data_2036sb15_0m _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C43 H34 F12 N8 P2 Ru' _chemical_formula_weight 1053.79 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ru' 'Ru' -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 19.5843(8) _cell_length_b 9.4572(4) _cell_length_c 23.4404(10) _cell_angle_alpha 90 _cell_angle_beta 96.134(2) _cell_angle_gamma 90 _cell_volume 4316.6(3) _cell_formula_units_Z 4 _cell_measurement_temperature 296(2) _cell_measurement_reflns_used 9867 _cell_measurement_theta_min 3.39 _cell_measurement_theta_max 28.79 _exptl_crystal_description block _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.622 _exptl_crystal_F_000 2120 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.250 _exptl_crystal_size_min 0.200 _exptl_absorpt_coefficient_mu 0.533 _shelx_estimated_absorpt_T_min 0.815 _shelx_estimated_absorpt_T_max 0.901 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6582 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 296(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 44716 _diffrn_reflns_av_unetI/netI 0.0396 _diffrn_reflns_av_R_equivalents 0.0346 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_theta_min 1.748 _diffrn_reflns_theta_max 28.700 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 11077 _reflns_number_gt 8339 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1128P)^2^+6.8930P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 11077 _refine_ls_number_parameters 572 _refine_ls_number_restraints 3 _refine_ls_R_factor_all 0.0858 _refine_ls_R_factor_gt 0.0653 _refine_ls_wR_factor_ref 0.2050 _refine_ls_wR_factor_gt 0.1884 _refine_ls_goodness_of_fit_ref 1.050 _refine_ls_restrained_S_all 1.050 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.26897(2) 0.65009(3) 0.61701(2) 0.03276(12) Uani 1 1 d . . . . . P2 P 0.08756(8) 0.36302(17) 0.37400(7) 0.0610(4) Uani 1 1 d . . . . . P1 P 0.42897(9) 0.31882(17) 0.86413(8) 0.0656(4) Uani 1 1 d . . . . . N6 N 0.27580(17) 0.8429(3) 0.66065(14) 0.0340(7) Uani 1 1 d . . . . . N4 N 0.35683(17) 0.5686(3) 0.66253(14) 0.0356(7) Uani 1 1 d . . . . . N2 N 0.32020(18) 0.7296(4) 0.55176(15) 0.0389(7) Uani 1 1 d . . . . . N5 N 0.21043(16) 0.5838(3) 0.68114(14) 0.0346(7) Uani 1 1 d . . . . . N3 N 0.27592(18) 0.4573(4) 0.57606(15) 0.0389(7) Uani 1 1 d . . . . . N1 N 0.18623(17) 0.7175(4) 0.56046(15) 0.0391(7) Uani 1 1 d . . . . . N7 N 0.16402(16) 0.8122(3) 0.68592(15) 0.0365(7) Uani 1 1 d . . . . . C24 C 0.3942(2) 0.6185(5) 0.70901(19) 0.0440(9) Uani 1 1 d . . . . . H24 H 0.377577 0.694887 0.728374 0.053 Uiso 1 1 calc R U . . . F3 F 0.4075(2) 0.4715(4) 0.84273(17) 0.0916(12) Uani 1 1 d . . . . . C37 C 0.22550(19) 0.8901(4) 0.69024(17) 0.0336(8) Uani 1 1 d . . . . . C41 C 0.3341(2) 0.9205(5) 0.66344(19) 0.0423(9) Uani 1 1 d . . . . . H41 H 0.369456 0.889393 0.643014 0.051 Uiso 1 1 calc R U . . . C6 C 0.2778(2) 0.7923(5) 0.50905(18) 0.0414(9) Uani 1 1 d . . . . . C23 C 0.4571(3) 0.5604(6) 0.7294(2) 0.0524(11) Uani 1 1 d . . . . . H23 H 0.481772 0.598861 0.761819 0.063 Uiso 1 1 calc R U . . . F2 F 0.5035(2) 0.3453(5) 0.8490(2) 0.1070(15) Uani 1 1 d . . . . . C18 C 0.3809(2) 0.4507(4) 0.63712(18) 0.0386(9) Uani 1 1 d . . . . . C17 C 0.3380(2) 0.3920(5) 0.59028(19) 0.0417(9) Uani 1 1 d . . . . . C5 C 0.2061(2) 0.7867(5) 0.51430(18) 0.0422(9) Uani 1 1 d . . . . . C39 C 0.2929(3) 1.0883(5) 0.7259(2) 0.0493(11) Uani 1 1 d . . . . . H39 H 0.298960 1.169785 0.748055 0.059 Uiso 1 1 calc R U . . . C40 C 0.3438(2) 1.0417(5) 0.6945(2) 0.0468(10) Uani 1 1 d . . . . . H40 H 0.384522 1.092453 0.694530 0.056 Uiso 1 1 calc R U . . . F6 F 0.4102(3) 0.2607(5) 0.8024(2) 0.1176(17) Uani 1 1 d . . . . . C7 C 0.3020(3) 0.8546(5) 0.4607(2) 0.0515(12) Uani 1 1 d . . . . . F12 F 0.0140(2) 0.4122(6) 0.3844(3) 0.134(2) Uani 1 1 d . . . . . C29 C 0.1670(2) 0.6717(4) 0.70462(19) 0.0374(8) Uani 1 1 d . . . . . F1 F 0.4537(4) 0.1687(5) 0.8883(3) 0.133(2) Uani 1 1 d . . . . . F5 F 0.4488(4) 0.3793(7) 0.9271(2) 0.149(3) Uani 1 1 d . . . . . C19 C 0.4446(2) 0.3897(5) 0.6555(2) 0.0456(10) Uani 1 1 d . . . . . C38 C 0.2330(2) 1.0124(4) 0.7240(2) 0.0433(9) Uani 1 1 d . . . . . H38 H 0.197738 1.041943 0.744794 0.052 Uiso 1 1 calc R U . . . C30 C 0.1007(2) 0.8905(5) 0.6938(2) 0.0466(10) Uani 1 1 d . . . . . H30A H 0.100947 0.913154 0.734223 0.056 Uiso 1 1 calc R U . . . H30B H 0.061710 0.829000 0.683384 0.056 Uiso 1 1 calc R U . . . C36 C 0.1168(3) 1.0475(5) 0.6080(2) 0.0560(12) Uani 1 1 d . . . . . H36 H 0.143736 0.977990 0.593466 0.067 Uiso 1 1 calc R U . . . C1 C 0.1194(2) 0.6978(6) 0.5629(2) 0.0507(11) Uani 1 1 d . . . . . H1 H 0.105199 0.646261 0.593317 0.061 Uiso 1 1 calc R U . . . C22 C 0.4832(3) 0.4477(6) 0.7028(2) 0.0553(12) Uani 1 1 d . . . . . H22 H 0.525906 0.410468 0.716029 0.066 Uiso 1 1 calc R U . . . C27 C 0.1303(3) 0.4867(5) 0.7633(2) 0.0572(13) Uani 1 1 d . . . . . H27 H 0.103211 0.454190 0.790808 0.069 Uiso 1 1 calc R U . . . C16 C 0.3593(3) 0.2724(5) 0.5618(2) 0.0504(11) Uani 1 1 d . . . . . C12 C 0.3867(2) 0.7269(5) 0.5458(2) 0.0505(11) Uani 1 1 d . . . . . H12 H 0.416371 0.685037 0.574517 0.061 Uiso 1 1 calc R U . . . C31 C 0.0906(2) 1.0256(5) 0.6596(2) 0.0451(10) Uani 1 1 d . . . . . C21 C 0.4249(3) 0.2125(6) 0.5806(3) 0.0598(14) Uani 1 1 d . . . . . H21 H 0.439710 0.132907 0.562106 0.072 Uiso 1 1 calc R U . . . F4 F 0.3535(3) 0.2953(7) 0.8799(3) 0.155(2) Uani 1 1 d . . . . . C10 C 0.3722(3) 0.8481(5) 0.4562(2) 0.0579(13) Uani 1 1 d . . . . . H10 H 0.390201 0.887184 0.424607 0.070 Uiso 1 1 calc R U . . . C25 C 0.2143(2) 0.4491(5) 0.7000(2) 0.0484(11) Uani 1 1 d . . . . . H25 H 0.245184 0.388454 0.684993 0.058 Uiso 1 1 calc R U . . . C35 C 0.1036(3) 1.1712(6) 0.5777(3) 0.0684(15) Uani 1 1 d . . . . . H35 H 0.121703 1.184470 0.543036 0.082 Uiso 1 1 calc R U . . . C2 C 0.0699(3) 0.7521(7) 0.5215(2) 0.0688(16) Uani 1 1 d . . . . . H2 H 0.023520 0.736779 0.524398 0.083 Uiso 1 1 calc R U . . . C28 C 0.1259(3) 0.6238(5) 0.7452(2) 0.0504(11) Uani 1 1 d . . . . . H28 H 0.095286 0.685256 0.760156 0.060 Uiso 1 1 calc R U . . . C20 C 0.4654(3) 0.2692(5) 0.6245(2) 0.0549(12) Uani 1 1 d . . . . . H20 H 0.508210 0.229072 0.635123 0.066 Uiso 1 1 calc R U . . . F11 F 0.1593(4) 0.3062(8) 0.3614(4) 0.1779(13) Uani 1 1 d . . . . . C15 C 0.3137(3) 0.2183(6) 0.5165(2) 0.0621(14) Uani 1 1 d . . . . . H15 H 0.325304 0.138817 0.496302 0.075 Uiso 1 1 calc R U . . . C11 C 0.4141(3) 0.7839(6) 0.4985(2) 0.0621(14) Uani 1 1 d . . . . . H11 H 0.461093 0.778133 0.495814 0.074 Uiso 1 1 calc R U . . . C8 C 0.2537(3) 0.9209(6) 0.4189(2) 0.0656(15) Uani 1 1 d . . . . . H8 H 0.269251 0.966912 0.387660 0.079 Uiso 1 1 calc R U . . . C14 C 0.2528(3) 0.2837(6) 0.5029(2) 0.0673(15) Uani 1 1 d . . . . . H14 H 0.222394 0.249084 0.472927 0.081 Uiso 1 1 calc R U . . . C26 C 0.1753(3) 0.3973(5) 0.7400(2) 0.0586(13) Uani 1 1 d . . . . . H26 H 0.179137 0.303213 0.751466 0.070 Uiso 1 1 calc R U . . . C4 C 0.1591(3) 0.8466(6) 0.4710(2) 0.0582(13) Uani 1 1 d . . . . . C3 C 0.0899(3) 0.8278(8) 0.4766(3) 0.0768(18) Uani 1 1 d . . . . . H3 H 0.056996 0.867029 0.449707 0.092 Uiso 1 1 calc R U . . . C13 C 0.2349(3) 0.4025(6) 0.5334(2) 0.0524(11) Uani 1 1 d . . . . . H13 H 0.192491 0.444798 0.523185 0.063 Uiso 1 1 calc R U . . . C9 C 0.1862(4) 0.9171(7) 0.4243(2) 0.0734(17) Uani 1 1 d . . . . . H9 H 0.155935 0.961865 0.396764 0.088 Uiso 1 1 calc R U . . . C34 C 0.0638(3) 1.2749(6) 0.5985(3) 0.0753(18) Uani 1 1 d . . . . . H34 H 0.055185 1.358712 0.578240 0.090 Uiso 1 1 calc R U . . . N8 N 0.3493(5) -0.1868(8) 0.8199(3) 0.108(2) Uani 1 1 d . . . . . C32 C 0.0511(3) 1.1305(6) 0.6800(3) 0.0632(14) Uani 1 1 d . . . . . H32 H 0.033514 1.118524 0.715025 0.076 Uiso 1 1 calc R U . . . C43 C 0.3241(4) -0.1179(7) 0.8493(3) 0.0803(19) Uani 1 1 d . . . . . C33 C 0.0372(4) 1.2532(7) 0.6492(3) 0.081(2) Uani 1 1 d . . . . . H33 H 0.009337 1.321955 0.663089 0.097 Uiso 1 1 calc R U . . . C42 C 0.2933(5) -0.0272(8) 0.8877(4) 0.112(3) Uani 1 1 d . . . . . H42A H 0.263267 0.038386 0.866161 0.168 Uiso 1 1 calc R U . . . H42B H 0.328429 0.023885 0.910818 0.168 Uiso 1 1 calc R U . . . H42C H 0.267319 -0.082752 0.912051 0.168 Uiso 1 1 calc R U . . . F10 F 0.0560(4) 0.2765(9) 0.3204(3) 0.1779(13) Uani 1 1 d D . . . . F9 F 0.0937(4) 0.4945(8) 0.3339(3) 0.1779(13) Uani 1 1 d D . . . . F8 F 0.1223(3) 0.4454(6) 0.4240(3) 0.1779(13) Uani 1 1 d D . . . . F7 F 0.0813(3) 0.2318(6) 0.4114(3) 0.1779(13) Uani 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.03437(17) 0.03195(18) 0.03318(19) -0.00059(12) 0.00925(12) -0.00165(12) P2 0.0577(8) 0.0673(9) 0.0590(9) -0.0013(7) 0.0110(6) 0.0080(7) P1 0.0669(9) 0.0618(8) 0.0719(10) -0.0047(7) 0.0254(7) 0.0078(7) N6 0.0345(16) 0.0324(16) 0.0355(17) 0.0022(13) 0.0059(13) -0.0017(12) N4 0.0383(16) 0.0346(17) 0.0354(17) 0.0014(14) 0.0101(13) 0.0007(13) N2 0.0425(17) 0.0388(18) 0.0373(18) -0.0026(14) 0.0139(14) -0.0062(14) N5 0.0385(16) 0.0304(16) 0.0366(17) 0.0014(13) 0.0122(13) -0.0002(13) N3 0.0460(18) 0.0360(17) 0.0361(18) -0.0027(14) 0.0109(14) -0.0042(14) N1 0.0389(17) 0.0423(19) 0.0364(18) -0.0014(15) 0.0055(13) -0.0043(14) N7 0.0323(15) 0.0318(16) 0.046(2) -0.0010(14) 0.0086(14) 0.0015(13) C24 0.051(2) 0.044(2) 0.038(2) 0.0029(18) 0.0078(18) -0.0020(19) F3 0.123(3) 0.075(2) 0.079(3) 0.007(2) 0.026(2) 0.024(2) C37 0.0341(18) 0.0299(17) 0.037(2) 0.0029(15) 0.0056(15) 0.0012(14) C41 0.037(2) 0.043(2) 0.047(2) 0.0069(19) 0.0070(17) -0.0041(17) C6 0.053(2) 0.037(2) 0.035(2) -0.0039(17) 0.0068(17) -0.0070(18) C23 0.056(3) 0.058(3) 0.042(2) 0.008(2) -0.0041(19) 0.003(2) F2 0.066(2) 0.125(4) 0.132(4) -0.006(3) 0.017(3) -0.008(2) C18 0.042(2) 0.036(2) 0.040(2) 0.0012(17) 0.0148(16) 0.0028(16) C17 0.048(2) 0.037(2) 0.044(2) -0.0006(18) 0.0208(18) 0.0010(17) C5 0.050(2) 0.041(2) 0.035(2) -0.0020(17) 0.0031(17) -0.0022(18) C39 0.057(3) 0.032(2) 0.057(3) -0.009(2) -0.003(2) -0.0012(19) C40 0.045(2) 0.039(2) 0.055(3) 0.002(2) -0.0007(19) -0.0126(18) F6 0.105(3) 0.118(4) 0.126(4) -0.057(3) -0.006(3) -0.010(3) C7 0.080(3) 0.041(2) 0.036(2) -0.0032(18) 0.017(2) -0.013(2) F12 0.091(3) 0.108(3) 0.216(6) 0.047(4) 0.071(4) 0.045(3) C29 0.0383(19) 0.0317(19) 0.044(2) -0.0016(16) 0.0119(16) -0.0016(15) F1 0.168(5) 0.074(3) 0.164(5) 0.022(3) 0.060(4) 0.028(3) F5 0.213(7) 0.150(5) 0.078(3) -0.018(3) -0.007(4) 0.085(5) C19 0.047(2) 0.045(2) 0.048(3) 0.009(2) 0.0177(19) 0.0097(19) C38 0.041(2) 0.035(2) 0.053(3) -0.0042(18) 0.0005(18) 0.0061(17) C30 0.038(2) 0.043(2) 0.060(3) 0.000(2) 0.0158(19) 0.0052(18) C36 0.053(3) 0.047(3) 0.069(3) 0.006(2) 0.012(2) 0.007(2) C1 0.044(2) 0.061(3) 0.046(3) 0.001(2) 0.0023(19) -0.007(2) C22 0.052(3) 0.061(3) 0.053(3) 0.014(2) 0.006(2) 0.012(2) C27 0.068(3) 0.048(3) 0.061(3) 0.010(2) 0.032(2) -0.004(2) C16 0.061(3) 0.040(2) 0.054(3) -0.007(2) 0.026(2) -0.003(2) C12 0.047(2) 0.059(3) 0.049(3) 0.002(2) 0.018(2) -0.004(2) C31 0.037(2) 0.042(2) 0.055(3) -0.003(2) -0.0008(18) 0.0042(17) C21 0.068(3) 0.047(3) 0.071(3) -0.003(2) 0.038(3) 0.014(2) F4 0.092(3) 0.149(5) 0.240(7) 0.030(5) 0.090(4) 0.002(3) C10 0.077(3) 0.054(3) 0.047(3) -0.002(2) 0.028(3) -0.018(2) C25 0.058(3) 0.034(2) 0.057(3) 0.003(2) 0.024(2) 0.0030(19) C35 0.067(3) 0.060(3) 0.078(4) 0.021(3) 0.003(3) -0.003(3) C2 0.045(3) 0.101(5) 0.059(3) 0.004(3) -0.003(2) -0.003(3) C28 0.054(3) 0.045(2) 0.056(3) 0.002(2) 0.028(2) 0.000(2) C20 0.057(3) 0.048(3) 0.063(3) 0.006(2) 0.022(2) 0.013(2) F11 0.143(2) 0.174(3) 0.224(3) -0.013(3) 0.051(2) 0.035(2) C15 0.085(4) 0.047(3) 0.059(3) -0.017(2) 0.027(3) -0.006(3) C11 0.058(3) 0.071(3) 0.063(3) 0.001(3) 0.031(3) -0.011(3) C8 0.096(4) 0.061(3) 0.040(3) 0.012(2) 0.013(3) -0.009(3) C14 0.082(4) 0.064(3) 0.057(3) -0.026(3) 0.012(3) -0.017(3) C26 0.077(3) 0.037(2) 0.067(3) 0.011(2) 0.029(3) -0.002(2) C4 0.066(3) 0.063(3) 0.043(3) 0.002(2) -0.005(2) -0.001(2) C3 0.064(4) 0.101(5) 0.060(4) 0.010(3) -0.020(3) 0.006(3) C13 0.056(3) 0.051(3) 0.051(3) -0.012(2) 0.009(2) -0.011(2) C9 0.099(5) 0.073(4) 0.045(3) 0.016(3) -0.005(3) 0.001(4) C34 0.079(4) 0.046(3) 0.094(5) 0.006(3) -0.022(4) 0.005(3) N8 0.159(7) 0.091(4) 0.081(4) 0.013(4) 0.043(5) 0.038(5) C32 0.059(3) 0.059(3) 0.070(4) -0.009(3) 0.001(3) 0.020(2) C43 0.093(5) 0.069(4) 0.083(5) 0.027(4) 0.027(4) 0.021(4) C33 0.084(4) 0.052(3) 0.103(5) -0.012(3) -0.013(4) 0.027(3) C42 0.151(8) 0.078(5) 0.117(7) 0.014(5) 0.058(6) 0.038(5) F10 0.143(2) 0.174(3) 0.224(3) -0.013(3) 0.051(2) 0.035(2) F9 0.143(2) 0.174(3) 0.224(3) -0.013(3) 0.051(2) 0.035(2) F8 0.143(2) 0.174(3) 0.224(3) -0.013(3) 0.051(2) 0.035(2) F7 0.143(2) 0.174(3) 0.224(3) -0.013(3) 0.051(2) 0.035(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 N2 2.059(3) . ? Ru1 N3 2.072(3) . ? Ru1 N4 2.074(3) . ? Ru1 N1 2.081(4) . ? Ru1 N5 2.082(3) . ? Ru1 N6 2.088(3) . ? P2 F8 1.508(6) . ? P2 F7 1.532(6) . ? P2 F12 1.557(4) . ? P2 F11 1.563(7) . ? P2 F10 1.570(8) . ? P2 F9 1.571(7) . ? P1 F6 1.555(5) . ? P1 F2 1.558(5) . ? P1 F3 1.571(4) . ? P1 F4 1.577(5) . ? P1 F1 1.585(5) . ? P1 F5 1.591(5) . ? N6 C37 1.340(5) . ? N6 C41 1.354(5) . ? N4 C24 1.332(6) . ? N4 C18 1.371(5) . ? N2 C12 1.325(5) . ? N2 C6 1.366(6) . ? N5 C25 1.348(5) . ? N5 C29 1.348(5) . ? N3 C13 1.320(6) . ? N3 C17 1.373(6) . ? N1 C1 1.329(6) . ? N1 C5 1.357(5) . ? N7 C29 1.399(5) . ? N7 C37 1.406(5) . ? N7 C30 1.473(5) . ? C24 C23 1.386(7) . ? C24 H24 0.9300 . ? C37 C38 1.400(6) . ? C41 C40 1.360(6) . ? C41 H41 0.9300 . ? C6 C7 1.403(6) . ? C6 C5 1.424(6) . ? C23 C22 1.362(7) . ? C23 H23 0.9300 . ? C18 C19 1.399(6) . ? C18 C17 1.422(6) . ? C17 C16 1.399(6) . ? C5 C4 1.413(7) . ? C39 C38 1.373(6) . ? C39 C40 1.373(7) . ? C39 H39 0.9300 . ? C40 H40 0.9300 . ? C7 C10 1.391(8) . ? C7 C8 1.433(8) . ? C29 C28 1.387(6) . ? C19 C22 1.386(7) . ? C19 C20 1.434(7) . ? C38 H38 0.9300 . ? C30 C31 1.511(6) . ? C30 H30A 0.9700 . ? C30 H30B 0.9700 . ? C36 C35 1.378(7) . ? C36 C31 1.380(7) . ? C36 H36 0.9300 . ? C1 C2 1.396(7) . ? C1 H1 0.9300 . ? C22 H22 0.9300 . ? C27 C28 1.363(7) . ? C27 C26 1.376(7) . ? C27 H27 0.9300 . ? C16 C15 1.408(8) . ? C16 C21 1.430(8) . ? C12 C11 1.391(6) . ? C12 H12 0.9300 . ? C31 C32 1.374(6) . ? C21 C20 1.342(8) . ? C21 H21 0.9300 . ? C10 C11 1.362(8) . ? C10 H10 0.9300 . ? C25 C26 1.362(6) . ? C25 H25 0.9300 . ? C35 C34 1.373(9) . ? C35 H35 0.9300 . ? C2 C3 1.363(9) . ? C2 H2 0.9300 . ? C28 H28 0.9300 . ? C20 H20 0.9300 . ? C15 C14 1.351(9) . ? C15 H15 0.9300 . ? C11 H11 0.9300 . ? C8 C9 1.342(9) . ? C8 H8 0.9300 . ? C14 C13 1.396(7) . ? C14 H14 0.9300 . ? C26 H26 0.9300 . ? C4 C3 1.388(9) . ? C4 C9 1.431(8) . ? C3 H3 0.9300 . ? C13 H13 0.9300 . ? C9 H9 0.9300 . ? C34 C33 1.363(10) . ? C34 H34 0.9300 . ? N8 C43 1.104(9) . ? C32 C33 1.379(9) . ? C32 H32 0.9300 . ? C43 C42 1.424(10) . ? C33 H33 0.9300 . ? C42 H42A 0.9600 . ? C42 H42B 0.9600 . ? C42 H42C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Ru1 N3 85.16(13) . . ? N2 Ru1 N4 94.27(13) . . ? N3 Ru1 N4 79.60(14) . . ? N2 Ru1 N1 79.81(14) . . ? N3 Ru1 N1 93.41(14) . . ? N4 Ru1 N1 171.26(13) . . ? N2 Ru1 N5 174.79(13) . . ? N3 Ru1 N5 97.94(13) . . ? N4 Ru1 N5 90.42(13) . . ? N1 Ru1 N5 95.78(13) . . ? N2 Ru1 N6 91.97(13) . . ? N3 Ru1 N6 172.56(13) . . ? N4 Ru1 N6 93.79(13) . . ? N1 Ru1 N6 92.84(13) . . ? N5 Ru1 N6 85.45(12) . . ? F8 P2 F7 91.8(2) . . ? F8 P2 F12 94.2(4) . . ? F7 P2 F12 91.2(3) . . ? F8 P2 F11 89.1(4) . . ? F7 P2 F11 87.6(4) . . ? F12 P2 F11 176.6(4) . . ? F8 P2 F10 176.3(4) . . ? F7 P2 F10 89.3(3) . . ? F12 P2 F10 89.4(4) . . ? F11 P2 F10 87.4(4) . . ? F8 P2 F9 90.0(3) . . ? F7 P2 F9 178.1(3) . . ? F12 P2 F9 89.4(3) . . ? F11 P2 F9 91.7(4) . . ? F10 P2 F9 89.0(4) . . ? F6 P1 F2 88.8(3) . . ? F6 P1 F3 90.0(3) . . ? F2 P1 F3 90.3(3) . . ? F6 P1 F4 92.0(4) . . ? F2 P1 F4 178.8(3) . . ? F3 P1 F4 88.8(3) . . ? F6 P1 F1 92.8(3) . . ? F2 P1 F1 88.1(3) . . ? F3 P1 F1 176.8(4) . . ? F4 P1 F1 92.8(4) . . ? F6 P1 F5 179.4(4) . . ? F2 P1 F5 90.7(4) . . ? F3 P1 F5 89.8(3) . . ? F4 P1 F5 88.5(4) . . ? F1 P1 F5 87.4(3) . . ? C37 N6 C41 117.2(3) . . ? C37 N6 Ru1 122.2(3) . . ? C41 N6 Ru1 120.4(3) . . ? C24 N4 C18 117.3(4) . . ? C24 N4 Ru1 130.0(3) . . ? C18 N4 Ru1 112.6(3) . . ? C12 N2 C6 117.3(4) . . ? C12 N2 Ru1 129.4(3) . . ? C6 N2 Ru1 113.4(3) . . ? C25 N5 C29 117.7(3) . . ? C25 N5 Ru1 120.4(3) . . ? C29 N5 Ru1 121.9(3) . . ? C13 N3 C17 117.3(4) . . ? C13 N3 Ru1 129.2(3) . . ? C17 N3 Ru1 112.6(3) . . ? C1 N1 C5 118.0(4) . . ? C1 N1 Ru1 129.3(3) . . ? C5 N1 Ru1 112.7(3) . . ? C29 N7 C37 117.9(3) . . ? C29 N7 C30 116.4(3) . . ? C37 N7 C30 117.0(3) . . ? N4 C24 C23 122.1(4) . . ? N4 C24 H24 118.9 . . ? C23 C24 H24 118.9 . . ? N6 C37 C38 121.9(4) . . ? N6 C37 N7 117.3(3) . . ? C38 C37 N7 120.7(3) . . ? N6 C41 C40 123.5(4) . . ? N6 C41 H41 118.3 . . ? C40 C41 H41 118.3 . . ? N2 C6 C7 122.9(4) . . ? N2 C6 C5 116.6(4) . . ? C7 C6 C5 120.4(4) . . ? C22 C23 C24 121.0(5) . . ? C22 C23 H23 119.5 . . ? C24 C23 H23 119.5 . . ? N4 C18 C19 122.6(4) . . ? N4 C18 C17 116.8(4) . . ? C19 C18 C17 120.6(4) . . ? N3 C17 C16 123.3(4) . . ? N3 C17 C18 116.5(4) . . ? C16 C17 C18 120.2(4) . . ? N1 C5 C4 123.1(4) . . ? N1 C5 C6 117.2(4) . . ? C4 C5 C6 119.7(4) . . ? C38 C39 C40 118.8(4) . . ? C38 C39 H39 120.6 . . ? C40 C39 H39 120.6 . . ? C41 C40 C39 119.3(4) . . ? C41 C40 H40 120.4 . . ? C39 C40 H40 120.4 . . ? C10 C7 C6 117.7(5) . . ? C10 C7 C8 123.5(5) . . ? C6 C7 C8 118.8(5) . . ? N5 C29 C28 121.1(4) . . ? N5 C29 N7 117.7(3) . . ? C28 C29 N7 121.2(4) . . ? C22 C19 C18 118.3(4) . . ? C22 C19 C20 124.0(4) . . ? C18 C19 C20 117.6(5) . . ? C39 C38 C37 119.2(4) . . ? C39 C38 H38 120.4 . . ? C37 C38 H38 120.4 . . ? N7 C30 C31 115.0(4) . . ? N7 C30 H30A 108.5 . . ? C31 C30 H30A 108.5 . . ? N7 C30 H30B 108.5 . . ? C31 C30 H30B 108.5 . . ? H30A C30 H30B 107.5 . . ? C35 C36 C31 120.8(5) . . ? C35 C36 H36 119.6 . . ? C31 C36 H36 119.6 . . ? N1 C1 C2 122.1(5) . . ? N1 C1 H1 118.9 . . ? C2 C1 H1 118.9 . . ? C23 C22 C19 118.5(4) . . ? C23 C22 H22 120.8 . . ? C19 C22 H22 120.8 . . ? C28 C27 C26 118.9(4) . . ? C28 C27 H27 120.6 . . ? C26 C27 H27 120.6 . . ? C17 C16 C15 117.2(5) . . ? C17 C16 C21 118.4(5) . . ? C15 C16 C21 124.4(5) . . ? N2 C12 C11 123.0(5) . . ? N2 C12 H12 118.5 . . ? C11 C12 H12 118.5 . . ? C32 C31 C36 118.2(5) . . ? C32 C31 C30 118.2(4) . . ? C36 C31 C30 123.5(4) . . ? C20 C21 C16 121.0(4) . . ? C20 C21 H21 119.5 . . ? C16 C21 H21 119.5 . . ? C11 C10 C7 119.2(4) . . ? C11 C10 H10 120.4 . . ? C7 C10 H10 120.4 . . ? N5 C25 C26 123.4(4) . . ? N5 C25 H25 118.3 . . ? C26 C25 H25 118.3 . . ? C34 C35 C36 120.4(6) . . ? C34 C35 H35 119.8 . . ? C36 C35 H35 119.8 . . ? C3 C2 C1 119.7(5) . . ? C3 C2 H2 120.2 . . ? C1 C2 H2 120.2 . . ? C27 C28 C29 120.1(4) . . ? C27 C28 H28 119.9 . . ? C29 C28 H28 119.9 . . ? C21 C20 C19 122.0(5) . . ? C21 C20 H20 119.0 . . ? C19 C20 H20 119.0 . . ? C14 C15 C16 119.0(5) . . ? C14 C15 H15 120.5 . . ? C16 C15 H15 120.5 . . ? C10 C11 C12 119.9(5) . . ? C10 C11 H11 120.0 . . ? C12 C11 H11 120.0 . . ? C9 C8 C7 120.5(5) . . ? C9 C8 H8 119.7 . . ? C7 C8 H8 119.7 . . ? C15 C14 C13 120.7(5) . . ? C15 C14 H14 119.7 . . ? C13 C14 H14 119.7 . . ? C25 C26 C27 118.8(4) . . ? C25 C26 H26 120.6 . . ? C27 C26 H26 120.6 . . ? C3 C4 C5 116.6(5) . . ? C3 C4 C9 125.3(5) . . ? C5 C4 C9 118.1(5) . . ? C2 C3 C4 120.3(5) . . ? C2 C3 H3 119.8 . . ? C4 C3 H3 119.8 . . ? N3 C13 C14 122.6(5) . . ? N3 C13 H13 118.7 . . ? C14 C13 H13 118.7 . . ? C8 C9 C4 122.3(5) . . ? C8 C9 H9 118.9 . . ? C4 C9 H9 118.9 . . ? C33 C34 C35 119.0(6) . . ? C33 C34 H34 120.5 . . ? C35 C34 H34 120.5 . . ? C31 C32 C33 120.8(6) . . ? C31 C32 H32 119.6 . . ? C33 C32 H32 119.6 . . ? N8 C43 C42 178.4(11) . . ? C34 C33 C32 120.8(6) . . ? C34 C33 H33 119.6 . . ? C32 C33 H33 119.6 . . ? C43 C42 H42A 109.5 . . ? C43 C42 H42B 109.5 . . ? H42A C42 H42B 109.5 . . ? C43 C42 H42C 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C18 N4 C24 C23 3.9(6) . . . . ? Ru1 N4 C24 C23 -171.0(3) . . . . ? C41 N6 C37 C38 -1.6(6) . . . . ? Ru1 N6 C37 C38 173.7(3) . . . . ? C41 N6 C37 N7 178.0(4) . . . . ? Ru1 N6 C37 N7 -6.7(5) . . . . ? C29 N7 C37 N6 61.2(5) . . . . ? C30 N7 C37 N6 -152.1(4) . . . . ? C29 N7 C37 C38 -119.2(4) . . . . ? C30 N7 C37 C38 27.5(6) . . . . ? C37 N6 C41 C40 0.3(6) . . . . ? Ru1 N6 C41 C40 -175.1(3) . . . . ? C12 N2 C6 C7 -1.1(6) . . . . ? Ru1 N2 C6 C7 179.4(3) . . . . ? C12 N2 C6 C5 176.3(4) . . . . ? Ru1 N2 C6 C5 -3.2(5) . . . . ? N4 C24 C23 C22 -0.6(7) . . . . ? C24 N4 C18 C19 -5.0(6) . . . . ? Ru1 N4 C18 C19 170.7(3) . . . . ? C24 N4 C18 C17 175.3(4) . . . . ? Ru1 N4 C18 C17 -9.0(4) . . . . ? C13 N3 C17 C16 0.2(6) . . . . ? Ru1 N3 C17 C16 -169.7(3) . . . . ? C13 N3 C17 C18 -178.8(4) . . . . ? Ru1 N3 C17 C18 11.3(4) . . . . ? N4 C18 C17 N3 -1.5(5) . . . . ? C19 C18 C17 N3 178.8(4) . . . . ? N4 C18 C17 C16 179.4(4) . . . . ? C19 C18 C17 C16 -0.3(6) . . . . ? C1 N1 C5 C4 4.3(7) . . . . ? Ru1 N1 C5 C4 -177.7(4) . . . . ? C1 N1 C5 C6 -172.9(4) . . . . ? Ru1 N1 C5 C6 5.1(5) . . . . ? N2 C6 C5 N1 -1.3(6) . . . . ? C7 C6 C5 N1 176.2(4) . . . . ? N2 C6 C5 C4 -178.6(4) . . . . ? C7 C6 C5 C4 -1.1(7) . . . . ? N6 C41 C40 C39 1.2(7) . . . . ? C38 C39 C40 C41 -1.4(7) . . . . ? N2 C6 C7 C10 1.6(7) . . . . ? C5 C6 C7 C10 -175.6(4) . . . . ? N2 C6 C7 C8 -178.5(4) . . . . ? C5 C6 C7 C8 4.2(7) . . . . ? C25 N5 C29 C28 -2.4(7) . . . . ? Ru1 N5 C29 C28 176.7(4) . . . . ? C25 N5 C29 N7 178.7(4) . . . . ? Ru1 N5 C29 N7 -2.2(5) . . . . ? C37 N7 C29 N5 -55.9(5) . . . . ? C30 N7 C29 N5 157.2(4) . . . . ? C37 N7 C29 C28 125.1(5) . . . . ? C30 N7 C29 C28 -21.8(6) . . . . ? N4 C18 C19 C22 2.9(6) . . . . ? C17 C18 C19 C22 -177.4(4) . . . . ? N4 C18 C19 C20 -178.1(4) . . . . ? C17 C18 C19 C20 1.6(6) . . . . ? C40 C39 C38 C37 0.1(7) . . . . ? N6 C37 C38 C39 1.5(6) . . . . ? N7 C37 C38 C39 -178.1(4) . . . . ? C29 N7 C30 C31 -164.2(4) . . . . ? C37 N7 C30 C31 48.6(6) . . . . ? C5 N1 C1 C2 -3.3(7) . . . . ? Ru1 N1 C1 C2 179.1(4) . . . . ? C24 C23 C22 C19 -1.7(7) . . . . ? C18 C19 C22 C23 0.5(7) . . . . ? C20 C19 C22 C23 -178.4(5) . . . . ? N3 C17 C16 C15 -0.1(7) . . . . ? C18 C17 C16 C15 178.8(4) . . . . ? N3 C17 C16 C21 -179.5(4) . . . . ? C18 C17 C16 C21 -0.5(6) . . . . ? C6 N2 C12 C11 -0.3(7) . . . . ? Ru1 N2 C12 C11 179.1(4) . . . . ? C35 C36 C31 C32 -0.1(8) . . . . ? C35 C36 C31 C30 177.5(5) . . . . ? N7 C30 C31 C32 -154.2(5) . . . . ? N7 C30 C31 C36 28.1(7) . . . . ? C17 C16 C21 C20 -0.1(7) . . . . ? C15 C16 C21 C20 -179.4(5) . . . . ? C6 C7 C10 C11 -0.7(7) . . . . ? C8 C7 C10 C11 179.4(5) . . . . ? C29 N5 C25 C26 2.0(7) . . . . ? Ru1 N5 C25 C26 -177.1(4) . . . . ? C31 C36 C35 C34 -0.1(9) . . . . ? N1 C1 C2 C3 0.1(9) . . . . ? C26 C27 C28 C29 -0.8(9) . . . . ? N5 C29 C28 C27 1.8(8) . . . . ? N7 C29 C28 C27 -179.3(5) . . . . ? C16 C21 C20 C19 1.5(8) . . . . ? C22 C19 C20 C21 176.7(5) . . . . ? C18 C19 C20 C21 -2.2(7) . . . . ? C17 C16 C15 C14 0.2(7) . . . . ? C21 C16 C15 C14 179.5(5) . . . . ? C7 C10 C11 C12 -0.6(8) . . . . ? N2 C12 C11 C10 1.1(8) . . . . ? C10 C7 C8 C9 176.5(6) . . . . ? C6 C7 C8 C9 -3.3(8) . . . . ? C16 C15 C14 C13 -0.4(9) . . . . ? N5 C25 C26 C27 -1.0(9) . . . . ? C28 C27 C26 C25 0.3(9) . . . . ? N1 C5 C4 C3 -2.0(8) . . . . ? C6 C5 C4 C3 175.2(5) . . . . ? N1 C5 C4 C9 -180.0(5) . . . . ? C6 C5 C4 C9 -2.8(7) . . . . ? C1 C2 C3 C4 2.3(10) . . . . ? C5 C4 C3 C2 -1.4(9) . . . . ? C9 C4 C3 C2 176.4(6) . . . . ? C17 N3 C13 C14 -0.4(7) . . . . ? Ru1 N3 C13 C14 167.6(4) . . . . ? C15 C14 C13 N3 0.5(9) . . . . ? C7 C8 C9 C4 -0.7(10) . . . . ? C3 C4 C9 C8 -174.0(6) . . . . ? C5 C4 C9 C8 3.8(9) . . . . ? C36 C35 C34 C33 -0.5(10) . . . . ? C36 C31 C32 C33 1.1(8) . . . . ? C30 C31 C32 C33 -176.7(5) . . . . ? C35 C34 C33 C32 1.5(10) . . . . ? C31 C32 C33 C34 -1.8(10) . . . . ? _refine_diff_density_max 1.812 _refine_diff_density_min -1.171 _refine_diff_density_rms 0.113 _shelx_res_file ; TITL 2036sb15_0m_a.res in P2(1)/c 2036sb15_0m.res created by SHELXL-2018/3 at 16:49:07 on 02-Nov-2022 REM Old TITL 2036SB15_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.136, Rweak 0.005, Alpha 0.052 REM 0.587 for 552 systematic absences, Orientation as input REM Formula found by SHELXT: C42 N7 F10B P2 Ru CELL 0.71073 19.5843 9.4572 23.4404 90 96.134 90 ZERR 4 0.0008 0.0004 0.001 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H F N P Ru UNIT 172 136 48 32 8 4 EADP F11 F7 F8 F9 F10 DANG 2.18 0.002 F7 F8 DANG 2.18 0.002 F10 F7 DANG 2.18 0.002 F9 F8 L.S. 20 PLAN 10 SIZE 0.4 0.25 0.2 TEMP 23(2) CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 2 1 2 OMIT 2 1 1 REM REM REM WGHT 0.112800 6.893000 FVAR 0.22942 RU1 6 0.268970 0.650095 0.617013 11.00000 0.03437 0.03195 = 0.03318 -0.00059 0.00925 -0.00165 P2 5 0.087560 0.363025 0.374005 11.00000 0.05771 0.06733 = 0.05903 -0.00133 0.01099 0.00797 P1 5 0.428970 0.318823 0.864129 11.00000 0.06686 0.06176 = 0.07194 -0.00470 0.02543 0.00785 N6 4 0.275797 0.842877 0.660653 11.00000 0.03452 0.03245 = 0.03551 0.00215 0.00593 -0.00167 N4 4 0.356828 0.568634 0.662529 11.00000 0.03825 0.03464 = 0.03536 0.00137 0.01013 0.00070 N2 4 0.320198 0.729583 0.551756 11.00000 0.04253 0.03883 = 0.03733 -0.00262 0.01392 -0.00621 N5 4 0.210434 0.583791 0.681142 11.00000 0.03846 0.03043 = 0.03660 0.00144 0.01219 -0.00018 N3 4 0.275923 0.457334 0.576061 11.00000 0.04603 0.03599 = 0.03607 -0.00270 0.01085 -0.00420 N1 4 0.186228 0.717451 0.560459 11.00000 0.03886 0.04232 = 0.03641 -0.00135 0.00549 -0.00428 N7 4 0.164023 0.812215 0.685918 11.00000 0.03225 0.03179 = 0.04629 -0.00095 0.00861 0.00147 C24 1 0.394199 0.618546 0.709006 11.00000 0.05115 0.04393 = 0.03761 0.00285 0.00779 -0.00204 AFIX 43 H24 2 0.377577 0.694887 0.728374 11.00000 -1.20000 AFIX 0 F3 3 0.407504 0.471473 0.842733 11.00000 0.12346 0.07528 = 0.07942 0.00652 0.02600 0.02413 C37 1 0.225497 0.890107 0.690241 11.00000 0.03411 0.02991 = 0.03709 0.00290 0.00557 0.00117 C41 1 0.334145 0.920538 0.663435 11.00000 0.03705 0.04288 = 0.04741 0.00690 0.00702 -0.00409 AFIX 43 H41 2 0.369456 0.889393 0.643014 11.00000 -1.20000 AFIX 0 C6 1 0.277815 0.792279 0.509046 11.00000 0.05271 0.03722 = 0.03470 -0.00389 0.00685 -0.00699 C23 1 0.457051 0.560370 0.729426 11.00000 0.05560 0.05777 = 0.04181 0.00776 -0.00412 0.00281 AFIX 43 H23 2 0.481772 0.598861 0.761819 11.00000 -1.20000 AFIX 0 F2 3 0.503469 0.345301 0.848989 11.00000 0.06592 0.12489 = 0.13153 -0.00611 0.01743 -0.00807 C18 1 0.380929 0.450738 0.637121 11.00000 0.04175 0.03634 = 0.04001 0.00123 0.01482 0.00282 C17 1 0.338034 0.391990 0.590278 11.00000 0.04789 0.03671 = 0.04404 -0.00058 0.02081 0.00103 C5 1 0.206111 0.786690 0.514300 11.00000 0.05019 0.04128 = 0.03493 -0.00201 0.00306 -0.00221 C39 1 0.292928 1.088281 0.725890 11.00000 0.05686 0.03168 = 0.05734 -0.00907 -0.00323 -0.00116 AFIX 43 H39 2 0.298960 1.169785 0.748055 11.00000 -1.20000 AFIX 0 C40 1 0.343845 1.041706 0.694522 11.00000 0.04513 0.03942 = 0.05462 0.00178 -0.00068 -0.01259 AFIX 43 H40 2 0.384522 1.092453 0.694530 11.00000 -1.20000 AFIX 0 F6 3 0.410241 0.260669 0.802380 11.00000 0.10487 0.11820 = 0.12584 -0.05699 -0.00580 -0.00966 C7 1 0.301984 0.854596 0.460745 11.00000 0.07981 0.04069 = 0.03627 -0.00318 0.01737 -0.01329 F12 3 0.014042 0.412209 0.384405 11.00000 0.09053 0.10816 = 0.21579 0.04683 0.07064 0.04519 C29 1 0.167010 0.671708 0.704619 11.00000 0.03825 0.03174 = 0.04374 -0.00161 0.01187 -0.00156 F1 3 0.453718 0.168689 0.888301 11.00000 0.16798 0.07444 = 0.16447 0.02167 0.05971 0.02817 F5 3 0.448752 0.379258 0.927090 11.00000 0.21327 0.14990 = 0.07840 -0.01842 -0.00742 0.08542 C19 1 0.444608 0.389728 0.655462 11.00000 0.04700 0.04455 = 0.04805 0.00881 0.01773 0.00967 C38 1 0.232976 1.012422 0.723953 11.00000 0.04089 0.03456 = 0.05341 -0.00418 0.00054 0.00615 AFIX 43 H38 2 0.197738 1.041943 0.744794 11.00000 -1.20000 AFIX 0 C30 1 0.100693 0.890466 0.693845 11.00000 0.03842 0.04342 = 0.06021 -0.00021 0.01580 0.00523 AFIX 23 H30A 2 0.100947 0.913154 0.734223 11.00000 -1.20000 H30B 2 0.061710 0.829000 0.683384 11.00000 -1.20000 AFIX 0 C36 1 0.116807 1.047517 0.607999 11.00000 0.05269 0.04714 = 0.06920 0.00569 0.01187 0.00715 AFIX 43 H36 2 0.143736 0.977990 0.593466 11.00000 -1.20000 AFIX 0 C1 1 0.119427 0.697849 0.562945 11.00000 0.04372 0.06148 = 0.04625 0.00088 0.00229 -0.00663 AFIX 43 H1 2 0.105199 0.646261 0.593317 11.00000 -1.20000 AFIX 0 C22 1 0.483179 0.447672 0.702781 11.00000 0.05199 0.06135 = 0.05266 0.01384 0.00609 0.01159 AFIX 43 H22 2 0.525906 0.410468 0.716029 11.00000 -1.20000 AFIX 0 C27 1 0.130253 0.486713 0.763267 11.00000 0.06842 0.04796 = 0.06060 0.01036 0.03212 -0.00426 AFIX 43 H27 2 0.103211 0.454190 0.790808 11.00000 -1.20000 AFIX 0 C16 1 0.359268 0.272430 0.561781 11.00000 0.06145 0.04000 = 0.05410 -0.00709 0.02584 -0.00313 C12 1 0.386685 0.726923 0.545782 11.00000 0.04680 0.05864 = 0.04891 0.00203 0.01803 -0.00384 AFIX 43 H12 2 0.416371 0.685037 0.574517 11.00000 -1.20000 AFIX 0 C31 1 0.090562 1.025649 0.659616 11.00000 0.03682 0.04209 = 0.05510 -0.00304 -0.00083 0.00417 C21 1 0.424883 0.212458 0.580589 11.00000 0.06813 0.04705 = 0.07086 -0.00304 0.03789 0.01363 AFIX 43 H21 2 0.439710 0.132907 0.562106 11.00000 -1.20000 AFIX 0 F4 3 0.353511 0.295291 0.879933 11.00000 0.09165 0.14880 = 0.24039 0.02967 0.08998 0.00151 C10 1 0.372167 0.848121 0.456183 11.00000 0.07689 0.05441 = 0.04716 -0.00177 0.02803 -0.01778 AFIX 43 H10 2 0.390201 0.887184 0.424607 11.00000 -1.20000 AFIX 0 C25 1 0.214308 0.449119 0.700046 11.00000 0.05812 0.03426 = 0.05689 0.00340 0.02434 0.00301 AFIX 43 H25 2 0.245184 0.388454 0.684993 11.00000 -1.20000 AFIX 0 C35 1 0.103585 1.171166 0.577733 11.00000 0.06697 0.05967 = 0.07755 0.02133 0.00344 -0.00278 AFIX 43 H35 2 0.121703 1.184470 0.543036 11.00000 -1.20000 AFIX 0 C2 1 0.069918 0.752149 0.521466 11.00000 0.04473 0.10059 = 0.05936 0.00365 -0.00299 -0.00279 AFIX 43 H2 2 0.023520 0.736779 0.524398 11.00000 -1.20000 AFIX 0 C28 1 0.125895 0.623779 0.745215 11.00000 0.05441 0.04513 = 0.05636 0.00245 0.02796 0.00024 AFIX 43 H28 2 0.095286 0.685256 0.760156 11.00000 -1.20000 AFIX 0 C20 1 0.465380 0.269170 0.624480 11.00000 0.05737 0.04789 = 0.06304 0.00589 0.02244 0.01321 AFIX 43 H20 2 0.508210 0.229072 0.635123 11.00000 -1.20000 AFIX 0 F11 3 0.159339 0.306176 0.361390 11.00000 0.14271 0.17430 = 0.22369 -0.01335 0.05139 0.03545 C15 1 0.313670 0.218322 0.516519 11.00000 0.08456 0.04676 = 0.05925 -0.01693 0.02729 -0.00569 AFIX 43 H15 2 0.325304 0.138817 0.496302 11.00000 -1.20000 AFIX 0 C11 1 0.414141 0.783891 0.498513 11.00000 0.05797 0.07064 = 0.06296 0.00141 0.03132 -0.01074 AFIX 43 H11 2 0.461093 0.778133 0.495814 11.00000 -1.20000 AFIX 0 C8 1 0.253693 0.920890 0.418865 11.00000 0.09642 0.06109 = 0.04048 0.01172 0.01329 -0.00937 AFIX 43 H8 2 0.269251 0.966912 0.387660 11.00000 -1.20000 AFIX 0 C14 1 0.252757 0.283656 0.502902 11.00000 0.08157 0.06417 = 0.05703 -0.02565 0.01208 -0.01698 AFIX 43 H14 2 0.222394 0.249084 0.472927 11.00000 -1.20000 AFIX 0 C26 1 0.175342 0.397315 0.740047 11.00000 0.07698 0.03671 = 0.06680 0.01131 0.02933 -0.00209 AFIX 43 H26 2 0.179137 0.303213 0.751466 11.00000 -1.20000 AFIX 0 C4 1 0.159139 0.846601 0.471007 11.00000 0.06574 0.06344 = 0.04301 0.00188 -0.00535 -0.00146 C3 1 0.089909 0.827803 0.476647 11.00000 0.06385 0.10060 = 0.06019 0.00996 -0.01963 0.00595 AFIX 43 H3 2 0.056996 0.867029 0.449707 11.00000 -1.20000 AFIX 0 C13 1 0.234924 0.402540 0.533368 11.00000 0.05569 0.05107 = 0.05116 -0.01216 0.00912 -0.01070 AFIX 43 H13 2 0.192491 0.444798 0.523185 11.00000 -1.20000 AFIX 0 C9 1 0.186179 0.917113 0.424301 11.00000 0.09946 0.07339 = 0.04466 0.01574 -0.00527 0.00135 AFIX 43 H9 2 0.155935 0.961865 0.396764 11.00000 -1.20000 AFIX 0 C34 1 0.063817 1.274891 0.598480 11.00000 0.07948 0.04591 = 0.09375 0.00580 -0.02155 0.00538 AFIX 43 H34 2 0.055185 1.358712 0.578240 11.00000 -1.20000 AFIX 0 N8 4 0.349311 -0.186841 0.819861 11.00000 0.15922 0.09057 = 0.08134 0.01349 0.04280 0.03774 C32 1 0.051075 1.130476 0.680013 11.00000 0.05932 0.05862 = 0.07023 -0.00932 0.00071 0.02038 AFIX 43 H32 2 0.033514 1.118524 0.715025 11.00000 -1.20000 AFIX 0 C43 1 0.324062 -0.117908 0.849285 11.00000 0.09332 0.06877 = 0.08272 0.02726 0.02699 0.02094 C33 1 0.037188 1.253211 0.649156 11.00000 0.08377 0.05161 = 0.10256 -0.01157 -0.01330 0.02744 AFIX 43 H33 2 0.009337 1.321955 0.663089 11.00000 -1.20000 AFIX 0 C42 1 0.293261 -0.027213 0.887707 11.00000 0.15061 0.07843 = 0.11678 0.01412 0.05788 0.03799 AFIX 137 H42A 2 0.263267 0.038386 0.866161 11.00000 -1.50000 H42B 2 0.328429 0.023885 0.910818 11.00000 -1.50000 H42C 2 0.267319 -0.082752 0.912051 11.00000 -1.50000 AFIX 0 F10 3 0.055986 0.276526 0.320410 11.00000 0.14271 0.17430 = 0.22369 -0.01335 0.05139 0.03545 F9 3 0.093739 0.494459 0.333878 11.00000 0.14271 0.17430 = 0.22369 -0.01335 0.05139 0.03545 F8 3 0.122347 0.445401 0.424009 11.00000 0.14271 0.17430 = 0.22369 -0.01335 0.05139 0.03545 F7 3 0.081316 0.231810 0.411409 11.00000 0.14271 0.17430 = 0.22369 -0.01335 0.05139 0.03545 HKLF 4 REM 2036sb15_0m_a.res in P2(1)/c REM wR2 = 0.2050, GooF = S = 1.050, Restrained GooF = 1.050 for all data REM R1 = 0.0653 for 8339 Fo > 4sig(Fo) and 0.0858 for all 11077 data REM 572 parameters refined using 3 restraints END WGHT 0.1128 6.8932 REM Highest difference peak 1.812, deepest hole -1.171, 1-sigma level 0.113 Q1 1 0.0581 0.1976 0.3770 11.00000 0.05 1.81 Q2 1 0.0983 0.3276 0.4436 11.00000 0.05 1.79 Q3 1 0.1166 0.5211 0.3824 11.00000 0.05 1.20 Q4 1 0.1008 0.5346 0.3679 11.00000 0.05 1.08 Q5 1 0.0863 0.3581 0.3025 11.00000 0.05 0.90 Q6 1 0.1056 0.3732 0.3131 11.00000 0.05 0.82 Q7 1 0.3803 0.3273 0.8962 11.00000 0.05 0.70 Q8 1 0.1555 0.4608 0.4153 11.00000 0.05 0.64 Q9 1 0.0388 0.4122 0.3210 11.00000 0.05 0.61 Q10 1 0.4020 0.5037 0.8404 11.00000 0.05 0.49 ; 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104.09 3.50 -2 -6 0 97.19 4.00 2 -6 0 91.89 3.50 2 6 0 106.79 3.40 2 6 0 103.69 4.30 -2 6 0 100.69 4.30 -2 6 0 96.09 3.90 2 6 0 98.69 3.50 -2 6 0 104.79 4.00 -3 -6 0 29.20 2.30 -3 -6 0 29.10 2.40 -3 -6 0 30.20 1.80 3 -6 0 28.00 1.60 3 6 0 31.10 1.40 -3 6 0 26.80 1.90 3 6 0 29.40 2.30 -3 6 0 30.00 2.60 -3 6 0 25.50 2.00 -4 -6 0 19.00 2.00 4 -6 0 14.40 1.20 -4 -6 0 16.40 1.40 4 6 0 17.30 2.20 4 6 0 18.80 0.90 -4 6 0 22.80 2.10 -4 6 0 15.30 2.20 -4 6 0 21.00 2.00 -5 -6 0 217.08 7.30 -5 -6 0 217.48 6.40 5 6 0 216.78 7.50 -5 6 0 232.08 8.20 -5 6 0 217.38 7.20 -5 6 0 207.78 6.50 -6 -6 0 308.37 8.60 -6 6 0 321.67 9.70 6 6 0 322.07 10.00 -6 6 0 307.17 10.70 -6 6 0 310.97 8.70 -7 -6 0 384.36 10.50 -7 6 0 401.76 13.00 -7 6 0 396.66 10.50 7 6 0 388.66 11.80 -7 6 0 409.76 11.70 -8 -6 0 67.19 2.80 -8 6 0 67.39 3.10 8 6 0 67.79 4.00 -9 -6 0 223.88 6.50 -9 6 0 228.08 6.80 9 6 0 226.48 8.40 -10 -6 0 15.50 1.40 -10 6 0 20.40 2.00 10 6 0 16.60 2.60 -10 6 0 13.40 2.80 -11 -6 0 164.58 5.00 -11 6 0 172.18 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33.10 3.20 -2 -8 0 1.00 1.20 -2 8 0 0.30 1.10 2 8 0 0.00 1.10 -3 -8 0 27.60 2.90 3 8 0 27.70 3.30 -3 8 0 18.50 2.40 -4 -8 0 7.20 1.90 4 8 0 11.50 2.40 -4 8 0 4.80 1.20 -4 8 0 7.60 1.80 -5 -8 0 41.90 3.40 -5 8 0 51.79 3.20 5 8 0 49.20 3.60 -6 -8 0 49.20 3.50 -6 8 0 50.89 3.10 6 8 0 50.99 3.80 -7 -8 0 -1.40 1.30 -7 8 0 0.10 0.90 7 8 0 -0.20 1.30 -8 -8 0 0.80 1.50 8 8 0 2.80 1.70 -8 8 0 1.80 1.20 -9 -8 0 4.10 1.90 -9 8 0 6.80 1.50 9 8 0 8.10 2.20 -10 -8 0 1.70 1.80 10 8 0 1.30 1.60 -10 8 0 0.80 1.20 -11 -8 0 -2.50 1.40 11 8 0 -1.10 1.30 -11 8 0 0.60 1.10 -12 -8 0 -0.20 1.60 -12 8 0 0.40 1.10 12 8 0 -1.00 1.60 -13 -8 0 1.50 1.70 13 8 0 -3.20 1.20 -13 8 0 2.00 1.30 -14 -8 0 3.00 2.10 14 8 0 1.30 1.80 -15 -8 0 3.60 2.20 15 8 0 4.80 2.20 -16 -8 0 1.30 1.80 16 8 0 2.60 2.20 -17 -8 0 2.30 2.00 17 8 0 5.40 2.50 -18 -8 0 -2.00 1.60 18 8 0 -1.20 2.00 -19 -8 0 -0.10 2.10 19 8 0 1.50 2.30 -20 -8 0 -0.10 2.20 20 8 0 -0.60 2.10 0 9 0 -0.50 1.10 1 9 0 22.00 2.90 -1 9 0 16.50 2.50 2 9 0 54.99 4.00 -2 9 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24.70 3.80 -7 10 0 28.10 3.30 -8 -10 0 28.30 3.80 -8 10 0 33.60 3.60 8 10 0 25.00 3.80 -9 -10 0 83.99 5.60 -9 10 0 109.59 5.30 9 10 0 93.79 6.30 -10 -10 0 6.90 2.40 -10 10 0 7.60 1.90 10 10 0 5.50 2.40 -11 -10 0 68.89 5.50 11 10 0 88.09 6.20 -12 -10 0 -2.30 1.90 12 10 0 1.60 1.90 -13 -10 0 34.00 4.60 13 10 0 43.10 5.70 -14 -10 0 0.80 2.20 14 10 0 0.90 2.10 -15 -10 0 30.40 4.60 15 10 0 40.50 5.60 -16 -10 0 -1.30 2.00 16 10 0 5.30 2.80 0 11 0 2.10 1.70 1 11 0 66.79 4.90 -1 11 0 73.99 4.90 2 11 0 6.30 2.40 -2 11 0 11.10 2.50 -3 11 0 38.10 4.20 3 11 0 42.80 4.90 -4 11 0 12.10 2.50 4 11 0 8.10 2.70 -5 11 0 17.60 3.00 5 11 0 21.10 3.70 -6 11 0 16.70 2.80 6 11 0 18.60 3.60 -7 11 0 11.80 2.60 7 11 0 11.80 3.10 -8 11 0 13.40 2.80 8 11 0 10.80 3.00 9 11 0 12.30 3.10 -10 -11 0 25.80 4.00 10 11 0 28.00 4.40 -11 -11 0 26.50 4.00 11 11 0 19.30 3.90 -12 -11 0 24.80 4.30 12 11 0 23.70 4.50 -13 -11 0 -1.30 2.00 13 11 0 0.90 2.20 0 12 0 1.90 1.80 -1 12 0 -0.10 1.60 1 12 0 -0.50 1.60 2 12 0 1.30 1.90 -2 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2.90 19 -2 -4 2.70 1.70 -19 -2 4 3.60 1.80 -19 2 4 4.10 1.30 19 2 -4 4.60 2.10 18 -2 -4 6.90 1.90 -18 -2 4 4.40 1.70 18 2 -4 2.40 1.70 -18 2 4 3.30 1.10 17 -2 -4 13.20 2.50 -17 -2 4 17.60 2.80 -17 2 4 14.10 1.80 17 2 -4 18.60 3.00 16 -2 -4 0.60 1.70 16 -2 -4 0.60 1.20 -16 -2 4 3.80 1.70 16 2 -4 3.20 1.60 -16 2 4 1.50 0.90 -15 -2 4 4.60 1.70 15 -2 -4 3.90 1.40 -15 -2 4 3.80 2.90 15 -2 -4 3.10 1.70 -15 2 4 5.10 1.10 15 2 -4 4.20 1.80 -14 -2 4 96.09 12.70 14 -2 -4 107.69 5.60 14 -2 -4 102.79 4.80 -14 -2 4 106.99 4.90 14 2 -4 107.19 5.40 -14 2 4 101.19 3.80 -14 2 4 102.39 3.20 13 -2 -4 21.50 3.00 -13 -2 4 20.20 8.30 -13 -2 4 23.50 2.60 13 -2 -4 21.40 2.60 -13 2 4 18.30 1.10 -13 2 4 20.00 2.10 -13 2 4 19.30 1.80 13 2 -4 19.50 2.70 -12 -2 4 -3.30 5.40 12 -2 -4 0.90 0.90 -12 -2 4 0.60 1.10 12 -2 -4 1.50 1.30 12 2 -4 0.10 1.00 -12 2 4 -2.10 0.70 -12 2 4 0.70 0.40 -12 2 4 1.00 0.70 -11 -2 4 7.40 1.60 11 -2 -4 10.50 2.00 11 -2 -4 14.70 5.50 11 -2 -4 9.30 1.60 -11 2 4 11.00 1.30 -11 2 4 10.80 0.90 11 2 -4 13.70 2.20 10 -2 -4 659.13 17.70 -10 -2 4 685.73 17.50 -10 -2 4 685.03 16.00 -10 -2 4 682.73 16.00 10 -2 -4 651.63 16.90 10 -2 -4 628.84 28.50 -10 2 4 664.43 16.50 -10 2 4 680.73 15.90 10 2 -4 679.83 17.70 -9 -2 4 2.30 0.40 9 -2 -4 3.10 3.30 9 -2 -4 -0.80 0.80 -9 -2 4 1.00 1.00 -9 -2 4 3.00 0.40 -9 2 4 1.90 0.50 -9 2 4 2.00 0.70 9 2 -4 2.00 1.30 8 -2 -4 157.88 5.20 -8 -2 4 149.88 4.20 -8 -2 4 152.18 5.30 -8 -2 4 160.38 4.30 -8 2 4 152.58 4.50 -8 2 4 154.58 4.40 8 2 -4 144.89 5.50 -7 -2 4 15.30 1.00 -7 -2 4 16.00 1.00 7 -2 -4 19.40 1.80 -7 -2 4 21.40 2.10 -7 2 4 15.20 1.00 -7 2 4 15.70 1.20 7 2 -4 18.10 2.10 -6 -2 4 137.69 4.00 -6 -2 4 133.89 4.60 -6 -2 4 138.19 4.10 -6 2 4 133.69 4.50 -6 2 4 134.39 3.90 -6 2 4 133.29 4.10 -5 -2 4 3.70 0.70 5 -2 -4 4.70 0.60 -5 -2 4 3.40 0.50 -5 -2 4 4.20 0.30 -5 -2 4 4.60 1.00 -5 -2 4 4.30 0.60 5 2 -4 3.80 0.30 -5 2 4 4.10 0.80 -5 2 4 3.90 0.50 -5 2 4 4.00 0.80 5 2 -4 3.80 0.30 -4 -2 4 317.57 8.90 -4 -2 4 336.77 8.90 -4 -2 4 341.97 8.70 4 -2 -4 329.07 8.50 -4 -2 4 338.77 8.00 -4 -2 4 346.77 9.30 -4 2 4 324.07 8.70 4 2 -4 332.17 8.40 -4 2 4 329.17 8.80 -4 2 4 326.27 8.40 4 2 -4 335.17 8.40 3 -2 -4 614.74 15.60 -3 -2 4 642.54 16.20 3 -2 -4 602.54 15.30 -3 -2 4 632.84 15.50 3 -2 -4 627.84 15.90 -3 -2 4 646.54 14.90 3 2 -4 637.84 15.10 3 2 -4 628.94 14.60 3 2 -4 623.14 15.40 -3 2 4 631.64 15.30 -3 2 4 621.24 15.30 -3 2 4 612.14 15.20 2 -2 -4 1055.59 25.50 2 -2 -4 1059.69 25.50 2 -2 -4 1063.19 25.50 -2 -2 4 1081.39 26.90 -2 -2 4 1041.00 25.00 -2 2 4 1052.29 25.20 -2 2 4 1065.79 25.40 2 2 -4 1075.29 26.20 2 2 -4 1098.79 26.00 2 2 -4 1061.89 24.90 -2 2 4 1020.80 25.20 2 2 -4 1107.59 25.80 -1 -2 4 2007.10 47.50 -1 -2 4 1989.90 49.00 1 -2 -4 1994.70 47.80 1 -2 -4 1992.60 46.80 1 -2 -4 1952.00 46.80 -1 2 4 2000.70 48.50 -1 2 4 1998.00 46.70 1 2 -4 2031.70 47.70 1 2 -4 2041.20 48.20 1 2 -4 2048.79 46.60 -1 2 4 2002.70 58.89 0 -2 4 9.00 1.60 0 -2 4 3.80 0.50 0 -2 -4 4.10 0.50 0 -2 -4 4.30 0.50 0 -2 -4 4.70 0.50 0 2 4 4.20 0.50 0 2 4 4.70 0.40 0 2 4 4.50 0.50 0 2 -4 8.40 1.50 0 2 -4 5.40 0.60 1 -2 4 1005.80 23.60 -1 -2 -4 1024.70 23.50 -1 -2 -4 1007.60 23.60 -1 -2 -4 1032.90 24.00 1 -2 4 960.40 25.50 1 2 4 994.80 23.60 -1 2 -4 1015.40 26.20 1 2 4 981.60 24.00 -1 2 -4 1018.00 23.70 1 2 4 1003.80 23.50 -2 -2 -4 17.50 0.80 2 -2 4 15.90 1.00 -2 -2 -4 19.30 0.70 2 -2 4 15.30 0.60 -2 -2 -4 16.60 0.80 -2 2 -4 20.80 2.30 -2 2 -4 15.50 0.80 -3 -2 -4 59.79 1.60 -3 -2 -4 59.39 1.70 -3 -2 -4 56.99 1.80 3 2 4 58.79 1.80 -3 2 -4 57.69 1.70 3 2 4 50.79 3.10 -3 2 -4 61.19 2.80 -4 -2 -4 359.46 8.80 4 -2 4 332.27 9.80 -4 2 -4 364.96 8.40 4 2 4 339.47 10.70 -4 2 -4 369.46 8.60 -5 -2 -4 25.90 1.00 5 -2 4 26.80 2.60 5 2 4 24.30 2.80 -6 -2 -4 131.09 3.20 -6 -2 -4 122.99 8.80 6 -2 4 118.29 5.10 6 2 4 114.79 5.40 -7 -2 -4 39.10 6.50 7 -2 4 45.00 3.10 7 2 4 39.30 3.10 8 -2 4 203.88 7.40 -8 -2 -4 199.78 13.60 8 2 4 185.28 6.20 8 2 4 198.78 7.80 8 2 4 201.68 7.40 9 -2 4 26.90 3.10 9 -2 4 25.60 2.70 -9 -2 -4 30.70 7.70 9 2 4 26.80 3.30 9 2 4 32.30 3.50 9 2 4 27.00 2.20 -10 -2 -4 98.99 11.90 10 -2 4 80.79 4.10 10 -2 4 83.79 4.80 10 2 4 81.39 4.80 10 2 4 86.79 4.80 10 2 4 91.99 4.10 11 -2 4 28.30 3.00 11 -2 4 20.40 1.70 11 -2 4 26.50 3.40 -11 2 -4 21.80 1.30 11 2 4 26.40 2.70 11 2 4 23.00 3.30 11 2 4 23.90 3.30 12 -2 4 2.50 1.00 12 -2 4 1.30 1.30 12 -2 4 -0.10 1.10 -12 2 -4 -0.20 0.50 12 2 4 1.40 1.10 12 2 4 2.10 1.40 12 2 4 -1.30 1.00 13 -2 4 31.10 2.20 13 -2 4 34.60 3.00 13 -2 4 50.69 4.90 -13 2 -4 38.20 1.80 13 2 4 40.10 4.60 13 2 4 41.20 4.50 13 2 4 41.60 3.10 14 -2 4 2.10 1.40 14 -2 4 3.70 1.30 14 2 4 0.90 1.70 14 2 4 2.90 1.50 -14 2 -4 2.80 0.80 14 2 4 0.30 1.30 15 -2 4 0.50 1.60 15 2 4 -0.50 1.40 -15 2 -4 1.20 0.80 15 2 4 -1.20 1.20 15 2 4 1.00 1.60 16 -2 4 3.30 2.00 16 2 4 0.50 1.60 16 2 4 0.00 1.40 16 2 4 1.80 1.80 17 -2 4 2.30 1.70 17 2 4 4.10 1.90 17 2 4 3.20 1.90 17 2 4 8.10 2.60 18 -2 4 5.10 2.10 18 2 4 4.20 2.10 18 2 4 4.80 2.00 18 2 4 5.20 2.10 19 -2 4 0.60 2.00 19 2 4 4.60 2.40 19 2 4 -0.10 1.70 19 2 4 1.80 1.80 20 -2 4 9.20 2.90 20 2 4 3.90 2.00 21 -2 4 -4.00 1.70 21 2 4 2.00 2.00 22 -2 4 4.10 2.40 23 -2 4 7.10 3.10 -25 -3 4 3.90 2.50 -25 -3 4 7.30 1.90 -25 3 4 6.40 1.90 25 3 -4 10.90 3.40 -24 -3 4 1.50 1.30 24 -3 -4 0.60 1.80 -24 -3 4 0.90 2.10 24 3 -4 1.60 2.00 -24 3 4 -0.80 1.20 -23 -3 4 6.00 1.70 -23 -3 4 5.40 2.40 23 -3 -4 5.60 2.00 -23 3 4 2.90 1.30 23 3 -4 10.10 3.10 -22 -3 4 0.90 1.90 22 -3 -4 0.80 1.40 -22 3 4 0.10 1.00 22 3 -4 -1.40 1.80 21 -3 -4 10.10 2.40 -21 -3 4 8.70 2.50 21 3 -4 8.50 2.80 -21 3 4 6.40 1.50 -20 -3 4 8.20 2.60 20 -3 -4 15.60 2.70 20 3 -4 14.40 3.20 -20 3 4 12.20 1.90 19 -3 -4 22.80 3.00 -19 -3 4 23.20 3.30 -19 3 4 24.00 2.40 19 3 -4 23.40 3.60 18 -3 -4 14.20 2.40 -18 -3 4 13.80 2.80 18 3 -4 13.60 2.90 -18 3 4 14.10 1.80 17 -3 -4 0.40 1.80 17 -3 -4 1.20 1.20 -17 -3 4 0.20 1.40 17 3 -4 1.90 1.60 -17 3 4 0.40 0.80 16 -3 -4 3.90 2.10 16 -3 -4 1.50 1.30 -16 -3 4 -0.10 1.40 16 3 -4 -1.00 1.50 -16 3 4 2.10 1.00 15 -3 -4 5.40 2.30 15 -3 -4 7.50 1.70 -15 -3 4 8.30 2.30 -15 3 4 7.20 1.30 15 3 -4 5.80 2.00 -14 -3 4 38.70 1.60 -14 -3 4 33.30 2.90 14 -3 -4 35.40 2.70 14 3 -4 34.10 3.70 -14 3 4 38.20 2.20 13 -3 -4 27.90 2.90 -13 -3 4 22.90 1.30 -13 -3 4 29.70 3.10 -13 3 4 24.00 1.60 -13 3 4 22.80 1.80 13 3 -4 24.30 3.10 -12 -3 4 19.30 1.20 -12 -3 4 25.00 2.80 12 -3 -4 25.70 2.60 -12 3 4 20.30 1.70 12 3 -4 26.60 3.10 -12 3 4 20.00 1.40 -11 -3 4 90.59 3.00 -11 -3 4 89.09 3.10 -11 -3 4 92.59 4.40 11 -3 -4 93.09 4.00 -11 3 4 96.69 3.30 -11 3 4 88.89 3.30 11 3 -4 91.39 4.60 -10 -3 4 303.27 8.10 -10 -3 4 295.47 9.30 -10 -3 4 305.37 8.20 10 -3 -4 307.87 8.90 10 3 -4 310.67 9.80 -10 3 4 309.57 8.10 -10 3 4 305.87 8.40 -9 -3 4 29.70 1.60 -9 -3 4 28.00 1.50 -9 -3 4 28.50 2.70 9 -3 -4 27.50 2.00 9 3 -4 26.20 2.70 -9 3 4 26.40 1.60 -9 3 4 29.10 1.90 -9 3 4 30.10 1.90 -9 3 4 29.20 1.70 -8 -3 4 6.10 0.40 -8 -3 4 5.20 0.80 -8 -3 4 5.90 0.30 8 -3 -4 7.30 1.20 -8 -3 4 5.90 1.30 -8 -3 4 5.10 0.80 -8 3 4 7.90 1.30 -8 3 4 7.30 0.90 -8 3 4 6.40 1.10 -8 3 4 5.80 0.90 8 3 -4 5.30 1.50 -7 -3 4 327.57 9.50 -7 -3 4 338.17 7.90 -7 -3 4 331.27 8.90 -7 -3 4 334.07 8.30 -7 -3 4 337.47 9.00 -7 3 4 325.57 9.10 7 3 -4 319.57 9.60 -7 3 4 319.07 8.30 -7 3 4 330.37 8.80 -6 -3 4 13.20 1.20 -6 -3 4 13.80 1.20 -6 -3 4 15.50 0.80 -6 -3 4 15.10 1.90 -6 -3 4 12.80 1.30 6 3 -4 16.50 2.00 6 3 -4 14.80 0.70 -6 3 4 17.00 1.70 -6 3 4 14.00 1.10 -6 3 4 16.60 1.20 6 3 -4 13.20 0.60 -6 3 4 16.00 1.20 5 -3 -4 65.59 2.60 -5 -3 4 60.09 2.50 -5 -3 4 65.39 2.80 -5 -3 4 56.99 2.90 -5 -3 4 63.99 2.00 -5 -3 4 65.49 2.90 -5 3 4 63.79 2.80 5 3 -4 62.29 2.00 -5 3 4 58.69 2.30 5 3 -4 65.39 2.30 5 3 -4 63.79 3.00 -5 3 4 68.09 2.40 -5 3 4 65.09 2.40 4 -3 -4 57.69 2.60 -4 -3 4 54.49 2.70 -4 -3 4 55.89 2.90 4 -3 -4 54.69 2.30 -4 -3 4 56.59 1.90 4 -3 -4 53.19 2.80 -4 -3 4 52.29 2.60 -4 3 4 52.59 2.10 4 3 -4 54.79 1.50 4 3 -4 56.99 2.20 -4 3 4 54.59 2.40 -4 3 4 52.49 2.10 -3 -3 4 369.86 10.10 -3 -3 4 382.26 9.50 3 -3 -4 381.76 10.50 -3 -3 4 382.76 10.90 3 -3 -4 367.76 9.80 3 -3 -4 371.26 9.90 -3 -3 4 379.96 11.00 -3 3 4 372.56 9.60 3 3 -4 369.86 9.60 3 3 -4 375.56 9.90 -3 3 4 389.86 9.70 3 3 -4 373.56 9.10 -3 3 4 373.86 9.90 3 3 -4 385.06 9.90 -2 -3 4 459.45 12.10 -2 -3 4 456.75 11.60 2 -3 -4 482.25 12.40 -2 -3 4 461.25 13.60 2 -3 -4 474.45 11.90 2 -3 -4 464.35 11.70 -2 3 4 443.66 11.50 2 3 -4 475.95 12.40 2 3 -4 469.25 11.40 -2 3 4 482.15 11.80 2 3 -4 461.65 12.00 2 3 -4 467.25 12.30 -2 3 4 480.15 11.80 -1 -3 4 344.07 9.00 1 -3 -4 353.16 9.00 1 -3 -4 367.66 9.50 -1 -3 4 360.76 11.40 1 -3 -4 343.87 9.20 -1 3 4 346.17 8.90 1 3 -4 367.86 10.40 1 3 -4 361.36 10.00 -1 3 4 351.36 9.10 1 3 -4 362.86 8.90 0 -3 4 316.57 10.70 0 -3 -4 309.17 8.00 0 -3 -4 317.17 8.30 0 -3 4 314.67 8.00 0 -3 -4 316.27 8.20 0 3 -4 303.77 8.00 0 3 4 325.97 7.80 0 3 -4 308.17 9.70 0 3 -4 314.57 9.30 0 3 4 312.77 7.90 0 3 4 321.47 8.10 1 -3 4 1061.79 27.90 1 -3 4 1052.79 25.10 -1 -3 -4 1014.70 24.80 1 -3 4 1060.79 24.70 -1 -3 -4 1049.79 24.90 -1 -3 -4 1027.60 25.20 -1 3 -4 1068.09 27.40 1 3 4 1012.10 25.10 -1 3 -4 1047.60 24.90 1 3 4 1049.09 24.50 1 3 4 1078.59 24.70 -2 -3 -4 734.73 17.80 -2 -3 -4 756.12 17.80 -2 -3 -4 747.43 18.10 2 -3 4 737.53 19.90 2 -3 4 730.43 17.60 2 -3 4 746.13 18.60 -2 3 -4 750.82 20.70 2 3 4 742.03 17.50 2 3 4 744.43 17.40 2 3 4 742.03 19.50 -2 3 -4 761.52 17.90 -3 -3 -4 162.28 4.20 3 -3 4 160.58 4.30 -3 -3 -4 157.08 4.40 3 -3 4 157.58 5.80 -3 -3 -4 170.08 4.40 3 3 4 155.78 4.40 -3 3 -4 167.48 6.90 -3 3 -4 164.78 4.40 3 3 4 154.78 6.10 -4 -3 -4 6.20 0.60 -4 -3 -4 7.60 0.50 4 -3 4 9.70 1.70 -4 -3 -4 9.30 0.70 4 3 4 7.80 1.20 -4 3 -4 5.90 1.60 -4 3 -4 8.60 0.70 4 3 4 7.40 0.60 4 3 4 10.10 1.90 -5 -3 -4 98.09 2.90 -5 -3 -4 95.99 2.50 5 -3 4 94.09 4.60 -5 -3 -4 99.59 2.60 -5 3 -4 107.79 4.60 5 3 4 94.39 4.80 -5 3 -4 100.29 2.80 5 3 4 96.49 3.70 6 -3 4 37.00 2.90 -6 -3 -4 39.40 1.50 6 3 4 38.90 2.30 -6 3 -4 33.60 2.00 6 3 4 34.80 3.00 -6 3 -4 37.70 1.30 7 -3 4 17.20 2.60 -7 -3 -4 17.00 0.90 7 3 4 17.20 1.90 7 3 4 22.20 2.90 8 -3 4 109.89 5.20 -8 -3 -4 101.69 2.90 8 3 4 94.19 4.10 8 3 4 96.29 5.20 -9 -3 -4 35.30 1.30 9 -3 4 38.00 3.90 9 3 4 35.10 2.40 9 3 4 26.60 3.40 -10 -3 -4 -0.50 2.40 10 -3 4 0.30 1.10 10 -3 4 1.80 1.10 -10 -3 -4 1.20 0.30 -10 -3 -4 1.30 0.30 10 3 4 2.00 1.40 10 3 4 1.10 1.00 10 3 4 1.10 1.20 11 -3 4 28.70 3.60 11 -3 4 24.50 1.80 -11 -3 -4 20.00 5.50 -11 3 -4 27.50 1.50 11 3 4 33.60 3.20 11 3 4 28.20 3.60 11 3 4 32.50 3.90 -12 -3 -4 6.70 5.00 12 -3 4 2.40 1.00 12 -3 4 1.20 1.50 12 3 4 4.70 1.90 -12 3 -4 2.90 0.70 12 3 4 4.90 2.00 12 3 4 1.40 1.30 13 -3 4 15.20 3.10 -13 -3 -4 19.00 6.80 13 3 4 17.90 3.20 -13 3 -4 15.50 1.30 13 3 4 18.80 3.20 13 3 4 17.60 2.60 14 -3 4 136.79 7.20 14 3 4 136.89 7.20 14 3 4 132.69 7.10 14 3 4 135.89 6.20 15 -3 4 23.50 3.80 15 3 4 37.30 4.70 15 3 4 34.70 3.70 15 3 4 38.20 4.80 16 -3 4 1.10 1.60 16 3 4 2.00 1.80 16 3 4 0.70 1.80 16 3 4 2.90 2.10 17 -3 4 8.40 2.80 17 3 4 5.90 2.50 17 3 4 7.00 2.60 17 3 4 10.40 2.70 18 -3 4 -0.70 1.80 18 3 4 1.10 1.80 18 3 4 -1.70 1.90 18 3 4 1.50 1.80 19 -3 4 0.80 2.20 19 3 4 -1.60 1.50 20 -3 4 1.30 2.20 20 3 4 1.30 1.60 21 -3 4 -0.70 2.30 21 3 4 2.70 2.00 22 -3 4 -0.40 2.10 22 3 4 -0.20 1.60 23 -3 4 0.70 2.20 24 -3 4 4.50 3.10 -25 -4 4 0.30 1.20 -25 -4 4 -1.80 2.10 25 4 -4 1.10 2.20 -24 -4 4 14.00 3.30 -24 4 4 17.80 2.50 24 4 -4 14.80 3.70 23 -4 -4 6.80 2.30 -23 -4 4 6.80 2.70 -23 4 4 8.80 1.90 23 4 -4 6.60 2.70 22 -4 -4 45.50 3.80 -22 -4 4 45.50 5.10 -22 4 4 48.40 3.10 22 4 -4 41.80 5.40 21 -4 -4 3.70 1.80 -21 -4 4 3.10 2.00 21 4 -4 3.70 2.20 -21 4 4 4.30 1.50 20 -4 -4 19.60 3.00 -20 -4 4 17.00 3.30 20 4 -4 21.90 3.80 -20 4 4 18.70 2.30 19 -4 -4 28.80 3.40 -19 -4 4 25.60 3.70 -19 4 4 27.90 2.70 19 4 -4 25.40 4.00 18 -4 -4 31.90 3.50 -18 -4 4 32.40 3.90 18 4 -4 27.40 4.00 -18 4 4 29.60 2.40 17 -4 -4 159.58 6.60 -17 -4 4 159.38 7.30 17 4 -4 172.98 8.10 -17 4 4 168.78 5.80 16 -4 -4 21.40 2.70 -16 -4 4 19.60 3.00 16 4 -4 20.50 3.20 -16 4 4 24.70 2.00 15 -4 -4 74.29 4.10 -15 -4 4 79.09 4.70 -15 4 4 76.69 3.50 15 4 -4 68.89 4.80 14 -4 -4 34.90 2.80 -14 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2.40 21 6 -4 2.40 2.20 -21 6 4 8.30 1.90 -20 -6 4 29.60 4.20 -20 6 4 29.90 3.10 20 6 -4 28.70 4.80 -19 -6 4 34.00 4.50 19 6 -4 28.10 4.70 -19 6 4 35.20 2.80 -18 -6 4 18.50 3.60 18 6 -4 22.40 4.00 -18 6 4 16.00 2.20 -17 -6 4 49.70 5.10 -17 6 4 42.80 3.00 17 6 -4 50.99 5.60 -16 -6 4 13.00 2.90 -16 6 4 21.40 2.50 16 6 -4 22.50 3.80 -15 -6 4 21.10 3.40 -15 6 4 23.70 2.60 15 6 -4 13.60 2.90 -14 -6 4 67.49 4.60 -14 6 4 60.79 3.40 14 6 -4 61.49 4.90 -13 -6 4 85.99 3.20 -13 -6 4 93.49 5.30 13 6 -4 95.69 5.60 -13 6 4 94.09 4.10 -12 -6 4 3.20 1.80 -12 -6 4 4.70 0.90 12 6 -4 3.90 2.00 -12 6 4 3.10 1.20 -11 -6 4 66.89 4.40 -11 -6 4 71.09 2.90 -11 6 4 73.59 3.50 11 6 -4 72.49 4.70 -10 -6 4 12.50 1.30 -10 -6 4 13.20 2.60 10 6 -4 17.10 2.80 -10 6 4 14.60 1.90 -9 -6 4 181.08 7.10 -9 -6 4 165.48 5.30 -9 6 4 160.88 7.00 9 6 -4 180.18 7.20 -9 6 4 164.88 5.70 -8 -6 4 30.50 3.30 -8 -6 4 31.30 1.90 -8 6 4 25.90 2.80 -8 6 4 33.50 2.20 8 6 -4 32.20 3.40 -7 -6 4 349.07 9.60 -7 -6 4 370.86 11.10 -7 6 4 352.06 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6 -4 125.69 4.80 0 -6 4 432.86 12.10 0 -6 -4 435.96 12.80 0 -6 -4 437.86 11.50 0 -6 4 443.16 11.40 0 6 -4 451.95 12.50 0 6 4 424.86 12.50 0 6 -4 438.66 12.80 0 6 -4 424.26 11.60 0 6 4 435.56 11.20 0 6 4 438.36 11.60 0 6 4 445.36 11.90 1 -6 4 31.70 2.40 -1 -6 -4 32.80 2.20 -1 -6 -4 37.80 1.90 1 -6 4 31.90 1.70 1 6 4 33.90 1.60 1 6 4 32.10 1.70 -1 6 -4 32.00 2.20 -1 6 -4 36.80 3.00 -1 6 -4 30.30 2.40 1 6 4 33.30 2.60 1 6 4 35.50 2.50 2 -6 4 109.69 4.50 -2 -6 -4 96.79 3.60 -2 -6 -4 108.19 4.30 2 -6 4 104.19 3.50 -2 6 -4 98.99 4.00 -2 6 -4 99.89 5.20 2 6 4 95.69 4.80 2 6 4 107.79 3.10 2 6 4 105.49 4.50 -2 6 -4 113.59 4.70 -3 -6 -4 1.40 0.60 3 -6 4 0.90 0.50 -3 -6 -4 -1.00 0.60 -3 6 -4 1.30 1.20 -3 6 -4 0.70 0.80 3 6 4 1.50 1.00 -3 6 -4 0.00 0.80 3 6 4 1.30 0.50 3 6 4 -0.20 1.10 -4 -6 -4 135.79 5.00 -4 -6 -4 140.99 4.50 4 -6 4 136.89 6.00 -4 6 -4 137.19 4.70 -4 6 -4 143.19 5.80 4 6 4 140.99 5.60 4 6 4 149.19 6.40 -5 -6 -4 28.90 1.70 5 6 4 29.90 3.10 -5 6 -4 26.80 3.40 -5 6 -4 29.90 2.60 5 6 4 30.90 3.60 -5 6 -4 23.00 1.80 -6 -6 -4 415.36 10.90 -6 6 -4 411.96 10.70 -6 6 -4 410.26 12.90 6 6 4 427.56 13.60 -6 6 -4 413.56 14.30 6 6 4 405.66 12.10 -7 -6 -4 78.09 3.00 -7 6 -4 73.79 3.10 7 6 4 78.29 4.90 -7 6 -4 75.99 5.60 7 6 4 79.49 4.20 -8 -6 -4 9.10 1.10 8 6 4 11.80 2.20 8 6 4 8.80 2.20 -8 6 -4 9.30 1.30 -8 6 -4 9.80 2.80 -9 -6 -4 75.69 3.00 9 6 4 81.49 4.50 -9 6 -4 77.49 3.20 9 6 4 84.19 5.40 -9 6 -4 73.09 5.90 -10 -6 -4 5.50 0.90 10 -6 4 8.90 3.00 10 6 4 9.00 2.50 -10 6 -4 6.50 2.70 10 6 4 6.00 1.80 11 -6 4 204.18 10.10 -11 -6 -4 199.58 5.90 -11 6 -4 194.68 10.00 11 6 4 227.28 8.60 11 6 4 220.08 9.50 12 -6 4 78.49 7.60 12 6 4 82.89 5.00 12 6 4 78.99 5.50 13 -6 4 96.99 7.10 13 6 4 117.49 7.00 13 6 4 112.79 6.20 14 -6 4 -4.20 1.50 14 6 4 -0.80 1.40 15 -6 4 49.80 6.20 15 6 4 55.19 4.50 15 6 4 52.89 6.20 16 -6 4 -2.10 2.20 16 6 4 2.10 2.00 17 -6 4 57.69 7.20 17 6 4 61.09 6.00 18 -6 4 -1.40 1.80 18 6 4 3.50 2.30 19 -6 4 10.20 4.10 19 6 4 17.80 3.60 20 -6 4 11.00 3.90 20 6 4 14.50 3.60 21 -6 4 2.90 3.00 21 6 4 3.20 2.40 22 -6 4 2.50 2.90 22 6 4 2.70 2.70 -22 -7 4 2.10 2.30 22 7 -4 0.90 2.60 -21 -7 4 0.50 2.20 21 7 -4 -3.00 1.90 -20 -7 4 6.40 2.60 20 7 -4 9.60 3.20 -20 7 4 4.60 1.60 -19 -7 4 -3.00 1.60 -19 7 4 1.00 1.30 19 7 -4 3.90 2.50 -18 -7 4 2.20 2.10 18 7 -4 3.20 2.50 -18 7 4 2.10 1.30 -17 -7 4 -1.90 1.80 17 7 -4 1.60 2.10 -17 7 4 1.10 1.30 -16 -7 4 7.60 2.50 16 7 -4 9.00 2.80 -16 7 4 8.10 1.80 -15 -7 4 12.30 2.80 -15 7 4 8.80 1.70 15 7 -4 6.30 2.30 -14 -7 4 8.90 2.60 14 7 -4 10.40 2.70 -14 7 4 10.70 1.90 -13 -7 4 4.70 2.10 13 7 -4 1.10 2.00 -13 7 4 3.10 1.30 -12 -7 4 0.10 1.60 12 7 -4 0.60 1.50 -12 7 4 1.10 1.10 -11 -7 4 -0.10 1.40 -11 7 4 0.10 1.10 11 7 -4 1.00 1.60 -10 -7 4 3.70 1.80 10 7 -4 10.60 2.50 -10 7 4 10.70 1.80 -9 -7 4 151.08 6.70 9 7 -4 153.08 7.10 -9 7 4 154.98 5.70 -8 -7 4 38.40 3.80 8 7 -4 33.30 3.70 -8 7 4 38.80 2.70 -7 -7 4 148.29 6.40 7 7 -4 147.59 6.50 -7 7 4 145.69 5.50 -6 -7 4 16.20 2.70 -6 7 4 16.20 1.80 6 7 -4 17.30 2.70 -6 7 4 19.70 2.30 -5 -7 4 37.10 3.10 -5 7 4 34.90 2.50 5 7 -4 38.30 3.00 -5 7 4 35.80 2.30 -4 -7 4 77.59 4.30 -4 7 4 76.99 3.50 4 7 -4 83.89 4.40 -4 7 4 82.99 3.80 -4 7 4 82.09 3.80 -3 -7 4 27.50 3.00 3 -7 -4 23.30 1.70 -3 -7 4 28.20 1.90 -3 7 4 22.90 1.90 -3 7 4 20.70 1.80 -3 7 4 25.10 2.50 3 7 -4 22.20 2.60 -2 -7 4 -1.60 1.00 -2 -7 4 0.30 0.50 2 -7 -4 0.40 0.50 2 7 -4 0.40 0.70 -2 7 4 -0.10 0.60 -2 7 4 0.00 0.60 -2 7 4 3.50 1.20 2 7 -4 -0.10 0.90 -1 -7 4 0.10 0.50 1 -7 -4 0.70 0.60 -1 -7 4 1.10 1.20 -1 7 4 -0.60 0.40 1 7 -4 -0.70 0.90 -1 7 4 0.00 1.00 1 7 -4 -0.80 0.70 0 -7 4 -0.10 1.00 0 -7 -4 0.40 0.50 0 -7 4 -0.40 0.50 0 7 -4 -0.50 0.70 0 7 -4 -1.60 0.70 0 7 4 -0.10 0.50 0 7 -4 0.20 1.00 0 7 4 -0.60 0.90 -1 -7 -4 3.50 0.80 1 -7 4 2.60 0.70 -1 7 -4 5.10 1.20 1 7 4 3.90 1.40 -1 7 -4 4.30 1.40 -1 7 -4 7.60 1.60 1 7 4 6.00 0.80 -2 -7 -4 31.90 2.00 2 -7 4 32.50 1.80 -2 7 -4 37.40 2.50 -2 7 -4 25.00 3.00 2 7 4 34.20 3.30 -2 7 -4 30.70 2.50 3 7 4 77.59 4.10 -3 7 -4 76.29 4.00 -3 7 -4 80.69 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2.20 7 8 4 15.60 2.70 8 8 4 3.00 1.80 9 8 4 1.60 1.90 10 8 4 6.50 2.10 11 8 4 1.00 1.80 12 8 4 -0.50 1.50 13 8 4 -0.10 1.60 14 8 4 -0.40 1.70 15 8 4 15.60 3.50 16 8 4 3.90 2.50 17 8 4 6.80 2.80 18 8 4 2.40 2.40 19 8 4 1.00 2.00 -18 -9 4 10.40 3.30 18 9 -4 4.50 2.90 -17 -9 4 11.60 3.30 17 9 -4 9.10 3.20 -17 9 4 7.00 2.10 -16 -9 4 7.90 3.00 -16 9 4 8.70 2.20 16 9 -4 13.40 3.60 -15 -9 4 4.20 2.50 15 9 -4 1.20 2.20 -15 9 4 1.00 1.40 -14 -9 4 55.49 5.80 14 9 -4 62.69 6.50 -14 9 4 58.99 4.00 -13 -9 4 4.10 2.30 13 9 -4 -0.50 2.10 -13 9 4 4.10 1.50 -12 -9 4 95.79 6.10 12 9 -4 78.59 5.90 -12 9 4 101.19 5.00 -11 -9 4 5.90 2.30 11 9 -4 3.30 2.10 -11 9 4 2.30 1.50 -10 -9 4 45.90 4.80 10 9 -4 54.49 5.60 -10 9 4 56.79 3.60 -9 -9 4 31.70 4.00 9 9 -4 34.40 4.20 -9 9 4 35.70 3.50 -8 -9 4 50.39 4.10 -8 9 4 50.99 3.50 8 9 -4 54.39 5.50 -7 -9 4 47.60 4.70 7 9 -4 38.60 4.30 -7 9 4 45.70 3.30 -6 -9 4 46.60 4.00 6 9 -4 45.20 4.50 -6 9 4 42.20 3.20 -5 -9 4 85.79 5.10 5 9 -4 88.49 5.20 -5 9 4 84.79 4.60 -4 -9 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52.39 5.20 -16 4 8 47.50 3.00 -15 -4 8 81.29 5.20 15 -4 -8 83.19 4.60 -15 4 8 78.69 3.80 15 4 -8 92.99 5.60 -14 -4 8 14.80 2.80 14 -4 -8 16.00 2.40 14 4 -8 11.00 2.40 -14 4 8 17.10 2.00 -14 4 8 13.40 1.90 -13 -4 8 184.38 5.00 -13 -4 8 181.28 7.60 -13 4 8 192.78 6.60 13 4 -8 204.78 8.30 -13 4 8 194.18 6.30 -12 -4 8 39.80 3.90 -12 -4 8 44.40 1.70 12 4 -8 40.40 4.10 -12 4 8 45.20 2.60 -12 4 8 39.80 2.60 -11 -4 8 202.48 7.80 -11 -4 8 200.08 5.50 11 4 -8 225.58 8.30 -11 4 8 197.48 6.70 -11 4 8 201.68 6.40 -10 -4 8 40.80 1.70 -10 -4 8 41.40 3.20 10 4 -8 47.20 3.40 -10 4 8 37.90 2.30 -10 4 8 40.50 2.50 -10 4 8 41.50 2.50 -9 -4 8 74.49 2.60 -9 -4 8 77.59 4.20 -9 -4 8 76.09 3.40 -9 4 8 78.89 3.20 -9 4 8 74.09 2.90 -9 4 8 75.39 3.30 -9 4 8 74.99 3.40 9 4 -8 73.49 4.10 -8 -4 8 5.50 0.80 -8 -4 8 3.70 1.60 -8 -4 8 4.80 1.10 -8 -4 8 7.70 1.90 -8 4 8 5.50 1.00 -8 4 8 7.20 1.30 8 4 -8 2.60 1.30 -8 4 8 3.20 0.70 -7 -4 8 159.08 5.30 -7 -4 8 142.89 6.90 -7 -4 8 150.18 4.60 -7 -4 8 150.78 6.00 -7 4 8 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106.19 6.20 16 -3 -9 43.50 3.60 -16 -3 9 43.80 4.50 16 3 -9 53.39 5.10 -16 3 9 41.60 2.80 15 -3 -9 137.49 6.00 -15 -3 9 146.69 6.60 15 3 -9 122.69 6.40 -15 3 9 125.99 4.90 -14 -3 9 3.00 2.00 14 -3 -9 5.60 1.70 14 3 -9 1.60 1.50 -14 3 9 4.60 1.30 -13 -3 9 155.98 6.90 -13 -3 9 168.18 4.40 13 -3 -9 160.68 6.30 -13 3 9 159.98 5.50 13 3 -9 176.38 7.30 -13 3 9 166.28 5.50 -12 -3 9 134.29 3.70 -12 -3 9 138.99 6.20 12 -3 -9 141.59 5.60 12 3 -9 140.19 6.30 -12 3 9 134.69 4.80 -12 3 9 134.89 4.80 11 -3 -9 234.88 7.70 -11 -3 9 234.88 8.40 -11 -3 9 226.58 5.80 -11 3 9 215.58 6.80 -11 3 9 226.28 6.80 11 3 -9 220.18 8.20 10 -3 -9 122.29 5.00 -10 -3 9 112.19 5.30 -10 -3 9 127.69 3.60 -10 -3 9 130.59 5.70 -10 -3 9 123.49 4.60 -10 3 9 134.09 4.50 10 3 -9 125.49 5.70 -10 3 9 125.69 4.30 -10 3 9 120.59 4.00 -10 3 9 124.89 5.40 -9 -3 9 312.47 9.30 9 -3 -9 322.97 8.50 9 -3 -9 313.77 9.40 -9 -3 9 319.47 8.10 -9 -3 9 316.47 10.70 -9 -3 9 331.67 10.40 -9 3 9 326.27 8.60 -9 3 9 304.57 10.80 -9 3 9 319.77 10.00 9 3 -9 328.37 10.20 -9 3 9 324.67 8.80 -9 3 9 309.17 8.60 8 -3 -9 403.16 31.00 -8 -3 9 464.95 13.10 -8 -3 9 445.26 14.00 -8 -3 9 445.16 10.90 -8 -3 9 435.66 12.10 -8 3 9 445.16 11.40 -8 3 9 447.96 12.60 8 3 -9 409.16 12.40 8 3 -9 428.36 11.00 -8 3 9 451.15 11.50 -8 3 9 416.66 13.70 -8 3 9 433.86 11.20 8 3 -9 451.85 10.90 7 -3 -9 89.99 16.40 -7 -3 9 84.69 5.40 -7 -3 9 94.59 3.00 -7 -3 9 101.59 4.70 -7 -3 9 89.99 3.80 7 3 -9 93.99 4.40 -7 3 9 96.49 3.90 -7 3 9 95.99 3.30 -7 3 9 96.09 5.20 -7 3 9 99.59 3.50 -7 3 9 98.29 3.30 7 3 -9 91.09 3.30 -6 -3 9 614.54 18.60 -6 -3 9 586.04 14.60 -6 -3 9 591.14 15.60 -6 -3 9 590.14 16.30 6 -3 -9 590.54 34.50 6 -3 -9 572.94 16.30 -6 3 9 574.74 15.40 -6 3 9 590.94 14.70 6 3 -9 582.54 15.50 -6 3 9 610.74 14.40 -6 3 9 600.54 14.90 -6 3 9 589.94 17.40 -5 -3 9 27.40 2.00 -5 -3 9 31.90 4.00 5 -3 -9 30.60 2.10 5 -3 -9 33.70 1.70 5 -3 -9 32.60 2.90 -5 -3 9 30.60 1.60 5 -3 -9 49.80 11.80 -5 -3 9 34.70 2.90 -5 3 9 29.50 1.80 -5 3 9 28.40 1.70 5 3 -9 30.10 1.80 5 3 -9 32.10 1.20 -5 3 9 32.80 1.60 -5 3 9 34.30 1.70 5 3 -9 33.90 2.00 5 3 -9 32.10 2.20 -5 3 9 31.00 3.60 5 3 -9 32.00 2.30 4 -3 -9 574.54 15.00 -4 -3 9 574.24 18.70 4 -3 -9 559.64 32.80 -4 -3 9 591.54 15.30 4 -3 -9 583.14 14.80 4 -3 -9 580.24 16.60 -4 -3 9 605.14 16.40 -4 -3 9 570.64 14.40 -4 3 9 573.74 14.00 4 3 -9 578.34 15.80 4 3 -9 586.14 15.20 4 3 -9 589.44 14.90 4 3 -9 562.64 16.20 -4 3 9 577.44 14.60 -4 3 9 598.24 14.30 -4 3 9 562.34 17.00 4 3 -9 578.04 13.90 3 -3 -9 36.10 2.50 3 -3 -9 57.49 12.80 -3 -3 9 38.30 3.10 -3 -3 9 44.40 4.90 3 -3 -9 36.80 2.00 3 -3 -9 31.40 1.70 -3 -3 9 32.40 1.70 -3 3 9 32.40 2.00 -3 3 9 46.10 3.60 -3 3 9 34.20 1.50 3 3 -9 33.60 2.10 -3 3 9 32.90 1.70 3 3 -9 40.70 3.10 -3 3 9 34.40 1.90 3 3 -9 29.20 1.40 2 -3 -9 389.16 10.60 -2 -3 9 403.76 12.40 -2 -3 9 409.66 10.50 2 -3 -9 399.36 26.70 2 -3 -9 397.16 11.20 -2 -3 9 401.36 14.50 2 -3 -9 405.46 10.60 -2 3 9 389.96 10.40 2 3 -9 410.36 11.10 2 3 -9 400.46 10.20 2 3 -9 427.56 13.40 -2 3 9 407.86 13.20 -2 3 9 402.76 10.20 -2 3 9 410.96 10.60 -2 3 9 421.06 10.10 -1 -3 9 237.38 7.30 1 -3 -9 235.28 19.90 -1 -3 9 232.38 8.70 1 -3 -9 231.28 6.40 -1 -3 9 223.98 9.50 1 -3 -9 221.18 6.30 1 -3 -9 230.58 6.80 -1 -3 9 230.08 6.40 -1 3 9 224.38 6.40 1 3 -9 229.68 9.40 -1 3 9 224.88 6.20 -1 3 9 239.48 6.00 -1 3 9 218.98 8.90 -1 3 9 229.58 6.50 1 3 -9 230.18 6.20 1 3 -9 242.18 7.00 0 -3 9 688.73 17.40 0 -3 9 689.93 20.10 0 -3 -9 696.63 17.20 0 -3 -9 710.93 36.80 0 -3 9 701.23 16.90 0 -3 -9 681.43 17.30 0 -3 -9 679.83 16.80 0 -3 9 669.73 19.80 0 3 9 691.63 16.80 0 3 9 681.53 20.00 0 3 9 695.63 16.50 0 3 9 658.43 16.30 0 3 -9 730.63 21.40 0 3 -9 680.03 16.90 0 3 9 692.03 17.30 0 3 -9 707.93 17.80 -1 -3 -9 42.50 2.00 1 -3 9 49.10 4.80 -1 -3 -9 41.20 1.70 1 -3 9 42.50 2.90 1 -3 9 45.80 1.80 -1 -3 -9 28.70 9.00 -1 -3 -9 41.60 1.90 1 -3 9 41.90 2.80 1 3 9 36.40 4.00 1 3 9 43.80 2.10 -1 3 -9 41.10 1.90 1 3 9 42.70 1.50 1 3 9 40.60 2.10 1 3 9 40.20 1.60 -1 3 -9 46.60 5.00 -1 3 -9 43.30 2.30 2 -3 9 422.16 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250.77 6.60 3 4 -9 237.98 7.40 -3 4 9 244.48 6.90 3 4 -9 248.18 8.40 -3 4 9 247.28 7.00 3 4 -9 248.38 8.50 2 -4 -9 38.20 2.00 -2 -4 9 38.60 1.90 -2 -4 9 38.30 3.10 2 -4 -9 40.40 2.30 -2 4 9 41.60 1.70 -2 4 9 35.90 1.80 -2 4 9 39.80 3.40 2 4 -9 43.00 3.20 2 4 -9 35.30 2.20 2 4 -9 41.60 3.40 -2 4 9 37.90 2.10 1 -4 -9 0.60 0.60 -1 -4 9 1.60 1.30 -1 -4 9 -0.20 0.40 -1 -4 9 -0.30 1.20 1 -4 -9 0.20 0.40 -1 4 9 0.00 1.20 -1 4 9 0.40 0.40 -1 4 9 -0.20 0.50 1 4 -9 -0.30 1.20 1 4 -9 -0.10 0.60 -1 4 9 -0.10 0.60 0 -4 9 39.20 2.90 0 -4 9 35.90 3.80 0 -4 9 42.10 1.90 0 -4 -9 39.10 2.00 0 -4 -9 43.50 2.00 0 4 9 52.29 4.00 0 4 -9 35.80 4.00 0 4 -9 45.00 2.50 0 4 9 39.20 2.20 0 4 9 38.10 1.60 0 4 9 40.10 2.00 -1 -4 -9 189.18 5.60 -1 -4 -9 195.38 16.70 1 -4 9 193.18 7.10 1 -4 9 174.58 8.00 -1 -4 -9 185.48 5.60 1 -4 9 185.58 5.30 1 4 9 184.88 5.60 1 4 9 192.48 5.00 1 4 9 190.88 5.80 1 4 9 185.88 8.10 -1 4 -9 196.08 9.00 1 4 9 185.78 5.20 -2 -4 -9 316.37 21.90 2 -4 9 333.87 8.30 2 -4 9 330.47 12.20 2 -4 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78.39 3.10 -2 -5 9 77.09 4.40 -2 5 9 79.49 2.70 -2 5 9 72.39 4.50 2 5 -9 76.69 4.50 2 5 -9 75.79 3.60 -2 5 9 80.99 3.10 2 5 -9 84.19 4.30 -2 5 9 81.59 3.50 -1 -5 9 1.30 1.50 1 -5 -9 0.60 0.60 -1 -5 9 0.30 0.50 1 5 -9 -1.00 0.80 1 5 -9 -0.10 0.90 -1 5 9 0.90 0.80 -1 5 9 0.60 0.50 -1 5 9 -0.10 0.40 -1 5 9 -0.50 1.20 0 -5 -9 134.79 4.50 0 -5 -9 127.79 4.50 0 -5 9 131.99 4.20 0 -5 9 130.89 6.30 0 5 -9 131.09 6.10 0 5 9 131.29 4.80 0 5 9 127.89 6.30 0 5 9 122.69 4.30 0 5 9 130.99 3.70 0 5 -9 133.79 6.80 0 5 -9 120.79 4.90 0 5 -9 130.99 4.60 1 -5 9 24.40 3.40 -1 -5 -9 20.80 1.50 -1 -5 -9 18.50 1.50 1 -5 9 21.00 1.30 1 -5 9 23.20 3.20 -1 5 -9 15.60 3.00 1 5 9 19.60 1.10 1 5 9 19.80 2.20 1 5 9 17.50 2.90 -2 -5 -9 84.99 3.30 2 -5 9 86.99 5.60 -2 -5 -9 82.49 3.30 2 -5 9 87.29 2.80 2 -5 9 91.49 5.20 2 5 9 83.19 2.70 2 5 9 85.19 5.40 2 5 9 91.29 3.90 -2 5 -9 90.89 6.20 3 -5 9 145.89 5.10 -3 -5 -9 154.38 4.80 3 -5 9 143.09 6.80 3 -5 9 157.38 8.00 -3 -5 -9 144.29 4.80 -3 5 -9 136.49 8.00 3 5 9 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1.80 13 5 9 -1.00 1.40 14 -5 9 10.10 3.10 14 5 9 5.60 2.60 14 5 9 6.10 2.90 14 5 9 2.80 1.80 15 -5 9 14.80 3.80 15 5 9 10.20 3.40 15 5 9 1.70 2.50 15 5 9 7.10 2.50 16 -5 9 1.10 2.00 16 5 9 1.40 1.80 16 5 9 3.00 2.40 16 5 9 0.20 2.20 17 -5 9 2.10 2.20 17 5 9 -1.80 2.40 17 5 9 0.50 1.80 17 5 9 2.60 2.50 18 -5 9 0.70 2.10 18 5 9 -1.40 2.00 18 5 9 -0.50 1.80 18 5 9 0.00 2.40 19 -5 9 6.50 2.90 19 5 9 1.10 2.50 19 5 9 2.90 2.60 20 -5 9 2.30 2.60 20 5 9 -0.40 2.40 20 5 9 7.30 3.00 21 -5 9 4.20 3.10 21 5 9 3.10 2.50 22 -5 9 4.60 3.30 22 5 9 -0.30 2.40 -22 -6 9 2.50 2.80 -22 6 9 3.80 1.70 22 6 -9 3.10 2.40 -21 -6 9 17.80 3.80 21 6 -9 14.30 3.80 -21 6 9 18.50 2.70 -20 -6 9 18.70 3.80 20 6 -9 19.70 4.20 -20 6 9 20.10 2.70 -19 -6 9 5.20 2.70 19 6 -9 0.30 2.10 -19 6 9 8.00 2.00 -18 -6 9 10.10 3.10 18 6 -9 4.70 2.40 -18 6 9 8.10 1.90 -17 -6 9 1.20 2.00 17 6 -9 1.80 2.00 -17 6 9 2.50 1.40 -16 -6 9 50.59 5.20 16 6 -9 48.30 5.40 -16 6 9 45.90 3.20 -15 -6 9 0.50 1.70 -15 6 9 0.30 1.10 15 6 -9 1.60 1.90 -14 -6 9 105.09 6.30 -14 6 9 104.19 4.70 14 6 -9 108.89 6.60 -13 -6 9 26.40 3.70 -13 6 9 26.20 2.70 13 6 -9 32.40 4.10 -12 -6 9 23.50 3.70 -12 6 9 29.20 2.40 12 6 -9 25.60 3.70 -11 -6 9 1.10 1.80 11 6 -9 0.40 1.60 -11 6 9 0.60 1.10 -10 -6 9 55.89 4.20 10 6 -9 65.99 4.50 -10 6 9 56.39 3.30 -9 -6 9 7.10 2.10 -9 6 9 5.30 1.30 9 6 -9 3.70 1.70 -8 -6 9 51.19 3.80 -8 6 9 50.59 3.00 8 6 -9 51.39 3.80 -7 -6 9 101.79 5.30 -7 6 9 89.29 3.70 -7 6 9 96.89 4.10 7 6 -9 90.79 4.90 -6 -6 9 46.80 3.80 -6 6 9 33.60 2.40 6 6 -9 50.49 3.50 -6 6 9 27.50 2.00 -5 -6 9 107.49 5.40 -5 -6 9 99.69 4.20 -5 6 9 106.99 3.80 -5 6 9 104.59 4.40 5 6 -9 108.69 5.00 -5 6 9 105.59 3.90 -4 -6 9 11.00 1.30 4 -6 -9 10.50 1.70 -4 -6 9 10.30 2.30 4 6 -9 14.90 2.30 -4 6 9 9.80 1.10 -4 6 9 11.90 1.90 -4 6 9 13.00 1.40 -3 -6 9 165.58 6.90 -3 -6 9 147.99 5.10 3 -6 -9 152.08 5.60 3 6 -9 155.18 6.00 -3 6 9 145.99 4.70 -3 6 9 146.89 5.00 -3 6 9 164.28 5.70 3 6 -9 168.38 6.10 2 -6 -9 50.09 2.70 -2 -6 9 46.20 2.30 -2 -6 9 43.40 3.70 -2 6 9 48.40 2.80 2 6 -9 44.70 3.00 -2 6 9 40.00 3.90 2 6 -9 46.60 3.40 -2 6 9 38.50 2.20 -2 6 9 43.30 2.00 -1 -6 9 140.59 4.70 1 -6 -9 147.09 5.20 -1 -6 9 142.19 6.70 -1 6 9 144.19 4.30 1 6 -9 145.09 5.40 1 6 -9 135.39 6.00 -1 6 9 144.59 6.70 -1 6 9 149.69 5.50 1 6 -9 150.78 6.80 0 -6 9 115.89 5.90 0 -6 -9 106.09 4.10 0 -6 9 105.39 3.80 0 6 9 111.29 5.80 0 6 -9 102.79 5.30 0 6 -9 112.19 4.40 0 6 9 114.59 4.60 0 6 -9 112.39 6.10 0 6 9 102.39 3.30 1 -6 9 187.08 8.20 1 -6 9 182.28 5.40 -1 -6 -9 179.78 5.90 1 6 9 175.78 7.90 -1 6 -9 173.48 5.90 1 6 9 191.38 6.50 -1 6 -9 181.08 7.60 -2 -6 -9 44.40 2.50 2 -6 9 52.89 5.50 -2 -6 -9 43.60 2.40 2 6 9 51.19 3.10 2 6 9 53.19 5.10 -2 6 -9 43.50 4.90 -2 6 -9 44.30 3.70 3 -6 9 113.59 6.90 3 -6 9 128.89 6.80 -3 6 -9 113.79 6.00 -3 6 -9 102.49 7.70 3 6 9 108.09 4.90 3 6 9 118.19 6.50 4 -6 9 7.60 2.50 4 6 9 9.90 1.90 4 6 9 7.10 2.40 -4 6 -9 7.10 1.90 5 -6 9 32.60 4.50 5 6 9 28.90 3.10 5 6 9 32.10 4.10 6 -6 9 96.89 6.40 6 6 9 89.09 6.00 6 6 9 93.69 4.60 7 -6 9 22.00 4.00 7 6 9 12.20 3.20 7 6 9 19.10 2.80 8 -6 9 96.39 6.60 8 6 9 85.39 6.10 8 6 9 92.49 4.80 9 -6 9 42.30 5.20 9 6 9 43.80 3.40 9 6 9 37.10 5.10 10 -6 9 49.50 6.10 10 6 9 45.20 3.60 10 6 9 47.20 5.50 11 -6 9 15.60 3.70 11 6 9 19.50 2.90 11 6 9 15.90 3.60 12 -6 9 20.80 4.10 12 6 9 28.90 4.60 12 6 9 32.80 4.10 13 -6 9 21.20 4.40 13 6 9 19.60 4.20 13 6 9 19.20 3.20 14 -6 9 33.60 5.50 14 6 9 19.00 4.40 14 6 9 26.70 3.90 14 6 9 19.60 4.10 15 -6 9 6.10 3.00 15 6 9 9.20 2.60 15 6 9 11.90 3.30 15 6 9 7.50 3.30 16 -6 9 7.90 3.20 16 6 9 13.10 3.10 16 6 9 9.30 3.70 16 6 9 9.60 3.40 17 -6 9 2.50 2.90 17 6 9 4.00 2.90 17 6 9 2.00 2.40 17 6 9 1.70 2.00 18 -6 9 5.00 3.10 18 6 9 9.90 3.00 18 6 9 6.20 2.80 18 6 9 3.30 3.20 19 -6 9 4.40 3.00 19 6 9 6.40 3.20 19 6 9 8.90 3.60 19 6 9 13.30 3.40 20 -6 9 7.30 3.50 20 6 9 0.10 2.30 21 -6 9 4.50 3.30 -21 -7 9 19.40 4.10 -21 7 9 14.70 2.60 21 7 -9 17.40 3.90 -20 -7 9 1.10 2.50 -20 7 9 0.90 1.40 20 7 -9 0.60 2.10 -19 -7 9 46.10 5.40 -19 7 9 44.50 3.40 19 7 -9 40.70 5.50 -18 -7 9 0.00 2.00 18 7 -9 2.10 2.20 -18 7 9 2.20 1.50 -17 -7 9 41.30 5.00 17 7 -9 37.90 5.30 -17 7 9 46.10 3.40 -16 -7 9 -0.80 1.80 16 7 -9 -1.20 1.60 -16 7 9 2.00 1.20 -15 -7 9 53.19 5.40 15 7 -9 54.99 5.90 -15 7 9 45.50 3.30 -14 -7 9 4.90 2.30 14 7 -9 2.70 2.00 -14 7 9 3.10 1.40 -13 -7 9 226.98 9.90 -13 7 9 237.18 8.20 13 7 -9 244.88 10.30 -12 -7 9 0.90 1.80 -12 7 9 3.10 1.40 12 7 -9 3.80 1.90 -11 -7 9 211.48 9.10 11 7 -9 205.68 9.00 -11 7 9 208.58 7.40 -10 -7 9 -1.00 1.50 -10 7 9 -0.10 1.20 10 7 -9 -0.90 1.60 -9 -7 9 80.99 5.40 -9 7 9 95.59 4.40 9 7 -9 86.59 5.40 -8 -7 9 63.39 4.60 -8 7 9 66.89 3.70 8 7 -9 71.99 4.60 -7 -7 9 35.50 4.00 -7 7 9 47.60 3.10 7 7 -9 44.50 3.70 -6 -7 9 208.48 8.70 -6 7 9 217.38 7.40 6 7 -9 223.58 8.30 -5 -7 9 35.50 4.00 -5 7 9 32.10 2.50 -5 7 9 35.10 2.20 5 7 -9 37.40 3.70 -4 -7 9 63.59 4.40 -4 7 9 57.29 3.40 4 7 -9 58.69 3.80 -3 -7 9 4.30 1.90 3 -7 -9 3.20 1.00 3 7 -9 4.00 1.60 -3 7 9 5.00 0.90 -3 7 9 2.90 1.30 -2 -7 9 150.18 7.10 2 -7 -9 159.48 5.70 -2 -7 9 153.68 5.20 -2 7 9 152.98 4.80 2 7 -9 163.38 6.60 -2 7 9 158.88 6.00 2 7 -9 151.18 6.10 1 -7 -9 22.50 1.90 -1 -7 9 25.10 3.50 -1 -7 9 23.50 1.70 1 7 -9 27.40 2.80 1 7 -9 21.30 2.80 -1 7 9 22.40 2.60 -1 7 9 20.40 1.40 0 -7 9 565.54 15.20 0 -7 9 605.44 18.20 0 7 -9 585.64 18.10 0 7 9 581.54 17.60 0 7 9 620.24 16.10 0 7 -9 607.74 15.80 1 -7 9 113.19 6.50 1 7 9 126.49 5.50 -1 7 -9 119.19 6.00 1 7 9 124.99 6.50 2 7 9 289.17 10.70 2 7 9 271.27 9.00 -2 7 -9 251.67 9.80 3 7 9 268.27 10.90 3 7 9 284.47 9.50 4 7 9 18.30 3.30 4 7 9 19.10 2.80 5 7 9 105.89 5.30 5 7 9 106.79 6.40 6 7 9 44.30 5.10 6 7 9 48.80 3.70 7 -7 9 72.69 6.00 7 7 9 59.99 4.10 7 7 9 71.29 5.60 8 -7 9 3.10 2.70 8 7 9 -1.10 1.60 8 7 9 -0.30 1.20 9 -7 9 129.99 8.40 9 7 9 141.99 6.70 9 7 9 129.59 7.90 10 -7 9 17.10 4.10 10 7 9 11.10 2.70 10 7 9 11.00 3.10 11 -7 9 77.49 7.90 11 7 9 71.69 4.90 11 7 9 66.59 5.70 12 -7 9 8.60 3.40 12 7 9 15.10 3.00 12 7 9 13.80 3.60 13 -7 9 57.39 7.30 13 7 9 52.09 6.40 13 7 9 59.99 4.70 14 -7 9 41.80 6.60 14 7 9 51.39 5.30 14 7 9 41.60 5.80 15 -7 9 20.50 4.70 15 7 9 32.10 4.40 15 7 9 24.00 4.60 15 7 9 22.90 5.00 16 -7 9 16.50 4.30 16 7 9 23.60 5.00 16 7 9 14.90 4.10 16 7 9 22.00 4.00 17 -7 9 24.70 5.40 17 7 9 25.20 5.50 17 7 9 17.70 4.30 17 7 9 28.80 4.40 18 -7 9 14.40 4.60 18 7 9 11.40 3.20 18 7 9 19.90 4.20 18 7 9 11.00 3.90 19 -7 9 5.10 3.60 19 7 9 7.00 2.90 -19 -8 9 12.90 3.50 19 8 -9 10.00 3.40 -19 8 9 12.80 2.50 -18 -8 9 23.20 4.20 18 8 -9 20.00 4.30 -18 8 9 22.20 3.10 -17 -8 9 2.60 2.30 17 8 -9 -0.30 1.80 -17 8 9 0.40 1.20 -16 -8 9 59.19 6.30 -16 8 9 66.59 4.30 16 8 -9 57.19 6.40 -15 -8 9 7.20 2.80 15 8 -9 4.40 2.30 -15 8 9 5.10 1.80 -14 -8 9 124.89 7.40 -14 8 9 110.29 5.50 14 8 -9 108.99 7.10 -13 -8 9 7.80 2.70 -13 8 9 10.60 2.10 13 8 -9 8.70 2.80 -12 -8 9 74.59 5.70 12 8 -9 82.19 5.70 -12 8 9 90.09 4.70 -11 -8 9 21.20 3.70 -11 8 9 23.70 3.10 11 8 -9 23.90 3.90 -10 -8 9 78.39 5.60 -10 8 9 76.99 4.40 10 8 -9 75.39 5.40 -9 -8 9 112.49 6.50 9 8 -9 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10 5.70 1.60 19 5 -10 0.50 1.90 -18 -5 10 49.20 5.30 18 5 -10 49.60 5.50 -18 5 10 55.09 3.50 -17 -5 10 27.80 4.00 17 5 -10 32.50 4.40 -17 5 10 25.00 2.80 -16 -5 10 38.60 4.50 16 5 -10 38.50 4.60 -16 5 10 44.20 3.00 -15 -5 10 56.39 5.50 -15 5 10 72.19 3.70 15 5 -10 65.19 5.00 -14 -5 10 19.00 3.30 -14 5 10 19.60 2.40 14 5 -10 19.80 3.40 -13 -5 10 197.18 8.50 13 5 -10 191.28 8.50 -13 5 10 201.88 6.80 -12 -5 10 16.40 3.00 -12 5 10 18.90 2.20 12 5 -10 15.80 3.10 -11 -5 10 282.17 10.30 -11 5 10 269.97 8.30 11 5 -10 272.07 10.10 -10 -5 10 2.90 1.90 -10 5 10 4.10 1.20 10 5 -10 1.10 1.40 -9 -5 10 67.19 4.30 -9 5 10 57.39 3.10 9 5 -10 69.79 4.30 -8 -5 10 17.60 2.80 -8 -5 10 18.60 1.60 -8 5 10 17.80 1.50 8 5 -10 20.80 2.70 -8 5 10 20.70 2.20 -7 -5 10 48.80 3.80 -7 -5 10 44.00 2.30 -7 5 10 47.10 2.40 7 5 -10 50.19 3.50 -7 5 10 52.59 2.80 -7 5 10 50.09 2.40 -6 -5 10 101.79 3.90 -6 -5 10 126.59 5.90 -6 5 10 106.59 3.80 6 5 -10 109.59 5.00 -6 5 10 107.19 3.90 -6 5 10 111.79 4.30 -5 -5 10 264.07 7.80 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5 10 332.17 12.80 -6 5 -10 313.77 13.80 6 5 10 329.17 9.80 7 -5 10 5.40 2.30 -7 -5 -10 4.60 0.80 -7 -5 -10 4.70 6.80 7 5 10 3.70 2.10 7 5 10 4.10 1.60 -7 5 -10 6.30 2.80 -8 -5 -10 69.19 2.70 -8 -5 -10 59.79 13.80 8 -5 10 66.99 5.00 -8 5 -10 65.49 7.20 8 5 10 65.09 3.80 8 5 10 77.29 5.80 9 -5 10 25.40 4.00 -9 -5 -10 23.90 1.50 -9 -5 -10 11.10 8.80 -9 5 -10 15.20 3.70 9 5 10 19.50 3.80 9 5 10 26.00 3.00 -10 -5 -10 23.30 1.40 10 -5 10 23.60 3.90 10 5 10 29.30 3.30 10 5 10 19.30 3.90 -10 5 -10 17.60 3.60 11 -5 10 15.80 3.30 11 5 10 14.90 2.50 -11 5 -10 16.50 3.50 11 5 10 20.80 4.10 12 -5 10 47.00 6.00 12 5 10 50.29 5.90 12 5 10 41.30 5.70 12 5 10 46.40 3.80 13 -5 10 27.10 4.70 13 5 10 29.40 4.90 13 5 10 37.10 4.20 13 5 10 29.00 4.80 14 -5 10 24.30 4.40 14 5 10 27.70 3.60 14 5 10 29.70 5.20 14 5 10 18.90 3.90 15 -5 10 44.70 6.00 15 5 10 47.10 4.70 15 5 10 44.40 6.00 15 5 10 41.20 6.30 16 -5 10 0.20 2.10 16 5 10 2.60 2.60 16 5 10 2.20 1.80 16 5 10 -0.20 2.00 17 -5 10 47.50 6.40 17 5 10 45.60 6.50 17 5 10 42.30 6.00 18 -5 10 3.20 2.60 18 5 10 -0.50 2.20 18 5 10 2.70 2.90 19 -5 10 37.00 6.00 19 5 10 43.80 6.70 19 5 10 38.60 5.90 20 -5 10 0.40 2.80 20 5 10 -0.30 2.70 20 5 10 0.60 2.10 21 -5 10 2.70 2.80 21 5 10 2.80 2.60 -22 -6 10 -2.60 1.90 22 6 -10 -0.40 2.20 -22 6 10 -1.20 1.30 -21 -6 10 28.00 4.60 -21 6 10 33.90 3.60 21 6 -10 27.40 4.50 -20 -6 10 5.70 3.00 -20 6 10 5.60 1.70 20 6 -10 10.80 3.00 -19 -6 10 22.30 4.00 -19 6 10 19.90 2.70 19 6 -10 20.00 3.90 -18 -6 10 3.30 2.30 -18 6 10 7.90 1.90 18 6 -10 5.90 2.60 -17 -6 10 25.80 4.10 -17 6 10 31.40 3.10 17 6 -10 36.90 5.00 -16 -6 10 37.70 4.70 16 6 -10 27.00 4.30 -16 6 10 35.00 2.80 -15 -6 10 44.30 4.90 15 6 -10 40.00 4.80 -15 6 10 38.50 2.90 -14 -6 10 171.28 8.20 14 6 -10 177.88 8.50 -14 6 10 172.48 6.50 -13 -6 10 5.60 2.30 13 6 -10 4.70 2.30 -13 6 10 6.90 1.60 -12 -6 10 70.19 5.00 -12 6 10 76.19 3.90 12 6 -10 71.39 5.00 -11 -6 10 32.20 4.10 11 6 -10 29.70 3.80 -11 6 10 28.00 2.80 -10 -6 10 112.19 6.30 10 6 -10 117.09 6.10 -10 6 10 108.99 4.80 -9 -6 10 3.40 1.90 -9 6 10 2.20 1.10 9 6 -10 3.60 1.90 -8 -6 10 47.70 3.90 8 6 -10 40.20 3.40 -8 6 10 42.90 2.80 -7 -6 10 25.60 3.40 -7 6 10 25.80 2.50 7 6 -10 22.00 2.90 -6 -6 10 34.70 3.80 6 6 -10 39.40 3.20 -6 6 10 29.10 2.30 -6 6 10 29.40 2.00 -5 -6 10 0.50 1.50 -5 6 10 0.80 1.00 5 6 -10 2.00 1.30 -5 6 10 0.50 0.60 -4 -6 10 75.49 4.70 -4 -6 10 70.99 3.10 4 -6 -10 65.49 3.80 -4 6 10 72.89 2.80 -4 6 10 70.99 3.10 4 6 -10 71.99 4.00 -4 6 10 70.59 3.50 -3 -6 10 175.88 5.70 3 -6 -10 180.98 6.50 -3 -6 10 198.28 8.00 -3 6 10 171.78 5.70 -3 6 10 177.18 5.20 3 6 -10 182.58 6.60 -3 6 10 177.68 6.20 3 6 -10 168.38 6.80 -2 -6 10 217.18 6.70 2 -6 -10 217.58 7.20 -2 -6 10 210.38 8.70 -2 6 10 237.18 7.40 2 6 -10 219.48 7.40 -2 6 10 213.98 6.10 2 6 -10 226.08 8.60 -2 6 10 225.18 8.80 -1 -6 10 27.40 3.60 1 -6 -10 29.70 2.10 -1 -6 10 27.30 1.80 -1 6 10 33.20 3.90 1 6 -10 27.20 2.90 1 6 -10 35.10 3.90 -1 6 10 30.40 2.40 -1 6 10 27.60 1.50 1 6 -10 30.40 2.40 0 -6 10 4.90 0.90 0 -6 10 3.00 2.00 0 -6 -10 4.80 1.10 0 6 -10 5.80 1.40 0 6 10 5.50 1.40 0 6 -10 1.20 1.30 0 6 10 5.10 2.10 0 6 10 3.80 0.70 1 -6 10 18.50 3.30 -1 -6 -10 16.70 1.70 -1 6 -10 22.80 3.60 1 6 10 24.00 2.60 -1 6 -10 24.30 3.10 1 6 10 23.70 3.50 2 -6 10 2.30 2.20 2 6 10 -0.90 0.90 2 6 10 1.00 1.50 -2 6 -10 0.20 1.10 3 -6 10 362.06 14.30 3 -6 10 378.56 13.40 -3 6 -10 374.46 13.40 3 6 10 377.66 11.20 3 6 10 386.26 13.70 4 -6 10 -1.70 2.20 4 -6 10 -1.00 1.60 4 6 10 2.30 1.70 4 6 10 2.90 1.30 5 -6 10 27.30 4.30 5 6 10 24.90 4.00 5 6 10 26.70 3.00 6 -6 10 11.00 2.90 6 6 10 6.20 2.20 6 6 10 7.70 1.80 -7 -6 -10 55.99 12.80 7 -6 10 45.70 5.60 7 6 10 45.20 3.40 7 6 10 45.50 5.40 8 -6 10 1.90 2.10 8 6 10 8.50 2.10 8 6 10 3.40 2.20 9 -6 10 121.19 7.70 9 6 10 139.49 6.30 9 6 10 139.59 8.20 10 -6 10 9.30 3.10 10 6 10 8.90 2.30 10 6 10 11.10 3.20 11 -6 10 47.70 6.00 11 6 10 60.89 6.60 11 6 10 59.69 4.30 12 -6 10 37.60 5.30 12 6 10 44.50 4.50 12 6 10 33.80 5.20 13 -6 10 1.00 2.20 13 6 10 3.40 1.80 13 6 10 2.10 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11.50 3.60 16 4 11 25.80 4.80 16 4 11 10.90 3.70 17 -4 11 22.60 4.60 17 4 11 21.30 4.80 17 4 11 28.70 5.00 18 -4 11 6.70 2.90 18 4 11 8.10 3.40 18 4 11 6.10 2.90 19 -4 11 2.40 2.60 19 4 11 1.70 2.50 19 4 11 3.20 2.60 20 -4 11 6.70 3.00 20 4 11 6.10 3.20 20 4 11 7.70 3.10 21 -4 11 2.80 2.70 21 4 11 5.90 3.40 21 4 11 6.60 3.50 22 -4 11 21.80 5.10 22 4 11 16.10 4.30 22 4 11 21.60 5.30 -23 -5 11 4.70 2.90 -23 -5 11 4.70 1.80 -23 5 11 2.30 1.50 23 5 -11 6.30 2.70 -22 -5 11 0.90 2.20 -22 5 11 2.20 1.50 22 5 -11 6.30 2.70 -21 -5 11 1.90 2.60 -21 5 11 6.70 1.90 21 5 -11 1.50 2.40 -20 -5 11 2.00 2.40 20 5 -11 2.10 2.20 -20 5 11 0.10 1.10 -19 -5 11 4.50 2.70 19 5 -11 5.50 2.50 -19 5 11 6.10 1.70 -18 -5 11 6.80 2.70 -18 5 11 3.40 1.40 18 5 -11 2.10 1.90 -17 -5 11 0.80 1.80 17 5 -11 1.00 1.70 -17 5 11 -1.10 0.90 -16 -5 11 0.00 2.00 16 5 -11 5.00 2.20 -16 5 11 3.20 1.40 -15 -5 11 1.50 1.90 15 5 -11 -2.40 1.30 -15 5 11 0.80 1.00 -14 -5 11 15.90 3.00 14 5 -11 14.40 3.00 -14 5 11 16.60 2.20 -13 -5 11 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3.10 2 6 -11 94.19 4.30 -2 6 11 98.29 4.30 -2 6 11 87.39 5.30 -1 -6 11 43.20 2.30 1 -6 -11 46.20 2.70 -1 -6 11 47.50 5.10 -1 6 11 44.40 2.90 -1 6 11 42.40 1.90 1 6 -11 48.40 4.80 -1 6 11 45.20 4.70 1 6 -11 44.90 2.80 0 -6 -11 324.77 9.90 0 -6 11 340.77 9.30 0 -6 11 362.36 13.10 0 6 11 343.97 10.10 0 6 11 350.26 12.60 0 6 -11 326.57 11.80 1 -6 11 11.80 3.20 1 6 11 4.70 2.10 1 6 11 4.10 1.50 -1 6 -11 5.80 1.80 -1 6 -11 5.20 2.40 2 -6 11 5.40 2.40 2 -6 11 12.50 3.40 -2 6 -11 8.90 2.30 2 6 11 9.20 1.80 2 6 11 9.50 2.70 3 -6 11 7.20 2.40 3 -6 11 2.00 2.50 3 6 11 9.60 2.70 3 6 11 8.70 1.80 4 -6 11 20.40 3.90 -4 -6 -11 29.10 10.50 4 -6 11 37.00 5.60 4 6 11 29.60 3.00 4 6 11 32.90 4.60 5 -6 11 3.00 2.10 -5 -6 -11 -0.50 6.10 5 6 11 -0.80 1.50 5 6 11 -1.60 0.80 6 -6 11 44.50 5.10 -6 -6 -11 40.30 12.30 6 6 11 42.70 3.30 6 6 11 47.50 5.60 7 -6 11 27.00 4.20 7 6 11 26.00 4.40 7 6 11 20.90 2.80 8 -6 11 -0.40 1.70 8 6 11 2.20 2.10 8 6 11 2.50 1.60 9 -6 11 81.49 6.30 9 6 11 96.79 7.00 9 6 11 106.59 5.40 10 -6 11 0.40 2.00 10 6 11 1.10 1.60 10 6 11 3.10 2.20 11 -6 11 55.49 6.30 11 6 11 54.69 6.50 11 6 11 51.49 4.10 12 -6 11 1.70 2.20 12 6 11 -0.30 1.90 12 6 11 2.30 1.70 13 -6 11 16.10 4.10 13 6 11 19.70 3.30 13 6 11 19.80 4.30 13 6 11 23.40 4.60 14 -6 11 6.80 3.00 14 6 11 3.90 2.10 14 6 11 6.80 3.30 14 6 11 11.40 3.40 15 -6 11 11.20 3.40 15 6 11 15.10 4.10 15 6 11 11.90 2.80 15 6 11 8.70 3.60 16 -6 11 5.70 2.80 16 6 11 3.30 2.90 16 6 11 4.50 3.20 16 6 11 4.10 2.10 17 -6 11 10.30 3.70 17 6 11 7.60 3.50 17 6 11 12.80 4.20 18 -6 11 3.70 3.00 18 6 11 -1.20 2.70 18 6 11 0.00 2.00 19 -6 11 2.20 3.00 19 6 11 1.40 3.20 19 6 11 0.10 2.10 20 -6 11 3.90 3.50 20 6 11 9.60 3.50 20 6 11 1.80 3.40 -21 -7 11 4.40 3.10 21 7 -11 8.70 3.20 -21 7 11 8.90 2.20 -20 -7 11 22.80 4.30 20 7 -11 20.10 4.10 -20 7 11 19.00 2.80 -19 -7 11 4.80 2.70 19 7 -11 10.30 3.10 -19 7 11 6.80 1.90 -18 -7 11 26.90 4.60 18 7 -11 40.30 5.50 -18 7 11 32.80 3.50 -17 -7 11 -1.30 1.80 -17 7 11 2.50 1.60 17 7 -11 0.50 2.20 -16 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14 9.70 3.60 13 3 14 13.10 4.00 14 -3 14 1.70 2.20 14 3 14 0.70 2.40 14 3 14 2.00 2.50 15 -3 14 3.80 2.50 15 3 14 10.00 3.40 15 3 14 8.10 3.20 16 -3 14 0.70 2.10 16 3 14 1.70 2.70 16 3 14 5.60 3.10 17 -3 14 20.50 4.50 17 3 14 9.90 3.90 17 3 14 14.90 4.20 18 -3 14 1.00 2.80 18 3 14 -1.40 2.40 18 3 14 0.70 2.70 19 -3 14 3.10 3.10 19 3 14 5.10 3.10 19 3 14 1.30 2.80 20 -3 14 -0.80 2.50 20 3 14 1.70 3.00 20 3 14 4.00 3.30 21 -3 14 2.10 3.30 21 3 14 2.90 3.10 21 3 14 0.70 2.80 -23 -4 14 12.40 2.40 23 -4 -14 15.30 3.40 -23 -4 14 21.60 4.50 -23 4 14 14.20 2.50 23 4 -14 22.00 4.30 -22 -4 14 8.00 3.20 -22 -4 14 6.70 1.80 22 -4 -14 11.10 2.80 -22 4 14 7.90 2.10 22 4 -14 17.20 3.80 -21 -4 14 16.50 2.50 -21 -4 14 14.70 3.70 21 -4 -14 17.10 3.30 -21 4 14 16.80 2.60 21 4 -14 16.80 3.80 -20 -4 14 2.20 1.40 -20 -4 14 4.20 2.50 20 -4 -14 0.00 1.70 20 4 -14 0.80 1.90 -20 4 14 -1.30 1.10 -19 -4 14 63.39 3.70 -19 -4 14 53.79 6.00 19 -4 -14 64.49 4.60 -19 4 14 56.19 3.60 19 4 -14 55.39 5.80 -18 -4 14 16.80 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-4 14 111.29 4.10 -5 4 14 111.89 7.00 5 4 -14 110.89 4.80 -5 4 14 118.49 4.30 -5 4 14 112.39 3.60 -5 4 14 113.79 4.40 -4 -4 14 126.79 7.30 -4 -4 14 131.39 4.60 4 -4 -14 141.59 7.00 -4 4 14 128.89 4.00 4 4 -14 123.19 6.50 4 4 -14 127.59 5.10 -4 4 14 149.49 8.10 -4 4 14 125.29 4.70 -4 4 14 138.39 4.90 -3 -4 14 195.78 6.10 -3 -4 14 204.08 9.60 3 -4 -14 188.58 7.90 3 -4 -14 239.68 37.80 3 4 -14 198.38 9.00 -3 4 14 187.68 9.40 -3 4 14 197.08 5.50 3 4 -14 184.68 6.40 -3 4 14 207.38 6.30 -3 4 14 192.48 6.40 -2 -4 14 199.08 6.20 -2 -4 14 202.28 7.30 2 -4 -14 203.38 7.90 2 -4 -14 180.48 31.70 -2 -4 14 226.68 10.50 -2 4 14 199.28 6.40 -2 4 14 209.68 5.80 -2 4 14 205.68 9.90 2 4 -14 214.58 10.00 -1 -4 14 66.59 5.70 1 -4 -14 74.79 4.00 -1 -4 14 76.09 4.30 1 -4 -14 109.69 26.00 -1 -4 14 73.99 2.90 1 4 -14 72.09 6.10 -1 4 14 68.89 2.60 -1 4 14 68.19 5.60 -1 4 14 72.79 3.30 0 -4 14 195.38 7.60 0 -4 -14 197.88 7.00 0 -4 14 206.68 5.90 0 -4 14 195.38 10.50 0 -4 -14 196.58 34.60 0 4 14 200.68 6.40 0 4 14 207.28 10.20 0 4 -14 189.18 10.30 1 -4 14 28.80 3.50 -1 -4 -14 24.20 2.10 1 -4 14 29.70 5.10 -1 -4 -14 17.90 15.50 -1 -4 -14 23.90 1.80 1 4 14 25.50 2.10 1 4 14 26.30 4.30 -1 4 -14 24.40 4.60 -2 -4 -14 191.08 6.30 -2 -4 -14 149.59 30.40 -2 -4 -14 181.38 5.80 2 -4 14 201.48 11.00 2 -4 14 186.98 7.70 2 4 14 200.88 9.90 -2 4 -14 186.38 10.70 -2 4 -14 178.48 6.60 2 4 14 182.28 6.10 3 -4 14 305.57 14.20 3 -4 14 295.27 10.60 -3 -4 -14 282.27 8.60 -3 -4 -14 272.77 42.40 -3 4 -14 299.77 15.40 3 4 14 289.27 12.80 3 4 14 289.57 8.70 -4 -4 -14 69.19 3.40 -4 -4 -14 69.79 23.30 4 -4 14 82.19 7.00 4 -4 14 71.29 4.90 4 4 14 67.59 5.90 4 4 14 72.19 3.50 5 -4 14 171.98 8.00 -5 -4 -14 149.29 32.40 5 -4 14 186.18 10.70 5 4 14 172.88 9.60 5 4 14 175.68 6.20 6 -4 14 11.00 3.90 6 -4 14 11.50 2.80 -6 -4 -14 14.00 14.50 6 4 14 20.00 4.20 6 4 14 13.40 2.00 7 -4 14 97.39 6.20 -7 -4 -14 89.09 24.80 7 -4 14 105.49 8.10 7 4 14 118.69 7.80 7 4 14 113.89 4.80 8 -4 14 9.60 2.80 8 -4 14 11.20 3.60 8 4 14 11.50 2.10 8 4 14 12.60 3.70 9 -4 14 76.29 8.10 9 -4 14 59.29 6.10 9 4 14 65.89 3.90 9 4 14 67.09 7.10 9 4 14 77.49 8.20 -10 -4 -14 3.70 0.80 10 -4 14 3.90 2.40 10 4 14 2.70 2.50 10 4 14 1.80 2.20 11 -4 14 37.00 5.10 11 4 14 39.30 6.00 11 4 14 45.80 6.30 12 -4 14 8.90 3.00 12 4 14 1.50 2.70 12 4 14 6.40 3.10 13 -4 14 21.50 4.30 13 4 14 9.50 3.50 13 4 14 15.30 4.10 14 -4 14 36.80 5.50 14 4 14 34.00 5.70 14 4 14 41.20 6.40 15 -4 14 5.70 2.80 15 4 14 1.20 2.50 15 4 14 1.50 2.40 16 -4 14 34.10 5.70 16 4 14 20.50 4.70 16 4 14 21.20 4.60 17 -4 14 2.10 2.10 17 4 14 2.90 2.70 17 4 14 -1.50 2.30 18 -4 14 18.70 4.80 18 4 14 21.80 4.90 18 4 14 19.60 4.90 19 -4 14 -0.50 2.50 19 4 14 2.90 3.10 19 4 14 -1.50 2.00 20 -4 14 14.50 4.10 20 4 14 27.60 5.80 20 4 14 29.10 5.50 -22 -5 14 22.30 2.90 -22 -5 14 13.60 3.80 -22 5 14 22.10 2.90 22 5 -14 18.70 4.20 -21 -5 14 -1.20 1.10 -21 -5 14 -1.10 2.30 -21 5 14 -0.60 1.20 21 5 -14 0.30 1.90 -20 -5 14 44.60 5.90 -20 -5 14 40.50 3.20 20 5 -14 48.30 5.90 -20 5 14 48.20 3.60 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7.60 2.50 -4 -5 14 6.40 1.20 -4 5 14 7.00 1.00 4 5 -14 8.50 1.80 -4 5 14 10.60 1.80 -4 5 14 5.60 2.40 3 -5 -14 42.40 3.40 -3 -5 14 38.50 2.20 -3 -5 14 39.60 5.10 -3 5 14 37.70 2.50 -3 5 14 41.90 5.10 -3 5 14 34.80 1.80 2 -5 -14 54.09 17.70 -2 -5 14 49.80 5.90 -2 -5 14 47.50 3.70 2 -5 -14 44.80 3.30 -2 -5 14 46.20 2.40 -2 5 14 60.59 6.20 -2 5 14 53.09 2.20 2 5 -14 51.19 5.30 -2 5 14 51.39 3.00 -1 -5 14 107.79 3.90 -1 -5 14 109.89 5.60 1 -5 -14 118.19 25.10 -1 -5 14 120.29 7.60 1 -5 -14 97.09 4.80 -1 5 14 113.29 4.60 1 5 -14 100.19 7.10 -1 5 14 120.29 7.30 0 -5 14 389.06 15.80 0 -5 -14 372.36 37.60 0 -5 14 380.96 12.60 0 5 14 388.86 11.00 0 5 -14 386.26 15.70 0 5 14 398.76 15.10 1 -5 14 89.59 8.80 1 -5 14 76.79 4.90 -1 -5 -14 90.59 24.00 1 5 14 76.29 3.80 1 5 14 77.89 6.10 2 -5 14 18.80 4.60 2 -5 14 22.80 3.40 -2 -5 -14 27.90 14.00 2 5 14 22.40 4.10 2 5 14 23.30 2.40 3 -5 14 37.10 6.40 3 -5 14 26.50 3.80 -3 -5 -14 20.30 14.30 3 5 14 33.30 5.00 3 5 14 30.70 2.60 4 -5 14 31.10 5.60 -4 -5 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0 0 31 7.00 4.90 1 0 31 3.00 5.00 2 0 31 1.10 4.10 -7 -1 31 -1.70 4.10 -7 1 31 -4.30 4.10 -6 -1 31 3.50 4.70 -6 1 31 4.50 4.80 -5 -1 31 -0.50 3.80 -5 1 31 2.60 4.40 -4 -1 31 11.20 6.10 -4 1 31 16.00 6.20 -3 -1 31 5.00 5.00 -3 1 31 0.10 4.30 -2 -1 31 8.70 5.10 -2 1 31 9.80 5.70 -1 -1 31 5.20 4.50 -1 1 31 -0.20 3.60 0 -1 31 9.00 5.20 0 1 31 3.80 4.40 1 -1 31 5.90 4.70 1 1 31 -0.30 3.90 2 -1 31 -0.70 4.80 2 1 31 6.60 4.90 -6 -2 31 -0.20 3.30 -6 2 31 3.80 4.60 -5 -2 31 27.00 8.40 -5 2 31 40.30 8.80 -4 -2 31 0.60 4.00 -4 2 31 3.40 4.10 -3 -2 31 10.70 6.00 -3 2 31 14.60 6.10 -2 -2 31 4.90 4.70 -2 2 31 1.10 4.40 -1 -2 31 15.40 6.80 -1 2 31 22.80 6.90 0 -2 31 16.60 6.60 0 2 31 10.80 5.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 3155