.40 1 4 9 150.68 7.20 1 4 9 127.39 7.90 1 4 9 155.08 8.80 2 -4 9 27.90 4.20 2 -4 9 23.80 5.00 -2 -4 -9 19.80 3.80 -2 -4 -9 29.70 3.50 2 -4 9 29.80 5.00 -2 -4 -9 33.60 4.70 -2 -4 -9 20.00 3.10 -2 -4 -9 22.40 3.00 -2 -4 -9 21.40 3.20 2 -4 9 24.30 3.90 -2 4 -9 23.80 3.60 2 4 9 15.60 4.20 -2 4 -9 19.90 4.10 2 4 9 27.40 3.70 2 4 9 18.40 4.70 -2 4 -9 27.70 4.10 2 4 9 21.00 3.20 -3 -4 -9 7.70 3.60 3 -4 9 7.00 4.20 -3 -4 -9 3.80 2.50 -3 -4 -9 10.10 2.80 -3 -4 -9 5.60 3.40 -3 -4 -9 6.80 2.60 3 -4 9 4.50 4.40 3 -4 9 6.60 3.40 -3 -4 -9 6.40 2.60 3 -4 9 1.70 2.90 -3 4 -9 7.60 3.00 3 4 9 6.10 2.90 3 4 9 6.30 4.20 -3 4 -9 1.40 3.10 3 4 9 9.20 2.70 -3 4 -9 1.00 3.60 3 4 9 6.10 4.00 -4 -4 -9 15.30 4.60 4 -4 9 20.00 5.60 -4 -4 -9 21.20 4.50 4 -4 9 22.30 4.70 4 -4 9 14.10 4.10 4 -4 9 19.20 6.00 -4 -4 -9 18.70 3.30 -4 -4 -9 12.00 3.00 -4 -4 -9 14.00 3.50 4 4 9 18.20 3.50 -4 4 -9 17.80 4.90 4 4 9 21.30 5.40 -4 4 -9 25.50 4.60 4 4 9 20.80 5.00 4 4 9 17.00 4.00 -4 4 -9 22.70 3.40 7 -5 -9 22.40 5.30 -7 -5 9 29.20 4.80 7 -5 -9 17.10 3.00 -7 -5 9 25.90 5.10 7 -5 -9 27.30 5.50 7 -5 -9 24.10 5.40 -7 -5 9 30.40 5.30 -7 -5 9 25.70 5.70 -7 5 9 20.30 4.90 7 5 -9 27.90 6.00 -7 5 9 12.70 4.60 7 5 -9 32.10 5.80 7 5 -9 19.80 5.30 -7 5 9 22.40 4.30 -7 5 9 21.60 3.90 -7 5 9 16.90 4.60 -6 -5 9 1.10 3.50 6 -5 -9 3.60 4.00 6 -5 -9 -0.20 3.90 6 -5 -9 5.50 2.00 6 -5 -9 5.80 4.00 -6 -5 9 1.20 3.40 -6 -5 9 0.50 3.20 -6 -5 9 2.30 1.90 -6 -5 9 3.70 3.60 -6 5 9 2.60 3.30 -6 5 9 2.30 3.10 -6 5 9 1.50 2.80 -6 5 9 3.90 3.60 6 5 -9 2.20 4.10 -6 5 9 0.70 3.30 6 5 -9 3.50 3.70 6 5 -9 0.40 3.60 5 -5 -9 6.90 3.90 5 -5 -9 3.70 3.70 -5 -5 9 4.70 3.40 -5 -5 9 8.30 3.30 5 -5 -9 10.30 4.20 -5 -5 9 10.50 3.60 -5 -5 9 7.30 2.50 5 -5 -9 5.50 2.00 -5 -5 9 9.40 3.80 5 5 -9 5.90 3.50 -5 5 9 9.40 3.50 5 5 -9 5.80 4.00 -5 5 9 9.30 2.80 -5 5 9 4.90 3.20 -5 5 9 6.30 3.30 -5 5 9 6.00 3.50 5 5 -9 9.90 3.80 4 -5 -9 204.68 10.60 4 -5 -9 220.48 11.10 -4 -5 9 201.58 9.60 4 -5 -9 224.78 10.80 -4 -5 9 208.68 10.60 -4 -5 9 208.58 10.30 -4 -5 9 208.58 10.70 -4 5 9 218.48 10.80 -4 5 9 210.38 10.00 4 5 -9 206.78 10.30 4 5 -9 213.88 10.80 4 5 -9 217.08 10.20 -4 5 9 214.18 8.90 -4 5 9 224.68 10.70 -4 5 9 227.18 10.60 -4 5 9 212.48 9.20 4 5 -9 237.68 10.70 -3 -5 9 6.80 3.00 -3 -5 9 15.90 3.50 3 -5 -9 15.40 3.70 3 -5 -9 8.80 3.60 3 -5 -9 13.10 2.50 -3 -5 9 8.80 3.00 -3 -5 9 5.60 2.90 -3 5 9 13.40 3.00 -3 5 9 13.30 3.40 -3 5 9 11.10 2.50 3 5 -9 8.80 2.80 3 5 -9 9.90 3.30 3 5 -9 14.00 3.30 -3 5 9 11.40 3.30 -3 5 9 14.50 3.60 3 5 -9 9.40 3.20 2 -5 -9 300.37 13.20 2 -5 -9 309.57 11.80 -2 -5 9 288.47 11.20 2 -5 -9 311.07 12.50 -2 -5 9 311.27 13.10 -2 -5 9 308.67 11.90 -2 -5 9 307.67 13.00 2 -5 -9 319.87 13.00 -2 -5 9 310.47 12.80 -2 -5 9 304.67 13.30 2 5 -9 302.57 12.10 2 5 -9 324.07 13.10 -2 5 9 280.47 12.10 -2 5 9 317.97 12.90 2 5 -9 311.47 11.90 2 5 -9 304.57 12.80 -2 5 9 288.77 12.20 -2 5 9 320.17 12.80 -2 5 9 324.87 13.60 1 -5 -9 5.10 3.10 -1 -5 9 4.90 2.70 -1 -5 9 3.30 2.30 -1 -5 9 3.30 3.00 -1 -5 9 4.70 1.60 -1 -5 9 3.10 2.10 1 -5 -9 0.60 2.50 1 -5 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2.70 -2 -5 -9 1.20 2.20 -2 -5 -9 -0.50 2.70 -2 -5 -9 2.10 2.00 2 -5 9 -2.60 3.30 2 5 9 0.30 2.30 2 5 9 0.20 2.10 2 5 9 0.60 3.40 2 5 9 -3.00 3.10 -2 5 -9 1.30 3.10 -2 5 -9 2.00 2.80 2 5 9 -2.00 1.80 -2 5 -9 -1.60 2.40 -3 -5 -9 19.50 4.30 -3 -5 -9 18.80 4.20 -3 -5 -9 24.50 3.40 3 -5 9 23.60 4.30 3 -5 9 19.10 4.00 -3 -5 -9 20.50 3.40 3 -5 9 18.90 5.40 -3 -5 -9 23.80 3.60 3 -5 9 24.60 5.20 3 5 9 19.10 4.80 -3 5 -9 17.50 4.00 -3 5 -9 21.00 4.70 3 5 9 19.90 4.80 3 5 9 22.00 3.20 3 5 9 24.90 3.60 3 5 9 16.10 3.70 -3 5 -9 19.80 3.30 4 -5 9 56.29 7.80 4 -5 9 53.09 6.40 -4 -5 -9 65.59 7.20 -4 -5 -9 64.19 5.40 -4 -5 -9 67.09 6.70 -4 -5 -9 53.99 5.20 4 -5 9 58.19 7.90 -4 -5 -9 73.49 5.60 4 5 9 64.89 7.10 4 5 9 65.39 4.80 4 5 9 68.49 7.60 -4 5 -9 60.19 6.40 -4 5 -9 53.59 7.00 -4 5 -9 71.69 4.90 4 5 9 72.99 5.20 7 -6 -9 333.27 15.70 -7 -6 9 335.47 16.30 7 -6 -9 329.47 17.00 7 -6 -9 325.97 16.80 -7 -6 9 346.37 15.10 -7 -6 9 308.87 15.80 -7 -6 9 353.96 15.90 7 -6 -9 312.97 13.60 -7 6 9 342.47 14.60 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24.20 4.30 -4 6 9 20.00 3.90 -4 6 9 19.90 3.50 -4 6 9 20.20 3.00 -3 -6 9 13.50 3.30 3 -6 -9 15.40 4.10 3 -6 -9 10.90 3.70 3 -6 -9 13.90 3.60 -3 -6 9 13.70 3.40 -3 -6 9 9.60 3.50 -3 -6 9 10.40 3.30 3 6 -9 11.50 3.10 -3 6 9 15.00 3.90 -3 6 9 12.70 2.90 3 6 -9 12.80 3.90 3 6 -9 10.00 2.90 3 6 -9 9.10 3.00 -3 6 9 10.10 3.30 -3 6 9 12.40 3.30 -3 6 9 9.80 2.60 -2 -6 9 47.20 4.80 2 -6 -9 40.20 3.60 2 -6 -9 49.70 5.40 -2 -6 9 35.00 3.00 -2 -6 9 50.89 5.10 -2 -6 9 48.80 5.10 -2 -6 9 50.79 3.80 -2 6 9 48.80 4.60 2 6 -9 36.20 3.80 2 6 -9 56.49 5.20 -2 6 9 37.80 4.40 2 6 -9 43.70 4.70 -2 6 9 63.09 5.60 -2 6 9 41.90 3.90 2 6 -9 48.80 3.90 -2 6 9 41.80 4.00 -1 -6 9 240.28 11.20 -1 -6 9 252.57 10.30 1 -6 -9 253.97 11.50 1 -6 -9 260.37 11.00 -1 -6 9 240.68 11.30 1 -6 -9 264.37 10.90 -1 -6 9 243.18 9.60 1 -6 -9 254.77 10.20 -1 -6 9 254.07 11.70 1 6 -9 260.47 9.60 -1 6 9 263.17 11.20 -1 6 9 265.87 11.10 1 6 -9 247.98 11.20 -1 6 9 256.77 12.00 1 6 -9 262.97 11.10 -1 6 9 284.47 11.10 -1 6 9 252.37 10.10 1 6 -9 249.28 9.70 1 6 -9 273.47 11.40 0 -6 -9 9.10 3.30 0 -6 9 5.60 3.00 0 -6 9 9.30 3.00 0 -6 -9 8.60 2.80 0 -6 -9 6.00 2.40 0 -6 -9 9.70 2.50 0 -6 9 6.00 2.70 0 -6 9 6.10 3.60 0 6 9 10.20 2.60 0 6 -9 1.60 2.60 0 6 9 6.20 2.00 0 6 9 11.50 3.90 0 6 9 6.10 2.60 0 6 9 8.90 3.10 0 6 -9 2.20 2.70 0 6 -9 2.90 2.60 0 6 9 5.10 1.90 1 -6 9 195.88 9.60 1 -6 9 175.88 10.00 -1 -6 -9 179.48 8.40 -1 -6 -9 174.48 8.70 1 -6 9 183.88 9.60 1 -6 9 189.78 9.40 -1 -6 -9 194.38 9.60 -1 -6 -9 191.98 8.70 -1 6 -9 205.88 9.50 1 6 9 202.88 8.70 -1 6 -9 198.28 8.60 1 6 9 198.18 10.20 1 6 9 198.38 9.70 -1 6 -9 183.68 9.60 1 6 9 195.88 8.40 1 6 9 161.78 7.90 2 -6 9 13.90 4.70 2 -6 9 13.40 3.80 -2 -6 -9 9.50 3.70 -2 -6 -9 9.80 3.20 2 -6 9 11.50 3.40 -2 -6 -9 9.50 2.80 2 -6 9 9.10 4.00 -2 -6 -9 9.40 2.90 -2 -6 -9 14.00 2.40 2 6 9 7.80 2.70 2 6 9 7.10 2.30 2 6 9 7.50 4.00 -2 6 -9 11.60 2.90 -2 6 -9 5.20 3.50 -2 6 -9 5.70 3.10 2 6 9 14.00 4.10 2 6 9 7.70 2.10 -3 -6 -9 7.40 3.80 3 -6 9 8.30 4.90 -3 -6 -9 14.50 3.30 -3 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11 -9 17.80 3.50 -3 11 9 18.00 4.50 -3 11 9 17.20 3.70 -3 11 9 21.40 3.70 -3 11 9 12.20 3.60 3 11 -9 19.60 4.20 3 11 -9 14.40 3.90 -2 -11 9 165.98 8.90 -2 -11 9 154.58 9.00 -2 -11 9 159.98 6.80 2 -11 -9 162.98 9.40 -2 -11 9 170.98 7.50 -2 -11 9 169.48 9.10 -2 -11 9 151.88 8.70 2 -11 -9 159.98 9.10 2 -11 -9 170.48 8.90 -2 11 9 168.98 8.50 -2 11 9 174.78 8.70 2 11 -9 173.68 7.70 -2 11 9 175.68 9.80 -2 11 9 183.38 7.40 -2 11 9 159.68 8.10 2 11 -9 162.08 7.40 2 11 -9 163.48 8.80 2 11 -9 152.38 8.80 -1 -11 9 17.60 3.00 1 -11 -9 22.40 4.30 -1 -11 9 15.40 3.60 1 -11 -9 19.40 3.70 1 -11 -9 23.40 4.20 -1 -11 9 15.90 3.80 -1 -11 9 18.50 4.30 1 -11 -9 19.80 2.20 -1 -11 9 22.00 2.50 -1 11 9 25.00 4.80 1 11 -9 19.20 3.80 -1 11 9 18.00 2.10 1 11 -9 14.90 2.00 1 11 -9 14.80 3.70 -1 11 9 20.60 3.90 -1 11 9 17.10 3.30 1 11 -9 20.70 3.70 -1 11 9 22.20 3.20 1 11 -9 16.40 2.30 0 -11 9 126.59 7.80 0 -11 -9 123.79 8.10 0 -11 -9 115.89 5.90 0 -11 9 127.19 7.10 0 -11 9 115.29 7.70 0 -11 -9 121.99 7.10 0 -11 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15.60 4.60 6 -12 -9 15.10 4.70 6 -12 -9 13.80 3.50 -6 -12 9 9.00 4.20 6 -12 -9 10.90 5.20 -6 -12 9 9.40 4.40 6 -12 -9 22.00 6.40 -6 -12 9 11.80 3.70 -6 12 9 2.90 3.10 -6 12 9 18.00 4.90 6 12 -9 8.60 4.50 6 12 -9 19.10 5.30 -6 12 9 12.10 4.10 -6 12 9 14.00 4.60 6 12 -9 15.10 4.80 -6 12 9 14.00 4.60 -5 -12 9 186.08 7.90 -5 -12 9 206.18 11.00 5 -12 -9 207.08 11.00 -5 -12 9 197.88 10.20 -5 -12 9 187.08 10.90 -5 -12 9 196.48 11.00 5 -12 -9 183.18 11.60 5 -12 -9 181.78 11.30 5 12 -9 196.98 10.40 5 12 -9 209.38 10.80 -5 12 9 190.58 10.80 5 12 -9 187.98 11.00 -5 12 9 194.78 11.20 -5 12 9 212.18 10.50 -5 12 9 183.18 9.60 -5 12 9 194.68 11.00 -5 12 9 168.38 7.40 -4 -12 9 65.59 6.20 -4 -12 9 68.69 5.10 -4 -12 9 68.59 6.60 4 -12 -9 59.29 6.60 4 -12 -9 65.09 6.50 -4 -12 9 65.19 6.40 4 -12 -9 59.19 6.00 4 12 -9 63.09 5.70 -4 12 9 61.79 5.70 -4 12 9 62.89 5.40 4 12 -9 59.69 5.90 -4 12 9 65.39 6.20 4 12 -9 75.29 6.70 4 12 -9 65.29 6.70 -4 12 9 69.49 6.70 -4 12 9 61.59 6.00 3 -12 -9 42.40 5.80 -3 -12 9 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4.50 -4 4 10 12.70 3.80 4 4 -10 12.10 4.00 4 4 -10 8.50 3.40 4 4 -10 16.30 3.70 -4 4 10 18.70 3.20 -4 4 10 11.90 3.50 -4 4 10 17.60 2.50 3 -4 -10 127.39 8.10 -3 -4 10 142.09 8.10 -3 -4 10 140.89 8.20 -3 -4 10 138.59 8.60 3 -4 -10 150.18 8.30 3 -4 -10 131.69 6.90 3 -4 -10 135.19 8.10 -3 -4 10 133.59 8.00 -3 4 10 132.29 8.50 3 4 -10 125.69 7.70 3 4 -10 143.59 8.40 3 4 -10 147.29 7.50 -3 4 10 140.39 8.20 -3 4 10 131.89 7.50 3 4 -10 150.48 7.80 -3 4 10 128.19 6.60 -3 4 10 132.59 7.90 2 -4 -10 36.60 5.00 2 -4 -10 39.80 4.70 2 -4 -10 34.30 4.20 -2 -4 10 40.60 4.90 -2 -4 10 29.40 3.10 2 -4 -10 32.60 3.60 -2 -4 10 40.20 5.20 -2 -4 10 38.40 3.40 -2 -4 10 34.90 4.70 -2 -4 10 34.50 4.30 2 4 -10 39.70 3.70 -2 4 10 31.60 4.20 -2 4 10 36.40 5.10 2 4 -10 42.70 5.10 2 4 -10 37.30 3.90 2 4 -10 38.20 4.50 -2 4 10 30.10 4.30 -2 4 10 34.80 4.00 -2 4 10 37.40 3.90 -1 -4 10 135.19 6.40 -1 -4 10 136.59 7.10 -1 -4 10 150.88 8.40 -1 -4 10 146.29 8.40 1 -4 -10 149.59 8.50 1 -4 -10 149.59 7.40 1 -4 -10 142.79 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5 -5 -10 10.20 4.30 5 -5 -10 7.30 4.10 -5 -5 10 8.00 3.60 -5 -5 10 7.00 3.80 -5 -5 10 7.40 2.90 5 5 -10 7.80 4.20 -5 5 10 9.40 3.90 -5 5 10 6.50 3.50 -5 5 10 11.20 4.00 5 5 -10 9.30 4.20 -5 5 10 8.90 3.60 -5 5 10 10.60 2.90 5 5 -10 17.10 4.10 -4 -5 10 98.89 7.40 4 -5 -10 88.49 7.00 -4 -5 10 89.19 6.30 4 -5 -10 79.99 7.30 4 -5 -10 90.49 7.00 -4 -5 10 87.59 7.20 -4 -5 10 91.49 7.30 -4 5 10 90.09 5.80 -4 5 10 93.19 6.70 -4 5 10 91.09 6.90 4 5 -10 96.19 7.40 -4 5 10 95.19 7.00 4 5 -10 83.29 6.70 -4 5 10 94.79 7.00 4 5 -10 100.99 6.90 4 5 -10 95.49 6.60 -4 5 10 91.59 5.10 -3 -5 10 72.69 6.30 3 -5 -10 75.29 6.30 3 -5 -10 66.69 6.50 -3 -5 10 59.19 6.00 3 -5 -10 65.79 5.80 -3 -5 10 65.09 5.90 3 -5 -10 60.79 4.60 -3 -5 10 68.59 6.30 -3 5 10 65.19 5.40 3 5 -10 70.09 5.90 3 5 -10 71.19 5.60 -3 5 10 58.99 4.70 -3 5 10 67.99 6.30 3 5 -10 78.59 6.50 -3 5 10 74.89 6.10 -3 5 10 65.09 5.80 3 5 -10 68.79 5.30 -2 -5 10 83.39 4.70 2 -5 -10 86.89 6.10 -2 -5 10 81.19 4.30 -2 -5 10 60.99 5.90 2 -5 -10 87.09 5.70 -2 -5 10 74.29 6.50 2 -5 -10 84.39 5.00 -2 -5 10 80.29 6.30 -2 -5 10 68.79 5.90 2 -5 -10 71.09 6.40 2 5 -10 72.59 5.00 -2 5 10 64.19 5.10 -2 5 10 78.69 6.70 -2 5 10 78.89 5.50 2 5 -10 66.19 5.90 -2 5 10 84.99 6.00 2 5 -10 77.89 6.20 -2 5 10 79.89 6.00 2 5 -10 75.69 4.80 1 -5 -10 61.69 4.90 1 -5 -10 56.39 4.90 -1 -5 10 68.39 6.00 1 -5 -10 59.59 4.60 1 -5 -10 70.99 6.20 -1 -5 10 59.69 4.50 -1 -5 10 65.39 6.00 -1 -5 10 55.99 5.70 -1 -5 10 51.79 3.60 1 5 -10 55.29 5.40 -1 5 10 60.39 5.20 1 5 -10 62.29 3.70 -1 5 10 53.49 4.50 -1 5 10 67.39 5.30 1 5 -10 60.99 3.90 1 5 -10 68.89 5.70 -1 5 10 67.99 5.30 -1 5 10 68.69 6.40 0 -5 -10 4.50 2.50 0 -5 10 -0.60 3.40 0 -5 10 4.80 3.10 0 -5 -10 2.00 2.40 0 -5 -10 0.20 3.10 0 -5 10 3.00 3.00 0 -5 -10 6.10 2.70 0 -5 10 4.50 2.70 0 5 10 10.10 4.00 0 5 -10 3.50 2.90 0 5 10 2.00 2.20 0 5 10 5.80 2.80 0 5 10 5.20 3.10 0 5 -10 8.20 3.20 0 5 -10 7.90 3.10 1 -5 10 4.80 3.40 1 -5 10 1.40 2.90 -1 -5 -10 2.00 3.50 -1 -5 -10 3.80 2.40 1 -5 10 -2.40 2.80 -1 -5 -10 4.80 2.60 -1 -5 -10 2.20 2.70 1 -5 10 -1.20 4.10 1 5 10 0.80 2.60 1 5 10 2.80 3.30 -1 5 -10 5.30 3.40 1 5 10 2.50 2.40 -1 5 -10 2.90 2.90 1 5 10 -1.10 3.70 -1 5 -10 1.60 2.70 -2 -5 -10 3.50 2.40 -2 -5 -10 7.60 2.60 -2 -5 -10 2.40 3.00 -2 -5 -10 10.00 2.90 2 -5 10 -4.80 4.00 2 -5 10 5.30 3.30 2 -5 10 5.00 3.50 2 -5 10 -1.00 3.30 -2 -5 -10 0.30 3.20 2 5 10 4.00 2.50 -2 5 -10 1.90 3.10 2 5 10 0.40 2.90 -2 5 -10 1.80 3.40 2 5 10 -1.70 3.60 -2 5 -10 6.10 3.20 2 5 10 -4.60 3.10 -3 -5 -10 35.60 3.90 -3 -5 -10 38.00 4.10 -3 -5 -10 36.80 4.20 3 -5 10 46.50 7.60 -3 -5 -10 37.20 5.70 3 -5 10 25.40 4.90 3 -5 10 52.39 7.10 3 -5 10 34.50 5.10 -3 -5 -10 48.20 5.80 3 5 10 43.70 5.50 -3 5 -10 42.90 4.70 3 5 10 40.40 6.40 3 5 10 35.80 4.40 -3 5 -10 46.60 6.20 -3 5 -10 26.80 4.70 3 5 10 32.20 6.50 6 -6 -10 20.30 3.00 6 -6 -10 18.70 5.40 -6 -6 10 24.40 4.80 6 -6 -10 20.20 5.80 -6 -6 10 16.80 4.80 -6 -6 10 23.30 2.80 -6 -6 10 24.10 5.30 6 -6 -10 22.10 5.50 -6 -6 10 20.10 4.80 6 6 -10 25.70 5.50 -6 6 10 13.60 4.30 6 6 -10 11.50 4.30 -6 6 10 20.10 4.40 -6 6 10 20.00 3.50 -6 6 10 24.20 5.10 -6 6 10 18.20 4.40 -5 -6 10 20.80 4.80 -5 -6 10 19.60 3.50 5 -6 -10 24.50 5.00 -5 -6 10 20.70 4.60 5 -6 -10 17.30 5.50 5 -6 -10 24.90 5.30 -5 -6 10 25.70 4.60 -5 -6 10 15.10 4.20 -5 6 10 20.70 4.50 5 6 -10 25.10 5.10 5 6 -10 22.60 5.20 -5 6 10 22.20 4.30 5 6 -10 26.10 4.70 -5 6 10 21.10 4.60 -5 6 10 26.80 4.70 -5 6 10 23.70 3.50 4 -6 -10 18.20 4.70 -4 -6 10 11.60 3.70 -4 -6 10 15.00 3.50 -4 -6 10 8.40 3.90 4 -6 -10 7.00 3.50 4 -6 -10 14.30 4.20 -4 -6 10 21.70 4.40 -4 6 10 12.40 3.30 4 6 -10 11.40 3.80 4 6 -10 14.00 3.50 -4 6 10 15.00 3.70 -4 6 10 13.90 2.70 4 6 -10 9.10 3.50 -4 6 10 12.10 3.70 -4 6 10 14.00 4.10 -4 6 10 15.30 2.90 4 6 -10 11.90 4.30 3 -6 -10 358.36 13.70 -3 -6 10 359.66 15.70 3 -6 -10 357.76 15.00 3 -6 -10 362.16 15.60 3 -6 -10 351.26 15.70 -3 -6 10 363.26 15.00 -3 -6 10 354.36 15.30 -3 -6 10 335.47 15.20 3 6 -10 360.26 14.60 3 6 -10 330.27 14.90 3 6 -10 383.76 14.40 -3 6 10 361.76 14.70 -3 6 10 376.76 15.60 -3 6 10 348.27 15.30 -3 6 10 381.76 15.80 -3 6 10 346.37 14.00 3 6 -10 377.96 15.50 2 -6 -10 31.50 4.10 -2 -6 10 32.50 4.30 -2 -6 10 25.60 2.80 -2 -6 10 30.50 4.40 2 -6 -10 40.30 4.90 2 -6 -10 31.00 3.40 -2 -6 10 39.10 3.30 -2 -6 10 30.90 4.60 -2 -6 10 39.60 5.00 2 -6 -10 38.80 5.40 -2 6 10 26.10 4.10 -2 6 10 30.90 4.10 2 6 -10 34.20 3.70 -2 6 10 41.70 5.50 2 6 -10 31.10 3.40 2 6 -10 33.70 4.60 -2 6 10 32.20 4.50 -2 6 10 31.10 3.70 2 6 -10 33.50 4.50 -1 -6 10 6.10 3.10 -1 -6 10 10.50 1.90 -1 -6 10 -0.30 2.60 1 -6 -10 5.40 2.70 -1 -6 10 4.70 3.40 1 -6 -10 5.20 2.30 -1 -6 10 4.30 2.40 1 -6 -10 2.40 2.90 1 -6 -10 6.60 3.70 1 6 -10 7.40 3.30 -1 6 10 7.10 3.00 1 6 -10 5.40 2.00 1 6 -10 9.80 3.20 -1 6 10 5.70 2.30 -1 6 10 13.50 3.30 -1 6 10 10.80 4.00 1 6 -10 9.20 1.80 -1 6 10 7.70 2.90 0 -6 -10 37.40 4.00 0 -6 -10 30.90 5.00 0 -6 -10 31.00 4.10 0 -6 10 29.00 4.90 0 -6 10 27.70 4.30 0 -6 -10 26.10 3.50 0 -6 10 26.60 4.00 0 -6 10 31.30 4.60 0 6 10 21.40 4.10 0 6 10 31.10 3.20 0 6 10 32.30 3.90 0 6 10 32.80 5.10 0 6 10 31.80 4.00 0 6 -10 27.30 4.40 0 6 -10 26.70 4.10 0 6 -10 32.60 4.40 1 -6 10 -0.20 3.00 1 -6 10 2.80 3.00 1 -6 10 -0.60 4.30 -1 -6 -10 2.40 2.40 -1 -6 -10 4.60 3.60 1 -6 10 -4.00 2.90 -1 -6 -10 -1.00 2.40 -1 -6 -10 2.30 2.70 1 6 10 -0.30 2.60 -1 6 -10 0.00 2.60 -1 6 -10 -1.60 2.70 1 6 10 2.30 3.40 1 6 10 -0.70 2.30 1 6 10 0.30 3.60 -1 6 -10 1.60 2.90 2 -6 10 7.50 3.70 -2 -6 -10 20.30 4.50 -2 -6 -10 13.00 2.90 2 -6 10 7.20 4.80 -2 -6 -10 10.90 2.60 -2 -6 -10 12.30 3.00 2 -6 10 11.30 4.50 2 -6 10 17.70 4.00 -2 -6 -10 7.20 3.30 2 6 10 13.40 2.90 2 6 10 8.30 4.30 -2 6 -10 19.10 3.20 -2 6 -10 13.00 4.10 2 6 10 15.20 4.40 -2 6 -10 7.10 3.50 2 6 10 16.40 3.50 3 -6 10 8.40 5.30 3 -6 10 2.30 3.70 -3 -6 -10 5.20 4.10 -3 -6 -10 4.60 3.70 -3 -6 -10 5.10 2.70 -3 -6 -10 9.90 3.00 3 -6 10 5.10 4.40 3 -6 10 -1.30 3.30 -3 -6 -10 9.10 2.60 3 6 10 4.20 2.90 -3 6 -10 3.60 3.90 -3 6 -10 7.30 3.60 3 6 10 7.00 2.30 -3 6 -10 7.40 3.20 3 6 10 7.30 4.40 3 6 10 4.50 4.30 -6 -7 10 -2.20 3.30 -6 -7 10 4.00 3.90 -6 -7 10 -5.20 3.30 -6 -7 10 0.90 1.70 6 -7 -10 4.30 4.40 6 -7 -10 -2.20 3.90 6 -7 -10 -0.30 4.80 6 -7 -10 -0.40 2.20 -6 -7 10 -1.00 3.30 -6 7 10 3.60 3.60 6 7 -10 -2.10 4.10 -6 7 10 0.30 2.80 -6 7 10 -5.00 3.50 -6 7 10 0.30 3.40 -6 7 10 -3.80 3.10 6 7 -10 15.00 4.70 6 7 -10 2.50 4.00 5 -7 -10 53.59 6.70 -5 -7 10 60.49 6.70 5 -7 -10 65.09 7.20 -5 -7 10 55.59 4.80 -5 -7 10 49.20 5.90 -5 -7 10 73.59 6.50 -5 -7 10 59.99 6.60 5 -7 -10 64.79 7.40 5 7 -10 62.79 6.50 -5 7 10 68.09 6.50 5 7 -10 59.09 6.40 -5 7 10 61.89 6.60 5 7 -10 64.79 6.30 -5 7 10 59.49 4.90 -5 7 10 65.99 6.70 -5 7 10 62.59 6.70 -5 7 10 48.90 4.40 4 -7 -10 -2.10 3.30 -4 -7 10 2.00 3.40 -4 -7 10 3.80 3.00 4 -7 -10 1.40 3.50 -4 -7 10 4.10 3.30 -4 -7 10 2.00 3.20 4 -7 -10 2.30 3.50 4 7 -10 3.30 3.30 -4 7 10 -3.90 2.50 4 7 -10 0.90 3.00 -4 7 10 1.30 3.20 -4 7 10 5.80 3.50 4 7 -10 0.20 3.20 -4 7 10 4.80 2.60 -4 7 10 2.30 2.10 -4 7 10 2.40 3.60 4 7 -10 -1.30 3.60 3 -7 -10 3.90 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61.99 7.20 -4 12 10 50.69 5.80 4 12 -10 55.69 5.80 -4 12 10 67.79 6.00 -3 -12 10 -1.90 3.30 3 -12 -10 4.60 3.70 -3 -12 10 0.60 3.20 -3 -12 10 1.30 3.00 3 -12 -10 2.90 3.30 3 -12 -10 2.50 3.80 -3 -12 10 1.00 3.10 3 12 -10 4.60 3.50 -3 12 10 0.40 3.80 -3 12 10 3.40 2.50 3 12 -10 -4.50 2.50 -3 12 10 -1.30 3.00 3 12 -10 -1.50 3.70 -3 12 10 1.80 2.80 3 12 -10 -0.60 2.60 -3 12 10 1.60 3.30 -2 -12 10 5.60 3.40 2 -12 -10 8.50 3.90 2 -12 -10 7.00 4.00 2 -12 -10 7.20 4.00 -2 -12 10 5.60 1.90 -2 -12 10 6.40 3.70 -2 -12 10 8.10 3.60 -2 -12 10 2.70 3.50 -2 -12 10 8.40 2.00 2 12 -10 5.30 2.50 -2 12 10 4.60 4.00 -2 12 10 11.10 3.70 2 12 -10 4.30 3.60 2 12 -10 3.60 2.50 2 12 -10 7.70 3.80 -2 12 10 4.10 2.90 -2 12 10 11.00 2.40 -2 12 10 7.70 3.00 -1 -12 10 32.50 5.70 -1 -12 10 27.10 4.90 -1 -12 10 34.80 2.40 1 -12 -10 26.80 5.00 1 -12 -10 25.70 4.80 1 -12 -10 23.70 4.40 -1 -12 10 31.80 3.90 -1 -12 10 37.00 5.20 1 -12 -10 26.80 2.90 1 12 -10 25.60 2.40 -1 12 10 32.00 5.10 -1 12 10 33.70 4.60 1 12 -10 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32.10 3.00 2 -13 -10 27.20 5.40 -2 -13 10 29.70 5.10 2 -13 -10 27.60 5.10 -2 -13 10 21.40 4.40 -2 -13 10 26.50 4.60 -2 -13 10 30.80 4.90 -2 -13 10 25.60 2.90 2 -13 -10 28.70 5.10 -2 13 10 25.60 4.70 -2 13 10 31.70 3.20 -2 13 10 29.60 4.50 2 13 -10 30.20 5.00 2 13 -10 31.50 3.70 -2 13 10 24.60 4.80 2 13 -10 27.80 4.90 -2 13 10 32.40 4.60 2 13 -10 26.10 3.40 1 -13 -10 16.70 2.20 1 -13 -10 16.70 4.40 1 -13 -10 17.20 4.60 1 -13 -10 13.60 4.10 -1 -13 10 17.10 4.50 -1 -13 10 17.90 3.20 -1 -13 10 10.70 4.80 -1 -13 10 10.40 3.80 1 13 -10 16.10 4.20 -1 13 10 17.30 3.70 1 13 -10 19.70 4.40 1 13 -10 17.80 2.00 -1 13 10 20.20 3.40 -1 13 10 13.00 4.60 -1 13 10 20.10 4.30 1 13 -10 14.90 2.00 1 13 -10 17.80 4.10 0 -13 -10 47.40 5.80 0 -13 10 37.60 5.10 0 -13 -10 43.80 3.80 0 -13 10 49.80 6.80 0 -13 -10 52.39 5.70 0 -13 10 46.90 6.10 0 -13 10 46.20 6.00 0 -13 -10 47.10 6.20 0 13 10 42.60 6.10 0 13 10 42.60 4.30 0 13 -10 52.09 6.00 0 13 10 44.80 4.80 0 13 10 49.90 6.40 0 13 -10 42.50 5.80 0 13 10 39.80 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2 -14 10 25.70 5.30 2 -14 10 31.00 5.90 -2 14 -10 24.10 5.10 -2 14 -10 37.50 3.90 -2 14 -10 25.60 5.60 2 14 10 31.20 6.10 2 14 10 33.30 3.80 2 14 10 39.80 6.30 -5 -15 10 1.40 4.10 -5 -15 10 8.30 2.20 5 -15 -10 1.10 4.50 -5 -15 10 8.80 4.10 -5 -15 10 -1.40 3.70 5 -15 -10 9.80 4.70 -5 -15 10 3.90 4.10 5 -15 -10 7.00 4.60 5 15 -10 10.10 4.40 -5 15 10 4.10 4.20 -5 15 10 3.20 4.80 -5 15 10 3.70 3.80 5 15 -10 9.40 5.30 -5 15 10 0.60 4.50 5 15 -10 0.90 3.80 -5 15 10 3.40 3.90 4 -15 -10 33.50 5.80 -4 -15 10 27.40 5.40 4 -15 -10 29.70 5.80 -4 -15 10 37.40 4.40 -4 -15 10 38.70 5.80 4 -15 -10 30.00 5.80 -4 -15 10 33.40 5.30 -4 15 10 19.50 4.90 -4 15 10 33.30 6.20 -4 15 10 34.50 4.30 4 15 -10 40.60 6.00 -4 15 10 33.50 5.00 4 15 -10 26.90 4.70 -4 15 10 32.40 5.20 4 15 -10 39.70 6.20 4 15 -10 33.50 5.00 3 -15 -10 32.10 5.70 -3 -15 10 39.70 5.80 3 -15 -10 42.00 6.30 -3 -15 10 45.20 5.20 -3 -15 10 37.50 5.70 -3 -15 10 50.09 6.10 3 -15 -10 40.90 6.30 -3 15 10 54.89 7.20 -3 15 10 33.60 4.90 3 15 -10 37.10 4.70 -3 15 10 37.30 4.00 -3 15 10 41.60 5.50 3 15 -10 44.20 6.00 -3 15 10 38.70 5.30 3 15 -10 39.60 4.90 3 15 -10 35.30 5.70 -2 -15 10 3.20 3.40 2 -15 -10 0.60 4.10 -2 -15 10 2.80 2.00 2 -15 -10 1.80 3.60 -2 -15 10 1.10 3.30 2 -15 -10 -2.20 3.50 -2 -15 10 0.70 3.60 -2 -15 10 6.60 3.80 -2 15 10 2.20 2.80 -2 15 10 5.00 4.00 2 15 -10 0.50 2.40 -2 15 10 2.80 3.60 2 15 -10 -2.20 3.50 -2 15 10 8.70 3.90 2 15 -10 1.40 2.60 -2 15 10 0.80 1.80 2 15 -10 0.80 3.70 1 -15 -10 86.09 7.10 -1 -15 10 89.79 7.90 -1 -15 10 80.49 7.70 -1 -15 10 89.29 6.10 -1 -15 10 93.79 4.10 1 -15 -10 89.59 7.40 -1 -15 10 77.19 7.60 1 -15 -10 90.39 8.00 1 15 -10 87.99 7.60 -1 15 10 78.49 7.60 1 15 -10 96.69 7.00 -1 15 10 96.59 6.60 -1 15 10 102.39 8.40 -1 15 10 85.39 5.80 1 15 -10 70.39 4.10 1 15 -10 88.89 7.60 0 -15 -10 78.09 7.80 0 -15 -10 73.09 4.40 0 -15 10 68.59 7.40 0 -15 10 74.59 8.10 0 -15 -10 74.09 7.00 0 -15 10 83.39 6.70 0 -15 10 73.49 7.60 0 -15 -10 79.99 6.80 0 15 10 66.79 4.40 0 15 -10 72.49 7.40 0 15 10 72.39 5.80 0 15 -10 67.79 7.10 0 15 10 90.69 7.40 0 15 10 76.09 7.90 0 15 10 84.69 5.10 0 15 -10 80.59 6.00 -1 -15 -10 8.00 2.60 1 -15 10 7.20 4.30 -1 -15 -10 8.30 4.20 1 -15 10 1.80 3.80 -1 -15 -10 6.70 3.90 1 -15 10 -0.60 4.70 1 -15 10 3.60 4.10 -1 -15 -10 1.90 4.30 -1 15 -10 5.20 3.90 1 15 10 4.10 4.20 1 15 10 3.80 4.40 -1 15 -10 3.80 4.00 1 15 10 6.10 3.00 -1 15 -10 7.20 3.10 2 -15 10 63.39 8.60 -2 -15 -10 62.19 5.50 2 -15 10 54.09 7.00 -2 -15 -10 58.59 6.90 -2 -15 -10 66.59 7.70 -2 -15 -10 63.59 6.90 2 -15 10 59.29 7.60 2 -15 10 61.99 7.40 2 15 10 64.59 8.70 -2 15 -10 57.79 7.10 2 15 10 65.79 5.80 -2 15 -10 54.69 6.80 -2 15 -10 65.59 4.40 2 15 10 80.59 7.80 -5 -16 10 36.60 6.20 5 -16 -10 33.10 6.40 5 -16 -10 31.10 6.20 -5 -16 10 40.80 5.70 -5 -16 10 32.50 6.00 -5 -16 10 30.90 6.10 5 -16 -10 37.60 6.40 -5 -16 10 38.10 3.60 5 16 -10 32.70 5.50 -5 16 10 32.00 5.30 -5 16 10 36.50 6.60 -5 16 10 28.50 5.70 -5 16 10 39.10 6.40 5 16 -10 35.10 5.70 -5 16 10 32.50 6.00 5 16 -10 35.40 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14 4.60 4.90 -2 -1 14 4.70 4.40 2 -1 -14 1.00 3.50 2 -1 -14 11.20 3.80 2 -1 -14 3.50 5.10 2 -1 -14 4.70 3.40 -2 -1 14 3.00 4.40 2 1 -14 2.80 3.70 -2 1 14 5.40 5.20 2 1 -14 6.10 3.20 2 1 -14 8.80 5.30 -2 1 14 2.80 4.20 -2 1 14 2.80 3.00 -2 1 14 11.00 4.60 2 1 -14 5.90 3.40 -2 1 14 -0.70 3.40 1 -1 -14 75.29 6.40 1 -1 -14 66.29 5.40 1 1 -14 68.09 5.40 1 1 -14 66.89 5.30 -3 -2 14 9.30 4.10 -3 -2 14 6.60 2.20 -3 -2 14 10.80 4.70 -3 -2 14 5.80 4.80 3 -2 -14 3.70 4.00 3 -2 -14 12.50 6.40 3 -2 -14 9.00 4.40 3 -2 -14 5.20 3.50 -3 -2 14 3.30 4.40 3 2 -14 5.30 5.20 3 2 -14 4.90 3.60 -3 2 14 0.30 3.60 3 2 -14 4.70 3.90 -3 2 14 3.60 4.50 -3 2 14 2.40 4.70 3 2 -14 1.90 3.60 -3 2 14 -0.30 3.90 -3 2 14 7.60 2.80 -2 -2 14 7.40 5.10 2 -2 -14 16.90 4.50 2 -2 -14 22.50 6.40 2 -2 -14 12.90 3.70 -2 -2 14 15.00 5.10 -2 -2 14 17.40 5.60 -2 -2 14 17.90 3.50 -2 -2 14 13.40 4.50 2 -2 -14 23.10 5.20 -2 2 14 18.80 4.70 2 2 -14 18.40 3.90 -2 2 14 25.50 6.40 -2 2 14 23.80 6.20 -2 2 14 18.10 5.00 2 2 -14 14.90 4.70 2 2 -14 24.30 6.10 2 2 -14 18.60 3.90 -2 2 14 20.60 4.10 -3 -3 14 71.19 8.10 -3 -3 14 75.79 8.50 3 -3 -14 85.29 7.00 -3 -3 14 85.89 9.40 3 -3 -14 96.59 7.80 3 -3 -14 85.19 7.60 3 -3 -14 91.49 9.90 -3 3 14 89.69 6.00 -3 3 14 76.49 9.40 3 3 -14 84.29 6.80 -3 3 14 82.99 8.70 3 3 -14 85.39 9.30 3 3 -14 89.59 7.00 3 3 -14 79.09 7.50 -3 3 14 87.49 8.80 -2 -3 14 14.40 5.60 2 -3 -14 10.90 3.70 -2 -3 14 12.10 3.20 2 -3 -14 16.30 4.10 2 -3 -14 15.40 4.10 2 -3 -14 16.10 5.80 -2 -3 14 12.60 5.20 -2 -3 14 14.10 4.50 -2 -3 14 16.70 5.20 2 3 -14 17.20 3.50 -2 3 14 8.80 4.40 -2 3 14 13.80 4.50 2 3 -14 15.70 4.60 -2 3 14 15.50 5.90 -2 3 14 33.10 4.70 -2 3 14 12.50 5.00 2 3 -14 12.20 3.20 2 3 -14 16.10 5.50 -2 -4 14 13.50 5.30 -2 -4 14 17.80 5.70 2 -4 -14 8.60 4.10 -2 -4 14 18.60 3.30 2 -4 -14 7.80 3.70 2 -4 -14 16.10 6.00 2 -4 -14 9.10 4.20 -2 -4 14 11.40 4.40 2 4 -14 15.00 4.70 2 4 -14 23.20 6.00 2 4 -14 17.50 3.50 -2 4 14 18.30 4.50 -2 4 14 15.20 3.70 -2 4 14 4.90 4.80 -2 4 14 12.50 4.70 -2 4 14 7.00 4.70 2 4 -14 14.70 3.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 2552