# Electronic Supplementary Material (ESI) for Chemical Communications. # This journal is © The Royal Society of Chemistry 2023 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_Cu2(pyalk)2(OAc)2 _database_code_depnum_ccdc_archive 'CCDC 2215584' loop_ _audit_author_name _audit_author_address 'Devi Prasad Adiyeri Saseendran' ;University of Zurich Switzerland ; _audit_update_record ; 2022-10-27 deposited with the CCDC. 2023-04-11 downloaded from the CCDC. ; _audit_creation_date 2022-10-27 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C20 H30 Cu2 N2 O8, 2(H2 O)' _chemical_formula_sum 'C20 H34 Cu2 N2 O10' _chemical_formula_weight 589.57 _chemical_melting_point ? _chemical_oxdiff_formula 'C10 H15 Cu N O5' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.02330(10) _cell_length_b 8.8028(2) _cell_length_c 9.65090(10) _cell_angle_alpha 71.0760(10) _cell_angle_beta 86.2810(10) _cell_angle_gamma 77.2790(10) _cell_volume 628.935(18) _cell_formula_units_Z 1 _cell_measurement_reflns_used 36194 _cell_measurement_temperature 160.00(10) _cell_measurement_theta_max 37.9080 _cell_measurement_theta_min 2.4940 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 1.745 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.408 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.39a (Rigaku Oxford Diffraction, 2019) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour blue _exptl_crystal_density_diffrn 1.557 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 306 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -5 5 11 0.0969 7 0 -10 0.0916 2 12 6 0.0873 -3 -12 -5 0.0852 10 -1 4 0.0990 -2 -12 1 0.0916 -3 -2 -13 0.0628 -6 -9 -11 0.0782 3 3 13 0.0713 -1 -5 10 0.0802 3 -5 -13 0.0763 0 10 11 0.0775 2 -11 -8 0.0954 6 11 0 0.1086 0 12 6 0.0891 -6 6 10 0.0969 -6 -11 0 0.1181 -2 -11 -10 0.0759 5 5 -9 0.0921 -3 3 13 0.0879 -6 6 -7 0.0765 0 10 -3 0.0805 9 -1 7 0.0922 6 -6 7 0.0850 1 -10 4 0.0855 4 9 11 0.0918 4 7 -7 0.0865 10 0 -5 0.1043 -7 7 -1 0.0928 -9 4 -1 0.0998 5 -9 0 0.0954 2 9 -5 0.0757 -3 3 -10 0.0617 -7 -6 -11 0.0736 -8 0 -9 0.0779 -9 -3 -8 0.0793 _exptl_crystal_size_max 0.256 _exptl_crystal_size_mid 0.181 _exptl_crystal_size_min 0.137 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -4.8854 5.1035 11.3568 0.2327 0.9718 -0.0385 6.6840 -0.0122 -10.2979 -0.2154 -0.9015 -0.3754 1.9607 12.2702 6.2062 0.1180 0.4894 -0.8640 -2.9759 -12.3942 -4.7367 -0.0871 -0.3602 0.9288 10.0814 -1.3597 3.6486 0.8516 -0.5210 -0.0582 -2.1362 -11.5808 0.5025 0.2486 -0.1533 0.9564 -2.6477 -1.8555 -13.0870 -0.8764 -0.4765 -0.0694 -5.6475 -9.3674 -10.5081 -0.6769 -0.3690 0.6369 3.0399 2.7099 13.1607 0.8785 0.4777 -0.0044 -0.7123 -4.7598 10.1885 0.7034 0.3817 0.5996 2.7652 -5.3176 -12.6582 -0.4285 -0.9001 0.0782 0.4382 10.2803 10.6252 0.3493 0.7353 -0.5809 2.1854 -10.7240 -7.8940 -0.0194 -0.7920 0.6102 5.6204 11.1762 -0.0281 -0.0029 -0.0609 -0.9981 0.1757 12.0262 6.1074 0.0141 0.5935 -0.8047 -6.0515 6.1259 9.5296 0.0251 0.9914 -0.1283 -5.6358 -11.1633 0.0509 0.0029 0.0633 0.9980 -2.2434 -11.2113 -9.5060 -0.3617 -0.5930 0.7194 5.1269 4.6491 -9.2663 -0.3850 -0.6275 -0.6768 -2.7659 2.8709 12.9476 0.5185 0.8470 0.1170 -5.5560 5.5041 -6.5146 -0.8778 0.2106 -0.4303 0.2021 10.2613 -3.2435 -0.4859 0.1173 -0.8661 8.5417 -0.8420 7.4804 0.9723 -0.2328 0.0192 5.5325 -5.5322 6.5042 0.8766 -0.2103 0.4328 0.9194 -9.6206 3.9756 0.5763 -0.1389 0.8053 3.8205 9.4645 11.3673 0.6171 0.5287 -0.5828 3.7132 7.4394 -7.3442 -0.4376 -0.3729 -0.8182 10.0148 0.0054 -5.4864 0.2657 -0.8964 -0.3547 -7.2882 7.0214 -0.5469 -0.6716 0.6358 -0.3804 -9.2428 4.3780 -0.7368 -0.7194 0.6816 -0.1336 4.7590 -9.2773 0.3124 0.5756 -0.5445 0.6101 1.7514 9.3917 -5.0716 -0.4769 -0.0897 -0.8744 -3.4293 3.0842 -10.4077 -0.9109 -0.1699 -0.3760 -7.4567 -5.9043 -10.6867 -0.8974 -0.1665 0.4086 -8.1748 -0.1165 -8.6475 -0.9913 0.1299 0.0215 -9.2527 -3.2760 -8.4142 -0.9470 0.1244 0.2962 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0360 _diffrn_reflns_av_unetI/netI 0.0208 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.945 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 58956 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.945 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 37.921 _diffrn_reflns_theta_min 2.231 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 160.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 200K' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.945 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 2.00 45.00 0.50 2.50 -- 14.35 57.00 30.00 86 2 \w 9.00 74.00 0.50 2.50 -- 14.35 57.00 150.00 130 3 \w 16.00 80.00 0.50 2.50 -- 14.35 57.00 60.00 128 4 \w 24.00 82.00 0.50 2.50 -- 14.35 19.00-180.00 116 5 \w 0.00 27.00 0.50 2.50 -- 14.35 -57.00-180.00 54 6 \w -84.00 -1.00 0.50 2.50 -- -15.76 -59.00-140.56 166 7 \w -90.00 -12.00 0.50 2.50 -- -15.76 -19.00 -60.00 156 8 \w -94.00 -7.00 0.50 2.50 -- -15.76 -19.00-150.00 174 9 \w -42.00 -8.00 0.50 2.50 -- -15.76 -57.00 0.00 68 10 \w -60.00 -2.00 0.50 2.50 -- -15.76 -57.00 120.00 116 11 \w -45.00 -19.00 0.50 2.50 -- -15.76 -60.00 -59.31 52 12 \w -31.00 32.00 0.50 2.50 -- -15.76 60.00 153.76 126 13 \w -31.00 -6.00 0.50 2.50 -- -15.76 60.00-163.40 50 14 \w 2.00 33.00 0.50 2.50 -- -15.76 60.00-163.40 62 15 \w -31.00 23.00 0.50 2.50 -- -15.76 60.00-117.52 108 16 \w -30.00 30.00 0.50 2.50 -- -15.76 57.00 -30.00 120 17 \w -30.00 37.00 0.50 2.50 -- -15.76 57.00 0.00 134 18 \w -30.00 28.00 0.50 2.50 -- -15.76 57.00 -90.00 116 19 \w -30.00 50.00 0.50 2.50 -- -15.76 57.00 30.00 160 20 \w -30.00 19.00 0.50 2.50 -- -15.76 57.00 -60.00 98 21 \w -30.00 41.00 0.50 2.50 -- -15.76 57.00 120.00 142 22 \w -30.00 31.00 0.50 2.50 -- -15.76 57.00 75.86 122 23 \w 12.00 37.00 0.50 2.50 -- 22.00 -60.00 -56.31 50 24 \w -94.00 -10.00 0.50 2.50 -- -22.09 -58.00 -78.21 168 25 \w -6.00 28.00 0.50 2.50 -- -22.09 57.00 0.00 68 26 \w -71.00 -14.00 0.50 2.50 -- -22.09 -60.00 4.16 114 27 \w -94.00 -48.00 0.50 2.50 -- -22.09 -59.00 32.97 92 28 \w -45.00 -9.00 0.50 2.50 -- -22.09 -59.00 32.97 72 29 \w -37.00 38.00 0.50 2.50 -- -22.09 60.00 69.65 150 30 \w -36.00 46.00 0.50 2.50 -- -22.09 57.00 -90.00 164 31 \w -89.00 -14.00 0.50 2.50 -- -22.09 -57.00-180.00 150 32 \w -36.00 1.00 0.50 2.50 -- -22.09 57.00-180.00 74 33 \w 4.00 42.00 0.50 2.50 -- -22.09 57.00-180.00 76 34 \w -84.00 -16.00 0.50 2.50 -- -22.09 -57.00 120.00 136 35 \w -36.00 36.00 0.50 2.50 -- -22.09 57.00 150.00 144 36 \w -36.00 -10.00 0.50 2.50 -- -22.09 57.00 0.00 52 37 \w -93.00 -7.00 0.50 2.50 -- -22.09 -60.00-136.64 172 38 \w -36.00 12.00 0.50 2.50 -- -22.09 57.00 120.00 96 39 \w -36.00 50.00 0.50 2.50 -- -22.09 57.00 -60.00 172 40 \w -36.00 32.00 0.50 2.50 -- -22.09 57.00 30.00 136 41 \w -37.00 23.00 0.50 2.50 -- -22.09 60.00-141.55 120 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 200K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0590069000 _diffrn_orient_matrix_UB_12 -0.0297830000 _diffrn_orient_matrix_UB_13 0.0592542000 _diffrn_orient_matrix_UB_21 -0.0645329000 _diffrn_orient_matrix_UB_22 0.0271209000 _diffrn_orient_matrix_UB_23 0.0456216000 _diffrn_orient_matrix_UB_31 -0.0238279000 _diffrn_orient_matrix_UB_32 -0.0772736000 _diffrn_orient_matrix_UB_33 0.0210808000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 5683 _reflns_number_total 6442 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.40.39a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.39a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.39a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.512 _refine_diff_density_min -0.613 _refine_diff_density_rms 0.065 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.062 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 173 _refine_ls_number_reflns 6442 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0310 _refine_ls_R_factor_gt 0.0247 _refine_ls_restrained_S_all 1.062 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0347P)^2^+0.1140P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0642 _refine_ls_wR_factor_ref 0.0662 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C1(H1), C4(H4), C3(H3), C2(H2) 2.b Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C10(H10A,H10B,H10C), C7(H7A,H7B,H7C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.64799(2) 0.55497(2) 0.90975(2) 0.01439(3) Uani 1 1 d . . . . . O1 O 0.42404(8) 0.64275(8) 0.96803(7) 0.01839(11) Uani 1 1 d . . . . . O2 O 0.85342(8) 0.45230(9) 0.82582(7) 0.01904(11) Uani 1 1 d . . . . . O4 O 0.80212(10) 0.61014(11) 1.07614(8) 0.02549(14) Uani 1 1 d . . . . . O3 O 0.69592(10) 0.48470(11) 0.63269(8) 0.02860(15) Uani 1 1 d . . . . . N1 N 0.62565(10) 0.78449(9) 0.77836(8) 0.01755(12) Uani 1 1 d . . . . . O5 O 0.65775(12) 0.49121(15) 0.34830(9) 0.0379(2) Uani 1 1 d . . . . . C5 C 0.47648(11) 0.88503(10) 0.78771(9) 0.01765(14) Uani 1 1 d . . . . . C9 C 0.83102(11) 0.42816(11) 0.70500(9) 0.01836(14) Uani 1 1 d . . . . . C6 C 0.34697(11) 0.80882(10) 0.89729(9) 0.01725(13) Uani 1 1 d . . . . . C1 C 0.74790(13) 0.84342(12) 0.68763(10) 0.02341(17) Uani 1 1 d . . . . . H1 H 0.853594 0.770966 0.683231 0.028 Uiso 1 1 calc R U . . . C4 C 0.44488(14) 1.05021(12) 0.70235(11) 0.02556(18) Uani 1 1 d . . . . . H4 H 0.338643 1.120751 0.709157 0.031 Uiso 1 1 calc R U . . . C3 C 0.56937(16) 1.11070(13) 0.60763(12) 0.0290(2) Uani 1 1 d . . . . . H3 H 0.548856 1.222663 0.548020 0.035 Uiso 1 1 calc R U . . . C8 C 0.30546(17) 0.90022(14) 1.01018(12) 0.0310(2) Uani 1 1 d . . . . . H8A H 0.215241 0.858763 1.075270 0.047 Uiso 1 1 calc R U . . . H8B H 0.266467 1.018004 0.959453 0.047 Uiso 1 1 calc R U . . . H8C H 0.408137 0.882324 1.068009 0.047 Uiso 1 1 calc R U . . . C2 C 0.72424(15) 1.00614(14) 0.60073(11) 0.02815(19) Uani 1 1 d . . . . . H2 H 0.812185 1.045366 0.537702 0.034 Uiso 1 1 calc R U . . . C10 C 0.97964(13) 0.32241(14) 0.65260(12) 0.02713(19) Uani 1 1 d . . . . . H10A H 1.080129 0.371635 0.640600 0.041 Uiso 1 1 calc R U . . . H10B H 0.950143 0.314779 0.558459 0.041 Uiso 1 1 calc R U . . . H10C H 1.005053 0.212222 0.724734 0.041 Uiso 1 1 calc R U . . . C7 C 0.18518(12) 0.81904(12) 0.81597(12) 0.02611(18) Uani 1 1 d . . . . . H7A H 0.214567 0.759676 0.744648 0.039 Uiso 1 1 calc R U . . . H7B H 0.134238 0.934418 0.764846 0.039 Uiso 1 1 calc R U . . . H7C H 0.103182 0.769549 0.886362 0.039 Uiso 1 1 calc R U . . . H5A H 0.561(3) 0.498(2) 0.338(2) 0.044(5) Uiso 1 1 d . . . . . H5B H 0.679(2) 0.492(2) 0.4232(19) 0.038(4) Uiso 1 1 d . . . . . H4A H 0.765(2) 0.571(2) 1.155(2) 0.044(5) Uiso 1 1 d . . . . . H4B H 0.902(2) 0.5937(19) 1.0916(17) 0.030(4) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01143(5) 0.01645(5) 0.01318(5) -0.00213(3) 0.00063(3) -0.00268(3) O1 0.0133(2) 0.0153(3) 0.0207(3) 0.0004(2) 0.0023(2) -0.00086(19) O2 0.0141(2) 0.0258(3) 0.0165(3) -0.0070(2) 0.00048(19) -0.0025(2) O4 0.0193(3) 0.0395(4) 0.0190(3) -0.0078(3) -0.0022(2) -0.0104(3) O3 0.0185(3) 0.0452(4) 0.0235(3) -0.0157(3) -0.0031(2) -0.0017(3) N1 0.0167(3) 0.0194(3) 0.0154(3) -0.0029(2) 0.0004(2) -0.0057(2) O5 0.0235(4) 0.0741(7) 0.0220(3) -0.0196(4) 0.0046(3) -0.0172(4) C5 0.0195(3) 0.0165(3) 0.0164(3) -0.0032(3) -0.0015(3) -0.0052(3) C9 0.0149(3) 0.0221(4) 0.0181(3) -0.0065(3) 0.0032(3) -0.0047(3) C6 0.0164(3) 0.0145(3) 0.0193(3) -0.0040(3) 0.0007(3) -0.0023(2) C1 0.0222(4) 0.0263(4) 0.0207(4) -0.0034(3) 0.0038(3) -0.0104(3) C4 0.0294(5) 0.0170(4) 0.0265(4) -0.0018(3) -0.0013(3) -0.0046(3) C3 0.0402(6) 0.0200(4) 0.0249(4) -0.0003(3) 0.0001(4) -0.0126(4) C8 0.0430(6) 0.0254(4) 0.0298(5) -0.0142(4) 0.0130(4) -0.0130(4) C2 0.0352(5) 0.0280(5) 0.0222(4) -0.0029(3) 0.0052(4) -0.0177(4) C10 0.0223(4) 0.0301(5) 0.0313(5) -0.0162(4) 0.0056(3) -0.0021(3) C7 0.0183(4) 0.0224(4) 0.0319(5) -0.0008(3) -0.0066(3) -0.0024(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O1 1.9187(6) . ? Cu1 O1 1.9435(6) 2_667 ? Cu1 O2 1.9583(6) . ? Cu1 O4 2.3178(7) . ? Cu1 N1 1.9825(7) . ? O1 C6 1.4124(10) . ? O2 C9 1.2813(11) . ? O4 H4A 0.791(19) . ? O4 H4B 0.797(17) . ? O3 C9 1.2430(11) . ? N1 C5 1.3398(12) . ? N1 C1 1.3475(12) . ? O5 H5A 0.78(2) . ? O5 H5B 0.757(17) . ? C5 C6 1.5339(12) . ? C5 C4 1.3946(13) . ? C9 C10 1.5108(13) . ? C6 C8 1.5325(13) . ? C6 C7 1.5310(13) . ? C1 H1 0.9500 . ? C1 C2 1.3830(14) . ? C4 H4 0.9500 . ? C4 C3 1.3845(15) . ? C3 H3 0.9500 . ? C3 C2 1.3860(18) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C2 H2 0.9500 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Cu1 O1 78.13(3) . 2_667 ? O1 Cu1 O2 98.82(3) 2_667 . ? O1 Cu1 O2 169.19(3) . . ? O1 Cu1 O4 97.44(3) . . ? O1 Cu1 O4 101.36(3) 2_667 . ? O1 Cu1 N1 158.08(3) 2_667 . ? O1 Cu1 N1 81.96(3) . . ? O2 Cu1 O4 93.32(3) . . ? O2 Cu1 N1 99.05(3) . . ? N1 Cu1 O4 90.17(3) . . ? Cu1 O1 Cu1 101.87(3) . 2_667 ? C6 O1 Cu1 137.33(5) . 2_667 ? C6 O1 Cu1 119.29(5) . . ? C9 O2 Cu1 115.53(6) . . ? Cu1 O4 H4A 106.6(13) . . ? Cu1 O4 H4B 132.5(11) . . ? H4A O4 H4B 103.1(17) . . ? C5 N1 Cu1 114.78(6) . . ? C5 N1 C1 119.96(8) . . ? C1 N1 Cu1 125.23(7) . . ? H5A O5 H5B 113.0(19) . . ? N1 C5 C6 116.45(7) . . ? N1 C5 C4 120.63(8) . . ? C4 C5 C6 122.91(8) . . ? O2 C9 C10 116.28(8) . . ? O3 C9 O2 123.71(8) . . ? O3 C9 C10 120.01(8) . . ? O1 C6 C5 107.45(7) . . ? O1 C6 C8 109.74(8) . . ? O1 C6 C7 109.92(7) . . ? C8 C6 C5 109.03(7) . . ? C7 C6 C5 109.79(7) . . ? C7 C6 C8 110.84(8) . . ? N1 C1 H1 119.0 . . ? N1 C1 C2 122.03(10) . . ? C2 C1 H1 119.0 . . ? C5 C4 H4 120.2 . . ? C3 C4 C5 119.56(10) . . ? C3 C4 H4 120.2 . . ? C4 C3 H3 120.4 . . ? C4 C3 C2 119.28(9) . . ? C2 C3 H3 120.4 . . ? C6 C8 H8A 109.5 . . ? C6 C8 H8B 109.5 . . ? C6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C1 C2 C3 118.52(10) . . ? C1 C2 H2 120.7 . . ? C3 C2 H2 120.7 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C6 C7 H7A 109.5 . . ? C6 C7 H7B 109.5 . . ? C6 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 O1 C6 C5 -2.84(9) . . . . ? Cu1 O1 C6 C5 -165.87(6) 2_667 . . . ? Cu1 O1 C6 C8 -121.26(7) . . . . ? Cu1 O1 C6 C8 75.72(11) 2_667 . . . ? Cu1 O1 C6 C7 116.59(7) . . . . ? Cu1 O1 C6 C7 -46.43(11) 2_667 . . . ? Cu1 O2 C9 O3 9.77(12) . . . . ? Cu1 O2 C9 C10 -169.36(7) . . . . ? Cu1 N1 C5 C6 0.08(10) . . . . ? Cu1 N1 C5 C4 179.30(7) . . . . ? Cu1 N1 C1 C2 -178.86(7) . . . . ? N1 C5 C6 O1 1.68(10) . . . . ? N1 C5 C6 C8 120.56(9) . . . . ? N1 C5 C6 C7 -117.84(9) . . . . ? N1 C5 C4 C3 -0.29(15) . . . . ? N1 C1 C2 C3 -0.20(16) . . . . ? C5 N1 C1 C2 -0.88(14) . . . . ? C5 C4 C3 C2 -0.78(16) . . . . ? C6 C5 C4 C3 178.88(9) . . . . ? C1 N1 C5 C6 -178.10(8) . . . . ? C1 N1 C5 C4 1.12(13) . . . . ? C4 C5 C6 O1 -177.52(8) . . . . ? C4 C5 C6 C8 -58.65(12) . . . . ? C4 C5 C6 C7 62.96(11) . . . . ? C4 C3 C2 C1 1.02(16) . . . . ? _shelx_res_file ; TITL dp-18-new-final_a.res in P-1 dp-18-new-final.res created by SHELXL-2018/3 at 04:37:44 on 27-Oct-2022 REM Old TITL DP-18-new-final in P-1 REM SHELXT solution in P-1: R1 0.069, Rweak 0.006, Alpha 0.044 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C10 N2 O4 Cu CELL 0.71073 8.0233 8.8028 9.6509 71.076 86.281 77.279 ZERR 1 0.0001 0.0002 0.0001 0.001 0.001 0.001 LATT 1 SFAC C H Cu N O UNIT 20 34 2 2 10 EQIV $1 1-X,1-Y,2-Z L.S. 10 PLAN 15 TEMP -113 CONF FREE Cu1 Cu1_$1 list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.034700 0.114000 FVAR 0.81578 CU1 3 0.647993 0.554965 0.909745 11.00000 0.01143 0.01645 = 0.01318 -0.00213 0.00063 -0.00268 O1 5 0.424037 0.642749 0.968026 11.00000 0.01335 0.01525 = 0.02066 0.00043 0.00228 -0.00086 O2 5 0.853418 0.452296 0.825823 11.00000 0.01407 0.02578 = 0.01653 -0.00697 0.00048 -0.00246 O4 5 0.802116 0.610143 1.076144 11.00000 0.01931 0.03947 = 0.01895 -0.00782 -0.00216 -0.01041 O3 5 0.695919 0.484697 0.632690 11.00000 0.01854 0.04525 = 0.02351 -0.01569 -0.00309 -0.00167 N1 4 0.625651 0.784489 0.778360 11.00000 0.01672 0.01944 = 0.01538 -0.00286 0.00037 -0.00568 O5 5 0.657748 0.491211 0.348301 11.00000 0.02350 0.07407 = 0.02196 -0.01960 0.00460 -0.01717 C5 1 0.476484 0.885034 0.787706 11.00000 0.01946 0.01646 = 0.01644 -0.00320 -0.00152 -0.00521 C9 1 0.831024 0.428161 0.705005 11.00000 0.01494 0.02214 = 0.01806 -0.00654 0.00315 -0.00469 C6 1 0.346965 0.808823 0.897293 11.00000 0.01641 0.01447 = 0.01932 -0.00403 0.00072 -0.00229 C1 1 0.747897 0.843424 0.687634 11.00000 0.02222 0.02628 = 0.02073 -0.00337 0.00383 -0.01038 AFIX 43 H1 2 0.853594 0.770966 0.683231 11.00000 -1.20000 AFIX 0 C4 1 0.444879 1.050211 0.702353 11.00000 0.02945 0.01697 = 0.02651 -0.00178 -0.00131 -0.00458 AFIX 43 H4 2 0.338643 1.120751 0.709157 11.00000 -1.20000 AFIX 0 C3 1 0.569367 1.110701 0.607634 11.00000 0.04015 0.01999 = 0.02488 -0.00034 0.00013 -0.01259 AFIX 43 H3 2 0.548856 1.222663 0.548020 11.00000 -1.20000 AFIX 0 C8 1 0.305462 0.900216 1.010181 11.00000 0.04296 0.02538 = 0.02982 -0.01420 0.01296 -0.01303 AFIX 137 H8A 2 0.215241 0.858763 1.075270 11.00000 -1.50000 H8B 2 0.266467 1.018004 0.959453 11.00000 -1.50000 H8C 2 0.408137 0.882324 1.068009 11.00000 -1.50000 AFIX 0 C2 1 0.724239 1.006140 0.600728 11.00000 0.03521 0.02798 = 0.02215 -0.00288 0.00523 -0.01769 AFIX 43 H2 2 0.812185 1.045366 0.537702 11.00000 -1.20000 AFIX 0 C10 1 0.979641 0.322411 0.652596 11.00000 0.02231 0.03005 = 0.03133 -0.01621 0.00565 -0.00206 AFIX 137 H10A 2 1.080129 0.371635 0.640600 11.00000 -1.50000 H10B 2 0.950143 0.314779 0.558459 11.00000 -1.50000 H10C 2 1.005053 0.212222 0.724734 11.00000 -1.50000 AFIX 0 C7 1 0.185182 0.819035 0.815970 11.00000 0.01826 0.02236 = 0.03189 -0.00076 -0.00658 -0.00238 AFIX 137 H7A 2 0.214567 0.759676 0.744648 11.00000 -1.50000 H7B 2 0.134238 0.934418 0.764846 11.00000 -1.50000 H7C 2 0.103182 0.769549 0.886362 11.00000 -1.50000 AFIX 0 H5A 2 0.561219 0.497701 0.337608 11.00000 0.04362 H5B 2 0.678911 0.492339 0.423198 11.00000 0.03847 H4A 2 0.764927 0.571192 1.154517 11.00000 0.04426 H4B 2 0.901956 0.593682 1.091561 11.00000 0.03016 HKLF 4 REM dp-18-new-final_a.res in P-1 REM wR2 = 0.0662, GooF = S = 1.062, Restrained GooF = 1.062 for all data REM R1 = 0.0247 for 5683 Fo > 4sig(Fo) and 0.0310 for all 6442 data REM 173 parameters refined using 0 restraints END WGHT 0.0347 0.1140 REM Highest difference peak 0.512, deepest hole -0.613, 1-sigma level 0.065 Q1 1 0.8447 0.4442 0.7646 11.00000 0.05 0.51 Q2 1 0.7440 0.9173 0.6463 11.00000 0.05 0.51 Q3 1 0.4587 0.9615 0.7445 11.00000 0.05 0.45 Q4 1 0.4165 0.8419 0.8386 11.00000 0.05 0.44 Q5 1 0.3282 0.8587 0.9481 11.00000 0.05 0.42 Q6 1 0.6383 1.0575 0.6095 11.00000 0.05 0.42 Q7 1 0.5481 0.8254 0.7806 11.00000 0.05 0.41 Q8 1 0.6837 0.8148 0.7363 11.00000 0.05 0.40 Q9 1 0.4993 1.0976 0.6614 11.00000 0.05 0.38 Q10 1 0.9090 0.3607 0.6920 11.00000 0.05 0.37 Q11 1 0.7578 0.4425 0.6644 11.00000 0.05 0.36 Q12 1 0.2638 0.8199 0.8598 11.00000 0.05 0.36 Q13 1 0.9470 0.6639 0.7364 11.00000 0.05 0.35 Q14 1 0.3882 0.5650 1.0304 11.00000 0.05 0.33 Q15 1 0.6360 0.7368 0.7753 11.00000 0.05 0.33 ; _shelx_res_checksum 3877 _shelx_hkl_file ; 0 0 -1 2130.79 62.13 0 0 -1 2040.95 61.84 0 0 -1 2277.89 62.03 0 0 1 2403.55 62.06 0 0 1 2352.27 62.07 0 0 -1 2236.17 62.04 0 0 -1 2173.94 62.06 0 0 -1 2215.91 62.06 0 0 -1 2346.18 61.94 0 0 -2 20.76 1.72 0 0 -2 27.57 1.94 0 0 2 31.04 1.41 0 0 -2 25.96 1.74 0 0 2 24.49 1.66 0 0 -2 26.19 1.73 0 0 -2 26.78 1.73 0 0 2 28.44 1.54 0 0 2 25.70 1.74 0 0 -2 25.55 1.62 0 0 2 27.17 1.34 0 0 -2 31.19 1.78 0 0 -2 27.85 1.65 0 0 2 25.81 1.35 0 0 3 892.60 25.83 0 0 -3 924.45 26.60 0 0 -3 898.14 26.14 0 0 3 901.16 26.17 0 0 3 883.07 25.78 0 0 3 884.10 26.58 0 0 3 934.06 25.89 0 0 -3 888.35 26.36 0 0 -3 934.24 26.78 0 0 -3 930.38 26.36 0 0 3 897.51 25.78 0 0 -3 874.13 25.79 0 0 -3 901.24 25.84 0 0 -3 962.84 26.63 0 0 -4 1338.81 39.40 0 0 4 1350.04 40.39 0 0 -4 1309.32 39.77 0 0 4 1386.74 39.88 0 0 4 1366.74 39.33 0 0 4 1372.13 39.41 0 0 -4 1347.55 40.61 0 0 4 1420.27 40.67 0 0 -4 1390.48 39.42 0 0 -4 1375.65 40.13 0 0 -4 1406.83 40.10 0 0 -4 1409.44 40.38 0 0 -4 1413.86 40.54 0 0 -4 1466.24 40.51 0 0 -4 1444.90 40.45 0 0 4 1443.33 41.02 0 0 4 1428.77 40.71 0 0 4 1388.49 39.32 0 0 -5 391.53 13.06 0 0 -5 366.62 13.21 0 0 5 371.47 13.00 0 0 5 374.36 12.44 0 0 5 374.81 11.92 0 0 -5 393.37 12.01 0 0 -5 374.61 12.79 0 0 -5 370.80 13.11 0 0 -5 353.44 12.27 0 0 -5 386.89 11.97 0 0 5 372.57 11.81 0 0 -5 398.40 13.13 0 0 5 363.26 11.80 0 0 -5 378.05 12.67 0 0 -5 395.12 13.41 0 0 6 325.53 10.91 0 0 6 343.45 11.66 0 0 -6 340.33 11.00 0 0 -6 328.52 12.50 0 0 -6 315.44 12.65 0 0 -6 329.56 11.79 0 0 -6 337.29 12.43 0 0 -6 337.48 12.21 0 0 6 312.23 10.76 0 0 -6 341.13 12.05 0 0 6 297.07 11.99 0 0 -6 330.94 10.98 0 0 -6 351.81 12.07 0 0 -6 349.25 12.79 0 0 -6 350.64 12.32 0 0 6 328.38 10.79 0 0 7 712.67 23.87 0 0 7 712.51 21.97 0 0 -7 723.79 22.00 0 0 -7 699.21 23.77 0 0 -7 745.60 24.10 0 0 7 758.47 24.31 0 0 -7 725.82 24.48 0 0 -7 700.16 23.24 0 0 -7 707.97 23.80 0 0 7 694.77 21.78 0 0 -7 718.20 23.17 0 0 -7 730.81 24.38 0 0 -7 726.77 22.04 0 0 7 721.23 21.78 0 0 7 695.94 23.77 0 0 -7 756.08 24.27 0 0 7 707.99 24.37 0 0 7 695.12 23.73 0 0 -7 736.59 24.16 0 0 7 771.41 24.89 0 0 -8 67.48 3.90 0 0 8 73.18 5.22 0 0 -8 68.35 5.08 0 0 8 74.62 5.47 0 0 -8 70.40 5.13 0 0 8 67.07 5.01 0 0 -8 73.74 3.91 0 0 8 59.41 5.07 0 0 8 77.50 5.33 0 0 -8 73.08 5.57 0 0 -8 70.62 5.37 0 0 8 71.24 3.76 0 0 -8 64.78 4.75 0 0 8 70.44 3.74 0 0 -8 79.56 5.54 0 0 -8 65.80 4.32 0 0 -8 78.15 5.62 0 0 -9 45.25 3.24 0 0 9 44.69 4.59 0 0 -9 48.10 4.58 0 0 -9 53.62 3.45 0 0 9 52.61 4.94 0 0 9 54.13 5.08 0 0 9 50.46 3.86 0 0 -9 36.73 4.25 0 0 9 45.54 4.40 0 0 -9 53.29 4.84 0 0 9 44.41 3.06 0 0 -9 45.88 3.71 0 0 -9 48.06 4.66 0 0 10 373.75 16.31 0 0 -10 378.12 16.33 0 0 -10 354.33 12.97 0 0 10 410.48 14.39 0 0 -10 377.18 14.11 0 0 -10 374.79 15.84 0 0 -10 355.60 14.43 0 0 10 395.78 16.00 0 0 -10 359.54 15.65 0 0 -10 378.71 16.02 0 0 10 384.04 15.68 0 0 10 391.55 16.68 0 0 -11 225.92 10.12 0 0 11 225.72 11.48 0 0 -11 238.23 12.25 0 0 11 248.75 12.90 0 0 11 243.40 10.30 0 0 -11 254.80 12.29 0 0 -11 251.43 12.61 0 0 11 198.72 11.27 0 0 11 227.07 12.33 0 0 -11 224.54 10.60 0 0 -12 72.28 6.95 0 0 -12 87.91 7.36 0 0 -12 70.80 6.59 0 0 12 66.07 6.93 0 0 -12 64.97 5.50 0 0 -12 63.30 5.08 0 0 12 70.54 6.33 0 0 12 79.66 6.74 0 0 12 70.18 6.96 0 0 13 39.91 5.80 0 0 -13 36.39 5.34 0 0 13 30.13 4.94 0 0 -13 44.50 4.58 0 0 13 45.02 6.15 0 0 13 51.45 5.79 0 0 -13 45.27 5.81 0 0 -13 42.40 6.03 0 0 -14 2.92 3.45 0 0 14 4.13 3.51 0 0 14 -1.65 3.14 0 0 -14 3.11 4.33 0 0 -14 -2.30 3.51 0 0 14 4.00 3.79 0 0 -14 2.34 3.25 0 0 15 50.35 7.16 0 0 -15 49.67 6.85 0 0 15 48.82 6.51 0 0 -15 41.76 6.43 0 -1 15 63.16 7.33 0 1 -15 67.79 7.90 0 -1 14 3.00 3.99 0 1 -14 5.47 4.15 0 -1 14 7.70 4.11 0 1 -14 5.55 3.99 0 -1 14 7.25 4.09 0 -1 13 3.24 3.17 0 -1 13 -1.40 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83.37 4.73 0 4 4 80.98 4.55 0 4 4 96.96 4.59 0 4 4 81.84 2.91 0 4 4 90.65 4.54 0 4 4 90.61 4.69 0 -4 -4 71.49 2.68 0 4 4 81.52 2.90 0 -4 -4 72.45 4.36 0 -4 -4 71.83 2.63 0 -4 -4 84.96 3.39 0 -4 -5 14.76 2.39 0 4 5 14.80 1.95 0 -4 -5 7.80 2.05 0 4 5 15.11 2.05 0 -4 -5 12.62 0.99 0 4 5 12.37 1.08 0 -4 -5 13.68 1.25 0 4 5 13.26 1.52 0 4 5 14.95 2.22 0 4 5 16.38 2.05 0 4 5 13.03 2.10 0 4 5 9.67 1.81 0 -4 -5 13.24 2.06 0 -4 -5 12.99 1.50 0 -4 -5 17.03 2.42 0 4 5 15.75 1.14 0 4 6 97.97 6.01 0 4 6 98.73 5.35 0 -4 -6 106.40 6.19 0 -4 -6 108.32 4.23 0 4 6 105.76 4.02 0 4 6 97.65 4.67 0 4 6 93.37 5.24 0 4 6 102.32 5.32 0 -4 -6 110.12 4.44 0 -4 -6 95.38 4.05 0 4 6 106.48 5.46 0 4 6 95.70 5.46 0 4 6 100.61 5.60 0 -4 -6 97.06 4.10 0 4 6 101.48 6.14 0 -4 -6 87.51 5.34 0 -4 -7 647.88 23.11 0 -4 -7 672.02 22.39 0 4 7 677.21 21.86 0 -4 -7 642.17 20.29 0 4 7 665.88 21.78 0 -4 -7 613.92 22.18 0 -4 -7 659.28 23.06 0 -4 -7 653.60 21.86 0 4 7 670.01 21.84 0 -4 -7 695.17 20.35 0 4 7 637.91 21.03 0 -4 -7 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-10 30.76 3.71 0 4 10 28.50 4.30 0 -4 -11 28.24 4.28 0 -4 -11 40.70 4.18 0 4 11 45.02 5.23 0 -4 -11 35.36 4.70 0 -4 -11 29.28 3.42 0 4 11 35.90 4.28 0 4 11 39.69 4.37 0 4 11 43.01 4.97 0 -4 -11 35.17 3.95 0 4 11 28.22 4.66 0 -4 -11 31.51 4.09 0 -4 -11 36.00 4.37 0 4 11 38.71 4.20 0 4 12 67.42 5.61 0 -4 -12 73.85 6.42 0 -4 -12 61.28 6.10 0 4 12 61.98 6.28 0 -4 -12 59.13 5.61 0 4 12 72.24 6.03 0 4 12 62.85 6.43 0 -4 -12 50.78 4.75 0 -4 -12 60.56 5.30 0 -4 -12 60.94 5.40 0 -4 -12 62.08 5.74 0 4 12 56.89 5.46 0 4 12 65.43 6.54 0 4 12 76.15 7.19 0 4 13 75.93 7.63 0 -4 -13 65.53 6.16 0 4 13 66.95 6.16 0 4 13 61.35 6.85 0 -4 -13 73.76 6.48 0 4 13 74.65 6.37 0 -4 -13 84.52 6.36 0 -4 -13 66.80 5.74 0 4 13 68.35 6.84 0 4 13 68.98 7.00 0 4 13 65.21 5.99 0 -4 -13 76.86 5.98 0 -4 -13 81.12 7.37 0 4 14 68.22 7.74 0 4 14 67.32 7.30 0 4 14 56.40 6.01 0 4 14 54.17 6.19 0 -4 -14 58.45 5.75 0 4 14 73.21 7.41 0 4 14 74.23 7.50 0 -4 -14 47.88 5.40 0 -4 -14 69.72 6.46 0 -4 -14 79.06 7.01 0 -4 -15 12.57 4.13 0 4 15 18.63 4.25 0 -4 -15 15.19 3.95 0 4 15 19.87 5.12 0 4 15 16.90 4.14 0 -4 -15 14.62 3.48 0 4 16 3.27 3.51 0 4 16 7.12 4.07 0 -4 -16 -0.75 3.59 0 4 16 1.67 3.96 0 5 -12 19.14 4.85 0 -5 12 22.23 5.07 0 5 -12 12.11 4.68 0 -5 12 24.51 5.79 0 -5 12 19.42 5.08 0 5 -11 7.28 4.19 0 5 -11 9.41 4.43 0 5 -11 13.56 4.25 0 -5 11 8.78 3.69 0 5 -11 9.07 3.92 0 -5 11 8.49 4.33 0 -5 11 7.40 4.02 0 -5 11 15.06 4.62 0 5 -10 5.25 3.11 0 -5 10 7.86 3.95 0 5 -10 2.24 3.24 0 -5 10 1.52 3.23 0 5 -10 2.76 3.31 0 5 -10 3.63 3.20 0 -5 10 1.41 3.49 0 -5 9 74.08 6.66 0 -5 9 61.21 6.70 0 5 -9 65.83 6.76 0 -5 9 61.80 6.27 0 5 -9 64.44 6.30 0 -5 9 55.10 6.29 0 5 -9 60.20 6.23 0 -5 8 506.32 20.56 0 -5 8 492.21 21.04 0 5 -8 533.35 20.81 0 5 -8 555.35 21.48 0 -5 8 519.63 20.91 0 -5 8 470.61 18.40 0 -5 8 502.33 21.27 0 -5 8 511.65 20.98 0 5 -8 543.50 20.39 0 -5 7 376.27 15.98 0 5 -7 349.13 15.09 0 -5 7 363.53 16.23 0 -5 7 378.63 16.23 0 -5 7 391.12 16.39 0 5 -7 374.92 15.69 0 -5 7 337.93 14.09 0 -5 7 348.30 16.22 0 5 -7 374.05 16.24 0 5 -6 128.09 8.32 0 -5 6 141.59 7.30 0 5 -6 143.88 6.59 0 -5 6 138.60 8.31 0 -5 6 138.52 8.45 0 -5 6 134.48 8.16 0 5 -6 149.36 8.55 0 5 -6 137.21 7.98 0 -5 6 130.00 8.51 0 5 -6 129.98 6.90 0 5 -6 142.21 7.64 0 -5 6 135.15 8.43 0 5 -6 146.61 8.02 0 5 -6 135.94 8.29 0 -5 5 10.16 2.41 0 5 -5 7.04 2.46 0 5 -5 11.56 2.85 0 -5 5 8.61 2.01 0 5 -5 7.28 2.28 0 5 -5 10.21 2.31 0 -5 5 7.38 2.37 0 -5 5 7.52 2.59 0 -5 5 12.77 2.79 0 5 -5 7.14 1.88 0 5 -5 12.38 2.53 0 -5 5 9.40 1.22 0 5 -5 12.88 2.74 0 5 -5 6.54 1.77 0 -5 5 7.52 1.22 0 -5 5 5.58 2.35 0 -5 4 199.19 9.60 0 5 -4 199.90 9.18 0 -5 4 183.29 9.49 0 5 -4 184.73 9.31 0 5 -4 189.41 9.21 0 5 -4 188.49 8.41 0 -5 4 193.05 7.05 0 -5 4 192.77 7.06 0 5 -4 197.35 7.97 0 -5 4 219.39 9.99 0 5 -4 201.54 8.05 0 -5 4 211.30 9.83 0 -5 4 199.79 9.66 0 5 -4 176.37 8.76 0 5 -4 198.85 9.40 0 5 -4 198.34 8.71 0 -5 4 189.65 9.40 0 5 -4 179.27 8.79 0 -5 3 258.41 9.18 0 -5 3 261.12 9.17 0 5 -3 255.17 10.68 0 5 -3 263.50 10.22 0 -5 3 270.16 11.21 0 5 -3 251.86 8.47 0 -5 3 288.63 11.51 0 -5 3 259.82 11.36 0 -5 3 272.37 11.47 0 5 -3 266.70 10.94 0 5 -3 275.09 10.70 0 -5 3 254.81 11.20 0 5 -3 255.13 10.88 0 -5 3 256.88 11.15 0 5 -3 283.70 10.05 0 5 -3 259.08 9.44 0 5 -2 440.97 14.86 0 -5 2 444.22 15.50 0 5 -2 433.71 12.17 0 5 -2 473.33 15.21 0 5 -2 432.85 14.52 0 5 -2 435.33 14.88 0 5 -2 461.62 13.36 0 -5 2 462.99 12.36 0 -5 2 450.02 15.54 0 5 -2 402.96 11.85 0 5 -2 475.95 15.25 0 -5 2 444.08 13.67 0 -5 2 457.11 13.78 0 5 -2 450.56 14.81 0 5 -2 469.99 14.96 0 -5 2 497.93 15.69 0 5 -2 443.36 14.12 0 -5 2 453.72 15.71 0 -5 2 454.95 15.72 0 5 -2 443.76 14.47 0 -5 2 469.95 12.37 0 5 -2 457.95 15.05 0 5 -1 241.84 9.82 0 5 -1 258.21 8.58 0 -5 1 254.02 10.36 0 -5 1 269.34 9.56 0 5 -1 284.65 10.62 0 5 -1 246.83 9.77 0 -5 1 266.24 9.49 0 -5 1 257.76 8.68 0 5 -1 254.18 9.73 0 -5 1 258.77 8.66 0 5 -1 268.77 10.06 0 5 -1 289.09 10.25 0 5 -1 282.77 10.50 0 5 -1 262.58 8.68 0 5 -1 268.37 10.33 0 5 -1 283.88 10.54 0 5 -1 266.28 9.54 0 5 0 53.24 3.58 0 -5 0 49.93 2.81 0 5 0 46.74 2.36 0 5 0 55.22 3.86 0 5 0 49.79 3.18 0 -5 0 54.22 2.92 0 5 0 47.31 3.09 0 5 0 54.36 3.40 0 5 0 45.86 2.94 0 5 0 45.87 2.10 0 5 0 57.91 3.84 0 -5 0 48.66 2.43 0 5 0 50.38 3.60 0 5 0 56.16 3.49 0 5 0 54.62 3.72 0 -5 0 50.61 2.83 0 5 1 238.49 7.62 0 5 1 235.79 8.41 0 5 1 214.72 9.51 0 -5 -1 249.96 8.17 0 5 1 246.41 8.59 0 -5 -1 231.06 8.08 0 5 1 244.92 9.34 0 5 1 252.39 9.43 0 -5 -1 237.85 8.53 0 -5 -1 243.88 7.67 0 5 1 240.02 9.46 0 -5 -1 234.67 7.03 0 -5 -1 237.65 8.55 0 5 1 232.77 7.91 0 5 1 243.00 7.61 0 5 1 237.76 8.84 0 5 1 232.43 9.30 0 5 1 239.35 9.48 0 5 1 239.46 9.09 0 5 1 255.50 8.94 0 5 1 199.86 6.82 0 5 2 362.88 11.48 0 5 2 462.12 13.65 0 -5 -2 432.95 12.11 0 5 2 430.97 14.30 0 -5 -2 421.32 13.04 0 -5 -2 449.38 13.39 0 -5 -2 464.66 12.87 0 5 2 429.19 11.94 0 5 2 437.76 14.77 0 5 2 374.46 11.47 0 5 2 446.92 13.97 0 5 2 456.23 14.46 0 5 2 364.26 11.49 0 5 2 436.06 14.12 0 -5 -3 2131.57 59.58 0 5 3 2162.90 59.02 0 -5 -3 2124.81 58.38 0 -5 -3 2170.21 57.73 0 -5 -3 1911.56 56.82 0 -5 -3 2015.86 58.48 0 5 3 2008.48 59.52 0 5 3 2019.64 59.79 0 -5 -4 308.34 11.36 0 5 4 305.60 11.18 0 5 4 298.85 11.11 0 5 4 289.21 11.30 0 5 4 278.40 11.43 0 -5 -4 310.27 9.47 0 -5 -4 284.95 10.63 0 -5 -4 303.54 11.52 0 5 4 290.01 8.99 0 5 4 306.53 11.57 0 -5 -4 276.70 10.72 0 5 4 275.88 11.27 0 5 4 295.92 9.05 0 5 5 565.35 18.71 0 5 5 557.14 18.22 0 5 5 572.72 17.82 0 -5 -5 549.59 17.90 0 5 5 574.66 17.70 0 -5 -5 587.88 17.68 0 5 5 578.12 19.27 0 5 5 536.16 15.09 0 -5 -5 570.16 18.25 0 5 5 563.30 18.23 0 -5 -5 589.46 18.22 0 -5 -5 596.09 18.26 0 5 5 556.36 17.89 0 5 5 570.18 15.98 0 -5 -5 591.52 18.75 0 5 5 524.49 15.10 0 5 5 548.97 18.58 0 -5 -5 590.80 18.29 0 5 5 584.82 18.09 0 -5 -5 560.15 18.02 0 -5 -6 142.17 5.93 0 -5 -6 152.82 7.32 0 5 6 141.43 7.23 0 5 6 143.15 7.09 0 5 6 130.66 7.47 0 -5 -6 145.33 7.18 0 -5 -6 153.13 7.39 0 5 6 132.49 7.04 0 5 6 144.00 6.85 0 5 6 141.82 4.86 0 -5 -6 147.20 7.71 0 5 6 141.39 5.81 0 5 6 146.69 7.93 0 5 6 146.68 7.96 0 -5 -6 144.70 7.94 0 -5 -6 149.36 5.15 0 -5 -6 153.00 7.32 0 -5 -7 718.65 22.03 0 -5 -7 777.06 25.93 0 5 7 760.44 26.16 0 -5 -7 713.73 24.73 0 5 7 744.35 25.04 0 -5 -7 782.33 22.61 0 -5 -7 771.70 25.23 0 5 7 764.98 23.37 0 -5 -7 666.46 24.44 0 -5 -7 763.62 25.14 0 5 7 770.51 25.22 0 5 7 763.66 24.53 0 5 7 793.08 26.56 0 5 7 797.49 25.00 0 -5 -8 383.39 13.83 0 5 8 376.57 13.49 0 -5 -8 364.61 12.42 0 -5 -8 383.40 12.49 0 -5 -8 378.13 12.85 0 5 8 407.46 15.17 0 -5 -8 420.09 16.27 0 5 8 365.18 15.82 0 5 8 394.08 14.52 0 -5 -8 370.64 14.78 0 5 8 397.80 15.42 0 -5 -8 358.97 14.51 0 5 8 398.84 14.75 0 5 8 394.50 16.12 0 -5 -9 91.04 6.10 0 -5 -9 81.12 4.43 0 5 9 89.76 5.81 0 -5 -9 84.58 6.02 0 -5 -9 95.70 5.68 0 -5 -9 99.08 7.11 0 5 9 106.95 7.40 0 5 9 90.02 6.84 0 5 9 105.91 6.84 0 5 9 92.02 5.69 0 -5 -10 210.68 9.84 0 5 10 229.38 11.72 0 5 10 213.57 10.23 0 -5 -10 211.13 10.41 0 -5 -10 199.74 10.19 0 5 10 232.43 11.06 0 -5 -10 208.60 11.33 0 5 10 220.58 11.60 0 5 10 202.81 9.68 0 5 11 22.84 4.28 0 5 11 26.95 4.14 0 5 11 29.26 3.85 0 5 11 23.45 4.35 0 5 11 22.00 3.36 0 -5 -11 22.36 3.88 0 5 11 36.95 5.21 0 -5 -11 23.88 3.54 0 -5 -11 22.43 3.41 0 -5 -11 25.64 3.63 0 -5 -11 25.48 2.93 0 5 12 6.43 3.00 0 -5 -12 7.94 2.77 0 5 12 0.67 3.06 0 -5 -12 8.29 2.99 0 5 12 3.99 3.15 0 5 12 11.51 3.58 0 5 12 6.84 2.49 0 -5 -12 5.35 2.85 0 5 12 9.34 3.67 0 -5 -12 6.93 2.89 0 5 13 14.97 4.23 0 5 13 19.53 4.00 0 5 13 23.09 4.14 0 5 13 17.30 4.61 0 -5 -13 19.49 4.02 0 -5 -13 18.00 3.87 0 -5 -13 18.83 3.71 0 -5 -13 23.51 3.93 0 5 13 16.40 4.43 0 5 13 16.32 3.55 0 5 14 65.95 6.39 0 5 14 72.64 6.62 0 -5 -14 58.91 6.02 0 -5 -14 69.48 6.58 0 5 14 63.09 6.10 0 5 14 74.52 7.62 0 5 14 45.36 6.85 0 -5 -14 53.63 6.11 0 5 14 77.54 7.73 0 -5 -14 65.36 6.15 0 5 15 70.60 7.02 0 -5 -15 85.15 7.30 0 5 15 91.69 8.81 0 -5 -15 84.74 7.53 0 5 15 91.20 8.72 0 -5 -15 91.47 7.47 0 -5 -16 24.14 5.21 0 5 16 33.17 6.06 0 5 16 31.03 5.19 0 -6 11 7.23 4.67 0 -6 11 5.53 3.92 0 6 -11 7.98 3.85 0 6 -10 -1.55 3.65 0 -6 10 3.28 4.06 0 -6 10 -2.25 4.17 0 6 -10 -1.46 3.62 0 -6 10 -2.18 3.71 0 -6 10 -0.85 3.67 0 6 -10 -1.35 3.43 0 -6 9 85.08 8.23 0 -6 9 98.30 8.36 0 -6 9 95.01 8.51 0 6 -9 111.65 8.72 0 -6 9 95.43 8.19 0 -6 9 81.26 7.57 0 6 -9 99.93 8.55 0 6 -9 88.23 7.41 0 6 -9 86.59 7.90 0 -6 8 179.65 10.79 0 -6 8 181.16 10.95 0 -6 8 180.45 11.18 0 -6 8 180.40 11.61 0 6 -8 192.64 11.37 0 6 -8 175.90 10.14 0 6 -8 172.45 10.67 0 -6 8 182.21 11.36 0 -6 7 115.32 8.59 0 -6 7 126.03 8.45 0 -6 7 120.56 8.60 0 6 -7 131.09 8.00 0 6 -7 122.63 8.26 0 -6 7 131.56 8.86 0 -6 7 108.57 8.57 0 6 -7 136.93 8.88 0 -6 7 121.42 7.17 0 6 -6 332.39 14.38 0 6 -6 293.91 12.89 0 -6 6 284.74 14.02 0 -6 6 296.13 13.97 0 -6 6 312.13 12.61 0 -6 6 289.04 13.69 0 6 -6 267.26 11.62 0 6 -6 309.24 13.56 0 -6 6 298.21 14.11 0 -6 6 308.74 14.60 0 6 -6 289.78 13.95 0 -6 5 10.62 2.89 0 -6 5 9.42 1.36 0 6 -5 8.87 2.40 0 6 -5 6.16 2.37 0 6 -5 13.52 3.02 0 6 -5 9.09 2.69 0 -6 5 8.75 1.38 0 -6 5 15.59 2.73 0 -6 5 7.62 2.74 0 6 -5 10.43 2.13 0 6 -5 8.55 2.20 0 6 -5 3.41 2.35 0 6 -5 8.40 1.38 0 -6 5 11.66 2.96 0 -6 5 5.96 2.61 0 -6 4 290.91 11.70 0 -6 4 279.79 9.78 0 6 -4 307.71 11.11 0 -6 4 264.16 12.81 0 -6 4 273.95 9.75 0 6 -4 280.23 12.56 0 -6 4 310.34 13.15 0 6 -4 266.85 8.91 0 6 -4 291.37 12.44 0 6 -4 276.88 12.01 0 -6 4 291.11 13.11 0 6 -4 264.74 10.39 0 6 -4 277.54 12.35 0 6 -4 283.56 11.26 0 6 -4 271.86 11.31 0 -6 4 300.39 13.02 0 -6 4 297.58 12.81 0 -6 3 88.30 6.24 0 6 -3 104.52 6.28 0 6 -3 99.63 5.48 0 6 -3 95.33 6.31 0 6 -3 114.39 6.44 0 6 -3 98.24 6.06 0 -6 3 99.51 6.65 0 6 -3 104.47 5.55 0 -6 3 100.32 6.79 0 6 -3 100.38 3.43 0 -6 3 99.07 5.88 0 -6 3 116.87 6.87 0 6 -3 99.68 5.82 0 6 -3 96.48 4.78 0 -6 3 95.68 6.53 0 6 -3 104.18 6.08 0 -6 2 272.79 12.06 0 6 -2 287.57 9.55 0 6 -2 245.73 8.06 0 6 -2 311.51 11.68 0 6 -2 232.94 8.06 0 -6 2 301.26 8.70 0 6 -2 280.63 10.21 0 6 -2 278.62 11.20 0 -6 2 285.63 11.76 0 6 -2 290.30 11.88 0 6 -2 292.35 11.23 0 6 -2 300.82 11.62 0 -6 2 282.01 11.22 0 -6 2 288.90 12.01 0 6 -2 287.05 11.03 0 6 -2 287.84 9.50 0 -6 2 313.79 8.75 0 -6 2 281.27 12.10 0 6 -1 300.93 11.75 0 6 -1 346.80 12.84 0 -6 1 327.68 10.62 0 -6 1 310.49 13.08 0 -6 1 340.62 12.65 0 -6 1 326.34 13.17 0 6 -1 335.93 12.28 0 6 -1 319.12 10.98 0 -6 1 320.05 12.67 0 6 -1 333.54 12.63 0 6 -1 312.06 11.68 0 6 -1 319.42 10.34 0 6 -1 334.64 12.76 0 6 -1 326.60 10.92 0 -6 1 313.43 10.54 0 6 -1 326.58 11.62 0 -6 1 316.67 13.05 0 6 -1 323.45 12.91 0 6 -1 295.92 11.78 0 -6 1 309.99 12.98 0 6 -1 329.33 10.29 0 6 -1 319.51 10.23 0 -6 0 24.37 1.76 0 6 0 22.02 1.97 0 6 0 25.08 3.17 0 -6 0 23.35 2.07 0 6 0 19.87 1.23 0 6 0 30.21 3.37 0 6 0 23.55 2.47 0 6 0 19.90 2.70 0 6 0 23.66 2.80 0 6 0 21.26 2.56 0 6 0 21.09 1.69 0 6 0 21.53 2.25 0 6 0 26.55 2.64 0 -6 0 20.43 2.71 0 6 0 21.66 2.34 0 6 0 22.06 2.76 0 -6 0 23.29 2.04 0 6 0 23.91 2.90 0 6 0 22.94 2.84 0 6 0 26.93 1.73 0 -6 0 16.04 2.48 0 -6 0 27.70 3.07 0 -6 0 27.97 2.21 0 -6 0 20.95 2.59 0 6 1 110.08 5.01 0 6 1 118.57 5.85 0 6 1 130.89 6.68 0 6 1 123.14 5.97 0 6 1 132.37 6.73 0 6 1 133.84 6.55 0 6 1 132.28 4.87 0 6 1 118.31 5.59 0 6 1 128.57 6.63 0 6 1 125.80 6.99 0 6 1 129.13 6.23 0 6 1 128.90 6.47 0 6 1 126.91 5.50 0 6 1 109.48 4.15 0 -6 -1 126.45 5.20 0 -6 -1 127.31 5.23 0 -6 -1 124.08 4.73 0 -6 -1 123.37 6.47 0 6 1 118.66 6.61 0 -6 -1 133.49 6.89 0 6 1 128.45 6.51 0 -6 -1 115.60 6.60 0 6 1 131.24 4.89 0 6 2 138.06 6.20 0 6 2 137.49 4.59 0 -6 -2 140.32 5.70 0 6 2 138.69 7.36 0 6 2 135.25 4.56 0 -6 -2 146.06 6.77 0 6 2 136.01 4.53 0 -6 -2 129.91 4.52 0 6 2 146.14 5.04 0 -6 -2 145.35 6.72 0 6 2 159.62 7.26 0 6 2 141.05 7.18 0 6 2 148.07 6.72 0 -6 -2 135.50 4.87 0 -6 -2 137.23 5.47 0 -6 -2 131.53 6.85 0 6 2 140.02 7.06 0 6 2 138.11 6.73 0 6 2 159.83 7.23 0 6 2 151.49 7.34 0 6 2 140.78 6.96 0 6 3 714.86 24.23 0 -6 -3 726.99 24.12 0 -6 -3 769.95 24.02 0 6 3 724.97 24.83 0 6 3 745.49 23.62 0 -6 -3 760.65 24.20 0 6 3 754.28 24.06 0 6 3 758.84 24.52 0 -6 -3 738.37 23.00 0 -6 -3 757.83 22.91 0 -6 -3 766.54 24.65 0 -6 -4 293.45 11.84 0 -6 -4 298.27 10.24 0 -6 -4 308.28 11.78 0 -6 -4 287.44 11.29 0 -6 -4 306.95 11.81 0 6 4 316.44 12.55 0 -6 -4 313.42 11.97 0 6 4 309.44 12.20 0 -6 -4 304.17 11.66 0 6 4 309.13 9.48 0 6 4 333.05 11.68 0 6 4 281.82 12.09 0 -6 -4 292.41 9.29 0 6 4 310.18 13.11 0 -6 -4 294.84 10.94 0 6 4 288.79 11.87 0 6 4 296.94 13.08 0 6 5 462.10 16.85 0 -6 -5 496.39 14.13 0 6 5 467.25 13.46 0 6 5 474.45 16.63 0 6 5 400.82 12.95 0 -6 -5 478.67 15.87 0 -6 -5 489.13 15.80 0 -6 -5 465.61 16.35 0 6 5 485.75 16.33 0 -6 -5 504.03 16.98 0 6 5 453.18 16.76 0 -6 -5 471.79 16.48 0 -6 -5 514.89 16.72 0 -6 -5 471.97 16.38 0 6 5 469.40 17.74 0 -6 -5 472.85 16.46 0 6 5 481.38 17.10 0 6 5 401.55 12.95 0 6 5 490.64 18.05 0 6 5 463.01 16.68 0 -6 -5 463.23 16.09 0 6 6 7.50 2.60 0 -6 -6 10.08 2.27 0 6 6 10.09 2.39 0 -6 -6 14.45 2.47 0 -6 -6 7.66 2.11 0 6 6 11.19 2.40 0 6 6 10.07 1.44 0 -6 -6 9.96 2.12 0 6 6 12.36 2.81 0 6 6 12.31 2.58 0 -6 -6 10.55 2.65 0 -6 -6 9.09 2.03 0 -6 -6 7.96 2.37 0 -6 -6 11.68 2.38 0 6 6 12.80 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113.30 8.43 0 -7 7 118.13 8.52 0 7 -7 102.28 7.33 0 7 -7 100.00 7.79 0 7 -7 130.42 8.88 0 7 -7 109.11 8.54 0 -7 7 102.51 8.54 0 -7 7 90.70 8.01 0 -7 6 137.07 9.07 0 7 -6 154.09 8.34 0 -7 6 131.24 9.26 0 7 -6 130.85 8.60 0 -7 6 139.23 9.59 0 -7 6 146.31 9.50 0 7 -6 132.01 9.00 0 7 -6 148.97 9.43 0 -7 6 134.71 7.82 0 -7 5 54.99 4.65 0 7 -5 65.30 5.50 0 -7 5 35.98 4.97 0 -7 5 52.24 5.47 0 -7 5 60.53 5.90 0 7 -5 50.26 5.29 0 7 -5 50.93 4.60 0 7 -5 60.77 5.60 0 -7 5 47.63 5.42 0 -7 4 -1.10 2.57 0 7 -4 -1.42 2.38 0 7 -4 0.48 1.64 0 -7 4 1.55 2.33 0 -7 4 2.27 2.41 0 -7 4 -0.40 1.74 0 7 -4 -0.33 1.81 0 7 -4 -0.70 1.73 0 7 -4 1.71 2.05 0 -7 4 1.57 2.13 0 7 -4 -0.50 2.11 0 -7 3 154.06 8.18 0 -7 3 172.35 9.31 0 7 -3 172.75 8.83 0 -7 3 171.24 9.24 0 -7 3 157.36 9.37 0 -7 3 153.00 9.12 0 7 -3 169.78 7.67 0 7 -3 178.19 9.39 0 7 -3 154.51 6.63 0 7 -3 157.66 8.20 0 7 -3 160.91 7.54 0 7 -3 161.29 6.79 0 7 -2 286.72 9.91 0 -7 2 265.68 12.22 0 -7 2 298.64 8.43 0 -7 2 325.98 12.58 0 -7 2 243.87 12.04 0 -7 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8 5.38 2.89 0 -7 -8 9.04 2.75 0 -7 -8 7.47 2.65 0 7 8 4.63 1.51 0 -7 -8 4.22 2.18 0 -7 -9 93.15 6.72 0 -7 -9 97.85 6.74 0 7 9 95.92 7.42 0 7 9 91.55 7.63 0 7 9 114.60 8.12 0 7 9 93.89 6.64 0 7 10 273.18 14.14 0 7 10 270.78 11.71 0 7 10 270.55 14.07 0 -7 -10 263.22 12.81 0 -7 -10 256.89 10.88 0 7 10 294.40 13.80 0 -7 -10 277.38 12.79 0 7 10 286.80 14.42 0 7 10 265.93 12.01 0 -7 -11 44.15 5.13 0 7 11 34.12 3.94 0 -7 -11 36.87 4.80 0 7 11 32.01 4.67 0 -7 -11 39.58 4.70 0 7 11 46.90 6.03 0 -7 -11 30.99 3.74 0 7 11 41.90 4.56 0 7 11 34.77 5.04 0 7 11 33.57 5.21 0 7 12 25.84 5.09 0 -7 -12 14.10 3.31 0 7 12 18.14 3.38 0 7 12 17.28 3.60 0 -7 -12 24.54 4.33 0 7 12 17.11 4.50 0 -7 -12 22.92 4.11 0 7 12 21.15 5.08 0 7 12 22.04 4.47 0 -7 -13 10.23 3.32 0 -7 -13 3.18 3.59 0 7 13 11.60 3.30 0 7 13 11.05 4.30 0 7 13 8.12 3.60 0 -7 -13 11.06 3.62 0 7 13 8.06 3.00 0 7 13 4.69 3.64 0 7 14 53.62 5.82 0 7 14 51.62 6.51 0 7 14 73.83 7.84 0 7 14 51.10 7.07 0 -7 -14 51.99 6.08 0 -7 -14 60.88 6.56 0 -7 -14 57.35 6.64 0 7 14 56.65 5.62 0 -7 -15 30.37 5.19 0 7 15 21.29 4.87 0 7 15 24.38 5.72 0 8 -10 30.50 5.28 0 8 -9 2.47 3.70 0 8 -9 0.63 3.13 0 8 -9 0.75 3.78 0 -8 9 2.73 4.17 0 8 -8 59.93 6.05 0 8 -8 68.05 7.24 0 -8 8 50.58 6.58 0 8 -8 68.03 7.52 0 8 -8 47.38 6.39 0 -8 8 58.51 7.59 0 -8 8 66.28 7.78 0 8 -7 46.47 6.16 0 8 -7 35.71 5.53 0 -8 7 51.18 6.44 0 8 -7 48.40 6.11 0 8 -7 49.95 6.13 0 -8 7 44.25 6.35 0 8 -7 45.45 5.21 0 -8 7 42.33 5.85 0 8 -6 40.44 5.17 0 -8 6 55.64 6.30 0 -8 6 42.64 5.63 0 8 -6 45.89 5.84 0 8 -6 47.50 5.80 0 8 -6 34.63 5.26 0 -8 6 37.41 5.72 0 8 -6 31.25 4.25 0 -8 5 97.36 7.97 0 8 -5 114.05 7.91 0 -8 5 103.58 8.47 0 8 -5 118.79 8.27 0 8 -5 105.67 7.44 0 8 -5 112.32 6.86 0 -8 5 106.72 6.99 0 -8 5 109.75 8.19 0 8 -4 5.59 2.93 0 -8 4 9.61 2.94 0 -8 4 5.81 2.96 0 8 -4 5.63 2.65 0 -8 4 9.75 2.72 0 -8 4 3.74 2.60 0 8 -4 7.57 2.44 0 -8 4 4.73 2.94 0 8 -4 5.69 2.75 0 -8 3 3.02 1.50 0 -8 3 -0.60 2.65 0 -8 3 2.83 2.45 0 8 -3 0.52 2.47 0 -8 3 1.50 1.33 0 8 -3 -0.84 2.26 0 8 -3 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231.44 11.78 0 8 1 112.60 7.19 0 -8 -1 107.24 6.46 0 8 1 92.31 3.37 0 -8 -1 99.86 6.53 0 8 1 112.68 5.73 0 -8 -1 108.43 6.21 0 8 1 109.11 4.75 0 8 1 108.29 5.18 0 -8 -1 103.28 6.12 0 8 1 114.34 6.36 0 8 1 115.01 7.70 0 8 1 104.68 5.35 0 8 1 113.23 6.16 0 -8 -1 108.39 7.12 0 8 1 109.66 6.94 0 8 1 115.81 4.82 0 -8 -1 107.65 5.61 0 -8 -1 100.33 5.48 0 8 2 107.36 4.13 0 8 2 106.55 6.96 0 -8 -2 110.17 6.87 0 -8 -2 108.53 5.95 0 -8 -2 118.37 5.24 0 -8 -2 114.93 4.84 0 8 2 116.20 5.29 0 8 2 98.39 7.19 0 -8 -2 114.01 6.53 0 -8 -2 131.22 6.86 0 -8 -2 103.40 5.88 0 8 2 105.08 4.05 0 8 2 104.06 6.37 0 8 2 118.44 4.81 0 8 2 110.04 4.09 0 8 3 150.35 8.97 0 -8 -3 170.59 7.52 0 -8 -3 168.14 8.37 0 8 3 162.24 6.33 0 -8 -3 155.02 7.87 0 -8 -3 179.06 8.58 0 -8 -3 164.93 6.77 0 -8 -3 168.31 8.84 0 8 3 157.92 8.21 0 -8 -3 147.43 7.78 0 8 4 301.95 13.83 0 -8 -4 314.89 10.39 0 8 4 324.95 10.12 0 -8 -4 316.18 12.84 0 8 4 321.80 13.34 0 -8 -4 323.21 13.27 0 -8 -4 314.12 12.28 0 -8 -4 292.27 9.86 0 -8 -4 319.65 13.14 0 -8 -4 310.56 12.79 0 -8 -4 326.28 11.47 0 -8 -5 1039.99 32.24 0 8 5 1012.64 32.54 0 -8 -5 1041.59 31.61 0 -8 -5 1025.32 32.32 0 8 5 914.78 27.66 0 -8 -5 1096.58 30.88 0 8 5 983.79 32.95 0 -8 -5 1030.71 29.42 0 -8 -5 1017.34 30.39 0 -8 -5 1057.05 32.28 0 -8 -5 1021.83 32.40 0 8 5 928.87 27.67 0 8 6 89.96 7.36 0 -8 -6 92.50 6.12 0 -8 -6 81.29 5.31 0 8 6 79.98 6.20 0 8 6 78.83 6.17 0 -8 -6 89.78 5.37 0 -8 -6 83.06 6.13 0 -8 -6 78.12 5.93 0 -8 -6 79.31 5.97 0 8 6 81.25 7.01 0 -8 -6 92.55 6.04 0 8 6 92.14 5.89 0 -8 -7 2.43 1.23 0 -8 -7 2.57 2.15 0 8 7 2.08 2.46 0 -8 -7 0.38 1.98 0 8 7 -4.43 2.79 0 -8 -7 3.70 1.80 0 8 7 4.40 2.39 0 -8 -7 0.85 1.63 0 -8 -7 0.35 1.80 0 -8 -7 3.20 2.13 0 -8 -7 4.65 2.41 0 8 7 3.29 2.26 0 -8 -7 0.46 1.98 0 8 8 -0.96 2.31 0 -8 -8 4.39 2.49 0 -8 -8 2.81 2.38 0 8 8 2.62 2.94 0 8 8 1.14 2.36 0 -8 -8 2.34 1.95 0 -8 -8 1.98 2.34 0 8 8 1.97 2.73 0 -8 -8 -0.43 2.27 0 -8 -9 100.47 7.38 0 8 9 103.40 7.28 0 -8 -9 115.50 6.81 0 -8 -9 104.94 5.80 0 -8 -9 118.36 7.81 0 8 9 130.55 9.10 0 -8 -9 113.88 7.64 0 8 9 115.94 8.30 0 8 9 105.53 8.42 0 -8 -10 101.90 5.99 0 -8 -10 106.59 7.60 0 8 10 102.34 7.94 0 8 10 103.91 8.41 0 -8 -10 98.11 7.37 0 8 10 115.44 8.63 0 8 10 90.27 8.06 0 8 11 107.84 8.55 0 8 11 128.84 9.76 0 -8 -11 128.33 8.54 0 8 11 111.48 8.96 0 8 11 108.05 7.00 0 8 11 115.63 7.55 0 8 12 76.22 7.83 0 8 12 75.73 7.97 0 8 12 68.92 5.70 0 -8 -12 65.39 6.44 0 8 12 72.71 6.02 0 8 12 82.72 8.10 0 -8 -12 70.78 6.59 0 -8 -12 58.49 6.24 0 8 12 74.53 7.28 0 8 13 2.20 3.57 0 8 13 6.68 4.02 0 8 13 9.09 4.15 0 8 13 4.21 2.64 0 -8 -13 4.61 3.36 0 8 13 4.75 2.81 0 8 13 9.18 4.14 0 -8 -13 6.44 3.20 0 8 14 10.36 4.79 0 -8 -14 17.44 4.38 0 -8 -14 29.00 5.35 0 -8 -14 23.31 4.80 0 8 14 27.91 5.77 0 8 14 23.01 5.35 0 8 14 21.11 5.08 0 8 14 20.49 4.48 0 -8 -15 91.17 8.45 0 8 15 126.28 9.85 0 8 15 109.28 10.23 0 -8 -15 107.79 9.38 0 -9 8 10.45 4.32 0 -9 8 2.77 4.44 0 9 -8 6.35 3.22 0 9 -8 6.41 4.03 0 9 -7 12.68 3.70 0 9 -7 12.26 4.53 0 -9 7 13.93 4.23 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17.04 1.75 1 -6 1 16.99 2.95 1 -6 1 18.08 2.81 -1 6 -1 17.66 2.38 1 -6 1 16.65 2.58 -1 6 -1 14.34 2.37 -1 6 -1 19.64 1.72 1 -6 1 18.90 2.34 1 -6 1 17.43 1.84 1 -6 1 13.20 2.12 -1 6 -1 17.07 1.91 1 -6 2 140.16 7.66 1 -6 2 149.63 8.47 -1 6 -2 159.26 7.62 1 -6 2 147.15 5.46 -1 6 -2 142.83 4.94 1 -6 2 145.36 8.26 -1 6 -2 145.29 5.26 1 -6 2 154.36 8.06 -1 6 -2 144.87 7.57 -1 6 -2 144.17 6.29 -1 6 -2 140.68 6.21 -1 6 -2 134.74 4.90 1 -6 2 141.18 8.11 -1 6 -2 164.83 8.03 1 -6 2 153.41 5.52 -1 6 -2 146.76 7.44 -1 6 -3 96.05 6.08 -1 6 -3 91.33 5.16 1 -6 3 93.96 6.79 1 -6 3 114.28 6.55 1 -6 3 102.25 5.26 -1 6 -3 90.08 6.06 1 -6 3 100.27 6.83 1 -6 3 92.33 3.24 1 -6 3 103.72 6.86 1 -6 3 85.99 6.41 -1 6 -3 94.81 4.94 1 -6 3 87.32 3.20 1 -6 3 99.18 6.55 1 -6 4 190.36 10.14 -1 6 -4 208.72 9.06 1 -6 4 191.61 10.61 -1 6 -4 205.55 10.06 1 -6 4 201.37 9.75 1 -6 4 189.97 10.31 1 -6 4 207.95 10.82 -1 6 -4 185.23 9.88 1 -6 4 185.70 10.40 -1 6 -4 206.52 8.61 -1 6 -5 147.73 8.75 1 -6 5 147.54 8.93 -1 6 -5 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206.99 11.55 1 -4 -12 183.72 9.24 1 -4 -12 197.45 10.31 1 -4 -12 175.30 10.09 1 -4 -11 126.77 7.44 -1 4 11 127.09 8.46 1 -4 -11 117.81 7.46 1 -4 -11 109.14 7.16 -1 4 11 119.78 7.80 -1 4 11 121.16 7.69 1 -4 -11 132.05 6.97 -1 4 11 132.20 7.81 -1 4 11 125.68 9.13 1 -4 -11 128.53 7.96 1 -4 -11 117.75 6.75 -1 4 11 150.77 9.30 -1 4 10 39.34 4.72 -1 4 10 50.45 5.50 -1 4 10 34.60 4.49 -1 4 10 37.25 4.18 1 -4 -10 40.24 4.05 -1 4 10 33.84 3.99 1 -4 -10 34.38 3.82 -1 4 10 42.05 4.20 1 -4 -10 46.83 3.75 1 -4 -10 33.62 3.26 1 -4 -10 35.11 3.94 -1 4 9 0.34 1.91 -1 4 9 1.90 1.89 -1 4 9 0.74 2.01 1 -4 -9 1.73 1.73 1 -4 -9 -0.70 1.75 -1 4 9 0.49 2.02 -1 4 9 0.79 1.74 1 -4 -9 1.55 1.46 -1 4 9 -0.54 2.17 1 -4 -9 1.60 1.65 1 -4 -9 2.24 1.90 -1 4 9 -0.41 1.74 1 -4 -9 0.68 1.71 -1 4 9 2.42 2.25 1 -4 -9 0.37 1.75 -1 4 8 52.64 4.68 -1 4 8 48.31 4.23 1 -4 -8 45.65 3.47 1 -4 -8 50.61 4.11 1 -4 -8 42.98 3.78 -1 4 8 55.02 4.21 1 -4 -8 45.44 3.37 -1 4 8 36.99 3.48 -1 4 8 52.28 4.20 1 -4 -8 50.36 4.91 -1 4 8 54.89 4.83 -1 4 8 49.59 4.20 1 -4 -8 45.22 3.84 1 -4 -8 45.99 3.68 1 -4 -8 45.12 4.00 -1 4 8 48.56 4.79 1 -4 -8 52.00 3.63 -1 4 8 51.89 3.27 1 -4 -7 598.57 18.19 1 -4 -7 577.37 18.49 1 -4 -7 578.93 19.67 -1 4 7 577.41 18.20 -1 4 7 575.29 21.00 -1 4 7 576.99 18.26 1 -4 -7 624.59 18.32 -1 4 7 571.40 18.85 1 -4 -7 567.32 18.51 1 -4 -7 560.74 19.62 -1 4 7 568.62 20.45 -1 4 7 578.34 21.37 -1 4 7 590.07 20.01 -1 4 7 582.96 19.71 -1 4 7 559.78 19.80 1 -4 -7 597.45 18.60 1 -4 -7 569.59 20.96 -1 4 7 579.93 20.91 -1 4 7 581.67 19.70 1 -4 -7 601.67 21.29 -1 4 6 1924.20 55.94 1 -4 -6 1802.36 55.57 1 -4 -6 1905.95 55.97 -1 4 6 1693.92 55.72 -1 4 6 1953.80 54.76 -1 4 6 1827.43 52.88 1 -4 -6 1755.76 54.36 1 -4 -6 1785.11 52.60 1 -4 -6 1888.78 55.35 -1 4 6 1879.00 54.60 1 -4 -6 1746.28 54.40 -1 4 6 1827.53 53.28 -1 4 6 1856.58 55.20 1 -4 -6 1864.85 52.94 1 -4 -6 1844.32 52.91 -1 4 6 1888.38 55.97 1 -4 -6 1840.29 55.87 -1 4 6 1794.16 52.87 -1 4 6 1952.03 54.70 1 -4 -6 1870.86 53.48 1 -4 -6 1961.52 52.58 -1 4 6 1806.36 54.59 -1 4 6 1868.55 55.31 -1 4 6 1938.66 54.94 1 -4 -5 796.78 26.27 1 -4 -5 848.29 23.63 1 -4 -5 792.99 24.31 1 -4 -5 831.63 23.97 1 -4 -5 869.52 26.95 -1 4 5 834.32 25.83 -1 4 5 767.51 24.25 -1 4 5 839.65 26.07 -1 4 5 863.57 25.97 -1 4 5 795.10 24.23 -1 4 5 800.64 25.76 -1 4 5 830.29 24.29 -1 4 5 810.67 25.73 1 -4 -5 816.83 23.90 -1 4 4 1.02 0.75 1 -4 -4 0.44 0.42 1 -4 -4 0.07 0.52 -1 4 4 -0.23 1.21 1 -4 -4 0.14 0.50 1 -4 -4 -0.29 1.44 -1 4 4 -0.52 1.32 -1 4 4 0.25 1.28 1 -4 -4 0.45 0.65 -1 4 4 0.22 1.19 1 -4 -4 1.37 1.49 -1 4 3 60.28 3.77 1 -4 -3 55.61 3.82 -1 4 3 60.50 3.90 1 -4 -3 53.01 3.61 -1 4 3 49.21 1.93 1 -4 -3 52.38 1.94 1 -4 -3 53.05 1.87 1 -4 -3 63.15 3.71 1 -4 -3 51.94 2.04 -1 4 3 63.99 3.66 -1 4 3 55.13 3.73 1 -4 -2 700.72 22.18 -1 4 2 695.32 22.00 -1 4 2 721.23 22.01 -1 4 2 727.24 22.17 -1 4 2 692.07 19.79 -1 4 2 690.92 19.80 1 -4 -2 660.71 19.89 -1 4 2 742.94 22.31 1 -4 -2 698.70 21.55 1 -4 -2 714.58 22.05 -1 4 2 676.50 19.52 1 -4 -1 655.76 20.19 -1 4 1 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29.02 4.05 -2 8 -1 34.58 4.24 2 -8 1 40.28 5.00 2 -8 1 38.37 2.98 2 -8 1 31.72 3.76 2 -8 1 31.08 3.78 -2 8 -1 35.75 5.12 -2 8 -1 36.28 3.48 2 -8 1 36.75 4.49 2 -8 1 27.56 4.33 2 -8 2 139.80 9.50 2 -8 2 142.18 7.78 2 -8 2 145.09 8.96 2 -8 2 135.41 9.45 -2 8 -2 138.04 5.68 2 -8 2 141.92 7.86 2 -8 2 140.30 9.50 2 -8 2 158.22 9.18 -2 8 -2 163.38 8.59 -2 8 -2 158.21 9.17 2 -8 3 241.65 10.60 2 -8 3 227.68 12.18 2 -8 3 226.23 10.35 -2 8 -3 229.55 9.53 -2 8 -3 216.34 11.23 2 -8 3 218.65 12.63 -2 8 -3 243.18 12.20 -2 8 -3 233.51 8.99 2 -8 3 240.28 13.18 2 -8 3 227.71 12.81 2 -8 3 234.41 12.02 2 -8 4 69.09 7.23 -2 8 -4 72.72 6.84 2 -8 4 79.49 5.48 2 -8 4 73.33 7.35 -2 8 -4 77.14 5.28 2 -8 4 80.71 7.39 2 -8 4 87.10 6.97 2 -8 4 75.43 7.17 2 -8 4 85.36 7.24 -2 8 -4 93.24 8.74 -2 8 -4 94.52 7.07 -2 8 -5 78.35 8.31 -2 8 -5 77.22 6.83 2 -8 5 56.53 6.65 2 -8 5 54.81 6.55 -2 8 -5 67.34 5.26 2 -8 5 70.79 6.90 2 -8 5 64.72 6.37 2 -8 5 50.67 6.62 -2 8 -5 63.34 6.72 -2 8 -6 56.35 5.20 2 -8 6 49.36 6.78 -2 8 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2 -7 488.19 15.68 -2 -2 7 576.24 19.98 2 2 -7 586.87 19.62 -2 -2 7 541.57 19.57 2 2 -7 564.41 19.70 -2 -2 7 531.59 16.97 2 2 -6 439.54 14.55 2 2 -6 517.74 17.12 -2 -2 6 500.55 18.02 -2 -2 6 515.32 17.92 2 2 -6 498.15 17.52 2 2 -6 523.07 17.12 -2 -2 6 512.27 15.90 -2 -2 6 484.78 17.71 2 2 -6 535.57 18.22 2 2 -6 536.49 15.19 2 2 -6 488.49 17.71 -2 -2 6 499.01 17.47 2 2 -6 521.79 18.09 -2 -2 6 524.01 18.34 -2 -2 6 464.42 17.44 2 2 -6 528.42 18.07 -2 -2 6 493.47 15.89 2 2 -6 516.14 15.13 -2 -2 5 17.18 2.36 2 2 -5 23.47 2.59 2 2 -5 23.90 2.90 2 2 -5 22.24 2.30 -2 -2 5 19.22 2.45 2 2 -5 20.14 2.59 2 2 -5 22.33 1.55 -2 -2 5 18.33 2.32 2 2 -5 18.82 2.65 -2 -2 5 18.65 1.76 2 2 -5 18.52 2.57 2 2 -5 23.60 2.36 2 2 -5 18.35 2.26 2 2 -5 19.44 2.34 -2 -2 5 20.69 2.51 -2 -2 5 19.33 1.81 2 2 -5 22.51 2.58 2 2 -5 15.92 0.92 2 2 -5 16.74 2.33 2 2 -4 -0.49 1.38 -2 -2 4 0.13 0.82 2 2 -4 0.27 1.35 -2 -2 4 -0.58 1.05 2 2 -4 0.71 1.29 2 2 -4 -0.25 1.30 -2 -2 4 -0.26 0.84 2 2 -4 -0.60 1.17 2 2 -4 0.57 0.70 2 2 -4 0.33 0.93 -2 -2 3 1977.18 55.34 2 2 -3 1951.02 55.44 2 2 -3 2053.90 56.86 -2 -2 3 1859.97 55.90 -2 -2 3 1937.27 55.63 2 2 -3 1941.30 56.55 -2 -2 3 1976.08 55.38 2 2 -3 1929.56 55.73 -2 -2 3 1937.88 55.33 2 2 -3 1975.28 56.54 2 2 -3 1982.70 55.33 2 2 -3 2034.75 55.44 -2 -2 3 1875.63 55.99 2 2 -3 1928.83 56.39 -2 -2 3 1929.45 56.05 -2 -2 2 1227.42 36.03 2 2 -2 1222.88 35.47 -2 -2 2 1251.83 35.34 2 2 -2 1173.03 36.22 -2 -2 2 1226.07 36.01 2 2 -2 1293.62 35.02 -2 -2 2 1151.08 35.40 -2 -2 2 1223.28 35.50 2 2 -2 1283.50 35.43 -2 -2 2 1235.26 34.92 2 2 -2 1186.66 35.12 -2 -2 2 1272.48 35.11 2 2 -2 1216.58 35.41 -2 -2 2 1222.91 35.51 -2 -2 2 1237.06 35.36 -2 -2 2 1223.36 34.95 -2 -2 1 178.36 5.64 -2 -2 1 160.84 6.02 2 2 -1 184.58 5.68 -2 -2 1 175.73 5.30 -2 -2 1 174.65 6.36 -2 -2 1 177.78 5.65 2 2 -1 148.84 5.84 2 2 -1 168.45 5.58 2 2 -1 136.11 5.16 -2 -2 1 158.93 5.29 2 2 -1 162.52 5.98 -2 -2 1 186.49 5.32 2 2 -1 163.44 5.96 -2 -2 1 171.76 5.20 2 2 -1 169.79 5.25 2 2 -1 165.89 5.11 -2 -2 1 168.46 6.07 2 2 -1 167.20 6.06 -2 -2 1 180.53 6.04 -2 -2 1 172.56 6.23 -2 -2 1 169.02 5.60 2 2 0 2568.45 73.78 2 2 0 2608.18 73.77 -2 -2 0 2774.51 74.92 -2 -2 0 2521.96 73.94 -2 -2 0 2767.20 74.45 -2 -2 0 2717.11 74.39 -2 -2 0 2698.08 74.73 -2 -2 0 2554.22 73.94 2 2 0 2751.43 73.51 2 2 0 2633.81 73.82 2 2 0 2672.77 73.52 2 2 0 2558.28 73.69 2 2 0 2722.24 73.99 -2 -2 0 2767.58 73.62 -2 -2 0 2681.91 73.60 2 2 0 2740.29 73.65 2 2 0 2544.28 74.05 2 2 0 2631.15 73.98 2 2 0 2707.48 73.52 2 2 0 2346.44 74.15 -2 -2 -1 11.85 1.20 2 2 1 12.47 1.12 2 2 1 12.90 1.12 2 2 1 12.09 1.38 -2 -2 -1 14.32 1.26 -2 -2 -1 16.02 1.11 -2 -2 -1 12.80 1.23 -2 -2 -1 15.80 1.45 -2 -2 -1 13.51 1.15 -2 -2 -1 14.41 1.40 2 2 1 14.21 0.97 -2 -2 -1 12.27 1.32 -2 -2 -1 11.98 0.99 2 2 1 15.92 1.46 2 2 1 9.55 1.34 -2 -2 -1 14.56 1.44 2 2 2 1.75 0.96 -2 -2 -2 3.37 0.96 -2 -2 -2 3.49 0.85 -2 -2 -2 2.92 0.96 -2 -2 -2 3.45 1.00 2 2 2 4.14 1.03 2 2 2 1.89 0.91 -2 -2 -2 3.22 1.03 2 2 2 3.79 1.02 -2 -2 -2 3.73 1.02 -2 -2 -2 2.31 0.66 2 2 2 4.56 1.05 -2 -2 -3 1936.30 55.55 2 2 3 1904.38 55.16 -2 -2 -3 1907.84 56.73 -2 -2 -3 1978.90 56.76 2 2 3 2154.43 56.58 -2 -2 -3 2060.37 56.43 -2 -2 -3 2005.40 56.84 -2 -2 -3 2102.68 56.32 2 2 3 2020.77 56.48 2 2 3 1947.32 55.19 -2 -2 -3 2011.49 55.49 2 2 3 1982.70 55.51 2 2 3 1971.43 56.50 -2 -2 -3 1945.59 56.92 -2 -2 -3 1990.14 56.34 2 2 3 2023.05 56.16 -2 -2 -4 5168.39 143.94 -2 -2 -4 5018.60 142.56 -2 -2 -4 5149.45 143.72 2 2 4 5055.27 143.18 2 2 4 5288.26 143.14 -2 -2 -4 5296.68 143.10 2 2 4 5066.28 142.47 -2 -2 -4 4627.68 143.36 -2 -2 -4 5022.19 143.84 2 2 4 5247.31 143.18 2 2 4 5187.47 142.20 -2 -2 -4 5331.44 143.64 2 2 4 5141.50 142.85 2 2 4 4954.52 142.11 -2 -2 -4 5349.04 142.53 -2 -2 -5 632.19 19.03 -2 -2 -5 596.18 19.18 2 2 5 570.15 18.63 -2 -2 -5 603.59 20.24 -2 -2 -5 620.84 19.58 -2 -2 -5 615.14 20.30 -2 -2 -5 610.06 20.09 2 2 5 606.50 19.15 2 2 5 599.33 19.68 2 2 5 633.76 19.40 -2 -2 -5 595.88 19.49 2 2 5 641.62 19.32 2 2 5 650.96 18.84 -2 -2 -5 610.64 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4 7 1369.90 40.13 4 4 7 1318.03 40.44 -4 -4 -7 1310.37 39.15 -4 -4 -8 213.38 8.83 4 4 8 248.09 10.17 4 4 8 231.23 9.39 4 4 8 222.43 10.15 4 4 8 223.70 11.12 -4 -4 -8 196.71 10.71 4 4 8 238.05 11.54 -4 -4 -8 217.06 10.16 4 4 8 223.90 8.17 -4 -4 -8 222.95 10.63 -4 -4 -8 230.52 9.98 -4 -4 -8 232.40 11.29 -4 -4 -9 46.04 3.70 4 4 9 48.59 3.92 4 4 9 57.00 4.90 -4 -4 -9 51.08 5.00 4 4 9 49.76 5.25 -4 -4 -9 55.14 4.84 4 4 9 47.50 3.27 -4 -4 -9 52.57 4.86 -4 -4 -9 51.56 5.13 -4 -4 -10 225.39 10.08 -4 -4 -10 220.19 11.64 4 4 10 239.81 11.58 -4 -4 -10 225.27 11.90 4 4 10 236.27 12.10 -4 -4 -10 250.16 11.49 4 4 10 215.73 9.07 -4 -4 -10 222.61 11.15 -4 -4 -10 229.63 12.04 -4 -4 -11 3.58 2.95 -4 -4 -11 5.57 2.24 4 4 11 4.36 2.66 -4 -4 -11 3.16 2.74 4 4 11 3.07 2.91 4 4 11 4.18 1.98 -4 -4 -11 2.57 2.47 -4 -4 -11 6.52 2.99 -4 -4 -11 3.74 3.04 4 4 12 1.24 2.89 -4 -4 -12 0.64 3.00 4 4 12 4.25 3.00 -4 -4 -12 2.91 3.27 -4 -4 -12 -2.76 3.57 -4 -4 -12 -0.45 2.20 4 4 12 0.65 2.94 4 4 12 2.04 2.14 -4 -4 -12 1.09 2.78 -4 -4 -12 -0.60 2.90 -4 -4 -12 1.35 2.99 -4 -4 -13 9.66 3.90 4 4 13 11.66 3.87 4 4 13 10.68 3.59 4 4 13 5.38 3.87 -4 -4 -13 6.89 3.75 -4 -4 -13 12.75 4.04 4 4 13 7.58 3.57 4 4 13 8.34 2.59 -4 -4 -13 9.18 3.69 -4 -4 -13 19.34 4.40 -4 -4 -13 7.31 3.52 4 4 14 100.24 8.72 4 4 14 82.75 7.93 -4 -4 -14 87.42 8.20 -4 -4 -14 80.66 8.31 -4 -4 -14 91.22 8.73 4 4 14 98.56 8.41 -4 -4 -14 104.44 8.72 -4 -4 -14 99.02 7.90 -4 -4 -14 94.99 8.71 -4 -4 -15 30.37 5.88 -4 -4 -15 24.09 5.45 4 4 15 42.86 6.06 4 4 15 37.75 6.06 -4 -4 -15 33.49 5.11 -4 -5 12 39.46 6.05 -4 -5 12 40.11 6.54 4 5 -12 41.92 6.34 4 5 -12 33.13 6.42 -4 -5 11 74.99 7.54 -4 -5 11 76.25 7.73 -4 -5 11 89.55 8.36 4 5 -11 69.72 7.58 4 5 -11 75.61 8.15 -4 -5 10 26.43 4.98 -4 -5 10 30.26 5.21 -4 -5 10 34.05 5.34 4 5 -10 43.48 6.21 4 5 -10 27.65 5.10 -4 -5 10 27.35 5.01 4 5 -10 37.63 5.61 4 5 -10 48.11 6.22 4 5 -9 4.65 3.34 -4 -5 9 0.58 2.76 4 5 -9 0.69 3.56 -4 -5 9 -1.19 3.04 -4 -5 9 -0.63 2.90 -4 -5 9 -1.99 2.87 4 5 -9 -2.09 3.14 4 5 -8 235.04 12.43 -4 -5 8 214.15 11.70 -4 -5 8 207.85 11.20 -4 -5 8 214.96 11.91 -4 -5 8 214.46 11.30 4 5 -8 218.92 11.81 4 5 -8 234.80 12.49 4 5 -7 330.03 14.64 -4 -5 7 302.26 13.99 -4 -5 7 303.88 13.51 -4 -5 7 296.72 13.35 -4 -5 7 299.13 14.10 4 5 -7 291.69 13.90 -4 -5 7 312.09 12.03 -4 -5 6 341.83 13.29 4 5 -6 325.73 11.55 -4 -5 6 347.15 14.03 4 5 -6 332.68 14.04 -4 -5 6 314.81 12.91 4 5 -6 322.91 11.43 4 5 -6 281.60 9.00 4 5 -6 289.46 9.00 -4 -5 6 333.71 14.00 4 5 -6 320.22 13.83 -4 -5 5 98.26 5.88 4 5 -5 91.08 4.86 -4 -5 5 88.59 6.15 4 5 -5 101.23 6.58 4 5 -5 95.37 4.72 -4 -5 5 92.84 6.37 4 5 -5 103.11 5.16 -4 -5 5 89.83 5.75 4 5 -5 100.07 4.70 4 5 -5 92.08 3.91 4 5 -5 99.77 3.96 -4 -5 5 93.72 6.36 4 5 -5 103.00 6.69 4 5 -4 52.09 2.90 -4 -5 4 64.99 4.78 4 5 -4 63.50 3.50 -4 -5 4 58.05 4.16 4 5 -4 61.51 3.14 4 5 -4 46.34 4.39 -4 -5 4 56.66 4.65 4 5 -4 64.96 3.65 -4 -5 4 63.27 4.31 -4 -5 4 64.88 3.54 -4 -5 4 59.96 3.48 4 5 -4 58.31 3.12 -4 -5 4 61.76 4.75 4 5 -4 65.86 3.76 4 5 -4 61.71 4.91 4 5 -4 53.60 4.95 4 5 -3 3.10 2.16 -4 -5 3 5.34 1.79 -4 -5 3 7.30 1.96 -4 -5 3 5.59 1.92 4 5 -3 4.32 1.41 4 5 -3 3.85 0.61 4 5 -3 1.73 1.15 -4 -5 3 2.84 1.10 4 5 -3 1.79 1.41 4 5 -3 4.79 1.76 4 5 -3 6.28 1.28 -4 -5 3 5.00 1.31 4 5 -3 3.06 0.58 4 5 -3 2.77 1.93 4 5 -3 4.49 1.28 4 5 -3 3.13 1.26 -4 -5 3 3.52 1.59 4 5 -3 7.11 2.18 4 5 -3 2.73 2.22 4 5 -2 133.04 7.00 -4 -5 2 122.44 5.56 4 5 -2 116.19 4.56 4 5 -2 109.99 5.93 -4 -5 2 119.46 6.06 4 5 -2 121.95 5.94 4 5 -2 124.20 6.50 4 5 -2 109.94 5.90 -4 -5 2 126.49 6.39 4 5 -2 115.69 4.57 -4 -5 2 129.06 6.43 4 5 -2 117.71 5.32 -4 -5 2 118.62 5.51 4 5 -2 115.56 6.27 4 5 -2 116.17 5.82 4 5 -2 127.10 5.38 4 5 -2 118.55 4.41 4 5 -2 115.20 5.20 4 5 -2 122.41 6.10 -4 -5 2 123.54 6.15 4 5 -2 123.99 5.92 4 5 -2 122.03 6.93 4 5 -1 766.88 24.74 4 5 -1 750.96 23.98 4 5 -1 758.15 22.51 4 5 -1 723.15 23.31 4 5 -1 762.24 22.64 4 5 -1 730.89 23.73 4 5 -1 777.29 22.55 -4 -5 1 720.99 22.72 4 5 -1 761.75 24.38 -4 -5 1 763.75 24.40 4 5 -1 721.71 23.76 4 5 -1 764.29 22.49 4 5 -1 757.46 23.13 4 5 -1 752.28 22.06 4 5 -1 766.14 24.73 -4 -5 1 750.00 22.78 4 5 -1 746.62 22.50 4 5 -1 767.44 22.27 4 5 -1 721.39 22.98 4 5 -1 768.32 23.45 4 5 -1 683.78 23.04 4 5 -1 749.64 23.65 4 5 -1 778.17 24.24 4 5 -1 746.92 24.77 4 5 -1 750.17 23.30 4 5 -1 712.48 22.57 4 5 0 231.60 8.47 4 5 0 223.29 8.55 4 5 0 239.87 8.44 -4 -5 0 240.30 8.54 4 5 0 245.03 9.60 4 5 0 236.20 9.96 4 5 0 238.15 7.95 4 5 0 232.03 8.52 4 5 0 240.96 8.60 4 5 0 238.12 8.62 4 5 0 225.41 8.45 4 5 0 239.07 7.96 -4 -5 0 239.25 8.99 4 5 0 250.25 9.77 4 5 0 245.01 8.02 4 5 0 247.45 9.63 4 5 0 237.01 9.23 4 5 0 224.32 9.43 4 5 0 232.91 8.94 4 5 0 247.19 8.16 4 5 0 220.65 8.65 4 5 0 236.95 8.94 4 5 0 241.58 8.44 4 5 0 217.40 8.36 -4 -5 0 246.42 8.56 4 5 0 232.71 9.23 4 5 0 223.35 7.65 4 5 0 240.46 8.13 4 5 0 232.33 9.81 4 5 1 79.13 3.93 4 5 1 70.61 3.11 4 5 1 72.05 3.42 4 5 1 82.86 4.75 -4 -5 -1 71.53 3.18 4 5 1 68.40 4.24 4 5 1 71.72 3.08 4 5 1 67.88 4.45 4 5 1 73.29 3.08 4 5 1 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-4 -5 -6 71.69 4.51 4 5 6 78.06 4.91 -4 -5 -6 75.67 5.24 -4 -5 -6 62.01 5.12 4 5 6 73.28 4.12 -4 -5 -6 62.50 3.04 -4 -5 -7 1.98 1.22 -4 -5 -7 1.34 1.86 -4 -5 -7 1.68 1.82 4 5 7 1.26 2.06 4 5 7 4.62 1.73 4 5 7 1.74 2.06 -4 -5 -7 1.72 1.71 -4 -5 -7 3.88 2.23 4 5 7 1.85 2.19 -4 -5 -7 1.33 2.28 4 5 7 1.42 0.63 -4 -5 -7 2.48 1.91 -4 -5 -7 3.52 2.05 4 5 7 2.28 1.54 4 5 8 211.33 8.65 4 5 8 214.70 10.80 -4 -5 -8 181.07 10.34 4 5 8 221.50 11.15 4 5 8 217.09 9.86 4 5 8 223.14 11.03 -4 -5 -8 215.79 10.77 -4 -5 -8 189.35 9.40 -4 -5 -8 218.42 9.58 -4 -5 -8 226.76 7.65 4 5 8 211.51 7.38 -4 -5 -8 202.15 10.61 -4 -5 -8 215.19 9.41 4 5 8 211.88 8.79 -4 -5 -9 268.49 13.49 4 5 9 283.53 13.64 4 5 9 300.23 11.34 4 5 9 303.16 12.79 4 5 9 302.00 13.85 -4 -5 -9 277.82 13.36 4 5 9 304.44 14.10 -4 -5 -9 301.43 12.56 4 5 9 291.04 10.17 -4 -5 -9 322.70 13.70 -4 -5 -9 285.72 12.05 -4 -5 -9 292.33 13.71 4 5 10 74.07 4.25 4 5 10 71.71 4.99 4 5 10 77.52 6.09 -4 -5 -10 82.44 7.34 -4 -5 -10 77.74 6.57 4 5 10 98.72 7.44 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5.75 -4 -6 10 48.44 6.48 4 6 -10 53.29 5.92 4 6 -10 48.67 6.38 -4 -6 10 44.57 6.19 -4 -6 9 3.84 3.17 -4 -6 9 -1.88 3.10 4 6 -9 -1.44 3.18 -4 -6 9 -2.01 3.31 -4 -6 9 -1.40 3.42 4 6 -9 1.12 2.73 4 6 -8 25.26 4.42 -4 -6 8 23.74 4.26 -4 -6 8 25.51 4.23 4 6 -8 30.33 4.93 -4 -6 8 27.72 4.61 -4 -6 8 16.74 3.81 4 6 -8 28.16 4.65 -4 -6 7 105.43 7.60 4 6 -7 118.81 8.26 -4 -6 7 107.54 7.43 -4 -6 7 92.35 7.04 4 6 -7 99.25 7.74 -4 -6 7 102.81 7.75 4 6 -7 114.28 7.86 -4 -6 6 298.41 13.49 4 6 -6 281.89 13.45 -4 -6 6 292.06 12.91 4 6 -6 294.82 13.73 -4 -6 6 282.24 13.38 4 6 -6 291.61 13.48 4 6 -6 281.75 13.69 -4 -6 6 269.98 12.57 4 6 -5 311.58 10.14 -4 -6 5 310.52 12.38 -4 -6 5 339.41 12.16 -4 -6 5 303.72 11.60 4 6 -5 285.71 8.63 4 6 -5 334.99 12.88 4 6 -5 321.07 12.80 -4 -6 5 313.42 12.56 4 6 -5 294.32 10.07 4 6 -5 337.47 12.82 4 6 -4 53.19 3.58 -4 -6 4 54.51 4.59 -4 -6 4 48.79 4.27 4 6 -4 62.22 4.92 4 6 -4 62.92 5.19 4 6 -4 51.68 3.65 -4 -6 4 57.01 4.44 4 6 -4 54.86 2.69 4 6 -4 62.09 3.46 4 6 -4 55.25 2.69 -4 -6 4 61.19 4.89 4 6 -4 57.30 4.81 4 6 -4 51.38 3.74 4 6 -3 97.71 5.83 -4 -6 3 94.22 5.76 4 6 -3 95.18 5.84 4 6 -3 77.17 3.00 4 6 -3 99.31 4.84 -4 -6 3 94.62 5.82 4 6 -3 83.16 5.00 4 6 -3 102.46 4.77 -4 -6 3 83.36 5.08 -4 -6 3 87.54 4.48 4 6 -3 94.92 4.80 4 6 -3 93.61 4.10 -4 -6 3 100.00 4.72 4 6 -3 79.76 2.99 -4 -6 3 94.96 5.41 4 6 -3 91.25 4.10 -4 -6 3 90.84 5.76 4 6 -3 95.19 5.08 4 6 -3 93.16 5.94 4 6 -3 90.04 6.13 4 6 -2 3.78 2.25 4 6 -2 5.96 2.13 4 6 -2 3.16 1.08 4 6 -2 4.37 1.63 4 6 -2 4.91 1.06 4 6 -2 5.35 1.57 -4 -6 2 8.23 1.94 4 6 -2 6.50 1.58 4 6 -2 3.65 2.07 4 6 -2 6.99 1.48 4 6 -2 6.99 1.76 4 6 -2 7.04 2.19 4 6 -2 5.60 1.23 -4 -6 2 5.63 1.81 4 6 -2 5.25 1.68 4 6 -2 5.11 1.45 -4 -6 2 2.42 1.57 4 6 -2 2.54 1.69 4 6 -2 5.57 1.74 4 6 -2 4.47 2.22 4 6 -1 126.07 6.77 4 6 -1 121.12 5.11 4 6 -1 113.03 5.79 4 6 -1 117.55 5.82 4 6 -1 116.19 5.31 4 6 -1 120.72 6.20 4 6 -1 120.75 5.45 4 6 -1 117.70 5.08 4 6 -1 111.18 5.76 -4 -6 1 119.82 6.10 4 6 -1 113.48 5.23 4 6 -1 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2.98 2.19 4 7 -3 13.95 1.92 4 7 -3 20.43 3.27 4 7 -3 17.14 2.69 -4 -7 3 14.41 2.69 4 7 -3 12.92 2.01 4 7 -3 16.32 1.59 4 7 -3 15.65 2.82 4 7 -3 19.29 2.86 4 7 -3 12.99 1.33 4 7 -3 16.58 1.67 -4 -7 3 9.98 2.64 4 7 -3 14.01 2.94 4 7 -3 15.52 2.30 4 7 -3 13.26 2.02 -4 -7 3 19.82 2.98 -4 -7 3 13.62 2.62 4 7 -2 143.91 7.53 4 7 -2 161.35 7.34 4 7 -2 140.38 7.55 4 7 -2 151.72 7.88 4 7 -2 156.09 6.79 4 7 -2 149.97 5.78 4 7 -2 160.15 7.17 -4 -7 2 147.79 7.32 4 7 -2 149.12 6.05 4 7 -2 139.78 6.64 4 7 -2 143.03 6.02 -4 -7 2 153.27 7.45 4 7 -2 148.97 6.03 4 7 -2 147.54 5.89 -4 -7 2 144.89 7.54 4 7 -2 148.53 6.74 4 7 -2 149.30 7.83 4 7 -2 138.55 7.88 4 7 -1 899.79 29.00 4 7 -1 876.93 27.88 4 7 -1 905.01 27.27 4 7 -1 904.82 27.78 4 7 -1 876.99 26.56 4 7 -1 854.55 26.55 4 7 -1 935.82 28.22 4 7 -1 914.31 27.35 4 7 -1 904.36 27.53 4 7 -1 920.54 27.84 4 7 -1 886.46 26.83 4 7 -1 901.43 27.09 4 7 -1 885.47 27.13 4 7 -1 886.69 28.31 4 7 -1 878.80 26.83 4 7 -1 893.35 26.78 4 7 -1 871.70 25.70 4 7 -1 790.06 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331.16 12.02 4 7 1 323.14 12.09 4 7 1 340.47 12.69 4 7 2 173.05 8.39 4 7 2 188.89 8.02 4 7 2 182.43 6.74 4 7 2 181.70 7.21 4 7 2 170.14 7.16 4 7 2 180.42 7.85 4 7 2 169.41 7.81 4 7 2 171.72 8.26 -4 -7 -2 174.72 8.76 4 7 2 184.25 7.31 4 7 2 177.05 7.66 -4 -7 -2 190.37 9.08 4 7 2 188.48 8.11 4 7 2 180.08 7.97 4 7 2 198.53 8.26 -4 -7 -2 177.96 8.54 4 7 2 163.02 8.29 4 7 2 203.15 8.23 4 7 2 179.49 7.88 4 7 2 177.78 6.89 4 7 2 179.56 8.01 4 7 2 184.94 8.20 -4 -7 -2 163.97 8.62 4 7 2 186.49 8.03 4 7 2 170.94 7.36 4 7 3 168.45 6.56 4 7 3 163.08 8.12 4 7 3 153.54 5.62 4 7 3 153.61 6.18 -4 -7 -3 166.28 8.51 4 7 3 163.61 6.93 -4 -7 -3 152.27 7.84 4 7 3 171.27 7.79 -4 -7 -3 167.98 8.65 4 7 3 167.16 7.77 4 7 3 157.92 6.84 4 7 3 167.83 7.77 4 7 3 169.65 7.42 4 7 3 174.79 8.19 4 7 3 181.89 8.58 4 7 3 155.91 7.67 4 7 3 164.88 6.00 4 7 3 163.94 7.65 -4 -7 -3 161.35 8.28 4 7 3 176.45 7.77 4 7 3 168.66 7.67 4 7 3 161.17 7.02 -4 -7 -3 170.46 8.53 4 7 4 253.18 8.57 4 7 4 280.79 11.46 4 7 4 267.07 10.80 4 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7 17.94 1.86 -4 -7 -7 30.01 4.28 -4 -7 -7 17.93 3.13 -4 -7 -7 18.99 3.33 -4 -7 -7 16.65 3.02 4 7 7 17.03 3.04 -4 -7 -7 22.36 3.32 -4 -7 -7 18.30 2.50 -4 -7 -7 20.69 3.46 -4 -7 -7 19.12 3.26 4 7 7 19.57 2.09 -4 -7 -8 44.31 4.95 4 7 8 33.20 2.61 4 7 8 35.63 2.56 4 7 8 37.18 4.41 -4 -7 -8 40.62 4.95 -4 -7 -8 33.35 4.10 4 7 8 40.42 4.38 4 7 8 30.46 4.41 4 7 8 42.80 4.71 -4 -7 -8 35.43 4.27 -4 -7 -8 28.84 3.22 -4 -7 -8 28.76 4.11 4 7 8 26.67 2.57 -4 -7 -8 31.93 4.12 -4 -7 -8 40.42 3.61 -4 -7 -9 2.44 1.96 4 7 9 1.75 2.48 4 7 9 0.57 2.28 -4 -7 -9 1.84 1.67 -4 -7 -9 -2.02 3.02 -4 -7 -9 -1.01 2.26 4 7 9 1.29 1.48 4 7 9 0.61 2.47 -4 -7 -9 3.50 2.57 -4 -7 -9 1.64 2.51 -4 -7 -9 -0.97 1.74 -4 -7 -9 -0.55 2.39 4 7 10 72.02 6.71 -4 -7 -10 89.00 7.23 -4 -7 -10 81.48 5.58 4 7 10 73.48 6.63 -4 -7 -10 83.92 6.63 4 7 10 85.07 7.18 -4 -7 -10 77.19 6.71 4 7 10 67.36 3.58 -4 -7 -10 83.97 6.98 4 7 11 154.47 10.17 -4 -7 -11 149.90 9.90 4 7 11 135.95 8.69 4 7 11 137.93 9.73 -4 -7 -11 157.37 10.66 -4 -7 -11 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158.01 9.55 4 8 -6 170.10 10.53 -4 -8 5 41.13 4.82 4 8 -5 37.41 4.83 -4 -8 5 43.13 4.92 4 8 -5 55.90 5.66 -4 -8 5 46.43 5.03 4 8 -5 44.85 4.85 4 8 -5 33.52 3.79 4 8 -5 40.67 5.16 -4 -8 4 30.67 4.06 4 8 -4 38.68 4.60 4 8 -4 32.71 4.47 -4 -8 4 33.97 4.13 -4 -8 4 38.13 4.59 4 8 -4 41.89 4.38 4 8 -4 28.51 3.14 4 8 -3 58.02 4.74 4 8 -3 59.65 3.40 4 8 -3 62.68 5.28 -4 -8 3 62.19 4.38 -4 -8 3 53.61 4.77 4 8 -3 56.51 3.32 4 8 -3 51.61 3.06 4 8 -3 55.00 5.04 -4 -8 3 58.23 5.05 4 8 -3 54.71 3.62 -4 -8 3 50.80 4.90 4 8 -3 69.51 5.31 4 8 -3 66.76 5.56 4 8 -2 13.63 2.84 4 8 -2 17.55 2.32 4 8 -2 15.72 2.59 4 8 -2 14.97 2.97 4 8 -2 16.66 2.18 4 8 -2 17.37 1.96 4 8 -2 14.89 2.08 4 8 -2 15.47 1.37 4 8 -2 19.99 1.83 -4 -8 2 16.29 2.79 4 8 -2 20.36 3.14 4 8 -2 13.46 2.23 4 8 -2 15.76 2.68 4 8 -1 332.22 13.79 4 8 -1 333.30 12.51 4 8 -1 330.22 13.03 4 8 -1 332.06 13.28 4 8 -1 321.98 11.74 4 8 -1 333.20 13.18 4 8 -1 345.07 13.44 4 8 -1 325.12 12.53 4 8 -1 346.01 12.93 4 8 -1 336.20 11.76 4 8 -1 331.01 12.48 4 8 -1 344.31 12.51 4 8 -1 355.98 12.55 4 8 -1 328.44 12.16 4 8 -1 348.70 11.80 4 8 -1 333.64 12.22 4 8 -1 330.69 13.27 4 8 -1 334.75 13.52 4 8 0 532.83 17.70 4 8 0 507.02 18.06 4 8 0 542.83 17.96 4 8 0 522.34 18.39 4 8 0 507.89 17.60 4 8 0 528.98 19.14 4 8 0 573.92 18.72 4 8 0 507.51 19.10 4 8 0 526.23 18.29 4 8 0 555.76 17.80 4 8 0 522.02 18.45 4 8 0 536.48 18.17 4 8 0 521.78 18.39 4 8 0 528.51 18.48 4 8 0 545.32 18.17 4 8 0 540.69 17.66 4 8 0 551.51 18.31 4 8 0 536.91 17.98 4 8 0 543.73 18.83 4 8 0 553.94 18.07 4 8 0 538.69 18.73 4 8 0 531.34 18.16 4 8 0 539.04 19.23 4 8 0 528.45 19.04 4 8 1 234.91 10.52 4 8 1 225.99 9.29 4 8 1 235.23 9.19 4 8 1 231.82 9.51 4 8 1 223.79 10.12 4 8 1 227.66 9.90 4 8 1 240.54 9.34 4 8 1 249.35 10.76 4 8 1 233.52 9.78 4 8 1 241.15 9.35 4 8 1 224.87 9.77 4 8 1 222.42 9.62 4 8 1 233.55 10.20 4 8 1 255.00 10.06 4 8 1 218.95 9.20 4 8 1 254.32 9.83 4 8 1 233.25 9.51 4 8 1 230.85 9.86 4 8 1 241.33 9.91 4 8 1 232.20 10.05 4 8 1 230.13 10.03 4 8 1 231.48 9.47 4 8 2 59.65 4.85 4 8 2 65.56 4.29 4 8 2 68.20 4.94 4 8 2 64.59 4.13 4 8 2 66.02 3.72 4 8 2 64.82 4.10 4 8 2 66.95 3.86 4 8 2 65.78 4.12 4 8 2 66.40 4.36 4 8 2 77.00 4.77 4 8 2 64.70 5.02 4 8 2 60.77 4.11 4 8 2 64.20 4.47 -4 -8 -2 62.43 4.55 -4 -8 -2 70.95 5.37 4 8 2 56.49 4.42 4 8 2 60.13 4.88 4 8 2 70.68 4.79 4 8 2 56.33 3.72 4 8 2 62.69 4.56 4 8 2 58.51 4.37 4 8 2 61.76 4.51 4 8 2 67.12 4.41 4 8 2 58.53 4.17 4 8 3 41.06 4.16 4 8 3 44.53 2.65 4 8 3 47.57 3.21 4 8 3 41.61 3.43 4 8 3 45.85 4.00 4 8 3 43.77 4.08 4 8 3 37.67 3.30 4 8 3 37.62 3.29 4 8 3 41.55 3.76 -4 -8 -3 39.27 3.73 -4 -8 -3 43.03 4.29 4 8 3 46.00 4.42 4 8 3 43.41 3.99 4 8 3 46.05 4.01 4 8 3 41.64 2.93 4 8 3 36.63 3.60 4 8 3 47.11 3.92 4 8 3 44.93 3.31 -4 -8 -3 44.53 4.14 4 8 3 48.07 3.48 4 8 4 208.38 7.90 4 8 4 190.08 9.73 4 8 4 189.76 6.59 4 8 4 197.23 8.56 -4 -8 -4 207.38 10.04 4 8 4 209.41 10.00 -4 -8 -4 196.50 10.37 4 8 4 198.28 8.60 4 8 4 195.02 9.34 -4 -8 -4 210.62 9.34 4 8 4 202.13 10.12 4 8 4 202.84 9.54 4 8 4 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8.68 4 9 -1 184.59 9.12 4 9 -1 163.35 9.07 4 9 0 197.75 9.33 4 9 0 218.53 9.64 4 9 0 218.97 10.16 4 9 0 223.68 9.54 4 9 0 202.99 10.47 4 9 0 225.49 9.67 4 9 0 232.15 9.99 4 9 0 209.32 9.35 4 9 0 218.26 8.84 4 9 0 215.24 9.45 4 9 0 218.74 9.54 4 9 0 202.70 9.30 4 9 0 226.70 9.74 4 9 0 191.66 8.78 4 9 0 218.23 9.64 4 9 0 209.66 9.54 4 9 0 228.76 10.07 4 9 0 235.15 10.84 4 9 0 214.22 9.98 4 9 0 211.69 10.51 4 9 1 362.55 15.28 4 9 1 372.54 14.14 4 9 1 345.78 13.48 4 9 1 378.04 13.95 4 9 1 351.02 14.34 4 9 1 372.35 13.70 4 9 1 398.94 14.11 4 9 1 389.69 13.78 4 9 1 361.68 15.37 4 9 1 384.44 13.78 4 9 1 404.83 14.64 4 9 1 386.29 14.47 4 9 1 354.63 13.70 4 9 1 384.55 14.18 4 9 1 385.99 14.20 4 9 1 389.52 14.40 4 9 1 388.78 14.45 4 9 1 354.01 14.69 4 9 2 313.85 13.14 4 9 2 281.67 11.07 4 9 2 288.88 11.54 4 9 2 264.76 10.49 4 9 2 292.31 12.30 4 9 2 269.19 10.43 4 9 2 281.85 12.71 4 9 2 280.44 11.24 4 9 2 267.67 11.27 4 9 2 298.45 12.10 4 9 2 311.24 10.82 4 9 2 288.78 12.52 4 9 2 281.58 11.94 4 9 2 282.56 11.39 4 9 2 294.84 11.43 4 9 2 285.73 11.27 4 9 2 286.66 11.83 4 9 3 18.67 2.70 4 9 3 16.29 1.99 4 9 3 14.78 1.79 4 9 3 9.52 2.72 4 9 3 15.94 3.34 4 9 3 14.89 2.47 4 9 3 15.34 1.99 4 9 3 16.81 2.35 -4 -9 -3 18.55 3.29 4 9 3 17.28 2.54 4 9 3 20.03 2.31 -4 -9 -3 15.78 2.54 4 9 3 10.03 2.83 4 9 3 18.12 2.99 4 9 3 15.10 2.18 4 9 4 0.27 1.49 -4 -9 -4 1.36 2.00 4 9 4 1.46 2.51 4 9 4 0.94 1.00 4 9 4 0.42 1.03 4 9 4 0.66 1.10 4 9 4 1.56 1.90 -4 -9 -4 -0.33 1.86 4 9 4 -0.49 2.36 4 9 4 0.18 1.15 4 9 4 0.50 2.27 -4 -9 -4 -1.33 2.23 -4 -9 -4 0.42 1.83 4 9 5 94.36 5.01 4 9 5 113.22 7.43 4 9 5 88.54 3.67 -4 -9 -5 107.04 7.10 4 9 5 95.09 6.97 4 9 5 106.60 5.46 -4 -9 -5 98.95 6.03 4 9 5 102.76 7.28 -4 -9 -5 104.02 7.05 -4 -9 -5 97.93 6.86 -4 -9 -5 122.71 7.17 4 9 5 102.59 4.85 4 9 5 98.77 5.98 4 9 6 124.63 5.63 4 9 6 122.93 5.48 4 9 6 125.94 8.18 4 9 6 119.12 6.58 -4 -9 -6 119.18 8.63 4 9 6 134.58 8.44 -4 -9 -6 121.70 7.02 4 9 6 128.62 8.43 -4 -9 -6 109.66 7.76 -4 -9 -6 133.60 8.26 -4 -9 -6 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2.33 -4 -10 -5 -0.52 2.64 -4 -10 -5 2.52 2.31 4 10 5 1.23 0.73 -4 -10 -5 2.24 2.40 4 10 6 45.36 3.58 4 10 6 57.50 5.90 -4 -10 -6 56.36 5.39 4 10 6 56.61 5.83 4 10 6 45.93 4.03 -4 -10 -6 51.51 4.34 4 10 6 55.07 5.91 -4 -10 -6 51.51 5.39 -4 -10 -6 48.72 5.27 -4 -10 -6 61.10 5.38 4 10 7 92.66 4.96 4 10 7 91.90 7.57 -4 -10 -7 84.64 7.03 4 10 7 109.13 8.03 4 10 7 94.09 6.18 -4 -10 -7 87.01 5.95 4 10 7 91.60 7.62 -4 -10 -7 101.84 7.79 -4 -10 -7 90.37 7.26 -4 -10 -7 102.05 7.18 4 10 8 95.67 7.87 -4 -10 -8 89.80 7.44 4 10 8 101.01 8.14 4 10 8 105.31 7.00 -4 -10 -8 90.07 6.32 4 10 8 96.33 7.98 -4 -10 -8 95.19 7.73 -4 -10 -8 91.91 7.50 4 10 9 36.60 5.35 4 10 9 32.77 5.10 -4 -10 -9 25.94 4.64 4 10 9 34.34 4.79 -4 -10 -9 43.28 5.56 -4 -10 -9 23.58 4.54 -4 -10 -10 2.14 3.48 4 10 10 -2.95 3.43 4 10 10 2.97 3.57 4 10 10 2.31 3.64 4 10 10 5.18 3.35 -4 -10 -10 4.13 3.15 -4 -10 -10 2.76 3.11 -4 -10 -10 1.24 2.98 -4 -10 -11 29.58 5.44 4 10 11 24.33 5.17 4 10 11 26.49 5.38 4 10 11 24.29 5.19 -4 -10 -11 24.48 4.75 -4 -10 -11 21.11 4.76 -4 -10 -11 28.73 4.93 -4 -10 -12 73.50 7.75 4 10 12 72.35 7.94 4 10 12 55.40 7.18 4 10 12 64.41 7.59 -4 -10 -12 67.15 7.43 -4 -10 -12 58.90 6.92 4 10 13 28.64 5.99 4 10 13 28.15 5.74 -4 -10 -13 28.19 5.76 -4 -10 -13 22.52 4.99 -4 -10 -13 23.74 5.21 4 10 14 -0.91 3.86 4 10 14 -2.73 5.12 -4 -10 -14 2.68 4.02 4 11 -6 5.95 4.29 4 11 -5 28.88 5.38 4 11 -5 30.07 5.17 4 11 -5 23.57 5.12 4 11 -4 37.85 5.18 4 11 -4 42.84 5.91 4 11 -4 29.90 4.61 4 11 -4 40.26 5.47 4 11 -3 102.30 7.61 4 11 -3 109.20 8.34 4 11 -3 106.16 7.87 4 11 -3 106.37 8.11 4 11 -2 71.47 6.46 4 11 -2 70.76 6.19 4 11 -2 73.14 5.60 4 11 -2 71.74 6.28 4 11 -2 72.49 6.34 4 11 -2 80.60 7.73 4 11 -2 82.15 7.19 4 11 -1 -1.28 3.36 4 11 -1 0.46 2.77 4 11 -1 -0.62 2.91 4 11 -1 -1.28 2.33 4 11 -1 0.49 2.66 4 11 -1 0.60 2.77 4 11 -1 2.30 2.25 4 11 -1 1.82 2.19 4 11 -1 -0.48 2.49 4 11 -1 1.39 2.39 4 11 0 4.70 2.82 4 11 0 7.21 3.16 4 11 0 2.44 3.06 4 11 0 4.79 2.26 4 11 0 5.76 2.47 4 11 0 5.72 2.34 4 11 0 5.93 3.31 4 11 0 6.30 2.94 4 11 0 5.22 2.56 4 11 0 4.27 2.09 4 11 0 4.07 2.35 4 11 0 5.23 2.44 4 11 1 10.20 3.37 4 11 1 14.89 3.15 4 11 1 9.41 3.23 4 11 1 16.05 3.83 4 11 1 10.23 2.52 4 11 1 10.27 3.54 4 11 1 13.16 2.47 4 11 1 15.37 2.82 4 11 1 18.96 2.72 4 11 1 12.66 2.80 4 11 2 83.55 7.36 4 11 2 93.85 6.32 4 11 2 94.55 6.46 4 11 2 100.61 7.21 4 11 2 81.90 6.13 4 11 2 106.83 7.85 4 11 2 103.59 5.42 4 11 2 83.02 5.25 4 11 2 86.04 6.67 4 11 3 55.37 4.77 4 11 3 54.18 5.27 4 11 3 54.87 5.96 4 11 3 61.15 6.22 4 11 3 64.43 5.97 4 11 3 49.33 3.75 4 11 3 53.34 5.05 4 11 4 0.39 2.01 -4 -11 -4 2.41 2.39 4 11 4 -0.62 2.64 4 11 4 -0.63 2.91 4 11 4 -0.59 3.14 4 11 4 0.24 1.53 4 11 5 3.12 2.19 4 11 5 5.78 3.28 4 11 5 5.73 3.01 4 11 5 -0.63 3.20 -4 -11 -5 4.75 3.17 -4 -11 -5 5.17 2.98 4 11 6 2.65 3.13 4 11 6 -0.30 1.87 -4 -11 -6 -0.55 2.70 4 11 6 -0.65 3.00 -4 -11 -6 -1.18 2.69 4 11 6 -0.66 2.93 4 11 6 -1.21 1.96 -4 -11 -6 -1.70 2.81 4 11 7 67.12 7.00 -4 -11 -7 60.68 6.11 4 11 7 49.46 4.48 4 11 7 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3.95 5 -6 7 -8.12 4.54 -5 6 -8 22.30 5.92 5 -6 8 26.70 5.62 -5 6 -8 12.50 5.06 5 -6 8 9.29 4.76 5 -6 8 25.84 5.53 -5 6 -8 18.87 4.98 -5 6 -8 17.67 4.15 -5 6 -8 16.32 4.66 5 -6 8 8.30 4.59 5 -6 8 17.19 4.76 -5 6 -8 22.24 5.59 5 -6 8 14.30 5.14 5 -6 9 108.78 10.49 5 -6 9 106.02 10.65 5 -5 -14 2.59 3.56 -5 5 14 0.83 3.88 5 -5 -13 1.25 3.09 5 -5 -13 6.36 3.63 -5 5 13 1.49 3.86 -5 5 13 6.57 2.99 -5 5 13 3.21 3.67 -5 5 12 74.75 7.67 -5 5 12 77.61 6.33 5 -5 -12 84.80 6.66 -5 5 12 97.83 6.86 -5 5 12 84.73 7.60 5 -5 -12 81.68 7.17 -5 5 12 79.18 8.58 5 -5 -12 88.40 7.55 -5 5 12 83.20 8.05 5 -5 -12 92.79 6.95 5 -5 -11 5.84 3.22 -5 5 11 6.75 3.44 -5 5 11 6.30 2.81 5 -5 -11 4.47 2.54 -5 5 11 5.32 3.18 -5 5 11 5.39 2.68 5 -5 -11 8.28 3.37 -5 5 11 7.17 3.52 -5 5 11 6.73 4.41 5 -5 -11 4.78 3.01 -5 5 11 7.23 3.74 -5 5 10 38.16 4.30 5 -5 -10 30.10 4.30 -5 5 10 39.58 4.44 5 -5 -10 37.19 4.60 -5 5 10 42.28 5.06 5 -5 -10 33.10 4.67 -5 5 10 40.78 5.94 5 -5 -10 48.73 5.37 -5 5 10 40.36 5.15 5 -5 -10 40.02 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483.93 18.52 5 -5 -5 469.56 18.88 5 -5 -5 490.96 16.71 -5 5 5 487.97 19.50 -5 5 4 147.30 9.08 -5 5 4 130.77 6.50 -5 5 4 138.83 8.62 -5 5 4 136.04 9.10 -5 5 4 133.02 6.78 5 -5 -4 134.69 7.82 5 -5 -4 137.31 8.04 5 -5 -4 139.20 6.60 5 -5 -4 142.86 8.25 -5 5 4 126.67 7.62 5 -5 -4 131.20 6.38 -5 5 4 154.60 8.89 -5 5 3 -0.57 2.34 -5 5 3 1.11 1.53 5 -5 -3 0.47 1.82 5 -5 -3 4.09 1.75 -5 5 3 0.94 1.57 -5 5 3 2.39 2.53 5 -5 -3 0.42 2.05 5 -5 -3 2.33 1.94 5 -5 -3 0.43 2.01 5 -5 -3 1.57 1.65 -5 5 2 47.42 5.21 -5 5 2 43.71 3.79 -5 5 2 34.04 3.85 5 -5 -2 50.24 4.78 -5 5 2 45.36 4.00 5 -5 -2 36.64 4.20 5 -5 -2 45.25 4.37 5 -5 -2 46.90 4.42 5 -5 -2 42.30 4.49 5 -5 -2 45.99 2.63 5 -5 -2 52.70 3.98 -5 5 2 46.34 3.83 -5 5 1 172.41 10.36 -5 5 1 189.25 8.65 -5 5 1 183.52 8.83 5 -5 -1 182.98 9.96 -5 5 1 175.85 8.64 -5 5 1 192.92 7.53 5 -5 -1 192.26 10.06 5 -5 -1 183.90 9.25 5 -5 -1 179.73 9.76 -5 5 1 162.66 10.27 -5 5 1 194.49 8.62 -5 5 0 16.71 3.78 -5 5 0 13.53 2.46 5 -5 0 12.90 2.86 -5 5 0 12.34 2.62 5 -5 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5.02 5 10 -6 27.36 5.09 5 10 -6 34.72 5.97 5 10 -5 -0.64 3.42 5 10 -5 0.63 3.26 5 10 -5 -1.16 2.83 5 10 -5 2.05 3.07 5 10 -4 8.84 3.33 5 10 -4 11.51 3.76 5 10 -4 4.85 3.05 5 10 -4 8.15 3.34 5 10 -3 70.74 6.40 5 10 -3 85.51 6.90 5 10 -3 96.11 6.88 5 10 -3 96.75 7.51 5 10 -2 54.45 4.77 5 10 -2 44.28 4.76 5 10 -2 53.14 5.33 5 10 -2 54.36 5.16 5 10 -2 48.51 5.02 5 10 -2 50.15 5.04 5 10 -2 50.37 5.24 5 10 -2 50.56 5.67 5 10 -1 52.71 4.98 5 10 -1 55.90 5.55 5 10 -1 49.21 4.87 5 10 -1 47.33 4.93 5 10 -1 47.14 4.16 5 10 -1 50.02 4.45 5 10 -1 43.50 4.01 5 10 -1 37.60 4.39 5 10 -1 54.52 4.22 5 10 -1 50.51 4.78 5 10 -1 47.25 4.89 5 10 0 18.52 3.55 5 10 0 21.72 3.17 5 10 0 28.16 3.56 5 10 0 18.56 3.50 5 10 0 19.92 3.33 5 10 0 29.85 3.86 5 10 0 23.78 3.33 5 10 0 16.65 3.02 5 10 0 26.39 3.41 5 10 0 27.92 3.55 5 10 0 29.48 4.13 5 10 0 23.87 3.47 5 10 1 27.31 3.70 5 10 1 33.37 4.20 5 10 1 33.04 3.81 5 10 1 29.11 3.90 5 10 1 34.05 3.55 5 10 1 29.13 3.69 5 10 1 30.94 3.33 5 10 1 32.30 4.03 5 10 1 26.48 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3.43 -6 9 5 17.55 4.88 -6 9 5 32.78 6.27 -6 9 5 20.86 3.93 -6 9 5 33.52 6.19 6 -9 -5 27.16 4.63 6 -9 -5 25.17 4.59 6 -9 -5 17.99 4.42 -6 9 5 18.30 5.20 6 -9 -5 25.79 4.71 6 -9 -5 31.44 5.28 -6 9 4 0.94 3.89 -6 9 4 -0.92 3.93 -6 9 4 -0.58 2.90 6 -9 -4 -0.69 2.94 -6 9 4 -1.84 3.67 6 -9 -4 0.59 2.99 6 -9 -4 -0.72 3.10 -6 9 4 3.61 3.60 6 -9 -4 -2.41 3.31 6 -9 -4 4.54 3.21 -6 9 3 38.75 6.79 -6 9 3 39.61 6.48 6 -9 -3 36.33 5.79 6 -9 -3 43.20 5.79 6 -9 -3 25.06 4.34 -6 9 3 32.38 5.95 6 -9 -3 38.81 5.08 -6 9 2 96.83 9.49 6 -9 -2 72.02 7.25 6 -9 -2 89.34 7.76 -6 9 2 85.34 8.81 6 -9 -2 85.72 6.76 6 -9 -2 84.97 6.73 6 -9 -2 86.00 8.22 -6 9 1 139.36 11.52 6 -9 -1 128.67 9.48 6 -9 -1 142.43 9.91 6 -9 -1 119.76 10.06 -6 9 1 143.93 11.12 -6 9 1 141.53 10.31 6 -9 -1 126.96 8.26 6 -9 -1 139.38 10.37 -6 9 0 122.48 10.80 -6 9 0 106.63 8.94 6 -9 0 104.11 8.52 -6 9 0 121.85 10.29 6 -9 0 89.32 8.00 6 -9 0 88.43 8.91 6 -9 0 90.29 8.63 -6 9 -1 1.56 3.86 6 -9 1 -2.07 3.36 6 -9 1 -0.66 3.03 6 -9 1 -0.83 3.67 -6 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6 30.72 5.65 -6 8 6 24.44 5.17 -6 8 6 20.21 3.96 -6 8 6 12.09 4.58 6 -8 -6 23.22 4.14 6 -8 -6 30.18 4.61 6 -8 -6 27.23 4.78 6 -8 -6 20.73 4.08 -6 8 5 36.76 6.31 -6 8 5 36.27 5.96 6 -8 -5 34.25 5.02 -6 8 5 28.58 5.44 -6 8 5 33.84 4.49 6 -8 -5 33.43 4.73 6 -8 -5 38.03 4.83 6 -8 -5 23.37 4.82 6 -8 -5 27.21 4.27 6 -8 -5 27.29 4.70 -6 8 4 -0.86 3.66 -6 8 4 -0.56 2.72 6 -8 -4 -0.67 2.78 6 -8 -4 3.23 2.63 -6 8 4 1.66 3.46 6 -8 -4 -0.56 2.48 -6 8 4 2.56 3.48 -6 8 4 -1.68 3.77 6 -8 -4 -1.74 2.99 6 -8 -4 0.70 3.01 6 -8 -4 -0.50 2.73 -6 8 3 18.19 4.73 -6 8 3 15.25 2.92 6 -8 -3 15.33 3.78 6 -8 -3 16.74 4.08 -6 8 3 17.78 4.79 6 -8 -3 15.45 3.66 6 -8 -3 20.06 3.53 -6 8 2 8.83 4.18 6 -8 -2 9.63 3.37 6 -8 -2 1.51 3.40 -6 8 2 4.55 2.43 -6 8 2 5.07 4.07 6 -8 -2 6.66 3.25 6 -8 -2 3.14 2.64 6 -8 -2 7.97 2.89 -6 8 1 153.18 11.76 6 -8 -1 162.58 10.42 6 -8 -1 179.90 11.60 -6 8 1 168.20 11.86 -6 8 1 140.07 8.31 6 -8 -1 148.00 9.95 6 -8 -1 161.96 9.14 6 -8 -1 156.88 10.73 -6 8 0 325.04 17.67 6 -8 0 334.23 15.93 6 -8 0 307.39 15.25 -6 8 0 383.97 16.99 6 -8 0 304.61 16.48 6 -8 0 328.28 16.65 6 -8 0 301.19 13.71 6 -8 0 313.99 16.26 -6 8 0 305.10 13.76 -6 8 0 351.57 17.41 -6 8 0 287.78 13.11 -6 8 -1 78.58 7.43 -6 8 -1 65.30 8.29 6 -8 1 72.26 7.11 6 -8 1 53.93 6.15 -6 8 -1 74.73 6.57 6 -8 1 65.91 7.38 6 -8 1 76.11 7.67 -6 8 -1 68.89 7.88 -6 8 -1 67.93 5.91 -6 8 -2 4.97 3.77 -6 8 -2 3.14 2.88 -6 8 -2 4.39 3.29 6 -8 2 3.28 3.16 6 -8 2 3.14 2.88 6 -8 2 0.80 3.65 -6 8 -2 7.06 4.31 -6 8 -3 47.35 7.40 6 -8 3 36.92 5.59 -6 8 -3 50.64 6.61 6 -8 3 36.99 5.78 -6 8 -3 34.93 6.44 -6 8 -4 73.66 9.27 -6 8 -4 73.15 9.17 6 -8 4 67.83 6.80 -6 8 -4 69.84 7.72 6 -8 4 64.86 8.20 6 -8 4 90.33 8.94 6 -8 4 60.69 7.34 -6 8 -4 61.40 8.09 -6 8 -5 23.21 6.34 6 -8 5 33.26 6.03 6 -8 5 26.85 6.02 -6 8 -6 28.47 7.12 6 -8 6 37.70 6.35 6 -8 6 44.37 7.09 6 -7 -13 1.88 3.20 6 -7 -12 21.00 4.45 6 -7 -12 15.40 4.39 -6 7 12 15.32 5.03 6 -7 -11 28.18 4.68 6 -7 -11 31.80 4.89 -6 7 11 26.18 4.98 6 -7 -11 32.00 5.38 6 -7 -11 24.99 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-3 102.42 5.77 6 3 -2 207.54 8.72 -6 -3 2 221.73 10.42 -6 -3 2 202.49 6.64 -6 -3 2 226.40 9.63 -6 -3 2 215.04 8.97 -6 -3 2 200.02 6.66 6 3 -2 214.68 10.54 -6 -3 2 204.69 9.62 6 3 -2 199.75 9.71 -6 -3 2 212.12 9.77 -6 -3 2 207.14 6.68 -6 -3 2 210.61 10.22 -6 -3 2 232.85 8.40 6 3 -2 212.22 9.80 -6 -3 2 233.79 10.87 6 3 -2 232.90 9.99 -6 -3 2 211.93 7.50 6 3 -2 212.97 6.98 6 3 -2 197.87 9.82 6 3 -2 220.03 9.54 6 3 -2 216.13 10.25 6 3 -2 205.99 9.95 6 3 -1 502.49 17.03 -6 -3 1 549.48 19.59 -6 -3 1 550.01 18.55 -6 -3 1 520.85 18.62 6 3 -1 521.16 18.94 -6 -3 1 532.51 18.70 -6 -3 1 527.88 17.10 -6 -3 1 514.46 19.30 -6 -3 1 506.12 16.59 6 3 -1 496.50 18.75 -6 -3 1 533.87 19.83 -6 -3 1 541.10 16.81 6 3 -1 514.16 16.81 6 3 -1 531.02 18.89 6 3 -1 526.07 18.18 6 3 -1 526.17 19.26 6 3 0 1831.46 55.10 -6 -3 0 1905.11 58.34 -6 -3 0 1950.15 57.18 -6 -3 0 1979.89 57.39 -6 -3 0 1898.01 54.55 -6 -3 0 1921.69 58.10 -6 -3 0 2030.06 59.01 -6 -3 0 1898.46 55.82 6 3 0 1950.67 56.04 6 3 0 1963.73 57.44 -6 -3 0 1938.84 55.37 6 3 0 1955.13 56.63 -6 -3 -1 1266.12 39.80 -6 -3 -1 1221.29 36.08 -6 -3 -1 1241.43 38.63 -6 -3 -1 1226.97 35.53 -6 -3 -1 1185.40 35.69 -6 -3 -1 1227.80 39.45 6 3 1 1275.73 36.01 -6 -3 -1 1332.92 40.33 -6 -3 -1 1228.55 37.71 6 3 1 1326.65 38.27 6 3 1 1297.31 38.76 -6 -3 -1 1295.49 36.39 6 3 1 1256.99 37.82 6 3 1 1288.70 38.55 6 3 1 1337.51 39.23 -6 -3 -1 1209.03 39.88 6 3 1 1291.26 36.06 6 3 1 1226.73 36.04 -6 -3 -2 161.94 6.53 6 3 2 156.68 6.43 -6 -3 -2 144.44 7.40 6 3 2 153.94 8.27 -6 -3 -2 174.27 8.20 -6 -3 -2 162.86 6.28 -6 -3 -2 146.99 8.12 6 3 2 155.65 8.22 -6 -3 -2 167.37 8.79 -6 -3 -2 156.78 7.35 6 3 2 153.96 7.63 6 3 2 165.84 7.80 6 3 2 148.57 6.86 -6 -3 -2 154.39 5.56 6 3 2 161.52 7.63 6 3 2 164.62 7.90 -6 -3 -2 145.77 8.47 -6 -3 -2 146.48 8.19 -6 -3 -3 49.11 3.47 -6 -3 -3 45.91 4.02 6 3 3 46.89 4.25 6 3 3 43.99 2.14 -6 -3 -3 42.93 3.15 6 3 3 42.07 2.12 -6 -3 -3 40.33 4.08 -6 -3 -3 43.50 3.70 6 3 3 54.17 4.57 6 3 3 45.65 3.81 6 3 3 46.95 4.00 6 3 3 42.53 3.34 -6 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1.40 7 7 2 4.36 1.31 -7 -7 -2 2.25 2.48 7 7 2 -0.53 2.28 -7 -7 -2 3.27 2.20 7 7 2 0.52 2.25 -7 -7 -2 6.28 2.48 7 7 2 0.46 2.33 7 7 2 3.09 1.14 7 7 2 2.66 1.94 7 7 2 1.45 1.76 7 7 2 4.06 1.70 -7 -7 -3 133.21 7.99 7 7 3 127.84 6.23 -7 -7 -3 119.14 8.54 7 7 3 134.99 8.53 -7 -7 -3 132.18 6.46 -7 -7 -3 128.83 6.45 7 7 3 132.56 6.06 -7 -7 -3 120.95 7.50 -7 -7 -3 139.55 8.07 7 7 3 120.03 8.26 7 7 3 122.68 6.22 -7 -7 -3 130.80 8.67 7 7 3 147.28 8.01 7 7 3 132.59 6.19 7 7 3 134.61 7.69 -7 -7 -3 136.56 8.96 -7 -7 -4 74.74 5.88 7 7 4 59.67 4.45 -7 -7 -4 60.88 6.22 7 7 4 66.33 5.96 -7 -7 -4 69.19 4.25 -7 -7 -4 68.53 4.26 7 7 4 68.05 4.50 -7 -7 -4 71.06 5.56 -7 -7 -4 62.84 5.65 -7 -7 -4 68.74 6.23 7 7 4 77.16 6.00 7 7 4 66.57 5.16 -7 -7 -4 74.80 6.74 -7 -7 -5 63.72 5.62 7 7 5 67.69 4.99 -7 -7 -5 63.56 6.20 7 7 5 70.70 4.95 7 7 5 57.00 2.53 -7 -7 -5 79.87 5.90 -7 -7 -5 57.81 5.86 -7 -7 -5 92.07 7.13 7 7 5 73.15 6.04 7 7 5 83.94 5.57 -7 -7 -5 74.12 6.64 7 7 6 109.57 6.88 -7 -7 -6 115.33 8.36 7 7 6 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30.43 2.70 -7 -8 -2 39.62 4.22 -7 -8 -2 27.95 3.63 7 8 2 36.36 4.54 7 8 2 26.94 2.59 -7 -8 -2 24.22 4.17 7 8 2 25.88 3.66 7 8 2 24.62 3.40 -7 -8 -3 13.64 3.18 -7 -8 -3 12.54 2.07 7 8 3 15.18 3.52 -7 -8 -3 9.43 2.02 7 8 3 9.25 2.25 7 8 3 9.11 1.97 -7 -8 -3 8.18 2.58 -7 -8 -3 7.68 2.66 7 8 3 9.71 2.97 7 8 3 8.51 2.72 -7 -8 -3 16.30 3.58 7 8 3 11.30 2.94 -7 -8 -3 11.83 3.48 -7 -8 -4 73.20 5.82 7 8 4 72.05 6.37 7 8 4 74.41 5.06 -7 -8 -4 75.74 6.86 7 8 4 69.76 4.79 -7 -8 -4 67.93 6.01 -7 -8 -4 78.08 5.74 -7 -8 -4 62.76 6.06 7 8 4 74.30 6.10 7 8 4 68.79 5.31 -7 -8 -4 73.18 6.76 -7 -8 -5 125.66 7.74 7 8 5 127.32 7.27 -7 -8 -5 120.21 8.85 7 8 5 113.55 8.43 7 8 5 128.42 7.03 -7 -8 -5 122.46 7.46 -7 -8 -5 119.59 8.38 -7 -8 -5 129.14 8.74 7 8 5 128.20 8.28 7 8 5 127.35 7.10 -7 -8 -5 110.27 8.48 -7 -8 -6 274.70 12.14 7 8 6 247.80 11.34 -7 -8 -6 229.69 13.14 7 8 6 256.28 11.27 7 8 6 214.46 8.33 -7 -8 -6 251.87 11.38 -7 -8 -6 219.81 12.54 -7 -8 -6 260.75 13.09 7 8 6 231.97 12.32 7 8 6 256.03 10.69 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101.37 8.45 8 -7 -8 133.32 9.73 8 -7 -8 106.50 9.04 -8 7 8 126.36 9.08 8 -7 -8 105.82 9.02 8 -7 -8 135.58 10.52 -8 7 7 128.95 10.59 -8 7 7 133.71 9.60 8 -7 -7 120.87 9.46 8 -7 -7 122.80 9.40 -8 7 7 117.69 10.70 8 -7 -7 128.11 9.61 8 -7 -7 131.80 9.54 8 -7 -7 128.10 10.19 -8 7 6 31.15 5.93 -8 7 6 36.34 5.51 8 -7 -6 48.59 6.55 8 -7 -6 50.27 6.17 -8 7 6 50.14 6.62 -8 7 6 39.86 6.97 8 -7 -6 51.06 6.21 8 -7 -6 44.68 5.96 8 -7 -6 49.87 6.41 -8 7 5 3.56 3.55 -8 7 5 0.78 3.69 -8 7 5 0.66 3.29 8 -7 -5 1.43 3.48 -8 7 5 -0.76 3.44 -8 7 5 0.96 4.07 8 -7 -5 2.76 3.42 8 -7 -5 1.41 3.54 8 -7 -5 1.35 3.33 -8 7 4 69.00 8.07 -8 7 4 40.29 6.65 -8 7 4 54.50 6.51 -8 7 4 63.14 7.02 -8 7 4 55.35 7.55 8 -7 -4 63.51 6.52 8 -7 -4 70.14 6.80 8 -7 -4 51.41 6.32 -8 7 3 26.05 5.72 -8 7 3 44.17 6.39 -8 7 3 35.73 5.59 8 -7 -3 35.29 5.44 8 -7 -3 22.30 4.61 -8 7 3 36.28 4.67 -8 7 3 24.75 5.95 8 -7 -3 38.20 5.32 8 -7 -3 23.82 5.01 8 -7 -3 32.91 4.96 -8 7 2 4.56 4.11 -8 7 2 7.94 3.93 8 -7 -2 6.06 3.53 8 -7 -2 6.50 3.53 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5 20.62 3.82 -8 -5 5 21.42 4.02 8 5 -5 14.80 3.31 8 5 -5 8.61 2.76 -8 -5 5 19.45 3.79 8 5 -5 14.44 3.92 -8 -5 4 15.95 3.28 -8 -5 4 8.66 2.82 8 5 -4 12.35 2.04 -8 -5 4 16.38 3.70 -8 -5 4 14.90 3.67 8 5 -4 11.84 3.04 -8 -5 4 16.81 3.23 8 5 -4 10.57 3.33 -8 -5 3 5.48 2.45 -8 -5 3 6.13 2.78 8 5 -3 1.01 2.40 -8 -5 3 5.15 2.56 -8 -5 3 4.18 2.64 8 5 -3 8.60 2.95 -8 -5 3 7.69 2.38 8 5 -3 9.26 3.03 -8 -5 2 73.69 6.54 8 5 -2 79.59 6.87 -8 -5 2 79.70 5.24 -8 -5 2 84.04 6.21 8 5 -2 88.26 6.54 -8 -5 2 90.69 6.50 -8 -5 2 79.74 6.72 8 5 -2 89.36 6.51 8 5 -2 79.53 6.16 -8 -5 2 64.42 4.82 8 5 -2 72.82 5.56 -8 -5 1 154.39 9.52 8 5 -1 151.39 9.49 -8 -5 1 144.65 7.03 -8 -5 1 152.77 8.49 8 5 -1 150.79 8.92 -8 -5 1 136.59 8.21 -8 -5 1 135.69 8.85 8 5 -1 144.92 8.83 -8 -5 1 151.52 9.66 8 5 -1 155.76 8.42 -8 -5 1 144.79 6.87 8 5 -1 137.50 7.44 8 5 0 385.76 16.40 -8 -5 0 341.85 15.91 -8 -5 0 342.09 14.83 8 5 0 344.25 15.64 -8 -5 0 368.15 15.01 -8 -5 0 376.86 16.19 8 5 0 369.55 16.00 -8 -5 0 375.80 16.94 8 5 0 372.39 13.54 8 5 0 382.53 14.99 8 5 0 349.03 13.49 -8 -5 -1 58.51 5.50 -8 -5 -1 50.71 4.65 8 5 1 53.62 5.32 -8 -5 -1 49.71 4.61 -8 -5 -1 54.12 5.38 8 5 1 53.10 5.42 -8 -5 -1 41.65 5.27 8 5 1 60.34 4.54 8 5 1 55.94 4.78 8 5 1 53.22 4.01 -8 -5 -1 55.69 3.00 8 5 1 55.74 5.52 -8 -5 -2 16.90 3.55 -8 -5 -2 16.81 1.58 8 5 2 11.60 2.00 -8 -5 -2 12.53 2.72 -8 -5 -2 21.29 3.62 8 5 2 20.79 3.53 -8 -5 -2 21.54 4.09 8 5 2 14.93 1.51 8 5 2 16.93 3.02 8 5 2 18.75 2.96 8 5 2 13.79 2.28 8 5 2 17.94 1.61 -8 -5 -2 18.94 3.93 -8 -5 -3 79.06 6.60 -8 -5 -3 73.78 5.43 -8 -5 -3 66.12 5.93 8 5 3 73.10 4.16 -8 -5 -3 86.07 7.21 8 5 3 76.27 5.44 8 5 3 84.28 6.10 8 5 3 72.47 4.53 8 5 3 74.83 6.01 -8 -5 -3 78.86 6.75 -8 -5 -4 240.69 13.42 8 5 4 266.50 13.41 -8 -5 -4 278.73 11.76 -8 -5 -4 285.08 13.43 8 5 4 252.57 13.24 8 5 4 307.56 12.19 -8 -5 -4 277.30 14.22 8 5 4 257.14 12.47 8 5 4 250.73 12.22 -8 -5 -4 269.17 11.72 -8 -5 -4 245.83 13.46 -8 -5 -4 261.25 13.24 -8 -5 -5 258.80 10.99 8 5 5 268.10 13.14 -8 -5 -5 234.70 12.31 8 5 5 246.20 12.97 -8 -5 -5 250.07 13.49 8 5 5 195.28 11.32 8 5 5 260.99 11.83 -8 -5 -5 225.90 11.00 -8 -5 -5 209.65 12.52 -8 -5 -5 236.52 12.48 -8 -5 -6 68.35 5.22 8 5 6 68.95 6.46 8 5 6 67.25 3.43 -8 -5 -6 63.62 6.21 8 5 6 59.84 6.33 8 5 6 72.60 6.48 -8 -5 -6 63.26 5.40 -8 -5 -6 76.73 7.03 -8 -5 -6 74.29 6.56 -8 -5 -7 5.83 2.80 -8 -5 -7 3.55 3.25 8 5 7 2.06 1.63 -8 -5 -7 2.38 2.16 8 5 7 1.32 2.80 8 5 7 0.91 1.54 -8 -5 -7 -1.26 2.83 8 5 7 1.35 2.86 -8 -5 -7 3.69 3.20 8 5 7 3.27 2.78 -8 -5 -7 3.64 2.54 -8 -5 -8 -1.36 2.94 -8 -5 -8 2.23 3.51 8 5 8 1.20 1.82 -8 -5 -8 0.41 2.27 8 5 8 2.04 3.01 8 5 8 -0.60 1.79 -8 -5 -8 -1.98 2.80 8 5 8 0.70 2.96 -8 -5 -8 6.23 3.92 -8 -5 -8 3.42 2.60 -8 -5 -9 58.95 6.91 8 5 9 63.83 6.84 8 5 9 56.57 4.89 8 5 9 58.17 4.85 -8 -5 -9 76.40 7.17 8 5 9 85.99 7.46 -8 -5 -9 61.80 7.25 -8 -5 -9 60.33 6.34 -8 -5 -9 74.34 7.25 -8 -5 -10 147.20 10.69 8 5 10 154.65 10.45 8 5 10 136.27 8.18 8 5 10 156.19 8.55 -8 -5 -10 132.27 9.92 8 5 10 155.16 10.41 -8 -5 -10 168.29 11.84 8 5 10 160.16 10.96 -8 -5 -10 131.20 9.71 -8 -5 -10 159.37 10.76 -8 -5 -11 26.06 5.42 -8 -5 -11 33.73 5.95 8 5 11 21.25 4.00 8 5 11 27.15 5.19 -8 -5 -11 23.02 5.06 8 5 11 32.26 5.42 -8 -5 -11 30.33 5.99 8 5 11 31.72 5.63 -8 -5 -11 21.11 4.80 -8 -5 -12 10.50 4.66 8 5 12 11.88 4.30 8 5 12 18.23 4.62 -8 -5 -12 14.49 5.07 8 5 12 13.96 4.58 -8 -5 -13 0.90 4.71 8 5 13 15.21 4.57 -8 -5 -13 11.07 4.91 8 5 13 9.94 4.68 -8 -6 9 12.31 4.50 8 6 -9 16.29 4.96 -8 -6 8 21.00 4.60 -8 -6 8 23.14 4.80 8 6 -8 16.16 4.20 -8 -6 8 20.94 4.37 -8 -6 7 6.67 3.42 -8 -6 7 9.29 3.78 8 6 -7 4.87 3.43 -8 -6 7 3.10 3.17 8 6 -7 1.84 3.90 -8 -6 6 68.71 6.42 -8 -6 6 63.37 6.42 -8 -6 6 61.34 6.33 8 6 -6 58.43 5.30 -8 -6 6 61.01 6.13 8 6 -6 78.04 8.36 8 6 -6 63.38 6.30 -8 -6 5 44.11 4.98 -8 -6 5 38.49 4.93 -8 -6 5 51.77 5.65 8 6 -5 47.36 4.93 8 6 -5 48.68 4.90 -8 -6 5 40.49 4.69 8 6 -5 39.95 6.12 8 6 -5 40.64 5.20 -8 -6 4 103.53 6.96 -8 -6 4 103.36 7.44 -8 -6 4 105.57 7.60 8 6 -4 97.68 7.00 -8 -6 4 99.13 6.77 8 6 -4 116.26 7.68 8 6 -4 98.17 6.50 -8 -6 3 82.53 5.75 8 6 -3 88.17 7.60 -8 -6 3 96.92 6.90 8 6 -3 71.51 6.16 -8 -6 3 72.43 6.32 -8 -6 3 90.81 7.21 8 6 -3 81.23 6.38 8 6 -3 78.50 6.23 -8 -6 3 83.14 5.74 8 6 -3 86.60 5.50 -8 -6 2 29.94 4.36 -8 -6 2 16.44 2.80 -8 -6 2 22.13 3.52 8 6 -2 21.61 3.81 -8 -6 2 21.85 3.70 -8 -6 2 27.95 4.30 8 6 -2 25.74 3.94 8 6 -2 24.04 4.56 -8 -6 2 21.86 2.85 8 6 -2 25.27 3.61 -8 -6 1 118.84 8.28 8 6 -1 112.88 8.31 -8 -6 1 118.72 6.12 -8 -6 1 117.33 7.43 8 6 -1 115.68 7.75 -8 -6 1 108.16 7.20 -8 -6 1 111.16 7.89 8 6 -1 105.41 7.58 8 6 -1 130.95 7.32 -8 -6 1 119.93 5.99 8 6 0 195.61 10.79 -8 -6 0 164.37 10.03 -8 -6 0 202.57 9.71 8 6 0 181.36 10.24 -8 -6 0 191.47 9.54 -8 -6 0 176.30 10.25 -8 -6 0 186.34 8.61 8 6 0 186.68 10.28 -8 -6 0 188.75 11.12 8 6 0 182.28 8.11 8 6 0 190.91 9.20 -8 -6 -1 264.74 13.01 8 6 1 241.40 12.54 -8 -6 -1 266.51 11.53 -8 -6 -1 250.03 11.36 -8 -6 -1 273.29 12.88 8 6 1 252.01 12.76 -8 -6 -1 262.29 13.69 8 6 1 255.70 10.91 8 6 1 276.64 11.41 8 6 1 243.61 9.53 8 6 1 271.02 12.95 -8 -6 -2 25.27 4.25 -8 -6 -2 30.96 3.73 8 6 2 23.55 4.09 -8 -6 -2 30.13 3.55 -8 -6 -2 32.27 4.40 8 6 2 28.56 4.43 8 6 2 25.25 3.86 -8 -6 -2 21.97 4.21 8 6 2 22.11 1.65 8 6 2 27.22 3.51 8 6 2 34.40 2.69 8 6 2 29.31 3.46 -8 -6 -3 25.42 4.31 -8 -6 -3 17.17 2.97 -8 -6 -3 19.62 2.94 -8 -6 -3 21.04 3.69 8 6 3 25.94 3.77 -8 -6 -3 30.04 4.65 8 6 3 19.57 3.27 8 6 3 25.38 3.21 -8 -6 -3 22.53 4.10 -8 -6 -4 118.44 8.20 -8 -6 -4 109.26 8.54 -8 -6 -4 110.25 6.60 -8 -6 -4 124.01 8.26 8 6 4 118.30 6.75 -8 -6 -4 119.54 8.82 8 6 4 110.80 7.53 8 6 4 127.77 7.85 -8 -6 -4 131.63 9.11 -8 -6 -5 134.69 9.50 8 6 5 146.79 9.55 -8 -6 -5 135.20 7.15 -8 -6 -5 139.29 8.82 8 6 5 121.59 9.00 -8 -6 -5 135.77 9.54 8 6 5 134.05 8.59 8 6 5 145.97 8.23 -8 -6 -5 141.68 7.35 -8 -6 -5 128.11 9.43 -8 -6 -5 126.01 8.67 -8 -6 -6 118.73 9.09 8 6 6 119.82 8.72 -8 -6 -6 110.82 6.46 -8 -6 -6 114.28 8.08 8 6 6 107.44 8.48 8 6 6 129.23 8.67 -8 -6 -6 110.82 6.92 -8 -6 -6 126.16 9.21 -8 -6 -6 126.41 8.55 8 6 7 146.65 10.08 8 6 7 146.89 6.30 8 6 7 152.98 8.60 8 6 7 148.70 6.29 -8 -6 -7 169.17 10.03 8 6 7 166.85 10.70 -8 -6 -7 165.54 10.70 8 6 7 146.81 9.81 -8 -6 -7 164.14 8.82 -8 -6 -7 169.56 11.01 -8 -6 -7 158.31 10.03 -8 -6 -8 43.98 5.67 8 6 8 38.73 3.40 8 6 8 35.48 5.42 8 6 8 44.00 3.59 -8 -6 -8 42.69 5.56 -8 -6 -8 49.15 6.46 8 6 8 55.68 6.36 -8 -6 -9 6.88 2.86 8 6 9 3.29 2.19 8 6 9 4.39 3.29 -8 -6 -9 -1.98 3.31 -8 -6 -9 1.65 3.56 -8 -6 -10 23.81 4.91 -8 -6 -10 26.12 5.85 8 6 10 25.26 3.56 8 6 10 21.82 4.91 -8 -6 -10 15.22 4.44 -8 -6 -10 26.05 5.51 -8 -6 -11 56.70 7.03 -8 -6 -11 50.05 7.27 8 6 11 70.13 7.42 -8 -6 -11 48.54 6.72 -8 -6 -11 63.13 8.02 -8 -6 -12 41.79 6.43 -8 -6 -12 34.50 6.38 8 6 12 43.88 6.35 -8 -6 -12 49.84 6.71 -8 -6 -12 39.40 6.98 8 6 12 48.36 6.70 -8 -6 -13 7.49 4.77 8 6 13 1.62 4.07 -8 -6 -13 1.00 4.17 8 6 13 -0.91 3.95 -8 -7 8 10.31 3.84 8 7 -8 7.32 3.85 -8 -7 7 1.85 3.27 -8 -7 7 -1.90 3.23 8 7 -7 0.78 3.38 -8 -7 6 29.92 4.82 -8 -7 6 18.54 4.27 8 7 -6 22.26 4.24 -8 -7 6 26.57 4.53 8 7 -6 32.80 5.53 8 7 -6 34.77 6.29 -8 -7 5 35.19 4.72 -8 -7 5 49.75 5.71 8 7 -5 40.08 4.75 8 7 -5 38.81 4.46 -8 -7 5 45.62 5.18 8 7 -5 38.49 5.66 8 7 -5 34.11 6.02 8 7 -5 41.84 5.38 -8 -7 4 54.89 5.35 -8 -7 4 75.82 6.51 -8 -7 4 65.57 6.18 8 7 -4 59.09 5.41 8 7 -4 72.20 6.14 -8 -7 4 65.92 5.57 8 7 -4 70.65 6.87 8 7 -4 60.42 7.12 8 7 -4 58.80 5.32 -8 -7 3 42.43 4.27 -8 -7 3 42.61 5.03 8 7 -3 38.15 4.53 -8 -7 3 44.92 5.02 8 7 -3 45.78 4.96 8 7 -3 52.21 4.91 -8 -7 3 32.90 4.05 8 7 -3 35.72 5.28 8 7 -3 49.09 6.12 8 7 -3 45.37 4.13 -8 -7 2 13.52 2.68 -8 -7 2 16.92 3.46 8 7 -2 14.30 3.57 -8 -7 2 17.52 3.46 8 7 -2 13.27 2.46 -8 -7 2 12.91 3.65 8 7 -2 11.24 3.24 8 7 -2 10.10 3.77 -8 -7 2 16.37 2.66 8 7 -2 13.13 2.91 -8 -7 1 39.97 5.10 -8 -7 1 29.24 3.90 8 7 -1 31.27 4.39 -8 -7 1 31.18 3.94 -8 -7 1 41.83 5.07 8 7 -1 38.82 4.71 8 7 -1 33.91 2.60 8 7 -1 29.58 4.53 8 7 -1 23.40 3.42 -8 -7 0 279.25 13.50 8 7 0 261.11 13.46 8 7 0 271.18 13.11 -8 -7 0 275.28 12.15 -8 -7 0 288.33 12.30 -8 -7 0 282.27 13.35 8 7 0 273.28 13.29 -8 -7 0 274.05 14.07 8 7 0 261.80 10.57 8 7 0 282.18 11.52 -8 -7 -1 177.55 10.28 8 7 1 189.27 10.50 -8 -7 -1 177.10 8.95 -8 -7 -1 172.25 8.89 -8 -7 -1 188.69 8.99 -8 -7 -1 177.70 10.14 8 7 1 175.76 10.30 -8 -7 -1 175.31 10.78 8 7 1 178.00 8.55 8 7 1 180.34 8.57 8 7 1 190.35 10.43 -8 -7 -2 127.18 8.64 8 7 2 149.33 9.31 -8 -7 -2 136.13 7.40 -8 -7 -2 146.69 7.60 -8 -7 -2 138.43 8.67 -8 -7 -2 150.58 8.24 8 7 2 131.92 8.91 -8 -7 -2 146.19 9.71 8 7 2 136.50 7.16 8 7 2 158.25 8.10 8 7 2 144.78 8.72 -8 -7 -3 91.54 7.07 8 7 3 84.31 7.13 -8 -7 -3 91.31 5.59 -8 -7 -3 83.85 5.41 -8 -7 -3 83.62 6.62 -8 -7 -3 92.10 6.73 8 7 3 94.41 7.49 8 7 3 84.50 5.35 -8 -7 -3 91.44 7.53 8 7 3 84.49 6.26 8 7 3 81.21 6.41 -8 -7 -3 75.87 7.25 -8 -7 -4 29.84 4.11 -8 -7 -4 21.50 4.38 -8 -7 -4 24.32 2.99 8 7 4 19.68 4.13 -8 -7 -4 19.18 2.81 8 7 4 21.17 2.59 8 7 4 31.26 4.06 -8 -7 -4 26.98 4.15 -8 -7 -4 25.10 4.29 -8 -7 -4 33.10 4.95 8 7 4 26.88 3.91 -8 -7 -4 27.24 4.90 -8 -7 -5 56.15 5.83 -8 -7 -5 45.80 5.98 -8 -7 -5 45.35 3.79 -8 -7 -5 49.41 3.94 8 7 5 49.86 3.99 -8 -7 -5 46.77 5.10 -8 -7 -5 54.88 6.02 8 7 5 46.60 5.21 8 7 5 50.63 4.80 -8 -7 -5 41.75 5.66 -8 -7 -6 8.82 3.16 -8 -7 -6 6.68 3.73 8 7 6 10.99 3.65 8 7 6 5.69 2.69 8 7 6 6.44 2.37 -8 -7 -6 9.37 3.11 8 7 6 4.22 2.93 -8 -7 -6 5.77 3.42 8 7 6 4.33 2.93 -8 -7 -6 8.23 3.66 -8 -7 -7 110.18 9.15 8 7 7 127.83 9.45 8 7 7 115.54 7.41 -8 -7 -7 124.75 8.49 8 7 7 129.50 9.11 -8 -7 -7 108.60 8.92 -8 -7 -7 140.98 9.02 -8 -7 -8 139.94 10.60 8 7 8 167.24 10.94 8 7 8 154.31 9.05 -8 -7 -8 172.81 10.16 -8 -7 -8 157.02 10.96 8 7 8 150.37 10.39 -8 -7 -8 152.95 9.94 -8 -7 -9 7.90 3.63 8 7 9 2.29 3.32 8 7 9 5.07 3.07 -8 -7 -9 6.18 3.45 -8 -7 -9 10.66 4.30 8 7 9 13.71 4.15 -8 -7 -10 1.38 3.60 8 7 10 -0.79 3.54 8 7 10 3.12 3.27 -8 -7 -10 6.47 3.73 -8 -7 -10 -0.86 4.15 -8 -7 -11 26.57 5.14 8 7 11 20.19 4.79 -8 -7 -11 20.94 4.67 -8 -7 -11 25.77 5.62 -8 -7 -11 19.97 5.04 8 7 11 24.66 5.25 -8 -7 -12 74.62 8.36 8 7 12 69.93 7.85 -8 -7 -12 56.19 7.78 8 7 12 75.55 8.38 -8 -7 -13 25.24 5.99 -8 -7 -13 24.78 6.23 8 7 13 25.83 6.01 8 8 -7 4.74 3.73 8 8 -7 0.82 3.95 8 8 -6 5.80 3.65 -8 -8 6 14.27 3.82 8 8 -6 7.58 3.87 8 8 -5 20.32 4.75 8 8 -5 32.71 6.24 8 8 -4 166.18 11.60 -8 -8 4 169.74 10.07 8 8 -4 168.80 9.13 8 8 -4 168.65 10.84 -8 -8 3 57.28 5.78 8 8 -3 47.30 5.07 8 8 -3 61.25 6.54 -8 -8 2 12.25 3.08 8 8 -2 11.06 3.16 -8 -8 2 11.77 3.27 8 8 -2 12.57 3.24 8 8 -2 8.34 3.88 8 8 -2 13.19 2.74 -8 -8 1 21.66 3.62 8 8 -1 17.48 3.86 -8 -8 1 18.53 3.60 -8 -8 1 20.93 3.94 8 8 -1 18.59 3.87 8 8 -1 22.01 4.60 8 8 -1 20.92 3.00 8 8 0 105.72 8.04 8 8 0 104.02 7.55 -8 -8 0 110.59 6.86 -8 -8 0 99.84 6.58 -8 -8 0 102.38 7.47 8 8 0 110.03 7.75 8 8 0 103.78 5.60 8 8 0 102.37 5.72 -8 -8 -1 184.47 10.55 8 8 1 192.74 10.88 -8 -8 -1 187.41 9.25 -8 -8 -1 206.85 9.55 -8 -8 -1 193.15 10.57 8 8 1 197.72 11.06 -8 -8 -1 173.09 11.07 8 8 1 198.78 8.50 8 8 1 194.34 9.04 8 8 1 220.48 11.27 -8 -8 -2 211.54 11.07 8 8 2 198.79 11.18 -8 -8 -2 195.70 9.10 -8 -8 -2 203.00 9.25 -8 -8 -2 183.26 9.74 -8 -8 -2 203.16 10.61 8 8 2 209.81 11.55 8 8 2 190.82 8.43 -8 -8 -2 196.31 11.63 8 8 2 199.58 9.77 8 8 2 201.38 10.77 -8 -8 -3 130.92 8.44 8 8 3 115.03 5.68 8 8 3 116.22 8.48 -8 -8 -3 124.11 6.48 -8 -8 -3 114.47 6.33 8 8 3 116.13 5.43 -8 -8 -3 117.29 7.84 -8 -8 -3 133.47 8.17 8 8 3 111.96 8.42 -8 -8 -3 120.85 8.85 8 8 3 120.36 7.55 8 8 3 117.69 7.79 -8 -8 -4 2.20 2.60 8 8 4 0.66 3.10 8 8 4 2.36 1.77 8 8 4 2.89 1.77 -8 -8 -4 5.08 2.73 8 8 4 3.68 2.62 8 8 4 -0.67 2.84 -8 -8 -4 2.83 2.80 -8 -8 -4 6.80 2.89 8 8 4 2.64 2.66 -8 -8 -4 0.72 3.33 -8 -8 -5 3.33 2.59 -8 -8 -5 1.49 3.10 8 8 5 1.37 3.02 8 8 5 0.36 2.06 8 8 5 4.27 1.97 8 8 5 2.61 2.70 -8 -8 -5 4.09 2.85 8 8 5 2.10 2.91 -8 -8 -5 3.74 2.80 -8 -8 -5 6.28 2.90 8 8 5 5.81 3.04 -8 -8 -5 3.69 3.01 -8 -8 -6 70.23 6.21 8 8 6 69.24 5.56 -8 -8 -6 55.44 6.89 8 8 6 59.37 5.02 -8 -8 -6 59.23 5.69 -8 -8 -6 50.22 6.12 -8 -8 -6 67.15 7.04 8 8 6 63.18 6.40 8 8 6 67.69 5.53 -8 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7.37 4.29 -10 -3 -10 0.94 4.47 10 3 10 1.62 4.02 -10 -3 -11 27.35 6.01 -10 -3 -11 29.93 6.48 -10 -3 -11 8.57 4.85 10 3 11 20.94 5.86 10 3 11 25.25 5.71 -10 -4 9 79.89 7.95 -10 -4 8 52.64 6.68 -10 -4 8 55.85 6.63 10 4 -8 38.77 6.38 -10 -4 7 0.65 3.20 -10 -4 7 -0.74 3.38 10 4 -7 -2.46 3.68 10 4 -7 -0.83 4.29 -10 -4 6 4.20 3.26 -10 -4 6 1.40 2.98 -10 -4 6 0.72 3.70 10 4 -6 -0.62 2.90 10 4 -6 0.90 3.74 -10 -4 6 7.81 3.42 10 4 -6 1.59 3.25 10 4 -6 1.57 3.88 -10 -4 5 38.14 5.22 -10 -4 5 38.10 5.50 -10 -4 5 42.79 5.81 -10 -4 5 51.20 6.41 10 4 -5 42.04 5.63 10 4 -5 52.83 6.94 -10 -4 5 46.49 5.61 10 4 -5 44.26 6.24 10 4 -5 51.68 6.48 10 4 -4 330.98 16.48 -10 -4 4 272.49 13.11 -10 -4 4 292.88 14.76 10 4 -4 270.39 12.12 -10 -4 4 313.26 15.17 -10 -4 4 298.04 15.74 10 4 -4 263.23 14.19 10 4 -4 283.96 14.94 -10 -4 4 312.16 13.57 10 4 -3 276.44 15.19 -10 -4 3 305.75 15.37 -10 -4 3 275.95 12.72 -10 -4 3 307.22 14.63 10 4 -3 268.57 12.47 -10 -4 3 284.83 14.35 -10 -4 3 278.78 14.99 10 4 -3 303.07 14.80 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4 209.53 12.90 -10 -4 -4 234.04 13.95 10 4 4 217.59 11.68 10 4 4 210.89 9.65 10 4 4 223.55 12.18 10 4 4 221.35 12.11 -10 -4 -4 230.31 12.33 -10 -4 -4 214.63 13.25 10 4 4 202.49 9.62 -10 -4 -4 230.35 13.38 -10 -4 -5 2.37 3.21 -10 -4 -5 2.32 2.95 10 4 5 1.50 3.37 10 4 5 1.21 3.17 -10 -4 -5 1.57 3.26 10 4 5 1.53 3.18 -10 -4 -5 -0.86 3.67 10 4 5 2.03 2.26 10 4 5 -0.68 3.11 10 4 5 1.14 2.73 -10 -4 -5 4.93 3.63 -10 -4 -5 0.65 3.17 10 4 5 0.41 2.16 -10 -4 -6 137.03 9.09 10 4 6 141.29 10.21 -10 -4 -6 154.60 10.87 10 4 6 133.28 10.26 -10 -4 -6 127.61 10.61 10 4 6 133.97 8.27 10 4 6 129.33 9.75 -10 -4 -6 139.87 9.85 -10 -4 -6 110.75 10.05 10 4 6 145.47 8.57 -10 -4 -6 150.77 10.80 -10 -4 -7 151.85 11.29 -10 -4 -7 146.06 9.73 10 4 7 152.85 10.94 -10 -4 -7 161.19 11.48 10 4 7 181.70 11.69 10 4 7 135.21 9.08 10 4 7 160.69 11.19 -10 -4 -7 158.31 10.85 -10 -4 -7 165.44 11.87 10 4 7 169.95 9.95 -10 -4 -7 180.14 11.95 -10 -4 -8 91.65 8.97 10 4 8 95.93 8.71 -10 -4 -8 91.57 8.96 10 4 8 86.83 8.34 10 4 8 92.41 7.67 10 4 8 103.41 9.20 -10 -4 -8 102.19 8.97 -10 -4 -8 93.92 9.26 10 4 8 68.27 7.03 -10 -4 -8 93.99 9.23 -10 -4 -9 11.85 4.71 -10 -4 -9 3.48 3.99 10 4 9 7.93 3.93 -10 -4 -9 6.33 4.35 10 4 9 7.29 4.08 -10 -4 -9 12.98 5.37 10 4 9 6.82 3.85 -10 -4 -9 13.39 5.39 10 4 9 7.08 3.71 -10 -4 -10 1.78 4.34 10 4 10 0.79 3.64 -10 -4 -10 4.68 4.63 10 4 10 8.11 4.08 -10 -4 -10 9.36 5.15 10 4 10 5.21 3.95 10 4 10 3.87 4.05 -10 -4 -11 -0.91 4.68 -10 -4 -11 4.81 4.41 10 4 11 5.63 4.27 -10 -4 -11 4.30 4.48 10 4 11 4.72 4.09 10 4 11 7.52 4.32 -10 -5 8 44.25 6.44 10 5 -8 63.07 7.62 -10 -5 7 33.98 5.72 10 5 -7 43.72 6.48 10 5 -7 43.11 6.73 -10 -5 6 7.03 3.49 -10 -5 6 9.99 3.79 10 5 -6 8.94 3.36 10 5 -6 5.73 3.82 10 5 -6 4.52 3.45 -10 -5 5 2.70 3.25 -10 -5 5 8.24 3.96 -10 -5 5 5.42 3.66 10 5 -5 3.09 3.15 10 5 -5 10.39 4.24 10 5 -5 4.26 3.77 -10 -5 4 46.96 5.93 -10 -5 4 35.03 5.45 -10 -5 4 46.78 6.45 10 5 -4 40.76 5.51 10 5 -4 43.49 6.02 -10 -5 3 274.78 14.87 -10 -5 3 279.12 14.11 10 5 -3 273.58 12.13 -10 -5 3 278.05 14.24 -10 -5 3 287.70 15.23 10 5 -3 288.44 14.49 10 5 -3 302.98 14.61 -10 -5 2 93.64 8.18 -10 -5 2 121.75 8.44 10 5 -2 121.52 8.73 -10 -5 2 116.29 8.39 -10 -5 2 114.80 9.11 10 5 -2 100.79 8.32 10 5 -2 103.62 8.10 10 5 -2 104.76 9.01 -10 -5 1 43.50 5.89 -10 -5 1 58.56 5.93 -10 -5 1 62.80 6.12 10 5 -1 58.80 6.36 -10 -5 1 58.18 6.48 10 5 -1 53.16 6.14 10 5 -1 66.15 6.96 10 5 -1 62.05 6.21 -10 -5 0 6.49 3.36 -10 -5 0 10.80 3.42 10 5 0 6.89 3.21 -10 -5 0 3.44 2.89 -10 -5 0 6.42 3.84 10 5 0 14.59 4.18 10 5 0 4.12 3.36 -10 -5 0 7.19 4.02 10 5 0 5.47 3.36 -10 -5 -1 52.76 6.16 -10 -5 -1 43.29 5.17 10 5 1 62.60 6.49 -10 -5 -1 49.62 5.30 -10 -5 -1 56.33 6.29 10 5 1 38.43 5.67 10 5 1 48.13 5.79 -10 -5 -1 58.58 6.91 10 5 1 41.93 5.10 -10 -5 -2 24.04 4.99 -10 -5 -2 39.11 4.83 -10 -5 -2 32.24 5.20 10 5 2 29.25 4.94 -10 -5 -2 35.64 5.70 10 5 2 38.02 4.53 10 5 2 27.63 4.22 -10 -5 -3 48.81 6.30 -10 -5 -3 42.87 5.15 10 5 3 55.75 6.35 10 5 3 49.46 5.63 -10 -5 -3 47.24 6.14 10 5 3 52.22 6.54 -10 -5 -3 59.37 7.00 10 5 3 47.52 5.48 10 5 3 49.33 5.21 -10 -5 -4 36.95 5.68 -10 -5 -4 46.23 5.23 10 5 4 44.30 5.86 10 5 4 41.13 5.30 -10 -5 -4 46.68 6.06 10 5 4 35.98 5.68 10 5 4 50.34 5.39 -10 -5 -4 43.94 6.29 10 5 4 46.89 5.56 -10 -5 -5 44.93 6.35 -10 -5 -5 52.08 5.45 10 5 5 58.31 6.75 -10 -5 -5 61.59 7.08 10 5 5 40.01 6.00 10 5 5 60.07 4.83 -10 -5 -5 58.36 7.29 10 5 5 59.66 6.49 10 5 5 65.83 6.24 10 5 5 47.18 4.55 -10 -5 -6 8.79 4.19 -10 -5 -6 -0.53 2.96 10 5 6 7.85 4.00 -10 -5 -6 0.78 3.59 10 5 6 0.80 3.73 -10 -5 -6 2.71 3.91 10 5 6 4.82 2.71 10 5 6 2.15 3.33 10 5 6 7.66 2.84 -10 -5 -7 213.59 13.50 10 5 7 221.88 13.33 -10 -5 -7 215.40 13.34 10 5 7 221.18 13.46 10 5 7 194.40 10.84 -10 -5 -7 211.46 13.96 10 5 7 200.94 12.65 -10 -5 -7 219.91 13.47 -10 -5 -8 169.24 12.12 10 5 8 152.47 11.38 -10 -5 -8 173.59 12.04 10 5 8 161.03 11.69 10 5 8 162.94 10.09 10 5 8 186.69 12.19 -10 -5 -8 171.51 12.62 -10 -5 -8 182.26 12.46 -10 -5 -9 29.24 6.26 -10 -5 -9 24.60 5.95 10 5 9 36.34 6.21 -10 -5 -9 36.48 6.40 10 5 9 18.60 4.83 10 5 9 32.41 5.20 10 5 9 26.68 5.67 -10 -5 -9 32.29 6.27 -10 -5 -10 12.12 4.89 10 5 10 11.66 4.81 -10 -5 -10 5.38 4.71 10 5 10 18.73 5.12 -10 -5 -10 7.28 4.85 10 5 10 9.96 4.41 -10 -5 -11 9.23 4.57 10 5 11 3.40 3.82 -10 -5 -11 -2.16 4.85 -10 -6 7 45.83 6.34 -10 -6 6 66.27 7.15 10 6 -6 68.40 6.46 -10 -6 5 1.35 3.19 -10 -6 5 3.42 3.44 10 6 -5 -2.36 3.14 10 6 -5 2.73 4.50 10 6 -5 1.34 3.21 10 6 -4 112.73 9.79 -10 -6 4 89.26 7.73 -10 -6 4 105.01 8.37 -10 -6 4 91.09 8.29 10 6 -4 88.48 7.60 10 6 -4 106.33 8.14 -10 -6 3 0.62 3.33 -10 -6 3 1.88 2.97 -10 -6 3 2.96 3.39 10 6 -3 5.13 3.49 10 6 -3 3.26 3.92 10 6 -3 -0.59 3.17 -10 -6 2 15.47 4.34 -10 -6 2 21.37 4.21 10 6 -2 28.99 4.96 -10 -6 2 22.86 4.51 -10 -6 2 19.60 4.66 10 6 -2 33.05 5.04 10 6 -2 30.21 5.59 10 6 -2 30.21 4.73 -10 -6 1 108.37 8.74 -10 -6 1 117.02 8.02 10 6 -1 92.44 7.98 -10 -6 1 119.68 8.24 -10 -6 1 117.10 9.22 10 6 -1 117.69 8.76 10 6 -1 101.87 7.56 10 6 -1 95.52 8.64 -10 -6 0 31.05 5.17 -10 -6 0 22.49 3.87 10 6 0 24.23 4.71 -10 -6 0 24.37 4.07 -10 -6 0 24.03 4.92 10 6 0 21.67 4.64 10 6 0 21.74 4.66 -10 -6 0 23.50 5.05 10 6 0 19.35 3.80 -10 -6 -1 5.76 3.67 -10 -6 -1 1.59 2.51 10 6 1 2.84 2.95 -10 -6 -1 -0.53 2.52 -10 -6 -1 4.23 3.44 10 6 1 1.44 3.39 10 6 1 0.67 3.27 -10 -6 -1 0.81 3.46 10 6 1 0.81 2.19 10 6 1 3.45 2.65 -10 -6 -2 34.00 5.28 -10 -6 -2 33.84 4.48 10 6 2 32.72 5.27 -10 -6 -2 22.70 4.06 -10 -6 -2 31.03 5.19 10 6 2 35.99 5.19 10 6 2 20.68 4.47 -10 -6 -2 45.98 6.37 10 6 2 26.09 3.87 10 6 2 36.85 4.63 -10 -6 -3 70.18 7.15 -10 -6 -3 76.46 6.18 -10 -6 -3 54.05 5.44 -10 -6 -3 59.67 6.67 10 6 3 66.72 5.84 -10 -6 -3 64.17 7.35 10 6 3 68.76 6.18 10 6 3 79.42 6.94 -10 -6 -4 54.29 6.61 -10 -6 -4 66.87 5.88 10 6 4 53.58 6.73 -10 -6 -4 64.18 6.98 10 6 4 67.25 7.45 10 6 4 58.91 5.65 -10 -6 -4 67.40 7.60 10 6 4 38.75 5.24 10 6 4 65.15 6.52 -10 -6 -4 63.22 7.30 -10 -6 -5 2.28 3.29 10 6 5 -1.57 4.06 10 6 5 0.59 2.97 -10 -6 -5 4.42 3.70 10 6 5 1.61 3.34 -10 -6 -5 0.88 3.80 10 6 5 2.61 2.83 -10 -6 -5 2.60 3.29 -10 -6 -6 -1.56 3.81 10 6 6 0.81 3.36 -10 -6 -6 2.27 3.58 10 6 6 -1.65 3.29 -10 -6 -6 -1.81 3.85 10 6 6 -0.71 3.18 -10 -6 -6 -0.90 3.73 -10 -6 -7 2.41 3.48 -10 -6 -7 2.68 4.09 10 6 7 1.65 3.58 -10 -6 -7 3.89 3.56 10 6 7 -0.85 3.66 -10 -6 -7 -2.82 4.08 10 6 7 1.44 2.61 10 6 7 2.28 3.30 -10 -6 -8 48.99 6.85 -10 -6 -8 64.47 8.07 10 6 8 58.20 6.99 -10 -6 -8 55.43 6.91 10 6 8 60.50 7.38 -10 -6 -8 49.96 7.45 10 6 8 49.14 5.60 10 6 8 46.19 6.59 -10 -6 -9 31.74 6.07 -10 -6 -9 33.13 6.68 10 6 9 49.73 6.89 -10 -6 -9 34.83 6.12 10 6 9 53.59 7.28 10 6 9 44.58 5.70 10 6 9 40.27 6.32 -10 -6 -10 38.04 6.40 -10 -6 -10 36.91 7.02 -10 -6 -10 31.61 6.19 10 6 10 30.21 5.97 10 6 10 33.48 5.50 10 6 10 36.84 6.41 -10 -6 -11 2.97 4.61 -10 -6 -11 -0.88 4.02 10 6 11 -1.78 4.15 -10 -6 -11 -1.07 4.38 -10 -7 6 90.93 8.25 10 7 -6 73.75 8.05 -10 -7 5 23.15 4.81 10 7 -5 24.01 5.49 -10 -7 4 5.15 3.24 -10 -7 4 13.04 3.92 10 7 -4 5.95 3.28 10 7 -4 3.53 3.98 10 7 -4 8.11 3.78 -10 -7 3 63.83 6.52 -10 -7 3 75.74 6.90 -10 -7 3 87.40 8.01 10 7 -3 70.01 6.94 10 7 -3 68.62 7.81 -10 -7 2 33.87 4.86 10 7 -2 21.46 4.48 -10 -7 2 28.93 4.76 -10 -7 2 30.37 5.26 10 7 -2 30.65 4.82 10 7 -2 18.23 5.04 10 7 -2 19.40 3.99 -10 -7 1 72.78 7.22 -10 -7 1 67.28 6.33 10 7 -1 64.56 6.72 -10 -7 1 71.51 6.42 -10 -7 1 78.71 7.23 10 7 -1 69.76 6.93 10 7 -1 62.38 7.31 10 7 -1 69.21 6.12 -10 -7 0 57.57 6.60 -10 -7 0 58.99 5.90 10 7 0 65.20 6.97 -10 -7 0 62.59 5.91 -10 -7 0 62.13 6.87 10 7 0 81.96 7.48 10 7 0 67.19 5.75 10 7 0 67.65 7.05 -10 -7 -1 8.59 3.70 -10 -7 -1 11.13 3.22 10 7 1 7.15 3.55 -10 -7 -1 11.70 3.12 -10 -7 -1 6.92 3.77 10 7 1 4.34 3.48 10 7 1 4.08 3.37 -10 -7 -1 9.85 3.83 10 7 1 8.45 2.53 10 7 1 2.25 2.45 -10 -7 -2 -0.72 2.92 -10 -7 -2 6.28 2.93 10 7 2 5.15 3.64 -10 -7 -2 2.43 2.52 -10 -7 -2 1.38 2.93 10 7 2 4.54 3.44 10 7 2 8.97 3.60 -10 -7 -2 4.98 3.53 10 7 2 5.03 2.61 10 7 2 3.99 2.53 -10 -7 -3 88.63 8.17 10 7 3 96.27 8.46 -10 -7 -3 91.88 6.68 -10 -7 -3 84.65 6.55 -10 -7 -3 81.70 7.64 10 7 3 112.89 8.93 10 7 3 104.75 7.00 -10 -7 -3 107.66 9.26 10 7 3 104.52 7.43 10 7 3 119.25 8.39 -10 -7 -4 157.54 10.48 -10 -7 -4 151.60 10.27 -10 -7 -4 156.15 11.43 10 7 4 127.76 8.93 10 7 4 153.57 9.70 -10 -7 -4 147.38 11.02 -10 -7 -5 14.11 4.26 10 7 5 8.71 3.45 -10 -7 -5 21.30 4.58 -10 -7 -5 14.95 4.63 10 7 5 22.68 4.39 -10 -7 -5 25.68 5.29 -10 -7 -6 2.28 3.47 10 7 6 -0.83 3.59 -10 -7 -6 -2.17 3.43 10 7 6 3.39 4.08 -10 -7 -6 0.91 3.93 10 7 6 -0.71 3.23 -10 -7 -6 -0.91 3.96 -10 -7 -7 40.51 6.15 10 7 7 45.04 6.53 -10 -7 -7 48.31 6.49 10 7 7 40.09 6.31 -10 -7 -7 47.89 6.97 10 7 7 41.71 6.06 -10 -7 -7 43.51 6.92 -10 -7 -8 23.27 5.16 10 7 8 11.31 4.51 -10 -7 -8 14.51 4.02 10 7 8 9.82 4.24 -10 -7 -8 12.69 5.19 10 7 8 12.94 4.25 -10 -7 -8 11.76 4.87 -10 -7 -9 3.31 3.72 -10 -7 -9 9.80 4.86 10 7 9 12.43 4.47 -10 -7 -9 13.35 4.63 10 7 9 2.73 3.95 -10 -7 -9 1.01 4.48 10 7 9 17.12 5.14 -10 -7 -9 5.08 4.81 -10 -7 -10 61.20 7.65 -10 -7 -10 46.32 7.34 -10 -7 -10 78.26 8.07 10 7 10 57.25 7.70 10 7 10 56.64 7.58 -10 -7 -11 11.31 5.03 10 7 11 17.67 5.19 10 7 11 11.22 4.58 -10 -8 5 58.39 6.80 10 8 -5 60.79 7.30 -10 -8 4 8.40 3.52 10 8 -4 3.26 3.67 -10 -8 3 0.61 2.98 10 8 -3 2.41 3.03 10 8 -3 2.56 4.42 10 8 -3 -0.80 3.40 -10 -8 2 43.25 5.43 10 8 -2 45.88 5.82 -10 -8 2 41.89 5.43 -10 -8 2 50.28 6.38 10 8 -2 51.69 5.98 10 8 -2 47.64 6.52 -10 -8 1 106.76 8.00 10 8 -1 111.27 8.85 -10 -8 1 134.49 8.56 -10 -8 1 135.29 9.58 10 8 -1 124.64 9.32 10 8 -1 128.26 10.02 -10 -8 0 52.90 6.61 -10 -8 0 49.76 5.38 10 8 0 46.46 5.97 -10 -8 0 49.63 5.37 -10 -8 0 52.28 6.21 10 8 0 53.83 6.41 10 8 0 56.38 6.90 -10 -8 -1 38.24 5.58 10 8 1 50.33 6.31 -10 -8 -1 36.42 4.60 -10 -8 -1 38.60 5.52 10 8 1 38.58 5.83 10 8 1 23.26 4.83 -10 -8 -1 45.28 6.30 -10 -8 -2 2.12 3.39 10 8 2 0.74 3.40 -10 -8 -2 1.34 3.42 10 8 2 0.76 3.34 10 8 2 3.89 3.49 -10 -8 -2 3.32 3.46 10 8 2 2.21 2.66 10 8 2 3.53 2.47 -10 -8 -3 23.30 4.88 10 8 3 26.18 5.31 -10 -8 -3 23.46 4.67 10 8 3 18.51 4.46 10 8 3 26.72 5.25 -10 -8 -3 20.22 5.10 10 8 3 29.95 4.37 10 8 3 21.06 3.55 -10 -8 -4 101.06 8.53 10 8 4 100.32 8.99 -10 -8 -4 113.05 8.66 10 8 4 101.00 9.17 -10 -8 -4 110.62 9.72 10 8 4 98.10 7.73 10 8 4 100.51 7.99 -10 -8 -5 191.12 11.89 10 8 5 208.20 13.01 -10 -8 -5 189.37 11.50 -10 -8 -5 179.08 11.46 -10 -8 -5 191.80 12.85 10 8 5 175.82 11.07 10 8 5 203.19 11.04 -10 -8 -5 164.13 12.48 -10 -8 -6 49.19 6.40 10 8 6 57.03 5.96 -10 -8 -6 39.94 5.79 -10 -8 -6 52.99 6.68 -10 -8 -6 51.58 7.37 10 8 6 40.13 5.91 -10 -8 -6 38.10 6.73 -10 -8 -7 0.75 3.61 -10 -8 -7 1.91 4.15 10 8 7 4.37 4.07 -10 -8 -7 4.91 3.77 10 8 7 3.59 3.66 -10 -8 -7 7.33 4.48 -10 -8 -7 5.61 4.13 10 8 7 -2.27 3.87 -10 -8 -7 1.92 4.16 -10 -8 -8 9.22 3.97 -10 -8 -8 0.99 3.93 10 8 8 4.49 3.58 -10 -8 -8 5.74 3.91 10 8 8 7.37 4.22 -10 -8 -8 9.55 4.30 -10 -8 -8 7.75 4.51 10 8 8 10.52 4.24 -10 -8 -8 4.97 4.14 -10 -8 -9 21.29 5.04 10 8 9 15.06 4.96 -10 -8 -9 21.09 5.68 10 8 9 17.15 5.33 10 8 10 56.47 7.59 -10 -8 -10 50.98 8.18 10 8 10 46.82 7.27 -10 -8 -11 13.78 5.35 10 8 11 25.11 6.05 10 8 11 18.75 5.65 -10 -9 4 26.96 4.93 10 9 -4 24.39 5.44 -10 -9 3 17.62 4.34 10 9 -3 12.81 4.37 -10 -9 2 9.14 3.44 10 9 -2 8.62 3.36 10 9 -2 9.81 4.66 10 9 -2 12.61 4.35 10 9 -1 58.22 6.76 -10 -9 1 62.16 6.66 10 9 -1 76.19 7.10 10 9 -1 59.33 7.27 10 9 0 52.32 6.52 -10 -9 0 47.77 5.99 10 9 0 42.29 5.99 10 9 0 61.03 7.25 -10 -9 -1 50.20 6.19 10 9 1 38.15 5.70 -10 -9 -1 41.55 5.73 10 9 1 35.69 5.60 10 9 1 30.79 5.31 -10 -9 -2 11.75 4.01 10 9 2 19.49 4.53 -10 -9 -2 16.24 4.19 10 9 2 20.59 4.78 10 9 2 16.11 4.23 -10 -9 -2 17.33 5.12 -10 -9 -3 24.09 4.76 10 9 3 28.05 5.38 -10 -9 -3 27.00 5.08 10 9 3 28.61 4.71 10 9 3 19.90 5.15 -10 -9 -3 19.26 5.18 10 9 3 27.44 4.37 -10 -9 -4 60.68 6.89 10 9 4 68.86 7.72 -10 -9 -4 65.34 6.73 10 9 4 59.68 7.44 -10 -9 -4 67.36 7.74 10 9 4 67.30 6.45 10 9 4 70.01 6.71 -10 -9 -5 45.11 6.03 10 9 5 48.77 6.81 10 9 5 49.52 5.76 -10 -9 -5 43.68 5.78 10 9 5 42.17 6.70 -10 -9 -5 45.32 6.82 10 9 5 47.84 6.02 -10 -9 -5 36.49 6.74 -10 -9 -6 106.86 8.87 10 9 6 87.02 8.94 -10 -9 -6 101.55 8.33 -10 -9 -6 111.85 9.41 10 9 6 109.77 9.66 -10 -9 -6 86.07 9.15 10 9 6 97.45 8.51 10 9 6 115.82 8.14 -10 -9 -6 90.28 9.25 -10 -9 -7 45.14 7.45 -10 -9 -7 54.59 7.03 -10 -9 -7 48.02 7.33 10 9 7 64.00 7.20 -10 -9 -7 43.67 6.94 -10 -9 -8 -3.03 4.55 10 9 8 3.79 4.03 -10 -9 -8 -1.74 3.91 -10 -9 -8 -1.91 4.29 10 9 8 1.63 3.72 -10 -9 -9 1.04 4.05 10 9 9 5.83 4.29 -10 -9 -9 7.91 4.82 10 9 9 0.86 3.80 -10 -9 -10 30.90 6.59 10 9 10 30.66 6.30 -10 -9 -10 38.79 7.16 10 9 10 36.17 6.45 10 10 -3 3.95 3.91 10 10 -2 -0.78 3.74 10 10 -1 32.36 5.28 10 10 -1 50.81 6.73 10 10 0 79.80 7.68 10 10 0 97.90 8.50 10 10 0 88.00 8.37 10 10 1 27.90 5.00 -10 -10 -1 31.20 5.14 10 10 1 28.88 5.16 10 10 1 27.10 5.01 10 10 2 9.01 4.04 -10 -10 -2 5.60 3.59 10 10 2 11.44 4.26 10 10 2 7.61 3.74 -10 -10 -3 1.33 3.38 10 10 3 4.71 4.11 10 10 3 -0.59 2.94 10 10 3 3.21 3.67 -10 -10 -3 -3.29 4.68 10 10 4 57.46 7.15 10 10 4 43.05 5.43 10 10 4 35.25 6.30 -10 -10 -4 46.06 6.90 10 10 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3.66 -12 -5 -3 2.69 4.04 12 5 3 -0.90 3.74 -12 -5 -3 4.99 4.24 12 5 3 -0.64 3.03 -12 -5 -4 27.72 5.88 12 5 4 40.47 6.50 12 5 4 21.10 5.13 -12 -5 -4 34.77 6.33 12 5 4 35.66 6.27 -12 -5 -4 36.71 6.48 12 5 4 29.72 5.19 -12 -5 -5 51.41 7.43 12 5 5 42.70 6.91 -12 -5 -5 47.12 7.55 -12 -5 -6 51.66 7.41 12 5 6 42.29 6.73 -12 -5 -6 33.40 7.18 -12 -5 -7 108.59 10.44 12 5 7 98.42 9.76 -12 -5 -7 99.73 10.72 12 5 7 78.24 8.72 -12 -5 -8 19.99 6.13 12 5 8 14.23 5.11 -12 -5 -8 13.66 5.65 12 5 8 7.32 4.55 12 6 -5 11.22 4.27 -12 -6 4 22.49 4.90 12 6 -4 27.97 5.49 -12 -6 3 17.60 4.52 -12 -6 3 21.59 5.32 12 6 -3 19.95 4.91 -12 -6 2 3.57 3.38 -12 -6 2 5.16 4.32 12 6 -2 1.59 3.76 12 6 -2 4.62 3.68 -12 -6 1 35.69 5.51 -12 -6 1 40.95 5.90 -12 -6 1 31.66 6.15 12 6 -1 31.92 5.63 12 6 -1 24.23 4.77 -12 -6 0 119.12 9.08 12 6 0 110.12 9.95 -12 -6 0 124.19 9.23 -12 -6 0 143.77 10.85 12 6 0 120.65 10.02 12 6 0 112.54 8.97 -12 -6 -1 175.05 12.32 -12 -6 -1 187.52 11.29 12 6 1 170.01 12.21 -12 -6 -1 158.20 10.66 -12 -6 -1 173.81 12.15 12 6 1 179.24 12.41 -12 -6 -1 181.58 13.05 12 6 1 178.53 10.84 12 6 1 156.50 11.54 -12 -6 -2 48.38 6.98 12 6 2 54.24 7.22 -12 -6 -2 41.35 5.63 12 6 2 56.86 7.16 -12 -6 -2 51.17 7.16 12 6 2 52.32 7.31 -12 -6 -2 60.21 7.89 12 6 2 42.15 5.72 -12 -6 -3 0.89 4.01 -12 -6 -3 2.53 3.04 12 6 3 -1.48 3.44 -12 -6 -3 -3.51 4.21 -12 -6 -3 5.02 4.44 12 6 3 -5.42 3.32 12 6 4 5.06 4.12 -12 -6 -4 0.89 4.14 12 6 4 4.64 3.78 -12 -6 -4 7.18 4.61 12 6 4 7.92 3.51 -12 -6 -5 6.34 4.15 12 6 5 17.98 5.40 -12 -6 -5 8.41 4.57 12 6 5 11.83 4.36 -12 -6 -6 10.16 4.97 12 6 6 11.54 4.77 -12 -6 -6 4.32 4.51 12 6 6 12.76 4.45 -12 -6 -7 83.85 9.23 12 6 7 73.97 8.77 -12 -6 -7 78.75 9.61 12 6 7 73.23 8.30 -12 -6 -8 60.49 8.07 12 6 8 54.86 7.89 12 6 8 61.10 7.95 12 7 -4 90.13 8.46 -12 -7 3 66.26 7.21 12 7 -3 50.53 6.84 -12 -7 2 2.76 3.71 -12 -7 2 7.63 4.83 12 7 -2 0.78 3.68 -12 -7 1 8.69 3.90 -12 -7 1 10.12 4.25 12 7 -1 9.69 4.24 -12 -7 0 1.29 3.20 -12 -7 0 -1.68 3.91 12 7 0 -0.84 3.63 -12 -7 -1 103.39 8.38 -12 -7 -1 116.81 10.20 12 7 1 111.55 9.97 -12 -7 -1 116.84 10.64 -12 -7 -2 67.56 7.90 12 7 2 68.64 8.14 -12 -7 -2 76.16 8.83 -12 -7 -3 48.56 7.08 12 7 3 35.72 6.48 -12 -7 -3 50.35 7.70 -12 -7 -4 6.89 4.20 -12 -7 -4 5.13 4.78 12 7 4 4.56 3.37 -12 -7 -5 8.72 4.44 12 7 5 0.96 3.84 -12 -7 -5 -1.05 4.89 12 7 5 0.72 3.61 -12 -7 -6 5.31 4.39 12 7 6 11.78 5.01 -12 -7 -6 9.71 5.11 12 7 6 9.35 4.54 -12 -7 -7 26.11 5.62 12 7 7 26.92 6.15 -12 -7 -7 27.65 6.75 -12 -7 -8 26.53 6.21 12 7 8 28.29 5.77 12 8 -2 22.60 5.31 -12 -8 1 1.65 3.90 12 8 -1 0.79 3.62 -12 -8 0 4.11 3.82 12 8 0 -4.13 3.85 -12 -8 -1 6.54 4.50 12 8 1 4.30 4.32 -12 -8 -2 33.52 5.77 12 8 2 18.71 5.30 -12 -8 -2 31.48 6.93 -12 -8 -3 73.03 8.10 12 8 3 47.85 7.40 -12 -8 -3 67.13 8.59 -12 -8 -4 77.68 8.41 12 8 4 71.12 8.59 -12 -8 -4 61.31 8.59 -12 -8 -5 10.00 4.43 -12 -8 -5 9.39 5.54 -12 -8 -6 0.84 3.98 -12 -8 -6 3.21 4.72 12 8 6 3.04 3.71 -12 -8 -7 21.30 5.32 12 8 7 36.03 6.07 12 9 -1 71.99 7.87 -12 -9 0 5.56 4.22 12 9 0 1.62 3.70 -12 -9 -1 53.65 6.97 12 9 1 34.78 6.19 -12 -9 -2 7.07 4.38 12 9 2 -0.89 3.83 -12 -9 -3 29.01 5.82 -12 -9 -3 25.67 6.49 -12 -9 -4 44.69 6.35 12 9 4 45.75 7.22 -12 -9 -4 51.39 7.86 12 9 5 15.72 5.23 -12 -9 -5 11.32 5.54 12 9 6 5.20 3.94 -13 1 -1 6.83 5.13 -13 1 -2 -1.76 4.66 13 0 -4 48.93 6.44 13 0 -3 13.80 4.53 -13 0 2 105.87 10.28 13 0 -1 73.85 8.55 -13 0 1 88.41 9.51 13 0 -1 94.04 9.14 13 0 0 50.57 7.51 -13 0 0 57.65 8.19 13 0 0 58.91 7.56 -13 0 0 64.34 8.22 13 0 1 23.97 5.88 -13 0 -1 19.70 5.38 13 0 1 18.36 4.90 -13 0 -1 11.72 5.28 13 0 2 -2.61 3.91 -13 0 -2 -0.93 4.38 -13 0 -3 5.69 4.90 13 1 -3 2.17 3.69 13 1 -2 1.54 3.94 -13 -1 2 9.73 4.58 -13 -1 2 6.50 4.80 13 1 -2 7.05 4.55 13 1 -1 47.33 7.16 -13 -1 1 64.24 8.25 13 1 -1 39.91 6.66 13 1 0 64.36 8.09 -13 -1 0 91.43 9.51 13 1 0 83.83 8.95 -13 -1 0 88.31 9.41 13 1 1 70.88 8.71 -13 -1 -1 72.73 8.97 13 1 1 83.98 8.81 -13 -1 -1 78.92 9.13 13 1 2 14.00 5.02 13 1 2 6.26 4.57 -13 -1 -2 13.47 5.55 13 1 3 -1.93 4.26 13 1 3 4.44 4.34 -13 -1 -3 -0.99 4.81 -13 -1 -4 7.07 4.78 13 2 -3 7.46 4.28 13 2 -2 4.39 3.89 -13 -2 2 3.45 3.88 -13 -2 2 7.45 4.48 13 2 -1 2.34 4.03 -13 -2 1 4.30 3.87 13 2 -1 11.59 4.48 13 2 0 37.20 6.58 13 2 0 39.57 6.59 -13 -2 0 55.18 7.88 13 2 1 20.00 5.72 13 2 1 22.66 5.43 -13 -2 -1 36.87 6.88 -13 -2 -2 21.98 6.15 13 2 2 20.04 5.28 -13 -2 -3 2.05 4.76 13 2 3 6.39 4.72 -13 -2 -3 -2.03 5.02 -13 -2 -4 10.48 5.13 13 2 4 12.75 4.91 -13 -2 -4 19.74 5.80 -13 -3 2 -2.52 3.77 13 3 -2 0.88 3.73 13 3 -1 7.43 3.85 -13 -3 1 13.33 4.91 -13 -3 1 11.30 4.67 13 3 0 33.33 5.98 -13 -3 0 35.67 6.28 -13 -3 0 28.66 6.08 13 3 0 26.26 5.66 -13 -3 0 29.31 6.43 -13 -3 -1 33.00 6.49 13 3 1 32.06 6.38 -13 -3 -1 25.85 6.43 -13 -3 -2 11.85 5.05 13 3 2 13.88 4.73 -13 -3 -3 2.02 4.11 13 3 3 10.26 4.76 -13 -3 -3 3.11 4.66 13 3 4 1.87 4.05 13 3 5 73.05 8.62 -13 -4 2 30.05 5.97 -13 -4 2 39.91 6.61 13 4 -2 31.33 5.89 13 4 -1 8.44 3.96 -13 -4 1 3.22 3.87 -13 -4 1 -0.94 4.35 13 4 -1 5.34 4.21 13 4 0 6.07 3.59 -13 -4 0 9.57 4.45 -13 -4 0 3.79 4.55 -13 -4 -1 45.10 6.53 -13 -4 -1 48.00 7.39 -13 -4 -1 39.51 7.30 -13 -4 -2 61.35 8.09 13 4 2 59.94 7.75 -13 -4 -2 50.61 8.29 -13 -4 -3 11.89 5.08 13 4 3 21.81 5.60 -13 -4 -3 24.26 6.72 -13 -4 -4 1.01 4.21 13 4 4 -2.87 4.38 -13 -4 -4 3.23 4.58 -13 -4 -5 26.85 6.43 13 4 5 28.86 6.22 -13 -5 2 46.40 6.70 -13 -5 1 17.83 4.96 -13 -5 1 23.15 5.54 13 5 -1 21.21 5.55 -13 -5 0 -1.53 3.84 -13 -5 0 2.80 4.35 13 5 0 -1.81 4.14 -13 -5 -1 13.59 4.63 -13 -5 -1 9.44 4.76 -13 -5 -2 20.11 5.10 -13 -5 -2 23.92 5.72 -13 -5 -3 76.36 7.91 -13 -5 -3 77.64 8.96 13 5 3 51.88 7.49 -13 -5 -4 16.78 5.45 13 5 4 16.56 5.44 -13 -5 -5 21.11 5.76 -13 -6 1 20.07 5.04 -13 -6 0 -2.91 3.76 -13 -6 0 -0.92 4.05 13 6 0 4.50 4.26 -13 -6 -1 16.66 5.75 13 6 1 29.58 6.21 -13 -6 -1 18.59 5.91 -13 -6 -2 29.93 6.41 13 6 2 29.36 6.44 -13 -6 -2 29.45 6.74 -13 -6 -3 53.00 7.62 -13 -6 -3 42.88 7.79 -13 -6 -4 30.69 6.41 13 6 4 23.66 5.79 -13 -7 -2 61.77 8.01 -13 -7 -3 113.65 10.42 0 0 0 0.00 0.00 TITL DP-18-new-final in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 8.023317 8.802786 9.650931 71.0762 86.2811 77.2794 ZERR 2.00 0.000120 0.000154 0.000135 0.0014 0.0012 0.0014 LATT 1 SFAC C H N O Cu UNIT 20.00 30.00 2.00 10.00 2.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 25276 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.219 _oxdiff_exptl_absorpt_empirical_full_min 0.880 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_Cu(pyalk)4(OAc)4_tetramer _database_code_depnum_ccdc_archive 'CCDC 2243591' loop_ _audit_author_name _audit_author_address 'Devi Prasad Adiyeri Saseendran' ;University of Zurich Switzerland ; _audit_update_record ; 2023-02-21 deposited with the CCDC. 2023-04-11 downloaded from the CCDC. ; # start Validation Reply Form _vrf_PLAT417_Cu(pyalk)4(OAc)4_tetramer ; PROBLEM: Short Inter D-H..H-D H3A ..H11A . 2.06 Ang. RESPONSE: The inter D-H ...H-D distance is short as a result of elongated N-H and O-H bonds due to presence of hydrogen bonding interactions. The H atoms were assigned by Q peaks associated with O and N atoms. ; _vrf_PLAT420_Cu(pyalk)4(OAc)4_tetramer ; PROBLEM: D-H Bond Without Acceptor O12A --H12A . Please Check RESPONSE: The Hydrogen atoms on O12 were fixed at calculated positions since they couldn't be identified from Q peaks. So hydrogen bonding interactions couldn't be precisely identified ; # Added during the CSD deposition process: Tuesday 21 February 2023 10:50 AM # end Validation Reply Form _audit_creation_date 2023-02-21 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _shelx_SHELXL_version_number 2018/3 _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C40 H52 Cu4 N4 O12), 4(C6 H16 N), 4(Cl O3.75), 6(H2 O)' _chemical_formula_sum 'C104 H180 Cl4 Cu8 N12 O45' _chemical_formula_weight 2968.71 _chemical_melting_point ? _chemical_oxdiff_formula 'C52 H92 Cl2 Cu4 N6 O24' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.15690(10) _cell_length_b 31.5203(3) _cell_length_c 11.78070(10) _cell_angle_alpha 90 _cell_angle_beta 97.8590(10) _cell_angle_gamma 90 _cell_volume 3368.31(6) _cell_formula_units_Z 1 _cell_measurement_reflns_used 21572 _cell_measurement_temperature 160.00(10) _cell_measurement_theta_max 73.0270 _cell_measurement_theta_min 4.8900 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 2.789 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.812 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.9b (Rigaku Oxford Diffraction, 2015) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour blue _exptl_crystal_density_diffrn 1.464 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description block _exptl_crystal_F_000 1548 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -3 -16 3 0.0334 5 1 -4 0.0448 4 -15 -2 0.0343 1 -20 1 0.0243 0 -20 -2 0.0285 2 -15 -5 0.0352 1 -7 -7 0.0353 -4 -15 -1 0.0348 -1 -4 -7 0.0369 -4 -13 -2 0.0357 4 12 -4 0.0428 -1 2 -7 0.0328 -5 -10 -2 0.0370 -2 4 -7 0.0339 -4 -1 -5 0.0345 0 16 -5 0.0343 -3 13 -4 0.0334 -1 17 -4 0.0328 1 20 -1 0.0322 -2 20 1 0.0409 1 11 6 0.0326 3 14 4 0.0289 2 12 6 0.0272 1 3 7 0.0288 2 4 7 0.0257 4 -2 4 0.0300 1 -9 6 0.0297 -3 -8 6 0.0319 -6 -5 3 0.0383 1 18 3 0.0311 _exptl_crystal_size_max 0.091 _exptl_crystal_size_mid 0.063 _exptl_crystal_size_min 0.063 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -3.0039 -15.9969 2.9992 0.1334 -0.2755 0.9377 5.0078 1.0006 -3.9920 0.2120 -0.4450 -0.7987 4.0062 -14.9943 -1.9902 0.4934 -0.8704 -0.1373 1.0011 -19.9925 1.0056 0.4820 -0.7274 0.4958 0.0049 -20.0030 -1.9913 0.0704 -0.9054 0.4471 2.0094 -15.0071 -4.9877 -0.0404 -1.0096 -0.0744 1.0109 -7.0158 -6.9883 -0.4609 -0.8111 -0.2913 -3.9989 -15.0102 -0.9967 -0.3878 -0.4878 0.8080 -0.9903 -4.0208 -6.9906 -0.7448 -0.6194 -0.1514 -3.9977 -13.0131 -1.9960 -0.5106 -0.4840 0.6992 4.0062 11.9970 -3.9961 -0.0550 0.0122 -0.9918 -0.9909 1.9784 -6.9924 -0.8238 -0.3911 -0.3176 -4.9985 -10.0158 -1.9976 -0.6723 -0.3310 0.7276 -1.9916 3.9759 -6.9937 -0.9724 -0.2762 -0.2615 -3.9948 -1.0227 -4.9960 -0.9580 -0.2443 0.2068 0.0053 15.9845 -4.9987 -0.6930 0.2473 -0.7100 -2.9972 12.9806 -4.0009 -0.9237 0.3218 -0.2391 -0.9966 16.9847 -4.0009 -0.7319 0.3964 -0.5728 0.9998 19.9971 -1.0043 -0.2376 0.6498 -0.7188 -2.0044 19.9956 0.9912 -0.4113 0.9107 -0.2775 0.9910 11.0172 5.9897 0.5562 0.8134 -0.0959 2.9944 14.0161 3.9926 0.5682 0.7054 -0.5087 1.9913 12.0194 5.9900 0.6652 0.8126 -0.2350 0.9904 3.0209 6.9909 0.7580 0.5813 0.1791 1.9908 4.0231 6.9912 0.8670 0.5806 0.0399 3.9965 -1.9796 3.9982 0.9011 0.0579 -0.1770 0.9930 -8.9803 5.9959 0.8195 0.0525 0.4580 -3.0089 -7.9897 5.9930 0.3175 0.2457 0.8763 -6.0064 -5.0052 2.9939 -0.3780 0.2594 0.9675 0.9944 18.0082 2.9913 0.1746 0.8628 -0.4499 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0373 _diffrn_reflns_av_unetI/netI 0.0231 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.978 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 39 _diffrn_reflns_limit_k_min -38 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 43173 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.978 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.569 _diffrn_reflns_theta_min 2.804 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 160.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_detector_type 'Pilatus 200K' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.978 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -54.00 20.00 0.50 10.26 -- 0.00 -75.00 45.00 148 2 \w -60.00 -15.00 0.50 10.26 -- -88.50 75.00 172.00 90 3 \w -145.00-114.00 0.50 10.26 -- -88.50 -75.00 45.00 62 4 \w -103.00 -69.00 0.50 10.26 -- -88.50 75.00 172.00 68 5 \w 58.00 83.00 0.50 10.26 -- 97.44 -75.00 45.00 50 6 \w 79.00 113.00 0.50 10.26 -- 97.44 75.00 172.00 68 7 \w -48.00 6.00 0.50 10.26 -- 0.00 -57.00 -90.00 108 8 \w 40.00 72.00 0.50 10.26 -- 0.00 37.00 150.00 64 9 \w -15.00 17.00 0.50 10.26 -- 0.00 37.00 150.00 64 10 \w -78.00 10.00 0.50 10.26 -- 0.00 -37.00-180.00 176 11 \w 16.00 41.00 0.50 10.26 -- 0.00 75.00 172.00 50 12 \w -104.00 -9.00 0.50 10.26 -- -88.50 30.00 150.00 190 13 \w -164.00 -81.00 0.50 10.26 -- -88.50-111.00 0.00 166 14 \w -145.00-114.00 0.50 10.26 -- -88.50 -30.00 90.00 62 15 \w -55.00 -11.00 0.50 10.26 -- -88.50 111.00 -90.00 88 16 \w -103.00 -73.00 0.50 10.26 -- -88.50 -30.00 90.00 60 17 \w -130.00 -78.00 0.50 10.26 -- -88.50 -45.00 -60.00 104 18 \w -83.00 -12.00 0.50 10.26 -- -88.50 111.00 -60.00 142 19 \w -87.00 -61.00 0.50 10.26 -- -88.50 45.00-180.00 52 20 \w -117.00 -91.00 0.50 10.26 -- -88.50 -94.00 150.00 52 21 \w 86.00 117.00 0.50 10.26 -- 97.44 61.00 -60.00 62 22 \w 73.00 143.00 0.50 10.26 -- 97.44 178.00 -30.00 140 23 \w 90.00 130.00 0.50 10.26 -- 97.44 45.00 -60.00 80 24 \w 130.00 176.00 0.50 10.26 -- 97.44 15.00 -30.00 92 25 \w 82.00 175.00 0.50 10.26 -- 97.44 30.00 -90.00 186 26 \w 59.00 107.00 0.50 10.26 -- 97.44-111.00 30.00 96 27 \w 24.00 50.00 0.50 10.26 -- 97.44-111.00 30.00 52 28 \w 39.00 109.00 0.50 10.26 -- 97.44-111.00 120.00 140 29 \w 84.00 170.00 0.50 10.26 -- 97.44 45.00-180.00 172 30 \w 113.00 162.00 0.50 10.26 -- 97.44 61.00 90.00 98 31 \w 83.00 108.00 0.50 10.26 -- 97.44 -45.00 -90.00 50 32 \w 21.00 96.00 0.50 10.26 -- 97.44 -45.00 0.00 150 33 \w 82.00 171.00 0.50 10.26 -- 97.44 30.00-120.00 178 34 \w 22.00 76.00 0.50 10.26 -- 97.44 -45.00 -90.00 108 35 \w 138.00 163.00 0.50 10.26 -- 97.44 61.00 -60.00 50 36 \w 80.00 107.00 0.50 10.26 -- 97.44 61.00 90.00 54 37 \w 48.00 73.00 0.50 10.26 -- 97.44 -75.00 45.00 50 38 \w 1.00 26.00 0.50 10.26 -- 0.00 75.00 172.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 200K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1221246000 _diffrn_orient_matrix_UB_12 -0.0131255000 _diffrn_orient_matrix_UB_13 0.0967976000 _diffrn_orient_matrix_UB_21 -0.0389083000 _diffrn_orient_matrix_UB_22 0.0380672000 _diffrn_orient_matrix_UB_23 0.0722146000 _diffrn_orient_matrix_UB_31 -0.1114068000 _diffrn_orient_matrix_UB_32 -0.0276936000 _diffrn_orient_matrix_UB_33 0.0533666000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 5758 _reflns_number_total 6646 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.9b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.9b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.9b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.894 _refine_diff_density_min -0.471 _refine_diff_density_rms 0.070 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.049 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 412 _refine_ls_number_reflns 6646 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0424 _refine_ls_R_factor_gt 0.0360 _refine_ls_restrained_S_all 1.049 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0644P)^2^+2.7649P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1072 _refine_ls_wR_factor_ref 0.1113 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H,H) groups 2. Others Fixed Sof: O8(0.75) O12A(0.5) H12A(0.5) H12B(0.5) 3.a Free rotating group: O11(H11A,H11B), O12A(H12A,H12B) 3.b Ternary CH refined with riding coordinates: N3(H3A) 3.c Secondary CH2 refined with riding coordinates: C25(H25A,H25B), C23(H23A,H23B), C21(H21A,H21B) 3.d Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C11(H11), C4(H4), C3(H3), C14(H14), C12(H12), C13(H13) 3.e Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C17(H17A,H17B,H17C), C10(H10A,H10B,H10C), C7(H7A,H7B, H7C), C20(H20A,H20B,H20C), C8(H8A,H8B,H8C), C22(H22A,H22B,H22C), C24(H24A,H24B, H24C), C26(H26A,H26B,H26C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.48168(3) 0.53407(2) 0.89195(3) 0.02156(10) Uani 1 1 d . . . . . Cu2 Cu 0.35937(4) 0.44833(2) 0.83761(3) 0.02290(10) Uani 1 1 d . . . . . Cl1 Cl 0.38479(8) 0.24510(3) 0.03503(7) 0.0529(2) Uani 1 1 d . . . . . O4 O 0.54789(17) 0.47421(5) 0.90548(13) 0.0224(3) Uani 1 1 d . . . . . O1 O 0.30520(17) 0.50789(5) 0.81955(14) 0.0261(3) Uani 1 1 d . . . . . O2 O 0.65953(17) 0.56208(5) 0.96449(13) 0.0244(3) Uani 1 1 d . . . . . O5 O 0.17541(19) 0.42017(5) 0.78244(14) 0.0299(4) Uani 1 1 d . . . . . O11 O 0.1957(2) 0.39261(6) 0.39573(15) 0.0352(4) Uani 1 1 d G . . . . H11A H 0.214744 0.406662 0.459771 0.053 Uiso 1 1 d G U . . . H11B H 0.235705 0.407743 0.346321 0.053 Uiso 1 1 d G U . . . O6 O 0.2522(2) 0.41900(6) 0.61253(15) 0.0379(4) Uani 1 1 d . . . . . O3 O 0.6972(2) 0.57752(7) 0.78829(15) 0.0398(4) Uani 1 1 d . . . . . N1 N 0.3683(2) 0.58677(6) 0.84458(16) 0.0246(4) Uani 1 1 d . . . . . N2 N 0.4899(2) 0.39742(6) 0.83827(16) 0.0272(4) Uani 1 1 d . . . . . N3 N 0.3837(2) 0.32666(7) 0.42811(18) 0.0332(5) Uani 1 1 d . . . . . H3A H 0.320612 0.352570 0.415116 0.040 Uiso 1 1 calc R U . . . O7 O 0.3407(3) 0.28810(8) 0.0445(2) 0.0654(7) Uani 1 1 d . . . . . C5 C 0.2451(3) 0.57928(7) 0.7717(2) 0.0250(5) Uani 1 1 d . . . . . C15 C 0.6343(3) 0.40762(8) 0.85050(19) 0.0267(5) Uani 1 1 d . . . . . O9 O 0.3109(3) 0.21814(9) 0.1068(3) 0.0691(7) Uani 1 1 d . . . . . C9 C 0.7314(3) 0.58127(8) 0.8930(2) 0.0277(5) Uani 1 1 d . . . . . C6 C 0.2182(3) 0.53285(7) 0.7369(2) 0.0267(5) Uani 1 1 d . . . . . C16 C 0.6666(3) 0.45513(7) 0.85500(19) 0.0247(5) Uani 1 1 d . . . . . C19 C 0.1598(3) 0.41012(8) 0.6768(2) 0.0294(5) Uani 1 1 d . . . . . C1 C 0.4040(3) 0.62671(7) 0.8775(2) 0.0272(5) Uani 1 1 d . . . . . H1 H 0.491906 0.631462 0.928881 0.033 Uiso 1 1 calc R U . . . C2 C 0.3178(3) 0.66090(8) 0.8395(2) 0.0322(5) Uani 1 1 d . . . . . H2 H 0.344487 0.688818 0.864699 0.039 Uiso 1 1 calc R U . . . C18 C 0.8129(3) 0.46517(8) 0.9270(2) 0.0314(5) Uani 1 1 d . . . . . H18A H 0.825316 0.496000 0.933308 0.047 Uiso 1 1 calc R U . . . H18B H 0.893443 0.453063 0.890507 0.047 Uiso 1 1 calc R U . . . H18C H 0.814535 0.452932 1.003619 0.047 Uiso 1 1 calc R U . . . C17 C 0.6636(3) 0.47098(8) 0.7313(2) 0.0316(5) Uani 1 1 d . . . . . H17A H 0.567160 0.464811 0.687400 0.047 Uiso 1 1 calc R U . . . H17B H 0.740759 0.456577 0.695807 0.047 Uiso 1 1 calc R U . . . H17C H 0.681064 0.501660 0.731775 0.047 Uiso 1 1 calc R U . . . C11 C 0.4490(3) 0.35664(8) 0.8331(2) 0.0326(5) Uani 1 1 d . . . . . H11 H 0.347026 0.349914 0.826432 0.039 Uiso 1 1 calc R U . . . C4 C 0.1541(3) 0.61252(8) 0.7292(2) 0.0310(5) Uani 1 1 d . . . . . H4 H 0.067379 0.607134 0.677226 0.037 Uiso 1 1 calc R U . . . C3 C 0.1913(3) 0.65368(8) 0.7635(2) 0.0346(6) Uani 1 1 d . . . . . H3 H 0.130187 0.676737 0.735040 0.041 Uiso 1 1 calc R U . . . C10 C 0.8566(3) 0.60915(9) 0.9438(3) 0.0387(6) Uani 1 1 d . . . . . H10A H 0.823524 0.638735 0.942638 0.058 Uiso 1 1 calc R U . . . H10B H 0.938625 0.606440 0.898903 0.058 Uiso 1 1 calc R U . . . H10C H 0.889296 0.600454 1.023099 0.058 Uiso 1 1 calc R U . . . C14 C 0.7413(3) 0.37609(8) 0.8539(2) 0.0350(6) Uani 1 1 d . . . . . H14 H 0.842781 0.383385 0.861107 0.042 Uiso 1 1 calc R U . . . O8 O 0.5391(3) 0.24319(10) 0.0695(4) 0.0724(11) Uani 0.75 1 d . . P . . C12 C 0.5502(3) 0.32403(8) 0.8371(2) 0.0391(6) Uani 1 1 d . . . . . H12 H 0.518478 0.295305 0.833393 0.047 Uiso 1 1 calc R U . . . C13 C 0.6979(3) 0.33388(9) 0.8465(2) 0.0413(7) Uani 1 1 d . . . . . H13 H 0.769421 0.311982 0.847960 0.050 Uiso 1 1 calc R U . . . C7 C 0.0558(3) 0.52100(9) 0.7339(3) 0.0406(7) Uani 1 1 d . . . . . H7A H 0.042444 0.490836 0.715108 0.061 Uiso 1 1 calc R U . . . H7B H -0.004276 0.538063 0.675613 0.061 Uiso 1 1 calc R U . . . H7C H 0.025199 0.526496 0.809055 0.061 Uiso 1 1 calc R U . . . C25 C 0.3428(3) 0.30645(10) 0.5336(2) 0.0410(6) Uani 1 1 d . . . . . H25A H 0.235089 0.301310 0.522456 0.049 Uiso 1 1 calc R U . . . H25B H 0.364741 0.326609 0.598166 0.049 Uiso 1 1 calc R U . . . C20 C 0.0208(3) 0.38676(11) 0.6323(2) 0.0430(7) Uani 1 1 d . . . . . H20A H 0.013927 0.360867 0.677290 0.064 Uiso 1 1 calc R U . . . H20B H 0.022205 0.379264 0.551718 0.064 Uiso 1 1 calc R U . . . H20C H -0.064556 0.404921 0.638820 0.064 Uiso 1 1 calc R U . . . C23 C 0.3489(3) 0.30034(11) 0.3214(3) 0.0461(7) Uani 1 1 d . . . . . H23A H 0.381293 0.315755 0.256023 0.055 Uiso 1 1 calc R U . . . H23B H 0.404833 0.273407 0.331278 0.055 Uiso 1 1 calc R U . . . C8 C 0.2687(4) 0.52717(9) 0.6187(2) 0.0408(6) Uani 1 1 d . . . . . H8A H 0.372304 0.535603 0.622747 0.061 Uiso 1 1 calc R U . . . H8B H 0.208050 0.544925 0.562440 0.061 Uiso 1 1 calc R U . . . H8C H 0.257985 0.497347 0.595497 0.061 Uiso 1 1 calc R U . . . O10 O 0.3510(5) 0.23269(13) -0.0817(3) 0.1158(15) Uani 1 1 d . . . . . C21 C 0.5400(3) 0.34212(10) 0.4376(3) 0.0412(6) Uani 1 1 d . . . . . H21A H 0.554278 0.356609 0.365423 0.049 Uiso 1 1 calc R U . . . H21B H 0.606974 0.317340 0.446696 0.049 Uiso 1 1 calc R U . . . C22 C 0.5822(3) 0.37207(11) 0.5359(3) 0.0468(7) Uani 1 1 d . . . . . H22A H 0.510587 0.395309 0.532045 0.070 Uiso 1 1 calc R U . . . H22B H 0.680565 0.383636 0.531433 0.070 Uiso 1 1 calc R U . . . H22C H 0.582940 0.356782 0.608466 0.070 Uiso 1 1 calc R U . . . C24 C 0.1875(4) 0.29061(12) 0.2947(3) 0.0560(9) Uani 1 1 d . . . . . H24A H 0.168798 0.275462 0.221519 0.084 Uiso 1 1 calc R U . . . H24B H 0.131256 0.317151 0.289475 0.084 Uiso 1 1 calc R U . . . H24C H 0.157133 0.272875 0.355649 0.084 Uiso 1 1 calc R U . . . C26 C 0.4197(4) 0.26551(12) 0.5661(4) 0.0639(10) Uani 1 1 d . . . . . H26A H 0.399155 0.245261 0.502788 0.096 Uiso 1 1 calc R U . . . H26B H 0.384147 0.253962 0.634527 0.096 Uiso 1 1 calc R U . . . H26C H 0.526143 0.270474 0.582181 0.096 Uiso 1 1 calc R U . . . O12A O 0.0792(7) 0.29856(18) -0.1738(6) 0.0843(19) Uani 0.5 1 d G . P A 2 H12A H 0.023594 0.276752 -0.164730 0.126 Uiso 0.5 1 d G U P A 2 H12B H 0.147567 0.288583 -0.210923 0.126 Uiso 0.5 1 d G U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.02091(18) 0.02196(18) 0.02121(18) 0.00259(12) 0.00075(12) 0.00070(12) Cu2 0.02360(18) 0.02293(18) 0.02188(18) -0.00028(12) 0.00207(13) -0.00048(12) Cl1 0.0435(4) 0.0532(4) 0.0656(5) -0.0235(4) 0.0207(4) -0.0128(3) O4 0.0223(8) 0.0237(8) 0.0217(8) 0.0000(6) 0.0050(6) 0.0026(6) O1 0.0246(8) 0.0241(8) 0.0277(8) 0.0037(6) -0.0035(6) 0.0008(6) O2 0.0236(8) 0.0270(8) 0.0224(8) 0.0025(6) 0.0025(6) -0.0012(6) O5 0.0296(9) 0.0335(9) 0.0264(9) -0.0030(7) 0.0024(7) -0.0028(7) O11 0.0353(10) 0.0435(10) 0.0268(9) 0.0029(8) 0.0043(7) -0.0032(8) O6 0.0356(10) 0.0486(11) 0.0305(9) -0.0036(8) 0.0077(8) -0.0085(8) O3 0.0440(11) 0.0517(12) 0.0253(9) 0.0026(8) 0.0103(8) -0.0075(9) N1 0.0253(10) 0.0267(10) 0.0220(9) 0.0031(7) 0.0035(7) 0.0008(8) N2 0.0355(11) 0.0258(10) 0.0206(9) -0.0010(8) 0.0046(8) 0.0021(8) N3 0.0283(11) 0.0378(12) 0.0335(11) -0.0028(9) 0.0046(9) -0.0009(9) O7 0.0764(18) 0.0558(15) 0.0659(16) -0.0027(12) 0.0159(13) 0.0084(13) C5 0.0231(11) 0.0274(12) 0.0250(11) 0.0052(9) 0.0051(9) -0.0002(9) C15 0.0330(12) 0.0294(12) 0.0186(10) 0.0004(9) 0.0064(9) 0.0045(10) O9 0.0569(15) 0.0637(16) 0.090(2) 0.0043(14) 0.0211(14) -0.0112(12) C9 0.0245(11) 0.0293(12) 0.0303(13) 0.0021(10) 0.0072(9) 0.0038(9) C6 0.0244(12) 0.0257(12) 0.0286(12) 0.0052(9) -0.0012(9) 0.0014(9) C16 0.0240(11) 0.0278(11) 0.0236(11) 0.0014(9) 0.0078(9) 0.0049(9) C19 0.0292(12) 0.0293(12) 0.0296(12) -0.0009(10) 0.0034(10) 0.0004(10) C1 0.0295(12) 0.0261(12) 0.0258(11) 0.0015(9) 0.0033(9) -0.0005(9) C2 0.0359(13) 0.0257(12) 0.0362(14) 0.0021(10) 0.0088(10) -0.0002(10) C18 0.0258(12) 0.0342(13) 0.0347(13) 0.0011(10) 0.0065(10) 0.0034(10) C17 0.0372(14) 0.0348(13) 0.0246(12) 0.0045(10) 0.0107(10) 0.0048(10) C11 0.0441(15) 0.0264(12) 0.0273(12) -0.0013(10) 0.0051(10) -0.0004(10) C4 0.0238(11) 0.0323(13) 0.0360(13) 0.0090(10) 0.0011(10) 0.0028(10) C3 0.0326(13) 0.0284(12) 0.0435(15) 0.0092(11) 0.0081(11) 0.0066(10) C10 0.0294(13) 0.0430(15) 0.0444(16) 0.0030(12) 0.0071(11) -0.0083(11) C14 0.0380(14) 0.0340(13) 0.0333(13) 0.0013(11) 0.0060(11) 0.0119(11) O8 0.0227(14) 0.0438(17) 0.153(4) -0.027(2) 0.0202(17) -0.0037(12) C12 0.0585(18) 0.0255(13) 0.0326(14) -0.0005(10) 0.0044(12) 0.0044(12) C13 0.0546(17) 0.0312(14) 0.0379(15) 0.0001(11) 0.0058(13) 0.0168(12) C7 0.0237(13) 0.0339(14) 0.0613(19) 0.0061(13) -0.0048(12) -0.0035(10) C25 0.0393(15) 0.0453(16) 0.0385(15) 0.0051(12) 0.0057(12) -0.0075(12) C20 0.0333(14) 0.0597(19) 0.0355(15) -0.0094(13) 0.0028(11) -0.0128(13) C23 0.0375(15) 0.0562(19) 0.0451(17) -0.0170(14) 0.0077(12) -0.0019(13) C8 0.0585(18) 0.0364(14) 0.0271(13) 0.0014(11) 0.0049(12) 0.0024(13) O10 0.163(4) 0.111(3) 0.081(2) -0.056(2) 0.044(2) -0.057(3) C21 0.0281(13) 0.0529(17) 0.0434(16) -0.0020(13) 0.0074(11) -0.0058(12) C22 0.0391(16) 0.0580(19) 0.0424(16) -0.0028(14) 0.0021(12) -0.0151(14) C24 0.0439(18) 0.064(2) 0.059(2) -0.0226(17) 0.0032(15) -0.0133(15) C26 0.065(2) 0.051(2) 0.071(2) 0.0176(18) -0.0089(18) -0.0008(17) O12A 0.085(4) 0.055(3) 0.098(5) 0.023(3) -0.040(3) -0.010(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O4 1.9814(16) . ? Cu1 O1 1.9086(16) . ? Cu1 O2 1.9446(16) . ? Cu1 N1 1.998(2) . ? Cu2 O4 1.9768(16) . ? Cu2 O1 1.9462(16) . ? Cu2 O2 2.3840(16) 3_667 ? Cu2 O5 1.9361(17) . ? Cu2 N2 2.000(2) . ? Cl1 O7 1.423(3) . ? Cl1 O9 1.432(3) . ? Cl1 O8 1.417(3) . ? Cl1 O10 1.423(3) . ? O4 C16 1.440(3) . ? O1 C6 1.410(3) . ? O2 C9 1.288(3) . ? O5 C19 1.273(3) . ? O11 H11A 0.8716 . ? O11 H11B 0.8710 . ? O6 C19 1.242(3) . ? O3 C9 1.236(3) . ? N1 C5 1.342(3) . ? N1 C1 1.345(3) . ? N2 C15 1.349(3) . ? N2 C11 1.338(3) . ? N3 H3A 1.0000 . ? N3 C25 1.490(3) . ? N3 C23 1.503(3) . ? N3 C21 1.501(3) . ? C5 C6 1.531(3) . ? C5 C4 1.388(3) . ? C15 C16 1.526(3) . ? C15 C14 1.392(3) . ? C9 C10 1.503(4) . ? C6 C7 1.529(3) . ? C6 C8 1.537(4) . ? C16 C18 1.518(3) . ? C16 C17 1.538(3) . ? C19 C20 1.502(4) . ? C1 H1 0.9500 . ? C1 C2 1.375(3) . ? C2 H2 0.9500 . ? C2 C3 1.382(4) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C11 H11 0.9500 . ? C11 C12 1.380(4) . ? C4 H4 0.9500 . ? C4 C3 1.387(4) . ? C3 H3 0.9500 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C14 H14 0.9500 . ? C14 C13 1.388(4) . ? C12 H12 0.9500 . ? C12 C13 1.378(4) . ? C13 H13 0.9500 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25 C26 1.495(5) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.500(4) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.503(4) . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? O12A H12A 0.8704 . ? O12A H12B 0.8700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Cu1 N1 162.92(8) . . ? O1 Cu1 O4 81.69(7) . . ? O1 Cu1 O2 178.60(7) . . ? O1 Cu1 N1 81.87(7) . . ? O2 Cu1 O4 99.69(7) . . ? O2 Cu1 N1 96.73(7) . . ? O4 Cu2 O2 80.64(6) . 3_667 ? O4 Cu2 N2 80.87(8) . . ? O1 Cu2 O4 80.88(7) . . ? O1 Cu2 O2 100.84(6) . 3_667 ? O1 Cu2 N2 156.58(8) . . ? O5 Cu2 O4 175.28(7) . . ? O5 Cu2 O1 102.04(7) . . ? O5 Cu2 O2 95.11(6) . 3_667 ? O5 Cu2 N2 97.20(8) . . ? N2 Cu2 O2 90.51(7) . 3_667 ? O7 Cl1 O9 110.88(16) . . ? O8 Cl1 O7 107.49(17) . . ? O8 Cl1 O9 109.8(2) . . ? O8 Cl1 O10 110.0(3) . . ? O10 Cl1 O7 108.1(2) . . ? O10 Cl1 O9 110.5(2) . . ? Cu2 O4 Cu1 96.88(7) . . ? C16 O4 Cu1 127.20(13) . . ? C16 O4 Cu2 109.10(13) . . ? Cu1 O1 Cu2 100.40(7) . . ? C6 O1 Cu1 115.54(14) . . ? C6 O1 Cu2 136.46(15) . . ? Cu1 O2 Cu2 101.47(6) . 3_667 ? C9 O2 Cu1 113.43(15) . . ? C9 O2 Cu2 144.68(15) . 3_667 ? C19 O5 Cu2 114.73(15) . . ? H11A O11 H11B 104.3 . . ? C5 N1 Cu1 113.06(16) . . ? C5 N1 C1 120.0(2) . . ? C1 N1 Cu1 126.95(16) . . ? C15 N2 Cu2 112.67(16) . . ? C11 N2 Cu2 127.39(18) . . ? C11 N2 C15 119.9(2) . . ? C25 N3 H3A 105.7 . . ? C25 N3 C23 114.4(2) . . ? C25 N3 C21 115.0(2) . . ? C23 N3 H3A 105.7 . . ? C21 N3 H3A 105.7 . . ? C21 N3 C23 109.4(2) . . ? N1 C5 C6 115.5(2) . . ? N1 C5 C4 120.5(2) . . ? C4 C5 C6 123.9(2) . . ? N2 C15 C16 114.8(2) . . ? N2 C15 C14 120.6(2) . . ? C14 C15 C16 124.6(2) . . ? O2 C9 C10 116.4(2) . . ? O3 C9 O2 121.7(2) . . ? O3 C9 C10 121.9(2) . . ? O1 C6 C5 107.06(19) . . ? O1 C6 C7 109.6(2) . . ? O1 C6 C8 110.4(2) . . ? C5 C6 C8 107.3(2) . . ? C7 C6 C5 111.1(2) . . ? C7 C6 C8 111.3(2) . . ? O4 C16 C15 105.70(18) . . ? O4 C16 C18 109.92(19) . . ? O4 C16 C17 109.83(18) . . ? C15 C16 C17 107.93(19) . . ? C18 C16 C15 112.10(19) . . ? C18 C16 C17 111.2(2) . . ? O5 C19 C20 116.1(2) . . ? O6 C19 O5 123.0(2) . . ? O6 C19 C20 120.9(2) . . ? N1 C1 H1 118.9 . . ? N1 C1 C2 122.2(2) . . ? C2 C1 H1 118.9 . . ? C1 C2 H2 120.8 . . ? C1 C2 C3 118.4(2) . . ? C3 C2 H2 120.8 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N2 C11 H11 118.9 . . ? N2 C11 C12 122.1(3) . . ? C12 C11 H11 118.9 . . ? C5 C4 H4 120.3 . . ? C3 C4 C5 119.3(2) . . ? C3 C4 H4 120.3 . . ? C2 C3 C4 119.5(2) . . ? C2 C3 H3 120.2 . . ? C4 C3 H3 120.2 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C15 C14 H14 120.4 . . ? C13 C14 C15 119.2(3) . . ? C13 C14 H14 120.4 . . ? C11 C12 H12 120.6 . . ? C13 C12 C11 118.8(3) . . ? C13 C12 H12 120.6 . . ? C14 C13 H13 120.3 . . ? C12 C13 C14 119.4(3) . . ? C12 C13 H13 120.3 . . ? C6 C7 H7A 109.5 . . ? C6 C7 H7B 109.5 . . ? C6 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? N3 C25 H25A 108.6 . . ? N3 C25 H25B 108.6 . . ? N3 C25 C26 114.8(3) . . ? H25A C25 H25B 107.6 . . ? C26 C25 H25A 108.6 . . ? C26 C25 H25B 108.6 . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N3 C23 H23A 109.2 . . ? N3 C23 H23B 109.2 . . ? H23A C23 H23B 107.9 . . ? C24 C23 N3 112.2(2) . . ? C24 C23 H23A 109.2 . . ? C24 C23 H23B 109.2 . . ? C6 C8 H8A 109.5 . . ? C6 C8 H8B 109.5 . . ? C6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N3 C21 H21A 108.8 . . ? N3 C21 H21B 108.8 . . ? N3 C21 C22 113.8(2) . . ? H21A C21 H21B 107.7 . . ? C22 C21 H21A 108.8 . . ? C22 C21 H21B 108.8 . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? H12A O12A H12B 104.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 O4 C16 C15 -158.25(14) . . . . ? Cu1 O4 C16 C18 80.6(2) . . . . ? Cu1 O4 C16 C17 -42.1(3) . . . . ? Cu1 O1 C6 C5 -28.9(2) . . . . ? Cu1 O1 C6 C7 -149.55(18) . . . . ? Cu1 O1 C6 C8 87.5(2) . . . . ? Cu1 O2 C9 O3 -7.8(3) . . . . ? Cu1 O2 C9 C10 170.87(17) . . . . ? Cu1 N1 C5 C6 -1.7(2) . . . . ? Cu1 N1 C5 C4 -179.28(18) . . . . ? Cu1 N1 C1 C2 179.91(18) . . . . ? Cu2 O4 C16 C15 -43.29(19) . . . . ? Cu2 O4 C16 C18 -164.46(15) . . . . ? Cu2 O4 C16 C17 72.9(2) . . . . ? Cu2 O1 C6 C5 -171.46(15) . . . . ? Cu2 O1 C6 C7 67.9(3) . . . . ? Cu2 O1 C6 C8 -55.0(3) . . . . ? Cu2 O2 C9 O3 -178.36(17) 3_667 . . . ? Cu2 O2 C9 C10 0.3(4) 3_667 . . . ? Cu2 O5 C19 O6 -2.6(3) . . . . ? Cu2 O5 C19 C20 177.80(19) . . . . ? Cu2 N2 C15 C16 -2.9(2) . . . . ? Cu2 N2 C15 C14 179.41(18) . . . . ? Cu2 N2 C11 C12 -178.35(19) . . . . ? N1 C5 C6 O1 19.1(3) . . . . ? N1 C5 C6 C7 138.7(2) . . . . ? N1 C5 C6 C8 -99.5(2) . . . . ? N1 C5 C4 C3 -0.5(4) . . . . ? N1 C1 C2 C3 -0.9(4) . . . . ? N2 C15 C16 O4 30.3(3) . . . . ? N2 C15 C16 C18 150.1(2) . . . . ? N2 C15 C16 C17 -87.1(2) . . . . ? N2 C15 C14 C13 -1.1(4) . . . . ? N2 C11 C12 C13 -0.1(4) . . . . ? C5 N1 C1 C2 0.3(3) . . . . ? C5 C4 C3 C2 -0.1(4) . . . . ? C15 N2 C11 C12 -1.6(4) . . . . ? C15 C14 C13 C12 -0.6(4) . . . . ? C6 C5 C4 C3 -177.8(2) . . . . ? C16 C15 C14 C13 -178.5(2) . . . . ? C1 N1 C5 C6 178.0(2) . . . . ? C1 N1 C5 C4 0.4(3) . . . . ? C1 C2 C3 C4 0.8(4) . . . . ? C11 N2 C15 C16 179.9(2) . . . . ? C11 N2 C15 C14 2.2(3) . . . . ? C11 C12 C13 C14 1.2(4) . . . . ? C4 C5 C6 O1 -163.4(2) . . . . ? C4 C5 C6 C7 -43.8(3) . . . . ? C4 C5 C6 C8 78.0(3) . . . . ? C14 C15 C16 O4 -152.1(2) . . . . ? C14 C15 C16 C18 -32.4(3) . . . . ? C14 C15 C16 C17 90.4(3) . . . . ? C25 N3 C23 C24 60.0(4) . . . . ? C25 N3 C21 C22 -54.8(3) . . . . ? C23 N3 C25 C26 61.3(3) . . . . ? C23 N3 C21 C22 174.8(3) . . . . ? C21 N3 C25 C26 -66.6(3) . . . . ? C21 N3 C23 C24 -169.3(3) . . . . ? _shelx_res_file ; TITL dp_511_dcmextractrt_auto_a.res in P2(1)/n dp_511_dcmextractrt_auto.res created by SHELXL-2018/3 at 11:36:45 on 21-Feb-2023 REM Old TITL dp_511_dcmextractrt_auto_a.res in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.102, Rweak 0.005, Alpha 0.039 REM 0.740 for 145 systematic absences, Orientation as input REM Formula found by SHELXT: C30 Cl Cu2 N4 O7 CELL 1.54184 9.1569 31.5203 11.7807 90 97.859 90 ZERR 1 0.0001 0.0003 0.0001 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl Cu N O UNIT 104 180 4 8 12 45 L.S. 25 PLAN 15 TEMP -113 CONF FREE Cu1 Cu2 LIST 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.064400 2.764900 FVAR 0.27607 CU1 4 0.481684 0.534068 0.891952 11.00000 0.02091 0.02196 = 0.02121 0.00259 0.00075 0.00070 CU2 4 0.359367 0.448329 0.837606 11.00000 0.02360 0.02293 = 0.02188 -0.00028 0.00207 -0.00048 CL1 3 0.384791 0.245095 0.035028 11.00000 0.04353 0.05322 = 0.06559 -0.02345 0.02072 -0.01281 O4 6 0.547895 0.474212 0.905476 11.00000 0.02226 0.02374 = 0.02174 0.00004 0.00502 0.00256 O1 6 0.305195 0.507895 0.819554 11.00000 0.02459 0.02413 = 0.02771 0.00374 -0.00349 0.00082 O2 6 0.659534 0.562080 0.964486 11.00000 0.02357 0.02697 = 0.02235 0.00250 0.00247 -0.00120 O5 6 0.175406 0.420168 0.782436 11.00000 0.02960 0.03347 = 0.02635 -0.00304 0.00238 -0.00277 AFIX 6 O11 6 0.195722 0.392613 0.395729 11.00000 0.03525 0.04346 = 0.02681 0.00294 0.00435 -0.00317 H11A 2 0.214744 0.406662 0.459771 11.00000 -1.50000 H11B 2 0.235705 0.407743 0.346321 11.00000 -1.50000 AFIX 0 O6 6 0.252181 0.418999 0.612532 11.00000 0.03555 0.04862 = 0.03055 -0.00362 0.00773 -0.00849 O3 6 0.697155 0.577522 0.788289 11.00000 0.04402 0.05165 = 0.02532 0.00256 0.01030 -0.00748 N1 5 0.368283 0.586775 0.844582 11.00000 0.02529 0.02667 = 0.02201 0.00311 0.00355 0.00083 N2 5 0.489863 0.397419 0.838271 11.00000 0.03550 0.02583 = 0.02058 -0.00103 0.00460 0.00215 N3 5 0.383687 0.326656 0.428106 11.00000 0.02827 0.03781 = 0.03351 -0.00276 0.00465 -0.00089 AFIX 13 H3A 2 0.320612 0.352570 0.415116 11.00000 -1.20000 AFIX 0 O7 6 0.340654 0.288100 0.044524 11.00000 0.07639 0.05580 = 0.06586 -0.00272 0.01592 0.00840 C5 1 0.245101 0.579284 0.771717 11.00000 0.02307 0.02742 = 0.02500 0.00519 0.00510 -0.00023 C15 1 0.634274 0.407624 0.850504 11.00000 0.03296 0.02943 = 0.01862 0.00039 0.00640 0.00455 O9 6 0.310890 0.218142 0.106769 11.00000 0.05690 0.06367 = 0.08971 0.00433 0.02106 -0.01124 C9 1 0.731352 0.581268 0.892992 11.00000 0.02446 0.02934 = 0.03034 0.00207 0.00722 0.00382 C6 1 0.218225 0.532847 0.736915 11.00000 0.02441 0.02571 = 0.02861 0.00521 -0.00116 0.00135 C16 1 0.666586 0.455126 0.855004 11.00000 0.02404 0.02780 = 0.02363 0.00136 0.00776 0.00493 C19 1 0.159824 0.410119 0.676789 11.00000 0.02917 0.02933 = 0.02965 -0.00087 0.00339 0.00038 C1 1 0.404044 0.626712 0.877535 11.00000 0.02947 0.02605 = 0.02582 0.00148 0.00327 -0.00045 AFIX 43 H1 2 0.491906 0.631462 0.928881 11.00000 -1.20000 AFIX 0 C2 1 0.317792 0.660904 0.839452 11.00000 0.03587 0.02571 = 0.03624 0.00208 0.00879 -0.00017 AFIX 43 H2 2 0.344487 0.688818 0.864699 11.00000 -1.20000 AFIX 0 C18 1 0.812938 0.465170 0.926988 11.00000 0.02581 0.03424 = 0.03469 0.00112 0.00654 0.00340 AFIX 137 H18A 2 0.825316 0.496000 0.933308 11.00000 -1.50000 H18B 2 0.893443 0.453063 0.890507 11.00000 -1.50000 H18C 2 0.814535 0.452932 1.003619 11.00000 -1.50000 AFIX 0 C17 1 0.663624 0.470981 0.731280 11.00000 0.03719 0.03476 = 0.02459 0.00448 0.01069 0.00475 AFIX 137 H17A 2 0.567160 0.464811 0.687400 11.00000 -1.50000 H17B 2 0.740759 0.456577 0.695807 11.00000 -1.50000 H17C 2 0.681064 0.501660 0.731775 11.00000 -1.50000 AFIX 0 C11 1 0.448969 0.356642 0.833081 11.00000 0.04406 0.02645 = 0.02728 -0.00129 0.00514 -0.00044 AFIX 43 H11 2 0.347026 0.349914 0.826432 11.00000 -1.20000 AFIX 0 C4 1 0.154150 0.612523 0.729241 11.00000 0.02383 0.03233 = 0.03596 0.00900 0.00108 0.00284 AFIX 43 H4 2 0.067379 0.607134 0.677226 11.00000 -1.20000 AFIX 0 C3 1 0.191280 0.653679 0.763533 11.00000 0.03257 0.02844 = 0.04352 0.00920 0.00805 0.00657 AFIX 43 H3 2 0.130187 0.676737 0.735040 11.00000 -1.20000 AFIX 0 C10 1 0.856591 0.609149 0.943829 11.00000 0.02939 0.04302 = 0.04440 0.00304 0.00711 -0.00831 AFIX 137 H10A 2 0.823524 0.638735 0.942638 11.00000 -1.50000 H10B 2 0.938625 0.606440 0.898903 11.00000 -1.50000 H10C 2 0.889296 0.600454 1.023099 11.00000 -1.50000 AFIX 0 C14 1 0.741269 0.376089 0.853863 11.00000 0.03800 0.03399 = 0.03327 0.00127 0.00605 0.01186 AFIX 43 H14 2 0.842781 0.383385 0.861107 11.00000 -1.20000 AFIX 0 O8 6 0.539114 0.243193 0.069521 10.75000 0.02265 0.04377 = 0.15293 -0.02677 0.02017 -0.00370 C12 1 0.550160 0.324032 0.837079 11.00000 0.05854 0.02554 = 0.03263 -0.00054 0.00437 0.00439 AFIX 43 H12 2 0.518478 0.295305 0.833393 11.00000 -1.20000 AFIX 0 C13 1 0.697901 0.333879 0.846507 11.00000 0.05456 0.03116 = 0.03791 0.00007 0.00578 0.01678 AFIX 43 H13 2 0.769421 0.311982 0.847960 11.00000 -1.20000 AFIX 0 C7 1 0.055819 0.520997 0.733902 11.00000 0.02366 0.03386 = 0.06130 0.00610 -0.00476 -0.00346 AFIX 137 H7A 2 0.042444 0.490836 0.715108 11.00000 -1.50000 H7B 2 -0.004276 0.538063 0.675613 11.00000 -1.50000 H7C 2 0.025199 0.526496 0.809055 11.00000 -1.50000 AFIX 0 C25 1 0.342755 0.306454 0.533642 11.00000 0.03930 0.04532 = 0.03854 0.00506 0.00574 -0.00754 AFIX 23 H25A 2 0.235089 0.301310 0.522456 11.00000 -1.20000 H25B 2 0.364741 0.326609 0.598166 11.00000 -1.20000 AFIX 0 C20 1 0.020771 0.386764 0.632289 11.00000 0.03328 0.05971 = 0.03547 -0.00942 0.00276 -0.01278 AFIX 137 H20A 2 0.013927 0.360867 0.677290 11.00000 -1.50000 H20B 2 0.022205 0.379264 0.551718 11.00000 -1.50000 H20C 2 -0.064556 0.404921 0.638820 11.00000 -1.50000 AFIX 0 C23 1 0.348919 0.300341 0.321429 11.00000 0.03745 0.05622 = 0.04511 -0.01704 0.00767 -0.00190 AFIX 23 H23A 2 0.381293 0.315755 0.256023 11.00000 -1.20000 H23B 2 0.404833 0.273407 0.331278 11.00000 -1.20000 AFIX 0 C8 1 0.268714 0.527166 0.618692 11.00000 0.05854 0.03643 = 0.02707 0.00142 0.00495 0.00243 AFIX 137 H8A 2 0.372304 0.535603 0.622747 11.00000 -1.50000 H8B 2 0.208050 0.544925 0.562440 11.00000 -1.50000 H8C 2 0.257985 0.497347 0.595497 11.00000 -1.50000 AFIX 0 O10 6 0.351018 0.232685 -0.081747 11.00000 0.16282 0.11108 = 0.08110 -0.05579 0.04408 -0.05688 C21 1 0.539970 0.342122 0.437647 11.00000 0.02807 0.05287 = 0.04340 -0.00197 0.00743 -0.00585 AFIX 23 H21A 2 0.554278 0.356609 0.365423 11.00000 -1.20000 H21B 2 0.606974 0.317340 0.446696 11.00000 -1.20000 AFIX 0 C22 1 0.582188 0.372067 0.535949 11.00000 0.03905 0.05802 = 0.04244 -0.00281 0.00212 -0.01512 AFIX 137 H22A 2 0.510587 0.395309 0.532045 11.00000 -1.50000 H22B 2 0.680565 0.383636 0.531433 11.00000 -1.50000 H22C 2 0.582940 0.356782 0.608466 11.00000 -1.50000 AFIX 0 C24 1 0.187544 0.290614 0.294702 11.00000 0.04387 0.06418 = 0.05880 -0.02261 0.00320 -0.01335 AFIX 137 H24A 2 0.168798 0.275462 0.221519 11.00000 -1.50000 H24B 2 0.131256 0.317151 0.289475 11.00000 -1.50000 H24C 2 0.157133 0.272875 0.355649 11.00000 -1.50000 AFIX 0 C26 1 0.419670 0.265514 0.566076 11.00000 0.06492 0.05096 = 0.07088 0.01763 -0.00895 -0.00084 AFIX 137 H26A 2 0.399155 0.245261 0.502788 11.00000 -1.50000 H26B 2 0.384147 0.253962 0.634527 11.00000 -1.50000 H26C 2 0.526143 0.270474 0.582181 11.00000 -1.50000 AFIX 6 PART 2 O12A 6 0.079157 0.298556 -0.173843 10.50000 0.08540 0.05515 = 0.09787 0.02264 -0.03966 -0.00979 H12A 2 0.023594 0.276752 -0.164730 10.50000 -1.50000 H12B 2 0.147567 0.288583 -0.210923 10.50000 -1.50000 AFIX 0 HKLF 4 REM dp_511_dcmextractrt_auto_a.res in P2(1)/n REM wR2 = 0.1113, GooF = S = 1.049, Restrained GooF = 1.049 for all data REM R1 = 0.0360 for 5758 Fo > 4sig(Fo) and 0.0424 for all 6646 data REM 412 parameters refined using 0 restraints END WGHT 0.0644 2.7651 REM Highest difference peak 0.894, deepest hole -0.471, 1-sigma level 0.070 Q1 1 0.5502 0.2391 0.1402 11.00000 0.05 0.89 Q2 1 0.5366 0.2444 0.0364 11.00000 0.05 0.70 Q3 1 0.5281 0.2549 0.0559 11.00000 0.05 0.69 Q4 1 0.4843 0.2430 0.0684 11.00000 0.05 0.67 Q5 1 0.0747 0.2995 -0.1249 11.00000 0.05 0.59 Q6 1 0.4489 0.2189 -0.0346 11.00000 0.05 0.59 Q7 1 0.0323 0.2975 -0.1973 11.00000 0.05 0.52 Q8 1 0.1411 0.2848 -0.1697 11.00000 0.05 0.50 Q9 1 0.0711 0.2838 -0.2082 11.00000 0.05 0.50 Q10 1 0.0969 0.3188 -0.1738 11.00000 0.05 0.50 Q11 1 0.2813 0.2582 -0.0327 11.00000 0.05 0.37 Q12 1 0.2220 0.5590 0.7493 11.00000 0.05 0.32 Q13 1 0.3347 0.2391 -0.0977 11.00000 0.05 0.32 Q14 1 0.4944 0.4590 0.8904 11.00000 0.05 0.29 Q15 1 -0.0460 0.3800 0.6834 11.00000 0.05 0.27 ; _shelx_res_checksum 27824 _shelx_hkl_file ; 0 0 1 0.30 0.35 0 0 -1 -0.02 0.41 0 0 2 369.73 13.59 0 0 -2 338.43 13.58 0 0 -2 353.89 13.65 0 0 3 5.05 1.28 0 0 -3 6.56 1.27 0 0 -3 6.65 1.20 0 0 4 3685.62 141.38 0 0 4 3661.73 141.29 0 0 -4 3658.70 141.37 0 0 -4 3840.12 141.30 0 0 5 -0.41 1.41 0 0 -5 0.41 1.18 0 0 5 -0.84 1.18 0 0 5 -0.35 1.04 0 0 -5 0.85 1.10 0 0 6 9.66 1.25 0 0 -6 12.08 1.29 0 0 6 10.65 1.81 0 0 6 9.25 1.43 0 0 7 0.10 2.08 0 0 7 -1.85 3.87 0 0 -7 -0.56 1.09 0 0 7 1.90 1.69 0 0 8 2.09 1.98 0 0 8 3.95 1.46 0 0 8 1.63 2.29 0 0 9 -1.36 2.21 0 0 9 0.42 5.92 0 0 9 -0.73 2.46 0 0 10 93.00 5.70 0 0 10 93.75 5.39 0 0 10 90.40 9.60 0 0 11 -3.66 2.83 0 0 11 -2.13 2.96 0 0 12 18.77 2.74 0 0 12 22.12 3.17 0 0 13 -1.40 1.74 0 0 13 -1.86 2.23 0 0 14 75.09 4.21 0 -1 1 3455.17 131.55 0 1 -1 3380.97 131.57 0 1 1 3471.28 131.56 0 -1 -1 3516.79 131.56 0 1 1 3498.30 131.56 0 1 -2 3.33 0.71 0 -1 -2 3.38 0.87 0 -1 -2 1.63 0.76 0 1 2 2.99 0.93 0 1 -2 2.84 0.85 0 1 2 4.33 0.76 0 -1 2 3.20 0.77 0 -1 -3 3840.22 148.04 0 1 3 4013.68 148.04 0 -1 -3 3940.92 148.10 0 1 -3 3905.62 148.09 0 1 -3 3825.03 148.03 0 -1 3 3860.62 148.03 0 -1 4 2458.60 93.19 0 1 4 2393.55 93.21 0 -1 -4 2509.03 93.22 0 -1 4 2507.47 93.31 0 1 -4 2454.32 93.20 0 -1 -4 2424.28 93.29 0 1 4 2382.76 93.28 0 1 -4 2451.84 93.29 0 -1 -5 5.02 1.35 0 -1 -5 2.59 1.25 0 1 -5 3.62 1.12 0 -1 5 2.15 1.11 0 1 5 3.87 1.17 0 -1 5 1.31 1.00 0 1 5 -0.23 1.41 0 -1 5 3.66 1.53 0 1 -5 1.96 1.16 0 1 6 114.44 5.15 0 -1 -6 102.56 4.94 0 1 -6 107.71 4.78 0 -1 -6 116.27 4.84 0 -1 6 109.35 5.13 0 -1 6 118.08 4.99 0 1 6 109.76 4.81 0 1 7 315.45 13.18 0 -1 -7 283.80 12.00 0 1 7 308.01 12.40 0 -1 -7 273.60 11.83 0 -1 7 305.75 12.36 0 1 7 290.57 12.21 0 -1 7 274.80 11.92 0 -1 7 292.34 12.25 0 -1 8 0.08 1.46 0 -1 8 1.04 2.07 0 1 8 2.44 2.97 0 1 8 -1.01 2.27 0 1 8 -1.38 4.71 0 1 8 0.47 2.19 0 -1 8 1.00 2.07 0 -1 8 2.31 5.12 0 1 9 94.19 9.06 0 -1 9 84.99 5.10 0 1 9 90.01 5.07 0 -1 9 92.45 4.58 0 -1 9 89.97 5.34 0 1 9 89.44 5.23 0 -1 10 262.76 11.07 0 1 10 270.96 11.15 0 -1 10 235.54 11.12 0 1 10 241.13 11.21 0 -1 10 258.95 15.06 0 1 10 256.91 15.10 0 -1 11 33.11 8.06 0 1 11 23.09 3.43 0 -1 11 34.51 3.66 0 1 11 31.14 3.33 0 -1 11 25.10 4.38 0 -1 11 22.74 3.11 0 1 12 40.06 3.59 0 -1 12 45.52 3.76 0 -1 12 38.95 3.43 0 1 12 38.30 3.41 0 1 13 17.77 3.20 0 1 13 16.42 2.55 0 -1 13 13.69 2.18 0 1 13 15.97 2.21 0 -1 13 17.64 2.49 0 1 14 20.02 2.33 0 2 0 1931.33 73.54 0 -2 0 1938.40 73.51 0 2 1 22.24 1.05 0 -2 -1 22.08 1.00 0 -2 1 19.99 1.00 0 -2 -1 20.10 0.99 0 2 -2 2946.54 115.27 0 2 2 3041.52 115.29 0 -2 -2 3032.66 115.30 0 -2 2 3134.87 115.31 0 2 3 3.33 1.22 0 -2 -3 2.88 1.11 0 -2 3 5.23 1.18 0 -2 -3 4.46 1.20 0 2 -3 3.55 1.13 0 2 -4 1193.85 46.23 0 -2 4 1232.45 46.33 0 -2 -4 1201.95 46.32 0 2 4 1219.10 46.26 0 -2 -4 1207.40 46.27 0 -2 5 1890.54 72.31 0 -2 -5 1971.15 72.23 0 2 5 1867.37 72.37 0 2 -5 1911.97 72.18 0 -2 -5 1841.94 72.29 0 -2 5 1769.02 72.34 0 2 5 1952.12 72.22 0 2 6 9.79 3.82 0 2 6 7.00 1.65 0 -2 -6 6.56 1.18 0 -2 6 4.00 1.27 0 2 -6 5.22 1.13 0 2 6 5.10 1.20 0 -2 6 4.13 1.55 0 -2 -6 5.18 1.53 0 2 6 4.13 1.77 0 -2 -7 621.72 24.89 0 -2 7 586.89 24.82 0 -2 -7 616.74 24.74 0 -2 7 626.21 25.16 0 2 7 610.99 25.16 0 2 7 703.57 27.33 0 -2 7 652.09 25.07 0 2 7 634.67 25.11 0 2 7 656.95 26.01 0 2 8 286.20 11.81 0 2 8 267.39 11.85 0 2 8 267.51 12.61 0 2 8 297.56 14.76 0 -2 8 267.66 11.78 0 -2 8 260.76 11.40 0 -2 8 276.21 11.71 0 -2 9 63.52 7.44 0 2 9 59.27 4.82 0 2 9 52.22 4.12 0 -2 9 58.04 3.83 0 -2 9 44.47 3.18 0 2 9 61.20 8.22 0 -2 9 52.93 3.97 0 2 9 56.32 3.88 0 -2 10 65.36 3.79 0 2 10 70.18 4.60 0 -2 10 73.34 8.81 0 2 10 66.51 4.71 0 2 10 58.96 5.40 0 -2 10 72.45 4.71 0 -2 10 63.70 4.45 0 -2 11 150.99 9.01 0 -2 11 173.78 12.20 0 2 11 161.86 8.09 0 2 11 164.32 7.95 0 -2 11 156.00 7.83 0 -2 11 152.21 7.92 0 2 11 173.83 9.09 0 -2 12 22.16 2.85 0 2 12 19.47 3.78 0 2 12 23.82 3.13 0 -2 12 24.53 4.10 0 -2 12 30.55 3.27 0 2 12 24.06 2.95 0 -2 13 3.17 1.78 0 2 13 -0.47 2.30 0 2 13 5.89 1.95 0 -2 13 3.58 2.81 0 2 13 1.93 2.64 0 -2 13 5.86 2.10 0 2 14 31.00 2.63 0 3 0 0.52 0.55 0 -3 0 0.32 0.35 0 3 1 3000.76 110.73 0 -3 1 2909.50 110.67 0 -3 -1 2836.64 110.67 0 -3 -1 2952.80 110.69 0 -3 2 102.14 3.93 0 3 2 97.44 3.98 0 -3 -2 99.56 3.94 0 3 -2 87.86 3.91 0 -3 -3 21.91 1.58 0 -3 3 21.56 1.45 0 -3 -3 19.77 1.48 0 3 -3 22.11 1.48 0 3 3 22.15 1.58 0 -3 4 0.08 1.06 0 -3 -4 1.56 1.03 0 3 4 0.68 1.05 0 -3 -4 0.39 1.12 0 3 4 -0.11 1.13 0 3 -4 -0.03 1.00 0 -3 5 524.99 22.51 0 -3 5 578.14 22.50 0 -3 -5 592.72 22.42 0 3 -5 583.50 22.36 0 3 5 580.47 22.51 0 3 5 602.12 22.44 0 -3 6 45.40 2.92 0 3 6 36.92 2.93 0 -3 6 34.86 3.45 0 3 -6 46.15 2.48 0 -3 6 58.94 2.77 0 3 6 48.63 2.60 0 3 6 51.78 2.74 0 -3 -6 49.83 2.63 0 -3 -6 47.32 2.78 0 3 6 43.00 4.79 0 -3 -6 49.31 2.55 0 -3 7 84.84 4.10 0 -3 -7 81.44 4.09 0 3 7 81.12 4.31 0 3 7 92.02 7.14 0 3 7 80.08 5.44 0 -3 -7 75.13 3.76 0 -3 7 79.99 4.35 0 -3 7 80.15 4.19 0 3 7 73.05 4.39 0 -3 8 509.69 21.54 0 3 8 546.14 21.88 0 3 8 565.41 22.84 0 3 8 518.29 21.93 0 -3 8 512.20 21.87 0 3 8 584.21 24.75 0 -3 8 554.20 21.81 0 3 9 5.68 2.70 0 3 9 5.20 3.31 0 3 9 9.63 6.44 0 -3 9 3.00 2.55 0 3 9 8.19 2.57 0 -3 9 6.27 5.69 0 -3 9 6.46 2.23 0 -3 9 7.10 1.94 0 3 9 11.95 3.55 0 3 10 72.82 4.80 0 -3 10 70.71 4.13 0 -3 10 89.39 5.13 0 -3 10 67.33 4.68 0 3 10 81.81 5.17 0 -3 10 79.29 8.81 0 3 10 77.16 5.57 0 3 10 72.08 5.85 0 3 11 102.14 6.76 0 -3 11 103.45 10.04 0 -3 11 98.07 5.63 0 3 11 105.17 5.78 0 3 11 96.11 5.96 0 -3 11 107.27 5.88 0 -3 11 89.34 6.89 0 3 12 93.38 5.45 0 3 12 110.75 5.77 0 3 12 107.08 6.41 0 -3 12 106.69 6.54 0 -3 12 90.27 5.29 0 -3 12 93.68 5.48 0 3 13 37.00 3.12 0 -3 13 27.95 2.64 0 -3 13 37.18 2.90 0 -3 13 32.46 3.64 0 3 13 25.50 2.67 0 3 13 38.88 3.44 0 3 14 57.36 3.42 0 -3 14 53.41 3.45 0 -4 0 497.93 18.98 0 4 0 497.47 19.06 0 4 -1 125.74 4.84 0 -4 1 126.82 4.85 0 -4 -1 124.57 4.88 0 -4 -1 126.06 4.83 0 4 1 119.75 4.85 0 4 1 124.32 4.97 0 -4 -2 668.15 25.51 0 4 -2 661.12 25.51 0 -4 -2 657.74 25.50 0 -4 2 670.80 25.51 0 4 2 668.30 25.55 0 4 2 676.42 25.51 0 -4 -3 122.25 4.89 0 4 -3 117.89 4.90 0 -4 -3 110.77 4.89 0 4 -3 124.43 4.89 0 -4 3 116.27 4.90 0 -4 -3 123.40 4.93 0 4 3 115.71 4.91 0 4 3 121.51 4.91 0 4 -4 30.48 1.76 0 -4 -4 32.56 1.90 0 4 4 33.28 1.91 0 -4 -4 28.03 1.84 0 4 4 26.71 1.82 0 4 -4 35.72 1.89 0 -4 -4 29.01 1.86 0 -4 4 32.95 1.86 0 4 5 240.93 9.38 0 4 -5 237.26 9.28 0 -4 -5 232.95 9.34 0 -4 5 214.38 9.45 0 -4 -5 230.74 9.39 0 4 5 233.53 9.39 0 -4 5 233.26 9.39 0 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2.60 0 4 13 -1.52 2.53 0 -4 13 -2.19 2.71 0 -4 13 3.03 1.95 0 4 13 2.09 2.12 0 4 13 3.69 1.87 0 4 14 37.50 2.41 0 4 14 36.62 2.77 0 -4 14 41.86 2.98 0 -5 0 -0.01 0.55 0 5 0 0.29 0.86 0 5 -1 83.58 3.26 0 5 1 83.71 3.28 0 -5 1 85.32 3.28 0 -5 -1 80.92 3.26 0 5 -1 82.71 3.48 0 5 1 79.92 3.35 0 -5 -1 83.32 3.33 0 5 -2 368.75 14.04 0 -5 -2 341.21 14.06 0 -5 2 378.00 14.05 0 -5 -2 357.55 14.03 0 5 2 364.68 14.13 0 5 2 375.94 14.05 0 5 -3 2.45 1.08 0 -5 -3 2.22 1.12 0 5 3 2.63 1.07 0 -5 -3 2.84 1.00 0 -5 -3 0.50 1.04 0 5 3 1.10 1.12 0 -5 3 1.52 1.01 0 5 -3 1.20 1.03 0 5 4 1173.99 44.40 0 5 -4 1145.76 44.39 0 -5 -4 1141.39 44.39 0 5 -4 1134.07 44.32 0 -5 -4 1163.35 44.38 0 5 4 1199.85 44.40 0 -5 -4 1136.14 44.37 0 -5 4 1184.04 44.39 0 5 5 343.82 13.44 0 -5 -5 339.00 13.31 0 -5 -5 331.37 13.42 0 5 5 347.22 13.32 0 -5 -5 337.45 13.29 0 -5 5 309.13 13.39 0 5 5 349.58 13.33 0 -5 5 332.59 13.29 0 5 -5 332.41 13.20 0 5 6 41.60 5.57 0 5 -6 44.24 2.36 0 -5 -6 43.55 2.73 0 -5 6 40.93 2.78 0 -5 6 51.12 2.62 0 -5 6 29.61 3.36 0 5 6 48.90 2.57 0 5 6 49.88 2.63 0 5 6 33.87 3.91 0 -5 -6 45.20 2.57 0 5 7 60.53 6.56 0 5 7 67.75 5.21 0 -5 7 64.30 3.78 0 -5 7 68.85 3.70 0 -5 -7 70.02 3.77 0 -5 7 57.64 3.59 0 -5 8 144.74 7.01 0 -5 8 149.07 6.96 0 -5 -8 152.04 7.00 0 5 8 144.66 7.90 0 -5 8 158.97 7.22 0 5 9 25.33 4.29 0 -5 9 23.89 3.05 0 -5 9 26.74 2.94 0 5 9 26.87 4.01 0 5 9 29.34 3.44 0 -5 9 21.40 2.51 0 5 10 149.08 7.88 0 -5 10 161.99 7.75 0 -5 10 150.31 7.62 0 5 10 159.91 8.60 0 -5 10 152.48 7.24 0 5 10 161.40 8.69 0 -5 10 175.54 11.56 0 5 11 115.48 6.38 0 -5 11 111.56 7.33 0 -5 11 123.49 10.29 0 5 11 117.50 7.14 0 -5 11 106.34 6.07 0 -5 11 114.28 6.08 0 5 11 110.74 6.70 0 5 12 106.85 5.97 0 5 12 108.00 6.42 0 -5 12 109.57 6.91 0 -5 12 107.16 5.74 0 -5 12 116.71 9.72 0 -5 12 113.02 5.74 0 5 12 107.51 5.83 0 5 13 45.11 3.28 0 -5 13 54.04 3.28 0 -5 13 50.08 4.10 0 5 14 19.52 1.83 0 5 14 21.91 2.18 0 -6 0 2153.22 81.47 0 6 0 2125.23 81.58 0 6 1 8.59 0.83 0 6 -1 9.12 0.86 0 6 1 9.36 0.68 0 6 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81.32 8.72 0 7 11 74.76 5.55 0 -7 11 70.42 4.58 0 -7 11 75.74 4.70 0 7 11 82.20 5.57 0 7 12 108.69 6.15 0 -7 12 107.12 6.67 0 -7 12 120.85 9.29 0 -7 12 95.68 5.37 0 -7 12 96.32 5.03 0 -7 12 105.58 5.32 0 -7 13 45.08 3.77 0 7 13 33.96 3.17 0 -7 14 3.90 1.64 0 8 0 72.75 3.34 0 -8 0 72.49 3.01 0 8 1 122.74 3.22 0 -8 1 114.09 3.00 0 8 1 119.92 3.00 0 8 -1 121.89 3.24 0 8 -1 122.47 3.61 0 -8 -2 896.50 34.36 0 8 2 904.06 34.30 0 8 -2 872.53 34.49 0 -8 -2 906.16 34.53 0 -8 2 909.08 34.30 0 8 2 890.18 34.50 0 -8 3 295.10 11.48 0 8 3 285.77 11.65 0 -8 -3 298.54 11.53 0 8 3 295.58 11.49 0 -8 -4 35.78 2.02 0 -8 4 36.82 1.98 0 8 -4 35.41 2.03 0 8 4 33.80 2.15 0 8 4 38.14 2.03 0 8 5 5.47 1.31 0 8 -5 5.62 1.11 0 8 5 4.45 1.50 0 -8 -5 3.83 1.75 0 -8 5 6.18 1.12 0 -8 5 6.35 2.27 0 8 5 6.47 1.14 0 8 5 4.79 1.29 0 -8 -5 4.92 1.21 0 -8 5 3.99 1.45 0 8 6 267.81 11.56 0 -8 6 272.39 10.72 0 -8 6 260.63 10.88 0 8 6 280.60 12.19 0 8 6 251.84 11.01 0 8 -6 266.62 10.60 0 8 6 262.16 10.92 0 -8 -6 260.99 10.99 0 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0 -9 8 9.24 3.55 0 -9 8 11.62 2.29 0 9 8 9.80 2.35 0 9 8 9.67 3.70 0 -9 8 7.57 2.11 0 9 8 10.03 2.74 0 9 8 9.40 2.65 0 -9 -8 5.74 2.29 0 -9 8 10.85 2.64 0 -9 8 9.12 2.11 0 -9 9 2.21 1.98 0 -9 9 1.71 2.34 0 -9 9 1.02 2.19 0 9 9 2.41 2.73 0 9 9 2.00 2.37 0 -9 -9 -1.19 2.37 0 9 9 2.58 2.95 0 9 9 1.99 3.87 0 9 9 4.38 2.75 0 -9 10 47.31 3.47 0 -9 10 39.81 3.39 0 9 10 41.08 4.79 0 9 10 41.15 4.01 0 9 10 43.54 3.90 0 -9 10 41.51 3.52 0 9 10 39.52 3.62 0 9 10 41.11 4.13 0 -9 11 3.21 2.15 0 9 11 -1.49 2.62 0 -9 11 -2.19 6.46 0 -9 11 -0.98 3.64 0 9 11 -0.21 3.45 0 9 11 -0.47 2.72 0 -9 11 0.14 2.16 0 9 11 -0.20 2.82 0 9 12 40.31 3.42 0 9 12 36.20 3.58 0 9 12 45.06 3.75 0 -9 12 38.86 4.21 0 9 12 33.95 3.08 0 -9 13 9.20 2.52 0 9 13 3.86 2.01 0 9 13 8.49 1.80 0 -9 14 7.51 1.56 0 -10 0 483.50 18.49 0 10 0 474.10 18.73 0 -10 0 484.90 18.68 0 10 1 121.71 4.91 0 -10 -1 118.74 4.92 0 10 -1 127.01 4.93 0 -10 -1 119.35 5.16 0 10 -1 125.68 5.20 0 10 -2 373.39 14.93 0 10 -2 374.44 14.73 0 10 2 382.90 14.60 0 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2.62 2.02 0 -10 8 4.28 2.09 0 10 8 3.18 4.01 0 10 8 4.18 2.39 0 10 8 7.62 2.35 0 10 9 -1.91 3.20 0 -10 -9 -1.92 2.43 0 -10 9 -0.13 2.08 0 10 9 -0.14 2.35 0 10 9 -0.51 4.01 0 -10 9 -0.54 2.28 0 -10 9 -0.37 2.07 0 10 9 1.72 2.76 0 10 9 2.14 2.88 0 -10 10 59.48 3.88 0 10 10 59.27 4.67 0 -10 10 62.98 4.21 0 -10 10 59.83 4.13 0 -10 10 76.37 7.96 0 10 10 66.71 4.38 0 10 10 53.20 4.66 0 10 10 62.84 4.60 0 10 10 61.37 5.50 0 10 11 76.72 5.22 0 10 11 86.54 5.76 0 10 11 72.94 4.74 0 -10 11 96.87 8.95 0 -10 11 71.99 5.95 0 10 11 85.31 5.11 0 -10 12 38.12 4.08 0 10 12 28.87 3.42 0 10 12 30.85 2.92 0 -10 12 37.14 7.14 0 10 12 28.80 3.25 0 10 13 17.41 1.99 0 10 13 15.11 2.22 0 -10 13 16.78 2.57 0 -11 0 0.34 1.13 0 11 0 -0.14 1.39 0 11 -1 211.86 8.35 0 -11 -1 210.63 8.59 0 11 -1 208.40 8.63 0 -11 -1 216.37 8.35 0 11 1 213.71 8.34 0 -11 -2 4.88 1.37 0 -11 2 3.87 0.63 0 11 2 5.22 1.48 0 11 -2 3.37 0.95 0 11 2 3.80 0.64 0 11 -2 2.81 1.44 0 11 -3 90.91 4.07 0 11 3 86.34 4.03 0 -11 -3 86.67 4.09 0 11 3 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38.37 3.91 0 17 4 34.97 2.46 0 -17 4 38.93 3.27 0 -17 4 33.81 2.56 0 -17 4 26.27 3.15 0 17 5 624.76 24.62 0 -17 5 597.27 24.12 0 -17 -5 584.68 23.56 0 17 5 613.95 24.43 0 17 5 559.19 23.22 0 -17 5 563.04 23.46 0 17 5 601.63 23.41 0 -17 5 606.33 23.74 0 -17 5 625.61 24.12 0 17 6 80.98 4.17 0 -17 -6 76.70 4.74 0 -17 6 80.78 5.40 0 17 6 76.70 4.26 0 -17 6 78.88 5.25 0 -17 6 78.85 4.50 0 17 6 91.56 5.77 0 -17 6 75.01 4.67 0 -17 -7 185.96 8.61 0 -17 7 188.29 9.16 0 17 7 189.51 9.69 0 -17 7 183.46 8.44 0 17 7 179.08 8.10 0 17 7 173.74 8.17 0 -17 7 176.39 9.39 0 17 8 299.53 12.67 0 17 8 324.83 14.49 0 17 8 305.72 14.06 0 -17 8 290.42 13.35 0 -17 8 294.35 13.94 0 -17 8 289.41 12.88 0 17 9 205.68 9.47 0 -17 9 209.54 9.70 0 17 9 234.78 11.24 0 17 9 212.40 10.71 0 -17 9 218.69 11.05 0 -17 9 212.15 10.02 0 17 10 5.73 2.13 0 17 10 2.92 3.10 0 -17 10 6.49 2.50 0 -17 10 4.78 2.76 0 17 10 0.23 3.71 0 17 11 1.30 2.44 0 -17 11 0.72 2.21 0 17 11 2.67 1.71 0 17 11 3.74 2.94 0 -17 11 -0.34 5.27 0 17 12 10.49 2.40 0 17 12 8.68 1.51 0 -17 12 12.64 4.73 0 -17 12 13.19 1.82 0 -18 0 255.72 10.56 0 -18 0 261.76 10.85 0 -18 0 271.27 11.03 0 18 0 249.67 10.50 0 -18 0 251.92 11.06 0 18 1 9.09 1.61 0 -18 -1 9.48 1.81 0 -18 1 8.33 2.35 0 -18 -1 9.94 1.55 0 -18 -1 8.23 2.47 0 -18 -1 7.73 2.35 0 18 1 7.88 2.41 0 -18 1 10.24 1.82 0 -18 2 7.48 2.46 0 -18 -2 2.48 2.32 0 18 2 5.66 1.44 0 18 2 5.61 2.46 0 -18 2 7.55 2.44 0 -18 -2 5.30 2.40 0 -18 2 3.19 1.81 0 18 2 8.56 2.21 0 -18 -3 182.16 7.94 0 -18 -3 181.08 8.19 0 18 3 198.49 8.02 0 -18 3 178.74 8.71 0 -18 3 197.04 8.56 0 -18 -3 183.73 8.44 0 -18 3 174.31 8.54 0 -18 3 192.44 7.99 0 -18 3 187.14 8.19 0 18 3 175.52 8.81 0 18 3 179.84 8.73 0 -18 4 21.10 3.40 0 -18 4 26.50 3.19 0 -18 4 20.40 2.25 0 18 4 18.95 3.26 0 -18 -4 20.34 2.06 0 -18 4 22.85 2.95 0 18 4 24.53 2.18 0 18 4 23.01 3.46 0 -18 -4 23.33 2.52 0 -18 4 20.24 2.60 0 18 4 22.08 1.79 0 18 5 168.07 7.40 0 -18 5 182.78 8.46 0 18 5 156.43 8.69 0 -18 5 174.47 8.11 0 -18 -5 166.50 7.82 0 18 5 173.99 7.56 0 -18 5 175.41 8.59 0 -18 5 169.60 7.70 0 18 5 175.97 9.02 0 -18 6 398.49 17.17 0 -18 -6 388.99 16.57 0 -18 6 402.03 16.60 0 18 6 408.27 17.59 0 -18 6 403.12 16.51 0 18 6 439.94 17.89 0 -18 6 417.65 17.38 0 18 6 382.35 16.15 0 18 7 88.89 6.40 0 -18 7 101.76 5.32 0 -18 7 90.58 6.01 0 -18 -7 90.22 5.41 0 18 7 87.54 4.82 0 18 8 197.29 9.95 0 18 8 173.27 8.03 0 -18 8 183.37 9.62 0 -18 8 170.23 8.91 0 -18 8 172.04 8.27 0 -18 -8 164.46 8.52 0 18 8 190.09 9.52 0 18 9 0.75 4.10 0 -18 9 3.85 2.85 0 18 9 0.66 3.54 0 -18 9 1.27 2.68 0 -18 9 -1.71 4.30 0 18 9 -1.24 2.08 0 -18 10 194.83 9.17 0 18 10 211.57 10.31 0 18 10 195.28 8.87 0 18 10 213.05 9.91 0 18 11 39.03 2.83 0 18 11 48.71 4.06 0 18 11 38.72 3.51 0 18 12 81.78 4.30 0 -18 12 84.88 6.45 0 -18 12 69.42 3.86 0 19 0 0.74 1.83 0 -19 0 -2.02 2.03 0 -19 0 -1.43 2.60 0 19 0 -0.98 1.48 0 -19 0 -1.19 1.47 0 19 1 98.89 4.71 0 -19 -1 96.97 4.75 0 -19 1 96.13 4.81 0 -19 1 100.42 5.32 0 19 1 106.69 5.34 0 -19 -1 105.26 5.42 0 -19 -1 102.01 4.93 0 -19 -1 102.02 5.36 0 -19 2 47.52 3.83 0 19 2 51.33 3.65 0 -19 2 45.75 3.87 0 -19 2 50.72 3.26 0 19 2 50.82 3.00 0 -19 -2 51.87 3.64 0 19 2 49.46 3.91 0 -19 -3 4.58 2.14 0 19 3 8.29 2.71 0 -19 3 6.23 1.59 0 -19 3 6.44 2.11 0 -19 3 8.22 2.71 0 19 3 5.14 1.70 0 -19 3 9.45 2.39 0 -19 -3 6.18 1.87 0 19 3 4.48 2.62 0 -19 3 4.19 2.88 0 -19 -3 7.05 1.57 0 -19 -4 143.93 6.74 0 -19 4 148.09 7.23 0 -19 4 143.64 6.88 0 -19 4 148.66 7.27 0 19 4 142.60 6.49 0 -19 -4 136.83 6.44 0 -19 4 140.02 6.55 0 19 4 144.79 6.27 0 19 4 160.54 7.71 0 19 4 132.12 7.55 0 19 5 275.90 11.47 0 19 5 281.36 11.67 0 -19 5 291.65 12.49 0 -19 5 266.90 12.54 0 19 5 314.80 13.04 0 -19 5 265.85 11.76 0 -19 -5 273.20 11.90 0 -19 5 279.81 12.16 0 19 6 14.04 3.83 0 19 6 10.62 1.95 0 -19 6 20.49 3.68 0 -19 -6 12.97 2.84 0 -19 6 17.19 2.64 0 -19 6 12.16 3.66 0 19 6 20.21 4.10 0 -19 6 16.61 2.82 0 -19 7 93.83 5.17 0 -19 -7 93.38 5.41 0 -19 7 78.15 6.31 0 19 7 90.13 4.72 0 19 7 81.74 6.32 0 -19 7 94.81 5.97 0 -19 8 58.51 5.55 0 -19 -8 55.47 4.29 0 -19 8 55.19 3.98 0 19 8 52.69 5.27 0 19 8 46.74 3.40 0 -19 8 50.32 4.58 0 19 9 617.18 23.89 0 19 9 541.98 22.24 0 -19 9 545.01 22.49 0 -19 9 563.65 22.84 0 19 9 546.68 23.43 0 -19 9 534.48 23.57 0 19 10 24.75 3.82 0 -19 10 27.62 3.02 0 19 10 32.16 4.19 0 19 10 24.37 2.42 0 -19 11 5.41 5.08 0 19 11 10.59 2.92 0 19 11 11.96 1.68 0 19 11 9.06 2.55 0 19 12 25.21 2.45 0 -19 12 23.53 4.58 0 -19 12 23.09 2.02 0 -20 0 2.67 2.70 0 20 0 0.11 1.94 0 -20 0 2.97 1.98 0 -20 0 1.61 1.66 0 20 0 3.17 1.55 0 20 1 3.28 2.36 0 -20 -1 2.17 1.53 0 -20 1 5.11 2.31 0 -20 1 2.59 1.61 0 -20 -1 4.50 1.85 0 20 1 3.78 1.52 0 -20 -1 3.46 2.47 0 20 2 -0.34 1.59 0 20 2 -0.89 2.52 0 -20 2 3.85 2.84 0 -20 2 1.65 2.50 0 20 2 1.82 2.13 0 -20 2 -0.10 1.91 0 -20 -2 -0.59 2.28 0 -20 -2 0.69 1.62 0 -20 3 9.97 2.80 0 -20 3 14.57 1.94 0 -20 -3 11.73 2.46 0 20 3 14.28 2.93 0 -20 3 19.36 2.58 0 -20 3 13.32 3.12 0 20 3 11.08 2.96 0 20 3 16.69 2.00 0 -20 -3 12.34 2.17 0 -20 3 15.49 2.23 0 -20 4 2.10 2.56 0 -20 4 3.95 1.75 0 20 4 5.34 2.94 0 -20 -4 7.63 2.19 0 20 4 3.50 1.79 0 20 4 5.41 2.99 0 -20 4 4.76 2.31 0 -20 4 3.94 2.60 0 20 5 313.13 13.86 0 -20 5 315.62 13.55 0 20 5 305.37 12.58 0 -20 5 281.37 13.27 0 -20 5 302.47 12.70 0 -20 5 292.21 13.09 0 20 5 301.85 12.37 0 -20 -5 303.91 12.85 0 -20 6 862.85 34.80 0 -20 -6 853.10 34.21 0 -20 6 887.21 34.89 0 20 6 901.87 35.35 0 -20 6 852.39 34.07 0 20 6 845.05 33.75 0 -20 6 881.98 34.25 0 20 6 853.77 35.17 0 -20 7 396.29 17.46 0 -20 -7 398.93 16.57 0 20 7 391.23 16.10 0 20 7 389.26 17.66 0 -20 7 397.82 17.12 0 -20 7 404.19 16.46 0 20 7 370.31 17.44 0 20 8 152.43 8.39 0 -20 8 151.24 8.49 0 -20 8 134.75 7.64 0 20 8 138.78 6.67 0 -20 -8 134.14 7.23 0 -20 8 147.65 7.09 0 20 9 3.91 1.87 0 -20 9 -0.70 3.99 0 -20 9 5.67 2.94 0 20 9 0.43 3.60 0 20 9 2.08 3.81 0 -20 9 -1.08 2.37 0 20 10 143.45 7.42 0 20 10 127.09 6.25 0 20 10 148.59 7.75 0 -20 10 143.39 6.83 0 20 11 24.97 2.84 0 -20 11 27.71 5.05 0 20 11 29.40 3.23 0 -20 12 63.10 5.08 0 20 12 64.12 3.48 0 -20 12 54.34 3.07 0 -21 0 -2.16 1.70 0 21 0 -0.70 1.94 0 -21 0 -0.94 2.67 0 -21 0 3.44 2.03 0 21 0 -0.09 1.52 0 -21 -1 22.37 2.21 0 -21 1 23.52 2.27 0 21 1 24.23 2.87 0 -21 1 21.86 2.87 0 21 1 24.49 2.20 0 -21 -1 22.89 3.18 0 -21 -1 20.32 2.22 0 21 2 478.39 18.88 0 -21 -2 472.50 18.88 0 21 2 476.49 19.57 0 -21 -2 475.71 19.27 0 -21 2 452.32 18.97 0 21 2 492.26 19.36 0 -21 2 459.84 19.48 0 -21 2 469.83 19.49 0 -21 -2 476.06 18.91 0 -21 -3 351.05 14.18 0 21 3 351.34 14.06 0 -21 3 363.21 14.67 0 -21 -3 330.81 14.25 0 -21 3 366.90 14.86 0 21 3 353.39 14.77 0 -21 3 326.92 13.98 0 21 3 360.72 15.01 0 -21 3 323.60 14.22 0 -21 3 332.33 14.64 0 21 4 74.86 5.29 0 -21 4 64.55 3.94 0 -21 4 66.00 4.35 0 -21 4 66.04 4.71 0 -21 -4 72.02 4.17 0 21 4 70.67 5.04 0 21 4 72.67 3.93 0 -21 4 73.99 4.83 0 -21 5 54.23 3.53 0 -21 5 45.09 4.05 0 -21 5 53.52 4.66 0 -21 5 56.00 4.54 0 21 -5 39.92 3.48 0 -21 -5 50.76 3.70 0 21 5 51.08 4.72 0 21 6 382.72 16.33 0 -21 6 377.50 15.95 0 21 6 353.04 16.29 0 -21 6 357.55 16.06 0 -21 -6 349.70 15.24 0 21 6 364.63 14.76 0 -21 6 348.86 15.08 0 -21 6 365.97 15.29 0 21 7 112.18 7.11 0 -21 7 111.78 6.71 0 -21 7 108.61 7.11 0 21 7 106.13 7.04 0 -21 7 101.86 5.77 0 -21 -7 108.51 6.00 0 21 7 110.12 5.37 0 21 8 117.13 5.72 0 -21 8 115.82 6.75 0 -21 -8 128.46 6.38 0 -21 8 118.24 7.46 0 21 8 117.71 7.36 0 -21 8 109.65 6.08 0 -21 9 54.44 4.27 0 21 9 54.07 4.87 0 -21 9 56.33 3.71 0 -21 -9 54.21 3.93 0 21 9 42.71 3.08 0 -21 9 49.64 5.15 0 -21 10 -0.60 2.20 0 21 10 2.82 2.91 0 21 10 0.90 2.99 0 21 11 1.35 2.04 0 -21 11 1.79 4.17 0 21 11 3.78 2.25 0 -21 12 31.52 3.77 0 -21 12 27.97 1.98 0 21 12 30.88 2.30 0 -22 0 14.17 1.94 0 22 0 17.81 2.35 0 -22 0 12.48 2.36 0 -22 0 15.20 3.20 0 22 0 16.27 2.01 0 -22 1 291.71 12.77 0 22 1 304.88 12.88 0 -22 -1 288.23 12.28 0 22 -1 303.03 12.35 0 -22 -1 297.33 12.89 0 22 1 301.68 12.30 0 -22 1 297.47 12.37 0 -22 -2 56.27 4.16 0 -22 2 68.11 4.52 0 22 2 56.92 3.91 0 22 2 62.34 3.56 0 -22 -2 58.90 3.49 0 -22 2 59.70 3.77 0 -22 2 55.55 4.56 0 -22 -2 63.25 3.57 0 22 2 68.63 4.52 0 22 -3 176.02 8.61 0 -22 -3 201.96 8.43 0 -22 3 191.99 8.69 0 -22 -3 179.35 8.65 0 -22 3 179.38 9.13 0 22 3 191.90 8.38 0 22 3 203.54 9.22 0 22 3 186.61 9.44 0 -22 3 230.48 9.24 0 -22 3 205.02 9.32 0 -22 -3 185.67 8.48 0 22 4 234.68 10.98 0 22 4 228.17 9.84 0 -22 4 237.85 10.56 0 -22 4 231.88 10.58 0 -22 4 212.69 10.05 0 -22 4 228.20 9.84 0 -22 -4 223.01 9.99 0 22 4 248.84 10.96 0 -22 -5 68.58 4.30 0 22 5 59.61 5.45 0 22 5 77.39 5.44 0 -22 5 78.77 5.32 0 -22 5 66.48 4.68 0 -22 5 65.23 5.38 0 22 -5 64.57 4.33 0 -22 5 74.91 4.24 0 -22 6 175.74 8.39 0 -22 6 174.93 9.28 0 22 6 195.56 9.50 0 -22 6 182.37 8.66 0 -22 6 179.45 9.35 0 -22 -6 182.13 8.56 0 22 7 2.55 3.80 0 22 7 2.56 3.64 0 -22 7 -1.09 2.42 0 -22 -7 -1.64 2.65 0 -22 7 4.21 3.68 0 -22 7 -1.52 3.41 0 -22 8 35.39 3.89 0 22 8 35.46 4.37 0 -22 -8 32.38 3.40 0 -22 8 33.65 3.33 0 -22 8 41.43 4.75 0 22 8 41.00 4.72 0 -22 9 13.26 3.86 0 22 9 11.20 3.60 0 -22 9 6.77 2.73 0 22 10 10.61 2.98 0 -22 10 13.33 2.47 0 22 10 13.95 2.93 0 -22 11 -1.49 1.62 0 22 11 -0.30 2.00 0 22 11 -1.99 2.10 0 -22 11 2.52 4.03 0 23 0 1.08 1.74 0 -23 0 0.75 2.83 0 -23 0 -0.61 1.69 0 23 0 0.76 1.99 0 -23 0 -0.60 2.19 0 23 1 181.24 7.81 0 -23 -1 181.11 8.52 0 -23 1 159.62 7.82 0 23 -1 197.54 7.93 0 23 1 178.16 8.38 0 -23 1 177.54 8.31 0 -23 -1 165.58 7.78 0 -23 -2 672.05 26.46 0 -23 -2 647.07 26.44 0 -23 2 685.74 27.13 0 23 2 694.32 26.49 0 23 2 685.77 26.87 0 -23 2 651.34 27.12 0 -23 -2 661.50 26.86 0 -23 2 656.02 26.60 0 23 2 687.46 27.26 0 -23 -3 159.30 7.29 0 -23 -3 158.74 7.47 0 23 -3 154.23 7.59 0 -23 3 151.66 8.10 0 -23 -3 160.09 7.64 0 23 3 165.44 7.34 0 23 3 161.96 8.44 0 -23 3 179.08 8.17 0 -23 3 167.77 8.31 0 23 3 172.33 8.02 0 -23 3 167.64 7.64 0 -23 4 10.10 2.48 0 23 4 10.03 3.62 0 -23 4 8.05 2.01 0 -23 4 8.55 2.96 0 -23 4 8.98 3.35 0 -23 4 10.55 3.09 0 23 4 7.11 2.92 0 23 4 8.23 1.95 0 -23 -4 7.02 2.35 0 -23 5 -2.49 3.11 0 -23 -5 2.15 2.33 0 23 5 -0.83 3.30 0 -23 5 -0.38 3.27 0 -23 5 3.52 2.18 0 23 -5 -0.71 2.30 0 23 5 1.10 3.45 0 -23 -6 96.75 5.54 0 -23 6 101.32 6.50 0 23 6 98.45 6.37 0 -23 6 90.81 5.57 0 -23 6 99.70 6.44 0 -23 6 99.18 5.34 0 -23 7 9.80 2.58 0 -23 -7 13.82 2.92 0 -23 7 8.95 3.86 0 23 7 13.27 3.85 0 23 7 17.32 4.06 0 -23 7 12.61 3.48 0 23 8 33.95 4.44 0 -23 8 29.68 3.64 0 -23 8 28.41 3.09 0 -23 8 30.71 4.52 0 -23 -8 32.76 3.33 0 23 8 28.80 4.19 0 -23 9 1.29 2.71 0 23 9 -0.56 3.15 0 -23 9 2.62 3.56 0 23 10 7.43 2.67 0 -23 10 8.81 2.16 0 23 11 11.70 1.93 0 -23 11 17.50 3.93 0 23 11 12.47 2.12 0 -23 11 10.50 1.64 0 -24 0 372.82 15.88 0 24 0 380.33 16.11 0 24 0 411.72 15.95 0 -24 0 410.75 16.68 0 -24 0 381.69 16.09 0 24 -1 550.13 21.24 0 24 1 543.50 21.19 0 -24 -1 514.78 21.73 0 24 1 536.27 21.70 0 -24 1 530.55 21.58 0 -24 1 517.58 21.25 0 -24 -1 510.95 21.13 0 -24 -2 3.39 2.65 0 -24 2 0.16 2.88 0 -24 -2 2.01 1.80 0 -24 2 4.14 2.26 0 -24 2 2.44 3.10 0 24 2 5.33 2.78 0 -24 -2 3.49 1.83 0 24 2 3.40 1.77 0 -24 -3 3.29 2.12 0 24 3 3.86 2.47 0 24 -3 6.16 2.37 0 -24 -3 5.26 2.58 0 -24 3 8.60 2.87 0 24 3 1.15 3.06 0 -24 3 4.29 2.34 0 24 3 3.69 1.87 0 -24 -3 6.59 1.84 0 -24 3 7.54 3.50 0 -24 3 5.69 3.32 0 24 4 35.95 2.92 0 -24 4 34.78 3.93 0 -24 4 33.35 4.18 0 24 4 42.32 4.41 0 -24 4 42.79 3.43 0 -24 4 38.92 2.86 0 -24 4 42.51 4.18 0 -24 -4 35.09 3.20 0 24 4 40.97 4.03 0 24 5 390.30 15.63 0 -24 5 354.74 15.08 0 -24 -5 331.74 14.68 0 24 -5 313.24 14.70 0 24 5 365.68 15.84 0 -24 5 359.65 15.45 0 -24 5 361.36 14.58 0 -24 6 11.08 3.41 0 24 6 19.52 3.50 0 -24 6 13.66 2.53 0 -24 6 18.21 4.14 0 -24 -6 12.37 2.77 0 -24 6 16.22 3.05 0 24 7 30.03 4.10 0 -24 -7 31.45 3.25 0 -24 7 19.69 2.88 0 24 7 32.16 4.53 0 -24 7 33.26 3.92 0 -24 7 29.55 4.48 0 24 8 9.76 3.42 0 -24 8 7.52 3.72 0 -24 8 7.46 2.98 0 24 8 9.42 3.58 0 -24 -8 7.80 2.49 0 24 9 7.62 3.05 0 24 9 5.18 2.96 0 -24 9 6.23 2.53 0 -24 10 -0.66 1.76 0 24 10 -1.43 2.37 0 24 11 5.21 1.64 0 -24 11 4.10 1.30 0 24 11 4.97 1.79 0 -24 11 9.64 3.30 0 -24 -11 7.03 1.84 0 25 0 3.27 2.12 0 25 0 0.87 1.85 0 -25 0 -1.11 1.87 0 -25 0 1.30 3.12 0 -25 0 1.24 2.13 0 -25 1 1.00 2.56 0 -25 -1 0.32 1.83 0 25 1 3.40 2.37 0 -25 -1 0.78 2.85 0 -25 1 0.23 1.96 0 25 1 -0.43 1.76 0 25 -1 3.09 1.94 0 -25 -2 145.74 7.38 0 25 2 148.20 7.57 0 25 2 143.59 6.67 0 -25 -2 137.61 6.69 0 -25 2 143.13 7.39 0 -25 2 163.05 7.57 0 -25 2 136.22 6.88 0 -25 2 146.30 7.77 0 25 -2 140.75 6.72 0 25 3 105.53 6.10 0 25 3 96.90 5.54 0 -25 3 97.14 6.01 0 -25 3 101.82 5.87 0 -25 3 91.53 5.31 0 -25 3 96.70 6.01 0 25 -3 90.14 5.26 0 25 3 99.76 4.97 0 -25 -3 98.31 5.13 0 -25 -3 88.30 5.33 0 -25 4 57.79 3.99 0 -25 4 63.27 4.67 0 -25 -4 61.45 4.00 0 -25 4 55.97 4.71 0 25 4 59.21 4.54 0 25 4 56.39 3.54 0 25 4 55.50 4.97 0 -25 4 55.14 4.92 0 -25 5 37.58 2.99 0 25 5 40.67 4.09 0 -25 5 32.45 4.13 0 -25 5 36.02 3.86 0 -25 -5 28.45 3.24 0 25 -5 37.21 3.47 0 25 5 36.25 4.41 0 -25 -6 65.06 4.37 0 -25 6 73.71 5.45 0 -25 6 61.42 4.49 0 -25 6 61.57 4.05 0 25 6 68.33 5.11 0 -25 6 76.56 5.35 0 -25 -7 9.27 2.56 0 25 7 6.34 3.35 0 -25 7 4.68 3.25 0 -25 7 5.86 2.24 0 -25 7 9.77 3.68 0 25 8 8.47 3.30 0 -25 -8 12.53 2.48 0 -25 8 13.53 3.05 0 25 8 11.53 3.17 0 -25 8 8.97 3.58 0 25 9 165.10 8.16 0 -25 9 162.18 7.73 0 25 9 165.23 8.08 0 -25 10 -1.73 3.77 0 -25 10 3.64 1.58 0 25 10 2.78 2.09 0 -25 10 1.70 1.64 0 -25 11 1.18 1.05 0 26 0 24.57 2.54 0 -26 0 24.05 2.77 0 -26 0 21.89 3.70 0 -26 0 22.27 2.60 0 26 1 134.86 6.49 0 26 1 149.29 7.11 0 26 -1 139.85 6.60 0 -26 -1 134.24 6.58 0 -26 1 140.07 7.00 0 -26 -1 145.73 7.32 0 -26 1 135.54 6.68 0 -26 2 14.70 2.57 0 -26 -2 17.16 3.31 0 -26 2 20.04 3.29 0 26 -2 22.59 2.51 0 26 2 19.48 2.26 0 -26 2 20.15 3.21 0 -26 2 20.53 3.68 0 26 2 15.02 3.17 0 -26 -2 18.15 2.34 0 -26 3 111.09 6.30 0 26 3 107.86 5.42 0 -26 3 106.11 5.78 0 -26 3 113.19 6.54 0 -26 3 115.25 6.31 0 -26 -3 108.12 5.83 0 -26 -3 111.05 5.52 0 26 3 119.14 6.01 0 26 -3 96.72 5.73 0 26 3 109.74 6.48 0 26 4 10.32 2.89 0 -26 -4 6.98 2.48 0 -26 -4 12.16 2.44 0 26 4 8.80 3.37 0 -26 4 10.31 3.20 0 -26 4 12.89 3.66 0 -26 4 8.59 3.35 0 26 4 8.18 2.04 0 26 5 -0.19 2.83 0 -26 5 1.92 3.17 0 -26 -5 1.99 2.33 0 -26 5 1.43 2.97 0 -26 5 1.15 2.05 0 26 -5 1.59 2.29 0 26 5 2.15 3.40 0 -26 6 291.10 12.84 0 26 6 290.79 12.88 0 26 6 284.12 13.16 0 -26 6 253.88 12.95 0 -26 6 285.63 12.33 0 -26 -6 282.70 12.22 0 -26 7 6.72 3.13 0 26 7 2.40 2.96 0 -26 7 5.15 3.64 0 -26 -7 1.05 2.32 0 -26 8 46.63 3.84 0 -26 8 38.24 4.33 0 26 8 42.77 3.87 0 26 8 40.36 4.23 0 -26 9 31.60 3.00 0 26 9 40.51 3.32 0 26 9 35.17 3.46 0 -26 -10 64.16 3.79 0 -26 10 66.25 3.53 0 -26 10 69.26 3.58 0 26 10 68.89 3.91 0 26 10 71.47 3.93 0 -27 0 -0.12 2.09 0 27 0 2.05 1.94 0 -27 0 2.23 2.16 0 -27 0 -1.87 3.42 0 -27 -1 26.69 2.67 0 -27 1 30.10 3.12 0 -27 1 23.86 2.78 0 27 1 25.16 2.54 0 -27 -1 26.26 3.53 0 27 1 27.72 3.17 0 27 -1 25.14 2.63 0 -27 2 -2.77 3.03 0 -27 2 -1.27 2.83 0 27 2 0.88 1.82 0 -27 -2 -0.30 2.80 0 -27 2 1.40 2.35 0 27 2 3.51 2.83 0 -27 2 -2.45 3.50 0 27 -2 -1.17 1.97 0 -27 -2 -2.51 2.09 0 -27 3 84.50 5.40 0 27 -3 86.64 4.94 0 -27 -3 81.09 4.88 0 -27 3 77.14 5.61 0 27 3 89.52 4.48 0 27 3 75.54 5.42 0 27 3 89.56 4.89 0 -27 3 82.41 5.46 0 -27 -3 84.10 4.52 0 27 -3 78.32 4.54 0 -27 3 68.15 4.74 0 27 4 11.89 2.08 0 -27 4 20.17 3.67 0 -27 -4 17.81 2.48 0 -27 4 17.41 3.49 0 27 4 17.73 3.63 0 -27 4 17.30 3.45 0 27 4 20.22 3.02 0 27 -5 31.46 3.26 0 -27 5 30.60 3.77 0 -27 -5 32.75 3.22 0 -27 -5 32.99 3.07 0 27 5 36.65 3.64 0 -27 5 33.29 4.07 0 27 5 28.86 4.19 0 27 6 1.83 3.44 0 -27 6 1.97 3.08 0 -27 6 -1.81 2.67 0 -27 6 -1.16 3.41 0 27 6 1.79 2.83 0 -27 -6 1.94 2.25 0 -27 -7 133.88 6.63 0 -27 7 143.00 7.17 0 -27 7 137.30 7.58 0 27 7 132.81 7.17 0 -27 8 28.96 3.11 0 -27 -8 25.39 2.89 0 -27 8 21.17 3.54 0 27 8 23.47 3.02 0 27 8 25.92 3.48 0 27 9 59.50 3.97 0 -27 -9 61.45 3.70 0 -27 9 52.27 3.53 0 -27 9 55.24 3.35 0 27 9 61.43 3.73 0 27 10 10.83 1.83 0 27 10 10.32 1.74 0 -27 10 11.77 3.03 0 -27 -10 6.62 1.64 0 -27 10 10.78 1.43 0 -28 0 8.55 3.27 0 28 0 11.52 2.11 0 -28 0 8.30 2.19 0 -28 0 13.69 2.33 0 -28 -1 1.37 1.97 0 -28 1 0.14 2.35 0 28 -1 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25.74 3.14 0 -28 8 29.03 2.99 0 -28 -9 3.36 1.63 0 28 9 4.50 2.05 0 -28 9 5.56 1.76 0 -28 9 3.54 1.39 0 28 9 1.28 1.81 0 28 10 96.88 4.35 0 28 10 86.83 4.20 0 29 0 -0.22 1.87 0 -29 0 -2.01 2.10 0 -29 0 0.51 3.29 0 -29 1 0.53 2.94 0 -29 1 2.45 2.13 0 -29 -1 0.79 2.04 0 -29 -1 0.80 2.84 0 29 -1 -2.74 2.00 0 -29 1 1.35 2.25 0 29 1 -0.28 2.23 0 29 1 -2.53 1.87 0 29 2 14.55 2.23 0 -29 2 13.63 2.42 0 -29 2 14.23 3.40 0 -29 -2 17.53 2.94 0 29 -2 15.61 2.21 0 -29 2 11.87 3.56 0 -29 2 9.25 2.84 0 29 -2 18.56 2.86 0 29 2 10.93 2.66 0 29 -3 37.88 3.29 0 -29 3 39.85 3.97 0 29 3 43.24 3.99 0 -29 -3 39.36 3.34 0 -29 3 43.87 4.13 0 29 3 37.89 2.87 0 29 -3 39.04 3.01 0 -29 3 43.53 3.42 0 -29 3 37.42 4.02 0 29 -4 2.73 1.94 0 -29 -4 1.90 1.95 0 -29 4 -0.54 3.04 0 29 4 -1.24 2.16 0 29 4 3.57 2.95 0 -29 4 0.97 3.02 0 29 -4 3.08 2.77 0 -29 4 1.70 2.99 0 -29 -5 94.79 5.10 0 29 5 92.23 6.08 0 29 -5 94.24 5.06 0 29 -5 95.41 5.30 0 -29 5 101.91 6.10 0 -29 5 100.67 5.94 0 -29 5 103.86 5.78 0 29 5 105.86 5.56 0 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7 0.72 1.55 -1 24 7 -2.16 3.50 -1 -24 7 -1.06 3.12 -1 -24 7 -4.66 3.30 -1 -24 6 103.15 6.46 -1 -24 6 93.32 6.28 -1 24 6 110.66 6.40 -1 -24 6 103.57 5.83 1 -24 -6 104.48 5.68 -1 24 6 99.79 4.98 1 -24 -5 15.56 2.83 -1 24 5 16.31 2.44 -1 -24 5 16.72 3.37 -1 24 5 15.65 1.93 -1 24 5 14.40 3.35 -1 -24 5 13.39 3.09 1 -24 -4 77.47 4.51 -1 -24 4 70.33 5.07 1 -24 -4 64.93 4.36 -1 -24 4 75.18 4.95 -1 24 4 74.87 5.59 -1 24 4 80.87 4.35 -1 -24 4 68.85 5.06 -1 24 4 71.88 5.00 -1 -24 3 6.95 3.08 -1 -24 3 9.96 2.82 -1 -24 3 2.59 2.23 -1 24 3 5.02 2.15 1 -24 -3 4.21 2.72 1 -24 -3 6.87 2.17 -1 24 3 7.04 2.62 -1 -24 3 7.20 2.89 -1 24 3 8.85 3.28 -1 -24 2 521.63 21.82 -1 -24 2 593.55 21.89 -1 24 2 562.10 21.70 -1 24 2 545.22 22.05 1 -24 -2 513.63 21.82 1 -24 -2 536.28 21.45 1 24 -2 504.56 21.18 -1 -24 2 525.09 21.33 -1 24 2 533.20 21.38 -1 -24 2 511.06 21.91 -1 24 1 47.25 3.79 -1 -24 1 42.74 3.08 -1 24 1 47.91 3.21 1 -24 -1 45.18 4.26 -1 -24 1 43.32 3.70 1 -24 -1 38.89 3.25 1 24 -1 46.82 2.93 1 -24 0 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4.99 3.51 -2 27 -2 3.42 2.99 2 -27 2 3.67 3.22 2 -27 2 4.10 2.84 2 -27 2 1.61 2.65 2 -27 3 98.48 6.38 2 27 3 102.99 6.13 -2 27 -3 103.72 5.68 -2 -27 -3 102.60 5.83 -2 27 -3 92.07 6.14 2 -27 3 98.15 6.13 2 -27 3 104.35 6.20 2 -27 3 92.57 5.63 -2 27 -3 90.76 5.24 2 -27 4 2.76 3.04 -2 -27 -4 4.69 2.92 2 -27 4 4.40 3.59 2 27 4 4.25 3.26 -2 27 -4 4.45 2.30 -2 27 -4 4.97 3.19 2 -27 4 3.68 3.31 2 -27 4 2.33 2.75 -2 27 -5 88.78 5.35 2 -27 5 93.73 4.91 2 -27 5 95.45 5.73 2 27 5 104.94 6.23 -2 27 -5 86.09 4.74 -2 -27 -5 102.66 5.83 2 -27 5 95.55 6.20 2 27 5 92.45 5.51 2 -27 5 101.14 6.14 2 -27 6 18.39 2.38 2 -27 6 13.74 3.82 2 -27 6 13.90 2.70 2 27 6 10.17 3.32 2 27 6 15.25 2.97 -2 -27 -6 17.58 3.20 2 -27 7 44.16 3.06 2 27 7 40.70 4.07 2 -27 7 39.40 4.34 2 -27 7 41.08 3.86 -2 -27 -7 49.35 3.87 2 27 7 45.30 3.67 2 27 8 38.25 3.17 2 -27 8 39.95 2.72 -2 -27 -8 44.11 3.39 2 -27 8 42.63 3.40 -2 -27 -9 42.70 2.79 2 -27 9 37.13 2.62 -2 28 10 9.70 1.43 -2 28 10 10.18 1.40 -2 28 9 2.45 1.78 -2 -28 9 2.04 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2.61 -2 30 -1 4.83 2.86 2 -30 1 2.24 2.13 -2 30 -2 20.64 3.16 2 -30 2 17.91 3.72 2 -30 2 23.37 3.77 -2 30 -2 15.51 2.51 -2 30 -2 15.70 3.74 2 -30 2 19.48 2.89 2 -30 2 20.07 3.04 -2 30 -3 8.05 2.14 2 30 3 4.86 2.47 -2 30 -3 7.70 2.43 2 -30 3 7.39 2.71 -2 30 -3 6.32 3.13 2 -30 3 2.33 3.31 2 -30 3 2.98 3.13 -2 -30 -3 10.17 2.51 2 -30 3 5.36 2.53 2 -30 4 283.00 12.66 2 -30 4 301.73 13.06 -2 30 -4 285.95 12.13 2 30 4 276.82 12.63 -2 -30 -4 285.81 12.37 -2 30 -4 297.06 12.64 -2 30 -4 281.35 12.15 2 -30 4 293.65 12.74 2 -30 5 32.98 3.21 2 30 5 30.22 3.41 -2 30 -5 23.55 2.75 -2 -30 -5 32.35 3.20 2 -30 5 30.66 3.90 2 -30 5 31.09 3.59 -2 30 -5 32.93 2.69 2 30 6 26.23 3.04 2 -30 6 24.69 2.58 -2 -30 -6 21.06 2.75 2 -30 6 23.49 3.53 2 -30 6 27.35 3.00 -2 30 -6 24.16 2.33 2 30 7 29.59 2.81 -2 -30 -7 32.37 2.69 -2 30 -7 32.17 2.33 2 -30 8 111.06 5.09 2 30 8 119.68 5.27 -2 31 8 38.61 2.42 -2 31 8 44.62 2.83 -2 -31 8 36.15 2.43 2 -31 -7 96.60 4.67 -2 31 7 92.83 4.83 -2 31 7 97.64 4.79 -2 -31 7 98.16 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3.65 -4 21 2 42.77 4.31 -4 -21 2 40.40 3.52 -4 21 2 43.78 3.37 -4 21 1 19.09 2.59 4 -21 -1 18.35 3.35 -4 -21 1 19.64 3.52 4 -21 -1 17.59 2.37 -4 21 1 21.59 3.14 -4 21 1 20.28 2.53 -4 21 1 15.98 3.50 -4 21 1 18.26 3.78 -4 -21 1 14.47 2.49 4 -21 0 36.59 2.86 -4 21 0 38.56 3.48 -4 21 0 41.95 4.16 -4 -21 0 40.16 4.02 -4 21 0 32.69 4.21 4 -21 0 42.10 3.88 4 -21 0 34.18 3.53 4 -21 0 39.46 3.44 -4 21 0 38.08 3.23 -4 21 -1 2.03 2.23 4 -21 1 3.76 1.79 -4 21 -1 5.39 2.33 -4 -21 -1 2.53 3.15 -4 21 -1 4.52 3.20 4 -21 1 4.24 2.60 4 -21 1 6.56 2.87 4 -21 1 4.73 2.37 -4 21 -2 114.13 5.85 -4 21 -2 120.79 6.51 -4 -21 -2 103.65 6.65 4 -21 2 110.20 6.33 4 -21 2 115.72 6.20 4 -21 2 110.13 5.91 -4 21 -2 112.87 5.91 -4 21 -3 97.34 5.05 -4 21 -3 97.59 5.74 -4 -21 -3 90.09 6.00 -4 21 -3 92.65 6.08 4 -21 3 96.52 5.79 4 -21 3 92.00 5.31 -4 21 -4 79.01 4.92 -4 21 -4 75.74 5.27 4 -21 4 72.45 5.29 4 21 4 66.76 5.72 4 -21 4 72.73 5.83 4 -21 4 63.27 4.55 4 -21 5 0.33 2.99 -4 21 -5 1.11 2.61 4 -21 5 3.05 3.42 4 21 5 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2.02 2.19 -4 22 7 132.99 6.34 -4 -22 7 138.51 6.61 -4 22 7 124.79 7.00 4 -22 -7 128.50 6.64 4 -22 -7 133.64 6.75 -4 22 7 128.16 7.12 -4 22 7 129.70 6.08 -4 22 7 131.28 7.46 -4 -22 7 116.52 6.59 -4 -22 6 59.60 3.96 -4 22 6 51.75 4.55 4 -22 -6 54.17 4.00 -4 22 6 53.85 4.06 -4 22 6 57.51 3.69 4 -22 -6 57.71 4.41 -4 22 6 53.74 3.38 -4 22 6 49.50 4.93 -4 -22 6 51.48 4.17 -4 -22 5 100.28 5.87 4 -22 -5 107.32 6.03 4 -22 -5 114.16 6.07 -4 -22 5 118.61 5.84 -4 22 5 111.76 6.61 -4 22 5 109.45 6.22 -4 -22 5 102.88 6.11 -4 22 5 129.28 6.47 -4 22 5 112.85 5.69 4 -22 -5 113.45 6.58 -4 22 5 109.75 5.38 -4 -22 5 96.93 6.17 -4 22 5 114.75 5.98 -4 -22 4 268.80 12.09 -4 -22 4 255.94 12.16 4 -22 -4 278.94 11.99 -4 22 4 264.27 12.19 -4 -22 4 284.70 11.84 -4 22 4 279.31 12.52 -4 22 4 275.91 11.60 -4 22 4 272.35 12.42 -4 -22 4 262.76 12.26 -4 22 4 282.94 11.75 4 -22 -4 275.77 12.61 -4 22 4 269.97 11.45 -4 22 4 283.54 12.35 -4 22 4 273.10 11.93 -4 22 3 10.73 2.54 -4 22 3 11.10 2.80 -4 -22 3 13.09 4.60 4 -22 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5.16 3.05 -4 -22 -3 5.37 3.29 -4 22 -3 5.51 3.47 4 -22 3 3.73 3.13 4 -22 3 3.53 3.49 -4 22 -4 74.67 5.18 4 -22 4 64.79 5.22 -4 22 -4 69.64 4.67 4 -22 4 61.56 5.14 4 22 4 73.20 5.36 4 -22 4 65.27 5.55 4 -22 4 61.53 4.42 4 -22 5 -0.33 2.98 -4 22 -5 2.44 2.43 4 22 5 2.06 3.44 4 -22 5 -1.41 3.25 4 22 6 10.83 3.75 -4 22 -6 10.50 2.45 -4 -22 -6 12.55 3.54 4 -22 6 14.06 3.70 4 22 6 19.33 3.90 4 -22 6 17.25 3.81 4 -22 7 243.18 10.25 4 22 7 215.53 11.02 -4 22 -7 230.87 9.99 -4 -22 -7 251.93 10.96 4 22 7 233.57 11.16 4 -22 7 256.69 11.18 4 -22 8 0.86 2.11 -4 22 -8 1.91 1.58 -4 -22 -8 -0.58 2.71 4 22 8 0.68 2.94 4 -22 8 -1.40 2.86 4 -22 9 2.05 1.71 4 22 9 0.93 2.49 -4 -22 -9 -2.80 2.27 4 22 9 3.00 2.37 4 -22 9 0.67 2.12 4 -22 9 -1.65 3.37 4 -22 10 9.21 1.33 4 22 10 9.25 1.78 -4 -22 -10 9.24 1.64 4 22 10 9.19 1.68 -4 -23 11 20.26 1.72 -4 23 11 22.61 1.88 -4 23 10 -0.32 1.82 -4 -23 10 0.73 1.59 -4 23 10 0.33 1.52 4 -23 -10 -0.25 1.55 -4 23 10 -0.86 1.42 -4 -23 9 11.33 1.97 -4 -23 9 16.41 2.30 4 -23 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3.77 3.58 -5 7 8 -0.36 2.04 -5 7 8 3.31 2.33 -5 -7 7 202.82 8.93 5 -7 -7 176.74 8.45 -5 7 7 213.39 8.60 -5 -7 7 193.28 8.51 -5 -7 7 187.16 8.90 -5 7 7 200.94 8.60 -5 7 7 181.11 8.77 -5 7 7 178.89 8.78 -5 -7 7 189.68 8.78 -5 7 7 194.38 8.51 -5 7 7 194.30 8.77 -5 7 7 195.58 9.82 -5 7 6 3.52 1.99 5 -7 -6 4.46 1.75 -5 -7 6 6.01 2.24 -5 7 6 7.34 1.70 -5 -7 6 4.28 1.55 -5 7 6 5.99 1.95 -5 -7 6 3.08 1.96 -5 7 6 3.06 2.14 -5 7 6 7.57 3.03 -5 7 6 6.22 1.80 5 -7 -5 11.82 1.83 -5 -7 5 8.54 2.14 -5 7 5 11.15 2.04 -5 7 5 11.73 2.08 -5 -7 5 13.14 3.12 -5 7 5 11.46 1.93 -5 -7 5 12.19 2.29 -5 -7 5 11.47 2.03 -5 7 5 11.95 2.27 -5 7 5 12.46 3.04 -5 7 5 12.24 1.88 -5 7 4 377.99 15.66 -5 -7 4 346.43 14.84 -5 -7 4 366.59 14.93 -5 -7 4 346.30 14.75 -5 7 4 359.53 14.79 -5 7 4 344.25 14.79 -5 7 4 365.42 14.73 -5 7 4 368.39 14.58 -5 -7 4 367.03 14.52 -5 -7 4 382.37 14.86 -5 -7 4 381.39 15.40 -5 7 4 352.57 14.91 -5 7 4 361.78 14.69 -5 -7 4 365.08 14.66 -5 7 4 344.80 14.42 -5 -7 3 1608.92 61.01 -5 7 3 1565.87 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28.59 2.74 -5 14 11 30.36 2.45 -5 14 11 32.51 2.66 5 -14 -11 39.60 2.90 -5 14 11 29.91 3.74 -5 -14 10 25.89 2.95 5 -14 -10 28.16 2.53 -5 14 10 29.76 2.94 -5 14 10 29.06 2.83 -5 14 10 31.71 4.20 -5 14 10 28.26 2.22 5 -14 -10 28.87 2.89 -5 14 10 22.14 2.26 -5 -14 9 80.03 4.36 5 -14 -9 71.83 4.31 -5 14 9 84.10 4.63 -5 14 9 66.12 4.08 5 -14 -9 71.15 4.60 -5 14 9 70.72 4.74 -5 14 9 76.14 4.47 -5 14 9 89.47 6.16 -5 14 9 68.60 3.89 -5 -14 8 40.97 3.32 -5 14 8 38.46 3.13 -5 -14 8 41.65 3.75 -5 14 8 34.61 2.60 -5 14 8 37.54 3.38 -5 14 8 37.94 2.87 -5 14 8 40.78 3.39 5 -14 -8 36.40 3.19 -5 14 8 43.46 3.85 -5 14 8 32.60 4.63 -5 14 8 32.40 2.62 5 -14 -7 30.54 3.04 -5 -14 7 32.11 3.14 -5 14 7 30.81 2.36 -5 -14 7 31.14 3.43 -5 14 7 31.33 3.31 -5 14 7 27.88 2.57 -5 14 7 27.40 2.55 -5 14 7 34.26 3.22 -5 14 7 34.29 3.03 -5 14 7 33.55 3.82 -5 14 7 29.80 4.32 -5 -14 7 26.15 2.87 -5 14 7 29.71 2.42 -5 14 6 295.62 13.74 5 -14 -6 295.13 12.46 -5 -14 6 306.96 12.65 5 -14 -6 288.18 12.45 -5 14 6 269.58 12.05 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3.18 -5 21 8 54.71 4.72 -5 -21 7 12.63 2.31 -5 -21 7 9.64 2.47 -5 21 7 13.60 2.92 5 -21 -7 16.01 2.65 5 -21 -7 9.80 2.87 -5 21 7 13.59 3.10 -5 21 7 12.78 1.98 -5 21 7 14.02 3.61 -5 21 7 13.78 2.34 -5 -21 7 9.32 2.49 -5 -21 6 22.57 2.87 -5 -21 6 28.76 3.03 -5 21 6 26.29 2.48 -5 21 6 27.52 3.57 5 -21 -6 28.72 3.12 -5 21 6 30.93 2.83 5 -21 -6 25.72 3.53 -5 21 6 29.05 3.64 -5 -21 6 24.27 2.99 -5 -21 5 104.60 5.88 5 -21 -5 116.62 6.06 -5 -21 5 108.07 5.79 -5 21 5 112.30 6.42 -5 21 5 109.46 5.51 -5 21 5 109.71 6.05 -5 -21 5 112.78 6.48 5 -21 -5 114.98 6.40 -5 21 5 116.21 5.70 -5 21 5 103.85 5.46 -5 -21 5 93.70 5.78 -5 21 5 116.29 5.88 -5 -21 4 35.81 3.47 5 -21 -4 43.03 3.52 -5 -21 4 39.61 3.21 -5 21 4 31.13 3.93 -5 21 4 38.36 3.12 -5 21 4 36.33 3.73 -5 -21 4 39.81 4.12 -5 21 4 39.10 3.20 -5 21 4 32.82 3.61 -5 21 4 38.95 3.86 -5 -21 4 30.93 3.31 -5 21 4 37.78 3.33 -5 -21 3 149.12 7.92 5 -21 -3 183.82 7.97 -5 -21 3 151.22 7.43 -5 21 3 153.49 8.18 -5 21 3 172.20 7.68 -5 21 3 170.32 8.32 -5 -21 3 160.64 8.53 -5 21 3 162.77 8.22 5 -21 -3 155.75 8.34 -5 21 3 156.27 7.65 -5 21 2 3.13 2.16 -5 -21 2 -3.11 4.41 5 -21 -2 3.70 2.35 -5 21 2 1.10 3.39 -5 21 2 2.81 2.31 -5 -21 2 1.17 3.24 -5 21 2 5.73 3.45 5 -21 -2 1.02 2.53 5 -21 -1 76.39 4.49 -5 21 1 73.64 5.00 -5 21 1 70.96 4.49 -5 21 1 79.38 5.41 -5 -21 1 73.40 5.48 -5 21 1 76.14 5.52 5 -21 -1 63.62 5.15 5 -21 -1 67.26 4.52 -5 21 1 76.60 4.45 -5 21 0 -0.65 2.23 5 -21 0 1.45 2.10 -5 -21 0 0.80 3.44 -5 21 0 3.37 2.77 -5 21 0 1.47 3.28 -5 21 0 4.29 3.54 5 -21 0 2.14 2.50 5 -21 0 1.03 2.93 5 -21 0 3.38 2.54 -5 21 -1 8.66 2.28 -5 21 -1 10.37 2.79 -5 21 -1 11.88 2.60 -5 -21 -1 15.39 3.61 -5 21 -1 12.87 3.70 5 -21 1 14.66 2.86 5 -21 1 14.45 3.12 5 -21 1 11.05 2.46 -5 21 -2 10.35 2.49 -5 21 -2 14.78 2.71 -5 21 -2 18.65 3.62 -5 21 -2 12.14 2.77 5 -21 2 13.61 3.02 5 -21 2 13.07 2.86 5 -21 2 8.66 2.57 -5 21 -3 16.01 2.49 -5 21 -3 21.95 2.69 -5 21 -3 23.77 3.70 -5 21 -3 13.90 2.69 -5 21 -3 18.86 3.65 5 -21 3 18.90 3.26 5 -21 3 13.95 2.70 -5 21 -4 2.74 2.08 -5 21 -4 2.96 2.33 -5 -21 -4 2.94 3.37 5 -21 4 1.81 2.93 5 21 4 -2.04 3.33 5 -21 4 2.33 2.41 5 -21 5 5.17 3.08 -5 21 -5 8.33 2.72 -5 21 -5 3.49 2.10 5 -21 5 6.89 3.25 5 21 5 6.32 3.68 -5 -21 -5 5.68 3.34 -5 -21 -6 3.71 3.04 -5 21 -6 0.25 2.21 -5 21 -6 -1.08 1.90 5 -21 6 3.67 2.99 5 21 6 -0.42 3.49 5 -21 6 -1.60 3.61 5 -21 7 119.53 5.81 5 21 7 97.64 6.50 -5 21 -7 114.88 5.62 -5 -21 -7 112.11 6.35 5 21 7 110.10 6.68 5 -21 7 125.49 6.75 -5 21 -8 11.04 1.58 5 -21 8 13.09 2.15 5 21 8 11.29 2.85 -5 21 -8 9.94 1.65 -5 -21 -8 11.45 2.61 5 21 8 10.51 2.85 5 -21 8 7.84 2.79 5 -21 8 8.70 3.43 5 -21 9 41.06 2.47 -5 -21 -9 37.81 2.75 5 21 9 34.98 2.92 -5 -22 11 3.65 1.08 -5 -22 10 3.79 1.55 5 -22 -10 7.31 1.58 -5 22 10 8.46 1.82 -5 22 10 3.77 1.35 -5 -22 9 2.67 1.86 5 -22 -9 0.79 1.83 -5 22 9 4.86 1.96 -5 22 9 1.94 2.23 -5 22 9 2.80 1.60 -5 -22 8 221.70 9.61 5 -22 -8 218.34 9.53 -5 22 8 220.78 9.67 5 -22 -8 212.92 9.61 -5 22 8 221.16 9.37 5 -22 -8 201.32 9.37 -5 22 8 216.04 9.86 -5 -22 7 124.20 6.37 -5 22 7 140.44 6.79 5 -22 -7 127.99 6.39 -5 22 7 137.01 6.27 5 -22 -7 132.36 6.67 -5 22 7 134.40 6.79 -5 22 7 124.12 5.94 -5 -22 6 31.03 3.27 -5 -22 6 35.73 3.18 -5 22 6 40.68 3.88 -5 22 6 38.46 3.02 5 -22 -6 36.86 3.79 -5 22 6 34.55 2.67 -5 22 6 32.79 3.59 -5 -22 6 27.86 3.12 -5 22 5 4.05 2.35 -5 -22 5 8.09 2.69 5 -22 -5 5.60 2.45 -5 -22 5 4.63 2.23 -5 22 5 4.80 3.03 -5 22 5 4.99 2.54 -5 22 5 1.75 1.77 -5 -22 5 5.36 3.10 5 -22 -5 3.26 3.16 -5 22 5 2.41 1.63 -5 22 5 0.76 2.09 -5 -22 5 1.42 2.49 -5 22 4 1.89 2.30 -5 -22 4 -0.75 2.89 5 -22 -4 3.78 2.45 -5 -22 4 3.20 2.03 -5 22 4 0.54 3.06 -5 22 4 2.06 2.83 -5 22 4 3.66 2.06 -5 -22 4 2.78 3.13 -5 22 4 1.88 2.79 -5 22 4 3.32 2.16 -5 22 4 4.87 2.85 -5 -22 4 2.03 2.65 -5 22 3 21.21 2.74 -5 -22 3 21.46 4.45 5 -22 -3 15.50 2.62 -5 22 3 18.73 3.26 -5 22 3 17.63 3.44 -5 22 3 18.45 2.59 -5 -22 3 22.43 3.68 -5 22 3 22.04 3.52 5 -22 -3 19.98 3.79 -5 22 2 9.95 2.37 5 -22 -2 10.68 2.46 -5 22 2 11.01 3.43 -5 22 2 9.94 2.46 -5 22 2 10.14 3.42 5 -22 -2 16.43 3.70 -5 -22 2 11.07 3.47 5 -22 -2 10.04 2.71 5 -22 -1 62.89 4.25 -5 22 1 76.30 4.82 -5 22 1 62.31 4.32 -5 22 1 70.41 5.24 -5 -22 1 73.23 5.27 -5 22 1 68.40 5.43 5 -22 -1 67.39 5.10 5 -22 -1 66.10 4.47 -5 22 1 69.59 4.36 -5 22 0 6.20 2.31 5 -22 0 3.94 2.12 -5 22 0 9.10 2.73 -5 22 0 10.08 3.42 -5 -22 0 7.58 3.33 -5 22 0 5.74 3.80 5 -22 0 6.10 2.64 5 -22 0 6.03 3.14 5 -22 0 8.43 2.80 5 -22 0 5.41 2.57 5 -22 1 65.49 4.16 -5 22 -1 71.96 4.59 -5 22 -1 71.05 4.65 -5 -22 -1 79.49 5.58 5 -22 1 64.44 4.65 5 -22 1 69.61 5.14 5 -22 1 66.95 4.48 -5 22 -1 73.52 4.50 -5 22 -1 79.76 5.55 5 -22 1 73.87 4.98 -5 22 -2 25.20 2.81 5 -22 2 26.80 2.52 -5 22 -2 26.64 3.00 -5 22 -2 31.55 3.84 -5 22 -2 20.87 2.97 5 -22 2 22.44 3.39 5 -22 2 27.75 3.39 5 -22 2 27.67 4.08 5 -22 2 25.24 3.04 -5 22 -3 67.40 4.43 -5 22 -3 72.60 5.02 -5 22 -3 69.11 5.25 5 -22 3 62.96 4.79 5 -22 3 63.92 5.29 5 -22 3 65.99 4.34 -5 22 -3 65.60 4.20 -5 22 -4 4.34 2.14 5 -22 4 7.13 3.51 -5 22 -4 2.53 2.25 -5 -22 -4 7.54 3.26 5 -22 4 5.74 3.06 5 -22 4 2.06 3.61 5 -22 4 5.87 2.43 -5 22 -5 3.57 2.04 5 -22 5 0.60 2.91 -5 22 -5 -2.13 2.39 -5 -22 -5 -3.89 3.29 -5 22 -5 0.73 2.10 5 -22 5 -0.18 3.03 5 22 5 -2.64 3.27 5 22 6 100.81 6.30 -5 22 -6 106.44 5.25 -5 22 -6 106.58 5.46 -5 -22 -6 115.74 6.30 5 -22 6 89.36 6.05 5 22 6 105.79 6.37 5 -22 6 100.17 6.44 -5 22 -6 105.86 5.23 5 -22 7 26.99 2.64 5 22 7 21.68 3.41 -5 22 -7 22.11 2.34 -5 -22 -7 22.93 3.20 5 22 7 21.98 3.35 5 -22 7 28.03 3.63 -5 22 -7 26.27 2.20 5 -22 8 46.76 3.02 5 22 8 47.99 3.68 -5 22 -8 45.41 2.59 -5 -22 -8 45.97 3.49 5 22 8 41.62 3.45 5 -22 8 46.01 3.49 5 -22 8 48.01 4.30 -5 22 -8 43.47 2.59 5 -22 9 6.43 1.34 -5 -22 -9 4.70 1.64 -5 -23 10 25.88 2.00 -5 23 10 25.13 1.87 -5 -23 9 206.31 8.77 -5 23 9 201.16 8.72 5 -23 -9 201.88 8.73 -5 23 9 193.66 8.59 -5 23 9 213.76 9.00 -5 -23 8 1.96 1.90 -5 23 8 2.34 2.18 -5 23 8 2.73 2.38 -5 23 8 3.22 1.74 -5 -23 7 27.15 2.81 -5 23 7 34.79 3.40 -5 23 7 28.76 2.67 5 -23 -7 32.39 3.25 -5 23 7 34.00 3.42 -5 23 7 29.17 2.32 -5 -23 6 13.82 2.41 -5 23 6 13.66 3.07 5 -23 -6 7.07 2.98 -5 23 6 9.40 1.71 -5 23 6 10.77 2.19 -5 -23 6 10.56 2.54 -5 23 5 16.85 2.57 5 -23 -5 14.49 2.81 -5 -23 5 14.01 2.36 -5 23 5 11.86 3.23 -5 23 5 16.05 2.93 -5 23 5 16.38 2.08 -5 -23 5 15.86 3.32 5 -23 -5 13.79 3.46 -5 23 5 11.96 3.04 -5 23 5 12.77 1.82 -5 23 5 10.53 2.30 -5 -23 5 11.86 2.68 -5 23 4 0.27 2.20 5 -23 -4 -1.19 2.29 -5 -23 4 1.01 1.90 -5 23 4 -0.71 2.89 -5 23 4 -4.28 3.01 -5 23 4 1.66 1.93 -5 -23 4 1.80 2.88 -5 23 4 0.78 2.72 -5 23 4 -0.51 2.73 -5 23 4 -1.60 1.52 -5 23 4 2.77 1.98 -5 -23 4 5.31 2.42 -5 23 3 19.10 2.73 5 -23 -3 23.07 2.95 -5 23 3 18.76 3.56 -5 23 3 19.44 2.52 -5 -23 3 23.10 3.61 -5 23 3 18.57 3.53 5 -23 -3 25.64 3.85 -5 23 2 11.78 2.52 5 -23 -2 8.91 2.49 -5 23 2 19.83 3.67 -5 23 2 12.16 2.46 -5 23 2 13.40 3.58 5 -23 -2 12.14 3.46 5 -23 -2 13.22 2.95 -5 -23 2 12.85 3.39 -5 23 1 3.75 2.33 5 -23 -1 7.20 2.25 -5 23 1 3.82 2.86 -5 23 1 7.16 3.56 -5 23 1 3.14 2.32 -5 -23 1 4.31 3.24 -5 23 1 3.15 3.42 5 -23 -1 6.00 3.19 5 -23 -1 5.94 2.78 -5 23 0 23.85 2.91 5 -23 0 22.62 2.52 -5 23 0 28.29 3.22 -5 23 0 24.79 3.88 -5 23 0 20.07 2.93 -5 -23 0 23.62 3.68 -5 23 0 25.51 4.04 5 -23 0 26.15 3.32 5 -23 0 20.82 3.65 5 -23 0 24.58 3.20 5 -23 0 20.77 2.88 -5 23 -1 20.17 2.84 5 -23 1 28.95 2.59 -5 -23 -1 24.79 4.12 -5 23 -1 26.83 3.15 -5 23 -1 22.33 2.88 -5 23 -1 29.70 4.21 5 -23 1 26.24 3.43 5 -23 1 24.15 3.49 5 -23 1 25.97 3.62 5 -23 1 25.73 3.11 -5 23 -2 1.45 2.25 -5 23 -2 3.97 2.41 -5 23 -2 3.06 3.28 -5 23 -2 1.40 2.38 -5 -23 -2 6.17 3.31 5 -23 2 0.50 2.65 5 -23 2 2.50 2.64 5 -23 2 3.45 3.27 5 -23 2 -2.04 2.35 5 23 3 127.90 7.07 -5 23 -3 127.91 6.40 -5 23 -3 130.46 6.87 5 -23 3 118.49 7.15 5 -23 3 119.00 6.76 5 -23 3 111.65 6.24 -5 23 -3 116.14 6.16 -5 23 -4 18.42 2.48 5 -23 4 16.20 3.71 5 23 4 16.61 3.62 -5 23 -4 21.09 2.72 5 -23 4 23.34 3.54 5 -23 4 24.13 4.01 5 -23 4 16.20 2.65 5 -23 5 30.79 3.43 -5 23 -5 27.23 2.79 5 23 5 31.33 4.05 -5 23 -5 29.84 3.02 -5 -23 -5 33.46 3.87 5 -23 5 37.41 3.80 5 23 5 30.05 3.62 5 -23 5 26.79 4.14 -5 23 -5 28.09 2.68 -5 23 -6 6.86 1.89 -5 -23 -6 4.84 2.91 5 -23 6 6.12 2.12 5 23 6 7.64 3.10 -5 23 -6 5.74 2.11 -5 23 -6 6.44 1.79 5 -23 6 4.61 2.99 5 23 6 3.58 2.71 5 -23 7 145.78 6.29 5 23 7 119.61 6.78 -5 23 -7 127.30 6.06 -5 -23 -7 142.35 6.80 5 23 7 126.90 6.69 5 -23 7 155.62 7.13 -5 23 -7 125.35 5.98 5 -23 8 61.07 3.21 5 23 8 55.13 3.76 -5 23 -8 49.43 2.76 -5 -23 -8 56.39 3.57 5 23 8 51.71 3.41 5 -23 8 63.93 3.76 5 -23 8 52.96 4.23 -5 24 10 0.19 1.19 -5 -24 10 0.31 1.18 5 -24 -10 -0.41 1.21 -5 -24 9 0.26 1.49 5 -24 -9 1.68 1.53 -5 24 9 -3.50 1.73 -5 24 9 0.61 1.87 -5 24 9 0.54 1.33 -5 -24 8 103.83 5.30 -5 24 8 101.97 5.45 -5 24 8 104.00 5.16 -5 -24 7 31.19 2.75 5 -24 -7 32.60 3.08 -5 24 7 32.14 3.23 -5 24 7 29.68 2.57 5 -24 -7 27.30 3.02 -5 24 7 31.61 3.24 -5 24 7 26.21 2.09 -5 -24 6 37.43 2.98 -5 24 6 35.93 3.64 -5 24 6 38.77 3.17 -5 24 6 30.59 2.85 5 -24 -6 38.22 3.77 -5 24 6 33.88 2.42 -5 24 5 4.52 2.32 -5 -24 5 2.37 1.97 -5 24 5 3.36 2.87 -5 24 5 3.91 2.62 -5 24 5 4.82 1.65 -5 -24 5 1.77 2.85 5 -24 -5 4.73 3.03 -5 24 5 0.33 2.73 -5 24 5 2.77 1.37 -5 24 5 4.55 2.07 -5 -24 5 5.14 2.43 5 -24 -5 2.27 2.31 5 -24 -4 48.62 3.65 -5 24 4 49.80 4.39 -5 24 4 46.99 3.23 -5 24 4 49.30 4.20 -5 24 4 50.65 4.02 -5 -24 4 41.25 4.09 -5 24 4 47.66 3.34 -5 24 4 43.53 3.53 -5 24 3 0.67 2.24 5 -24 -3 3.00 2.35 -5 24 3 -2.89 3.04 -5 24 3 -1.50 2.06 -5 -24 3 -0.36 3.13 -5 24 3 1.90 2.98 5 -24 -3 -0.58 3.34 -5 24 3 0.50 1.94 -5 24 2 3.62 2.31 5 -24 -2 3.61 2.07 -5 24 2 8.99 3.07 -5 -24 2 4.49 3.00 -5 24 2 5.96 3.34 -5 24 2 1.98 2.16 -5 24 2 3.19 3.29 5 -24 -2 5.02 3.46 -5 24 1 -1.21 2.25 5 -24 -1 -0.40 2.05 -5 24 1 0.49 2.66 -5 24 1 -1.88 3.20 -5 24 1 2.98 2.21 -5 -24 1 3.65 3.09 -5 24 1 -1.17 3.50 5 -24 -1 2.22 2.67 5 -24 -1 -0.38 3.30 5 -24 -1 3.21 2.56 -5 24 0 7.53 2.44 5 -24 0 12.22 2.21 -5 24 0 7.10 2.54 -5 24 0 6.55 3.38 -5 24 0 10.87 2.55 -5 -24 0 9.00 3.43 -5 24 0 15.28 3.99 5 -24 0 7.02 2.68 5 -24 0 11.85 3.29 5 -24 0 10.98 2.72 -5 24 -1 -1.20 2.21 5 -24 1 1.55 1.90 -5 24 -1 2.01 2.38 -5 -24 -1 1.96 3.06 -5 24 -1 3.33 3.56 5 -24 1 1.13 2.66 5 -24 1 1.85 2.76 5 -24 1 -2.88 2.91 5 -24 1 2.93 2.46 -5 24 -2 110.05 5.75 -5 24 -2 111.50 5.87 -5 24 -2 116.53 6.53 -5 -24 -2 100.83 6.62 5 -24 2 113.30 6.26 5 -24 2 110.27 5.99 5 -24 2 110.97 6.46 5 -24 2 100.66 5.78 -5 24 -2 105.04 5.69 5 -24 3 69.99 5.33 5 24 3 57.37 4.57 -5 24 -3 62.58 4.12 -5 -24 -3 52.83 4.79 -5 24 -3 62.05 4.91 5 -24 3 59.37 4.59 5 -24 3 61.28 4.93 5 -24 3 54.17 3.97 -5 24 -3 59.06 3.95 5 -24 4 37.73 4.21 -5 24 -4 34.16 3.11 5 24 4 30.19 3.92 5 -24 4 43.77 4.03 5 -24 4 35.82 4.28 5 -24 4 32.80 3.11 -5 24 -4 33.58 2.91 -5 24 -5 16.53 2.31 5 -24 5 22.02 3.10 5 24 5 21.62 3.41 -5 24 -5 20.08 2.69 -5 24 -5 19.37 2.45 5 -24 5 19.80 3.40 5 -24 5 21.51 3.70 5 -24 6 108.86 5.09 5 24 6 98.27 5.88 -5 24 -6 96.42 4.91 -5 24 -6 103.76 5.07 -5 -24 -6 108.68 5.94 5 -24 6 88.12 5.61 5 24 6 93.39 5.45 -5 24 -6 100.92 4.93 -5 24 -7 7.60 1.56 5 -24 7 8.46 1.90 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25 3 63.12 4.84 -5 -25 3 59.71 4.62 -5 25 3 62.14 3.86 5 -25 -3 69.80 4.93 -5 25 3 61.79 4.02 -5 25 2 7.71 2.47 5 -25 -2 9.70 2.33 -5 25 2 14.82 3.07 -5 25 2 16.33 3.57 -5 25 2 12.88 2.41 -5 -25 2 10.31 3.26 -5 25 2 10.48 3.45 5 -25 -2 13.96 3.54 -5 25 1 4.67 2.28 -5 -25 1 2.24 3.01 5 -25 -1 5.32 2.03 -5 25 1 1.11 2.55 -5 25 1 2.60 3.13 -5 25 1 4.27 2.27 -5 25 1 1.73 3.45 5 -25 -1 1.10 2.57 5 -25 -1 3.72 3.21 5 -25 -1 3.04 2.56 5 -25 0 50.52 3.56 -5 25 0 60.39 4.13 -5 25 0 58.21 3.91 -5 25 0 53.45 4.76 -5 -25 0 49.93 4.71 -5 25 0 54.34 5.03 5 -25 0 60.74 4.29 5 -25 0 55.89 4.45 5 -25 0 57.02 4.02 -5 25 0 53.98 3.90 -5 25 -1 -1.06 2.13 5 -25 1 1.47 1.74 -5 25 -1 1.24 2.21 -5 -25 -1 -0.96 3.18 -5 25 -1 -0.19 3.55 5 -25 1 2.26 2.71 5 -25 1 -1.48 2.83 5 -25 1 2.54 2.72 5 -25 1 -1.95 2.49 -5 25 -2 5.03 2.25 -5 25 -2 6.63 2.13 -5 25 -2 6.31 3.13 -5 25 -2 4.44 2.37 -5 -25 -2 2.66 3.34 5 -25 2 4.09 2.91 5 -25 2 8.59 2.62 5 -25 2 5.61 3.08 5 -25 2 8.98 2.68 5 -25 3 119.07 6.90 5 25 3 106.59 6.31 -5 25 -3 121.58 6.02 -5 -25 -3 121.34 6.82 -5 25 -3 129.14 6.80 5 -25 3 106.16 6.33 5 -25 3 104.74 6.66 5 -25 3 110.93 5.95 -5 25 -3 113.68 5.83 5 -25 4 29.91 3.80 -5 25 -4 30.86 2.83 5 25 4 29.89 3.59 -5 25 -4 30.77 3.10 5 -25 4 35.78 3.81 5 -25 4 28.69 3.88 -5 25 -4 32.94 2.81 5 -25 5 36.89 3.38 5 -25 5 37.50 2.85 5 25 5 36.72 3.73 -5 25 -5 37.87 2.90 -5 25 -5 42.96 3.17 5 -25 5 31.67 3.66 5 -25 5 38.35 4.00 -5 25 -5 34.85 2.75 -5 25 -6 8.16 1.71 5 -25 6 3.22 1.70 5 25 6 2.71 2.52 -5 25 -6 5.65 1.77 -5 25 -6 7.09 1.69 -5 -25 -6 9.68 2.65 5 -25 6 6.71 2.53 5 -25 7 85.88 4.13 5 25 7 74.02 4.60 -5 25 -7 81.66 3.93 -5 -25 -7 85.40 4.78 5 -25 7 93.82 4.82 -5 25 -7 80.32 3.93 5 -25 8 9.22 1.40 5 25 8 7.97 1.75 -5 -25 -8 13.25 1.85 -5 26 9 0.24 1.04 -5 -26 9 3.14 1.17 -5 26 9 2.74 1.34 5 -26 -9 3.81 1.29 5 -26 -9 2.26 1.30 -5 26 8 86.54 4.34 -5 -26 8 92.16 4.41 -5 26 8 97.46 4.70 5 -26 -8 84.65 4.48 5 -26 -8 95.86 4.55 -5 -26 7 1.03 1.60 5 -26 -7 0.74 1.88 -5 26 7 -3.02 2.14 -5 26 7 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105.94 6.19 5 -26 6 143.49 6.52 -5 26 -6 140.69 5.78 5 -26 7 28.76 2.01 5 26 7 24.13 2.54 -5 -26 -7 28.00 2.64 5 -27 -9 -0.05 1.07 -5 -27 8 12.51 1.47 5 -27 -8 11.11 1.71 -5 27 8 11.24 1.87 -5 27 8 10.12 1.40 5 -27 -8 9.41 1.70 -5 -27 7 23.16 1.96 5 -27 -7 23.68 2.34 -5 27 7 23.19 2.52 -5 27 7 22.61 1.99 5 -27 -7 19.29 2.24 5 -27 -6 3.40 1.99 -5 27 6 0.51 2.29 -5 27 6 4.65 1.85 5 -27 -6 -0.38 2.39 -5 27 6 -0.18 1.52 5 -27 -6 1.07 1.98 -5 27 5 2.27 2.54 -5 27 5 2.58 2.34 5 -27 -5 2.38 2.72 -5 27 5 2.56 1.69 5 -27 -5 3.44 2.18 5 -27 -4 79.04 4.97 -5 27 4 77.50 4.18 -5 27 4 88.43 5.26 -5 -27 4 87.38 4.96 -5 27 4 81.15 4.40 -5 27 4 87.57 4.98 5 -27 -4 87.66 4.87 -5 27 4 83.14 4.63 -5 27 3 9.85 2.34 5 -27 -3 11.71 2.25 5 -27 -3 10.81 3.21 -5 27 3 11.39 2.87 -5 27 3 7.47 3.10 -5 27 3 9.15 1.99 -5 -27 3 11.52 2.75 -5 27 3 11.63 3.01 5 -27 -3 8.24 3.34 -5 27 3 11.16 1.97 5 -27 -3 9.04 2.58 5 -27 -2 113.05 5.75 5 -27 -2 109.43 6.66 -5 27 2 118.28 6.22 -5 27 2 111.58 5.71 -5 27 2 118.56 6.63 -5 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3.98 1.97 -7 -6 -2 6.63 1.92 -7 -6 -2 5.55 2.90 -7 6 -2 4.97 3.00 -7 6 -3 57.08 3.91 -7 6 -3 58.02 4.02 -7 -6 -3 63.97 4.00 7 6 3 51.40 3.86 7 6 4 3.14 2.41 7 -6 4 -1.72 3.22 -7 6 -4 1.96 2.41 -7 6 -4 -3.07 3.42 7 6 4 3.25 2.67 7 -6 4 2.67 2.45 -7 6 -4 1.26 2.45 -7 -6 -4 3.52 2.34 -7 6 -5 43.95 3.60 -7 6 -5 42.86 4.18 -7 6 -5 40.18 3.31 -7 -6 -5 45.09 3.44 7 6 5 35.74 3.58 7 -6 5 47.24 3.59 7 6 5 42.81 3.62 7 -6 5 41.48 3.96 -7 6 -6 57.55 4.22 -7 6 -6 62.54 4.57 -7 6 -6 66.26 4.12 -7 -6 -6 70.02 4.14 7 6 6 58.85 4.22 7 -6 6 69.17 4.12 7 6 6 59.56 4.29 7 -6 6 59.48 4.68 7 6 7 8.06 2.43 7 -6 7 6.14 2.81 -7 6 -7 2.24 2.29 7 6 7 5.68 2.38 7 -6 7 2.56 2.32 -7 6 -7 8.30 2.29 -7 -6 -7 1.90 2.05 7 6 8 10.13 2.09 7 -6 8 5.16 2.48 -7 6 -8 7.78 2.14 7 6 8 10.43 2.24 7 -6 8 8.12 2.17 7 6 8 7.40 4.37 -7 6 -8 8.50 1.93 -7 -6 -8 8.06 1.93 7 -6 9 55.89 3.15 -7 6 -9 77.05 3.49 -7 -6 -9 75.55 3.46 7 6 9 69.26 5.02 7 -6 9 49.87 4.11 7 6 9 62.00 3.47 7 -6 9 73.41 3.87 -7 7 12 26.45 2.05 7 -7 -12 27.22 1.84 -7 7 12 25.10 2.53 -7 7 12 27.82 1.66 -7 -7 12 25.59 1.69 -7 7 11 6.02 1.48 -7 -7 11 5.96 1.41 -7 -7 11 5.99 1.68 -7 7 11 5.91 1.84 7 -7 -11 9.05 1.77 -7 7 11 9.76 2.83 -7 -7 10 49.74 3.30 -7 7 10 45.07 3.42 -7 -7 10 43.04 3.09 -7 7 10 43.41 2.81 -7 -7 10 47.55 2.83 -7 7 10 42.42 3.20 -7 -7 10 36.99 3.08 7 -7 -10 46.53 3.16 -7 7 10 40.47 2.75 -7 7 10 42.01 2.98 -7 7 10 45.27 4.39 -7 7 10 47.88 3.07 -7 -7 10 45.32 2.94 -7 -7 9 91.87 5.10 -7 -7 9 86.14 5.01 -7 7 9 88.22 4.65 -7 -7 9 94.77 4.66 -7 7 9 88.26 4.73 -7 7 9 83.63 4.98 -7 -7 9 76.60 4.88 7 -7 -9 81.02 4.73 -7 7 9 92.78 4.55 -7 7 9 89.73 4.83 -7 7 9 89.49 6.21 -7 7 9 94.08 4.83 -7 -7 9 93.07 4.80 -7 -7 8 101.82 5.78 -7 7 8 95.78 5.63 -7 7 8 104.08 5.28 -7 -7 8 109.46 5.25 -7 -7 8 99.89 5.71 -7 7 8 102.39 5.39 -7 7 8 93.33 5.60 -7 -7 8 97.49 5.56 7 -7 -8 105.81 5.37 -7 7 8 100.64 5.11 -7 7 8 99.02 5.49 -7 7 8 97.65 6.91 -7 7 8 101.54 5.39 -7 -7 8 108.34 5.43 -7 7 7 287.00 13.75 -7 -7 7 336.07 14.08 -7 7 7 308.46 13.88 7 -7 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2.28 -7 -7 -5 2.12 2.24 -7 7 -6 216.14 9.98 -7 7 -6 212.39 10.27 -7 7 -6 241.15 9.88 -7 -7 -6 240.41 9.80 7 7 6 232.00 9.92 7 -7 6 217.75 9.80 7 7 6 207.49 9.85 7 -7 6 199.92 10.23 -7 7 -7 91.69 5.04 7 7 7 90.04 4.90 7 -7 7 96.17 4.94 -7 7 -7 98.67 4.86 -7 -7 -7 90.75 4.80 7 7 7 81.53 4.88 7 -7 7 80.86 5.28 7 7 8 5.01 1.97 7 -7 8 7.93 2.47 -7 7 -8 4.85 2.03 7 7 8 7.85 2.05 7 -7 8 5.96 2.01 7 7 8 8.62 4.25 -7 7 -8 9.25 1.91 -7 -7 -8 8.96 1.87 7 7 9 8.33 1.49 7 -7 9 6.12 1.89 7 -7 9 4.96 1.24 7 7 9 2.85 3.00 -7 7 -9 5.69 1.47 -7 -7 -9 2.77 1.36 -7 8 12 16.10 1.70 7 -8 -12 21.09 1.56 -7 8 12 15.64 2.18 -7 8 11 8.61 1.49 -7 -8 11 5.40 1.40 -7 -8 11 10.49 1.65 -7 8 11 13.08 1.95 7 -8 -11 8.09 1.69 -7 8 11 11.35 2.87 -7 8 10 13.53 1.87 -7 -8 10 14.81 1.84 -7 -8 10 15.71 2.37 -7 -8 10 13.60 2.18 -7 8 10 13.13 1.76 -7 -8 10 10.70 1.72 7 -8 -10 14.66 2.09 -7 8 10 12.12 1.97 -7 8 10 9.07 3.39 -7 8 10 12.45 1.85 -7 -8 9 168.09 7.83 -7 -8 9 168.32 7.78 -7 8 9 168.75 7.39 -7 -8 9 166.48 7.37 -7 8 9 156.33 7.40 -7 8 9 152.63 7.65 -7 -8 9 148.52 7.57 7 -8 -9 164.13 7.60 -7 8 9 162.44 7.34 -7 8 9 163.41 7.62 -7 8 9 163.96 9.01 -7 8 9 174.65 7.54 -7 -8 9 171.25 7.53 -7 -8 8 60.92 4.04 -7 8 8 51.33 3.97 -7 8 8 49.09 3.40 -7 -8 8 46.34 3.31 -7 -8 8 56.58 4.02 -7 8 8 53.94 3.67 -7 8 8 54.48 3.81 -7 -8 8 55.01 3.80 7 -8 -8 56.33 3.71 -7 8 8 47.00 3.29 -7 8 8 56.34 3.69 -7 8 8 63.12 5.34 -7 8 8 54.50 3.56 -7 -8 8 47.16 3.48 -7 8 7 12.38 2.28 -7 -8 7 12.22 2.29 -7 -8 7 10.68 2.90 7 -8 -7 11.68 2.18 -7 8 7 8.23 2.59 -7 8 7 13.04 2.12 -7 -8 7 12.61 2.16 -7 8 7 10.64 2.45 7 -8 -7 8.61 2.23 -7 8 7 12.65 4.21 -7 8 7 12.15 2.12 -7 8 6 6.21 2.07 -7 -8 6 5.60 2.08 -7 -8 6 8.78 2.82 7 -8 -6 6.06 2.13 -7 8 6 5.63 2.34 -7 8 6 6.66 1.89 -7 -8 6 7.28 1.93 -7 8 6 1.82 2.39 7 -8 -6 3.92 2.11 -7 8 6 7.81 4.16 -7 8 6 5.93 1.96 7 -8 -5 1.21 2.00 -7 8 5 2.29 2.33 -7 -8 5 0.17 2.64 -7 8 5 1.93 1.99 -7 8 5 -0.56 2.37 -7 -8 5 1.48 3.56 -7 -8 5 2.20 2.64 7 -8 -5 0.63 1.96 -7 8 5 2.23 3.90 -7 8 5 1.25 1.82 -7 8 5 2.47 2.03 -7 -8 5 2.55 1.93 -7 8 4 104.29 5.51 -7 -8 4 108.68 6.03 -7 8 4 110.54 5.63 -7 8 4 102.37 5.26 -7 -8 4 109.56 5.69 -7 -8 4 98.14 5.18 -7 -8 4 117.38 6.83 7 -8 -4 107.71 5.35 -7 8 4 104.25 7.22 -7 -8 4 97.88 5.34 -7 -8 3 169.96 8.27 -7 8 3 159.49 7.80 -7 -8 3 169.00 8.33 -7 8 3 178.03 8.24 -7 8 3 178.80 7.90 -7 -8 3 184.92 7.90 -7 8 3 174.53 8.19 -7 -8 3 183.35 8.21 -7 -8 3 189.25 9.22 -7 -8 2 153.12 7.48 -7 8 2 144.43 7.50 -7 8 2 165.30 7.24 -7 -8 2 158.30 7.11 -7 8 2 158.01 7.45 -7 -8 2 158.00 7.33 -7 -8 2 151.32 8.24 -7 -8 1 7.09 2.40 -7 8 1 8.00 2.54 -7 8 1 5.59 2.33 -7 -8 1 8.72 3.38 -7 -8 1 9.65 2.06 -7 8 1 8.76 2.00 -7 -8 1 10.76 1.90 -7 -8 0 738.94 30.89 -7 8 0 780.23 30.78 -7 -8 0 819.53 30.71 -7 8 0 781.98 31.11 -7 8 0 758.11 30.78 -7 -8 0 795.47 31.54 -7 8 -1 181.98 8.14 -7 -8 -1 178.07 8.01 -7 -8 -1 169.71 8.20 -7 8 -1 181.39 8.09 -7 8 -1 170.24 8.13 -7 -8 -1 191.29 8.97 7 8 2 23.00 2.61 -7 8 -2 27.52 2.58 -7 8 -2 27.93 2.99 -7 -8 -2 29.94 3.73 -7 8 -2 25.60 2.64 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50.65 3.06 -7 9 11 49.07 4.03 -7 9 11 58.76 2.86 -7 -9 11 52.64 2.78 -7 9 10 0.82 1.48 -7 -9 10 1.41 1.43 -7 -9 10 0.33 1.76 -7 -9 10 2.33 1.90 -7 9 10 2.67 1.36 -7 -9 10 -0.16 1.31 7 -9 -10 -0.32 1.82 -7 9 10 1.66 1.58 -7 9 10 0.20 3.14 -7 9 10 0.43 1.49 -7 -9 9 23.54 2.32 -7 -9 9 34.88 3.07 -7 9 9 25.57 2.91 -7 -9 9 28.87 2.94 -7 9 9 27.12 2.32 -7 -9 9 26.65 2.30 -7 9 9 25.62 2.44 7 -9 -9 33.62 2.76 -7 9 9 25.55 2.49 -7 9 9 27.88 2.67 -7 9 9 34.88 4.30 -7 9 9 28.15 2.51 -7 9 8 21.57 2.39 -7 -9 8 16.72 2.23 -7 -9 8 20.87 3.02 -7 9 8 24.26 2.93 -7 -9 8 22.70 3.03 -7 9 8 19.79 2.25 -7 -9 8 17.98 2.15 -7 9 8 17.91 2.61 7 -9 -8 20.53 2.52 -7 9 8 21.58 2.67 -7 9 8 21.05 4.32 -7 9 8 21.56 2.36 -7 9 7 20.62 2.45 -7 -9 7 18.27 2.38 -7 -9 7 23.69 3.09 7 -9 -7 19.67 2.41 -7 9 7 21.87 2.42 -7 9 7 22.82 2.98 -7 -9 7 18.67 2.28 -7 9 7 17.18 2.50 7 -9 -7 24.11 2.67 -7 9 7 19.81 4.56 -7 9 7 19.16 2.36 -7 9 6 9.39 2.12 -7 -9 6 11.30 2.20 -7 -9 6 16.81 2.96 7 -9 -6 10.21 2.31 -7 9 6 13.92 2.65 -7 -9 6 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8 -5 6 83.55 4.54 -8 5 -6 86.24 4.35 -8 -5 -6 78.11 4.20 8 5 6 69.38 4.37 8 5 7 1.85 1.76 -8 5 -7 0.25 1.43 -8 -5 -7 3.46 1.48 8 5 7 1.12 1.94 8 -5 7 2.74 1.91 8 5 8 -0.12 1.26 -8 5 -8 -1.17 1.06 -8 -5 -8 1.94 1.08 8 5 8 -0.80 2.83 8 -5 8 0.59 2.55 -8 -6 11 2.79 1.18 -8 6 11 2.83 1.39 -8 -6 10 119.79 5.54 -8 6 10 119.67 5.24 -8 -6 10 124.31 5.23 8 -6 -10 101.24 5.12 -8 6 10 101.07 6.11 -8 6 10 121.22 5.31 -8 -6 10 122.57 5.30 -8 -6 9 128.26 6.26 -8 6 9 121.77 6.18 -8 6 9 126.98 5.90 -8 -6 9 134.92 5.89 -8 6 9 130.10 6.00 8 -6 -9 123.27 5.80 -8 6 9 120.24 5.90 -8 6 9 121.40 7.07 -8 6 9 137.55 6.01 -8 -6 9 125.73 5.92 -8 -6 8 10.09 2.58 -8 6 8 4.39 2.33 -8 6 8 11.27 2.00 -8 -6 8 6.32 1.85 -8 6 8 3.64 2.19 8 -6 -8 8.04 1.75 -8 6 8 7.98 1.94 -8 6 8 4.64 3.45 -8 6 8 9.00 2.03 -8 -6 8 6.64 1.93 -8 -6 7 234.40 10.80 -8 6 7 236.99 10.64 -8 6 7 253.41 10.44 -8 -6 7 254.62 10.42 -8 6 7 238.48 10.65 -8 6 7 230.88 10.50 -8 6 7 210.16 11.64 -8 6 7 248.09 10.55 -8 -6 7 242.01 10.51 -8 6 6 133.28 6.84 8 -6 -6 138.25 6.53 -8 -6 6 145.27 6.60 -8 -6 6 131.39 6.94 8 -6 -5 186.24 8.09 -8 -6 5 175.36 8.41 -8 6 5 162.93 8.06 -8 6 5 170.05 8.14 -8 -6 5 167.23 8.20 -8 6 4 -0.61 1.98 -8 -6 4 -1.88 1.89 -8 -6 4 -0.16 2.39 -8 6 4 2.58 2.01 -8 -6 4 0.40 3.33 -8 6 4 0.29 2.33 -8 -6 4 -3.31 2.64 -8 -6 3 220.05 10.27 -8 6 3 226.27 9.89 -8 6 3 227.87 10.01 -8 -6 3 230.72 9.96 -8 6 3 226.74 10.20 -8 -6 3 239.98 10.26 -8 -6 3 228.08 10.89 -8 -6 2 17.49 2.78 -8 6 2 28.79 2.69 -8 -6 2 34.29 2.84 -8 6 2 21.07 2.75 -8 -6 2 23.33 3.74 -8 -6 2 30.54 2.87 -8 6 2 22.10 3.14 -8 -6 1 1.78 2.13 -8 6 1 2.35 2.24 -8 -6 1 -1.62 3.05 -8 -6 1 -1.62 2.00 -8 6 1 1.57 2.85 -8 6 1 1.13 1.90 -8 -6 1 3.75 1.98 -8 -6 0 179.41 8.93 -8 6 0 214.17 9.03 -8 -6 0 214.88 8.98 -8 6 0 194.85 8.95 -8 -6 0 196.81 9.58 -8 6 0 202.28 9.72 8 6 1 29.63 2.89 -8 6 -1 24.92 2.70 -8 -6 -1 30.33 2.72 -8 6 -1 28.82 2.65 -8 6 -1 27.88 2.73 -8 6 -1 31.55 3.98 -8 6 -2 81.12 4.63 -8 -6 -2 81.61 4.55 -8 6 -2 84.61 4.56 -8 6 -2 77.57 5.57 8 6 2 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10.74 -8 7 8 250.43 10.40 -8 -7 8 246.20 10.35 -8 7 8 255.96 10.62 8 -7 -8 230.09 10.28 -8 7 8 238.14 10.51 -8 7 8 211.53 11.56 -8 7 8 251.78 10.52 -8 -7 8 243.93 10.45 -8 -7 7 -0.60 2.44 -8 7 7 0.14 2.25 -8 7 7 1.03 1.75 -8 -7 7 -0.88 1.78 -8 7 7 0.80 2.29 8 -7 -7 0.21 1.58 -8 7 7 -0.78 1.96 -8 7 7 -0.76 3.73 -8 7 7 2.47 1.91 -8 -7 7 3.52 2.03 -8 7 6 36.49 3.21 8 -7 -6 32.81 2.78 -8 7 6 33.88 2.84 -8 -7 6 33.71 2.75 -8 7 6 37.40 3.27 -8 7 6 31.55 2.52 8 -7 -5 20.43 2.63 -8 -7 5 20.68 3.03 -8 7 5 23.29 2.72 -8 -7 5 26.82 3.09 -8 7 5 23.69 2.23 -8 -7 4 67.23 4.46 -8 7 4 69.75 4.05 -8 7 4 69.69 4.46 -8 -7 4 69.32 4.40 -8 7 4 65.44 3.97 -8 -7 4 58.08 3.78 -8 -7 4 72.63 5.33 -8 7 4 61.13 3.71 -8 -7 3 175.87 8.53 -8 7 3 187.73 8.19 -8 -7 3 192.98 8.22 -8 7 3 160.33 8.34 -8 -7 3 178.45 8.40 -8 -7 3 193.38 9.29 -8 -7 2 1.62 2.35 -8 7 2 1.90 2.18 -8 -7 2 1.34 3.31 -8 -7 2 5.58 2.11 -8 7 2 3.52 2.56 -8 7 2 3.90 1.89 -8 -7 2 5.36 2.01 -8 -7 1 35.02 3.17 -8 7 1 30.21 2.89 -8 -7 1 32.32 2.74 -8 7 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7 7 20.38 4.10 8 -7 7 27.03 2.73 8 -7 8 3.29 1.61 8 -7 8 -0.12 2.40 -8 -8 11 5.90 1.12 -8 -8 10 13.33 1.88 -8 8 10 11.14 1.88 8 -8 -10 12.05 1.50 -8 -8 9 62.15 3.77 -8 8 9 66.34 3.76 -8 8 9 55.41 3.24 -8 -8 9 60.37 3.23 -8 8 9 57.53 3.42 8 -8 -9 57.76 3.33 -8 8 9 59.58 3.46 -8 8 9 51.63 4.56 -8 -8 9 62.86 3.32 -8 -8 8 -0.40 2.25 -8 8 8 1.53 2.03 -8 8 8 -1.18 1.61 -8 -8 8 -0.38 1.58 -8 8 8 0.23 1.97 8 -8 -8 3.86 1.67 -8 8 8 -0.94 1.73 -8 8 8 5.76 3.40 -8 -8 8 1.57 1.68 -8 -8 7 73.29 4.60 -8 8 7 73.20 4.41 -8 8 7 72.24 3.98 -8 -8 7 69.40 3.92 -8 8 7 77.20 4.38 8 -8 -7 64.00 3.85 -8 8 7 69.05 3.79 -8 8 7 70.85 4.23 -8 8 6 33.60 3.18 8 -8 -6 38.33 3.05 -8 8 6 39.69 2.98 -8 -8 6 47.77 3.08 -8 8 6 44.45 3.40 -8 8 6 37.62 2.78 -8 -8 5 86.35 5.27 8 -8 -5 96.92 5.03 -8 8 5 86.63 4.94 -8 8 5 87.97 4.59 8 -8 -4 288.79 12.22 -8 -8 4 275.32 12.37 -8 8 4 265.81 11.90 -8 8 4 273.49 12.01 -8 8 4 283.19 12.27 -8 -8 4 281.05 12.22 -8 8 4 296.56 11.94 -8 -8 4 289.00 12.97 -8 -8 4 289.67 11.90 -8 8 4 273.62 11.78 -8 -8 3 117.13 6.18 -8 8 3 113.33 6.01 -8 8 3 114.39 5.67 -8 8 3 111.12 6.05 -8 -8 3 114.79 5.64 -8 -8 3 113.34 5.94 -8 -8 3 125.01 7.03 -8 -8 2 8.94 2.48 -8 8 2 10.55 2.60 -8 -8 2 13.69 3.43 -8 -8 2 13.50 2.36 -8 8 2 12.13 2.89 -8 8 2 10.27 2.04 -8 -8 2 11.69 2.12 -8 -8 1 14.54 2.57 -8 8 1 13.47 2.41 -8 -8 1 15.31 3.49 -8 8 1 13.67 3.24 -8 8 1 11.38 2.27 -8 -8 1 9.28 2.06 -8 -8 0 33.18 3.14 -8 8 0 37.03 3.04 -8 -8 0 33.76 2.88 -8 8 0 35.29 3.11 -8 -8 0 44.09 3.99 -8 8 0 41.26 4.16 -8 8 -1 45.62 3.23 -8 -8 -1 42.37 3.09 -8 8 -1 41.25 3.17 -8 8 -1 37.65 3.05 -8 -8 -1 32.34 3.82 -8 8 -1 40.91 4.39 -8 8 -2 48.55 3.36 -8 -8 -2 43.94 3.13 -8 8 -2 42.72 3.37 -8 8 -2 42.90 3.07 -8 -8 -2 44.56 3.91 -8 8 -2 41.82 4.43 -8 8 -3 131.04 6.17 -8 -8 -3 129.28 6.04 -8 8 -3 121.12 6.30 -8 8 -3 111.57 7.04 8 8 3 133.66 6.29 8 8 3 116.86 6.03 8 -8 3 131.21 6.94 8 8 4 3.53 1.92 8 -8 4 4.44 2.99 -8 8 -4 5.01 2.24 -8 8 -4 6.97 1.98 -8 -8 -4 3.68 1.78 8 8 4 3.23 2.35 8 -8 4 3.98 2.33 -8 8 -5 102.66 5.07 -8 -8 -5 98.34 4.93 -8 8 -5 99.14 5.25 -8 8 -5 96.95 5.77 8 8 5 105.41 5.27 8 -8 5 101.21 5.25 8 8 5 93.68 5.02 8 -8 5 97.53 5.71 -8 8 -6 22.80 2.23 -8 -8 -6 23.86 2.14 8 8 6 18.47 2.20 8 -8 6 24.76 3.09 -8 8 -6 24.62 2.57 8 8 6 26.46 2.54 8 -8 6 27.07 2.53 8 8 6 24.74 4.66 -8 8 -7 18.73 1.74 8 -8 7 16.98 2.42 -8 8 -7 16.34 2.05 8 -8 7 21.09 2.05 -8 -8 -7 13.83 1.62 8 8 7 18.55 2.01 8 8 7 13.27 3.75 8 -8 8 3.92 1.62 -8 -9 10 3.06 1.57 -8 9 10 2.77 1.58 8 -9 -10 2.16 1.29 -8 -9 9 9.57 2.08 -8 9 9 10.44 2.13 -8 9 9 9.06 1.50 -8 -9 9 9.50 1.47 -8 9 9 10.85 1.81 8 -9 -9 9.08 1.72 -8 9 9 12.42 1.75 -8 -9 8 8.42 2.31 -8 9 8 8.05 1.69 -8 -9 8 9.25 1.68 -8 9 8 11.16 2.14 8 -9 -8 10.66 1.88 -8 9 8 8.70 1.99 -8 9 8 9.62 1.69 -8 -9 7 2.94 2.38 -8 9 7 0.66 2.12 8 -9 -7 3.35 1.76 -8 9 7 -0.11 1.78 -8 -9 7 2.93 1.59 -8 9 7 3.86 2.22 8 -9 -7 2.64 1.73 -8 9 7 0.52 1.89 -8 9 7 2.72 1.66 -8 -9 6 52.41 4.12 -8 9 6 53.96 3.79 8 -9 -6 59.94 3.80 -8 9 6 66.10 3.61 -8 -9 6 59.31 3.48 -8 9 6 62.62 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13 -4 6.14 2.96 -8 13 -4 2.57 1.51 8 13 4 8.43 4.17 8 13 4 5.54 1.75 8 -13 4 2.95 1.77 8 -13 5 1.52 2.24 -8 13 -5 -2.26 2.09 -8 13 -5 0.14 2.34 -8 13 -5 0.64 1.25 8 13 5 -0.21 1.50 8 13 5 1.91 3.74 8 -13 6 2.40 1.85 -8 13 -6 1.63 1.80 -8 13 -6 0.62 1.90 8 13 6 3.15 3.04 8 -13 7 0.07 1.49 -8 13 -7 0.21 1.35 8 13 7 -1.26 2.23 8 -13 7 -1.88 1.80 -8 14 10 18.08 1.49 -8 -14 9 2.45 1.57 -8 14 9 1.85 1.44 -8 14 9 3.32 1.23 -8 14 9 2.53 1.26 -8 -14 8 3.56 1.91 -8 14 8 4.01 1.75 -8 14 8 3.17 1.51 8 -14 -8 4.77 1.92 -8 14 8 3.95 1.60 -8 14 8 3.25 1.53 -8 -14 7 23.15 2.84 -8 14 7 24.25 2.34 -8 14 7 27.51 2.46 -8 14 7 24.37 2.32 -8 -14 6 0.99 2.37 -8 14 6 0.73 1.68 8 -14 -6 1.83 1.99 -8 14 6 -0.52 1.77 -8 14 6 2.25 1.30 -8 14 6 3.76 2.16 -8 14 6 3.31 1.78 -8 -14 5 11.19 2.76 8 -14 -5 11.60 2.36 -8 14 5 15.21 2.50 -8 14 5 15.00 1.69 -8 14 5 13.66 2.42 -8 14 5 18.19 2.25 8 -14 -5 14.33 2.14 8 -14 -4 21.55 2.79 -8 14 4 25.57 3.00 -8 -14 4 23.53 3.90 -8 14 4 25.13 2.46 8 -14 -4 16.25 2.18 -8 -14 3 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2.51 -10 -2 -2 28.40 2.13 10 -2 2 23.55 2.54 10 2 2 28.35 2.41 10 2 3 15.83 1.95 10 -2 3 18.64 2.14 -10 -2 -3 21.34 1.79 10 -2 3 20.61 2.17 10 -2 4 -0.07 1.48 10 -2 4 1.02 1.59 -10 -2 -4 0.86 1.06 10 -2 5 64.97 3.18 -10 -3 8 -0.13 1.21 -10 -3 7 33.36 2.32 -10 3 7 27.39 2.07 -10 3 7 30.30 2.05 -10 -3 7 33.10 2.06 -10 -3 6 3.25 1.58 -10 3 6 1.62 1.33 -10 -3 6 1.11 1.24 -10 3 6 2.93 1.65 -10 3 6 1.28 1.07 -10 -3 5 60.11 3.54 -10 -3 5 68.84 3.52 -10 3 5 64.71 3.68 -10 -3 4 17.60 2.04 -10 3 4 25.88 2.38 -10 -3 4 22.62 2.31 -10 3 3 50.27 3.16 -10 -3 3 44.78 2.98 -10 -3 2 6.28 1.73 -10 3 2 4.91 1.77 -10 -3 1 40.41 2.72 -10 3 1 37.57 2.65 10 3 0 1.48 1.91 10 -3 0 2.72 2.05 -10 -3 0 1.72 1.54 -10 -3 -1 35.00 2.40 10 3 1 31.36 2.61 10 -3 1 30.92 2.87 -10 -3 -2 84.44 3.77 10 3 2 70.24 3.99 10 -3 2 82.78 4.13 10 3 2 64.16 3.82 10 -3 2 60.70 3.97 10 -3 3 17.28 2.18 -10 -3 -3 21.62 1.77 10 3 3 18.78 2.19 10 -3 3 18.61 2.18 -10 -3 -4 32.69 1.98 10 3 4 29.05 2.26 10 -3 4 33.16 2.32 10 -3 4 30.86 2.27 10 3 5 5.53 1.21 10 -3 5 5.30 1.28 -10 -4 8 11.20 1.41 -10 -4 7 2.24 1.44 -10 4 7 1.88 1.22 -10 4 7 0.99 1.08 -10 -4 7 0.71 1.09 -10 -4 6 24.18 2.23 -10 4 6 24.79 1.95 -10 4 6 28.27 2.02 -10 -4 6 27.42 1.99 -10 4 6 25.73 2.25 -10 4 6 24.32 1.86 -10 -4 5 8.26 1.77 -10 4 5 8.83 1.56 -10 -4 5 9.23 1.54 -10 4 5 7.16 1.87 -10 -4 4 -0.55 1.64 -10 4 4 -1.21 1.84 -10 -4 3 3.15 1.55 10 -4 -3 1.95 1.45 -10 4 3 0.90 1.74 -10 4 2 31.61 2.60 -10 4 2 33.03 2.50 -10 -4 2 38.46 2.58 -10 4 1 13.21 1.93 -10 -4 1 12.93 1.86 -10 4 1 14.99 1.89 10 -4 0 2.50 2.20 -10 4 0 2.91 1.51 -10 -4 0 2.37 1.38 -10 4 -1 84.84 4.30 -10 -4 -1 94.32 4.35 10 -4 1 84.08 4.77 10 -4 2 8.13 2.14 10 4 2 10.92 1.96 10 -4 2 9.77 2.11 -10 4 -2 8.76 1.59 -10 -4 -2 8.53 1.55 10 -4 3 24.92 2.48 -10 4 -3 30.54 2.10 -10 -4 -3 28.05 2.06 10 4 3 30.52 2.39 10 -4 3 34.49 2.51 10 -4 4 -2.47 1.58 10 4 4 0.80 1.42 10 -4 4 1.15 1.46 -10 4 -4 -1.06 1.01 -10 -4 -4 -0.56 1.00 -10 -5 8 1.51 1.13 -10 -5 7 21.09 1.92 -10 5 7 18.65 1.58 -10 5 7 20.79 1.63 -10 -5 7 20.24 1.60 -10 -5 6 8.31 1.79 -10 5 6 9.92 1.41 -10 -5 6 8.16 1.37 -10 5 6 9.86 1.72 -10 5 6 9.53 1.41 -10 -5 5 5.68 1.73 -10 5 5 5.53 1.43 -10 -5 5 5.85 1.39 -10 5 5 7.26 1.80 -10 -5 4 12.53 1.90 -10 5 4 13.79 2.04 -10 -5 3 7.05 1.67 10 -5 -3 6.41 1.64 -10 5 3 5.69 1.82 -10 5 2 -1.63 1.63 -10 -5 2 0.35 1.48 -10 5 2 0.10 1.67 -10 5 1 4.98 1.58 -10 -5 1 4.01 1.46 -10 5 1 3.80 1.63 10 -5 0 -2.85 2.19 -10 5 0 -2.12 1.54 -10 -5 0 -2.20 1.53 10 -5 1 11.76 2.36 -10 5 -1 10.25 1.67 -10 -5 -1 13.34 1.68 -10 5 -2 119.14 5.43 -10 -5 -2 122.26 5.38 10 5 2 122.17 5.63 10 -5 2 127.26 5.71 10 -5 2 108.65 5.74 10 -5 3 14.71 2.08 -10 5 -3 18.77 1.67 -10 -5 -3 16.63 1.57 10 5 3 15.36 1.95 10 -5 3 16.21 2.02 10 5 4 49.82 2.67 10 -5 4 48.92 2.76 10 -5 4 43.53 2.83 -10 -6 8 0.06 1.12 -10 -6 7 22.24 1.99 -10 6 7 21.98 1.65 -10 -6 7 24.66 1.67 -10 -6 6 0.26 1.57 -10 6 6 0.50 1.22 -10 -6 6 0.48 1.17 -10 6 6 2.38 1.55 -10 6 6 -0.22 1.24 -10 -6 5 4.26 1.68 -10 6 5 4.42 1.38 -10 -6 5 4.17 1.38 -10 6 5 7.56 1.74 -10 -6 4 2.24 1.62 -10 6 4 1.19 1.65 -10 -6 3 -1.15 1.69 10 -6 -3 -1.15 1.53 -10 6 3 -0.10 1.68 -10 6 2 11.86 1.71 -10 -6 2 10.77 1.72 -10 6 2 9.03 1.93 -10 6 1 7.95 1.65 -10 -6 1 6.74 1.54 -10 6 1 5.52 1.75 10 -6 0 18.88 2.66 -10 6 0 19.09 1.95 -10 -6 0 24.86 1.99 -10 6 -1 78.48 3.84 -10 -6 -1 78.38 3.81 10 -6 1 67.51 4.29 10 -6 2 2.51 2.05 10 6 2 3.70 1.79 10 -6 2 3.36 1.92 -10 6 -2 5.13 1.40 -10 -6 -2 3.83 1.30 10 -6 3 2.56 1.83 10 6 3 6.00 1.65 10 -6 3 5.43 1.72 -10 6 -3 4.94 1.25 -10 -6 -3 5.77 1.20 10 6 4 30.97 2.08 10 -6 4 26.37 2.25 -10 -7 8 8.05 1.21 -10 -7 7 11.59 1.58 -10 7 7 10.07 1.56 -10 -7 6 1.44 1.59 -10 7 6 0.47 1.15 -10 -7 6 -1.02 1.12 -10 7 6 1.37 1.50 -10 7 6 1.46 1.18 -10 -7 5 32.54 2.58 -10 7 5 32.01 2.24 -10 -7 5 35.99 2.28 -10 7 5 31.65 2.53 -10 -7 4 3.90 1.72 10 -7 -4 5.47 1.46 -10 7 4 7.98 1.85 -10 -7 3 8.85 1.98 10 -7 -3 7.84 1.76 -10 7 3 7.53 1.83 10 -7 -2 7.59 1.84 -10 7 2 3.96 1.51 -10 -7 2 2.07 1.45 -10 7 2 6.17 1.81 -10 7 1 1.09 1.49 -10 -7 1 1.03 1.42 -10 7 1 3.36 1.56 10 -7 0 10.54 2.41 -10 7 0 12.64 1.67 -10 -7 0 8.86 1.55 -10 7 -1 42.00 2.54 -10 -7 -1 37.12 2.46 10 7 1 45.08 2.89 10 -7 1 43.70 2.88 10 -7 1 36.75 3.13 -10 7 -2 218.63 8.95 -10 -7 -2 210.85 8.87 10 7 2 222.70 9.08 10 -7 2 234.49 9.16 10 -7 3 13.33 2.06 10 7 3 14.23 3.24 10 7 3 12.29 1.71 10 -7 3 12.05 1.78 -10 7 -3 12.13 1.42 -10 -7 -3 12.68 1.34 10 7 4 19.54 1.61 10 -7 4 20.29 1.69 10 -7 4 21.91 1.99 -10 -8 8 25.37 1.70 -10 -8 7 14.70 1.71 -10 8 7 16.18 1.60 -10 -8 6 13.65 1.88 -10 8 6 13.24 1.39 -10 -8 6 14.12 1.35 -10 8 6 11.37 1.45 -10 -8 5 22.69 2.22 -10 8 5 19.40 1.82 -10 -8 5 23.03 1.83 -10 8 5 22.79 2.18 -10 -8 4 3.95 1.71 10 -8 -4 4.92 1.50 -10 -8 4 2.42 1.29 -10 8 4 3.16 1.64 -10 -8 3 4.94 2.08 10 -8 -3 1.65 1.60 -10 8 3 1.26 1.69 -10 8 2 27.38 2.48 -10 8 2 31.77 2.29 -10 8 1 12.59 1.63 -10 -8 1 10.52 1.53 -10 8 1 9.34 1.76 -10 8 0 71.21 3.63 -10 -8 0 69.61 3.54 10 -8 0 71.99 4.25 -10 8 -1 98.84 4.61 -10 -8 -1 91.47 4.49 10 8 1 108.43 4.86 10 -8 1 103.74 4.87 10 -8 1 97.78 5.17 -10 8 -2 27.07 1.95 10 8 2 30.02 2.28 10 -8 2 34.01 2.39 10 8 3 3.84 1.42 10 -8 3 7.40 1.48 -10 8 -3 4.55 1.14 -10 -9 7 19.96 1.79 -10 -9 6 31.68 2.34 -10 9 6 32.66 2.02 -10 9 6 31.65 2.06 -10 -9 5 98.76 5.00 -10 9 5 104.52 4.74 -10 -9 5 103.24 4.67 -10 9 5 114.05 5.04 -10 -9 4 77.66 4.22 10 -9 -4 87.40 4.19 -10 9 4 84.74 4.04 -10 -9 4 83.50 3.93 -10 9 4 81.17 4.25 -10 -9 3 69.91 4.43 10 -9 -3 75.36 3.93 -10 9 3 66.37 3.82 10 -9 -2 98.93 4.97 -10 9 2 97.57 4.79 -10 -9 1 15.55 1.60 -10 9 1 18.12 1.73 -10 9 1 14.35 1.92 -10 -9 0 15.85 1.64 -10 9 0 20.23 1.77 -10 9 -1 21.44 1.83 -10 -9 -1 21.02 1.70 10 9 1 28.16 2.26 10 -9 1 23.81 2.23 -10 9 -2 69.15 3.31 -10 -9 -2 61.56 3.17 10 9 2 67.26 3.50 10 -9 2 75.15 3.57 10 9 3 12.74 1.56 10 -9 3 10.97 1.50 -10 -10 7 3.43 1.26 -10 -10 6 110.56 5.02 -10 10 6 105.23 4.82 -10 -10 5 -0.34 1.65 -10 10 5 -0.06 1.06 -10 10 5 -0.77 1.44 -10 -10 4 1.41 1.85 10 -10 -4 2.08 1.44 -10 10 4 1.89 1.17 -10 -10 4 1.35 1.01 -10 10 4 0.63 1.55 10 -10 -3 13.76 1.93 -10 10 3 13.18 1.93 10 -10 -2 45.27 3.00 -10 10 2 45.82 2.98 -10 10 1 8.19 1.39 -10 -10 1 9.24 1.33 -10 10 1 7.35 1.74 -10 10 0 1.66 1.20 -10 -10 0 3.60 1.16 -10 10 0 4.08 1.45 -10 10 0 3.81 2.04 -10 10 -1 23.96 1.87 -10 -10 -1 28.50 1.77 10 10 1 29.32 2.24 10 -10 1 31.88 2.26 10 -10 2 3.98 1.95 10 10 2 2.00 1.33 10 -10 2 2.20 1.43 10 -10 3 0.24 1.64 10 -10 3 1.18 0.98 10 -10 4 24.66 1.95 -10 -11 7 18.24 1.64 -10 -11 6 12.31 1.73 -10 11 6 15.14 1.61 -10 11 6 15.80 1.47 -10 -11 5 71.20 3.98 -10 11 5 79.44 3.90 -10 11 5 78.67 3.80 -10 -11 4 37.76 3.21 10 -11 -4 42.92 2.56 -10 11 4 35.59 2.22 -10 11 4 38.63 2.62 10 -11 -3 121.15 5.41 -10 11 3 105.52 5.27 10 -11 -2 2.14 1.61 -10 11 2 1.59 1.56 10 -11 -1 1.48 1.54 -10 11 1 2.31 1.55 -10 11 1 1.06 1.82 -10 11 0 63.17 3.47 -10 11 0 66.35 3.30 -10 11 0 58.81 3.93 10 11 0 81.12 3.64 10 -11 0 76.17 3.53 10 -11 0 66.14 4.00 -10 11 -1 40.74 2.27 -10 11 -1 44.91 3.13 10 11 1 44.91 2.59 10 -11 1 37.47 2.37 10 -11 1 46.75 3.15 10 -11 2 11.23 2.05 10 11 2 15.43 1.56 10 -11 3 0.97 1.54 -10 -12 6 106.60 4.93 -10 -12 5 53.93 3.46 -10 12 5 58.54 2.99 10 -12 -4 4.64 1.47 -10 12 4 5.09 1.56 -10 12 3 90.55 4.13 -10 12 3 85.01 4.45 10 -12 -2 133.48 5.84 -10 12 2 117.74 5.68 10 -12 -1 47.23 2.92 -10 12 1 46.13 2.80 -10 12 1 41.56 2.98 10 -12 0 2.93 2.06 -10 12 0 2.31 1.31 -10 12 0 5.20 1.94 10 12 0 5.21 1.47 10 -12 1 3.75 1.90 -10 12 -1 2.89 1.89 10 -12 2 22.73 2.26 10 -12 3 -0.48 1.44 -10 13 5 28.51 1.91 10 -13 -4 119.31 5.14 -10 13 4 104.36 5.09 10 -13 -3 77.58 3.85 -10 13 3 70.51 3.79 10 -13 -2 7.39 1.63 -10 13 2 3.42 1.56 10 -13 -1 9.25 1.65 -10 13 1 8.80 1.65 -10 13 1 9.88 1.85 10 -13 0 5.25 2.00 -10 13 0 2.22 1.28 -10 13 0 3.40 1.85 10 -13 1 8.64 2.01 -10 13 -1 9.48 2.01 10 -13 2 38.32 2.64 10 -13 3 3.29 1.35 -10 14 5 13.31 1.31 -10 14 4 3.18 1.36 10 -14 -3 13.34 1.70 -10 14 3 12.69 1.68 10 -14 -2 105.19 4.83 -10 14 2 97.57 4.70 10 -14 -1 25.92 2.07 -10 14 1 24.69 1.95 -10 14 1 25.00 2.13 10 -14 0 0.62 1.83 -10 14 0 4.76 1.80 10 -14 1 0.24 1.67 10 -14 1 1.47 1.12 -10 14 -1 -0.52 1.65 10 -14 2 7.22 1.61 -10 15 4 41.98 2.44 10 -15 -3 5.30 1.40 -10 15 3 4.91 1.36 10 -15 -2 23.76 1.95 -10 15 2 24.86 1.94 10 -15 -1 15.52 2.09 -10 15 1 19.42 1.74 -10 15 1 16.74 1.72 10 -15 0 13.10 1.96 10 -15 0 15.17 1.51 -10 15 0 13.52 1.93 10 -15 1 5.35 1.57 -10 15 -1 3.91 1.64 10 -15 2 3.45 1.34 -10 16 3 17.09 1.65 10 -16 -3 20.82 2.06 10 -16 -2 5.62 1.34 -10 16 2 4.38 1.27 10 -16 -1 5.41 1.65 10 -16 0 6.81 1.67 -10 16 0 11.71 1.67 10 -16 1 4.94 1.44 -10 16 -1 5.65 1.46 10 -17 -2 2.19 1.46 10 -17 -1 35.86 2.37 10 -17 0 2.55 1.41 10 -18 -2 0.17 1.17 11 0 0 0.88 1.37 11 0 1 12.47 1.49 11 -1 0 23.20 1.91 11 -1 1 3.30 1.28 11 -2 0 12.75 1.63 11 -2 1 25.01 1.86 11 3 0 -0.28 1.33 11 -3 0 -0.80 1.36 11 3 1 166.68 7.24 11 -3 1 185.62 7.29 11 -4 -2 4.02 1.35 11 -4 -1 3.53 1.33 11 4 0 21.26 1.72 11 -4 0 17.55 1.71 11 4 1 25.27 1.74 11 -4 1 23.97 1.78 11 -5 -2 -0.88 1.18 11 -5 -1 7.74 1.36 11 5 0 1.13 1.19 11 -5 0 1.80 1.25 11 -6 -3 7.63 1.32 11 -6 -2 6.93 1.31 11 6 -1 63.28 2.88 11 -6 -1 68.60 2.89 11 6 0 94.42 4.14 11 -6 0 91.08 4.16 11 -7 -3 12.35 1.44 11 -7 -2 5.09 1.35 11 -7 -1 0.99 1.29 11 -7 -1 1.24 1.13 11 -8 -2 30.78 2.11 11 -8 -1 4.69 1.32 11 -9 -2 0.11 1.14 0 0 0 0.00 0.00 TITL DP_511_DCM extract RT_auto in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 9.156898 31.520255 11.780728 90.0000 97.8589 90.0000 ZERR 2.00 0.000109 0.000340 0.000137 0.0000 0.0010 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Cl Cu UNIT 104.00 184.00 12.00 48.00 4.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 51678 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.348 _oxdiff_exptl_absorpt_empirical_full_min 0.671