############################################################################## # # # This CIF contains the data in a paper accepted for publication in # # Acta Crystallographica Section E. It conforms to the requirements of # # Notes for Authors for Acta Crystallographica Section E, and has been # # peer reviewed under the auspices of the IUCr Commission on Journals. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the journal # # article from which it was obtained. # # # ############################################################################## data_I _audit_creation_method SHELXL-2018/3 _chemical_name_systematic ;\ trans-Bis{(2E)-N-phenyl-2-[(2E)-3-phenyl-2-propen-\ 1-ylidene]hydrazinecarbothioamidato-\k^2^N^1^,S}palladium(II) ; _chemical_name_common ? _chemical_formula_moiety 'C32 H28 N6 Pd S2' _chemical_formula_sum 'C32 H28 N6 Pd S2' _chemical_formula_iupac '[Pd (C16 H14 N3 S1)2]' _chemical_formula_weight 667.12 _chemical_melting_point ? _chemical_absolute_configuration ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 15.084(5) _cell_length_b 11.418(4) _cell_length_c 17.097(6) _cell_angle_alpha 90 _cell_angle_beta 91.097(9) _cell_angle_gamma 90 _cell_volume 2944.0(16) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9138 _cell_measurement_theta_min 2.24 _cell_measurement_theta_max 28.33 _cell_measurement_temperature 299(2) _exptl_crystal_description block _exptl_crystal_colour orange _exptl_crystal_size_max 0.253 _exptl_crystal_size_mid 0.180 _exptl_crystal_size_min 0.106 _exptl_crystal_density_diffrn 1.505 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1360 _exptl_absorpt_coefficient_mu 0.805 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_absorpt_correction_T_min 0.6992 _exptl_absorpt_correction_T_max 0.7457 _diffrn_ambient_temperature 299(2) _diffrn_source 'microfocus X ray tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_measurement_device_type 'Bruker D8 Venture Photon 100 area detector diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 87933 _diffrn_reflns_av_R_equivalents 0.0418 _diffrn_reflns_av_unetI/netI 0.0177 _diffrn_reflns_theta_min 2.145 _diffrn_reflns_theta_max 28.357 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_limit_l_max 22 _diffrn_radiation_probe x-ray _refine_special_details ? _reflns_number_total 7344 _reflns_number_gt 6204 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0360 _refine_ls_R_factor_gt 0.0255 _refine_ls_wR_factor_gt 0.0582 _refine_ls_wR_factor_ref 0.0628 _refine_ls_goodness_of_fit_ref 1.048 _refine_ls_restrained_S_all 1.048 _refine_ls_number_reflns 7344 _refine_ls_number_parameters 370 _refine_ls_number_restraints 0 _refine_ls_hydrogen_treatment constr _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0241P)^2^+1.5227P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.338 _refine_diff_density_min -0.499 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX3 (Bruker, 2015) ; _computing_cell_refinement ; SAINT (Bruker, 2015) ; _computing_data_reduction ; SAINT (Bruker, 2015) ; _computing_structure_solution ; SHELXT2014/5 (Sheldrick, 2015a) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 2006), CrystalExplorer (Wolff et al., 2012) ; _computing_publication_material ; WinGX (Farrugia, 2012), publCIF (Westrip, 2010) and enCIFer (Allen et al., 2004) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.93114(12) 0.25646(18) 0.41478(10) 0.0408(4) Uani d 1 . . H H1 0.911357 0.222755 0.368099 0.049 Uiso calc 1 . . C C2 1.02188(12) 0.29262(18) 0.41878(11) 0.0429(4) Uani d 1 . . H H2 1.042322 0.334403 0.462190 0.052 Uiso calc 1 . . C C3 1.07777(12) 0.26780(19) 0.36174(11) 0.0434(4) Uani d 1 . . H H3 1.054715 0.228656 0.318196 0.052 Uiso calc 1 . . C C4 1.17186(12) 0.29659(18) 0.36156(11) 0.0436(4) Uani d 1 . . C C5 1.20873(15) 0.3801(2) 0.41107(14) 0.0566(5) Uani d 1 . . H H4 1.172634 0.422924 0.444057 0.068 Uiso calc 1 . . C C6 1.29897(17) 0.4000(3) 0.41148(17) 0.0738(8) Uani d 1 . . H H5 1.323135 0.457206 0.444183 0.089 Uiso calc 1 . . C C7 1.35360(16) 0.3362(3) 0.36419(19) 0.0765(8) Uani d 1 . . H H6 1.414532 0.348617 0.366163 0.092 Uiso calc 1 . . C C8 1.31865(17) 0.2555(3) 0.31492(18) 0.0745(8) Uani d 1 . . H H7 1.355493 0.212955 0.282440 0.089 Uiso calc 1 . . C C9 1.22814(15) 0.2358(2) 0.31256(14) 0.0613(6) Uani d 1 . . H H8 1.204591 0.181127 0.277638 0.074 Uiso calc 1 . . C C10 0.85343(12) 0.31504(17) 0.59615(10) 0.0377(4) Uani d 1 . . C C11 0.95766(12) 0.42049(17) 0.68829(10) 0.0397(4) Uani d 1 . . C C12 0.95571(14) 0.48633(19) 0.75646(11) 0.0466(5) Uani d 1 . . H H9 0.904012 0.489377 0.785175 0.056 Uiso calc 1 . . C C13 1.02970(15) 0.5473(2) 0.78205(13) 0.0559(5) Uani d 1 . . H H10 1.027308 0.591307 0.827731 0.067 Uiso calc 1 . . C C14 1.10674(15) 0.5437(2) 0.74084(14) 0.0584(6) Uani d 1 . . H H11 1.156512 0.585126 0.757969 0.070 Uiso calc 1 . . C C15 1.10894(14) 0.4777(2) 0.67371(14) 0.0597(6) Uani d 1 . . H H12 1.161063 0.474407 0.645610 0.072 Uiso calc 1 . . C C16 1.03566(13) 0.4160(2) 0.64695(12) 0.0516(5) Uani d 1 . . H H13 1.038671 0.371677 0.601430 0.062 Uiso calc 1 . . C C17 0.55839(12) 0.16720(18) 0.50233(11) 0.0416(4) Uani d 1 . . H H14 0.578917 0.185524 0.552491 0.050 Uiso calc 1 . . C C18 0.46597(12) 0.14045(18) 0.49358(11) 0.0429(4) Uani d 1 . . H H15 0.444566 0.115183 0.445071 0.052 Uiso calc 1 . . C C19 0.40947(13) 0.15030(19) 0.55209(12) 0.0472(5) Uani d 1 . . H H16 0.433316 0.172755 0.600361 0.057 Uiso calc 1 . . C C20 0.31419(13) 0.12958(18) 0.54837(12) 0.0454(4) Uani d 1 . . C C21 0.27211(14) 0.0746(2) 0.48604(13) 0.0513(5) Uani d 1 . . H H17 0.305174 0.047797 0.444312 0.062 Uiso calc 1 . . C C22 0.18134(15) 0.0590(2) 0.48519(16) 0.0644(6) Uani d 1 . . H H18 0.153934 0.021536 0.442935 0.077 Uiso calc 1 . . C C23 0.13142(16) 0.0979(3) 0.54540(18) 0.0713(8) Uani d 1 . . H H19 0.070293 0.087173 0.544212 0.086 Uiso calc 1 . . C C24 0.17159(17) 0.1526(3) 0.60741(18) 0.0739(8) Uani d 1 . . H H20 0.137628 0.180199 0.648339 0.089 Uiso calc 1 . . C C25 0.26240(16) 0.1673(2) 0.60978(15) 0.0653(6) Uani d 1 . . H H21 0.289272 0.202928 0.653032 0.078 Uiso calc 1 . . C C26 0.63696(12) 0.14116(18) 0.31857(11) 0.0406(4) Uani d 1 . . C C27 0.52836(12) 0.06730(19) 0.21755(12) 0.0456(5) Uani d 1 . . C C28 0.50883(17) 0.0809(2) 0.13948(14) 0.0657(7) Uani d 1 . . H H22 0.547569 0.121832 0.107827 0.079 Uiso calc 1 . . C C29 0.4319(2) 0.0341(3) 0.10764(19) 0.0878(10) Uani d 1 . . H H23 0.418657 0.044846 0.054772 0.105 Uiso calc 1 . . C C30 0.37560(18) -0.0272(3) 0.1525(2) 0.0837(9) Uani d 1 . . H H24 0.323855 -0.058496 0.130698 0.100 Uiso calc 1 . . C C31 0.39511(18) -0.0431(3) 0.23033(19) 0.0803(8) Uani d 1 . . H H25 0.356585 -0.085945 0.261047 0.096 Uiso calc 1 . . C C32 0.47140(16) 0.0038(2) 0.26388(15) 0.0633(6) Uani d 1 . . H H26 0.484228 -0.007087 0.316803 0.076 Uiso calc 1 . . N N1 0.87363(10) 0.26614(14) 0.47008(8) 0.0375(3) Uani d 1 . . N N2 0.90767(10) 0.31587(16) 0.53850(9) 0.0428(4) Uani d 1 . . N N3 0.87873(10) 0.36111(16) 0.66658(9) 0.0442(4) Uani d 1 . . H H27 0.841082 0.352842 0.703313 0.053 Uiso calc 1 . . N N4 0.61600(10) 0.16837(14) 0.44748(9) 0.0383(3) Uani d 1 . . N N5 0.58090(10) 0.13619(16) 0.37463(9) 0.0437(4) Uani d 1 . . N N6 0.61038(11) 0.11296(18) 0.24427(9) 0.0521(5) Uani d 1 . . H H28 0.649000 0.124627 0.208750 0.063 Uiso calc 1 . . Pd Pd1 0.74528(2) 0.21629(2) 0.46039(2) 0.03379(5) Uani d 1 . . S S1 0.74605(3) 0.25655(5) 0.59231(3) 0.04797(12) Uani d 1 . . S S2 0.74676(3) 0.18416(6) 0.32859(3) 0.04861(13) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0320(9) 0.0589(11) 0.0314(9) -0.0018(8) 0.0020(7) -0.0014(8) C2 0.0327(9) 0.0625(12) 0.0337(9) -0.0045(8) -0.0002(7) 0.0005(8) C3 0.0337(9) 0.0606(12) 0.0358(9) -0.0037(9) 0.0015(7) 0.0006(9) C4 0.0326(9) 0.0575(12) 0.0407(10) -0.0026(8) 0.0018(7) 0.0101(9) C5 0.0445(12) 0.0656(14) 0.0596(13) -0.0060(10) -0.0040(10) 0.0032(11) C6 0.0551(15) 0.0816(18) 0.0838(18) -0.0223(14) -0.0209(14) 0.0151(15) C7 0.0348(12) 0.094(2) 0.100(2) -0.0080(13) -0.0040(13) 0.0419(18) C8 0.0416(13) 0.097(2) 0.0858(19) 0.0078(13) 0.0206(13) 0.0207(17) C9 0.0445(12) 0.0805(17) 0.0594(14) -0.0030(11) 0.0151(10) -0.0011(12) C10 0.0314(9) 0.0475(10) 0.0343(9) 0.0002(7) 0.0017(7) -0.0005(7) C11 0.0351(9) 0.0486(10) 0.0354(9) 0.0000(8) -0.0029(7) 0.0001(8) C12 0.0446(11) 0.0557(12) 0.0396(10) -0.0024(9) 0.0016(8) -0.0032(9) C13 0.0578(13) 0.0596(13) 0.0499(12) -0.0054(11) -0.0067(10) -0.0103(10) C14 0.0443(12) 0.0655(14) 0.0650(14) -0.0103(10) -0.0128(10) -0.0005(11) C15 0.0341(10) 0.0826(17) 0.0624(14) -0.0034(11) 0.0010(10) -0.0032(12) C16 0.0361(10) 0.0735(14) 0.0453(11) 0.0009(10) 0.0016(8) -0.0096(10) C17 0.0360(9) 0.0542(11) 0.0347(9) -0.0016(8) 0.0036(7) -0.0037(8) C18 0.0356(9) 0.0542(11) 0.0392(10) -0.0007(8) 0.0053(8) -0.0008(8) C19 0.0413(10) 0.0586(12) 0.0420(10) -0.0018(9) 0.0078(8) -0.0009(9) C20 0.0390(10) 0.0505(11) 0.0471(11) 0.0018(8) 0.0116(8) 0.0071(9) C21 0.0415(11) 0.0609(13) 0.0516(12) 0.0024(10) 0.0072(9) 0.0081(10) C22 0.0468(13) 0.0740(16) 0.0722(16) -0.0050(12) -0.0071(11) 0.0167(13) C23 0.0379(12) 0.0804(18) 0.096(2) 0.0040(12) 0.0149(13) 0.0283(16) C24 0.0539(14) 0.0804(18) 0.089(2) 0.0055(13) 0.0362(14) 0.0086(16) C25 0.0539(14) 0.0782(16) 0.0645(15) -0.0027(12) 0.0246(11) -0.0050(13) C26 0.0315(9) 0.0554(11) 0.0351(9) -0.0013(8) 0.0021(7) -0.0016(8) C27 0.0323(9) 0.0553(12) 0.0488(11) 0.0009(8) -0.0040(8) -0.0101(9) C28 0.0631(15) 0.0751(16) 0.0582(14) -0.0127(13) -0.0205(12) 0.0074(12) C29 0.084(2) 0.095(2) 0.083(2) -0.0132(18) -0.0477(17) 0.0046(17) C30 0.0520(15) 0.089(2) 0.109(2) -0.0128(14) -0.0269(16) -0.0201(18) C31 0.0566(15) 0.087(2) 0.098(2) -0.0283(14) 0.0074(15) -0.0243(17) C32 0.0520(13) 0.0787(16) 0.0592(14) -0.0154(12) 0.0031(11) -0.0121(12) N1 0.0299(7) 0.0523(9) 0.0303(7) -0.0014(6) 0.0009(6) -0.0023(6) N2 0.0324(8) 0.0645(10) 0.0316(8) -0.0058(7) 0.0017(6) -0.0059(7) N3 0.0348(8) 0.0659(11) 0.0319(8) -0.0070(8) 0.0045(6) -0.0067(7) N4 0.0304(7) 0.0496(9) 0.0349(8) -0.0023(7) 0.0030(6) -0.0023(7) N5 0.0322(8) 0.0646(11) 0.0342(8) -0.0057(7) 0.0027(6) -0.0055(7) N6 0.0341(8) 0.0878(14) 0.0346(8) -0.0110(9) 0.0028(7) -0.0081(8) Pd1 0.02574(7) 0.04563(8) 0.03007(7) -0.00040(5) 0.00212(5) -0.00124(5) S1 0.0344(2) 0.0749(3) 0.0349(2) -0.0119(2) 0.00699(18) -0.0100(2) S2 0.0275(2) 0.0866(4) 0.0319(2) -0.0068(2) 0.00370(17) -0.0071(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 N1 . 1.300(2) ? C1 C2 . 1.430(3) ? C1 H1 . 0.9300 ? C2 C3 . 1.332(3) ? C2 H2 . 0.9300 ? C3 C4 . 1.457(3) ? C3 H3 . 0.9300 ? C4 C5 . 1.385(3) ? C4 C9 . 1.389(3) ? C5 C6 . 1.380(3) ? C5 H4 . 0.9300 ? C6 C7 . 1.374(4) ? C6 H5 . 0.9300 ? C7 C8 . 1.349(4) ? C7 H6 . 0.9300 ? C8 C9 . 1.383(3) ? C8 H7 . 0.9300 ? C9 H8 . 0.9300 ? C10 N2 . 1.293(2) ? C10 N3 . 1.362(2) ? C10 S1 . 1.7520(19) ? C11 C16 . 1.385(3) ? C11 C12 . 1.388(3) ? C11 N3 . 1.413(2) ? C12 C13 . 1.380(3) ? C12 H9 . 0.9300 ? C13 C14 . 1.371(3) ? C13 H10 . 0.9300 ? C14 C15 . 1.374(3) ? C14 H11 . 0.9300 ? C15 C16 . 1.381(3) ? C15 H12 . 0.9300 ? C16 H13 . 0.9300 ? C17 N4 . 1.291(2) ? C17 C18 . 1.432(3) ? C17 H14 . 0.9300 ? C18 C19 . 1.331(3) ? C18 H15 . 0.9300 ? C19 C20 . 1.457(3) ? C19 H16 . 0.9300 ? C20 C21 . 1.381(3) ? C20 C25 . 1.389(3) ? C21 C22 . 1.380(3) ? C21 H17 . 0.9300 ? C22 C23 . 1.361(4) ? C22 H18 . 0.9300 ? C23 C24 . 1.363(4) ? C23 H19 . 0.9300 ? C24 C25 . 1.380(3) ? C24 H20 . 0.9300 ? C25 H21 . 0.9300 ? C26 N5 . 1.291(2) ? C26 N6 . 1.363(2) ? C26 S2 . 1.7328(19) ? C27 C28 . 1.370(3) ? C27 C32 . 1.384(3) ? C27 N6 . 1.410(2) ? C28 C29 . 1.380(3) ? C28 H22 . 0.9300 ? C29 C30 . 1.351(4) ? C29 H23 . 0.9300 ? C30 C31 . 1.369(4) ? C30 H24 . 0.9300 ? C31 C32 . 1.384(3) ? C31 H25 . 0.9300 ? C32 H26 . 0.9300 ? N1 N2 . 1.390(2) ? N1 Pd1 . 2.0217(16) ? N3 H27 . 0.8600 ? N4 N5 . 1.393(2) ? N4 Pd1 . 2.0333(16) ? N6 H28 . 0.8600 ? Pd1 S2 . 2.2836(9) ? Pd1 S1 . 2.3016(9) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 C1 C2 . . 126.30(17) ? N1 C1 H1 . . 116.8 ? C2 C1 H1 . . 116.8 ? C3 C2 C1 . . 121.49(18) ? C3 C2 H2 . . 119.3 ? C1 C2 H2 . . 119.3 ? C2 C3 C4 . . 125.73(19) ? C2 C3 H3 . . 117.1 ? C4 C3 H3 . . 117.1 ? C5 C4 C9 . . 118.0(2) ? C5 C4 C3 . . 122.27(19) ? C9 C4 C3 . . 119.7(2) ? C6 C5 C4 . . 120.0(2) ? C6 C5 H4 . . 120.0 ? C4 C5 H4 . . 120.0 ? C7 C6 C5 . . 120.8(3) ? C7 C6 H5 . . 119.6 ? C5 C6 H5 . . 119.6 ? C8 C7 C6 . . 119.9(2) ? C8 C7 H6 . . 120.1 ? C6 C7 H6 . . 120.1 ? C7 C8 C9 . . 120.2(3) ? C7 C8 H7 . . 119.9 ? C9 C8 H7 . . 119.9 ? C8 C9 C4 . . 121.0(3) ? C8 C9 H8 . . 119.5 ? C4 C9 H8 . . 119.5 ? N2 C10 N3 . . 120.03(17) ? N2 C10 S1 . . 124.91(14) ? N3 C10 S1 . . 115.06(13) ? C16 C11 C12 . . 118.73(18) ? C16 C11 N3 . . 124.58(18) ? C12 C11 N3 . . 116.68(17) ? C13 C12 C11 . . 120.6(2) ? C13 C12 H9 . . 119.7 ? C11 C12 H9 . . 119.7 ? C14 C13 C12 . . 120.7(2) ? C14 C13 H10 . . 119.7 ? C12 C13 H10 . . 119.7 ? C13 C14 C15 . . 118.7(2) ? C13 C14 H11 . . 120.7 ? C15 C14 H11 . . 120.7 ? C14 C15 C16 . . 121.6(2) ? C14 C15 H12 . . 119.2 ? C16 C15 H12 . . 119.2 ? C15 C16 C11 . . 119.6(2) ? C15 C16 H13 . . 120.2 ? C11 C16 H13 . . 120.2 ? N4 C17 C18 . . 126.43(17) ? N4 C17 H14 . . 116.8 ? C18 C17 H14 . . 116.8 ? C19 C18 C17 . . 122.63(19) ? C19 C18 H15 . . 118.7 ? C17 C18 H15 . . 118.7 ? C18 C19 C20 . . 126.8(2) ? C18 C19 H16 . . 116.6 ? C20 C19 H16 . . 116.6 ? C21 C20 C25 . . 117.9(2) ? C21 C20 C19 . . 123.10(18) ? C25 C20 C19 . . 119.0(2) ? C22 C21 C20 . . 120.5(2) ? C22 C21 H17 . . 119.7 ? C20 C21 H17 . . 119.7 ? C23 C22 C21 . . 120.9(3) ? C23 C22 H18 . . 119.6 ? C21 C22 H18 . . 119.6 ? C22 C23 C24 . . 119.6(2) ? C22 C23 H19 . . 120.2 ? C24 C23 H19 . . 120.2 ? C23 C24 C25 . . 120.3(2) ? C23 C24 H20 . . 119.8 ? C25 C24 H20 . . 119.8 ? C24 C25 C20 . . 120.8(3) ? C24 C25 H21 . . 119.6 ? C20 C25 H21 . . 119.6 ? N5 C26 N6 . . 119.74(17) ? N5 C26 S2 . . 125.25(14) ? N6 C26 S2 . . 115.00(13) ? C28 C27 C32 . . 119.5(2) ? C28 C27 N6 . . 116.4(2) ? C32 C27 N6 . . 123.9(2) ? C27 C28 C29 . . 120.3(3) ? C27 C28 H22 . . 119.9 ? C29 C28 H22 . . 119.9 ? C30 C29 C28 . . 120.6(3) ? C30 C29 H23 . . 119.7 ? C28 C29 H23 . . 119.7 ? C29 C30 C31 . . 119.7(2) ? C29 C30 H24 . . 120.2 ? C31 C30 H24 . . 120.2 ? C30 C31 C32 . . 120.9(3) ? C30 C31 H25 . . 119.6 ? C32 C31 H25 . . 119.6 ? C31 C32 C27 . . 119.0(2) ? C31 C32 H26 . . 120.5 ? C27 C32 H26 . . 120.5 ? C1 N1 N2 . . 113.95(15) ? C1 N1 Pd1 . . 124.60(13) ? N2 N1 Pd1 . . 121.45(11) ? C10 N2 N1 . . 114.18(15) ? C10 N3 C11 . . 129.63(16) ? C10 N3 H27 . . 115.2 ? C11 N3 H27 . . 115.2 ? C17 N4 N5 . . 113.40(15) ? C17 N4 Pd1 . . 125.56(13) ? N5 N4 Pd1 . . 121.01(11) ? C26 N5 N4 . . 114.13(15) ? C26 N6 C27 . . 129.03(17) ? C26 N6 H28 . . 115.5 ? C27 N6 H28 . . 115.5 ? N1 Pd1 N4 . . 178.31(6) ? N1 Pd1 S2 . . 95.66(4) ? N4 Pd1 S2 . . 82.94(4) ? N1 Pd1 S1 . . 82.92(4) ? N4 Pd1 S1 . . 98.45(4) ? S2 Pd1 S1 . . 177.57(2) ? C10 S1 Pd1 . . 95.74(6) ? C26 S2 Pd1 . . 96.65(6) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag N1 C1 C2 C3 . . . . 172.9(2) ? C1 C2 C3 C4 . . . . -177.50(19) ? C2 C3 C4 C5 . . . . -17.8(3) ? C2 C3 C4 C9 . . . . 159.6(2) ? C9 C4 C5 C6 . . . . -0.8(3) ? C3 C4 C5 C6 . . . . 176.7(2) ? C4 C5 C6 C7 . . . . -1.2(4) ? C5 C6 C7 C8 . . . . 2.0(4) ? C6 C7 C8 C9 . . . . -0.8(4) ? C7 C8 C9 C4 . . . . -1.3(4) ? C5 C4 C9 C8 . . . . 2.0(4) ? C3 C4 C9 C8 . . . . -175.5(2) ? C16 C11 C12 C13 . . . . 0.8(3) ? N3 C11 C12 C13 . . . . -179.92(19) ? C11 C12 C13 C14 . . . . -0.3(3) ? C12 C13 C14 C15 . . . . -0.3(4) ? C13 C14 C15 C16 . . . . 0.4(4) ? C14 C15 C16 C11 . . . . 0.2(4) ? C12 C11 C16 C15 . . . . -0.7(3) ? N3 C11 C16 C15 . . . . -180.0(2) ? N4 C17 C18 C19 . . . . -174.5(2) ? C17 C18 C19 C20 . . . . 177.5(2) ? C18 C19 C20 C21 . . . . 13.0(4) ? C18 C19 C20 C25 . . . . -166.5(2) ? C25 C20 C21 C22 . . . . 0.5(3) ? C19 C20 C21 C22 . . . . -178.9(2) ? C20 C21 C22 C23 . . . . 0.3(4) ? C21 C22 C23 C24 . . . . -0.2(4) ? C22 C23 C24 C25 . . . . -0.8(4) ? C23 C24 C25 C20 . . . . 1.7(4) ? C21 C20 C25 C24 . . . . -1.5(4) ? C19 C20 C25 C24 . . . . 178.0(2) ? C32 C27 C28 C29 . . . . 1.5(4) ? N6 C27 C28 C29 . . . . 177.0(3) ? C27 C28 C29 C30 . . . . -1.1(5) ? C28 C29 C30 C31 . . . . 0.0(5) ? C29 C30 C31 C32 . . . . 0.6(5) ? C30 C31 C32 C27 . . . . -0.1(4) ? C28 C27 C32 C31 . . . . -0.9(4) ? N6 C27 C32 C31 . . . . -176.0(2) ? C2 C1 N1 N2 . . . . -0.7(3) ? C2 C1 N1 Pd1 . . . . 178.74(16) ? N3 C10 N2 N1 . . . . 179.95(17) ? S1 C10 N2 N1 . . . . 0.6(3) ? C1 N1 N2 C10 . . . . -173.45(18) ? Pd1 N1 N2 C10 . . . . 7.1(2) ? N2 C10 N3 C11 . . . . 4.6(3) ? S1 C10 N3 C11 . . . . -175.92(16) ? C16 C11 N3 C10 . . . . -18.5(3) ? C12 C11 N3 C10 . . . . 162.2(2) ? C18 C17 N4 N5 . . . . -2.1(3) ? C18 C17 N4 Pd1 . . . . 176.05(16) ? N6 C26 N5 N4 . . . . -179.31(18) ? S2 C26 N5 N4 . . . . -0.4(3) ? C17 N4 N5 C26 . . . . 177.55(18) ? Pd1 N4 N5 C26 . . . . -0.7(2) ? N5 C26 N6 C27 . . . . -6.0(4) ? S2 C26 N6 C27 . . . . 175.02(18) ? C28 C27 N6 C26 . . . . 160.2(2) ? C32 C27 N6 C26 . . . . -24.6(4) ? N2 C10 S1 Pd1 . . . . -6.03(18) ? N3 C10 S1 Pd1 . . . . 174.54(14) ? N5 C26 S2 Pd1 . . . . 1.1(2) ? N6 C26 S2 Pd1 . . . . 179.99(15) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C1 H1 S2 . 0.93 2.60 3.230(2) 125.6 yes C16 H13 N2 . 0.93 2.32 2.887(3) 118.8 yes C17 H14 S1 . 0.93 2.72 3.355(2) 126.0 yes C32 H26 N5 . 0.93 2.39 2.911(3) 115.1 yes N3 H27 S2 4_566 0.86 2.63 3.4805(18) 171.2 yes N6 H28 S1 4_565 0.86 2.84 3.6554(19) 159.2 yes _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.822 _shelx_estimated_absorpt_T_max 0.919 _shelx_hkl_file ; -2 0 0 2516.55 51.79 -3 0 0 1.40 0.60 -3 0 0 1.50 0.70 -3 0 0 1.40 0.60 -3 0 0 2.80 0.70 -4 0 0 1448.66 30.70 -4 0 0 1496.95 30.10 -4 0 0 1503.95 30.20 -4 0 0 1519.25 30.40 4 0 0 1527.25 30.50 -5 0 0 121.49 3.50 -5 0 0 120.09 3.70 -5 0 0 119.89 4.10 -5 0 0 119.19 3.40 5 0 0 121.79 3.80 -6 0 0 4209.18 85.99 6 0 0 4352.86 85.29 -7 0 0 268.57 6.80 -7 0 0 271.57 7.00 -7 0 0 271.27 7.30 -7 0 0 272.07 7.80 7 0 0 264.57 7.30 -8 0 0 2712.23 54.99 8 0 0 2656.53 55.19 -8 0 0 2696.83 54.39 -8 0 0 2693.43 54.79 -8 0 0 2741.83 55.89 -9 0 0 333.97 8.90 -9 0 0 317.37 8.30 9 0 0 330.47 9.00 -9 0 0 327.17 9.60 -9 0 0 323.97 8.70 -10 0 0 1544.05 32.60 10 0 0 1571.04 33.70 -10 0 0 1548.55 33.20 -10 0 0 1626.44 33.60 -10 0 0 1526.05 34.40 -11 0 0 67.89 3.60 -11 0 0 81.99 4.10 -11 0 0 75.19 4.90 11 0 0 78.39 4.30 -11 0 0 80.99 4.30 12 0 0 601.44 15.40 -12 0 0 596.64 15.20 -12 0 0 593.94 16.30 -12 0 0 588.24 14.90 -12 0 0 600.34 14.20 -13 0 0 158.88 6.60 -13 0 0 165.68 5.80 -13 0 0 152.28 7.60 -13 0 0 165.28 6.50 13 0 0 159.78 6.50 13 0 0 157.68 6.70 14 0 0 1094.89 25.40 -14 0 0 1039.20 27.00 14 0 0 1111.59 25.80 -14 0 0 1095.19 25.40 -14 0 0 1089.89 25.50 -14 0 0 1070.29 23.90 -15 0 0 60.79 4.30 -15 0 0 71.29 6.50 -15 0 0 69.39 5.40 15 0 0 74.19 5.30 16 0 0 383.16 12.10 -16 0 0 403.26 14.40 16 0 0 415.46 12.90 -16 0 0 406.46 12.70 -16 0 0 365.86 10.50 17 0 0 77.19 6.00 -17 0 0 93.39 7.00 -17 0 0 96.99 8.80 -17 0 0 68.69 4.90 17 0 0 78.29 6.50 18 0 0 293.97 11.20 -18 0 0 296.47 9.20 -18 0 0 351.76 14.50 18 0 0 308.97 11.70 -18 0 0 302.37 12.00 -19 0 0 59.39 5.20 19 0 0 71.69 7.60 -19 0 0 80.29 8.60 19 0 0 68.89 7.70 -20 0 0 49.30 8.10 -20 0 0 51.79 7.00 -1 -1 0 6434.96 130.79 -2 -1 0 4.30 0.70 -2 -1 0 3.90 0.60 2 -1 0 6.90 0.90 -2 1 0 6.10 0.80 -2 1 0 5.90 0.60 2 1 0 5.40 0.70 2 1 0 4.90 0.70 -2 1 0 5.60 0.80 -3 -1 0 723.83 15.40 -3 -1 0 738.73 15.30 -3 1 0 746.33 15.00 3 1 0 741.33 15.40 -3 1 0 747.03 15.60 3 1 0 736.93 15.70 -3 1 0 744.93 15.70 3 1 0 735.73 15.30 -4 -1 0 11.60 1.40 -4 -1 0 9.60 1.20 4 -1 0 11.20 1.00 -4 -1 0 11.10 1.20 -4 -1 0 11.30 1.30 -4 1 0 12.20 0.90 -4 1 0 10.90 1.10 4 1 0 12.00 1.40 4 1 0 10.10 1.20 4 1 0 12.30 1.30 -4 1 0 9.30 1.20 -4 1 0 11.50 1.40 -5 -1 0 2969.50 61.39 -5 1 0 3193.28 61.59 5 1 0 3042.40 60.89 -5 1 0 3044.20 61.49 5 1 0 3034.60 61.49 -6 -1 0 224.98 6.60 -6 -1 0 230.58 6.40 -6 -1 0 224.08 5.80 -6 -1 0 218.38 6.10 -6 1 0 228.18 5.90 6 1 0 223.98 6.40 -6 1 0 235.28 5.60 6 1 0 224.38 5.90 -6 1 0 232.18 6.60 -7 -1 0 5814.62 115.99 -7 1 0 5809.72 116.09 8 -1 0 97.19 3.70 -8 -1 0 91.79 4.40 -8 -1 0 92.19 3.80 -8 -1 0 88.09 4.00 -8 -1 0 86.49 3.50 -8 1 0 96.09 3.40 -8 1 0 87.69 3.50 8 1 0 86.09 3.50 -8 1 0 91.29 4.40 -8 1 0 90.89 3.60 8 1 0 90.99 4.00 -8 1 0 84.49 4.30 -9 -1 0 2351.16 48.50 -9 -1 0 2353.76 47.40 -9 -1 0 2352.66 49.00 -9 -1 0 2311.67 48.10 9 -1 0 2321.77 47.90 -9 1 0 2274.67 47.40 9 1 0 2329.97 48.60 -9 1 0 2382.86 49.00 -9 1 0 2301.57 47.40 -9 1 0 2289.97 48.90 -9 1 0 2325.07 47.70 -10 -1 0 137.59 6.10 -10 -1 0 147.39 5.60 10 -1 0 150.88 5.40 -10 -1 0 143.99 5.00 -10 -1 0 144.99 5.80 -10 1 0 153.08 6.30 -10 1 0 157.58 5.20 -10 1 0 152.28 5.40 -10 1 0 151.78 6.50 10 1 0 147.69 5.90 -10 1 0 145.69 5.00 -11 -1 0 1032.80 24.60 11 -1 0 1048.30 23.40 -11 -1 0 1058.69 23.70 -11 -1 0 1054.89 24.00 -11 -1 0 1028.50 22.60 -11 1 0 1013.20 22.60 -11 1 0 1024.10 24.60 -11 1 0 1054.09 23.30 -11 1 0 1034.20 23.00 11 1 0 1046.20 24.20 -12 -1 0 83.09 4.70 12 -1 0 79.49 4.30 -12 -1 0 81.19 5.50 12 -1 0 78.69 4.20 -12 -1 0 85.39 4.70 -12 -1 0 77.19 3.90 -12 1 0 80.09 5.40 12 1 0 82.69 4.90 -12 1 0 82.69 4.40 -12 1 0 84.19 4.30 -12 1 0 83.09 4.10 13 -1 0 524.35 13.70 -13 -1 0 500.65 15.00 -13 -1 0 520.55 14.00 -13 -1 0 498.75 12.60 -13 -1 0 517.25 14.20 -13 1 0 510.95 13.40 13 1 0 521.65 14.10 -13 1 0 496.35 12.60 13 1 0 515.25 14.40 -13 1 0 512.55 13.50 -13 1 0 517.75 15.10 14 -1 0 129.39 5.80 -14 -1 0 128.29 6.60 -14 -1 0 135.29 5.40 14 -1 0 131.79 6.20 -14 -1 0 130.79 6.60 -14 -1 0 139.99 7.80 -14 1 0 117.69 5.30 -14 1 0 145.89 8.20 14 1 0 131.99 6.70 14 1 0 135.49 6.50 -14 1 0 131.19 6.10 15 -1 0 564.84 15.10 -15 -1 0 585.14 16.10 15 -1 0 571.54 15.50 -15 -1 0 559.64 14.20 -15 -1 0 598.04 17.50 -15 1 0 566.04 15.40 15 1 0 608.24 16.60 -15 1 0 592.64 17.60 -15 1 0 544.45 14.10 -16 -1 0 95.19 7.90 -16 -1 0 89.99 5.10 16 -1 0 101.19 6.00 -16 1 0 96.99 6.30 16 1 0 92.69 6.40 16 1 0 97.59 6.80 -16 1 0 110.79 8.00 -16 1 0 92.59 5.00 17 -1 0 316.07 10.90 17 -1 0 313.87 10.50 -17 -1 0 316.97 11.80 -17 -1 0 293.77 9.30 -17 -1 0 324.87 13.50 -17 1 0 304.77 9.40 17 1 0 303.77 11.40 -17 1 0 322.97 13.40 -17 1 0 335.37 12.00 17 1 0 334.47 12.10 18 -1 0 109.79 7.10 -18 -1 0 94.99 5.60 18 -1 0 98.79 6.70 -18 -1 0 116.79 10.10 -18 -1 0 110.29 8.40 18 1 0 98.49 7.90 -18 1 0 107.29 10.00 18 1 0 111.89 7.80 -18 1 0 94.39 5.60 -18 1 0 99.99 7.80 -19 -1 0 140.09 6.70 -19 -1 0 149.59 10.10 19 -1 0 151.68 8.70 19 -1 0 139.59 8.40 -19 -1 0 137.89 11.90 -19 1 0 176.98 12.20 -19 1 0 160.48 9.50 19 1 0 167.58 9.80 -19 1 0 142.49 6.50 -20 -1 0 4.30 6.90 -20 -1 0 11.30 5.40 20 1 0 18.00 7.40 -20 1 0 12.60 5.40 -20 1 0 19.10 7.10 0 -2 0 289.17 5.80 -1 -2 0 228.38 5.40 1 -2 0 232.38 5.40 -1 -2 0 228.68 5.30 -1 -2 0 229.48 5.50 1 -2 0 242.58 5.50 -1 -2 0 227.78 5.50 1 -2 0 240.18 5.10 -1 -2 0 231.58 5.50 1 2 0 237.28 5.40 -1 2 0 234.38 5.40 -1 2 0 236.98 4.80 -1 2 0 245.58 5.50 1 2 0 232.58 5.60 -1 2 0 233.78 5.00 1 2 0 225.78 5.50 -1 2 0 236.18 4.80 2 2 0 7967.70 160.98 3 -2 0 36.90 1.90 -3 -2 0 36.10 2.10 3 -2 0 37.00 1.10 -3 -2 0 37.60 1.80 -3 -2 0 35.90 1.90 3 2 0 38.50 1.90 3 2 0 36.50 2.00 -3 2 0 37.00 1.90 -3 2 0 38.20 1.20 3 2 0 38.50 1.90 -3 2 0 36.90 1.90 -4 -2 0 2167.98 44.30 -4 -2 0 2207.78 44.10 -4 -2 0 2147.79 44.50 -4 -2 0 2230.38 44.60 4 -2 0 2157.48 44.40 -4 2 0 2272.47 44.40 -4 2 0 2193.58 44.30 4 2 0 2177.98 44.10 4 2 0 2120.99 44.50 4 2 0 2217.28 44.20 -5 -2 0 81.29 3.30 -5 -2 0 83.89 3.20 -5 -2 0 74.89 3.10 -5 -2 0 71.69 2.90 5 2 0 77.09 3.30 -5 2 0 85.99 3.40 5 2 0 79.99 3.00 -5 2 0 84.49 3.30 -5 2 0 80.29 2.20 -5 2 0 81.89 2.40 5 2 0 76.69 3.10 -6 -2 0 3060.89 62.99 -6 -2 0 3138.29 62.49 -6 -2 0 3228.18 63.29 -6 -2 0 3027.30 62.89 6 2 0 3105.59 63.29 -6 2 0 3045.20 63.09 6 2 0 3054.19 62.59 -6 2 0 3305.47 63.29 6 2 0 3097.99 62.69 -7 -2 0 59.59 2.90 -7 -2 0 69.79 3.60 -7 -2 0 60.19 3.40 7 -2 0 74.89 3.20 -7 -2 0 66.39 3.30 -7 2 0 66.89 2.50 -7 2 0 70.99 3.70 -7 2 0 66.49 2.70 7 2 0 66.39 3.60 -7 2 0 68.99 3.60 7 2 0 61.49 3.00 -8 -2 0 1471.15 31.20 -8 -2 0 1467.55 31.60 -8 -2 0 1464.95 31.50 -8 -2 0 1456.95 30.50 8 -2 0 1468.35 30.20 -8 2 0 1440.26 31.60 -8 2 0 1475.05 31.60 8 2 0 1461.35 31.60 -8 2 0 1424.96 30.10 -8 2 0 1450.85 29.90 8 2 0 1463.95 30.70 9 -2 0 18.60 1.80 -9 -2 0 21.10 2.50 -9 -2 0 16.40 2.10 -9 -2 0 17.70 2.40 -9 -2 0 17.90 2.10 -9 2 0 28.20 3.40 -9 2 0 19.40 2.00 9 2 0 17.80 2.50 9 2 0 18.40 2.30 -9 2 0 19.20 2.80 -9 2 0 20.10 1.90 -10 -2 0 1356.36 29.90 -10 -2 0 1336.87 30.10 -10 -2 0 1321.37 29.50 -10 -2 0 1329.27 28.50 10 -2 0 1220.18 29.50 -10 2 0 1343.07 28.50 -10 2 0 1328.17 28.30 -10 2 0 1435.96 31.80 10 2 0 1353.16 28.90 -10 2 0 1376.56 28.50 -10 2 0 1325.77 30.10 10 2 0 1360.86 30.10 11 -2 0 100.49 4.10 -11 -2 0 106.29 5.20 -11 -2 0 88.59 4.10 -11 -2 0 95.69 5.40 -11 -2 0 95.49 4.90 -11 2 0 93.99 4.20 -11 2 0 113.79 5.80 -11 2 0 94.89 4.10 11 2 0 97.59 5.20 -11 2 0 99.59 4.20 12 -2 0 1308.37 28.30 -12 -2 0 1303.47 29.50 -12 -2 0 1302.77 28.00 -12 -2 0 1309.07 29.30 -12 -2 0 1314.27 30.10 12 -2 0 1279.87 27.90 12 2 0 1295.67 29.50 -12 2 0 1249.97 27.80 -12 2 0 1279.27 30.20 -12 2 0 1276.47 28.00 12 2 0 1306.07 29.90 -12 2 0 1278.07 28.10 13 -2 0 10.90 2.10 -13 -2 0 8.20 2.90 -13 -2 0 3.80 2.30 -13 -2 0 10.80 2.20 -13 -2 0 6.40 2.30 13 -2 0 7.80 2.10 -13 2 0 9.40 3.10 -13 2 0 8.50 2.20 -13 2 0 9.00 2.20 13 2 0 9.90 2.50 -13 2 0 9.00 2.10 13 2 0 10.40 2.90 -14 -2 0 242.18 9.10 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10.30 3 5 0 394.86 10.20 -3 5 0 385.16 8.70 -3 5 0 403.66 9.20 -3 5 0 390.96 9.90 -4 -5 0 52.99 3.40 -4 -5 0 51.19 3.20 4 -5 0 59.39 3.20 -4 -5 0 51.09 3.10 4 5 0 49.70 3.30 4 5 0 49.90 3.30 4 5 0 49.30 3.00 -4 5 0 66.29 3.30 -4 5 0 61.09 1.60 -4 5 0 58.49 2.00 -4 5 0 56.79 2.80 4 5 0 52.59 3.40 -4 5 0 60.09 1.60 -5 -5 0 522.85 13.20 -5 -5 0 525.15 13.30 -5 -5 0 537.15 12.90 -5 -5 0 526.05 13.00 5 -5 0 524.95 13.10 -5 -5 0 533.05 13.00 -5 -5 0 527.45 12.10 5 5 0 514.65 13.10 -5 5 0 535.95 12.90 -5 5 0 538.45 12.50 5 5 0 516.35 13.50 5 5 0 526.65 13.00 -5 5 0 553.04 13.10 -6 -5 0 0.50 1.40 -6 -5 0 1.40 1.50 6 -5 0 0.00 1.30 -6 -5 0 1.00 1.30 -6 -5 0 1.40 1.20 -6 -5 0 0.90 1.50 -6 -5 0 0.70 1.10 -6 5 0 0.50 1.30 6 5 0 -0.20 1.30 6 5 0 -0.20 1.20 -6 5 0 -0.50 1.50 -6 5 0 -0.80 1.20 6 5 0 1.80 1.50 -7 -5 0 72.69 4.10 -7 -5 0 73.89 4.40 -7 -5 0 78.69 3.80 -7 -5 0 72.29 4.20 -7 -5 0 73.49 3.90 7 -5 0 68.39 4.10 7 5 0 75.79 4.00 -7 5 0 83.39 4.20 7 5 0 73.69 4.50 -7 5 0 76.09 4.40 7 5 0 75.19 4.10 -7 5 0 78.99 4.00 -8 -5 0 7.50 2.40 -8 -5 0 10.20 2.40 -8 -5 0 9.50 2.20 -8 -5 0 9.80 2.00 -8 5 0 11.50 2.20 8 5 0 6.40 1.90 -8 5 0 11.30 2.60 -8 5 0 7.50 1.90 8 5 0 8.30 2.10 -8 5 0 11.10 1.00 8 5 0 11.10 2.10 -9 -5 0 336.17 10.80 -9 -5 0 350.86 10.10 -9 -5 0 352.96 9.90 -9 -5 0 339.67 10.30 -9 -5 0 340.17 10.70 -9 5 0 346.77 10.40 9 5 0 340.57 10.70 -9 5 0 332.87 7.70 9 5 0 349.47 10.20 9 5 0 348.07 11.00 -10 -5 0 34.40 3.90 -10 -5 0 31.30 3.40 -10 -5 0 28.20 3.20 -10 -5 0 34.20 4.10 -10 5 0 40.90 4.30 10 5 0 33.20 4.10 10 5 0 36.20 3.70 10 5 0 31.60 4.20 -10 5 0 37.90 2.10 -11 -5 0 60.09 5.30 -11 -5 0 58.89 4.20 -11 -5 0 53.59 4.80 -11 -5 0 57.79 4.80 -11 5 0 54.19 5.10 11 5 0 59.89 5.20 11 5 0 58.89 5.20 11 5 0 56.79 4.40 -11 5 0 59.29 2.90 -12 -5 0 -1.90 2.00 -12 -5 0 -2.00 2.20 -12 -5 0 -4.10 2.10 -12 5 0 -1.20 1.30 12 5 0 -3.20 2.20 12 5 0 0.00 2.30 -12 5 0 2.50 2.50 12 5 0 -1.00 2.10 -13 -5 0 128.99 7.20 -13 -5 0 120.79 6.00 -13 -5 0 124.69 7.20 13 5 0 108.19 6.90 -13 5 0 131.09 7.70 13 5 0 135.09 7.50 -13 5 0 118.19 4.90 13 5 0 134.69 6.50 -14 -5 0 58.79 5.10 -14 -5 0 51.89 6.40 -14 -5 0 58.59 6.30 14 5 0 69.39 6.40 -14 5 0 53.29 4.00 14 5 0 62.39 5.30 -14 5 0 61.99 6.70 -15 -5 0 34.10 5.00 -15 -5 0 28.40 5.10 -15 -5 0 41.70 5.00 -15 -5 0 46.90 5.00 -15 5 0 62.09 7.30 -15 5 0 39.80 4.00 15 5 0 45.20 5.80 15 5 0 46.80 6.10 -15 5 0 41.20 5.00 15 5 0 39.00 5.00 -16 -5 0 6.60 3.40 -16 -5 0 15.80 4.40 -16 -5 0 9.20 5.00 -16 -5 0 3.60 3.80 16 5 0 4.30 4.70 -16 5 0 15.30 4.70 -16 5 0 7.40 3.30 16 5 0 6.70 4.40 16 5 0 6.50 3.20 -16 5 0 6.00 2.80 -17 -5 0 19.60 5.40 -17 -5 0 18.10 5.70 -17 -5 0 19.50 5.00 -17 -5 0 19.00 5.50 17 5 0 21.30 5.80 -17 5 0 23.00 5.60 -17 5 0 14.70 3.90 -17 5 0 17.90 3.50 17 5 0 15.70 6.40 -18 -5 0 6.40 5.20 -18 -5 0 12.50 4.20 -18 -5 0 7.20 5.50 -18 5 0 8.60 5.70 18 5 0 9.40 5.10 -18 5 0 4.80 3.80 -18 5 0 4.10 3.80 -19 -5 0 37.10 7.00 -19 -5 0 27.20 7.60 -19 5 0 33.40 4.70 -19 5 0 26.20 7.80 0 -6 0 65.69 2.50 0 -6 0 70.69 3.50 0 -6 0 73.79 2.60 0 -6 0 60.59 3.40 0 6 0 69.89 3.00 0 6 0 67.19 3.50 0 6 0 65.79 3.00 0 6 0 66.59 3.70 0 6 0 64.69 3.10 0 6 0 70.09 3.10 -1 -6 0 148.79 5.30 1 -6 0 142.19 3.50 -1 -6 0 157.18 4.60 1 -6 0 142.19 5.10 1 -6 0 142.79 5.20 1 -6 0 145.09 3.50 -1 -6 0 159.18 4.50 1 6 0 157.78 5.40 1 6 0 152.78 5.10 -1 6 0 151.58 5.20 -1 6 0 142.49 5.40 1 6 0 152.18 5.10 -1 6 0 148.49 4.40 -1 6 0 143.79 4.40 -1 6 0 145.49 4.70 1 6 0 161.18 5.70 -1 6 0 142.39 4.60 1 6 0 152.58 4.90 -2 -6 0 153.78 4.90 -2 -6 0 149.39 3.60 -2 -6 0 148.59 5.50 -2 -6 0 139.99 3.70 2 -6 0 145.49 5.20 -2 -6 0 151.98 4.80 2 -6 0 152.38 5.30 -2 -6 0 154.78 5.50 2 6 0 152.88 5.10 -2 6 0 149.59 5.50 -2 6 0 145.89 4.20 -2 6 0 151.88 4.30 -2 6 0 150.78 4.50 -2 6 0 150.08 3.90 2 6 0 151.28 5.70 -2 6 0 149.29 4.40 -2 6 0 148.79 5.20 2 6 0 149.39 5.50 2 6 0 152.98 5.40 2 6 0 153.88 5.40 3 -6 0 11.40 1.90 -3 -6 0 11.30 1.70 -3 -6 0 14.10 1.90 3 -6 0 16.20 2.20 -3 -6 0 11.40 2.10 -3 -6 0 12.20 2.20 -3 -6 0 10.80 1.20 3 6 0 7.50 1.50 -3 6 0 13.60 1.60 3 6 0 8.00 1.90 3 6 0 9.40 2.00 -3 6 0 14.20 1.40 -3 6 0 11.80 1.50 -3 6 0 10.90 1.40 -3 6 0 11.80 1.30 3 6 0 15.30 2.50 -3 6 0 12.10 1.80 3 6 0 12.60 2.20 -3 6 0 19.00 2.50 -4 -6 0 474.05 10.60 -4 -6 0 463.95 12.20 4 -6 0 464.15 12.00 -4 -6 0 470.15 11.90 -4 -6 0 487.15 11.80 -4 -6 0 462.75 12.20 -4 6 0 474.25 11.10 4 6 0 482.65 12.50 -4 6 0 466.55 10.30 -4 6 0 493.55 12.10 -4 6 0 482.75 11.90 4 6 0 485.55 12.50 4 6 0 474.85 12.50 -4 6 0 464.65 10.10 4 6 0 471.65 12.40 -4 6 0 464.05 10.10 4 6 0 474.05 12.00 -4 6 0 470.35 12.10 -5 -6 0 79.29 4.40 -5 -6 0 79.19 3.20 5 -6 0 85.09 4.20 -5 -6 0 75.39 4.20 -5 -6 0 83.69 4.20 -5 -6 0 73.49 4.00 -5 6 0 83.19 4.00 -5 6 0 82.99 2.40 5 6 0 74.49 4.40 -5 6 0 87.29 2.40 5 6 0 72.49 4.30 -5 6 0 88.39 4.10 -5 6 0 77.39 2.50 5 6 0 72.49 4.30 5 6 0 75.69 4.30 -5 6 0 81.99 2.20 -5 6 0 81.59 3.60 -5 6 0 82.99 4.30 -6 -6 0 48.90 3.40 -6 -6 0 43.40 3.50 -6 -6 0 51.29 3.80 -6 -6 0 57.99 3.00 6 -6 0 40.70 3.40 -6 -6 0 52.99 3.60 6 6 0 47.30 3.60 6 6 0 48.00 3.50 -6 6 0 43.00 3.80 -6 6 0 49.90 3.50 6 6 0 45.80 3.80 6 6 0 49.90 3.90 -6 6 0 53.89 3.30 -7 -6 0 3.70 1.90 -7 -6 0 0.10 1.60 7 -6 0 -0.20 1.60 -7 -6 0 -0.80 1.50 -7 -6 0 1.40 1.30 -7 -6 0 -1.00 1.50 -7 6 0 2.90 2.20 7 6 0 -0.90 1.70 7 6 0 1.70 1.60 -7 6 0 -0.10 1.70 -7 6 0 0.80 1.40 7 6 0 -0.60 1.70 7 6 0 0.30 1.70 -8 -6 0 11.10 2.50 -8 -6 0 14.70 2.50 -8 -6 0 13.70 2.50 -8 -6 0 18.70 2.30 8 -6 0 17.10 3.20 -8 -6 0 20.10 2.80 8 6 0 19.00 2.80 -8 6 0 9.80 2.80 8 6 0 22.80 3.00 -8 6 0 15.70 2.40 8 6 0 13.30 2.50 -8 6 0 14.20 2.60 8 6 0 16.10 2.80 -9 -6 0 14.90 2.60 -9 -6 0 22.10 2.90 -9 -6 0 23.20 3.40 9 6 0 15.30 2.90 9 6 0 15.00 2.90 -9 6 0 23.90 3.10 9 6 0 20.80 3.30 -9 6 0 21.60 2.90 -9 6 0 21.90 1.50 -10 -6 0 18.60 2.70 -10 -6 0 14.00 2.80 -10 -6 0 20.90 3.40 -10 -6 0 19.20 3.00 -10 -6 0 19.70 3.60 -10 6 0 25.40 3.50 10 6 0 18.40 3.50 -10 6 0 16.70 1.70 10 6 0 19.70 3.70 -10 6 0 19.00 3.30 10 6 0 20.70 3.20 -11 -6 0 14.90 2.80 -11 -6 0 9.80 2.60 -11 -6 0 13.00 3.00 -11 -6 0 14.10 3.30 -11 6 0 8.70 2.90 -11 6 0 9.70 2.80 11 6 0 9.60 3.00 -11 6 0 8.50 1.50 11 6 0 12.30 3.00 11 6 0 8.00 2.90 -12 -6 0 11.00 3.60 -12 -6 0 16.10 3.20 -12 -6 0 20.20 3.30 12 6 0 12.90 3.00 -12 6 0 9.90 3.10 12 6 0 15.80 3.20 12 6 0 18.10 3.50 -12 6 0 14.40 3.30 -12 6 0 15.90 1.90 -13 -6 0 4.90 2.80 -13 -6 0 6.80 3.20 -13 -6 0 2.30 2.90 -13 6 0 9.20 3.40 -13 6 0 5.00 1.70 13 6 0 -0.20 3.30 13 6 0 9.00 2.80 13 6 0 0.70 2.90 -13 6 0 2.60 3.00 -14 -6 0 8.00 3.50 -14 -6 0 7.20 4.50 -14 -6 0 0.20 3.90 -14 -6 0 4.60 3.20 -14 6 0 10.30 2.20 14 6 0 9.90 4.10 -14 6 0 12.50 3.80 -14 6 0 10.90 3.90 14 6 0 7.10 3.70 14 6 0 9.30 3.30 -15 -6 0 13.20 4.10 -15 -6 0 16.50 4.50 -15 -6 0 17.10 3.80 -15 -6 0 10.70 4.70 -15 -6 0 19.20 4.10 15 6 0 11.30 5.10 -15 6 0 20.80 2.90 15 6 0 27.20 5.00 -15 6 0 18.30 4.70 15 6 0 22.80 4.10 -16 -6 0 13.90 4.40 -16 -6 0 17.40 5.90 -16 -6 0 8.90 4.50 -16 -6 0 15.10 4.90 -16 -6 0 10.20 4.00 16 6 0 15.20 4.00 -16 6 0 13.60 5.00 16 6 0 3.50 5.00 16 6 0 10.60 4.60 -16 6 0 4.80 3.80 -16 6 0 7.50 2.80 -17 -6 0 -1.10 4.80 -17 -6 0 4.90 4.70 -17 -6 0 -1.00 3.90 17 6 0 1.40 3.80 17 6 0 8.90 4.90 -17 6 0 2.60 3.10 -17 6 0 0.50 3.10 -17 6 0 4.60 4.10 -17 6 0 8.60 5.50 -18 -6 0 3.50 5.50 -18 -6 0 3.00 4.60 -18 -6 0 8.00 5.70 -18 6 0 10.80 4.10 -18 6 0 16.30 6.80 18 6 0 7.10 5.80 -18 6 0 7.40 3.50 -18 6 0 4.50 4.50 0 -7 0 3.60 0.90 0 -7 0 1.90 1.40 0 -7 0 3.80 1.50 0 -7 0 4.50 0.90 0 7 0 2.90 1.20 0 7 0 2.10 1.20 0 7 0 1.80 1.50 0 7 0 3.00 1.30 0 7 0 3.80 1.20 0 7 0 3.30 1.50 -1 -7 0 7.20 1.30 1 -7 0 7.00 1.70 -1 -7 0 8.20 1.30 -1 -7 0 7.30 1.90 1 -7 0 8.50 1.90 -1 7 0 6.70 1.70 -1 7 0 7.30 1.50 1 7 0 9.90 1.90 1 7 0 8.20 1.50 -1 7 0 7.50 1.40 1 7 0 7.00 1.60 -1 7 0 8.40 1.50 1 7 0 7.00 1.80 -1 7 0 7.20 2.00 -1 7 0 6.20 1.50 1 7 0 6.40 1.80 -2 -7 0 1.10 1.50 2 -7 0 3.70 1.50 -2 -7 0 -1.00 1.30 2 -7 0 1.10 1.30 -2 -7 0 -1.30 1.10 2 7 0 -1.10 1.20 2 7 0 -0.40 1.40 -2 7 0 3.10 1.50 -2 7 0 -0.40 1.50 2 7 0 -1.90 1.40 -2 7 0 -1.90 1.10 -2 7 0 -2.50 0.90 -2 7 0 -1.60 1.00 -2 7 0 -1.20 0.70 2 7 0 -2.50 1.20 -2 7 0 -1.20 1.10 2 7 0 -0.40 1.50 -3 -7 0 19.90 2.50 3 -7 0 22.60 2.70 3 -7 0 18.00 2.40 -3 -7 0 21.30 1.30 -3 -7 0 22.00 2.70 -3 -7 0 20.60 2.80 -3 -7 0 21.70 2.40 -3 7 0 23.00 1.80 -3 7 0 20.80 1.80 -3 7 0 22.60 2.80 3 7 0 18.30 2.50 3 7 0 23.00 2.80 3 7 0 19.30 2.80 3 7 0 19.70 2.80 -3 7 0 17.00 2.40 -3 7 0 20.40 2.00 -3 7 0 17.40 1.80 -3 7 0 22.80 1.80 3 7 0 23.50 2.70 4 -7 0 18.50 2.50 -4 -7 0 19.50 1.60 4 -7 0 15.10 2.30 -4 -7 0 19.70 2.70 -4 -7 0 19.00 2.30 -4 -7 0 25.90 3.20 -4 -7 0 21.10 2.60 4 7 0 25.70 3.20 -4 7 0 14.20 2.20 -4 7 0 15.20 1.60 -4 7 0 17.70 1.70 4 7 0 21.00 3.20 4 7 0 23.30 3.00 4 7 0 15.60 2.50 -4 7 0 14.20 1.60 -4 7 0 17.70 2.10 -4 7 0 18.00 2.80 -4 7 0 13.40 1.60 4 7 0 15.10 2.10 -5 -7 0 -2.90 1.50 -5 -7 0 0.80 1.00 -5 -7 0 0.40 1.50 -5 -7 0 -1.20 1.40 5 -7 0 2.40 1.70 -5 -7 0 0.00 1.60 -5 7 0 0.30 0.70 -5 7 0 -0.50 0.70 -5 7 0 1.00 1.60 5 7 0 0.30 1.50 5 7 0 4.30 2.00 5 7 0 -0.40 1.70 5 7 0 2.90 1.90 5 7 0 3.40 2.00 -5 7 0 0.40 0.80 -5 7 0 1.50 0.80 -5 7 0 0.00 1.50 -5 7 0 0.20 1.20 -5 7 0 0.90 2.00 -6 -7 0 -3.10 1.40 -6 -7 0 0.70 1.90 -6 -7 0 -2.40 1.60 -6 -7 0 -1.70 1.60 -6 -7 0 0.90 1.20 6 -7 0 0.30 1.60 -6 7 0 0.10 1.70 -6 7 0 2.60 1.70 -6 7 0 1.90 2.50 6 7 0 -0.40 1.60 6 7 0 -0.30 1.80 -6 7 0 0.90 0.70 -6 7 0 0.10 1.30 6 7 0 1.30 2.10 6 7 0 -1.30 1.80 -7 -7 0 13.90 2.40 7 -7 0 10.40 2.60 -7 -7 0 13.80 2.00 -7 -7 0 10.80 2.20 -7 -7 0 12.90 2.80 -7 -7 0 15.40 2.60 -7 7 0 15.70 1.20 7 7 0 10.20 2.70 7 7 0 16.60 2.90 -7 7 0 12.50 2.40 7 7 0 13.30 2.70 -7 7 0 7.70 3.00 -7 7 0 14.00 2.10 -7 7 0 11.20 2.20 7 7 0 11.00 2.20 8 -7 0 6.10 2.10 -8 -7 0 4.40 2.70 -8 -7 0 2.10 1.60 -8 -7 0 3.70 2.20 -8 -7 0 2.90 2.00 8 7 0 2.80 2.10 -8 7 0 1.60 1.90 -8 7 0 6.40 2.30 8 7 0 5.40 3.00 8 7 0 3.20 2.00 -8 7 0 7.70 2.20 8 7 0 3.40 2.40 -9 -7 0 3.30 2.10 9 -7 0 1.40 2.20 -9 -7 0 8.10 2.80 -9 -7 0 5.10 2.30 -9 -7 0 4.00 2.10 -9 -7 0 5.30 2.30 -9 7 0 3.50 2.00 9 7 0 2.60 2.30 9 7 0 8.00 4.70 -9 7 0 5.70 1.00 9 7 0 7.50 2.70 -9 7 0 3.80 2.20 -9 7 0 3.40 2.30 -10 -7 0 2.50 2.10 -10 -7 0 9.50 2.70 -10 -7 0 2.30 2.40 -10 -7 0 4.10 3.00 -10 -7 0 4.50 2.50 10 7 0 6.20 2.70 -10 7 0 9.50 2.90 10 7 0 5.90 2.90 10 7 0 4.20 2.90 -10 7 0 6.70 2.60 -10 7 0 10.30 2.40 -11 -7 0 24.40 4.80 -11 -7 0 24.10 3.30 -11 7 0 23.70 2.10 11 7 0 20.00 3.90 -11 7 0 24.20 3.60 -11 7 0 23.30 3.60 11 7 0 33.30 4.20 11 7 0 33.40 5.10 -12 -7 0 7.40 2.90 -12 -7 0 16.70 3.90 -12 -7 0 16.00 3.70 -12 -7 0 8.80 3.10 -12 -7 0 10.70 3.20 -12 7 0 13.20 3.40 12 7 0 7.90 3.30 12 7 0 9.10 3.10 -12 7 0 13.30 1.80 -12 7 0 14.30 2.90 12 7 0 9.70 3.60 -12 7 0 12.40 3.30 -13 -7 0 4.20 3.30 -13 -7 0 1.40 2.90 -13 -7 0 4.90 3.00 -13 -7 0 3.40 3.80 -13 -7 0 3.00 2.90 -13 7 0 3.80 2.40 13 7 0 -0.60 3.10 -13 7 0 0.90 1.60 -13 7 0 8.20 3.70 13 7 0 3.00 3.00 13 7 0 3.00 4.00 -14 -7 0 16.80 3.80 -14 -7 0 22.60 5.50 -14 -7 0 21.20 4.40 -14 -7 0 15.90 4.00 14 7 0 17.70 4.30 -14 7 0 22.80 2.80 14 7 0 20.30 4.20 14 7 0 14.20 3.80 -14 7 0 16.90 4.50 -14 7 0 21.20 3.30 -14 7 0 26.20 4.60 -15 -7 0 0.80 3.40 -15 -7 0 -0.70 3.70 -15 -7 0 3.20 3.70 -15 -7 0 4.00 4.80 -15 -7 0 6.70 4.10 15 7 0 5.50 4.30 -15 7 0 2.30 2.70 15 7 0 4.50 3.70 -15 7 0 -7.60 3.60 15 7 0 0.30 4.40 -15 7 0 -1.30 4.10 -15 7 0 1.60 2.30 -16 -7 0 -0.80 4.10 -16 -7 0 0.60 4.20 -16 -7 0 -2.30 4.60 16 7 0 6.60 5.10 -16 7 0 -2.30 3.00 -16 7 0 2.40 4.90 16 7 0 1.80 6.20 -16 7 0 5.00 5.00 16 7 0 -9.70 3.90 -16 7 0 1.30 2.70 -17 -7 0 0.00 4.70 -17 -7 0 6.70 5.50 -17 -7 0 -3.40 5.20 -17 7 0 1.40 3.30 17 7 0 8.00 5.70 -17 7 0 2.20 3.70 -17 7 0 12.90 5.70 -17 7 0 0.20 4.60 17 7 0 -2.40 5.00 -17 7 0 1.20 6.20 0 -8 0 0.70 1.60 0 -8 0 1.30 0.90 0 -8 0 1.60 1.60 0 -8 0 1.50 0.90 0 8 0 0.90 1.70 0 8 0 1.60 1.30 0 8 0 0.10 1.80 0 8 0 1.30 1.50 0 8 0 0.70 1.30 0 8 0 1.90 1.40 -1 -8 0 6.80 1.50 -1 -8 0 4.50 1.80 1 -8 0 8.50 2.10 -1 -8 0 7.20 1.50 1 -8 0 7.30 2.10 1 8 0 6.70 1.80 1 8 0 9.20 2.30 1 8 0 7.80 1.70 -1 8 0 9.00 1.70 1 8 0 8.20 2.10 -1 8 0 10.10 1.90 1 8 0 4.00 1.80 -1 8 0 8.70 1.70 -1 8 0 7.10 2.00 -1 8 0 7.10 1.70 -1 8 0 7.10 2.10 -2 -8 0 -0.40 1.60 -2 -8 0 1.30 1.30 2 -8 0 1.50 1.60 -2 -8 0 0.60 1.20 2 -8 0 0.50 1.60 -2 8 0 0.00 1.60 2 8 0 0.00 1.30 -2 8 0 -0.70 1.60 2 8 0 -0.50 1.70 2 8 0 0.80 1.60 -2 8 0 0.00 1.20 -2 8 0 0.30 1.10 2 8 0 1.00 1.40 -2 8 0 0.10 1.10 -2 8 0 0.30 1.10 2 8 0 0.10 1.70 3 -8 0 1.90 1.70 -3 -8 0 1.90 1.80 3 -8 0 0.40 1.50 -3 -8 0 2.40 0.60 -3 -8 0 0.20 1.40 -3 -8 0 -0.90 1.50 -3 8 0 0.90 1.10 -3 8 0 1.70 1.30 3 8 0 -2.50 1.60 3 8 0 0.40 1.60 -3 8 0 1.30 1.20 -3 8 0 1.80 1.20 3 8 0 3.00 2.00 -3 8 0 2.50 1.90 -3 8 0 1.00 1.70 3 8 0 1.00 1.80 -3 8 0 1.60 1.00 -4 -8 0 26.90 3.10 4 -8 0 31.20 3.20 -4 -8 0 32.70 3.80 -4 -8 0 28.10 3.00 -4 -8 0 28.40 1.80 4 -8 0 28.60 3.40 -4 -8 0 28.00 3.60 -4 8 0 26.00 2.30 -4 8 0 27.50 3.50 4 8 0 26.00 3.40 -4 8 0 29.90 2.10 -4 8 0 28.30 2.10 -4 8 0 25.90 2.10 4 8 0 29.40 3.80 4 8 0 33.20 3.80 4 8 0 27.50 3.60 -4 8 0 30.90 2.30 -4 8 0 35.10 3.60 4 8 0 27.20 3.10 5 -8 0 4.20 1.80 -5 -8 0 4.80 2.30 -5 -8 0 3.60 1.10 -5 -8 0 3.00 1.70 -5 -8 0 4.50 2.30 -5 -8 0 2.50 1.90 5 8 0 0.90 1.70 5 8 0 4.20 2.20 5 8 0 1.70 2.10 -5 8 0 7.10 2.00 5 8 0 -0.10 1.90 -5 8 0 4.70 1.20 -5 8 0 4.60 2.20 5 8 0 2.80 2.60 -5 8 0 5.00 1.30 -5 8 0 5.30 1.20 -5 8 0 4.60 1.60 -5 8 0 7.40 1.30 -6 -8 0 -1.30 2.00 -6 -8 0 -1.60 1.70 -6 -8 0 0.10 2.00 -6 -8 0 0.30 1.60 -6 -8 0 -1.20 1.10 6 -8 0 -0.40 1.60 -6 8 0 0.80 1.90 -6 8 0 -0.10 0.90 -6 8 0 -1.40 1.70 6 8 0 -0.80 2.00 6 8 0 -1.30 1.90 -6 8 0 -1.30 3.00 6 8 0 -4.40 3.00 6 8 0 1.30 2.50 -6 8 0 0.20 1.30 -7 -8 0 14.50 2.90 -7 -8 0 9.30 1.80 -7 -8 0 11.30 3.00 -7 -8 0 12.60 2.70 7 -8 0 9.70 2.40 -7 -8 0 7.60 2.20 -7 8 0 11.00 2.50 7 8 0 9.10 2.40 -7 8 0 11.50 2.30 -7 8 0 11.90 2.70 -7 8 0 10.00 1.20 7 8 0 7.50 2.40 7 8 0 14.80 3.20 7 8 0 14.30 3.50 -8 -8 0 20.20 3.30 -8 -8 0 14.50 2.80 8 -8 0 14.20 2.80 -8 -8 0 14.40 4.00 -8 -8 0 16.80 2.40 -8 -8 0 10.20 3.20 -8 8 0 22.10 1.70 -8 8 0 19.20 3.10 -8 8 0 15.90 2.60 -8 8 0 19.50 3.20 8 8 0 17.70 3.80 8 8 0 15.40 3.20 8 8 0 14.40 2.90 -9 -8 0 19.70 3.50 -9 -8 0 19.30 3.70 -9 -8 0 24.80 3.50 -9 -8 0 21.40 2.80 9 -8 0 19.60 3.40 -9 -8 0 20.70 3.50 -9 8 0 20.00 3.40 -9 8 0 19.50 3.20 -9 8 0 19.30 1.70 9 8 0 18.60 4.00 9 8 0 20.60 4.10 -9 8 0 17.80 3.00 9 8 0 21.20 3.70 -10 -8 0 4.10 2.80 -10 -8 0 6.60 2.90 -10 -8 0 7.00 2.40 10 8 0 5.50 3.00 -10 8 0 9.90 2.60 10 8 0 7.40 3.30 -10 8 0 8.60 2.70 10 8 0 7.50 2.80 -10 8 0 8.10 1.30 -10 8 0 5.50 2.70 -11 -8 0 21.50 4.20 -11 -8 0 15.60 4.00 -11 -8 0 22.00 3.80 -11 -8 0 19.90 3.90 -11 -8 0 24.60 3.30 11 8 0 20.00 3.90 11 8 0 20.20 3.80 -11 8 0 25.00 4.00 11 8 0 19.60 4.30 -11 8 0 21.10 2.10 -11 8 0 24.50 3.40 -11 8 0 23.90 4.00 -12 -8 0 8.10 3.50 -12 -8 0 8.50 3.80 -12 -8 0 11.70 3.10 -12 -8 0 3.30 3.40 -12 -8 0 8.00 3.40 12 8 0 13.20 3.80 12 8 0 3.70 3.50 -12 8 0 6.80 3.40 -12 8 0 12.00 3.50 -12 8 0 11.00 1.80 12 8 0 17.20 4.70 -12 8 0 10.20 3.00 -13 -8 0 7.40 3.80 -13 -8 0 1.30 3.30 -13 -8 0 6.50 4.40 -13 -8 0 -2.70 3.30 -13 -8 0 4.20 3.30 13 8 0 8.50 4.10 -13 8 0 10.00 3.10 -13 8 0 6.70 1.80 13 8 0 3.90 4.00 -13 8 0 10.50 4.00 13 8 0 6.40 3.50 -14 -8 0 8.30 7.40 -14 -8 0 7.70 4.10 -14 -8 0 3.60 3.90 -14 -8 0 11.00 4.80 -14 -8 0 10.80 4.00 14 8 0 7.60 4.50 -14 8 0 6.90 4.40 -14 8 0 4.70 2.20 -14 8 0 6.00 3.20 14 8 0 5.10 3.70 -14 8 0 10.90 4.50 -15 -8 0 -4.00 4.00 -15 -8 0 3.90 4.40 -15 -8 0 -3.90 3.80 -15 -8 0 0.00 5.10 -15 -8 0 1.50 5.50 15 8 0 7.50 4.50 -15 8 0 -0.80 3.20 -15 8 0 -4.30 4.50 15 8 0 4.90 5.00 -15 8 0 4.80 4.70 15 8 0 0.80 4.80 -15 8 0 3.50 2.50 -16 -8 0 -4.80 4.50 -16 -8 0 5.10 4.70 -16 -8 0 3.90 5.10 -16 8 0 0.70 5.10 16 8 0 8.80 4.70 16 8 0 0.00 5.60 -16 8 0 -0.50 5.40 -16 8 0 -1.90 2.90 -16 8 0 1.30 3.90 -17 -8 0 1.40 5.50 -17 -8 0 7.10 5.80 -17 -8 0 3.00 5.40 17 8 0 10.70 5.30 17 8 0 9.80 6.20 -17 8 0 11.10 6.60 -17 8 0 1.80 6.60 -17 8 0 2.40 4.30 -17 8 0 3.10 3.50 0 -9 0 0.40 1.60 0 -9 0 -1.90 0.90 0 -9 0 -3.70 1.70 0 -9 0 1.10 0.90 0 9 0 -0.90 1.60 0 9 0 -1.00 1.40 0 9 0 -1.60 1.80 0 9 0 -1.10 1.80 0 9 0 -2.20 1.40 -1 -9 0 18.30 3.00 1 -9 0 17.00 2.90 -1 -9 0 15.40 1.90 1 -9 0 14.20 2.40 -1 -9 0 14.60 1.80 -1 -9 0 16.30 2.60 1 9 0 11.70 2.20 -1 9 0 16.80 2.80 1 9 0 15.00 2.80 1 9 0 18.50 3.00 1 9 0 14.20 2.30 -1 9 0 16.70 3.10 -1 9 0 15.60 2.30 -1 9 0 12.30 2.00 -1 9 0 16.10 2.30 -1 9 0 15.70 2.30 -2 -9 0 2.80 1.50 -2 -9 0 1.40 1.60 -2 -9 0 2.00 2.10 2 -9 0 0.70 1.80 2 -9 0 2.90 1.60 2 9 0 1.00 1.90 2 9 0 5.70 2.50 -2 9 0 1.40 1.60 -2 9 0 1.30 1.50 -2 9 0 -0.10 1.40 -2 9 0 3.70 2.20 2 9 0 3.40 2.00 -2 9 0 4.10 2.20 2 9 0 1.20 2.30 2 9 0 4.10 2.40 -2 9 0 1.20 1.50 -3 -9 0 42.80 3.50 -3 -9 0 42.50 3.30 3 -9 0 49.60 4.10 -3 -9 0 34.30 4.20 3 -9 0 36.90 4.40 -3 9 0 41.70 2.00 -3 9 0 40.00 2.90 3 9 0 41.00 4.40 3 9 0 44.70 4.10 -3 9 0 32.30 4.10 3 9 0 42.80 4.70 -3 9 0 41.70 2.90 -3 9 0 40.80 3.00 3 9 0 34.70 3.90 -3 9 0 48.80 4.20 -3 9 0 41.20 3.00 3 9 0 38.20 3.70 -4 -9 0 3.30 0.90 4 -9 0 4.10 1.90 -4 -9 0 2.20 2.20 -4 -9 0 1.00 1.80 -4 -9 0 3.10 0.80 -4 -9 0 0.60 1.70 4 -9 0 9.90 2.50 -4 9 0 3.20 1.50 4 9 0 0.30 2.00 -4 9 0 6.10 2.30 -4 9 0 2.60 1.40 -4 9 0 -1.10 2.00 4 9 0 1.80 2.10 4 9 0 3.10 2.20 -4 9 0 3.90 1.30 -4 9 0 2.10 1.30 -4 9 0 5.00 1.50 4 9 0 6.30 2.50 4 9 0 0.80 2.90 -5 -9 0 41.40 3.80 5 -9 0 38.60 3.80 -5 -9 0 39.30 2.20 -5 -9 0 42.50 4.00 -5 -9 0 28.20 6.50 5 9 0 38.20 4.80 5 9 0 36.70 4.40 5 9 0 38.90 4.00 -5 9 0 36.70 2.40 5 9 0 38.80 4.50 -5 9 0 43.40 4.50 -5 9 0 40.20 2.60 -5 9 0 40.20 2.60 -5 9 0 37.90 3.00 -5 9 0 42.80 4.30 5 9 0 35.90 4.60 6 -9 0 14.80 2.80 -6 -9 0 16.40 3.00 -6 -9 0 17.70 2.20 -6 -9 0 21.40 3.60 -6 -9 0 17.80 3.20 -6 -9 0 14.60 2.80 -6 9 0 18.60 3.00 -6 9 0 17.30 2.00 6 9 0 25.40 4.10 -6 9 0 13.80 1.80 -6 9 0 17.20 2.40 -6 9 0 20.80 3.40 6 9 0 17.70 3.60 6 9 0 16.00 3.50 -6 9 0 14.10 1.80 6 9 0 17.90 3.30 -7 -9 0 0.10 2.10 -7 -9 0 0.20 2.50 -7 -9 0 1.00 1.50 -7 -9 0 -0.40 1.90 -7 -9 0 -4.80 2.30 7 -9 0 -0.70 2.10 7 9 0 -4.60 2.10 -7 9 0 0.80 1.10 -7 9 0 3.10 2.50 7 9 0 -0.80 2.20 -7 9 0 0.90 2.20 7 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2.90 12 9 0 -1.20 4.30 12 9 0 4.20 3.50 -12 9 0 4.70 1.60 -12 9 0 2.20 3.50 12 9 0 -3.70 4.20 -12 9 0 -1.60 3.60 -12 9 0 4.60 3.10 -13 -9 0 18.90 4.70 -13 -9 0 23.30 6.10 -13 -9 0 35.40 5.70 -13 -9 0 28.50 5.10 -13 -9 0 22.60 4.10 -13 9 0 28.60 3.30 -13 9 0 32.60 5.20 13 9 0 23.10 4.90 -13 9 0 25.00 4.30 13 9 0 25.60 5.70 13 9 0 25.70 5.90 -13 9 0 28.40 5.30 -14 -9 0 -1.90 4.40 -14 -9 0 -1.00 4.50 -14 -9 0 2.60 5.30 -14 -9 0 -0.50 4.40 -14 9 0 -0.70 2.20 14 9 0 0.70 5.60 14 9 0 -2.80 4.00 14 9 0 5.70 4.30 -14 9 0 -0.20 4.30 -14 9 0 0.80 3.50 -14 9 0 -3.70 4.50 -15 -9 0 1.10 4.90 -15 -9 0 0.30 4.20 -15 -9 0 2.50 4.90 -15 9 0 7.80 5.50 15 9 0 6.00 5.00 -15 9 0 -7.30 5.00 -15 9 0 3.40 2.60 15 9 0 -1.70 5.20 -16 -9 0 3.60 5.20 -16 -9 0 15.40 5.90 -16 -9 0 -0.30 5.80 -16 9 0 4.30 4.70 -16 9 0 -2.50 6.00 16 9 0 -0.60 5.60 -16 9 0 -1.20 4.40 -16 9 0 13.70 6.10 16 9 0 9.50 6.70 0 -10 0 1.10 0.90 0 -10 0 0.60 0.80 0 -10 0 2.30 2.00 0 -10 0 -1.20 2.20 0 10 0 0.80 2.30 0 10 0 -1.70 2.30 0 10 0 1.90 1.80 0 10 0 -0.10 1.80 0 10 0 0.50 1.80 -1 -10 0 6.80 1.60 -1 -10 0 8.90 1.60 1 -10 0 12.80 2.70 -1 -10 0 9.60 2.70 -1 -10 0 7.00 2.30 1 -10 0 8.10 2.60 -1 10 0 10.60 2.30 -1 10 0 12.60 2.50 1 10 0 5.10 2.60 -1 10 0 12.80 2.30 1 10 0 7.10 2.30 -1 10 0 9.10 2.80 -1 10 0 15.50 3.40 1 10 0 10.40 2.50 1 10 0 8.50 2.50 1 10 0 5.80 3.00 -2 -10 0 43.10 3.30 2 -10 0 40.10 3.90 2 -10 0 40.80 4.50 -2 -10 0 38.80 5.60 -2 -10 0 40.40 3.10 -2 10 0 39.90 4.90 -2 10 0 39.10 3.40 -2 10 0 41.60 3.60 -2 10 0 43.60 3.60 2 10 0 37.70 4.40 2 10 0 32.30 4.10 -2 10 0 43.20 4.60 -2 10 0 36.10 3.50 2 10 0 43.90 4.50 2 10 0 39.40 4.20 2 10 0 41.00 4.60 3 -10 0 -0.20 2.30 3 -10 0 0.70 1.70 -3 -10 0 -0.60 1.70 -3 -10 0 2.10 2.50 -3 -10 0 -0.50 1.90 -3 10 0 -1.40 1.60 -3 10 0 -2.10 1.60 -3 10 0 -3.10 2.10 3 10 0 0.70 2.20 3 10 0 -2.00 2.40 -3 10 0 0.80 1.60 3 10 0 -3.20 2.20 3 10 0 -0.30 2.00 -3 10 0 -0.50 1.70 3 10 0 -2.10 2.30 -3 10 0 -0.20 2.50 -4 -10 0 82.69 4.70 -4 -10 0 80.99 4.80 -4 -10 0 79.19 5.70 4 -10 0 77.29 5.50 4 -10 0 77.29 5.00 -4 10 0 78.99 4.00 -4 10 0 82.69 5.90 4 10 0 75.09 5.50 -4 10 0 77.19 3.80 -4 10 0 81.89 4.00 -4 10 0 78.19 3.10 4 10 0 86.19 6.10 -4 10 0 80.39 5.60 4 10 0 76.59 6.10 4 10 0 68.79 5.20 4 10 0 77.29 5.70 -5 -10 0 4.70 2.20 -5 -10 0 6.10 2.60 -5 -10 0 2.20 2.20 -5 -10 0 3.70 0.80 5 -10 0 2.90 2.30 -5 10 0 2.80 2.60 -5 10 0 2.80 1.40 5 10 0 1.10 2.80 -5 10 0 -0.30 1.40 5 10 0 0.40 2.80 -5 10 0 0.50 1.40 -5 10 0 3.80 1.50 -5 10 0 5.40 2.60 5 10 0 1.20 2.70 5 10 0 0.00 3.10 5 10 0 4.10 2.50 -6 -10 0 4.10 1.20 6 -10 0 6.50 2.40 -6 -10 0 3.50 2.40 -6 -10 0 4.70 2.90 6 10 0 6.30 2.60 -6 10 0 3.60 1.60 -6 10 0 2.90 1.30 -6 10 0 2.80 1.30 -6 10 0 7.30 1.90 -6 10 0 8.50 3.10 -6 10 0 3.00 2.90 6 10 0 5.10 2.80 6 10 0 3.90 2.80 6 10 0 8.40 3.20 7 -10 0 6.20 2.40 -7 -10 0 2.50 2.50 -7 -10 0 0.80 2.40 -7 -10 0 2.80 1.50 -7 -10 0 0.80 3.00 -7 10 0 2.20 2.80 -7 10 0 1.90 1.30 -7 10 0 0.50 2.00 7 10 0 2.60 2.70 7 10 0 -0.40 3.10 -7 10 0 1.50 2.80 -8 -10 0 26.50 3.10 -8 -10 0 24.00 3.60 8 -10 0 25.30 4.00 8 10 0 20.90 4.00 -8 10 0 23.80 3.20 -8 10 0 23.00 3.90 8 10 0 27.40 4.90 8 10 0 27.90 4.70 -8 10 0 27.10 3.80 -8 10 0 23.30 2.40 -9 -10 0 6.50 3.80 -9 -10 0 5.50 2.20 9 -10 0 9.20 3.10 -9 -10 0 8.30 3.40 9 10 0 3.20 3.30 9 10 0 10.50 3.70 -9 10 0 6.30 1.60 -9 10 0 12.50 3.40 9 10 0 6.80 4.20 -9 10 0 8.70 3.20 -9 10 0 7.50 2.90 -10 -10 0 24.00 4.20 -10 -10 0 23.10 5.10 -10 -10 0 20.90 4.50 -10 -10 0 18.50 4.10 10 -10 0 25.30 4.20 -10 -10 0 26.70 3.30 10 10 0 26.10 4.90 -10 10 0 22.50 4.50 10 10 0 17.50 4.70 10 10 0 17.50 4.80 -10 10 0 22.40 3.70 -10 10 0 19.30 2.40 -11 -10 0 5.00 3.70 -11 -10 0 1.60 4.60 -11 -10 0 -1.00 2.70 -11 -10 0 3.70 3.70 -11 -10 0 6.90 3.90 -11 10 0 1.80 1.50 -11 10 0 1.70 3.50 11 10 0 2.20 3.90 -11 10 0 1.50 3.70 11 10 0 -1.60 3.60 -11 10 0 0.90 3.60 11 10 0 -8.50 4.10 -12 -10 0 8.50 5.40 -12 -10 0 0.50 4.20 -12 -10 0 7.50 4.50 -12 -10 0 5.40 3.10 -12 -10 0 5.20 4.20 -12 10 0 8.60 3.80 12 10 0 14.00 4.70 12 10 0 13.40 5.30 -12 10 0 7.80 1.90 12 10 0 6.40 3.90 -12 10 0 6.70 4.00 -12 10 0 9.60 4.30 -13 -10 0 1.30 4.90 -13 -10 0 1.80 5.50 -13 -10 0 6.60 3.70 -13 -10 0 4.60 4.80 13 10 0 -3.40 4.40 -13 10 0 -4.80 4.10 -13 10 0 3.10 2.10 13 10 0 0.20 6.30 -13 10 0 2.80 3.90 13 10 0 -3.00 4.10 -13 10 0 0.80 4.30 -14 -10 0 6.10 5.50 -14 10 0 6.80 2.40 14 10 0 3.60 5.20 -14 10 0 7.20 5.20 -14 10 0 -8.10 5.10 -14 10 0 1.20 4.40 14 10 0 1.00 5.50 -15 -10 0 -8.60 4.70 -15 -10 0 1.60 5.80 -15 10 0 -1.10 4.90 -15 10 0 -1.70 5.70 -15 10 0 2.40 6.00 15 10 0 -4.30 6.60 15 10 0 8.20 6.00 0 -11 0 -2.70 2.10 0 -11 0 -3.50 2.30 0 11 0 1.00 2.20 0 11 0 2.40 3.20 0 11 0 -2.40 2.50 0 11 0 1.00 2.40 0 11 0 0.00 2.90 -1 -11 0 44.90 5.10 1 -11 0 39.40 4.30 1 -11 0 46.50 4.90 -1 -11 0 32.40 2.50 -1 -11 0 39.10 2.70 -1 -11 0 35.20 4.50 1 11 0 38.10 4.40 -1 11 0 41.30 5.10 -1 11 0 37.50 4.20 1 11 0 40.20 4.70 1 11 0 36.60 4.50 1 11 0 46.20 5.50 -1 11 0 39.40 4.00 1 11 0 41.00 4.30 -1 11 0 37.30 4.10 -1 11 0 40.80 4.10 -2 -11 0 3.40 1.70 -2 -11 0 1.70 2.50 2 -11 0 -1.40 2.20 -2 -11 0 -0.10 2.80 -2 -11 0 1.60 1.60 2 -11 0 3.10 2.50 2 11 0 4.80 2.70 -2 11 0 3.30 2.80 2 11 0 -1.50 2.40 2 11 0 2.50 2.40 -2 11 0 2.30 2.20 2 11 0 -0.70 2.60 -2 11 0 2.70 2.10 -2 11 0 0.70 3.00 3 -11 0 72.59 5.70 -3 -11 0 75.39 4.40 3 -11 0 76.99 5.20 -3 -11 0 79.89 4.60 -3 -11 0 75.09 6.10 -3 11 0 72.29 4.40 -3 11 0 72.89 4.40 3 11 0 68.99 5.40 -3 11 0 64.59 6.40 3 11 0 74.89 5.90 3 11 0 77.89 6.80 -3 11 0 74.19 5.90 -3 11 0 68.09 4.40 3 11 0 79.69 6.40 3 11 0 79.59 6.00 -4 -11 0 2.90 2.20 4 -11 0 4.30 2.40 -4 -11 0 -2.00 2.00 4 -11 0 -0.60 2.70 -4 -11 0 4.10 3.00 4 11 0 2.90 2.80 -4 11 0 5.80 3.20 4 11 0 1.20 2.50 4 11 0 -3.00 3.00 -4 11 0 2.70 2.90 -4 11 0 2.80 1.80 4 11 0 3.90 3.10 -4 11 0 -1.00 1.70 -4 11 0 3.40 2.10 5 -11 0 24.60 3.70 -5 -11 0 27.10 3.50 -5 -11 0 22.90 3.30 -5 11 0 23.50 3.00 -5 11 0 22.60 4.20 -5 11 0 27.70 3.90 -5 11 0 25.30 2.80 -5 11 0 22.30 2.80 5 11 0 22.70 3.80 5 11 0 20.20 7.00 5 11 0 20.30 3.90 -5 11 0 25.30 2.40 5 11 0 27.10 5.00 6 -11 0 -2.40 2.20 -6 -11 0 -4.00 2.30 -6 -11 0 -2.80 2.30 -6 11 0 -2.50 1.40 6 11 0 -1.20 3.00 -6 11 0 3.00 3.20 -6 11 0 -1.00 1.50 -6 11 0 -1.90 1.70 6 11 0 -1.10 3.20 6 11 0 -1.90 2.60 -6 11 0 1.70 2.80 -6 11 0 0.80 1.60 -7 -11 0 54.89 6.90 7 -11 0 51.99 5.30 -7 -11 0 45.80 2.70 -7 -11 0 48.40 5.70 -7 -11 0 47.80 2.80 -7 -11 0 54.59 5.40 7 11 0 53.49 6.50 -7 11 0 58.29 6.20 -7 11 0 48.20 3.40 -7 11 0 60.29 6.20 7 11 0 51.79 6.10 -7 11 0 50.19 4.20 7 11 0 53.99 6.40 -8 -11 0 4.60 1.80 -8 -11 0 11.40 4.30 8 -11 0 9.10 3.40 -8 11 0 7.60 3.70 -8 11 0 9.00 3.60 -8 11 0 5.10 1.80 8 11 0 7.80 3.90 8 11 0 4.20 4.00 8 11 0 11.60 4.50 -8 11 0 8.20 2.70 -9 -11 0 9.70 3.80 -9 -11 0 19.80 5.20 9 -11 0 22.50 4.20 -9 -11 0 20.10 2.60 -9 -11 0 22.90 4.10 9 11 0 18.10 4.40 9 11 0 30.00 5.40 9 11 0 10.20 4.50 -9 11 0 14.20 4.10 -9 11 0 19.40 4.40 -9 11 0 18.00 2.20 -9 11 0 23.50 3.60 -10 -11 0 6.70 3.90 -10 -11 0 7.80 2.60 -10 -11 0 8.80 3.90 -10 -11 0 5.80 4.70 10 -11 0 10.20 3.70 10 11 0 5.20 4.50 10 11 0 4.20 4.20 -10 11 0 11.10 4.00 -10 11 0 5.80 3.40 -10 11 0 7.30 1.90 10 11 0 5.40 5.10 -10 11 0 8.10 4.00 -11 -11 0 31.50 3.70 -11 -11 0 27.70 5.20 -11 -11 0 33.70 6.40 -11 -11 0 37.70 5.40 11 11 0 30.50 6.20 -11 11 0 23.80 5.00 11 11 0 31.40 6.50 11 11 0 30.70 6.10 -11 11 0 29.60 4.70 -11 11 0 30.90 5.20 -11 11 0 32.90 3.30 -12 -11 0 5.00 3.30 -12 -11 0 -1.80 4.80 -12 -11 0 -0.50 4.50 12 11 0 -2.80 5.00 12 11 0 -4.40 4.10 12 11 0 10.10 7.00 -12 11 0 3.20 2.20 -12 11 0 1.10 4.30 -12 11 0 13.50 4.90 -12 11 0 8.60 4.40 -13 -11 0 16.80 6.00 -13 -11 0 25.40 4.50 -13 11 0 8.70 5.00 -13 11 0 17.90 5.00 -13 11 0 13.20 2.40 13 11 0 32.10 8.90 13 11 0 27.20 6.20 13 11 0 14.80 5.80 -13 11 0 16.10 5.70 0 -12 0 20.30 3.80 0 -12 0 25.40 4.20 0 12 0 16.20 3.20 0 12 0 30.30 4.20 0 12 0 20.40 3.90 0 12 0 16.00 4.30 -1 -12 0 4.40 2.90 -1 -12 0 -0.90 1.10 -1 -12 0 -2.10 2.40 -1 -12 0 0.20 1.10 1 -12 0 -0.10 2.60 1 -12 0 0.80 2.90 -1 12 0 3.60 3.20 1 12 0 -1.10 2.50 -1 12 0 -1.50 3.30 1 12 0 -0.30 2.60 1 12 0 -3.80 2.90 1 12 0 -1.90 3.30 -1 12 0 -1.50 2.40 -1 12 0 1.60 2.50 -2 -12 0 52.69 3.60 2 -12 0 54.49 5.90 -2 -12 0 58.49 5.50 -2 -12 0 55.19 3.70 2 -12 0 54.59 5.20 -2 12 0 59.29 4.90 -2 12 0 50.09 5.90 -2 12 0 54.69 4.80 2 12 0 52.99 5.60 -2 12 0 52.69 5.90 2 12 0 40.50 5.30 2 12 0 49.70 5.70 -3 -12 0 -2.30 2.60 -3 -12 0 0.60 2.00 3 -12 0 -0.90 3.10 -3 -12 0 -1.00 2.00 3 -12 0 2.10 2.40 -3 12 0 1.20 2.30 3 12 0 6.90 4.00 -3 12 0 1.50 2.20 3 12 0 -0.50 3.00 -3 12 0 1.50 3.20 -3 12 0 -7.30 3.00 3 12 0 -0.50 3.00 3 12 0 6.10 3.40 4 -12 0 21.50 3.70 -4 -12 0 20.40 3.10 4 -12 0 29.50 4.50 -4 -12 0 19.40 3.20 4 12 0 20.90 4.20 -4 12 0 22.00 4.30 -4 12 0 22.60 2.90 -4 12 0 21.90 2.80 4 12 0 16.00 4.30 4 12 0 23.60 4.70 -4 12 0 28.90 5.10 4 12 0 21.90 4.60 5 -12 0 1.80 2.70 -5 -12 0 -5.30 3.40 -5 -12 0 1.80 2.80 -5 -12 0 -0.40 2.60 -5 12 0 3.40 2.20 5 12 0 6.60 3.90 -5 12 0 -1.70 3.40 -5 12 0 0.00 3.90 5 12 0 2.80 3.70 -5 12 0 3.10 1.90 -5 12 0 0.60 2.00 5 12 0 -4.50 3.70 5 12 0 0.30 3.80 -6 -12 0 17.70 3.60 -6 -12 0 22.10 4.70 -6 -12 0 14.90 3.50 6 -12 0 20.80 3.80 -6 12 0 13.50 2.70 6 12 0 23.00 5.20 -6 12 0 19.70 2.20 -6 12 0 17.50 2.20 6 12 0 12.90 4.40 6 12 0 15.40 4.10 -6 12 0 18.80 2.00 -6 12 0 19.80 4.70 -7 -12 0 4.90 3.30 -7 -12 0 2.60 3.20 -7 -12 0 8.70 4.40 7 -12 0 6.90 3.30 7 12 0 5.70 4.60 -7 12 0 7.90 4.40 -7 12 0 3.90 2.30 7 12 0 3.00 4.30 -7 12 0 5.50 2.30 -7 12 0 3.50 3.80 7 12 0 3.30 4.20 -8 -12 0 19.30 5.10 -8 -12 0 21.80 4.20 -8 -12 0 19.60 2.10 8 -12 0 20.00 4.30 -8 -12 0 16.20 1.70 -8 -12 0 16.80 4.60 -8 12 0 20.10 4.70 8 12 0 25.30 5.60 8 12 0 18.40 5.10 -8 12 0 17.00 2.60 -8 12 0 20.00 3.20 8 12 0 25.10 6.30 -8 12 0 23.00 4.60 -9 -12 0 6.40 5.70 -9 -12 0 3.80 3.90 -9 -12 0 1.40 1.90 -9 -12 0 7.90 3.90 9 -12 0 4.90 3.50 9 12 0 -4.50 4.50 -9 12 0 0.10 4.30 9 12 0 2.10 4.50 -9 12 0 2.40 2.20 9 12 0 -5.70 4.60 -9 12 0 4.60 4.60 -9 12 0 5.90 3.20 10 -12 0 6.80 3.50 -10 -12 0 -3.60 5.60 -10 -12 0 7.00 2.50 -10 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2.90 -2 13 0 -0.30 2.70 -2 13 0 -0.70 3.70 -2 13 0 -0.30 4.00 2 13 0 -3.40 3.80 -3 -13 0 26.80 5.20 -3 -13 0 34.70 5.00 -3 -13 0 35.70 4.00 3 -13 0 32.20 4.50 -3 -13 0 37.70 4.20 -3 13 0 40.00 4.80 3 13 0 28.10 4.70 3 13 0 37.10 5.60 3 13 0 29.80 5.40 -3 13 0 41.00 5.40 -3 13 0 34.60 3.90 3 13 0 32.70 6.20 -3 13 0 45.70 6.50 -4 -13 0 -5.30 4.30 4 -13 0 4.40 3.20 -4 -13 0 1.80 2.50 -4 -13 0 -1.40 2.50 -4 -13 0 5.20 3.50 -4 13 0 0.50 4.40 -4 13 0 0.20 3.10 4 13 0 2.00 3.60 -4 13 0 -0.50 3.90 -4 13 0 1.80 2.30 4 13 0 3.80 4.80 4 13 0 0.30 4.00 4 13 0 -2.30 4.10 -5 -13 0 17.90 3.60 -5 -13 0 15.40 4.60 5 -13 0 19.50 4.00 -5 -13 0 26.00 5.20 -5 13 0 18.80 2.90 -5 13 0 24.50 3.10 -5 13 0 25.10 5.60 5 13 0 31.00 5.00 5 13 0 29.50 5.90 -5 13 0 23.10 4.90 5 13 0 21.80 5.20 -6 -13 0 8.50 3.40 -6 -13 0 5.40 5.20 6 -13 0 3.90 3.30 -6 -13 0 5.80 3.70 -6 13 0 2.90 2.00 -6 13 0 -3.80 4.30 6 13 0 4.30 4.00 6 13 0 14.30 5.70 6 13 0 2.90 4.90 -6 13 0 2.20 2.10 -6 13 0 12.00 4.70 -7 -13 0 35.50 6.40 -7 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5.30 8 -11 -6 14.40 6.00 -8 11 6 25.70 5.20 8 11 -6 24.70 5.10 -8 11 6 31.30 4.00 8 11 -6 20.10 5.10 8 11 -6 36.60 6.30 -8 11 6 25.20 4.20 -8 11 6 25.60 3.40 7 -11 -6 4.80 2.90 -7 -11 6 3.10 3.60 -7 -11 6 3.30 3.20 -7 -11 6 1.70 3.40 -7 -11 6 7.70 4.70 -7 11 6 8.40 3.20 -7 11 6 3.50 2.60 7 11 -6 7.70 4.40 -7 11 6 2.30 3.70 -7 11 6 8.40 2.90 7 11 -6 1.20 3.70 -7 11 6 -2.50 4.00 7 11 -6 3.80 4.50 -6 -11 6 43.30 6.10 -6 -11 6 56.89 5.10 6 -11 -6 49.40 4.90 -6 -11 6 51.79 5.80 -6 -11 6 48.00 5.40 -6 11 6 43.90 5.20 6 11 -6 38.00 5.00 -6 11 6 52.89 5.30 -6 11 6 45.70 4.80 6 11 -6 49.30 6.60 6 11 -6 47.70 6.30 -6 11 6 60.19 6.50 -6 11 6 50.09 6.30 -5 -11 6 17.70 3.30 -5 -11 6 12.40 3.20 -5 -11 6 16.60 4.60 -5 -11 6 17.90 2.90 -5 -11 6 20.10 4.20 5 -11 -6 6.60 2.80 5 -11 -6 14.00 2.70 -5 11 6 10.20 3.10 -5 11 6 14.00 3.20 5 11 -6 6.90 3.70 5 11 -6 16.90 4.30 -5 11 6 15.40 4.20 5 11 -6 10.60 3.30 -5 11 6 16.20 3.10 -5 11 6 13.00 4.20 4 -11 -6 33.40 3.60 -4 -11 6 32.30 3.80 -4 -11 6 41.10 5.00 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-12 6 40.60 5.20 -5 12 6 43.50 5.60 -5 12 6 37.90 5.60 5 12 -6 38.40 6.20 5 12 -6 31.90 6.40 -5 12 6 31.60 4.20 -5 12 6 40.10 5.10 -4 -12 6 12.50 3.70 4 -12 -6 7.20 2.60 -4 -12 6 3.70 3.60 4 -12 -6 3.10 4.60 -4 -12 6 5.40 2.40 4 -12 -6 7.80 2.40 -4 -12 6 6.50 2.60 -4 -12 6 2.50 4.40 -4 12 6 6.90 3.10 -4 12 6 3.70 2.80 -4 12 6 5.40 3.50 -4 12 6 5.00 4.20 4 12 -6 9.30 4.70 4 12 -6 4.00 3.40 -4 12 6 11.20 5.00 4 12 -6 4.00 3.80 3 -12 -6 78.79 4.70 3 -12 -6 57.99 6.70 -3 -12 6 77.89 6.30 -3 -12 6 69.99 8.00 -3 -12 6 77.49 4.00 -3 -12 6 76.39 4.20 -3 -12 6 70.99 7.00 3 -12 -6 73.89 4.60 -3 12 6 81.09 7.60 3 12 -6 71.79 8.40 3 12 -6 80.69 7.00 -3 12 6 67.79 5.80 -3 12 6 79.89 6.60 -3 12 6 75.39 6.20 -3 12 6 74.09 8.40 3 12 -6 80.09 7.00 3 12 -6 76.49 7.10 2 -12 -6 11.90 4.50 -2 -12 6 4.00 3.60 2 -12 -6 1.40 2.20 -2 -12 6 3.90 3.50 2 -12 -6 1.50 2.10 -2 -12 6 -0.50 3.10 2 12 -6 1.40 3.10 2 12 -6 4.30 4.70 2 12 -6 4.60 3.80 -2 12 6 3.50 3.40 -2 12 6 1.20 3.60 -2 12 6 1.40 3.00 2 12 -6 2.80 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5 -10 146.59 7.80 -8 5 10 147.39 7.50 8 5 -10 143.09 7.80 7 -5 -10 4.30 2.40 -7 -5 10 1.80 2.40 7 -5 -10 2.30 2.00 7 -5 -10 2.50 1.60 -7 -5 10 2.10 2.60 -7 -5 10 3.50 2.30 -7 -5 10 -1.30 1.90 -7 5 10 4.50 2.50 7 5 -10 1.20 1.90 -7 5 10 1.30 2.20 7 5 -10 2.90 2.70 -7 5 10 3.20 2.10 -7 5 10 -0.50 2.20 7 5 -10 5.00 2.30 7 5 -10 2.20 2.10 -7 5 10 1.70 1.60 -6 -5 10 202.18 7.60 6 -5 -10 225.28 8.00 -6 -5 10 215.08 8.70 -6 -5 10 203.88 8.60 6 -5 -10 219.98 7.10 6 -5 -10 220.38 8.90 -6 -5 10 215.48 8.00 -6 5 10 214.68 7.70 6 5 -10 207.28 7.70 -6 5 10 221.28 8.70 6 5 -10 210.78 8.70 -6 5 10 208.98 8.20 -6 5 10 217.28 8.70 6 5 -10 212.98 8.10 6 5 -10 206.98 9.00 -5 -5 10 3.60 2.00 -5 -5 10 3.10 2.60 -5 -5 10 4.10 1.90 5 -5 -10 3.00 2.20 5 -5 -10 3.70 1.70 5 -5 -10 7.00 2.40 -5 -5 10 1.30 2.00 5 5 -10 4.50 2.10 -5 5 10 3.90 2.10 5 5 -10 10.70 3.00 5 5 -10 6.80 2.10 -5 5 10 2.90 2.00 -5 5 10 4.60 2.30 -5 5 10 4.40 2.00 4 -5 -10 34.00 4.20 4 -5 -10 35.80 3.20 -4 -5 10 31.60 3.40 -4 -5 10 31.10 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8.40 3 1 22 68.19 6.30 3 1 22 83.19 8.40 -3 1 -22 75.49 9.90 4 -1 22 50.39 7.00 4 -1 22 43.60 5.40 4 -1 22 51.39 6.30 -4 -1 -22 48.40 7.90 -4 1 -22 43.40 6.50 4 1 22 46.10 6.90 4 1 22 36.40 5.80 4 1 22 45.00 4.80 5 -2 -22 48.60 7.50 5 2 -22 64.39 9.00 4 -2 -22 25.30 6.50 -4 -2 22 40.10 5.70 -4 -2 22 36.30 6.40 -4 -2 22 34.40 4.40 -4 2 22 26.30 5.30 -4 2 22 27.60 6.10 4 2 -22 32.40 6.50 -3 -2 22 45.90 6.40 -3 -2 22 60.19 6.40 -3 -2 22 51.59 5.50 3 -2 -22 45.20 7.50 -3 2 22 51.39 5.90 -3 2 22 54.99 7.60 -3 2 22 58.99 5.50 -2 -2 22 52.19 9.00 2 -2 -22 80.59 10.20 -2 -2 22 65.79 7.50 -2 -2 22 72.39 8.40 -2 -2 22 57.79 5.50 -2 2 22 67.99 4.80 -2 2 22 64.89 7.40 -2 2 22 76.99 9.60 2 2 -22 87.29 10.70 -1 -2 22 42.90 5.00 -1 -2 22 51.99 6.20 1 -2 -22 44.40 7.30 -1 -2 22 44.00 8.30 -1 -2 22 57.59 7.30 -1 2 22 51.59 5.50 -1 2 22 51.19 6.70 1 2 -22 43.40 7.40 -1 2 22 43.70 7.90 0 -2 22 106.09 8.20 0 -2 -22 109.89 10.90 0 -2 22 98.69 10.90 0 -2 22 94.39 8.20 0 2 22 87.09 9.50 0 2 22 92.69 11.80 0 2 22 103.59 9.20 1 -2 22 89.19 10.30 1 -2 22 79.39 7.60 1 -2 22 65.09 7.60 -1 -2 -22 58.19 8.00 -1 2 -22 71.59 9.40 1 2 22 65.19 7.00 1 2 22 76.39 9.00 1 2 22 45.40 7.70 2 -2 22 40.50 5.40 2 -2 22 57.99 7.70 2 -2 22 31.90 6.60 -2 -2 -22 42.70 7.40 -2 2 -22 37.30 6.40 2 2 22 48.20 5.20 2 2 22 43.30 6.20 2 2 22 47.20 7.30 3 -2 22 24.10 5.40 -3 -2 -22 17.50 6.00 3 -2 22 31.00 4.70 3 -2 22 40.20 6.50 3 2 22 33.50 5.70 3 2 22 27.10 4.80 -3 2 -22 16.70 5.70 4 -2 22 48.30 6.50 4 -2 22 46.80 7.10 -4 -2 -22 37.60 6.60 4 -2 22 42.20 5.20 -4 2 -22 30.50 6.40 4 2 22 47.20 6.30 4 2 22 32.20 6.90 4 2 22 43.30 5.20 4 -3 -22 42.00 7.60 -3 -3 22 48.80 6.40 -3 -3 22 58.59 6.80 -3 3 22 57.19 7.40 -3 3 22 38.00 6.10 3 3 -22 42.80 7.20 2 -3 -22 32.40 7.30 -2 -3 22 46.80 6.20 -2 -3 22 45.10 6.20 2 3 -22 27.30 5.40 -2 3 22 40.70 5.60 -2 3 22 40.80 6.60 -1 -3 22 42.20 7.60 -1 -3 22 56.39 6.30 1 -3 -22 68.69 8.70 1 3 -22 59.79 8.00 -1 3 22 50.39 6.00 -1 3 22 63.69 7.50 0 -3 22 41.70 6.10 0 -3 22 38.30 5.40 0 -3 -22 33.30 6.70 0 -3 22 29.10 7.40 0 3 22 29.60 6.90 0 3 22 44.30 5.60 0 3 22 30.20 6.10 0 3 -22 40.70 7.50 1 -3 22 25.90 4.80 -1 -3 -22 39.60 7.40 1 -3 22 33.30 5.90 1 -3 22 29.30 7.30 -1 3 -22 26.40 6.40 1 3 22 37.60 5.10 1 3 22 36.20 6.20 1 3 22 24.70 7.10 2 -3 22 9.30 6.00 2 -3 22 17.20 4.50 2 -3 22 12.70 5.00 -2 -3 -22 24.60 5.80 2 3 22 15.00 5.50 2 3 22 8.80 6.70 -2 3 -22 18.70 6.50 3 -3 22 39.20 6.70 3 -3 22 24.30 4.70 -3 -3 -22 21.30 6.20 3 3 22 32.70 5.20 -3 3 -22 28.90 7.10 3 3 22 27.90 5.70 3 3 22 19.10 6.60 1 -4 -22 19.50 7.00 0 -4 -22 25.90 6.50 0 -4 22 33.20 5.10 0 -4 22 12.50 7.00 0 4 22 27.00 5.60 0 4 22 18.10 5.80 0 4 -22 28.60 6.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 31094 _shelx_res_file ; TITL Pd-TSC in P2(1)/c shelx.res created by SHELXL-2018/3 at 13:53:16 on 23-Jul-2023 CELL 0.71073 15.0839 11.4179 17.0970 90.000 91.097 90.000 ZERR 4.000 0.0046 0.0036 0.0055 0.000 0.009 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N PD S UNIT 128 112 24 4 8 L.S. 25 LIST 4 FMAP 2 PLAN 20 CONF BOND $H ACTA OMIT 0 2 0 OMIT 1 1 0 OMIT 3 9 6 TEMP 25.930 SIZE 0.106 0.18 0.253 EQIV $1 x, -y+1/2, z+1/2 EQIV $2 x, -y+1/2, z-1/2 HTAB C1 S2 HTAB C16 N2 HTAB C17 S1 HTAB C32 N5 HTAB N3 S2_$1 HTAB N6 S1_$2 MPLA Pd1 N1 N4 S1 S2 MPLA Pd1 C10 C26 S1 S2 N1 N2 N4 N5 MPLA C4 C5 C6 C7 C8 C9 MPLA C20 C21 C22 C23 C24 C25 MPLA C11 C12 C13 C14 C15 C16 MPLA C27 C28 C29 C30 C31 C32 MPLA C4 C5 C6 C7 C8 C9 MPLA C11 C12 C13 C14 C15 C16 MPLA C20 C21 C22 C23 C24 C25 MPLA C27 C28 C29 C30 C31 C32 WGHT 0.024100 1.522700 FVAR 0.29085 C1 1 0.931142 0.256459 0.414776 11.00000 0.03195 0.05894 = 0.03145 -0.00140 0.00196 -0.00180 AFIX 43 H1 2 0.911357 0.222755 0.368099 11.00000 -1.20000 AFIX 0 C2 1 1.021878 0.292615 0.418776 11.00000 0.03267 0.06245 = 0.03366 0.00053 -0.00015 -0.00454 AFIX 43 H2 2 1.042322 0.334403 0.462190 11.00000 -1.20000 AFIX 0 C3 1 1.077771 0.267799 0.361735 11.00000 0.03369 0.06062 = 0.03583 0.00060 0.00154 -0.00372 AFIX 43 H3 2 1.054715 0.228656 0.318196 11.00000 -1.20000 AFIX 0 C4 1 1.171862 0.296588 0.361555 11.00000 0.03265 0.05748 = 0.04073 0.01011 0.00182 -0.00256 C5 1 1.208727 0.380142 0.411067 11.00000 0.04446 0.06558 = 0.05964 0.00318 -0.00395 -0.00597 AFIX 43 H4 2 1.172634 0.422924 0.444057 11.00000 -1.20000 AFIX 0 C6 1 1.298970 0.399957 0.411483 11.00000 0.05515 0.08157 = 0.08377 0.01509 -0.02093 -0.02225 AFIX 43 H5 2 1.323135 0.457206 0.444183 11.00000 -1.20000 AFIX 0 C7 1 1.353599 0.336177 0.364195 11.00000 0.03483 0.09400 = 0.10044 0.04186 -0.00402 -0.00805 AFIX 43 H6 2 1.414532 0.348617 0.366163 11.00000 -1.20000 AFIX 0 C8 1 1.318647 0.255491 0.314917 11.00000 0.04164 0.09681 = 0.08576 0.02066 0.02063 0.00777 AFIX 43 H7 2 1.355493 0.212955 0.282440 11.00000 -1.20000 AFIX 0 C9 1 1.228138 0.235847 0.312562 11.00000 0.04452 0.08050 = 0.05945 -0.00114 0.01509 -0.00298 AFIX 43 H8 2 1.204591 0.181127 0.277638 11.00000 -1.20000 AFIX 0 C10 1 0.853426 0.315036 0.596148 11.00000 0.03137 0.04747 = 0.03430 -0.00055 0.00167 0.00020 C11 1 0.957661 0.420488 0.688286 11.00000 0.03507 0.04861 = 0.03536 0.00005 -0.00292 0.00001 C12 1 0.955706 0.486328 0.756460 11.00000 0.04462 0.05574 = 0.03962 -0.00316 0.00164 -0.00239 AFIX 43 H9 2 0.904012 0.489377 0.785175 11.00000 -1.20000 AFIX 0 C13 1 1.029703 0.547299 0.782048 11.00000 0.05778 0.05956 = 0.04994 -0.01031 -0.00667 -0.00540 AFIX 43 H10 2 1.027308 0.591307 0.827731 11.00000 -1.20000 AFIX 0 C14 1 1.106736 0.543695 0.740835 11.00000 0.04433 0.06549 = 0.06498 -0.00047 -0.01280 -0.01028 AFIX 43 H11 2 1.156512 0.585126 0.757969 11.00000 -1.20000 AFIX 0 C15 1 1.108938 0.477657 0.673715 11.00000 0.03406 0.08260 = 0.06241 -0.00318 0.00098 -0.00339 AFIX 43 H12 2 1.161063 0.474407 0.645610 11.00000 -1.20000 AFIX 0 C16 1 1.035655 0.415978 0.646948 11.00000 0.03606 0.07349 = 0.04530 -0.00962 0.00160 0.00088 AFIX 43 H13 2 1.038671 0.371677 0.601430 11.00000 -1.20000 AFIX 0 C17 1 0.558386 0.167195 0.502334 11.00000 0.03597 0.05422 = 0.03473 -0.00372 0.00362 -0.00158 AFIX 43 H14 2 0.578917 0.185524 0.552491 11.00000 -1.20000 AFIX 0 C18 1 0.465970 0.140448 0.493575 11.00000 0.03558 0.05423 = 0.03918 -0.00079 0.00530 -0.00068 AFIX 43 H15 2 0.444566 0.115183 0.445071 11.00000 -1.20000 AFIX 0 C19 1 0.409473 0.150302 0.552087 11.00000 0.04129 0.05857 = 0.04197 -0.00092 0.00776 -0.00176 AFIX 43 H16 2 0.433316 0.172755 0.600361 11.00000 -1.20000 AFIX 0 C20 1 0.314195 0.129576 0.548371 11.00000 0.03896 0.05051 = 0.04713 0.00712 0.01156 0.00183 C21 1 0.272107 0.074578 0.486041 11.00000 0.04147 0.06092 = 0.05161 0.00810 0.00721 0.00243 AFIX 43 H17 2 0.305174 0.047797 0.444312 11.00000 -1.20000 AFIX 0 C22 1 0.181343 0.059044 0.485194 11.00000 0.04677 0.07403 = 0.07217 0.01668 -0.00709 -0.00500 AFIX 43 H18 2 0.153934 0.021536 0.442935 11.00000 -1.20000 AFIX 0 C23 1 0.131422 0.097901 0.545397 11.00000 0.03794 0.08038 = 0.09625 0.02827 0.01490 0.00396 AFIX 43 H19 2 0.070293 0.087173 0.544212 11.00000 -1.20000 AFIX 0 C24 1 0.171589 0.152622 0.607412 11.00000 0.05387 0.08038 = 0.08888 0.00857 0.03624 0.00549 AFIX 43 H20 2 0.137628 0.180199 0.648339 11.00000 -1.20000 AFIX 0 C25 1 0.262403 0.167316 0.609782 11.00000 0.05390 0.07823 = 0.06454 -0.00499 0.02457 -0.00268 AFIX 43 H21 2 0.289272 0.202928 0.653032 11.00000 -1.20000 AFIX 0 C26 1 0.636958 0.141160 0.318569 11.00000 0.03152 0.05539 = 0.03507 -0.00163 0.00208 -0.00125 C27 1 0.528361 0.067302 0.217546 11.00000 0.03234 0.05533 = 0.04881 -0.01014 -0.00397 0.00095 C28 1 0.508830 0.080899 0.139482 11.00000 0.06310 0.07506 = 0.05825 0.00745 -0.02047 -0.01273 AFIX 43 H22 2 0.547569 0.121832 0.107827 11.00000 -1.20000 AFIX 0 C29 1 0.431881 0.034084 0.107637 11.00000 0.08378 0.09476 = 0.08301 0.00465 -0.04766 -0.01322 AFIX 43 H23 2 0.418657 0.044846 0.054772 11.00000 -1.20000 AFIX 0 C30 1 0.375598 -0.027221 0.152536 11.00000 0.05203 0.08910 = 0.10901 -0.02010 -0.02689 -0.01283 AFIX 43 H24 2 0.323855 -0.058496 0.130698 11.00000 -1.20000 AFIX 0 C31 1 0.395111 -0.043070 0.230328 11.00000 0.05660 0.08652 = 0.09811 -0.02432 0.00739 -0.02829 AFIX 43 H25 2 0.356585 -0.085945 0.261047 11.00000 -1.20000 AFIX 0 C32 1 0.471403 0.003849 0.263884 11.00000 0.05199 0.07875 = 0.05917 -0.01214 0.00313 -0.01543 AFIX 43 H26 2 0.484228 -0.007087 0.316803 11.00000 -1.20000 AFIX 0 N1 3 0.873631 0.266143 0.470076 11.00000 0.02990 0.05229 = 0.03026 -0.00227 0.00091 -0.00142 N2 3 0.907672 0.315867 0.538497 11.00000 0.03239 0.06447 = 0.03161 -0.00593 0.00167 -0.00578 N3 3 0.878732 0.361108 0.666575 11.00000 0.03481 0.06588 = 0.03193 -0.00670 0.00451 -0.00695 AFIX 43 H27 2 0.841082 0.352842 0.703313 11.00000 -1.20000 AFIX 0 N4 3 0.616000 0.168373 0.447479 11.00000 0.03040 0.04960 = 0.03490 -0.00231 0.00299 -0.00231 N5 3 0.580901 0.136193 0.374630 11.00000 0.03220 0.06463 = 0.03423 -0.00546 0.00275 -0.00575 N6 3 0.610377 0.112956 0.244274 11.00000 0.03410 0.08778 = 0.03463 -0.00812 0.00278 -0.01105 AFIX 43 H28 2 0.649000 0.124627 0.208750 11.00000 -1.20000 AFIX 0 PD1 4 0.745280 0.216290 0.460394 11.00000 0.02574 0.04563 = 0.03007 -0.00124 0.00212 -0.00040 S1 5 0.746048 0.256546 0.592313 11.00000 0.03440 0.07490 = 0.03486 -0.00998 0.00699 -0.01189 S2 5 0.746757 0.184163 0.328592 11.00000 0.02752 0.08657 = 0.03186 -0.00707 0.00370 -0.00685 HKLF 4 REM Pd-TSC in P2(1)/c REM wR2 = 0.0628, GooF = S = 1.048, Restrained GooF = 1.048 for all data REM R1 = 0.0255 for 6204 Fo > 4sig(Fo) and 0.0360 for all 7344 data REM 370 parameters refined using 0 restraints END WGHT 0.0241 1.5228 REM Highest difference peak 0.338, deepest hole -0.499, 1-sigma level 0.049 Q1 1 0.7347 0.3084 0.5621 11.00000 0.05 0.34 Q2 1 0.7374 0.2888 0.4461 11.00000 0.05 0.25 Q3 1 0.6826 0.1555 0.3347 11.00000 0.05 0.23 Q4 1 0.4794 0.0784 0.2400 11.00000 0.05 0.22 Q5 1 0.9624 0.4390 0.7245 11.00000 0.05 0.21 Q6 1 1.1820 0.3495 0.3813 11.00000 0.05 0.21 Q7 1 1.3216 0.3413 0.4093 11.00000 0.05 0.21 Q8 1 0.8859 0.3060 0.5005 11.00000 0.05 0.21 Q9 1 0.9971 0.4035 0.6694 11.00000 0.05 0.21 Q10 1 1.0393 0.3567 0.6476 11.00000 0.05 0.21 Q11 1 0.7156 0.2176 0.6307 11.00000 0.05 0.20 Q12 1 1.0805 0.4224 0.6793 11.00000 0.05 0.20 Q13 1 0.7443 0.1189 0.3563 11.00000 0.05 0.20 Q14 1 0.9014 0.2649 0.4459 11.00000 0.05 0.20 Q15 1 0.7348 0.0914 0.3280 11.00000 0.05 0.20 Q16 1 0.3791 0.0249 0.2076 11.00000 0.05 0.20 Q17 1 0.8930 0.2780 0.5085 11.00000 0.05 0.19 Q18 1 0.7986 0.3073 0.5906 11.00000 0.05 0.19 Q19 1 0.5002 0.1158 0.1835 11.00000 0.05 0.18 Q20 1 0.7406 0.2610 0.3336 11.00000 0.05 0.18 ; _shelx_res_checksum 36882 data_publication_text _journal_date_recd_electronic 2023-09-04 _journal_date_accepted 2023-10-02 _journal_name_full 'Acta Crystallographica, Section E' _journal_year 2023 _journal_volume 79 _journal_issue 1 _journal_page_first 0 _journal_page_last 0 _journal_paper_category GM _journal_paper_doi 10.1107/S2056989023008654 _journal_coeditor_code ZN2032 _publ_contact_author_name 'Leandro Bresolin' _publ_contact_author_address ;Escola de Qu\'imica e Alimentos Universidade Federal do Rio Grande Av. It\'alia km 08, Campus Carreiros 96203-900 Rio Grande-RS Brazil ; _publ_contact_author_email leandro_bresolin@yahoo.com.br _publ_contact_author_fax 0E9(5) _publ_contact_author_phone 0E9(5) _publ_section_title ;\ Synthesis, crystal structure and Hirshfeld analysis of trans-bis{(2E)-N-phenyl-2-[(2E)-3-phenyl-2-\ propen-1-ylidene]hydrazinecarbothioamidato-\k^2^N^1^,S}\ palladium(II) ; loop_ _publ_author_name _publ_author_address 'Melo, Ana Paula Lopes de' ;Escola de Qu\'imica e Alimentos Universidade Federal do Rio Grande Av. It\'alia km 08, Campus Carreiros 96203-900 Rio Grande-RS Brazil ; 'Martins, Bianca Barreto' ;Escola de Qu\'imica e Alimentos Universidade Federal do Rio Grande Av. It\'alia km 08, Campus Carreiros 96203-900 Rio Grande-RS Brazil ; 'Bresolin, Leandro' ;Escola de Qu\'imica e Alimentos Universidade Federal do Rio Grande Av. It\'alia km 08, Campus Carreiros 96203-900 Rio Grande-RS Brazil ; "Tirloni, B\'arbara" ;Departamento de Qu\'imica Universidade Federal de Santa Maria Av. Roraima s/n, Campus Universit\'ario, 97105-900 Santa Maria-RS Brazil ; 'Oliveira, Adriano Bof de' ;Departamento de Qu\'imica Universidade Federal de Sergipe Av. Marcelo Deda Chagas s/n, Campus Universit\'ario, 49107-230 S\~ao Crist\'ov\~ao-SE Brazil ; _publ_section_synopsis ; The synthesis, crystal structure and Hirshfeld surface analysis of a new Pd^II^ cinnamaldehyde 4-thiosemicarbazone homoleptic complex is reported. As a result of H...S intramolecular interactions, graph-set motif S(5), the coordination sphere resembles a hydrogen-bonded macrocyclic environment-type. In the crystal, the molecules are linked by H...S interactions, with graph-set motifs R~2~^2^(8), forming a one-dimensional hydrogen-bonded polymer along [001]. ;