# Electronic Supplementary Material (ESI) for Chemical Science. # This journal is © The Royal Society of Chemistry 2024 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_mini-21065 _database_code_depnum_ccdc_archive 'CCDC 2226338' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _vrf_PLAT910_mini-21065 ; PROBLEM: RESPONSE: Due to instrument limitations, additional reflections were not collected. However, the data to parameter ration remains high (~18). ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C33 H52 Fe N2 Si, C20 H40 K O8, C4 H8 O' _chemical_formula_sum 'C57 H100 Fe K N2 O9 Si' _chemical_formula_weight 1080.42 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 24.2280(7) _cell_length_b 19.8535(4) _cell_length_c 27.1355(9) _cell_angle_alpha 90 _cell_angle_beta 114.199(4) _cell_angle_gamma 90 _cell_volume 11905.5(7) _cell_formula_units_Z 8 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 61210 _cell_measurement_theta_min 2.7650 _cell_measurement_theta_max 26.6630 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.206 _exptl_crystal_F_000 4696 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 0.396 _shelx_estimated_absorpt_T_min 0.925 _shelx_estimated_absorpt_T_max 0.961 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.84720 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_measurement_device_type 'Rigaku Mercury275R CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 6.8 _diffrn_reflns_number 189898 _diffrn_reflns_av_unetI/netI 0.0355 _diffrn_reflns_av_R_equivalents 0.0713 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 30 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_theta_min 2.740 _diffrn_reflns_theta_max 26.372 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 24308 _reflns_number_gt 20016 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were first found in the difference map, then generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0846P)^2^+12.0001P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 24308 _refine_ls_number_parameters 1305 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0889 _refine_ls_R_factor_gt 0.0725 _refine_ls_wR_factor_ref 0.1809 _refine_ls_wR_factor_gt 0.1680 _refine_ls_goodness_of_fit_ref 1.107 _refine_ls_restrained_S_all 1.107 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.34576(2) 0.55335(2) 0.20981(2) 0.02525(10) Uani 1 1 d . . . . . Si14 Si 0.46033(4) 0.60624(5) 0.32246(4) 0.0353(2) Uani 1 1 d . . . . . N11 N 0.25951(11) 0.56126(12) 0.17422(10) 0.0268(5) Uani 1 1 d . . . . . N21 N 0.35871(10) 0.51188(11) 0.15190(9) 0.0258(5) Uani 1 1 d . . . . . C11 C 0.16033(14) 0.55559(17) 0.09714(13) 0.0355(7) Uani 1 1 d . . . . . H11A H 0.1425 0.5331 0.1193 0.053 Uiso 1 1 calc R U . . . H11B H 0.1434 0.5363 0.0607 0.053 Uiso 1 1 calc R U . . . H11C H 0.1511 0.6038 0.0951 0.053 Uiso 1 1 calc R U . . . C21 C 0.22728(13) 0.54575(14) 0.12202(11) 0.0276(6) Uani 1 1 d . . . . . C31 C 0.25384(13) 0.51842(14) 0.08988(11) 0.0278(6) Uani 1 1 d . . . . . H31 H 0.2271 0.5117 0.0531 0.033 Uiso 1 1 calc R U . . . C41 C 0.31346(13) 0.49938(14) 0.10324(11) 0.0278(6) Uani 1 1 d . . . . . C51 C 0.32665(15) 0.46169(17) 0.06180(12) 0.0378(7) Uani 1 1 d . . . . . H51A H 0.3607 0.4829 0.0572 0.057 Uiso 1 1 calc R U . . . H51B H 0.2909 0.4624 0.0274 0.057 Uiso 1 1 calc R U . . . H51C H 0.3370 0.4150 0.0736 0.057 Uiso 1 1 calc R U . . . C12 C 0.22932(12) 0.57807(15) 0.20736(11) 0.0272(6) Uani 1 1 d . . . . . C22 C 0.22386(13) 0.52955(15) 0.24230(12) 0.0304(6) Uani 1 1 d . . . . . C32 C 0.19675(13) 0.54756(16) 0.27618(12) 0.0332(7) Uani 1 1 d . . . . . H32 H 0.1924 0.5147 0.2998 0.040 Uiso 1 1 calc R U . . . C42 C 0.17605(14) 0.61124(17) 0.27667(12) 0.0356(7) Uani 1 1 d . . . . . H42 H 0.1567 0.6223 0.2998 0.043 Uiso 1 1 calc R U . . . C52 C 0.18324(14) 0.65882(16) 0.24373(12) 0.0345(7) Uani 1 1 d . . . . . H52 H 0.1698 0.7035 0.2450 0.041 Uiso 1 1 calc R U . . . C62 C 0.20951(13) 0.64391(15) 0.20865(12) 0.0315(6) Uani 1 1 d . . . . . C72 C 0.24918(14) 0.46020(15) 0.24412(12) 0.0324(6) Uani 1 1 d . . . . . H72 H 0.2882 0.4657 0.2401 0.039 Uiso 1 1 calc R U . . . C92 C 0.26402(17) 0.42438(17) 0.29691(13) 0.0413(8) Uani 1 1 d . . . . . H92A H 0.2893 0.4535 0.3268 0.062 Uiso 1 1 calc R U . . . H92B H 0.2859 0.3827 0.2976 0.062 Uiso 1 1 calc R U . . . H92C H 0.2265 0.4136 0.3007 0.062 Uiso 1 1 calc R U . . . C82 C 0.20889(16) 0.41646(16) 0.19757(13) 0.0390(7) Uani 1 1 d . . . . . H82A H 0.1695 0.4108 0.1993 0.059 Uiso 1 1 calc R U . . . H82B H 0.2278 0.3723 0.2000 0.059 Uiso 1 1 calc R U . . . H82C H 0.2032 0.4380 0.1633 0.059 Uiso 1 1 calc R U . . . C102 C 0.22072(15) 0.69863(15) 0.17593(13) 0.0360(7) Uani 1 1 d . . . . . H102 H 0.2318 0.6769 0.1479 0.043 Uiso 1 1 calc R U . . . C112 C 0.27395(16) 0.74077(17) 0.21203(15) 0.0437(8) Uani 1 1 d . . . . . H11D H 0.2643 0.7624 0.2400 0.065 Uiso 1 1 calc R U . . . H11E H 0.2825 0.7754 0.1904 0.065 Uiso 1 1 calc R U . . . H11F H 0.3095 0.7118 0.2291 0.065 Uiso 1 1 calc R U . . . C122 C 0.16535(16) 0.74241(18) 0.14696(14) 0.0446(8) Uani 1 1 d . . . . . H12A H 0.1314 0.7141 0.1241 0.067 Uiso 1 1 calc R U . . . H12B H 0.1742 0.7755 0.1244 0.067 Uiso 1 1 calc R U . . . H12C H 0.1547 0.7659 0.1736 0.067 Uiso 1 1 calc R U . . . C13 C 0.41409(13) 0.47753(15) 0.16529(11) 0.0300(6) Uani 1 1 d . . . . . C23 C 0.41865(15) 0.41075(15) 0.18369(12) 0.0339(7) Uani 1 1 d . . . . . C33 C 0.47297(16) 0.37806(18) 0.19841(14) 0.0439(8) Uani 1 1 d . . . . . H33 H 0.4767 0.3328 0.2108 0.053 Uiso 1 1 calc R U . . . C43 C 0.52148(17) 0.4092(2) 0.19556(14) 0.0508(10) Uani 1 1 d . . . . . H43 H 0.5585 0.3854 0.2055 0.061 Uiso 1 1 calc R U . . . C53 C 0.51735(15) 0.47473(19) 0.17837(14) 0.0441(8) Uani 1 1 d . . . . . H53 H 0.5518 0.4962 0.1771 0.053 Uiso 1 1 calc R U . . . C63 C 0.46373(14) 0.50972(17) 0.16286(12) 0.0356(7) Uani 1 1 d . . . . . C73 C 0.36743(16) 0.37601(16) 0.19069(13) 0.0391(7) Uani 1 1 d . . . . . H73 H 0.3320 0.4074 0.1776 0.047 Uiso 1 1 calc R U . . . C93 C 0.38351(18) 0.36220(18) 0.24953(14) 0.0467(8) Uani 1 1 d . . . . . H93A H 0.4169 0.3298 0.2631 0.070 Uiso 1 1 calc R U . . . H93B H 0.3482 0.3435 0.2537 0.070 Uiso 1 1 calc R U . . . H93C H 0.3958 0.4043 0.2700 0.070 Uiso 1 1 calc R U . . . C83 C 0.3480(2) 0.3118(2) 0.15836(16) 0.0598(11) Uani 1 1 d . . . . . H83A H 0.3354 0.3219 0.1199 0.090 Uiso 1 1 calc R U . . . H83B H 0.3140 0.2919 0.1640 0.090 Uiso 1 1 calc R U . . . H83C H 0.3819 0.2800 0.1702 0.090 Uiso 1 1 calc R U . . . C103 C 0.45912(15) 0.58099(19) 0.14304(16) 0.0466(9) Uani 1 1 d . . . . . H103 H 0.4200 0.5993 0.1415 0.056 Uiso 1 1 calc R U . . . C123 C 0.5077(2) 0.6260(2) 0.17942(18) 0.0669(12) Uani 1 1 d . . . . . H12D H 0.5089 0.6240 0.2159 0.100 Uiso 1 1 calc R U . . . H12E H 0.4996 0.6723 0.1659 0.100 Uiso 1 1 calc R U . . . H12F H 0.5468 0.6113 0.1804 0.100 Uiso 1 1 calc R U . . . C113 C 0.4563(3) 0.5850(3) 0.08740(19) 0.106(2) Uani 1 1 d . . . . . H11G H 0.4954 0.5717 0.0878 0.159 Uiso 1 1 calc R U . . . H11H H 0.4470 0.6313 0.0741 0.159 Uiso 1 1 calc R U . . . H11I H 0.4247 0.5547 0.0636 0.159 Uiso 1 1 calc R U . . . C14 C 0.38496(14) 0.57154(16) 0.28984(12) 0.0336(7) Uani 1 1 d . . . . . H14A H 0.3577 0.6023 0.2980 0.040 Uiso 1 1 calc R U . . . H14B H 0.3851 0.5284 0.3081 0.040 Uiso 1 1 calc R U . . . C34 C 0.51705(15) 0.5496(2) 0.31470(14) 0.0459(8) Uani 1 1 d . . . . . H34A H 0.5221 0.5094 0.3371 0.069 Uiso 1 1 calc R U . . . H34B H 0.5559 0.5732 0.3262 0.069 Uiso 1 1 calc R U . . . H34C H 0.5032 0.5363 0.2767 0.069 Uiso 1 1 calc R U . . . C24 C 0.4645(2) 0.6910(2) 0.29532(18) 0.0603(11) Uani 1 1 d . . . . . H24A H 0.4535 0.6877 0.2564 0.090 Uiso 1 1 calc R U . . . H24B H 0.5058 0.7085 0.3134 0.090 Uiso 1 1 calc R U . . . H24C H 0.4363 0.7214 0.3018 0.090 Uiso 1 1 calc R U . . . C44 C 0.48518(17) 0.6182(2) 0.39678(14) 0.0569(10) Uani 1 1 d . . . . . H44A H 0.4580 0.6501 0.4033 0.085 Uiso 1 1 calc R U . . . H44B H 0.5266 0.6359 0.4124 0.085 Uiso 1 1 calc R U . . . H44C H 0.4840 0.5748 0.4136 0.085 Uiso 1 1 calc R U . . . Fe2 Fe 0.85742(2) 0.54202(2) 0.22308(2) 0.02592(11) Uani 1 1 d . . . . . Si Si 0.96219(4) 0.60072(5) 0.34128(4) 0.0377(2) Uani 1 1 d . . . . . N15 N 0.77205(10) 0.54684(12) 0.17918(9) 0.0261(5) Uani 1 1 d . . . . . N25 N 0.88110(10) 0.50367(12) 0.17022(9) 0.0261(5) Uani 1 1 d . . . . . C55 C 0.86401(16) 0.45891(19) 0.08056(13) 0.0443(8) Uani 1 1 d . . . . . H55A H 0.8926 0.4896 0.0750 0.066 Uiso 1 1 calc R U . . . H55B H 0.8297 0.4505 0.0459 0.066 Uiso 1 1 calc R U . . . H55C H 0.8844 0.4162 0.0954 0.066 Uiso 1 1 calc R U . . . C45 C 0.84162(13) 0.48997(14) 0.11921(11) 0.0275(6) Uani 1 1 d . . . . . C35 C 0.78063(13) 0.50387(14) 0.10023(11) 0.0278(6) Uani 1 1 d . . . . . H35 H 0.7582 0.4952 0.0628 0.033 Uiso 1 1 calc R U . . . C25 C 0.74676(13) 0.52853(14) 0.12690(11) 0.0282(6) Uani 1 1 d . . . . . C15 C 0.67940(14) 0.53343(18) 0.09582(13) 0.0402(8) Uani 1 1 d . . . . . H15A H 0.6593 0.5038 0.1122 0.060 Uiso 1 1 calc R U . . . H15B H 0.6685 0.5197 0.0583 0.060 Uiso 1 1 calc R U . . . H15C H 0.6664 0.5800 0.0966 0.060 Uiso 1 1 calc R U . . . C16 C 0.73390(13) 0.56143(15) 0.20557(11) 0.0282(6) Uani 1 1 d . . . . . C26 C 0.71721(15) 0.51040(16) 0.23174(13) 0.0363(7) Uani 1 1 d . . . . . C36 C 0.68211(15) 0.52546(17) 0.25924(14) 0.0406(8) Uani 1 1 d . . . . . H36 H 0.6709 0.4905 0.2772 0.049 Uiso 1 1 calc R U . . . C46 C 0.66325(15) 0.58936(18) 0.26122(13) 0.0392(7) Uani 1 1 d . . . . . H46 H 0.6389 0.5989 0.2803 0.047 Uiso 1 1 calc R U . . . C56 C 0.67944(14) 0.63980(17) 0.23562(13) 0.0376(7) Uani 1 1 d . . . . . H56 H 0.6664 0.6846 0.2373 0.045 Uiso 1 1 calc R U . . . C66 C 0.71429(13) 0.62684(15) 0.20749(12) 0.0313(6) Uani 1 1 d . . . . . C76 C 0.73575(19) 0.43867(18) 0.22979(17) 0.0514(10) Uani 1 1 d . . . . . H76 H 0.7587 0.4364 0.2065 0.062 Uiso 1 1 calc R U . . . C96 C 0.77603(17) 0.41334(19) 0.28537(19) 0.0616(12) Uani 1 1 d . . . . . H96A H 0.8115 0.4427 0.3013 0.092 Uiso 1 1 calc R U . . . H96B H 0.7892 0.3673 0.2827 0.092 Uiso 1 1 calc R U . . . H96C H 0.7536 0.4135 0.3083 0.092 Uiso 1 1 calc R U . . . C86 C 0.6800(2) 0.3930(2) 0.20520(17) 0.0623(11) Uani 1 1 d . . . . . H86A H 0.6580 0.3932 0.2285 0.093 Uiso 1 1 calc R U . . . H86B H 0.6929 0.3470 0.2022 0.093 Uiso 1 1 calc R U . . . H86C H 0.6535 0.4097 0.1693 0.093 Uiso 1 1 calc R U . . . C106 C 0.73229(15) 0.68339(15) 0.18091(13) 0.0352(7) Uani 1 1 d . . . . . H106 H 0.7516 0.6634 0.1580 0.042 Uiso 1 1 calc R U . . . C126 C 0.77885(17) 0.72794(17) 0.22292(15) 0.0440(8) Uani 1 1 d . . . . . H12G H 0.7613 0.7475 0.2464 0.066 Uiso 1 1 calc R U . . . H12H H 0.7909 0.7641 0.2048 0.066 Uiso 1 1 calc R U . . . H12I H 0.8144 0.7010 0.2447 0.066 Uiso 1 1 calc R U . . . C116 C 0.67850(18) 0.7249(2) 0.14449(15) 0.0533(10) Uani 1 1 d . . . . . H11J H 0.6498 0.6959 0.1164 0.080 Uiso 1 1 calc R U . . . H11K H 0.6924 0.7608 0.1275 0.080 Uiso 1 1 calc R U . . . H11L H 0.6585 0.7447 0.1660 0.080 Uiso 1 1 calc R U . . . C17 C 0.94004(13) 0.47648(15) 0.18756(11) 0.0292(6) Uani 1 1 d . . . . . C27 C 0.95115(14) 0.41226(15) 0.21069(12) 0.0317(6) Uani 1 1 d . . . . . C37 C 1.00827(15) 0.38505(17) 0.22684(13) 0.0376(7) Uani 1 1 d . . . . . H37 H 1.0158 0.3408 0.2415 0.045 Uiso 1 1 calc R U . . . C47 C 1.05418(15) 0.42059(18) 0.22211(13) 0.0395(8) Uani 1 1 d . . . . . H47 H 1.0932 0.4011 0.2332 0.047 Uiso 1 1 calc R U . . . C57 C 1.04352(14) 0.48440(18) 0.20136(13) 0.0374(7) Uani 1 1 d . . . . . H57 H 1.0758 0.5094 0.1990 0.045 Uiso 1 1 calc R U . . . C67 C 0.98687(14) 0.51328(16) 0.18370(12) 0.0325(6) Uani 1 1 d . . . . . C77 C 0.90270(15) 0.37300(16) 0.21969(14) 0.0376(7) Uani 1 1 d . . . . . H77 H 0.8698 0.4056 0.2160 0.045 Uiso 1 1 calc R U . . . C97 C 0.9252(2) 0.3443(3) 0.27552(17) 0.0719(14) Uani 1 1 d . . . . . H97A H 0.9556 0.3096 0.2799 0.108 Uiso 1 1 calc R U . . . H97B H 0.8913 0.3242 0.2812 0.108 Uiso 1 1 calc R U . . . H97C H 0.9433 0.3802 0.3020 0.108 Uiso 1 1 calc R U . . . C87 C 0.8751(2) 0.3197(3) 0.1790(2) 0.0813(15) Uani 1 1 d . . . . . H87A H 0.8596 0.3394 0.1427 0.122 Uiso 1 1 calc R U . . . H87B H 0.8418 0.2986 0.1849 0.122 Uiso 1 1 calc R U . . . H87C H 0.9057 0.2856 0.1823 0.122 Uiso 1 1 calc R U . . . C107 C 0.97731(14) 0.58351(16) 0.16124(13) 0.0370(7) Uani 1 1 d . . . . . H107 H 0.9333 0.5942 0.1483 0.044 Uiso 1 1 calc R U . . . C117 C 1.01142(19) 0.6339(2) 0.20332(17) 0.0589(11) Uani 1 1 d . . . . . H11M H 0.9979 0.6319 0.2328 0.088 Uiso 1 1 calc R U . . . H11N H 1.0040 0.6791 0.1874 0.088 Uiso 1 1 calc R U . . . H11O H 1.0548 0.6238 0.2175 0.088 Uiso 1 1 calc R U . . . C127 C 0.9946(3) 0.5913(2) 0.1135(2) 0.0800(15) Uani 1 1 d . . . . . H12J H 1.0385 0.5868 0.1261 0.120 Uiso 1 1 calc R U . . . H12K H 0.9819 0.6357 0.0971 0.120 Uiso 1 1 calc R U . . . H12L H 0.9744 0.5563 0.0867 0.120 Uiso 1 1 calc R U . . . C68 C 0.89194(15) 0.55663(18) 0.30363(12) 0.0398(8) Uani 1 1 d . . . . . H68A H 0.8603 0.5803 0.3112 0.048 Uiso 1 1 calc R U . . . H68B H 0.8963 0.5114 0.3202 0.048 Uiso 1 1 calc R U . . . C69 C 0.97953(18) 0.6060(2) 0.41516(14) 0.0570(11) Uani 1 1 d . . . . . H69A H 0.9460 0.6283 0.4200 0.086 Uiso 1 1 calc R U . . . H69B H 1.0168 0.6320 0.4337 0.086 Uiso 1 1 calc R U . . . H69C H 0.9849 0.5605 0.4304 0.086 Uiso 1 1 calc R U . . . C64 C 0.95937(17) 0.68901(19) 0.31822(17) 0.0541(10) Uani 1 1 d . . . . . H64A H 0.9483 0.6897 0.2792 0.081 Uiso 1 1 calc R U . . . H64B H 0.9992 0.7100 0.3371 0.081 Uiso 1 1 calc R U . . . H64C H 0.9291 0.7141 0.3262 0.081 Uiso 1 1 calc R U . . . C71 C 1.02768(15) 0.5564(2) 0.33674(14) 0.0460(8) Uani 1 1 d . . . . . H71A H 1.0354 0.5143 0.3573 0.069 Uiso 1 1 calc R U . . . H71B H 1.0636 0.5852 0.3517 0.069 Uiso 1 1 calc R U . . . H71C H 1.0185 0.5464 0.2988 0.069 Uiso 1 1 calc R U . . . K10 K 0.65108(3) 0.31823(3) 0.47335(3) 0.02948(14) Uani 1 1 d . . . . . O10 O 0.65914(10) 0.18600(10) 0.44845(9) 0.0348(5) Uani 1 1 d . . . . . O20 O 0.68502(10) 0.22099(10) 0.55480(9) 0.0345(5) Uani 1 1 d . . . . . O30 O 0.65838(10) 0.35169(10) 0.57493(8) 0.0344(5) Uani 1 1 d . . . . . O40 O 0.66614(9) 0.45094(10) 0.50651(8) 0.0328(5) Uani 1 1 d . . . . . O50 O 0.63134(9) 0.41691(10) 0.39708(8) 0.0325(5) Uani 1 1 d . . . . . O60 O 0.65192(9) 0.28591(11) 0.37221(8) 0.0347(5) Uani 1 1 d . . . . . O70 O 0.53122(11) 0.33435(14) 0.43573(10) 0.0488(6) Uani 1 1 d . . . . . O80 O 0.77045(10) 0.33583(12) 0.50102(10) 0.0419(5) Uani 1 1 d . . . . . C10 C 0.69321(16) 0.14413(16) 0.49213(14) 0.0395(7) Uani 1 1 d . . . . . H10A H 0.7367 0.1554 0.5053 0.047 Uiso 1 1 calc R U . . . H10B H 0.6877 0.0964 0.4805 0.047 Uiso 1 1 calc R U . . . C20 C 0.67241(17) 0.15437(16) 0.53578(15) 0.0427(8) Uani 1 1 d . . . . . H20A H 0.6284 0.1458 0.5219 0.051 Uiso 1 1 calc R U . . . H20B H 0.6934 0.1225 0.5657 0.051 Uiso 1 1 calc R U . . . C30 C 0.66226(16) 0.23587(17) 0.59379(13) 0.0395(7) Uani 1 1 d . . . . . H30A H 0.6764 0.2017 0.6229 0.047 Uiso 1 1 calc R U . . . H30B H 0.6175 0.2351 0.5769 0.047 Uiso 1 1 calc R U . . . C40 C 0.68384(16) 0.30339(17) 0.61652(13) 0.0389(7) Uani 1 1 d . . . . . H40A H 0.6714 0.3130 0.6463 0.047 Uiso 1 1 calc R U . . . H40B H 0.7286 0.3052 0.6311 0.047 Uiso 1 1 calc R U . . . C50 C 0.67863(16) 0.41728(16) 0.59364(14) 0.0406(8) Uani 1 1 d . . . . . H50A H 0.7231 0.4201 0.6059 0.049 Uiso 1 1 calc R U . . . H50B H 0.6685 0.4286 0.6245 0.049 Uiso 1 1 calc R U . . . C60 C 0.64832(16) 0.46522(16) 0.54847(14) 0.0397(7) Uani 1 1 d . . . . . H60A H 0.6038 0.4609 0.5352 0.048 Uiso 1 1 calc R U . . . H60B H 0.6597 0.5120 0.5612 0.048 Uiso 1 1 calc R U . . . C70 C 0.64246(16) 0.49771(16) 0.46385(14) 0.0416(8) Uani 1 1 d . . . . . H70A H 0.6582 0.5433 0.4770 0.050 Uiso 1 1 calc R U . . . H70B H 0.5978 0.4990 0.4501 0.050 Uiso 1 1 calc R U . . . C80 C 0.66034(15) 0.47755(16) 0.41994(14) 0.0399(8) Uani 1 1 d . . . . . H80A H 0.6487 0.5131 0.3919 0.048 Uiso 1 1 calc R U . . . H80B H 0.7048 0.4716 0.4345 0.048 Uiso 1 1 calc R U . . . C90 C 0.63850(16) 0.40028(18) 0.34976(13) 0.0407(8) Uani 1 1 d . . . . . H90A H 0.6819 0.4023 0.3566 0.049 Uiso 1 1 calc R U . . . H90B H 0.6162 0.4329 0.3208 0.049 Uiso 1 1 calc R U . . . C100 C 0.61501(15) 0.33177(17) 0.33271(13) 0.0397(7) Uani 1 1 d . . . . . H10C H 0.5727 0.3285 0.3290 0.048 Uiso 1 1 calc R U . . . H10D H 0.6157 0.3212 0.2973 0.048 Uiso 1 1 calc R U . . . C110 C 0.63356(15) 0.21859(17) 0.35882(13) 0.0401(7) Uani 1 1 d . . . . . H11P H 0.6370 0.2061 0.3249 0.048 Uiso 1 1 calc R U . . . H11Q H 0.5908 0.2133 0.3533 0.048 Uiso 1 1 calc R U . . . C120 C 0.67239(15) 0.17417(16) 0.40308(13) 0.0366(7) Uani 1 1 d . . . . . H12M H 0.6645 0.1264 0.3918 0.044 Uiso 1 1 calc R U . . . H12N H 0.7156 0.1839 0.4122 0.044 Uiso 1 1 calc R U . . . C160 C 0.50572(19) 0.3389(2) 0.47308(17) 0.0564(10) Uani 1 1 d . . . . . H16A H 0.5375 0.3420 0.5103 0.068 Uiso 1 1 calc R U . . . H16B H 0.4800 0.2992 0.4706 0.068 Uiso 1 1 calc R U . . . C150 C 0.46864(19) 0.4018(2) 0.45819(16) 0.0580(10) Uani 1 1 d . . . . . H15D H 0.4356 0.4002 0.4707 0.070 Uiso 1 1 calc R U . . . H15E H 0.4939 0.4421 0.4736 0.070 Uiso 1 1 calc R U . . . C140 C 0.44452(18) 0.4017(2) 0.39879(16) 0.0603(11) Uani 1 1 d . . . . . H14C H 0.4431 0.4480 0.3848 0.072 Uiso 1 1 calc R U . . . H14D H 0.4033 0.3823 0.3829 0.072 Uiso 1 1 calc R U . . . C130 C 0.48753(18) 0.3592(2) 0.38599(15) 0.0594(11) Uani 1 1 d . . . . . H13A H 0.4658 0.3213 0.3622 0.071 Uiso 1 1 calc R U . . . H13B H 0.5074 0.3862 0.3673 0.071 Uiso 1 1 calc R U . . . C170 C 0.80876(17) 0.31643(19) 0.55457(15) 0.0475(9) Uani 1 1 d . . . . . H17A H 0.7888 0.2821 0.5681 0.057 Uiso 1 1 calc R U . . . H17B H 0.8190 0.3558 0.5791 0.057 Uiso 1 1 calc R U . . . C180 C 0.86427(18) 0.2882(3) 0.55145(17) 0.0721(14) Uani 1 1 d . . . . . H18A H 0.8968 0.3224 0.5619 0.087 Uiso 1 1 calc R U . . . H18B H 0.8792 0.2485 0.5754 0.087 Uiso 1 1 calc R U . . . C190 C 0.8451(2) 0.2694(4) 0.4958(2) 0.105(2) Uani 1 1 d . . . . . H19A H 0.8316 0.2219 0.4904 0.126 Uiso 1 1 calc R U . . . H19B H 0.8788 0.2747 0.4844 0.126 Uiso 1 1 calc R U . . . C200 C 0.79573(16) 0.31370(18) 0.46508(14) 0.0432(8) Uani 1 1 d . . . . . H20C H 0.8106 0.3525 0.4511 0.052 Uiso 1 1 calc R U . . . H20D H 0.7651 0.2894 0.4341 0.052 Uiso 1 1 calc R U . . . K20 K 0.82121(3) 0.67206(3) 0.50749(3) 0.03318(15) Uani 1 1 d . . . . . O90 O 0.81509(11) 0.63706(12) 0.40789(9) 0.0447(6) Uani 1 1 d . . . . . O100 O 0.81210(10) 0.53784(10) 0.47833(9) 0.0348(5) Uani 1 1 d . . . . . O110 O 0.85091(9) 0.57469(10) 0.58566(8) 0.0321(5) Uani 1 1 d . . . . . O120 O 0.83439(9) 0.70805(10) 0.61139(8) 0.0339(5) Uani 1 1 d . . . . . O130 O 0.82344(10) 0.80641(11) 0.53378(9) 0.0378(5) Uani 1 1 d . . . . . O140 O 0.78954(12) 0.76939(12) 0.42716(10) 0.0475(6) Uani 1 1 d . . . . . O150 O 0.70283(11) 0.66448(13) 0.48446(10) 0.0483(6) Uani 1 1 d . . . . . O160 O 0.94074(13) 0.66542(15) 0.54900(14) 0.0725(9) Uani 1 1 d . . . . . C210 C 0.79534(18) 0.57099(18) 0.39085(14) 0.0461(8) Uani 1 1 d . . . . . H21A H 0.8034 0.5595 0.3589 0.055 Uiso 1 1 calc R U . . . H21B H 0.7512 0.5675 0.3805 0.055 Uiso 1 1 calc R U . . . C220 C 0.82767(18) 0.52412(19) 0.43509(15) 0.0475(9) Uani 1 1 d . . . . . H22A H 0.8166 0.4772 0.4227 0.057 Uiso 1 1 calc R U . . . H22B H 0.8719 0.5293 0.4467 0.057 Uiso 1 1 calc R U . . . C230 C 0.83724(17) 0.49125(16) 0.52123(14) 0.0429(8) Uani 1 1 d . . . . . H23A H 0.8817 0.4893 0.5333 0.051 Uiso 1 1 calc R U . . . H23B H 0.8206 0.4457 0.5089 0.051 Uiso 1 1 calc R U . . . C240 C 0.82235(16) 0.51282(16) 0.56631(13) 0.0392(7) Uani 1 1 d . . . . . H24D H 0.7780 0.5177 0.5537 0.047 Uiso 1 1 calc R U . . . H24E H 0.8366 0.4788 0.5955 0.047 Uiso 1 1 calc R U . . . C250 C 0.84744(15) 0.59366(16) 0.63429(12) 0.0359(7) Uani 1 1 d . . . . . H25A H 0.8705 0.5614 0.6633 0.043 Uiso 1 1 calc R U . . . H25B H 0.8047 0.5931 0.6297 0.043 Uiso 1 1 calc R U . . . C260 C 0.87271(15) 0.66188(16) 0.64926(13) 0.0378(7) Uani 1 1 d . . . . . H26A H 0.8760 0.6733 0.6859 0.045 Uiso 1 1 calc R U . . . H26B H 0.9137 0.6638 0.6496 0.045 Uiso 1 1 calc R U . . . C270 C 0.85469(15) 0.77481(16) 0.62412(13) 0.0386(7) Uani 1 1 d . . . . . H27A H 0.8968 0.7788 0.6273 0.046 Uiso 1 1 calc R U . . . H27B H 0.8541 0.7878 0.6591 0.046 Uiso 1 1 calc R U . . . C280 C 0.81460(15) 0.81970(16) 0.58096(14) 0.0399(7) Uani 1 1 d . . . . . H28A H 0.7718 0.8114 0.5744 0.048 Uiso 1 1 calc R U . . . H28B H 0.8243 0.8674 0.5918 0.048 Uiso 1 1 calc R U . . . C290 C 0.78979(18) 0.84965(17) 0.49073(15) 0.0477(9) Uani 1 1 d . . . . . H29A H 0.7987 0.8972 0.5023 0.057 Uiso 1 1 calc R U . . . H29B H 0.7460 0.8418 0.4796 0.057 Uiso 1 1 calc R U . . . C300 C 0.8060(2) 0.83642(17) 0.44512(16) 0.0519(9) Uani 1 1 d . . . . . H30C H 0.7845 0.8683 0.4154 0.062 Uiso 1 1 calc R U . . . H30D H 0.8501 0.8427 0.4565 0.062 Uiso 1 1 calc R U . . . C310 C 0.8064(2) 0.7525(2) 0.38541(17) 0.0667(12) Uani 1 1 d . . . . . H31A H 0.8509 0.7549 0.3985 0.080 Uiso 1 1 calc R U . . . H31B H 0.7883 0.7850 0.3553 0.080 Uiso 1 1 calc R U . . . C320 C 0.7854(2) 0.6839(2) 0.36610(15) 0.0595(11) Uani 1 1 d . . . . . H32A H 0.7411 0.6809 0.3548 0.071 Uiso 1 1 calc R U . . . H32B H 0.7943 0.6734 0.3344 0.071 Uiso 1 1 calc R U . . . C330 C 0.68209(17) 0.68082(19) 0.52437(15) 0.0471(8) Uani 1 1 d . . . . . H33A H 0.7166 0.6920 0.5588 0.057 Uiso 1 1 calc R U . . . H33B H 0.6598 0.6424 0.5307 0.057 Uiso 1 1 calc R U . . . C340 C 0.64113(19) 0.7405(2) 0.50383(18) 0.0613(11) Uani 1 1 d . . . . . H34D H 0.6031 0.7336 0.5085 0.074 Uiso 1 1 calc R U . . . H34E H 0.6611 0.7818 0.5234 0.074 Uiso 1 1 calc R U . . . C350 C 0.6287(2) 0.7458(2) 0.44585(18) 0.0606(11) Uani 1 1 d . . . . . H35A H 0.5845 0.7455 0.4234 0.073 Uiso 1 1 calc R U . . . H35B H 0.6460 0.7879 0.4386 0.073 Uiso 1 1 calc R U . . . C360 C 0.65782(18) 0.6864(2) 0.43422(16) 0.0550(10) Uani 1 1 d . . . . . H36A H 0.6277 0.6503 0.4176 0.066 Uiso 1 1 calc R U . . . H36B H 0.6764 0.6984 0.4090 0.066 Uiso 1 1 calc R U . . . C370 C 0.98210(19) 0.6133(3) 0.56462(19) 0.0679(12) Uani 1 1 d . . . . . H37A H 0.9716 0.5784 0.5361 0.081 Uiso 1 1 calc R U . . . H37B H 0.9846 0.5922 0.5985 0.081 Uiso 1 1 calc R U . . . C380 C 1.04270(19) 0.6499(3) 0.57301(19) 0.0850(18) Uani 1 1 d . . . . . H38A H 1.0754 0.6389 0.6086 0.102 Uiso 1 1 calc R U . . . H38B H 1.0560 0.6382 0.5441 0.102 Uiso 1 1 calc R U . . . C390 C 1.0245(2) 0.7227(3) 0.5699(2) 0.0928(17) Uani 1 1 d . . . . . H39A H 1.0299 0.7398 0.6059 0.111 Uiso 1 1 calc R U . . . H39B H 1.0487 0.7508 0.5560 0.111 Uiso 1 1 calc R U . . . C400 C 0.9621(2) 0.7232(3) 0.5334(3) 0.0862(16) Uani 1 1 d . . . . . H40C H 0.9414 0.7641 0.5381 0.103 Uiso 1 1 calc R U . . . H40D H 0.9570 0.7202 0.4954 0.103 Uiso 1 1 calc R U . . . O170 O 0.50603(12) 0.19982(12) 0.54999(10) 0.0494(6) Uani 1 1 d . . . . . C410 C 0.4897(3) 0.1592(2) 0.50430(18) 0.0897(19) Uani 1 1 d . . . . . H41A H 0.5135 0.1715 0.4835 0.108 Uiso 1 1 calc R U . . . H41B H 0.4462 0.1651 0.4807 0.108 Uiso 1 1 calc R U . . . C420 C 0.5021(2) 0.0880(2) 0.52300(18) 0.0720(13) Uani 1 1 d . . . . . H42A H 0.4641 0.0636 0.5164 0.086 Uiso 1 1 calc R U . . . H42B H 0.5239 0.0640 0.5044 0.086 Uiso 1 1 calc R U . . . C430 C 0.5402(2) 0.0939(2) 0.58163(17) 0.0593(11) Uani 1 1 d . . . . . H43A H 0.5323 0.0564 0.6019 0.071 Uiso 1 1 calc R U . . . H43B H 0.5838 0.0942 0.5890 0.071 Uiso 1 1 calc R U . . . C440 C 0.52145(18) 0.15883(18) 0.59591(15) 0.0489(9) Uani 1 1 d . . . . . H44D H 0.4862 0.1527 0.6051 0.059 Uiso 1 1 calc R U . . . H44E H 0.5550 0.1792 0.6273 0.059 Uiso 1 1 calc R U . . . O180 O 0.95016(15) 0.84354(16) 0.43597(16) 0.0817(10) Uani 1 1 d . . . . . C480 C 0.96090(19) 0.9104(2) 0.4520(2) 0.0636(11) Uani 1 1 d . . . . . H48A H 0.9393 0.9228 0.4747 0.076 Uiso 1 1 calc R U . . . H48B H 0.9473 0.9406 0.4201 0.076 Uiso 1 1 calc R U . . . C470 C 1.0274(2) 0.9156(3) 0.4834(2) 0.0832(16) Uani 1 1 d . . . . . H47A H 1.0421 0.9616 0.4814 0.100 Uiso 1 1 calc R U . . . H47B H 1.0392 0.9033 0.5217 0.100 Uiso 1 1 calc R U . . . C460 C 1.0496(2) 0.8687(3) 0.4570(3) 0.104(2) Uani 1 1 d . . . . . H46A H 1.0862 0.8461 0.4834 0.125 Uiso 1 1 calc R U . . . H46B H 1.0601 0.8914 0.4296 0.125 Uiso 1 1 calc R U . . . C450 C 1.0015(3) 0.8199(2) 0.4315(2) 0.0748(14) Uani 1 1 d . . . . . H45A H 0.9938 0.8144 0.3930 0.090 Uiso 1 1 calc R U . . . H45B H 1.0132 0.7756 0.4496 0.090 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0262(2) 0.0266(2) 0.0232(2) -0.00279(15) 0.01038(17) -0.00061(15) Si14 0.0310(4) 0.0422(5) 0.0291(4) -0.0051(4) 0.0087(4) -0.0054(4) N11 0.0298(12) 0.0257(12) 0.0271(13) -0.0018(9) 0.0138(10) -0.0015(9) N21 0.0264(12) 0.0262(12) 0.0251(12) -0.0002(9) 0.0108(10) 0.0020(9) C11 0.0303(16) 0.0430(18) 0.0295(16) -0.0028(13) 0.0084(13) 0.0001(13) C21 0.0271(14) 0.0287(14) 0.0241(14) 0.0015(11) 0.0077(12) -0.0012(11) C31 0.0293(14) 0.0293(14) 0.0200(14) 0.0003(11) 0.0051(12) 0.0007(11) C41 0.0349(15) 0.0268(14) 0.0223(14) -0.0019(11) 0.0124(12) -0.0009(12) C51 0.0418(18) 0.0445(18) 0.0263(16) -0.0062(13) 0.0131(14) 0.0041(14) C12 0.0222(13) 0.0324(15) 0.0258(14) -0.0042(11) 0.0085(12) -0.0036(11) C22 0.0266(14) 0.0339(15) 0.0286(15) -0.0047(12) 0.0093(12) -0.0068(12) C32 0.0287(15) 0.0446(18) 0.0278(16) -0.0024(13) 0.0132(13) -0.0060(13) C42 0.0285(15) 0.0494(19) 0.0301(16) -0.0054(14) 0.0133(13) 0.0004(13) C52 0.0324(16) 0.0388(17) 0.0332(17) -0.0056(13) 0.0143(14) 0.0038(13) C62 0.0271(15) 0.0351(16) 0.0311(16) -0.0022(12) 0.0108(13) -0.0005(12) C72 0.0360(16) 0.0301(15) 0.0325(16) -0.0023(12) 0.0154(14) -0.0062(12) C92 0.055(2) 0.0355(17) 0.0358(18) 0.0015(14) 0.0211(16) -0.0006(15) C82 0.0464(19) 0.0343(17) 0.0366(18) -0.0065(13) 0.0171(15) -0.0085(14) C102 0.0446(18) 0.0307(16) 0.0386(18) -0.0010(13) 0.0231(15) 0.0065(13) C112 0.048(2) 0.0332(17) 0.055(2) -0.0006(15) 0.0263(18) 0.0002(14) C122 0.052(2) 0.0417(19) 0.0410(19) 0.0044(15) 0.0204(17) 0.0148(16) C13 0.0319(15) 0.0350(16) 0.0224(14) -0.0024(12) 0.0107(12) 0.0067(12) C23 0.0432(18) 0.0350(16) 0.0221(15) 0.0010(12) 0.0120(13) 0.0092(13) C33 0.051(2) 0.0423(19) 0.0380(19) 0.0035(15) 0.0185(16) 0.0152(16) C43 0.047(2) 0.066(2) 0.0368(19) 0.0056(17) 0.0151(17) 0.0311(19) C53 0.0339(17) 0.064(2) 0.0389(19) 0.0049(16) 0.0195(15) 0.0132(16) C63 0.0338(16) 0.0444(18) 0.0285(16) 0.0027(13) 0.0127(13) 0.0070(13) C73 0.050(2) 0.0307(16) 0.0353(18) 0.0022(13) 0.0156(15) 0.0003(14) C93 0.065(2) 0.0388(19) 0.041(2) 0.0031(15) 0.0271(18) 0.0056(17) C83 0.087(3) 0.045(2) 0.046(2) -0.0089(17) 0.026(2) -0.017(2) C103 0.0296(17) 0.051(2) 0.059(2) 0.0173(17) 0.0178(16) 0.0039(15) C123 0.082(3) 0.059(3) 0.055(3) 0.001(2) 0.023(2) -0.012(2) C113 0.170(6) 0.080(4) 0.043(3) 0.017(2) 0.019(3) -0.043(4) C14 0.0333(16) 0.0404(17) 0.0282(16) -0.0047(13) 0.0137(13) -0.0009(13) C34 0.0352(18) 0.065(2) 0.0379(19) 0.0068(16) 0.0156(15) 0.0049(16) C24 0.060(2) 0.046(2) 0.068(3) -0.0033(19) 0.019(2) -0.0134(18) C44 0.044(2) 0.087(3) 0.035(2) -0.0165(19) 0.0112(17) -0.014(2) Fe2 0.0241(2) 0.0297(2) 0.0236(2) -0.00291(16) 0.00946(17) -0.00073(16) Si 0.0329(5) 0.0472(5) 0.0293(5) -0.0084(4) 0.0091(4) -0.0058(4) N15 0.0254(12) 0.0280(12) 0.0253(12) 0.0000(9) 0.0110(10) -0.0017(9) N25 0.0232(11) 0.0290(12) 0.0243(12) -0.0014(9) 0.0080(10) 0.0011(9) C55 0.0436(19) 0.059(2) 0.0263(16) -0.0050(15) 0.0099(15) 0.0157(16) C45 0.0326(15) 0.0258(14) 0.0236(14) 0.0009(11) 0.0112(12) 0.0009(11) C35 0.0331(15) 0.0264(14) 0.0200(14) -0.0002(11) 0.0070(12) -0.0003(11) C25 0.0285(14) 0.0286(14) 0.0258(15) 0.0010(11) 0.0094(12) -0.0023(11) C15 0.0287(16) 0.056(2) 0.0325(17) -0.0030(15) 0.0090(14) -0.0017(14) C16 0.0240(14) 0.0359(16) 0.0252(15) 0.0001(12) 0.0105(12) -0.0041(11) C26 0.0384(17) 0.0379(17) 0.0393(18) 0.0009(14) 0.0229(15) -0.0029(13) C36 0.0410(18) 0.0433(19) 0.046(2) -0.0014(15) 0.0262(16) -0.0066(14) C46 0.0351(17) 0.051(2) 0.0375(18) -0.0043(15) 0.0214(15) -0.0019(14) C56 0.0322(16) 0.0440(18) 0.0371(18) -0.0036(14) 0.0148(14) 0.0051(14) C66 0.0296(15) 0.0345(16) 0.0292(16) 0.0007(12) 0.0115(13) 0.0007(12) C76 0.068(2) 0.0373(19) 0.070(3) 0.0157(17) 0.049(2) 0.0050(17) C96 0.042(2) 0.037(2) 0.094(3) 0.001(2) 0.016(2) -0.0045(16) C86 0.080(3) 0.043(2) 0.056(3) -0.0063(18) 0.021(2) -0.006(2) C106 0.0420(18) 0.0306(16) 0.0364(17) 0.0044(13) 0.0196(15) 0.0067(13) C126 0.057(2) 0.0313(17) 0.049(2) 0.0037(14) 0.0270(18) -0.0029(15) C116 0.060(2) 0.050(2) 0.045(2) 0.0126(17) 0.0172(19) 0.0173(18) C17 0.0288(15) 0.0343(15) 0.0234(14) -0.0053(12) 0.0097(12) 0.0042(12) C27 0.0325(15) 0.0350(16) 0.0253(15) -0.0015(12) 0.0095(13) 0.0047(12) C37 0.0385(17) 0.0426(18) 0.0313(17) 0.0046(13) 0.0140(14) 0.0145(14) C47 0.0336(17) 0.053(2) 0.0324(17) 0.0039(14) 0.0137(14) 0.0149(15) C57 0.0301(16) 0.053(2) 0.0314(17) 0.0000(14) 0.0151(14) 0.0048(14) C67 0.0309(15) 0.0412(17) 0.0267(15) 0.0011(13) 0.0130(13) 0.0035(13) C77 0.0365(17) 0.0308(16) 0.0471(19) 0.0038(14) 0.0187(15) 0.0043(13) C97 0.072(3) 0.098(4) 0.045(2) 0.006(2) 0.023(2) -0.031(3) C87 0.084(3) 0.092(4) 0.065(3) -0.020(3) 0.028(3) -0.046(3) C107 0.0322(16) 0.0387(17) 0.0420(19) 0.0038(14) 0.0172(15) 0.0027(13) C117 0.055(2) 0.044(2) 0.060(3) 0.0011(18) 0.005(2) -0.0016(18) C127 0.133(5) 0.061(3) 0.073(3) 0.020(2) 0.070(3) 0.015(3) C68 0.0374(17) 0.056(2) 0.0268(16) -0.0088(14) 0.0138(14) -0.0087(15) C69 0.049(2) 0.085(3) 0.0325(19) -0.0182(19) 0.0121(17) -0.019(2) C64 0.046(2) 0.045(2) 0.062(3) -0.0129(18) 0.0127(19) -0.0075(16) C71 0.0360(18) 0.061(2) 0.0357(19) 0.0042(16) 0.0094(15) 0.0028(16) K10 0.0317(3) 0.0281(3) 0.0286(3) 0.0024(2) 0.0123(3) 0.0027(2) O10 0.0385(12) 0.0294(11) 0.0388(12) 0.0013(9) 0.0179(10) 0.0033(9) O20 0.0417(12) 0.0299(11) 0.0352(12) 0.0066(9) 0.0190(10) 0.0032(9) O30 0.0387(12) 0.0341(11) 0.0293(11) 0.0013(9) 0.0126(10) 0.0014(9) O40 0.0347(11) 0.0282(11) 0.0325(11) 0.0015(9) 0.0108(9) 0.0028(9) O50 0.0344(11) 0.0334(11) 0.0306(11) 0.0041(9) 0.0142(9) -0.0024(9) O60 0.0344(11) 0.0377(12) 0.0273(11) -0.0010(9) 0.0077(9) 0.0014(9) O70 0.0362(13) 0.0745(18) 0.0357(13) 0.0041(12) 0.0147(11) 0.0100(12) O80 0.0345(12) 0.0460(13) 0.0451(14) -0.0024(11) 0.0164(11) -0.0022(10) C10 0.0438(18) 0.0301(16) 0.0431(19) 0.0035(14) 0.0163(16) 0.0039(14) C20 0.053(2) 0.0261(16) 0.052(2) 0.0064(14) 0.0238(18) 0.0012(14) C30 0.0452(19) 0.0425(18) 0.0361(18) 0.0099(14) 0.0220(15) 0.0056(15) C40 0.0453(19) 0.0448(19) 0.0281(16) 0.0075(14) 0.0166(15) 0.0077(15) C50 0.049(2) 0.0376(17) 0.0367(18) -0.0073(14) 0.0186(16) -0.0007(15) C60 0.0461(19) 0.0318(16) 0.0432(19) -0.0034(14) 0.0203(16) 0.0040(14) C70 0.0452(19) 0.0270(16) 0.0414(19) 0.0055(13) 0.0065(16) 0.0040(14) C80 0.0408(18) 0.0320(16) 0.0435(19) 0.0085(14) 0.0139(16) -0.0061(13) C90 0.0415(18) 0.050(2) 0.0356(18) 0.0152(15) 0.0209(15) 0.0083(15) C100 0.0412(18) 0.052(2) 0.0248(16) 0.0042(14) 0.0121(14) 0.0071(15) C110 0.0392(18) 0.0434(19) 0.0343(18) -0.0087(14) 0.0116(15) -0.0062(14) C120 0.0375(17) 0.0331(16) 0.0385(18) -0.0098(13) 0.0150(15) -0.0022(13) C160 0.060(2) 0.066(3) 0.055(2) 0.023(2) 0.035(2) 0.018(2) C150 0.059(2) 0.066(3) 0.047(2) 0.0089(19) 0.019(2) 0.021(2) C140 0.043(2) 0.081(3) 0.049(2) 0.008(2) 0.0105(18) 0.014(2) C130 0.044(2) 0.097(3) 0.033(2) 0.007(2) 0.0124(17) 0.015(2) C170 0.048(2) 0.049(2) 0.045(2) -0.0007(16) 0.0183(17) -0.0093(16) C180 0.036(2) 0.126(4) 0.052(3) 0.023(3) 0.0149(19) 0.004(2) C190 0.071(3) 0.189(7) 0.061(3) 0.032(4) 0.034(3) 0.063(4) C200 0.0401(18) 0.049(2) 0.0403(19) -0.0067(15) 0.0164(16) -0.0064(15) K20 0.0394(4) 0.0304(3) 0.0307(3) 0.0015(3) 0.0154(3) -0.0001(3) O90 0.0561(15) 0.0472(14) 0.0350(13) -0.0020(10) 0.0230(12) -0.0084(11) O100 0.0381(12) 0.0339(11) 0.0323(12) -0.0019(9) 0.0142(10) -0.0004(9) O110 0.0360(11) 0.0313(11) 0.0309(11) -0.0001(9) 0.0157(9) -0.0017(9) O120 0.0353(11) 0.0335(11) 0.0286(11) 0.0001(9) 0.0086(9) 0.0027(9) O130 0.0399(12) 0.0310(11) 0.0390(13) 0.0012(9) 0.0126(10) 0.0022(9) O140 0.0658(16) 0.0382(13) 0.0395(13) 0.0062(10) 0.0225(12) -0.0084(11) O150 0.0398(13) 0.0590(16) 0.0477(15) -0.0046(12) 0.0195(12) 0.0025(11) O160 0.0472(16) 0.0638(19) 0.108(3) 0.0288(17) 0.0326(17) -0.0033(14) C210 0.056(2) 0.050(2) 0.0384(19) -0.0099(16) 0.0257(17) -0.0094(17) C220 0.054(2) 0.047(2) 0.049(2) -0.0092(16) 0.0277(18) -0.0006(17) C230 0.051(2) 0.0286(16) 0.0428(19) -0.0025(14) 0.0134(16) 0.0012(14) C240 0.0426(18) 0.0325(16) 0.0369(18) 0.0047(13) 0.0104(15) -0.0047(14) C250 0.0408(17) 0.0418(18) 0.0280(16) 0.0066(13) 0.0171(14) 0.0074(14) C260 0.0399(18) 0.0432(18) 0.0267(16) 0.0030(13) 0.0098(14) 0.0061(14) C270 0.0395(17) 0.0366(17) 0.0362(18) -0.0076(14) 0.0121(15) -0.0048(14) C280 0.0391(18) 0.0333(17) 0.047(2) -0.0062(14) 0.0173(16) -0.0001(13) C290 0.055(2) 0.0312(17) 0.049(2) 0.0079(15) 0.0123(18) 0.0016(15) C300 0.069(3) 0.0350(18) 0.048(2) 0.0092(16) 0.021(2) -0.0048(17) C310 0.106(4) 0.058(3) 0.047(2) 0.0066(19) 0.041(3) -0.012(2) C320 0.089(3) 0.062(3) 0.033(2) 0.0027(17) 0.031(2) -0.007(2) C330 0.052(2) 0.047(2) 0.047(2) -0.0011(16) 0.0249(18) 0.0002(16) C340 0.049(2) 0.072(3) 0.063(3) 0.000(2) 0.023(2) 0.013(2) C350 0.065(3) 0.046(2) 0.062(3) 0.0017(19) 0.017(2) 0.0013(19) C360 0.046(2) 0.074(3) 0.044(2) -0.0005(19) 0.0170(18) 0.0014(19) C370 0.055(3) 0.084(3) 0.060(3) 0.014(2) 0.019(2) 0.014(2) C380 0.035(2) 0.165(6) 0.051(3) -0.016(3) 0.014(2) 0.013(3) C390 0.070(3) 0.111(5) 0.091(4) -0.029(3) 0.026(3) -0.015(3) C400 0.079(3) 0.072(3) 0.121(5) 0.000(3) 0.055(3) -0.017(3) O170 0.0621(16) 0.0413(13) 0.0388(14) 0.0006(11) 0.0147(12) 0.0033(12) C410 0.114(4) 0.067(3) 0.046(3) -0.013(2) -0.011(3) 0.044(3) C420 0.089(3) 0.055(3) 0.059(3) -0.011(2) 0.017(3) -0.006(2) C430 0.082(3) 0.046(2) 0.051(2) 0.0079(18) 0.028(2) 0.003(2) C440 0.056(2) 0.046(2) 0.046(2) 0.0021(16) 0.0222(18) -0.0035(17) O180 0.063(2) 0.0580(19) 0.114(3) -0.0208(18) 0.025(2) -0.0136(15) C480 0.052(2) 0.052(2) 0.080(3) -0.006(2) 0.021(2) -0.0012(19) C470 0.051(3) 0.082(3) 0.114(4) -0.047(3) 0.031(3) -0.012(2) C460 0.067(3) 0.064(3) 0.195(7) -0.023(4) 0.066(4) -0.004(3) C450 0.112(4) 0.049(2) 0.091(4) -0.016(2) 0.069(3) -0.015(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N21 1.910(2) . ? Fe1 N11 1.916(2) . ? Fe1 C14 2.014(3) . ? Si14 C14 1.808(3) . ? Si14 C34 1.853(4) . ? Si14 C24 1.855(4) . ? Si14 C44 1.868(4) . ? N11 C21 1.343(4) . ? N11 C12 1.413(4) . ? N21 C41 1.349(4) . ? N21 C13 1.413(4) . ? C11 C21 1.492(4) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C21 C31 1.389(4) . ? C31 C41 1.390(4) . ? C31 H31 0.9500 . ? C41 C51 1.491(4) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C12 C22 1.395(4) . ? C12 C62 1.398(4) . ? C22 C32 1.378(4) . ? C22 C72 1.500(4) . ? C32 C42 1.362(5) . ? C32 H32 0.9500 . ? C42 C52 1.360(5) . ? C42 H42 0.9500 . ? C52 C62 1.377(4) . ? C52 H52 0.9500 . ? C62 C102 1.497(4) . ? C72 C92 1.505(4) . ? C72 C82 1.514(4) . ? C72 H72 1.0000 . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C82 H82A 0.9800 . ? C82 H82B 0.9800 . ? C82 H82C 0.9800 . ? C102 C112 1.512(5) . ? C102 C122 1.519(4) . ? C102 H102 1.0000 . ? C112 H11D 0.9800 . ? C112 H11E 0.9800 . ? C112 H11F 0.9800 . ? C122 H12A 0.9800 . ? C122 H12B 0.9800 . ? C122 H12C 0.9800 . ? C13 C63 1.387(4) . ? C13 C23 1.405(4) . ? C23 C33 1.372(4) . ? C23 C73 1.498(5) . ? C33 C43 1.358(5) . ? C33 H33 0.9500 . ? C43 C53 1.372(5) . ? C43 H43 0.9500 . ? C53 C63 1.378(4) . ? C53 H53 0.9500 . ? C63 C103 1.502(5) . ? C73 C93 1.506(5) . ? C73 C83 1.509(5) . ? C73 H73 1.0000 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? C103 C123 1.486(6) . ? C103 C113 1.486(6) . ? C103 H103 1.0000 . ? C123 H12D 0.9800 . ? C123 H12E 0.9800 . ? C123 H12F 0.9800 . ? C113 H11G 0.9800 . ? C113 H11H 0.9800 . ? C113 H11I 0.9800 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? Fe2 N25 1.908(2) . ? Fe2 N15 1.920(2) . ? Fe2 C68 2.016(3) . ? Si C68 1.812(3) . ? Si C64 1.853(4) . ? Si C71 1.862(4) . ? Si C69 1.875(4) . ? N15 C25 1.344(4) . ? N15 C16 1.412(4) . ? N25 C45 1.349(4) . ? N25 C17 1.414(4) . ? C55 C45 1.497(4) . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? C45 C35 1.379(4) . ? C35 C25 1.387(4) . ? C35 H35 0.9500 . ? C25 C15 1.502(4) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 C26 1.389(4) . ? C16 C66 1.391(4) . ? C26 C36 1.375(4) . ? C26 C76 1.501(5) . ? C36 C46 1.357(5) . ? C36 H36 0.9500 . ? C46 C56 1.365(5) . ? C46 H46 0.9500 . ? C56 C66 1.375(4) . ? C56 H56 0.9500 . ? C66 C106 1.493(4) . ? C76 C96 1.508(6) . ? C76 C86 1.533(6) . ? C76 H76 1.0000 . ? C96 H96A 0.9800 . ? C96 H96B 0.9800 . ? C96 H96C 0.9800 . ? C86 H86A 0.9800 . ? C86 H86B 0.9800 . ? C86 H86C 0.9800 . ? C106 C116 1.516(5) . ? C106 C126 1.517(5) . ? C106 H106 1.0000 . ? C126 H12G 0.9800 . ? C126 H12H 0.9800 . ? C126 H12I 0.9800 . ? C116 H11J 0.9800 . ? C116 H11K 0.9800 . ? C116 H11L 0.9800 . ? C17 C67 1.389(4) . ? C17 C27 1.398(4) . ? C27 C37 1.379(4) . ? C27 C77 1.510(4) . ? C37 C47 1.367(5) . ? C37 H37 0.9500 . ? C47 C57 1.367(5) . ? C47 H47 0.9500 . ? C57 C67 1.379(4) . ? C57 H57 0.9500 . ? C67 C107 1.501(4) . ? C77 C87 1.478(5) . ? C77 C97 1.497(5) . ? C77 H77 1.0000 . ? C97 H97A 0.9800 . ? C97 H97B 0.9800 . ? C97 H97C 0.9800 . ? C87 H87A 0.9800 . ? C87 H87B 0.9800 . ? C87 H87C 0.9800 . ? C107 C117 1.487(5) . ? C107 C127 1.523(5) . ? C107 H107 1.0000 . ? C117 H11M 0.9800 . ? C117 H11N 0.9800 . ? C117 H11O 0.9800 . ? C127 H12J 0.9800 . ? C127 H12K 0.9800 . ? C127 H12L 0.9800 . ? C68 H68A 0.9900 . ? C68 H68B 0.9900 . ? C69 H69A 0.9800 . ? C69 H69B 0.9800 . ? C69 H69C 0.9800 . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C71 H71A 0.9800 . ? C71 H71B 0.9800 . ? C71 H71C 0.9800 . ? K10 O70 2.674(2) . ? K10 O80 2.696(2) . ? K10 O10 2.738(2) . ? K10 O50 2.746(2) . ? K10 O40 2.760(2) . ? K10 O30 2.770(2) . ? K10 O20 2.793(2) . ? K10 O60 2.827(2) . ? K10 C80 3.524(3) . ? O10 C10 1.405(4) . ? O10 C120 1.413(4) . ? O20 C20 1.407(4) . ? O20 C30 1.410(4) . ? O30 C50 1.411(4) . ? O30 C40 1.415(4) . ? O40 C60 1.402(4) . ? O40 C70 1.410(4) . ? O50 C90 1.404(4) . ? O50 C80 1.404(4) . ? O60 C110 1.408(4) . ? O60 C100 1.411(4) . ? O70 C160 1.389(4) . ? O70 C130 1.419(4) . ? O80 C200 1.418(4) . ? O80 C170 1.420(4) . ? C10 C20 1.479(5) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C30 C40 1.479(5) . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C50 C60 1.487(5) . ? C50 H50A 0.9900 . ? C50 H50B 0.9900 . ? C60 H60A 0.9900 . ? C60 H60B 0.9900 . ? C70 C80 1.480(5) . ? C70 H70A 0.9900 . ? C70 H70B 0.9900 . ? C80 H80A 0.9900 . ? C80 H80B 0.9900 . ? C90 C100 1.474(5) . ? C90 H90A 0.9900 . ? C90 H90B 0.9900 . ? C100 H10C 0.9900 . ? C100 H10D 0.9900 . ? C110 C120 1.476(5) . ? C110 H11P 0.9900 . ? C110 H11Q 0.9900 . ? C120 H12M 0.9900 . ? C120 H12N 0.9900 . ? C160 C150 1.493(5) . ? C160 H16A 0.9900 . ? C160 H16B 0.9900 . ? C150 C140 1.472(5) . ? C150 H15D 0.9900 . ? C150 H15E 0.9900 . ? C140 C130 1.488(5) . ? C140 H14C 0.9900 . ? C140 H14D 0.9900 . ? C130 H13A 0.9900 . ? C130 H13B 0.9900 . ? C170 C180 1.491(6) . ? C170 H17A 0.9900 . ? C170 H17B 0.9900 . ? C180 C190 1.435(7) . ? C180 H18A 0.9900 . ? C180 H18B 0.9900 . ? C190 C200 1.443(6) . ? C190 H19A 0.9900 . ? C190 H19B 0.9900 . ? C200 H20C 0.9900 . ? C200 H20D 0.9900 . ? K20 O160 2.645(3) . ? K20 O150 2.678(2) . ? K20 O90 2.735(2) . ? K20 O110 2.739(2) . ? K20 O130 2.756(2) . ? K20 O100 2.763(2) . ? K20 O140 2.775(2) . ? K20 O120 2.797(2) . ? K20 C400 3.348(5) . ? K20 C260 3.530(3) . ? K20 C240 3.537(3) . ? O90 C210 1.408(4) . ? O90 C320 1.414(5) . ? O100 C220 1.399(4) . ? O100 C230 1.414(4) . ? O110 C240 1.402(4) . ? O110 C250 1.407(4) . ? O120 C260 1.406(4) . ? O120 C270 1.407(4) . ? O130 C280 1.407(4) . ? O130 C290 1.409(4) . ? O140 C310 1.393(5) . ? O140 C300 1.417(4) . ? O150 C330 1.406(4) . ? O150 C360 1.421(5) . ? O160 C370 1.381(5) . ? O160 C400 1.393(5) . ? C210 C220 1.466(5) . ? C210 H21A 0.9900 . ? C210 H21B 0.9900 . ? C220 H22A 0.9900 . ? C220 H22B 0.9900 . ? C230 C240 1.474(5) . ? C230 H23A 0.9900 . ? C230 H23B 0.9900 . ? C240 H24D 0.9900 . ? C240 H24E 0.9900 . ? C250 C260 1.473(5) . ? C250 H25A 0.9900 . ? C250 H25B 0.9900 . ? C260 H26A 0.9900 . ? C260 H26B 0.9900 . ? C270 C280 1.475(5) . ? C270 H27A 0.9900 . ? C270 H27B 0.9900 . ? C280 H28A 0.9900 . ? C280 H28B 0.9900 . ? C290 C300 1.468(5) . ? C290 H29A 0.9900 . ? C290 H29B 0.9900 . ? C300 H30C 0.9900 . ? C300 H30D 0.9900 . ? C310 C320 1.473(6) . ? C310 H31A 0.9900 . ? C310 H31B 0.9900 . ? C320 H32A 0.9900 . ? C320 H32B 0.9900 . ? C330 C340 1.498(5) . ? C330 H33A 0.9900 . ? C330 H33B 0.9900 . ? C340 C350 1.479(6) . ? C340 H34D 0.9900 . ? C340 H34E 0.9900 . ? C350 C360 1.475(6) . ? C350 H35A 0.9900 . ? C350 H35B 0.9900 . ? C360 H36A 0.9900 . ? C360 H36B 0.9900 . ? C370 C380 1.569(7) . ? C370 H37A 0.9900 . ? C370 H37B 0.9900 . ? C380 C390 1.502(8) . ? C380 H38A 0.9900 . ? C380 H38B 0.9900 . ? C390 C400 1.429(7) . ? C390 H39A 0.9900 . ? C390 H39B 0.9900 . ? C400 H40C 0.9900 . ? C400 H40D 0.9900 . ? O170 C410 1.394(5) . ? O170 C440 1.405(4) . ? C410 C420 1.490(6) . ? C410 H41A 0.9900 . ? C410 H41B 0.9900 . ? C420 C430 1.481(6) . ? C420 H42A 0.9900 . ? C420 H42B 0.9900 . ? C430 C440 1.471(5) . ? C430 H43A 0.9900 . ? C430 H43B 0.9900 . ? C440 H44D 0.9900 . ? C440 H44E 0.9900 . ? O180 C450 1.380(6) . ? O180 C480 1.389(5) . ? C480 C470 1.486(6) . ? C480 H48A 0.9900 . ? C480 H48B 0.9900 . ? C470 C460 1.407(7) . ? C470 H47A 0.9900 . ? C470 H47B 0.9900 . ? C460 C450 1.453(7) . ? C460 H46A 0.9900 . ? C460 H46B 0.9900 . ? C450 H45A 0.9900 . ? C450 H45B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N21 Fe1 N11 97.68(10) . . ? N21 Fe1 C14 143.14(11) . . ? N11 Fe1 C14 117.63(11) . . ? C14 Si14 C34 111.13(16) . . ? C14 Si14 C24 111.06(17) . . ? C34 Si14 C24 109.98(19) . . ? C14 Si14 C44 113.01(16) . . ? C34 Si14 C44 105.89(18) . . ? C24 Si14 C44 105.5(2) . . ? C21 N11 C12 119.8(2) . . ? C21 N11 Fe1 123.74(19) . . ? C12 N11 Fe1 116.17(18) . . ? C41 N21 C13 117.9(2) . . ? C41 N21 Fe1 122.86(19) . . ? C13 N21 Fe1 117.07(18) . . ? C21 C11 H11A 109.5 . . ? C21 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C21 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N11 C21 C31 122.2(3) . . ? N11 C21 C11 120.1(3) . . ? C31 C21 C11 117.7(3) . . ? C21 C31 C41 129.9(3) . . ? C21 C31 H31 115.0 . . ? C41 C31 H31 115.0 . . ? N21 C41 C31 123.1(3) . . ? N21 C41 C51 119.4(3) . . ? C31 C41 C51 117.5(3) . . ? C41 C51 H51A 109.5 . . ? C41 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C41 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C22 C12 C62 120.0(3) . . ? C22 C12 N11 119.2(3) . . ? C62 C12 N11 120.6(3) . . ? C32 C22 C12 118.5(3) . . ? C32 C22 C72 121.1(3) . . ? C12 C22 C72 120.3(3) . . ? C42 C32 C22 121.7(3) . . ? C42 C32 H32 119.2 . . ? C22 C32 H32 119.2 . . ? C52 C42 C32 119.4(3) . . ? C52 C42 H42 120.3 . . ? C32 C42 H42 120.3 . . ? C42 C52 C62 121.7(3) . . ? C42 C52 H52 119.2 . . ? C62 C52 H52 119.2 . . ? C52 C62 C12 118.6(3) . . ? C52 C62 C102 120.1(3) . . ? C12 C62 C102 121.1(3) . . ? C22 C72 C92 113.6(3) . . ? C22 C72 C82 112.6(3) . . ? C92 C72 C82 110.1(3) . . ? C22 C72 H72 106.7 . . ? C92 C72 H72 106.7 . . ? C82 C72 H72 106.7 . . ? C72 C92 H92A 109.5 . . ? C72 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C72 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C72 C82 H82A 109.5 . . ? C72 C82 H82B 109.5 . . ? H82A C82 H82B 109.5 . . ? C72 C82 H82C 109.5 . . ? H82A C82 H82C 109.5 . . ? H82B C82 H82C 109.5 . . ? C62 C102 C112 109.3(3) . . ? C62 C102 C122 112.7(3) . . ? C112 C102 C122 110.9(3) . . ? C62 C102 H102 107.9 . . ? C112 C102 H102 107.9 . . ? C122 C102 H102 107.9 . . ? C102 C112 H11D 109.5 . . ? C102 C112 H11E 109.5 . . ? H11D C112 H11E 109.5 . . ? C102 C112 H11F 109.5 . . ? H11D C112 H11F 109.5 . . ? H11E C112 H11F 109.5 . . ? C102 C122 H12A 109.5 . . ? C102 C122 H12B 109.5 . . ? H12A C122 H12B 109.5 . . ? C102 C122 H12C 109.5 . . ? H12A C122 H12C 109.5 . . ? H12B C122 H12C 109.5 . . ? C63 C13 C23 120.5(3) . . ? C63 C13 N21 121.0(3) . . ? C23 C13 N21 118.3(3) . . ? C33 C23 C13 118.4(3) . . ? C33 C23 C73 119.4(3) . . ? C13 C23 C73 122.1(3) . . ? C43 C33 C23 121.2(3) . . ? C43 C33 H33 119.4 . . ? C23 C33 H33 119.4 . . ? C33 C43 C53 120.5(3) . . ? C33 C43 H43 119.8 . . ? C53 C43 H43 119.8 . . ? C43 C53 C63 120.7(3) . . ? C43 C53 H53 119.7 . . ? C63 C53 H53 119.7 . . ? C53 C63 C13 118.7(3) . . ? C53 C63 C103 120.4(3) . . ? C13 C63 C103 120.8(3) . . ? C23 C73 C93 110.5(3) . . ? C23 C73 C83 113.1(3) . . ? C93 C73 C83 110.2(3) . . ? C23 C73 H73 107.6 . . ? C93 C73 H73 107.6 . . ? C83 C73 H73 107.6 . . ? C73 C93 H93A 109.5 . . ? C73 C93 H93B 109.5 . . ? H93A C93 H93B 109.5 . . ? C73 C93 H93C 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C73 C83 H83A 109.5 . . ? C73 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C73 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? C123 C103 C113 109.7(4) . . ? C123 C103 C63 114.0(3) . . ? C113 C103 C63 112.4(4) . . ? C123 C103 H103 106.8 . . ? C113 C103 H103 106.8 . . ? C63 C103 H103 106.8 . . ? C103 C123 H12D 109.5 . . ? C103 C123 H12E 109.5 . . ? H12D C123 H12E 109.5 . . ? C103 C123 H12F 109.5 . . ? H12D C123 H12F 109.5 . . ? H12E C123 H12F 109.5 . . ? C103 C113 H11G 109.5 . . ? C103 C113 H11H 109.5 . . ? H11G C113 H11H 109.5 . . ? C103 C113 H11I 109.5 . . ? H11G C113 H11I 109.5 . . ? H11H C113 H11I 109.5 . . ? Si14 C14 Fe1 122.11(16) . . ? Si14 C14 H14A 106.8 . . ? Fe1 C14 H14A 106.8 . . ? Si14 C14 H14B 106.8 . . ? Fe1 C14 H14B 106.8 . . ? H14A C14 H14B 106.6 . . ? Si14 C34 H34A 109.5 . . ? Si14 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? Si14 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? Si14 C24 H24A 109.5 . . ? Si14 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? Si14 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? Si14 C44 H44A 109.5 . . ? Si14 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? Si14 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? N25 Fe2 N15 97.64(10) . . ? N25 Fe2 C68 138.91(12) . . ? N15 Fe2 C68 121.88(12) . . ? C68 Si C64 111.75(17) . . ? C68 Si C71 111.32(17) . . ? C64 Si C71 109.82(18) . . ? C68 Si C69 112.14(16) . . ? C64 Si C69 105.6(2) . . ? C71 Si C69 105.89(18) . . ? C25 N15 C16 118.7(2) . . ? C25 N15 Fe2 123.38(19) . . ? C16 N15 Fe2 117.28(18) . . ? C45 N25 C17 117.3(2) . . ? C45 N25 Fe2 123.13(19) . . ? C17 N25 Fe2 118.41(18) . . ? C45 C55 H55A 109.5 . . ? C45 C55 H55B 109.5 . . ? H55A C55 H55B 109.5 . . ? C45 C55 H55C 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? N25 C45 C35 122.9(3) . . ? N25 C45 C55 119.6(3) . . ? C35 C45 C55 117.5(3) . . ? C45 C35 C25 130.4(3) . . ? C45 C35 H35 114.8 . . ? C25 C35 H35 114.8 . . ? N15 C25 C35 122.3(3) . . ? N15 C25 C15 119.7(3) . . ? C35 C25 C15 118.0(3) . . ? C25 C15 H15A 109.5 . . ? C25 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C25 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C26 C16 C66 119.1(3) . . ? C26 C16 N15 119.9(3) . . ? C66 C16 N15 121.0(3) . . ? C36 C26 C16 119.6(3) . . ? C36 C26 C76 119.1(3) . . ? C16 C26 C76 121.3(3) . . ? C46 C36 C26 121.2(3) . . ? C46 C36 H36 119.4 . . ? C26 C36 H36 119.4 . . ? C36 C46 C56 119.6(3) . . ? C36 C46 H46 120.2 . . ? C56 C46 H46 120.2 . . ? C46 C56 C66 121.0(3) . . ? C46 C56 H56 119.5 . . ? C66 C56 H56 119.5 . . ? C56 C66 C16 119.5(3) . . ? C56 C66 C106 119.7(3) . . ? C16 C66 C106 120.8(3) . . ? C26 C76 C96 111.2(3) . . ? C26 C76 C86 110.7(3) . . ? C96 C76 C86 109.4(3) . . ? C26 C76 H76 108.5 . . ? C96 C76 H76 108.5 . . ? C86 C76 H76 108.5 . . ? C76 C96 H96A 109.5 . . ? C76 C96 H96B 109.5 . . ? H96A C96 H96B 109.5 . . ? C76 C96 H96C 109.5 . . ? H96A C96 H96C 109.5 . . ? H96B C96 H96C 109.5 . . ? C76 C86 H86A 109.5 . . ? C76 C86 H86B 109.5 . . ? H86A C86 H86B 109.5 . . ? C76 C86 H86C 109.5 . . ? H86A C86 H86C 109.5 . . ? H86B C86 H86C 109.5 . . ? C66 C106 C116 112.3(3) . . ? C66 C106 C126 110.5(3) . . ? C116 C106 C126 110.4(3) . . ? C66 C106 H106 107.8 . . ? C116 C106 H106 107.8 . . ? C126 C106 H106 107.8 . . ? C106 C126 H12G 109.5 . . ? C106 C126 H12H 109.5 . . ? H12G C126 H12H 109.5 . . ? C106 C126 H12I 109.5 . . ? H12G C126 H12I 109.5 . . ? H12H C126 H12I 109.5 . . ? C106 C116 H11J 109.5 . . ? C106 C116 H11K 109.5 . . ? H11J C116 H11K 109.5 . . ? C106 C116 H11L 109.5 . . ? H11J C116 H11L 109.5 . . ? H11K C116 H11L 109.5 . . ? C67 C17 C27 120.0(3) . . ? C67 C17 N25 121.2(3) . . ? C27 C17 N25 118.7(3) . . ? C37 C27 C17 118.9(3) . . ? C37 C27 C77 119.5(3) . . ? C17 C27 C77 121.6(3) . . ? C47 C37 C27 121.1(3) . . ? C47 C37 H37 119.4 . . ? C27 C37 H37 119.4 . . ? C37 C47 C57 119.6(3) . . ? C37 C47 H47 120.2 . . ? C57 C47 H47 120.2 . . ? C47 C57 C67 121.4(3) . . ? C47 C57 H57 119.3 . . ? C67 C57 H57 119.3 . . ? C57 C67 C17 118.8(3) . . ? C57 C67 C107 119.5(3) . . ? C17 C67 C107 121.6(3) . . ? C87 C77 C97 110.4(4) . . ? C87 C77 C27 113.1(3) . . ? C97 C77 C27 112.1(3) . . ? C87 C77 H77 107.0 . . ? C97 C77 H77 107.0 . . ? C27 C77 H77 107.0 . . ? C77 C97 H97A 109.5 . . ? C77 C97 H97B 109.5 . . ? H97A C97 H97B 109.5 . . ? C77 C97 H97C 109.5 . . ? H97A C97 H97C 109.5 . . ? H97B C97 H97C 109.5 . . ? C77 C87 H87A 109.5 . . ? C77 C87 H87B 109.5 . . ? H87A C87 H87B 109.5 . . ? C77 C87 H87C 109.5 . . ? H87A C87 H87C 109.5 . . ? H87B C87 H87C 109.5 . . ? C117 C107 C67 111.6(3) . . ? C117 C107 C127 109.0(3) . . ? C67 C107 C127 112.9(3) . . ? C117 C107 H107 107.7 . . ? C67 C107 H107 107.7 . . ? C127 C107 H107 107.7 . . ? C107 C117 H11M 109.5 . . ? C107 C117 H11N 109.5 . . ? H11M C117 H11N 109.5 . . ? C107 C117 H11O 109.5 . . ? H11M C117 H11O 109.5 . . ? H11N C117 H11O 109.5 . . ? C107 C127 H12J 109.5 . . ? C107 C127 H12K 109.5 . . ? H12J C127 H12K 109.5 . . ? C107 C127 H12L 109.5 . . ? H12J C127 H12L 109.5 . . ? H12K C127 H12L 109.5 . . ? Si C68 Fe2 123.87(17) . . ? Si C68 H68A 106.4 . . ? Fe2 C68 H68A 106.4 . . ? Si C68 H68B 106.4 . . ? Fe2 C68 H68B 106.4 . . ? H68A C68 H68B 106.4 . . ? Si C69 H69A 109.5 . . ? Si C69 H69B 109.5 . . ? H69A C69 H69B 109.5 . . ? Si C69 H69C 109.5 . . ? H69A C69 H69C 109.5 . . ? H69B C69 H69C 109.5 . . ? Si C64 H64A 109.5 . . ? Si C64 H64B 109.5 . . ? H64A C64 H64B 109.5 . . ? Si C64 H64C 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? Si C71 H71A 109.5 . . ? Si C71 H71B 109.5 . . ? H71A C71 H71B 109.5 . . ? Si C71 H71C 109.5 . . ? H71A C71 H71C 109.5 . . ? H71B C71 H71C 109.5 . . ? O70 K10 O80 164.60(8) . . ? O70 K10 O10 101.35(8) . . ? O80 K10 O10 90.93(7) . . ? O70 K10 O50 78.49(7) . . ? O80 K10 O50 87.31(7) . . ? O10 K10 O50 120.42(7) . . ? O70 K10 O40 89.31(8) . . ? O80 K10 O40 78.59(7) . . ? O10 K10 O40 169.35(7) . . ? O50 K10 O40 61.54(6) . . ? O70 K10 O30 88.14(7) . . ? O80 K10 O30 93.91(7) . . ? O10 K10 O30 119.58(7) . . ? O50 K10 O30 119.96(7) . . ? O40 K10 O30 60.03(6) . . ? O70 K10 O20 107.83(7) . . ? O80 K10 O20 86.27(7) . . ? O10 K10 O20 60.31(6) . . ? O50 K10 O20 173.55(7) . . ? O40 K10 O20 116.44(7) . . ? O30 K10 O20 60.01(6) . . ? O70 K10 O60 95.48(7) . . ? O80 K10 O60 82.30(7) . . ? O10 K10 O60 60.86(6) . . ? O50 K10 O60 59.90(6) . . ? O40 K10 O60 118.73(6) . . ? O30 K10 O60 176.20(7) . . ? O20 K10 O60 119.64(6) . . ? O70 K10 C80 88.73(8) . . ? O80 K10 C80 75.90(8) . . ? O10 K10 C80 137.41(8) . . ? O50 K10 C80 21.64(7) . . ? O40 K10 C80 41.85(7) . . ? O30 K10 C80 101.83(7) . . ? O20 K10 C80 153.92(8) . . ? O60 K10 C80 77.15(7) . . ? C10 O10 C120 111.8(2) . . ? C10 O10 K10 115.83(18) . . ? C120 O10 K10 116.03(17) . . ? C20 O20 C30 112.3(2) . . ? C20 O20 K10 114.22(18) . . ? C30 O20 K10 111.72(17) . . ? C50 O30 C40 111.4(2) . . ? C50 O30 K10 116.77(18) . . ? C40 O30 K10 117.41(18) . . ? C60 O40 C70 112.1(2) . . ? C60 O40 K10 114.48(17) . . ? C70 O40 K10 113.97(18) . . ? C90 O50 C80 112.3(2) . . ? C90 O50 K10 118.23(18) . . ? C80 O50 K10 112.20(17) . . ? C110 O60 C100 112.4(2) . . ? C110 O60 K10 109.79(18) . . ? C100 O60 K10 109.66(17) . . ? C160 O70 C130 106.8(3) . . ? C160 O70 K10 117.9(2) . . ? C130 O70 K10 132.4(2) . . ? C200 O80 C170 109.5(3) . . ? C200 O80 K10 119.01(19) . . ? C170 O80 K10 115.25(19) . . ? O10 C10 C20 108.6(3) . . ? O10 C10 H10A 110.0 . . ? C20 C10 H10A 110.0 . . ? O10 C10 H10B 110.0 . . ? C20 C10 H10B 110.0 . . ? H10A C10 H10B 108.4 . . ? O20 C20 C10 109.2(3) . . ? O20 C20 H20A 109.8 . . ? C10 C20 H20A 109.8 . . ? O20 C20 H20B 109.8 . . ? C10 C20 H20B 109.8 . . ? H20A C20 H20B 108.3 . . ? O20 C30 C40 108.8(3) . . ? O20 C30 H30A 109.9 . . ? C40 C30 H30A 109.9 . . ? O20 C30 H30B 109.9 . . ? C40 C30 H30B 109.9 . . ? H30A C30 H30B 108.3 . . ? O30 C40 C30 108.5(3) . . ? O30 C40 H40A 110.0 . . ? C30 C40 H40A 110.0 . . ? O30 C40 H40B 110.0 . . ? C30 C40 H40B 110.0 . . ? H40A C40 H40B 108.4 . . ? O30 C50 C60 108.2(3) . . ? O30 C50 H50A 110.1 . . ? C60 C50 H50A 110.1 . . ? O30 C50 H50B 110.1 . . ? C60 C50 H50B 110.1 . . ? H50A C50 H50B 108.4 . . ? O40 C60 C50 109.1(3) . . ? O40 C60 H60A 109.9 . . ? C50 C60 H60A 109.9 . . ? O40 C60 H60B 109.9 . . ? C50 C60 H60B 109.9 . . ? H60A C60 H60B 108.3 . . ? O40 C70 C80 109.1(3) . . ? O40 C70 H70A 109.9 . . ? C80 C70 H70A 109.9 . . ? O40 C70 H70B 109.9 . . ? C80 C70 H70B 109.9 . . ? H70A C70 H70B 108.3 . . ? O50 C80 C70 109.2(3) . . ? O50 C80 K10 46.16(13) . . ? C70 C80 K10 79.79(17) . . ? O50 C80 H80A 109.8 . . ? C70 C80 H80A 109.8 . . ? K10 C80 H80A 155.5 . . ? O50 C80 H80B 109.8 . . ? C70 C80 H80B 109.8 . . ? K10 C80 H80B 88.3 . . ? H80A C80 H80B 108.3 . . ? O50 C90 C100 109.1(3) . . ? O50 C90 H90A 109.9 . . ? C100 C90 H90A 109.9 . . ? O50 C90 H90B 109.9 . . ? C100 C90 H90B 109.9 . . ? H90A C90 H90B 108.3 . . ? O60 C100 C90 108.3(3) . . ? O60 C100 H10C 110.0 . . ? C90 C100 H10C 110.0 . . ? O60 C100 H10D 110.0 . . ? C90 C100 H10D 110.0 . . ? H10C C100 H10D 108.4 . . ? O60 C110 C120 109.2(3) . . ? O60 C110 H11P 109.8 . . ? C120 C110 H11P 109.8 . . ? O60 C110 H11Q 109.8 . . ? C120 C110 H11Q 109.8 . . ? H11P C110 H11Q 108.3 . . ? O10 C120 C110 108.2(3) . . ? O10 C120 H12M 110.1 . . ? C110 C120 H12M 110.1 . . ? O10 C120 H12N 110.1 . . ? C110 C120 H12N 110.1 . . ? H12M C120 H12N 108.4 . . ? O70 C160 C150 104.8(3) . . ? O70 C160 H16A 110.8 . . ? C150 C160 H16A 110.8 . . ? O70 C160 H16B 110.8 . . ? C150 C160 H16B 110.8 . . ? H16A C160 H16B 108.9 . . ? C140 C150 C160 102.7(3) . . ? C140 C150 H15D 111.2 . . ? C160 C150 H15D 111.2 . . ? C140 C150 H15E 111.2 . . ? C160 C150 H15E 111.2 . . ? H15D C150 H15E 109.1 . . ? C150 C140 C130 104.7(3) . . ? C150 C140 H14C 110.8 . . ? C130 C140 H14C 110.8 . . ? C150 C140 H14D 110.8 . . ? C130 C140 H14D 110.8 . . ? H14C C140 H14D 108.9 . . ? O70 C130 C140 107.2(3) . . ? O70 C130 H13A 110.3 . . ? C140 C130 H13A 110.3 . . ? O70 C130 H13B 110.3 . . ? C140 C130 H13B 110.3 . . ? H13A C130 H13B 108.5 . . ? O80 C170 C180 105.7(3) . . ? O80 C170 H17A 110.6 . . ? C180 C170 H17A 110.6 . . ? O80 C170 H17B 110.6 . . ? C180 C170 H17B 110.6 . . ? H17A C170 H17B 108.7 . . ? C190 C180 C170 104.3(3) . . ? C190 C180 H18A 110.9 . . ? C170 C180 H18A 110.9 . . ? C190 C180 H18B 110.9 . . ? C170 C180 H18B 110.9 . . ? H18A C180 H18B 108.9 . . ? C180 C190 C200 106.5(4) . . ? C180 C190 H19A 110.4 . . ? C200 C190 H19A 110.4 . . ? C180 C190 H19B 110.4 . . ? C200 C190 H19B 110.4 . . ? H19A C190 H19B 108.6 . . ? O80 C200 C190 106.3(3) . . ? O80 C200 H20C 110.5 . . ? C190 C200 H20C 110.5 . . ? O80 C200 H20D 110.5 . . ? C190 C200 H20D 110.5 . . ? H20C C200 H20D 108.7 . . ? O160 K20 O150 167.81(9) . . ? O160 K20 O90 90.83(10) . . ? O150 K20 O90 97.82(8) . . ? O160 K20 O110 74.98(8) . . ? O150 K20 O110 93.28(7) . . ? O90 K20 O110 118.46(7) . . ? O160 K20 O130 92.07(9) . . ? O150 K20 O130 91.17(7) . . ? O90 K20 O130 119.28(7) . . ? O110 K20 O130 120.77(7) . . ? O160 K20 O100 91.08(9) . . ? O150 K20 O100 85.80(7) . . ? O90 K20 O100 60.42(7) . . ? O110 K20 O100 60.38(6) . . ? O130 K20 O100 176.84(7) . . ? O160 K20 O140 105.73(9) . . ? O150 K20 O140 86.05(8) . . ? O90 K20 O140 61.00(7) . . ? O110 K20 O140 179.05(8) . . ? O130 K20 O140 59.95(7) . . ? O100 K20 O140 118.86(7) . . ? O160 K20 O120 86.03(9) . . ? O150 K20 O120 85.32(7) . . ? O90 K20 O120 176.85(7) . . ? O110 K20 O120 60.95(6) . . ? O130 K20 O120 60.65(6) . . ? O100 K20 O120 119.85(6) . . ? O140 K20 O120 119.63(7) . . ? O160 K20 C400 23.33(11) . . ? O150 K20 C400 165.56(11) . . ? O90 K20 C400 85.54(12) . . ? O110 K20 C400 97.45(11) . . ? O130 K20 C400 75.05(11) . . ? O100 K20 C400 107.91(11) . . ? O140 K20 C400 83.32(12) . . ? O120 K20 C400 91.46(12) . . ? O160 K20 C260 72.35(10) . . ? O150 K20 C260 96.75(8) . . ? O90 K20 C260 156.07(8) . . ? O110 K20 C260 41.62(7) . . ? O130 K20 C260 79.20(7) . . ? O100 K20 C260 102.00(7) . . ? O140 K20 C260 139.13(8) . . ? O120 K20 C260 22.01(7) . . ? C400 K20 C260 85.06(12) . . ? O160 K20 C240 87.62(8) . . ? O150 K20 C240 82.22(8) . . ? O90 K20 C240 101.89(8) . . ? O110 K20 C240 21.35(7) . . ? O130 K20 C240 138.82(7) . . ? O100 K20 C240 41.58(7) . . ? O140 K20 C240 157.72(8) . . ? O120 K20 C240 78.28(7) . . ? C400 K20 C240 110.95(11) . . ? C260 K20 C240 61.52(8) . . ? C210 O90 C320 110.9(3) . . ? C210 O90 K20 115.77(18) . . ? C320 O90 K20 115.4(2) . . ? C220 O100 C230 112.9(3) . . ? C220 O100 K20 114.26(19) . . ? C230 O100 K20 116.00(18) . . ? C240 O110 C250 112.1(2) . . ? C240 O110 K20 113.31(17) . . ? C250 O110 K20 116.07(17) . . ? C260 O120 C270 112.0(2) . . ? C260 O120 K20 109.78(17) . . ? C270 O120 K20 111.84(18) . . ? C280 O130 C290 112.8(3) . . ? C280 O130 K20 115.01(18) . . ? C290 O130 K20 115.57(19) . . ? C310 O140 C300 111.7(3) . . ? C310 O140 K20 113.1(2) . . ? C300 O140 K20 115.8(2) . . ? C330 O150 C360 107.0(3) . . ? C330 O150 K20 119.6(2) . . ? C360 O150 K20 122.3(2) . . ? C370 O160 C400 113.4(4) . . ? C370 O160 K20 134.3(3) . . ? C400 O160 K20 107.9(3) . . ? O90 C210 C220 109.1(3) . . ? O90 C210 H21A 109.9 . . ? C220 C210 H21A 109.9 . . ? O90 C210 H21B 109.9 . . ? C220 C210 H21B 109.9 . . ? H21A C210 H21B 108.3 . . ? O100 C220 C210 109.0(3) . . ? O100 C220 H22A 109.9 . . ? C210 C220 H22A 109.9 . . ? O100 C220 H22B 109.9 . . ? C210 C220 H22B 109.9 . . ? H22A C220 H22B 108.3 . . ? O100 C230 C240 108.9(3) . . ? O100 C230 H23A 109.9 . . ? C240 C230 H23A 109.9 . . ? O100 C230 H23B 109.9 . . ? C240 C230 H23B 109.9 . . ? H23A C230 H23B 108.3 . . ? O110 C240 C230 108.3(3) . . ? O110 C240 K20 45.35(13) . . ? C230 C240 K20 81.05(18) . . ? O110 C240 H24D 110.0 . . ? C230 C240 H24D 110.0 . . ? K20 C240 H24D 87.1 . . ? O110 C240 H24E 110.0 . . ? C230 C240 H24E 110.0 . . ? K20 C240 H24E 155.2 . . ? H24D C240 H24E 108.4 . . ? O110 C250 C260 109.1(3) . . ? O110 C250 H25A 109.9 . . ? C260 C250 H25A 109.9 . . ? O110 C250 H25B 109.9 . . ? C260 C250 H25B 109.9 . . ? H25A C250 H25B 108.3 . . ? O120 C260 C250 108.8(3) . . ? O120 C260 K20 48.21(13) . . ? C250 C260 K20 80.27(17) . . ? O120 C260 H26A 109.9 . . ? C250 C260 H26A 109.9 . . ? K20 C260 H26A 158.0 . . ? O120 C260 H26B 109.9 . . ? C250 C260 H26B 109.9 . . ? K20 C260 H26B 85.0 . . ? H26A C260 H26B 108.3 . . ? O120 C270 C280 108.9(3) . . ? O120 C270 H27A 109.9 . . ? C280 C270 H27A 109.9 . . ? O120 C270 H27B 109.9 . . ? C280 C270 H27B 109.9 . . ? H27A C270 H27B 108.3 . . ? O130 C280 C270 108.2(3) . . ? O130 C280 H28A 110.1 . . ? C270 C280 H28A 110.1 . . ? O130 C280 H28B 110.1 . . ? C270 C280 H28B 110.1 . . ? H28A C280 H28B 108.4 . . ? O130 C290 C300 109.0(3) . . ? O130 C290 H29A 109.9 . . ? C300 C290 H29A 109.9 . . ? O130 C290 H29B 109.9 . . ? C300 C290 H29B 109.9 . . ? H29A C290 H29B 108.3 . . ? O140 C300 C290 108.9(3) . . ? O140 C300 H30C 109.9 . . ? C290 C300 H30C 109.9 . . ? O140 C300 H30D 109.9 . . ? C290 C300 H30D 109.9 . . ? H30C C300 H30D 108.3 . . ? O140 C310 C320 109.8(3) . . ? O140 C310 H31A 109.7 . . ? C320 C310 H31A 109.7 . . ? O140 C310 H31B 109.7 . . ? C320 C310 H31B 109.7 . . ? H31A C310 H31B 108.2 . . ? O90 C320 C310 109.6(3) . . ? O90 C320 H32A 109.8 . . ? C310 C320 H32A 109.8 . . ? O90 C320 H32B 109.8 . . ? C310 C320 H32B 109.8 . . ? H32A C320 H32B 108.2 . . ? O150 C330 C340 106.7(3) . . ? O150 C330 H33A 110.4 . . ? C340 C330 H33A 110.4 . . ? O150 C330 H33B 110.4 . . ? C340 C330 H33B 110.4 . . ? H33A C330 H33B 108.6 . . ? C350 C340 C330 105.6(3) . . ? C350 C340 H34D 110.6 . . ? C330 C340 H34D 110.6 . . ? C350 C340 H34E 110.6 . . ? C330 C340 H34E 110.6 . . ? H34D C340 H34E 108.8 . . ? C360 C350 C340 105.3(3) . . ? C360 C350 H35A 110.7 . . ? C340 C350 H35A 110.7 . . ? C360 C350 H35B 110.7 . . ? C340 C350 H35B 110.7 . . ? H35A C350 H35B 108.8 . . ? O150 C360 C350 106.6(3) . . ? O150 C360 H36A 110.4 . . ? C350 C360 H36A 110.4 . . ? O150 C360 H36B 110.4 . . ? C350 C360 H36B 110.4 . . ? H36A C360 H36B 108.6 . . ? O160 C370 C380 102.4(4) . . ? O160 C370 H37A 111.3 . . ? C380 C370 H37A 111.3 . . ? O160 C370 H37B 111.3 . . ? C380 C370 H37B 111.3 . . ? H37A C370 H37B 109.2 . . ? C390 C380 C370 101.7(4) . . ? C390 C380 H38A 111.4 . . ? C370 C380 H38A 111.4 . . ? C390 C380 H38B 111.4 . . ? C370 C380 H38B 111.4 . . ? H38A C380 H38B 109.3 . . ? C400 C390 C380 104.4(4) . . ? C400 C390 H39A 110.9 . . ? C380 C390 H39A 110.9 . . ? C400 C390 H39B 110.9 . . ? C380 C390 H39B 110.9 . . ? H39A C390 H39B 108.9 . . ? O160 C400 C390 101.7(5) . . ? O160 C400 K20 48.8(2) . . ? C390 C400 K20 147.4(4) . . ? O160 C400 H40C 111.4 . . ? C390 C400 H40C 111.4 . . ? K20 C400 H40C 75.4 . . ? O160 C400 H40D 111.4 . . ? C390 C400 H40D 111.4 . . ? K20 C400 H40D 94.8 . . ? H40C C400 H40D 109.3 . . ? C410 O170 C440 109.2(3) . . ? O170 C410 C420 107.6(4) . . ? O170 C410 H41A 110.2 . . ? C420 C410 H41A 110.2 . . ? O170 C410 H41B 110.2 . . ? C420 C410 H41B 110.2 . . ? H41A C410 H41B 108.5 . . ? C430 C420 C410 103.9(4) . . ? C430 C420 H42A 111.0 . . ? C410 C420 H42A 111.0 . . ? C430 C420 H42B 111.0 . . ? C410 C420 H42B 111.0 . . ? H42A C420 H42B 109.0 . . ? C440 C430 C420 103.2(4) . . ? C440 C430 H43A 111.1 . . ? C420 C430 H43A 111.1 . . ? C440 C430 H43B 111.1 . . ? C420 C430 H43B 111.1 . . ? H43A C430 H43B 109.1 . . ? O170 C440 C430 105.8(3) . . ? O170 C440 H44D 110.6 . . ? C430 C440 H44D 110.6 . . ? O170 C440 H44E 110.6 . . ? C430 C440 H44E 110.6 . . ? H44D C440 H44E 108.7 . . ? C450 O180 C480 107.0(3) . . ? O180 C480 C470 105.4(4) . . ? O180 C480 H48A 110.7 . . ? C470 C480 H48A 110.7 . . ? O180 C480 H48B 110.7 . . ? C470 C480 H48B 110.7 . . ? H48A C480 H48B 108.8 . . ? C460 C470 C480 102.3(4) . . ? C460 C470 H47A 111.3 . . ? C480 C470 H47A 111.3 . . ? C460 C470 H47B 111.3 . . ? C480 C470 H47B 111.3 . . ? H47A C470 H47B 109.2 . . ? C470 C460 C450 106.6(4) . . ? C470 C460 H46A 110.4 . . ? C450 C460 H46A 110.4 . . ? C470 C460 H46B 110.4 . . ? C450 C460 H46B 110.4 . . ? H46A C460 H46B 108.6 . . ? O180 C450 C460 107.9(4) . . ? O180 C450 H45A 110.1 . . ? C460 C450 H45A 110.1 . . ? O180 C450 H45B 110.1 . . ? C460 C450 H45B 110.1 . . ? H45A C450 H45B 108.4 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C12 N11 C21 C31 -169.3(3) . . . . ? Fe1 N11 C21 C31 4.0(4) . . . . ? C12 N11 C21 C11 8.6(4) . . . . ? Fe1 N11 C21 C11 -178.0(2) . . . . ? N11 C21 C31 C41 3.3(5) . . . . ? C11 C21 C31 C41 -174.7(3) . . . . ? C13 N21 C41 C31 166.0(3) . . . . ? Fe1 N21 C41 C31 3.2(4) . . . . ? C13 N21 C41 C51 -12.1(4) . . . . ? Fe1 N21 C41 C51 -174.9(2) . . . . ? C21 C31 C41 N21 -7.3(5) . . . . ? C21 C31 C41 C51 170.8(3) . . . . ? C21 N11 C12 C22 100.6(3) . . . . ? Fe1 N11 C12 C22 -73.2(3) . . . . ? C21 N11 C12 C62 -84.7(3) . . . . ? Fe1 N11 C12 C62 101.5(3) . . . . ? C62 C12 C22 C32 2.3(4) . . . . ? N11 C12 C22 C32 177.1(3) . . . . ? C62 C12 C22 C72 -175.4(3) . . . . ? N11 C12 C22 C72 -0.7(4) . . . . ? C12 C22 C32 C42 -0.8(4) . . . . ? C72 C22 C32 C42 177.0(3) . . . . ? C22 C32 C42 C52 -1.3(5) . . . . ? C32 C42 C52 C62 1.8(5) . . . . ? C42 C52 C62 C12 -0.2(5) . . . . ? C42 C52 C62 C102 -175.6(3) . . . . ? C22 C12 C62 C52 -1.8(4) . . . . ? N11 C12 C62 C52 -176.5(3) . . . . ? C22 C12 C62 C102 173.4(3) . . . . ? N11 C12 C62 C102 -1.2(4) . . . . ? C32 C22 C72 C92 -22.4(4) . . . . ? C12 C22 C72 C92 155.3(3) . . . . ? C32 C22 C72 C82 103.6(3) . . . . ? C12 C22 C72 C82 -78.7(3) . . . . ? C52 C62 C102 C112 74.4(4) . . . . ? C12 C62 C102 C112 -100.9(3) . . . . ? C52 C62 C102 C122 -49.4(4) . . . . ? C12 C62 C102 C122 135.4(3) . . . . ? C41 N21 C13 C63 102.9(3) . . . . ? Fe1 N21 C13 C63 -93.3(3) . . . . ? C41 N21 C13 C23 -80.1(3) . . . . ? Fe1 N21 C13 C23 83.7(3) . . . . ? C63 C13 C23 C33 -0.9(4) . . . . ? N21 C13 C23 C33 -177.9(3) . . . . ? C63 C13 C23 C73 175.5(3) . . . . ? N21 C13 C23 C73 -1.5(4) . . . . ? C13 C23 C33 C43 0.2(5) . . . . ? C73 C23 C33 C43 -176.3(3) . . . . ? C23 C33 C43 C53 0.8(5) . . . . ? C33 C43 C53 C63 -1.1(5) . . . . ? C43 C53 C63 C13 0.4(5) . . . . ? C43 C53 C63 C103 -178.8(3) . . . . ? C23 C13 C63 C53 0.6(5) . . . . ? N21 C13 C63 C53 177.5(3) . . . . ? C23 C13 C63 C103 179.8(3) . . . . ? N21 C13 C63 C103 -3.3(5) . . . . ? C33 C23 C73 C93 63.3(4) . . . . ? C13 C23 C73 C93 -113.1(3) . . . . ? C33 C23 C73 C83 -60.9(4) . . . . ? C13 C23 C73 C83 122.8(3) . . . . ? C53 C63 C103 C123 -50.9(5) . . . . ? C13 C63 C103 C123 129.9(4) . . . . ? C53 C63 C103 C113 74.7(5) . . . . ? C13 C63 C103 C113 -104.5(4) . . . . ? C34 Si14 C14 Fe1 -61.3(2) . . . . ? C24 Si14 C14 Fe1 61.4(3) . . . . ? C44 Si14 C14 Fe1 179.8(2) . . . . ? C17 N25 C45 C35 169.1(3) . . . . ? Fe2 N25 C45 C35 1.5(4) . . . . ? C17 N25 C45 C55 -11.5(4) . . . . ? Fe2 N25 C45 C55 -179.1(2) . . . . ? N25 C45 C35 C25 -4.8(5) . . . . ? C55 C45 C35 C25 175.8(3) . . . . ? C16 N15 C25 C35 -170.3(3) . . . . ? Fe2 N15 C25 C35 0.5(4) . . . . ? C16 N15 C25 C15 8.6(4) . . . . ? Fe2 N15 C25 C15 179.4(2) . . . . ? C45 C35 C25 N15 3.6(5) . . . . ? C45 C35 C25 C15 -175.3(3) . . . . ? C25 N15 C16 C26 90.1(3) . . . . ? Fe2 N15 C16 C26 -81.3(3) . . . . ? C25 N15 C16 C66 -92.2(3) . . . . ? Fe2 N15 C16 C66 96.4(3) . . . . ? C66 C16 C26 C36 -0.4(5) . . . . ? N15 C16 C26 C36 177.3(3) . . . . ? C66 C16 C26 C76 178.4(3) . . . . ? N15 C16 C26 C76 -3.8(5) . . . . ? C16 C26 C36 C46 0.2(5) . . . . ? C76 C26 C36 C46 -178.7(3) . . . . ? C26 C36 C46 C56 -0.2(5) . . . . ? C36 C46 C56 C66 0.4(5) . . . . ? C46 C56 C66 C16 -0.7(5) . . . . ? C46 C56 C66 C106 -178.7(3) . . . . ? C26 C16 C66 C56 0.7(5) . . . . ? N15 C16 C66 C56 -177.0(3) . . . . ? C26 C16 C66 C106 178.7(3) . . . . ? N15 C16 C66 C106 1.0(4) . . . . ? C36 C26 C76 C96 -64.1(4) . . . . ? C16 C26 C76 C96 117.0(4) . . . . ? C36 C26 C76 C86 57.6(5) . . . . ? C16 C26 C76 C86 -121.2(4) . . . . ? C56 C66 C106 C116 -52.7(4) . . . . ? C16 C66 C106 C116 129.3(3) . . . . ? C56 C66 C106 C126 71.2(4) . . . . ? C16 C66 C106 C126 -106.8(3) . . . . ? C45 N25 C17 C67 93.6(3) . . . . ? Fe2 N25 C17 C67 -98.2(3) . . . . ? C45 N25 C17 C27 -88.6(3) . . . . ? Fe2 N25 C17 C27 79.6(3) . . . . ? C67 C17 C27 C37 -3.3(4) . . . . ? N25 C17 C27 C37 178.9(3) . . . . ? C67 C17 C27 C77 175.0(3) . . . . ? N25 C17 C27 C77 -2.7(4) . . . . ? C17 C27 C37 C47 2.1(5) . . . . ? C77 C27 C37 C47 -176.3(3) . . . . ? C27 C37 C47 C57 0.4(5) . . . . ? C37 C47 C57 C67 -1.7(5) . . . . ? C47 C57 C67 C17 0.4(5) . . . . ? C47 C57 C67 C107 180.0(3) . . . . ? C27 C17 C67 C57 2.1(4) . . . . ? N25 C17 C67 C57 179.8(3) . . . . ? C27 C17 C67 C107 -177.4(3) . . . . ? N25 C17 C67 C107 0.3(4) . . . . ? C37 C27 C77 C87 -79.3(4) . . . . ? C17 C27 C77 C87 102.4(4) . . . . ? C37 C27 C77 C97 46.3(4) . . . . ? C17 C27 C77 C97 -132.0(4) . . . . ? C57 C67 C107 C117 -66.0(4) . . . . ? C17 C67 C107 C117 113.6(4) . . . . ? C57 C67 C107 C127 57.1(5) . . . . ? C17 C67 C107 C127 -123.3(4) . . . . ? C64 Si C68 Fe2 60.6(3) . . . . ? C71 Si C68 Fe2 -62.6(3) . . . . ? C69 Si C68 Fe2 179.0(2) . . . . ? C120 O10 C10 C20 -174.2(3) . . . . ? K10 O10 C10 C20 49.8(3) . . . . ? C30 O20 C20 C10 175.5(3) . . . . ? K10 O20 C20 C10 47.0(3) . . . . ? O10 C10 C20 O20 -64.4(4) . . . . ? C20 O20 C30 C40 173.0(3) . . . . ? K10 O20 C30 C40 -57.1(3) . . . . ? C50 O30 C40 C30 -178.3(3) . . . . ? K10 O30 C40 C30 -39.9(3) . . . . ? O20 C30 C40 O30 64.8(3) . . . . ? C40 O30 C50 C60 -177.9(3) . . . . ? K10 O30 C50 C60 43.4(3) . . . . ? C70 O40 C60 C50 -175.7(3) . . . . ? K10 O40 C60 C50 52.5(3) . . . . ? O30 C50 C60 O40 -63.3(3) . . . . ? C60 O40 C70 C80 -177.0(3) . . . . ? K10 O40 C70 C80 -45.0(3) . . . . ? C90 O50 C80 C70 170.5(3) . . . . ? K10 O50 C80 C70 -53.5(3) . . . . ? C90 O50 C80 K10 -136.0(3) . . . . ? O40 C70 C80 O50 67.0(3) . . . . ? O40 C70 C80 K10 30.9(2) . . . . ? C80 O50 C90 C100 171.6(3) . . . . ? K10 O50 C90 C100 38.5(3) . . . . ? C110 O60 C100 C90 -178.9(3) . . . . ? K10 O60 C100 C90 58.7(3) . . . . ? O50 C90 C100 O60 -65.7(3) . . . . ? C100 O60 C110 C120 -177.4(3) . . . . ? K10 O60 C110 C120 -55.0(3) . . . . ? C10 O10 C120 C110 178.4(3) . . . . ? K10 O10 C120 C110 -45.7(3) . . . . ? O60 C110 C120 O10 68.8(3) . . . . ? C130 O70 C160 C150 -35.5(4) . . . . ? K10 O70 C160 C150 127.7(3) . . . . ? O70 C160 C150 C140 36.4(5) . . . . ? C160 C150 C140 C130 -23.1(5) . . . . ? C160 O70 C130 C140 20.6(5) . . . . ? K10 O70 C130 C140 -139.2(3) . . . . ? C150 C140 C130 O70 2.8(5) . . . . ? C200 O80 C170 C180 7.2(4) . . . . ? K10 O80 C170 C180 144.6(3) . . . . ? O80 C170 C180 C190 -21.7(5) . . . . ? C170 C180 C190 C200 28.0(6) . . . . ? C170 O80 C200 C190 10.2(5) . . . . ? K10 O80 C200 C190 -125.4(4) . . . . ? C180 C190 C200 O80 -24.2(6) . . . . ? C320 O90 C210 C220 179.4(3) . . . . ? K20 O90 C210 C220 -46.6(3) . . . . ? C230 O100 C220 C210 174.9(3) . . . . ? K20 O100 C220 C210 -49.6(3) . . . . ? O90 C210 C220 O100 64.0(4) . . . . ? C220 O100 C230 C240 175.6(3) . . . . ? K20 O100 C230 C240 41.0(3) . . . . ? C250 O110 C240 C230 -170.2(3) . . . . ? K20 O110 C240 C230 56.1(3) . . . . ? C250 O110 C240 K20 133.7(3) . . . . ? O100 C230 C240 O110 -64.5(3) . . . . ? O100 C230 C240 K20 -27.8(2) . . . . ? C240 O110 C250 C260 -174.3(3) . . . . ? K20 O110 C250 C260 -42.0(3) . . . . ? C270 O120 C260 C250 178.1(3) . . . . ? K20 O120 C260 C250 -57.0(3) . . . . ? C270 O120 C260 K20 -124.9(3) . . . . ? O110 C250 C260 O120 67.6(3) . . . . ? O110 C250 C260 K20 28.2(2) . . . . ? C260 O120 C270 C280 176.4(3) . . . . ? K20 O120 C270 C280 52.7(3) . . . . ? C290 O130 C280 C270 -176.4(3) . . . . ? K20 O130 C280 C270 48.1(3) . . . . ? O120 C270 C280 O130 -68.3(3) . . . . ? C280 O130 C290 C300 174.8(3) . . . . ? K20 O130 C290 C300 -49.9(3) . . . . ? C310 O140 C300 C290 -177.2(3) . . . . ? K20 O140 C300 C290 -45.7(4) . . . . ? O130 C290 C300 O140 63.0(4) . . . . ? C300 O140 C310 C320 -176.9(4) . . . . ? K20 O140 C310 C320 50.2(4) . . . . ? C210 O90 C320 C310 179.2(3) . . . . ? K20 O90 C320 C310 45.0(4) . . . . ? O140 C310 C320 O90 -64.2(5) . . . . ? C360 O150 C330 C340 -27.3(4) . . . . ? K20 O150 C330 C340 117.4(3) . . . . ? O150 C330 C340 C350 13.3(4) . . . . ? C330 C340 C350 C360 5.0(5) . . . . ? C330 O150 C360 C350 30.8(4) . . . . ? K20 O150 C360 C350 -112.8(3) . . . . ? C340 C350 C360 O150 -21.5(5) . . . . ? C400 O160 C370 C380 15.3(5) . . . . ? K20 O160 C370 C380 168.1(3) . . . . ? O160 C370 C380 C390 10.5(5) . . . . ? C370 C380 C390 C400 -31.4(6) . . . . ? C370 O160 C400 C390 -35.9(6) . . . . ? K20 O160 C400 C390 164.1(3) . . . . ? C370 O160 C400 K20 159.9(5) . . . . ? C380 C390 C400 O160 40.4(6) . . . . ? C380 C390 C400 K20 62.8(9) . . . . ? C440 O170 C410 C420 -6.6(6) . . . . ? O170 C410 C420 C430 -13.7(6) . . . . ? C410 C420 C430 C440 27.6(5) . . . . ? C410 O170 C440 C430 24.7(5) . . . . ? C420 C430 C440 O170 -32.4(4) . . . . ? C450 O180 C480 C470 -28.7(6) . . . . ? O180 C480 C470 C460 33.3(6) . . . . ? C480 C470 C460 C450 -25.0(7) . . . . ? C480 O180 C450 C460 13.0(6) . . . . ? C470 C460 C450 O180 8.7(7) . . . . ? _refine_diff_density_max 0.967 _refine_diff_density_min -0.597 _refine_diff_density_rms 0.069 _shelx_res_file ; mini-21065.res created by SHELXL-2014/7 TITL mini-21065 CELL 0.71073 24.228 19.8535 27.1355 90 114.199 90 ZERR 8 0.0007 0.0004 0.0009 0 0.004 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Fe K N O Si UNIT 456 800 8 8 16 72 8 L.S. 30 TEMP -180 SIZE 0.20 0.20 0.10 CONF MORE -1 ACTA BOND $H WGHT 0.084600 12.000100 FVAR 0.12676 FE1 3 0.345761 0.553350 0.209808 11.00000 0.02618 0.02664 = 0.02319 -0.00279 0.01038 -0.00061 SI14 7 0.460330 0.606242 0.322460 11.00000 0.03096 0.04220 = 0.02906 -0.00510 0.00869 -0.00541 N11 5 0.259512 0.561257 0.174215 11.00000 0.02976 0.02567 = 0.02707 -0.00177 0.01379 -0.00146 N21 5 0.358714 0.511877 0.151901 11.00000 0.02644 0.02623 = 0.02510 -0.00025 0.01085 0.00204 C11 1 0.160332 0.555594 0.097144 11.00000 0.03033 0.04297 = 0.02951 -0.00282 0.00841 0.00007 AFIX 137 H11A 2 0.142506 0.533079 0.119293 11.00000 -1.50000 H11B 2 0.143391 0.536318 0.060694 11.00000 -1.50000 H11C 2 0.151137 0.603849 0.095107 11.00000 -1.50000 AFIX 0 C21 1 0.227283 0.545749 0.122025 11.00000 0.02710 0.02869 = 0.02414 0.00155 0.00773 -0.00125 C31 1 0.253842 0.518419 0.089883 11.00000 0.02927 0.02929 = 0.01998 0.00031 0.00515 0.00066 AFIX 43 H31 2 0.227149 0.511710 0.053114 11.00000 -1.20000 AFIX 0 C41 1 0.313456 0.499380 0.103239 11.00000 0.03491 0.02683 = 0.02234 -0.00193 0.01242 -0.00085 C51 1 0.326650 0.461685 0.061796 11.00000 0.04177 0.04450 = 0.02627 -0.00616 0.01314 0.00410 AFIX 137 H51A 2 0.360719 0.482931 0.057153 11.00000 -1.50000 H51B 2 0.290891 0.462374 0.027356 11.00000 -1.50000 H51C 2 0.337014 0.414967 0.073632 11.00000 -1.50000 AFIX 0 C12 1 0.229315 0.578070 0.207362 11.00000 0.02225 0.03238 = 0.02578 -0.00422 0.00854 -0.00364 C22 1 0.223863 0.529547 0.242300 11.00000 0.02664 0.03387 = 0.02863 -0.00466 0.00933 -0.00676 C32 1 0.196750 0.547559 0.276177 11.00000 0.02874 0.04455 = 0.02779 -0.00240 0.01322 -0.00600 AFIX 43 H32 2 0.192387 0.514719 0.299794 11.00000 -1.20000 AFIX 0 C42 1 0.176047 0.611239 0.276670 11.00000 0.02848 0.04942 = 0.03013 -0.00536 0.01326 0.00044 AFIX 43 H42 2 0.156747 0.622313 0.299822 11.00000 -1.20000 AFIX 0 C52 1 0.183244 0.658824 0.243733 11.00000 0.03238 0.03885 = 0.03320 -0.00556 0.01433 0.00376 AFIX 43 H52 2 0.169807 0.703494 0.244963 11.00000 -1.20000 AFIX 0 C62 1 0.209507 0.643906 0.208655 11.00000 0.02715 0.03515 = 0.03108 -0.00220 0.01076 -0.00046 C72 1 0.249180 0.460202 0.244123 11.00000 0.03604 0.03006 = 0.03251 -0.00230 0.01536 -0.00622 AFIX 13 H72 2 0.288168 0.465738 0.240131 11.00000 -1.20000 AFIX 0 C92 1 0.264022 0.424385 0.296908 11.00000 0.05505 0.03548 = 0.03584 0.00151 0.02113 -0.00063 AFIX 137 H92A 2 0.289300 0.453522 0.326800 11.00000 -1.50000 H92B 2 0.285946 0.382670 0.297582 11.00000 -1.50000 H92C 2 0.226485 0.413635 0.300719 11.00000 -1.50000 AFIX 0 C82 1 0.208890 0.416464 0.197570 11.00000 0.04636 0.03425 = 0.03657 -0.00650 0.01712 -0.00850 AFIX 137 H82A 2 0.169516 0.410847 0.199258 11.00000 -1.50000 H82B 2 0.227848 0.372268 0.200000 11.00000 -1.50000 H82C 2 0.203225 0.437963 0.163316 11.00000 -1.50000 AFIX 0 C102 1 0.220724 0.698626 0.175926 11.00000 0.04462 0.03072 = 0.03857 -0.00098 0.02310 0.00646 AFIX 13 H102 2 0.231757 0.676924 0.147945 11.00000 -1.20000 AFIX 0 C112 1 0.273954 0.740772 0.212029 11.00000 0.04828 0.03316 = 0.05462 -0.00057 0.02628 0.00019 AFIX 137 H11D 2 0.264321 0.762370 0.240017 11.00000 -1.50000 H11E 2 0.282488 0.775410 0.190378 11.00000 -1.50000 H11F 2 0.309546 0.711846 0.229087 11.00000 -1.50000 AFIX 0 C122 1 0.165354 0.742413 0.146961 11.00000 0.05216 0.04170 = 0.04103 0.00435 0.02036 0.01479 AFIX 137 H12A 2 0.131368 0.714065 0.124128 11.00000 -1.50000 H12B 2 0.174243 0.775524 0.124427 11.00000 -1.50000 H12C 2 0.154741 0.765890 0.173647 11.00000 -1.50000 AFIX 0 C13 1 0.414091 0.477531 0.165293 11.00000 0.03194 0.03502 = 0.02245 -0.00241 0.01069 0.00673 C23 1 0.418655 0.410752 0.183694 11.00000 0.04322 0.03501 = 0.02214 0.00096 0.01201 0.00925 C33 1 0.472966 0.378056 0.198408 11.00000 0.05149 0.04232 = 0.03803 0.00349 0.01845 0.01517 AFIX 43 H33 2 0.476709 0.332835 0.210811 11.00000 -1.20000 AFIX 0 C43 1 0.521482 0.409198 0.195557 11.00000 0.04748 0.06601 = 0.03684 0.00559 0.01508 0.03108 AFIX 43 H43 2 0.558535 0.385436 0.205533 11.00000 -1.20000 AFIX 0 C53 1 0.517351 0.474733 0.178369 11.00000 0.03395 0.06385 = 0.03889 0.00491 0.01948 0.01316 AFIX 43 H53 2 0.551806 0.496212 0.177145 11.00000 -1.20000 AFIX 0 C63 1 0.463733 0.509721 0.162861 11.00000 0.03377 0.04439 = 0.02846 0.00272 0.01270 0.00704 C73 1 0.367426 0.376011 0.190685 11.00000 0.04959 0.03066 = 0.03525 0.00221 0.01559 0.00032 AFIX 13 H73 2 0.332045 0.407412 0.177589 11.00000 -1.20000 AFIX 0 C93 1 0.383509 0.362202 0.249531 11.00000 0.06518 0.03878 = 0.04125 0.00312 0.02713 0.00556 AFIX 137 H93A 2 0.416919 0.329797 0.263117 11.00000 -1.50000 H93B 2 0.348236 0.343547 0.253734 11.00000 -1.50000 H93C 2 0.395840 0.404272 0.270044 11.00000 -1.50000 AFIX 0 C83 1 0.347965 0.311810 0.158363 11.00000 0.08676 0.04494 = 0.04633 -0.00888 0.02596 -0.01692 AFIX 137 H83A 2 0.335400 0.321866 0.119920 11.00000 -1.50000 H83B 2 0.313983 0.291864 0.163967 11.00000 -1.50000 H83C 2 0.381873 0.280007 0.170212 11.00000 -1.50000 AFIX 0 C103 1 0.459125 0.580991 0.143044 11.00000 0.02962 0.05124 = 0.05857 0.01727 0.01784 0.00388 AFIX 13 H103 2 0.419992 0.599343 0.141454 11.00000 -1.20000 AFIX 0 C123 1 0.507731 0.626000 0.179423 11.00000 0.08150 0.05913 = 0.05498 0.00122 0.02295 -0.01244 AFIX 137 H12D 2 0.508861 0.624009 0.215910 11.00000 -1.50000 H12E 2 0.499597 0.672348 0.165933 11.00000 -1.50000 H12F 2 0.546800 0.611337 0.180425 11.00000 -1.50000 AFIX 0 C113 1 0.456314 0.585033 0.087399 11.00000 0.16982 0.07990 = 0.04285 0.01659 0.01860 -0.04349 AFIX 137 H11G 2 0.495439 0.571711 0.087789 11.00000 -1.50000 H11H 2 0.446966 0.631344 0.074066 11.00000 -1.50000 H11I 2 0.424683 0.554711 0.063635 11.00000 -1.50000 AFIX 0 C14 1 0.384964 0.571539 0.289835 11.00000 0.03334 0.04038 = 0.02821 -0.00472 0.01373 -0.00087 AFIX 23 H14A 2 0.357652 0.602286 0.298012 11.00000 -1.20000 H14B 2 0.385112 0.528369 0.308149 11.00000 -1.20000 AFIX 0 C34 1 0.517048 0.549622 0.314703 11.00000 0.03517 0.06522 = 0.03786 0.00675 0.01560 0.00493 AFIX 137 H34A 2 0.522060 0.509402 0.337072 11.00000 -1.50000 H34B 2 0.555855 0.573220 0.326193 11.00000 -1.50000 H34C 2 0.503225 0.536300 0.276742 11.00000 -1.50000 AFIX 0 C24 1 0.464471 0.690968 0.295320 11.00000 0.05970 0.04552 = 0.06822 -0.00328 0.01867 -0.01341 AFIX 137 H24A 2 0.453534 0.687716 0.256399 11.00000 -1.50000 H24B 2 0.505757 0.708512 0.313430 11.00000 -1.50000 H24C 2 0.436309 0.721426 0.301796 11.00000 -1.50000 AFIX 0 C44 1 0.485178 0.618180 0.396775 11.00000 0.04383 0.08657 = 0.03545 -0.01651 0.01120 -0.01406 AFIX 137 H44A 2 0.458009 0.650065 0.403280 11.00000 -1.50000 H44B 2 0.526562 0.635903 0.412435 11.00000 -1.50000 H44C 2 0.483996 0.574835 0.413596 11.00000 -1.50000 AFIX 0 FE2 3 0.857417 0.542022 0.223076 11.00000 0.02413 0.02972 = 0.02360 -0.00291 0.00946 -0.00073 SI 7 0.962194 0.600725 0.341278 11.00000 0.03293 0.04723 = 0.02928 -0.00839 0.00910 -0.00577 N15 5 0.772049 0.546836 0.179184 11.00000 0.02542 0.02804 = 0.02530 -0.00003 0.01095 -0.00168 N25 5 0.881100 0.503666 0.170215 11.00000 0.02316 0.02899 = 0.02434 -0.00139 0.00797 0.00111 C55 1 0.864015 0.458908 0.080556 11.00000 0.04355 0.05859 = 0.02629 -0.00504 0.00988 0.01574 AFIX 137 H55A 2 0.892601 0.489643 0.074998 11.00000 -1.50000 H55B 2 0.829729 0.450508 0.045942 11.00000 -1.50000 H55C 2 0.884373 0.416244 0.095425 11.00000 -1.50000 AFIX 0 C45 1 0.841619 0.489967 0.119210 11.00000 0.03260 0.02583 = 0.02359 0.00086 0.01115 0.00094 C35 1 0.780628 0.503871 0.100232 11.00000 0.03307 0.02644 = 0.01998 -0.00025 0.00699 -0.00032 AFIX 43 H35 2 0.758176 0.495151 0.062849 11.00000 -1.20000 AFIX 0 C25 1 0.746764 0.528531 0.126905 11.00000 0.02853 0.02860 = 0.02580 0.00102 0.00943 -0.00226 C15 1 0.679405 0.533433 0.095818 11.00000 0.02868 0.05576 = 0.03253 -0.00298 0.00896 -0.00167 AFIX 137 H15A 2 0.659323 0.503752 0.112243 11.00000 -1.50000 H15B 2 0.668516 0.519732 0.058289 11.00000 -1.50000 H15C 2 0.666424 0.580015 0.096638 11.00000 -1.50000 AFIX 0 C16 1 0.733899 0.561433 0.205569 11.00000 0.02401 0.03593 = 0.02522 0.00008 0.01051 -0.00413 C26 1 0.717214 0.510399 0.231744 11.00000 0.03837 0.03789 = 0.03934 0.00094 0.02285 -0.00288 C36 1 0.682113 0.525462 0.259237 11.00000 0.04097 0.04334 = 0.04573 -0.00138 0.02616 -0.00659 AFIX 43 H36 2 0.670851 0.490492 0.277182 11.00000 -1.20000 AFIX 0 C46 1 0.663251 0.589362 0.261219 11.00000 0.03512 0.05122 = 0.03751 -0.00430 0.02137 -0.00188 AFIX 43 H46 2 0.638917 0.598931 0.280312 11.00000 -1.20000 AFIX 0 C56 1 0.679441 0.639796 0.235625 11.00000 0.03224 0.04398 = 0.03711 -0.00356 0.01476 0.00508 AFIX 43 H56 2 0.666432 0.684554 0.237273 11.00000 -1.20000 AFIX 0 C66 1 0.714291 0.626839 0.207488 11.00000 0.02964 0.03447 = 0.02918 0.00068 0.01152 0.00068 C76 1 0.735752 0.438671 0.229795 11.00000 0.06756 0.03731 = 0.06991 0.01567 0.04905 0.00495 AFIX 13 H76 2 0.758731 0.436395 0.206502 11.00000 -1.20000 AFIX 0 C96 1 0.776026 0.413336 0.285366 11.00000 0.04229 0.03650 = 0.09393 0.00087 0.01557 -0.00447 AFIX 137 H96A 2 0.811500 0.442685 0.301271 11.00000 -1.50000 H96B 2 0.789198 0.367335 0.282670 11.00000 -1.50000 H96C 2 0.753559 0.413517 0.308280 11.00000 -1.50000 AFIX 0 C86 1 0.680014 0.393025 0.205203 11.00000 0.08045 0.04295 = 0.05611 -0.00626 0.02050 -0.00583 AFIX 137 H86A 2 0.657974 0.393151 0.228475 11.00000 -1.50000 H86B 2 0.692912 0.347003 0.202165 11.00000 -1.50000 H86C 2 0.653536 0.409748 0.169252 11.00000 -1.50000 AFIX 0 C106 1 0.732292 0.683395 0.180912 11.00000 0.04199 0.03062 = 0.03639 0.00441 0.01960 0.00667 AFIX 13 H106 2 0.751559 0.663431 0.157989 11.00000 -1.20000 AFIX 0 C126 1 0.778854 0.727938 0.222925 11.00000 0.05714 0.03126 = 0.04881 0.00366 0.02705 -0.00291 AFIX 137 H12G 2 0.761336 0.747493 0.246448 11.00000 -1.50000 H12H 2 0.790892 0.764138 0.204820 11.00000 -1.50000 H12I 2 0.814420 0.700967 0.244654 11.00000 -1.50000 AFIX 0 C116 1 0.678495 0.724873 0.144493 11.00000 0.06040 0.05033 = 0.04484 0.01259 0.01722 0.01730 AFIX 137 H11J 2 0.649837 0.695861 0.116426 11.00000 -1.50000 H11K 2 0.692350 0.760833 0.127546 11.00000 -1.50000 H11L 2 0.658518 0.744743 0.165961 11.00000 -1.50000 AFIX 0 C17 1 0.940036 0.476481 0.187559 11.00000 0.02884 0.03430 = 0.02340 -0.00529 0.00966 0.00420 C27 1 0.951151 0.412258 0.210689 11.00000 0.03253 0.03498 = 0.02525 -0.00149 0.00954 0.00473 C37 1 1.008271 0.385051 0.226840 11.00000 0.03845 0.04264 = 0.03132 0.00457 0.01401 0.01454 AFIX 43 H37 2 1.015844 0.340842 0.241504 11.00000 -1.20000 AFIX 0 C47 1 1.054181 0.420592 0.222114 11.00000 0.03360 0.05273 = 0.03244 0.00393 0.01374 0.01486 AFIX 43 H47 2 1.093237 0.401091 0.233179 11.00000 -1.20000 AFIX 0 C57 1 1.043516 0.484398 0.201355 11.00000 0.03005 0.05342 = 0.03136 0.00002 0.01512 0.00476 AFIX 43 H57 2 1.075814 0.509377 0.199040 11.00000 -1.20000 AFIX 0 C67 1 0.986871 0.513284 0.183700 11.00000 0.03086 0.04118 = 0.02670 0.00110 0.01301 0.00350 C77 1 0.902703 0.373004 0.219691 11.00000 0.03655 0.03081 = 0.04707 0.00381 0.01868 0.00427 AFIX 13 H77 2 0.869766 0.405585 0.216021 11.00000 -1.20000 AFIX 0 C97 1 0.925168 0.344265 0.275521 11.00000 0.07198 0.09795 = 0.04490 0.00624 0.02308 -0.03121 AFIX 137 H97A 2 0.955640 0.309622 0.279892 11.00000 -1.50000 H97B 2 0.891275 0.324169 0.281179 11.00000 -1.50000 H97C 2 0.943294 0.380192 0.302041 11.00000 -1.50000 AFIX 0 C87 1 0.875139 0.319652 0.178969 11.00000 0.08449 0.09211 = 0.06501 -0.02033 0.02828 -0.04573 AFIX 137 H87A 2 0.859640 0.339426 0.142708 11.00000 -1.50000 H87B 2 0.841781 0.298595 0.184897 11.00000 -1.50000 H87C 2 0.905717 0.285555 0.182298 11.00000 -1.50000 AFIX 0 C107 1 0.977311 0.583506 0.161244 11.00000 0.03222 0.03865 = 0.04205 0.00378 0.01719 0.00268 AFIX 13 H107 2 0.933258 0.594187 0.148267 11.00000 -1.20000 AFIX 0 C117 1 1.011420 0.633860 0.203323 11.00000 0.05505 0.04405 = 0.05972 0.00111 0.00540 -0.00159 AFIX 137 H11M 2 0.997926 0.631926 0.232758 11.00000 -1.50000 H11N 2 1.004024 0.679056 0.187404 11.00000 -1.50000 H11O 2 1.054782 0.623774 0.217531 11.00000 -1.50000 AFIX 0 C127 1 0.994578 0.591252 0.113528 11.00000 0.13320 0.06094 = 0.07345 0.02028 0.07023 0.01520 AFIX 137 H12J 2 1.038526 0.586755 0.126079 11.00000 -1.50000 H12K 2 0.981908 0.635734 0.097116 11.00000 -1.50000 H12L 2 0.974412 0.556251 0.086685 11.00000 -1.50000 AFIX 0 C68 1 0.891940 0.556628 0.303634 11.00000 0.03739 0.05577 = 0.02682 -0.00885 0.01381 -0.00869 AFIX 23 H68A 2 0.860313 0.580301 0.311234 11.00000 -1.20000 H68B 2 0.896284 0.511418 0.320203 11.00000 -1.20000 AFIX 0 C69 1 0.979528 0.606030 0.415156 11.00000 0.04895 0.08506 = 0.03252 -0.01819 0.01209 -0.01865 AFIX 137 H69A 2 0.945992 0.628337 0.419971 11.00000 -1.50000 H69B 2 1.016765 0.631990 0.433671 11.00000 -1.50000 H69C 2 0.984886 0.560538 0.430436 11.00000 -1.50000 AFIX 0 C64 1 0.959368 0.689007 0.318224 11.00000 0.04565 0.04505 = 0.06241 -0.01291 0.01274 -0.00751 AFIX 137 H64A 2 0.948307 0.689667 0.279205 11.00000 -1.50000 H64B 2 0.999163 0.709981 0.337085 11.00000 -1.50000 H64C 2 0.929138 0.714067 0.326187 11.00000 -1.50000 AFIX 0 C71 1 1.027680 0.556420 0.336739 11.00000 0.03598 0.06108 = 0.03567 0.00424 0.00943 0.00284 AFIX 137 H71A 2 1.035372 0.514314 0.357331 11.00000 -1.50000 H71B 2 1.063610 0.585249 0.351674 11.00000 -1.50000 H71C 2 1.018528 0.546378 0.298825 11.00000 -1.50000 AFIX 0 K10 4 0.651082 0.318227 0.473347 11.00000 0.03172 0.02810 = 0.02856 0.00236 0.01230 0.00272 O10 6 0.659140 0.185995 0.448449 11.00000 0.03846 0.02937 = 0.03879 0.00133 0.01794 0.00333 O20 6 0.685017 0.220985 0.554802 11.00000 0.04167 0.02988 = 0.03525 0.00655 0.01904 0.00324 O30 6 0.658382 0.351688 0.574931 11.00000 0.03867 0.03408 = 0.02930 0.00134 0.01262 0.00144 O40 6 0.666138 0.450936 0.506512 11.00000 0.03467 0.02821 = 0.03253 0.00145 0.01077 0.00278 O50 6 0.631344 0.416910 0.397081 11.00000 0.03438 0.03342 = 0.03064 0.00415 0.01422 -0.00238 O60 6 0.651923 0.285907 0.372206 11.00000 0.03438 0.03772 = 0.02728 -0.00096 0.00772 0.00139 O70 6 0.531218 0.334349 0.435734 11.00000 0.03620 0.07445 = 0.03574 0.00406 0.01468 0.01001 O80 6 0.770447 0.335825 0.501019 11.00000 0.03448 0.04603 = 0.04510 -0.00238 0.01635 -0.00219 C10 1 0.693215 0.144132 0.492129 11.00000 0.04377 0.03013 = 0.04310 0.00353 0.01628 0.00386 AFIX 23 H10A 2 0.736725 0.155394 0.505311 11.00000 -1.20000 H10B 2 0.687747 0.096419 0.480505 11.00000 -1.20000 AFIX 0 C20 1 0.672413 0.154366 0.535775 11.00000 0.05277 0.02615 = 0.05170 0.00636 0.02383 0.00116 AFIX 23 H20A 2 0.628366 0.145790 0.521880 11.00000 -1.20000 H20B 2 0.693404 0.122460 0.565681 11.00000 -1.20000 AFIX 0 C30 1 0.662262 0.235870 0.593790 11.00000 0.04516 0.04250 = 0.03607 0.00986 0.02205 0.00559 AFIX 23 H30A 2 0.676437 0.201696 0.622907 11.00000 -1.20000 H30B 2 0.617474 0.235070 0.576899 11.00000 -1.20000 AFIX 0 C40 1 0.683841 0.303390 0.616522 11.00000 0.04529 0.04476 = 0.02810 0.00750 0.01657 0.00775 AFIX 23 H40A 2 0.671443 0.313006 0.646330 11.00000 -1.20000 H40B 2 0.728556 0.305216 0.631110 11.00000 -1.20000 AFIX 0 C50 1 0.678634 0.417279 0.593638 11.00000 0.04867 0.03755 = 0.03672 -0.00725 0.01865 -0.00073 AFIX 23 H50A 2 0.723090 0.420084 0.605897 11.00000 -1.20000 H50B 2 0.668514 0.428551 0.624505 11.00000 -1.20000 AFIX 0 C60 1 0.648317 0.465219 0.548467 11.00000 0.04609 0.03182 = 0.04318 -0.00337 0.02026 0.00404 AFIX 23 H60A 2 0.603846 0.460880 0.535242 11.00000 -1.20000 H60B 2 0.659679 0.511999 0.561227 11.00000 -1.20000 AFIX 0 C70 1 0.642455 0.497713 0.463846 11.00000 0.04521 0.02701 = 0.04141 0.00552 0.00648 0.00397 AFIX 23 H70A 2 0.658226 0.543292 0.476969 11.00000 -1.20000 H70B 2 0.597787 0.498962 0.450122 11.00000 -1.20000 AFIX 0 C80 1 0.660341 0.477549 0.419944 11.00000 0.04078 0.03201 = 0.04347 0.00852 0.01388 -0.00610 AFIX 23 H80A 2 0.648700 0.513133 0.391948 11.00000 -1.20000 H80B 2 0.704770 0.471583 0.434543 11.00000 -1.20000 AFIX 0 C90 1 0.638500 0.400285 0.349763 11.00000 0.04154 0.04998 = 0.03561 0.01518 0.02088 0.00832 AFIX 23 H90A 2 0.681851 0.402318 0.356552 11.00000 -1.20000 H90B 2 0.616188 0.432903 0.320829 11.00000 -1.20000 AFIX 0 C100 1 0.615014 0.331772 0.332709 11.00000 0.04118 0.05174 = 0.02479 0.00418 0.01207 0.00711 AFIX 23 H10C 2 0.572708 0.328517 0.328986 11.00000 -1.20000 H10D 2 0.615695 0.321194 0.297309 11.00000 -1.20000 AFIX 0 C110 1 0.633564 0.218595 0.358820 11.00000 0.03920 0.04338 = 0.03428 -0.00875 0.01160 -0.00617 AFIX 23 H11P 2 0.636976 0.206120 0.324854 11.00000 -1.20000 H11Q 2 0.590775 0.213349 0.353257 11.00000 -1.20000 AFIX 0 C120 1 0.672393 0.174172 0.403083 11.00000 0.03746 0.03314 = 0.03852 -0.00975 0.01501 -0.00224 AFIX 23 H12M 2 0.664476 0.126435 0.391841 11.00000 -1.20000 H12N 2 0.715565 0.183911 0.412238 11.00000 -1.20000 AFIX 0 C160 1 0.505716 0.338947 0.473079 11.00000 0.05953 0.06567 = 0.05534 0.02325 0.03490 0.01759 AFIX 23 H16A 2 0.537545 0.342038 0.510302 11.00000 -1.20000 H16B 2 0.479997 0.299248 0.470643 11.00000 -1.20000 AFIX 0 C150 1 0.468643 0.401797 0.458188 11.00000 0.05883 0.06588 = 0.04709 0.00891 0.01946 0.02119 AFIX 23 H15D 2 0.435613 0.400227 0.470719 11.00000 -1.20000 H15E 2 0.493914 0.442109 0.473570 11.00000 -1.20000 AFIX 0 C140 1 0.444524 0.401700 0.398792 11.00000 0.04284 0.08127 = 0.04864 0.00772 0.01045 0.01432 AFIX 23 H14C 2 0.443070 0.448005 0.384773 11.00000 -1.20000 H14D 2 0.403275 0.382280 0.382865 11.00000 -1.20000 AFIX 0 C130 1 0.487526 0.359173 0.385992 11.00000 0.04417 0.09713 = 0.03331 0.00731 0.01239 0.01468 AFIX 23 H13A 2 0.465789 0.321321 0.362204 11.00000 -1.20000 H13B 2 0.507414 0.386234 0.367257 11.00000 -1.20000 AFIX 0 C170 1 0.808761 0.316434 0.554570 11.00000 0.04775 0.04917 = 0.04487 -0.00075 0.01829 -0.00928 AFIX 23 H17A 2 0.788761 0.282073 0.568076 11.00000 -1.20000 H17B 2 0.818981 0.355824 0.579076 11.00000 -1.20000 AFIX 0 C180 1 0.864268 0.288218 0.551453 11.00000 0.03613 0.12566 = 0.05151 0.02306 0.01490 0.00433 AFIX 23 H18A 2 0.896815 0.322428 0.561947 11.00000 -1.20000 H18B 2 0.879153 0.248532 0.575368 11.00000 -1.20000 AFIX 0 C190 1 0.845141 0.269433 0.495816 11.00000 0.07129 0.18923 = 0.06069 0.03215 0.03399 0.06319 AFIX 23 H19A 2 0.831631 0.221894 0.490373 11.00000 -1.20000 H19B 2 0.878825 0.274750 0.484409 11.00000 -1.20000 AFIX 0 C200 1 0.795734 0.313696 0.465076 11.00000 0.04005 0.04907 = 0.04028 -0.00671 0.01638 -0.00641 AFIX 23 H20C 2 0.810615 0.352541 0.451120 11.00000 -1.20000 H20D 2 0.765061 0.289356 0.434104 11.00000 -1.20000 AFIX 0 K20 4 0.821208 0.672065 0.507491 11.00000 0.03944 0.03038 = 0.03069 0.00151 0.01537 -0.00012 O90 6 0.815089 0.637063 0.407894 11.00000 0.05612 0.04716 = 0.03499 -0.00197 0.02304 -0.00835 O100 6 0.812103 0.537840 0.478334 11.00000 0.03812 0.03388 = 0.03230 -0.00186 0.01419 -0.00042 O110 6 0.850907 0.574686 0.585664 11.00000 0.03596 0.03128 = 0.03089 -0.00009 0.01570 -0.00172 O120 6 0.834388 0.708054 0.611394 11.00000 0.03528 0.03347 = 0.02862 0.00005 0.00860 0.00268 O130 6 0.823445 0.806412 0.533783 11.00000 0.03993 0.03102 = 0.03900 0.00124 0.01264 0.00219 O140 6 0.789544 0.769389 0.427163 11.00000 0.06576 0.03818 = 0.03951 0.00618 0.02246 -0.00836 O150 6 0.702830 0.664478 0.484458 11.00000 0.03976 0.05903 = 0.04770 -0.00462 0.01946 0.00245 O160 6 0.940736 0.665416 0.549004 11.00000 0.04717 0.06380 = 0.10755 0.02880 0.03264 -0.00327 C210 1 0.795336 0.570992 0.390848 11.00000 0.05622 0.04999 = 0.03842 -0.00987 0.02569 -0.00938 AFIX 23 H21A 2 0.803389 0.559505 0.358904 11.00000 -1.20000 H21B 2 0.751223 0.567525 0.380532 11.00000 -1.20000 AFIX 0 C220 1 0.827668 0.524118 0.435094 11.00000 0.05368 0.04665 = 0.04884 -0.00916 0.02772 -0.00065 AFIX 23 H22A 2 0.816606 0.477164 0.422695 11.00000 -1.20000 H22B 2 0.871873 0.529339 0.446749 11.00000 -1.20000 AFIX 0 C230 1 0.837235 0.491245 0.521227 11.00000 0.05147 0.02863 = 0.04283 -0.00246 0.01343 0.00122 AFIX 23 H23A 2 0.881698 0.489298 0.533278 11.00000 -1.20000 H23B 2 0.820557 0.445750 0.508912 11.00000 -1.20000 AFIX 0 C240 1 0.822353 0.512823 0.566314 11.00000 0.04256 0.03247 = 0.03690 0.00473 0.01039 -0.00473 AFIX 23 H24D 2 0.777996 0.517716 0.553727 11.00000 -1.20000 H24E 2 0.836565 0.478753 0.595509 11.00000 -1.20000 AFIX 0 C250 1 0.847438 0.593658 0.634291 11.00000 0.04080 0.04184 = 0.02798 0.00665 0.01707 0.00735 AFIX 23 H25A 2 0.870526 0.561415 0.663258 11.00000 -1.20000 H25B 2 0.804740 0.593095 0.629699 11.00000 -1.20000 AFIX 0 C260 1 0.872712 0.661881 0.649257 11.00000 0.03987 0.04317 = 0.02668 0.00300 0.00982 0.00614 AFIX 23 H26A 2 0.875968 0.673326 0.685860 11.00000 -1.20000 H26B 2 0.913699 0.663844 0.649604 11.00000 -1.20000 AFIX 0 C270 1 0.854694 0.774806 0.624120 11.00000 0.03953 0.03663 = 0.03624 -0.00765 0.01215 -0.00479 AFIX 23 H27A 2 0.896758 0.778778 0.627302 11.00000 -1.20000 H27B 2 0.854129 0.787819 0.659129 11.00000 -1.20000 AFIX 0 C280 1 0.814600 0.819695 0.580964 11.00000 0.03905 0.03328 = 0.04704 -0.00620 0.01735 -0.00007 AFIX 23 H28A 2 0.771845 0.811422 0.574373 11.00000 -1.20000 H28B 2 0.824297 0.867353 0.591785 11.00000 -1.20000 AFIX 0 C290 1 0.789793 0.849647 0.490732 11.00000 0.05455 0.03119 = 0.04852 0.00795 0.01230 0.00156 AFIX 23 H29A 2 0.798715 0.897163 0.502344 11.00000 -1.20000 H29B 2 0.745974 0.841791 0.479646 11.00000 -1.20000 AFIX 0 C300 1 0.806008 0.836415 0.445120 11.00000 0.06917 0.03497 = 0.04837 0.00923 0.02084 -0.00482 AFIX 23 H30C 2 0.784526 0.868326 0.415352 11.00000 -1.20000 H30D 2 0.850078 0.842655 0.456547 11.00000 -1.20000 AFIX 0 C310 1 0.806354 0.752527 0.385407 11.00000 0.10571 0.05778 = 0.04651 0.00661 0.04124 -0.01222 AFIX 23 H31A 2 0.850923 0.754883 0.398464 11.00000 -1.20000 H31B 2 0.788324 0.784976 0.355317 11.00000 -1.20000 AFIX 0 C320 1 0.785411 0.683928 0.366104 11.00000 0.08931 0.06220 = 0.03278 0.00273 0.03080 -0.00746 AFIX 23 H32A 2 0.741111 0.680893 0.354846 11.00000 -1.20000 H32B 2 0.794264 0.673428 0.334415 11.00000 -1.20000 AFIX 0 C330 1 0.682091 0.680825 0.524374 11.00000 0.05167 0.04678 = 0.04740 -0.00114 0.02489 0.00016 AFIX 23 H33A 2 0.716587 0.691996 0.558793 11.00000 -1.20000 H33B 2 0.659781 0.642381 0.530693 11.00000 -1.20000 AFIX 0 C340 1 0.641131 0.740459 0.503827 11.00000 0.04938 0.07223 = 0.06260 0.00046 0.02325 0.01285 AFIX 23 H34D 2 0.603116 0.733579 0.508549 11.00000 -1.20000 H34E 2 0.661117 0.781827 0.523391 11.00000 -1.20000 AFIX 0 C350 1 0.628660 0.745830 0.445852 11.00000 0.06538 0.04572 = 0.06203 0.00171 0.01725 0.00129 AFIX 23 H35A 2 0.584545 0.745480 0.423362 11.00000 -1.20000 H35B 2 0.645994 0.787900 0.438618 11.00000 -1.20000 AFIX 0 C360 1 0.657820 0.686388 0.434220 11.00000 0.04565 0.07430 = 0.04369 -0.00050 0.01700 0.00143 AFIX 23 H36A 2 0.627689 0.650293 0.417579 11.00000 -1.20000 H36B 2 0.676436 0.698416 0.409037 11.00000 -1.20000 AFIX 0 C370 1 0.982099 0.613303 0.564616 11.00000 0.05503 0.08366 = 0.06011 0.01362 0.01871 0.01406 AFIX 23 H37A 2 0.971618 0.578428 0.536140 11.00000 -1.20000 H37B 2 0.984650 0.592223 0.598548 11.00000 -1.20000 AFIX 0 C380 1 1.042697 0.649946 0.573013 11.00000 0.03548 0.16515 = 0.05077 -0.01588 0.01395 0.01327 AFIX 23 H38A 2 1.075358 0.638947 0.608605 11.00000 -1.20000 H38B 2 1.056042 0.638201 0.544147 11.00000 -1.20000 AFIX 0 C390 1 1.024514 0.722695 0.569911 11.00000 0.07009 0.11073 = 0.09096 -0.02907 0.02640 -0.01542 AFIX 23 H39A 2 1.029948 0.739760 0.605894 11.00000 -1.20000 H39B 2 1.048742 0.750762 0.555974 11.00000 -1.20000 AFIX 0 C400 1 0.962081 0.723188 0.533411 11.00000 0.07858 0.07246 = 0.12112 -0.00047 0.05466 -0.01717 AFIX 23 H40C 2 0.941353 0.764091 0.538093 11.00000 -1.20000 H40D 2 0.957047 0.720234 0.495381 11.00000 -1.20000 AFIX 0 O170 6 0.506026 0.199820 0.549993 11.00000 0.06205 0.04133 = 0.03884 0.00056 0.01475 0.00329 C410 1 0.489675 0.159165 0.504302 11.00000 0.11353 0.06657 = 0.04605 -0.01281 -0.01077 0.04361 AFIX 23 H41A 2 0.513490 0.171500 0.483464 11.00000 -1.20000 H41B 2 0.446193 0.165061 0.480744 11.00000 -1.20000 AFIX 0 C420 1 0.502116 0.087956 0.522996 11.00000 0.08926 0.05450 = 0.05939 -0.01088 0.01749 -0.00575 AFIX 23 H42A 2 0.464064 0.063611 0.516382 11.00000 -1.20000 H42B 2 0.523938 0.063990 0.504380 11.00000 -1.20000 AFIX 0 C430 1 0.540245 0.093895 0.581631 11.00000 0.08173 0.04605 = 0.05138 0.00789 0.02841 0.00256 AFIX 23 H43A 2 0.532334 0.056433 0.601937 11.00000 -1.20000 H43B 2 0.583778 0.094240 0.588958 11.00000 -1.20000 AFIX 0 C440 1 0.521454 0.158827 0.595912 11.00000 0.05631 0.04556 = 0.04606 0.00205 0.02216 -0.00355 AFIX 23 H44D 2 0.486240 0.152739 0.605131 11.00000 -1.20000 H44E 2 0.554958 0.179222 0.627251 11.00000 -1.20000 AFIX 0 O180 6 0.950159 0.843536 0.435969 11.00000 0.06274 0.05802 = 0.11392 -0.02075 0.02550 -0.01364 C480 1 0.960901 0.910447 0.451977 11.00000 0.05225 0.05185 = 0.08040 -0.00581 0.02072 -0.00118 AFIX 23 H48A 2 0.939258 0.922818 0.474690 11.00000 -1.20000 H48B 2 0.947320 0.940602 0.420138 11.00000 -1.20000 AFIX 0 C470 1 1.027408 0.915613 0.483357 11.00000 0.05078 0.08156 = 0.11417 -0.04661 0.03060 -0.01199 AFIX 23 H47A 2 1.042148 0.961627 0.481431 11.00000 -1.20000 H47B 2 1.039209 0.903269 0.521693 11.00000 -1.20000 AFIX 0 C460 1 1.049553 0.868670 0.457032 11.00000 0.06653 0.06409 = 0.19489 -0.02330 0.06603 -0.00450 AFIX 23 H46A 2 1.086202 0.846095 0.483383 11.00000 -1.20000 H46B 2 1.060054 0.891441 0.429564 11.00000 -1.20000 AFIX 0 C450 1 1.001488 0.819917 0.431533 11.00000 0.11170 0.04917 = 0.09099 -0.01634 0.06934 -0.01462 AFIX 23 H45A 2 0.993812 0.814355 0.393011 11.00000 -1.20000 H45B 2 1.013217 0.775647 0.449636 11.00000 -1.20000 AFIX 0 HKLF 4 REM mini-21065 REM R1 = 0.0725 for 20016 Fo > 4sig(Fo) and 0.0889 for all 24308 data REM 1305 parameters refined using 0 restraints END WGHT 0.0836 12.1841 REM Highest difference peak 0.967, deepest hole -0.597, 1-sigma level 0.069 Q1 1 1.0369 0.5916 0.5707 11.00000 0.05 0.86 Q2 1 0.7232 0.3978 0.1964 11.00000 0.05 0.82 Q3 1 0.8623 0.3169 0.4998 11.00000 0.05 0.73 Q4 1 1.0305 0.8227 0.5084 11.00000 0.05 0.72 Q5 1 0.3762 0.5486 0.2422 11.00000 0.05 0.71 Q6 1 1.0521 0.8481 0.4959 11.00000 0.05 0.56 Q7 1 0.8212 0.5487 0.1915 11.00000 0.05 0.54 Q8 1 0.4494 0.1473 0.5070 11.00000 0.05 0.46 Q9 1 0.9907 0.7052 0.5787 11.00000 0.05 0.46 Q10 1 0.4799 0.6033 0.3609 11.00000 0.05 0.42 Q11 1 0.9908 0.7924 0.4653 11.00000 0.05 0.41 Q12 1 0.4824 0.0770 0.5593 11.00000 0.05 0.38 Q13 1 0.7714 0.4465 0.2520 11.00000 0.05 0.38 Q14 1 0.6433 0.1764 0.5921 11.00000 0.05 0.37 Q15 1 0.2872 0.5521 0.1952 11.00000 0.05 0.36 Q16 1 0.4673 0.1089 0.5140 11.00000 0.05 0.35 Q17 1 0.9593 0.5841 0.1125 11.00000 0.05 0.35 Q18 1 1.0384 0.6818 0.5484 11.00000 0.05 0.35 Q19 1 0.8661 0.6787 0.5452 11.00000 0.05 0.35 Q20 1 0.8983 0.5839 0.2680 11.00000 0.05 0.35 ; _shelx_res_checksum 27031 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-22141 _database_code_depnum_ccdc_archive 'CCDC 2226342' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C35 H57 Fe N4 Si2' _chemical_formula_sum 'C35 H57 Fe N4 Si2' _chemical_formula_weight 645.87 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 10.6104(5) _cell_length_b 20.3504(8) _cell_length_c 17.3268(8) _cell_angle_alpha 90 _cell_angle_beta 95.909(4) _cell_angle_gamma 90 _cell_volume 3721.4(3) _cell_formula_units_Z 4 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 26108 _cell_measurement_theta_min 4.7260 _cell_measurement_theta_max 67.0760 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.153 _exptl_crystal_F_000 1396 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.020 _exptl_absorpt_coefficient_mu 4.065 _shelx_estimated_absorpt_T_min 0.497 _shelx_estimated_absorpt_T_max 0.923 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.84505 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 6549 _diffrn_reflns_av_unetI/netI 0.0482 _diffrn_reflns_av_R_equivalents 0.1175 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 3.360 _diffrn_reflns_theta_max 66.652 _diffrn_reflns_theta_full 66.652 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 0.995 _reflns_number_total 6549 _reflns_number_gt 4992 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. The hydrazido-disilyl group is present in partial occupancy. The site occupancy factors (SOFs) for atoms Si1a, Si2a N1a, N2a, C30a, C31a were freely refined and converged near a value of 0.75. These SOFs were subsequently fixed at 0.75. The minor component was modeled at SOFs of 0.25, the chemical nature of this species requires additional work to characterize. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0967P)^2^+9.3780P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6549 _refine_ls_number_parameters 436 _refine_ls_number_restraints 6 _refine_ls_R_factor_all 0.1047 _refine_ls_R_factor_gt 0.0819 _refine_ls_wR_factor_ref 0.2464 _refine_ls_wR_factor_gt 0.2318 _refine_ls_goodness_of_fit_ref 1.087 _refine_ls_restrained_S_all 1.087 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.45983(8) 0.25149(4) 0.65531(5) 0.0318(3) Uani 1 1 d . . . . . Si1A Si 0.5394(4) 0.32083(18) 0.8803(2) 0.0352(8) Uani 0.75 1 d . . P A 1 Si1B Si 0.5417(13) 0.3282(6) 0.8477(6) 0.039(2) Uani 0.25 1 d . . P A 2 Si2A Si 0.4246(3) 0.18550(15) 0.87788(19) 0.0377(7) Uani 0.75 1 d . . P A 1 Si2B Si 0.3934(11) 0.1758(5) 0.8426(7) 0.051(3) Uani 0.25 1 d . . P A 2 N1 N 0.4395(4) 0.3203(2) 0.5799(3) 0.0277(10) Uani 1 1 d . . . . . N2 N 0.4875(4) 0.1860(2) 0.5793(3) 0.0302(10) Uani 1 1 d . . . . . N3A N 0.4663(7) 0.2519(4) 0.7463(6) 0.035(2) Uani 0.75 1 d . . P A 1 N3B N 0.484(2) 0.2821(12) 0.7641(13) 0.034(4) Uani 0.25 1 d . U P A 2 N4A N 0.4750(6) 0.2532(3) 0.8244(4) 0.0350(14) Uani 0.75 1 d . . P A 1 N4B N 0.441(2) 0.2234(12) 0.7591(14) 0.034(4) Uani 0.25 1 d . U P A 2 C1 C 0.3998(6) 0.3742(3) 0.4518(4) 0.0378(14) Uani 1 1 d . . . . . H1A H 0.3243 0.3962 0.4675 0.057 Uiso 1 1 calc R U . . . H1B H 0.3840 0.3605 0.3974 0.057 Uiso 1 1 calc R U . . . H1C H 0.4717 0.4046 0.4576 0.057 Uiso 1 1 calc R U . . . C2 C 0.4297(5) 0.3145(2) 0.5024(3) 0.0286(12) Uani 1 1 d . . . . . C3 C 0.4512(5) 0.2545(2) 0.4662(3) 0.0285(11) Uani 1 1 d . . . . . H3 H 0.4417 0.2546 0.4110 0.034 Uiso 1 1 calc R U . . . C4 C 0.4854(5) 0.1943(3) 0.5021(3) 0.0304(12) Uani 1 1 d . . . . . C5 C 0.5231(6) 0.1383(3) 0.4513(4) 0.0402(14) Uani 1 1 d . . . . . H5A H 0.6100 0.1246 0.4685 0.060 Uiso 1 1 calc R U . . . H5B H 0.5183 0.1530 0.3972 0.060 Uiso 1 1 calc R U . . . H5C H 0.4654 0.1012 0.4554 0.060 Uiso 1 1 calc R U . . . C6 C 0.4436(5) 0.3857(3) 0.6125(3) 0.0290(12) Uani 1 1 d . . . . . C7 C 0.5596(5) 0.4209(3) 0.6167(3) 0.0296(12) Uani 1 1 d . . . . . C8 C 0.5677(6) 0.4806(3) 0.6560(3) 0.0340(13) Uani 1 1 d . . . . . H8 H 0.6452 0.5043 0.6602 0.041 Uiso 1 1 calc R U . . . C9 C 0.4647(6) 0.5063(3) 0.6893(4) 0.0380(14) Uani 1 1 d . . . . . H9 H 0.4724 0.5468 0.7166 0.046 Uiso 1 1 calc R U . . . C10 C 0.3505(6) 0.4726(3) 0.6825(3) 0.0366(13) Uani 1 1 d . . . . . H10 H 0.2799 0.4907 0.7045 0.044 Uiso 1 1 calc R U . . . C11 C 0.3374(5) 0.4120(3) 0.6435(4) 0.0344(13) Uani 1 1 d . . . . . C12 C 0.6746(5) 0.3940(3) 0.5798(3) 0.0306(12) Uani 1 1 d . . . . . H12 H 0.6420 0.3609 0.5400 0.037 Uiso 1 1 calc R U . . . C13 C 0.7441(6) 0.4470(3) 0.5374(4) 0.0411(15) Uani 1 1 d . . . . . H13A H 0.6835 0.4699 0.5002 0.062 Uiso 1 1 calc R U . . . H13B H 0.8098 0.4265 0.5097 0.062 Uiso 1 1 calc R U . . . H13C H 0.7833 0.4787 0.5752 0.062 Uiso 1 1 calc R U . . . C14 C 0.7652(6) 0.3576(3) 0.6403(4) 0.0371(13) Uani 1 1 d . . . . . H14A H 0.8044 0.3891 0.6781 0.056 Uiso 1 1 calc R U . . . H14B H 0.8313 0.3355 0.6143 0.056 Uiso 1 1 calc R U . . . H14C H 0.7176 0.3248 0.6669 0.056 Uiso 1 1 calc R U . . . C15 C 0.2094(5) 0.3777(3) 0.6350(4) 0.0378(14) Uani 1 1 d . . . . . H15 H 0.2159 0.3388 0.6004 0.045 Uiso 1 1 calc R U . . . C16 C 0.1075(6) 0.4238(4) 0.5955(5) 0.0570(19) Uani 1 1 d . . . . . H16A H 0.0989 0.4624 0.6284 0.086 Uiso 1 1 calc R U . . . H16B H 0.0263 0.4005 0.5878 0.086 Uiso 1 1 calc R U . . . H16C H 0.1323 0.4379 0.5451 0.086 Uiso 1 1 calc R U . . . C17 C 0.1693(6) 0.3531(3) 0.7123(4) 0.0493(17) Uani 1 1 d . . . . . H17A H 0.2343 0.3233 0.7366 0.074 Uiso 1 1 calc R U . . . H17B H 0.0885 0.3296 0.7031 0.074 Uiso 1 1 calc R U . . . H17C H 0.1596 0.3905 0.7467 0.074 Uiso 1 1 calc R U . . . C18 C 0.5201(5) 0.1218(3) 0.6117(3) 0.0315(12) Uani 1 1 d . . . . . C19 C 0.4272(6) 0.0718(3) 0.6091(3) 0.0350(13) Uani 1 1 d . . . . . C20 C 0.4581(7) 0.0120(3) 0.6465(4) 0.0413(15) Uani 1 1 d . . . . . H20 H 0.3957 -0.0215 0.6469 0.050 Uiso 1 1 calc R U . . . C21 C 0.5783(7) 0.0013(3) 0.6829(4) 0.0446(16) Uani 1 1 d . . . . . H21 H 0.5979 -0.0395 0.7082 0.054 Uiso 1 1 calc R U . . . C22 C 0.6702(7) 0.0493(3) 0.6829(4) 0.0438(16) Uani 1 1 d . . . . . H22 H 0.7529 0.0409 0.7074 0.053 Uiso 1 1 calc R U . . . C23 C 0.6433(6) 0.1103(3) 0.6474(3) 0.0367(14) Uani 1 1 d . . . . . C24 C 0.2939(6) 0.0817(3) 0.5691(4) 0.0409(15) Uani 1 1 d . . . . . H24 H 0.2947 0.1219 0.5360 0.049 Uiso 1 1 calc R U . . . C25 C 0.2519(7) 0.0230(3) 0.5152(4) 0.0543(18) Uani 1 1 d . . . . . H25A H 0.3143 0.0161 0.4780 0.081 Uiso 1 1 calc R U . . . H25B H 0.1691 0.0325 0.4871 0.081 Uiso 1 1 calc R U . . . H25C H 0.2460 -0.0168 0.5465 0.081 Uiso 1 1 calc R U . . . C26 C 0.2017(7) 0.0937(4) 0.6293(5) 0.064(2) Uani 1 1 d . . . . . H26A H 0.2071 0.0573 0.6666 0.096 Uiso 1 1 calc R U . . . H26B H 0.1152 0.0964 0.6035 0.096 Uiso 1 1 calc R U . . . H26C H 0.2234 0.1349 0.6566 0.096 Uiso 1 1 calc R U . . . C27 C 0.7461(6) 0.1631(3) 0.6498(4) 0.0423(15) Uani 1 1 d . . . . . H27 H 0.7090 0.2028 0.6220 0.051 Uiso 1 1 calc R U . . . C28 C 0.8580(7) 0.1393(4) 0.6074(5) 0.063(2) Uani 1 1 d . . . . . H28A H 0.8946 0.0997 0.6329 0.095 Uiso 1 1 calc R U . . . H28B H 0.9227 0.1738 0.6091 0.095 Uiso 1 1 calc R U . . . H28C H 0.8282 0.1293 0.5533 0.095 Uiso 1 1 calc R U . . . C29 C 0.7917(7) 0.1829(4) 0.7327(4) 0.0562(18) Uani 1 1 d . . . . . H29A H 0.7196 0.1985 0.7587 0.084 Uiso 1 1 calc R U . . . H29B H 0.8545 0.2182 0.7320 0.084 Uiso 1 1 calc R U . . . H29C H 0.8302 0.1449 0.7607 0.084 Uiso 1 1 calc R U . . . C30A C 0.5726(9) 0.2736(4) 0.9734(5) 0.0418(19) Uani 0.75 1 d . . P A 1 H30A H 0.6546 0.2503 0.9743 0.050 Uiso 0.75 1 calc R U P A 1 H30B H 0.5770 0.3040 1.0182 0.050 Uiso 0.75 1 calc R U P A 1 C30B C 0.561(3) 0.2642(13) 0.9273(17) 0.0418(19) Uani 0.25 1 d . . P A 2 H30C H 0.6284 0.2331 0.9160 0.050 Uiso 0.25 1 calc R U P A 2 H30D H 0.5889 0.2862 0.9771 0.050 Uiso 0.25 1 calc R U P A 2 C31 C 0.4204(7) 0.3866(3) 0.8829(4) 0.0493(17) Uani 1 1 d . . . . . H31A H 0.4083 0.4084 0.8322 0.074 Uiso 0.75 1 calc R U P A 1 H31B H 0.4497 0.4187 0.9228 0.074 Uiso 0.75 1 calc R U P A 1 H31C H 0.3398 0.3676 0.8949 0.074 Uiso 0.75 1 calc R U P A 1 H31D H 0.4565 0.4083 0.9306 0.074 Uiso 0.25 1 calc R U P A 2 H31E H 0.3447 0.3619 0.8933 0.074 Uiso 0.25 1 calc R U P A 2 H31F H 0.3972 0.4198 0.8429 0.074 Uiso 0.25 1 calc R U P A 2 C31A C 0.4632(9) 0.2233(4) 0.9783(5) 0.043(2) Uani 0.75 1 d . . P A 1 H31G H 0.3876 0.2456 0.9948 0.052 Uiso 0.75 1 calc R U P A 1 H31H H 0.4896 0.1886 1.0166 0.052 Uiso 0.75 1 calc R U P A 1 C31B C 0.443(3) 0.2268(14) 0.9359(17) 0.043(2) Uani 0.25 1 d . . P A 2 H31I H 0.3745 0.2576 0.9455 0.052 Uiso 0.25 1 calc R U P A 2 H31J H 0.4575 0.1969 0.9810 0.052 Uiso 0.25 1 calc R U P A 2 C32 C 0.6817(7) 0.3571(4) 0.8380(4) 0.0547(18) Uani 1 1 d . . . . . H32A H 0.7434 0.3223 0.8311 0.082 Uiso 0.75 1 calc R U P A 1 H32B H 0.7209 0.3906 0.8734 0.082 Uiso 0.75 1 calc R U P A 1 H32C H 0.6545 0.3773 0.7877 0.082 Uiso 0.75 1 calc R U P A 1 H32D H 0.6740 0.4018 0.8168 0.082 Uiso 0.25 1 calc R U P A 2 H32E H 0.7238 0.3290 0.8026 0.082 Uiso 0.25 1 calc R U P A 2 H32F H 0.7319 0.3582 0.8887 0.082 Uiso 0.25 1 calc R U P A 2 C33 C 0.2463(8) 0.1703(4) 0.8494(5) 0.070(2) Uani 1 1 d . . . . . H33A H 0.1986 0.2103 0.8586 0.106 Uiso 0.75 1 calc R U P A 1 H33B H 0.2173 0.1343 0.8809 0.106 Uiso 0.75 1 calc R U P A 1 H33C H 0.2324 0.1584 0.7944 0.106 Uiso 0.75 1 calc R U P A 1 H33D H 0.1993 0.1819 0.7996 0.106 Uiso 0.25 1 calc R U P A 2 H33E H 0.2228 0.2003 0.8898 0.106 Uiso 0.25 1 calc R U P A 2 H33F H 0.2255 0.1251 0.8631 0.106 Uiso 0.25 1 calc R U P A 2 C34 C 0.5125(9) 0.1086(4) 0.8578(4) 0.065(2) Uani 1 1 d . . . . . H34A H 0.4806 0.0914 0.8067 0.098 Uiso 0.75 1 calc R U P A 1 H34B H 0.4999 0.0757 0.8976 0.098 Uiso 0.75 1 calc R U P A 1 H34C H 0.6031 0.1184 0.8587 0.098 Uiso 0.75 1 calc R U P A 1 H34D H 0.4727 0.0696 0.8781 0.098 Uiso 0.25 1 calc R U P A 2 H34E H 0.5829 0.1230 0.8951 0.098 Uiso 0.25 1 calc R U P A 2 H34F H 0.5446 0.0978 0.8083 0.098 Uiso 0.25 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0397(5) 0.0199(4) 0.0370(5) 0.0015(4) 0.0090(4) 0.0012(4) Si1A 0.0467(15) 0.0274(14) 0.033(2) -0.0018(16) 0.0117(18) 0.0002(10) Si1B 0.056(5) 0.033(5) 0.028(6) -0.002(5) 0.012(5) -0.008(3) Si2A 0.0476(16) 0.0276(15) 0.0401(18) 0.0021(13) 0.0146(14) -0.0037(11) Si2B 0.074(7) 0.034(5) 0.046(6) -0.014(5) 0.016(5) -0.023(4) N1 0.030(2) 0.020(2) 0.034(3) 0.0004(19) 0.0072(19) 0.0006(17) N2 0.032(2) 0.018(2) 0.041(3) 0.005(2) 0.007(2) 0.0029(18) N3A 0.037(5) 0.016(5) 0.053(5) 0.001(4) 0.004(3) -0.003(4) N3B 0.037(9) 0.036(12) 0.030(8) -0.018(8) 0.016(6) -0.017(8) N4A 0.041(4) 0.025(3) 0.039(4) -0.001(3) 0.009(3) 0.001(3) N4B 0.038(9) 0.036(12) 0.031(8) -0.018(8) 0.015(6) -0.016(8) C1 0.050(4) 0.023(3) 0.040(4) 0.004(3) 0.000(3) 0.002(2) C2 0.032(3) 0.017(2) 0.037(3) 0.002(2) 0.003(2) -0.002(2) C3 0.037(3) 0.021(3) 0.027(3) 0.003(2) 0.002(2) -0.002(2) C4 0.035(3) 0.017(3) 0.039(3) -0.002(2) 0.006(2) 0.000(2) C5 0.048(4) 0.029(3) 0.045(4) -0.003(3) 0.010(3) 0.009(3) C6 0.036(3) 0.025(3) 0.027(3) 0.002(2) 0.004(2) 0.001(2) C7 0.034(3) 0.025(3) 0.031(3) 0.004(2) 0.006(2) 0.000(2) C8 0.042(3) 0.026(3) 0.034(3) -0.001(2) 0.006(3) -0.008(2) C9 0.047(3) 0.028(3) 0.040(3) -0.004(3) 0.008(3) -0.003(3) C10 0.042(3) 0.033(3) 0.036(3) 0.000(3) 0.012(3) 0.006(3) C11 0.039(3) 0.024(3) 0.041(3) 0.002(2) 0.010(3) -0.001(2) C12 0.038(3) 0.028(3) 0.026(3) 0.000(2) 0.008(2) -0.005(2) C13 0.046(4) 0.039(3) 0.040(4) 0.005(3) 0.014(3) -0.002(3) C14 0.040(3) 0.032(3) 0.040(3) 0.004(3) 0.009(3) 0.002(2) C15 0.036(3) 0.031(3) 0.048(4) -0.001(3) 0.011(3) -0.002(2) C16 0.042(4) 0.052(4) 0.077(5) 0.007(4) 0.003(4) -0.003(3) C17 0.041(4) 0.044(4) 0.064(5) 0.007(3) 0.014(3) -0.002(3) C18 0.042(3) 0.017(3) 0.036(3) -0.002(2) 0.008(2) 0.006(2) C19 0.049(3) 0.022(3) 0.035(3) 0.000(2) 0.010(3) 0.005(2) C20 0.065(4) 0.024(3) 0.037(3) -0.003(3) 0.011(3) 0.006(3) C21 0.068(4) 0.028(3) 0.039(4) 0.004(3) 0.008(3) 0.020(3) C22 0.058(4) 0.040(4) 0.034(4) 0.002(3) 0.005(3) 0.020(3) C23 0.046(3) 0.033(3) 0.032(3) -0.002(3) 0.007(3) 0.009(3) C24 0.050(4) 0.033(3) 0.041(4) 0.011(3) 0.010(3) -0.002(3) C25 0.066(5) 0.033(4) 0.061(5) 0.008(3) -0.003(4) -0.014(3) C26 0.055(4) 0.074(6) 0.065(5) 0.014(4) 0.022(4) 0.014(4) C27 0.041(3) 0.042(4) 0.044(4) 0.003(3) 0.002(3) 0.009(3) C28 0.050(4) 0.079(6) 0.063(5) -0.005(4) 0.017(4) 0.005(4) C29 0.057(4) 0.063(5) 0.047(4) 0.000(4) -0.007(3) -0.001(4) C30A 0.056(5) 0.035(4) 0.035(5) -0.001(4) 0.007(5) 0.003(3) C30B 0.056(5) 0.035(4) 0.035(5) -0.001(4) 0.007(5) 0.003(3) C31 0.058(4) 0.035(3) 0.055(4) -0.005(3) 0.007(3) 0.003(3) C31A 0.064(5) 0.036(4) 0.031(5) 0.019(5) 0.016(5) 0.000(4) C31B 0.064(5) 0.036(4) 0.031(5) 0.019(5) 0.016(5) 0.000(4) C32 0.062(4) 0.064(5) 0.039(4) -0.009(3) 0.011(3) -0.005(4) C33 0.078(6) 0.060(5) 0.078(6) 0.014(4) 0.033(5) -0.006(4) C34 0.098(6) 0.055(5) 0.048(5) 0.012(4) 0.030(4) 0.020(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N3A 1.571(11) . ? Fe1 N1 1.912(4) . ? Fe1 N4B 1.92(2) . ? Fe1 N2 1.917(5) . ? Fe1 N3B 1.98(2) . ? Si1A N4A 1.779(7) . ? Si1A C31 1.844(8) . ? Si1A C30A 1.881(9) . ? Si1A C32 1.894(8) . ? Si1B C32 1.623(14) . ? Si1B N3B 1.78(2) . ? Si1B C30B 1.89(3) . ? Si1B C31 1.898(15) . ? Si2A N4A 1.773(7) . ? Si2A C34 1.873(8) . ? Si2A C31A 1.908(10) . ? Si2A C33 1.930(9) . ? Si2B C33 1.581(14) . ? Si2B N4B 1.86(3) . ? Si2B C34 1.863(14) . ? Si2B C31B 1.95(3) . ? N1 C2 1.343(7) . ? N1 C6 1.444(7) . ? N2 C4 1.347(8) . ? N2 C18 1.451(7) . ? N3A N4A 1.348(12) . ? N3B N4B 1.28(3) . ? C1 C2 1.513(7) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C2 C3 1.402(7) . ? C3 C4 1.405(7) . ? C3 H3 0.9500 . ? C4 C5 1.518(7) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C11 1.404(8) . ? C6 C7 1.420(8) . ? C7 C8 1.390(8) . ? C7 C12 1.536(8) . ? C8 C9 1.389(8) . ? C8 H8 0.9500 . ? C9 C10 1.387(8) . ? C9 H9 0.9500 . ? C10 C11 1.405(8) . ? C10 H10 0.9500 . ? C11 C15 1.521(8) . ? C12 C13 1.536(8) . ? C12 C14 1.537(8) . ? C12 H12 1.0000 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C17 1.532(9) . ? C15 C16 1.537(9) . ? C15 H15 1.0000 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 C23 1.406(8) . ? C18 C19 1.413(8) . ? C19 C20 1.402(8) . ? C19 C24 1.524(9) . ? C20 C21 1.380(9) . ? C20 H20 0.9500 . ? C21 C22 1.381(10) . ? C21 H21 0.9500 . ? C22 C23 1.403(8) . ? C22 H22 0.9500 . ? C23 C27 1.528(9) . ? C24 C26 1.522(9) . ? C24 C25 1.553(9) . ? C24 H24 1.0000 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 C29 1.523(10) . ? C27 C28 1.537(9) . ? C27 H27 1.0000 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30A C31A 1.557(12) . ? C30A H30A 0.9900 . ? C30A H30B 0.9900 . ? C30B C31B 1.48(4) . ? C30B H30C 0.9900 . ? C30B H30D 0.9900 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C31 H31D 0.9800 . ? C31 H31E 0.9800 . ? C31 H31F 0.9800 . ? C31A H31G 0.9900 . ? C31A H31H 0.9900 . ? C31B H31I 0.9900 . ? C31B H31J 0.9900 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C32 H32D 0.9800 . ? C32 H32E 0.9800 . ? C32 H32F 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C33 H33D 0.9800 . ? C33 H33E 0.9800 . ? C33 H33F 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C34 H34D 0.9800 . ? C34 H34E 0.9800 . ? C34 H34F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Fe1 N1 132.2(3) . . ? N1 Fe1 N4B 147.6(8) . . ? N3A Fe1 N2 134.4(3) . . ? N1 Fe1 N2 93.12(19) . . ? N4B Fe1 N2 118.4(7) . . ? N1 Fe1 N3B 114.5(7) . . ? N4B Fe1 N3B 38.3(10) . . ? N2 Fe1 N3B 149.3(8) . . ? N4A Si1A C31 110.4(4) . . ? N4A Si1A C30A 95.6(4) . . ? C31 Si1A C30A 114.7(4) . . ? N4A Si1A C32 111.6(3) . . ? C31 Si1A C32 107.6(4) . . ? C30A Si1A C32 116.4(4) . . ? C32 Si1B N3B 110.3(9) . . ? C32 Si1B C30B 107.1(12) . . ? N3B Si1B C30B 103.4(13) . . ? C32 Si1B C31 117.7(8) . . ? N3B Si1B C31 113.9(11) . . ? C30B Si1B C31 102.9(10) . . ? N4A Si2A C34 111.7(3) . . ? N4A Si2A C31A 96.6(4) . . ? C34 Si2A C31A 116.2(4) . . ? N4A Si2A C33 109.4(4) . . ? C34 Si2A C33 108.2(4) . . ? C31A Si2A C33 114.2(4) . . ? C33 Si2B N4B 116.6(11) . . ? C33 Si2B C34 126.7(7) . . ? N4B Si2B C34 104.9(10) . . ? C33 Si2B C31B 99.4(11) . . ? N4B Si2B C31B 107.2(11) . . ? C34 Si2B C31B 98.7(11) . . ? C2 N1 C6 117.9(4) . . ? C2 N1 Fe1 127.7(3) . . ? C6 N1 Fe1 114.3(4) . . ? C4 N2 C18 118.5(5) . . ? C4 N2 Fe1 127.4(4) . . ? C18 N2 Fe1 114.1(4) . . ? N4A N3A Fe1 178.3(7) . . ? N4B N3B Si1B 130(2) . . ? N4B N3B Fe1 68.3(15) . . ? Si1B N3B Fe1 160.5(14) . . ? N3A N4A Si2A 121.1(6) . . ? N3A N4A Si1A 123.0(6) . . ? Si2A N4A Si1A 115.9(4) . . ? N3B N4B Si2B 124.0(18) . . ? N3B N4B Fe1 73.5(15) . . ? Si2B N4B Fe1 161.9(14) . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? H1A C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? N1 C2 C3 121.7(5) . . ? N1 C2 C1 120.0(5) . . ? C3 C2 C1 118.3(5) . . ? C2 C3 C4 127.4(5) . . ? C2 C3 H3 116.3 . . ? C4 C3 H3 116.3 . . ? N2 C4 C3 121.8(5) . . ? N2 C4 C5 120.2(5) . . ? C3 C4 C5 118.0(5) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C11 C6 C7 120.9(5) . . ? C11 C6 N1 120.6(5) . . ? C7 C6 N1 118.4(5) . . ? C8 C7 C6 118.3(5) . . ? C8 C7 C12 120.3(5) . . ? C6 C7 C12 121.3(5) . . ? C9 C8 C7 121.4(5) . . ? C9 C8 H8 119.3 . . ? C7 C8 H8 119.3 . . ? C10 C9 C8 119.7(6) . . ? C10 C9 H9 120.1 . . ? C8 C9 H9 120.1 . . ? C9 C10 C11 121.1(5) . . ? C9 C10 H10 119.4 . . ? C11 C10 H10 119.4 . . ? C6 C11 C10 118.4(5) . . ? C6 C11 C15 122.1(5) . . ? C10 C11 C15 119.5(5) . . ? C7 C12 C13 112.9(5) . . ? C7 C12 C14 110.8(5) . . ? C13 C12 C14 111.6(5) . . ? C7 C12 H12 107.1 . . ? C13 C12 H12 107.1 . . ? C14 C12 H12 107.1 . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C12 C14 H14A 109.5 . . ? C12 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C12 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C11 C15 C17 113.0(5) . . ? C11 C15 C16 110.1(5) . . ? C17 C15 C16 110.1(5) . . ? C11 C15 H15 107.8 . . ? C17 C15 H15 107.8 . . ? C16 C15 H15 107.8 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C15 C17 H17A 109.5 . . ? C15 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C15 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C23 C18 C19 120.6(5) . . ? C23 C18 N2 119.5(5) . . ? C19 C18 N2 119.9(5) . . ? C20 C19 C18 118.7(6) . . ? C20 C19 C24 119.1(5) . . ? C18 C19 C24 122.1(5) . . ? C21 C20 C19 120.6(6) . . ? C21 C20 H20 119.7 . . ? C19 C20 H20 119.7 . . ? C20 C21 C22 120.5(6) . . ? C20 C21 H21 119.8 . . ? C22 C21 H21 119.8 . . ? C21 C22 C23 121.0(6) . . ? C21 C22 H22 119.5 . . ? C23 C22 H22 119.5 . . ? C22 C23 C18 118.5(6) . . ? C22 C23 C27 119.8(6) . . ? C18 C23 C27 121.6(5) . . ? C26 C24 C19 109.9(6) . . ? C26 C24 C25 111.8(6) . . ? C19 C24 C25 111.6(5) . . ? C26 C24 H24 107.8 . . ? C19 C24 H24 107.8 . . ? C25 C24 H24 107.8 . . ? C24 C25 H25A 109.5 . . ? C24 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C24 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C24 C26 H26A 109.5 . . ? C24 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C24 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C29 C27 C23 111.6(6) . . ? C29 C27 C28 110.4(6) . . ? C23 C27 C28 110.5(6) . . ? C29 C27 H27 108.1 . . ? C23 C27 H27 108.1 . . ? C28 C27 H27 108.1 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C27 C29 H29A 109.5 . . ? C27 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C27 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C31A C30A Si1A 108.0(6) . . ? C31A C30A H30A 110.1 . . ? Si1A C30A H30A 110.1 . . ? C31A C30A H30B 110.1 . . ? Si1A C30A H30B 110.1 . . ? H30A C30A H30B 108.4 . . ? C31B C30B Si1B 113(2) . . ? C31B C30B H30C 108.9 . . ? Si1B C30B H30C 108.9 . . ? C31B C30B H30D 108.9 . . ? Si1B C30B H30D 108.9 . . ? H30C C30B H30D 107.7 . . ? Si1A C31 H31A 109.5 . . ? Si1A C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? Si1A C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? Si1B C31 H31D 109.5 . . ? Si1B C31 H31E 109.5 . . ? H31D C31 H31E 109.5 . . ? Si1B C31 H31F 109.5 . . ? H31D C31 H31F 109.5 . . ? H31E C31 H31F 109.5 . . ? C30A C31A Si2A 107.9(6) . . ? C30A C31A H31G 110.1 . . ? Si2A C31A H31G 110.1 . . ? C30A C31A H31H 110.1 . . ? Si2A C31A H31H 110.1 . . ? H31G C31A H31H 108.4 . . ? C30B C31B Si2B 110.5(19) . . ? C30B C31B H31I 109.5 . . ? Si2B C31B H31I 109.5 . . ? C30B C31B H31J 109.5 . . ? Si2B C31B H31J 109.5 . . ? H31I C31B H31J 108.1 . . ? Si1A C32 H32A 109.5 . . ? Si1A C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? Si1A C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? Si1B C32 H32D 109.5 . . ? Si1B C32 H32E 109.5 . . ? H32D C32 H32E 109.5 . . ? Si1B C32 H32F 109.5 . . ? H32D C32 H32F 109.5 . . ? H32E C32 H32F 109.5 . . ? Si2A C33 H33A 109.5 . . ? Si2A C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? Si2A C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? Si2B C33 H33D 109.5 . . ? Si2B C33 H33E 109.5 . . ? H33D C33 H33E 109.5 . . ? Si2B C33 H33F 109.5 . . ? H33D C33 H33F 109.5 . . ? H33E C33 H33F 109.5 . . ? Si2A C34 H34A 109.5 . . ? Si2A C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? Si2A C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? Si2B C34 H34D 109.5 . . ? Si2B C34 H34E 109.5 . . ? H34D C34 H34E 109.5 . . ? Si2B C34 H34F 109.5 . . ? H34D C34 H34F 109.5 . . ? H34E C34 H34F 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C32 Si1B N3B N4B 127(2) . . . . ? C30B Si1B N3B N4B 13(3) . . . . ? C31 Si1B N3B N4B -98(3) . . . . ? C32 Si1B N3B Fe1 -27(5) . . . . ? C30B Si1B N3B Fe1 -141(4) . . . . ? C31 Si1B N3B Fe1 108(4) . . . . ? C34 Si2A N4A N3A 59.1(7) . . . . ? C31A Si2A N4A N3A -179.3(6) . . . . ? C33 Si2A N4A N3A -60.7(7) . . . . ? C34 Si2A N4A Si1A -119.8(5) . . . . ? C31A Si2A N4A Si1A 1.8(5) . . . . ? C33 Si2A N4A Si1A 120.4(5) . . . . ? C31 Si1A N4A N3A 80.6(7) . . . . ? C30A Si1A N4A N3A -160.4(6) . . . . ? C32 Si1A N4A N3A -39.0(7) . . . . ? C31 Si1A N4A Si2A -100.5(4) . . . . ? C30A Si1A N4A Si2A 18.5(5) . . . . ? C32 Si1A N4A Si2A 139.9(4) . . . . ? Si1B N3B N4B Si2B 15(4) . . . . ? Fe1 N3B N4B Si2B -175(2) . . . . ? Si1B N3B N4B Fe1 -171(2) . . . . ? C33 Si2B N4B N3B 102(3) . . . . ? C34 Si2B N4B N3B -112(2) . . . . ? C31B Si2B N4B N3B -8(3) . . . . ? C33 Si2B N4B Fe1 -61(5) . . . . ? C34 Si2B N4B Fe1 85(5) . . . . ? C31B Si2B N4B Fe1 -171(5) . . . . ? C6 N1 C2 C3 166.6(5) . . . . ? Fe1 N1 C2 C3 -9.2(7) . . . . ? C6 N1 C2 C1 -10.9(7) . . . . ? Fe1 N1 C2 C1 173.4(4) . . . . ? N1 C2 C3 C4 -0.4(9) . . . . ? C1 C2 C3 C4 177.1(5) . . . . ? C18 N2 C4 C3 178.2(5) . . . . ? Fe1 N2 C4 C3 -5.1(8) . . . . ? C18 N2 C4 C5 -3.1(8) . . . . ? Fe1 N2 C4 C5 173.5(4) . . . . ? C2 C3 C4 N2 7.8(9) . . . . ? C2 C3 C4 C5 -170.9(5) . . . . ? C2 N1 C6 C11 105.0(6) . . . . ? Fe1 N1 C6 C11 -78.7(6) . . . . ? C2 N1 C6 C7 -79.0(6) . . . . ? Fe1 N1 C6 C7 97.3(5) . . . . ? C11 C6 C7 C8 3.4(8) . . . . ? N1 C6 C7 C8 -172.7(5) . . . . ? C11 C6 C7 C12 -177.3(5) . . . . ? N1 C6 C7 C12 6.7(8) . . . . ? C6 C7 C8 C9 -1.2(8) . . . . ? C12 C7 C8 C9 179.4(5) . . . . ? C7 C8 C9 C10 -1.0(9) . . . . ? C8 C9 C10 C11 1.1(9) . . . . ? C7 C6 C11 C10 -3.2(8) . . . . ? N1 C6 C11 C10 172.7(5) . . . . ? C7 C6 C11 C15 175.6(5) . . . . ? N1 C6 C11 C15 -8.4(9) . . . . ? C9 C10 C11 C6 1.0(9) . . . . ? C9 C10 C11 C15 -177.9(6) . . . . ? C8 C7 C12 C13 -42.7(7) . . . . ? C6 C7 C12 C13 137.9(6) . . . . ? C8 C7 C12 C14 83.2(6) . . . . ? C6 C7 C12 C14 -96.1(6) . . . . ? C6 C11 C15 C17 113.3(7) . . . . ? C10 C11 C15 C17 -67.8(7) . . . . ? C6 C11 C15 C16 -123.1(6) . . . . ? C10 C11 C15 C16 55.7(8) . . . . ? C4 N2 C18 C23 100.7(6) . . . . ? Fe1 N2 C18 C23 -76.4(6) . . . . ? C4 N2 C18 C19 -81.0(7) . . . . ? Fe1 N2 C18 C19 101.9(5) . . . . ? C23 C18 C19 C20 3.6(8) . . . . ? N2 C18 C19 C20 -174.7(5) . . . . ? C23 C18 C19 C24 -178.3(5) . . . . ? N2 C18 C19 C24 3.4(8) . . . . ? C18 C19 C20 C21 -2.3(9) . . . . ? C24 C19 C20 C21 179.6(6) . . . . ? C19 C20 C21 C22 -0.1(9) . . . . ? C20 C21 C22 C23 1.1(9) . . . . ? C21 C22 C23 C18 0.2(9) . . . . ? C21 C22 C23 C27 178.7(6) . . . . ? C19 C18 C23 C22 -2.6(8) . . . . ? N2 C18 C23 C22 175.7(5) . . . . ? C19 C18 C23 C27 178.9(5) . . . . ? N2 C18 C23 C27 -2.8(8) . . . . ? C20 C19 C24 C26 75.3(7) . . . . ? C18 C19 C24 C26 -102.8(7) . . . . ? C20 C19 C24 C25 -49.3(7) . . . . ? C18 C19 C24 C25 132.6(6) . . . . ? C22 C23 C27 C29 -60.8(7) . . . . ? C18 C23 C27 C29 117.7(6) . . . . ? C22 C23 C27 C28 62.4(8) . . . . ? C18 C23 C27 C28 -119.1(6) . . . . ? N4A Si1A C30A C31A -36.9(6) . . . . ? C31 Si1A C30A C31A 78.7(7) . . . . ? C32 Si1A C30A C31A -154.5(6) . . . . ? C32 Si1B C30B C31B -172.3(19) . . . . ? N3B Si1B C30B C31B -56(2) . . . . ? C31 Si1B C30B C31B 63(2) . . . . ? Si1A C30A C31A Si2A 41.8(7) . . . . ? Si1B C30B C31B Si2B 64(2) . . . . ? _refine_diff_density_max 0.843 _refine_diff_density_min -0.675 _refine_diff_density_rms 0.106 _shelx_res_file ; 007a-22141.res created by SHELXL-2014/7 TITL 007a-22141 CELL 1.54184 10.6104 20.3504 17.3268 90 95.909 90 ZERR 4 0.0005 0.0008 0.0008 0 0.004 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Fe N Si UNIT 140 228 4 16 8 EADP C30A C30B EADP C31A C31B SIMU 0.002 0.004 2 N3B N4B L.S. 30 SIZE 0.2 0.2 0.02 TEMP -180 CONF MORE -1 BOND $H ACTA MERG 0 OMIT 0 5 7 OMIT 0 6 7 OMIT -6 5 1 OMIT 1 17 1 OMIT 0 4 0 OMIT -6 7 1 OMIT 1 13 1 WGHT 0.096700 9.378000 BASF 0.46359 FVAR 13.31390 FE1 3 0.459835 0.251491 0.655306 11.00000 0.03968 0.01985 = 0.03696 0.00150 0.00895 0.00121 PART 1 SI1A 5 0.539442 0.320833 0.880251 10.75000 0.04674 0.02739 = 0.03301 -0.00184 0.01170 0.00016 PART 2 SI1B 5 0.541712 0.328182 0.847732 10.25000 0.05635 0.03323 = 0.02809 -0.00250 0.01192 -0.00828 PART 1 SI2A 5 0.424552 0.185501 0.877882 10.75000 0.04764 0.02762 = 0.04007 0.00208 0.01460 -0.00367 PART 2 SI2B 5 0.393369 0.175809 0.842627 10.25000 0.07448 0.03373 = 0.04629 -0.01408 0.01635 -0.02324 PART 0 N1 4 0.439537 0.320305 0.579946 11.00000 0.02950 0.02013 = 0.03433 0.00039 0.00725 0.00060 N2 4 0.487486 0.186017 0.579299 11.00000 0.03178 0.01847 = 0.04094 0.00498 0.00705 0.00289 PART 1 N3A 4 0.466262 0.251908 0.746276 10.75000 0.03667 0.01551 = 0.05325 0.00058 0.00386 -0.00328 PART 2 N3B 4 0.484338 0.282075 0.764115 10.25000 0.03723 0.03599 = 0.03020 -0.01835 0.01557 -0.01660 PART 1 N4A 4 0.475022 0.253161 0.824417 10.75000 0.04132 0.02513 = 0.03940 -0.00067 0.00859 0.00126 PART 2 N4B 4 0.441342 0.223446 0.759084 10.25000 0.03754 0.03640 = 0.03069 -0.01810 0.01529 -0.01629 PART 0 C1 1 0.399799 0.374223 0.451792 11.00000 0.04975 0.02289 = 0.03991 0.00357 -0.00005 0.00160 AFIX 137 H1A 2 0.324325 0.396178 0.467542 11.00000 -1.50000 H1B 2 0.383989 0.360531 0.397431 11.00000 -1.50000 H1C 2 0.471742 0.404649 0.457632 11.00000 -1.50000 AFIX 0 C2 1 0.429654 0.314507 0.502371 11.00000 0.03204 0.01684 = 0.03692 0.00162 0.00338 -0.00198 C3 1 0.451245 0.254550 0.466162 11.00000 0.03688 0.02121 = 0.02734 0.00342 0.00227 -0.00186 AFIX 43 H3 2 0.441717 0.254645 0.411041 11.00000 -1.20000 AFIX 0 C4 1 0.485375 0.194312 0.502076 11.00000 0.03533 0.01734 = 0.03885 -0.00154 0.00600 0.00031 C5 1 0.523094 0.138307 0.451313 11.00000 0.04812 0.02880 = 0.04476 -0.00333 0.01021 0.00923 AFIX 137 H5A 2 0.609981 0.124579 0.468542 11.00000 -1.50000 H5B 2 0.518267 0.153034 0.397239 11.00000 -1.50000 H5C 2 0.465381 0.101159 0.455394 11.00000 -1.50000 AFIX 0 C6 1 0.443555 0.385715 0.612472 11.00000 0.03556 0.02466 = 0.02707 0.00216 0.00432 0.00050 C7 1 0.559640 0.420914 0.616695 11.00000 0.03412 0.02478 = 0.03065 0.00377 0.00637 0.00002 C8 1 0.567657 0.480574 0.655984 11.00000 0.04202 0.02606 = 0.03446 -0.00088 0.00638 -0.00797 AFIX 43 H8 2 0.645216 0.504258 0.660165 11.00000 -1.20000 AFIX 0 C9 1 0.464665 0.506305 0.689267 11.00000 0.04704 0.02770 = 0.04018 -0.00381 0.00848 -0.00303 AFIX 43 H9 2 0.472437 0.546827 0.716564 11.00000 -1.20000 AFIX 0 C10 1 0.350483 0.472586 0.682471 11.00000 0.04234 0.03342 = 0.03557 -0.00038 0.01183 0.00558 AFIX 43 H10 2 0.279899 0.490747 0.704530 11.00000 -1.20000 AFIX 0 C11 1 0.337379 0.412035 0.643530 11.00000 0.03935 0.02391 = 0.04124 0.00229 0.01009 -0.00071 C12 1 0.674647 0.393957 0.579754 11.00000 0.03814 0.02814 = 0.02646 0.00029 0.00804 -0.00457 AFIX 13 H12 2 0.641955 0.360857 0.539970 11.00000 -1.20000 AFIX 0 C13 1 0.744102 0.447048 0.537381 11.00000 0.04630 0.03949 = 0.03955 0.00467 0.01369 -0.00208 AFIX 137 H13A 2 0.683468 0.469897 0.500171 11.00000 -1.50000 H13B 2 0.809832 0.426452 0.509731 11.00000 -1.50000 H13C 2 0.783305 0.478656 0.575216 11.00000 -1.50000 AFIX 0 C14 1 0.765193 0.357569 0.640253 11.00000 0.04040 0.03234 = 0.03975 0.00437 0.00938 0.00230 AFIX 137 H14A 2 0.804396 0.389138 0.678136 11.00000 -1.50000 H14B 2 0.831268 0.335543 0.614253 11.00000 -1.50000 H14C 2 0.717642 0.324826 0.666941 11.00000 -1.50000 AFIX 0 C15 1 0.209356 0.377731 0.634956 11.00000 0.03578 0.03068 = 0.04832 -0.00120 0.01062 -0.00205 AFIX 13 H15 2 0.215881 0.338772 0.600420 11.00000 -1.20000 AFIX 0 C16 1 0.107478 0.423808 0.595484 11.00000 0.04164 0.05157 = 0.07734 0.00734 0.00346 -0.00330 AFIX 137 H16A 2 0.098890 0.462399 0.628369 11.00000 -1.50000 H16B 2 0.026306 0.400524 0.587811 11.00000 -1.50000 H16C 2 0.132291 0.437875 0.545110 11.00000 -1.50000 AFIX 0 C17 1 0.169346 0.353058 0.712306 11.00000 0.04146 0.04396 = 0.06426 0.00693 0.01439 -0.00204 AFIX 137 H17A 2 0.234287 0.323261 0.736636 11.00000 -1.50000 H17B 2 0.088546 0.329593 0.703060 11.00000 -1.50000 H17C 2 0.159604 0.390532 0.746715 11.00000 -1.50000 AFIX 0 C18 1 0.520102 0.121750 0.611732 11.00000 0.04244 0.01717 = 0.03550 -0.00164 0.00754 0.00617 C19 1 0.427248 0.071812 0.609089 11.00000 0.04922 0.02221 = 0.03476 -0.00029 0.00972 0.00465 C20 1 0.458106 0.011991 0.646540 11.00000 0.06464 0.02361 = 0.03696 -0.00254 0.01091 0.00577 AFIX 43 H20 2 0.395724 -0.021467 0.646867 11.00000 -1.20000 AFIX 0 C21 1 0.578266 0.001264 0.682934 11.00000 0.06775 0.02751 = 0.03905 0.00369 0.00794 0.01993 AFIX 43 H21 2 0.597872 -0.039464 0.708156 11.00000 -1.20000 AFIX 0 C22 1 0.670186 0.049301 0.682950 11.00000 0.05755 0.04009 = 0.03387 0.00182 0.00489 0.02001 AFIX 43 H22 2 0.752886 0.040890 0.707425 11.00000 -1.20000 AFIX 0 C23 1 0.643298 0.110321 0.647378 11.00000 0.04590 0.03281 = 0.03210 -0.00201 0.00700 0.00930 C24 1 0.293854 0.081675 0.569052 11.00000 0.04954 0.03328 = 0.04092 0.01121 0.01014 -0.00205 AFIX 13 H24 2 0.294716 0.121942 0.536032 11.00000 -1.20000 AFIX 0 C25 1 0.251949 0.022964 0.515188 11.00000 0.06635 0.03313 = 0.06139 0.00837 -0.00253 -0.01406 AFIX 137 H25A 2 0.314316 0.016144 0.477989 11.00000 -1.50000 H25B 2 0.169052 0.032496 0.487070 11.00000 -1.50000 H25C 2 0.246030 -0.016804 0.546506 11.00000 -1.50000 AFIX 0 C26 1 0.201680 0.093659 0.629321 11.00000 0.05548 0.07382 = 0.06516 0.01444 0.02184 0.01399 AFIX 137 H26A 2 0.207114 0.057321 0.666631 11.00000 -1.50000 H26B 2 0.115223 0.096428 0.603496 11.00000 -1.50000 H26C 2 0.223355 0.134943 0.656641 11.00000 -1.50000 AFIX 0 C27 1 0.746103 0.163054 0.649757 11.00000 0.04098 0.04170 = 0.04361 0.00297 0.00150 0.00943 AFIX 13 H27 2 0.709008 0.202759 0.622008 11.00000 -1.20000 AFIX 0 C28 1 0.858027 0.139293 0.607427 11.00000 0.05016 0.07876 = 0.06280 -0.00457 0.01685 0.00525 AFIX 137 H28A 2 0.894551 0.099653 0.632892 11.00000 -1.50000 H28B 2 0.922678 0.173799 0.609105 11.00000 -1.50000 H28C 2 0.828232 0.129273 0.553288 11.00000 -1.50000 AFIX 0 C29 1 0.791667 0.182935 0.732691 11.00000 0.05653 0.06257 = 0.04704 -0.00035 -0.00656 -0.00052 AFIX 137 H29A 2 0.719565 0.198508 0.758733 11.00000 -1.50000 H29B 2 0.854513 0.218164 0.732013 11.00000 -1.50000 H29C 2 0.830243 0.144925 0.760695 11.00000 -1.50000 AFIX 0 PART 1 C30A 1 0.572563 0.273590 0.973415 10.75000 0.05613 0.03456 = 0.03520 -0.00115 0.00701 0.00314 AFIX 23 H30A 2 0.654626 0.250313 0.974270 10.75000 -1.20000 H30B 2 0.577014 0.303967 1.018242 10.75000 -1.20000 AFIX 0 PART 2 C30B 1 0.560997 0.264199 0.927252 10.25000 0.05613 0.03456 = 0.03520 -0.00115 0.00701 0.00314 AFIX 23 H30C 2 0.628411 0.233051 0.916007 10.25000 -1.20000 H30D 2 0.588853 0.286214 0.977051 10.25000 -1.20000 AFIX 0 PART 0 C31 1 0.420355 0.386603 0.882860 11.00000 0.05758 0.03510 = 0.05537 -0.00463 0.00700 0.00316 PART 1 AFIX 137 H31A 2 0.408304 0.408417 0.832213 10.75000 -1.50000 H31B 2 0.449675 0.418749 0.922846 10.75000 -1.50000 H31C 2 0.339809 0.367588 0.894906 10.75000 -1.50000 AFIX 137 PART 2 H31D 2 0.456507 0.408317 0.930567 10.25000 -1.50000 H31E 2 0.344659 0.361885 0.893263 10.25000 -1.50000 H31F 2 0.397246 0.419767 0.842885 10.25000 -1.50000 AFIX 0 PART 1 C31A 1 0.463181 0.223256 0.978301 10.75000 0.06432 0.03643 = 0.03053 0.01854 0.01574 0.00020 AFIX 23 H31G 2 0.387552 0.245622 0.994803 10.75000 -1.20000 H31H 2 0.489645 0.188563 1.016636 10.75000 -1.20000 AFIX 0 PART 2 C31B 1 0.443383 0.226771 0.935870 10.25000 0.06432 0.03643 = 0.03053 0.01854 0.01574 0.00020 AFIX 23 H31I 2 0.374545 0.257604 0.945493 10.25000 -1.20000 H31J 2 0.457516 0.196885 0.981015 10.25000 -1.20000 AFIX 0 PART 0 C32 1 0.681725 0.357146 0.838017 11.00000 0.06227 0.06382 = 0.03907 -0.00925 0.01093 -0.00481 PART 1 AFIX 137 H32A 2 0.743372 0.322320 0.831138 10.75000 -1.50000 H32B 2 0.720916 0.390627 0.873393 10.75000 -1.50000 H32C 2 0.654497 0.377277 0.787670 10.75000 -1.50000 AFIX 137 PART 2 H32D 2 0.674001 0.401781 0.816827 10.25000 -1.50000 H32E 2 0.723793 0.328987 0.802608 10.25000 -1.50000 H32F 2 0.731922 0.358158 0.888750 10.25000 -1.50000 AFIX 0 PART 0 C33 1 0.246262 0.170268 0.849419 11.00000 0.07830 0.06020 = 0.07798 0.01361 0.03330 -0.00574 PART 1 AFIX 137 H33A 2 0.198632 0.210290 0.858575 10.75000 -1.50000 H33B 2 0.217261 0.134344 0.880856 10.75000 -1.50000 H33C 2 0.232374 0.158438 0.794373 10.75000 -1.50000 AFIX 137 PART 2 H33D 2 0.199316 0.181945 0.799627 10.25000 -1.50000 H33E 2 0.222837 0.200328 0.889762 10.25000 -1.50000 H33F 2 0.225468 0.125098 0.863075 10.25000 -1.50000 AFIX 0 PART 0 C34 1 0.512541 0.108593 0.857842 11.00000 0.09843 0.05476 = 0.04761 0.01184 0.03008 0.01977 PART 1 AFIX 137 H34A 2 0.480649 0.091421 0.806690 10.75000 -1.50000 H34B 2 0.499912 0.075706 0.897639 10.75000 -1.50000 H34C 2 0.603097 0.118415 0.858711 10.75000 -1.50000 AFIX 137 PART 2 H34D 2 0.472749 0.069648 0.878122 10.25000 -1.50000 H34E 2 0.582912 0.123011 0.895065 10.25000 -1.50000 H34F 2 0.544650 0.097762 0.808343 10.25000 -1.50000 AFIX 0 HKLF 5 REM 007a-22141 REM R1 = 0.0819 for 4992 Fo > 4sig(Fo) and 0.1047 for all 6549 data REM 436 parameters refined using 6 restraints END WGHT 0.0967 9.3868 REM Highest difference peak 0.843, deepest hole -0.675, 1-sigma level 0.106 Q1 1 0.4590 0.2527 0.5843 11.00000 0.05 0.84 Q2 1 0.5857 0.2512 0.6594 11.00000 0.05 0.78 Q3 1 0.4626 0.2524 0.5370 11.00000 0.05 0.73 Q4 1 0.3615 0.2506 0.6535 11.00000 0.05 0.67 Q5 1 0.6196 0.2525 0.7230 11.00000 0.05 0.59 Q6 1 0.6207 0.2518 0.6024 11.00000 0.05 0.57 Q7 1 0.3567 0.2519 0.7044 11.00000 0.05 0.49 Q8 1 0.2899 0.2508 0.6470 11.00000 0.05 0.41 Q9 1 0.6854 0.1393 0.4589 11.00000 0.05 0.41 Q10 1 0.4914 0.2647 0.9369 11.00000 0.05 0.39 Q11 1 0.4185 0.1779 0.7490 11.00000 0.05 0.38 Q12 1 0.4279 0.3856 0.7245 11.00000 0.05 0.38 Q13 1 0.5750 0.2531 0.7797 11.00000 0.05 0.37 Q14 1 0.5319 0.1164 0.7469 11.00000 0.05 0.36 Q15 1 0.5120 0.1898 0.6992 11.00000 0.05 0.35 Q16 1 0.4092 0.3132 0.3832 11.00000 0.05 0.35 Q17 1 0.6338 0.2534 0.7811 11.00000 0.05 0.35 Q18 1 0.6783 0.1384 0.3935 11.00000 0.05 0.35 Q19 1 0.3066 0.2540 0.5839 11.00000 0.05 0.35 Q20 1 0.6431 0.1431 0.3396 11.00000 0.05 0.35 ; _shelx_res_checksum 83595 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-23018 _database_code_depnum_ccdc_archive 'CCDC 2303073' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2023-10-24 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H60 Fe N4 Si2' _chemical_formula_sum 'C36 H60 Fe N4 Si2' _chemical_formula_weight 660.91 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.6993(4) _cell_length_b 12.0566(4) _cell_length_c 18.0449(6) _cell_angle_alpha 88.974(3) _cell_angle_beta 82.392(3) _cell_angle_gamma 83.828(3) _cell_volume 1865.07(12) _cell_formula_units_Z 2 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 39904 _cell_measurement_theta_min 2.3450 _cell_measurement_theta_max 66.8160 _exptl_crystal_description plate _exptl_crystal_colour brown _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.177 _exptl_crystal_F_000 716 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.400 _exptl_crystal_size_min 0.050 _exptl_absorpt_coefficient_mu 4.065 _shelx_estimated_absorpt_T_min 0.293 _shelx_estimated_absorpt_T_max 0.823 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.48700 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 57657 _diffrn_reflns_av_unetI/netI 0.0333 _diffrn_reflns_av_R_equivalents 0.0834 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_theta_min 2.470 _diffrn_reflns_theta_max 66.587 _diffrn_reflns_theta_full 66.587 _diffrn_measured_fraction_theta_max 0.979 _diffrn_measured_fraction_theta_full 0.979 _diffrn_reflns_Laue_measured_fraction_max 0.979 _diffrn_reflns_Laue_measured_fraction_full 0.979 _diffrn_reflns_point_group_measured_fraction_max 0.979 _diffrn_reflns_point_group_measured_fraction_full 0.979 _reflns_number_total 6463 _reflns_number_gt 5788 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. The Si-N-N-CH3 coordinated to Fe1 is disordered over two positions. The site occupancies were freely refined and converged near a population distribution of 0.75/0.25. The major component has atom suffixes \^a\/Eoe4\^a\/E?, the minor has \^a\/EoeB\^a\/E?. Due to the low occupancies, the thermal parameters of the minor component were constrained to be similar to their major counterpart with a small uncertainty 0.002). The disordered Si-N distances were restrained to be similar with a small uncertainty (0.002). No additional restraints were needed for a stable refinement. Two reflections were omitted from the least squares refinement due to detector artifacts. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0864P)^2^+1.0566P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 6463 _refine_ls_number_parameters 440 _refine_ls_number_restraints 48 _refine_ls_R_factor_all 0.0600 _refine_ls_R_factor_gt 0.0533 _refine_ls_wR_factor_ref 0.1613 _refine_ls_wR_factor_gt 0.1468 _refine_ls_goodness_of_fit_ref 1.160 _refine_ls_restrained_S_all 1.156 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.32011(5) 0.31456(3) 0.74911(2) 0.03450(17) Uani 1 1 d . . . . . C1 C 0.1467(6) 0.0781(4) 0.8175(3) 0.0477(12) Uani 0.773(4) 1 d . . P A 1 H1A H 0.0366 0.0843 0.8390 0.072 Uiso 0.773(4) 1 calc R U P A 1 H1B H 0.1976 0.0049 0.8299 0.072 Uiso 0.773(4) 1 calc R U P A 1 H1C H 0.1545 0.0866 0.7631 0.072 Uiso 0.773(4) 1 calc R U P A 1 N1 N 0.1635(4) 0.2802(3) 0.82730(19) 0.0374(7) Uani 0.773(4) 1 d D U P A 1 N11 N 0.3765(3) 0.46238(18) 0.70610(12) 0.0276(5) Uani 1 1 d . . . . . N21 N 0.4466(3) 0.22775(18) 0.66338(12) 0.0299(5) Uani 1 1 d . . . . . C11 C 0.5245(3) 0.5890(2) 0.62325(17) 0.0349(6) Uani 1 1 d . . . . . H11A H 0.4290 0.6330 0.6118 0.052 Uiso 1 1 calc R U . . . H11B H 0.6016 0.5831 0.5783 0.052 Uiso 1 1 calc R U . . . H11C H 0.5668 0.6258 0.6629 0.052 Uiso 1 1 calc R U . . . N2 N 0.2232(4) 0.1652(3) 0.84819(18) 0.0383(7) Uani 0.773(4) 1 d D U P A 1 C21 C 0.4879(3) 0.4738(2) 0.64893(15) 0.0289(6) Uani 1 1 d . . . . . C31 C 0.5702(3) 0.3837(2) 0.60776(15) 0.0303(6) Uani 1 1 d . . . . . H31 H 0.6547 0.4020 0.5724 0.036 Uiso 1 1 calc R U . . . C41 C 0.5460(3) 0.2712(2) 0.61120(15) 0.0310(6) Uani 1 1 d . . . . . C51 C 0.6318(4) 0.1984(2) 0.54827(17) 0.0397(7) Uani 1 1 d . . . . . H51A H 0.6803 0.1297 0.5690 0.059 Uiso 1 1 calc R U . . . H51B H 0.7127 0.2387 0.5200 0.059 Uiso 1 1 calc R U . . . H51C H 0.5581 0.1798 0.5150 0.059 Uiso 1 1 calc R U . . . C12 C 0.2873(3) 0.5630(2) 0.73630(15) 0.0308(6) Uani 1 1 d . . . . . C22 C 0.3393(3) 0.6229(2) 0.79251(15) 0.0329(6) Uani 1 1 d . . . . . C32 C 0.2482(4) 0.7199(2) 0.81986(17) 0.0392(7) Uani 1 1 d . . . . . H32 H 0.2814 0.7616 0.8579 0.047 Uiso 1 1 calc R U . . . C42 C 0.1100(4) 0.7560(2) 0.79221(18) 0.0419(7) Uani 1 1 d . . . . . H42 H 0.0503 0.8228 0.8107 0.050 Uiso 1 1 calc R U . . . C52 C 0.0589(4) 0.6951(2) 0.73770(17) 0.0387(7) Uani 1 1 d . . . . . H52 H -0.0361 0.7208 0.7193 0.046 Uiso 1 1 calc R U . . . C62 C 0.1440(3) 0.5969(2) 0.70918(16) 0.0321(6) Uani 1 1 d . . . . . C72 C 0.4864(4) 0.5831(2) 0.82533(17) 0.0387(7) Uani 1 1 d . . . . . H72 H 0.5433 0.5208 0.7934 0.046 Uiso 1 1 calc R U . . . C82 C 0.4454(5) 0.5365(3) 0.9045(2) 0.0527(9) Uani 1 1 d . . . . . H82A H 0.5409 0.5036 0.9232 0.079 Uiso 1 1 calc R U . . . H82B H 0.3741 0.4791 0.9030 0.079 Uiso 1 1 calc R U . . . H82C H 0.3950 0.5970 0.9377 0.079 Uiso 1 1 calc R U . . . C92 C 0.5968(4) 0.6744(3) 0.8271(2) 0.0504(8) Uani 1 1 d . . . . . H92A H 0.5450 0.7355 0.8594 0.076 Uiso 1 1 calc R U . . . H92B H 0.6234 0.7030 0.7763 0.076 Uiso 1 1 calc R U . . . H92C H 0.6922 0.6429 0.8465 0.076 Uiso 1 1 calc R U . . . C102 C 0.0819(4) 0.5266(3) 0.65342(18) 0.0407(7) Uani 1 1 d . . . . . H102 H 0.1113 0.4469 0.6665 0.049 Uiso 1 1 calc R U . . . C112 C -0.0957(4) 0.5425(3) 0.6589(2) 0.0533(9) Uani 1 1 d . . . . . H11D H -0.1411 0.5360 0.7113 0.080 Uiso 1 1 calc R U . . . H11E H -0.1309 0.4852 0.6293 0.080 Uiso 1 1 calc R U . . . H11F H -0.1290 0.6165 0.6398 0.080 Uiso 1 1 calc R U . . . C122 C 0.1528(4) 0.5427(4) 0.57354(19) 0.0563(9) Uani 1 1 d . . . . . H12A H 0.1293 0.6206 0.5587 0.084 Uiso 1 1 calc R U . . . H12B H 0.1089 0.4939 0.5408 0.084 Uiso 1 1 calc R U . . . H12C H 0.2660 0.5240 0.5692 0.084 Uiso 1 1 calc R U . . . C13 C 0.4129(3) 0.1148(2) 0.65325(15) 0.0322(6) Uani 1 1 d . . . . . C23 C 0.4977(4) 0.0254(2) 0.68562(17) 0.0371(7) Uani 1 1 d . . . . . C33 C 0.4483(4) -0.0809(2) 0.68064(18) 0.0436(7) Uani 1 1 d . . . . . H33 H 0.5027 -0.1427 0.7028 0.052 Uiso 1 1 calc R U . . . C43 C 0.3231(4) -0.0980(3) 0.64455(18) 0.0426(7) Uani 1 1 d . . . . . H43 H 0.2903 -0.1705 0.6429 0.051 Uiso 1 1 calc R U . . . C53 C 0.2456(4) -0.0091(3) 0.61079(18) 0.0422(7) Uani 1 1 d . . . . . H53 H 0.1610 -0.0217 0.5848 0.051 Uiso 1 1 calc R U . . . C63 C 0.2884(4) 0.0981(2) 0.61388(16) 0.0365(6) Uani 1 1 d . . . . . C73 C 0.6387(4) 0.0401(3) 0.72407(19) 0.0436(7) Uani 1 1 d . . . . . H73 H 0.6585 0.1203 0.7192 0.052 Uiso 1 1 calc R U . . . C93 C 0.7856(4) -0.0309(4) 0.6881(2) 0.0599(10) Uani 1 1 d . . . . . H93A H 0.7679 -0.1099 0.6909 0.090 Uiso 1 1 calc R U . . . H93B H 0.8736 -0.0193 0.7148 0.090 Uiso 1 1 calc R U . . . H93C H 0.8092 -0.0089 0.6356 0.090 Uiso 1 1 calc R U . . . C83 C 0.6111(5) 0.0120(4) 0.8067(2) 0.0598(10) Uani 1 1 d . . . . . H83A H 0.5189 0.0584 0.8304 0.090 Uiso 1 1 calc R U . . . H83B H 0.7023 0.0263 0.8302 0.090 Uiso 1 1 calc R U . . . H83C H 0.5941 -0.0669 0.8129 0.090 Uiso 1 1 calc R U . . . C103 C 0.1995(4) 0.1940(3) 0.5753(2) 0.0471(8) Uani 1 1 d . . . . . H103 H 0.2556 0.2616 0.5784 0.057 Uiso 1 1 calc R U . . . C123 C 0.1986(6) 0.1698(4) 0.4921(2) 0.0772(13) Uani 1 1 d . . . . . H12D H 0.3058 0.1497 0.4683 0.116 Uiso 1 1 calc R U . . . H12E H 0.1531 0.2363 0.4676 0.116 Uiso 1 1 calc R U . . . H12F H 0.1365 0.1078 0.4871 0.116 Uiso 1 1 calc R U . . . C113 C 0.0355(5) 0.2214(4) 0.6134(3) 0.0681(11) Uani 1 1 d . . . . . H11G H -0.0232 0.1571 0.6105 0.102 Uiso 1 1 calc R U . . . H11H H -0.0150 0.2857 0.5886 0.102 Uiso 1 1 calc R U . . . H11I H 0.0380 0.2394 0.6660 0.102 Uiso 1 1 calc R U . . . Si14 Si -0.02474(12) 0.32686(7) 0.86855(5) 0.0498(3) Uani 1 1 d D . . . . Si2B Si 0.269(3) 0.1851(13) 0.9371(9) 0.0489(13) Uani 0.227(4) 1 d D U P A 2 C34 C -0.1882(5) 0.3082(4) 0.8132(3) 0.0728(12) Uani 1 1 d . . . . . H34A H -0.2860 0.3454 0.8388 0.109 Uiso 1 1 calc R U . . . H34B H -0.1978 0.2285 0.8084 0.109 Uiso 1 1 calc R U . . . H34C H -0.1662 0.3411 0.7633 0.109 Uiso 1 1 calc R U . . . C44 C -0.0219(5) 0.4779(3) 0.8856(2) 0.0552(9) Uani 1 1 d . . . . . H44A H -0.0046 0.5171 0.8376 0.083 Uiso 1 1 calc R U . . . H44B H 0.0624 0.4884 0.9150 0.083 Uiso 1 1 calc R U . . . H44C H -0.1219 0.5080 0.9131 0.083 Uiso 1 1 calc R U . . . C54 C -0.0574(5) 0.2527(3) 0.9601(2) 0.0703(13) Uani 1 1 d . . . . . H54A H -0.1453 0.2933 0.9926 0.084 Uiso 1 1 calc R U . . . H54B H -0.0846 0.1766 0.9519 0.084 Uiso 1 1 calc R U . . . C64 C 0.0916(6) 0.2457(4) 0.9985(2) 0.0768(14) Uani 1 1 d . . . . . H64C H 0.0768 0.1994 1.0443 0.092 Uiso 0.227(4) 1 calc R U P A 2 H64D H 0.1080 0.3215 1.0139 0.092 Uiso 0.227(4) 1 calc R U P A 2 H64A H 0.0718 0.2104 1.0483 0.092 Uiso 0.773(4) 1 calc R U P A 1 H64B H 0.1195 0.3219 1.0058 0.092 Uiso 0.773(4) 1 calc R U P A 1 C74 C 0.4456(6) 0.2214(4) 0.9524(3) 0.0791(13) Uani 1 1 d . . . . . H74D H 0.4677 0.1954 1.0020 0.119 Uiso 0.227(4) 1 calc R U P A 2 H74E H 0.5266 0.1870 0.9142 0.119 Uiso 0.227(4) 1 calc R U P A 2 H74F H 0.4444 0.3027 0.9496 0.119 Uiso 0.227(4) 1 calc R U P A 2 H74A H 0.4610 0.2180 1.0052 0.119 Uiso 0.773(4) 1 calc R U P A 1 H74B H 0.5333 0.1779 0.9226 0.119 Uiso 0.773(4) 1 calc R U P A 1 H74C H 0.4398 0.2992 0.9353 0.119 Uiso 0.773(4) 1 calc R U P A 1 C84 C 0.2725(6) 0.0159(4) 0.9694(3) 0.0808(14) Uani 1 1 d . . . . . H84D H 0.2284 0.0108 1.0220 0.121 Uiso 0.227(4) 1 calc R U P A 2 H84E H 0.3803 -0.0193 0.9627 0.121 Uiso 0.227(4) 1 calc R U P A 2 H84F H 0.2104 -0.0224 0.9384 0.121 Uiso 0.227(4) 1 calc R U P A 2 H84A H 0.3093 0.0087 1.0184 0.121 Uiso 0.773(4) 1 calc R U P A 1 H84B H 0.3460 -0.0285 0.9327 0.121 Uiso 0.773(4) 1 calc R U P A 1 H84C H 0.1695 -0.0112 0.9725 0.121 Uiso 0.773(4) 1 calc R U P A 1 N2B N 0.2634(14) 0.2415(9) 0.8468(6) 0.0379(9) Uani 0.227(4) 1 d D U P A 2 N1B N 0.1171(15) 0.2415(10) 0.8095(6) 0.0380(9) Uani 0.227(4) 1 d D U P A 2 C1B C 0.097(2) 0.1229(14) 0.7884(10) 0.051(4) Uani 0.227(4) 1 d . . P A 2 H1BA H 0.0312 0.1248 0.7482 0.076 Uiso 0.227(4) 1 calc R U P A 2 H1BB H 0.0473 0.0846 0.8321 0.076 Uiso 0.227(4) 1 calc R U P A 2 H1BC H 0.1992 0.0829 0.7713 0.076 Uiso 0.227(4) 1 calc R U P A 2 Si24 Si 0.2587(8) 0.1621(3) 0.9406(2) 0.0482(7) Uani 0.773(4) 1 d D U P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0467(3) 0.0252(2) 0.0292(3) -0.00111(17) 0.00473(19) -0.00439(18) C1 0.062(3) 0.031(2) 0.048(3) 0.001(2) 0.002(2) -0.004(2) N1 0.0484(16) 0.0263(15) 0.0359(14) 0.0029(11) 0.0000(12) -0.0035(12) N11 0.0316(12) 0.0229(11) 0.0265(11) -0.0011(8) -0.0016(9) 0.0033(9) N21 0.0392(13) 0.0208(11) 0.0289(11) -0.0004(8) -0.0023(9) -0.0015(9) C11 0.0366(15) 0.0277(14) 0.0388(15) 0.0040(11) -0.0009(12) -0.0024(11) N2 0.0493(16) 0.0269(14) 0.0365(13) 0.0027(11) 0.0007(12) -0.0019(11) C21 0.0332(14) 0.0251(13) 0.0282(13) 0.0027(10) -0.0062(11) -0.0004(11) C31 0.0330(14) 0.0284(14) 0.0279(13) 0.0012(10) 0.0011(11) -0.0020(11) C41 0.0367(15) 0.0284(14) 0.0275(13) -0.0008(11) -0.0056(11) -0.0005(11) C51 0.0475(18) 0.0311(15) 0.0376(16) -0.0067(12) 0.0039(13) -0.0022(13) C12 0.0382(15) 0.0210(12) 0.0305(13) 0.0041(10) 0.0006(11) 0.0023(11) C22 0.0412(16) 0.0266(13) 0.0302(14) -0.0005(11) -0.0049(12) -0.0007(11) C32 0.0476(18) 0.0313(15) 0.0365(15) -0.0035(12) -0.0029(13) 0.0023(13) C42 0.0452(18) 0.0281(15) 0.0470(17) 0.0002(13) 0.0044(14) 0.0067(13) C52 0.0358(16) 0.0312(15) 0.0461(17) 0.0098(13) -0.0011(13) 0.0026(12) C62 0.0327(15) 0.0285(14) 0.0338(14) 0.0074(11) -0.0007(11) -0.0022(11) C72 0.0475(18) 0.0316(15) 0.0373(15) -0.0051(12) -0.0131(13) 0.0044(13) C82 0.062(2) 0.051(2) 0.0460(19) 0.0113(15) -0.0154(16) -0.0025(17) C92 0.054(2) 0.0418(18) 0.059(2) 0.0001(15) -0.0186(16) -0.0057(15) C102 0.0385(17) 0.0378(16) 0.0459(17) 0.0016(13) -0.0098(13) 0.0008(13) C112 0.0394(18) 0.056(2) 0.067(2) 0.0066(17) -0.0130(16) -0.0066(15) C122 0.045(2) 0.083(3) 0.0441(19) 0.0003(18) -0.0145(15) -0.0104(18) C13 0.0426(16) 0.0227(13) 0.0302(13) -0.0033(10) 0.0002(12) -0.0036(11) C23 0.0451(17) 0.0251(14) 0.0389(15) -0.0003(11) -0.0005(13) -0.0003(12) C33 0.056(2) 0.0242(14) 0.0473(18) 0.0010(12) 0.0002(15) 0.0003(13) C43 0.0531(19) 0.0288(15) 0.0454(17) -0.0074(13) 0.0028(14) -0.0120(13) C53 0.0491(18) 0.0368(16) 0.0401(16) -0.0072(13) 0.0004(14) -0.0091(13) C63 0.0422(17) 0.0327(15) 0.0337(14) -0.0051(12) -0.0021(12) -0.0034(12) C73 0.0524(19) 0.0264(15) 0.0533(19) 0.0040(13) -0.0158(15) 0.0008(13) C93 0.049(2) 0.063(2) 0.067(2) -0.0031(19) -0.0131(18) 0.0065(17) C83 0.067(2) 0.066(2) 0.048(2) -0.0034(17) -0.0137(18) -0.0064(19) C103 0.051(2) 0.0385(17) 0.056(2) 0.0024(14) -0.0201(16) -0.0084(14) C123 0.103(4) 0.078(3) 0.055(2) 0.012(2) -0.032(2) -0.007(3) C113 0.061(2) 0.057(2) 0.088(3) 0.004(2) -0.023(2) 0.0030(19) Si14 0.0561(6) 0.0356(5) 0.0492(5) 0.0074(4) 0.0160(4) 0.0047(4) Si2B 0.074(2) 0.036(3) 0.0336(17) 0.006(2) 0.0014(17) -0.002(3) C34 0.071(3) 0.050(2) 0.092(3) -0.006(2) 0.007(2) -0.0022(19) C44 0.064(2) 0.0422(19) 0.056(2) 0.0071(16) -0.0002(17) -0.0017(16) C54 0.085(3) 0.051(2) 0.059(2) 0.0168(18) 0.033(2) 0.010(2) C64 0.118(4) 0.064(3) 0.0351(18) 0.0055(17) 0.016(2) 0.018(2) C74 0.106(4) 0.053(2) 0.084(3) -0.003(2) -0.034(3) -0.006(2) C84 0.090(3) 0.055(3) 0.092(3) 0.006(2) 0.007(3) -0.008(2) N2B 0.0489(19) 0.0268(17) 0.0360(17) 0.0027(15) 0.0004(15) -0.0028(15) N1B 0.0490(19) 0.0266(18) 0.0362(17) 0.0033(15) 0.0012(16) -0.0030(15) C1B 0.068(12) 0.034(9) 0.047(9) -0.003(7) 0.023(8) -0.029(8) Si24 0.0731(12) 0.0344(17) 0.0340(7) 0.0041(9) 0.0012(7) -0.0028(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.900(3) . ? Fe1 N2B 1.983(10) . ? Fe1 N11 2.014(2) . ? Fe1 N21 2.014(2) . ? Fe1 N1B 2.208(12) . ? C1 N2 1.457(6) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? N1 N2 1.487(5) . ? N1 Si14 1.745(3) . ? N11 C21 1.334(4) . ? N11 C12 1.443(3) . ? N21 C41 1.332(4) . ? N21 C13 1.443(3) . ? C11 C21 1.510(4) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? N2 Si24 1.734(5) . ? C21 C31 1.402(4) . ? C31 C41 1.395(4) . ? C31 H31 0.9500 . ? C41 C51 1.512(4) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C12 C22 1.404(4) . ? C12 C62 1.416(4) . ? C22 C32 1.399(4) . ? C22 C72 1.509(4) . ? C32 C42 1.386(5) . ? C32 H32 0.9500 . ? C42 C52 1.384(5) . ? C42 H42 0.9500 . ? C52 C62 1.396(4) . ? C52 H52 0.9500 . ? C62 C102 1.515(4) . ? C72 C82 1.537(4) . ? C72 C92 1.541(5) . ? C72 H72 1.0000 . ? C82 H82A 0.9800 . ? C82 H82B 0.9800 . ? C82 H82C 0.9800 . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C102 C122 1.509(5) . ? C102 C112 1.526(5) . ? C102 H102 1.0000 . ? C112 H11D 0.9800 . ? C112 H11E 0.9800 . ? C112 H11F 0.9800 . ? C122 H12A 0.9800 . ? C122 H12B 0.9800 . ? C122 H12C 0.9800 . ? C13 C23 1.403(4) . ? C13 C63 1.406(4) . ? C23 C33 1.402(4) . ? C23 C73 1.515(5) . ? C33 C43 1.376(5) . ? C33 H33 0.9500 . ? C43 C53 1.380(5) . ? C43 H43 0.9500 . ? C53 C63 1.387(4) . ? C53 H53 0.9500 . ? C63 C103 1.530(4) . ? C73 C83 1.517(5) . ? C73 C93 1.534(5) . ? C73 H73 1.0000 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? C103 C113 1.504(6) . ? C103 C123 1.537(5) . ? C103 H103 1.0000 . ? C123 H12D 0.9800 . ? C123 H12E 0.9800 . ? C123 H12F 0.9800 . ? C113 H11G 0.9800 . ? C113 H11H 0.9800 . ? C113 H11I 0.9800 . ? Si14 N1B 1.770(10) . ? Si14 C44 1.856(4) . ? Si14 C54 1.868(4) . ? Si14 C34 1.878(5) . ? Si2B C74 1.70(2) . ? Si2B N2B 1.760(13) . ? Si2B C64 1.86(2) . ? Si2B C84 2.110(14) . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C54 C64 1.543(7) . ? C54 H54A 0.9900 . ? C54 H54B 0.9900 . ? C64 Si24 1.882(7) . ? C64 H64C 0.9900 . ? C64 H64D 0.9900 . ? C64 H64A 0.9900 . ? C64 H64B 0.9900 . ? C74 Si24 1.884(7) . ? C74 H74D 0.9800 . ? C74 H74E 0.9800 . ? C74 H74F 0.9800 . ? C74 H74A 0.9800 . ? C74 H74B 0.9800 . ? C74 H74C 0.9800 . ? C84 Si24 1.824(6) . ? C84 H84D 0.9800 . ? C84 H84E 0.9800 . ? C84 H84F 0.9800 . ? C84 H84A 0.9800 . ? C84 H84B 0.9800 . ? C84 H84C 0.9800 . ? N2B N1B 1.516(19) . ? N1B C1B 1.52(2) . ? C1B H1BA 0.9800 . ? C1B H1BB 0.9800 . ? C1B H1BC 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N11 130.83(12) . . ? N2B Fe1 N11 140.6(3) . . ? N1 Fe1 N21 134.32(13) . . ? N2B Fe1 N21 120.8(3) . . ? N11 Fe1 N21 93.08(9) . . ? N2B Fe1 N1B 42.0(5) . . ? N11 Fe1 N1B 139.2(3) . . ? N21 Fe1 N1B 118.0(3) . . ? N2 C1 H1A 109.5 . . ? N2 C1 H1B 109.5 . . ? H1A C1 H1B 109.5 . . ? N2 C1 H1C 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? N2 N1 Si14 115.6(2) . . ? N2 N1 Fe1 101.6(2) . . ? Si14 N1 Fe1 141.8(2) . . ? C21 N11 C12 117.1(2) . . ? C21 N11 Fe1 124.26(17) . . ? C12 N11 Fe1 118.59(17) . . ? C41 N21 C13 117.9(2) . . ? C41 N21 Fe1 124.36(18) . . ? C13 N21 Fe1 117.29(17) . . ? C21 C11 H11A 109.5 . . ? C21 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C21 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C1 N2 N1 113.9(4) . . ? C1 N2 Si24 121.5(3) . . ? N1 N2 Si24 110.0(3) . . ? N11 C21 C31 123.5(2) . . ? N11 C21 C11 119.7(2) . . ? C31 C21 C11 116.7(2) . . ? C41 C31 C21 129.4(3) . . ? C41 C31 H31 115.3 . . ? C21 C31 H31 115.3 . . ? N21 C41 C31 123.8(2) . . ? N21 C41 C51 119.7(2) . . ? C31 C41 C51 116.4(2) . . ? C41 C51 H51A 109.5 . . ? C41 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C41 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C22 C12 C62 121.5(2) . . ? C22 C12 N11 120.7(2) . . ? C62 C12 N11 117.8(2) . . ? C32 C22 C12 118.3(3) . . ? C32 C22 C72 119.9(3) . . ? C12 C22 C72 121.7(2) . . ? C42 C32 C22 120.9(3) . . ? C42 C32 H32 119.6 . . ? C22 C32 H32 119.6 . . ? C52 C42 C32 120.2(3) . . ? C52 C42 H42 119.9 . . ? C32 C42 H42 119.9 . . ? C42 C52 C62 121.4(3) . . ? C42 C52 H52 119.3 . . ? C62 C52 H52 119.3 . . ? C52 C62 C12 117.7(3) . . ? C52 C62 C102 121.1(3) . . ? C12 C62 C102 121.2(2) . . ? C22 C72 C82 110.1(3) . . ? C22 C72 C92 113.1(3) . . ? C82 C72 C92 110.0(3) . . ? C22 C72 H72 107.8 . . ? C82 C72 H72 107.8 . . ? C92 C72 H72 107.8 . . ? C72 C82 H82A 109.5 . . ? C72 C82 H82B 109.5 . . ? H82A C82 H82B 109.5 . . ? C72 C82 H82C 109.5 . . ? H82A C82 H82C 109.5 . . ? H82B C82 H82C 109.5 . . ? C72 C92 H92A 109.5 . . ? C72 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C72 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C122 C102 C62 113.9(3) . . ? C122 C102 C112 109.8(3) . . ? C62 C102 C112 112.8(3) . . ? C122 C102 H102 106.6 . . ? C62 C102 H102 106.6 . . ? C112 C102 H102 106.6 . . ? C102 C112 H11D 109.5 . . ? C102 C112 H11E 109.5 . . ? H11D C112 H11E 109.5 . . ? C102 C112 H11F 109.5 . . ? H11D C112 H11F 109.5 . . ? H11E C112 H11F 109.5 . . ? C102 C122 H12A 109.5 . . ? C102 C122 H12B 109.5 . . ? H12A C122 H12B 109.5 . . ? C102 C122 H12C 109.5 . . ? H12A C122 H12C 109.5 . . ? H12B C122 H12C 109.5 . . ? C23 C13 C63 121.4(3) . . ? C23 C13 N21 120.3(3) . . ? C63 C13 N21 118.2(2) . . ? C33 C23 C13 117.4(3) . . ? C33 C23 C73 120.1(3) . . ? C13 C23 C73 122.5(3) . . ? C43 C33 C23 121.8(3) . . ? C43 C33 H33 119.1 . . ? C23 C33 H33 119.1 . . ? C33 C43 C53 119.5(3) . . ? C33 C43 H43 120.3 . . ? C53 C43 H43 120.3 . . ? C43 C53 C63 121.6(3) . . ? C43 C53 H53 119.2 . . ? C63 C53 H53 119.2 . . ? C53 C63 C13 118.2(3) . . ? C53 C63 C103 119.8(3) . . ? C13 C63 C103 122.0(3) . . ? C23 C73 C83 111.7(3) . . ? C23 C73 C93 112.1(3) . . ? C83 C73 C93 108.9(3) . . ? C23 C73 H73 108.0 . . ? C83 C73 H73 108.0 . . ? C93 C73 H73 108.0 . . ? C73 C93 H93A 109.5 . . ? C73 C93 H93B 109.5 . . ? H93A C93 H93B 109.5 . . ? C73 C93 H93C 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C73 C83 H83A 109.5 . . ? C73 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C73 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? C113 C103 C63 112.3(3) . . ? C113 C103 C123 110.3(3) . . ? C63 C103 C123 111.5(3) . . ? C113 C103 H103 107.5 . . ? C63 C103 H103 107.5 . . ? C123 C103 H103 107.5 . . ? C103 C123 H12D 109.5 . . ? C103 C123 H12E 109.5 . . ? H12D C123 H12E 109.5 . . ? C103 C123 H12F 109.5 . . ? H12D C123 H12F 109.5 . . ? H12E C123 H12F 109.5 . . ? C103 C113 H11G 109.5 . . ? C103 C113 H11H 109.5 . . ? H11G C113 H11H 109.5 . . ? C103 C113 H11I 109.5 . . ? H11G C113 H11I 109.5 . . ? H11H C113 H11I 109.5 . . ? N1 Si14 C44 105.33(18) . . ? N1B Si14 C44 125.9(5) . . ? N1 Si14 C54 106.96(18) . . ? N1B Si14 C54 107.2(4) . . ? C44 Si14 C54 109.26(19) . . ? N1 Si14 C34 116.8(2) . . ? N1B Si14 C34 94.7(5) . . ? C44 Si14 C34 108.85(19) . . ? C54 Si14 C34 109.4(2) . . ? C74 Si2B N2B 98.8(10) . . ? C74 Si2B C64 118.6(10) . . ? N2B Si2B C64 108.4(11) . . ? C74 Si2B C84 104.7(10) . . ? N2B Si2B C84 127.7(10) . . ? C64 Si2B C84 100.3(8) . . ? Si14 C34 H34A 109.5 . . ? Si14 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? Si14 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? Si14 C44 H44A 109.5 . . ? Si14 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? Si14 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? C64 C54 Si14 109.8(3) . . ? C64 C54 H54A 109.7 . . ? Si14 C54 H54A 109.7 . . ? C64 C54 H54B 109.7 . . ? Si14 C54 H54B 109.7 . . ? H54A C54 H54B 108.2 . . ? C54 C64 Si2B 113.0(6) . . ? C54 C64 Si24 110.8(3) . . ? C54 C64 H64C 109.0 . . ? Si2B C64 H64C 109.0 . . ? C54 C64 H64D 109.0 . . ? Si2B C64 H64D 109.0 . . ? H64C C64 H64D 107.8 . . ? C54 C64 H64A 109.5 . . ? Si24 C64 H64A 109.5 . . ? C54 C64 H64B 109.5 . . ? Si24 C64 H64B 109.5 . . ? H64A C64 H64B 108.1 . . ? Si2B C74 H74D 109.5 . . ? Si2B C74 H74E 109.5 . . ? H74D C74 H74E 109.5 . . ? Si2B C74 H74F 109.5 . . ? H74D C74 H74F 109.5 . . ? H74E C74 H74F 109.5 . . ? Si24 C74 H74A 109.5 . . ? Si24 C74 H74B 109.5 . . ? H74A C74 H74B 109.5 . . ? Si24 C74 H74C 109.5 . . ? H74A C74 H74C 109.5 . . ? H74B C74 H74C 109.5 . . ? Si2B C84 H84D 109.5 . . ? Si2B C84 H84E 109.5 . . ? H84D C84 H84E 109.5 . . ? Si2B C84 H84F 109.5 . . ? H84D C84 H84F 109.5 . . ? H84E C84 H84F 109.5 . . ? Si24 C84 H84A 109.5 . . ? Si24 C84 H84B 109.5 . . ? H84A C84 H84B 109.5 . . ? Si24 C84 H84C 109.5 . . ? H84A C84 H84C 109.5 . . ? H84B C84 H84C 109.5 . . ? N1B N2B Si2B 120.0(11) . . ? N1B N2B Fe1 77.0(6) . . ? Si2B N2B Fe1 163.0(11) . . ? N2B N1B C1B 109.6(12) . . ? N2B N1B Si14 103.6(8) . . ? C1B N1B Si14 123.6(10) . . ? N2B N1B Fe1 61.0(6) . . ? C1B N1B Fe1 116.2(8) . . ? Si14 N1B Fe1 119.6(6) . . ? N1B C1B H1BA 109.5 . . ? N1B C1B H1BB 109.5 . . ? H1BA C1B H1BB 109.5 . . ? N1B C1B H1BC 109.5 . . ? H1BA C1B H1BC 109.5 . . ? H1BB C1B H1BC 109.5 . . ? N2 Si24 C84 106.7(3) . . ? N2 Si24 C64 108.7(4) . . ? C84 Si24 C64 110.9(3) . . ? N2 Si24 C74 112.2(3) . . ? C84 Si24 C74 109.4(4) . . ? C64 Si24 C74 109.0(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Si14 N1 N2 C1 70.2(4) . . . . ? Fe1 N1 N2 C1 -101.0(3) . . . . ? Si14 N1 N2 Si24 -70.1(4) . . . . ? Fe1 N1 N2 Si24 118.7(3) . . . . ? C12 N11 C21 C31 -171.6(2) . . . . ? Fe1 N11 C21 C31 5.6(4) . . . . ? C12 N11 C21 C11 5.2(4) . . . . ? Fe1 N11 C21 C11 -177.57(19) . . . . ? N11 C21 C31 C41 7.1(5) . . . . ? C11 C21 C31 C41 -169.7(3) . . . . ? C13 N21 C41 C31 169.5(3) . . . . ? Fe1 N21 C41 C31 -2.8(4) . . . . ? C13 N21 C41 C51 -6.2(4) . . . . ? Fe1 N21 C41 C51 -178.5(2) . . . . ? C21 C31 C41 N21 -8.7(5) . . . . ? C21 C31 C41 C51 167.1(3) . . . . ? C21 N11 C12 C22 -87.3(3) . . . . ? Fe1 N11 C12 C22 95.3(3) . . . . ? C21 N11 C12 C62 94.7(3) . . . . ? Fe1 N11 C12 C62 -82.6(3) . . . . ? C62 C12 C22 C32 -2.1(4) . . . . ? N11 C12 C22 C32 -179.9(3) . . . . ? C62 C12 C22 C72 175.8(3) . . . . ? N11 C12 C22 C72 -2.1(4) . . . . ? C12 C22 C32 C42 0.0(4) . . . . ? C72 C22 C32 C42 -177.9(3) . . . . ? C22 C32 C42 C52 1.1(5) . . . . ? C32 C42 C52 C62 -0.1(5) . . . . ? C42 C52 C62 C12 -1.9(4) . . . . ? C42 C52 C62 C102 175.8(3) . . . . ? C22 C12 C62 C52 3.0(4) . . . . ? N11 C12 C62 C52 -179.1(2) . . . . ? C22 C12 C62 C102 -174.7(3) . . . . ? N11 C12 C62 C102 3.2(4) . . . . ? C32 C22 C72 C82 71.6(4) . . . . ? C12 C22 C72 C82 -106.3(3) . . . . ? C32 C22 C72 C92 -51.9(4) . . . . ? C12 C22 C72 C92 130.3(3) . . . . ? C52 C62 C102 C122 100.9(3) . . . . ? C12 C62 C102 C122 -81.6(4) . . . . ? C52 C62 C102 C112 -25.1(4) . . . . ? C12 C62 C102 C112 152.5(3) . . . . ? C41 N21 C13 C23 93.8(3) . . . . ? Fe1 N21 C13 C23 -93.3(3) . . . . ? C41 N21 C13 C63 -89.6(3) . . . . ? Fe1 N21 C13 C63 83.3(3) . . . . ? C63 C13 C23 C33 -3.3(4) . . . . ? N21 C13 C23 C33 173.2(3) . . . . ? C63 C13 C23 C73 176.0(3) . . . . ? N21 C13 C23 C73 -7.5(4) . . . . ? C13 C23 C33 C43 1.0(5) . . . . ? C73 C23 C33 C43 -178.4(3) . . . . ? C23 C33 C43 C53 1.5(5) . . . . ? C33 C43 C53 C63 -1.6(5) . . . . ? C43 C53 C63 C13 -0.6(5) . . . . ? C43 C53 C63 C103 179.8(3) . . . . ? C23 C13 C63 C53 3.1(4) . . . . ? N21 C13 C63 C53 -173.4(3) . . . . ? C23 C13 C63 C103 -177.3(3) . . . . ? N21 C13 C63 C103 6.2(4) . . . . ? C33 C23 C73 C83 -64.7(4) . . . . ? C13 C23 C73 C83 116.1(3) . . . . ? C33 C23 C73 C93 58.0(4) . . . . ? C13 C23 C73 C93 -121.3(3) . . . . ? C53 C63 C103 C113 68.9(4) . . . . ? C13 C63 C103 C113 -110.7(4) . . . . ? C53 C63 C103 C123 -55.5(4) . . . . ? C13 C63 C103 C123 124.9(4) . . . . ? N2 N1 Si14 C44 144.5(3) . . . . ? Fe1 N1 Si14 C44 -49.5(4) . . . . ? N2 N1 Si14 C54 28.3(4) . . . . ? Fe1 N1 Si14 C54 -165.7(4) . . . . ? N2 N1 Si14 C34 -94.6(3) . . . . ? Fe1 N1 Si14 C34 71.3(4) . . . . ? N1 Si14 C54 C64 40.5(3) . . . . ? N1B Si14 C54 C64 66.3(6) . . . . ? C44 Si14 C54 C64 -73.0(3) . . . . ? C34 Si14 C54 C64 167.9(3) . . . . ? Si14 C54 C64 Si2B -52.8(6) . . . . ? Si14 C54 C64 Si24 -62.5(4) . . . . ? C74 Si2B C64 C54 153.4(7) . . . . ? N2B Si2B C64 C54 42.1(11) . . . . ? C84 Si2B C64 C54 -93.5(7) . . . . ? C74 Si2B N2B N1B -173.7(9) . . . . ? C64 Si2B N2B N1B -49.6(13) . . . . ? C84 Si2B N2B N1B 70(2) . . . . ? C74 Si2B N2B Fe1 4(4) . . . . ? C64 Si2B N2B Fe1 128(3) . . . . ? C84 Si2B N2B Fe1 -112(3) . . . . ? Si2B N2B N1B C1B -70.8(13) . . . . ? Fe1 N2B N1B C1B 109.8(9) . . . . ? Si2B N2B N1B Si14 62.8(12) . . . . ? Fe1 N2B N1B Si14 -116.6(6) . . . . ? Si2B N2B N1B Fe1 179.4(11) . . . . ? C44 Si14 N1B N2B 64.5(8) . . . . ? C54 Si14 N1B N2B -66.1(8) . . . . ? C34 Si14 N1B N2B -178.1(7) . . . . ? C44 Si14 N1B C1B -170.4(12) . . . . ? C54 Si14 N1B C1B 59.0(14) . . . . ? C34 Si14 N1B C1B -53.0(13) . . . . ? C44 Si14 N1B Fe1 0.3(10) . . . . ? C54 Si14 N1B Fe1 -130.3(6) . . . . ? C34 Si14 N1B Fe1 117.7(6) . . . . ? C1 N2 Si24 C84 26.2(6) . . . . ? N1 N2 Si24 C84 163.0(3) . . . . ? C1 N2 Si24 C64 -93.5(4) . . . . ? N1 N2 Si24 C64 43.3(4) . . . . ? C1 N2 Si24 C74 145.9(4) . . . . ? N1 N2 Si24 C74 -77.3(4) . . . . ? C54 C64 Si24 N2 23.8(4) . . . . ? C54 C64 Si24 C84 -93.2(4) . . . . ? C54 C64 Si24 C74 146.3(3) . . . . ? _refine_diff_density_max 0.394 _refine_diff_density_min -0.717 _refine_diff_density_rms 0.064 _shelx_res_file ; 007a-23018.res created by SHELXL-2014/7 TITL 007a-23018 CELL 1.54184 8.6993 12.0566 18.0449 88.974 82.392 83.828 ZERR 2 0.0004 0.0004 0.0006 0.003 0.003 0.003 LATT 1 SFAC C H Fe N Si UNIT 72 120 2 8 4 SIMU 0.002 0.004 2 N1 N2 N1B N2B SADI Si14 N1 Si14 N1B si24 N2 Si2B N2B SIMU 0.002 0.004 2 si24 Si2B L.S. 30 PLAN 14 SIZE 0.4 0.4 0.05 TEMP -180 CONF MORE -1 BOND $H fmap 2 53 acta OMIT -9 -1 7 OMIT -9 0 7 REM REM REM WGHT 0.086400 1.056600 FVAR 0.91020 0.77261 FE1 3 0.320108 0.314557 0.749107 11.00000 0.04668 0.02517 = 0.02920 -0.00111 0.00473 -0.00439 PART 1 C1 1 0.146731 0.078116 0.817523 21.00000 0.06185 0.03081 = 0.04795 0.00082 0.00162 -0.00446 AFIX 137 H1A 2 0.036640 0.084279 0.839001 21.00000 -1.50000 H1B 2 0.197610 0.004864 0.829854 21.00000 -1.50000 H1C 2 0.154463 0.086583 0.763082 21.00000 -1.50000 AFIX 0 N1 4 0.163467 0.280207 0.827295 21.00000 0.04839 0.02631 = 0.03587 0.00289 -0.00002 -0.00353 PART 0 N11 4 0.376499 0.462378 0.706098 11.00000 0.03159 0.02290 = 0.02653 -0.00112 -0.00164 0.00328 N21 4 0.446552 0.227751 0.663384 11.00000 0.03917 0.02077 = 0.02886 -0.00042 -0.00230 -0.00152 C11 1 0.524550 0.589016 0.623253 11.00000 0.03661 0.02767 = 0.03880 0.00397 -0.00092 -0.00239 AFIX 137 H11A 2 0.429035 0.632974 0.611842 11.00000 -1.50000 H11B 2 0.601646 0.583074 0.578309 11.00000 -1.50000 H11C 2 0.566792 0.625785 0.662936 11.00000 -1.50000 AFIX 0 PART 1 N2 4 0.223245 0.165247 0.848188 21.00000 0.04928 0.02687 = 0.03655 0.00272 0.00070 -0.00190 PART 0 C21 1 0.487854 0.473820 0.648933 11.00000 0.03324 0.02511 = 0.02823 0.00266 -0.00615 -0.00040 C31 1 0.570203 0.383732 0.607761 11.00000 0.03298 0.02842 = 0.02787 0.00121 0.00108 -0.00205 AFIX 43 H31 2 0.654735 0.402027 0.572382 11.00000 -1.20000 AFIX 0 C41 1 0.546042 0.271153 0.611200 11.00000 0.03667 0.02840 = 0.02755 -0.00075 -0.00559 -0.00046 C51 1 0.631828 0.198425 0.548273 11.00000 0.04753 0.03109 = 0.03758 -0.00673 0.00390 -0.00223 AFIX 137 H51A 2 0.680301 0.129706 0.569047 11.00000 -1.50000 H51B 2 0.712699 0.238666 0.519980 11.00000 -1.50000 H51C 2 0.558092 0.179762 0.515002 11.00000 -1.50000 AFIX 0 C12 1 0.287313 0.563035 0.736302 11.00000 0.03815 0.02104 = 0.03046 0.00409 0.00063 0.00230 C22 1 0.339308 0.622906 0.792514 11.00000 0.04115 0.02662 = 0.03024 -0.00052 -0.00486 -0.00072 C32 1 0.248181 0.719931 0.819862 11.00000 0.04758 0.03135 = 0.03651 -0.00346 -0.00287 0.00228 AFIX 43 H32 2 0.281422 0.761591 0.857874 11.00000 -1.20000 AFIX 0 C42 1 0.110043 0.756039 0.792207 11.00000 0.04524 0.02814 = 0.04702 0.00025 0.00444 0.00670 AFIX 43 H42 2 0.050290 0.822759 0.810708 11.00000 -1.20000 AFIX 0 C52 1 0.058920 0.695137 0.737700 11.00000 0.03581 0.03123 = 0.04611 0.00983 -0.00111 0.00260 AFIX 43 H52 2 -0.036074 0.720764 0.719312 11.00000 -1.20000 AFIX 0 C62 1 0.143982 0.596863 0.709178 11.00000 0.03267 0.02846 = 0.03378 0.00742 -0.00067 -0.00217 C72 1 0.486394 0.583072 0.825334 11.00000 0.04751 0.03156 = 0.03727 -0.00510 -0.01313 0.00439 AFIX 13 H72 2 0.543256 0.520801 0.793431 11.00000 -1.20000 AFIX 0 C82 1 0.445367 0.536461 0.904476 11.00000 0.06186 0.05137 = 0.04603 0.01125 -0.01538 -0.00255 AFIX 137 H82A 2 0.540851 0.503585 0.923227 11.00000 -1.50000 H82B 2 0.374093 0.479117 0.902986 11.00000 -1.50000 H82C 2 0.394995 0.596959 0.937678 11.00000 -1.50000 AFIX 0 C92 1 0.596800 0.674434 0.827055 11.00000 0.05396 0.04180 = 0.05857 0.00014 -0.01863 -0.00569 AFIX 137 H92A 2 0.545037 0.735466 0.859450 11.00000 -1.50000 H92B 2 0.623409 0.703024 0.776316 11.00000 -1.50000 H92C 2 0.692188 0.642929 0.846492 11.00000 -1.50000 AFIX 0 C102 1 0.081911 0.526580 0.653422 11.00000 0.03854 0.03777 = 0.04590 0.00162 -0.00979 0.00076 AFIX 13 H102 2 0.111309 0.446865 0.666521 11.00000 -1.20000 AFIX 0 C112 1 -0.095667 0.542503 0.658932 11.00000 0.03938 0.05567 = 0.06669 0.00660 -0.01295 -0.00664 AFIX 137 H11D 2 -0.141070 0.536035 0.711305 11.00000 -1.50000 H11E 2 -0.130913 0.485173 0.629277 11.00000 -1.50000 H11F 2 -0.129041 0.616526 0.639751 11.00000 -1.50000 AFIX 0 C122 1 0.152753 0.542687 0.573535 11.00000 0.04511 0.08271 = 0.04409 0.00032 -0.01451 -0.01042 AFIX 137 H12A 2 0.129340 0.620623 0.558695 11.00000 -1.50000 H12B 2 0.108910 0.493907 0.540809 11.00000 -1.50000 H12C 2 0.266026 0.523995 0.569207 11.00000 -1.50000 AFIX 0 C13 1 0.412935 0.114786 0.653251 11.00000 0.04258 0.02270 = 0.03019 -0.00330 0.00019 -0.00364 C23 1 0.497673 0.025352 0.685625 11.00000 0.04514 0.02513 = 0.03888 -0.00030 -0.00046 -0.00032 C33 1 0.448265 -0.080857 0.680637 11.00000 0.05649 0.02415 = 0.04730 0.00102 0.00019 0.00034 AFIX 43 H33 2 0.502674 -0.142665 0.702775 11.00000 -1.20000 AFIX 0 C43 1 0.323126 -0.098010 0.644554 11.00000 0.05309 0.02881 = 0.04540 -0.00737 0.00276 -0.01203 AFIX 43 H43 2 0.290323 -0.170477 0.642897 11.00000 -1.20000 AFIX 0 C53 1 0.245638 -0.009129 0.610791 11.00000 0.04911 0.03685 = 0.04009 -0.00717 0.00037 -0.00915 AFIX 43 H53 2 0.161007 -0.021674 0.584814 11.00000 -1.20000 AFIX 0 C63 1 0.288354 0.098071 0.613876 11.00000 0.04223 0.03274 = 0.03374 -0.00508 -0.00213 -0.00343 C73 1 0.638687 0.040123 0.724066 11.00000 0.05243 0.02639 = 0.05328 0.00395 -0.01575 0.00079 AFIX 13 H73 2 0.658510 0.120273 0.719220 11.00000 -1.20000 AFIX 0 C93 1 0.785629 -0.030924 0.688079 11.00000 0.04865 0.06257 = 0.06729 -0.00308 -0.01310 0.00651 AFIX 137 H93A 2 0.767920 -0.109887 0.690876 11.00000 -1.50000 H93B 2 0.873607 -0.019329 0.714775 11.00000 -1.50000 H93C 2 0.809215 -0.008934 0.635600 11.00000 -1.50000 AFIX 0 C83 1 0.611053 0.011994 0.806694 11.00000 0.06716 0.06635 = 0.04763 -0.00343 -0.01365 -0.00637 AFIX 137 H83A 2 0.518889 0.058438 0.830384 11.00000 -1.50000 H83B 2 0.702267 0.026253 0.830212 11.00000 -1.50000 H83C 2 0.594149 -0.066884 0.812875 11.00000 -1.50000 AFIX 0 C103 1 0.199461 0.194034 0.575329 11.00000 0.05147 0.03846 = 0.05575 0.00238 -0.02011 -0.00840 AFIX 13 H103 2 0.255576 0.261627 0.578436 11.00000 -1.20000 AFIX 0 C123 1 0.198622 0.169755 0.492052 11.00000 0.10307 0.07792 = 0.05549 0.01158 -0.03185 -0.00737 AFIX 137 H12D 2 0.305775 0.149680 0.468320 11.00000 -1.50000 H12E 2 0.153091 0.236316 0.467625 11.00000 -1.50000 H12F 2 0.136464 0.107792 0.487122 11.00000 -1.50000 AFIX 0 C113 1 0.035536 0.221434 0.613409 11.00000 0.06083 0.05668 = 0.08816 0.00396 -0.02292 0.00301 AFIX 137 H11G 2 -0.023249 0.157064 0.610519 11.00000 -1.50000 H11H 2 -0.014954 0.285674 0.588560 11.00000 -1.50000 H11I 2 0.038002 0.239418 0.665958 11.00000 -1.50000 AFIX 0 SI14 5 -0.024737 0.326857 0.868548 11.00000 0.05608 0.03558 = 0.04918 0.00743 0.01596 0.00475 PART 2 SI2B 5 0.268887 0.185094 0.937143 -21.00000 0.07422 0.03554 = 0.03355 0.00596 0.00144 -0.00191 PART 0 C34 1 -0.188240 0.308233 0.813152 11.00000 0.07081 0.04976 = 0.09241 -0.00649 0.00719 -0.00223 AFIX 137 H34A 2 -0.286023 0.345416 0.838834 11.00000 -1.50000 H34B 2 -0.197797 0.228498 0.808407 11.00000 -1.50000 H34C 2 -0.166232 0.341063 0.763303 11.00000 -1.50000 AFIX 0 C44 1 -0.021870 0.477906 0.885574 11.00000 0.06414 0.04222 = 0.05603 0.00708 -0.00021 -0.00173 AFIX 137 H44A 2 -0.004560 0.517067 0.837624 11.00000 -1.50000 H44B 2 0.062407 0.488448 0.914967 11.00000 -1.50000 H44C 2 -0.121941 0.507974 0.913121 11.00000 -1.50000 AFIX 0 C54 1 -0.057399 0.252679 0.960122 11.00000 0.08531 0.05107 = 0.05867 0.01683 0.03292 0.00993 AFIX 23 H54A 2 -0.145330 0.293274 0.992650 11.00000 -1.20000 H54B 2 -0.084582 0.176584 0.951950 11.00000 -1.20000 AFIX 0 C64 1 0.091625 0.245681 0.998530 11.00000 0.11777 0.06427 = 0.03505 0.00553 0.01576 0.01802 PART 2 AFIX 23 H64C 2 0.076800 0.199414 1.044280 -21.00000 -1.20000 H64D 2 0.108004 0.321500 1.013875 -21.00000 -1.20000 AFIX 23 PART 1 H64A 2 0.071775 0.210382 1.048349 21.00000 -1.20000 H64B 2 0.119500 0.321863 1.005773 21.00000 -1.20000 AFIX 0 PART 0 C74 1 0.445616 0.221404 0.952354 11.00000 0.10616 0.05278 = 0.08377 -0.00259 -0.03424 -0.00639 PART 2 AFIX 33 H74D 2 0.467675 0.195370 1.002000 -21.00000 -1.50000 H74E 2 0.526588 0.187031 0.914227 -21.00000 -1.50000 H74F 2 0.444438 0.302738 0.949602 -21.00000 -1.50000 AFIX 33 PART 1 H74A 2 0.461023 0.217987 1.005204 21.00000 -1.50000 H74B 2 0.533309 0.177887 0.922643 21.00000 -1.50000 H74C 2 0.439762 0.299211 0.935341 21.00000 -1.50000 AFIX 0 PART 0 C84 1 0.272465 0.015876 0.969373 11.00000 0.09045 0.05502 = 0.09151 0.00590 0.00714 -0.00777 PART 2 AFIX 137 H84D 2 0.228376 0.010777 1.022036 -21.00000 -1.50000 H84E 2 0.380269 -0.019316 0.962675 -21.00000 -1.50000 H84F 2 0.210413 -0.022443 0.938382 -21.00000 -1.50000 AFIX 137 PART 1 H84A 2 0.309262 0.008727 1.018445 21.00000 -1.50000 H84B 2 0.346027 -0.028452 0.932685 21.00000 -1.50000 H84C 2 0.169516 -0.011164 0.972456 21.00000 -1.50000 AFIX 0 PART 2 N2B 4 0.263387 0.241515 0.846769 -21.00000 0.04888 0.02675 = 0.03602 0.00273 0.00040 -0.00277 N1B 4 0.117085 0.241498 0.809540 -21.00000 0.04898 0.02661 = 0.03621 0.00330 0.00121 -0.00302 C1B 1 0.096917 0.122903 0.788409 -21.00000 0.06761 0.03429 = 0.04726 -0.00320 0.02329 -0.02905 AFIX 137 H1BA 2 0.031169 0.124754 0.748208 -21.00000 -1.50000 H1BB 2 0.047344 0.084606 0.832097 -21.00000 -1.50000 H1BC 2 0.199238 0.082909 0.771302 -21.00000 -1.50000 AFIX 0 PART 1 SI24 5 0.258672 0.162055 0.940579 21.00000 0.07314 0.03442 = 0.03402 0.00407 0.00125 -0.00277 HKLF 4 REM 007a-23018 REM R1 = 0.0533 for 5788 Fo > 4sig(Fo) and 0.0600 for all 6463 data REM 440 parameters refined using 48 restraints END WGHT 0.0862 1.0605 REM Highest difference peak 0.394, deepest hole -0.717, 1-sigma level 0.064 Q1 1 0.0745 0.6161 0.5743 11.00000 0.05 0.39 Q2 1 0.1043 0.1400 0.9528 11.00000 0.05 0.37 Q3 1 0.4586 0.3156 0.7801 11.00000 0.05 0.35 Q4 1 0.1535 0.2772 0.7410 11.00000 0.05 0.34 Q5 1 0.7736 0.0491 0.6973 11.00000 0.05 0.32 Q6 1 0.0219 0.1573 0.5780 11.00000 0.05 0.32 Q7 1 0.2712 0.0568 0.9241 11.00000 0.05 0.31 Q8 1 0.3925 0.2577 0.7577 11.00000 0.05 0.29 Q9 1 0.4559 0.0785 0.6643 11.00000 0.05 0.29 Q10 1 0.1737 0.2906 0.7875 11.00000 0.05 0.28 Q11 1 0.6049 0.4064 0.5631 11.00000 0.05 0.28 Q12 1 -0.0537 0.3157 0.9182 11.00000 0.05 0.28 Q13 1 0.2531 0.3862 0.6959 11.00000 0.05 0.28 Q14 1 -0.0011 0.4180 0.8679 11.00000 0.05 0.27 ; _shelx_res_checksum 23586 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-22088 _database_code_depnum_ccdc_archive 'CCDC 2226340' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C39 H68 Fe N4 Si3' _chemical_formula_sum 'C39 H68 Fe N4 Si3' _chemical_formula_weight 733.09 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.3800(4) _cell_length_b 11.5329(4) _cell_length_c 20.2705(6) _cell_angle_alpha 76.000(3) _cell_angle_beta 82.547(3) _cell_angle_gamma 72.992(3) _cell_volume 2247.01(14) _cell_formula_units_Z 2 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 36746 _cell_measurement_theta_min 2.1950 _cell_measurement_theta_max 66.7580 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.084 _exptl_crystal_F_000 796 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 3.663 _shelx_estimated_absorpt_T_min 0.528 _shelx_estimated_absorpt_T_max 0.711 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.61604 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 66616 _diffrn_reflns_av_unetI/netI 0.0210 _diffrn_reflns_av_R_equivalents 0.0490 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_theta_min 2.251 _diffrn_reflns_theta_max 66.600 _diffrn_reflns_theta_full 66.600 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measured_fraction_theta_full 0.980 _diffrn_reflns_Laue_measured_fraction_max 0.980 _diffrn_reflns_Laue_measured_fraction_full 0.980 _diffrn_reflns_point_group_measured_fraction_max 0.980 _diffrn_reflns_point_group_measured_fraction_full 0.980 _reflns_number_total 7797 _reflns_number_gt 7241 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. The program SQUEEZE (see A.L.Spek, J. Appl. Cryst. 2015, C71, 9-18) was used to compensate for the contribution of disordered solvents contained in voids within the crystal lattice from the diffraction intensities. This procedure was applied to the data file and the submitted model is based on the solvent removed data. Based on the total electron density found in the voids (47 e/A^3^), it is likely that a hexane molecule is present in the unit cell. See "_platon_squeeze_details" in this .cif for more information. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0619P)^2^+1.7656P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7797 _refine_ls_number_parameters 441 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0488 _refine_ls_R_factor_gt 0.0455 _refine_ls_wR_factor_ref 0.1211 _refine_ls_wR_factor_gt 0.1182 _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_restrained_S_all 1.051 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.28854(4) 0.36658(3) 0.75032(2) 0.02828(11) Uani 1 1 d . . . . . Si15 Si 0.25363(7) 0.03209(6) 0.88408(3) 0.03426(16) Uani 1 1 d . . . . . Si25 Si 0.18504(7) 0.24065(6) 0.95807(3) 0.03595(17) Uani 1 1 d . . . . . Si14 Si 0.02100(7) 0.48773(6) 0.64475(3) 0.03662(17) Uani 1 1 d . . . . . N1 N 0.2995(2) 0.26039(18) 0.82869(10) 0.0324(4) Uani 1 1 d . . . . . N2 N 0.2603(2) 0.18559(18) 0.88317(10) 0.0323(4) Uani 1 1 d . . . . . N21 N 0.4442(2) 0.31410(17) 0.68200(10) 0.0305(4) Uani 1 1 d . . . . . N11 N 0.34064(19) 0.52514(17) 0.75287(10) 0.0296(4) Uani 1 1 d . . . . . C11 C 0.4365(3) 0.7006(2) 0.69678(14) 0.0387(6) Uani 1 1 d . . . . . H11A H 0.3767 0.7414 0.7309 0.058 Uiso 1 1 calc R U . . . H11B H 0.4198 0.7538 0.6513 0.058 Uiso 1 1 calc R U . . . H11C H 0.5307 0.6863 0.7063 0.058 Uiso 1 1 calc R U . . . C21 C 0.4090(2) 0.5778(2) 0.69955(12) 0.0320(5) Uani 1 1 d . . . . . C31 C 0.4656(3) 0.5235(2) 0.64355(12) 0.0343(5) Uani 1 1 d . . . . . H31 H 0.4894 0.5789 0.6041 0.041 Uiso 1 1 calc R U . . . C41 C 0.4921(2) 0.4003(2) 0.63716(12) 0.0317(5) Uani 1 1 d . . . . . C51 C 0.5817(3) 0.3659(2) 0.57597(13) 0.0401(6) Uani 1 1 d . . . . . H51A H 0.6590 0.2954 0.5912 0.060 Uiso 1 1 calc R U . . . H51B H 0.6141 0.4370 0.5507 0.060 Uiso 1 1 calc R U . . . H51C H 0.5302 0.3429 0.5463 0.060 Uiso 1 1 calc R U . . . C12 C 0.3145(2) 0.5754(2) 0.81322(12) 0.0310(5) Uani 1 1 d . . . . . C62 C 0.4207(2) 0.5511(2) 0.85608(12) 0.0330(5) Uani 1 1 d . . . . . C52 C 0.3928(3) 0.5961(2) 0.91587(13) 0.0360(5) Uani 1 1 d . . . . . H52 H 0.4637 0.5809 0.9448 0.043 Uiso 1 1 calc R U . . . C42 C 0.2642(3) 0.6623(2) 0.93384(13) 0.0365(5) Uani 1 1 d . . . . . H42 H 0.2468 0.6909 0.9751 0.044 Uiso 1 1 calc R U . . . C32 C 0.1605(3) 0.6867(2) 0.89128(13) 0.0352(5) Uani 1 1 d . . . . . H32 H 0.0725 0.7329 0.9036 0.042 Uiso 1 1 calc R U . . . C22 C 0.1832(2) 0.6445(2) 0.83088(12) 0.0332(5) Uani 1 1 d . . . . . C102 C 0.5643(2) 0.4764(2) 0.84050(13) 0.0375(6) Uani 1 1 d . . . . . H102 H 0.5698 0.4593 0.7940 0.045 Uiso 1 1 calc R U . . . C112 C 0.5986(3) 0.3521(3) 0.89194(14) 0.0455(6) Uani 1 1 d . . . . . H11D H 0.5864 0.3672 0.9382 0.068 Uiso 1 1 calc R U . . . H11E H 0.6927 0.3068 0.8830 0.068 Uiso 1 1 calc R U . . . H11F H 0.5389 0.3029 0.8875 0.068 Uiso 1 1 calc R U . . . C122 C 0.6678(3) 0.5477(3) 0.84130(17) 0.0517(7) Uani 1 1 d . . . . . H12A H 0.6396 0.6310 0.8123 0.078 Uiso 1 1 calc R U . . . H12B H 0.7565 0.5031 0.8241 0.078 Uiso 1 1 calc R U . . . H12C H 0.6733 0.5545 0.8880 0.078 Uiso 1 1 calc R U . . . C72 C 0.0676(3) 0.6782(2) 0.78401(13) 0.0362(5) Uani 1 1 d . . . . . H72 H 0.0784 0.6060 0.7626 0.043 Uiso 1 1 calc R U . . . C82 C -0.0718(3) 0.7033(2) 0.82159(14) 0.0406(6) Uani 1 1 d . . . . . H82A H -0.0902 0.7803 0.8379 0.061 Uiso 1 1 calc R U . . . H82B H -0.0743 0.6341 0.8605 0.061 Uiso 1 1 calc R U . . . H82C H -0.1404 0.7116 0.7905 0.061 Uiso 1 1 calc R U . . . C92 C 0.0735(3) 0.7908(3) 0.72665(14) 0.0441(6) Uani 1 1 d . . . . . H92A H -0.0042 0.8127 0.6989 0.066 Uiso 1 1 calc R U . . . H92B H 0.1571 0.7707 0.6980 0.066 Uiso 1 1 calc R U . . . H92C H 0.0714 0.8611 0.7463 0.066 Uiso 1 1 calc R U . . . C13 C 0.5049(2) 0.1857(2) 0.67795(12) 0.0321(5) Uani 1 1 d . . . . . C63 C 0.6185(2) 0.1181(2) 0.71571(13) 0.0351(5) Uani 1 1 d . . . . . C53 C 0.6828(3) -0.0029(2) 0.70841(14) 0.0417(6) Uani 1 1 d . . . . . H53 H 0.7606 -0.0485 0.7328 0.050 Uiso 1 1 calc R U . . . C43 C 0.6359(3) -0.0580(2) 0.66661(15) 0.0468(7) Uani 1 1 d . . . . . H43 H 0.6827 -0.1395 0.6610 0.056 Uiso 1 1 calc R U . . . C33 C 0.5204(3) 0.0068(2) 0.63303(14) 0.0428(6) Uani 1 1 d . . . . . H33 H 0.4865 -0.0323 0.6056 0.051 Uiso 1 1 calc R U . . . C23 C 0.4516(3) 0.1284(2) 0.63820(13) 0.0373(6) Uani 1 1 d . . . . . C103 C 0.6707(3) 0.1736(2) 0.76413(13) 0.0368(6) Uani 1 1 d . . . . . H103 H 0.5926 0.2377 0.7798 0.044 Uiso 1 1 calc R U . . . C113 C 0.7258(3) 0.0770(3) 0.82759(15) 0.0480(7) Uani 1 1 d . . . . . H11G H 0.6590 0.0316 0.8482 0.072 Uiso 1 1 calc R U . . . H11H H 0.7443 0.1189 0.8605 0.072 Uiso 1 1 calc R U . . . H11I H 0.8095 0.0186 0.8146 0.072 Uiso 1 1 calc R U . . . C123 C 0.7782(3) 0.2386(3) 0.72965(16) 0.0508(7) Uani 1 1 d . . . . . H12D H 0.8529 0.1798 0.7101 0.076 Uiso 1 1 calc R U . . . H12E H 0.8121 0.2687 0.7633 0.076 Uiso 1 1 calc R U . . . H12F H 0.7388 0.3088 0.6934 0.076 Uiso 1 1 calc R U . . . C73 C 0.3204(3) 0.1890(2) 0.60306(13) 0.0406(6) Uani 1 1 d . . . . . H73 H 0.2829 0.2739 0.6127 0.049 Uiso 1 1 calc R U . . . C83 C 0.2185(3) 0.1137(3) 0.63344(16) 0.0486(7) Uani 1 1 d . . . . . H83A H 0.2540 0.0293 0.6253 0.073 Uiso 1 1 calc R U . . . H83B H 0.1328 0.1538 0.6118 0.073 Uiso 1 1 calc R U . . . H83C H 0.2036 0.1099 0.6826 0.073 Uiso 1 1 calc R U . . . C93 C 0.3395(3) 0.2024(3) 0.52559(15) 0.0527(7) Uani 1 1 d . . . . . H93A H 0.4006 0.2547 0.5067 0.079 Uiso 1 1 calc R U . . . H93B H 0.2519 0.2410 0.5056 0.079 Uiso 1 1 calc R U . . . H93C H 0.3782 0.1203 0.5149 0.079 Uiso 1 1 calc R U . . . C55 C 0.2338(3) -0.0166(2) 0.97918(13) 0.0382(6) Uani 1 1 d . . . . . H55A H 0.1953 -0.0886 0.9922 0.046 Uiso 1 1 calc R U . . . H55B H 0.3225 -0.0404 0.9991 0.046 Uiso 1 1 calc R U . . . C65 C 0.1370(3) 0.0963(2) 1.00550(13) 0.0370(5) Uani 1 1 d . . . . . H65A H 0.1446 0.0849 1.0550 0.044 Uiso 1 1 calc R U . . . H65B H 0.0425 0.1035 0.9978 0.044 Uiso 1 1 calc R U . . . C25 C 0.4050(3) -0.0564(3) 0.84101(15) 0.0479(7) Uani 1 1 d . . . . . H25A H 0.3945 -0.1381 0.8409 0.072 Uiso 1 1 calc R U . . . H25B H 0.4848 -0.0670 0.8653 0.072 Uiso 1 1 calc R U . . . H25C H 0.4161 -0.0111 0.7940 0.072 Uiso 1 1 calc R U . . . C15 C 0.0967(3) 0.0445(3) 0.84457(15) 0.0464(7) Uani 1 1 d . . . . . H15A H 0.0181 0.0865 0.8706 0.070 Uiso 1 1 calc R U . . . H15B H 0.0907 -0.0388 0.8447 0.070 Uiso 1 1 calc R U . . . H15C H 0.0986 0.0923 0.7975 0.070 Uiso 1 1 calc R U . . . C45 C 0.3092(4) 0.2783(3) 1.00173(16) 0.0588(8) Uani 1 1 d . . . . . H45A H 0.3899 0.2077 1.0084 0.088 Uiso 1 1 calc R U . . . H45B H 0.2691 0.2954 1.0461 0.088 Uiso 1 1 calc R U . . . H45C H 0.3341 0.3515 0.9738 0.088 Uiso 1 1 calc R U . . . C35 C 0.0401(3) 0.3772(3) 0.93432(16) 0.0547(8) Uani 1 1 d . . . . . H35A H 0.0722 0.4444 0.9038 0.082 Uiso 1 1 calc R U . . . H35B H -0.0057 0.4048 0.9755 0.082 Uiso 1 1 calc R U . . . H35C H -0.0232 0.3548 0.9110 0.082 Uiso 1 1 calc R U . . . C14 C 0.0976(2) 0.3826(2) 0.72381(13) 0.0349(5) Uani 1 1 d . . . . . H14A H 0.0956 0.2980 0.7223 0.042 Uiso 1 1 calc R U . . . H14B H 0.0346 0.4062 0.7624 0.042 Uiso 1 1 calc R U . . . C34 C -0.1440(3) 0.5977(3) 0.66590(16) 0.0559(8) Uani 1 1 d . . . . . H34A H -0.1821 0.6518 0.6238 0.084 Uiso 1 1 calc R U . . . H34B H -0.1291 0.6484 0.6951 0.084 Uiso 1 1 calc R U . . . H34C H -0.2070 0.5502 0.6899 0.084 Uiso 1 1 calc R U . . . C44 C 0.1347(3) 0.5795(3) 0.59310(15) 0.0532(8) Uani 1 1 d . . . . . H44A H 0.2165 0.5231 0.5769 0.080 Uiso 1 1 calc R U . . . H44B H 0.1593 0.6268 0.6213 0.080 Uiso 1 1 calc R U . . . H44C H 0.0879 0.6369 0.5540 0.080 Uiso 1 1 calc R U . . . C24 C -0.0246(3) 0.4040(3) 0.58637(14) 0.0434(6) Uani 1 1 d . . . . . H24A H 0.0576 0.3611 0.5629 0.065 Uiso 1 1 calc R U . . . H24B H -0.0845 0.4639 0.5527 0.065 Uiso 1 1 calc R U . . . H24C H -0.0709 0.3432 0.6130 0.065 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0320(2) 0.02190(19) 0.0283(2) -0.00096(14) -0.00306(14) -0.00630(15) Si15 0.0407(4) 0.0261(3) 0.0338(3) -0.0017(3) -0.0010(3) -0.0103(3) Si25 0.0453(4) 0.0277(3) 0.0333(4) -0.0026(3) 0.0001(3) -0.0117(3) Si14 0.0408(4) 0.0328(4) 0.0344(4) -0.0027(3) -0.0087(3) -0.0082(3) N1 0.0327(10) 0.0273(10) 0.0333(10) 0.0014(8) -0.0059(8) -0.0071(8) N2 0.0372(11) 0.0246(10) 0.0311(10) 0.0015(8) -0.0030(8) -0.0080(8) N21 0.0352(10) 0.0215(9) 0.0307(10) -0.0015(8) -0.0035(8) -0.0043(8) N11 0.0305(10) 0.0223(9) 0.0329(10) -0.0019(8) -0.0046(8) -0.0046(8) C11 0.0428(14) 0.0284(13) 0.0447(14) -0.0032(11) -0.0015(11) -0.0135(11) C21 0.0353(12) 0.0239(11) 0.0332(12) 0.0018(9) -0.0065(10) -0.0072(10) C31 0.0402(13) 0.0276(12) 0.0320(12) 0.0024(10) -0.0024(10) -0.0115(10) C41 0.0347(12) 0.0259(12) 0.0304(12) -0.0004(9) -0.0039(9) -0.0057(10) C51 0.0484(15) 0.0331(13) 0.0347(13) -0.0024(10) 0.0039(11) -0.0114(12) C12 0.0370(13) 0.0226(11) 0.0332(12) -0.0016(9) -0.0057(10) -0.0097(10) C62 0.0358(13) 0.0270(12) 0.0356(13) -0.0022(10) -0.0060(10) -0.0098(10) C52 0.0411(14) 0.0289(12) 0.0378(13) -0.0035(10) -0.0092(11) -0.0094(11) C42 0.0465(15) 0.0281(12) 0.0347(13) -0.0065(10) -0.0043(11) -0.0094(11) C32 0.0386(13) 0.0241(12) 0.0402(14) -0.0072(10) -0.0027(10) -0.0044(10) C22 0.0367(13) 0.0232(11) 0.0370(13) 0.0009(9) -0.0064(10) -0.0085(10) C102 0.0333(13) 0.0388(14) 0.0402(14) -0.0090(11) -0.0063(10) -0.0072(11) C112 0.0442(15) 0.0423(15) 0.0432(15) -0.0095(12) -0.0097(12) 0.0018(12) C122 0.0407(15) 0.0613(19) 0.0598(19) -0.0197(15) -0.0021(13) -0.0192(14) C72 0.0373(13) 0.0278(12) 0.0428(14) -0.0087(10) -0.0086(11) -0.0041(10) C82 0.0385(14) 0.0312(13) 0.0484(15) -0.0047(11) -0.0065(11) -0.0056(11) C92 0.0442(15) 0.0430(15) 0.0395(14) -0.0021(12) -0.0066(11) -0.0073(12) C13 0.0359(13) 0.0228(11) 0.0327(12) -0.0037(9) 0.0023(10) -0.0041(10) C63 0.0357(13) 0.0253(12) 0.0381(13) -0.0010(10) 0.0012(10) -0.0049(10) C53 0.0412(14) 0.0274(13) 0.0470(15) -0.0034(11) 0.0007(11) -0.0002(11) C43 0.0546(17) 0.0280(13) 0.0507(16) -0.0092(12) 0.0048(13) -0.0034(12) C33 0.0544(16) 0.0312(13) 0.0437(15) -0.0124(11) 0.0027(12) -0.0119(12) C23 0.0456(14) 0.0289(12) 0.0335(13) -0.0038(10) 0.0019(11) -0.0085(11) C103 0.0361(13) 0.0274(12) 0.0424(14) -0.0020(10) -0.0051(11) -0.0053(10) C113 0.0562(17) 0.0364(14) 0.0465(16) 0.0024(12) -0.0132(13) -0.0100(13) C123 0.0495(16) 0.0482(17) 0.0528(17) 0.0013(13) -0.0069(13) -0.0187(14) C73 0.0525(16) 0.0312(13) 0.0396(14) -0.0077(11) -0.0061(12) -0.0121(12) C83 0.0524(17) 0.0385(15) 0.0559(18) -0.0101(13) -0.0049(13) -0.0133(13) C93 0.067(2) 0.0530(18) 0.0404(15) -0.0092(13) -0.0053(13) -0.0187(15) C55 0.0451(14) 0.0266(12) 0.0387(14) -0.0003(10) -0.0016(11) -0.0092(11) C65 0.0430(14) 0.0301(13) 0.0351(13) -0.0018(10) -0.0010(10) -0.0108(11) C25 0.0565(17) 0.0353(14) 0.0484(16) -0.0064(12) 0.0081(13) -0.0140(13) C15 0.0566(17) 0.0419(15) 0.0442(15) -0.0025(12) -0.0070(13) -0.0228(13) C45 0.076(2) 0.068(2) 0.0472(17) -0.0197(15) 0.0060(15) -0.0402(18) C35 0.0641(19) 0.0318(14) 0.0514(17) 0.0010(12) 0.0133(14) -0.0027(14) C14 0.0365(13) 0.0307(12) 0.0355(13) -0.0044(10) -0.0027(10) -0.0081(10) C34 0.0625(19) 0.0492(17) 0.0494(17) -0.0129(14) -0.0196(14) 0.0036(15) C44 0.070(2) 0.0491(17) 0.0441(16) 0.0099(13) -0.0204(14) -0.0315(15) C24 0.0527(16) 0.0436(15) 0.0349(13) -0.0027(11) -0.0059(12) -0.0179(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.7494(19) . ? Fe1 N21 2.036(2) . ? Fe1 C14 2.065(2) . ? Fe1 N11 2.0665(19) . ? Si15 N2 1.788(2) . ? Si15 C25 1.847(3) . ? Si15 C15 1.861(3) . ? Si15 C55 1.875(3) . ? Si25 N2 1.785(2) . ? Si25 C35 1.847(3) . ? Si25 C45 1.855(3) . ? Si25 C65 1.879(2) . ? Si14 C44 1.866(3) . ? Si14 C14 1.870(2) . ? Si14 C24 1.877(3) . ? Si14 C34 1.878(3) . ? N1 N2 1.325(3) . ? N21 C41 1.340(3) . ? N21 C13 1.448(3) . ? N11 C21 1.333(3) . ? N11 C12 1.439(3) . ? C11 C21 1.512(3) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C21 C31 1.407(4) . ? C31 C41 1.402(3) . ? C31 H31 0.9500 . ? C41 C51 1.511(3) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C12 C62 1.413(3) . ? C12 C22 1.414(4) . ? C62 C52 1.395(4) . ? C62 C102 1.524(4) . ? C52 C42 1.381(4) . ? C52 H52 0.9500 . ? C42 C32 1.389(4) . ? C42 H42 0.9500 . ? C32 C22 1.392(4) . ? C32 H32 0.9500 . ? C22 C72 1.529(3) . ? C102 C112 1.531(4) . ? C102 C122 1.536(4) . ? C102 H102 1.0000 . ? C112 H11D 0.9800 . ? C112 H11E 0.9800 . ? C112 H11F 0.9800 . ? C122 H12A 0.9800 . ? C122 H12B 0.9800 . ? C122 H12C 0.9800 . ? C72 C82 1.527(4) . ? C72 C92 1.530(4) . ? C72 H72 1.0000 . ? C82 H82A 0.9800 . ? C82 H82B 0.9800 . ? C82 H82C 0.9800 . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C13 C23 1.407(4) . ? C13 C63 1.411(3) . ? C63 C53 1.394(4) . ? C63 C103 1.521(4) . ? C53 C43 1.381(4) . ? C53 H53 0.9500 . ? C43 C33 1.379(4) . ? C43 H43 0.9500 . ? C33 C23 1.397(4) . ? C33 H33 0.9500 . ? C23 C73 1.519(4) . ? C103 C123 1.526(4) . ? C103 C113 1.532(3) . ? C103 H103 1.0000 . ? C113 H11G 0.9800 . ? C113 H11H 0.9800 . ? C113 H11I 0.9800 . ? C123 H12D 0.9800 . ? C123 H12E 0.9800 . ? C123 H12F 0.9800 . ? C73 C93 1.532(4) . ? C73 C83 1.537(4) . ? C73 H73 1.0000 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C55 C65 1.556(4) . ? C55 H55A 0.9900 . ? C55 H55B 0.9900 . ? C65 H65A 0.9900 . ? C65 H65B 0.9900 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N21 112.85(9) . . ? N1 Fe1 C14 102.39(9) . . ? N21 Fe1 C14 116.42(9) . . ? N1 Fe1 N11 113.28(9) . . ? N21 Fe1 N11 93.31(8) . . ? C14 Fe1 N11 119.15(9) . . ? N2 Si15 C25 112.62(12) . . ? N2 Si15 C15 108.09(11) . . ? C25 Si15 C15 111.61(14) . . ? N2 Si15 C55 95.40(10) . . ? C25 Si15 C55 117.00(13) . . ? C15 Si15 C55 110.83(13) . . ? N2 Si25 C35 108.80(12) . . ? N2 Si25 C45 111.46(13) . . ? C35 Si25 C45 111.33(17) . . ? N2 Si25 C65 97.21(11) . . ? C35 Si25 C65 114.29(13) . . ? C45 Si25 C65 112.90(14) . . ? C44 Si14 C14 112.60(12) . . ? C44 Si14 C24 106.55(13) . . ? C14 Si14 C24 113.62(12) . . ? C44 Si14 C34 108.86(16) . . ? C14 Si14 C34 110.95(13) . . ? C24 Si14 C34 103.77(14) . . ? N2 N1 Fe1 158.36(17) . . ? N1 N2 Si25 121.29(16) . . ? N1 N2 Si15 123.75(16) . . ? Si25 N2 Si15 114.29(11) . . ? C41 N21 C13 117.3(2) . . ? C41 N21 Fe1 119.96(16) . . ? C13 N21 Fe1 122.75(15) . . ? C21 N11 C12 118.39(19) . . ? C21 N11 Fe1 119.87(16) . . ? C12 N11 Fe1 121.54(14) . . ? C21 C11 H11A 109.5 . . ? C21 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C21 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N11 C21 C31 124.0(2) . . ? N11 C21 C11 121.2(2) . . ? C31 C21 C11 114.8(2) . . ? C41 C31 C21 129.8(2) . . ? C41 C31 H31 115.1 . . ? C21 C31 H31 115.1 . . ? N21 C41 C31 123.8(2) . . ? N21 C41 C51 119.9(2) . . ? C31 C41 C51 116.4(2) . . ? C41 C51 H51A 109.5 . . ? C41 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C41 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C62 C12 C22 120.2(2) . . ? C62 C12 N11 119.3(2) . . ? C22 C12 N11 120.5(2) . . ? C52 C62 C12 118.7(2) . . ? C52 C62 C102 118.3(2) . . ? C12 C62 C102 123.0(2) . . ? C42 C52 C62 121.3(2) . . ? C42 C52 H52 119.3 . . ? C62 C52 H52 119.3 . . ? C52 C42 C32 119.7(2) . . ? C52 C42 H42 120.1 . . ? C32 C42 H42 120.1 . . ? C42 C32 C22 121.2(2) . . ? C42 C32 H32 119.4 . . ? C22 C32 H32 119.4 . . ? C32 C22 C12 118.8(2) . . ? C32 C22 C72 119.5(2) . . ? C12 C22 C72 121.6(2) . . ? C62 C102 C112 110.1(2) . . ? C62 C102 C122 111.8(2) . . ? C112 C102 C122 109.8(2) . . ? C62 C102 H102 108.4 . . ? C112 C102 H102 108.4 . . ? C122 C102 H102 108.4 . . ? C102 C112 H11D 109.5 . . ? C102 C112 H11E 109.5 . . ? H11D C112 H11E 109.5 . . ? C102 C112 H11F 109.5 . . ? H11D C112 H11F 109.5 . . ? H11E C112 H11F 109.5 . . ? C102 C122 H12A 109.5 . . ? C102 C122 H12B 109.5 . . ? H12A C122 H12B 109.5 . . ? C102 C122 H12C 109.5 . . ? H12A C122 H12C 109.5 . . ? H12B C122 H12C 109.5 . . ? C82 C72 C22 113.3(2) . . ? C82 C72 C92 109.0(2) . . ? C22 C72 C92 111.3(2) . . ? C82 C72 H72 107.7 . . ? C22 C72 H72 107.7 . . ? C92 C72 H72 107.7 . . ? C72 C82 H82A 109.5 . . ? C72 C82 H82B 109.5 . . ? H82A C82 H82B 109.5 . . ? C72 C82 H82C 109.5 . . ? H82A C82 H82C 109.5 . . ? H82B C82 H82C 109.5 . . ? C72 C92 H92A 109.5 . . ? C72 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C72 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C23 C13 C63 120.4(2) . . ? C23 C13 N21 121.2(2) . . ? C63 C13 N21 118.4(2) . . ? C53 C63 C13 118.6(2) . . ? C53 C63 C103 119.8(2) . . ? C13 C63 C103 121.6(2) . . ? C43 C53 C63 121.5(3) . . ? C43 C53 H53 119.2 . . ? C63 C53 H53 119.2 . . ? C33 C43 C53 119.2(2) . . ? C33 C43 H43 120.4 . . ? C53 C43 H43 120.4 . . ? C43 C33 C23 121.9(3) . . ? C43 C33 H33 119.0 . . ? C23 C33 H33 119.0 . . ? C33 C23 C13 118.2(2) . . ? C33 C23 C73 118.0(2) . . ? C13 C23 C73 123.8(2) . . ? C63 C103 C123 112.5(2) . . ? C63 C103 C113 112.4(2) . . ? C123 C103 C113 109.4(2) . . ? C63 C103 H103 107.4 . . ? C123 C103 H103 107.4 . . ? C113 C103 H103 107.4 . . ? C103 C113 H11G 109.5 . . ? C103 C113 H11H 109.5 . . ? H11G C113 H11H 109.5 . . ? C103 C113 H11I 109.5 . . ? H11G C113 H11I 109.5 . . ? H11H C113 H11I 109.5 . . ? C103 C123 H12D 109.5 . . ? C103 C123 H12E 109.5 . . ? H12D C123 H12E 109.5 . . ? C103 C123 H12F 109.5 . . ? H12D C123 H12F 109.5 . . ? H12E C123 H12F 109.5 . . ? C23 C73 C93 112.8(2) . . ? C23 C73 C83 109.2(2) . . ? C93 C73 C83 110.5(2) . . ? C23 C73 H73 108.0 . . ? C93 C73 H73 108.0 . . ? C83 C73 H73 108.0 . . ? C73 C83 H83A 109.5 . . ? C73 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C73 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? C73 C93 H93A 109.5 . . ? C73 C93 H93B 109.5 . . ? H93A C93 H93B 109.5 . . ? C73 C93 H93C 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C65 C55 Si15 107.17(16) . . ? C65 C55 H55A 110.3 . . ? Si15 C55 H55A 110.3 . . ? C65 C55 H55B 110.3 . . ? Si15 C55 H55B 110.3 . . ? H55A C55 H55B 108.5 . . ? C55 C65 Si25 108.46(17) . . ? C55 C65 H65A 110.0 . . ? Si25 C65 H65A 110.0 . . ? C55 C65 H65B 110.0 . . ? Si25 C65 H65B 110.0 . . ? H65A C65 H65B 108.4 . . ? Si15 C25 H25A 109.5 . . ? Si15 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? Si15 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? Si15 C15 H15A 109.5 . . ? Si15 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? Si15 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? Si25 C45 H45A 109.5 . . ? Si25 C45 H45B 109.5 . . ? H45A C45 H45B 109.5 . . ? Si25 C45 H45C 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? Si25 C35 H35A 109.5 . . ? Si25 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? Si25 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? Si14 C14 Fe1 123.88(13) . . ? Si14 C14 H14A 106.4 . . ? Fe1 C14 H14A 106.4 . . ? Si14 C14 H14B 106.4 . . ? Fe1 C14 H14B 106.4 . . ? H14A C14 H14B 106.4 . . ? Si14 C34 H34A 109.5 . . ? Si14 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? Si14 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? Si14 C44 H44A 109.5 . . ? Si14 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? Si14 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? Si14 C24 H24A 109.5 . . ? Si14 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? Si14 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N21 Fe1 N1 N2 -130.3(5) . . . . ? C14 Fe1 N1 N2 -4.4(5) . . . . ? N11 Fe1 N1 N2 125.2(5) . . . . ? Fe1 N1 N2 Si25 -89.7(5) . . . . ? Fe1 N1 N2 Si15 80.5(5) . . . . ? C35 Si25 N2 N1 54.0(2) . . . . ? C45 Si25 N2 N1 -69.2(2) . . . . ? C65 Si25 N2 N1 172.73(18) . . . . ? C35 Si25 N2 Si15 -117.00(15) . . . . ? C45 Si25 N2 Si15 119.86(15) . . . . ? C65 Si25 N2 Si15 1.75(14) . . . . ? C25 Si15 N2 N1 44.5(2) . . . . ? C15 Si15 N2 N1 -79.3(2) . . . . ? C55 Si15 N2 N1 166.73(19) . . . . ? C25 Si15 N2 Si25 -144.78(14) . . . . ? C15 Si15 N2 Si25 91.46(14) . . . . ? C55 Si15 N2 Si25 -22.54(14) . . . . ? C12 N11 C21 C31 166.1(2) . . . . ? Fe1 N11 C21 C31 -8.9(3) . . . . ? C12 N11 C21 C11 -11.2(3) . . . . ? Fe1 N11 C21 C11 173.76(17) . . . . ? N11 C21 C31 C41 -16.6(4) . . . . ? C11 C21 C31 C41 160.9(3) . . . . ? C13 N21 C41 C31 -165.6(2) . . . . ? Fe1 N21 C41 C31 16.1(3) . . . . ? C13 N21 C41 C51 13.6(3) . . . . ? Fe1 N21 C41 C51 -164.73(17) . . . . ? C21 C31 C41 N21 12.6(4) . . . . ? C21 C31 C41 C51 -166.7(2) . . . . ? C21 N11 C12 C62 -75.0(3) . . . . ? Fe1 N11 C12 C62 100.0(2) . . . . ? C21 N11 C12 C22 107.3(3) . . . . ? Fe1 N11 C12 C22 -77.8(2) . . . . ? C22 C12 C62 C52 0.3(3) . . . . ? N11 C12 C62 C52 -177.4(2) . . . . ? C22 C12 C62 C102 179.5(2) . . . . ? N11 C12 C62 C102 1.8(3) . . . . ? C12 C62 C52 C42 0.6(4) . . . . ? C102 C62 C52 C42 -178.6(2) . . . . ? C62 C52 C42 C32 -1.1(4) . . . . ? C52 C42 C32 C22 0.7(4) . . . . ? C42 C32 C22 C12 0.2(3) . . . . ? C42 C32 C22 C72 -177.4(2) . . . . ? C62 C12 C22 C32 -0.7(3) . . . . ? N11 C12 C22 C32 177.0(2) . . . . ? C62 C12 C22 C72 176.9(2) . . . . ? N11 C12 C22 C72 -5.4(3) . . . . ? C52 C62 C102 C112 67.8(3) . . . . ? C12 C62 C102 C112 -111.4(3) . . . . ? C52 C62 C102 C122 -54.5(3) . . . . ? C12 C62 C102 C122 126.3(3) . . . . ? C32 C22 C72 C82 -26.2(3) . . . . ? C12 C22 C72 C82 156.2(2) . . . . ? C32 C22 C72 C92 97.1(3) . . . . ? C12 C22 C72 C92 -80.5(3) . . . . ? C41 N21 C13 C23 -91.8(3) . . . . ? Fe1 N21 C13 C23 86.5(2) . . . . ? C41 N21 C13 C63 89.1(3) . . . . ? Fe1 N21 C13 C63 -92.6(2) . . . . ? C23 C13 C63 C53 5.1(4) . . . . ? N21 C13 C63 C53 -175.8(2) . . . . ? C23 C13 C63 C103 -174.3(2) . . . . ? N21 C13 C63 C103 4.8(3) . . . . ? C13 C63 C53 C43 -1.5(4) . . . . ? C103 C63 C53 C43 177.9(2) . . . . ? C63 C53 C43 C33 -2.1(4) . . . . ? C53 C43 C33 C23 2.2(4) . . . . ? C43 C33 C23 C13 1.3(4) . . . . ? C43 C33 C23 C73 -176.1(2) . . . . ? C63 C13 C23 C33 -5.0(4) . . . . ? N21 C13 C23 C33 175.9(2) . . . . ? C63 C13 C23 C73 172.2(2) . . . . ? N21 C13 C23 C73 -6.9(4) . . . . ? C53 C63 C103 C123 89.1(3) . . . . ? C13 C63 C103 C123 -91.5(3) . . . . ? C53 C63 C103 C113 -34.9(3) . . . . ? C13 C63 C103 C113 144.5(2) . . . . ? C33 C23 C73 C93 -62.3(3) . . . . ? C13 C23 C73 C93 120.5(3) . . . . ? C33 C23 C73 C83 61.0(3) . . . . ? C13 C23 C73 C83 -116.2(3) . . . . ? N2 Si15 C55 C65 39.59(18) . . . . ? C25 Si15 C55 C65 158.39(17) . . . . ? C15 Si15 C55 C65 -72.1(2) . . . . ? Si15 C55 C65 Si25 -42.7(2) . . . . ? N2 Si25 C65 C55 25.65(19) . . . . ? C35 Si25 C65 C55 140.07(19) . . . . ? C45 Si25 C65 C55 -91.3(2) . . . . ? C44 Si14 C14 Fe1 -1.2(2) . . . . ? C24 Si14 C14 Fe1 120.00(16) . . . . ? C34 Si14 C14 Fe1 -123.55(17) . . . . ? _refine_diff_density_max 0.542 _refine_diff_density_min -0.586 _refine_diff_density_rms 0.050 _shelx_res_file ; 007a-22088.res created by SHELXL-2014/7 TITL 007a-22088 CELL 1.54184 10.38 11.5329 20.2705 76 82.547 72.992 ZERR 2 0.0004 0.0004 0.0006 0.003 0.003 0.003 LATT 1 SFAC C H Fe N Si UNIT 78 136 2 8 6 L.S. 30 TEMP -180 SIZE 0.20 0.20 0.10 CONF MORE -1 BOND $H ABIN ACTA WGHT 0.061900 1.765600 FVAR 0.83071 FE1 3 0.288545 0.366583 0.750315 11.00000 0.03196 0.02190 = 0.02826 -0.00096 -0.00306 -0.00630 SI15 5 0.253630 0.032088 0.884081 11.00000 0.04074 0.02610 = 0.03384 -0.00167 -0.00104 -0.01032 SI25 5 0.185039 0.240654 0.958066 11.00000 0.04528 0.02768 = 0.03326 -0.00263 0.00008 -0.01172 SI14 5 0.020996 0.487727 0.644753 11.00000 0.04079 0.03278 = 0.03444 -0.00266 -0.00873 -0.00816 N1 4 0.299505 0.260395 0.828685 11.00000 0.03268 0.02729 = 0.03333 0.00137 -0.00590 -0.00710 N2 4 0.260332 0.185595 0.883168 11.00000 0.03719 0.02458 = 0.03108 0.00152 -0.00302 -0.00797 N21 4 0.444165 0.314102 0.681998 11.00000 0.03525 0.02146 = 0.03069 -0.00151 -0.00351 -0.00426 N11 4 0.340637 0.525141 0.752867 11.00000 0.03051 0.02226 = 0.03288 -0.00194 -0.00462 -0.00465 C11 1 0.436460 0.700621 0.696775 11.00000 0.04276 0.02840 = 0.04471 -0.00320 -0.00146 -0.01349 AFIX 137 H11A 2 0.376702 0.741401 0.730918 11.00000 -1.50000 H11B 2 0.419761 0.753801 0.651339 11.00000 -1.50000 H11C 2 0.530710 0.686302 0.706273 11.00000 -1.50000 AFIX 0 C21 1 0.409014 0.577764 0.699547 11.00000 0.03529 0.02387 = 0.03319 0.00180 -0.00647 -0.00723 C31 1 0.465573 0.523544 0.643551 11.00000 0.04020 0.02764 = 0.03204 0.00238 -0.00238 -0.01153 AFIX 43 H31 2 0.489385 0.578892 0.604084 11.00000 -1.20000 AFIX 0 C41 1 0.492117 0.400265 0.637160 11.00000 0.03474 0.02589 = 0.03043 -0.00041 -0.00391 -0.00566 C51 1 0.581748 0.365879 0.575968 11.00000 0.04841 0.03308 = 0.03467 -0.00238 0.00393 -0.01144 AFIX 137 H51A 2 0.659028 0.295441 0.591200 11.00000 -1.50000 H51B 2 0.614097 0.436970 0.550713 11.00000 -1.50000 H51C 2 0.530239 0.342931 0.546313 11.00000 -1.50000 AFIX 0 C12 1 0.314518 0.575406 0.813221 11.00000 0.03698 0.02262 = 0.03321 -0.00159 -0.00571 -0.00969 C62 1 0.420672 0.551112 0.856082 11.00000 0.03580 0.02696 = 0.03559 -0.00219 -0.00603 -0.00983 C52 1 0.392794 0.596101 0.915871 11.00000 0.04107 0.02888 = 0.03776 -0.00345 -0.00924 -0.00941 AFIX 43 H52 2 0.463654 0.580928 0.944802 11.00000 -1.20000 AFIX 0 C42 1 0.264227 0.662260 0.933839 11.00000 0.04647 0.02813 = 0.03472 -0.00645 -0.00426 -0.00940 AFIX 43 H42 2 0.246842 0.690945 0.975132 11.00000 -1.20000 AFIX 0 C32 1 0.160493 0.686663 0.891282 11.00000 0.03864 0.02411 = 0.04018 -0.00719 -0.00271 -0.00435 AFIX 43 H32 2 0.072462 0.732941 0.903632 11.00000 -1.20000 AFIX 0 C22 1 0.183177 0.644548 0.830876 11.00000 0.03668 0.02325 = 0.03702 0.00087 -0.00640 -0.00855 C102 1 0.564260 0.476424 0.840501 11.00000 0.03333 0.03878 = 0.04021 -0.00903 -0.00627 -0.00722 AFIX 13 H102 2 0.569803 0.459270 0.794011 11.00000 -1.20000 AFIX 0 C112 1 0.598626 0.352138 0.891942 11.00000 0.04422 0.04230 = 0.04322 -0.00950 -0.00971 0.00183 AFIX 137 H11D 2 0.586366 0.367173 0.938203 11.00000 -1.50000 H11E 2 0.692660 0.306773 0.883019 11.00000 -1.50000 H11F 2 0.538853 0.302900 0.887537 11.00000 -1.50000 AFIX 0 C122 1 0.667785 0.547705 0.841299 11.00000 0.04066 0.06126 = 0.05984 -0.01971 -0.00206 -0.01915 AFIX 137 H12A 2 0.639627 0.630970 0.812299 11.00000 -1.50000 H12B 2 0.756451 0.503091 0.824063 11.00000 -1.50000 H12C 2 0.673340 0.554538 0.888046 11.00000 -1.50000 AFIX 0 C72 1 0.067551 0.678158 0.784011 11.00000 0.03732 0.02778 = 0.04282 -0.00875 -0.00861 -0.00412 AFIX 13 H72 2 0.078360 0.606038 0.762607 11.00000 -1.20000 AFIX 0 C82 1 -0.071832 0.703275 0.821589 11.00000 0.03853 0.03117 = 0.04836 -0.00467 -0.00648 -0.00555 AFIX 137 H82A 2 -0.090223 0.780270 0.837882 11.00000 -1.50000 H82B 2 -0.074255 0.634117 0.860471 11.00000 -1.50000 H82C 2 -0.140448 0.711552 0.790524 11.00000 -1.50000 AFIX 0 C92 1 0.073519 0.790787 0.726649 11.00000 0.04415 0.04302 = 0.03953 -0.00215 -0.00659 -0.00726 AFIX 137 H92A 2 -0.004198 0.812720 0.698909 11.00000 -1.50000 H92B 2 0.157130 0.770657 0.698027 11.00000 -1.50000 H92C 2 0.071447 0.861130 0.746267 11.00000 -1.50000 AFIX 0 C13 1 0.504944 0.185672 0.677955 11.00000 0.03594 0.02279 = 0.03267 -0.00367 0.00230 -0.00407 C63 1 0.618518 0.118068 0.715707 11.00000 0.03570 0.02526 = 0.03811 -0.00099 0.00117 -0.00490 C53 1 0.682793 -0.002913 0.708410 11.00000 0.04123 0.02740 = 0.04701 -0.00338 0.00072 -0.00024 AFIX 43 H53 2 0.760639 -0.048515 0.732764 11.00000 -1.20000 AFIX 0 C43 1 0.635930 -0.057987 0.666609 11.00000 0.05463 0.02800 = 0.05065 -0.00925 0.00484 -0.00345 AFIX 43 H43 2 0.682707 -0.139512 0.661045 11.00000 -1.20000 AFIX 0 C33 1 0.520362 0.006819 0.633027 11.00000 0.05440 0.03123 = 0.04366 -0.01239 0.00266 -0.01187 AFIX 43 H33 2 0.486488 -0.032348 0.605579 11.00000 -1.20000 AFIX 0 C23 1 0.451647 0.128389 0.638195 11.00000 0.04558 0.02895 = 0.03347 -0.00385 0.00186 -0.00846 C103 1 0.670676 0.173612 0.764133 11.00000 0.03614 0.02736 = 0.04237 -0.00201 -0.00505 -0.00527 AFIX 13 H103 2 0.592614 0.237708 0.779782 11.00000 -1.20000 AFIX 0 C113 1 0.725833 0.076998 0.827586 11.00000 0.05622 0.03641 = 0.04652 0.00241 -0.01318 -0.00999 AFIX 137 H11G 2 0.659005 0.031640 0.848155 11.00000 -1.50000 H11H 2 0.744275 0.118928 0.860542 11.00000 -1.50000 H11I 2 0.809494 0.018638 0.814640 11.00000 -1.50000 AFIX 0 C123 1 0.778233 0.238553 0.729647 11.00000 0.04949 0.04824 = 0.05278 0.00127 -0.00694 -0.01865 AFIX 137 H12D 2 0.852894 0.179798 0.710068 11.00000 -1.50000 H12E 2 0.812108 0.268748 0.763341 11.00000 -1.50000 H12F 2 0.738758 0.308813 0.693389 11.00000 -1.50000 AFIX 0 C73 1 0.320384 0.188989 0.603055 11.00000 0.05251 0.03119 = 0.03962 -0.00774 -0.00606 -0.01206 AFIX 13 H73 2 0.282904 0.273935 0.612745 11.00000 -1.20000 AFIX 0 C83 1 0.218474 0.113658 0.633435 11.00000 0.05243 0.03846 = 0.05590 -0.01008 -0.00492 -0.01334 AFIX 137 H83A 2 0.254031 0.029335 0.625341 11.00000 -1.50000 H83B 2 0.132778 0.153755 0.611771 11.00000 -1.50000 H83C 2 0.203641 0.109857 0.682564 11.00000 -1.50000 AFIX 0 C93 1 0.339478 0.202448 0.525590 11.00000 0.06653 0.05297 = 0.04039 -0.00925 -0.00528 -0.01873 AFIX 137 H93A 2 0.400582 0.254680 0.506744 11.00000 -1.50000 H93B 2 0.251898 0.240991 0.505589 11.00000 -1.50000 H93C 2 0.378164 0.120281 0.514898 11.00000 -1.50000 AFIX 0 C55 1 0.233773 -0.016566 0.979181 11.00000 0.04514 0.02663 = 0.03870 -0.00034 -0.00155 -0.00922 AFIX 23 H55A 2 0.195332 -0.088626 0.992221 11.00000 -1.20000 H55B 2 0.322467 -0.040433 0.999063 11.00000 -1.20000 AFIX 0 C65 1 0.137012 0.096309 1.005504 11.00000 0.04301 0.03013 = 0.03509 -0.00178 -0.00100 -0.01078 AFIX 23 H65A 2 0.144586 0.084866 1.054989 11.00000 -1.20000 H65B 2 0.042460 0.103530 0.997812 11.00000 -1.20000 AFIX 0 C25 1 0.404997 -0.056410 0.841012 11.00000 0.05645 0.03525 = 0.04836 -0.00643 0.00806 -0.01404 AFIX 137 H25A 2 0.394493 -0.138086 0.840896 11.00000 -1.50000 H25B 2 0.484766 -0.066984 0.865296 11.00000 -1.50000 H25C 2 0.416064 -0.011128 0.793986 11.00000 -1.50000 AFIX 0 C15 1 0.096694 0.044484 0.844565 11.00000 0.05663 0.04194 = 0.04419 -0.00255 -0.00699 -0.02281 AFIX 137 H15A 2 0.018086 0.086520 0.870619 11.00000 -1.50000 H15B 2 0.090748 -0.038840 0.844729 11.00000 -1.50000 H15C 2 0.098597 0.092302 0.797537 11.00000 -1.50000 AFIX 0 C45 1 0.309202 0.278258 1.001731 11.00000 0.07638 0.06771 = 0.04716 -0.01973 0.00597 -0.04024 AFIX 137 H45A 2 0.389948 0.207682 1.008438 11.00000 -1.50000 H45B 2 0.269127 0.295425 1.046055 11.00000 -1.50000 H45C 2 0.334123 0.351531 0.973768 11.00000 -1.50000 AFIX 0 C35 1 0.040066 0.377202 0.934316 11.00000 0.06409 0.03185 = 0.05142 0.00097 0.01327 -0.00266 AFIX 137 H35A 2 0.072189 0.444448 0.903834 11.00000 -1.50000 H35B 2 -0.005669 0.404845 0.975473 11.00000 -1.50000 H35C 2 -0.023246 0.354769 0.911040 11.00000 -1.50000 AFIX 0 C14 1 0.097574 0.382616 0.723810 11.00000 0.03646 0.03072 = 0.03553 -0.00437 -0.00268 -0.00815 AFIX 23 H14A 2 0.095618 0.297991 0.722297 11.00000 -1.20000 H14B 2 0.034625 0.406182 0.762433 11.00000 -1.20000 AFIX 0 C34 1 -0.144034 0.597682 0.665903 11.00000 0.06254 0.04924 = 0.04943 -0.01285 -0.01962 0.00359 AFIX 137 H34A 2 -0.182139 0.651765 0.623772 11.00000 -1.50000 H34B 2 -0.129100 0.648405 0.695085 11.00000 -1.50000 H34C 2 -0.206968 0.550245 0.689888 11.00000 -1.50000 AFIX 0 C44 1 0.134657 0.579527 0.593098 11.00000 0.07044 0.04906 = 0.04413 0.00991 -0.02038 -0.03153 AFIX 137 H44A 2 0.216462 0.523066 0.576907 11.00000 -1.50000 H44B 2 0.159307 0.626845 0.621291 11.00000 -1.50000 H44C 2 0.087884 0.636874 0.553972 11.00000 -1.50000 AFIX 0 C24 1 -0.024650 0.403953 0.586375 11.00000 0.05268 0.04362 = 0.03492 -0.00272 -0.00594 -0.01790 AFIX 137 H24A 2 0.057597 0.361068 0.562949 11.00000 -1.50000 H24B 2 -0.084454 0.463895 0.552673 11.00000 -1.50000 H24C 2 -0.070919 0.343169 0.613029 11.00000 -1.50000 AFIX 0 HKLF 4 REM 007a-22088 REM R1 = 0.0455 for 7241 Fo > 4sig(Fo) and 0.0488 for all 7797 data REM 441 parameters refined using 0 restraints END WGHT 0.0614 1.7538 REM Highest difference peak 0.542, deepest hole -0.586, 1-sigma level 0.050 Q1 1 0.1937 0.3571 0.7645 11.00000 0.05 0.54 Q2 1 0.2851 0.3608 0.7027 11.00000 0.05 0.50 Q3 1 0.3845 0.3750 0.7396 11.00000 0.05 0.46 Q4 1 0.2857 0.3792 0.7994 11.00000 0.05 0.41 Q5 1 -0.0698 0.4974 0.6532 11.00000 0.05 0.38 Q6 1 0.1930 0.2222 0.9073 11.00000 0.05 0.35 Q7 1 0.2520 0.0252 0.9391 11.00000 0.05 0.32 Q8 1 0.2380 0.0269 0.8356 11.00000 0.05 0.32 Q9 1 0.0157 0.4787 0.5949 11.00000 0.05 0.32 Q10 1 0.2015 0.2612 1.0043 11.00000 0.05 0.32 Q11 1 0.3593 0.3084 0.6932 11.00000 0.05 0.30 Q12 1 0.1462 0.0326 0.8907 11.00000 0.05 0.29 Q13 1 0.0928 0.5316 0.6257 11.00000 0.05 0.28 Q14 1 0.2488 0.5009 0.7531 11.00000 0.05 0.27 Q15 1 0.3074 0.2236 0.7637 11.00000 0.05 0.26 Q16 1 0.5358 0.5404 0.6260 11.00000 0.05 0.26 Q17 1 0.1139 0.1777 0.9757 11.00000 0.05 0.26 Q18 1 0.3489 0.0044 0.8771 11.00000 0.05 0.26 Q19 1 0.2801 0.2524 0.9499 11.00000 0.05 0.26 Q20 1 0.2474 -0.0342 0.9314 11.00000 0.05 0.25 ; _shelx_res_checksum 46092 _shelx_fab_file ; 0 0 1 -46.86 0.00 0 0 3 -31.45 0.00 0 0 4 22.09 0.00 0 0 5 -13.87 0.00 0 0 6 7.55 0.00 0 0 7 -3.20 0.00 0 0 8 0.45 0.00 0 0 9 1.14 0.00 0 0 10 -1.95 0.00 0 0 11 2.29 0.00 0 0 12 -2.34 0.00 0 0 13 2.25 0.00 0 0 14 -2.13 0.00 0 0 15 2.03 0.00 0 0 16 -1.99 0.00 0 0 17 2.01 0.00 0 0 18 -2.02 0.00 0 0 19 1.97 0.00 0 0 20 -1.82 0.00 0 0 21 1.55 0.00 0 0 22 -1.22 0.00 0 0 23 0.89 0.00 0 -1 22 -0.85 0.00 0 -1 21 1.23 0.00 0 -1 20 -1.56 0.00 0 -1 19 1.78 0.00 0 -1 18 -1.88 0.00 0 -1 17 1.90 0.00 0 -1 16 -1.94 0.00 0 -1 15 2.05 0.00 0 -1 14 -2.24 0.00 0 -1 13 2.46 0.00 0 -1 12 -2.64 0.00 0 -1 11 2.70 0.00 0 -1 10 -2.59 0.00 0 -1 9 2.23 0.00 0 -1 8 -1.46 0.00 0 -1 7 -0.02 0.00 0 -1 6 2.65 0.00 0 -1 5 -6.94 0.00 0 -1 4 13.07 0.00 0 -1 3 -20.62 0.00 0 1 2 34.11 0.00 0 1 3 -27.97 0.00 0 1 4 20.95 0.00 0 1 5 -14.30 0.00 0 1 6 8.78 0.00 0 1 7 -4.64 0.00 0 1 8 1.84 0.00 0 1 9 -0.17 0.00 0 1 10 -0.66 0.00 0 1 11 0.95 0.00 0 1 12 -0.97 0.00 0 1 13 0.93 0.00 0 1 14 -0.90 0.00 0 1 15 0.91 0.00 0 1 16 -0.97 0.00 0 1 17 1.06 0.00 0 1 18 -1.17 0.00 0 1 19 1.25 0.00 0 1 20 -1.27 0.00 0 1 21 1.21 0.00 0 1 22 -1.07 0.00 0 1 23 0.89 0.00 0 -2 22 -0.49 0.00 0 -2 21 0.72 0.00 0 -2 20 -0.91 0.00 0 -2 19 1.03 0.00 0 -2 18 -1.06 0.00 0 -2 17 1.05 0.00 0 -2 16 -1.08 0.00 0 -2 15 1.16 0.00 0 -2 14 -1.31 0.00 0 -2 13 1.47 0.00 0 -2 12 -1.65 0.00 0 -2 11 1.82 0.00 0 -2 10 -1.98 0.00 0 -2 9 2.11 0.00 0 -2 8 -2.16 0.00 0 -2 7 2.02 0.00 0 -2 6 -1.42 0.00 0 -2 5 0.03 0.00 0 -2 4 2.39 0.00 0 -2 3 -5.82 0.00 0 -2 2 9.77 0.00 0 2 0 15.84 0.00 0 2 1 -16.58 0.00 0 2 2 15.61 0.00 0 2 3 -13.37 0.00 0 2 5 -7.48 0.00 0 2 6 4.79 0.00 0 2 7 -2.66 0.00 0 2 8 1.20 0.00 0 2 9 -0.42 0.00 0 2 10 0.20 0.00 0 2 11 -0.29 0.00 0 2 12 0.49 0.00 0 2 13 -0.65 0.00 0 2 14 0.73 0.00 0 2 15 -0.71 0.00 0 2 16 0.62 0.00 0 2 17 -0.46 0.00 0 2 18 0.24 0.00 0 2 19 -0.02 0.00 0 2 20 -0.16 0.00 0 2 21 0.25 0.00 0 2 22 -0.28 0.00 0 2 23 0.25 0.00 0 -3 21 0.27 0.00 0 -3 20 -0.30 0.00 0 -3 19 0.28 0.00 0 -3 18 -0.23 0.00 0 -3 17 0.17 0.00 0 -3 16 -0.12 0.00 0 -3 15 0.06 0.00 0 -3 14 0.00 0.00 0 -3 13 -0.06 0.00 0 -3 12 0.03 0.00 0 -3 11 0.15 0.00 0 -3 10 -0.49 0.00 0 -3 9 0.96 0.00 0 -3 8 -1.52 0.00 0 -3 7 2.12 0.00 0 -3 6 -2.70 0.00 0 -3 5 3.16 0.00 0 -3 4 -3.30 0.00 0 -3 3 3.01 0.00 0 -3 2 -2.29 0.00 0 -3 1 1.36 0.00 0 3 0 -0.48 0.00 0 3 1 -0.13 0.00 0 3 2 0.39 0.00 0 3 3 -0.35 0.00 0 3 4 0.12 0.00 0 3 5 0.22 0.00 0 3 6 -0.54 0.00 0 3 7 0.74 0.00 0 3 8 -0.72 0.00 0 3 9 0.45 0.00 0 3 10 0.00 0.00 0 3 11 -0.49 0.00 0 3 12 0.92 0.00 0 3 13 -1.25 0.00 0 3 14 1.48 0.00 0 3 15 -1.61 0.00 0 3 16 1.61 0.00 0 3 17 -1.48 0.00 0 3 18 1.23 0.00 0 3 19 -0.95 0.00 0 3 20 0.71 0.00 0 3 21 -0.54 0.00 0 3 22 0.45 0.00 0 3 23 -0.38 0.00 0 -4 20 0.05 0.00 0 -4 19 -0.09 0.00 0 -4 18 0.17 0.00 0 -4 17 -0.29 0.00 0 -4 16 0.44 0.00 0 -4 15 -0.65 0.00 0 -4 14 0.91 0.00 0 -4 13 -1.15 0.00 0 -4 12 1.24 0.00 0 -4 11 -1.10 0.00 0 -4 10 0.72 0.00 0 -4 9 -0.15 0.00 0 -4 8 -0.54 0.00 0 -4 7 1.34 0.00 0 -4 6 -2.27 0.00 0 -4 5 3.32 0.00 0 -4 4 -4.33 0.00 0 -4 3 5.13 0.00 0 -4 2 -5.58 0.00 0 -4 1 5.64 0.00 0 4 0 -5.43 0.00 0 4 1 5.07 0.00 0 4 2 -4.66 0.00 0 4 3 4.27 0.00 0 4 4 -3.89 0.00 0 4 5 3.49 0.00 0 4 6 -3.06 0.00 0 4 7 2.55 0.00 0 4 8 -1.97 0.00 0 4 9 1.36 0.00 0 4 10 -0.79 0.00 0 4 11 0.30 0.00 0 4 12 0.10 0.00 0 4 13 -0.46 0.00 0 4 14 0.80 0.00 0 4 15 -1.07 0.00 0 4 16 1.22 0.00 0 4 17 -1.20 0.00 0 4 18 1.05 0.00 0 4 19 -0.84 0.00 0 4 20 0.65 0.00 0 4 21 -0.52 0.00 0 4 22 0.44 0.00 0 4 23 -0.37 0.00 0 -5 19 0.00 0.00 0 -5 18 0.08 0.00 0 -5 17 -0.25 0.00 0 -5 16 0.49 0.00 0 -5 15 -0.79 0.00 0 -5 14 1.11 0.00 0 -5 13 -1.35 0.00 0 -5 12 1.41 0.00 0 -5 11 -1.26 0.00 0 -5 10 0.92 0.00 0 -5 9 -0.48 0.00 0 -5 8 -0.04 0.00 0 -5 7 0.67 0.00 0 -5 6 -1.46 0.00 0 -5 5 2.39 0.00 0 -5 4 -3.32 0.00 0 -5 3 4.03 0.00 0 -5 2 -4.35 0.00 0 -5 1 4.27 0.00 0 5 0 -3.93 0.00 0 5 1 3.50 0.00 0 5 2 -3.14 0.00 0 5 3 2.90 0.00 0 5 4 -2.73 0.00 0 5 5 2.57 0.00 0 5 6 -2.36 0.00 0 5 7 2.08 0.00 0 5 8 -1.78 0.00 0 5 9 1.51 0.00 0 5 10 -1.31 0.00 0 5 11 1.17 0.00 0 5 12 -1.01 0.00 0 5 13 0.78 0.00 0 5 14 -0.48 0.00 0 5 15 0.19 0.00 0 5 16 0.00 0.00 0 5 17 -0.05 0.00 0 5 18 -0.01 0.00 0 5 19 0.11 0.00 0 5 20 -0.19 0.00 0 5 21 0.22 0.00 0 5 22 -0.22 0.00 0 5 23 0.18 0.00 0 -6 18 -0.26 0.00 0 -6 17 0.10 0.00 0 -6 16 0.15 0.00 0 -6 15 -0.45 0.00 0 -6 14 0.73 0.00 0 -6 13 -0.91 0.00 0 -6 12 0.93 0.00 0 -6 11 -0.81 0.00 0 -6 10 0.60 0.00 0 -6 9 -0.39 0.00 0 -6 8 0.16 0.00 0 -6 7 0.15 0.00 0 -6 6 -0.61 0.00 0 -6 5 1.18 0.00 0 -6 4 -1.72 0.00 0 -6 3 2.01 0.00 0 -6 2 -1.94 0.00 0 -6 1 1.52 0.00 0 6 0 -0.93 0.00 0 6 1 0.37 0.00 0 6 2 0.01 0.00 0 6 3 -0.16 0.00 0 6 4 0.13 0.00 0 6 5 0.01 0.00 0 6 6 -0.18 0.00 0 6 7 0.36 0.00 0 6 8 -0.56 0.00 0 6 9 0.78 0.00 0 6 10 -1.01 0.00 0 6 11 1.21 0.00 0 6 12 -1.32 0.00 0 6 13 1.29 0.00 0 6 14 -1.15 0.00 0 6 15 0.99 0.00 0 6 16 -0.88 0.00 0 6 17 0.84 0.00 0 6 18 -0.87 0.00 0 6 19 0.92 0.00 0 6 20 -0.96 0.00 0 6 21 0.97 0.00 0 6 22 -0.91 0.00 0 6 23 0.78 0.00 0 -7 17 0.32 0.00 0 -7 16 -0.18 0.00 0 -7 15 -0.01 0.00 0 -7 14 0.19 0.00 0 -7 13 -0.32 0.00 0 -7 12 0.36 0.00 0 -7 11 -0.33 0.00 0 -7 10 0.30 0.00 0 -7 9 -0.30 0.00 0 -7 8 0.31 0.00 0 -7 7 -0.26 0.00 0 -7 6 0.11 0.00 0 -7 5 0.11 0.00 0 -7 4 -0.27 0.00 0 -7 3 0.24 0.00 0 -7 2 0.07 0.00 0 -7 1 -0.61 0.00 0 7 0 1.24 0.00 0 7 1 -1.82 0.00 0 7 2 2.23 0.00 0 7 3 -2.41 0.00 0 7 4 2.35 0.00 0 7 5 -2.10 0.00 0 7 6 1.70 0.00 0 7 7 -1.22 0.00 0 7 8 0.74 0.00 0 7 9 -0.27 0.00 0 7 10 -0.14 0.00 0 7 11 0.48 0.00 0 7 12 -0.73 0.00 0 7 13 0.88 0.00 0 7 14 -0.95 0.00 0 7 15 0.97 0.00 0 7 16 -0.97 0.00 0 7 17 0.96 0.00 0 7 18 -0.97 0.00 0 7 19 1.00 0.00 0 7 20 -1.06 0.00 0 7 21 1.11 0.00 0 7 22 -1.09 0.00 0 -8 15 0.00 0.00 0 -8 14 0.07 0.00 0 -8 13 -0.08 0.00 0 -8 12 0.04 0.00 0 -8 11 0.02 0.00 0 -8 10 -0.06 0.00 0 -8 9 0.03 0.00 0 -8 8 0.05 0.00 0 -8 7 -0.13 0.00 0 -8 6 0.20 0.00 0 -8 5 -0.26 0.00 0 -8 4 0.38 0.00 0 -8 3 -0.61 0.00 0 -8 2 0.97 0.00 0 -8 1 -1.45 0.00 0 8 0 1.98 0.00 0 8 1 -2.51 0.00 0 8 2 2.95 0.00 0 8 3 -3.20 0.00 0 8 4 3.20 0.00 0 8 5 -2.91 0.00 0 8 6 2.40 0.00 0 8 7 -1.79 0.00 0 8 8 1.18 0.00 0 8 9 -0.67 0.00 0 8 10 0.27 0.00 0 8 11 0.03 0.00 0 8 12 -0.24 0.00 0 8 13 0.38 0.00 0 8 14 -0.47 0.00 0 8 15 0.51 0.00 0 8 16 -0.51 0.00 0 8 17 0.50 0.00 0 8 18 -0.51 0.00 0 8 19 0.56 0.00 0 8 20 -0.65 0.00 0 8 21 0.73 0.00 0 -9 13 -0.29 0.00 0 -9 12 0.14 0.00 0 -9 11 0.07 0.00 0 -9 10 -0.25 0.00 0 -9 9 0.35 0.00 0 -9 8 -0.36 0.00 0 -9 7 0.27 0.00 0 -9 6 -0.11 0.00 0 -9 5 -0.12 0.00 0 -9 4 0.39 0.00 0 -9 3 -0.69 0.00 0 -9 2 1.01 0.00 0 -9 1 -1.38 0.00 0 9 0 1.80 0.00 0 9 1 -2.27 0.00 0 9 2 2.72 0.00 0 9 3 -3.03 0.00 0 9 4 3.07 0.00 0 9 5 -2.78 0.00 0 9 6 2.24 0.00 0 9 7 -1.56 0.00 0 9 8 0.88 0.00 0 9 9 -0.32 0.00 0 9 10 -0.10 0.00 0 9 11 0.35 0.00 0 9 12 -0.45 0.00 0 9 13 0.41 0.00 0 9 14 -0.27 0.00 0 9 15 0.07 0.00 0 9 16 0.11 0.00 0 9 17 -0.22 0.00 0 9 18 0.22 0.00 0 9 19 -0.10 0.00 0 9 20 -0.07 0.00 0 -10 11 -0.16 0.00 0 -10 10 0.01 0.00 0 -10 9 0.08 0.00 0 -10 8 -0.08 0.00 0 -10 7 0.01 0.00 0 -10 6 0.14 0.00 0 -10 5 -0.34 0.00 0 -10 4 0.54 0.00 0 -10 3 -0.71 0.00 0 -10 2 0.86 0.00 0 -10 1 -1.02 0.00 0 10 0 1.24 0.00 0 10 1 -1.54 0.00 0 10 2 1.85 0.00 0 10 3 -2.06 0.00 0 10 4 2.08 0.00 0 10 5 -1.86 0.00 0 10 6 1.45 0.00 0 10 7 -0.94 0.00 0 10 8 0.43 0.00 0 10 9 0.03 0.00 0 10 10 -0.39 0.00 0 10 11 0.62 0.00 0 10 12 -0.69 0.00 0 10 13 0.56 0.00 0 10 14 -0.28 0.00 0 10 15 -0.09 0.00 0 10 16 0.45 0.00 0 10 17 -0.70 0.00 0 10 18 0.77 0.00 0 10 19 -0.66 0.00 0 -11 8 0.48 0.00 0 -11 7 -0.61 0.00 0 -11 6 0.73 0.00 0 -11 5 -0.81 0.00 0 -11 4 0.83 0.00 0 -11 3 -0.81 0.00 0 -11 2 0.74 0.00 0 -11 1 -0.69 0.00 0 11 0 0.67 0.00 0 11 1 -0.68 0.00 0 11 2 0.69 0.00 0 11 3 -0.63 0.00 0 11 4 0.48 0.00 0 11 5 -0.28 0.00 0 11 6 0.08 0.00 0 11 7 0.08 0.00 0 11 8 -0.18 0.00 0 11 9 0.25 0.00 0 11 10 -0.31 0.00 0 11 11 0.37 0.00 0 11 12 -0.38 0.00 0 11 13 0.33 0.00 0 11 14 -0.18 0.00 0 11 15 -0.05 0.00 0 11 16 0.32 0.00 0 11 17 -0.55 0.00 0 -12 4 0.58 0.00 0 -12 3 -0.51 0.00 0 -12 2 0.45 0.00 0 -12 1 -0.40 0.00 0 12 0 0.35 0.00 0 12 1 -0.28 0.00 0 12 2 0.13 0.00 0 12 3 0.10 0.00 0 12 4 -0.38 0.00 0 12 5 0.63 0.00 0 12 6 -0.78 0.00 0 12 7 0.79 0.00 0 12 8 -0.68 0.00 0 12 9 0.49 0.00 0 12 10 -0.29 0.00 0 12 11 0.12 0.00 0 12 12 0.00 0.00 0 12 13 -0.04 0.00 0 12 14 0.05 0.00 0 13 2 0.27 0.00 0 13 3 -0.16 0.00 0 13 4 -0.01 0.00 0 13 5 0.20 0.00 0 13 6 -0.35 0.00 0 13 7 0.43 0.00 0 13 8 -0.45 0.00 -1 12 12 -0.42 0.00 -1 12 11 0.38 0.00 -1 12 10 -0.29 0.00 -1 12 9 0.17 0.00 -1 12 8 -0.08 0.00 -1 12 7 0.07 0.00 -1 12 6 -0.12 0.00 -1 12 5 0.17 0.00 -1 12 4 -0.15 0.00 -1 12 3 0.05 0.00 -1 12 2 0.12 0.00 -1 12 1 -0.29 0.00 -1 12 0 0.42 0.00 1 -12 1 -0.48 0.00 1 -12 2 0.49 0.00 1 -12 3 -0.46 0.00 -1 11 15 0.01 0.00 -1 11 14 -0.12 0.00 -1 11 13 0.28 0.00 -1 11 12 -0.46 0.00 -1 11 11 0.61 0.00 -1 11 10 -0.73 0.00 -1 11 9 0.81 0.00 -1 11 8 -0.89 0.00 -1 11 7 0.95 0.00 -1 11 6 -0.97 0.00 -1 11 5 0.90 0.00 -1 11 4 -0.70 0.00 -1 11 3 0.42 0.00 -1 11 2 -0.11 0.00 -1 11 1 -0.17 0.00 -1 11 0 0.42 0.00 1 -11 1 -0.63 0.00 1 -11 2 0.82 0.00 1 -11 3 -0.98 0.00 1 -11 4 1.10 0.00 1 -11 5 -1.15 0.00 1 -11 6 1.13 0.00 1 -11 7 -1.03 0.00 -1 10 18 0.11 0.00 -1 10 17 -0.19 0.00 -1 10 16 0.21 0.00 -1 10 15 -0.15 0.00 -1 10 14 0.00 0.00 -1 10 13 0.21 0.00 -1 10 12 -0.44 0.00 -1 10 11 0.65 0.00 -1 10 10 -0.83 0.00 -1 10 9 0.96 0.00 -1 10 8 -1.03 0.00 -1 10 7 1.02 0.00 -1 10 6 -0.88 0.00 -1 10 5 0.63 0.00 -1 10 4 -0.32 0.00 -1 10 3 0.04 0.00 -1 10 2 0.15 0.00 -1 10 1 -0.26 0.00 -1 10 0 0.34 0.00 1 -10 1 -0.46 0.00 1 -10 2 0.62 0.00 1 -10 3 -0.81 0.00 1 -10 4 0.96 0.00 1 -10 5 -1.04 0.00 1 -10 6 1.05 0.00 1 -10 7 -0.98 0.00 1 -10 8 0.86 0.00 1 -10 9 -0.69 0.00 1 -10 10 0.51 0.00 -1 9 19 -0.10 0.00 -1 9 18 0.12 0.00 -1 9 17 -0.09 0.00 -1 9 16 -0.01 0.00 -1 9 15 0.15 0.00 -1 9 14 -0.30 0.00 -1 9 13 0.43 0.00 -1 9 12 -0.53 0.00 -1 9 11 0.60 0.00 -1 9 10 -0.65 0.00 -1 9 9 0.65 0.00 -1 9 8 -0.57 0.00 -1 9 7 0.36 0.00 -1 9 6 -0.01 0.00 -1 9 5 -0.41 0.00 -1 9 4 0.79 0.00 -1 9 3 -0.99 0.00 -1 9 2 0.99 0.00 -1 9 1 -0.85 0.00 -1 9 0 0.67 0.00 1 -9 1 -0.54 0.00 1 -9 2 0.49 0.00 1 -9 3 -0.47 0.00 1 -9 4 0.44 0.00 1 -9 5 -0.37 0.00 1 -9 6 0.28 0.00 1 -9 7 -0.20 0.00 1 -9 8 0.14 0.00 1 -9 9 -0.12 0.00 1 -9 10 0.12 0.00 1 -9 11 -0.15 0.00 1 -9 12 0.19 0.00 -1 8 20 0.22 0.00 -1 8 19 -0.27 0.00 -1 8 18 0.22 0.00 -1 8 17 -0.05 0.00 -1 8 16 -0.17 0.00 -1 8 15 0.38 0.00 -1 8 14 -0.49 0.00 -1 8 13 0.48 0.00 -1 8 12 -0.38 0.00 -1 8 11 0.23 0.00 -1 8 10 -0.05 0.00 -1 8 9 -0.15 0.00 -1 8 8 0.41 0.00 -1 8 7 -0.77 0.00 -1 8 6 1.22 0.00 -1 8 5 -1.67 0.00 -1 8 4 1.98 0.00 -1 8 3 -2.07 0.00 -1 8 2 1.93 0.00 -1 8 1 -1.63 0.00 -1 8 0 1.29 0.00 1 -8 1 -0.99 0.00 1 -8 2 0.74 0.00 1 -8 3 -0.53 0.00 1 -8 4 0.34 0.00 1 -8 5 -0.15 0.00 1 -8 6 -0.02 0.00 1 -8 7 0.17 0.00 1 -8 8 -0.30 0.00 1 -8 9 0.38 0.00 1 -8 10 -0.39 0.00 1 -8 11 0.34 0.00 1 -8 12 -0.24 0.00 1 -8 13 0.14 0.00 1 -8 14 -0.05 0.00 -1 7 21 0.32 0.00 -1 7 20 -0.07 0.00 -1 7 19 -0.13 0.00 -1 7 18 0.19 0.00 -1 7 17 -0.11 0.00 -1 7 16 -0.07 0.00 -1 7 15 0.26 0.00 -1 7 14 -0.36 0.00 -1 7 13 0.32 0.00 -1 7 12 -0.14 0.00 -1 7 11 -0.17 0.00 -1 7 10 0.57 0.00 -1 7 9 -1.03 0.00 -1 7 8 1.55 0.00 -1 7 7 -2.10 0.00 -1 7 6 2.61 0.00 -1 7 5 -3.01 0.00 -1 7 4 3.20 0.00 -1 7 3 -3.14 0.00 -1 7 2 2.84 0.00 -1 7 1 -2.36 0.00 -1 7 0 1.78 0.00 1 -7 1 -1.18 0.00 1 -7 2 0.64 0.00 1 -7 3 -0.22 0.00 1 -7 4 -0.03 0.00 1 -7 5 0.13 0.00 1 -7 6 -0.14 0.00 1 -7 7 0.14 0.00 1 -7 8 -0.20 0.00 1 -7 9 0.30 0.00 1 -7 10 -0.39 0.00 1 -7 11 0.42 0.00 1 -7 12 -0.41 0.00 1 -7 13 0.38 0.00 1 -7 14 -0.35 0.00 1 -7 15 0.33 0.00 1 -7 16 -0.29 0.00 -1 6 22 -1.24 0.00 -1 6 21 1.17 0.00 -1 6 20 -0.95 0.00 -1 6 19 0.67 0.00 -1 6 18 -0.43 0.00 -1 6 17 0.27 0.00 -1 6 16 -0.22 0.00 -1 6 15 0.27 0.00 -1 6 14 -0.37 0.00 -1 6 13 0.43 0.00 -1 6 12 -0.36 0.00 -1 6 11 0.11 0.00 -1 6 10 0.34 0.00 -1 6 9 -0.94 0.00 -1 6 8 1.62 0.00 -1 6 7 -2.32 0.00 -1 6 6 2.93 0.00 -1 6 5 -3.39 0.00 -1 6 4 3.64 0.00 -1 6 3 -3.61 0.00 -1 6 2 3.28 0.00 -1 6 1 -2.66 0.00 -1 6 0 1.79 0.00 1 -6 1 -0.79 0.00 1 -6 2 -0.16 0.00 1 -6 3 0.85 0.00 1 -6 4 -1.18 0.00 1 -6 5 1.14 0.00 1 -6 6 -0.88 0.00 1 -6 7 0.58 0.00 1 -6 8 -0.35 0.00 1 -6 9 0.19 0.00 1 -6 10 -0.06 0.00 1 -6 11 -0.05 0.00 1 -6 12 0.11 0.00 1 -6 13 -0.07 0.00 1 -6 14 -0.07 0.00 1 -6 15 0.27 0.00 1 -6 16 -0.43 0.00 1 -6 17 0.52 0.00 1 -6 18 -0.53 0.00 -1 5 23 1.00 0.00 -1 5 22 -1.30 0.00 -1 5 21 1.48 0.00 -1 5 20 -1.52 0.00 -1 5 19 1.40 0.00 -1 5 18 -1.17 0.00 -1 5 17 0.89 0.00 -1 5 16 -0.67 0.00 -1 5 15 0.59 0.00 -1 5 14 -0.68 0.00 -1 5 13 0.83 0.00 -1 5 12 -0.95 0.00 -1 5 11 0.92 0.00 -1 5 10 -0.70 0.00 -1 5 9 0.34 0.00 -1 5 8 0.13 0.00 -1 5 7 -0.66 0.00 -1 5 6 1.20 0.00 -1 5 5 -1.71 0.00 -1 5 4 2.09 0.00 -1 5 3 -2.25 0.00 -1 5 2 2.09 0.00 -1 5 1 -1.54 0.00 -1 5 0 0.65 0.00 1 -5 1 0.41 0.00 1 -5 2 -1.40 0.00 1 -5 3 2.05 0.00 1 -5 4 -2.21 0.00 1 -5 5 1.96 0.00 1 -5 6 -1.48 0.00 1 -5 7 0.97 0.00 1 -5 8 -0.52 0.00 1 -5 9 0.12 0.00 1 -5 10 0.28 0.00 1 -5 11 -0.63 0.00 1 -5 12 0.85 0.00 1 -5 13 -0.84 0.00 1 -5 14 0.60 0.00 1 -5 15 -0.23 0.00 1 -5 16 -0.13 0.00 1 -5 17 0.41 0.00 1 -5 18 -0.56 0.00 1 -5 19 0.59 0.00 -1 4 23 0.34 0.00 -1 4 22 -0.57 0.00 -1 4 21 0.81 0.00 -1 4 20 -0.99 0.00 -1 4 19 1.04 0.00 -1 4 18 -0.94 0.00 -1 4 17 0.74 0.00 -1 4 16 -0.56 0.00 -1 4 15 0.53 0.00 -1 4 14 -0.68 0.00 -1 4 13 0.96 0.00 -1 4 12 -1.28 0.00 -1 4 11 1.58 0.00 -1 4 10 -1.83 0.00 -1 4 9 2.02 0.00 -1 4 8 -2.11 0.00 -1 4 7 2.06 0.00 -1 4 6 -1.85 0.00 -1 4 5 1.52 0.00 -1 4 4 -1.18 0.00 -1 4 3 0.99 0.00 -1 4 2 -1.07 0.00 -1 4 1 1.45 0.00 -1 4 0 -2.07 0.00 1 -4 1 2.73 0.00 1 -4 2 -3.18 0.00 1 -4 3 3.20 0.00 1 -4 4 -2.76 0.00 1 -4 5 2.01 0.00 1 -4 6 -1.19 0.00 1 -4 7 0.50 0.00 1 -4 8 0.02 0.00 1 -4 9 -0.45 0.00 1 -4 10 0.87 0.00 1 -4 11 -1.23 0.00 1 -4 12 1.45 0.00 1 -4 13 -1.43 0.00 1 -4 14 1.18 0.00 1 -4 15 -0.80 0.00 1 -4 16 0.42 0.00 1 -4 17 -0.09 0.00 1 -4 18 -0.15 0.00 1 -4 19 0.31 0.00 1 -4 20 -0.36 0.00 -1 3 23 -0.23 0.00 -1 3 22 0.17 0.00 -1 3 21 -0.05 0.00 -1 3 20 -0.03 0.00 -1 3 19 0.03 0.00 -1 3 18 0.09 0.00 -1 3 17 -0.25 0.00 -1 3 16 0.33 0.00 -1 3 15 -0.25 0.00 -1 3 14 -0.03 0.00 -1 3 13 0.50 0.00 -1 3 12 -1.10 0.00 -1 3 11 1.83 0.00 -1 3 10 -2.64 0.00 -1 3 9 3.47 0.00 -1 3 8 -4.20 0.00 -1 3 7 4.68 0.00 -1 3 6 -4.88 0.00 -1 3 5 4.83 0.00 -1 3 4 -4.68 0.00 -1 3 3 4.55 0.00 -1 3 2 -4.52 0.00 -1 3 1 4.62 0.00 -1 3 0 -4.79 0.00 1 -3 1 4.88 0.00 1 -3 2 -4.72 0.00 1 -3 3 4.16 0.00 1 -3 4 -3.19 0.00 1 -3 5 2.00 0.00 1 -3 6 -0.84 0.00 1 -3 7 -0.08 0.00 1 -3 8 0.71 0.00 1 -3 9 -1.13 0.00 1 -3 10 1.45 0.00 1 -3 11 -1.68 0.00 1 -3 12 1.79 0.00 1 -3 13 -1.72 0.00 1 -3 14 1.51 0.00 1 -3 15 -1.23 0.00 1 -3 16 0.94 0.00 1 -3 17 -0.65 0.00 1 -3 18 0.36 0.00 1 -3 19 -0.08 0.00 1 -3 20 -0.13 0.00 1 -3 21 0.22 0.00 -1 2 23 -0.29 0.00 -1 2 22 0.29 0.00 -1 2 21 -0.28 0.00 -1 2 20 0.32 0.00 -1 2 19 -0.45 0.00 -1 2 18 0.66 0.00 -1 2 17 -0.87 0.00 -1 2 16 0.97 0.00 -1 2 15 -0.89 0.00 -1 2 14 0.59 0.00 -1 2 13 -0.07 0.00 -1 2 12 -0.67 0.00 -1 2 11 1.63 0.00 -1 2 10 -2.75 0.00 -1 2 9 3.90 0.00 -1 2 8 -4.91 0.00 -1 2 7 5.60 0.00 -1 2 6 -5.89 0.00 -1 2 5 5.79 0.00 -1 2 3 4.69 0.00 -1 2 1 3.21 0.00 -1 2 0 -2.76 0.00 1 -2 1 2.63 0.00 1 -2 3 2.71 0.00 1 -2 4 -2.44 0.00 1 -2 5 1.82 0.00 1 -2 6 -1.00 0.00 1 -2 7 0.19 0.00 1 -2 8 0.45 0.00 1 -2 9 -0.88 0.00 1 -2 10 1.15 0.00 1 -2 11 -1.32 0.00 1 -2 12 1.39 0.00 1 -2 13 -1.39 0.00 1 -2 14 1.31 0.00 1 -2 15 -1.17 0.00 1 -2 16 0.98 0.00 1 -2 17 -0.72 0.00 1 -2 18 0.40 0.00 1 -2 19 -0.08 0.00 1 -2 20 -0.16 0.00 1 -2 21 0.27 0.00 1 -2 22 -0.25 0.00 -1 1 23 0.06 0.00 -1 1 22 -0.07 0.00 -1 1 21 0.07 0.00 -1 1 20 -0.02 0.00 -1 1 19 -0.12 0.00 -1 1 18 0.31 0.00 -1 1 17 -0.51 0.00 -1 1 16 0.62 0.00 -1 1 15 -0.59 0.00 -1 1 14 0.38 0.00 -1 1 13 0.01 0.00 -1 1 12 -0.57 0.00 -1 1 11 1.29 0.00 -1 1 10 -2.10 0.00 -1 1 9 2.86 0.00 -1 1 8 -3.37 0.00 -1 1 7 3.47 0.00 -1 1 6 -3.00 0.00 -1 1 5 1.84 0.00 -1 1 2 5.27 0.00 -1 1 1 -7.59 0.00 -1 1 0 8.82 0.00 1 -1 2 6.89 0.00 1 -1 3 -4.47 0.00 1 -1 4 2.10 0.00 1 -1 5 -0.37 0.00 1 -1 6 -0.52 0.00 1 -1 7 0.76 0.00 1 -1 8 -0.65 0.00 1 -1 9 0.44 0.00 1 -1 10 -0.25 0.00 1 -1 11 0.09 0.00 1 -1 12 0.05 0.00 1 -1 13 -0.17 0.00 1 -1 14 0.24 0.00 1 -1 15 -0.24 0.00 1 -1 16 0.13 0.00 1 -1 17 0.08 0.00 1 -1 18 -0.35 0.00 1 -1 19 0.57 0.00 1 -1 20 -0.67 0.00 1 -1 21 0.60 0.00 1 -1 22 -0.42 0.00 -1 0 23 0.39 0.00 -1 0 22 -0.47 0.00 -1 0 21 0.54 0.00 -1 0 20 -0.58 0.00 -1 0 19 0.55 0.00 -1 0 18 -0.45 0.00 -1 0 17 0.34 0.00 -1 0 16 -0.28 0.00 -1 0 15 0.34 0.00 -1 0 14 -0.52 0.00 -1 0 13 0.80 0.00 -1 0 12 -1.12 0.00 -1 0 11 1.41 0.00 -1 0 10 -1.58 0.00 -1 0 9 1.49 0.00 -1 0 8 -1.01 0.00 -1 0 7 -0.06 0.00 -1 0 6 1.93 0.00 -1 0 5 -4.88 0.00 -1 0 4 9.05 0.00 -1 0 3 -14.22 0.00 -1 0 2 19.65 0.00 1 0 3 -16.80 0.00 1 0 4 10.98 0.00 1 0 5 -5.92 0.00 1 0 6 2.26 0.00 1 0 7 0.01 0.00 1 0 8 -1.19 0.00 1 0 9 1.70 0.00 1 0 10 -1.83 0.00 1 0 11 1.74 0.00 1 0 12 -1.55 0.00 1 0 13 1.34 0.00 1 0 14 -1.17 0.00 1 0 15 1.10 0.00 1 0 16 -1.14 0.00 1 0 17 1.28 0.00 1 0 18 -1.43 0.00 1 0 19 1.51 0.00 1 0 20 -1.43 0.00 1 0 21 1.19 0.00 1 0 22 -0.85 0.00 1 0 23 0.49 0.00 -1 -1 22 -0.65 0.00 -1 -1 21 0.87 0.00 -1 -1 20 -1.06 0.00 -1 -1 19 1.17 0.00 -1 -1 18 -1.18 0.00 -1 -1 17 1.14 0.00 -1 -1 16 -1.14 0.00 -1 -1 15 1.24 0.00 -1 -1 14 -1.47 0.00 -1 -1 13 1.74 0.00 -1 -1 12 -1.98 0.00 -1 -1 11 2.06 0.00 -1 -1 10 -1.87 0.00 -1 -1 9 1.31 0.00 -1 -1 8 -0.26 0.00 -1 -1 7 -1.45 0.00 -1 -1 6 4.12 0.00 -1 -1 5 -8.09 0.00 -1 -1 4 13.57 0.00 -1 -1 2 27.42 0.00 1 1 0 36.83 0.00 1 1 2 32.87 0.00 1 1 3 -26.59 0.00 1 1 4 19.29 0.00 1 1 5 -12.38 0.00 1 1 6 6.74 0.00 1 1 7 -2.65 0.00 1 1 8 -0.02 0.00 1 1 9 1.54 0.00 1 1 10 -2.23 0.00 1 1 11 2.39 0.00 1 1 12 -2.26 0.00 1 1 13 2.04 0.00 1 1 14 -1.86 0.00 1 1 15 1.76 0.00 1 1 16 -1.75 0.00 1 1 17 1.80 0.00 1 1 18 -1.86 0.00 1 1 19 1.86 0.00 1 1 20 -1.76 0.00 1 1 21 1.54 0.00 1 1 22 -1.22 0.00 1 1 23 0.85 0.00 -1 -2 22 -0.63 0.00 -1 -2 21 0.93 0.00 -1 -2 20 -1.23 0.00 -1 -2 19 1.44 0.00 -1 -2 18 -1.56 0.00 -1 -2 17 1.60 0.00 -1 -2 16 -1.65 0.00 -1 -2 15 1.78 0.00 -1 -2 14 -1.97 0.00 -1 -2 13 2.20 0.00 -1 -2 12 -2.38 0.00 -1 -2 11 2.45 0.00 -1 -2 10 -2.33 0.00 -1 -2 9 1.94 0.00 -1 -2 8 -1.19 0.00 -1 -2 7 -0.10 0.00 -1 -2 6 2.21 0.00 -1 -2 5 -5.46 0.00 -1 -2 3 -15.85 0.00 -1 -2 2 22.12 0.00 -1 -2 1 -27.68 0.00 1 2 0 31.28 0.00 1 2 2 29.96 0.00 1 2 3 -25.62 0.00 1 2 4 20.08 0.00 1 2 5 -14.38 0.00 1 2 6 9.26 0.00 1 2 7 -5.10 0.00 1 2 8 2.06 0.00 1 2 9 -0.10 0.00 1 2 10 -0.95 0.00 1 2 11 1.35 0.00 1 2 12 -1.38 0.00 1 2 13 1.28 0.00 1 2 14 -1.18 0.00 1 2 15 1.13 0.00 1 2 16 -1.11 0.00 1 2 17 1.12 0.00 1 2 18 -1.15 0.00 1 2 19 1.17 0.00 1 2 20 -1.16 0.00 1 2 21 1.08 0.00 1 2 22 -0.94 0.00 1 2 23 0.73 0.00 -1 -3 21 0.66 0.00 -1 -3 20 -0.90 0.00 -1 -3 19 1.11 0.00 -1 -3 18 -1.28 0.00 -1 -3 17 1.41 0.00 -1 -3 16 -1.53 0.00 -1 -3 15 1.63 0.00 -1 -3 14 -1.72 0.00 -1 -3 13 1.76 0.00 -1 -3 12 -1.79 0.00 -1 -3 11 1.83 0.00 -1 -3 10 -1.91 0.00 -1 -3 9 1.97 0.00 -1 -3 8 -1.91 0.00 -1 -3 7 1.56 0.00 -1 -3 6 -0.70 0.00 -1 -3 5 -0.87 0.00 -1 -3 4 3.32 0.00 -1 -3 3 -6.56 0.00 -1 -3 2 10.23 0.00 -1 -3 1 -13.67 0.00 1 3 0 16.19 0.00 1 3 4 12.69 0.00 1 3 5 -9.89 0.00 1 3 6 7.13 0.00 1 3 7 -4.70 0.00 1 3 8 2.80 0.00 1 3 9 -1.51 0.00 1 3 10 0.78 0.00 1 3 11 -0.47 0.00 1 3 12 0.38 0.00 1 3 13 -0.37 0.00 1 3 14 0.37 0.00 1 3 15 -0.38 0.00 1 3 16 0.38 0.00 1 3 17 -0.35 0.00 1 3 18 0.27 0.00 1 3 19 -0.14 0.00 1 3 20 0.00 0.00 1 3 21 0.10 0.00 1 3 22 -0.14 0.00 1 3 23 0.13 0.00 1 3 24 -0.08 0.00 -1 -4 20 -0.31 0.00 -1 -4 19 0.43 0.00 -1 -4 18 -0.55 0.00 -1 -4 17 0.67 0.00 -1 -4 16 -0.76 0.00 -1 -4 15 0.79 0.00 -1 -4 14 -0.73 0.00 -1 -4 13 0.61 0.00 -1 -4 12 -0.49 0.00 -1 -4 11 0.50 0.00 -1 -4 10 -0.71 0.00 -1 -4 9 1.10 0.00 -1 -4 8 -1.55 0.00 -1 -4 7 1.93 0.00 -1 -4 6 -2.11 0.00 -1 -4 5 1.96 0.00 -1 -4 4 -1.41 0.00 -1 -4 3 0.44 0.00 -1 -4 2 0.84 0.00 -1 -4 1 -2.20 0.00 1 4 0 3.34 0.00 1 4 1 -4.06 0.00 1 4 2 4.29 0.00 1 4 3 -4.10 0.00 1 4 4 3.63 0.00 1 4 5 -3.04 0.00 1 4 6 2.45 0.00 1 4 7 -1.95 0.00 1 4 8 1.61 0.00 1 4 9 -1.45 0.00 1 4 10 1.40 0.00 1 4 11 -1.40 0.00 1 4 12 1.40 0.00 1 4 13 -1.40 0.00 1 4 14 1.45 0.00 1 4 15 -1.55 0.00 1 4 16 1.64 0.00 1 4 17 -1.65 0.00 1 4 18 1.53 0.00 1 4 19 -1.29 0.00 1 4 20 1.00 0.00 1 4 21 -0.71 0.00 1 4 22 0.48 0.00 1 4 23 -0.31 0.00 1 4 24 0.20 0.00 -1 -5 19 0.00 0.00 -1 -5 18 -0.01 0.00 -1 -5 17 -0.02 0.00 -1 -5 16 0.08 0.00 -1 -5 15 -0.18 0.00 -1 -5 14 0.32 0.00 -1 -5 13 -0.47 0.00 -1 -5 12 0.53 0.00 -1 -5 11 -0.43 0.00 -1 -5 10 0.12 0.00 -1 -5 9 0.36 0.00 -1 -5 8 -0.93 0.00 -1 -5 7 1.53 0.00 -1 -5 6 -2.13 0.00 -1 -5 5 2.70 0.00 -1 -5 4 -3.16 0.00 -1 -5 3 3.42 0.00 -1 -5 2 -3.40 0.00 -1 -5 1 3.14 0.00 1 5 0 -2.74 0.00 1 5 1 2.33 0.00 1 5 2 -2.01 0.00 1 5 3 1.78 0.00 1 5 4 -1.57 0.00 1 5 5 1.31 0.00 1 5 6 -0.96 0.00 1 5 7 0.50 0.00 1 5 8 -0.01 0.00 1 5 9 -0.43 0.00 1 5 10 0.73 0.00 1 5 11 -0.87 0.00 1 5 12 0.91 0.00 1 5 13 -0.97 0.00 1 5 14 1.12 0.00 1 5 15 -1.38 0.00 1 5 16 1.65 0.00 1 5 17 -1.81 0.00 1 5 18 1.81 0.00 1 5 19 -1.64 0.00 1 5 20 1.36 0.00 1 5 21 -1.03 0.00 1 5 22 0.69 0.00 1 5 23 -0.39 0.00 -1 -6 18 -0.01 0.00 -1 -6 17 -0.14 0.00 -1 -6 16 0.36 0.00 -1 -6 15 -0.60 0.00 -1 -6 14 0.80 0.00 -1 -6 13 -0.90 0.00 -1 -6 12 0.84 0.00 -1 -6 11 -0.60 0.00 -1 -6 10 0.23 0.00 -1 -6 9 0.20 0.00 -1 -6 8 -0.63 0.00 -1 -6 7 1.09 0.00 -1 -6 6 -1.62 0.00 -1 -6 5 2.25 0.00 -1 -6 4 -2.92 0.00 -1 -6 3 3.47 0.00 -1 -6 2 -3.77 0.00 -1 -6 1 3.77 0.00 1 6 0 -3.54 0.00 1 6 1 3.22 0.00 1 6 2 -2.94 0.00 1 6 3 2.71 0.00 1 6 4 -2.50 0.00 1 6 5 2.22 0.00 1 6 6 -1.83 0.00 1 6 7 1.35 0.00 1 6 8 -0.87 0.00 1 6 9 0.49 0.00 1 6 10 -0.29 0.00 1 6 11 0.25 0.00 1 6 12 -0.27 0.00 1 6 13 0.24 0.00 1 6 14 -0.07 0.00 1 6 15 -0.19 0.00 1 6 16 0.50 0.00 1 6 17 -0.75 0.00 1 6 18 0.90 0.00 1 6 19 -0.94 0.00 1 6 20 0.89 0.00 1 6 21 -0.75 0.00 1 6 22 0.55 0.00 1 6 23 -0.33 0.00 -1 -7 17 0.14 0.00 -1 -7 16 0.08 0.00 -1 -7 15 -0.37 0.00 -1 -7 14 0.64 0.00 -1 -7 13 -0.80 0.00 -1 -7 12 0.80 0.00 -1 -7 11 -0.64 0.00 -1 -7 10 0.36 0.00 -1 -7 9 -0.06 0.00 -1 -7 8 -0.23 0.00 -1 -7 7 0.54 0.00 -1 -7 6 -0.91 0.00 -1 -7 5 1.35 0.00 -1 -7 4 -1.79 0.00 -1 -7 3 2.09 0.00 -1 -7 2 -2.15 0.00 -1 -7 1 1.98 0.00 1 7 0 -1.67 0.00 1 7 1 1.37 0.00 1 7 2 -1.16 0.00 1 7 3 1.07 0.00 1 7 4 -1.05 0.00 1 7 5 1.02 0.00 1 7 6 -0.96 0.00 1 7 7 0.85 0.00 1 7 8 -0.76 0.00 1 7 9 0.73 0.00 1 7 10 -0.78 0.00 1 7 11 0.90 0.00 1 7 12 -1.01 0.00 1 7 13 1.05 0.00 1 7 14 -1.01 0.00 1 7 15 0.91 0.00 1 7 16 -0.77 0.00 1 7 17 0.62 0.00 1 7 18 -0.46 0.00 1 7 19 0.29 0.00 1 7 20 -0.15 0.00 1 7 21 0.04 0.00 1 7 22 0.01 0.00 -1 -8 15 0.02 0.00 -1 -8 14 0.23 0.00 -1 -8 13 -0.47 0.00 -1 -8 12 0.63 0.00 -1 -8 11 -0.69 0.00 -1 -8 10 0.65 0.00 -1 -8 9 -0.54 0.00 -1 -8 8 0.35 0.00 -1 -8 7 -0.10 0.00 -1 -8 6 -0.21 0.00 -1 -8 5 0.51 0.00 -1 -8 4 -0.71 0.00 -1 -8 3 0.71 0.00 -1 -8 2 -0.48 0.00 -1 -8 1 0.10 0.00 1 8 0 0.33 0.00 1 8 1 -0.68 0.00 1 8 2 0.89 0.00 1 8 3 -0.96 0.00 1 8 4 0.92 0.00 1 8 5 -0.78 0.00 1 8 6 0.59 0.00 1 8 7 -0.35 0.00 1 8 8 0.08 0.00 1 8 9 0.22 0.00 1 8 10 -0.51 0.00 1 8 11 0.79 0.00 1 8 12 -1.01 0.00 1 8 13 1.18 0.00 1 8 14 -1.28 0.00 1 8 15 1.33 0.00 1 8 16 -1.35 0.00 1 8 17 1.32 0.00 1 8 18 -1.25 0.00 1 8 19 1.13 0.00 1 8 20 -0.98 0.00 1 8 21 0.82 0.00 1 8 22 -0.64 0.00 -1 -9 13 -0.18 0.00 -1 -9 12 0.29 0.00 -1 -9 11 -0.36 0.00 -1 -9 10 0.42 0.00 -1 -9 9 -0.43 0.00 -1 -9 8 0.40 0.00 -1 -9 7 -0.29 0.00 -1 -9 6 0.15 0.00 -1 -9 5 -0.04 0.00 -1 -9 4 0.05 0.00 -1 -9 3 -0.22 0.00 -1 -9 2 0.54 0.00 -1 -9 1 -0.95 0.00 1 9 0 1.37 0.00 1 9 1 -1.74 0.00 1 9 2 2.04 0.00 1 9 3 -2.22 0.00 1 9 4 2.26 0.00 1 9 5 -2.14 0.00 1 9 6 1.86 0.00 1 9 7 -1.44 0.00 1 9 8 0.94 0.00 1 9 9 -0.43 0.00 1 9 10 -0.06 0.00 1 9 11 0.48 0.00 1 9 12 -0.81 0.00 1 9 13 1.04 0.00 1 9 14 -1.17 0.00 1 9 15 1.21 0.00 1 9 16 -1.19 0.00 1 9 17 1.14 0.00 1 9 18 -1.09 0.00 1 9 19 1.07 0.00 1 9 20 -1.04 0.00 1 9 21 0.98 0.00 -1 -10 11 0.07 0.00 -1 -10 10 -0.14 0.00 -1 -10 9 0.14 0.00 -1 -10 8 -0.08 0.00 -1 -10 7 -0.02 0.00 -1 -10 6 0.15 0.00 -1 -10 5 -0.34 0.00 -1 -10 4 0.59 0.00 -1 -10 3 -0.88 0.00 -1 -10 2 1.20 0.00 -1 -10 1 -1.52 0.00 1 10 0 1.85 0.00 1 10 1 -2.18 0.00 1 10 2 2.50 0.00 1 10 3 -2.74 0.00 1 10 4 2.82 0.00 1 10 5 -2.69 0.00 1 10 6 2.34 0.00 1 10 7 -1.82 0.00 1 10 8 1.23 0.00 1 10 9 -0.62 0.00 1 10 10 0.07 0.00 1 10 11 0.40 0.00 1 10 12 -0.75 0.00 1 10 13 0.95 0.00 1 10 14 -0.98 0.00 1 10 15 0.87 0.00 1 10 16 -0.68 0.00 1 10 17 0.49 0.00 1 10 18 -0.38 0.00 1 10 19 0.37 0.00 -1 -11 9 0.30 0.00 -1 -11 8 -0.23 0.00 -1 -11 7 0.07 0.00 -1 -11 6 0.17 0.00 -1 -11 5 -0.44 0.00 -1 -11 4 0.73 0.00 -1 -11 3 -1.00 0.00 -1 -11 2 1.23 0.00 -1 -11 1 -1.45 0.00 1 11 0 1.69 0.00 1 11 1 -1.96 0.00 1 11 2 2.24 0.00 1 11 3 -2.43 0.00 1 11 4 2.46 0.00 1 11 5 -2.27 0.00 1 11 6 1.90 0.00 1 11 7 -1.42 0.00 1 11 8 0.91 0.00 1 11 9 -0.44 0.00 1 11 10 0.03 0.00 1 11 11 0.31 0.00 1 11 12 -0.57 0.00 1 11 13 0.70 0.00 1 11 14 -0.70 0.00 1 11 15 0.56 0.00 1 11 16 -0.31 0.00 1 11 17 0.04 0.00 -1 -12 5 -0.29 0.00 -1 -12 4 0.37 0.00 -1 -12 3 -0.42 0.00 -1 -12 2 0.48 0.00 -1 -12 1 -0.56 0.00 1 12 0 0.71 0.00 1 12 1 -0.92 0.00 1 12 2 1.14 0.00 1 12 3 -1.27 0.00 1 12 4 1.25 0.00 1 12 5 -1.07 0.00 1 12 6 0.78 0.00 1 12 7 -0.47 0.00 1 12 8 0.21 0.00 1 12 9 -0.03 0.00 1 12 10 -0.07 0.00 1 12 11 0.13 0.00 1 12 12 -0.19 0.00 1 12 13 0.25 0.00 1 12 14 -0.28 0.00 1 12 15 0.26 0.00 1 13 0 -0.15 0.00 1 13 1 0.01 0.00 1 13 2 0.15 0.00 1 13 3 -0.25 0.00 1 13 4 0.23 0.00 1 13 5 -0.10 0.00 1 13 6 -0.09 0.00 1 13 7 0.28 0.00 1 13 8 -0.39 0.00 1 13 9 0.40 0.00 1 13 10 -0.31 0.00 1 13 11 0.17 0.00 -2 12 7 -1.41 0.00 -2 12 6 1.42 0.00 -2 12 5 -1.15 0.00 -2 12 4 0.75 0.00 -2 12 3 -0.38 0.00 -2 12 2 0.14 0.00 -2 12 1 -0.03 0.00 -2 12 0 0.02 0.00 -2 11 14 -0.42 0.00 -2 11 13 0.60 0.00 -2 11 12 -0.75 0.00 -2 11 11 0.77 0.00 -2 11 10 -0.57 0.00 -2 11 9 0.18 0.00 -2 11 8 0.29 0.00 -2 11 7 -0.66 0.00 -2 11 6 0.85 0.00 -2 11 5 -0.85 0.00 -2 11 4 0.73 0.00 -2 11 3 -0.59 0.00 -2 11 2 0.48 0.00 -2 11 1 -0.42 0.00 -2 11 0 0.37 0.00 2 -11 1 -0.32 0.00 2 -11 2 0.27 0.00 2 -11 3 -0.22 0.00 2 -11 4 0.18 0.00 2 -11 5 -0.17 0.00 2 -11 6 0.19 0.00 -2 10 16 -0.22 0.00 -2 10 15 0.09 0.00 -2 10 14 -0.08 0.00 -2 10 13 0.23 0.00 -2 10 12 -0.50 0.00 -2 10 11 0.77 0.00 -2 10 10 -0.96 0.00 -2 10 9 1.01 0.00 -2 10 8 -0.93 0.00 -2 10 7 0.77 0.00 -2 10 6 -0.55 0.00 -2 10 5 0.29 0.00 -2 10 4 0.00 0.00 -2 10 3 -0.28 0.00 -2 10 2 0.48 0.00 -2 10 1 -0.59 0.00 -2 10 0 0.60 0.00 2 -10 1 -0.56 0.00 2 -10 2 0.51 0.00 2 -10 3 -0.49 0.00 2 -10 4 0.48 0.00 2 -10 5 -0.49 0.00 2 -10 6 0.49 0.00 2 -10 7 -0.48 0.00 2 -10 8 0.42 0.00 2 -10 9 -0.32 0.00 -2 9 18 -0.54 0.00 -2 9 17 0.55 0.00 -2 9 12 -0.52 0.00 -2 9 11 0.73 0.00 -2 9 10 -0.99 0.00 -2 9 9 1.26 0.00 -2 9 8 -1.47 0.00 -2 9 7 1.56 0.00 -2 9 6 -1.44 0.00 -2 9 5 1.11 0.00 -2 9 4 -0.65 0.00 -2 9 3 0.19 0.00 -2 9 2 0.16 0.00 -2 9 1 -0.35 0.00 -2 9 0 0.42 0.00 2 -9 1 -0.45 0.00 2 -9 2 0.48 0.00 2 -9 3 -0.52 0.00 2 -9 4 0.55 0.00 2 -9 5 -0.57 0.00 2 -9 6 0.56 0.00 2 -9 7 -0.53 0.00 2 -9 8 0.48 0.00 2 -9 9 -0.39 0.00 2 -9 10 0.26 0.00 2 -9 11 -0.09 0.00 2 -9 12 -0.07 0.00 -2 8 20 0.09 0.00 -2 8 19 -0.01 0.00 -2 8 18 -0.14 0.00 -2 8 17 0.35 0.00 -2 8 16 -0.58 0.00 -2 8 15 0.80 0.00 -2 8 14 -0.95 0.00 -2 8 13 1.02 0.00 -2 8 12 -1.03 0.00 -2 8 11 1.05 0.00 -2 8 10 -1.12 0.00 -2 8 9 1.25 0.00 -2 8 8 -1.39 0.00 -2 8 7 1.43 0.00 -2 8 6 -1.29 0.00 -2 8 5 0.98 0.00 -2 8 4 -0.57 0.00 -2 8 3 0.19 0.00 -2 8 2 0.08 0.00 -2 8 1 -0.24 0.00 -2 8 0 0.34 0.00 2 -8 1 -0.43 0.00 2 -8 2 0.51 0.00 2 -8 3 -0.55 0.00 2 -8 4 0.53 0.00 2 -8 5 -0.46 0.00 2 -8 6 0.36 0.00 2 -8 7 -0.29 0.00 2 -8 8 0.23 0.00 2 -8 9 -0.19 0.00 2 -8 10 0.13 0.00 2 -8 11 -0.03 0.00 2 -8 12 -0.08 0.00 2 -8 13 0.21 0.00 2 -8 14 -0.31 0.00 -2 7 21 -0.24 0.00 -2 7 20 0.42 0.00 -2 7 19 -0.54 0.00 -2 7 18 0.50 0.00 -2 7 17 -0.29 0.00 -2 7 16 -0.07 0.00 -2 7 15 0.46 0.00 -2 7 14 -0.79 0.00 -2 7 13 0.98 0.00 -2 7 12 -1.04 0.00 -2 7 11 1.00 0.00 -2 7 10 -0.91 0.00 -2 7 9 0.79 0.00 -2 7 8 -0.64 0.00 -2 7 7 0.41 0.00 -2 7 6 -0.12 0.00 -2 7 5 -0.21 0.00 -2 7 4 0.49 0.00 -2 7 3 -0.65 0.00 -2 7 2 0.70 0.00 -2 7 1 -0.70 0.00 -2 7 0 0.68 0.00 2 -7 1 -0.66 0.00 2 -7 2 0.61 0.00 2 -7 3 -0.50 0.00 2 -7 4 0.32 0.00 2 -7 5 -0.13 0.00 2 -7 6 -0.05 0.00 2 -7 7 0.17 0.00 2 -7 8 -0.26 0.00 2 -7 9 0.31 0.00 2 -7 10 -0.34 0.00 2 -7 11 0.35 0.00 2 -7 12 -0.36 0.00 2 -7 13 0.38 0.00 2 -7 14 -0.40 0.00 2 -7 15 0.40 0.00 2 -7 16 -0.34 0.00 -2 6 21 0.11 0.00 -2 6 20 0.18 0.00 -2 6 19 -0.46 0.00 -2 6 18 0.63 0.00 -2 6 17 -0.63 0.00 -2 6 16 0.49 0.00 -2 6 15 -0.26 0.00 -2 6 14 0.00 0.00 -2 6 13 0.19 0.00 -2 6 12 -0.28 0.00 -2 6 11 0.22 0.00 -2 6 10 0.00 0.00 -2 6 9 -0.37 0.00 -2 6 8 0.84 0.00 -2 6 7 -1.38 0.00 -2 6 6 1.89 0.00 -2 6 5 -2.29 0.00 -2 6 4 2.49 0.00 -2 6 3 -2.47 0.00 -2 6 2 2.26 0.00 -2 6 1 -1.91 0.00 -2 6 0 1.45 0.00 2 -6 1 -0.91 0.00 2 -6 2 0.31 0.00 2 -6 3 0.26 0.00 2 -6 4 -0.72 0.00 2 -6 5 0.99 0.00 2 -6 6 -1.08 0.00 2 -6 7 1.05 0.00 2 -6 8 -0.98 0.00 2 -6 9 0.90 0.00 2 -6 10 -0.80 0.00 2 -6 11 0.68 0.00 2 -6 12 -0.56 0.00 2 -6 13 0.47 0.00 2 -6 14 -0.44 0.00 2 -6 15 0.43 0.00 2 -6 16 -0.40 0.00 2 -6 17 0.32 0.00 -2 5 22 -0.79 0.00 -2 5 21 0.78 0.00 -2 5 20 -0.64 0.00 -2 5 19 0.41 0.00 -2 5 18 -0.16 0.00 -2 5 17 -0.07 0.00 -2 5 16 0.24 0.00 -2 5 15 -0.32 0.00 -2 5 14 0.31 0.00 -2 5 13 -0.26 0.00 -2 5 12 0.24 0.00 -2 5 11 -0.36 0.00 -2 5 10 0.67 0.00 -2 5 9 -1.18 0.00 -2 5 8 1.84 0.00 -2 5 7 -2.58 0.00 -2 5 6 3.30 0.00 -2 5 5 -3.91 0.00 -2 5 4 4.32 0.00 -2 5 3 -4.43 0.00 -2 5 2 4.19 0.00 -2 5 1 -3.58 0.00 -2 5 0 2.59 0.00 2 -5 1 -1.32 0.00 2 -5 2 -0.04 0.00 2 -5 3 1.24 0.00 2 -5 4 -2.07 0.00 2 -5 5 2.43 0.00 2 -5 6 -2.41 0.00 2 -5 7 2.16 0.00 2 -5 8 -1.84 0.00 2 -5 9 1.49 0.00 2 -5 10 -1.12 0.00 2 -5 11 0.74 0.00 2 -5 12 -0.43 0.00 2 -5 13 0.27 0.00 2 -5 14 -0.27 0.00 2 -5 15 0.38 0.00 2 -5 16 -0.48 0.00 2 -5 17 0.51 0.00 2 -5 18 -0.47 0.00 2 -5 19 0.39 0.00 -2 4 22 -0.85 0.00 -2 4 21 1.05 0.00 -2 4 20 -1.17 0.00 -2 4 19 1.18 0.00 -2 4 18 -1.05 0.00 -2 4 17 0.81 0.00 -2 4 16 -0.52 0.00 -2 4 15 0.28 0.00 -2 4 14 -0.15 0.00 -2 4 13 0.11 0.00 -2 4 12 -0.08 0.00 -2 4 11 -0.01 0.00 -2 4 10 0.22 0.00 -2 4 9 -0.58 0.00 -2 4 8 1.09 0.00 -2 4 7 -1.76 0.00 -2 4 6 2.58 0.00 -2 4 5 -3.48 0.00 -2 4 4 4.32 0.00 -2 4 3 -4.88 0.00 -2 4 2 4.97 0.00 -2 4 1 -4.44 0.00 -2 4 0 3.29 0.00 2 -4 1 -1.70 0.00 2 -4 2 0.00 0.00 2 -4 3 1.43 0.00 2 -4 4 -2.32 0.00 2 -4 5 2.64 0.00 2 -4 6 -2.53 0.00 2 -4 7 2.22 0.00 2 -4 8 -1.86 0.00 2 -4 9 1.46 0.00 2 -4 10 -1.01 0.00 2 -4 11 0.53 0.00 2 -4 12 -0.13 0.00 2 -4 13 -0.06 0.00 2 -4 14 0.01 0.00 2 -4 15 0.19 0.00 2 -4 16 -0.40 0.00 2 -4 17 0.54 0.00 2 -4 18 -0.58 0.00 2 -4 19 0.56 0.00 2 -4 20 -0.50 0.00 -2 3 23 0.21 0.00 -2 3 22 -0.39 0.00 -2 3 21 0.61 0.00 -2 3 20 -0.84 0.00 -2 3 19 0.98 0.00 -2 3 18 -0.99 0.00 -2 3 17 0.86 0.00 -2 3 16 -0.69 0.00 -2 3 15 0.58 0.00 -2 3 14 -0.59 0.00 -2 3 13 0.71 0.00 -2 3 12 -0.89 0.00 -2 3 11 1.09 0.00 -2 3 10 -1.28 0.00 -2 3 9 1.42 0.00 -2 3 8 -1.41 0.00 -2 3 7 1.13 0.00 -2 3 6 -0.48 0.00 -2 3 5 -0.50 0.00 -2 3 4 1.63 0.00 -2 3 3 -2.61 0.00 -2 3 2 3.15 0.00 -2 3 1 -3.06 0.00 -2 3 0 2.34 0.00 2 -3 1 -1.19 0.00 2 -3 2 -0.04 0.00 2 -3 3 0.97 0.00 2 -3 4 -1.38 0.00 2 -3 5 1.31 0.00 2 -3 6 -0.96 0.00 2 -3 7 0.57 0.00 2 -3 8 -0.27 0.00 2 -3 9 0.04 0.00 2 -3 10 0.20 0.00 2 -3 11 -0.46 0.00 2 -3 12 0.66 0.00 2 -3 13 -0.71 0.00 2 -3 14 0.58 0.00 2 -3 15 -0.33 0.00 2 -3 16 0.09 0.00 2 -3 17 0.10 0.00 2 -3 18 -0.23 0.00 2 -3 19 0.34 0.00 2 -3 20 -0.41 0.00 2 -3 21 0.42 0.00 -2 2 23 -0.17 0.00 -2 2 22 0.11 0.00 -2 2 21 0.00 0.00 -2 2 20 -0.12 0.00 -2 2 19 0.19 0.00 -2 2 18 -0.17 0.00 -2 2 17 0.10 0.00 -2 2 16 -0.07 0.00 -2 2 15 0.19 0.00 -2 2 14 -0.51 0.00 -2 2 13 0.99 0.00 -2 2 12 -1.61 0.00 -2 2 11 2.35 0.00 -2 2 10 -3.20 0.00 -2 2 9 4.07 0.00 -2 2 8 -4.82 0.00 -2 2 7 5.23 0.00 -2 2 6 -5.16 0.00 -2 2 4 -3.62 0.00 -2 2 3 2.50 0.00 -2 2 2 -1.46 0.00 -2 2 1 0.69 0.00 -2 2 0 -0.28 0.00 2 -2 1 0.19 0.00 2 -2 2 -0.26 0.00 2 -2 3 0.26 0.00 2 -2 4 -0.02 0.00 2 -2 5 -0.48 0.00 2 -2 6 1.08 0.00 2 -2 7 -1.60 0.00 2 -2 8 1.92 0.00 2 -2 9 -2.07 0.00 2 -2 10 2.13 0.00 2 -2 11 -2.15 0.00 2 -2 12 2.09 0.00 2 -2 13 -1.93 0.00 2 -2 14 1.66 0.00 2 -2 15 -1.34 0.00 2 -2 16 1.01 0.00 2 -2 17 -0.69 0.00 2 -2 18 0.37 0.00 2 -2 19 -0.06 0.00 2 -2 20 -0.20 0.00 2 -2 21 0.34 0.00 2 -2 22 -0.34 0.00 -2 1 22 0.39 0.00 -2 1 21 -0.37 0.00 -2 1 20 0.35 0.00 -2 1 19 -0.38 0.00 -2 1 18 0.48 0.00 -2 1 17 -0.58 0.00 -2 1 16 0.56 0.00 -2 1 15 -0.34 0.00 -2 1 14 -0.15 0.00 -2 1 13 0.89 0.00 -2 1 12 -1.85 0.00 -2 1 11 3.03 0.00 -2 1 10 -4.39 0.00 -2 1 9 5.84 0.00 -2 1 8 -7.22 0.00 -2 1 7 8.34 0.00 -2 1 6 -9.03 0.00 -2 1 5 9.19 0.00 -2 1 4 -8.75 0.00 -2 1 3 7.71 0.00 -2 1 2 -6.15 0.00 -2 1 1 4.27 0.00 -2 1 0 -2.39 0.00 2 -1 2 0.25 0.00 2 -1 4 1.40 0.00 2 -1 5 -1.83 0.00 2 -1 6 2.28 0.00 2 -1 7 -2.68 0.00 2 -1 8 2.95 0.00 2 -1 9 -3.07 0.00 2 -1 10 3.09 0.00 2 -1 11 -3.04 0.00 2 -1 12 2.94 0.00 2 -1 13 -2.77 0.00 2 -1 14 2.50 0.00 2 -1 15 -2.16 0.00 2 -1 16 1.74 0.00 2 -1 17 -1.25 0.00 2 -1 18 0.72 0.00 2 -1 19 -0.20 0.00 2 -1 20 -0.20 0.00 2 -1 21 0.41 0.00 2 -1 22 -0.43 0.00 -2 0 22 0.47 0.00 -2 0 21 -0.51 0.00 -2 0 20 0.54 0.00 -2 0 19 -0.59 0.00 -2 0 18 0.69 0.00 -2 0 17 -0.78 0.00 -2 0 16 0.77 0.00 -2 0 15 -0.57 0.00 -2 0 14 0.11 0.00 -2 0 13 0.61 0.00 -2 0 12 -1.55 0.00 -2 0 11 2.68 0.00 -2 0 10 -3.96 0.00 -2 0 9 5.30 0.00 -2 0 8 -6.60 0.00 -2 0 7 7.74 0.00 -2 0 6 -8.60 0.00 -2 0 5 9.00 0.00 -2 0 4 -8.73 0.00 -2 0 3 7.59 0.00 -2 0 2 -5.55 0.00 2 0 0 -0.26 0.00 2 0 2 2.94 0.00 2 0 4 2.86 0.00 2 0 5 -2.45 0.00 2 0 6 2.17 0.00 2 0 7 -2.06 0.00 2 0 8 2.03 0.00 2 0 9 -2.01 0.00 2 0 10 1.97 0.00 2 0 11 -1.96 0.00 2 0 12 1.98 0.00 2 0 13 -2.00 0.00 2 0 14 1.95 0.00 2 0 15 -1.78 0.00 2 0 16 1.45 0.00 2 0 17 -0.98 0.00 2 0 18 0.44 0.00 2 0 19 0.07 0.00 2 0 20 -0.44 0.00 2 0 21 0.61 0.00 2 0 22 -0.58 0.00 2 0 23 0.43 0.00 -2 -1 22 0.30 0.00 -2 -1 21 -0.35 0.00 -2 -1 20 0.38 0.00 -2 -1 19 -0.44 0.00 -2 -1 18 0.53 0.00 -2 -1 17 -0.62 0.00 -2 -1 16 0.64 0.00 -2 -1 15 -0.50 0.00 -2 -1 14 0.16 0.00 -2 -1 13 0.38 0.00 -2 -1 12 -1.06 0.00 -2 -1 11 1.81 0.00 -2 -1 10 -2.55 0.00 -2 -1 9 3.21 0.00 -2 -1 8 -3.73 0.00 -2 -1 7 4.07 0.00 -2 -1 6 -4.13 0.00 -2 -1 5 3.75 0.00 -2 -1 4 -2.69 0.00 -2 -1 3 0.76 0.00 -2 -1 2 1.94 0.00 -2 -1 1 -4.92 0.00 2 1 1 -8.77 0.00 2 1 3 -7.23 0.00 2 1 5 -3.24 0.00 2 1 6 1.69 0.00 2 1 7 -0.65 0.00 2 1 8 0.01 0.00 2 1 9 0.36 0.00 2 1 10 -0.52 0.00 2 1 11 0.49 0.00 2 1 12 -0.31 0.00 2 1 13 0.06 0.00 2 1 14 0.16 0.00 2 1 15 -0.25 0.00 2 1 16 0.19 0.00 2 1 17 0.01 0.00 2 1 18 -0.30 0.00 2 1 19 0.58 0.00 2 1 20 -0.76 0.00 2 1 21 0.79 0.00 2 1 22 -0.68 0.00 2 1 23 0.48 0.00 -2 -2 21 0.13 0.00 -2 -2 20 -0.16 0.00 -2 -2 19 0.14 0.00 -2 -2 18 -0.05 0.00 -2 -2 17 -0.06 0.00 -2 -2 16 0.12 0.00 -2 -2 15 -0.05 0.00 -2 -2 14 -0.18 0.00 -2 -2 13 0.51 0.00 -2 -2 12 -0.88 0.00 -2 -2 11 1.21 0.00 -2 -2 10 -1.45 0.00 -2 -2 9 1.52 0.00 -2 -2 8 -1.39 0.00 -2 -2 7 0.97 0.00 -2 -2 6 -0.14 0.00 -2 -2 5 -1.28 0.00 -2 -2 4 3.47 0.00 -2 -2 2 9.96 0.00 -2 -2 1 -13.29 0.00 2 2 0 15.62 0.00 2 2 1 -16.26 0.00 2 2 2 15.03 0.00 2 2 3 -12.32 0.00 2 2 4 8.89 0.00 2 2 5 -5.49 0.00 2 2 6 2.61 0.00 2 2 7 -0.41 0.00 2 2 8 -1.11 0.00 2 2 9 2.06 0.00 2 2 10 -2.50 0.00 2 2 11 2.53 0.00 2 2 12 -2.29 0.00 2 2 13 1.92 0.00 2 2 14 -1.57 0.00 2 2 15 1.30 0.00 2 2 16 -1.13 0.00 2 2 17 1.04 0.00 2 2 18 -1.00 0.00 2 2 19 0.98 0.00 2 2 20 -0.94 0.00 2 2 21 0.83 0.00 2 2 22 -0.65 0.00 2 2 23 0.42 0.00 -2 -3 21 0.49 0.00 -2 -3 20 -0.62 0.00 -2 -3 19 0.69 0.00 -2 -3 18 -0.68 0.00 -2 -3 17 0.63 0.00 -2 -3 16 -0.61 0.00 -2 -3 15 0.67 0.00 -2 -3 14 -0.80 0.00 -2 -3 13 0.93 0.00 -2 -3 12 -1.02 0.00 -2 -3 11 1.04 0.00 -2 -3 10 -0.99 0.00 -2 -3 9 0.88 0.00 -2 -3 8 -0.63 0.00 -2 -3 7 0.13 0.00 -2 -3 6 0.83 0.00 -2 -3 5 -2.45 0.00 -2 -3 4 4.90 0.00 -2 -3 3 -8.11 0.00 -2 -3 2 11.72 0.00 -2 -3 1 -15.08 0.00 2 3 0 17.42 0.00 2 3 1 -18.15 0.00 2 3 2 17.13 0.00 2 3 3 -14.67 0.00 2 3 4 11.38 0.00 2 3 5 -7.88 0.00 2 3 6 4.62 0.00 2 3 7 -1.87 0.00 2 3 8 -0.25 0.00 2 3 9 1.67 0.00 2 3 10 -2.44 0.00 2 3 11 2.68 0.00 2 3 12 -2.58 0.00 2 3 13 2.33 0.00 2 3 14 -2.05 0.00 2 3 15 1.80 0.00 2 3 16 -1.57 0.00 2 3 17 1.36 0.00 2 3 18 -1.17 0.00 2 3 19 1.01 0.00 2 3 20 -0.85 0.00 2 3 21 0.68 0.00 2 3 22 -0.49 0.00 2 3 23 0.27 0.00 2 3 24 -0.08 0.00 -2 -4 20 -0.58 0.00 -2 -4 19 0.71 0.00 -2 -4 18 -0.79 0.00 -2 -4 17 0.83 0.00 -2 -4 16 -0.88 0.00 -2 -4 15 0.95 0.00 -2 -4 14 -1.01 0.00 -2 -4 13 1.01 0.00 -2 -4 12 -0.94 0.00 -2 -4 11 0.82 0.00 -2 -4 10 -0.72 0.00 -2 -4 9 0.68 0.00 -2 -4 8 -0.62 0.00 -2 -4 7 0.41 0.00 -2 -4 6 0.14 0.00 -2 -4 5 -1.22 0.00 -2 -4 4 2.93 0.00 -2 -4 3 -5.22 0.00 -2 -4 2 7.85 0.00 -2 -4 1 -10.36 0.00 2 4 0 12.26 0.00 2 4 1 -13.16 0.00 2 4 2 12.91 0.00 2 4 3 -11.67 0.00 2 4 4 9.73 0.00 2 4 5 -7.46 0.00 2 4 6 5.15 0.00 2 4 7 -3.04 0.00 2 4 8 1.31 0.00 2 4 9 -0.06 0.00 2 4 10 -0.71 0.00 2 4 11 1.09 0.00 2 4 12 -1.21 0.00 2 4 13 1.19 0.00 2 4 14 -1.10 0.00 2 4 15 0.97 0.00 2 4 16 -0.80 0.00 2 4 17 0.65 0.00 2 4 18 -0.55 0.00 2 4 19 0.50 0.00 2 4 20 -0.47 0.00 2 4 21 0.42 0.00 2 4 22 -0.33 0.00 2 4 23 0.21 0.00 2 4 24 -0.09 0.00 -2 -5 19 0.44 0.00 -2 -5 18 -0.52 0.00 -2 -5 17 0.54 0.00 -2 -5 16 -0.51 0.00 -2 -5 15 0.48 0.00 -2 -5 14 -0.45 0.00 -2 -5 13 0.41 0.00 -2 -5 12 -0.36 0.00 -2 -5 11 0.37 0.00 -2 -5 10 -0.47 0.00 -2 -5 9 0.64 0.00 -2 -5 8 -0.81 0.00 -2 -5 7 0.87 0.00 -2 -5 6 -0.70 0.00 -2 -5 5 0.25 0.00 -2 -5 4 0.52 0.00 -2 -5 3 -1.57 0.00 -2 -5 2 2.81 0.00 -2 -5 1 -4.04 0.00 2 5 0 5.08 0.00 2 5 1 -5.72 0.00 2 5 2 5.88 0.00 2 5 3 -5.59 0.00 2 5 4 4.96 0.00 2 5 5 -4.15 0.00 2 5 6 3.29 0.00 2 5 7 -2.49 0.00 2 5 8 1.83 0.00 2 5 9 -1.31 0.00 2 5 10 0.93 0.00 2 5 11 -0.64 0.00 2 5 12 0.44 0.00 2 5 13 -0.33 0.00 2 5 14 0.35 0.00 2 5 15 -0.48 0.00 2 5 16 0.65 0.00 2 5 17 -0.75 0.00 2 5 18 0.71 0.00 2 5 19 -0.52 0.00 2 5 20 0.25 0.00 2 5 21 0.01 0.00 2 5 22 -0.19 0.00 2 5 23 0.27 0.00 -2 -6 18 -0.39 0.00 -2 -6 17 0.31 0.00 -2 -6 16 -0.13 0.00 -2 -6 15 -0.07 0.00 -2 -6 14 0.23 0.00 -2 -6 13 -0.30 0.00 -2 -6 12 0.24 0.00 -2 -6 11 -0.01 0.00 -2 -6 10 -0.36 0.00 -2 -6 9 0.78 0.00 -2 -6 8 -1.15 0.00 -2 -6 7 1.39 0.00 -2 -6 6 -1.47 0.00 -2 -6 5 1.43 0.00 -2 -6 4 -1.31 0.00 -2 -6 3 1.10 0.00 -2 -6 2 -0.82 0.00 -2 -6 1 0.45 0.00 2 6 0 -0.07 0.00 2 6 1 -0.27 0.00 2 6 2 0.49 0.00 2 6 3 -0.60 0.00 2 6 4 0.64 0.00 2 6 5 -0.68 0.00 2 6 6 0.78 0.00 2 6 7 -0.94 0.00 2 6 8 1.13 0.00 2 6 9 -1.26 0.00 2 6 10 1.28 0.00 2 6 11 -1.18 0.00 2 6 12 1.06 0.00 2 6 13 -1.00 0.00 2 6 14 1.11 0.00 2 6 15 -1.35 0.00 2 6 16 1.62 0.00 2 6 17 -1.78 0.00 2 6 18 1.75 0.00 2 6 19 -1.50 0.00 2 6 20 1.10 0.00 2 6 21 -0.65 0.00 2 6 22 0.23 0.00 2 6 23 0.10 0.00 -2 -7 17 0.34 0.00 -2 -7 16 -0.15 0.00 -2 -7 15 -0.10 0.00 -2 -7 14 0.35 0.00 -2 -7 13 -0.49 0.00 -2 -7 12 0.45 0.00 -2 -7 11 -0.21 0.00 -2 -7 10 -0.20 0.00 -2 -7 9 0.68 0.00 -2 -7 8 -1.15 0.00 -2 -7 7 1.52 0.00 -2 -7 6 -1.82 0.00 -2 -7 5 2.07 0.00 -2 -7 4 -2.27 0.00 -2 -7 3 2.40 0.00 -2 -7 2 -2.41 0.00 -2 -7 1 2.30 0.00 2 7 0 -2.08 0.00 2 7 1 1.84 0.00 2 7 2 -1.64 0.00 2 7 3 1.48 0.00 2 7 4 -1.30 0.00 2 7 5 1.05 0.00 2 7 6 -0.70 0.00 2 7 7 0.29 0.00 2 7 8 0.12 0.00 2 7 9 -0.41 0.00 2 7 10 0.55 0.00 2 7 11 -0.56 0.00 2 7 12 0.54 0.00 2 7 13 -0.59 0.00 2 7 14 0.78 0.00 2 7 15 -1.07 0.00 2 7 16 1.38 0.00 2 7 17 -1.61 0.00 2 7 18 1.69 0.00 2 7 19 -1.62 0.00 2 7 20 1.41 0.00 2 7 21 -1.10 0.00 2 7 22 0.75 0.00 2 7 23 -0.40 0.00 -2 -8 15 0.19 0.00 -2 -8 14 0.02 0.00 -2 -8 13 -0.24 0.00 -2 -8 12 0.37 0.00 -2 -8 11 -0.38 0.00 -2 -8 10 0.23 0.00 -2 -8 9 0.06 0.00 -2 -8 8 -0.46 0.00 -2 -8 7 0.93 0.00 -2 -8 6 -1.43 0.00 -2 -8 5 1.90 0.00 -2 -8 4 -2.27 0.00 -2 -8 3 2.44 0.00 -2 -8 2 -2.39 0.00 -2 -8 1 2.17 0.00 2 8 0 -1.88 0.00 2 8 1 1.62 0.00 2 8 2 -1.44 0.00 2 8 3 1.32 0.00 2 8 4 -1.20 0.00 2 8 5 1.00 0.00 2 8 6 -0.73 0.00 2 8 7 0.45 0.00 2 8 8 -0.23 0.00 2 8 9 0.15 0.00 2 8 10 -0.20 0.00 2 8 11 0.32 0.00 2 8 12 -0.43 0.00 2 8 13 0.44 0.00 2 8 14 -0.32 0.00 2 8 15 0.11 0.00 2 8 16 0.15 0.00 2 8 17 -0.38 0.00 2 8 18 0.58 0.00 2 8 19 -0.71 0.00 2 8 20 0.78 0.00 2 8 21 -0.78 0.00 2 8 22 0.70 0.00 -2 -9 13 0.12 0.00 -2 -9 12 0.09 0.00 -2 -9 11 -0.29 0.00 -2 -9 10 0.42 0.00 -2 -9 9 -0.43 0.00 -2 -9 8 0.24 0.00 -2 -9 7 0.14 0.00 -2 -9 6 -0.66 0.00 -2 -9 5 1.19 0.00 -2 -9 4 -1.58 0.00 -2 -9 3 1.70 0.00 -2 -9 2 -1.56 0.00 -2 -9 1 1.25 0.00 2 9 0 -0.90 0.00 2 9 1 0.62 0.00 2 9 2 -0.45 0.00 2 9 3 0.31 0.00 2 9 4 -0.16 0.00 2 9 5 -0.04 0.00 2 9 6 0.25 0.00 2 9 7 -0.39 0.00 2 9 8 0.38 0.00 2 9 9 -0.18 0.00 2 9 10 -0.20 0.00 2 9 11 0.66 0.00 2 9 12 -1.09 0.00 2 9 13 1.40 0.00 2 9 14 -1.55 0.00 2 9 15 1.52 0.00 2 9 16 -1.34 0.00 2 9 17 1.08 0.00 2 9 18 -0.79 0.00 2 9 19 0.51 0.00 2 9 20 -0.27 0.00 2 9 21 0.08 0.00 -2 -10 11 0.17 0.00 -2 -10 10 -0.02 0.00 -2 -10 9 -0.14 0.00 -2 -10 8 0.21 0.00 -2 -10 7 -0.14 0.00 -2 -10 6 -0.07 0.00 -2 -10 5 0.31 0.00 -2 -10 4 -0.47 0.00 -2 -10 3 0.45 0.00 -2 -10 2 -0.27 0.00 -2 -10 1 -0.01 0.00 2 10 0 0.30 0.00 2 10 1 -0.53 0.00 2 10 2 0.71 0.00 2 10 3 -0.88 0.00 2 10 4 1.06 0.00 2 10 5 -1.24 0.00 2 10 6 1.37 0.00 2 10 7 -1.37 0.00 2 10 8 1.20 0.00 2 10 9 -0.84 0.00 2 10 10 0.29 0.00 2 10 11 0.37 0.00 2 10 12 -1.06 0.00 2 10 13 1.66 0.00 2 10 14 -2.08 0.00 2 10 15 2.25 0.00 2 10 16 -2.19 0.00 2 10 17 1.95 0.00 2 10 18 -1.61 0.00 2 10 19 1.26 0.00 2 10 20 -0.96 0.00 -2 -11 9 0.36 0.00 -2 -11 8 -0.18 0.00 -2 -11 7 -0.01 0.00 -2 -11 6 0.18 0.00 -2 -11 5 -0.34 0.00 -2 -11 4 0.52 0.00 -2 -11 3 -0.73 0.00 -2 -11 2 0.97 0.00 -2 -11 1 -1.20 0.00 2 11 0 1.41 0.00 2 11 1 -1.60 0.00 2 11 2 1.79 0.00 2 11 3 -1.96 0.00 2 11 4 2.08 0.00 2 11 5 -2.10 0.00 2 11 6 2.00 0.00 2 11 7 -1.77 0.00 2 11 8 1.45 0.00 2 11 9 -1.06 0.00 2 11 10 0.59 0.00 2 11 11 -0.06 0.00 2 11 12 -0.51 0.00 2 11 13 1.07 0.00 2 11 14 -1.53 0.00 2 11 15 1.80 0.00 2 11 16 -1.86 0.00 2 11 17 1.73 0.00 2 11 18 -1.48 0.00 -2 -12 6 0.18 0.00 -2 -12 5 -0.44 0.00 -2 -12 4 0.71 0.00 -2 -12 3 -0.94 0.00 -2 -12 2 1.14 0.00 -2 -12 1 -1.31 0.00 2 12 0 1.49 0.00 2 12 1 -1.70 0.00 2 12 2 1.94 0.00 2 12 3 -2.16 0.00 2 12 4 2.27 0.00 2 12 5 -2.20 0.00 2 12 6 1.96 0.00 2 12 7 -1.60 0.00 2 12 8 1.22 0.00 2 12 9 -0.87 0.00 2 12 10 0.58 0.00 2 12 11 -0.32 0.00 2 12 12 0.04 0.00 2 12 13 0.25 0.00 2 12 14 -0.54 0.00 2 12 15 0.76 0.00 2 12 16 -0.87 0.00 -2 -13 1 -0.41 0.00 2 13 0 0.50 0.00 2 13 1 -0.68 0.00 2 13 2 0.92 0.00 2 13 3 -1.16 0.00 2 13 4 1.33 0.00 2 13 5 -1.35 0.00 2 13 6 1.22 0.00 2 13 7 -0.98 0.00 2 13 8 0.73 0.00 2 13 9 -0.52 0.00 2 13 10 0.38 0.00 2 13 11 -0.30 0.00 2 13 12 0.24 0.00 -3 11 11 0.33 0.00 -3 11 10 -0.23 0.00 -3 11 9 -0.12 0.00 -3 11 8 0.60 0.00 -3 11 7 -1.06 0.00 -3 11 6 1.30 0.00 -3 11 5 -1.25 0.00 -3 11 4 0.98 0.00 -3 11 3 -0.62 0.00 -3 11 2 0.30 0.00 -3 11 1 -0.09 0.00 -3 11 0 -0.03 0.00 3 -11 1 0.09 0.00 3 -11 2 -0.13 0.00 3 -11 3 0.15 0.00 -3 10 15 0.05 0.00 -3 10 14 0.07 0.00 -3 10 13 -0.05 0.00 -3 10 12 -0.11 0.00 -3 10 11 0.28 0.00 -3 10 10 -0.32 0.00 -3 10 9 0.16 0.00 -3 10 8 0.18 0.00 -3 10 7 -0.57 0.00 -3 10 6 0.88 0.00 -3 10 5 -1.04 0.00 -3 10 4 1.06 0.00 -3 10 3 -0.98 0.00 -3 10 2 0.85 0.00 -3 10 1 -0.68 0.00 -3 10 0 0.47 0.00 3 -10 1 -0.22 0.00 3 -10 2 -0.04 0.00 3 -10 3 0.27 0.00 3 -10 4 -0.41 0.00 3 -10 5 0.45 0.00 3 -10 6 -0.36 0.00 3 -10 7 0.21 0.00 -3 9 17 0.70 0.00 -3 9 16 -0.59 0.00 -3 9 15 0.39 0.00 -3 9 14 -0.21 0.00 -3 9 13 0.15 0.00 -3 9 12 -0.21 0.00 -3 9 11 0.35 0.00 -3 9 10 -0.49 0.00 -3 9 9 0.55 0.00 -3 9 8 -0.51 0.00 -3 9 7 0.39 0.00 -3 9 6 -0.19 0.00 -3 9 5 -0.06 0.00 -3 9 4 0.35 0.00 -3 9 3 -0.61 0.00 -3 9 2 0.80 0.00 -3 9 1 -0.85 0.00 -3 9 0 0.75 0.00 3 -9 1 -0.55 0.00 3 -9 2 0.30 0.00 3 -9 3 -0.05 0.00 3 -9 4 -0.15 0.00 3 -9 5 0.29 0.00 3 -9 6 -0.34 0.00 3 -9 7 0.32 0.00 3 -9 8 -0.25 0.00 3 -9 9 0.19 0.00 3 -9 10 -0.17 0.00 -3 8 18 -0.45 0.00 -3 8 17 0.59 0.00 -3 8 16 -0.67 0.00 -3 8 15 0.70 0.00 -3 8 14 -0.70 0.00 -3 8 13 0.71 0.00 -3 8 12 -0.73 0.00 -3 8 11 0.79 0.00 -3 8 10 -0.87 0.00 -3 8 8 -1.10 0.00 -3 8 7 1.16 0.00 -3 8 6 -1.10 0.00 -3 8 5 0.91 0.00 -3 8 4 -0.60 0.00 -3 8 3 0.26 0.00 -3 8 2 0.03 0.00 -3 8 1 -0.24 0.00 -3 8 0 0.39 0.00 3 -8 1 -0.50 0.00 3 -8 2 0.57 0.00 3 -8 3 -0.61 0.00 3 -8 4 0.58 0.00 3 -8 5 -0.49 0.00 3 -8 6 0.38 0.00 3 -8 7 -0.28 0.00 3 -8 8 0.21 0.00 3 -8 9 -0.14 0.00 3 -8 10 0.06 0.00 3 -8 11 0.05 0.00 3 -8 12 -0.19 0.00 3 -8 13 0.33 0.00 -3 7 20 0.19 0.00 -3 7 19 -0.16 0.00 -3 7 18 0.06 0.00 -3 7 17 0.12 0.00 -3 7 16 -0.38 0.00 -3 7 15 0.68 0.00 -3 7 14 -0.97 0.00 -3 7 13 1.22 0.00 -3 7 12 -1.40 0.00 -3 7 11 1.54 0.00 -3 7 10 -1.65 0.00 -3 7 9 1.74 0.00 -3 7 8 -1.79 0.00 -3 7 7 1.75 0.00 -3 7 6 -1.61 0.00 -3 7 5 1.36 0.00 -3 7 4 -1.07 0.00 -3 7 3 0.81 0.00 -3 7 2 -0.57 0.00 -3 7 1 0.33 0.00 -3 7 0 -0.03 0.00 3 -7 1 -0.34 0.00 3 -7 2 0.72 0.00 3 -7 3 -0.99 0.00 3 -7 4 1.09 0.00 3 -7 5 -1.04 0.00 3 -7 6 0.89 0.00 3 -7 7 -0.72 0.00 3 -7 8 0.58 0.00 3 -7 9 -0.47 0.00 3 -7 10 0.35 0.00 3 -7 11 -0.21 0.00 3 -7 12 0.03 0.00 3 -7 13 0.19 0.00 3 -7 14 -0.42 0.00 3 -7 15 0.59 0.00 -3 6 20 0.54 0.00 -3 6 19 -0.61 0.00 -3 6 18 0.57 0.00 -3 6 17 -0.40 0.00 -3 6 16 0.10 0.00 -3 6 15 0.29 0.00 -3 6 14 -0.70 0.00 -3 6 13 1.10 0.00 -3 6 12 -1.45 0.00 -3 6 11 1.74 0.00 -3 6 10 -1.93 0.00 -3 6 9 2.00 0.00 -3 6 8 -1.92 0.00 -3 6 7 1.68 0.00 -3 6 6 -1.33 0.00 -3 6 5 0.95 0.00 -3 6 4 -0.64 0.00 -3 6 3 0.43 0.00 -3 6 2 -0.29 0.00 -3 6 1 0.12 0.00 -3 6 0 0.12 0.00 3 -6 1 -0.43 0.00 3 -6 2 0.69 0.00 3 -6 3 -0.84 0.00 3 -6 4 0.81 0.00 3 -6 5 -0.67 0.00 3 -6 6 0.48 0.00 3 -6 7 -0.31 0.00 3 -6 8 0.17 0.00 3 -6 9 -0.07 0.00 3 -6 10 0.01 0.00 3 -6 11 0.02 0.00 3 -6 12 -0.06 0.00 3 -6 13 0.14 0.00 3 -6 14 -0.28 0.00 3 -6 15 0.43 0.00 3 -6 16 -0.53 0.00 -3 5 21 -0.43 0.00 -3 5 20 0.63 0.00 -3 5 19 -0.75 0.00 -3 5 18 0.76 0.00 -3 5 17 -0.65 0.00 -3 5 16 0.44 0.00 -3 5 15 -0.17 0.00 -3 5 14 -0.13 0.00 -3 5 13 0.43 0.00 -3 5 12 -0.71 0.00 -3 5 11 0.91 0.00 -3 5 10 -0.99 0.00 -3 5 9 0.89 0.00 -3 5 8 -0.61 0.00 -3 5 7 0.18 0.00 -3 5 6 0.34 0.00 -3 5 5 -0.82 0.00 -3 5 4 1.19 0.00 -3 5 3 -1.39 0.00 -3 5 2 1.44 0.00 -3 5 1 -1.37 0.00 -3 5 0 1.20 0.00 3 -5 1 -0.92 0.00 3 -5 2 0.53 0.00 3 -5 3 -0.07 0.00 3 -5 4 -0.35 0.00 3 -5 5 0.65 0.00 3 -5 6 -0.79 0.00 3 -5 7 0.82 0.00 3 -5 8 -0.79 0.00 3 -5 9 0.75 0.00 3 -5 10 -0.66 0.00 3 -5 11 0.53 0.00 3 -5 12 -0.37 0.00 3 -5 13 0.26 0.00 3 -5 14 -0.25 0.00 3 -5 15 0.31 0.00 3 -5 16 -0.39 0.00 3 -5 17 0.40 0.00 3 -5 18 -0.35 0.00 -3 4 22 -0.23 0.00 -3 4 21 0.08 0.00 -3 4 20 0.10 0.00 -3 4 19 -0.26 0.00 -3 4 18 0.37 0.00 -3 4 17 -0.43 0.00 -3 4 16 0.44 0.00 -3 4 15 -0.41 0.00 -3 4 14 0.34 0.00 -3 4 13 -0.25 0.00 -3 4 12 0.19 0.00 -3 4 11 -0.21 0.00 -3 4 10 0.37 0.00 -3 4 9 -0.68 0.00 -3 4 8 1.14 0.00 -3 4 7 -1.73 0.00 -3 4 6 2.41 0.00 -3 4 5 -3.12 0.00 -3 4 4 3.77 0.00 -3 4 3 -4.25 0.00 -3 4 2 4.42 0.00 -3 4 1 -4.17 0.00 -3 4 0 3.45 0.00 3 -4 1 -2.29 0.00 3 -4 2 0.89 0.00 3 -4 3 0.48 0.00 3 -4 4 -1.53 0.00 3 -4 5 2.11 0.00 3 -4 6 -2.25 0.00 3 -4 7 2.12 0.00 3 -4 8 -1.88 0.00 3 -4 9 1.61 0.00 3 -4 10 -1.30 0.00 3 -4 11 0.95 0.00 3 -4 12 -0.61 0.00 3 -4 13 0.38 0.00 3 -4 14 -0.31 0.00 3 -4 15 0.36 0.00 3 -4 16 -0.45 0.00 3 -4 17 0.46 0.00 3 -4 18 -0.38 0.00 3 -4 19 0.28 0.00 -3 3 22 -0.64 0.00 -3 3 21 0.64 0.00 -3 3 20 -0.58 0.00 -3 3 19 0.46 0.00 -3 3 18 -0.28 0.00 -3 3 17 0.05 0.00 -3 3 16 0.20 0.00 -3 3 15 -0.41 0.00 -3 3 14 0.54 0.00 -3 3 13 -0.60 0.00 -3 3 12 0.66 0.00 -3 3 11 -0.77 0.00 -3 3 10 0.94 0.00 -3 3 9 -1.20 0.00 -3 3 8 1.55 0.00 -3 3 7 -2.06 0.00 -3 3 6 2.81 0.00 -3 3 5 -3.82 0.00 -3 3 4 4.97 0.00 -3 3 3 -6.02 0.00 -3 3 2 6.66 0.00 -3 3 1 -6.59 0.00 -3 3 0 5.69 0.00 3 -3 1 -4.05 0.00 3 -3 2 2.01 0.00 3 -3 3 -0.03 0.00 3 -3 4 -1.49 0.00 3 -3 5 2.36 0.00 3 -3 6 -2.64 0.00 3 -3 7 2.55 0.00 3 -3 8 -2.29 0.00 3 -3 9 1.97 0.00 3 -3 10 -1.57 0.00 3 -3 11 1.11 0.00 3 -3 12 -0.66 0.00 3 -3 13 0.36 0.00 3 -3 14 -0.27 0.00 3 -3 15 0.33 0.00 3 -3 16 -0.42 0.00 3 -3 17 0.44 0.00 3 -3 18 -0.38 0.00 3 -3 19 0.30 0.00 3 -3 20 -0.24 0.00 -3 2 22 -0.47 0.00 -3 2 21 0.58 0.00 -3 2 20 -0.66 0.00 -3 2 19 0.65 0.00 -3 2 18 -0.52 0.00 -3 2 17 0.27 0.00 -3 2 16 0.03 0.00 -3 2 15 -0.27 0.00 -3 2 14 0.41 0.00 -3 2 13 -0.44 0.00 -3 2 12 0.41 0.00 -3 2 11 -0.33 0.00 -3 2 10 0.22 0.00 -3 2 9 -0.07 0.00 -3 2 8 -0.03 0.00 -3 2 7 -0.09 0.00 -3 2 6 0.63 0.00 -3 2 5 -1.67 0.00 -3 2 4 3.07 0.00 -3 2 3 -4.55 0.00 -3 2 2 5.70 0.00 -3 2 1 -6.17 0.00 -3 2 0 5.78 0.00 3 -2 1 -4.62 0.00 3 -2 2 2.99 0.00 3 -2 3 -1.33 0.00 3 -2 4 0.00 0.00 3 -2 5 0.80 0.00 3 -2 6 -1.12 0.00 3 -2 7 1.15 0.00 3 -2 8 -1.03 0.00 3 -2 9 0.85 0.00 3 -2 10 -0.59 0.00 3 -2 11 0.26 0.00 3 -2 12 0.05 0.00 3 -2 13 -0.24 0.00 3 -2 14 0.27 0.00 3 -2 15 -0.19 0.00 3 -2 16 0.07 0.00 3 -2 17 0.00 0.00 3 -2 18 -0.04 0.00 3 -2 19 0.08 0.00 3 -2 20 -0.16 0.00 3 -2 21 0.23 0.00 -3 1 22 0.07 0.00 -3 1 21 0.02 0.00 -3 1 20 -0.14 0.00 -3 1 19 0.20 0.00 -3 1 18 -0.17 0.00 -3 1 17 0.04 0.00 -3 1 16 0.10 0.00 -3 1 15 -0.15 0.00 -3 1 14 0.05 0.00 -3 1 13 0.21 0.00 -3 1 12 -0.59 0.00 -3 1 11 1.10 0.00 -3 1 10 -1.73 0.00 -3 1 9 2.47 0.00 -3 1 8 -3.17 0.00 -3 1 7 3.61 0.00 -3 1 6 -3.57 0.00 -3 1 5 2.95 0.00 -3 1 4 -1.82 0.00 -3 1 3 0.40 0.00 -3 1 2 1.05 0.00 -3 1 1 -2.25 0.00 -3 1 0 3.01 0.00 3 -1 1 -3.26 0.00 3 -1 2 3.06 0.00 3 -1 3 -2.61 0.00 3 -1 4 2.13 0.00 3 -1 5 -1.80 0.00 3 -1 6 1.65 0.00 3 -1 7 -1.62 0.00 3 -1 8 1.62 0.00 3 -1 9 -1.64 0.00 3 -1 10 1.67 0.00 3 -1 11 -1.72 0.00 3 -1 12 1.73 0.00 3 -1 13 -1.66 0.00 3 -1 14 1.50 0.00 3 -1 15 -1.26 0.00 3 -1 16 1.00 0.00 3 -1 17 -0.75 0.00 3 -1 18 0.50 0.00 3 -1 19 -0.23 0.00 3 -1 20 -0.03 0.00 3 -1 21 0.22 0.00 3 -1 22 -0.29 0.00 -3 0 22 0.56 0.00 -3 0 21 -0.57 0.00 -3 0 20 0.51 0.00 -3 0 19 -0.43 0.00 -3 0 18 0.39 0.00 -3 0 17 -0.38 0.00 -3 0 16 0.33 0.00 -3 0 15 -0.16 0.00 -3 0 14 -0.22 0.00 -3 0 13 0.81 0.00 -3 0 12 -1.59 0.00 -3 0 11 2.57 0.00 -3 0 10 -3.73 0.00 -3 0 9 5.00 0.00 -3 0 8 -6.22 0.00 -3 0 7 7.20 0.00 -3 0 6 -7.76 0.00 -3 0 5 7.81 0.00 -3 0 4 -7.34 0.00 -3 0 3 6.36 0.00 -3 0 2 -4.93 0.00 -3 0 1 3.15 0.00 3 0 0 -1.24 0.00 3 0 1 -0.52 0.00 3 0 2 1.91 0.00 3 0 4 3.37 0.00 3 0 5 -3.64 0.00 3 0 6 3.78 0.00 3 0 7 -3.83 0.00 3 0 8 3.79 0.00 3 0 9 -3.67 0.00 3 0 10 3.51 0.00 3 0 11 -3.33 0.00 3 0 12 3.14 0.00 3 0 13 -2.91 0.00 3 0 14 2.63 0.00 3 0 15 -2.29 0.00 3 0 16 1.89 0.00 3 0 17 -1.43 0.00 3 0 18 0.94 0.00 3 0 19 -0.45 0.00 3 0 20 0.02 0.00 3 0 21 0.28 0.00 3 0 22 -0.41 0.00 -3 -1 21 -0.87 0.00 -3 -1 20 0.91 0.00 -3 -1 19 -0.90 0.00 -3 -1 18 0.87 0.00 -3 -1 17 -0.81 0.00 -3 -1 16 0.69 0.00 -3 -1 15 -0.42 0.00 -3 -1 14 -0.06 0.00 -3 -1 13 0.75 0.00 -3 -1 12 -1.66 0.00 -3 -1 11 2.78 0.00 -3 -1 10 -4.07 0.00 -3 -1 9 5.47 0.00 -3 -1 8 -6.83 0.00 -3 -1 7 8.02 0.00 -3 -1 6 -8.93 0.00 -3 -1 5 9.46 0.00 -3 -1 4 -9.55 0.00 -3 -1 3 9.07 0.00 -3 -1 2 -7.93 0.00 -3 -1 1 6.14 0.00 3 1 0 -3.95 0.00 3 1 1 1.73 0.00 3 1 2 0.17 0.00 3 1 3 -1.56 0.00 3 1 4 2.47 0.00 3 1 5 -3.04 0.00 3 1 6 3.40 0.00 3 1 7 -3.60 0.00 3 1 8 3.62 0.00 3 1 9 -3.48 0.00 3 1 10 3.24 0.00 3 1 11 -3.01 0.00 3 1 12 2.84 0.00 3 1 13 -2.71 0.00 3 1 14 2.59 0.00 3 1 15 -2.40 0.00 3 1 16 2.10 0.00 3 1 17 -1.68 0.00 3 1 18 1.18 0.00 3 1 19 -0.65 0.00 3 1 20 0.18 0.00 3 1 21 0.18 0.00 3 1 22 -0.38 0.00 3 1 23 0.44 0.00 -3 -2 21 -0.60 0.00 -3 -2 20 0.75 0.00 -3 -2 19 -0.89 0.00 -3 -2 18 1.00 0.00 -3 -2 17 -1.06 0.00 -3 -2 16 1.02 0.00 -3 -2 15 -0.81 0.00 -3 -2 14 0.42 0.00 -3 -2 13 0.15 0.00 -3 -2 12 -0.85 0.00 -3 -2 11 1.67 0.00 -3 -2 10 -2.59 0.00 -3 -2 9 3.59 0.00 -3 -2 8 -4.60 0.00 -3 -2 7 5.53 0.00 -3 -2 6 -6.29 0.00 -3 -2 5 6.78 0.00 -3 -2 4 -6.87 0.00 -3 -2 3 6.43 0.00 -3 -2 2 -5.39 0.00 -3 -2 1 3.87 0.00 3 2 0 -2.17 0.00 3 2 1 0.66 0.00 3 2 2 0.37 0.00 3 2 3 -0.87 0.00 3 2 4 1.02 0.00 3 2 5 -1.05 0.00 3 2 6 1.08 0.00 3 2 7 -1.12 0.00 3 2 8 1.10 0.00 3 2 9 -0.99 0.00 3 2 10 0.84 0.00 3 2 11 -0.77 0.00 3 2 12 0.83 0.00 3 2 13 -1.00 0.00 3 2 14 1.19 0.00 3 2 15 -1.32 0.00 3 2 16 1.34 0.00 3 2 17 -1.22 0.00 3 2 18 0.99 0.00 3 2 19 -0.70 0.00 3 2 20 0.40 0.00 3 2 21 -0.13 0.00 3 2 22 -0.06 0.00 3 2 23 0.15 0.00 -3 -3 20 0.04 0.00 -3 -3 19 -0.25 0.00 -3 -3 18 0.51 0.00 -3 -3 17 -0.76 0.00 -3 -3 16 0.89 0.00 -3 -3 15 -0.83 0.00 -3 -3 14 0.60 0.00 -3 -3 13 -0.26 0.00 -3 -3 12 -0.10 0.00 -3 -3 11 0.45 0.00 -3 -3 10 -0.80 0.00 -3 -3 9 1.19 0.00 -3 -3 8 -1.65 0.00 -3 -3 7 2.10 0.00 -3 -3 6 -2.45 0.00 -3 -3 5 2.51 0.00 -3 -3 4 -2.13 0.00 -3 -3 3 1.21 0.00 -3 -3 2 0.19 0.00 -3 -3 1 -1.80 0.00 3 3 0 3.20 0.00 3 3 1 -4.00 0.00 3 3 2 3.98 0.00 3 3 3 -3.24 0.00 3 3 4 2.10 0.00 3 3 5 -0.90 0.00 3 3 6 -0.14 0.00 3 3 7 0.94 0.00 3 3 8 -1.53 0.00 3 3 9 1.92 0.00 3 3 10 -2.08 0.00 3 3 11 2.00 0.00 3 3 12 -1.70 0.00 3 3 13 1.28 0.00 3 3 14 -0.84 0.00 3 3 15 0.45 0.00 3 3 16 -0.16 0.00 3 3 17 -0.05 0.00 3 3 18 0.18 0.00 3 3 19 -0.25 0.00 3 3 20 0.26 0.00 3 3 21 -0.24 0.00 3 3 22 0.21 0.00 3 3 23 -0.20 0.00 -3 -4 20 -0.59 0.00 -3 -4 19 0.52 0.00 -3 -4 18 -0.32 0.00 -3 -4 17 0.05 0.00 -3 -4 16 0.17 0.00 -3 -4 15 -0.25 0.00 -3 -4 14 0.20 0.00 -3 -4 13 -0.09 0.00 -3 -4 12 0.02 0.00 -3 -4 11 -0.03 0.00 -3 -4 10 0.10 0.00 -3 -4 9 -0.13 0.00 -3 -4 8 0.08 0.00 -3 -4 7 -0.01 0.00 -3 -4 6 0.04 0.00 -3 -4 5 -0.37 0.00 -3 -4 4 1.16 0.00 -3 -4 3 -2.48 0.00 -3 -4 2 4.19 0.00 -3 -4 1 -5.98 0.00 3 4 0 7.42 0.00 3 4 1 -8.10 0.00 3 4 2 7.85 0.00 3 4 3 -6.73 0.00 3 4 4 5.02 0.00 3 4 5 -3.05 0.00 3 4 6 1.11 0.00 3 4 7 0.60 0.00 3 4 8 -1.98 0.00 3 4 9 2.93 0.00 3 4 10 -3.42 0.00 3 4 11 3.49 0.00 3 4 12 -3.25 0.00 3 4 13 2.84 0.00 3 4 14 -2.39 0.00 3 4 15 1.95 0.00 3 4 16 -1.54 0.00 3 4 17 1.17 0.00 3 4 18 -0.85 0.00 3 4 19 0.57 0.00 3 4 20 -0.33 0.00 3 4 21 0.13 0.00 3 4 22 0.05 0.00 3 4 23 -0.20 0.00 -3 -5 19 0.79 0.00 -3 -5 18 -0.82 0.00 -3 -5 17 0.71 0.00 -3 -5 16 -0.53 0.00 -3 -5 15 0.36 0.00 -3 -5 14 -0.27 0.00 -3 -5 13 0.21 0.00 -3 -5 12 -0.13 0.00 -3 -5 11 0.02 0.00 -3 -5 10 0.11 0.00 -3 -5 9 -0.22 0.00 -3 -5 8 0.30 0.00 -3 -5 7 -0.42 0.00 -3 -5 6 0.70 0.00 -3 -5 5 -1.25 0.00 -3 -5 4 2.16 0.00 -3 -5 3 -3.40 0.00 -3 -5 2 4.86 0.00 -3 -5 1 -6.32 0.00 3 5 0 7.50 0.00 3 5 1 -8.14 0.00 3 5 2 8.09 0.00 3 5 3 -7.38 0.00 3 5 4 6.11 0.00 3 5 5 -4.48 0.00 3 5 6 2.71 0.00 3 5 7 -0.98 0.00 3 5 8 -0.53 0.00 3 5 9 1.70 0.00 3 5 10 -2.47 0.00 3 5 11 2.86 0.00 3 5 12 -2.95 0.00 3 5 13 2.82 0.00 3 5 14 -2.54 0.00 3 5 15 2.18 0.00 3 5 16 -1.80 0.00 3 5 17 1.45 0.00 3 5 18 -1.18 0.00 3 5 19 0.99 0.00 3 5 20 -0.83 0.00 3 5 21 0.66 0.00 3 5 22 -0.45 0.00 3 5 23 0.21 0.00 -3 -6 18 -0.79 0.00 -3 -6 17 0.81 0.00 -3 -6 16 -0.68 0.00 -3 -6 15 0.49 0.00 -3 -6 14 -0.31 0.00 -3 -6 13 0.17 0.00 -3 -6 12 -0.10 0.00 -3 -6 11 0.10 0.00 -3 -6 10 -0.15 0.00 -3 -6 9 0.25 0.00 -3 -6 8 -0.30 0.00 -3 -6 7 0.21 0.00 -3 -6 6 0.10 0.00 -3 -6 5 -0.67 0.00 -3 -6 4 1.44 0.00 -3 -6 3 -2.34 0.00 -3 -6 2 3.26 0.00 -3 -6 1 -4.10 0.00 3 6 0 4.75 0.00 3 6 1 -5.15 0.00 3 6 2 5.22 0.00 3 6 3 -4.96 0.00 3 6 4 4.41 0.00 3 6 5 -3.62 0.00 3 6 6 2.71 0.00 3 6 7 -1.76 0.00 3 6 8 0.86 0.00 3 6 9 -0.07 0.00 3 6 10 -0.57 0.00 3 6 11 1.06 0.00 3 6 12 -1.35 0.00 3 6 13 1.44 0.00 3 6 14 -1.32 0.00 3 6 15 1.04 0.00 3 6 16 -0.71 0.00 3 6 17 0.45 0.00 3 6 18 -0.37 0.00 3 6 19 0.45 0.00 3 6 20 -0.61 0.00 3 6 21 0.74 0.00 3 6 22 -0.76 0.00 3 6 23 0.65 0.00 -3 -7 16 -0.47 0.00 -3 -7 15 0.31 0.00 -3 -7 14 -0.15 0.00 -3 -7 13 0.04 0.00 -3 -7 12 -0.02 0.00 -3 -7 11 0.13 0.00 -3 -7 10 -0.35 0.00 -3 -7 9 0.61 0.00 -3 -7 8 -0.84 0.00 -3 -7 7 0.93 0.00 -3 -7 6 -0.82 0.00 -3 -7 5 0.52 0.00 -3 -7 4 -0.11 0.00 -3 -7 3 -0.36 0.00 -3 -7 2 0.83 0.00 -3 -7 1 -1.25 0.00 3 7 0 1.62 0.00 3 7 1 -1.89 0.00 3 7 2 2.04 0.00 3 7 3 -2.07 0.00 3 7 4 1.98 0.00 3 7 5 -1.81 0.00 3 7 6 1.62 0.00 3 7 7 -1.42 0.00 3 7 8 1.22 0.00 3 7 9 -0.99 0.00 3 7 10 0.72 0.00 3 7 11 -0.45 0.00 3 7 12 0.24 0.00 3 7 13 -0.18 0.00 3 7 14 0.30 0.00 3 7 15 -0.56 0.00 3 7 16 0.85 0.00 3 7 17 -1.01 0.00 3 7 18 0.97 0.00 3 7 19 -0.71 0.00 3 7 20 0.32 0.00 3 7 21 0.09 0.00 3 7 22 -0.40 0.00 3 7 23 0.56 0.00 -3 -8 15 0.20 0.00 -3 -8 14 -0.14 0.00 -3 -8 13 0.12 0.00 -3 -8 12 -0.15 0.00 -3 -8 11 0.25 0.00 -3 -8 10 -0.42 0.00 -3 -8 9 0.64 0.00 -3 -8 8 -0.88 0.00 -3 -8 7 1.11 0.00 -3 -8 6 -1.29 0.00 -3 -8 5 1.40 0.00 -3 -8 4 -1.44 0.00 -3 -8 3 1.39 0.00 -3 -8 2 -1.24 0.00 -3 -8 1 1.00 0.00 3 8 0 -0.71 0.00 3 8 1 0.42 0.00 3 8 2 -0.18 0.00 3 8 3 0.00 0.00 3 8 4 0.16 0.00 3 8 5 -0.32 0.00 3 8 6 0.52 0.00 3 8 7 -0.74 0.00 3 8 8 0.93 0.00 3 8 9 -1.04 0.00 3 8 10 1.05 0.00 3 8 11 -1.02 0.00 3 8 12 0.99 0.00 3 8 13 -1.06 0.00 3 8 14 1.23 0.00 3 8 15 -1.47 0.00 3 8 16 1.69 0.00 3 8 17 -1.79 0.00 3 8 18 1.73 0.00 3 8 19 -1.50 0.00 3 8 20 1.16 0.00 3 8 21 -0.77 0.00 3 8 22 0.40 0.00 -3 -9 13 0.31 0.00 -3 -9 12 -0.37 0.00 -3 -9 11 0.41 0.00 -3 -9 10 -0.46 0.00 -3 -9 9 0.55 0.00 -3 -9 8 -0.70 0.00 -3 -9 7 0.97 0.00 -3 -9 6 -1.33 0.00 -3 -9 5 1.73 0.00 -3 -9 4 -2.07 0.00 -3 -9 3 2.26 0.00 -3 -9 2 -2.26 0.00 -3 -9 1 2.10 0.00 3 9 0 -1.86 0.00 3 9 1 1.62 0.00 3 9 2 -1.40 0.00 3 9 3 1.17 0.00 3 9 4 -0.88 0.00 3 9 5 0.50 0.00 3 9 6 -0.06 0.00 3 9 7 -0.36 0.00 3 9 8 0.67 0.00 3 9 9 -0.81 0.00 3 9 10 0.81 0.00 3 9 11 -0.72 0.00 3 9 12 0.66 0.00 3 9 13 -0.67 0.00 3 9 14 0.80 0.00 3 9 15 -0.99 0.00 3 9 16 1.18 0.00 3 9 17 -1.32 0.00 3 9 18 1.36 0.00 3 9 19 -1.31 0.00 3 9 20 1.18 0.00 3 9 21 -1.00 0.00 -3 -10 11 0.57 0.00 -3 -10 10 -0.58 0.00 -3 -10 9 0.58 0.00 -3 -10 8 -0.65 0.00 -3 -10 7 0.85 0.00 -3 -10 6 -1.19 0.00 -3 -10 5 1.61 0.00 -3 -10 4 -1.96 0.00 -3 -10 3 2.14 0.00 -3 -10 2 -2.12 0.00 -3 -10 1 1.96 0.00 3 10 0 -1.76 0.00 3 10 1 1.59 0.00 3 10 2 -1.44 0.00 3 10 3 1.24 0.00 3 10 4 -0.90 0.00 3 10 5 0.45 0.00 3 10 6 0.06 0.00 3 10 7 -0.48 0.00 3 10 8 0.69 0.00 3 10 9 -0.65 0.00 3 10 10 0.38 0.00 3 10 11 0.01 0.00 3 10 12 -0.39 0.00 3 10 13 0.66 0.00 3 10 14 -0.76 0.00 3 10 15 0.68 0.00 3 10 16 -0.46 0.00 3 10 17 0.17 0.00 3 10 18 0.10 0.00 3 10 19 -0.32 0.00 3 10 20 0.45 0.00 -3 -11 9 0.62 0.00 -3 -11 8 -0.60 0.00 -3 -11 7 0.64 0.00 -3 -11 6 -0.79 0.00 -3 -11 5 0.98 0.00 -3 -11 4 -1.13 0.00 -3 -11 3 1.15 0.00 -3 -11 2 -1.04 0.00 -3 -11 1 0.87 0.00 3 11 0 -0.71 0.00 3 11 1 0.58 0.00 3 11 2 -0.46 0.00 3 11 3 0.28 0.00 3 11 4 -0.01 0.00 3 11 5 -0.33 0.00 3 11 6 0.63 0.00 3 11 7 -0.81 0.00 3 11 8 0.78 0.00 3 11 9 -0.52 0.00 3 11 10 0.06 0.00 3 11 11 0.52 0.00 3 11 12 -1.14 0.00 3 11 13 1.68 0.00 3 11 14 -2.03 0.00 3 11 15 2.12 0.00 3 11 16 -1.96 0.00 3 11 17 1.61 0.00 3 11 18 -1.17 0.00 -3 -12 6 -0.23 0.00 -3 -12 5 0.17 0.00 -3 -12 4 -0.09 0.00 -3 -12 3 -0.03 0.00 -3 -12 2 0.17 0.00 -3 -12 1 -0.31 0.00 3 12 0 0.42 0.00 3 12 1 -0.52 0.00 3 12 2 0.65 0.00 3 12 3 -0.81 0.00 3 12 4 0.98 0.00 3 12 5 -1.11 0.00 3 12 6 1.14 0.00 3 12 7 -1.03 0.00 3 12 8 0.80 0.00 3 12 9 -0.46 0.00 3 12 10 0.05 0.00 3 12 11 0.43 0.00 3 12 12 -0.95 0.00 3 12 13 1.45 0.00 3 12 14 -1.85 0.00 3 12 15 2.06 0.00 3 12 16 -2.05 0.00 -3 -13 1 -0.67 0.00 3 13 0 0.74 0.00 3 13 1 -0.82 0.00 3 13 2 0.94 0.00 3 13 3 -1.09 0.00 3 13 4 1.22 0.00 3 13 5 -1.27 0.00 3 13 6 1.19 0.00 3 13 7 -1.02 0.00 3 13 8 0.78 0.00 3 13 9 -0.53 0.00 3 13 10 0.29 0.00 3 13 11 -0.05 0.00 3 13 12 -0.22 0.00 -4 10 12 0.59 0.00 -4 10 11 -0.38 0.00 -4 10 10 0.13 0.00 -4 10 9 0.01 0.00 -4 10 8 0.02 0.00 -4 10 2 0.04 0.00 -4 10 1 0.04 0.00 -4 10 0 -0.09 0.00 4 -10 1 0.13 0.00 4 -10 2 -0.18 0.00 4 -10 3 0.24 0.00 4 -10 4 -0.25 0.00 4 -10 5 0.18 0.00 -4 9 15 0.44 0.00 -4 9 14 -0.10 0.00 -4 9 13 -0.16 0.00 -4 9 12 0.24 0.00 -4 9 11 -0.18 0.00 -4 9 10 0.08 0.00 -4 9 9 -0.03 0.00 -4 9 8 0.08 0.00 -4 9 7 -0.20 0.00 -4 9 6 0.31 0.00 -4 9 5 -0.36 0.00 -4 9 4 0.36 0.00 -4 9 3 -0.32 0.00 -4 9 2 0.26 0.00 -4 9 1 -0.18 0.00 -4 9 0 0.04 0.00 4 -9 1 0.17 0.00 4 -9 2 -0.42 0.00 4 -9 3 0.65 0.00 4 -9 4 -0.80 0.00 4 -9 5 0.81 0.00 4 -9 6 -0.68 0.00 4 -9 7 0.46 0.00 4 -9 8 -0.22 0.00 4 -9 9 0.05 0.00 -4 8 17 1.07 0.00 -4 8 16 -1.04 0.00 -4 8 15 0.88 0.00 -4 8 14 -0.66 0.00 -4 8 12 -0.42 0.00 -4 8 11 0.41 0.00 -4 8 10 -0.42 0.00 -4 8 9 0.39 0.00 -4 8 8 -0.31 0.00 -4 8 7 0.19 0.00 -4 8 6 -0.06 0.00 -4 8 5 -0.05 0.00 -4 8 4 0.14 0.00 -4 8 3 -0.19 0.00 -4 8 2 0.20 0.00 -4 8 1 -0.15 0.00 -4 8 0 0.04 0.00 4 -8 1 0.10 0.00 4 -8 2 -0.26 0.00 4 -8 3 0.42 0.00 4 -8 4 -0.55 0.00 4 -8 5 0.62 0.00 4 -8 6 -0.63 0.00 4 -8 7 0.57 0.00 4 -8 8 -0.48 0.00 4 -8 9 0.40 0.00 4 -8 10 -0.35 0.00 4 -8 11 0.33 0.00 4 -8 12 -0.33 0.00 -4 7 18 -0.64 0.00 -4 7 17 0.79 0.00 -4 7 16 -0.86 0.00 -4 7 15 0.88 0.00 -4 7 14 -0.88 0.00 -4 7 13 0.90 0.00 -4 7 12 -0.95 0.00 -4 7 11 1.01 0.00 -4 7 10 -1.06 0.00 -4 7 9 1.07 0.00 -4 7 8 -1.02 0.00 -4 7 7 0.90 0.00 -4 7 6 -0.73 0.00 -4 7 5 0.54 0.00 -4 7 4 -0.38 0.00 -4 7 3 0.29 0.00 -4 7 2 -0.27 0.00 -4 7 1 0.28 0.00 -4 7 0 -0.25 0.00 4 -7 1 0.12 0.00 4 -7 2 0.09 0.00 4 -7 3 -0.30 0.00 4 -7 4 0.43 0.00 4 -7 5 -0.45 0.00 4 -7 6 0.38 0.00 4 -7 7 -0.27 0.00 4 -7 8 0.14 0.00 4 -7 9 -0.01 0.00 4 -7 10 -0.11 0.00 4 -7 11 0.23 0.00 4 -7 12 -0.35 0.00 4 -7 13 0.46 0.00 4 -7 14 -0.54 0.00 -4 6 19 -0.10 0.00 -4 6 18 -0.12 0.00 -4 6 17 0.36 0.00 -4 6 16 -0.62 0.00 -4 6 15 0.86 0.00 -4 6 14 -1.10 0.00 -4 6 13 1.34 0.00 -4 6 12 -1.59 0.00 -4 6 11 1.84 0.00 -4 6 10 -2.07 0.00 -4 6 9 2.21 0.00 -4 6 8 -2.21 0.00 -4 6 7 2.04 0.00 -4 6 6 -1.73 0.00 -4 6 5 1.36 0.00 -4 6 4 -1.05 0.00 -4 6 3 0.85 0.00 -4 6 2 -0.76 0.00 -4 6 1 0.68 0.00 -4 6 0 -0.48 0.00 4 -6 1 0.12 0.00 4 -6 2 0.35 0.00 4 -6 3 -0.80 0.00 4 -6 4 1.10 0.00 4 -6 5 -1.22 0.00 4 -6 6 1.17 0.00 4 -6 7 -1.01 0.00 4 -6 8 0.80 0.00 4 -6 9 -0.58 0.00 4 -6 10 0.35 0.00 4 -6 11 -0.13 0.00 4 -6 12 -0.09 0.00 4 -6 13 0.31 0.00 4 -6 14 -0.54 0.00 4 -6 15 0.73 0.00 4 -6 16 -0.84 0.00 -4 5 20 0.85 0.00 -4 5 19 -0.72 0.00 -4 5 18 0.45 0.00 -4 5 17 -0.06 0.00 -4 5 16 -0.40 0.00 -4 5 15 0.88 0.00 -4 5 14 -1.33 0.00 -4 5 13 1.77 0.00 -4 5 12 -2.18 0.00 -4 5 11 2.58 0.00 -4 5 10 -2.91 0.00 -4 5 9 3.12 0.00 -4 5 8 -3.12 0.00 -4 5 7 2.89 0.00 -4 5 6 -2.47 0.00 -4 5 5 1.96 0.00 -4 5 4 -1.48 0.00 -4 5 3 1.11 0.00 -4 5 2 -0.83 0.00 -4 5 1 0.57 0.00 -4 5 0 -0.24 0.00 4 -5 1 -0.16 0.00 4 -5 2 0.57 0.00 4 -5 3 -0.90 0.00 4 -5 4 1.09 0.00 4 -5 5 -1.16 0.00 4 -5 6 1.14 0.00 4 -5 7 -1.05 0.00 4 -5 8 0.90 0.00 4 -5 9 -0.70 0.00 4 -5 10 0.49 0.00 4 -5 11 -0.30 0.00 4 -5 12 0.14 0.00 4 -5 13 0.03 0.00 4 -5 14 -0.24 0.00 4 -5 15 0.50 0.00 4 -5 16 -0.74 0.00 4 -5 17 0.87 0.00 -4 4 21 -0.80 0.00 -4 4 20 0.96 0.00 -4 4 19 -0.96 0.00 -4 4 18 0.79 0.00 -4 4 17 -0.44 0.00 -4 4 16 -0.03 0.00 -4 4 15 0.54 0.00 -4 4 14 -1.04 0.00 -4 4 13 1.52 0.00 -4 4 12 -1.94 0.00 -4 4 11 2.28 0.00 -4 4 10 -2.51 0.00 -4 4 9 2.58 0.00 -4 4 8 -2.47 0.00 -4 4 7 2.18 0.00 -4 4 6 -1.74 0.00 -4 4 5 1.21 0.00 -4 4 4 -0.66 0.00 -4 4 3 0.14 0.00 -4 4 2 0.32 0.00 -4 4 1 -0.70 0.00 -4 4 0 0.97 0.00 4 -4 1 -1.08 0.00 4 -4 2 1.01 0.00 4 -4 3 -0.83 0.00 4 -4 4 0.62 0.00 4 -4 5 -0.50 0.00 4 -4 6 0.48 0.00 4 -4 7 -0.52 0.00 4 -4 8 0.52 0.00 4 -4 9 -0.44 0.00 4 -4 10 0.32 0.00 4 -4 11 -0.23 0.00 4 -4 12 0.20 0.00 4 -4 13 -0.17 0.00 4 -4 14 0.06 0.00 4 -4 15 0.15 0.00 4 -4 16 -0.40 0.00 4 -4 17 0.58 0.00 4 -4 18 -0.62 0.00 -4 3 21 -0.06 0.00 -4 3 20 0.29 0.00 -4 3 19 -0.47 0.00 -4 3 18 0.55 0.00 -4 3 17 -0.51 0.00 -4 3 16 0.38 0.00 -4 3 15 -0.16 0.00 -4 3 14 -0.12 0.00 -4 3 13 0.43 0.00 -4 3 12 -0.70 0.00 -4 3 11 0.87 0.00 -4 3 10 -0.91 0.00 -4 3 9 0.81 0.00 -4 3 8 -0.60 0.00 -4 3 7 0.30 0.00 -4 3 6 0.13 0.00 -4 3 5 -0.70 0.00 -4 3 4 1.41 0.00 -4 3 3 -2.19 0.00 -4 3 2 2.90 0.00 -4 3 1 -3.34 0.00 -4 3 0 3.35 0.00 4 -3 1 -2.87 0.00 4 -3 2 1.98 0.00 4 -3 3 -0.94 0.00 4 -3 4 0.03 0.00 4 -3 5 0.53 0.00 4 -3 6 -0.72 0.00 4 -3 7 0.65 0.00 4 -3 8 -0.51 0.00 4 -3 9 0.40 0.00 4 -3 10 -0.30 0.00 4 -3 11 0.17 0.00 4 -3 12 0.00 0.00 4 -3 13 -0.14 0.00 4 -3 14 0.16 0.00 4 -3 15 -0.03 0.00 4 -3 16 -0.16 0.00 4 -3 17 0.30 0.00 4 -3 18 -0.33 0.00 4 -3 19 0.26 0.00 4 -3 20 -0.15 0.00 -4 2 21 0.58 0.00 -4 2 20 -0.48 0.00 -4 2 19 0.30 0.00 -4 2 18 -0.07 0.00 -4 2 17 -0.21 0.00 -4 2 16 0.48 0.00 -4 2 15 -0.68 0.00 -4 2 14 0.78 0.00 -4 2 13 -0.77 0.00 -4 2 12 0.73 0.00 -4 2 11 -0.71 0.00 -4 2 10 0.73 0.00 -4 2 9 -0.77 0.00 -4 2 8 0.82 0.00 -4 2 7 -0.93 0.00 -4 2 6 1.23 0.00 -4 2 5 -1.86 0.00 -4 2 4 2.81 0.00 -4 2 3 -3.96 0.00 -4 2 2 4.99 0.00 -4 2 1 -5.58 0.00 -4 2 0 5.46 0.00 4 -2 1 -4.57 0.00 4 -2 2 3.09 0.00 4 -2 3 -1.39 0.00 4 -2 4 -0.13 0.00 4 -2 5 1.20 0.00 4 -2 6 -1.73 0.00 4 -2 7 1.85 0.00 4 -2 8 -1.74 0.00 4 -2 9 1.50 0.00 4 -2 10 -1.19 0.00 4 -2 11 0.79 0.00 4 -2 12 -0.38 0.00 4 -2 13 0.04 0.00 4 -2 14 0.14 0.00 4 -2 15 -0.14 0.00 4 -2 16 0.05 0.00 4 -2 17 0.02 0.00 4 -2 18 -0.03 0.00 4 -2 19 0.00 0.00 4 -2 20 0.02 0.00 4 -2 21 -0.01 0.00 -4 1 21 0.48 0.00 -4 1 20 -0.52 0.00 -4 1 19 0.49 0.00 -4 1 18 -0.33 0.00 -4 1 17 0.03 0.00 -4 1 16 0.35 0.00 -4 1 15 -0.73 0.00 -4 1 14 1.03 0.00 -4 1 13 -1.22 0.00 -4 1 12 1.32 0.00 -4 1 11 -1.33 0.00 -4 1 10 1.25 0.00 -4 1 9 -1.02 0.00 -4 1 8 0.71 0.00 -4 1 7 -0.45 0.00 -4 1 6 0.50 0.00 -4 1 5 -1.01 0.00 -4 1 4 2.01 0.00 -4 1 3 -3.29 0.00 -4 1 2 4.50 0.00 -4 1 1 -5.28 0.00 -4 1 0 5.37 0.00 4 -1 1 -4.72 0.00 4 -1 2 3.48 0.00 4 -1 3 -1.95 0.00 4 -1 4 0.50 0.00 4 -1 5 0.62 0.00 4 -1 6 -1.30 0.00 4 -1 7 1.59 0.00 4 -1 8 -1.58 0.00 4 -1 9 1.38 0.00 4 -1 10 -1.05 0.00 4 -1 11 0.64 0.00 4 -1 12 -0.21 0.00 4 -1 13 -0.13 0.00 4 -1 14 0.32 0.00 4 -1 15 -0.37 0.00 4 -1 16 0.35 0.00 4 -1 17 -0.32 0.00 4 -1 18 0.30 0.00 4 -1 19 -0.26 0.00 4 -1 20 0.18 0.00 4 -1 21 -0.07 0.00 -4 0 21 -0.08 0.00 -4 0 20 0.03 0.00 -4 0 19 0.03 0.00 -4 0 18 -0.01 0.00 -4 0 17 -0.12 0.00 -4 0 16 0.34 0.00 -4 0 15 -0.56 0.00 -4 0 14 0.72 0.00 -4 0 13 -0.79 0.00 -4 0 12 0.74 0.00 -4 0 11 -0.56 0.00 -4 0 10 0.20 0.00 -4 0 9 0.38 0.00 -4 0 8 -1.06 0.00 -4 0 7 1.65 0.00 -4 0 6 -1.87 0.00 -4 0 5 1.56 0.00 -4 0 4 -0.74 0.00 -4 0 3 -0.41 0.00 -4 0 2 1.61 0.00 -4 0 1 -2.59 0.00 4 0 0 3.19 0.00 4 0 1 -3.32 0.00 4 0 2 3.04 0.00 4 0 3 -2.45 0.00 4 0 4 1.74 0.00 4 0 5 -1.10 0.00 4 0 6 0.65 0.00 4 0 7 -0.43 0.00 4 0 8 0.39 0.00 4 0 9 -0.47 0.00 4 0 10 0.62 0.00 4 0 11 -0.78 0.00 4 0 12 0.90 0.00 4 0 13 -0.94 0.00 4 0 14 0.90 0.00 4 0 15 -0.80 0.00 4 0 16 0.68 0.00 4 0 17 -0.57 0.00 4 0 18 0.46 0.00 4 0 19 -0.33 0.00 4 0 20 0.18 0.00 4 0 21 -0.04 0.00 4 0 22 -0.05 0.00 -4 -1 21 -0.53 0.00 -4 -1 20 0.53 0.00 -4 -1 19 -0.49 0.00 -4 -1 18 0.45 0.00 -4 -1 17 -0.44 0.00 -4 -1 16 0.45 0.00 -4 -1 15 -0.41 0.00 -4 -1 14 0.29 0.00 -4 -1 13 -0.05 0.00 -4 -1 12 -0.32 0.00 -4 -1 11 0.85 0.00 -4 -1 10 -1.58 0.00 -4 -1 9 2.50 0.00 -4 -1 8 -3.50 0.00 -4 -1 7 4.34 0.00 -4 -1 6 -4.80 0.00 -4 -1 5 4.76 0.00 -4 -1 4 -4.24 0.00 -4 -1 3 3.36 0.00 -4 -1 2 -2.28 0.00 -4 -1 1 1.10 0.00 4 1 0 0.05 0.00 4 1 1 -1.08 0.00 4 1 2 1.87 0.00 4 1 3 -2.36 0.00 4 1 4 2.58 0.00 4 1 5 -2.63 0.00 4 1 6 2.61 0.00 4 1 7 -2.60 0.00 4 1 8 2.60 0.00 4 1 9 -2.56 0.00 4 1 10 2.47 0.00 4 1 11 -2.32 0.00 4 1 12 2.13 0.00 4 1 13 -1.90 0.00 4 1 14 1.64 0.00 4 1 15 -1.37 0.00 4 1 16 1.10 0.00 4 1 17 -0.84 0.00 4 1 18 0.57 0.00 4 1 19 -0.32 0.00 4 1 20 0.07 0.00 4 1 21 0.13 0.00 4 1 22 -0.25 0.00 -4 -2 20 0.72 0.00 -4 -2 19 -0.76 0.00 -4 -2 18 0.77 0.00 -4 -2 17 -0.75 0.00 -4 -2 16 0.67 0.00 -4 -2 15 -0.48 0.00 -4 -2 14 0.15 0.00 -4 -2 13 0.32 0.00 -4 -2 12 -0.90 0.00 -4 -2 11 1.62 0.00 -4 -2 10 -2.50 0.00 -4 -2 9 3.54 0.00 -4 -2 8 -4.64 0.00 -4 -2 7 5.65 0.00 -4 -2 6 -6.39 0.00 -4 -2 5 6.74 0.00 -4 -2 4 -6.69 0.00 -4 -2 3 6.25 0.00 -4 -2 2 -5.45 0.00 -4 -2 1 4.32 0.00 4 2 0 -2.94 0.00 4 2 1 1.46 0.00 4 2 2 -0.09 0.00 4 2 3 -1.02 0.00 4 2 4 1.83 0.00 4 2 5 -2.41 0.00 4 2 6 2.82 0.00 4 2 7 -3.09 0.00 4 2 8 3.21 0.00 4 2 9 -3.15 0.00 4 2 10 2.95 0.00 4 2 11 -2.68 0.00 4 2 12 2.42 0.00 4 2 13 -2.20 0.00 4 2 14 2.01 0.00 4 2 15 -1.82 0.00 4 2 16 1.59 0.00 4 2 17 -1.32 0.00 4 2 18 0.99 0.00 4 2 19 -0.65 0.00 4 2 20 0.30 0.00 4 2 21 0.02 0.00 4 2 22 -0.27 0.00 4 2 23 0.40 0.00 -4 -3 20 0.51 0.00 -4 -3 19 -0.68 0.00 -4 -3 18 0.86 0.00 -4 -3 17 -0.99 0.00 -4 -3 16 1.00 0.00 -4 -3 15 -0.82 0.00 -4 -3 14 0.44 0.00 -4 -3 13 0.08 0.00 -4 -3 12 -0.67 0.00 -4 -3 11 1.28 0.00 -4 -3 10 -1.95 0.00 -4 -3 9 2.72 0.00 -4 -3 8 -3.59 0.00 -4 -3 7 4.49 0.00 -4 -3 6 -5.33 0.00 -4 -3 5 5.97 0.00 -4 -3 4 -6.31 0.00 -4 -3 3 6.28 0.00 -4 -3 2 -5.83 0.00 -4 -3 1 4.96 0.00 4 3 0 -3.81 0.00 4 3 1 2.56 0.00 4 3 2 -1.43 0.00 4 3 3 0.54 0.00 4 3 4 0.13 0.00 4 3 5 -0.65 0.00 4 3 6 1.09 0.00 4 3 7 -1.43 0.00 4 3 8 1.64 0.00 4 3 9 -1.67 0.00 4 3 10 1.58 0.00 4 3 11 -1.46 0.00 4 3 12 1.41 0.00 4 3 13 -1.45 0.00 4 3 14 1.54 0.00 4 3 15 -1.62 0.00 4 3 16 1.64 0.00 4 3 17 -1.56 0.00 4 3 18 1.40 0.00 4 3 19 -1.15 0.00 4 3 20 0.84 0.00 4 3 21 -0.49 0.00 4 3 22 0.16 0.00 4 3 23 0.08 0.00 -4 -4 19 -0.18 0.00 -4 -4 18 0.47 0.00 -4 -4 17 -0.78 0.00 -4 -4 16 0.98 0.00 -4 -4 15 -0.97 0.00 -4 -4 14 0.73 0.00 -4 -4 13 -0.34 0.00 -4 -4 12 -0.09 0.00 -4 -4 11 0.46 0.00 -4 -4 10 -0.77 0.00 -4 -4 9 1.10 0.00 -4 -4 8 -1.52 0.00 -4 -4 7 2.06 0.00 -4 -4 6 -2.65 0.00 -4 -4 5 3.15 0.00 -4 -4 4 -3.43 0.00 -4 -4 3 3.37 0.00 -4 -4 2 -2.94 0.00 -4 -4 1 2.22 0.00 4 4 0 -1.38 0.00 4 4 1 0.67 0.00 4 4 2 -0.24 0.00 4 4 3 0.14 0.00 4 4 4 -0.28 0.00 4 4 5 0.51 0.00 4 4 6 -0.72 0.00 4 4 7 0.85 0.00 4 4 8 -0.93 0.00 4 4 9 0.97 0.00 4 4 10 -0.96 0.00 4 4 11 0.85 0.00 4 4 12 -0.62 0.00 4 4 13 0.30 0.00 4 4 14 0.06 0.00 4 4 15 -0.40 0.00 4 4 16 0.68 0.00 4 4 17 -0.89 0.00 4 4 18 1.01 0.00 4 4 19 -1.04 0.00 4 4 20 0.96 0.00 4 4 21 -0.80 0.00 4 4 22 0.58 0.00 4 4 23 -0.38 0.00 -4 -5 18 -0.28 0.00 -4 -5 17 0.03 0.00 -4 -5 16 0.23 0.00 -4 -5 15 -0.40 0.00 -4 -5 14 0.41 0.00 -4 -5 13 -0.30 0.00 -4 -5 12 0.16 0.00 -4 -5 11 -0.07 0.00 -4 -5 10 0.04 0.00 -4 -5 9 -0.01 0.00 -4 -5 8 -0.09 0.00 -4 -5 7 0.27 0.00 -4 -5 6 -0.45 0.00 -4 -5 5 0.51 0.00 -4 -5 4 -0.34 0.00 -4 -5 3 -0.12 0.00 -4 -5 2 0.81 0.00 -4 -5 1 -1.59 0.00 4 5 0 2.26 0.00 4 5 1 -2.61 0.00 4 5 2 2.52 0.00 4 5 3 -2.00 0.00 4 5 4 1.16 0.00 4 5 5 -0.16 0.00 4 5 6 -0.83 0.00 4 5 7 1.69 0.00 4 5 8 -2.36 0.00 4 5 9 2.80 0.00 4 5 10 -2.98 0.00 4 5 11 2.93 0.00 4 5 12 -2.68 0.00 4 5 13 2.30 0.00 4 5 14 -1.86 0.00 4 5 15 1.39 0.00 4 5 16 -0.93 0.00 4 5 17 0.50 0.00 4 5 18 -0.12 0.00 4 5 19 -0.17 0.00 4 5 20 0.35 0.00 4 5 21 -0.43 0.00 4 5 22 0.46 0.00 4 5 23 -0.45 0.00 -4 -6 17 0.72 0.00 -4 -6 16 -0.59 0.00 -4 -6 15 0.42 0.00 -4 -6 14 -0.26 0.00 -4 -6 13 0.14 0.00 -4 -6 12 -0.04 0.00 -4 -6 11 -0.08 0.00 -4 -6 10 0.20 0.00 -4 -6 9 -0.27 0.00 -4 -6 8 0.28 0.00 -4 -6 7 -0.28 0.00 -4 -6 6 0.36 0.00 -4 -6 5 -0.66 0.00 -4 -6 4 1.21 0.00 -4 -6 3 -1.97 0.00 -4 -6 2 2.82 0.00 -4 -6 1 -3.61 0.00 4 6 0 4.16 0.00 4 6 1 -4.38 0.00 4 6 2 4.19 0.00 4 6 3 -3.62 0.00 4 6 4 2.72 0.00 4 6 5 -1.60 0.00 4 6 6 0.39 0.00 4 6 7 0.78 0.00 4 6 8 -1.81 0.00 4 6 9 2.62 0.00 4 6 10 -3.16 0.00 4 6 11 3.44 0.00 4 6 12 -3.49 0.00 4 6 13 3.35 0.00 4 6 14 -3.04 0.00 4 6 15 2.59 0.00 4 6 16 -2.07 0.00 4 6 17 1.55 0.00 4 6 18 -1.09 0.00 4 6 19 0.73 0.00 4 6 20 -0.48 0.00 4 6 21 0.29 0.00 4 6 22 -0.12 0.00 4 6 23 -0.06 0.00 -4 -7 16 -0.66 0.00 -4 -7 15 0.59 0.00 -4 -7 14 -0.49 0.00 -4 -7 13 0.38 0.00 -4 -7 12 -0.25 0.00 -4 -7 11 0.11 0.00 -4 -7 10 0.01 0.00 -4 -7 9 -0.08 0.00 -4 -7 8 0.10 0.00 -4 -7 7 -0.14 0.00 -4 -7 6 0.29 0.00 -4 -7 5 -0.65 0.00 -4 -7 4 1.22 0.00 -4 -7 3 -1.93 0.00 -4 -7 2 2.66 0.00 -4 -7 1 -3.30 0.00 4 7 0 3.76 0.00 4 7 1 -3.99 0.00 4 7 2 3.97 0.00 4 7 3 -3.69 0.00 4 7 4 3.16 0.00 4 7 5 -2.40 0.00 4 7 6 1.50 0.00 4 7 7 -0.55 0.00 4 7 8 -0.37 0.00 4 7 9 1.18 0.00 4 7 10 -1.84 0.00 4 7 11 2.34 0.00 4 7 12 -2.66 0.00 4 7 13 2.78 0.00 4 7 14 -2.67 0.00 4 7 15 2.38 0.00 4 7 16 -1.96 0.00 4 7 17 1.53 0.00 4 7 18 -1.18 0.00 4 7 19 0.97 0.00 4 7 20 -0.85 0.00 4 7 21 0.76 0.00 4 7 22 -0.63 0.00 -4 -8 14 -0.17 0.00 -4 -8 13 0.22 0.00 -4 -8 12 -0.26 0.00 -4 -8 11 0.28 0.00 -4 -8 10 -0.26 0.00 -4 -8 9 0.24 0.00 -4 -8 8 -0.21 0.00 -4 -8 7 0.16 0.00 -4 -8 6 -0.05 0.00 -4 -8 5 -0.16 0.00 -4 -8 4 0.47 0.00 -4 -8 3 -0.86 0.00 -4 -8 2 1.28 0.00 -4 -8 1 -1.69 0.00 4 8 0 2.07 0.00 4 8 1 -2.37 0.00 4 8 2 2.57 0.00 4 8 3 -2.61 0.00 4 8 4 2.47 0.00 4 8 5 -2.17 0.00 4 8 6 1.75 0.00 4 8 7 -1.25 0.00 4 8 8 0.75 0.00 4 8 9 -0.28 0.00 4 8 10 -0.14 0.00 4 8 11 0.51 0.00 4 8 12 -0.79 0.00 4 8 13 0.96 0.00 4 8 14 -0.99 0.00 4 8 15 0.90 0.00 4 8 16 -0.74 0.00 4 8 17 0.58 0.00 4 8 18 -0.50 0.00 4 8 19 0.51 0.00 4 8 20 -0.58 0.00 4 8 21 0.64 0.00 4 8 22 -0.65 0.00 -4 -9 13 0.04 0.00 -4 -9 12 -0.24 0.00 -4 -9 11 0.44 0.00 -4 -9 10 -0.58 0.00 -4 -9 9 0.65 0.00 -4 -9 8 -0.66 0.00 -4 -9 7 0.65 0.00 -4 -9 6 -0.65 0.00 -4 -9 5 0.64 0.00 -4 -9 4 -0.63 0.00 -4 -9 3 0.58 0.00 -4 -9 2 -0.45 0.00 -4 -9 1 0.25 0.00 4 9 0 0.00 0.00 4 9 1 -0.29 0.00 4 9 2 0.57 0.00 4 9 3 -0.81 0.00 4 9 4 1.00 0.00 4 9 5 -1.14 0.00 4 9 6 1.24 0.00 4 9 7 -1.29 0.00 4 9 8 1.30 0.00 4 9 9 -1.27 0.00 4 9 10 1.21 0.00 4 9 11 -1.13 0.00 4 9 12 1.07 0.00 4 9 13 -1.02 0.00 4 9 14 0.97 0.00 4 9 15 -0.91 0.00 4 9 16 0.80 0.00 4 9 17 -0.64 0.00 4 9 18 0.43 0.00 4 9 19 -0.21 0.00 4 9 20 0.01 0.00 4 9 21 0.13 0.00 -4 -10 11 0.57 0.00 -4 -10 10 -0.82 0.00 -4 -10 9 1.00 0.00 -4 -10 8 -1.13 0.00 -4 -10 7 1.25 0.00 -4 -10 6 -1.41 0.00 -4 -10 5 1.59 0.00 -4 -10 4 -1.76 0.00 -4 -10 3 1.86 0.00 -4 -10 2 -1.85 0.00 -4 -10 1 1.75 0.00 4 10 0 -1.59 0.00 4 10 1 1.40 0.00 4 10 2 -1.17 0.00 4 10 3 0.86 0.00 4 10 4 -0.45 0.00 4 10 5 -0.04 0.00 4 10 6 0.56 0.00 4 10 7 -1.03 0.00 4 10 8 1.37 0.00 4 10 9 -1.57 0.00 4 10 10 1.65 0.00 4 10 11 -1.69 0.00 4 10 12 1.71 0.00 4 10 13 -1.75 0.00 4 10 14 1.76 0.00 4 10 15 -1.71 0.00 4 10 16 1.56 0.00 4 10 17 -1.33 0.00 4 10 18 1.03 0.00 4 10 19 -0.73 0.00 4 10 20 0.47 0.00 -4 -11 8 -1.12 0.00 -4 -11 7 1.33 0.00 -4 -11 6 -1.59 0.00 -4 -11 5 1.88 0.00 -4 -11 4 -2.11 0.00 -4 -11 3 2.23 0.00 -4 -11 2 -2.22 0.00 -4 -11 1 2.12 0.00 4 11 0 -2.00 0.00 4 11 1 1.86 0.00 4 11 2 -1.68 0.00 4 11 3 1.39 0.00 4 11 4 -0.94 0.00 4 11 5 0.36 0.00 4 11 6 0.24 0.00 4 11 7 -0.73 0.00 4 11 8 1.02 0.00 4 11 9 -1.09 0.00 4 11 10 1.00 0.00 4 11 11 -0.85 0.00 4 11 12 0.74 0.00 4 11 13 -0.69 0.00 4 11 14 0.72 0.00 4 11 15 -0.79 0.00 4 11 16 0.86 0.00 4 11 17 -0.88 0.00 4 11 18 0.82 0.00 -4 -12 6 -0.90 0.00 -4 -12 5 1.14 0.00 -4 -12 4 -1.34 0.00 -4 -12 3 1.44 0.00 -4 -12 2 -1.44 0.00 -4 -12 1 1.38 0.00 4 12 0 -1.30 0.00 4 12 1 1.22 0.00 4 12 2 -1.10 0.00 4 12 3 0.87 0.00 4 12 4 -0.54 0.00 4 12 5 0.14 0.00 4 12 6 0.21 0.00 4 12 7 -0.43 0.00 4 12 8 0.45 0.00 4 12 9 -0.28 0.00 4 12 10 -0.01 0.00 4 12 11 0.34 0.00 4 12 12 -0.65 0.00 4 12 13 0.86 0.00 4 12 14 -0.93 0.00 4 12 15 0.84 0.00 4 12 16 -0.60 0.00 -4 -13 1 0.37 0.00 4 13 0 -0.37 0.00 4 13 1 0.35 0.00 4 13 2 -0.30 0.00 4 13 3 0.18 0.00 4 13 4 -0.02 0.00 4 13 5 -0.13 0.00 4 13 6 0.21 0.00 4 13 7 -0.18 0.00 4 13 8 0.05 0.00 4 13 9 0.17 0.00 4 13 10 -0.43 0.00 4 13 11 0.73 0.00 4 13 12 -1.03 0.00 -5 9 11 -0.51 0.00 -5 9 10 0.32 0.00 -5 9 0 -0.17 0.00 5 -9 1 0.15 0.00 5 -9 2 -0.15 0.00 5 -9 3 0.18 0.00 5 -9 4 -0.17 0.00 5 -9 5 0.08 0.00 5 -9 6 0.09 0.00 5 -9 7 -0.30 0.00 -5 8 15 0.52 0.00 -5 8 14 -0.21 0.00 -5 8 13 -0.05 0.00 -5 8 11 -0.17 0.00 -5 8 10 0.09 0.00 -5 8 9 -0.04 0.00 -5 8 8 0.07 0.00 -5 8 7 -0.15 0.00 -5 8 1 0.45 0.00 -5 8 0 -0.60 0.00 5 -8 1 0.75 0.00 5 -8 2 -0.88 0.00 5 -8 3 0.97 0.00 5 -8 4 -0.96 0.00 5 -8 5 0.82 0.00 5 -8 6 -0.57 0.00 5 -8 7 0.25 0.00 5 -8 8 0.05 0.00 5 -8 9 -0.22 0.00 5 -8 10 0.25 0.00 -5 7 16 -0.83 0.00 -5 7 15 0.64 0.00 -5 7 14 -0.40 0.00 -5 7 13 0.22 0.00 -5 7 12 -0.15 0.00 -5 7 11 0.17 0.00 -5 7 10 -0.21 0.00 -5 7 9 0.22 0.00 -5 7 8 -0.13 0.00 -5 7 7 -0.02 0.00 -5 7 6 0.18 0.00 -5 7 5 -0.28 0.00 -5 7 1 0.51 0.00 -5 7 0 -0.83 0.00 5 -7 1 1.07 0.00 5 -7 2 -1.19 0.00 5 -7 3 1.20 0.00 5 -7 4 -1.12 0.00 5 -7 5 0.98 0.00 5 -7 6 -0.79 0.00 5 -7 7 0.59 0.00 5 -7 8 -0.41 0.00 5 -7 9 0.29 0.00 5 -7 10 -0.24 0.00 5 -7 11 0.25 0.00 5 -7 12 -0.27 0.00 -5 6 18 -0.42 0.00 -5 6 17 0.56 0.00 -5 6 16 -0.59 0.00 -5 6 15 0.56 0.00 -5 6 14 -0.49 0.00 -5 6 13 0.44 0.00 -5 6 12 -0.47 0.00 -5 6 11 0.56 0.00 -5 6 10 -0.67 0.00 -5 6 9 0.74 0.00 -5 6 8 -0.70 0.00 -5 6 7 0.54 0.00 -5 6 6 -0.28 0.00 -5 6 5 0.00 0.00 -5 6 4 0.18 0.00 -5 6 3 -0.17 0.00 -5 6 2 -0.04 0.00 -5 6 1 0.37 0.00 -5 6 0 -0.69 0.00 5 -6 1 0.89 0.00 5 -6 2 -0.91 0.00 5 -6 3 0.79 0.00 5 -6 4 -0.62 0.00 5 -6 5 0.45 0.00 5 -6 6 -0.34 0.00 5 -6 7 0.30 0.00 5 -6 8 -0.32 0.00 5 -6 9 0.40 0.00 5 -6 10 -0.50 0.00 5 -6 11 0.60 0.00 5 -6 12 -0.67 0.00 5 -6 13 0.69 0.00 5 -6 14 -0.67 0.00 -5 5 19 -0.22 0.00 -5 5 18 0.01 0.00 -5 5 17 0.24 0.00 -5 5 16 -0.49 0.00 -5 5 15 0.72 0.00 -5 5 14 -0.94 0.00 -5 5 13 1.15 0.00 -5 5 12 -1.38 0.00 -5 5 11 1.63 0.00 -5 5 10 -1.87 0.00 -5 5 9 2.04 0.00 -5 5 8 -2.05 0.00 -5 5 7 1.84 0.00 -5 5 6 -1.44 0.00 -5 5 5 0.92 0.00 -5 5 4 -0.45 0.00 -5 5 3 0.15 0.00 -5 5 2 -0.06 0.00 -5 5 1 0.15 0.00 -5 5 0 -0.27 0.00 5 -5 1 0.33 0.00 5 -5 2 -0.28 0.00 5 -5 3 0.16 0.00 5 -5 4 -0.02 0.00 5 -5 5 -0.10 0.00 5 -5 6 0.17 0.00 5 -5 7 -0.18 0.00 5 -5 8 0.11 0.00 5 -5 9 0.04 0.00 5 -5 10 -0.25 0.00 5 -5 11 0.46 0.00 5 -5 12 -0.64 0.00 5 -5 13 0.76 0.00 5 -5 14 -0.84 0.00 5 -5 15 0.92 0.00 5 -5 16 -0.97 0.00 -5 4 19 -0.46 0.00 -5 4 18 0.21 0.00 -5 4 17 0.15 0.00 -5 4 16 -0.58 0.00 -5 4 15 1.04 0.00 -5 4 14 -1.52 0.00 -5 4 13 1.98 0.00 -5 4 12 -2.43 0.00 -5 4 11 2.86 0.00 -5 4 10 -3.22 0.00 -5 4 9 3.44 0.00 -5 4 8 -3.46 0.00 -5 4 7 3.23 0.00 -5 4 6 -2.77 0.00 -5 4 5 2.14 0.00 -5 4 4 -1.47 0.00 -5 4 3 0.85 0.00 -5 4 2 -0.35 0.00 -5 4 1 -0.04 0.00 -5 4 0 0.34 0.00 5 -4 1 -0.56 0.00 5 -4 2 0.70 0.00 5 -4 3 -0.76 0.00 5 -4 4 0.75 0.00 5 -4 5 -0.74 0.00 5 -4 6 0.75 0.00 5 -4 7 -0.75 0.00 5 -4 8 0.69 0.00 5 -4 9 -0.53 0.00 5 -4 10 0.28 0.00 5 -4 11 -0.03 0.00 5 -4 12 -0.16 0.00 5 -4 13 0.29 0.00 5 -4 14 -0.40 0.00 5 -4 15 0.57 0.00 5 -4 16 -0.78 0.00 5 -4 17 0.96 0.00 -5 3 20 0.44 0.00 -5 3 19 -0.37 0.00 -5 3 18 0.18 0.00 -5 3 17 0.13 0.00 -5 3 16 -0.53 0.00 -5 3 15 1.00 0.00 -5 3 14 -1.50 0.00 -5 3 13 2.01 0.00 -5 3 12 -2.51 0.00 -5 3 11 2.95 0.00 -5 3 10 -3.28 0.00 -5 3 9 3.45 0.00 -5 3 8 -3.45 0.00 -5 3 7 3.27 0.00 -5 3 6 -2.94 0.00 -5 3 5 2.45 0.00 -5 3 4 -1.82 0.00 -5 3 3 1.08 0.00 -5 3 2 -0.27 0.00 -5 3 1 -0.53 0.00 -5 3 0 1.21 0.00 5 -3 1 -1.66 0.00 5 -3 2 1.82 0.00 5 -3 3 -1.73 0.00 5 -3 4 1.51 0.00 5 -3 5 -1.32 0.00 5 -3 6 1.23 0.00 5 -3 7 -1.19 0.00 5 -3 8 1.12 0.00 5 -3 9 -0.92 0.00 5 -3 10 0.65 0.00 5 -3 11 -0.38 0.00 5 -3 12 0.22 0.00 5 -3 13 -0.17 0.00 5 -3 14 0.12 0.00 5 -3 15 0.00 0.00 5 -3 16 -0.21 0.00 5 -3 17 0.44 0.00 5 -3 18 -0.58 0.00 5 -3 19 0.58 0.00 -5 2 20 0.09 0.00 -5 2 19 -0.09 0.00 -5 2 18 0.03 0.00 -5 2 17 0.09 0.00 -5 2 16 -0.26 0.00 -5 2 15 0.50 0.00 -5 2 14 -0.79 0.00 -5 2 13 1.13 0.00 -5 2 12 -1.46 0.00 -5 2 11 1.74 0.00 -5 2 10 -1.90 0.00 -5 2 9 1.95 0.00 -5 2 8 -1.94 0.00 -5 2 7 1.88 0.00 -5 2 6 -1.76 0.00 -5 2 5 1.50 0.00 -5 2 4 -1.00 0.00 -5 2 3 0.25 0.00 -5 2 2 0.68 0.00 -5 2 1 -1.61 0.00 -5 2 0 2.32 0.00 5 -2 1 -2.64 0.00 5 -2 2 2.50 0.00 5 -2 3 -2.03 0.00 5 -2 4 1.44 0.00 5 -2 5 -0.95 0.00 5 -2 6 0.68 0.00 5 -2 7 -0.59 0.00 5 -2 8 0.55 0.00 5 -2 9 -0.47 0.00 5 -2 10 0.35 0.00 5 -2 11 -0.24 0.00 5 -2 12 0.22 0.00 5 -2 13 -0.27 0.00 5 -2 14 0.30 0.00 5 -2 15 -0.25 0.00 5 -2 16 0.11 0.00 5 -2 17 0.04 0.00 5 -2 18 -0.13 0.00 5 -2 19 0.13 0.00 5 -2 20 -0.08 0.00 -5 1 20 -0.13 0.00 -5 1 19 0.12 0.00 -5 1 18 -0.10 0.00 -5 1 17 0.04 0.00 -5 1 16 0.03 0.00 -5 1 15 -0.10 0.00 -5 1 14 0.11 0.00 -5 1 13 -0.05 0.00 -5 1 12 -0.03 0.00 -5 1 11 0.09 0.00 -5 1 10 -0.12 0.00 -5 1 9 0.16 0.00 -5 1 8 -0.26 0.00 -5 1 7 0.43 0.00 -5 1 6 -0.56 0.00 -5 1 5 0.49 0.00 -5 1 4 -0.07 0.00 -5 1 3 -0.68 0.00 -5 1 2 1.61 0.00 -5 1 1 -2.46 0.00 -5 1 0 2.96 0.00 5 -1 1 -2.95 0.00 5 -1 2 2.43 0.00 5 -1 3 -1.54 0.00 5 -1 4 0.56 0.00 5 -1 5 0.25 0.00 5 -1 6 -0.75 0.00 5 -1 7 0.92 0.00 5 -1 8 -0.86 0.00 5 -1 9 0.67 0.00 5 -1 10 -0.43 0.00 5 -1 11 0.16 0.00 5 -1 12 0.10 0.00 5 -1 13 -0.31 0.00 5 -1 14 0.42 0.00 5 -1 15 -0.39 0.00 5 -1 16 0.28 0.00 5 -1 17 -0.17 0.00 5 -1 18 0.11 0.00 5 -1 19 -0.11 0.00 5 -1 20 0.13 0.00 5 -1 21 -0.13 0.00 -5 0 20 0.02 0.00 -5 0 19 -0.01 0.00 -5 0 18 0.05 0.00 -5 0 17 -0.17 0.00 -5 0 16 0.37 0.00 -5 0 15 -0.61 0.00 -5 0 14 0.82 0.00 -5 0 13 -0.97 0.00 -5 0 12 1.08 0.00 -5 0 11 -1.16 0.00 -5 0 10 1.16 0.00 -5 0 9 -1.01 0.00 -5 0 8 0.68 0.00 -5 0 7 -0.22 0.00 -5 0 6 -0.15 0.00 -5 0 5 0.23 0.00 -5 0 4 0.10 0.00 -5 0 3 -0.78 0.00 -5 0 2 1.60 0.00 -5 0 1 -2.29 0.00 5 0 0 2.62 0.00 5 0 1 -2.47 0.00 5 0 2 1.88 0.00 5 0 3 -0.97 0.00 5 0 4 -0.03 0.00 5 0 5 0.91 0.00 5 0 6 -1.50 0.00 5 0 7 1.72 0.00 5 0 8 -1.59 0.00 5 0 9 1.23 0.00 5 0 10 -0.73 0.00 5 0 11 0.21 0.00 5 0 12 0.23 0.00 5 0 13 -0.54 0.00 5 0 14 0.67 0.00 5 0 15 -0.65 0.00 5 0 16 0.54 0.00 5 0 17 -0.41 0.00 5 0 18 0.31 0.00 5 0 19 -0.26 0.00 5 0 20 0.22 0.00 5 0 21 -0.19 0.00 -5 -1 20 0.25 0.00 -5 -1 19 -0.28 0.00 -5 -1 18 0.35 0.00 -5 -1 17 -0.50 0.00 -5 -1 16 0.73 0.00 -5 -1 15 -0.98 0.00 -5 -1 14 1.20 0.00 -5 -1 13 -1.36 0.00 -5 -1 12 1.46 0.00 -5 -1 11 -1.49 0.00 -5 -1 10 1.39 0.00 -5 -1 9 -1.08 0.00 -5 -1 8 0.57 0.00 -5 -1 7 0.03 0.00 -5 -1 6 -0.48 0.00 -5 -1 5 0.60 0.00 -5 -1 4 -0.31 0.00 -5 -1 3 -0.28 0.00 -5 -1 2 0.96 0.00 -5 -1 1 -1.51 0.00 5 1 0 1.80 0.00 5 1 1 -1.80 0.00 5 1 2 1.52 0.00 5 1 3 -1.01 0.00 5 1 4 0.38 0.00 5 1 5 0.25 0.00 5 1 6 -0.72 0.00 5 1 7 0.93 0.00 5 1 8 -0.85 0.00 5 1 9 0.55 0.00 5 1 10 -0.14 0.00 5 1 11 -0.25 0.00 5 1 12 0.56 0.00 5 1 13 -0.75 0.00 5 1 14 0.80 0.00 5 1 15 -0.75 0.00 5 1 16 0.64 0.00 5 1 17 -0.50 0.00 5 1 18 0.38 0.00 5 1 19 -0.27 0.00 5 1 20 0.19 0.00 5 1 21 -0.13 0.00 5 1 22 0.09 0.00 -5 -2 19 -0.30 0.00 -5 -2 18 0.40 0.00 -5 -2 17 -0.57 0.00 -5 -2 16 0.78 0.00 -5 -2 15 -0.96 0.00 -5 -2 14 1.06 0.00 -5 -2 13 -1.06 0.00 -5 -2 12 0.96 0.00 -5 -2 11 -0.78 0.00 -5 -2 10 0.49 0.00 -5 -2 9 -0.03 0.00 -5 -2 8 -0.56 0.00 -5 -2 7 1.15 0.00 -5 -2 6 -1.55 0.00 -5 -2 5 1.62 0.00 -5 -2 4 -1.35 0.00 -5 -2 3 0.86 0.00 -5 -2 2 -0.29 0.00 -5 -2 1 -0.24 0.00 5 2 0 0.70 0.00 5 2 1 -1.07 0.00 5 2 2 1.32 0.00 5 2 3 -1.40 0.00 5 2 4 1.31 0.00 5 2 5 -1.10 0.00 5 2 6 0.88 0.00 5 2 7 -0.75 0.00 5 2 8 0.74 0.00 5 2 9 -0.80 0.00 5 2 10 0.88 0.00 5 2 11 -0.91 0.00 5 2 12 0.90 0.00 5 2 13 -0.85 0.00 5 2 14 0.78 0.00 5 2 15 -0.68 0.00 5 2 16 0.56 0.00 5 2 17 -0.42 0.00 5 2 18 0.27 0.00 5 2 19 -0.12 0.00 5 2 20 -0.02 0.00 5 2 21 0.14 0.00 5 2 22 -0.22 0.00 -5 -3 19 -0.17 0.00 -5 -3 18 0.25 0.00 -5 -3 17 -0.40 0.00 -5 -3 16 0.55 0.00 -5 -3 15 -0.63 0.00 -5 -3 14 0.58 0.00 -5 -3 13 -0.38 0.00 -5 -3 12 0.06 0.00 -5 -3 11 0.33 0.00 -5 -3 10 -0.79 0.00 -5 -3 9 1.32 0.00 -5 -3 8 -1.91 0.00 -5 -3 7 2.47 0.00 -5 -3 6 -2.87 0.00 -5 -3 5 3.03 0.00 -5 -3 4 -2.94 0.00 -5 -3 3 2.66 0.00 -5 -3 2 -2.23 0.00 -5 -3 1 1.69 0.00 5 3 0 -1.04 0.00 5 3 1 0.29 0.00 5 3 2 0.45 0.00 5 3 3 -1.07 0.00 5 3 4 1.50 0.00 5 3 5 -1.74 0.00 5 3 6 1.86 0.00 5 3 7 -1.92 0.00 5 3 8 1.93 0.00 5 3 9 -1.86 0.00 5 3 10 1.68 0.00 5 3 11 -1.44 0.00 5 3 12 1.20 0.00 5 3 13 -1.02 0.00 5 3 14 0.90 0.00 5 3 15 -0.81 0.00 5 3 16 0.71 0.00 5 3 17 -0.57 0.00 5 3 18 0.39 0.00 5 3 19 -0.19 0.00 5 3 20 -0.03 0.00 5 3 21 0.25 0.00 5 3 22 -0.44 0.00 5 3 23 0.55 0.00 -5 -4 18 0.28 0.00 -5 -4 17 -0.42 0.00 -5 -4 16 0.53 0.00 -5 -4 15 -0.52 0.00 -5 -4 14 0.34 0.00 -5 -4 13 0.01 0.00 -5 -4 12 -0.46 0.00 -5 -4 11 0.94 0.00 -5 -4 10 -1.41 0.00 -5 -4 9 1.88 0.00 -5 -4 8 -2.36 0.00 -5 -4 7 2.85 0.00 -5 -4 6 -3.29 0.00 -5 -4 5 3.61 0.00 -5 -4 4 -3.76 0.00 -5 -4 3 3.72 0.00 -5 -4 2 -3.47 0.00 -5 -4 1 3.01 0.00 5 4 0 -2.36 0.00 5 4 1 1.59 0.00 5 4 2 -0.81 0.00 5 4 3 0.13 0.00 5 4 4 0.41 0.00 5 4 5 -0.82 0.00 5 4 6 1.15 0.00 5 4 7 -1.41 0.00 5 4 8 1.58 0.00 5 4 9 -1.61 0.00 5 4 10 1.51 0.00 5 4 11 -1.32 0.00 5 4 12 1.13 0.00 5 4 13 -1.01 0.00 5 4 14 0.96 0.00 5 4 15 -0.95 0.00 5 4 16 0.93 0.00 5 4 17 -0.86 0.00 5 4 18 0.74 0.00 5 4 19 -0.57 0.00 5 4 20 0.35 0.00 5 4 21 -0.08 0.00 5 4 22 -0.18 0.00 5 4 23 0.38 0.00 -5 -5 17 -0.52 0.00 -5 -5 16 0.63 0.00 -5 -5 15 -0.61 0.00 -5 -5 14 0.41 0.00 -5 -5 13 -0.05 0.00 -5 -5 12 -0.39 0.00 -5 -5 11 0.80 0.00 -5 -5 10 -1.14 0.00 -5 -5 9 1.45 0.00 -5 -5 8 -1.76 0.00 -5 -5 7 2.12 0.00 -5 -5 6 -2.50 0.00 -5 -5 5 2.79 0.00 -5 -5 4 -2.93 0.00 -5 -5 3 2.85 0.00 -5 -5 2 -2.58 0.00 -5 -5 1 2.17 0.00 5 5 0 -1.70 0.00 5 5 1 1.27 0.00 5 5 2 -0.96 0.00 5 5 3 0.79 0.00 5 5 4 -0.72 0.00 5 5 5 0.68 0.00 5 5 6 -0.60 0.00 5 5 7 0.45 0.00 5 5 8 -0.26 0.00 5 5 9 0.10 0.00 5 5 10 0.01 0.00 5 5 11 -0.07 0.00 5 5 12 0.12 0.00 5 5 13 -0.18 0.00 5 5 14 0.27 0.00 5 5 15 -0.37 0.00 5 5 16 0.49 0.00 5 5 17 -0.60 0.00 5 5 18 0.68 0.00 5 5 19 -0.70 0.00 5 5 20 0.64 0.00 5 5 21 -0.47 0.00 5 5 22 0.26 0.00 5 5 23 -0.06 0.00 -5 -6 16 0.38 0.00 -5 -6 15 -0.40 0.00 -5 -6 14 0.28 0.00 -5 -6 13 -0.06 0.00 -5 -6 12 -0.21 0.00 -5 -6 11 0.42 0.00 -5 -6 10 -0.56 0.00 -5 -6 9 0.68 0.00 -5 -6 8 -0.84 0.00 -5 -6 7 1.07 0.00 -5 -6 6 -1.30 0.00 -5 -6 5 1.41 0.00 -5 -6 4 -1.31 0.00 -5 -6 3 0.97 0.00 -5 -6 2 -0.48 0.00 -5 -6 1 -0.01 0.00 5 6 0 0.36 0.00 5 6 1 -0.47 0.00 5 6 2 0.34 0.00 5 6 3 0.01 0.00 5 6 4 -0.48 0.00 5 6 5 0.96 0.00 5 6 6 -1.37 0.00 5 6 7 1.65 0.00 5 6 8 -1.79 0.00 5 6 9 1.81 0.00 5 6 10 -1.74 0.00 5 6 11 1.63 0.00 5 6 12 -1.49 0.00 5 6 13 1.34 0.00 5 6 14 -1.18 0.00 5 6 15 0.97 0.00 5 6 16 -0.70 0.00 5 6 17 0.38 0.00 5 6 18 -0.05 0.00 5 6 19 -0.23 0.00 5 6 20 0.39 0.00 5 6 21 -0.43 0.00 5 6 22 0.36 0.00 -5 -7 15 -0.02 0.00 -5 -7 14 -0.02 0.00 -5 -7 13 0.11 0.00 -5 -7 12 -0.18 0.00 -5 -7 11 0.18 0.00 -5 -7 10 -0.12 0.00 -5 -7 9 0.07 0.00 -5 -7 8 -0.10 0.00 -5 -7 7 0.22 0.00 -5 -7 6 -0.33 0.00 -5 -7 5 0.29 0.00 -5 -7 4 -0.01 0.00 -5 -7 3 -0.50 0.00 -5 -7 2 1.11 0.00 -5 -7 1 -1.65 0.00 5 7 0 1.99 0.00 5 7 1 -2.05 0.00 5 7 2 1.85 0.00 5 7 3 -1.44 0.00 5 7 4 0.87 0.00 5 7 5 -0.21 0.00 5 7 6 -0.49 0.00 5 7 7 1.16 0.00 5 7 8 -1.72 0.00 5 7 9 2.14 0.00 5 7 10 -2.39 0.00 5 7 11 2.52 0.00 5 7 12 -2.55 0.00 5 7 13 2.51 0.00 5 7 14 -2.40 0.00 5 7 15 2.19 0.00 5 7 16 -1.86 0.00 5 7 17 1.42 0.00 5 7 18 -0.96 0.00 5 7 19 0.53 0.00 5 7 20 -0.22 0.00 5 7 21 0.03 0.00 5 7 22 0.07 0.00 -5 -8 14 -0.01 0.00 -5 -8 13 0.05 0.00 -5 -8 12 -0.06 0.00 -5 -8 11 0.00 0.00 -5 -8 10 0.13 0.00 -5 -8 9 -0.27 0.00 -5 -8 8 0.35 0.00 -5 -8 7 -0.36 0.00 -5 -8 6 0.36 0.00 -5 -8 5 -0.46 0.00 -5 -8 4 0.75 0.00 -5 -8 3 -1.20 0.00 -5 -8 2 1.73 0.00 -5 -8 1 -2.19 0.00 5 8 0 2.50 0.00 5 8 1 -2.63 0.00 5 8 2 2.59 0.00 5 8 3 -2.37 0.00 5 8 4 1.98 0.00 5 8 5 -1.42 0.00 5 8 6 0.72 0.00 5 8 7 0.04 0.00 5 8 8 -0.78 0.00 5 8 9 1.40 0.00 5 8 10 -1.88 0.00 5 8 11 2.21 0.00 5 8 12 -2.43 0.00 5 8 13 2.55 0.00 5 8 14 -2.56 0.00 5 8 15 2.46 0.00 5 8 16 -2.22 0.00 5 8 17 1.87 0.00 5 8 18 -1.48 0.00 5 8 19 1.11 0.00 5 8 20 -0.80 0.00 5 8 21 0.55 0.00 -5 -9 12 0.14 0.00 -5 -9 11 -0.12 0.00 -5 -9 10 0.15 0.00 -5 -9 9 -0.23 0.00 -5 -9 8 0.32 0.00 -5 -9 7 -0.39 0.00 -5 -9 6 0.46 0.00 -5 -9 5 -0.57 0.00 -5 -9 4 0.77 0.00 -5 -9 3 -1.06 0.00 -5 -9 2 1.40 0.00 -5 -9 1 -1.72 0.00 5 9 0 1.99 0.00 5 9 1 -2.17 0.00 5 9 2 2.24 0.00 5 9 3 -2.20 0.00 5 9 4 2.00 0.00 5 9 5 -1.65 0.00 5 9 6 1.16 0.00 5 9 7 -0.61 0.00 5 9 8 0.06 0.00 5 9 9 0.41 0.00 5 9 10 -0.78 0.00 5 9 11 1.06 0.00 5 9 12 -1.27 0.00 5 9 13 1.43 0.00 5 9 14 -1.55 0.00 5 9 15 1.61 0.00 5 9 16 -1.61 0.00 5 9 17 1.54 0.00 5 9 18 -1.41 0.00 5 9 19 1.24 0.00 5 9 20 -1.04 0.00 5 9 21 0.82 0.00 -5 -10 10 -0.13 0.00 -5 -10 9 0.23 0.00 -5 -10 8 -0.28 0.00 -5 -10 7 0.31 0.00 -5 -10 6 -0.31 0.00 -5 -10 5 0.29 0.00 -5 -10 4 -0.23 0.00 -5 -10 3 0.10 0.00 -5 -10 2 0.09 0.00 -5 -10 1 -0.32 0.00 5 10 0 0.56 0.00 5 10 1 -0.77 0.00 5 10 2 0.94 0.00 5 10 3 -1.06 0.00 5 10 4 1.12 0.00 5 10 5 -1.12 0.00 5 10 6 1.05 0.00 5 10 7 -0.94 0.00 5 10 8 0.80 0.00 5 10 9 -0.65 0.00 5 10 10 0.54 0.00 5 10 11 -0.45 0.00 5 10 12 0.38 0.00 5 10 13 -0.28 0.00 5 10 14 0.13 0.00 5 10 15 0.08 0.00 5 10 16 -0.33 0.00 5 10 17 0.58 0.00 5 10 18 -0.77 0.00 5 10 19 0.87 0.00 -5 -11 8 -0.83 0.00 -5 -11 7 1.01 0.00 -5 -11 6 -1.19 0.00 -5 -11 5 1.34 0.00 -5 -11 4 -1.44 0.00 -5 -11 3 1.45 0.00 -5 -11 2 -1.36 0.00 -5 -11 1 1.19 0.00 5 11 0 -0.98 0.00 5 11 1 0.75 0.00 5 11 2 -0.51 0.00 5 11 3 0.23 0.00 5 11 4 0.11 0.00 5 11 5 -0.48 0.00 5 11 6 0.83 0.00 5 11 7 -1.10 0.00 5 11 8 1.27 0.00 5 11 9 -1.34 0.00 5 11 10 1.37 0.00 5 11 11 -1.40 0.00 5 11 12 1.42 0.00 5 11 13 -1.42 0.00 5 11 14 1.34 0.00 5 11 15 -1.14 0.00 5 11 16 0.84 0.00 5 11 17 -0.47 0.00 5 11 18 0.10 0.00 -5 -12 5 1.37 0.00 -5 -12 4 -1.59 0.00 -5 -12 3 1.71 0.00 -5 -12 2 -1.71 0.00 -5 -12 1 1.63 0.00 5 12 0 -1.50 0.00 5 12 1 1.34 0.00 5 12 2 -1.13 0.00 5 12 3 0.82 0.00 5 12 4 -0.42 0.00 5 12 5 -0.06 0.00 5 12 6 0.50 0.00 5 12 7 -0.84 0.00 5 12 8 1.02 0.00 5 12 9 -1.07 0.00 5 12 10 1.07 0.00 5 12 11 -1.07 0.00 5 12 12 1.11 0.00 5 12 13 -1.16 0.00 5 12 14 1.18 0.00 5 12 15 -1.14 0.00 -5 -13 1 1.01 0.00 5 13 0 -0.99 0.00 5 13 1 0.94 0.00 5 13 2 -0.83 0.00 5 13 3 0.64 0.00 5 13 4 -0.36 0.00 5 13 5 0.07 0.00 5 13 6 0.18 0.00 5 13 7 -0.31 0.00 5 13 8 0.33 0.00 5 13 9 -0.27 0.00 5 13 10 0.20 0.00 5 13 11 -0.15 0.00 5 13 12 0.14 0.00 6 -8 1 -0.31 0.00 6 -8 2 0.41 0.00 6 -8 3 -0.46 0.00 6 -8 4 0.48 0.00 6 -8 5 -0.50 0.00 6 -8 6 0.58 0.00 6 -8 7 -0.69 0.00 -6 7 13 -0.02 0.00 -6 7 12 0.01 0.00 -6 7 11 0.08 0.00 -6 7 10 -0.20 0.00 -6 7 9 0.26 0.00 -6 7 8 -0.22 0.00 -6 7 7 0.08 0.00 -6 7 6 0.07 0.00 -6 7 1 0.53 0.00 -6 7 0 -0.67 0.00 6 -7 1 0.71 0.00 6 -7 2 -0.68 0.00 6 -7 3 0.57 0.00 6 -7 4 -0.39 0.00 6 -7 5 0.16 0.00 6 -7 6 0.12 0.00 6 -7 7 -0.40 0.00 6 -7 8 0.61 0.00 6 -7 9 -0.71 0.00 6 -7 10 0.68 0.00 -6 6 16 0.13 0.00 -6 6 15 -0.25 0.00 -6 6 14 0.36 0.00 -6 6 13 -0.42 0.00 -6 6 12 0.38 0.00 -6 6 11 -0.26 0.00 -6 6 10 0.10 0.00 -6 6 9 0.03 0.00 -6 6 8 -0.07 0.00 -6 6 7 0.03 0.00 -6 6 6 0.07 0.00 -6 6 5 -0.14 0.00 -6 6 4 0.11 0.00 -6 6 3 0.04 0.00 -6 6 2 -0.33 0.00 -6 6 1 0.70 0.00 -6 6 0 -1.06 0.00 6 -6 1 1.32 0.00 6 -6 2 -1.42 0.00 6 -6 3 1.35 0.00 6 -6 4 -1.14 0.00 6 -6 5 0.83 0.00 6 -6 6 -0.50 0.00 6 -6 7 0.20 0.00 6 -6 8 0.03 0.00 6 -6 9 -0.15 0.00 6 -6 10 0.18 0.00 6 -6 11 -0.15 0.00 6 -6 12 0.11 0.00 6 -6 13 -0.09 0.00 -6 5 17 -0.36 0.00 -6 5 16 0.47 0.00 -6 5 15 -0.56 0.00 -6 5 14 0.59 0.00 -6 5 13 -0.56 0.00 -6 5 12 0.43 0.00 -6 5 11 -0.23 0.00 -6 5 10 0.00 0.00 -6 5 9 0.22 0.00 -6 5 8 -0.37 0.00 -6 5 7 0.40 0.00 -6 5 6 -0.32 0.00 -6 5 5 0.16 0.00 -6 5 4 -0.02 0.00 -6 5 3 -0.02 0.00 -6 5 2 -0.10 0.00 -6 5 1 0.38 0.00 -6 5 0 -0.75 0.00 6 -5 1 1.08 0.00 6 -5 2 -1.31 0.00 6 -5 3 1.37 0.00 6 -5 4 -1.29 0.00 6 -5 5 1.11 0.00 6 -5 6 -0.87 0.00 6 -5 7 0.64 0.00 6 -5 8 -0.47 0.00 6 -5 9 0.39 0.00 6 -5 10 -0.41 0.00 6 -5 11 0.46 0.00 6 -5 12 -0.49 0.00 6 -5 13 0.45 0.00 6 -5 14 -0.36 0.00 6 -5 15 0.27 0.00 -6 4 18 0.08 0.00 -6 4 17 -0.14 0.00 -6 4 16 0.19 0.00 -6 4 15 -0.17 0.00 -6 4 14 0.07 0.00 -6 4 13 0.12 0.00 -6 4 12 -0.40 0.00 -6 4 11 0.73 0.00 -6 4 10 -1.05 0.00 -6 4 9 1.32 0.00 -6 4 8 -1.47 0.00 -6 4 7 1.44 0.00 -6 4 6 -1.24 0.00 -6 4 5 0.89 0.00 -6 4 4 -0.49 0.00 -6 4 3 0.15 0.00 -6 4 2 0.05 0.00 -6 4 1 -0.08 0.00 -6 4 0 -0.03 0.00 6 -4 1 0.22 0.00 6 -4 2 -0.42 0.00 6 -4 3 0.60 0.00 6 -4 4 -0.71 0.00 6 -4 5 0.73 0.00 6 -4 6 -0.65 0.00 6 -4 7 0.52 0.00 6 -4 8 -0.39 0.00 6 -4 9 0.36 0.00 6 -4 10 -0.45 0.00 6 -4 11 0.59 0.00 6 -4 12 -0.69 0.00 6 -4 13 0.69 0.00 6 -4 14 -0.61 0.00 6 -4 15 0.52 0.00 6 -4 16 -0.48 0.00 -6 3 18 -0.28 0.00 -6 3 17 0.37 0.00 -6 3 16 -0.49 0.00 -6 3 15 0.66 0.00 -6 3 14 -0.90 0.00 -6 3 13 1.24 0.00 -6 3 12 -1.64 0.00 -6 3 11 2.07 0.00 -6 3 10 -2.46 0.00 -6 3 9 2.71 0.00 -6 3 8 -2.78 0.00 -6 3 7 2.63 0.00 -6 3 6 -2.29 0.00 -6 3 5 1.79 0.00 -6 3 4 -1.21 0.00 -6 3 3 0.61 0.00 -6 3 2 -0.04 0.00 -6 3 1 -0.44 0.00 -6 3 0 0.81 0.00 6 -3 1 -1.04 0.00 6 -3 2 1.08 0.00 6 -3 3 -0.96 0.00 6 -3 4 0.75 0.00 6 -3 5 -0.55 0.00 6 -3 6 0.43 0.00 6 -3 7 -0.41 0.00 6 -3 8 0.39 0.00 6 -3 9 -0.29 0.00 6 -3 10 0.08 0.00 6 -3 11 0.17 0.00 6 -3 12 -0.36 0.00 6 -3 13 0.40 0.00 6 -3 14 -0.34 0.00 6 -3 15 0.27 0.00 6 -3 16 -0.29 0.00 6 -3 17 0.39 0.00 6 -3 18 -0.49 0.00 -6 2 19 0.13 0.00 -6 2 18 -0.31 0.00 -6 2 17 0.55 0.00 -6 2 16 -0.82 0.00 -6 2 15 1.13 0.00 -6 2 14 -1.49 0.00 -6 2 13 1.90 0.00 -6 2 12 -2.34 0.00 -6 2 11 2.76 0.00 -6 2 10 -3.08 0.00 -6 2 9 3.24 0.00 -6 2 8 -3.22 0.00 -6 2 7 3.02 0.00 -6 2 6 -2.70 0.00 -6 2 5 2.26 0.00 -6 2 4 -1.72 0.00 -6 2 3 1.06 0.00 -6 2 2 -0.28 0.00 -6 2 1 -0.57 0.00 -6 2 0 1.38 0.00 6 -2 1 -2.02 0.00 6 -2 2 2.37 0.00 6 -2 3 -2.40 0.00 6 -2 4 2.20 0.00 6 -2 5 -1.90 0.00 6 -2 6 1.64 0.00 6 -2 7 -1.44 0.00 6 -2 8 1.26 0.00 6 -2 9 -1.01 0.00 6 -2 10 0.68 0.00 6 -2 11 -0.33 0.00 6 -2 12 0.09 0.00 6 -2 13 0.00 0.00 6 -2 14 0.04 0.00 6 -2 15 -0.09 0.00 6 -2 16 0.06 0.00 6 -2 17 0.06 0.00 6 -2 18 -0.18 0.00 6 -2 19 0.24 0.00 -6 1 19 -0.04 0.00 -6 1 18 -0.10 0.00 -6 1 17 0.31 0.00 -6 1 16 -0.59 0.00 -6 1 15 0.91 0.00 -6 1 14 -1.28 0.00 -6 1 13 1.67 0.00 -6 1 12 -2.06 0.00 -6 1 11 2.38 0.00 -6 1 10 -2.56 0.00 -6 1 9 2.58 0.00 -6 1 8 -2.49 0.00 -6 1 7 2.36 0.00 -6 1 6 -2.21 0.00 -6 1 5 2.01 0.00 -6 1 4 -1.70 0.00 -6 1 3 1.18 0.00 -6 1 2 -0.43 0.00 -6 1 1 -0.46 0.00 -6 1 0 1.34 0.00 6 -1 1 -2.03 0.00 6 -1 2 2.42 0.00 6 -1 3 -2.45 0.00 6 -1 4 2.21 0.00 6 -1 5 -1.85 0.00 6 -1 6 1.53 0.00 6 -1 7 -1.31 0.00 6 -1 8 1.17 0.00 6 -1 9 -1.03 0.00 6 -1 10 0.86 0.00 6 -1 11 -0.66 0.00 6 -1 12 0.49 0.00 6 -1 13 -0.39 0.00 6 -1 14 0.34 0.00 6 -1 15 -0.28 0.00 6 -1 16 0.17 0.00 6 -1 17 -0.04 0.00 6 -1 18 -0.07 0.00 6 -1 19 0.10 0.00 6 -1 20 -0.07 0.00 -6 0 19 -0.08 0.00 -6 0 18 0.02 0.00 -6 0 17 0.07 0.00 -6 0 16 -0.18 0.00 -6 0 15 0.31 0.00 -6 0 14 -0.49 0.00 -6 0 13 0.72 0.00 -6 0 12 -0.96 0.00 -6 0 11 1.12 0.00 -6 0 10 -1.18 0.00 -6 0 9 1.16 0.00 -6 0 8 -1.13 0.00 -6 0 7 1.18 0.00 -6 0 6 -1.29 0.00 -6 0 5 1.38 0.00 -6 0 4 -1.31 0.00 -6 0 3 1.00 0.00 -6 0 2 -0.45 0.00 -6 0 1 -0.20 0.00 6 0 0 0.82 0.00 6 0 1 -1.24 0.00 6 0 2 1.39 0.00 6 0 3 -1.25 0.00 6 0 4 0.91 0.00 6 0 5 -0.50 0.00 6 0 6 0.17 0.00 6 0 7 -0.04 0.00 6 0 8 0.10 0.00 6 0 9 -0.30 0.00 6 0 10 0.54 0.00 6 0 11 -0.74 0.00 6 0 12 0.86 0.00 6 0 13 -0.89 0.00 6 0 14 0.82 0.00 6 0 15 -0.65 0.00 6 0 16 0.42 0.00 6 0 17 -0.18 0.00 6 0 18 0.01 0.00 6 0 19 0.07 0.00 6 0 20 -0.07 0.00 -6 -1 19 -0.16 0.00 -6 -1 18 0.15 0.00 -6 -1 17 -0.19 0.00 -6 -1 16 0.30 0.00 -6 -1 15 -0.44 0.00 -6 -1 14 0.53 0.00 -6 -1 13 -0.55 0.00 -6 -1 12 0.52 0.00 -6 -1 11 -0.48 0.00 -6 -1 10 0.47 0.00 -6 -1 9 -0.43 0.00 -6 -1 8 0.29 0.00 -6 -1 7 -0.02 0.00 -6 -1 6 -0.31 0.00 -6 -1 5 0.58 0.00 -6 -1 4 -0.65 0.00 -6 -1 3 0.51 0.00 -6 -1 2 -0.21 0.00 -6 -1 1 -0.10 0.00 6 1 0 0.33 0.00 6 1 1 -0.40 0.00 6 1 2 0.30 0.00 6 1 3 -0.05 0.00 6 1 4 -0.33 0.00 6 1 5 0.73 0.00 6 1 6 -1.03 0.00 6 1 7 1.11 0.00 6 1 8 -0.91 0.00 6 1 9 0.49 0.00 6 1 10 0.04 0.00 6 1 11 -0.54 0.00 6 1 12 0.91 0.00 6 1 13 -1.13 0.00 6 1 14 1.17 0.00 6 1 15 -1.08 0.00 6 1 16 0.89 0.00 6 1 17 -0.66 0.00 6 1 18 0.45 0.00 6 1 19 -0.29 0.00 6 1 20 0.18 0.00 6 1 21 -0.11 0.00 -6 -2 18 0.39 0.00 -6 -2 17 -0.54 0.00 -6 -2 16 0.80 0.00 -6 -2 15 -1.12 0.00 -6 -2 14 1.38 0.00 -6 -2 13 -1.55 0.00 -6 -2 12 1.61 0.00 -6 -2 11 -1.60 0.00 -6 -2 10 1.53 0.00 -6 -2 9 -1.37 0.00 -6 -2 8 1.11 0.00 -6 -2 7 -0.76 0.00 -6 -2 6 0.43 0.00 -6 -2 5 -0.22 0.00 -6 -2 4 0.19 0.00 -6 -2 3 -0.29 0.00 -6 -2 2 0.40 0.00 -6 -2 1 -0.41 0.00 6 2 0 0.30 0.00 6 2 1 -0.11 0.00 6 2 2 -0.12 0.00 6 2 3 0.38 0.00 6 2 4 -0.67 0.00 6 2 5 0.98 0.00 6 2 6 -1.22 0.00 6 2 7 1.28 0.00 6 2 8 -1.10 0.00 6 2 9 0.73 0.00 6 2 10 -0.26 0.00 6 2 11 -0.18 0.00 6 2 12 0.52 0.00 6 2 13 -0.75 0.00 6 2 14 0.89 0.00 6 2 15 -0.96 0.00 6 2 16 0.96 0.00 6 2 17 -0.90 0.00 6 2 18 0.79 0.00 6 2 19 -0.66 0.00 6 2 20 0.52 0.00 6 2 21 -0.38 0.00 -6 -3 18 0.33 0.00 -6 -3 17 -0.54 0.00 -6 -3 16 0.87 0.00 -6 -3 15 -1.23 0.00 -6 -3 14 1.54 0.00 -6 -3 13 -1.71 0.00 -6 -3 12 1.72 0.00 -6 -3 11 -1.60 0.00 -6 -3 10 1.39 0.00 -6 -3 9 -1.10 0.00 -6 -3 8 0.77 0.00 -6 -3 7 -0.46 0.00 -6 -3 6 0.28 0.00 -6 -3 5 -0.27 0.00 -6 -3 4 0.42 0.00 -6 -3 3 -0.61 0.00 -6 -3 2 0.72 0.00 -6 -3 1 -0.67 0.00 6 3 0 0.51 0.00 6 3 1 -0.33 0.00 6 3 2 0.18 0.00 6 3 3 -0.05 0.00 6 3 4 -0.09 0.00 6 3 5 0.26 0.00 6 3 6 -0.42 0.00 6 3 7 0.48 0.00 6 3 8 -0.40 0.00 6 3 9 0.21 0.00 6 3 10 0.00 0.00 6 3 11 -0.16 0.00 6 3 12 0.25 0.00 6 3 13 -0.32 0.00 6 3 14 0.39 0.00 6 3 15 -0.47 0.00 6 3 16 0.53 0.00 6 3 17 -0.56 0.00 6 3 18 0.53 0.00 6 3 19 -0.46 0.00 6 3 20 0.37 0.00 6 3 21 -0.26 0.00 6 3 22 0.13 0.00 -6 -4 17 -0.16 0.00 -6 -4 16 0.42 0.00 -6 -4 15 -0.72 0.00 -6 -4 14 0.95 0.00 -6 -4 13 -1.04 0.00 -6 -4 12 0.96 0.00 -6 -4 11 -0.72 0.00 -6 -4 10 0.37 0.00 -6 -4 9 0.02 0.00 -6 -4 8 -0.41 0.00 -6 -4 7 0.71 0.00 -6 -4 6 -0.85 0.00 -6 -4 5 0.80 0.00 -6 -4 4 -0.59 0.00 -6 -4 3 0.30 0.00 -6 -4 2 -0.05 0.00 -6 -4 1 -0.14 0.00 6 4 0 0.27 0.00 6 4 1 -0.41 0.00 6 4 2 0.57 0.00 6 4 3 -0.72 0.00 6 4 4 0.80 0.00 6 4 5 -0.79 0.00 6 4 6 0.74 0.00 6 4 7 -0.72 0.00 6 4 8 0.75 0.00 6 4 9 -0.79 0.00 6 4 10 0.78 0.00 6 4 11 -0.70 0.00 6 4 12 0.59 0.00 6 4 13 -0.49 0.00 6 4 14 0.43 0.00 6 4 15 -0.40 0.00 6 4 16 0.36 0.00 6 4 17 -0.27 0.00 6 4 18 0.16 0.00 6 4 19 -0.04 0.00 6 4 20 -0.06 0.00 6 4 21 0.15 0.00 6 4 22 -0.24 0.00 -6 -5 16 0.16 0.00 -6 -5 15 -0.28 0.00 -6 -5 14 0.33 0.00 -6 -5 13 -0.26 0.00 -6 -5 12 0.04 0.00 -6 -5 11 0.27 0.00 -6 -5 10 -0.64 0.00 -6 -5 9 1.03 0.00 -6 -5 8 -1.41 0.00 -6 -5 7 1.76 0.00 -6 -5 6 -2.01 0.00 -6 -5 5 2.10 0.00 -6 -5 4 -2.01 0.00 -6 -5 3 1.74 0.00 -6 -5 2 -1.36 0.00 -6 -5 1 0.93 0.00 6 5 0 -0.48 0.00 6 5 1 0.05 0.00 6 5 2 0.35 0.00 6 5 3 -0.67 0.00 6 5 4 0.89 0.00 6 5 5 -1.02 0.00 6 5 6 1.11 0.00 6 5 7 -1.20 0.00 6 5 8 1.29 0.00 6 5 9 -1.33 0.00 6 5 10 1.29 0.00 6 5 11 -1.17 0.00 6 5 12 1.02 0.00 6 5 13 -0.87 0.00 6 5 14 0.76 0.00 6 5 15 -0.65 0.00 6 5 16 0.52 0.00 6 5 17 -0.35 0.00 6 5 18 0.17 0.00 6 5 19 -0.01 0.00 6 5 20 -0.12 0.00 6 5 21 0.24 0.00 6 5 22 -0.33 0.00 -6 -6 15 -0.36 0.00 -6 -6 14 0.22 0.00 -6 -6 13 0.04 0.00 -6 -6 12 -0.40 0.00 -6 -6 11 0.77 0.00 -6 -6 10 -1.11 0.00 -6 -6 9 1.42 0.00 -6 -6 8 -1.73 0.00 -6 -6 7 2.06 0.00 -6 -6 6 -2.39 0.00 -6 -6 5 2.62 0.00 -6 -6 4 -2.65 0.00 -6 -6 3 2.43 0.00 -6 -6 2 -2.02 0.00 -6 -6 1 1.51 0.00 6 6 0 -1.03 0.00 6 6 1 0.63 0.00 6 6 2 -0.33 0.00 6 6 3 0.13 0.00 6 6 4 0.03 0.00 6 6 5 -0.16 0.00 6 6 6 0.31 0.00 6 6 7 -0.48 0.00 6 6 8 0.65 0.00 6 6 9 -0.77 0.00 6 6 10 0.83 0.00 6 6 11 -0.81 0.00 6 6 12 0.74 0.00 6 6 13 -0.65 0.00 6 6 14 0.54 0.00 6 6 15 -0.43 0.00 6 6 16 0.31 0.00 6 6 17 -0.22 0.00 6 6 18 0.17 0.00 6 6 19 -0.14 0.00 6 6 20 0.10 0.00 6 6 21 -0.04 0.00 6 6 22 -0.06 0.00 -6 -7 14 0.34 0.00 -6 -7 13 -0.04 0.00 -6 -7 12 -0.33 0.00 -6 -7 11 0.69 0.00 -6 -7 10 -0.96 0.00 -6 -7 9 1.18 0.00 -6 -7 8 -1.41 0.00 -6 -7 7 1.71 0.00 -6 -7 6 -2.04 0.00 -6 -7 5 2.29 0.00 -6 -7 4 -2.31 0.00 -6 -7 3 2.07 0.00 -6 -7 2 -1.64 0.00 -6 -7 1 1.18 0.00 6 7 0 -0.82 0.00 6 7 1 0.63 0.00 6 7 2 -0.57 0.00 6 7 3 0.57 0.00 6 7 4 -0.56 0.00 6 7 5 0.52 0.00 6 7 6 -0.46 0.00 6 7 7 0.39 0.00 6 7 8 -0.33 0.00 6 7 9 0.28 0.00 6 7 10 -0.22 0.00 6 7 11 0.18 0.00 6 7 12 -0.17 0.00 6 7 13 0.21 0.00 6 7 14 -0.29 0.00 6 7 15 0.38 0.00 6 7 16 -0.43 0.00 6 7 17 0.39 0.00 6 7 18 -0.24 0.00 6 7 19 0.05 0.00 6 7 20 0.11 0.00 6 7 21 -0.17 0.00 -6 -8 13 -0.17 0.00 -6 -8 12 -0.04 0.00 -6 -8 11 0.22 0.00 -6 -8 10 -0.33 0.00 -6 -8 9 0.41 0.00 -6 -8 8 -0.56 0.00 -6 -8 7 0.81 0.00 -6 -8 6 -1.11 0.00 -6 -8 5 1.33 0.00 -6 -8 4 -1.33 0.00 -6 -8 3 1.07 0.00 -6 -8 2 -0.64 0.00 -6 -8 1 0.23 0.00 6 8 0 0.03 0.00 6 8 1 -0.11 0.00 6 8 2 0.07 0.00 6 8 3 0.02 0.00 6 8 4 -0.11 0.00 6 8 5 0.20 0.00 6 8 6 -0.34 0.00 6 8 7 0.53 0.00 6 8 8 -0.74 0.00 6 8 9 0.92 0.00 6 8 10 -1.02 0.00 6 8 11 1.06 0.00 6 8 12 -1.05 0.00 6 8 13 1.06 0.00 6 8 14 -1.11 0.00 6 8 15 1.15 0.00 6 8 16 -1.14 0.00 6 8 17 1.02 0.00 6 8 18 -0.78 0.00 6 8 19 0.49 0.00 6 8 20 -0.21 0.00 6 8 21 0.03 0.00 -6 -9 11 -0.27 0.00 -6 -9 10 0.36 0.00 -6 -9 9 -0.46 0.00 -6 -9 8 0.46 0.00 -6 -9 7 -0.33 0.00 -6 -9 6 0.11 0.00 -6 -9 5 0.07 0.00 -6 -9 4 -0.08 0.00 -6 -9 3 -0.11 0.00 -6 -9 2 0.43 0.00 -6 -9 1 -0.76 0.00 6 9 0 0.96 0.00 6 9 1 -1.02 0.00 6 9 2 0.97 0.00 6 9 3 -0.85 0.00 6 9 4 0.67 0.00 6 9 5 -0.42 0.00 6 9 6 0.08 0.00 6 9 7 0.32 0.00 6 9 8 -0.73 0.00 6 9 9 1.08 0.00 6 9 10 -1.30 0.00 6 9 11 1.41 0.00 6 9 12 -1.44 0.00 6 9 13 1.45 0.00 6 9 14 -1.47 0.00 6 9 15 1.47 0.00 6 9 16 -1.42 0.00 6 9 17 1.29 0.00 6 9 18 -1.08 0.00 6 9 19 0.82 0.00 6 9 20 -0.56 0.00 -6 -10 9 -0.71 0.00 -6 -10 8 0.82 0.00 -6 -10 7 -0.83 0.00 -6 -10 6 0.75 0.00 -6 -10 5 -0.64 0.00 -6 -10 4 0.60 0.00 -6 -10 3 -0.68 0.00 -6 -10 2 0.86 0.00 -6 -10 1 -1.06 0.00 6 10 0 1.22 0.00 6 10 1 -1.29 0.00 6 10 2 1.27 0.00 6 10 3 -1.15 0.00 6 10 4 0.94 0.00 6 10 5 -0.64 0.00 6 10 6 0.27 0.00 6 10 7 0.14 0.00 6 10 8 -0.51 0.00 6 10 9 0.80 0.00 6 10 10 -0.99 0.00 6 10 11 1.09 0.00 6 10 12 -1.13 0.00 6 10 13 1.17 0.00 6 10 14 -1.20 0.00 6 10 15 1.24 0.00 6 10 16 -1.24 0.00 6 10 17 1.18 0.00 6 10 18 -1.06 0.00 6 10 19 0.89 0.00 -6 -11 7 -0.31 0.00 -6 -11 6 0.29 0.00 -6 -11 5 -0.24 0.00 -6 -11 4 0.20 0.00 -6 -11 3 -0.21 0.00 -6 -11 2 0.29 0.00 -6 -11 1 -0.42 0.00 6 11 0 0.56 0.00 6 11 1 -0.67 0.00 6 11 2 0.73 0.00 6 11 3 -0.74 0.00 6 11 4 0.69 0.00 6 11 5 -0.57 0.00 6 11 6 0.40 0.00 6 11 7 -0.20 0.00 6 11 8 0.01 0.00 6 11 9 0.13 0.00 6 11 10 -0.21 0.00 6 11 11 0.24 0.00 6 11 12 -0.25 0.00 6 11 13 0.28 0.00 6 11 14 -0.36 0.00 6 11 15 0.49 0.00 6 11 16 -0.63 0.00 6 11 17 0.74 0.00 -6 -12 4 -0.52 0.00 -6 -12 3 0.53 0.00 -6 -12 2 -0.49 0.00 -6 -12 1 0.40 0.00 6 12 0 -0.29 0.00 6 12 1 0.18 0.00 6 12 2 -0.05 0.00 6 12 3 -0.08 0.00 6 12 4 0.22 0.00 6 12 5 -0.33 0.00 6 12 6 0.40 0.00 6 12 7 -0.41 0.00 6 12 8 0.36 0.00 6 12 9 -0.32 0.00 6 12 10 0.32 0.00 6 12 11 -0.38 0.00 6 12 12 0.48 0.00 6 12 13 -0.55 0.00 6 12 14 0.52 0.00 6 12 15 -0.38 0.00 6 13 1 0.46 0.00 6 13 2 -0.40 0.00 6 13 3 0.29 0.00 6 13 4 -0.14 0.00 6 13 5 -0.02 0.00 6 13 6 0.12 0.00 6 13 7 -0.15 0.00 6 13 8 0.11 0.00 6 13 9 -0.07 0.00 6 13 10 0.09 0.00 6 13 11 -0.22 0.00 -7 7 10 -0.77 0.00 -7 7 9 0.74 0.00 -7 7 8 -0.59 0.00 -7 7 0 0.40 0.00 7 -7 1 -0.56 0.00 7 -7 2 0.73 0.00 7 -7 3 -0.85 0.00 7 -7 4 0.91 0.00 7 -7 5 -0.91 0.00 7 -7 6 0.87 0.00 7 -7 7 -0.82 0.00 7 -7 8 0.73 0.00 -7 6 13 0.26 0.00 -7 6 12 -0.38 0.00 -7 6 11 0.51 0.00 -7 6 10 -0.61 0.00 -7 6 9 0.64 0.00 -7 6 8 -0.57 0.00 -7 6 7 0.43 0.00 -7 6 6 -0.25 0.00 -7 6 5 0.10 0.00 -7 6 4 -0.02 0.00 -7 6 3 0.04 0.00 -7 6 2 -0.11 0.00 -7 6 1 0.20 0.00 -7 6 0 -0.25 0.00 7 -6 1 0.25 0.00 7 -6 2 -0.19 0.00 7 -6 3 0.06 0.00 7 -6 4 0.12 0.00 7 -6 5 -0.34 0.00 7 -6 6 0.55 0.00 7 -6 7 -0.71 0.00 7 -6 8 0.79 0.00 7 -6 9 -0.75 0.00 7 -6 10 0.64 0.00 -7 5 15 -0.79 0.00 -7 5 14 0.75 0.00 -7 5 13 -0.62 0.00 -7 5 12 0.42 0.00 -7 5 11 -0.19 0.00 -7 5 10 -0.03 0.00 -7 5 9 0.22 0.00 -7 5 8 -0.37 0.00 -7 5 7 0.48 0.00 -7 5 6 -0.56 0.00 -7 5 5 0.61 0.00 -7 5 4 -0.65 0.00 -7 5 3 0.67 0.00 -7 5 2 -0.70 0.00 -7 5 1 0.75 0.00 -7 5 0 -0.82 0.00 7 -5 1 0.89 0.00 7 -5 2 -0.92 0.00 7 -5 3 0.88 0.00 7 -5 4 -0.75 0.00 7 -5 5 0.52 0.00 7 -5 6 -0.23 0.00 7 -5 7 -0.07 0.00 7 -5 8 0.31 0.00 7 -5 9 -0.45 0.00 7 -5 10 0.48 0.00 7 -5 11 -0.44 0.00 7 -5 12 0.38 0.00 7 -5 13 -0.33 0.00 -7 4 16 0.97 0.00 -7 4 15 -1.21 0.00 -7 4 14 1.30 0.00 -7 4 13 -1.21 0.00 -7 4 12 0.98 0.00 -7 4 11 -0.66 0.00 -7 4 10 0.32 0.00 -7 4 9 0.02 0.00 -7 4 8 -0.35 0.00 -7 4 7 0.66 0.00 -7 4 6 -0.93 0.00 -7 4 5 1.13 0.00 -7 4 4 -1.24 0.00 -7 4 3 1.26 0.00 -7 4 2 -1.22 0.00 -7 4 1 1.16 0.00 -7 4 0 -1.13 0.00 7 -4 1 1.13 0.00 7 -4 2 -1.15 0.00 7 -4 3 1.17 0.00 7 -4 4 -1.14 0.00 7 -4 5 1.04 0.00 7 -4 6 -0.84 0.00 7 -4 7 0.57 0.00 7 -4 8 -0.29 0.00 7 -4 9 0.06 0.00 7 -4 10 0.07 0.00 7 -4 11 -0.10 0.00 7 -4 12 0.10 0.00 7 -4 13 -0.13 0.00 7 -4 14 0.22 0.00 7 -4 15 -0.30 0.00 -7 3 17 -0.22 0.00 -7 3 16 0.53 0.00 -7 3 15 -0.79 0.00 -7 3 14 0.90 0.00 -7 3 13 -0.82 0.00 -7 3 12 0.57 0.00 -7 3 11 -0.21 0.00 -7 3 10 -0.19 0.00 -7 3 9 0.57 0.00 -7 3 8 -0.89 0.00 -7 3 7 1.13 0.00 -7 3 6 -1.28 0.00 -7 3 5 1.34 0.00 -7 3 4 -1.33 0.00 -7 3 3 1.26 0.00 -7 3 2 -1.13 0.00 -7 3 1 0.99 0.00 -7 3 0 -0.83 0.00 7 -3 1 0.70 0.00 7 -3 2 -0.62 0.00 7 -3 3 0.61 0.00 7 -3 4 -0.64 0.00 7 -3 5 0.67 0.00 7 -3 6 -0.63 0.00 7 -3 7 0.50 0.00 7 -3 8 -0.32 0.00 7 -3 9 0.17 0.00 7 -3 10 -0.12 0.00 7 -3 11 0.15 0.00 7 -3 12 -0.19 0.00 7 -3 13 0.15 0.00 7 -3 14 -0.01 0.00 7 -3 15 -0.17 0.00 7 -3 16 0.28 0.00 -7 2 17 0.11 0.00 -7 2 16 -0.03 0.00 -7 2 15 0.00 0.00 -7 2 14 -0.06 0.00 -7 2 13 0.27 0.00 -7 2 12 -0.61 0.00 -7 2 11 1.03 0.00 -7 2 10 -1.45 0.00 -7 2 9 1.78 0.00 -7 2 8 -1.93 0.00 -7 2 7 1.91 0.00 -7 2 6 -1.73 0.00 -7 2 5 1.47 0.00 -7 2 4 -1.17 0.00 -7 2 3 0.86 0.00 -7 2 2 -0.54 0.00 -7 2 1 0.20 0.00 -7 2 0 0.16 0.00 7 -2 1 -0.50 0.00 7 -2 2 0.76 0.00 7 -2 3 -0.87 0.00 7 -2 4 0.83 0.00 7 -2 5 -0.69 0.00 7 -2 6 0.53 0.00 7 -2 7 -0.42 0.00 7 -2 8 0.37 0.00 7 -2 9 -0.31 0.00 7 -2 10 0.18 0.00 7 -2 11 -0.01 0.00 7 -2 12 -0.12 0.00 7 -2 13 0.14 0.00 7 -2 14 -0.03 0.00 7 -2 15 -0.13 0.00 7 -2 16 0.24 0.00 7 -2 17 -0.23 0.00 -7 1 17 0.06 0.00 -7 1 16 -0.25 0.00 -7 1 15 0.50 0.00 -7 1 14 -0.85 0.00 -7 1 13 1.27 0.00 -7 1 12 -1.76 0.00 -7 1 11 2.24 0.00 -7 1 10 -2.64 0.00 -7 1 9 2.85 0.00 -7 1 8 -2.82 0.00 -7 1 7 2.58 0.00 -7 1 6 -2.19 0.00 -7 1 5 1.73 0.00 -7 1 4 -1.27 0.00 -7 1 3 0.79 0.00 -7 1 2 -0.29 0.00 -7 1 1 -0.28 0.00 -7 1 0 0.88 0.00 7 -1 1 -1.48 0.00 7 -1 2 1.95 0.00 7 -1 3 -2.21 0.00 7 -1 4 2.22 0.00 7 -1 5 -2.03 0.00 7 -1 6 1.74 0.00 7 -1 7 -1.44 0.00 7 -1 8 1.19 0.00 7 -1 9 -0.96 0.00 7 -1 10 0.73 0.00 7 -1 11 -0.49 0.00 7 -1 12 0.30 0.00 7 -1 13 -0.21 0.00 7 -1 14 0.23 0.00 7 -1 15 -0.29 0.00 7 -1 16 0.29 0.00 7 -1 17 -0.21 0.00 7 -1 18 0.09 0.00 -7 0 17 0.05 0.00 -7 0 16 -0.30 0.00 -7 0 15 0.66 0.00 -7 0 14 -1.11 0.00 -7 0 13 1.62 0.00 -7 0 12 -2.16 0.00 -7 0 11 2.63 0.00 -7 0 10 -2.93 0.00 -7 0 9 3.00 0.00 -7 0 8 -2.83 0.00 -7 0 7 2.52 0.00 -7 0 6 -2.14 0.00 -7 0 5 1.77 0.00 -7 0 4 -1.41 0.00 -7 0 3 1.03 0.00 -7 0 2 -0.57 0.00 -7 0 1 0.01 0.00 7 0 0 0.64 0.00 7 0 1 -1.28 0.00 7 0 2 1.83 0.00 7 0 3 -2.19 0.00 7 0 4 2.30 0.00 7 0 5 -2.19 0.00 7 0 6 1.95 0.00 7 0 7 -1.68 0.00 7 0 8 1.47 0.00 7 0 9 -1.30 0.00 7 0 10 1.16 0.00 7 0 11 -1.00 0.00 7 0 12 0.84 0.00 7 0 13 -0.71 0.00 7 0 14 0.61 0.00 7 0 15 -0.50 0.00 7 0 16 0.36 0.00 7 0 17 -0.19 0.00 7 0 18 0.03 0.00 7 0 19 0.08 0.00 -7 -1 17 0.27 0.00 -7 -1 16 -0.40 0.00 -7 -1 15 0.57 0.00 -7 -1 14 -0.82 0.00 -7 -1 13 1.16 0.00 -7 -1 12 -1.54 0.00 -7 -1 11 1.88 0.00 -7 -1 10 -2.08 0.00 -7 -1 9 2.07 0.00 -7 -1 8 -1.91 0.00 -7 -1 7 1.67 0.00 -7 -1 6 -1.45 0.00 -7 -1 5 1.27 0.00 -7 -1 4 -1.11 0.00 -7 -1 3 0.91 0.00 -7 -1 2 -0.64 0.00 -7 -1 1 0.30 0.00 7 1 0 0.08 0.00 7 1 1 -0.47 0.00 7 1 2 0.83 0.00 7 1 3 -1.09 0.00 7 1 4 1.23 0.00 7 1 5 -1.22 0.00 7 1 6 1.13 0.00 7 1 7 -1.05 0.00 7 1 8 1.05 0.00 7 1 9 -1.12 0.00 7 1 10 1.21 0.00 7 1 11 -1.25 0.00 7 1 12 1.20 0.00 7 1 13 -1.07 0.00 7 1 14 0.91 0.00 7 1 15 -0.72 0.00 7 1 16 0.53 0.00 7 1 17 -0.34 0.00 7 1 18 0.17 0.00 7 1 19 -0.05 0.00 7 1 20 -0.02 0.00 -7 -2 17 0.26 0.00 -7 -2 16 -0.20 0.00 -7 -2 15 0.10 0.00 -7 -2 14 -0.03 0.00 -7 -2 13 0.05 0.00 -7 -2 12 -0.18 0.00 -7 -2 11 0.36 0.00 -7 -2 10 -0.52 0.00 -7 -2 9 0.61 0.00 -7 -2 8 -0.62 0.00 -7 -2 7 0.60 0.00 -7 -2 6 -0.58 0.00 -7 -2 5 0.53 0.00 -7 -2 4 -0.45 0.00 -7 -2 3 0.31 0.00 -7 -2 2 -0.18 0.00 -7 -2 1 0.10 0.00 7 2 0 -0.08 0.00 7 2 1 0.10 0.00 7 2 2 -0.10 0.00 7 2 3 0.07 0.00 7 2 4 -0.04 0.00 7 2 5 0.04 0.00 7 2 6 -0.05 0.00 7 2 7 -0.01 0.00 7 2 8 0.18 0.00 7 2 9 -0.46 0.00 7 2 10 0.76 0.00 7 2 11 -0.97 0.00 7 2 12 1.04 0.00 7 2 13 -1.00 0.00 7 2 14 0.90 0.00 7 2 15 -0.80 0.00 7 2 16 0.73 0.00 7 2 17 -0.67 0.00 7 2 18 0.61 0.00 7 2 19 -0.54 0.00 7 2 20 0.45 0.00 -7 -3 17 -0.19 0.00 -7 -3 16 0.36 0.00 -7 -3 15 -0.64 0.00 -7 -3 14 0.95 0.00 -7 -3 13 -1.17 0.00 -7 -3 12 1.24 0.00 -7 -3 11 -1.16 0.00 -7 -3 10 0.96 0.00 -7 -3 9 -0.71 0.00 -7 -3 8 0.44 0.00 -7 -3 7 -0.21 0.00 -7 -3 6 0.05 0.00 -7 -3 5 -0.02 0.00 -7 -3 4 0.11 0.00 -7 -3 3 -0.25 0.00 -7 -3 2 0.32 0.00 -7 -3 1 -0.23 0.00 7 3 0 -0.03 0.00 7 3 1 0.35 0.00 7 3 2 -0.63 0.00 7 3 3 0.81 0.00 7 3 4 -0.92 0.00 7 3 5 0.98 0.00 7 3 6 -1.00 0.00 7 3 7 0.92 0.00 7 3 8 -0.69 0.00 7 3 9 0.34 0.00 7 3 10 0.04 0.00 7 3 11 -0.33 0.00 7 3 12 0.48 0.00 7 3 13 -0.53 0.00 7 3 14 0.56 0.00 7 3 15 -0.61 0.00 7 3 16 0.70 0.00 7 3 17 -0.80 0.00 7 3 18 0.87 0.00 7 3 19 -0.88 0.00 7 3 20 0.84 0.00 7 3 21 -0.74 0.00 -7 -4 16 0.67 0.00 -7 -4 15 -1.03 0.00 -7 -4 14 1.43 0.00 -7 -4 13 -1.78 0.00 -7 -4 12 1.97 0.00 -7 -4 11 -1.96 0.00 -7 -4 10 1.75 0.00 -7 -4 9 -1.40 0.00 -7 -4 8 0.99 0.00 -7 -4 7 -0.60 0.00 -7 -4 6 0.33 0.00 -7 -4 5 -0.23 0.00 -7 -4 4 0.30 0.00 -7 -4 3 -0.43 0.00 -7 -4 2 0.50 0.00 -7 -4 1 -0.39 0.00 7 4 0 0.12 0.00 7 4 1 0.22 0.00 7 4 2 -0.53 0.00 7 4 3 0.74 0.00 7 4 4 -0.89 0.00 7 4 5 0.99 0.00 7 4 6 -1.05 0.00 7 4 7 1.01 0.00 7 4 8 -0.84 0.00 7 4 9 0.56 0.00 7 4 10 -0.25 0.00 7 4 11 0.02 0.00 7 4 12 0.12 0.00 7 4 13 -0.21 0.00 7 4 14 0.31 0.00 7 4 15 -0.43 0.00 7 4 16 0.55 0.00 7 4 17 -0.63 0.00 7 4 18 0.66 0.00 7 4 19 -0.65 0.00 7 4 20 0.63 0.00 7 4 21 -0.58 0.00 -7 -5 15 -0.71 0.00 -7 -5 14 1.10 0.00 -7 -5 13 -1.45 0.00 -7 -5 12 1.67 0.00 -7 -5 11 -1.71 0.00 -7 -5 10 1.55 0.00 -7 -5 9 -1.24 0.00 -7 -5 8 0.85 0.00 -7 -5 7 -0.46 0.00 -7 -5 6 0.16 0.00 -7 -5 5 0.00 0.00 -7 -5 4 0.01 0.00 -7 -5 3 -0.15 0.00 -7 -5 2 0.31 0.00 -7 -5 1 -0.40 0.00 7 5 0 0.39 0.00 7 5 1 -0.32 0.00 7 5 2 0.23 0.00 7 5 3 -0.16 0.00 7 5 4 0.11 0.00 7 5 5 -0.05 0.00 7 5 6 0.00 0.00 7 5 7 0.00 0.00 7 5 8 0.07 0.00 7 5 9 -0.19 0.00 7 5 10 0.30 0.00 7 5 11 -0.36 0.00 7 5 12 0.39 0.00 7 5 13 -0.43 0.00 7 5 14 0.51 0.00 7 5 15 -0.58 0.00 7 5 16 0.61 0.00 7 5 17 -0.54 0.00 7 5 18 0.40 0.00 7 5 19 -0.25 0.00 7 5 20 0.15 0.00 7 5 21 -0.09 0.00 -7 -6 14 0.45 0.00 -7 -6 13 -0.62 0.00 -7 -6 12 0.70 0.00 -7 -6 11 -0.66 0.00 -7 -6 10 0.51 0.00 -7 -6 9 -0.29 0.00 -7 -6 8 0.02 0.00 -7 -6 7 0.29 0.00 -7 -6 6 -0.58 0.00 -7 -6 5 0.78 0.00 -7 -6 4 -0.81 0.00 -7 -6 3 0.66 0.00 -7 -6 2 -0.35 0.00 -7 -6 1 0.00 0.00 7 6 0 0.31 0.00 7 6 1 -0.53 0.00 7 6 2 0.67 0.00 7 6 3 -0.79 0.00 7 6 4 0.89 0.00 7 6 5 -1.00 0.00 7 6 6 1.10 0.00 7 6 7 -1.19 0.00 7 6 8 1.25 0.00 7 6 9 -1.26 0.00 7 6 10 1.19 0.00 7 6 11 -1.08 0.00 7 6 12 0.96 0.00 7 6 13 -0.88 0.00 7 6 14 0.85 0.00 7 6 15 -0.81 0.00 7 6 16 0.70 0.00 7 6 17 -0.53 0.00 7 6 18 0.31 0.00 7 6 19 -0.11 0.00 7 6 20 -0.03 0.00 7 6 21 0.10 0.00 -7 -7 13 -0.06 0.00 -7 -7 12 -0.12 0.00 -7 -7 11 0.35 0.00 -7 -7 10 -0.59 0.00 -7 -7 9 0.81 0.00 -7 -7 8 -1.03 0.00 -7 -7 7 1.30 0.00 -7 -7 6 -1.60 0.00 -7 -7 5 1.84 0.00 -7 -7 4 -1.92 0.00 -7 -7 3 1.74 0.00 -7 -7 2 -1.35 0.00 -7 -7 1 0.87 0.00 7 7 0 -0.45 0.00 7 7 1 0.14 0.00 7 7 2 0.08 0.00 7 7 3 -0.29 0.00 7 7 4 0.55 0.00 7 7 5 -0.86 0.00 7 7 6 1.18 0.00 7 7 7 -1.43 0.00 7 7 8 1.57 0.00 7 7 9 -1.59 0.00 7 7 10 1.49 0.00 7 7 11 -1.34 0.00 7 7 12 1.18 0.00 7 7 13 -1.03 0.00 7 7 14 0.87 0.00 7 7 15 -0.68 0.00 7 7 16 0.45 0.00 7 7 17 -0.24 0.00 7 7 18 0.08 0.00 7 7 19 0.00 0.00 7 7 20 -0.01 0.00 -7 -8 12 -0.33 0.00 -7 -8 11 0.64 0.00 -7 -8 10 -0.91 0.00 -7 -8 9 1.15 0.00 -7 -8 8 -1.39 0.00 -7 -8 7 1.70 0.00 -7 -8 6 -2.07 0.00 -7 -8 5 2.40 0.00 -7 -8 4 -2.54 0.00 -7 -8 3 2.39 0.00 -7 -8 2 -2.00 0.00 -7 -8 1 1.53 0.00 7 8 0 -1.14 0.00 7 8 1 0.89 0.00 7 8 2 -0.71 0.00 7 8 3 0.50 0.00 7 8 4 -0.19 0.00 7 8 5 -0.20 0.00 7 8 6 0.58 0.00 7 8 7 -0.85 0.00 7 8 8 0.96 0.00 7 8 9 -0.96 0.00 7 8 10 0.89 0.00 7 8 11 -0.81 0.00 7 8 12 0.74 0.00 7 8 13 -0.64 0.00 7 8 14 0.46 0.00 7 8 15 -0.21 0.00 7 8 16 -0.06 0.00 7 8 17 0.27 0.00 7 8 18 -0.35 0.00 7 8 19 0.29 0.00 7 8 20 -0.15 0.00 -7 -9 10 -0.41 0.00 -7 -9 9 0.50 0.00 -7 -9 8 -0.66 0.00 -7 -9 7 0.96 0.00 -7 -9 6 -1.37 0.00 -7 -9 5 1.78 0.00 -7 -9 4 -2.01 0.00 -7 -9 3 1.97 0.00 -7 -9 2 -1.69 0.00 -7 -9 1 1.33 0.00 7 9 0 -1.04 0.00 7 9 1 0.86 0.00 7 9 2 -0.73 0.00 7 9 3 0.58 0.00 7 9 4 -0.34 0.00 7 9 5 0.08 0.00 7 9 6 0.13 0.00 7 9 7 -0.20 0.00 7 9 8 0.15 0.00 7 9 9 -0.04 0.00 7 9 10 -0.04 0.00 7 9 11 0.07 0.00 7 9 12 -0.05 0.00 7 9 13 0.05 0.00 7 9 14 -0.14 0.00 7 9 15 0.30 0.00 7 9 16 -0.49 0.00 7 9 17 0.63 0.00 7 9 18 -0.64 0.00 7 9 19 0.53 0.00 -7 -10 8 0.40 0.00 -7 -10 7 -0.28 0.00 -7 -10 6 -0.01 0.00 -7 -10 5 0.37 0.00 -7 -10 4 -0.65 0.00 -7 -10 3 0.77 0.00 -7 -10 2 -0.71 0.00 -7 -10 1 0.56 0.00 7 10 0 -0.42 0.00 7 10 1 0.33 0.00 7 10 2 -0.27 0.00 7 10 3 0.20 0.00 7 10 4 -0.11 0.00 7 10 5 0.06 0.00 7 10 6 -0.08 0.00 7 10 7 0.19 0.00 7 10 8 -0.35 0.00 7 10 9 0.49 0.00 7 10 10 -0.58 0.00 7 10 11 0.58 0.00 7 10 12 -0.55 0.00 7 10 13 0.53 0.00 7 10 14 -0.55 0.00 7 10 15 0.62 0.00 7 10 16 -0.69 0.00 7 10 17 0.71 0.00 7 10 18 -0.66 0.00 -7 -11 6 0.74 0.00 -7 -11 5 -0.59 0.00 -7 -11 4 0.39 0.00 -7 -11 3 -0.23 0.00 -7 -11 2 0.13 0.00 -7 -11 1 -0.08 0.00 7 11 0 0.06 0.00 7 11 1 -0.05 0.00 7 11 2 0.06 0.00 7 11 3 -0.07 0.00 7 11 4 0.07 0.00 7 11 5 -0.02 0.00 7 11 6 -0.09 0.00 7 11 7 0.24 0.00 7 11 8 -0.39 0.00 7 11 9 0.48 0.00 7 11 10 -0.51 0.00 7 11 11 0.49 0.00 7 11 12 -0.46 0.00 7 11 13 0.46 0.00 7 11 14 -0.49 0.00 7 11 15 0.54 0.00 7 11 16 -0.58 0.00 -7 -12 2 0.32 0.00 -7 -12 1 -0.24 0.00 7 12 0 0.18 0.00 7 12 1 -0.15 0.00 7 12 2 0.15 0.00 7 12 3 -0.18 0.00 7 12 4 0.19 0.00 7 12 5 -0.17 0.00 7 12 6 0.09 0.00 7 12 7 0.02 0.00 7 12 8 -0.14 0.00 7 12 9 0.22 0.00 7 12 10 -0.23 0.00 7 12 11 0.18 0.00 7 12 12 -0.10 0.00 7 12 13 0.04 0.00 7 13 4 0.14 0.00 7 13 5 -0.17 0.00 7 13 6 0.14 0.00 7 13 7 -0.06 0.00 7 13 8 -0.06 0.00 -8 6 10 -0.75 0.00 -8 6 9 0.73 0.00 -8 6 8 -0.63 0.00 -8 6 7 0.45 0.00 -8 6 6 -0.21 0.00 -8 6 5 -0.05 0.00 -8 6 4 0.27 0.00 -8 6 3 -0.39 0.00 -8 6 2 0.43 0.00 -8 6 1 -0.41 0.00 -8 6 0 0.35 0.00 8 -6 1 -0.28 0.00 8 -6 2 0.22 0.00 8 -6 3 -0.18 0.00 8 -6 4 0.18 0.00 8 -6 5 -0.23 0.00 8 -6 6 0.30 0.00 8 -6 7 -0.35 0.00 -8 5 12 -0.45 0.00 -8 5 11 0.59 0.00 -8 5 10 -0.65 0.00 -8 5 9 0.64 0.00 -8 5 8 -0.57 0.00 -8 5 7 0.48 0.00 -8 5 6 -0.38 0.00 -8 5 5 0.28 0.00 -8 5 4 -0.18 0.00 -8 5 3 0.06 0.00 -8 5 2 0.06 0.00 -8 5 1 -0.16 0.00 -8 5 0 0.20 0.00 8 -5 1 -0.17 0.00 8 -5 2 0.06 0.00 8 -5 3 0.05 0.00 8 -5 4 -0.11 0.00 8 -5 5 0.08 0.00 8 -5 6 0.03 0.00 8 -5 7 -0.18 0.00 8 -5 8 0.30 0.00 8 -5 9 -0.35 0.00 8 -5 10 0.31 0.00 -8 4 13 -0.57 0.00 -8 4 12 0.33 0.00 -8 4 11 -0.08 0.00 -8 4 10 -0.11 0.00 -8 4 9 0.25 0.00 -8 4 8 -0.37 0.00 -8 4 7 0.53 0.00 -8 4 6 -0.73 0.00 -8 4 5 0.95 0.00 -8 4 4 -1.10 0.00 -8 4 3 1.14 0.00 -8 4 2 -1.04 0.00 -8 4 1 0.85 0.00 -8 4 0 -0.65 0.00 8 -4 1 0.52 0.00 8 -4 2 -0.48 0.00 8 -4 3 0.51 0.00 8 -4 4 -0.55 0.00 8 -4 5 0.53 0.00 8 -4 6 -0.42 0.00 8 -4 7 0.22 0.00 8 -4 8 0.02 0.00 8 -4 9 -0.25 0.00 8 -4 10 0.41 0.00 8 -4 11 -0.47 0.00 8 -4 12 0.44 0.00 -8 3 14 1.33 0.00 -8 3 13 -1.31 0.00 -8 3 12 1.11 0.00 -8 3 11 -0.80 0.00 -8 3 10 0.46 0.00 -8 3 9 -0.12 0.00 -8 3 8 -0.23 0.00 -8 3 7 0.61 0.00 -8 3 6 -1.03 0.00 -8 3 5 1.44 0.00 -8 3 4 -1.77 0.00 -8 3 3 1.96 0.00 -8 3 2 -1.98 0.00 -8 3 1 1.85 0.00 -8 3 0 -1.64 0.00 8 -3 1 1.40 0.00 8 -3 2 -1.19 0.00 8 -3 3 1.05 0.00 8 -3 4 -0.96 0.00 8 -3 5 0.90 0.00 8 -3 6 -0.79 0.00 8 -3 7 0.60 0.00 8 -3 8 -0.33 0.00 8 -3 9 0.03 0.00 8 -3 10 0.23 0.00 8 -3 11 -0.39 0.00 8 -3 12 0.47 0.00 8 -3 13 -0.49 0.00 8 -3 14 0.51 0.00 -8 2 15 -1.21 0.00 -8 2 14 1.45 0.00 -8 2 13 -1.50 0.00 -8 2 12 1.34 0.00 -8 2 11 -1.01 0.00 -8 2 10 0.57 0.00 -8 2 9 -0.09 0.00 -8 2 8 -0.37 0.00 -8 2 7 0.78 0.00 -8 2 6 -1.14 0.00 -8 2 5 1.41 0.00 -8 2 4 -1.62 0.00 -8 2 3 1.75 0.00 -8 2 2 -1.79 0.00 -8 2 1 1.75 0.00 -8 2 0 -1.61 0.00 8 -2 1 1.39 0.00 8 -2 2 -1.13 0.00 8 -2 3 0.90 0.00 8 -2 4 -0.73 0.00 8 -2 5 0.65 0.00 8 -2 6 -0.60 0.00 8 -2 7 0.54 0.00 8 -2 8 -0.41 0.00 8 -2 9 0.23 0.00 8 -2 10 -0.06 0.00 8 -2 11 -0.07 0.00 8 -2 12 0.15 0.00 8 -2 13 -0.24 0.00 8 -2 14 0.35 0.00 8 -2 15 -0.48 0.00 8 -2 16 0.56 0.00 -8 1 15 -1.04 0.00 -8 1 14 1.14 0.00 -8 1 13 -1.08 0.00 -8 1 12 0.86 0.00 -8 1 11 -0.48 0.00 -8 1 10 -0.01 0.00 -8 1 9 0.51 0.00 -8 1 8 -0.92 0.00 -8 1 7 1.18 0.00 -8 1 6 -1.27 0.00 -8 1 5 1.23 0.00 -8 1 4 -1.13 0.00 -8 1 3 1.00 0.00 -8 1 2 -0.88 0.00 -8 1 1 0.75 0.00 -8 1 0 -0.57 0.00 8 -1 1 0.33 0.00 8 -1 2 -0.05 0.00 8 -1 3 -0.20 0.00 8 -1 4 0.35 0.00 8 -1 5 -0.36 0.00 8 -1 6 0.26 0.00 8 -1 7 -0.11 0.00 8 -1 8 0.00 0.00 8 -1 9 0.05 0.00 8 -1 10 -0.06 0.00 8 -1 11 0.05 0.00 8 -1 12 -0.01 0.00 8 -1 13 -0.06 0.00 8 -1 14 0.18 0.00 8 -1 15 -0.31 0.00 8 -1 16 0.38 0.00 8 -1 17 -0.35 0.00 -8 0 16 0.62 0.00 -8 0 15 -0.56 0.00 -8 0 14 0.41 0.00 -8 0 13 -0.15 0.00 -8 0 12 -0.20 0.00 -8 0 11 0.63 0.00 -8 0 10 -1.06 0.00 -8 0 9 1.43 0.00 -8 0 8 -1.64 0.00 -8 0 7 1.66 0.00 -8 0 6 -1.51 0.00 -8 0 5 1.26 0.00 -8 0 4 -0.98 0.00 -8 0 3 0.71 0.00 -8 0 2 -0.46 0.00 -8 0 1 0.20 0.00 8 0 0 0.11 0.00 8 0 1 -0.47 0.00 8 0 2 0.85 0.00 8 0 3 -1.18 0.00 8 0 4 1.38 0.00 8 0 5 -1.37 0.00 8 0 6 1.20 0.00 8 0 7 -0.93 0.00 8 0 8 0.67 0.00 8 0 9 -0.48 0.00 8 0 10 0.36 0.00 8 0 11 -0.28 0.00 8 0 12 0.24 0.00 8 0 13 -0.24 0.00 8 0 14 0.27 0.00 8 0 15 -0.29 0.00 8 0 16 0.27 0.00 8 0 17 -0.17 0.00 8 0 18 0.03 0.00 -8 -1 16 0.13 0.00 -8 -1 15 0.09 0.00 -8 -1 14 -0.40 0.00 -8 -1 13 0.78 0.00 -8 -1 12 -1.19 0.00 -8 -1 11 1.60 0.00 -8 -1 10 -1.92 0.00 -8 -1 9 2.08 0.00 -8 -1 8 -2.03 0.00 -8 -1 7 1.81 0.00 -8 -1 6 -1.51 0.00 -8 -1 5 1.21 0.00 -8 -1 4 -0.96 0.00 -8 -1 3 0.76 0.00 -8 -1 2 -0.55 0.00 -8 -1 1 0.31 0.00 8 1 0 -0.01 0.00 8 1 1 -0.37 0.00 8 1 2 0.79 0.00 8 1 3 -1.18 0.00 8 1 4 1.47 0.00 8 1 5 -1.59 0.00 8 1 6 1.54 0.00 8 1 7 -1.37 0.00 8 1 8 1.18 0.00 8 1 9 -1.03 0.00 8 1 10 0.92 0.00 8 1 11 -0.81 0.00 8 1 12 0.68 0.00 8 1 13 -0.53 0.00 8 1 14 0.40 0.00 8 1 15 -0.28 0.00 8 1 16 0.16 0.00 8 1 17 -0.05 0.00 8 1 18 -0.06 0.00 -8 -2 15 0.47 0.00 -8 -2 14 -0.69 0.00 -8 -2 13 0.98 0.00 -8 -2 12 -1.32 0.00 -8 -2 11 1.66 0.00 -8 -2 10 -1.90 0.00 -8 -2 9 1.97 0.00 -8 -2 8 -1.82 0.00 -8 -2 7 1.53 0.00 -8 -2 6 -1.19 0.00 -8 -2 5 0.88 0.00 -8 -2 4 -0.63 0.00 -8 -2 3 0.43 0.00 -8 -2 2 -0.26 0.00 -8 -2 1 0.11 0.00 8 2 0 0.04 0.00 8 2 1 -0.21 0.00 8 2 2 0.42 0.00 8 2 3 -0.67 0.00 8 2 4 0.90 0.00 8 2 5 -1.07 0.00 8 2 6 1.13 0.00 8 2 7 -1.12 0.00 8 2 8 1.11 0.00 8 2 9 -1.13 0.00 8 2 10 1.16 0.00 8 2 11 -1.11 0.00 8 2 12 0.96 0.00 8 2 13 -0.71 0.00 8 2 14 0.45 0.00 8 2 15 -0.23 0.00 8 2 16 0.08 0.00 8 2 17 -0.02 0.00 8 2 18 0.00 0.00 8 2 19 -0.02 0.00 -8 -3 15 0.33 0.00 -8 -3 14 -0.33 0.00 -8 -3 13 0.37 0.00 -8 -3 12 -0.51 0.00 -8 -3 11 0.72 0.00 -8 -3 10 -0.94 0.00 -8 -3 9 1.09 0.00 -8 -3 8 -1.12 0.00 -8 -3 7 1.03 0.00 -8 -3 6 -0.84 0.00 -8 -3 5 0.60 0.00 -8 -3 4 -0.31 0.00 -8 -3 3 0.00 0.00 -8 -3 2 0.26 0.00 -8 -3 1 -0.41 0.00 8 3 0 0.42 0.00 8 3 1 -0.33 0.00 8 3 2 0.23 0.00 8 3 3 -0.17 0.00 8 3 4 0.18 0.00 8 3 5 -0.21 0.00 8 3 6 0.23 0.00 8 3 7 -0.26 0.00 8 3 8 0.36 0.00 8 3 9 -0.53 0.00 8 3 10 0.74 0.00 8 3 11 -0.87 0.00 8 3 12 0.85 0.00 8 3 13 -0.70 0.00 8 3 14 0.50 0.00 8 3 15 -0.34 0.00 8 3 16 0.27 0.00 8 3 17 -0.27 0.00 8 3 18 0.31 0.00 8 3 19 -0.36 0.00 -8 -4 15 -0.10 0.00 -8 -4 14 0.29 0.00 -8 -4 13 -0.49 0.00 -8 -4 12 0.62 0.00 -8 -4 11 -0.61 0.00 -8 -4 10 0.47 0.00 -8 -4 9 -0.23 0.00 -8 -4 8 -0.04 0.00 -8 -4 7 0.28 0.00 -8 -4 6 -0.42 0.00 -8 -4 5 0.43 0.00 -8 -4 4 -0.28 0.00 -8 -4 3 0.02 0.00 -8 -4 2 0.24 0.00 -8 -4 1 -0.38 0.00 8 4 0 0.32 0.00 8 4 1 -0.09 0.00 8 4 2 -0.18 0.00 8 4 3 0.41 0.00 8 4 4 -0.57 0.00 8 4 5 0.66 0.00 8 4 6 -0.72 0.00 8 4 7 0.72 0.00 8 4 8 -0.60 0.00 8 4 9 0.36 0.00 8 4 10 -0.06 0.00 8 4 11 -0.21 0.00 8 4 12 0.37 0.00 8 4 13 -0.44 0.00 8 4 14 0.48 0.00 8 4 15 -0.54 0.00 8 4 16 0.63 0.00 8 4 17 -0.71 0.00 8 4 18 0.75 0.00 8 4 19 -0.74 0.00 8 4 20 0.68 0.00 -8 -5 14 0.70 0.00 -8 -5 13 -1.06 0.00 -8 -5 12 1.39 0.00 -8 -5 11 -1.60 0.00 -8 -5 10 1.61 0.00 -8 -5 9 -1.43 0.00 -8 -5 8 1.11 0.00 -8 -5 7 -0.71 0.00 -8 -5 6 0.33 0.00 -8 -5 5 -0.05 0.00 -8 -5 4 -0.07 0.00 -8 -5 3 0.04 0.00 -8 -5 2 0.05 0.00 -8 -5 1 -0.09 0.00 8 5 0 -0.01 0.00 8 5 1 0.24 0.00 8 5 2 -0.54 0.00 8 5 3 0.80 0.00 8 5 4 -0.98 0.00 8 5 5 1.09 0.00 8 5 6 -1.13 0.00 8 5 7 1.10 0.00 8 5 8 -0.97 0.00 8 5 9 0.76 0.00 8 5 10 -0.50 0.00 8 5 11 0.28 0.00 8 5 12 -0.09 0.00 8 5 13 -0.09 0.00 8 5 14 0.32 0.00 8 5 15 -0.59 0.00 8 5 16 0.83 0.00 8 5 17 -0.98 0.00 8 5 18 0.99 0.00 8 5 19 -0.89 0.00 8 5 20 0.73 0.00 -8 -6 13 -1.02 0.00 -8 -6 12 1.41 0.00 -8 -6 11 -1.69 0.00 -8 -6 10 1.82 0.00 -8 -6 9 -1.77 0.00 -8 -6 8 1.57 0.00 -8 -6 7 -1.26 0.00 -8 -6 6 0.90 0.00 -8 -6 5 -0.56 0.00 -8 -6 4 0.32 0.00 -8 -6 3 -0.23 0.00 -8 -6 2 0.27 0.00 -8 -6 1 -0.32 0.00 8 6 0 0.29 0.00 8 6 1 -0.13 0.00 8 6 2 -0.12 0.00 8 6 3 0.37 0.00 8 6 4 -0.55 0.00 8 6 5 0.63 0.00 8 6 6 -0.62 0.00 8 6 7 0.53 0.00 8 6 8 -0.40 0.00 8 6 9 0.26 0.00 8 6 10 -0.17 0.00 8 6 11 0.12 0.00 8 6 12 -0.07 0.00 8 6 13 -0.04 0.00 8 6 14 0.25 0.00 8 6 15 -0.53 0.00 8 6 16 0.77 0.00 8 6 17 -0.89 0.00 8 6 18 0.86 0.00 8 6 19 -0.73 0.00 8 6 20 0.56 0.00 -8 -7 12 0.72 0.00 -8 -7 11 -0.89 0.00 -8 -7 10 0.96 0.00 -8 -7 9 -0.95 0.00 -8 -7 8 0.87 0.00 -8 -7 7 -0.71 0.00 -8 -7 6 0.47 0.00 -8 -7 5 -0.21 0.00 -8 -7 4 0.03 0.00 -8 -7 3 -0.02 0.00 -8 -7 2 0.19 0.00 -8 -7 1 -0.44 0.00 8 7 0 0.62 0.00 8 7 1 -0.65 0.00 8 7 2 0.54 0.00 8 7 3 -0.39 0.00 8 7 4 0.30 0.00 8 7 5 -0.32 0.00 8 7 6 0.44 0.00 8 7 7 -0.60 0.00 8 7 8 0.71 0.00 8 7 9 -0.74 0.00 8 7 10 0.67 0.00 8 7 11 -0.53 0.00 8 7 12 0.42 0.00 8 7 13 -0.38 0.00 8 7 14 0.43 0.00 8 7 15 -0.52 0.00 8 7 16 0.57 0.00 8 7 17 -0.54 0.00 8 7 18 0.45 0.00 8 7 19 -0.34 0.00 -8 -8 10 -0.17 0.00 -8 -8 9 0.22 0.00 -8 -8 8 -0.29 0.00 -8 -8 7 0.40 0.00 -8 -8 6 -0.61 0.00 -8 -8 5 0.84 0.00 -8 -8 4 -1.00 0.00 -8 -8 3 0.94 0.00 -8 -8 2 -0.66 0.00 -8 -8 1 0.27 0.00 8 8 0 0.09 0.00 8 8 1 -0.29 0.00 8 8 2 0.37 0.00 8 8 3 -0.44 0.00 8 8 4 0.60 0.00 8 8 5 -0.86 0.00 8 8 6 1.17 0.00 8 8 7 -1.41 0.00 8 8 8 1.50 0.00 8 8 9 -1.44 0.00 8 8 10 1.27 0.00 8 8 11 -1.07 0.00 8 8 12 0.90 0.00 8 8 13 -0.79 0.00 8 8 14 0.70 0.00 8 8 15 -0.56 0.00 8 8 16 0.36 0.00 8 8 17 -0.13 0.00 8 8 18 -0.05 0.00 8 8 19 0.13 0.00 -8 -9 9 0.68 0.00 -8 -9 8 -0.73 0.00 -8 -9 7 0.85 0.00 -8 -9 6 -1.06 0.00 -8 -9 5 1.33 0.00 -8 -9 4 -1.53 0.00 -8 -9 3 1.53 0.00 -8 -9 2 -1.32 0.00 -8 -9 1 0.99 0.00 8 9 0 -0.69 0.00 8 9 1 0.48 0.00 8 9 2 -0.33 0.00 8 9 3 0.12 0.00 8 9 4 0.22 0.00 8 9 5 -0.65 0.00 8 9 6 1.06 0.00 8 9 7 -1.32 0.00 8 9 8 1.38 0.00 8 9 9 -1.28 0.00 8 9 10 1.12 0.00 8 9 11 -0.99 0.00 8 9 12 0.91 0.00 8 9 13 -0.85 0.00 8 9 14 0.74 0.00 8 9 15 -0.51 0.00 8 9 16 0.19 0.00 8 9 17 0.13 0.00 8 9 18 -0.35 0.00 -8 -10 7 0.35 0.00 -8 -10 6 -0.52 0.00 -8 -10 5 0.77 0.00 -8 -10 4 -0.98 0.00 -8 -10 3 1.07 0.00 -8 -10 2 -1.00 0.00 -8 -10 1 0.87 0.00 8 10 0 -0.77 0.00 8 10 1 0.71 0.00 8 10 2 -0.65 0.00 8 10 3 0.50 0.00 8 10 4 -0.21 0.00 8 10 5 -0.13 0.00 8 10 6 0.43 0.00 8 10 7 -0.59 0.00 8 10 8 0.60 0.00 8 10 9 -0.53 0.00 8 10 10 0.47 0.00 8 10 11 -0.46 0.00 8 10 12 0.49 0.00 8 10 13 -0.51 0.00 8 10 14 0.45 0.00 8 10 15 -0.28 0.00 8 10 16 0.03 0.00 -8 -11 4 -0.10 0.00 -8 -11 3 0.21 0.00 -8 -11 2 -0.28 0.00 -8 -11 1 0.32 0.00 8 11 0 -0.39 0.00 8 11 1 0.47 0.00 8 11 2 -0.51 0.00 8 11 3 0.47 0.00 8 11 4 -0.34 0.00 8 11 5 0.19 0.00 8 11 6 -0.09 0.00 8 11 7 0.05 0.00 8 11 8 -0.06 0.00 8 11 9 0.07 0.00 8 11 10 -0.05 0.00 8 11 11 -0.02 0.00 8 11 12 0.10 0.00 8 11 13 -0.14 0.00 8 11 14 0.11 0.00 8 12 0 -0.08 0.00 8 12 1 0.17 0.00 8 12 2 -0.21 0.00 8 12 3 0.19 0.00 8 12 4 -0.13 0.00 8 12 5 0.09 0.00 8 12 6 -0.09 0.00 8 12 7 0.14 0.00 8 12 8 -0.19 0.00 8 12 9 0.21 0.00 8 12 10 -0.18 0.00 8 12 11 0.12 0.00 -9 5 8 -0.52 0.00 -9 5 7 0.47 0.00 -9 5 6 -0.36 0.00 -9 5 5 0.21 0.00 -9 5 4 -0.01 0.00 -9 5 3 -0.22 0.00 -9 5 2 0.42 0.00 -9 5 1 -0.55 0.00 -9 5 0 0.55 0.00 9 -5 1 -0.42 0.00 9 -5 2 0.18 0.00 9 -5 3 0.08 0.00 9 -5 4 -0.27 0.00 9 -5 5 0.34 0.00 9 -5 6 -0.27 0.00 -9 4 10 -0.43 0.00 -9 4 9 0.42 0.00 -9 4 8 -0.35 0.00 -9 4 7 0.30 0.00 -9 4 6 -0.27 0.00 -9 4 5 0.25 0.00 -9 4 4 -0.20 0.00 -9 4 3 0.07 0.00 -9 4 2 0.13 0.00 -9 4 1 -0.36 0.00 -9 4 0 0.53 0.00 9 -4 1 -0.56 0.00 9 -4 2 0.45 0.00 9 -4 3 -0.24 0.00 9 -4 4 0.03 0.00 9 -4 5 0.11 0.00 9 -4 6 -0.12 0.00 9 -4 7 0.05 0.00 9 -4 8 0.06 0.00 9 -4 9 -0.16 0.00 -9 3 12 0.23 0.00 -9 3 11 -0.07 0.00 -9 3 10 -0.07 0.00 -9 3 9 0.16 0.00 -9 3 8 -0.23 0.00 -9 3 7 0.34 0.00 -9 3 6 -0.50 0.00 -9 3 5 0.69 0.00 -9 3 4 -0.84 0.00 -9 3 3 0.88 0.00 -9 3 2 -0.78 0.00 -9 3 1 0.57 0.00 -9 3 0 -0.34 0.00 9 -3 1 0.17 0.00 9 -3 2 -0.08 0.00 9 -3 3 0.07 0.00 9 -3 4 -0.09 0.00 9 -3 5 0.09 0.00 9 -3 6 -0.04 0.00 9 -3 7 -0.07 0.00 9 -3 8 0.21 0.00 9 -3 9 -0.36 0.00 9 -3 10 0.48 0.00 9 -3 11 -0.51 0.00 9 -3 12 0.46 0.00 -9 2 13 -0.91 0.00 -9 2 12 0.86 0.00 -9 2 11 -0.71 0.00 -9 2 10 0.48 0.00 -9 2 9 -0.20 0.00 -9 2 8 -0.14 0.00 -9 2 7 0.53 0.00 -9 2 6 -0.93 0.00 -9 2 5 1.30 0.00 -9 2 4 -1.56 0.00 -9 2 3 1.69 0.00 -9 2 2 -1.68 0.00 -9 2 1 1.58 0.00 -9 2 0 -1.42 0.00 9 -2 1 1.24 0.00 9 -2 2 -1.06 0.00 9 -2 3 0.86 0.00 9 -2 4 -0.65 0.00 9 -2 5 0.44 0.00 9 -2 6 -0.24 0.00 9 -2 7 0.05 0.00 9 -2 8 0.15 0.00 9 -2 9 -0.35 0.00 9 -2 10 0.52 0.00 9 -2 11 -0.62 0.00 9 -2 12 0.63 0.00 9 -2 13 -0.56 0.00 -9 1 13 -1.36 0.00 -9 1 12 1.38 0.00 -9 1 11 -1.25 0.00 -9 1 10 0.97 0.00 -9 1 9 -0.54 0.00 -9 1 8 0.00 0.00 -9 1 7 0.57 0.00 -9 1 6 -1.08 0.00 -9 1 5 1.47 0.00 -9 1 4 -1.71 0.00 -9 1 3 1.80 0.00 -9 1 2 -1.80 0.00 -9 1 1 1.75 0.00 -9 1 0 -1.69 0.00 9 -1 1 1.59 0.00 9 -1 2 -1.44 0.00 9 -1 3 1.21 0.00 9 -1 4 -0.94 0.00 9 -1 5 0.67 0.00 9 -1 6 -0.45 0.00 9 -1 7 0.27 0.00 9 -1 8 -0.12 0.00 9 -1 9 -0.05 0.00 9 -1 10 0.21 0.00 9 -1 11 -0.35 0.00 9 -1 12 0.44 0.00 9 -1 13 -0.48 0.00 9 -1 14 0.49 0.00 9 -1 15 -0.48 0.00 -9 0 13 -1.44 0.00 -9 0 12 1.43 0.00 -9 0 11 -1.29 0.00 -9 0 10 1.00 0.00 -9 0 9 -0.56 0.00 -9 0 8 0.04 0.00 -9 0 7 0.46 0.00 -9 0 6 -0.87 0.00 -9 0 5 1.12 0.00 -9 0 4 -1.24 0.00 -9 0 3 1.25 0.00 -9 0 2 -1.21 0.00 -9 0 1 1.17 0.00 9 0 0 -1.13 0.00 9 0 1 1.07 0.00 9 0 2 -0.97 0.00 9 0 3 0.81 0.00 9 0 4 -0.62 0.00 9 0 5 0.45 0.00 9 0 6 -0.34 0.00 9 0 7 0.28 0.00 9 0 8 -0.23 0.00 9 0 9 0.15 0.00 9 0 10 -0.03 0.00 9 0 11 -0.11 0.00 9 0 12 0.23 0.00 9 0 13 -0.31 0.00 9 0 14 0.36 0.00 9 0 15 -0.37 0.00 9 0 16 0.33 0.00 -9 -1 14 0.95 0.00 -9 -1 13 -0.94 0.00 -9 -1 12 0.86 0.00 -9 -1 11 -0.68 0.00 -9 -1 10 0.42 0.00 -9 -1 9 -0.11 0.00 -9 -1 8 -0.21 0.00 -9 -1 7 0.46 0.00 -9 -1 6 -0.63 0.00 -9 -1 5 0.73 0.00 -9 -1 4 -0.77 0.00 -9 -1 3 0.77 0.00 -9 -1 2 -0.73 0.00 -9 -1 1 0.66 0.00 9 1 0 -0.57 0.00 9 1 1 0.46 0.00 9 1 2 -0.33 0.00 9 1 3 0.19 0.00 9 1 4 -0.06 0.00 9 1 5 -0.02 0.00 9 1 6 0.02 0.00 9 1 7 0.04 0.00 9 1 8 -0.09 0.00 9 1 9 0.08 0.00 9 1 10 0.00 0.00 9 1 11 -0.11 0.00 9 1 12 0.19 0.00 9 1 13 -0.22 0.00 9 1 14 0.19 0.00 9 1 15 -0.13 0.00 9 1 16 0.03 0.00 9 1 17 0.09 0.00 -9 -2 13 -0.26 0.00 -9 -2 12 0.11 0.00 -9 -2 11 0.07 0.00 -9 -2 10 -0.28 0.00 -9 -2 9 0.46 0.00 -9 -2 8 -0.55 0.00 -9 -2 7 0.56 0.00 -9 -2 6 -0.53 0.00 -9 -2 5 0.51 0.00 -9 -2 3 0.54 0.00 -9 -2 2 -0.52 0.00 -9 -2 1 0.43 0.00 9 2 0 -0.29 0.00 9 2 1 0.11 0.00 9 2 2 0.06 0.00 9 2 3 -0.23 0.00 9 2 4 0.36 0.00 9 2 5 -0.42 0.00 9 2 6 0.37 0.00 9 2 7 -0.25 0.00 9 2 8 0.13 0.00 9 2 9 -0.07 0.00 9 2 10 0.10 0.00 9 2 11 -0.16 0.00 9 2 12 0.19 0.00 9 2 13 -0.13 0.00 9 2 14 -0.01 0.00 9 2 15 0.17 0.00 9 2 16 -0.32 0.00 9 2 17 0.43 0.00 -9 -3 13 0.07 0.00 -9 -3 12 -0.21 0.00 -9 -3 11 0.38 0.00 -9 -3 10 -0.54 0.00 -9 -3 9 0.64 0.00 -9 -3 8 -0.64 0.00 -9 -3 7 0.54 0.00 -9 -3 6 -0.41 0.00 -9 -3 5 0.30 0.00 -9 -3 4 -0.24 0.00 -9 -3 3 0.19 0.00 -9 -3 2 -0.09 0.00 -9 -3 1 -0.04 0.00 9 3 0 0.18 0.00 9 3 1 -0.29 0.00 9 3 2 0.38 0.00 9 3 3 -0.46 0.00 9 3 4 0.53 0.00 9 3 5 -0.56 0.00 9 3 6 0.49 0.00 9 3 7 -0.34 0.00 9 3 8 0.18 0.00 9 3 9 -0.08 0.00 9 3 10 0.09 0.00 9 3 11 -0.14 0.00 9 3 12 0.15 0.00 9 3 13 -0.08 0.00 9 3 14 -0.08 0.00 9 3 15 0.25 0.00 9 3 16 -0.40 0.00 9 3 17 0.46 0.00 9 3 18 -0.45 0.00 -9 -4 13 0.13 0.00 -9 -4 12 -0.17 0.00 -9 -4 11 0.24 0.00 -9 -4 10 -0.34 0.00 -9 -4 9 0.42 0.00 -9 -4 8 -0.44 0.00 -9 -4 7 0.39 0.00 -9 -4 6 -0.30 0.00 -9 -4 5 0.18 0.00 -9 -4 4 -0.04 0.00 -9 -4 3 -0.15 0.00 -9 -4 2 0.39 0.00 -9 -4 1 -0.60 0.00 9 4 0 0.71 0.00 9 4 1 -0.69 0.00 9 4 2 0.58 0.00 9 4 3 -0.46 0.00 9 4 4 0.38 0.00 9 4 5 -0.32 0.00 9 4 6 0.23 0.00 9 4 7 -0.10 0.00 9 4 8 -0.02 0.00 9 4 9 0.06 0.00 9 4 10 -0.01 0.00 9 4 11 -0.10 0.00 9 4 12 0.17 0.00 9 4 13 -0.17 0.00 9 4 14 0.12 0.00 9 4 15 -0.05 0.00 9 4 16 0.01 0.00 9 4 17 0.00 0.00 9 4 18 0.00 0.00 -9 -5 12 -0.02 0.00 -9 -5 11 -0.05 0.00 -9 -5 10 0.08 0.00 -9 -5 9 -0.05 0.00 -9 -5 8 -0.02 0.00 -9 -5 7 0.11 0.00 -9 -5 6 -0.19 0.00 -9 -5 5 0.22 0.00 -9 -5 4 -0.16 0.00 -9 -5 3 -0.03 0.00 -9 -5 2 0.30 0.00 -9 -5 1 -0.55 0.00 9 5 0 0.67 0.00 9 5 1 -0.59 0.00 9 5 2 0.36 0.00 9 5 3 -0.09 0.00 9 5 4 -0.12 0.00 9 5 5 0.25 0.00 9 5 6 -0.33 0.00 9 5 7 0.38 0.00 9 5 8 -0.36 0.00 9 5 9 0.27 0.00 9 5 10 -0.12 0.00 9 5 11 -0.05 0.00 9 5 12 0.17 0.00 9 5 13 -0.24 0.00 9 5 14 0.31 0.00 9 5 15 -0.41 0.00 9 5 16 0.53 0.00 9 5 17 -0.62 0.00 9 5 18 0.63 0.00 -9 -6 11 -0.45 0.00 -9 -6 10 0.59 0.00 -9 -6 9 -0.62 0.00 -9 -6 8 0.54 0.00 -9 -6 7 -0.37 0.00 -9 -6 6 0.14 0.00 -9 -6 5 0.10 0.00 -9 -6 4 -0.26 0.00 -9 -6 3 0.26 0.00 -9 -6 2 -0.12 0.00 -9 -6 1 -0.09 0.00 9 6 0 0.22 0.00 9 6 1 -0.16 0.00 9 6 2 -0.07 0.00 9 6 3 0.38 0.00 9 6 4 -0.66 0.00 9 6 5 0.83 0.00 9 6 6 -0.88 0.00 9 6 7 0.81 0.00 9 6 8 -0.65 0.00 9 6 9 0.43 0.00 9 6 10 -0.20 0.00 9 6 11 0.02 0.00 9 6 12 0.09 0.00 9 6 13 -0.17 0.00 9 6 14 0.31 0.00 9 6 15 -0.51 0.00 9 6 16 0.74 0.00 9 6 17 -0.91 0.00 9 6 18 0.95 0.00 -9 -7 10 0.82 0.00 -9 -7 9 -0.89 0.00 -9 -7 8 0.86 0.00 -9 -7 7 -0.72 0.00 -9 -7 6 0.47 0.00 -9 -7 5 -0.15 0.00 -9 -7 4 -0.15 0.00 -9 -7 3 0.31 0.00 -9 -7 2 -0.28 0.00 -9 -7 1 0.12 0.00 9 7 0 0.03 0.00 9 7 1 -0.03 0.00 9 7 2 -0.16 0.00 9 7 3 0.45 0.00 9 7 4 -0.73 0.00 9 7 5 0.89 0.00 9 7 6 -0.90 0.00 9 7 7 0.78 0.00 9 7 8 -0.57 0.00 9 7 9 0.34 0.00 9 7 10 -0.15 0.00 9 7 11 0.03 0.00 9 7 12 0.04 0.00 9 7 13 -0.13 0.00 9 7 14 0.28 0.00 9 7 15 -0.48 0.00 9 7 16 0.68 0.00 9 7 17 -0.80 0.00 9 7 18 0.80 0.00 -9 -8 8 0.52 0.00 -9 -8 7 -0.47 0.00 -9 -8 6 0.30 0.00 -9 -8 5 -0.04 0.00 -9 -8 4 -0.25 0.00 -9 -8 3 0.43 0.00 -9 -8 2 -0.41 0.00 -9 -8 1 0.23 0.00 9 8 0 -0.04 0.00 9 8 1 -0.04 0.00 9 8 2 -0.03 0.00 9 8 3 0.18 0.00 9 8 4 -0.30 0.00 9 8 5 0.30 0.00 9 8 6 -0.19 0.00 9 8 7 0.03 0.00 9 8 8 0.11 0.00 9 8 9 -0.18 0.00 9 8 10 0.18 0.00 9 8 11 -0.16 0.00 9 8 12 0.17 0.00 9 8 13 -0.24 0.00 9 8 14 0.36 0.00 9 8 15 -0.49 0.00 9 8 16 0.54 0.00 9 8 17 -0.50 0.00 -9 -9 7 0.05 0.00 -9 -9 6 -0.13 0.00 -9 -9 5 0.31 0.00 -9 -9 4 -0.53 0.00 -9 -9 3 0.66 0.00 -9 -9 2 -0.64 0.00 -9 -9 1 0.48 0.00 9 9 0 -0.31 0.00 9 9 1 0.22 0.00 9 9 2 -0.19 0.00 9 9 3 0.16 0.00 9 9 4 -0.02 0.00 9 9 5 -0.25 0.00 9 9 6 0.56 0.00 9 9 7 -0.79 0.00 9 9 8 0.88 0.00 9 9 9 -0.81 0.00 9 9 10 0.66 0.00 9 9 11 -0.53 0.00 9 9 12 0.47 0.00 9 9 13 -0.50 0.00 9 9 14 0.55 0.00 9 9 15 -0.54 0.00 9 9 16 0.43 0.00 -9 -10 4 -0.38 0.00 -9 -10 3 0.45 0.00 -9 -10 2 -0.44 0.00 -9 -10 1 0.38 0.00 9 10 0 -0.37 0.00 9 10 1 0.42 0.00 9 10 2 -0.48 0.00 9 10 3 0.43 0.00 9 10 4 -0.21 0.00 9 10 5 -0.14 0.00 9 10 6 0.52 0.00 9 10 7 -0.79 0.00 9 10 8 0.89 0.00 9 10 9 -0.85 0.00 9 10 10 0.75 0.00 9 10 11 -0.69 0.00 9 10 12 0.69 0.00 9 10 13 -0.73 0.00 9 10 14 0.72 0.00 -9 -11 1 -0.09 0.00 9 11 0 -0.03 0.00 9 11 1 0.23 0.00 9 11 2 -0.43 0.00 9 11 3 0.52 0.00 9 11 4 -0.45 0.00 9 11 5 0.26 0.00 9 11 6 -0.04 0.00 9 11 7 -0.12 0.00 9 11 8 0.22 0.00 9 11 9 -0.27 0.00 9 11 10 0.34 0.00 9 11 11 -0.45 0.00 9 11 12 0.57 0.00 -10 4 4 -0.17 0.00 -10 4 3 0.00 0.00 -10 4 2 0.22 0.00 -10 4 1 -0.43 0.00 -10 4 0 0.56 0.00 10 -4 1 -0.55 0.00 10 -4 2 0.41 0.00 10 -4 3 -0.19 0.00 10 -4 4 -0.02 0.00 -10 3 7 0.08 0.00 -10 3 6 -0.08 0.00 -10 3 5 0.09 0.00 -10 3 4 -0.06 0.00 -10 3 3 -0.06 0.00 -10 3 2 0.25 0.00 -10 3 1 -0.46 0.00 -10 3 0 0.62 0.00 10 -3 1 -0.66 0.00 10 -3 2 0.56 0.00 10 -3 3 -0.39 0.00 10 -3 4 0.22 0.00 10 -3 5 -0.13 0.00 10 -3 6 0.13 0.00 10 -3 7 -0.18 0.00 10 -3 8 0.23 0.00 -10 2 9 -0.26 0.00 -10 2 8 0.22 0.00 -10 2 7 -0.11 0.00 -10 2 6 -0.07 0.00 -10 2 5 0.24 0.00 -10 2 4 -0.34 0.00 -10 2 3 0.31 0.00 -10 2 2 -0.16 0.00 -10 2 1 -0.04 0.00 -10 2 0 0.21 0.00 10 -2 1 -0.27 0.00 10 -2 2 0.25 0.00 10 -2 3 -0.19 0.00 10 -2 4 0.18 0.00 10 -2 5 -0.25 0.00 10 -2 6 0.38 0.00 10 -2 7 -0.51 0.00 10 -2 8 0.59 0.00 10 -2 9 -0.61 0.00 10 -2 10 0.57 0.00 -10 1 10 0.58 0.00 -10 1 9 -0.59 0.00 -10 1 8 0.44 0.00 -10 1 7 -0.13 0.00 -10 1 6 -0.27 0.00 -10 1 5 0.67 0.00 -10 1 4 -0.93 0.00 -10 1 3 1.02 0.00 -10 1 2 -0.94 0.00 -10 1 1 0.79 0.00 -10 1 0 -0.65 0.00 10 -1 1 0.58 0.00 10 -1 2 -0.54 0.00 10 -1 3 0.47 0.00 10 -1 4 -0.31 0.00 10 -1 5 0.05 0.00 10 -1 6 0.24 0.00 10 -1 7 -0.49 0.00 10 -1 8 0.66 0.00 10 -1 9 -0.73 0.00 10 -1 10 0.73 0.00 10 -1 11 -0.67 0.00 10 -1 12 0.56 0.00 -10 0 11 -0.56 0.00 -10 0 10 0.65 0.00 -10 0 9 -0.62 0.00 -10 0 8 0.41 0.00 -10 0 7 -0.03 0.00 -10 0 6 -0.43 0.00 -10 0 5 0.88 0.00 -10 0 4 -1.20 0.00 -10 0 3 1.37 0.00 -10 0 2 -1.39 0.00 -10 0 1 1.35 0.00 10 0 0 -1.30 0.00 10 0 1 1.29 0.00 10 0 2 -1.27 0.00 10 0 3 1.18 0.00 10 0 4 -0.97 0.00 10 0 5 0.64 0.00 10 0 6 -0.27 0.00 10 0 7 -0.05 0.00 10 0 8 0.29 0.00 10 0 9 -0.45 0.00 10 0 10 0.54 0.00 10 0 11 -0.59 0.00 10 0 12 0.58 0.00 10 0 13 -0.53 0.00 -10 -1 11 -0.56 0.00 -10 -1 10 0.53 0.00 -10 -1 9 -0.41 0.00 -10 -1 8 0.19 0.00 -10 -1 7 0.10 0.00 -10 -1 6 -0.41 0.00 -10 -1 5 0.70 0.00 -10 -1 4 -0.92 0.00 -10 -1 3 1.07 0.00 -10 -1 2 -1.15 0.00 -10 -1 1 1.19 0.00 10 1 0 -1.23 0.00 10 1 1 1.30 0.00 10 1 2 -1.36 0.00 10 1 3 1.37 0.00 10 1 4 -1.27 0.00 10 1 5 1.05 0.00 10 1 6 -0.77 0.00 10 1 7 0.48 0.00 10 1 8 -0.22 0.00 10 1 9 -0.01 0.00 10 1 10 0.21 0.00 10 1 11 -0.37 0.00 10 1 12 0.46 0.00 10 1 13 -0.48 0.00 10 1 14 0.43 0.00 -10 -2 11 -0.63 0.00 -10 -2 10 0.50 0.00 -10 -2 9 -0.30 0.00 -10 -2 8 0.08 0.00 -10 -2 7 0.12 0.00 -10 -2 6 -0.28 0.00 -10 -2 5 0.42 0.00 -10 -2 4 -0.54 0.00 -10 -2 3 0.63 0.00 -10 -2 2 -0.67 0.00 -10 -2 1 0.66 0.00 10 2 0 -0.63 0.00 10 2 1 0.64 0.00 10 2 2 -0.71 0.00 10 2 3 0.80 0.00 10 2 4 -0.86 0.00 10 2 5 0.85 0.00 10 2 6 -0.79 0.00 10 2 7 0.70 0.00 10 2 8 -0.59 0.00 10 2 9 0.44 0.00 10 2 10 -0.24 0.00 10 2 11 0.02 0.00 10 2 12 0.15 0.00 10 2 13 -0.23 0.00 10 2 14 0.19 0.00 10 2 15 -0.07 0.00 -10 -3 11 -0.71 0.00 -10 -3 10 0.60 0.00 -10 -3 9 -0.42 0.00 -10 -3 8 0.23 0.00 -10 -3 7 -0.07 0.00 -10 -3 6 -0.05 0.00 -10 -3 5 0.16 0.00 -10 -3 4 -0.28 0.00 -10 -3 3 0.35 0.00 -10 -3 2 -0.33 0.00 -10 -3 1 0.20 0.00 10 3 0 -0.02 0.00 10 3 1 -0.12 0.00 10 3 2 0.16 0.00 10 3 3 -0.11 0.00 10 3 4 0.01 0.00 10 3 5 0.12 0.00 10 3 6 -0.27 0.00 10 3 7 0.45 0.00 10 3 8 -0.64 0.00 10 3 9 0.74 0.00 10 3 10 -0.72 0.00 10 3 11 0.57 0.00 10 3 12 -0.38 0.00 10 3 13 0.25 0.00 10 3 14 -0.22 0.00 10 3 15 0.28 0.00 10 3 16 -0.38 0.00 -10 -4 10 0.55 0.00 -10 -4 9 -0.48 0.00 -10 -4 8 0.39 0.00 -10 -4 7 -0.32 0.00 -10 -4 6 0.25 0.00 -10 -4 5 -0.15 0.00 -10 -4 4 0.03 0.00 -10 -4 3 0.02 0.00 -10 -4 2 0.04 0.00 -10 -4 1 -0.22 0.00 10 4 0 0.45 0.00 10 4 1 -0.62 0.00 10 4 2 0.67 0.00 10 4 3 -0.64 0.00 10 4 4 0.56 0.00 10 4 5 -0.46 0.00 10 4 6 0.28 0.00 10 4 7 -0.01 0.00 10 4 8 -0.33 0.00 10 4 9 0.64 0.00 10 4 10 -0.80 0.00 10 4 11 0.79 0.00 10 4 12 -0.68 0.00 10 4 13 0.56 0.00 10 4 14 -0.49 0.00 10 4 15 0.48 0.00 10 4 16 -0.49 0.00 -10 -5 10 0.17 0.00 -10 -5 9 -0.20 0.00 -10 -5 8 0.24 0.00 -10 -5 7 -0.27 0.00 -10 -5 6 0.28 0.00 -10 -5 5 -0.25 0.00 -10 -5 4 0.21 0.00 -10 -5 3 -0.23 0.00 -10 -5 2 0.35 0.00 -10 -5 1 -0.57 0.00 10 5 0 0.76 0.00 10 5 1 -0.84 0.00 10 5 2 0.78 0.00 10 5 3 -0.64 0.00 10 5 4 0.52 0.00 10 5 5 -0.44 0.00 10 5 6 0.35 0.00 10 5 7 -0.20 0.00 10 5 8 -0.01 0.00 10 5 9 0.22 0.00 10 5 10 -0.36 0.00 10 5 11 0.40 0.00 10 5 12 -0.39 0.00 10 5 13 0.38 0.00 10 5 14 -0.39 0.00 10 5 15 0.40 0.00 10 5 16 -0.37 0.00 -10 -6 9 0.13 0.00 -10 -6 8 -0.07 0.00 -10 -6 7 0.03 0.00 -10 -6 6 -0.02 0.00 -10 -6 5 0.06 0.00 -10 -6 4 -0.09 0.00 -10 -6 3 0.04 0.00 -10 -6 2 0.13 0.00 -10 -6 1 -0.40 0.00 10 6 0 0.63 0.00 10 6 1 -0.71 0.00 10 6 2 0.60 0.00 10 6 3 -0.39 0.00 10 6 4 0.18 0.00 10 6 5 -0.05 0.00 10 6 6 -0.01 0.00 10 6 7 0.02 0.00 10 6 8 -0.01 0.00 10 6 9 -0.03 0.00 10 6 10 0.10 0.00 10 6 11 -0.14 0.00 10 6 12 0.14 0.00 10 6 13 -0.06 0.00 10 6 14 -0.05 0.00 10 6 15 0.12 0.00 10 6 16 -0.12 0.00 -10 -7 7 0.06 0.00 -10 -7 6 -0.13 0.00 -10 -7 5 0.28 0.00 -10 -7 4 -0.45 0.00 -10 -7 3 0.54 0.00 -10 -7 2 -0.46 0.00 -10 -7 1 0.24 0.00 10 7 0 0.01 0.00 10 7 1 -0.15 0.00 10 7 2 0.11 0.00 10 7 3 0.07 0.00 10 7 4 -0.29 0.00 10 7 5 0.43 0.00 10 7 6 -0.47 0.00 10 7 7 0.39 0.00 10 7 8 -0.23 0.00 10 7 9 0.01 0.00 10 7 10 0.21 0.00 10 7 11 -0.37 0.00 10 7 12 0.43 0.00 10 7 13 -0.39 0.00 10 7 14 0.31 0.00 10 7 15 -0.24 0.00 -10 -8 6 0.10 0.00 -10 -8 5 0.09 0.00 -10 -8 4 -0.36 0.00 -10 -8 3 0.60 0.00 -10 -8 2 -0.71 0.00 -10 -8 1 0.64 0.00 10 8 0 -0.50 0.00 10 8 1 0.41 0.00 10 8 2 -0.44 0.00 10 8 3 0.57 0.00 10 8 4 -0.70 0.00 10 8 5 0.75 0.00 10 8 6 -0.68 0.00 10 8 7 0.52 0.00 10 8 8 -0.29 0.00 10 8 9 0.06 0.00 10 8 10 0.16 0.00 10 8 11 -0.32 0.00 10 8 12 0.43 0.00 10 8 13 -0.49 0.00 10 8 14 0.53 0.00 10 8 15 -0.56 0.00 -10 -9 4 -0.17 0.00 -10 -9 3 0.38 0.00 -10 -9 2 -0.51 0.00 -10 -9 1 0.52 0.00 10 9 0 -0.49 0.00 10 9 1 0.50 0.00 10 9 2 -0.58 0.00 10 9 3 0.69 0.00 10 9 4 -0.72 0.00 10 9 5 0.63 0.00 10 9 6 -0.42 0.00 10 9 7 0.18 0.00 10 9 8 0.02 0.00 10 9 9 -0.16 0.00 10 9 10 0.23 0.00 10 9 11 -0.27 0.00 10 9 12 0.33 0.00 10 9 13 -0.43 0.00 -10 -10 1 0.23 0.00 10 10 0 -0.21 0.00 10 10 1 0.27 0.00 10 10 2 -0.38 0.00 10 10 3 0.47 0.00 10 10 4 -0.44 0.00 10 10 5 0.27 0.00 10 10 6 -0.01 0.00 10 10 7 -0.23 0.00 10 10 8 0.37 0.00 10 10 9 -0.40 0.00 10 10 10 0.36 0.00 10 10 11 -0.32 0.00 -11 2 3 0.08 0.00 -11 2 2 0.03 0.00 -11 2 1 -0.17 0.00 -11 2 0 0.25 0.00 11 -2 1 -0.21 0.00 11 -2 2 0.05 0.00 11 -2 3 0.17 0.00 11 -2 4 -0.33 0.00 -11 1 5 -0.28 0.00 -11 1 4 0.09 0.00 -11 1 3 -0.02 0.00 -11 1 2 0.08 0.00 -11 1 1 -0.21 0.00 -11 1 0 0.30 0.00 11 -1 1 -0.26 0.00 11 -1 2 0.09 0.00 11 -1 3 0.13 0.00 11 -1 4 -0.29 0.00 11 -1 5 0.30 0.00 11 -1 6 -0.19 0.00 11 -1 7 0.03 0.00 -11 0 7 -0.83 0.00 -11 0 6 0.63 0.00 -11 0 5 -0.33 0.00 -11 0 4 0.04 0.00 -11 0 3 0.14 0.00 -11 0 2 -0.17 0.00 -11 0 1 0.10 0.00 11 0 0 -0.03 0.00 11 0 1 0.04 0.00 11 0 2 -0.15 0.00 11 0 3 0.28 0.00 11 0 4 -0.33 0.00 11 0 5 0.26 0.00 11 0 6 -0.09 0.00 11 0 7 -0.09 0.00 11 0 8 0.21 0.00 11 0 9 -0.23 0.00 -11 -1 7 -0.46 0.00 -11 -1 6 0.30 0.00 -11 -1 5 -0.06 0.00 -11 -1 4 -0.21 0.00 -11 -1 3 0.42 0.00 -11 -1 2 -0.54 0.00 -11 -1 1 0.56 0.00 11 1 0 -0.54 0.00 11 1 1 0.56 0.00 11 1 2 -0.61 0.00 11 1 3 0.65 0.00 11 1 4 -0.61 0.00 11 1 5 0.44 0.00 11 1 6 -0.19 0.00 11 1 7 -0.06 0.00 11 1 8 0.22 0.00 11 1 9 -0.28 0.00 11 1 10 0.25 0.00 11 1 11 -0.21 0.00 -11 -2 8 0.03 0.00 -11 -2 7 0.02 0.00 -11 -2 6 -0.10 0.00 -11 -2 5 0.23 0.00 -11 -2 4 -0.38 0.00 -11 -2 3 0.55 0.00 -11 -2 2 -0.67 0.00 -11 -2 1 0.73 0.00 11 2 0 -0.75 0.00 11 2 1 0.77 0.00 11 2 2 -0.81 0.00 11 2 3 0.85 0.00 11 2 4 -0.80 0.00 11 2 5 0.63 0.00 11 2 6 -0.35 0.00 11 2 7 0.06 0.00 11 2 8 0.15 0.00 11 2 9 -0.26 0.00 11 2 10 0.29 0.00 11 2 11 -0.27 0.00 11 2 12 0.24 0.00 -11 -3 8 0.04 0.00 -11 -3 7 0.07 0.00 -11 -3 6 -0.15 0.00 -11 -3 5 0.21 0.00 -11 -3 4 -0.29 0.00 -11 -3 3 0.38 0.00 -11 -3 2 -0.43 0.00 -11 -3 1 0.41 0.00 11 3 0 -0.34 0.00 11 3 1 0.31 0.00 11 3 2 -0.36 0.00 11 3 3 0.46 0.00 11 3 4 -0.52 0.00 11 3 5 0.48 0.00 11 3 6 -0.34 0.00 11 3 7 0.18 0.00 11 3 8 -0.05 0.00 11 3 9 -0.01 0.00 11 3 10 0.03 0.00 11 3 11 -0.07 0.00 11 3 12 0.11 0.00 11 3 13 -0.12 0.00 -11 -4 7 -0.19 0.00 -11 -4 6 0.10 0.00 -11 -4 5 -0.03 0.00 -11 -4 4 -0.05 0.00 -11 -4 3 0.09 0.00 -11 -4 2 -0.05 0.00 -11 -4 1 -0.10 0.00 11 4 0 0.29 0.00 11 4 1 -0.41 0.00 11 4 2 0.38 0.00 11 4 3 -0.23 0.00 11 4 4 0.06 0.00 11 4 5 0.04 0.00 11 4 6 -0.08 0.00 11 4 7 0.11 0.00 11 4 8 -0.20 0.00 11 4 9 0.32 0.00 11 4 10 -0.39 0.00 11 4 11 0.36 0.00 11 4 12 -0.25 0.00 11 4 13 0.11 0.00 -11 -5 6 0.25 0.00 -11 -5 5 -0.17 0.00 -11 -5 4 0.10 0.00 -11 -5 3 -0.07 0.00 -11 -5 2 0.15 0.00 -11 -5 1 -0.35 0.00 11 5 0 0.58 0.00 11 5 1 -0.71 0.00 11 5 2 0.68 0.00 11 5 3 -0.52 0.00 11 5 4 0.35 0.00 11 5 5 -0.25 0.00 11 5 6 0.19 0.00 11 5 7 -0.10 0.00 11 5 8 -0.07 0.00 11 5 9 0.29 0.00 11 5 10 -0.44 0.00 11 5 11 0.47 0.00 11 5 12 -0.37 0.00 11 5 13 0.23 0.00 -11 -6 5 -0.06 0.00 -11 -6 4 0.01 0.00 -11 -6 3 0.01 0.00 -11 -6 2 0.07 0.00 -11 -6 1 -0.26 0.00 11 6 0 0.46 0.00 11 6 1 -0.55 0.00 11 6 2 0.49 0.00 11 6 3 -0.32 0.00 11 6 4 0.17 0.00 11 6 5 -0.12 0.00 11 6 6 0.13 0.00 11 6 7 -0.14 0.00 11 6 8 0.07 0.00 11 6 9 0.03 0.00 11 6 10 -0.12 0.00 11 6 11 0.13 0.00 11 6 12 -0.09 0.00 11 6 13 0.06 0.00 -11 -7 4 -0.20 0.00 -11 -7 3 0.24 0.00 -11 -7 2 -0.19 0.00 -11 -7 1 0.04 0.00 11 7 0 0.14 0.00 11 7 1 -0.22 0.00 11 7 2 0.17 0.00 11 7 3 -0.01 0.00 11 7 4 -0.15 0.00 11 7 5 0.21 0.00 11 7 6 -0.18 0.00 11 7 7 0.11 0.00 11 7 8 -0.05 0.00 11 7 9 -0.01 0.00 11 7 10 0.09 0.00 11 7 11 -0.16 0.00 11 7 12 0.20 0.00 -11 -8 2 -0.38 0.00 -11 -8 1 0.32 0.00 11 8 0 -0.22 0.00 11 8 1 0.16 0.00 11 8 2 -0.21 0.00 11 8 3 0.35 0.00 11 8 4 -0.49 0.00 11 8 5 0.55 0.00 11 8 6 -0.51 0.00 11 8 7 0.40 0.00 11 8 8 -0.25 0.00 11 8 9 0.08 0.00 11 8 10 0.09 0.00 11 8 11 -0.23 0.00 11 9 1 0.33 0.00 11 9 2 -0.44 0.00 11 9 3 0.60 0.00 11 9 4 -0.72 0.00 11 9 5 0.74 0.00 11 9 6 -0.64 0.00 11 9 7 0.46 0.00 11 9 8 -0.25 0.00 11 9 9 0.05 0.00 12 1 0 0.12 0.00 12 1 1 -0.13 0.00 12 1 2 0.05 0.00 12 1 3 0.10 0.00 12 1 4 -0.24 0.00 -12 -2 2 -0.35 0.00 -12 -2 1 0.36 0.00 12 2 0 -0.29 0.00 12 2 1 0.19 0.00 12 2 2 -0.14 0.00 12 2 3 0.12 0.00 12 2 4 -0.11 0.00 12 2 5 0.04 0.00 12 2 6 0.10 0.00 -12 -3 2 -0.65 0.00 -12 -3 1 0.70 0.00 12 3 0 -0.65 0.00 12 3 1 0.52 0.00 12 3 2 -0.39 0.00 12 3 3 0.28 0.00 12 3 4 -0.15 0.00 12 3 5 -0.05 0.00 12 3 6 0.32 0.00 12 3 7 -0.58 0.00 12 3 8 0.71 0.00 -12 -4 2 -0.37 0.00 -12 -4 1 0.40 0.00 12 4 0 -0.34 0.00 12 4 1 0.25 0.00 12 4 2 -0.21 0.00 12 4 3 0.22 0.00 12 4 4 -0.19 0.00 12 4 5 0.04 0.00 12 4 6 0.22 0.00 12 4 7 -0.50 0.00 12 4 8 0.67 0.00 -12 -5 1 -0.16 0.00 12 5 0 0.28 0.00 12 5 1 -0.33 0.00 12 5 2 0.24 0.00 12 5 3 -0.06 0.00 12 5 4 -0.10 0.00 12 5 5 0.12 0.00 12 5 6 0.03 0.00 12 5 7 -0.22 0.00 12 5 8 0.33 0.00 12 6 0 0.39 0.00 12 6 1 -0.44 0.00 12 6 2 0.31 0.00 12 6 3 -0.08 0.00 12 6 4 -0.13 0.00 12 6 5 0.18 0.00 12 6 6 -0.08 0.00 12 6 7 -0.08 0.00 12 6 8 0.16 0.00 12 7 4 -0.39 0.00 12 7 5 0.40 0.00 1 0 0 26.43 0.00 12 0 0 0.12 0.00 -12 1 0 -0.07 0.00 0 1 0 38.24 0.00 2 1 0 7.44 0.00 13 1 0 0.06 0.00 -12 2 0 -0.15 0.00 13 2 0 -0.04 0.00 -11 3 0 0.10 0.00 13 3 0 -0.38 0.00 -11 4 0 0.12 0.00 13 4 0 -0.54 0.00 -10 5 0 0.36 0.00 13 5 0 -0.21 0.00 -10 6 0 0.20 0.00 -9 6 0 0.06 0.00 13 6 0 0.20 0.00 -9 7 0 -0.26 0.00 -8 7 0 0.07 0.00 12 7 0 0.13 0.00 13 7 0 0.20 0.00 -8 8 0 -0.14 0.00 -7 8 0 0.64 0.00 -6 8 0 0.17 0.00 12 8 0 0.04 0.00 -7 9 0 0.29 0.00 -6 9 0 0.50 0.00 11 9 0 -0.29 0.00 12 9 0 0.07 0.00 -6 10 0 0.12 0.00 -5 10 0 0.04 0.00 11 10 0 0.00 0.00 -5 11 0 -0.03 0.00 -4 11 0 -0.10 0.00 10 11 0 0.03 0.00 11 11 0 0.19 0.00 -4 12 0 -0.09 0.00 -3 12 0 -0.17 0.00 9 12 0 0.16 0.00 10 12 0 0.13 0.00 -2 13 0 -0.04 0.00 -1 13 0 0.20 0.00 0 13 0 0.23 0.00 6 13 0 -0.51 0.00 7 13 0 0.11 0.00 8 13 0 0.08 0.00 9 13 0 0.04 0.00 0 14 0 0.13 0.00 1 14 0 -0.22 0.00 2 14 0 -0.21 0.00 3 14 0 0.37 0.00 4 14 0 0.10 0.00 5 14 0 -0.35 0.00 6 14 0 -0.23 0.00 7 14 0 0.06 0.00 -6 -14 1 0.22 0.00 -5 -14 1 0.32 0.00 -4 -14 1 -0.10 0.00 -3 -14 1 -0.33 0.00 -2 -14 1 0.20 0.00 -1 -14 1 0.26 0.00 -8 -13 1 -0.14 0.00 -7 -13 1 -0.13 0.00 -6 -13 1 0.56 0.00 -1 -13 1 0.24 0.00 0 -13 1 -0.14 0.00 1 -13 1 -0.16 0.00 2 -13 1 -0.01 0.00 -10 -12 1 -0.18 0.00 -9 -12 1 -0.28 0.00 -8 -12 1 -0.03 0.00 2 -12 1 -0.03 0.00 3 -12 1 0.11 0.00 4 -12 1 0.09 0.00 -11 -11 1 -0.12 0.00 -10 -11 1 -0.03 0.00 4 -11 1 0.05 0.00 5 -11 1 -0.02 0.00 -11 -10 1 -0.02 0.00 5 -10 1 -0.13 0.00 6 -10 1 -0.22 0.00 -12 -9 1 -0.02 0.00 -11 -9 1 0.27 0.00 6 -9 1 -0.65 0.00 7 -9 1 -0.43 0.00 -12 -8 1 0.02 0.00 7 -8 1 -0.86 0.00 8 -8 1 0.00 0.00 -13 -7 1 -0.08 0.00 -12 -7 1 -0.02 0.00 8 -7 1 -0.13 0.00 9 -7 1 0.29 0.00 -13 -6 1 -0.10 0.00 -12 -6 1 -0.24 0.00 9 -6 1 0.09 0.00 10 -6 1 -0.10 0.00 -13 -5 1 0.26 0.00 10 -5 1 -0.30 0.00 -13 -4 1 0.58 0.00 11 -4 1 -0.17 0.00 -13 -3 1 0.42 0.00 11 -3 1 -0.11 0.00 -13 -2 1 0.09 0.00 0 -2 1 -13.40 0.00 12 -2 1 0.12 0.00 -13 -1 1 0.00 0.00 -12 -1 1 -0.06 0.00 -1 -1 1 -33.43 0.00 0 -1 1 -34.82 0.00 1 -1 1 -8.54 0.00 2 -1 1 0.83 0.00 12 -1 1 0.08 0.00 -12 0 1 -0.08 0.00 -2 0 1 2.92 0.00 -1 0 1 -24.15 0.00 1 0 1 -25.73 0.00 2 0 1 -1.81 0.00 12 0 1 -0.10 0.00 -12 1 1 0.12 0.00 0 1 1 -37.92 0.00 1 1 1 -36.62 0.00 13 1 1 -0.11 0.00 -12 2 1 0.21 0.00 1 2 1 -32.07 0.00 13 2 1 -0.03 0.00 -11 3 1 0.00 0.00 1 3 1 -17.29 0.00 13 3 1 0.26 0.00 -11 4 1 -0.01 0.00 13 4 1 0.43 0.00 -10 5 1 -0.31 0.00 13 5 1 0.14 0.00 -10 6 1 -0.22 0.00 -9 6 1 -0.16 0.00 13 6 1 -0.25 0.00 -9 7 1 0.19 0.00 -8 7 1 -0.07 0.00 -7 7 1 -0.31 0.00 12 7 1 -0.14 0.00 13 7 1 -0.24 0.00 -8 8 1 0.22 0.00 -7 8 1 -0.47 0.00 -6 8 1 -0.07 0.00 12 8 1 -0.02 0.00 -8 9 1 0.13 0.00 -7 9 1 -0.18 0.00 -6 9 1 -0.37 0.00 -5 9 1 0.19 0.00 12 9 1 -0.06 0.00 -7 10 1 0.06 0.00 -6 10 1 -0.08 0.00 -5 10 1 0.02 0.00 11 10 1 0.07 0.00 12 10 1 -0.05 0.00 -5 11 1 0.05 0.00 -4 11 1 0.10 0.00 10 11 1 0.07 0.00 11 11 1 -0.19 0.00 -4 12 1 0.06 0.00 -3 12 1 0.17 0.00 9 12 1 0.02 0.00 10 12 1 -0.01 0.00 -2 13 1 0.09 0.00 -1 13 1 -0.21 0.00 0 13 1 -0.29 0.00 7 13 1 -0.09 0.00 8 13 1 -0.05 0.00 9 13 1 0.01 0.00 0 14 1 -0.21 0.00 1 14 1 0.14 0.00 2 14 1 0.15 0.00 3 14 1 -0.42 0.00 4 14 1 -0.11 0.00 5 14 1 0.35 0.00 6 14 1 0.24 0.00 7 14 1 -0.03 0.00 -6 -14 2 -0.22 0.00 -5 -14 2 -0.26 0.00 -4 -14 2 0.08 0.00 -3 -14 2 0.27 0.00 -2 -14 2 -0.15 0.00 -1 -14 2 -0.25 0.00 -8 -13 2 0.19 0.00 -7 -13 2 0.12 0.00 -6 -13 2 -0.60 0.00 -5 -13 2 -0.99 0.00 -4 -13 2 -0.38 0.00 -3 -13 2 0.58 0.00 -2 -13 2 0.36 0.00 -1 -13 2 -0.23 0.00 0 -13 2 0.06 0.00 1 -13 2 0.07 0.00 2 -13 2 0.03 0.00 -9 -12 2 0.31 0.00 -8 -12 2 0.14 0.00 2 -12 2 0.03 0.00 3 -12 2 -0.05 0.00 4 -12 2 -0.08 0.00 -10 -11 2 -0.03 0.00 -9 -11 2 0.11 0.00 4 -11 2 0.00 0.00 5 -11 2 0.09 0.00 -11 -10 2 0.04 0.00 -10 -10 2 -0.26 0.00 5 -10 2 0.21 0.00 6 -10 2 0.31 0.00 -12 -9 2 -0.02 0.00 -11 -9 2 -0.22 0.00 6 -9 2 0.75 0.00 7 -9 2 0.53 0.00 -12 -8 2 -0.09 0.00 7 -8 2 1.04 0.00 8 -8 2 0.15 0.00 -12 -7 2 -0.10 0.00 8 -7 2 0.22 0.00 9 -7 2 -0.28 0.00 -13 -6 2 0.03 0.00 -12 -6 2 0.09 0.00 9 -6 2 -0.25 0.00 10 -6 2 -0.02 0.00 -13 -5 2 -0.24 0.00 -12 -5 2 0.08 0.00 10 -5 2 0.14 0.00 -13 -4 2 -0.51 0.00 11 -4 2 0.15 0.00 -13 -3 2 -0.37 0.00 11 -3 2 0.03 0.00 -13 -2 2 -0.09 0.00 1 -2 2 -2.69 0.00 12 -2 2 -0.15 0.00 -13 -1 2 -0.01 0.00 -12 -1 2 0.04 0.00 0 -1 2 28.43 0.00 12 -1 2 -0.19 0.00 -12 0 2 0.05 0.00 0 0 2 40.36 0.00 1 0 2 22.18 0.00 12 0 2 -0.04 0.00 -12 1 2 -0.17 0.00 2 1 2 8.62 0.00 13 1 2 0.11 0.00 -12 2 2 -0.26 0.00 -1 2 2 -3.91 0.00 13 2 2 0.07 0.00 -11 3 2 -0.14 0.00 1 3 2 16.86 0.00 13 3 2 -0.15 0.00 -11 4 2 -0.12 0.00 13 4 2 -0.29 0.00 -10 5 2 0.15 0.00 13 5 2 -0.11 0.00 -10 6 2 0.16 0.00 -9 6 2 0.17 0.00 13 6 2 0.18 0.00 -9 7 2 -0.12 0.00 -8 7 2 0.12 0.00 -7 7 2 0.30 0.00 -6 7 2 -0.32 0.00 -5 7 2 -0.18 0.00 12 7 2 0.01 0.00 13 7 2 0.16 0.00 -8 8 2 -0.21 0.00 -7 8 2 0.39 0.00 -6 8 2 0.06 0.00 -5 8 2 -0.27 0.00 12 8 2 -0.13 0.00 13 8 2 -0.04 0.00 -8 9 2 -0.15 0.00 -7 9 2 0.15 0.00 -6 9 2 0.32 0.00 -5 9 2 -0.17 0.00 12 9 2 -0.05 0.00 -7 10 2 -0.05 0.00 -6 10 2 0.11 0.00 -5 10 2 -0.01 0.00 11 10 2 -0.22 0.00 12 10 2 0.00 0.00 -5 11 2 0.00 0.00 -4 11 2 -0.03 0.00 10 11 2 -0.21 0.00 11 11 2 0.11 0.00 -4 12 2 0.01 0.00 -3 12 2 -0.05 0.00 9 12 2 -0.19 0.00 10 12 2 -0.13 0.00 -3 13 2 -0.09 0.00 -2 13 2 -0.08 0.00 -1 13 2 0.19 0.00 7 13 2 0.08 0.00 8 13 2 0.06 0.00 9 13 2 -0.03 0.00 0 14 2 0.27 0.00 1 14 2 -0.05 0.00 2 14 2 -0.04 0.00 3 14 2 0.49 0.00 4 14 2 0.13 0.00 5 14 2 -0.30 0.00 6 14 2 -0.23 0.00 7 14 2 -0.02 0.00 -5 -14 3 0.20 0.00 -4 -14 3 -0.05 0.00 -3 -14 3 -0.19 0.00 -2 -14 3 0.09 0.00 -8 -13 3 -0.21 0.00 -7 -13 3 -0.09 0.00 -6 -13 3 0.61 0.00 -5 -13 3 0.91 0.00 -4 -13 3 0.37 0.00 -3 -13 3 -0.45 0.00 -2 -13 3 -0.32 0.00 -1 -13 3 0.17 0.00 0 -13 3 -0.02 0.00 1 -13 3 0.04 0.00 -9 -12 3 -0.27 0.00 -8 -12 3 -0.23 0.00 -7 -12 3 -0.39 0.00 2 -12 3 0.00 0.00 3 -12 3 0.00 0.00 -10 -11 3 0.08 0.00 -9 -11 3 -0.09 0.00 4 -11 3 -0.05 0.00 5 -11 3 -0.12 0.00 -11 -10 3 -0.09 0.00 -10 -10 3 0.24 0.00 5 -10 3 -0.25 0.00 6 -10 3 -0.35 0.00 -11 -9 3 0.09 0.00 6 -9 3 -0.75 0.00 7 -9 3 -0.53 0.00 -12 -8 3 0.12 0.00 -11 -8 3 0.32 0.00 7 -8 3 -1.08 0.00 8 -8 3 -0.25 0.00 -12 -7 3 0.16 0.00 8 -7 3 -0.31 0.00 9 -7 3 0.22 0.00 -12 -6 3 0.00 0.00 9 -6 3 0.35 0.00 10 -6 3 0.13 0.00 -13 -5 3 0.16 0.00 -12 -5 3 -0.06 0.00 10 -5 3 0.05 0.00 -13 -4 3 0.37 0.00 -12 -4 3 0.26 0.00 11 -4 3 -0.08 0.00 -13 -3 3 0.27 0.00 -12 -3 3 0.49 0.00 11 -3 3 0.09 0.00 -13 -2 3 0.04 0.00 -12 -2 3 0.25 0.00 -2 -2 3 -6.46 0.00 12 -2 3 0.22 0.00 -12 -1 3 -0.10 0.00 -1 -1 3 -20.31 0.00 2 -1 3 -0.93 0.00 12 -1 3 0.36 0.00 -12 0 3 -0.08 0.00 2 0 3 -3.17 0.00 3 0 3 -2.84 0.00 12 0 3 0.26 0.00 -12 1 3 0.16 0.00 -1 1 3 -2.53 0.00 13 1 3 -0.03 0.00 -12 2 3 0.27 0.00 13 2 3 -0.04 0.00 -11 3 3 0.25 0.00 1 3 3 -15.17 0.00 13 3 3 0.07 0.00 -11 4 3 0.22 0.00 13 4 3 0.19 0.00 -10 5 3 0.05 0.00 13 5 3 0.14 0.00 -10 6 3 -0.04 0.00 -9 6 3 -0.08 0.00 13 6 3 -0.01 0.00 -9 7 3 0.10 0.00 -8 7 3 -0.17 0.00 -7 7 3 -0.33 0.00 -6 7 3 0.09 0.00 -5 7 3 -0.09 0.00 12 7 3 0.21 0.00 13 7 3 0.03 0.00 -8 8 3 0.17 0.00 -7 8 3 -0.39 0.00 -6 8 3 -0.12 0.00 -5 8 3 0.08 0.00 12 8 3 0.35 0.00 13 8 3 0.21 0.00 -8 9 3 0.15 0.00 -7 9 3 -0.19 0.00 -6 9 3 -0.35 0.00 -5 9 3 0.09 0.00 12 9 3 0.24 0.00 -7 10 3 0.02 0.00 -6 10 3 -0.19 0.00 -5 10 3 -0.04 0.00 -4 10 3 -0.16 0.00 11 10 3 0.39 0.00 12 10 3 0.11 0.00 -5 11 3 -0.07 0.00 -4 11 3 -0.10 0.00 10 11 3 0.31 0.00 11 11 3 0.01 0.00 -4 12 3 -0.11 0.00 -3 12 3 -0.19 0.00 9 12 3 0.30 0.00 10 12 3 0.23 0.00 -3 13 3 0.00 0.00 -2 13 3 -0.05 0.00 -1 13 3 -0.20 0.00 7 13 3 -0.11 0.00 8 13 3 -0.12 0.00 9 13 3 0.03 0.00 0 14 3 -0.31 0.00 1 14 3 -0.02 0.00 2 14 3 -0.09 0.00 3 14 3 -0.59 0.00 4 14 3 -0.17 0.00 5 14 3 0.20 0.00 6 14 3 0.18 0.00 7 14 3 0.05 0.00 8 14 3 -0.13 0.00 -7 -13 4 0.06 0.00 -6 -13 4 -0.56 0.00 -5 -13 4 -0.76 0.00 -4 -13 4 -0.33 0.00 -3 -13 4 0.30 0.00 -2 -13 4 0.26 0.00 -1 -13 4 -0.07 0.00 0 -13 4 0.02 0.00 1 -13 4 -0.12 0.00 -9 -12 4 0.22 0.00 -8 -12 4 0.30 0.00 -7 -12 4 0.45 0.00 1 -12 4 0.42 0.00 2 -12 4 -0.04 0.00 3 -12 4 0.03 0.00 -10 -11 4 -0.09 0.00 -9 -11 4 0.08 0.00 3 -11 4 -0.14 0.00 4 -11 4 0.08 0.00 5 -11 4 0.12 0.00 -11 -10 4 0.16 0.00 -10 -10 4 -0.16 0.00 5 -10 4 0.25 0.00 6 -10 4 0.32 0.00 -11 -9 4 0.06 0.00 6 -9 4 0.68 0.00 7 -9 4 0.43 0.00 -12 -8 4 -0.12 0.00 -11 -8 4 -0.21 0.00 7 -8 4 0.98 0.00 8 -8 4 0.25 0.00 -12 -7 4 -0.17 0.00 8 -7 4 0.35 0.00 9 -7 4 -0.14 0.00 -12 -6 4 -0.03 0.00 9 -6 4 -0.38 0.00 10 -6 4 -0.19 0.00 -12 -5 4 0.07 0.00 10 -5 4 -0.22 0.00 -13 -4 4 -0.23 0.00 -12 -4 4 -0.13 0.00 11 -4 4 0.01 0.00 -13 -3 4 -0.17 0.00 -12 -3 4 -0.31 0.00 11 -3 4 -0.20 0.00 -12 -2 4 -0.10 0.00 -9 -2 4 -0.52 0.00 -1 -2 4 10.07 0.00 12 -2 4 -0.28 0.00 -12 -1 4 0.21 0.00 12 -1 4 -0.52 0.00 -12 0 4 0.19 0.00 12 0 4 -0.46 0.00 -12 1 4 -0.08 0.00 -1 1 4 0.04 0.00 2 1 4 5.22 0.00 13 1 4 -0.08 0.00 -12 2 4 -0.23 0.00 -11 2 4 -0.10 0.00 -1 2 4 -5.36 0.00 0 2 4 10.47 0.00 13 2 4 -0.02 0.00 -11 3 4 -0.30 0.00 13 3 4 -0.02 0.00 -11 4 4 -0.28 0.00 13 4 4 -0.09 0.00 -10 5 4 -0.24 0.00 13 5 4 -0.17 0.00 -10 6 4 -0.10 0.00 -9 6 4 -0.09 0.00 13 6 4 -0.17 0.00 -9 7 4 -0.15 0.00 -8 7 4 0.14 0.00 -7 7 4 0.31 0.00 -6 7 4 0.08 0.00 -5 7 4 0.25 0.00 13 7 4 -0.21 0.00 -8 8 4 -0.13 0.00 -7 8 4 0.39 0.00 -6 8 4 0.18 0.00 -5 8 4 0.10 0.00 12 8 4 -0.54 0.00 13 8 4 -0.36 0.00 -8 9 4 -0.15 0.00 -7 9 4 0.23 0.00 -6 9 4 0.37 0.00 -5 9 4 0.00 0.00 12 9 4 -0.42 0.00 -7 10 4 0.01 0.00 -6 10 4 0.26 0.00 -5 10 4 0.08 0.00 -4 10 4 0.28 0.00 11 10 4 -0.51 0.00 12 10 4 -0.23 0.00 -5 11 4 0.11 0.00 -4 11 4 0.22 0.00 10 11 4 -0.30 0.00 11 11 4 -0.08 0.00 -4 12 4 0.19 0.00 -3 12 4 0.50 0.00 9 12 4 -0.33 0.00 10 12 4 -0.25 0.00 -3 13 4 0.13 0.00 -2 13 4 0.29 0.00 -1 13 4 0.27 0.00 8 13 4 0.19 0.00 9 13 4 -0.01 0.00 -1 14 4 0.10 0.00 0 14 4 0.32 0.00 1 14 4 0.04 0.00 2 14 4 0.20 0.00 3 14 4 0.68 0.00 4 14 4 0.21 0.00 5 14 4 -0.08 0.00 6 14 4 -0.11 0.00 7 14 4 -0.06 0.00 8 14 4 0.19 0.00 -6 -13 5 0.46 0.00 -5 -13 5 0.55 0.00 -4 -13 5 0.24 0.00 -3 -13 5 -0.15 0.00 -2 -13 5 -0.17 0.00 -1 -13 5 -0.01 0.00 0 -13 5 -0.04 0.00 -8 -12 5 -0.35 0.00 -7 -12 5 -0.48 0.00 -6 -12 5 0.46 0.00 0 -12 5 -0.62 0.00 1 -12 5 -0.39 0.00 2 -12 5 0.06 0.00 3 -12 5 -0.06 0.00 -9 -11 5 -0.09 0.00 -8 -11 5 -0.05 0.00 3 -11 5 0.08 0.00 4 -11 5 -0.12 0.00 -10 -10 5 0.07 0.00 -9 -10 5 0.26 0.00 5 -10 5 -0.26 0.00 6 -10 5 -0.25 0.00 -11 -9 5 -0.16 0.00 -10 -9 5 -0.04 0.00 6 -9 5 -0.58 0.00 7 -9 5 -0.28 0.00 -11 -8 5 0.10 0.00 7 -8 5 -0.80 0.00 8 -8 5 -0.19 0.00 -12 -7 5 0.16 0.00 -11 -7 5 0.14 0.00 8 -7 5 -0.34 0.00 9 -7 5 0.06 0.00 -12 -6 5 0.04 0.00 9 -6 5 0.31 0.00 -12 -5 5 -0.08 0.00 10 -5 5 0.28 0.00 -12 -4 5 0.04 0.00 10 -4 5 0.15 0.00 11 -4 5 0.03 0.00 -12 -3 5 0.17 0.00 11 -3 5 0.23 0.00 -12 -2 5 -0.04 0.00 11 -2 5 0.37 0.00 12 -2 5 0.28 0.00 -12 -1 5 -0.34 0.00 12 -1 5 0.56 0.00 -12 0 5 -0.31 0.00 12 0 5 0.55 0.00 -12 1 5 -0.02 0.00 12 1 5 0.31 0.00 13 1 5 0.16 0.00 -12 2 5 0.16 0.00 -11 2 5 0.04 0.00 -2 2 5 4.58 0.00 13 2 5 0.07 0.00 -11 3 5 0.30 0.00 13 3 5 -0.05 0.00 -11 4 5 0.28 0.00 -10 4 5 0.27 0.00 13 4 5 -0.06 0.00 -10 5 5 0.37 0.00 13 5 5 0.10 0.00 -10 6 5 0.21 0.00 -9 6 5 0.29 0.00 13 6 5 0.21 0.00 -9 7 5 0.24 0.00 -8 7 5 -0.01 0.00 -7 7 5 -0.19 0.00 -6 7 5 -0.14 0.00 13 7 5 0.26 0.00 -8 8 5 0.13 0.00 -7 8 5 -0.31 0.00 -6 8 5 -0.18 0.00 -5 8 5 -0.20 0.00 12 8 5 0.59 0.00 13 8 5 0.39 0.00 -7 9 5 -0.24 0.00 -6 9 5 -0.34 0.00 -5 9 5 -0.07 0.00 12 9 5 0.53 0.00 -7 10 5 -0.02 0.00 -6 10 5 -0.28 0.00 -5 10 5 -0.06 0.00 -4 10 5 -0.35 0.00 11 10 5 0.52 0.00 12 10 5 0.31 0.00 -5 11 5 -0.06 0.00 -4 11 5 -0.25 0.00 10 11 5 0.16 0.00 11 11 5 0.08 0.00 -4 12 5 -0.19 0.00 -3 12 5 -0.77 0.00 9 12 5 0.31 0.00 10 12 5 0.21 0.00 -3 13 5 -0.26 0.00 -2 13 5 -0.58 0.00 -1 13 5 -0.40 0.00 8 13 5 -0.22 0.00 9 13 5 0.02 0.00 -1 14 5 -0.21 0.00 0 14 5 -0.32 0.00 1 14 5 0.00 0.00 2 14 5 -0.27 0.00 3 14 5 -0.73 0.00 4 14 5 -0.22 0.00 5 14 5 -0.03 0.00 6 14 5 0.05 0.00 7 14 5 0.06 0.00 8 14 5 -0.24 0.00 -6 -13 6 -0.34 0.00 -5 -13 6 -0.33 0.00 -4 -13 6 -0.14 0.00 -3 -13 6 0.03 0.00 -2 -13 6 0.08 0.00 -1 -13 6 0.06 0.00 -8 -12 6 0.35 0.00 -7 -12 6 0.45 0.00 -6 -12 6 -0.38 0.00 -5 -12 6 -1.10 0.00 -1 -12 6 0.19 0.00 0 -12 6 0.62 0.00 1 -12 6 0.36 0.00 2 -12 6 -0.04 0.00 -9 -11 6 0.09 0.00 -8 -11 6 0.19 0.00 3 -11 6 0.04 0.00 4 -11 6 0.19 0.00 -10 -10 6 -0.04 0.00 -9 -10 6 -0.17 0.00 4 -10 6 -0.02 0.00 5 -10 6 0.28 0.00 -11 -9 6 0.17 0.00 -10 -9 6 0.15 0.00 6 -9 6 0.50 0.00 7 -9 6 0.15 0.00 -11 -8 6 -0.05 0.00 7 -8 6 0.60 0.00 8 -8 6 0.11 0.00 -12 -7 6 -0.16 0.00 -11 -7 6 -0.12 0.00 8 -7 6 0.31 0.00 -12 -6 6 -0.06 0.00 -11 -6 6 0.10 0.00 9 -6 6 -0.17 0.00 -12 -5 6 0.07 0.00 10 -5 6 -0.24 0.00 -12 -4 6 0.01 0.00 10 -4 6 -0.16 0.00 11 -4 6 -0.02 0.00 -12 -3 6 -0.07 0.00 11 -3 6 -0.17 0.00 -12 -2 6 0.13 0.00 11 -2 6 -0.29 0.00 12 -2 6 -0.21 0.00 -12 -1 6 0.41 0.00 12 -1 6 -0.49 0.00 -12 0 6 0.38 0.00 12 0 6 -0.50 0.00 -12 1 6 0.09 0.00 -11 1 6 0.49 0.00 12 1 6 -0.26 0.00 13 1 6 -0.16 0.00 -11 2 6 0.05 0.00 13 2 6 -0.05 0.00 -11 3 6 -0.26 0.00 13 3 6 0.16 0.00 -11 4 6 -0.24 0.00 -10 4 6 -0.32 0.00 13 4 6 0.27 0.00 -10 5 6 -0.42 0.00 13 5 6 0.11 0.00 -10 6 6 -0.24 0.00 -9 6 6 -0.44 0.00 13 6 6 -0.08 0.00 -9 7 6 -0.30 0.00 -8 7 6 -0.17 0.00 -7 7 6 -0.05 0.00 12 7 6 -0.27 0.00 13 7 6 -0.15 0.00 -8 8 6 -0.16 0.00 -7 8 6 0.14 0.00 -6 8 6 0.07 0.00 -5 8 6 0.22 0.00 12 8 6 -0.51 0.00 13 8 6 -0.28 0.00 -7 9 6 0.20 0.00 -6 9 6 0.22 0.00 -5 9 6 0.08 0.00 12 9 6 -0.53 0.00 -6 10 6 0.22 0.00 -5 10 6 -0.05 0.00 -4 10 6 0.30 0.00 11 10 6 -0.41 0.00 12 10 6 -0.32 0.00 -5 11 6 -0.08 0.00 -4 11 6 0.12 0.00 10 11 6 0.02 0.00 11 11 6 -0.02 0.00 -4 12 6 0.07 0.00 -3 12 6 0.87 0.00 9 12 6 -0.28 0.00 10 12 6 -0.15 0.00 11 12 6 0.13 0.00 -3 13 6 0.31 0.00 -2 13 6 0.82 0.00 -1 13 6 0.53 0.00 8 13 6 0.21 0.00 9 13 6 -0.06 0.00 -1 14 6 0.31 0.00 0 14 6 0.28 0.00 1 14 6 -0.09 0.00 2 14 6 0.27 0.00 3 14 6 0.71 0.00 4 14 6 0.18 0.00 5 14 6 0.06 0.00 6 14 6 -0.04 0.00 7 14 6 -0.08 0.00 8 14 6 0.26 0.00 -4 -13 7 0.06 0.00 -3 -13 7 0.06 0.00 -2 -13 7 0.00 0.00 -7 -12 7 -0.35 0.00 -6 -12 7 0.30 0.00 -5 -12 7 0.85 0.00 -4 -12 7 0.69 0.00 -3 -12 7 0.29 0.00 -2 -12 7 0.06 0.00 -1 -12 7 -0.08 0.00 0 -12 7 -0.56 0.00 1 -12 7 -0.33 0.00 2 -12 7 -0.01 0.00 -9 -11 7 -0.05 0.00 -8 -11 7 -0.24 0.00 -7 -11 7 -0.78 0.00 2 -11 7 -0.23 0.00 3 -11 7 -0.18 0.00 4 -11 7 -0.26 0.00 -10 -10 7 0.07 0.00 -9 -10 7 0.17 0.00 4 -10 7 -0.17 0.00 5 -10 7 -0.32 0.00 -10 -9 7 -0.15 0.00 6 -9 7 -0.45 0.00 -11 -8 7 0.05 0.00 -10 -8 7 -0.17 0.00 7 -8 7 -0.45 0.00 -11 -7 7 0.13 0.00 8 -7 7 -0.27 0.00 -12 -6 7 0.06 0.00 -11 -6 7 -0.10 0.00 9 -6 7 0.01 0.00 -12 -5 7 -0.07 0.00 -11 -5 7 -0.30 0.00 9 -5 7 0.13 0.00 10 -5 7 0.14 0.00 -12 -4 7 -0.05 0.00 10 -4 7 0.10 0.00 -12 -3 7 0.01 0.00 11 -3 7 0.06 0.00 -12 -2 7 -0.16 0.00 11 -2 7 0.14 0.00 -12 -1 7 -0.40 0.00 12 -1 7 0.33 0.00 -12 0 7 -0.35 0.00 12 0 7 0.38 0.00 -12 1 7 -0.09 0.00 -11 1 7 -0.63 0.00 12 1 7 0.17 0.00 -11 2 7 -0.12 0.00 12 2 7 -0.24 0.00 13 2 7 -0.01 0.00 -11 3 7 0.21 0.00 13 3 7 -0.29 0.00 -10 4 7 0.33 0.00 13 4 7 -0.49 0.00 -10 5 7 0.40 0.00 13 5 7 -0.36 0.00 -9 6 7 0.52 0.00 13 6 7 -0.13 0.00 -9 7 7 0.30 0.00 -8 7 7 0.34 0.00 -7 7 7 0.34 0.00 12 7 7 0.08 0.00 13 7 7 -0.04 0.00 -8 8 7 0.18 0.00 -7 8 7 0.08 0.00 -6 8 7 0.11 0.00 12 8 7 0.35 0.00 13 8 7 0.10 0.00 -7 9 7 -0.13 0.00 -6 9 7 -0.05 0.00 -5 9 7 -0.04 0.00 12 9 7 0.44 0.00 -6 10 7 -0.12 0.00 -5 10 7 0.18 0.00 -4 10 7 -0.16 0.00 11 10 7 0.24 0.00 12 10 7 0.28 0.00 -5 11 7 0.26 0.00 -4 11 7 0.11 0.00 10 11 7 -0.18 0.00 11 11 7 -0.06 0.00 -4 12 7 0.15 0.00 -3 12 7 -0.74 0.00 9 12 7 0.27 0.00 10 12 7 0.11 0.00 -3 13 7 -0.26 0.00 -2 13 7 -0.90 0.00 -1 13 7 -0.59 0.00 8 13 7 -0.13 0.00 9 13 7 0.12 0.00 -1 14 7 -0.36 0.00 0 14 7 -0.20 0.00 1 14 7 0.21 0.00 2 14 7 -0.21 0.00 3 14 7 -0.65 0.00 4 14 7 -0.08 0.00 5 14 7 -0.02 0.00 6 14 7 0.09 0.00 7 14 7 0.14 0.00 8 14 7 -0.23 0.00 -6 -12 8 -0.24 0.00 -5 -12 8 -0.64 0.00 -4 -12 8 -0.55 0.00 -3 -12 8 -0.37 0.00 -2 -12 8 -0.24 0.00 -1 -12 8 -0.01 0.00 0 -12 8 0.43 0.00 1 -12 8 0.27 0.00 -8 -11 8 0.19 0.00 -7 -11 8 0.68 0.00 -6 -11 8 0.29 0.00 1 -11 8 0.85 0.00 2 -11 8 0.24 0.00 3 -11 8 0.29 0.00 -9 -10 8 -0.22 0.00 -8 -10 8 -0.30 0.00 3 -10 8 -0.04 0.00 4 -10 8 0.33 0.00 5 -10 8 0.32 0.00 -10 -9 8 0.10 0.00 -9 -9 8 -0.07 0.00 5 -9 8 0.47 0.00 6 -9 8 0.42 0.00 -11 -8 8 -0.06 0.00 -10 -8 8 0.17 0.00 6 -8 8 0.76 0.00 7 -8 8 0.34 0.00 -11 -7 8 -0.14 0.00 -10 -7 8 -0.05 0.00 8 -7 8 0.21 0.00 -11 -6 8 0.09 0.00 8 -6 8 0.34 0.00 9 -6 8 0.10 0.00 -12 -5 8 0.10 0.00 -11 -5 8 0.36 0.00 9 -5 8 0.01 0.00 10 -5 8 -0.04 0.00 -12 -4 8 0.09 0.00 -11 -4 8 0.32 0.00 10 -4 8 -0.02 0.00 -12 -3 8 0.03 0.00 11 -3 8 0.03 0.00 -12 -2 8 0.15 0.00 11 -2 8 0.00 0.00 -12 -1 8 0.30 0.00 -11 -1 8 0.47 0.00 11 -1 8 0.10 0.00 12 -1 8 -0.18 0.00 -12 0 8 0.21 0.00 -11 0 8 0.84 0.00 12 0 8 -0.25 0.00 -11 1 8 0.64 0.00 12 1 8 -0.10 0.00 -11 2 8 0.14 0.00 12 2 8 0.30 0.00 13 2 8 0.06 0.00 -11 3 8 -0.17 0.00 -10 3 8 -0.10 0.00 13 3 8 0.35 0.00 -10 4 8 -0.33 0.00 13 4 8 0.61 0.00 -10 5 8 -0.33 0.00 13 5 8 0.53 0.00 -9 6 8 -0.50 0.00 13 6 8 0.29 0.00 -9 7 8 -0.24 0.00 -8 7 8 -0.44 0.00 12 7 8 0.05 0.00 13 7 8 0.18 0.00 -8 8 8 -0.18 0.00 -7 8 8 -0.28 0.00 -6 8 8 -0.26 0.00 12 8 8 -0.19 0.00 -7 9 8 0.06 0.00 -6 9 8 -0.09 0.00 -5 9 8 0.04 0.00 12 9 8 -0.31 0.00 -6 10 8 0.04 0.00 -5 10 8 -0.23 0.00 11 10 8 -0.07 0.00 12 10 8 -0.19 0.00 -5 11 8 -0.39 0.00 -4 11 8 -0.35 0.00 10 11 8 0.26 0.00 11 11 8 0.11 0.00 -4 12 8 -0.39 0.00 -3 12 8 0.41 0.00 -2 12 8 1.11 0.00 9 12 8 -0.25 0.00 10 12 8 -0.08 0.00 -2 13 8 0.79 0.00 -1 13 8 0.53 0.00 8 13 8 0.03 0.00 9 13 8 -0.18 0.00 0 14 8 0.10 0.00 1 14 8 -0.32 0.00 2 14 8 0.14 0.00 3 14 8 0.57 0.00 4 14 8 -0.03 0.00 5 14 8 -0.06 0.00 6 14 8 -0.19 0.00 7 14 8 -0.24 0.00 8 14 8 0.15 0.00 -6 -12 9 0.18 0.00 -5 -12 9 0.47 0.00 -4 -12 9 0.46 0.00 -3 -12 9 0.42 0.00 -2 -12 9 0.33 0.00 -1 -12 9 0.07 0.00 0 -12 9 -0.26 0.00 -8 -11 9 -0.09 0.00 -7 -11 9 -0.47 0.00 -6 -11 9 -0.23 0.00 -5 -11 9 0.62 0.00 -4 -11 9 0.94 0.00 0 -11 9 -0.35 0.00 1 -11 9 -0.61 0.00 2 -11 9 -0.21 0.00 3 -11 9 -0.32 0.00 -9 -10 9 0.27 0.00 -8 -10 9 0.33 0.00 -7 -10 9 -0.34 0.00 3 -10 9 -0.08 0.00 4 -10 9 -0.38 0.00 -10 -9 9 -0.06 0.00 -9 -9 9 0.11 0.00 5 -9 9 -0.50 0.00 6 -9 9 -0.35 0.00 -10 -8 9 -0.14 0.00 -9 -8 9 -0.51 0.00 6 -8 9 -0.75 0.00 7 -8 9 -0.26 0.00 -11 -7 9 0.13 0.00 -10 -7 9 0.07 0.00 7 -7 9 -0.60 0.00 8 -7 9 -0.14 0.00 -11 -6 9 -0.09 0.00 8 -6 9 -0.26 0.00 9 -6 9 -0.12 0.00 -11 -5 9 -0.42 0.00 9 -5 9 -0.08 0.00 -11 -4 9 -0.46 0.00 10 -4 9 -0.03 0.00 -12 -3 9 -0.05 0.00 -11 -3 9 -0.17 0.00 10 -3 9 -0.25 0.00 11 -3 9 -0.06 0.00 -12 -2 9 -0.09 0.00 -11 -2 9 -0.04 0.00 11 -2 9 -0.07 0.00 -11 -1 9 -0.36 0.00 11 -1 9 -0.15 0.00 12 -1 9 0.07 0.00 -11 0 9 -0.68 0.00 12 0 9 0.17 0.00 -11 1 9 -0.51 0.00 12 1 9 0.10 0.00 -11 2 9 -0.11 0.00 12 2 9 -0.26 0.00 -11 3 9 0.12 0.00 -10 3 9 0.12 0.00 12 3 9 -0.67 0.00 13 3 9 -0.32 0.00 -10 4 9 0.32 0.00 12 4 9 -0.66 0.00 13 4 9 -0.57 0.00 -10 5 9 0.26 0.00 -9 5 9 0.53 0.00 12 5 9 -0.31 0.00 13 5 9 -0.53 0.00 -9 6 9 0.42 0.00 12 6 9 -0.13 0.00 13 6 9 -0.30 0.00 -9 7 9 0.14 0.00 -8 7 9 0.47 0.00 12 7 9 -0.09 0.00 13 7 9 -0.19 0.00 -8 8 9 0.14 0.00 -7 8 9 0.41 0.00 -6 8 9 0.32 0.00 -3 8 9 0.99 0.00 12 8 9 0.07 0.00 -7 9 9 0.01 0.00 -6 9 9 0.15 0.00 -5 9 9 -0.14 0.00 12 9 9 0.17 0.00 -6 10 9 0.00 0.00 -5 10 9 0.14 0.00 11 10 9 -0.07 0.00 12 10 9 0.09 0.00 -5 11 9 0.40 0.00 -4 11 9 0.46 0.00 10 11 9 -0.27 0.00 11 11 9 -0.14 0.00 -4 12 9 0.53 0.00 -3 12 9 -0.03 0.00 -2 12 9 -0.61 0.00 9 12 9 0.19 0.00 10 12 9 0.06 0.00 -2 13 9 -0.55 0.00 -1 13 9 -0.37 0.00 0 13 9 0.39 0.00 7 13 9 0.16 0.00 8 13 9 0.07 0.00 9 13 9 0.20 0.00 0 14 9 0.01 0.00 1 14 9 0.37 0.00 2 14 9 -0.08 0.00 3 14 9 -0.49 0.00 4 14 9 0.14 0.00 5 14 9 0.15 0.00 6 14 9 0.26 0.00 7 14 9 0.33 0.00 8 14 9 -0.05 0.00 -4 -12 10 -0.37 0.00 -3 -12 10 -0.42 0.00 -2 -12 10 -0.32 0.00 -1 -12 10 -0.08 0.00 -7 -11 10 0.25 0.00 -6 -11 10 0.17 0.00 -5 -11 10 -0.40 0.00 -4 -11 10 -0.75 0.00 -3 -11 10 -0.64 0.00 -2 -11 10 -0.46 0.00 -1 -11 10 -0.26 0.00 0 -11 10 0.25 0.00 1 -11 10 0.36 0.00 2 -11 10 0.13 0.00 -8 -10 10 -0.35 0.00 -7 -10 10 0.19 0.00 -6 -10 10 0.54 0.00 2 -10 10 0.18 0.00 3 -10 10 0.12 0.00 4 -10 10 0.31 0.00 -9 -9 10 -0.11 0.00 -8 -9 10 -0.62 0.00 4 -9 10 0.01 0.00 5 -9 10 0.39 0.00 -10 -8 10 0.10 0.00 -9 -8 10 0.46 0.00 6 -8 10 0.62 0.00 -10 -7 10 -0.12 0.00 7 -7 10 0.44 0.00 -11 -6 10 0.09 0.00 -10 -6 10 -0.19 0.00 8 -6 10 0.13 0.00 -11 -5 10 0.44 0.00 9 -5 10 0.08 0.00 -11 -4 10 0.55 0.00 9 -4 10 0.21 0.00 10 -4 10 0.04 0.00 -11 -3 10 0.27 0.00 10 -3 10 0.23 0.00 -11 -2 10 0.03 0.00 11 -2 10 0.09 0.00 -11 -1 10 0.17 0.00 11 -1 10 0.15 0.00 -11 0 10 0.41 0.00 11 0 10 0.20 0.00 12 0 10 -0.13 0.00 -11 1 10 0.32 0.00 12 1 10 -0.13 0.00 -11 2 10 0.06 0.00 -10 2 10 0.24 0.00 12 2 10 0.13 0.00 -10 3 10 -0.12 0.00 12 3 10 0.50 0.00 -10 4 10 -0.27 0.00 12 4 10 0.52 0.00 13 4 10 0.40 0.00 -9 5 10 -0.51 0.00 12 5 10 0.22 0.00 13 5 10 0.37 0.00 -9 6 10 -0.32 0.00 12 6 10 0.06 0.00 13 6 10 0.18 0.00 -8 7 10 -0.44 0.00 12 7 10 0.10 0.00 -8 8 10 -0.11 0.00 -7 8 10 -0.47 0.00 -6 8 10 -0.28 0.00 12 8 10 0.03 0.00 -7 9 10 -0.08 0.00 -6 9 10 -0.15 0.00 11 9 10 0.12 0.00 12 9 10 -0.04 0.00 -6 10 10 -0.01 0.00 -5 10 10 0.07 0.00 11 10 10 0.17 0.00 12 10 10 0.00 0.00 -5 11 10 -0.27 0.00 -4 11 10 -0.36 0.00 10 11 10 0.27 0.00 11 11 10 0.14 0.00 -4 12 10 -0.53 0.00 -3 12 10 -0.27 0.00 -2 12 10 0.08 0.00 9 12 10 -0.07 0.00 10 12 10 0.00 0.00 -2 13 10 0.26 0.00 -1 13 10 0.17 0.00 0 13 10 -0.27 0.00 7 13 10 -0.19 0.00 8 13 10 -0.13 0.00 9 13 10 -0.17 0.00 0 14 10 -0.07 0.00 1 14 10 -0.35 0.00 2 14 10 0.06 0.00 3 14 10 0.42 0.00 4 14 10 -0.24 0.00 5 14 10 -0.22 0.00 6 14 10 -0.26 0.00 7 14 10 -0.34 0.00 8 14 10 -0.04 0.00 -6 -11 11 -0.14 0.00 -5 -11 11 0.17 0.00 -4 -11 11 0.52 0.00 -3 -11 11 0.59 0.00 -2 -11 11 0.44 0.00 -1 -11 11 0.13 0.00 0 -11 11 -0.19 0.00 1 -11 11 -0.14 0.00 -8 -10 11 0.30 0.00 -7 -10 11 -0.06 0.00 -6 -10 11 -0.37 0.00 -5 -10 11 -0.01 0.00 1 -10 11 -0.34 0.00 2 -10 11 -0.03 0.00 3 -10 11 -0.10 0.00 -9 -9 11 0.09 0.00 -8 -9 11 0.50 0.00 -7 -9 11 0.30 0.00 3 -9 11 0.17 0.00 4 -9 11 0.01 0.00 5 -9 11 -0.20 0.00 -9 -8 11 -0.38 0.00 -8 -8 11 0.10 0.00 5 -8 11 -0.16 0.00 6 -8 11 -0.41 0.00 -10 -7 11 0.18 0.00 -9 -7 11 -0.67 0.00 6 -7 11 -0.56 0.00 7 -7 11 -0.27 0.00 -10 -6 11 0.25 0.00 7 -6 11 -0.48 0.00 8 -6 11 -0.01 0.00 -11 -5 11 -0.40 0.00 -10 -5 11 -0.13 0.00 8 -5 11 -0.22 0.00 9 -5 11 -0.03 0.00 -11 -4 11 -0.53 0.00 -10 -4 11 -0.57 0.00 9 -4 11 -0.20 0.00 10 -4 11 -0.03 0.00 -11 -3 11 -0.30 0.00 10 -3 11 -0.19 0.00 -11 -2 11 0.01 0.00 10 -2 11 -0.48 0.00 11 -2 11 -0.08 0.00 -11 -1 11 0.01 0.00 11 -1 11 -0.13 0.00 -11 0 11 -0.15 0.00 11 0 11 -0.15 0.00 12 0 11 0.09 0.00 -11 1 11 -0.14 0.00 -10 1 11 -0.48 0.00 12 1 11 0.14 0.00 -10 2 11 -0.21 0.00 12 2 11 -0.01 0.00 -10 3 11 0.09 0.00 12 3 11 -0.30 0.00 -10 4 11 0.20 0.00 -9 4 11 0.38 0.00 12 4 11 -0.35 0.00 -9 5 11 0.45 0.00 12 5 11 -0.14 0.00 -9 6 11 0.22 0.00 -8 6 11 0.73 0.00 12 6 11 -0.05 0.00 -8 7 11 0.40 0.00 -7 7 11 0.74 0.00 12 7 11 -0.13 0.00 -7 8 11 0.50 0.00 -6 8 11 0.19 0.00 12 8 11 -0.13 0.00 -7 9 11 0.15 0.00 -6 9 11 0.12 0.00 11 9 11 -0.24 0.00 12 9 11 -0.08 0.00 -6 10 11 0.02 0.00 -5 10 11 -0.33 0.00 11 10 11 -0.22 0.00 -5 11 11 0.08 0.00 -4 11 11 0.09 0.00 10 11 11 -0.28 0.00 11 11 11 -0.15 0.00 -3 12 11 0.39 0.00 -2 12 11 0.34 0.00 9 12 11 -0.08 0.00 10 12 11 -0.10 0.00 -2 13 11 -0.03 0.00 -1 13 11 0.01 0.00 0 13 11 0.11 0.00 7 13 11 0.11 0.00 8 13 11 0.12 0.00 9 13 11 0.12 0.00 0 14 11 0.07 0.00 1 14 11 0.24 0.00 2 14 11 -0.08 0.00 3 14 11 -0.34 0.00 4 14 11 0.35 0.00 5 14 11 0.27 0.00 6 14 11 0.17 0.00 7 14 11 0.26 0.00 -5 -11 12 0.00 0.00 -4 -11 12 -0.28 0.00 -3 -11 12 -0.45 0.00 -2 -11 12 -0.32 0.00 -1 -11 12 0.05 0.00 0 -11 12 0.17 0.00 -7 -10 12 -0.01 0.00 -6 -10 12 0.25 0.00 -5 -10 12 0.16 0.00 -4 -10 12 -0.30 0.00 -3 -10 12 -0.51 0.00 -2 -10 12 -0.27 0.00 -1 -10 12 0.04 0.00 0 -10 12 0.31 0.00 1 -10 12 0.21 0.00 2 -10 12 -0.07 0.00 3 -10 12 0.08 0.00 -8 -9 12 -0.35 0.00 -7 -9 12 -0.17 0.00 -6 -9 12 0.22 0.00 3 -9 12 -0.18 0.00 4 -9 12 -0.05 0.00 -9 -8 12 0.26 0.00 -8 -8 12 -0.05 0.00 5 -8 12 0.03 0.00 6 -8 12 0.20 0.00 -10 -7 12 -0.22 0.00 -9 -7 12 0.45 0.00 6 -7 12 0.40 0.00 7 -7 12 0.14 0.00 -10 -6 12 -0.28 0.00 -9 -6 12 0.25 0.00 7 -6 12 0.34 0.00 8 -6 12 -0.07 0.00 -10 -5 12 0.07 0.00 8 -5 12 0.12 0.00 9 -5 12 -0.01 0.00 -11 -4 12 0.42 0.00 -10 -4 12 0.52 0.00 9 -4 12 0.15 0.00 -11 -3 12 0.26 0.00 -10 -3 12 0.72 0.00 10 -3 12 0.13 0.00 -11 -2 12 -0.03 0.00 -10 -2 12 0.68 0.00 10 -2 12 0.36 0.00 -11 -1 12 -0.12 0.00 -10 -1 12 0.54 0.00 11 -1 12 0.10 0.00 -11 0 12 -0.02 0.00 -10 0 12 0.43 0.00 11 0 12 0.12 0.00 -10 1 12 0.34 0.00 11 1 12 0.16 0.00 12 1 12 -0.12 0.00 -10 2 12 0.18 0.00 12 2 12 -0.07 0.00 -10 3 12 -0.03 0.00 12 3 12 0.12 0.00 -9 4 12 -0.25 0.00 12 4 12 0.22 0.00 -9 5 12 -0.37 0.00 12 5 12 0.15 0.00 -9 6 12 -0.15 0.00 -8 6 12 -0.67 0.00 12 6 12 0.12 0.00 -8 7 12 -0.37 0.00 -7 7 12 -0.68 0.00 12 7 12 0.20 0.00 -7 8 12 -0.50 0.00 -6 8 12 -0.14 0.00 -5 8 12 0.18 0.00 11 8 12 0.30 0.00 12 8 12 0.20 0.00 -6 9 12 -0.12 0.00 -5 9 12 0.58 0.00 11 9 12 0.31 0.00 12 9 12 0.14 0.00 -5 10 12 0.50 0.00 10 10 12 0.32 0.00 11 10 12 0.27 0.00 -4 11 12 0.22 0.00 -3 11 12 -0.24 0.00 10 11 12 0.33 0.00 11 11 12 0.16 0.00 -3 12 12 -0.36 0.00 -2 12 12 -0.56 0.00 8 12 12 -0.04 0.00 9 12 12 0.22 0.00 10 12 12 0.20 0.00 -2 13 12 -0.13 0.00 -1 13 12 -0.13 0.00 0 13 12 0.04 0.00 1 13 12 -0.02 0.00 6 13 12 0.41 0.00 7 13 12 0.04 0.00 8 13 12 -0.07 0.00 9 13 12 -0.05 0.00 1 14 12 -0.09 0.00 2 14 12 0.12 0.00 3 14 12 0.25 0.00 4 14 12 -0.51 0.00 5 14 12 -0.31 0.00 6 14 12 -0.02 0.00 7 14 12 -0.10 0.00 -6 -10 13 -0.17 0.00 -5 -10 13 -0.25 0.00 -4 -10 13 0.06 0.00 -3 -10 13 0.40 0.00 -2 -10 13 0.29 0.00 -1 -10 13 -0.15 0.00 0 -10 13 -0.42 0.00 1 -10 13 -0.13 0.00 2 -10 13 0.11 0.00 -7 -9 13 0.02 0.00 -6 -9 13 -0.21 0.00 -5 -9 13 -0.20 0.00 1 -9 13 -0.21 0.00 2 -9 13 0.19 0.00 3 -9 13 0.18 0.00 4 -9 13 0.07 0.00 -8 -8 13 0.05 0.00 -7 -8 13 0.06 0.00 4 -8 13 0.31 0.00 5 -8 13 0.07 0.00 -9 -7 13 -0.24 0.00 -8 -7 13 -0.49 0.00 5 -7 13 0.27 0.00 6 -7 13 -0.25 0.00 -10 -6 13 0.26 0.00 -9 -6 13 -0.06 0.00 7 -6 13 -0.24 0.00 -10 -5 13 -0.03 0.00 -9 -5 13 0.12 0.00 8 -5 13 -0.05 0.00 -10 -4 13 -0.40 0.00 8 -4 13 -0.38 0.00 9 -4 13 -0.08 0.00 -10 -3 13 -0.62 0.00 9 -3 13 -0.35 0.00 10 -3 13 -0.08 0.00 -10 -2 13 -0.66 0.00 10 -2 13 -0.21 0.00 -10 -1 13 -0.52 0.00 10 -1 13 -0.42 0.00 11 -1 13 -0.07 0.00 -10 0 13 -0.32 0.00 11 0 13 -0.09 0.00 -10 1 13 -0.22 0.00 11 1 13 -0.12 0.00 -10 2 13 -0.14 0.00 11 2 13 -0.18 0.00 12 2 13 0.10 0.00 -10 3 13 -0.01 0.00 -9 3 13 -0.37 0.00 12 3 13 0.00 0.00 -9 4 13 0.10 0.00 12 4 13 -0.14 0.00 -9 5 13 0.25 0.00 -8 5 13 0.27 0.00 12 5 13 -0.21 0.00 -8 6 13 0.57 0.00 12 6 13 -0.24 0.00 -8 7 13 0.33 0.00 -7 7 13 0.62 0.00 11 7 13 -0.16 0.00 12 7 13 -0.27 0.00 -7 8 13 0.47 0.00 -6 8 13 0.15 0.00 -4 8 13 0.50 0.00 11 8 13 -0.29 0.00 12 8 13 -0.22 0.00 -6 9 13 0.14 0.00 -5 9 13 -0.48 0.00 -2 9 13 0.40 0.00 11 9 13 -0.34 0.00 -5 10 13 -0.53 0.00 -4 10 13 -0.65 0.00 10 10 13 -0.39 0.00 11 10 13 -0.30 0.00 -4 11 13 -0.43 0.00 -3 11 13 0.08 0.00 9 11 13 -0.66 0.00 10 11 13 -0.39 0.00 -3 12 13 0.24 0.00 -2 12 13 0.62 0.00 -1 12 13 0.42 0.00 8 12 13 0.00 0.00 9 12 13 -0.33 0.00 10 12 13 -0.27 0.00 -1 13 13 0.22 0.00 0 13 13 -0.13 0.00 1 13 13 -0.06 0.00 2 13 13 -0.16 0.00 3 13 13 0.51 0.00 4 13 13 1.30 0.00 5 13 13 -0.14 0.00 6 13 13 -0.59 0.00 7 13 13 -0.20 0.00 8 13 13 -0.01 0.00 9 13 13 -0.02 0.00 1 14 13 -0.05 0.00 2 14 13 -0.14 0.00 3 14 13 -0.12 0.00 4 14 13 0.67 0.00 5 14 13 0.36 0.00 6 14 13 -0.13 0.00 7 14 13 -0.08 0.00 -5 -10 14 0.25 0.00 -4 -10 14 0.07 0.00 -3 -10 14 -0.27 0.00 -2 -10 14 -0.26 0.00 -1 -10 14 0.19 0.00 0 -10 14 0.44 0.00 1 -10 14 0.08 0.00 -7 -9 14 0.08 0.00 -6 -9 14 0.20 0.00 -5 -9 14 0.23 0.00 -4 -9 14 0.10 0.00 -3 -9 14 -0.26 0.00 -2 -9 14 -0.27 0.00 -1 -9 14 0.06 0.00 0 -9 14 0.36 0.00 1 -9 14 0.21 0.00 2 -9 14 -0.26 0.00 3 -9 14 -0.15 0.00 -8 -8 14 -0.08 0.00 -7 -8 14 0.11 0.00 -6 -8 14 0.32 0.00 3 -8 14 -0.43 0.00 4 -8 14 -0.27 0.00 5 -8 14 -0.11 0.00 -8 -7 14 0.25 0.00 -7 -7 14 0.13 0.00 5 -7 14 -0.25 0.00 6 -7 14 0.15 0.00 -9 -6 14 -0.06 0.00 -8 -6 14 0.64 0.00 6 -6 14 0.09 0.00 7 -6 14 0.17 0.00 -9 -5 14 -0.17 0.00 7 -5 14 0.31 0.00 8 -5 14 0.01 0.00 -10 -4 14 0.27 0.00 -9 -4 14 -0.12 0.00 8 -4 14 0.31 0.00 9 -4 14 0.02 0.00 -10 -3 14 0.47 0.00 -9 -3 14 0.01 0.00 9 -3 14 0.23 0.00 -10 -2 14 0.58 0.00 -9 -2 14 0.35 0.00 9 -2 14 0.47 0.00 10 -2 14 0.07 0.00 -10 -1 14 0.49 0.00 10 -1 14 0.27 0.00 -10 0 14 0.25 0.00 -9 0 14 1.34 0.00 10 0 14 0.44 0.00 11 0 14 0.05 0.00 -10 1 14 0.11 0.00 -9 1 14 1.22 0.00 11 1 14 0.08 0.00 -10 2 14 0.08 0.00 -9 2 14 0.84 0.00 11 2 14 0.10 0.00 -9 3 14 0.43 0.00 11 3 14 0.08 0.00 12 3 14 -0.07 0.00 -9 4 14 0.03 0.00 -8 4 14 0.73 0.00 11 4 14 -0.03 0.00 12 4 14 0.08 0.00 -8 5 14 -0.07 0.00 11 5 14 -0.13 0.00 12 5 14 0.25 0.00 -8 6 14 -0.44 0.00 -7 6 14 -0.14 0.00 11 6 14 -0.08 0.00 12 6 14 0.32 0.00 -7 7 14 -0.54 0.00 -6 7 14 -0.06 0.00 11 7 14 0.06 0.00 12 7 14 0.29 0.00 -7 8 14 -0.41 0.00 -6 8 14 -0.21 0.00 11 8 14 0.21 0.00 12 8 14 0.19 0.00 -6 9 14 -0.16 0.00 -5 9 14 0.23 0.00 -2 9 14 -0.36 0.00 10 9 14 0.55 0.00 11 9 14 0.34 0.00 -5 10 14 0.41 0.00 -4 10 14 0.50 0.00 10 10 14 0.47 0.00 11 10 14 0.34 0.00 -4 11 14 0.49 0.00 -3 11 14 0.04 0.00 9 11 14 0.67 0.00 10 11 14 0.42 0.00 -2 12 14 -0.57 0.00 -1 12 14 -0.39 0.00 7 12 14 -0.04 0.00 8 12 14 0.00 0.00 9 12 14 0.36 0.00 -1 13 14 -0.27 0.00 0 13 14 0.15 0.00 1 13 14 0.07 0.00 2 13 14 0.05 0.00 3 13 14 -0.77 0.00 4 13 14 -1.47 0.00 5 13 14 0.17 0.00 6 13 14 0.68 0.00 7 13 14 0.30 0.00 8 13 14 0.07 0.00 2 14 14 0.13 0.00 3 14 14 0.00 0.00 4 14 14 -0.81 0.00 5 14 14 -0.39 0.00 6 14 14 0.23 0.00 -6 -9 15 -0.16 0.00 -5 -9 15 -0.20 0.00 -4 -9 15 -0.16 0.00 -3 -9 15 0.20 0.00 -2 -9 15 0.35 0.00 -1 -9 15 0.06 0.00 0 -9 15 -0.32 0.00 1 -9 15 -0.19 0.00 2 -9 15 0.25 0.00 -7 -8 15 -0.16 0.00 -6 -8 15 -0.36 0.00 -5 -8 15 0.00 0.00 -4 -8 15 0.15 0.00 1 -8 15 -0.01 0.00 2 -8 15 0.35 0.00 3 -8 15 0.46 0.00 4 -8 15 0.21 0.00 -8 -7 15 -0.05 0.00 -7 -7 15 -0.13 0.00 -6 -7 15 -0.50 0.00 4 -7 15 0.56 0.00 5 -7 15 0.19 0.00 -8 -6 15 -0.33 0.00 -7 -6 15 -0.24 0.00 5 -6 15 0.62 0.00 6 -6 15 -0.10 0.00 -9 -5 15 0.17 0.00 -8 -5 15 -0.39 0.00 7 -5 15 -0.28 0.00 -9 -4 15 0.10 0.00 8 -4 15 -0.25 0.00 -9 -3 15 -0.06 0.00 8 -3 15 -0.53 0.00 9 -3 15 -0.12 0.00 -10 -2 15 -0.46 0.00 -9 -2 15 -0.39 0.00 9 -2 15 -0.38 0.00 10 -2 15 0.03 0.00 -10 -1 15 -0.44 0.00 -9 -1 15 -0.89 0.00 10 -1 15 -0.14 0.00 -10 0 15 -0.18 0.00 -9 0 15 -1.16 0.00 10 0 15 -0.34 0.00 -9 1 15 -0.97 0.00 10 1 15 -0.33 0.00 11 1 15 -0.04 0.00 -9 2 15 -0.64 0.00 11 2 15 -0.02 0.00 -9 3 15 -0.37 0.00 -8 3 15 -1.15 0.00 11 3 15 -0.01 0.00 -9 4 15 -0.09 0.00 -8 4 15 -0.75 0.00 11 4 15 0.03 0.00 12 4 15 -0.02 0.00 -8 5 15 -0.10 0.00 11 5 15 0.10 0.00 12 5 15 -0.23 0.00 -8 6 15 0.27 0.00 -7 6 15 0.02 0.00 11 6 15 0.14 0.00 12 6 15 -0.31 0.00 -7 7 15 0.42 0.00 -6 7 15 0.17 0.00 11 7 15 0.08 0.00 -6 8 15 0.26 0.00 11 8 15 -0.11 0.00 -6 9 15 0.16 0.00 -5 9 15 0.08 0.00 -2 9 15 0.40 0.00 10 9 15 -0.64 0.00 11 9 15 -0.32 0.00 -5 10 15 -0.23 0.00 -4 10 15 -0.20 0.00 9 10 15 -0.62 0.00 10 10 15 -0.51 0.00 11 10 15 -0.35 0.00 -3 11 15 -0.07 0.00 -2 11 15 0.30 0.00 8 11 15 -0.01 0.00 9 11 15 -0.57 0.00 10 11 15 -0.38 0.00 -2 12 15 0.45 0.00 -1 12 15 0.35 0.00 0 12 15 -0.04 0.00 7 12 15 0.10 0.00 8 12 15 0.04 0.00 9 12 15 -0.32 0.00 0 13 15 -0.10 0.00 1 13 15 -0.03 0.00 2 13 15 0.07 0.00 3 13 15 0.95 0.00 4 13 15 1.46 0.00 5 13 15 -0.23 0.00 6 13 15 -0.65 0.00 7 13 15 -0.28 0.00 8 13 15 -0.09 0.00 3 14 15 0.10 0.00 4 14 15 0.86 0.00 5 14 15 0.37 0.00 -4 -9 16 0.13 0.00 -3 -9 16 -0.15 0.00 -2 -9 16 -0.33 0.00 -1 -9 16 -0.14 0.00 0 -9 16 0.21 0.00 1 -9 16 0.16 0.00 -6 -8 16 0.30 0.00 -5 -8 16 -0.03 0.00 -4 -8 16 -0.16 0.00 -3 -8 16 -0.25 0.00 -2 -8 16 -0.34 0.00 -1 -8 16 -0.21 0.00 0 -8 16 -0.08 0.00 1 -8 16 0.05 0.00 2 -8 16 -0.31 0.00 3 -8 16 -0.40 0.00 -7 -7 16 0.07 0.00 -6 -7 16 0.50 0.00 -5 -7 16 0.00 0.00 3 -7 16 -0.64 0.00 4 -7 16 -0.50 0.00 5 -7 16 -0.11 0.00 -8 -6 16 0.14 0.00 -7 -6 16 0.06 0.00 -6 -6 16 0.38 0.00 5 -6 16 -0.53 0.00 6 -6 16 0.10 0.00 -8 -5 16 0.20 0.00 -7 -5 16 0.39 0.00 6 -5 16 -0.20 0.00 7 -5 16 0.22 0.00 -9 -4 16 -0.09 0.00 -8 -4 16 -0.03 0.00 7 -4 16 0.32 0.00 8 -4 16 0.18 0.00 -9 -3 16 0.08 0.00 -8 -3 16 -0.34 0.00 8 -3 16 0.51 0.00 9 -3 16 0.06 0.00 -9 -2 16 0.38 0.00 -8 -2 16 -0.30 0.00 9 -2 16 0.31 0.00 -9 -1 16 0.77 0.00 9 -1 16 0.44 0.00 10 -1 16 0.06 0.00 -9 0 16 0.90 0.00 10 0 16 0.25 0.00 -9 1 16 0.66 0.00 -8 1 16 0.83 0.00 10 1 16 0.21 0.00 11 1 16 0.02 0.00 -9 2 16 0.39 0.00 -8 2 16 0.84 0.00 10 2 16 -0.07 0.00 11 2 16 -0.03 0.00 -9 3 16 0.24 0.00 -8 3 16 0.82 0.00 11 3 16 -0.08 0.00 -8 4 16 0.63 0.00 11 4 16 -0.07 0.00 -8 5 16 0.20 0.00 -7 5 16 0.73 0.00 11 5 16 -0.11 0.00 -7 6 16 0.08 0.00 11 6 16 -0.20 0.00 -7 7 16 -0.27 0.00 -6 7 16 -0.25 0.00 10 7 16 0.22 0.00 11 7 16 -0.18 0.00 -6 8 16 -0.27 0.00 -5 8 16 -0.75 0.00 10 8 16 0.54 0.00 11 8 16 0.02 0.00 -5 9 16 -0.32 0.00 -4 9 16 -0.74 0.00 -2 9 16 -0.48 0.00 10 9 16 0.62 0.00 11 9 16 0.27 0.00 -4 10 16 -0.10 0.00 -3 10 16 -0.24 0.00 9 10 16 0.41 0.00 10 10 16 0.45 0.00 -3 11 16 0.04 0.00 -2 11 16 -0.24 0.00 -1 11 16 0.03 0.00 8 11 16 -0.12 0.00 9 11 16 0.39 0.00 10 11 16 0.28 0.00 -2 12 16 -0.31 0.00 -1 12 16 -0.29 0.00 0 12 16 0.07 0.00 1 12 16 -0.17 0.00 5 12 16 1.02 0.00 6 12 16 0.15 0.00 7 12 16 -0.18 0.00 8 12 16 -0.09 0.00 9 12 16 0.24 0.00 0 13 16 0.05 0.00 1 13 16 -0.01 0.00 2 13 16 -0.15 0.00 3 13 16 -1.00 0.00 4 13 16 -1.27 0.00 5 13 16 0.30 0.00 6 13 16 0.50 0.00 7 13 16 0.18 0.00 -5 -8 17 0.07 0.00 -4 -8 17 0.17 0.00 -3 -8 17 0.27 0.00 -2 -8 17 0.37 0.00 -1 -8 17 0.31 0.00 0 -8 17 0.15 0.00 1 -8 17 -0.07 0.00 2 -8 17 0.20 0.00 -6 -7 17 -0.40 0.00 -5 -7 17 0.04 0.00 -4 -7 17 0.65 0.00 -3 -7 17 0.55 0.00 1 -7 17 0.24 0.00 2 -7 17 0.23 0.00 3 -7 17 0.56 0.00 4 -7 17 0.36 0.00 -7 -6 17 0.05 0.00 -6 -6 17 -0.32 0.00 -5 -6 17 -0.29 0.00 3 -6 17 0.54 0.00 4 -6 17 0.81 0.00 5 -6 17 0.40 0.00 -8 -5 17 -0.12 0.00 -7 -5 17 -0.17 0.00 -6 -5 17 -0.04 0.00 5 -5 17 0.95 0.00 6 -5 17 0.18 0.00 -8 -4 17 0.08 0.00 -7 -4 17 -0.43 0.00 6 -4 17 0.50 0.00 7 -4 17 -0.24 0.00 -8 -3 17 0.31 0.00 7 -3 17 -0.26 0.00 8 -3 17 -0.41 0.00 -9 -2 17 -0.32 0.00 -8 -2 17 0.18 0.00 8 -2 17 -0.52 0.00 9 -2 17 -0.22 0.00 -9 -1 17 -0.58 0.00 -8 -1 17 -0.25 0.00 9 -1 17 -0.35 0.00 -9 0 17 -0.60 0.00 -8 0 17 -0.58 0.00 9 0 17 -0.22 0.00 10 0 17 -0.15 0.00 -9 1 17 -0.36 0.00 -8 1 17 -0.58 0.00 10 1 17 -0.10 0.00 -8 2 17 -0.44 0.00 10 2 17 0.19 0.00 -8 3 17 -0.44 0.00 10 3 17 0.45 0.00 11 3 17 0.14 0.00 -8 4 17 -0.43 0.00 -7 4 17 -0.63 0.00 10 4 17 0.48 0.00 11 4 17 0.12 0.00 -7 5 17 -0.59 0.00 10 5 17 0.30 0.00 11 5 17 0.13 0.00 -7 6 17 -0.16 0.00 -6 6 17 -0.06 0.00 10 6 17 0.06 0.00 11 6 17 0.21 0.00 -6 7 17 0.24 0.00 -5 7 17 0.88 0.00 10 7 17 -0.21 0.00 11 7 17 0.22 0.00 -6 8 17 0.21 0.00 -5 8 17 0.83 0.00 10 8 17 -0.46 0.00 11 8 17 0.05 0.00 -5 9 17 0.42 0.00 -4 9 17 0.87 0.00 9 9 17 -0.23 0.00 10 9 17 -0.50 0.00 -4 10 17 0.30 0.00 -3 10 17 0.39 0.00 -2 10 17 0.38 0.00 8 10 17 0.21 0.00 9 10 17 -0.15 0.00 10 10 17 -0.31 0.00 -3 11 17 -0.01 0.00 -2 11 17 0.23 0.00 -1 11 17 -0.04 0.00 7 11 17 0.57 0.00 8 11 17 0.22 0.00 9 11 17 -0.19 0.00 -1 12 17 0.21 0.00 0 12 17 -0.15 0.00 1 12 17 0.01 0.00 2 12 17 0.85 0.00 3 12 17 1.81 0.00 4 12 17 0.29 0.00 5 12 17 -0.83 0.00 6 12 17 0.10 0.00 7 12 17 0.25 0.00 8 12 17 0.13 0.00 1 13 17 0.02 0.00 2 13 17 0.19 0.00 3 13 17 0.91 0.00 4 13 17 0.92 0.00 5 13 17 -0.38 0.00 6 13 17 -0.31 0.00 -3 -8 18 -0.23 0.00 -2 -8 18 -0.31 0.00 -1 -8 18 -0.29 0.00 0 -8 18 -0.19 0.00 -5 -7 18 -0.05 0.00 -4 -7 18 -0.52 0.00 -3 -7 18 -0.51 0.00 -2 -7 18 -0.41 0.00 -1 -7 18 -0.26 0.00 0 -7 18 -0.39 0.00 1 -7 18 -0.18 0.00 2 -7 18 -0.11 0.00 3 -7 18 -0.38 0.00 -6 -6 18 0.23 0.00 -5 -6 18 0.19 0.00 -4 -6 18 -0.71 0.00 2 -6 18 -0.21 0.00 3 -6 18 -0.45 0.00 4 -6 18 -0.65 0.00 -7 -5 18 0.07 0.00 -6 -5 18 -0.04 0.00 -5 -5 18 0.36 0.00 4 -5 18 -0.84 0.00 5 -5 18 -0.82 0.00 6 -5 18 -0.16 0.00 -7 -4 18 0.32 0.00 -6 -4 18 0.00 0.00 5 -4 18 -1.00 0.00 6 -4 18 -0.51 0.00 7 -4 18 0.10 0.00 -8 -3 18 -0.24 0.00 -7 -3 18 0.15 0.00 7 -3 18 0.14 0.00 8 -3 18 0.25 0.00 -8 -2 18 -0.11 0.00 -7 -2 18 -0.22 0.00 7 -2 18 0.14 0.00 8 -2 18 0.39 0.00 -8 -1 18 0.27 0.00 -7 -1 18 -0.18 0.00 8 -1 18 0.24 0.00 9 -1 18 0.21 0.00 -8 0 18 0.46 0.00 -7 0 18 0.09 0.00 9 0 18 0.08 0.00 -8 1 18 0.33 0.00 -7 1 18 0.04 0.00 9 1 18 -0.20 0.00 10 1 18 0.00 0.00 -8 2 18 0.13 0.00 -7 2 18 -0.17 0.00 9 2 18 -0.46 0.00 10 2 18 -0.25 0.00 -8 3 18 0.13 0.00 -7 3 18 -0.05 0.00 10 3 18 -0.46 0.00 -7 4 18 0.30 0.00 10 4 18 -0.44 0.00 -7 5 18 0.40 0.00 -6 5 18 0.25 0.00 10 5 18 -0.22 0.00 11 5 18 -0.11 0.00 -6 6 18 0.04 0.00 10 6 18 0.02 0.00 11 6 18 -0.18 0.00 -6 7 18 -0.17 0.00 -5 7 18 -0.78 0.00 10 7 18 0.20 0.00 -5 8 18 -0.73 0.00 -4 8 18 -0.92 0.00 9 8 18 0.39 0.00 10 8 18 0.33 0.00 -4 9 18 -0.79 0.00 -3 9 18 -0.65 0.00 9 9 18 0.03 0.00 10 9 18 0.31 0.00 -3 10 18 -0.41 0.00 -2 10 18 -0.49 0.00 8 10 18 -0.36 0.00 9 10 18 -0.07 0.00 -2 11 18 -0.22 0.00 -1 11 18 0.02 0.00 0 11 18 0.69 0.00 1 11 18 0.16 0.00 6 11 18 -0.78 0.00 7 11 18 -0.50 0.00 8 11 18 -0.26 0.00 9 11 18 0.03 0.00 0 12 18 0.24 0.00 1 12 18 0.16 0.00 2 12 18 -0.75 0.00 3 12 18 -1.45 0.00 4 12 18 0.00 0.00 5 12 18 0.58 0.00 6 12 18 -0.30 0.00 7 12 18 -0.27 0.00 2 13 18 -0.17 0.00 3 13 18 -0.74 0.00 4 13 18 -0.53 0.00 5 13 18 0.42 0.00 -4 -7 19 0.31 0.00 -3 -7 19 0.35 0.00 -2 -7 19 0.33 0.00 -1 -7 19 0.25 0.00 0 -7 19 0.37 0.00 1 -7 19 0.14 0.00 -5 -6 19 -0.12 0.00 -4 -6 19 0.57 0.00 -3 -6 19 0.62 0.00 -2 -6 19 0.34 0.00 -1 -6 19 0.06 0.00 0 -6 19 0.31 0.00 1 -6 19 0.47 0.00 2 -6 19 0.12 0.00 3 -6 19 0.31 0.00 -6 -5 19 0.07 0.00 -5 -5 19 -0.22 0.00 -4 -5 19 0.42 0.00 3 -5 19 0.26 0.00 4 -5 19 0.67 0.00 5 -5 19 0.59 0.00 -7 -4 19 -0.29 0.00 -6 -4 19 0.06 0.00 -5 -4 19 -0.17 0.00 4 -4 19 0.53 0.00 5 -4 19 0.87 0.00 6 -4 19 0.46 0.00 -7 -3 19 -0.20 0.00 -6 -3 19 -0.24 0.00 6 -3 19 0.51 0.00 7 -3 19 -0.01 0.00 -7 -2 19 0.14 0.00 -6 -2 19 -0.34 0.00 7 -2 19 -0.05 0.00 8 -2 19 -0.23 0.00 -8 -1 19 -0.21 0.00 -7 -1 19 0.13 0.00 7 -1 19 -0.01 0.00 8 -1 19 -0.12 0.00 -8 0 19 -0.30 0.00 -7 0 19 -0.12 0.00 8 0 19 0.08 0.00 9 0 19 0.03 0.00 -8 1 19 -0.13 0.00 -7 1 19 -0.08 0.00 8 1 19 0.13 0.00 9 1 19 0.24 0.00 -7 2 19 0.18 0.00 9 2 19 0.41 0.00 10 2 19 0.24 0.00 -7 3 19 0.19 0.00 -6 3 19 0.19 0.00 9 3 19 0.36 0.00 10 3 19 0.39 0.00 -7 4 19 -0.05 0.00 -6 4 19 -0.03 0.00 9 4 19 -0.01 0.00 10 4 19 0.35 0.00 -6 5 19 -0.16 0.00 9 5 19 -0.55 0.00 10 5 19 0.14 0.00 -6 6 19 -0.05 0.00 -5 6 19 0.23 0.00 9 6 19 -0.85 0.00 10 6 19 -0.07 0.00 -5 7 19 0.57 0.00 -4 7 19 0.42 0.00 9 7 19 -0.70 0.00 10 7 19 -0.18 0.00 -5 8 19 0.52 0.00 -4 8 19 0.65 0.00 -3 8 19 0.27 0.00 9 8 19 -0.28 0.00 10 8 19 -0.19 0.00 -4 9 19 0.55 0.00 -3 9 19 0.46 0.00 -2 9 19 0.46 0.00 8 9 19 0.41 0.00 9 9 19 0.10 0.00 -3 10 19 0.30 0.00 -2 10 19 0.48 0.00 -1 10 19 -0.01 0.00 7 10 19 0.54 0.00 8 10 19 0.39 0.00 9 10 19 0.18 0.00 -1 11 19 0.03 0.00 0 11 19 -0.70 0.00 1 11 19 -0.25 0.00 2 11 19 1.20 0.00 3 11 19 0.74 0.00 4 11 19 -0.70 0.00 5 11 19 0.19 0.00 6 11 19 0.73 0.00 7 11 19 0.40 0.00 8 11 19 0.24 0.00 1 12 19 -0.29 0.00 2 12 19 0.60 0.00 3 12 19 1.05 0.00 4 12 19 -0.19 0.00 5 12 19 -0.33 0.00 6 12 19 0.40 0.00 7 12 19 0.23 0.00 -4 -6 20 -0.34 0.00 -3 -6 20 -0.35 0.00 -2 -6 20 -0.20 0.00 -1 -6 20 -0.02 0.00 0 -6 20 -0.25 0.00 1 -6 20 -0.37 0.00 2 -6 20 -0.06 0.00 -5 -5 20 0.12 0.00 -4 -5 20 -0.42 0.00 -3 -5 20 -0.64 0.00 -2 -5 20 -0.31 0.00 -1 -5 20 0.05 0.00 0 -5 20 0.00 0.00 1 -5 20 -0.51 0.00 2 -5 20 -0.31 0.00 3 -5 20 -0.18 0.00 4 -5 20 -0.44 0.00 -6 -4 20 -0.05 0.00 -5 -4 20 0.11 0.00 -4 -4 20 -0.03 0.00 3 -4 20 -0.19 0.00 4 -4 20 -0.37 0.00 5 -4 20 -0.61 0.00 -6 -3 20 0.21 0.00 -5 -3 20 0.13 0.00 5 -3 20 -0.44 0.00 6 -3 20 -0.40 0.00 -7 -2 20 -0.05 0.00 -6 -2 20 0.33 0.00 -5 -2 20 0.25 0.00 6 -2 20 -0.20 0.00 7 -2 20 0.02 0.00 -7 -1 20 -0.11 0.00 -6 -1 20 0.19 0.00 7 -1 20 0.00 0.00 8 -1 20 0.07 0.00 -7 0 20 0.07 0.00 -6 0 20 0.10 0.00 7 0 20 -0.10 0.00 8 0 20 -0.10 0.00 -7 1 20 0.06 0.00 -6 1 20 0.10 0.00 8 1 20 -0.13 0.00 9 1 20 -0.21 0.00 -7 2 20 -0.14 0.00 -6 2 20 -0.01 0.00 8 2 20 0.05 0.00 9 2 20 -0.29 0.00 -7 3 20 -0.21 0.00 -6 3 20 -0.09 0.00 8 3 20 0.39 0.00 9 3 20 -0.23 0.00 -6 4 20 0.01 0.00 -5 4 20 0.58 0.00 9 4 20 0.02 0.00 10 4 20 -0.23 0.00 -6 5 20 0.10 0.00 -5 5 20 0.37 0.00 9 5 20 0.41 0.00 10 5 20 -0.08 0.00 -5 6 20 -0.05 0.00 -4 6 20 0.27 0.00 9 6 20 0.66 0.00 10 6 20 0.07 0.00 -5 7 20 -0.33 0.00 -4 7 20 -0.19 0.00 8 7 20 0.26 0.00 9 7 20 0.55 0.00 10 7 20 0.13 0.00 -4 8 20 -0.34 0.00 -3 8 20 -0.08 0.00 8 8 20 -0.10 0.00 9 8 20 0.20 0.00 -3 9 20 -0.20 0.00 -2 9 20 -0.30 0.00 -1 9 20 0.06 0.00 7 9 20 -0.35 0.00 8 9 20 -0.33 0.00 9 9 20 -0.12 0.00 -2 10 20 -0.39 0.00 -1 10 20 -0.08 0.00 0 10 20 0.45 0.00 1 10 20 -0.43 0.00 5 10 20 -0.84 0.00 6 10 20 -0.70 0.00 7 10 20 -0.39 0.00 8 10 20 -0.31 0.00 0 11 20 0.59 0.00 1 11 20 0.22 0.00 2 11 20 -0.95 0.00 3 11 20 -0.40 0.00 4 11 20 0.53 0.00 5 11 20 -0.36 0.00 6 11 20 -0.60 0.00 7 11 20 -0.28 0.00 2 12 20 -0.46 0.00 3 12 20 -0.69 0.00 4 12 20 0.26 0.00 5 12 20 0.10 0.00 -1 -6 21 -0.07 0.00 -4 -5 21 0.34 0.00 -3 -5 21 0.42 0.00 -2 -5 21 0.16 0.00 -1 -5 21 -0.10 0.00 0 -5 21 -0.07 0.00 1 -5 21 0.35 0.00 2 -5 21 0.21 0.00 3 -5 21 0.13 0.00 -5 -4 21 -0.08 0.00 -4 -4 21 0.14 0.00 -3 -4 21 0.55 0.00 -2 -4 21 0.42 0.00 -1 -4 21 0.20 0.00 0 -4 21 -0.05 0.00 1 -4 21 0.30 0.00 2 -4 21 0.41 0.00 3 -4 21 0.15 0.00 4 -4 21 0.22 0.00 -6 -3 21 -0.17 0.00 -5 -3 21 -0.12 0.00 -4 -3 21 -0.35 0.00 -3 -3 21 0.09 0.00 3 -3 21 0.22 0.00 4 -3 21 0.08 0.00 5 -3 21 0.25 0.00 -6 -2 21 -0.29 0.00 -5 -2 21 -0.19 0.00 -4 -2 21 -0.64 0.00 5 -2 21 0.01 0.00 6 -2 21 0.11 0.00 -6 -1 21 -0.19 0.00 -5 -1 21 -0.20 0.00 6 -1 21 0.02 0.00 7 -1 21 -0.04 0.00 -6 0 21 -0.09 0.00 -5 0 21 -0.02 0.00 6 0 21 0.04 0.00 7 0 21 0.07 0.00 8 0 21 0.05 0.00 -6 1 21 -0.09 0.00 -5 1 21 0.13 0.00 7 1 21 0.05 0.00 8 1 21 0.10 0.00 -6 2 21 -0.05 0.00 -5 2 21 -0.04 0.00 7 2 21 -0.34 0.00 8 2 21 -0.07 0.00 9 2 21 0.15 0.00 -6 3 21 0.01 0.00 -5 3 21 -0.41 0.00 8 3 21 -0.37 0.00 9 3 21 0.10 0.00 -6 4 21 -0.01 0.00 -5 4 21 -0.58 0.00 8 4 21 -0.59 0.00 9 4 21 -0.03 0.00 -5 5 21 -0.41 0.00 -4 5 21 -0.84 0.00 8 5 21 -0.56 0.00 9 5 21 -0.25 0.00 -5 6 21 -0.07 0.00 -4 6 21 -0.37 0.00 -3 6 21 -0.42 0.00 8 6 21 -0.39 0.00 9 6 21 -0.42 0.00 -4 7 21 0.02 0.00 -3 7 21 -0.18 0.00 7 7 21 0.01 0.00 8 7 21 -0.20 0.00 9 7 21 -0.38 0.00 -3 8 21 -0.07 0.00 -2 8 21 -0.13 0.00 -1 8 21 -0.11 0.00 7 8 21 0.02 0.00 8 8 21 0.02 0.00 9 8 21 -0.15 0.00 -2 9 21 0.12 0.00 -1 9 21 -0.04 0.00 0 9 21 0.22 0.00 6 9 21 0.35 0.00 7 9 21 0.17 0.00 8 9 21 0.19 0.00 -1 10 21 0.11 0.00 0 10 21 -0.23 0.00 1 10 21 0.49 0.00 2 10 21 0.71 0.00 3 10 21 -0.49 0.00 4 10 21 -0.29 0.00 5 10 21 0.71 0.00 6 10 21 0.50 0.00 7 10 21 0.25 0.00 1 11 21 -0.13 0.00 2 11 21 0.72 0.00 3 11 21 0.18 0.00 4 11 21 -0.36 0.00 5 11 21 0.38 0.00 6 11 21 0.43 0.00 -1 -5 22 0.13 0.00 0 -5 22 0.15 0.00 -3 -4 22 -0.41 0.00 -2 -4 22 -0.27 0.00 -1 -4 22 -0.14 0.00 0 -4 22 0.08 0.00 1 -4 22 -0.16 0.00 2 -4 22 -0.26 0.00 3 -4 22 -0.12 0.00 -4 -3 22 0.22 0.00 -3 -3 22 -0.14 0.00 -2 -3 22 -0.32 0.00 -1 -3 22 -0.45 0.00 0 -3 22 -0.20 0.00 1 -3 22 -0.19 0.00 2 -3 22 -0.34 0.00 3 -3 22 -0.20 0.00 4 -3 22 -0.04 0.00 -5 -2 22 0.11 0.00 -4 -2 22 0.50 0.00 -3 -2 22 0.43 0.00 -2 -2 22 -0.07 0.00 3 -2 22 -0.24 0.00 4 -2 22 -0.02 0.00 5 -2 22 0.02 0.00 -5 -1 22 0.11 0.00 -4 -1 22 0.44 0.00 -3 -1 22 0.73 0.00 4 -1 22 -0.01 0.00 5 -1 22 0.10 0.00 6 -1 22 0.00 0.00 -5 0 22 0.01 0.00 -4 0 22 0.10 0.00 5 0 22 0.16 0.00 6 0 22 -0.02 0.00 7 0 22 -0.04 0.00 -6 1 22 0.06 0.00 -5 1 22 -0.12 0.00 -4 1 22 -0.40 0.00 6 1 22 0.08 0.00 7 1 22 -0.07 0.00 -5 2 22 0.01 0.00 -4 2 22 -0.61 0.00 6 2 22 0.25 0.00 7 2 22 0.22 0.00 8 2 22 0.05 0.00 -5 3 22 0.32 0.00 -4 3 22 -0.13 0.00 7 3 22 0.57 0.00 8 3 22 0.30 0.00 -5 4 22 0.49 0.00 -4 4 22 0.56 0.00 7 4 22 0.49 0.00 8 4 22 0.46 0.00 -5 5 22 0.36 0.00 -4 5 22 0.72 0.00 -3 5 22 0.24 0.00 7 5 22 0.07 0.00 8 5 22 0.41 0.00 -4 6 22 0.37 0.00 -3 6 22 0.29 0.00 -2 6 22 -0.31 0.00 7 6 22 -0.13 0.00 8 6 22 0.26 0.00 -3 7 22 0.14 0.00 -2 7 22 0.08 0.00 -1 7 22 -0.51 0.00 6 7 22 0.14 0.00 7 7 22 -0.01 0.00 8 7 22 0.15 0.00 -3 8 22 0.12 0.00 -2 8 22 0.14 0.00 -1 8 22 0.02 0.00 0 8 22 -0.75 0.00 5 8 22 -0.35 0.00 6 8 22 0.06 0.00 7 8 22 0.05 0.00 8 8 22 0.04 0.00 -1 9 22 0.06 0.00 0 9 22 -0.28 0.00 1 9 22 -0.85 0.00 2 9 22 0.06 0.00 3 9 22 0.79 0.00 4 9 22 -0.21 0.00 5 9 22 -0.59 0.00 6 9 22 -0.18 0.00 7 9 22 -0.05 0.00 0 10 22 0.08 0.00 1 10 22 -0.48 0.00 2 10 22 -0.49 0.00 3 10 22 0.48 0.00 4 10 22 0.18 0.00 5 10 22 -0.50 0.00 6 10 22 -0.31 0.00 2 11 22 -0.52 0.00 3 11 22 -0.03 0.00 4 11 22 0.23 0.00 -1 -4 23 0.12 0.00 0 -4 23 -0.09 0.00 -3 -3 23 0.11 0.00 -2 -3 23 0.15 0.00 -1 -3 23 0.30 0.00 0 -3 23 0.15 0.00 1 -3 23 0.09 0.00 2 -3 23 0.19 0.00 3 -3 23 0.14 0.00 -4 -2 23 -0.32 0.00 -3 -2 23 -0.25 0.00 -2 -2 23 0.00 0.00 -1 -2 23 0.37 0.00 0 -2 23 0.30 0.00 1 -2 23 0.15 0.00 2 -2 23 0.22 0.00 3 -2 23 0.19 0.00 4 -2 23 0.04 0.00 -4 -1 23 -0.30 0.00 -3 -1 23 -0.51 0.00 -2 -1 23 -0.22 0.00 -1 -1 23 0.44 0.00 0 -1 23 0.51 0.00 1 -1 23 0.21 0.00 2 -1 23 0.31 0.00 3 -1 23 0.24 0.00 4 -1 23 0.04 0.00 5 -1 23 -0.07 0.00 -5 0 23 0.00 0.00 -4 0 23 -0.08 0.00 -3 0 23 -0.47 0.00 -2 0 23 -0.38 0.00 3 0 23 0.40 0.00 4 0 23 0.08 0.00 5 0 23 -0.13 0.00 6 0 23 0.01 0.00 -5 1 23 0.07 0.00 -4 1 23 0.29 0.00 -3 1 23 -0.12 0.00 -2 1 23 -0.37 0.00 4 1 23 0.29 0.00 5 1 23 -0.08 0.00 6 1 23 -0.06 0.00 7 1 23 0.08 0.00 -5 2 23 -0.01 0.00 -4 2 23 0.53 0.00 -3 2 23 0.34 0.00 5 2 23 0.25 0.00 6 2 23 -0.15 0.00 7 2 23 -0.10 0.00 -4 3 23 0.24 0.00 -3 3 23 0.57 0.00 6 3 23 0.00 0.00 7 3 23 -0.37 0.00 -4 4 23 -0.33 0.00 -3 4 23 0.30 0.00 -2 4 23 0.61 0.00 6 4 23 0.31 0.00 7 4 23 -0.36 0.00 8 4 23 -0.31 0.00 -4 5 23 -0.52 0.00 -3 5 23 -0.11 0.00 -2 5 23 0.66 0.00 6 5 23 0.38 0.00 7 5 23 -0.05 0.00 8 5 23 -0.28 0.00 -3 6 23 -0.18 0.00 -2 6 23 0.34 0.00 -1 6 23 1.10 0.00 5 6 23 -0.26 0.00 6 6 23 0.15 0.00 7 6 23 0.12 0.00 8 6 23 -0.16 0.00 -2 7 23 0.01 0.00 -1 7 23 0.56 0.00 0 7 23 0.97 0.00 1 7 23 -0.03 0.00 4 7 23 0.44 0.00 5 7 23 -0.12 0.00 6 7 23 -0.06 0.00 7 7 23 0.04 0.00 -2 8 23 -0.13 0.00 -1 8 23 0.01 0.00 0 8 23 0.67 0.00 1 8 23 0.45 0.00 2 8 23 -0.58 0.00 3 8 23 -0.09 0.00 4 8 23 0.57 0.00 5 8 23 0.18 0.00 6 8 23 -0.06 0.00 7 8 23 -0.05 0.00 0 9 23 0.23 0.00 1 9 23 0.64 0.00 2 9 23 -0.16 0.00 3 9 23 -0.58 0.00 4 9 23 0.23 0.00 5 9 23 0.36 0.00 6 9 23 0.07 0.00 2 10 23 0.29 0.00 3 10 23 -0.43 0.00 4 10 23 -0.13 0.00 5 10 23 0.29 0.00 -2 -2 24 0.05 0.00 -1 -2 24 -0.18 0.00 0 -2 24 -0.17 0.00 1 -2 24 -0.06 0.00 2 -2 24 -0.07 0.00 3 -2 24 -0.11 0.00 -3 -1 24 0.27 0.00 -2 -1 24 0.12 0.00 -1 -1 24 -0.28 0.00 0 -1 24 -0.27 0.00 1 -1 24 -0.05 0.00 2 -1 24 -0.15 0.00 3 -1 24 -0.14 0.00 4 -1 24 -0.04 0.00 -3 0 24 0.32 0.00 -2 0 24 0.25 0.00 -1 0 24 -0.32 0.00 0 0 24 -0.60 0.00 1 0 24 -0.20 0.00 2 0 24 -0.25 0.00 3 0 24 -0.29 0.00 4 0 24 -0.06 0.00 5 0 24 0.11 0.00 -4 1 24 -0.17 0.00 -3 1 24 0.13 0.00 -2 1 24 0.30 0.00 -1 1 24 -0.05 0.00 0 1 24 -0.69 0.00 1 1 24 -0.50 0.00 2 1 24 -0.26 0.00 3 1 24 -0.39 0.00 4 1 24 -0.25 0.00 5 1 24 0.10 0.00 6 1 24 0.05 0.00 -4 2 24 -0.37 0.00 -3 2 24 -0.21 0.00 -2 2 24 0.17 0.00 -1 2 24 0.26 0.00 0 2 24 -0.20 0.00 1 2 24 -0.49 0.00 2 2 24 -0.18 0.00 3 2 24 -0.16 0.00 4 2 24 -0.42 0.00 5 2 24 -0.21 0.00 6 2 24 0.08 0.00 -3 3 24 -0.42 0.00 -2 3 24 -0.09 0.00 -1 3 24 0.23 0.00 0 3 24 0.31 0.00 3 3 24 0.21 0.00 4 3 24 -0.21 0.00 5 3 24 -0.55 0.00 6 3 24 -0.08 0.00 -3 4 24 -0.26 0.00 -2 4 24 -0.35 0.00 -1 4 24 -0.16 0.00 0 4 24 0.28 0.00 3 4 24 0.29 0.00 4 4 24 0.23 0.00 5 4 24 -0.47 0.00 6 4 24 -0.33 0.00 7 4 24 0.22 0.00 -3 5 24 0.04 0.00 -2 5 24 -0.41 0.00 -1 5 24 -0.64 0.00 0 5 24 -0.13 0.00 1 5 24 0.17 0.00 2 5 24 -0.28 0.00 3 5 24 -0.01 0.00 4 5 24 0.41 0.00 5 5 24 -0.08 0.00 6 5 24 -0.36 0.00 7 5 24 0.04 0.00 -2 6 24 -0.24 0.00 -1 6 24 -0.79 0.00 0 6 24 -0.56 0.00 1 6 24 0.14 0.00 2 6 24 -0.29 0.00 3 6 24 -0.47 0.00 4 6 24 0.20 0.00 5 6 24 0.17 0.00 6 6 24 -0.18 0.00 7 6 24 -0.08 0.00 -1 7 24 -0.45 0.00 0 7 24 -0.73 0.00 1 7 24 0.04 0.00 2 7 24 0.12 0.00 3 7 24 -0.58 0.00 4 7 24 -0.21 0.00 5 7 24 0.13 0.00 6 7 24 -0.02 0.00 0 8 24 -0.50 0.00 1 8 24 -0.26 0.00 2 8 24 0.44 0.00 3 8 24 -0.11 0.00 4 8 24 -0.42 0.00 5 8 24 -0.05 0.00 6 8 24 0.03 0.00 1 9 24 -0.41 0.00 2 9 24 0.22 0.00 3 9 24 0.39 0.00 4 9 24 -0.21 0.00 5 9 24 -0.18 0.00 -1 -1 25 0.16 0.00 0 -1 25 0.12 0.00 1 -1 25 -0.02 0.00 2 -1 25 0.03 0.00 -2 0 25 -0.11 0.00 -1 0 25 0.25 0.00 0 0 25 0.37 0.00 1 0 25 0.02 0.00 2 0 25 0.12 0.00 3 0 25 0.17 0.00 -2 1 25 -0.21 0.00 -1 1 25 0.05 0.00 0 1 25 0.49 0.00 1 1 25 0.21 0.00 2 1 25 0.09 0.00 3 1 25 0.29 0.00 4 1 25 0.16 0.00 -2 2 25 -0.13 0.00 -1 2 25 -0.20 0.00 0 2 25 0.16 0.00 1 2 25 0.28 0.00 2 2 25 -0.02 0.00 3 2 25 0.11 0.00 4 2 25 0.34 0.00 5 2 25 0.12 0.00 -2 3 25 0.03 0.00 -1 3 25 -0.17 0.00 0 3 25 -0.23 0.00 1 3 25 0.04 0.00 2 3 25 -0.07 0.00 3 3 25 -0.22 0.00 4 3 25 0.22 0.00 5 3 25 0.44 0.00 -2 4 25 0.13 0.00 -1 4 25 0.05 0.00 0 4 25 -0.20 0.00 1 4 25 -0.12 0.00 2 4 25 0.01 0.00 3 4 25 -0.31 0.00 4 4 25 -0.13 0.00 5 4 25 0.43 0.00 6 4 25 0.28 0.00 -2 5 25 0.15 0.00 -1 5 25 0.29 0.00 0 5 25 0.07 0.00 1 5 25 -0.03 0.00 2 5 25 0.24 0.00 3 5 25 -0.09 0.00 4 5 25 -0.33 0.00 5 5 25 0.13 0.00 6 5 25 0.28 0.00 -1 6 25 0.41 0.00 0 6 25 0.31 0.00 1 6 25 -0.02 0.00 2 6 25 0.34 0.00 3 6 25 0.28 0.00 4 6 25 -0.26 0.00 5 6 25 -0.09 0.00 0 7 25 0.43 0.00 1 7 25 -0.06 0.00 2 7 25 0.04 0.00 3 7 25 0.47 0.00 4 7 25 0.01 0.00 5 7 25 -0.12 0.00 2 8 25 -0.31 0.00 3 8 25 0.19 0.00 4 8 25 0.25 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 200618) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.500 199 47 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 0 0 4.463 0 1 0 4.105 2 1 0 8.781 0 -2 1 8.997 -1 -1 1 6.101 0 -1 1 5.091 1 -1 1 7.395 2 -1 1 11.147 -2 0 1 9.377 -1 0 1 5.128 1 0 1 4.871 2 0 1 9.096 0 1 1 4.236 1 1 1 5.164 1 2 1 7.973 1 3 1 11.628 1 -2 2 11.944 0 -1 2 6.725 0 0 2 4.505 1 0 2 6.143 2 1 2 9.189 -1 2 2 10.737 1 3 2 11.716 -2 -2 3 13.700 -1 -1 3 9.428 2 -1 3 12.997 2 0 3 10.903 3 0 3 14.759 -1 1 3 9.211 1 3 3 12.237 -1 -2 4 13.740 -1 1 4 10.876 2 1 4 11.542 -1 2 4 12.810 0 2 4 10.860 -2 2 5 17.172 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL new_a.res in P-1 CELL 10.3800 11.5329 20.2705 76.00 82.55 72.99 SPGR P-1 # Solvent Accessible Volume = 199 # Electrons Found in S.A.V. = 47 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.750 0.148 0.468 ! 3.74 eA-3 C102 0.159 0.890 0.471 ! 3.69 eA-3 C103 0.044 1.000 0.470 ! 2.89 eA-3 C104 0.054 0.079 0.468 ! 1.57 eA-3 C105 0.955 0.066 0.500 ! 1.46 eA-3 Q106 0.805 0.640 0.236 ! 0.63 eA-3 Q107 0.715 0.628 0.299 ! 0.62 eA-3 Q108 0.749 0.976 0.109 ! 0.61 eA-3 Q109 0.611 0.619 0.266 ! 0.59 eA-3 Q110 0.977 0.512 0.357 ! 0.56 eA-3 Q111 0.813 0.761 0.044 ! 0.54 eA-3 Q112 0.714 0.623 0.204 ! 0.53 eA-3 Q113 0.803 0.199 0.477 ! 0.53 eA-3 ) ; _shelx_fab_checksum 43566 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-22067 _database_code_depnum_ccdc_archive 'CCDC 2226341' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C35 H57 Fe N3 Si2' _chemical_formula_sum 'C35 H57 Fe N3 Si2' _chemical_formula_weight 631.86 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 60 _space_group_name_H-M_alt 'P b c n' _space_group_name_Hall '-P 2n 2ab' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 10.11510(10) _cell_length_b 17.6923(2) _cell_length_c 20.5843(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3683.75(8) _cell_formula_units_Z 4 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 56632 _cell_measurement_theta_min 2.4280 _cell_measurement_theta_max 66.5610 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.139 _exptl_crystal_F_000 1368 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.020 _exptl_absorpt_coefficient_mu 4.087 _shelx_estimated_absorpt_T_min 0.495 _shelx_estimated_absorpt_T_max 0.923 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.66668 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 107553 _diffrn_reflns_av_unetI/netI 0.0224 _diffrn_reflns_av_R_equivalents 0.1035 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 5.000 _diffrn_reflns_theta_max 66.583 _diffrn_reflns_theta_full 66.583 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 3248 _reflns_number_gt 2998 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. Carbon 4 was disordered over two, equally occupied positions. No addition restraints or constraints were needed for the disordered model to converge. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0634P)^2^+4.0656P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3248 _refine_ls_number_parameters 203 _refine_ls_number_restraints 6 _refine_ls_R_factor_all 0.0521 _refine_ls_R_factor_gt 0.0488 _refine_ls_wR_factor_ref 0.1324 _refine_ls_wR_factor_gt 0.1297 _refine_ls_goodness_of_fit_ref 1.100 _refine_ls_restrained_S_all 1.099 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.5000 0.67213(3) 0.7500 0.01974(18) Uani 1 2 d S T P . . Si1 Si 0.41186(9) 0.83700(4) 0.80536(5) 0.0438(3) Uani 1 1 d . . . . . N11 N 0.47241(19) 0.59590(11) 0.68037(10) 0.0203(4) Uani 1 1 d . . . . . C11 C 0.4311(3) 0.46832(14) 0.63629(12) 0.0288(6) Uani 1 1 d . . . . . H11A H 0.3529 0.4880 0.6138 0.043 Uiso 1 1 calc R U . . . H11B H 0.4113 0.4183 0.6542 0.043 Uiso 1 1 calc R U . . . H11C H 0.5047 0.4643 0.6055 0.043 Uiso 1 1 calc R U . . . C21 C 0.4687(2) 0.52139(13) 0.69083(11) 0.0214(5) Uani 1 1 d . . . . . C31 C 0.5000 0.48772(19) 0.7500 0.0227(7) Uani 1 2 d S T P . . H31 H 0.5000 0.4340 0.7500 0.027 Uiso 1 2 calc R U P . . C12 C 0.4521(2) 0.62212(12) 0.61522(11) 0.0212(5) Uani 1 1 d . . . . . C22 C 0.3329(2) 0.65856(13) 0.59955(12) 0.0261(5) Uani 1 1 d . . . . . C32 C 0.3153(3) 0.68290(14) 0.53570(12) 0.0297(6) Uani 1 1 d . . . . . H32 H 0.2345 0.7065 0.5237 0.036 Uiso 1 1 calc R U . . . C42 C 0.4125(3) 0.67335(14) 0.48980(13) 0.0313(6) Uani 1 1 d . . . . . H42 H 0.3982 0.6898 0.4464 0.038 Uiso 1 1 calc R U . . . C52 C 0.5312(3) 0.63988(13) 0.50654(12) 0.0281(6) Uani 1 1 d . . . . . H52 H 0.5987 0.6350 0.4747 0.034 Uiso 1 1 calc R U . . . C62 C 0.5536(2) 0.61332(13) 0.56893(11) 0.0236(5) Uani 1 1 d . . . . . C72 C 0.2268(3) 0.67029(14) 0.65080(14) 0.0321(6) Uani 1 1 d . . . . . H72 H 0.2732 0.6833 0.6922 0.039 Uiso 1 1 calc R U . . . C82 C 0.1334(3) 0.73512(17) 0.63579(15) 0.0416(7) Uani 1 1 d . . . . . H82A H 0.1847 0.7810 0.6271 0.062 Uiso 1 1 calc R U . . . H82B H 0.0750 0.7437 0.6731 0.062 Uiso 1 1 calc R U . . . H82C H 0.0801 0.7225 0.5975 0.062 Uiso 1 1 calc R U . . . C92 C 0.1490(3) 0.59852(18) 0.66326(18) 0.0486(8) Uani 1 1 d . . . . . H92A H 0.1098 0.5808 0.6225 0.073 Uiso 1 1 calc R U . . . H92B H 0.0786 0.6088 0.6948 0.073 Uiso 1 1 calc R U . . . H92C H 0.2082 0.5596 0.6806 0.073 Uiso 1 1 calc R U . . . C102 C 0.6867(2) 0.57924(14) 0.58728(13) 0.0284(6) Uani 1 1 d . . . . . H102 H 0.6712 0.5449 0.6251 0.034 Uiso 1 1 calc R U . . . C112 C 0.7793(3) 0.6405(2) 0.6097(2) 0.0653(11) Uani 1 1 d . . . . . H11D H 0.7998 0.6741 0.5732 0.098 Uiso 1 1 calc R U . . . H11E H 0.8611 0.6176 0.6260 0.098 Uiso 1 1 calc R U . . . H11F H 0.7373 0.6696 0.6446 0.098 Uiso 1 1 calc R U . . . C122 C 0.7483(3) 0.53169(18) 0.53352(15) 0.0455(7) Uani 1 1 d . . . . . H12A H 0.6838 0.4944 0.5182 0.068 Uiso 1 1 calc R U . . . H12B H 0.8265 0.5056 0.5504 0.068 Uiso 1 1 calc R U . . . H12C H 0.7741 0.5645 0.4974 0.068 Uiso 1 1 calc R U . . . N1 N 0.5000 0.7797(2) 0.7500 0.0434(10) Uani 1 2 d S T P A . C24 C 0.4538(4) 0.8250(2) 0.89230(19) 0.0567(9) Uani 1 1 d . . . . . H24A H 0.4322 0.7735 0.9060 0.085 Uiso 1 1 calc R U . . . H24B H 0.4029 0.8612 0.9183 0.085 Uiso 1 1 calc R U . . . H24C H 0.5485 0.8342 0.8986 0.085 Uiso 1 1 calc R U . . . C34 C 0.2306(4) 0.8264(2) 0.79633(18) 0.0636(11) Uani 1 1 d . . . . . H34A H 0.2052 0.8379 0.7515 0.095 Uiso 1 1 calc R U . . . H34B H 0.1856 0.8613 0.8259 0.095 Uiso 1 1 calc R U . . . H34C H 0.2052 0.7743 0.8068 0.095 Uiso 1 1 calc R U . . . C4A C 0.4327(12) 0.9349(6) 0.7679(6) 0.057(3) Uani 0.5 1 d . U P A 1 H4AA H 0.3600 0.9453 0.7369 0.069 Uiso 0.5 1 calc R U P A 1 H4AB H 0.4316 0.9741 0.8021 0.069 Uiso 0.5 1 calc R U P A 1 C4B C 0.4902(10) 0.9313(5) 0.7875(5) 0.043(2) Uani 0.5 1 d . U P A 2 H4BA H 0.4317 0.9732 0.8011 0.052 Uiso 0.5 1 calc R U P A 2 H4BB H 0.5761 0.9363 0.8102 0.052 Uiso 0.5 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0243(3) 0.0165(3) 0.0185(3) 0.000 -0.00047(19) 0.000 Si1 0.0528(5) 0.0208(4) 0.0579(6) 0.0020(3) 0.0209(4) 0.0067(3) N11 0.0228(9) 0.0193(9) 0.0188(10) 0.0017(8) -0.0031(8) 0.0001(8) C11 0.0401(15) 0.0219(12) 0.0245(13) -0.0006(10) -0.0057(11) -0.0047(10) C21 0.0239(11) 0.0210(12) 0.0193(12) -0.0019(9) 0.0000(9) 0.0000(9) C31 0.0305(19) 0.0159(16) 0.0218(18) 0.000 -0.0011(13) 0.000 C12 0.0273(12) 0.0181(11) 0.0183(11) 0.0001(9) -0.0026(10) -0.0033(9) C22 0.0269(12) 0.0227(11) 0.0285(14) 0.0023(10) -0.0047(10) -0.0028(10) C32 0.0330(14) 0.0288(13) 0.0274(14) 0.0040(10) -0.0083(11) -0.0005(10) C42 0.0449(16) 0.0275(13) 0.0214(13) 0.0032(10) -0.0066(12) -0.0044(11) C52 0.0384(14) 0.0236(12) 0.0221(13) -0.0026(10) 0.0035(11) -0.0041(11) C62 0.0300(13) 0.0195(11) 0.0212(12) -0.0026(9) -0.0006(10) -0.0036(10) C72 0.0286(14) 0.0372(15) 0.0307(14) 0.0043(11) -0.0011(11) 0.0033(11) C82 0.0370(15) 0.0400(16) 0.0479(18) 0.0023(13) 0.0032(13) 0.0075(12) C92 0.0342(15) 0.0434(17) 0.068(2) 0.0164(16) 0.0130(15) 0.0025(13) C102 0.0302(13) 0.0275(12) 0.0275(13) -0.0026(10) 0.0014(10) 0.0010(10) C112 0.0383(18) 0.0454(19) 0.112(3) -0.016(2) -0.026(2) -0.0002(15) C122 0.0487(17) 0.0480(17) 0.0397(16) -0.0036(13) 0.0084(14) 0.0163(14) N1 0.0308(18) 0.0282(18) 0.071(3) 0.000 0.0092(15) 0.000 C24 0.057(2) 0.053(2) 0.061(2) -0.0079(16) 0.0105(19) 0.0123(16) C34 0.057(2) 0.080(3) 0.053(2) 0.0163(18) 0.0135(18) 0.0383(19) C4A 0.082(8) 0.029(4) 0.061(7) -0.001(4) 0.010(5) 0.009(5) C4B 0.076(7) 0.018(3) 0.035(5) 0.000(3) 0.014(4) -0.003(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.903(4) . ? Fe1 N11 1.988(2) . ? Fe1 N11 1.988(2) 3_656 ? Si1 N1 1.767(2) . ? Si1 C24 1.851(4) . ? Si1 C34 1.852(4) . ? Si1 C4B 1.883(9) . ? Si1 C4A 1.907(11) . ? N11 C21 1.336(3) . ? N11 C12 1.434(3) . ? C11 C21 1.512(3) . ? C21 C31 1.392(3) . ? C31 C21 1.393(3) 3_656 ? C12 C22 1.405(3) . ? C12 C62 1.409(3) . ? C22 C32 1.395(4) . ? C22 C72 1.519(4) . ? C32 C42 1.374(4) . ? C42 C52 1.382(4) . ? C52 C62 1.386(3) . ? C62 C102 1.523(3) . ? C72 C92 1.516(4) . ? C72 C82 1.518(4) . ? C102 C112 1.505(4) . ? C102 C122 1.523(4) . ? N1 Si1 1.767(2) 3_656 ? C4A C4A 1.55(2) 3_656 ? C4B C4B 1.557(19) 3_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N11 132.73(6) . . ? N1 Fe1 N11 132.73(6) . 3_656 ? N11 Fe1 N11 94.54(11) . 3_656 ? N1 Si1 C24 116.25(13) . . ? N1 Si1 C34 112.11(14) . . ? C24 Si1 C34 108.19(17) . . ? N1 Si1 C4B 99.8(3) . . ? C24 Si1 C4B 101.1(3) . . ? C34 Si1 C4B 119.2(3) . . ? N1 Si1 C4A 101.8(4) . . ? C24 Si1 C4A 118.0(4) . . ? C34 Si1 C4A 99.3(4) . . ? C21 N11 C12 117.76(19) . . ? C21 N11 Fe1 123.87(16) . . ? C12 N11 Fe1 118.35(14) . . ? N11 C21 C31 123.8(2) . . ? N11 C21 C11 120.0(2) . . ? C31 C21 C11 116.2(2) . . ? C21 C31 C21 129.3(3) . 3_656 ? C22 C12 C62 121.4(2) . . ? C22 C12 N11 119.1(2) . . ? C62 C12 N11 119.5(2) . . ? C32 C22 C12 117.9(2) . . ? C32 C22 C72 121.5(2) . . ? C12 C22 C72 120.6(2) . . ? C42 C32 C22 121.2(2) . . ? C32 C42 C52 120.2(2) . . ? C42 C52 C62 121.2(2) . . ? C52 C62 C12 118.0(2) . . ? C52 C62 C102 120.6(2) . . ? C12 C62 C102 121.3(2) . . ? C92 C72 C82 110.1(2) . . ? C92 C72 C22 111.7(2) . . ? C82 C72 C22 113.7(2) . . ? C112 C102 C62 110.0(2) . . ? C112 C102 C122 111.5(3) . . ? C62 C102 C122 113.6(2) . . ? Si1 N1 Si1 109.97(19) 3_656 . ? Si1 N1 Fe1 125.01(10) 3_656 . ? Si1 N1 Fe1 125.01(10) . . ? C4A C4A Si1 106.8(5) 3_656 . ? C4B C4B Si1 104.3(4) 3_656 . ? _refine_diff_density_max 0.982 _refine_diff_density_min -0.735 _refine_diff_density_rms 0.060 _shelx_res_file ; 007a-22067.res created by SHELXL-2014/7 TITL 007a-22067 CELL 1.54184 10.1151 17.6923 20.5843 90 90 90 ZERR 4 0.0001 0.0002 0.0003 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Fe N Si UNIT 140 228 4 12 8 SIMU C4A C4B C24 C34 L.S. 30 PLAN 20 SIZE 0.2 0.2 0.02 TEMP -180 list 4 fmap 2 53 ACTA WGHT 0.063400 4.065600 FVAR 0.48384 FE1 3 0.500000 0.672131 0.750000 10.50000 0.02428 0.01647 = 0.01848 0.00000 -0.00047 0.00000 SI1 5 0.411856 0.836999 0.805362 11.00000 0.05283 0.02075 = 0.05786 0.00198 0.02087 0.00671 N11 4 0.472407 0.595897 0.680374 11.00000 0.02284 0.01935 = 0.01884 0.00173 -0.00309 0.00011 C11 1 0.431107 0.468320 0.636291 11.00000 0.04012 0.02189 = 0.02447 -0.00055 -0.00568 -0.00468 AFIX 137 H11A 2 0.352940 0.487969 0.613797 11.00000 -1.50000 H11B 2 0.411298 0.418262 0.654199 11.00000 -1.50000 H11C 2 0.504727 0.464333 0.605532 11.00000 -1.50000 AFIX 0 C21 1 0.468686 0.521390 0.690826 11.00000 0.02395 0.02101 = 0.01928 -0.00187 -0.00003 0.00001 C31 1 0.500000 0.487717 0.750000 10.50000 0.03052 0.01592 = 0.02177 0.00000 -0.00109 0.00000 AFIX 43 H31 2 0.500001 0.434022 0.750000 10.50000 -1.20000 AFIX 0 C12 1 0.452117 0.622122 0.615220 11.00000 0.02735 0.01810 = 0.01828 0.00012 -0.00261 -0.00331 C22 1 0.332892 0.658557 0.599550 11.00000 0.02695 0.02271 = 0.02851 0.00228 -0.00475 -0.00282 C32 1 0.315261 0.682895 0.535699 11.00000 0.03305 0.02880 = 0.02740 0.00403 -0.00826 -0.00048 AFIX 43 H32 2 0.234525 0.706511 0.523701 11.00000 -1.20000 AFIX 0 C42 1 0.412539 0.673347 0.489803 11.00000 0.04493 0.02754 = 0.02139 0.00319 -0.00658 -0.00441 AFIX 43 H42 2 0.398155 0.689799 0.446444 11.00000 -1.20000 AFIX 0 C52 1 0.531228 0.639883 0.506543 11.00000 0.03843 0.02364 = 0.02212 -0.00261 0.00352 -0.00407 AFIX 43 H52 2 0.598693 0.634998 0.474711 11.00000 -1.20000 AFIX 0 C62 1 0.553593 0.613324 0.568930 11.00000 0.03003 0.01950 = 0.02124 -0.00260 -0.00063 -0.00361 C72 1 0.226776 0.670293 0.650798 11.00000 0.02856 0.03723 = 0.03065 0.00432 -0.00111 0.00329 AFIX 13 H72 2 0.273166 0.683290 0.692218 11.00000 -1.20000 AFIX 0 C82 1 0.133356 0.735115 0.635791 11.00000 0.03704 0.04002 = 0.04788 0.00234 0.00325 0.00751 AFIX 137 H82A 2 0.184669 0.780995 0.627086 11.00000 -1.50000 H82B 2 0.074988 0.743735 0.673061 11.00000 -1.50000 H82C 2 0.080091 0.722471 0.597537 11.00000 -1.50000 AFIX 0 C92 1 0.148965 0.598517 0.663264 11.00000 0.03416 0.04343 = 0.06827 0.01637 0.01304 0.00254 AFIX 137 H92A 2 0.109781 0.580773 0.622481 11.00000 -1.50000 H92B 2 0.078644 0.608808 0.694797 11.00000 -1.50000 H92C 2 0.208166 0.559568 0.680574 11.00000 -1.50000 AFIX 0 C102 1 0.686720 0.579237 0.587284 11.00000 0.03016 0.02748 = 0.02752 -0.00261 0.00136 0.00097 AFIX 13 H102 2 0.671239 0.544944 0.625144 11.00000 -1.20000 AFIX 0 C112 1 0.779297 0.640478 0.609723 11.00000 0.03835 0.04545 = 0.11200 -0.01647 -0.02604 -0.00016 AFIX 137 H11D 2 0.799808 0.674080 0.573241 11.00000 -1.50000 H11E 2 0.861109 0.617626 0.625991 11.00000 -1.50000 H11F 2 0.737269 0.669613 0.644551 11.00000 -1.50000 AFIX 0 C122 1 0.748286 0.531687 0.533525 11.00000 0.04872 0.04802 = 0.03974 -0.00364 0.00842 0.01629 AFIX 137 H12A 2 0.683817 0.494356 0.518245 11.00000 -1.50000 H12B 2 0.826535 0.505571 0.550385 11.00000 -1.50000 H12C 2 0.774117 0.564540 0.497357 11.00000 -1.50000 AFIX 0 N1 4 0.500000 0.779703 0.750000 10.50000 0.03076 0.02824 = 0.07125 0.00000 0.00917 0.00000 C24 1 0.453810 0.825046 0.892304 11.00000 0.05650 0.05311 = 0.06052 -0.00789 0.01052 0.01227 AFIX 137 H24A 2 0.432222 0.773450 0.905996 11.00000 -1.50000 H24B 2 0.402915 0.861174 0.918321 11.00000 -1.50000 H24C 2 0.548499 0.834186 0.898616 11.00000 -1.50000 AFIX 0 C34 1 0.230645 0.826357 0.796335 11.00000 0.05709 0.08030 = 0.05348 0.01626 0.01349 0.03833 AFIX 137 H34A 2 0.205206 0.837851 0.751471 11.00000 -1.50000 H34B 2 0.185633 0.861271 0.825946 11.00000 -1.50000 H34C 2 0.205204 0.774317 0.806810 11.00000 -1.50000 AFIX 0 PART 1 C4A 1 0.432661 0.934862 0.767861 10.50000 0.08225 0.02854 = 0.06112 -0.00087 0.00979 0.00883 AFIX 23 H4AA 2 0.359984 0.945311 0.736926 10.50000 -1.20000 H4AB 2 0.431586 0.974146 0.802107 10.50000 -1.20000 AFIX 0 PART 0 PART 2 C4B 1 0.490236 0.931293 0.787512 10.50000 0.07649 0.01798 = 0.03490 -0.00004 0.01436 -0.00303 AFIX 23 H4BA 2 0.431652 0.973228 0.801123 10.50000 -1.20000 H4BB 2 0.576088 0.936310 0.810201 10.50000 -1.20000 AFIX 0 HKLF 4 REM 007a-22067 REM R1 = 0.0488 for 2998 Fo > 4sig(Fo) and 0.0521 for all 3248 data REM 203 parameters refined using 6 restraints END WGHT 0.0634 4.0672 REM Highest difference peak 0.982, deepest hole -0.735, 1-sigma level 0.060 Q1 1 0.4868 0.7599 0.7079 11.00000 0.05 0.98 Q2 1 0.4430 0.8355 0.8424 11.00000 0.05 0.71 Q3 1 0.4490 0.8832 0.8031 11.00000 0.05 0.38 Q4 1 0.4668 0.7954 0.7542 11.00000 0.05 0.35 Q5 1 0.7934 0.6578 0.5643 11.00000 0.05 0.25 Q6 1 0.4956 0.5594 0.6823 11.00000 0.05 0.22 Q7 1 0.6164 0.5940 0.5796 11.00000 0.05 0.22 Q8 1 0.3331 0.8233 0.8035 11.00000 0.05 0.22 Q9 1 0.5229 0.6204 0.6950 11.00000 0.05 0.21 Q10 1 0.6057 0.6758 0.7418 11.00000 0.05 0.21 Q11 1 0.1940 0.6356 0.6529 11.00000 0.05 0.20 Q12 1 0.4708 0.5032 0.6617 11.00000 0.05 0.20 Q13 1 0.2947 0.8368 0.8195 11.00000 0.05 0.19 Q14 1 0.4747 0.8382 0.9337 11.00000 0.05 0.19 Q15 1 0.4535 0.6017 0.6529 11.00000 0.05 0.19 Q16 1 0.5264 0.8174 0.8003 11.00000 0.05 0.18 Q17 1 0.5101 0.6248 0.5933 11.00000 0.05 0.18 Q18 1 0.4743 0.6566 0.5019 11.00000 0.05 0.18 Q19 1 0.1768 0.6974 0.6426 11.00000 0.05 0.18 Q20 1 0.4783 0.5121 0.7200 11.00000 0.05 0.18 ; _shelx_res_checksum 87824 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-21112 _database_code_depnum_ccdc_archive 'CCDC 2226339' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ' C36 H48 Fe N2, C20 H40 K O8' _chemical_formula_sum 'C56 H88 Fe K N2 O8' _chemical_formula_weight 1012.23 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.3868 1.0657 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.0503(6) _cell_length_b 13.4395(6) _cell_length_c 20.4096(7) _cell_angle_alpha 83.732(3) _cell_angle_beta 71.934(4) _cell_angle_gamma 66.707(4) _cell_volume 3125.4(3) _cell_formula_units_Z 2 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 34589 _cell_measurement_theta_min 2.1600 _cell_measurement_theta_max 66.6690 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.076 _exptl_crystal_F_000 1094 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_absorpt_coefficient_mu 2.897 _shelx_estimated_absorpt_T_min 0.595 _shelx_estimated_absorpt_T_max 0.760 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.75467 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 112250 _diffrn_reflns_av_unetI/netI 0.0340 _diffrn_reflns_av_R_equivalents 0.0757 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 2.277 _diffrn_reflns_theta_max 66.559 _diffrn_reflns_theta_full 66.559 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measured_fraction_theta_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_point_group_measured_fraction_full 0.986 _reflns_number_total 10888 _reflns_number_gt 8540 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. One THF coordinated to the 18-crown-6 is disordered over two positions. The disordered, chemically equivalent C-C distances were restrained to be similar. The disordered thermal parameters were also restrained to be similar. The site occupancies were freely refined and converged near populations of 0.75/0.25. The program SQUEEZE (see A.L.Spek, J. Appl. Cryst. 2015, C71, 9-18) was used to compensate for the contribution of disordered solvents contained in voids within the crystal lattice from the diffraction intensities. This procedure was applied to the data file and the submitted model is based on the solvent removed data. The total electron density found in the voids was 95 e/A^3^. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1219P)^2^+3.0830P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 10888 _refine_ls_number_parameters 645 _refine_ls_number_restraints 75 _refine_ls_R_factor_all 0.0901 _refine_ls_R_factor_gt 0.0734 _refine_ls_wR_factor_ref 0.2118 _refine_ls_wR_factor_gt 0.1986 _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_restrained_S_all 1.046 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.71537(5) 0.55917(4) 0.25503(3) 0.03704(18) Uani 1 1 d . . . . . N11 N 0.7476(3) 0.6625(2) 0.29513(15) 0.0365(7) Uani 1 1 d . . . . . N21 N 0.5979(3) 0.6589(2) 0.21632(15) 0.0377(7) Uani 1 1 d . . . . . C11 C 0.7181(4) 0.8456(3) 0.32924(19) 0.0429(9) Uani 1 1 d . . . . . H11A H 0.7060 0.8275 0.3781 0.064 Uiso 1 1 calc R U . . . H11B H 0.6675 0.9211 0.3248 0.064 Uiso 1 1 calc R U . . . H11C H 0.7998 0.8361 0.3077 0.064 Uiso 1 1 calc R U . . . C21 C 0.6887(3) 0.7719(3) 0.29384(17) 0.0354(8) Uani 1 1 d . . . . . C31 C 0.6028(3) 0.8178(3) 0.26013(18) 0.0390(8) Uani 1 1 d . . . . . H31 H 0.5679 0.8947 0.2623 0.047 Uiso 1 1 calc R U . . . C41 C 0.5594(3) 0.7683(3) 0.22337(19) 0.0400(8) Uani 1 1 d . . . . . C51 C 0.4683(4) 0.8409(3) 0.1898(2) 0.0593(12) Uani 1 1 d . . . . . H51A H 0.5009 0.8329 0.1396 0.089 Uiso 1 1 calc R U . . . H51B H 0.4446 0.9164 0.2032 0.089 Uiso 1 1 calc R U . . . H51C H 0.4003 0.8206 0.2048 0.089 Uiso 1 1 calc R U . . . C12 C 0.8429(3) 0.6203(3) 0.32417(18) 0.0376(8) Uani 1 1 d . . . . . C72 C 0.8232(3) 0.5912(3) 0.39452(19) 0.0391(8) Uani 1 1 d . . . . . C32 C 0.9197(4) 0.5395(3) 0.4191(2) 0.0447(9) Uani 1 1 d . . . . . H32 H 0.9080 0.5186 0.4660 0.054 Uiso 1 1 calc R U . . . C42 C 1.0320(4) 0.5179(3) 0.3767(2) 0.0509(10) Uani 1 1 d . . . . . H42 H 1.0966 0.4828 0.3944 0.061 Uiso 1 1 calc R U . . . C52 C 1.0497(4) 0.5476(4) 0.3087(2) 0.0546(11) Uani 1 1 d . . . . . H52 H 1.1270 0.5325 0.2797 0.065 Uiso 1 1 calc R U . . . C62 C 0.9564(4) 0.5994(4) 0.2816(2) 0.0496(10) Uani 1 1 d . . . . . C82 C 0.7013(4) 0.6125(3) 0.44121(19) 0.0433(9) Uani 1 1 d . . . . . H82 H 0.6457 0.6660 0.4178 0.052 Uiso 1 1 calc R U . . . C102 C 0.6784(4) 0.6620(4) 0.5109(2) 0.0551(11) Uani 1 1 d . . . . . H10A H 0.7289 0.6098 0.5363 0.083 Uiso 1 1 calc R U . . . H10B H 0.5965 0.6798 0.5376 0.083 Uiso 1 1 calc R U . . . H10C H 0.6950 0.7280 0.5036 0.083 Uiso 1 1 calc R U . . . C92 C 0.6757(4) 0.5085(4) 0.4511(2) 0.0547(11) Uani 1 1 d . . . . . H92A H 0.6846 0.4815 0.4062 0.082 Uiso 1 1 calc R U . . . H92B H 0.5958 0.5246 0.4807 0.082 Uiso 1 1 calc R U . . . H92C H 0.7306 0.4534 0.4727 0.082 Uiso 1 1 calc R U . . . C112 C 0.9799(4) 0.6312(5) 0.2058(2) 0.0630(13) Uani 1 1 d . . . . . H112 H 0.9028 0.6751 0.1977 0.076 Uiso 1 1 calc R U . . . C132 C 1.0530(4) 0.6997(4) 0.1858(2) 0.0648(12) Uani 1 1 d . . . . . H13A H 1.0179 0.7619 0.2176 0.097 Uiso 1 1 calc R U . . . H13B H 1.0563 0.7254 0.1387 0.097 Uiso 1 1 calc R U . . . H13C H 1.1322 0.6560 0.1883 0.097 Uiso 1 1 calc R U . . . C122 C 1.0379(7) 0.5299(7) 0.1587(3) 0.121(3) Uani 1 1 d . . . . . H12A H 1.1113 0.4826 0.1679 0.182 Uiso 1 1 calc R U . . . H12B H 1.0539 0.5519 0.1104 0.182 Uiso 1 1 calc R U . . . H12C H 0.9856 0.4908 0.1678 0.182 Uiso 1 1 calc R U . . . C13 C 0.5427(3) 0.6143(3) 0.18343(18) 0.0374(8) Uani 1 1 d . . . . . C23 C 0.4431(3) 0.5944(3) 0.22276(19) 0.0415(8) Uani 1 1 d . . . . . C33 C 0.3992(4) 0.5393(3) 0.1915(2) 0.0481(9) Uani 1 1 d . . . . . H33 H 0.3328 0.5244 0.2177 0.058 Uiso 1 1 calc R U . . . C43 C 0.4504(4) 0.5060(3) 0.1230(2) 0.0483(10) Uani 1 1 d . . . . . H43 H 0.4203 0.4672 0.1029 0.058 Uiso 1 1 calc R U . . . C53 C 0.5451(4) 0.5291(3) 0.0844(2) 0.0454(9) Uani 1 1 d . . . . . H53 H 0.5790 0.5070 0.0373 0.054 Uiso 1 1 calc R U . . . C63 C 0.5925(3) 0.5844(3) 0.11270(19) 0.0403(8) Uani 1 1 d . . . . . C73 C 0.3852(4) 0.6289(3) 0.2975(2) 0.0476(9) Uani 1 1 d . . . . . H73 H 0.4246 0.6726 0.3085 0.057 Uiso 1 1 calc R U . . . C93 C 0.2560(4) 0.7027(4) 0.3103(3) 0.0696(14) Uani 1 1 d . . . . . H93A H 0.2482 0.7594 0.2755 0.104 Uiso 1 1 calc R U . . . H93B H 0.2252 0.7360 0.3563 0.104 Uiso 1 1 calc R U . . . H93C H 0.2120 0.6596 0.3072 0.104 Uiso 1 1 calc R U . . . C83 C 0.4018(5) 0.5328(4) 0.3445(2) 0.0720(14) Uani 1 1 d . . . . . H83A H 0.3702 0.4846 0.3324 0.108 Uiso 1 1 calc R U . . . H83B H 0.3608 0.5579 0.3924 0.108 Uiso 1 1 calc R U . . . H83C H 0.4852 0.4935 0.3393 0.108 Uiso 1 1 calc R U . . . C103 C 0.6965(4) 0.6091(3) 0.06847(19) 0.0427(9) Uani 1 1 d . . . . . H103 H 0.7046 0.6638 0.0940 0.051 Uiso 1 1 calc R U . . . C123 C 0.6802(5) 0.6579(4) -0.0005(2) 0.0639(12) Uani 1 1 d . . . . . H12D H 0.6727 0.6057 -0.0268 0.096 Uiso 1 1 calc R U . . . H12E H 0.7480 0.6750 -0.0266 0.096 Uiso 1 1 calc R U . . . H12F H 0.6096 0.7243 0.0076 0.096 Uiso 1 1 calc R U . . . C113 C 0.8096(4) 0.5087(3) 0.0558(2) 0.0534(10) Uani 1 1 d . . . . . H11D H 0.8236 0.4812 0.1000 0.080 Uiso 1 1 calc R U . . . H11E H 0.8747 0.5278 0.0271 0.080 Uiso 1 1 calc R U . . . H11F H 0.8031 0.4528 0.0322 0.080 Uiso 1 1 calc R U . . . C2 C 0.8012(4) 0.3930(3) 0.2532(2) 0.0488(10) Uani 1 1 d . . . . . H2A H 0.8588 0.3709 0.2073 0.059 Uiso 1 1 calc R U . . . H2B H 0.8452 0.3738 0.2876 0.059 Uiso 1 1 calc R U . . . C34 C 0.7276(4) 0.3293(3) 0.2674(2) 0.0451(9) Uani 1 1 d . . . . . C35 C 0.7082(4) 0.2708(3) 0.3284(2) 0.0566(11) Uani 1 1 d . . . . . H35 H 0.7450 0.2713 0.3619 0.068 Uiso 1 1 calc R U . . . C36 C 0.6376(5) 0.2133(4) 0.3411(2) 0.0673(14) Uani 1 1 d . . . . . H36 H 0.6275 0.1742 0.3828 0.081 Uiso 1 1 calc R U . . . C37 C 0.5810(5) 0.2112(4) 0.2945(3) 0.0682(13) Uani 1 1 d . . . . . H37 H 0.5307 0.1726 0.3042 0.082 Uiso 1 1 calc R U . . . C38 C 0.5991(4) 0.2662(4) 0.2338(3) 0.0622(12) Uani 1 1 d . . . . . H38 H 0.5621 0.2644 0.2008 0.075 Uiso 1 1 calc R U . . . C39 C 0.6708(4) 0.3244(3) 0.2201(2) 0.0488(10) Uani 1 1 d . . . . . H39 H 0.6817 0.3618 0.1778 0.059 Uiso 1 1 calc R U . . . K1 K 1.0000 0.0000 0.0000 0.0556(4) Uani 1 2 d S . P A . O10 O 0.9130(3) 0.0949(2) 0.12831(13) 0.0505(7) Uani 1 1 d . . . . . O20 O 1.0866(3) 0.1488(2) 0.02986(13) 0.0523(7) Uani 1 1 d . . . . . O30 O 1.1372(3) 0.0824(2) -0.10670(14) 0.0564(8) Uani 1 1 d . . . . . O40 O 1.1694(4) -0.1601(4) 0.0312(2) 0.0974(10) Uani 1 1 d D U . . . C10 C 0.8661(4) 0.0358(4) 0.1834(2) 0.0539(11) Uani 1 1 d . . . . . H10D H 0.8197 0.0834 0.2247 0.065 Uiso 1 1 calc R U . . . H10E H 0.9303 -0.0258 0.1954 0.065 Uiso 1 1 calc R U . . . C20 C 0.9800(4) 0.1435(3) 0.1466(2) 0.0496(10) Uani 1 1 d . . . . . H20A H 1.0517 0.0868 0.1541 0.060 Uiso 1 1 calc R U . . . H20B H 0.9341 0.1868 0.1897 0.060 Uiso 1 1 calc R U . . . C30 C 1.0113(4) 0.2149(3) 0.0890(2) 0.0511(10) Uani 1 1 d . . . . . H30A H 0.9398 0.2677 0.0788 0.061 Uiso 1 1 calc R U . . . H30B H 1.0508 0.2556 0.1022 0.061 Uiso 1 1 calc R U . . . C40 C 1.1140(5) 0.2121(4) -0.0287(2) 0.0653(14) Uani 1 1 d . . . . . H40A H 1.1493 0.2593 -0.0184 0.078 Uiso 1 1 calc R U . . . H40B H 1.0422 0.2585 -0.0411 0.078 Uiso 1 1 calc R U . . . C50 C 1.1986(5) 0.1356(5) -0.0874(2) 0.0706(15) Uani 1 1 d . . . . . H50A H 1.2292 0.1761 -0.1268 0.085 Uiso 1 1 calc R U . . . H50B H 1.2650 0.0820 -0.0727 0.085 Uiso 1 1 calc R U . . . C60 C 1.2100(4) 0.0056(4) -0.1615(2) 0.0594(12) Uani 1 1 d . . . . . H60A H 1.2702 -0.0551 -0.1457 0.071 Uiso 1 1 calc R U . . . H60B H 1.2496 0.0405 -0.2007 0.071 Uiso 1 1 calc R U . . . C64B C 1.2374(18) -0.1760(19) 0.0831(9) 0.0953(13) Uani 0.338(11) 1 d D U P A 1 H64A H 1.1897 -0.1327 0.1260 0.114 Uiso 0.338(11) 1 calc R U P A 1 H64B H 1.2755 -0.2531 0.0940 0.114 Uiso 0.338(11) 1 calc R U P A 1 C90 C 1.3407(9) -0.2008(10) 0.0600(5) 0.0958(13) Uani 0.662(11) 1 d D U P A 2 H90A H 1.3523 -0.2626 0.0918 0.115 Uiso 0.662(11) 1 calc R U P A 2 H90B H 1.3912 -0.1628 0.0616 0.115 Uiso 0.662(11) 1 calc R U P A 2 C80 C 1.3667(6) -0.2406(6) -0.0181(4) 0.0985(12) Uani 1 1 d D U . . . H80C H 1.3817 -0.1865 -0.0527 0.118 Uiso 0.662(11) 1 calc R U P A 2 H80D H 1.4327 -0.3115 -0.0299 0.118 Uiso 0.662(11) 1 calc R U P A 2 H80A H 1.4039 -0.2245 -0.0660 0.118 Uiso 0.338(11) 1 calc R U P A 1 H80B H 1.4214 -0.3074 -0.0030 0.118 Uiso 0.338(11) 1 calc R U P A 1 C70 C 1.2607(6) -0.2479(5) -0.0113(4) 0.0945(12) Uani 1 1 d . U . . . H70A H 1.2603 -0.3177 0.0099 0.113 Uiso 1 1 calc R U . . . H70B H 1.2488 -0.2446 -0.0572 0.113 Uiso 1 1 calc R U . . . K2 K 0.0000 1.0000 0.5000 0.0436(3) Uani 1 2 d S . P . . O50 O 0.0195(3) 0.9157(2) 0.62785(13) 0.0477(7) Uani 1 1 d . . . . . O60 O -0.0483(3) 0.8119(2) 0.54668(14) 0.0486(7) Uani 1 1 d . . . . . O70 O -0.0191(2) 0.8750(2) 0.40994(13) 0.0445(6) Uani 1 1 d . . . . . O80 O 0.2303(3) 0.8951(3) 0.44292(18) 0.0717(9) Uani 1 1 d . . . . . C110 C -0.0160(5) 0.9991(4) 0.6763(2) 0.0584(12) Uani 1 1 d . . . . . H11G H -0.0018 0.9673 0.7203 0.070 Uiso 1 1 calc R U . . . H11H H -0.1005 1.0427 0.6854 0.070 Uiso 1 1 calc R U . . . C120 C -0.0324(5) 0.8393(3) 0.6550(2) 0.0564(11) Uani 1 1 d . . . . . H12G H -0.1183 0.8767 0.6711 0.068 Uiso 1 1 calc R U . . . H12H H -0.0053 0.8024 0.6947 0.068 Uiso 1 1 calc R U . . . C130 C 0.0009(5) 0.7577(3) 0.5999(2) 0.0597(12) Uani 1 1 d . . . . . H13D H 0.0869 0.7237 0.5814 0.072 Uiso 1 1 calc R U . . . H13E H -0.0288 0.7001 0.6192 0.072 Uiso 1 1 calc R U . . . C140 C -0.0252(4) 0.7389(3) 0.4928(2) 0.0521(11) Uani 1 1 d . . . . . H14A H -0.0603 0.6847 0.5115 0.063 Uiso 1 1 calc R U . . . H14B H 0.0600 0.7000 0.4732 0.063 Uiso 1 1 calc R U . . . C150 C -0.0764(4) 0.8026(3) 0.4380(2) 0.0476(10) Uani 1 1 d . . . . . H15A H -0.0651 0.7533 0.4015 0.057 Uiso 1 1 calc R U . . . H15B H -0.1611 0.8438 0.4579 0.057 Uiso 1 1 calc R U . . . C160 C -0.0518(5) 0.9299(4) 0.3518(2) 0.0571(11) Uani 1 1 d . . . . . H16A H -0.1365 0.9746 0.3653 0.069 Uiso 1 1 calc R U . . . H16B H -0.0351 0.8768 0.3161 0.069 Uiso 1 1 calc R U . . . C200 C 0.3133(6) 0.9366(6) 0.4029(4) 0.102(2) Uani 1 1 d . . . . . H20C H 0.2807 1.0168 0.4016 0.122 Uiso 1 1 calc R U . . . H20D H 0.3493 0.9061 0.3555 0.122 Uiso 1 1 calc R U . . . C190 C 0.4051(6) 0.8889(8) 0.4510(5) 0.135(3) Uani 1 1 d . . . . . H19A H 0.4847 0.8854 0.4259 0.162 Uiso 1 1 calc R U . . . H19B H 0.3756 0.9290 0.4952 0.162 Uiso 1 1 calc R U . . . C180 C 0.3963(7) 0.7739(8) 0.4598(4) 0.122(3) Uani 1 1 d . . . . . H18A H 0.4375 0.7307 0.4164 0.147 Uiso 1 1 calc R U . . . H18B H 0.4284 0.7327 0.4970 0.147 Uiso 1 1 calc R U . . . C170 C 0.2720(7) 0.8025(7) 0.4778(4) 0.117(3) Uani 1 1 d . . . . . H17A H 0.2548 0.7440 0.4638 0.141 Uiso 1 1 calc R U . . . H17B H 0.2360 0.8152 0.5281 0.141 Uiso 1 1 calc R U . . . C100 C 1.2184(8) -0.1271(10) 0.0768(6) 0.0946(13) Uani 0.662(11) 1 d D U P A 2 H10F H 1.2115 -0.0511 0.0684 0.114 Uiso 0.662(11) 1 calc R U P A 2 H10G H 1.1773 -0.1338 0.1258 0.114 Uiso 0.662(11) 1 calc R U P A 2 C65A C 1.3194(18) -0.1316(16) 0.0377(9) 0.0956(13) Uani 0.338(11) 1 d D U P A 1 H65A H 1.3794 -0.1311 0.0575 0.115 Uiso 0.338(11) 1 calc R U P A 1 H65B H 1.2817 -0.0602 0.0185 0.115 Uiso 0.338(11) 1 calc R U P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0492(4) 0.0336(3) 0.0354(3) -0.0055(2) -0.0194(3) -0.0163(3) N11 0.0425(17) 0.0389(16) 0.0344(15) -0.0048(12) -0.0145(13) -0.0181(13) N21 0.0477(18) 0.0399(16) 0.0330(15) -0.0082(12) -0.0150(13) -0.0199(14) C11 0.054(2) 0.043(2) 0.0387(19) -0.0076(16) -0.0147(17) -0.0233(18) C21 0.046(2) 0.0352(18) 0.0284(16) -0.0058(14) -0.0070(15) -0.0198(16) C31 0.054(2) 0.0335(18) 0.0339(18) -0.0041(14) -0.0156(17) -0.0177(16) C41 0.052(2) 0.0370(19) 0.0370(19) -0.0015(15) -0.0187(17) -0.0182(17) C51 0.084(3) 0.037(2) 0.068(3) -0.0021(19) -0.049(3) -0.013(2) C12 0.048(2) 0.0378(18) 0.0361(18) -0.0076(15) -0.0191(17) -0.0180(16) C72 0.051(2) 0.0326(18) 0.0403(19) -0.0065(15) -0.0184(17) -0.0170(16) C32 0.069(3) 0.0336(19) 0.047(2) 0.0010(16) -0.033(2) -0.0231(18) C42 0.057(3) 0.040(2) 0.068(3) -0.0091(19) -0.037(2) -0.0134(18) C52 0.047(2) 0.067(3) 0.056(3) -0.023(2) -0.017(2) -0.020(2) C62 0.046(2) 0.067(3) 0.040(2) -0.0202(19) -0.0132(18) -0.021(2) C82 0.059(2) 0.043(2) 0.0343(19) -0.0001(16) -0.0171(18) -0.0237(18) C102 0.074(3) 0.056(3) 0.041(2) -0.0069(19) -0.015(2) -0.030(2) C92 0.070(3) 0.054(2) 0.049(2) -0.0045(19) -0.013(2) -0.035(2) C112 0.046(2) 0.114(4) 0.034(2) -0.017(2) -0.0054(18) -0.035(3) C132 0.068(3) 0.078(3) 0.052(3) -0.005(2) -0.023(2) -0.025(3) C122 0.175(7) 0.173(7) 0.050(3) -0.051(4) 0.020(4) -0.127(6) C13 0.045(2) 0.0334(18) 0.0375(18) -0.0046(14) -0.0192(16) -0.0127(16) C23 0.044(2) 0.041(2) 0.040(2) -0.0094(16) -0.0155(17) -0.0122(17) C33 0.045(2) 0.056(2) 0.049(2) -0.0106(19) -0.0153(18) -0.0221(19) C43 0.057(3) 0.050(2) 0.048(2) -0.0131(18) -0.024(2) -0.021(2) C53 0.058(2) 0.043(2) 0.042(2) -0.0081(16) -0.0209(19) -0.0190(19) C63 0.052(2) 0.0349(18) 0.0356(18) -0.0036(15) -0.0181(17) -0.0136(17) C73 0.048(2) 0.056(2) 0.043(2) -0.0102(18) -0.0100(18) -0.0240(19) C93 0.056(3) 0.076(3) 0.067(3) -0.032(3) -0.012(2) -0.011(2) C83 0.085(4) 0.068(3) 0.045(2) -0.007(2) -0.004(2) -0.020(3) C103 0.061(3) 0.039(2) 0.0347(19) -0.0022(15) -0.0173(18) -0.0232(18) C123 0.090(4) 0.069(3) 0.046(2) 0.012(2) -0.030(2) -0.039(3) C113 0.058(3) 0.052(2) 0.048(2) -0.0035(19) -0.010(2) -0.023(2) C2 0.064(3) 0.037(2) 0.047(2) -0.0059(17) -0.023(2) -0.0147(19) C34 0.059(2) 0.0351(19) 0.040(2) -0.0077(15) -0.0170(18) -0.0125(18) C35 0.084(3) 0.042(2) 0.039(2) -0.0047(17) -0.018(2) -0.018(2) C36 0.088(4) 0.051(3) 0.049(3) -0.003(2) -0.001(2) -0.027(3) C37 0.072(3) 0.057(3) 0.075(3) -0.008(2) -0.006(3) -0.034(3) C38 0.072(3) 0.051(3) 0.069(3) -0.007(2) -0.026(3) -0.023(2) C39 0.062(3) 0.044(2) 0.046(2) -0.0065(17) -0.019(2) -0.0223(19) K1 0.0988(11) 0.0399(6) 0.0338(6) -0.0019(5) -0.0171(6) -0.0336(7) O10 0.080(2) 0.0486(15) 0.0318(13) -0.0034(11) -0.0142(13) -0.0343(15) O20 0.085(2) 0.0430(15) 0.0360(14) -0.0007(11) -0.0145(14) -0.0336(15) O30 0.085(2) 0.0608(18) 0.0361(14) -0.0038(13) -0.0128(14) -0.0430(17) O40 0.101(2) 0.092(2) 0.093(2) -0.0275(17) -0.0375(17) -0.0160(18) C10 0.077(3) 0.054(2) 0.033(2) -0.0046(17) -0.012(2) -0.029(2) C20 0.072(3) 0.045(2) 0.036(2) -0.0110(16) -0.0144(19) -0.025(2) C30 0.075(3) 0.039(2) 0.044(2) -0.0065(17) -0.018(2) -0.023(2) C40 0.119(4) 0.061(3) 0.044(2) 0.007(2) -0.026(3) -0.064(3) C50 0.107(4) 0.087(4) 0.043(2) 0.001(2) -0.014(3) -0.069(3) C60 0.078(3) 0.071(3) 0.036(2) -0.006(2) -0.009(2) -0.039(3) C64B 0.101(2) 0.092(2) 0.091(2) -0.031(2) -0.040(2) -0.017(2) C90 0.102(2) 0.092(2) 0.091(2) -0.032(2) -0.041(2) -0.015(2) C80 0.103(2) 0.092(2) 0.094(2) -0.0319(19) -0.038(2) -0.016(2) C70 0.100(2) 0.089(2) 0.094(2) -0.0335(19) -0.041(2) -0.016(2) K2 0.0687(8) 0.0325(5) 0.0403(6) -0.0024(4) -0.0284(6) -0.0200(5) O50 0.0736(19) 0.0375(14) 0.0422(14) -0.0033(11) -0.0268(14) -0.0231(13) O60 0.0735(19) 0.0358(13) 0.0475(15) -0.0052(11) -0.0303(14) -0.0211(13) O70 0.0649(17) 0.0404(14) 0.0416(14) -0.0042(11) -0.0242(13) -0.0259(13) O80 0.074(2) 0.071(2) 0.061(2) 0.0042(17) -0.0152(18) -0.0241(18) C110 0.094(4) 0.059(3) 0.040(2) -0.0085(19) -0.020(2) -0.045(3) C120 0.097(4) 0.045(2) 0.044(2) 0.0030(18) -0.032(2) -0.036(2) C130 0.106(4) 0.041(2) 0.051(2) 0.0044(18) -0.045(3) -0.033(2) C140 0.082(3) 0.035(2) 0.050(2) -0.0080(17) -0.031(2) -0.022(2) C150 0.067(3) 0.039(2) 0.051(2) -0.0052(17) -0.027(2) -0.0250(19) C160 0.091(3) 0.063(3) 0.043(2) 0.0016(19) -0.032(2) -0.046(3) C200 0.073(4) 0.100(5) 0.100(5) 0.017(4) -0.002(4) -0.021(4) C190 0.072(5) 0.177(9) 0.157(8) 0.059(7) -0.032(5) -0.063(5) C180 0.104(6) 0.180(9) 0.084(5) -0.001(5) -0.044(4) -0.043(6) C170 0.102(6) 0.110(6) 0.087(5) -0.005(4) -0.017(4) 0.009(4) C100 0.101(2) 0.090(2) 0.090(2) -0.0310(19) -0.0401(19) -0.016(2) C65A 0.101(2) 0.091(2) 0.091(2) -0.031(2) -0.040(2) -0.017(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N21 1.914(3) . ? Fe1 N11 1.923(3) . ? Fe1 C2 2.064(4) . ? N11 C21 1.366(5) . ? N11 C12 1.430(4) . ? N21 C41 1.361(5) . ? N21 C13 1.435(4) . ? C11 C21 1.509(5) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C21 C31 1.396(5) . ? C31 C41 1.413(5) . ? C31 H31 0.9500 . ? C41 C51 1.508(5) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C12 C62 1.398(6) . ? C12 C72 1.417(5) . ? C72 C32 1.394(5) . ? C72 C82 1.510(6) . ? C32 C42 1.384(6) . ? C32 H32 0.9500 . ? C42 C52 1.375(6) . ? C42 H42 0.9500 . ? C52 C62 1.392(6) . ? C52 H52 0.9500 . ? C62 C112 1.527(6) . ? C82 C102 1.531(5) . ? C82 C92 1.539(5) . ? C82 H82 1.0000 . ? C102 H10A 0.9800 . ? C102 H10B 0.9800 . ? C102 H10C 0.9800 . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C112 C132 1.515(7) . ? C112 C122 1.539(8) . ? C112 H112 1.0000 . ? C132 H13A 0.9800 . ? C132 H13B 0.9800 . ? C132 H13C 0.9800 . ? C122 H12A 0.9800 . ? C122 H12B 0.9800 . ? C122 H12C 0.9800 . ? C13 C23 1.410(5) . ? C13 C63 1.416(5) . ? C23 C33 1.396(5) . ? C23 C73 1.509(5) . ? C33 C43 1.386(6) . ? C33 H33 0.9500 . ? C43 C53 1.375(6) . ? C43 H43 0.9500 . ? C53 C63 1.396(5) . ? C53 H53 0.9500 . ? C63 C103 1.516(6) . ? C73 C83 1.507(7) . ? C73 C93 1.535(6) . ? C73 H73 1.0000 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? C103 C123 1.527(5) . ? C103 C113 1.526(6) . ? C103 H103 1.0000 . ? C123 H12D 0.9800 . ? C123 H12E 0.9800 . ? C123 H12F 0.9800 . ? C113 H11D 0.9800 . ? C113 H11E 0.9800 . ? C113 H11F 0.9800 . ? C2 C34 1.471(6) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C34 C39 1.407(6) . ? C34 C35 1.408(6) . ? C35 C36 1.372(7) . ? C35 H35 0.9500 . ? C36 C37 1.382(8) . ? C36 H36 0.9500 . ? C37 C38 1.378(7) . ? C37 H37 0.9500 . ? C38 C39 1.390(6) . ? C38 H38 0.9500 . ? C39 H39 0.9500 . ? K1 O40 2.595(4) 2_755 ? K1 O40 2.595(4) . ? K1 O10 2.741(2) 2_755 ? K1 O10 2.741(2) . ? K1 O30 2.792(3) . ? K1 O30 2.792(3) 2_755 ? K1 O20 2.852(3) 2_755 ? K1 O20 2.852(3) . ? K1 C100 3.440(10) . ? K1 C100 3.440(10) 2_755 ? O10 C10 1.426(5) . ? O10 C20 1.428(5) . ? O20 C30 1.421(5) . ? O20 C40 1.426(5) . ? O30 C50 1.421(5) . ? O30 C60 1.426(5) . ? O40 C70 1.426(7) . ? O40 C100 1.469(9) . ? O40 C64B 1.530(14) . ? C10 C60 1.505(6) 2_755 ? C10 H10D 0.9900 . ? C10 H10E 0.9900 . ? C20 C30 1.495(6) . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C40 C50 1.503(7) . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C50 H50A 0.9900 . ? C50 H50B 0.9900 . ? C60 C10 1.505(6) 2_755 ? C60 H60A 0.9900 . ? C60 H60B 0.9900 . ? C64B C65A 1.459(18) . ? C64B H64A 0.9900 . ? C64B H64B 0.9900 . ? C90 C100 1.459(12) . ? C90 C80 1.627(10) . ? C90 H90A 0.9900 . ? C90 H90B 0.9900 . ? C80 C70 1.389(9) . ? C80 C65A 1.741(15) . ? C80 H80C 0.9900 . ? C80 H80D 0.9900 . ? C80 H80A 0.9900 . ? C80 H80B 0.9900 . ? C70 H70A 0.9900 . ? C70 H70B 0.9900 . ? K2 O80 2.686(4) 2_576 ? K2 O80 2.686(4) . ? K2 O70 2.749(2) 2_576 ? K2 O70 2.749(2) . ? K2 O50 2.774(3) . ? K2 O50 2.774(3) 2_576 ? K2 O60 2.839(3) 2_576 ? K2 O60 2.839(3) . ? K2 C170 3.415(7) . ? K2 C170 3.415(7) 2_576 ? K2 C110 3.538(4) 2_576 ? K2 C110 3.538(4) . ? O50 C110 1.414(5) . ? O50 C120 1.419(5) . ? O60 C130 1.420(5) . ? O60 C140 1.435(4) . ? O70 C160 1.417(5) . ? O70 C150 1.421(5) . ? O80 C170 1.364(8) . ? O80 C200 1.407(7) . ? C110 C160 1.502(6) 2_576 ? C110 H11G 0.9900 . ? C110 H11H 0.9900 . ? C120 C130 1.497(6) . ? C120 H12G 0.9900 . ? C120 H12H 0.9900 . ? C130 H13D 0.9900 . ? C130 H13E 0.9900 . ? C140 C150 1.494(6) . ? C140 H14A 0.9900 . ? C140 H14B 0.9900 . ? C150 H15A 0.9900 . ? C150 H15B 0.9900 . ? C160 C110 1.502(6) 2_576 ? C160 H16A 0.9900 . ? C160 H16B 0.9900 . ? C200 C190 1.671(10) . ? C200 H20C 0.9900 . ? C200 H20D 0.9900 . ? C190 C180 1.582(13) . ? C190 H19A 0.9900 . ? C190 H19B 0.9900 . ? C180 C170 1.443(10) . ? C180 H18A 0.9900 . ? C180 H18B 0.9900 . ? C170 H17A 0.9900 . ? C170 H17B 0.9900 . ? C100 H10F 0.9900 . ? C100 H10G 0.9900 . ? C65A H65A 0.9900 . ? C65A H65B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N21 Fe1 N11 98.45(12) . . ? N21 Fe1 C2 135.22(14) . . ? N11 Fe1 C2 126.17(15) . . ? C21 N11 C12 119.6(3) . . ? C21 N11 Fe1 123.5(2) . . ? C12 N11 Fe1 116.8(2) . . ? C41 N21 C13 119.4(3) . . ? C41 N21 Fe1 123.0(2) . . ? C13 N21 Fe1 117.4(2) . . ? C21 C11 H11A 109.5 . . ? C21 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C21 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N11 C21 C31 121.9(3) . . ? N11 C21 C11 119.1(3) . . ? C31 C21 C11 119.0(3) . . ? C21 C31 C41 130.4(3) . . ? C21 C31 H31 114.8 . . ? C41 C31 H31 114.8 . . ? N21 C41 C31 122.6(3) . . ? N21 C41 C51 119.4(3) . . ? C31 C41 C51 117.9(3) . . ? C41 C51 H51A 109.5 . . ? C41 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C41 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C62 C12 C72 120.3(3) . . ? C62 C12 N11 119.6(3) . . ? C72 C12 N11 119.9(3) . . ? C32 C72 C12 118.2(4) . . ? C32 C72 C82 120.7(3) . . ? C12 C72 C82 121.0(3) . . ? C42 C32 C72 121.4(4) . . ? C42 C32 H32 119.3 . . ? C72 C32 H32 119.3 . . ? C52 C42 C32 119.7(4) . . ? C52 C42 H42 120.2 . . ? C32 C42 H42 120.2 . . ? C42 C52 C62 121.2(4) . . ? C42 C52 H52 119.4 . . ? C62 C52 H52 119.4 . . ? C52 C62 C12 119.2(4) . . ? C52 C62 C112 119.5(4) . . ? C12 C62 C112 121.3(4) . . ? C72 C82 C102 112.8(3) . . ? C72 C82 C92 110.9(3) . . ? C102 C82 C92 110.7(3) . . ? C72 C82 H82 107.4 . . ? C102 C82 H82 107.4 . . ? C92 C82 H82 107.4 . . ? C82 C102 H10A 109.5 . . ? C82 C102 H10B 109.5 . . ? H10A C102 H10B 109.5 . . ? C82 C102 H10C 109.5 . . ? H10A C102 H10C 109.5 . . ? H10B C102 H10C 109.5 . . ? C82 C92 H92A 109.5 . . ? C82 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C82 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C132 C112 C62 113.4(4) . . ? C132 C112 C122 109.8(4) . . ? C62 C112 C122 110.7(5) . . ? C132 C112 H112 107.6 . . ? C62 C112 H112 107.6 . . ? C122 C112 H112 107.6 . . ? C112 C132 H13A 109.5 . . ? C112 C132 H13B 109.5 . . ? H13A C132 H13B 109.5 . . ? C112 C132 H13C 109.5 . . ? H13A C132 H13C 109.5 . . ? H13B C132 H13C 109.5 . . ? C112 C122 H12A 109.5 . . ? C112 C122 H12B 109.5 . . ? H12A C122 H12B 109.5 . . ? C112 C122 H12C 109.5 . . ? H12A C122 H12C 109.5 . . ? H12B C122 H12C 109.5 . . ? C23 C13 C63 120.3(3) . . ? C23 C13 N21 119.7(3) . . ? C63 C13 N21 119.9(3) . . ? C33 C23 C13 118.5(3) . . ? C33 C23 C73 119.8(4) . . ? C13 C23 C73 121.7(3) . . ? C43 C33 C23 121.3(4) . . ? C43 C33 H33 119.3 . . ? C23 C33 H33 119.3 . . ? C53 C43 C33 119.7(3) . . ? C53 C43 H43 120.2 . . ? C33 C43 H43 120.2 . . ? C43 C53 C63 121.6(4) . . ? C43 C53 H53 119.2 . . ? C63 C53 H53 119.2 . . ? C53 C63 C13 118.4(4) . . ? C53 C63 C103 120.1(3) . . ? C13 C63 C103 121.4(3) . . ? C83 C73 C23 111.6(3) . . ? C83 C73 C93 112.0(4) . . ? C23 C73 C93 111.4(3) . . ? C83 C73 H73 107.2 . . ? C23 C73 H73 107.2 . . ? C93 C73 H73 107.2 . . ? C73 C93 H93A 109.5 . . ? C73 C93 H93B 109.5 . . ? H93A C93 H93B 109.5 . . ? C73 C93 H93C 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C73 C83 H83A 109.5 . . ? C73 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C73 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? C63 C103 C123 112.2(3) . . ? C63 C103 C113 111.8(3) . . ? C123 C103 C113 109.5(4) . . ? C63 C103 H103 107.7 . . ? C123 C103 H103 107.7 . . ? C113 C103 H103 107.7 . . ? C103 C123 H12D 109.5 . . ? C103 C123 H12E 109.5 . . ? H12D C123 H12E 109.5 . . ? C103 C123 H12F 109.5 . . ? H12D C123 H12F 109.5 . . ? H12E C123 H12F 109.5 . . ? C103 C113 H11D 109.5 . . ? C103 C113 H11E 109.5 . . ? H11D C113 H11E 109.5 . . ? C103 C113 H11F 109.5 . . ? H11D C113 H11F 109.5 . . ? H11E C113 H11F 109.5 . . ? C34 C2 Fe1 116.2(3) . . ? C34 C2 H2A 108.2 . . ? Fe1 C2 H2A 108.2 . . ? C34 C2 H2B 108.2 . . ? Fe1 C2 H2B 108.2 . . ? H2A C2 H2B 107.4 . . ? C39 C34 C35 115.9(4) . . ? C39 C34 C2 121.3(4) . . ? C35 C34 C2 122.9(4) . . ? C36 C35 C34 122.0(4) . . ? C36 C35 H35 119.0 . . ? C34 C35 H35 119.0 . . ? C35 C36 C37 121.3(5) . . ? C35 C36 H36 119.4 . . ? C37 C36 H36 119.4 . . ? C38 C37 C36 118.4(5) . . ? C38 C37 H37 120.8 . . ? C36 C37 H37 120.8 . . ? C37 C38 C39 121.0(5) . . ? C37 C38 H38 119.5 . . ? C39 C38 H38 119.5 . . ? C38 C39 C34 121.5(4) . . ? C38 C39 H39 119.2 . . ? C34 C39 H39 119.2 . . ? O40 K1 O40 180.0 2_755 . ? O40 K1 O10 93.72(11) 2_755 2_755 ? O40 K1 O10 86.28(11) . 2_755 ? O40 K1 O10 86.28(11) 2_755 . ? O40 K1 O10 93.72(11) . . ? O10 K1 O10 180.0 2_755 . ? O40 K1 O30 82.73(13) 2_755 . ? O40 K1 O30 97.27(13) . . ? O10 K1 O30 61.22(8) 2_755 . ? O10 K1 O30 118.78(8) . . ? O40 K1 O30 97.27(13) 2_755 2_755 ? O40 K1 O30 82.73(13) . 2_755 ? O10 K1 O30 118.78(8) 2_755 2_755 ? O10 K1 O30 61.22(8) . 2_755 ? O30 K1 O30 180.0 . 2_755 ? O40 K1 O20 89.95(12) 2_755 2_755 ? O40 K1 O20 90.05(12) . 2_755 ? O10 K1 O20 60.11(8) 2_755 2_755 ? O10 K1 O20 119.89(8) . 2_755 ? O30 K1 O20 120.12(8) . 2_755 ? O30 K1 O20 59.88(8) 2_755 2_755 ? O40 K1 O20 90.05(12) 2_755 . ? O40 K1 O20 89.95(12) . . ? O10 K1 O20 119.89(8) 2_755 . ? O10 K1 O20 60.11(8) . . ? O30 K1 O20 59.88(8) . . ? O30 K1 O20 120.12(8) 2_755 . ? O20 K1 O20 180.0 2_755 . ? O40 K1 C100 156.81(19) 2_755 . ? O40 K1 C100 23.19(19) . . ? O10 K1 C100 104.68(16) 2_755 . ? O10 K1 C100 75.32(16) . . ? O30 K1 C100 93.7(2) . . ? O30 K1 C100 86.3(2) 2_755 . ? O20 K1 C100 111.3(2) 2_755 . ? O20 K1 C100 68.7(2) . . ? O40 K1 C100 23.19(19) 2_755 2_755 ? O40 K1 C100 156.81(19) . 2_755 ? O10 K1 C100 75.32(16) 2_755 2_755 ? O10 K1 C100 104.68(16) . 2_755 ? O30 K1 C100 86.3(2) . 2_755 ? O30 K1 C100 93.7(2) 2_755 2_755 ? O20 K1 C100 68.7(2) 2_755 2_755 ? O20 K1 C100 111.3(2) . 2_755 ? C100 K1 C100 180.0 . 2_755 ? C10 O10 C20 112.7(3) . . ? C10 O10 K1 116.0(2) . . ? C20 O10 K1 117.1(2) . . ? C30 O20 C40 111.7(3) . . ? C30 O20 K1 112.9(2) . . ? C40 O20 K1 111.4(2) . . ? C50 O30 C60 112.3(4) . . ? C50 O30 K1 116.6(2) . . ? C60 O30 K1 112.5(2) . . ? C70 O40 C100 108.0(5) . . ? C70 O40 C64B 92.3(9) . . ? C70 O40 K1 129.2(4) . . ? C100 O40 K1 112.7(5) . . ? C64B O40 K1 134.7(9) . . ? O10 C10 C60 109.0(3) . 2_755 ? O10 C10 H10D 109.9 . . ? C60 C10 H10D 109.9 2_755 . ? O10 C10 H10E 109.9 . . ? C60 C10 H10E 109.9 2_755 . ? H10D C10 H10E 108.3 . . ? O10 C20 C30 108.2(3) . . ? O10 C20 H20A 110.1 . . ? C30 C20 H20A 110.1 . . ? O10 C20 H20B 110.1 . . ? C30 C20 H20B 110.1 . . ? H20A C20 H20B 108.4 . . ? O20 C30 C20 108.5(3) . . ? O20 C30 H30A 110.0 . . ? C20 C30 H30A 110.0 . . ? O20 C30 H30B 110.0 . . ? C20 C30 H30B 110.0 . . ? H30A C30 H30B 108.4 . . ? O20 C40 C50 107.9(4) . . ? O20 C40 H40A 110.1 . . ? C50 C40 H40A 110.1 . . ? O20 C40 H40B 110.1 . . ? C50 C40 H40B 110.1 . . ? H40A C40 H40B 108.4 . . ? O30 C50 C40 107.4(4) . . ? O30 C50 H50A 110.2 . . ? C40 C50 H50A 110.2 . . ? O30 C50 H50B 110.2 . . ? C40 C50 H50B 110.2 . . ? H50A C50 H50B 108.5 . . ? O30 C60 C10 107.9(4) . 2_755 ? O30 C60 H60A 110.1 . . ? C10 C60 H60A 110.1 2_755 . ? O30 C60 H60B 110.1 . . ? C10 C60 H60B 110.1 2_755 . ? H60A C60 H60B 108.4 . . ? C65A C64B O40 93.7(13) . . ? C65A C64B H64A 113.0 . . ? O40 C64B H64A 113.0 . . ? C65A C64B H64B 113.0 . . ? O40 C64B H64B 113.0 . . ? H64A C64B H64B 110.4 . . ? C100 C90 C80 102.6(7) . . ? C100 C90 H90A 111.2 . . ? C80 C90 H90A 111.2 . . ? C100 C90 H90B 111.2 . . ? C80 C90 H90B 111.2 . . ? H90A C90 H90B 109.2 . . ? C70 C80 C90 98.8(6) . . ? C70 C80 C65A 99.8(8) . . ? C70 C80 H80C 112.0 . . ? C90 C80 H80C 112.0 . . ? C70 C80 H80D 112.0 . . ? C90 C80 H80D 112.0 . . ? H80C C80 H80D 109.7 . . ? C70 C80 H80A 111.8 . . ? C65A C80 H80A 111.8 . . ? C70 C80 H80B 111.8 . . ? C65A C80 H80B 111.8 . . ? H80A C80 H80B 109.5 . . ? C80 C70 O40 108.9(5) . . ? C80 C70 H70A 109.9 . . ? O40 C70 H70A 109.9 . . ? C80 C70 H70B 109.9 . . ? O40 C70 H70B 109.9 . . ? H70A C70 H70B 108.3 . . ? O80 K2 O80 180.00(16) 2_576 . ? O80 K2 O70 83.97(10) 2_576 2_576 ? O80 K2 O70 96.04(10) . 2_576 ? O80 K2 O70 96.03(10) 2_576 . ? O80 K2 O70 83.96(10) . . ? O70 K2 O70 180.00(11) 2_576 . ? O80 K2 O50 89.37(10) 2_576 . ? O80 K2 O50 90.63(10) . . ? O70 K2 O50 61.73(7) 2_576 . ? O70 K2 O50 118.27(7) . . ? O80 K2 O50 90.63(10) 2_576 2_576 ? O80 K2 O50 89.37(10) . 2_576 ? O70 K2 O50 118.27(7) 2_576 2_576 ? O70 K2 O50 61.73(7) . 2_576 ? O50 K2 O50 180.0 . 2_576 ? O80 K2 O60 96.04(10) 2_576 2_576 ? O80 K2 O60 83.96(10) . 2_576 ? O70 K2 O60 59.67(7) 2_576 2_576 ? O70 K2 O60 120.33(7) . 2_576 ? O50 K2 O60 120.06(7) . 2_576 ? O50 K2 O60 59.94(7) 2_576 2_576 ? O80 K2 O60 83.96(10) 2_576 . ? O80 K2 O60 96.04(10) . . ? O70 K2 O60 120.34(7) 2_576 . ? O70 K2 O60 59.66(7) . . ? O50 K2 O60 59.94(7) . . ? O50 K2 O60 120.06(7) 2_576 . ? O60 K2 O60 180.0 2_576 . ? O80 K2 C170 158.06(15) 2_576 . ? O80 K2 C170 21.95(15) . . ? O70 K2 C170 95.74(17) 2_576 . ? O70 K2 C170 84.27(17) . . ? O50 K2 C170 71.49(14) . . ? O50 K2 C170 108.51(14) 2_576 . ? O60 K2 C170 102.75(17) 2_576 . ? O60 K2 C170 77.25(17) . . ? O80 K2 C170 21.94(15) 2_576 2_576 ? O80 K2 C170 158.06(15) . 2_576 ? O70 K2 C170 84.27(17) 2_576 2_576 ? O70 K2 C170 95.73(17) . 2_576 ? O50 K2 C170 108.50(14) . 2_576 ? O50 K2 C170 71.50(14) 2_576 2_576 ? O60 K2 C170 77.26(17) 2_576 2_576 ? O60 K2 C170 102.74(17) . 2_576 ? C170 K2 C170 180.0 . 2_576 ? O80 K2 C110 101.06(12) 2_576 2_576 ? O80 K2 C110 78.94(12) . 2_576 ? O70 K2 C110 137.94(9) 2_576 2_576 ? O70 K2 C110 42.06(9) . 2_576 ? O50 K2 C110 158.12(9) . 2_576 ? O50 K2 C110 21.88(9) 2_576 2_576 ? O60 K2 C110 78.28(8) 2_576 2_576 ? O60 K2 C110 101.72(8) . 2_576 ? C170 K2 C110 93.84(16) . 2_576 ? C170 K2 C110 86.16(16) 2_576 2_576 ? O80 K2 C110 78.94(12) 2_576 . ? O80 K2 C110 101.06(12) . . ? O70 K2 C110 42.06(9) 2_576 . ? O70 K2 C110 137.94(9) . . ? O50 K2 C110 21.88(9) . . ? O50 K2 C110 158.12(9) 2_576 . ? O60 K2 C110 101.72(8) 2_576 . ? O60 K2 C110 78.28(8) . . ? C170 K2 C110 86.16(16) . . ? C170 K2 C110 93.84(16) 2_576 . ? C110 K2 C110 180.0 2_576 . ? C110 O50 C120 111.4(3) . . ? C110 O50 K2 111.1(2) . . ? C120 O50 K2 116.7(2) . . ? C130 O60 C140 112.2(3) . . ? C130 O60 K2 113.6(2) . . ? C140 O60 K2 114.5(2) . . ? C160 O70 C150 112.2(3) . . ? C160 O70 K2 115.3(2) . . ? C150 O70 K2 117.9(2) . . ? C170 O80 C200 116.1(5) . . ? C170 O80 K2 110.7(4) . . ? C200 O80 K2 129.0(3) . . ? O50 C110 C160 109.1(4) . 2_576 ? O50 C110 K2 46.99(17) . . ? C160 C110 K2 79.8(2) 2_576 . ? O50 C110 H11G 109.9 . . ? C160 C110 H11G 109.9 2_576 . ? K2 C110 H11G 156.5 . . ? O50 C110 H11H 109.9 . . ? C160 C110 H11H 109.9 2_576 . ? K2 C110 H11H 87.2 . . ? H11G C110 H11H 108.3 . . ? O50 C120 C130 109.1(4) . . ? O50 C120 H12G 109.9 . . ? C130 C120 H12G 109.9 . . ? O50 C120 H12H 109.9 . . ? C130 C120 H12H 109.9 . . ? H12G C120 H12H 108.3 . . ? O60 C130 C120 108.2(3) . . ? O60 C130 H13D 110.1 . . ? C120 C130 H13D 110.1 . . ? O60 C130 H13E 110.1 . . ? C120 C130 H13E 110.1 . . ? H13D C130 H13E 108.4 . . ? O60 C140 C150 108.8(3) . . ? O60 C140 H14A 109.9 . . ? C150 C140 H14A 109.9 . . ? O60 C140 H14B 109.9 . . ? C150 C140 H14B 109.9 . . ? H14A C140 H14B 108.3 . . ? O70 C150 C140 108.1(3) . . ? O70 C150 H15A 110.1 . . ? C140 C150 H15A 110.1 . . ? O70 C150 H15B 110.1 . . ? C140 C150 H15B 110.1 . . ? H15A C150 H15B 108.4 . . ? O70 C160 C110 108.8(3) . 2_576 ? O70 C160 H16A 109.9 . . ? C110 C160 H16A 109.9 2_576 . ? O70 C160 H16B 109.9 . . ? C110 C160 H16B 109.9 2_576 . ? H16A C160 H16B 108.3 . . ? O80 C200 C190 96.6(5) . . ? O80 C200 H20C 112.4 . . ? C190 C200 H20C 112.4 . . ? O80 C200 H20D 112.4 . . ? C190 C200 H20D 112.4 . . ? H20C C200 H20D 110.0 . . ? C180 C190 C200 93.9(6) . . ? C180 C190 H19A 112.9 . . ? C200 C190 H19A 112.9 . . ? C180 C190 H19B 112.9 . . ? C200 C190 H19B 112.9 . . ? H19A C190 H19B 110.4 . . ? C170 C180 C190 102.0(7) . . ? C170 C180 H18A 111.4 . . ? C190 C180 H18A 111.4 . . ? C170 C180 H18B 111.4 . . ? C190 C180 H18B 111.4 . . ? H18A C180 H18B 109.2 . . ? O80 C170 C180 105.8(7) . . ? O80 C170 K2 47.4(3) . . ? C180 C170 K2 148.4(7) . . ? O80 C170 H17A 110.6 . . ? C180 C170 H17A 110.6 . . ? K2 C170 H17A 96.6 . . ? O80 C170 H17B 110.6 . . ? C180 C170 H17B 110.6 . . ? K2 C170 H17B 73.5 . . ? H17A C170 H17B 108.7 . . ? C90 C100 O40 105.3(7) . . ? C90 C100 K1 140.5(7) . . ? O40 C100 K1 44.1(4) . . ? C90 C100 H10F 110.7 . . ? O40 C100 H10F 110.7 . . ? K1 C100 H10F 72.1 . . ? C90 C100 H10G 110.7 . . ? O40 C100 H10G 110.7 . . ? K1 C100 H10G 104.9 . . ? H10F C100 H10G 108.8 . . ? C64B C65A C80 87.5(13) . . ? C64B C65A H65A 114.1 . . ? C80 C65A H65A 114.1 . . ? C64B C65A H65B 114.1 . . ? C80 C65A H65B 114.1 . . ? H65A C65A H65B 111.3 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C12 N11 C21 C31 173.6(3) . . . . ? Fe1 N11 C21 C31 -2.9(5) . . . . ? C12 N11 C21 C11 -5.8(5) . . . . ? Fe1 N11 C21 C11 177.7(2) . . . . ? N11 C21 C31 C41 0.4(6) . . . . ? C11 C21 C31 C41 179.8(4) . . . . ? C13 N21 C41 C31 174.6(3) . . . . ? Fe1 N21 C41 C31 -0.1(5) . . . . ? C13 N21 C41 C51 -6.6(5) . . . . ? Fe1 N21 C41 C51 178.7(3) . . . . ? C21 C31 C41 N21 1.3(7) . . . . ? C21 C31 C41 C51 -177.6(4) . . . . ? C21 N11 C12 C62 -92.3(4) . . . . ? Fe1 N11 C12 C62 84.3(4) . . . . ? C21 N11 C12 C72 93.1(4) . . . . ? Fe1 N11 C12 C72 -90.3(3) . . . . ? C62 C12 C72 C32 -1.5(5) . . . . ? N11 C12 C72 C32 173.1(3) . . . . ? C62 C12 C72 C82 -179.6(3) . . . . ? N11 C12 C72 C82 -5.0(5) . . . . ? C12 C72 C32 C42 0.8(5) . . . . ? C82 C72 C32 C42 179.0(3) . . . . ? C72 C32 C42 C52 -0.2(6) . . . . ? C32 C42 C52 C62 0.1(6) . . . . ? C42 C52 C62 C12 -0.8(6) . . . . ? C42 C52 C62 C112 179.9(4) . . . . ? C72 C12 C62 C52 1.5(6) . . . . ? N11 C12 C62 C52 -173.1(3) . . . . ? C72 C12 C62 C112 -179.2(4) . . . . ? N11 C12 C62 C112 6.2(6) . . . . ? C32 C72 C82 C102 47.3(5) . . . . ? C12 C72 C82 C102 -134.6(4) . . . . ? C32 C72 C82 C92 -77.5(4) . . . . ? C12 C72 C82 C92 100.6(4) . . . . ? C52 C62 C112 C132 -54.2(6) . . . . ? C12 C62 C112 C132 126.5(4) . . . . ? C52 C62 C112 C122 69.7(6) . . . . ? C12 C62 C112 C122 -109.6(5) . . . . ? C41 N21 C13 C23 -86.8(4) . . . . ? Fe1 N21 C13 C23 88.2(4) . . . . ? C41 N21 C13 C63 97.1(4) . . . . ? Fe1 N21 C13 C63 -87.9(4) . . . . ? C63 C13 C23 C33 3.6(6) . . . . ? N21 C13 C23 C33 -172.5(3) . . . . ? C63 C13 C23 C73 -177.7(4) . . . . ? N21 C13 C23 C73 6.2(5) . . . . ? C13 C23 C33 C43 -1.0(6) . . . . ? C73 C23 C33 C43 -179.7(4) . . . . ? C23 C33 C43 C53 -1.3(6) . . . . ? C33 C43 C53 C63 1.0(6) . . . . ? C43 C53 C63 C13 1.6(6) . . . . ? C43 C53 C63 C103 -179.7(4) . . . . ? C23 C13 C63 C53 -3.9(5) . . . . ? N21 C13 C63 C53 172.2(3) . . . . ? C23 C13 C63 C103 177.4(3) . . . . ? N21 C13 C63 C103 -6.5(5) . . . . ? C33 C23 C73 C83 68.1(5) . . . . ? C13 C23 C73 C83 -110.5(5) . . . . ? C33 C23 C73 C93 -57.9(5) . . . . ? C13 C23 C73 C93 123.5(4) . . . . ? C53 C63 C103 C123 47.8(5) . . . . ? C13 C63 C103 C123 -133.5(4) . . . . ? C53 C63 C103 C113 -75.7(4) . . . . ? C13 C63 C103 C113 103.0(4) . . . . ? Fe1 C2 C34 C39 69.5(4) . . . . ? Fe1 C2 C34 C35 -109.8(4) . . . . ? C39 C34 C35 C36 -0.4(6) . . . . ? C2 C34 C35 C36 178.9(4) . . . . ? C34 C35 C36 C37 -0.8(7) . . . . ? C35 C36 C37 C38 1.6(7) . . . . ? C36 C37 C38 C39 -1.2(7) . . . . ? C37 C38 C39 C34 0.1(7) . . . . ? C35 C34 C39 C38 0.7(6) . . . . ? C2 C34 C39 C38 -178.6(4) . . . . ? C20 O10 C10 C60 175.9(4) . . . 2_755 ? K1 O10 C10 C60 -45.3(4) . . . 2_755 ? C10 O10 C20 C30 -172.6(3) . . . . ? K1 O10 C20 C30 49.1(4) . . . . ? C40 O20 C30 C20 176.1(4) . . . . ? K1 O20 C30 C20 49.6(4) . . . . ? O10 C20 C30 O20 -65.4(4) . . . . ? C30 O20 C40 C50 177.1(4) . . . . ? K1 O20 C40 C50 -55.6(5) . . . . ? C60 O30 C50 C40 -178.9(4) . . . . ? K1 O30 C50 C40 -46.8(5) . . . . ? O20 C40 C50 O30 68.7(5) . . . . ? C50 O30 C60 C10 -173.3(4) . . . 2_755 ? K1 O30 C60 C10 52.6(4) . . . 2_755 ? C70 O40 C64B C65A 73.3(14) . . . . ? K1 O40 C64B C65A -84.9(16) . . . . ? C100 C90 C80 C70 -37.9(12) . . . . ? C90 C80 C70 O40 38.5(8) . . . . ? C65A C80 C70 O40 5.0(10) . . . . ? C100 O40 C70 C80 -26.3(9) . . . . ? C64B O40 C70 C80 -44.4(10) . . . . ? K1 O40 C70 C80 115.7(6) . . . . ? C120 O50 C110 C160 173.5(4) . . . 2_576 ? K2 O50 C110 C160 -54.5(4) . . . 2_576 ? C120 O50 C110 K2 -132.0(4) . . . . ? C110 O50 C120 C130 175.8(4) . . . . ? K2 O50 C120 C130 46.6(4) . . . . ? C140 O60 C130 C120 -177.4(4) . . . . ? K2 O60 C130 C120 50.7(5) . . . . ? O50 C120 C130 O60 -64.7(5) . . . . ? C130 O60 C140 C150 -178.2(4) . . . . ? K2 O60 C140 C150 -46.8(4) . . . . ? C160 O70 C150 C140 172.9(3) . . . . ? K2 O70 C150 C140 -49.5(4) . . . . ? O60 C140 C150 O70 62.8(4) . . . . ? C150 O70 C160 C110 -177.7(4) . . . 2_576 ? K2 O70 C160 C110 43.5(4) . . . 2_576 ? C170 O80 C200 C190 -28.8(8) . . . . ? K2 O80 C200 C190 125.6(5) . . . . ? O80 C200 C190 C180 43.4(6) . . . . ? C200 C190 C180 C170 -46.7(7) . . . . ? C200 O80 C170 C180 -1.5(9) . . . . ? K2 O80 C170 C180 -160.5(5) . . . . ? C200 O80 C170 K2 159.0(6) . . . . ? C190 C180 C170 O80 33.4(8) . . . . ? C190 C180 C170 K2 5.4(13) . . . . ? C80 C90 C100 O40 23.3(13) . . . . ? C80 C90 C100 K1 -9.7(19) . . . . ? C70 O40 C100 C90 -1.2(13) . . . . ? K1 O40 C100 C90 -150.1(9) . . . . ? C70 O40 C100 K1 148.9(7) . . . . ? O40 C64B C65A C80 -64.2(14) . . . . ? C70 C80 C65A C64B 38.7(14) . . . . ? _refine_diff_density_max 1.585 _refine_diff_density_min -0.710 _refine_diff_density_rms 0.070 _shelx_res_file ; 007a-21112.res created by SHELXL-2014/7 TITL 007a-21112 CELL 1.54184 13.0503 13.4395 20.4096 83.732 71.934 66.707 ZERR 2 0.0006 0.0006 0.0007 0.003 0.004 0.004 LATT 1 SFAC C H Fe K N O UNIT 112 176 2 2 4 16 SADI C90 C100 C65A C64B SADI C80 C90 C80 C65A SIMU 0.002 0.004 2 C100 C64B O40 C70 C80 C90 C65A SADI O40 C100 O40 C64B L.S. 30 0 54 PLAN 29 SIZE 0.2 0.2 0.1 TEMP -180 CONF MORE -1 BOND $H ABIN ACTA WGHT 0.121900 3.083000 FVAR 0.45072 0.33804 FE1 3 0.715370 0.559171 0.255025 11.00000 0.04922 0.03363 = 0.03544 -0.00550 -0.01942 -0.01628 N11 5 0.747575 0.662451 0.295130 11.00000 0.04250 0.03891 = 0.03442 -0.00481 -0.01451 -0.01814 N21 5 0.597942 0.658885 0.216316 11.00000 0.04771 0.03995 = 0.03298 -0.00819 -0.01497 -0.01986 C11 1 0.718083 0.845592 0.329236 11.00000 0.05410 0.04349 = 0.03865 -0.00759 -0.01472 -0.02327 AFIX 137 H11A 2 0.706020 0.827454 0.378145 11.00000 -1.50000 H11B 2 0.667503 0.921075 0.324805 11.00000 -1.50000 H11C 2 0.799801 0.836090 0.307745 11.00000 -1.50000 AFIX 0 C21 1 0.688711 0.771930 0.293841 11.00000 0.04566 0.03518 = 0.02840 -0.00583 -0.00703 -0.01978 C31 1 0.602777 0.817788 0.260132 11.00000 0.05366 0.03347 = 0.03392 -0.00412 -0.01556 -0.01766 AFIX 43 H31 2 0.567866 0.894679 0.262257 11.00000 -1.20000 AFIX 0 C41 1 0.559352 0.768303 0.223366 11.00000 0.05192 0.03698 = 0.03698 -0.00145 -0.01872 -0.01821 C51 1 0.468309 0.840927 0.189821 11.00000 0.08406 0.03653 = 0.06843 -0.00211 -0.04900 -0.01330 AFIX 137 H51A 2 0.500859 0.832906 0.139604 11.00000 -1.50000 H51B 2 0.444597 0.916440 0.203234 11.00000 -1.50000 H51C 2 0.400310 0.820625 0.204827 11.00000 -1.50000 AFIX 0 C12 1 0.842894 0.620258 0.324167 11.00000 0.04779 0.03780 = 0.03607 -0.00763 -0.01914 -0.01798 C72 1 0.823201 0.591198 0.394517 11.00000 0.05082 0.03255 = 0.04035 -0.00651 -0.01842 -0.01695 C32 1 0.919665 0.539501 0.419078 11.00000 0.06852 0.03364 = 0.04706 0.00105 -0.03275 -0.02306 AFIX 43 H32 2 0.908028 0.518611 0.465964 11.00000 -1.20000 AFIX 0 C42 1 1.032007 0.517937 0.376666 11.00000 0.05671 0.03964 = 0.06767 -0.00913 -0.03654 -0.01341 AFIX 43 H42 2 1.096607 0.482786 0.394428 11.00000 -1.20000 AFIX 0 C52 1 1.049704 0.547617 0.308705 11.00000 0.04712 0.06659 = 0.05576 -0.02324 -0.01707 -0.01996 AFIX 43 H52 2 1.126994 0.532517 0.279741 11.00000 -1.20000 AFIX 0 C62 1 0.956377 0.599415 0.281561 11.00000 0.04634 0.06710 = 0.04036 -0.02016 -0.01317 -0.02121 C82 1 0.701328 0.612464 0.441210 11.00000 0.05891 0.04349 = 0.03429 -0.00010 -0.01714 -0.02366 AFIX 13 H82 2 0.645673 0.666026 0.417825 11.00000 -1.20000 AFIX 0 C102 1 0.678370 0.661958 0.510947 11.00000 0.07432 0.05571 = 0.04104 -0.00694 -0.01536 -0.02983 AFIX 137 H10A 2 0.728858 0.609764 0.536292 11.00000 -1.50000 H10B 2 0.596503 0.679827 0.537622 11.00000 -1.50000 H10C 2 0.695047 0.727972 0.503578 11.00000 -1.50000 AFIX 0 C92 1 0.675745 0.508545 0.451117 11.00000 0.07035 0.05413 = 0.04889 -0.00446 -0.01299 -0.03525 AFIX 137 H92A 2 0.684584 0.481463 0.406196 11.00000 -1.50000 H92B 2 0.595777 0.524552 0.480737 11.00000 -1.50000 H92C 2 0.730582 0.453441 0.472727 11.00000 -1.50000 AFIX 0 C112 1 0.979866 0.631184 0.205801 11.00000 0.04552 0.11400 = 0.03412 -0.01717 -0.00538 -0.03545 AFIX 13 H112 2 0.902797 0.675112 0.197681 11.00000 -1.20000 AFIX 0 C132 1 1.053013 0.699661 0.185831 11.00000 0.06797 0.07761 = 0.05184 -0.00479 -0.02291 -0.02540 AFIX 137 H13A 2 1.017907 0.761900 0.217572 11.00000 -1.50000 H13B 2 1.056283 0.725395 0.138697 11.00000 -1.50000 H13C 2 1.132160 0.655977 0.188307 11.00000 -1.50000 AFIX 0 C122 1 1.037934 0.529919 0.158688 11.00000 0.17461 0.17299 = 0.05000 -0.05066 0.01992 -0.12732 AFIX 137 H12A 2 1.111319 0.482581 0.167867 11.00000 -1.50000 H12B 2 1.053862 0.551856 0.110372 11.00000 -1.50000 H12C 2 0.985592 0.490846 0.167830 11.00000 -1.50000 AFIX 0 C13 1 0.542710 0.614319 0.183426 11.00000 0.04546 0.03342 = 0.03747 -0.00465 -0.01919 -0.01273 C23 1 0.443056 0.594388 0.222759 11.00000 0.04406 0.04094 = 0.04050 -0.00942 -0.01547 -0.01224 C33 1 0.399181 0.539321 0.191486 11.00000 0.04536 0.05646 = 0.04908 -0.01065 -0.01532 -0.02209 AFIX 43 H33 2 0.332827 0.524401 0.217664 11.00000 -1.20000 AFIX 0 C43 1 0.450444 0.505953 0.123007 11.00000 0.05675 0.05041 = 0.04816 -0.01311 -0.02394 -0.02114 AFIX 43 H43 2 0.420337 0.467247 0.102865 11.00000 -1.20000 AFIX 0 C53 1 0.545076 0.529143 0.084373 11.00000 0.05788 0.04299 = 0.04186 -0.00814 -0.02094 -0.01901 AFIX 43 H53 2 0.578987 0.507019 0.037282 11.00000 -1.20000 AFIX 0 C63 1 0.592498 0.584419 0.112703 11.00000 0.05228 0.03491 = 0.03565 -0.00365 -0.01814 -0.01356 C73 1 0.385157 0.628941 0.297534 11.00000 0.04818 0.05642 = 0.04253 -0.01017 -0.00997 -0.02404 AFIX 13 H73 2 0.424646 0.672595 0.308544 11.00000 -1.20000 AFIX 0 C93 1 0.255968 0.702656 0.310300 11.00000 0.05589 0.07627 = 0.06720 -0.03240 -0.01226 -0.01138 AFIX 137 H93A 2 0.248191 0.759404 0.275545 11.00000 -1.50000 H93B 2 0.225158 0.736046 0.356321 11.00000 -1.50000 H93C 2 0.212050 0.659595 0.307185 11.00000 -1.50000 AFIX 0 C83 1 0.401792 0.532832 0.344521 11.00000 0.08543 0.06770 = 0.04478 -0.00699 -0.00445 -0.01991 AFIX 137 H83A 2 0.370245 0.484614 0.332366 11.00000 -1.50000 H83B 2 0.360780 0.557904 0.392418 11.00000 -1.50000 H83C 2 0.485167 0.493491 0.339328 11.00000 -1.50000 AFIX 0 C103 1 0.696507 0.609142 0.068471 11.00000 0.06116 0.03928 = 0.03467 -0.00219 -0.01728 -0.02321 AFIX 13 H103 2 0.704606 0.663766 0.093975 11.00000 -1.20000 AFIX 0 C123 1 0.680250 0.657892 -0.000521 11.00000 0.08985 0.06928 = 0.04574 0.01203 -0.02954 -0.03922 AFIX 137 H12D 2 0.672680 0.605690 -0.026835 11.00000 -1.50000 H12E 2 0.748009 0.674984 -0.026636 11.00000 -1.50000 H12F 2 0.609624 0.724295 0.007624 11.00000 -1.50000 AFIX 0 C113 1 0.809584 0.508744 0.055826 11.00000 0.05817 0.05224 = 0.04817 -0.00346 -0.00982 -0.02259 AFIX 137 H11D 2 0.823619 0.481229 0.100032 11.00000 -1.50000 H11E 2 0.874665 0.527766 0.027116 11.00000 -1.50000 H11F 2 0.803066 0.452780 0.032212 11.00000 -1.50000 AFIX 0 C2 1 0.801194 0.392965 0.253249 11.00000 0.06350 0.03741 = 0.04744 -0.00587 -0.02278 -0.01468 AFIX 23 H2A 2 0.858843 0.370868 0.207303 11.00000 -1.20000 H2B 2 0.845172 0.373765 0.287590 11.00000 -1.20000 AFIX 0 C34 1 0.727572 0.329284 0.267374 11.00000 0.05886 0.03508 = 0.04000 -0.00769 -0.01703 -0.01246 C35 1 0.708152 0.270849 0.328446 11.00000 0.08421 0.04212 = 0.03855 -0.00468 -0.01754 -0.01821 AFIX 43 H35 2 0.744975 0.271263 0.361868 11.00000 -1.20000 AFIX 0 C36 1 0.637623 0.213306 0.341143 11.00000 0.08779 0.05110 = 0.04949 -0.00256 -0.00057 -0.02679 AFIX 43 H36 2 0.627546 0.174207 0.382751 11.00000 -1.20000 AFIX 0 C37 1 0.580968 0.211152 0.294549 11.00000 0.07155 0.05726 = 0.07529 -0.00813 -0.00559 -0.03368 AFIX 43 H37 2 0.530745 0.172628 0.304186 11.00000 -1.20000 AFIX 0 C38 1 0.599125 0.266242 0.233796 11.00000 0.07167 0.05129 = 0.06924 -0.00663 -0.02572 -0.02345 AFIX 43 H38 2 0.562124 0.264444 0.200778 11.00000 -1.20000 AFIX 0 C39 1 0.670790 0.324431 0.220085 11.00000 0.06241 0.04386 = 0.04605 -0.00645 -0.01885 -0.02231 AFIX 43 H39 2 0.681682 0.361785 0.177809 11.00000 -1.20000 AFIX 0 K1 4 1.000000 0.000000 0.000000 10.50000 0.09878 0.03995 = 0.03377 -0.00188 -0.01714 -0.03357 O10 6 0.913001 0.094857 0.128311 11.00000 0.08010 0.04859 = 0.03178 -0.00340 -0.01421 -0.03434 O20 6 1.086614 0.148831 0.029864 11.00000 0.08479 0.04297 = 0.03604 -0.00071 -0.01447 -0.03359 O30 6 1.137214 0.082360 -0.106695 11.00000 0.08465 0.06083 = 0.03613 -0.00379 -0.01280 -0.04297 O40 6 1.169419 -0.160140 0.031195 11.00000 0.10093 0.09229 = 0.09267 -0.02747 -0.03751 -0.01603 C10 1 0.866140 0.035755 0.183449 11.00000 0.07654 0.05432 = 0.03328 -0.00463 -0.01171 -0.02942 AFIX 23 H10D 2 0.819661 0.083375 0.224695 11.00000 -1.20000 H10E 2 0.930305 -0.025795 0.195419 11.00000 -1.20000 AFIX 0 C20 1 0.980031 0.143531 0.146565 11.00000 0.07248 0.04454 = 0.03642 -0.01102 -0.01444 -0.02529 AFIX 23 H20A 2 1.051695 0.086785 0.154144 11.00000 -1.20000 H20B 2 0.934069 0.186784 0.189664 11.00000 -1.20000 AFIX 0 C30 1 1.011274 0.214891 0.088966 11.00000 0.07469 0.03856 = 0.04411 -0.00654 -0.01838 -0.02312 AFIX 23 H30A 2 0.939844 0.267673 0.078798 11.00000 -1.20000 H30B 2 1.050837 0.255578 0.102176 11.00000 -1.20000 AFIX 0 C40 1 1.113986 0.212079 -0.028744 11.00000 0.11912 0.06133 = 0.04425 0.00694 -0.02600 -0.06385 AFIX 23 H40A 2 1.149276 0.259318 -0.018425 11.00000 -1.20000 H40B 2 1.042235 0.258509 -0.041118 11.00000 -1.20000 AFIX 0 C50 1 1.198556 0.135575 -0.087368 11.00000 0.10723 0.08733 = 0.04250 0.00094 -0.01356 -0.06932 AFIX 23 H50A 2 1.229174 0.176064 -0.126792 11.00000 -1.20000 H50B 2 1.265029 0.081963 -0.072743 11.00000 -1.20000 AFIX 0 C60 1 1.209965 0.005636 -0.161465 11.00000 0.07791 0.07080 = 0.03560 -0.00631 -0.00872 -0.03896 AFIX 23 H60A 2 1.270207 -0.055056 -0.145662 11.00000 -1.20000 H60B 2 1.249610 0.040466 -0.200673 11.00000 -1.20000 AFIX 0 PART 1 C64B 1 1.237427 -0.176048 0.083106 21.00000 0.10078 0.09164 = 0.09077 -0.03118 -0.03966 -0.01693 AFIX 23 H64A 2 1.189711 -0.132730 0.126017 21.00000 -1.20000 H64B 2 1.275474 -0.253119 0.093983 21.00000 -1.20000 AFIX 0 PART 2 C90 1 1.340659 -0.200788 0.059969 -21.00000 0.10152 0.09158 = 0.09101 -0.03216 -0.04145 -0.01489 AFIX 23 H90A 2 1.352253 -0.262638 0.091825 -21.00000 -1.20000 H90B 2 1.391246 -0.162839 0.061552 -21.00000 -1.20000 AFIX 0 PART 0 C80 1 1.366748 -0.240558 -0.018112 11.00000 0.10261 0.09235 = 0.09435 -0.03188 -0.03778 -0.01554 PART 2 AFIX 23 H80C 2 1.381695 -0.186455 -0.052714 -21.00000 -1.20000 H80D 2 1.432737 -0.311467 -0.029872 -21.00000 -1.20000 AFIX 23 PART 1 H80A 2 1.403900 -0.224541 -0.066022 21.00000 -1.20000 H80B 2 1.421405 -0.307362 -0.002966 21.00000 -1.20000 AFIX 0 PART 0 C70 1 1.260712 -0.247866 -0.011269 11.00000 0.09967 0.08925 = 0.09355 -0.03354 -0.04118 -0.01632 AFIX 23 H70A 2 1.260347 -0.317671 0.009866 11.00000 -1.20000 H70B 2 1.248803 -0.244634 -0.057178 11.00000 -1.20000 AFIX 0 K2 4 0.000000 1.000000 0.500000 10.50000 0.06871 0.03254 = 0.04025 -0.00238 -0.02844 -0.01998 O50 6 0.019513 0.915690 0.627850 11.00000 0.07357 0.03747 = 0.04219 -0.00334 -0.02675 -0.02307 O60 6 -0.048334 0.811861 0.546684 11.00000 0.07355 0.03577 = 0.04751 -0.00523 -0.03032 -0.02106 O70 6 -0.019121 0.874979 0.409937 11.00000 0.06486 0.04039 = 0.04165 -0.00419 -0.02422 -0.02587 O80 6 0.230346 0.895057 0.442918 11.00000 0.07433 0.07143 = 0.06140 0.00421 -0.01515 -0.02411 C110 1 -0.016009 0.999139 0.676323 11.00000 0.09435 0.05926 = 0.03952 -0.00849 -0.02010 -0.04485 AFIX 23 H11G 2 -0.001821 0.967341 0.720323 11.00000 -1.20000 H11H 2 -0.100522 1.042735 0.685359 11.00000 -1.20000 AFIX 0 C120 1 -0.032409 0.839252 0.654991 11.00000 0.09707 0.04492 = 0.04373 0.00299 -0.03240 -0.03550 AFIX 23 H12G 2 -0.118335 0.876728 0.671142 11.00000 -1.20000 H12H 2 -0.005339 0.802408 0.694748 11.00000 -1.20000 AFIX 0 C130 1 0.000905 0.757670 0.599948 11.00000 0.10649 0.04063 = 0.05142 0.00439 -0.04477 -0.03255 AFIX 23 H13D 2 0.086893 0.723677 0.581404 11.00000 -1.20000 H13E 2 -0.028829 0.700114 0.619244 11.00000 -1.20000 AFIX 0 C140 1 -0.025192 0.738871 0.492804 11.00000 0.08226 0.03503 = 0.05007 -0.00800 -0.03136 -0.02229 AFIX 23 H14A 2 -0.060261 0.684693 0.511547 11.00000 -1.20000 H14B 2 0.060021 0.699965 0.473181 11.00000 -1.20000 AFIX 0 C150 1 -0.076365 0.802597 0.438024 11.00000 0.06679 0.03867 = 0.05102 -0.00517 -0.02724 -0.02497 AFIX 23 H15A 2 -0.065121 0.753294 0.401477 11.00000 -1.20000 H15B 2 -0.161087 0.843757 0.457897 11.00000 -1.20000 AFIX 0 C160 1 -0.051849 0.929897 0.351813 11.00000 0.09138 0.06288 = 0.04275 0.00162 -0.03239 -0.04625 AFIX 23 H16A 2 -0.136523 0.974584 0.365333 11.00000 -1.20000 H16B 2 -0.035119 0.876766 0.316112 11.00000 -1.20000 AFIX 0 C200 1 0.313290 0.936641 0.402939 11.00000 0.07285 0.09965 = 0.09974 0.01708 -0.00202 -0.02125 AFIX 23 H20C 2 0.280698 1.016779 0.401605 11.00000 -1.20000 H20D 2 0.349282 0.906134 0.355454 11.00000 -1.20000 AFIX 0 C190 1 0.405093 0.888928 0.450969 11.00000 0.07159 0.17694 = 0.15680 0.05932 -0.03236 -0.06320 AFIX 23 H19A 2 0.484701 0.885423 0.425914 11.00000 -1.20000 H19B 2 0.375630 0.929020 0.495198 11.00000 -1.20000 AFIX 0 C180 1 0.396278 0.773869 0.459843 11.00000 0.10376 0.17985 = 0.08449 -0.00055 -0.04355 -0.04255 AFIX 23 H18A 2 0.437519 0.730747 0.416435 11.00000 -1.20000 H18B 2 0.428394 0.732704 0.497033 11.00000 -1.20000 AFIX 0 C170 1 0.271979 0.802529 0.477789 11.00000 0.10157 0.10956 = 0.08655 -0.00479 -0.01659 0.00861 AFIX 23 H17A 2 0.254752 0.743974 0.463802 11.00000 -1.20000 H17B 2 0.236029 0.815216 0.528110 11.00000 -1.20000 AFIX 0 PART 2 C100 1 1.218365 -0.127099 0.076836 -21.00000 0.10079 0.09026 = 0.08984 -0.03101 -0.04014 -0.01605 AFIX 23 H10F 2 1.211537 -0.051098 0.068373 -21.00000 -1.20000 H10G 2 1.177270 -0.133784 0.125789 -21.00000 -1.20000 AFIX 0 PART 1 C65A 1 1.319371 -0.131634 0.037664 21.00000 0.10144 0.09122 = 0.09139 -0.03130 -0.04009 -0.01674 AFIX 23 H65A 2 1.379427 -0.131119 0.057507 21.00000 -1.20000 H65B 2 1.281718 -0.060202 0.018505 21.00000 -1.20000 AFIX 0 HKLF 4 REM 007a-21112 REM R1 = 0.0734 for 8540 Fo > 4sig(Fo) and 0.0901 for all 10888 data REM 645 parameters refined using 75 restraints END WGHT 0.1238 2.8653 REM Highest difference peak 1.585, deepest hole -0.710, 1-sigma level 0.070 Q1 1 1.2712 -0.1249 -0.0196 11.00000 0.05 1.58 Q2 1 0.3781 0.9836 0.4128 11.00000 0.05 1.44 Q3 1 0.3210 0.8538 0.4951 11.00000 0.05 0.91 Q4 1 1.2607 -0.2780 0.0411 11.00000 0.05 0.89 Q5 1 1.2721 -0.2174 0.0885 11.00000 0.05 0.59 Q6 1 1.3812 -0.1818 0.0313 11.00000 0.05 0.47 Q7 1 1.3025 -0.2201 -0.0400 11.00000 0.05 0.40 Q8 1 0.4030 0.8659 0.4474 11.00000 0.05 0.39 Q9 1 1.2871 -0.1030 0.0539 11.00000 0.05 0.35 Q10 1 0.6128 0.5776 0.2950 11.00000 0.05 0.27 Q11 1 0.8214 0.5380 0.2133 11.00000 0.05 0.23 Q12 1 1.0047 0.5786 0.1635 11.00000 0.05 0.23 Q13 1 0.9815 0.5877 0.2629 11.00000 0.05 0.23 Q14 1 0.5932 0.3051 0.2309 11.00000 0.05 0.21 Q15 1 0.7022 0.6343 0.2391 11.00000 0.05 0.21 Q16 1 0.7919 0.4460 0.2399 11.00000 0.05 0.20 Q17 1 0.7357 0.4779 0.2729 11.00000 0.05 0.19 Q18 1 0.9784 0.0632 0.0600 11.00000 0.05 0.19 Q19 1 1.0434 0.4551 0.1697 11.00000 0.05 0.18 Q20 1 0.6769 0.5779 0.3290 11.00000 0.05 0.18 Q21 1 0.8197 0.4886 0.2792 11.00000 0.05 0.18 Q22 1 0.7243 0.7221 0.2923 11.00000 0.05 0.18 Q23 1 0.7440 0.5976 0.1810 11.00000 0.05 0.18 Q24 1 0.0749 0.8853 0.4735 11.00000 0.05 0.17 Q25 1 0.7187 0.6836 0.3093 11.00000 0.05 0.17 Q26 1 0.6139 0.5785 0.2263 11.00000 0.05 0.17 Q27 1 0.7573 0.6451 0.2606 11.00000 0.05 0.17 Q28 1 -0.0692 0.9090 0.5275 11.00000 0.05 0.17 Q29 1 0.6788 0.4800 0.2316 11.00000 0.05 0.17 ; _shelx_res_checksum 40025 _shelx_fab_file ; -14 -9 1 1.0174 -0.1279 -14 -8 1 -0.2943 -0.0051 -14 -7 1 0.2780 0.0537 -14 -6 1 0.9606 -0.2604 -13 -11 1 0.7159 -0.0562 -13 -11 2 -0.4055 0.1982 -13 -10 1 -0.2568 0.2129 -13 -10 2 -1.0119 -0.3152 -13 -10 3 -0.9705 -0.1770 -13 -9 1 -1.0546 -0.3940 -13 -9 2 -0.4290 0.1326 -13 -9 3 -0.6620 0.1226 -13 -9 4 0.1742 -0.0555 -13 -8 1 -0.4198 0.3906 -13 -8 2 0.5222 -0.0059 -13 -8 3 -0.3061 -0.0832 -13 -8 4 0.4062 0.0111 -13 -7 1 0.9774 -0.4128 -13 -7 2 -0.1192 0.0471 -13 -7 3 -0.5485 0.2040 -13 -7 4 -0.3608 0.0261 -13 -6 1 -0.3122 0.4143 -13 -6 2 -1.0483 0.1888 -13 -6 3 -0.6416 -0.1124 -13 -5 1 -1.0567 -0.2413 -13 -5 2 -0.1653 -0.2694 -13 -4 1 0.0768 0.0834 -13 -3 1 0.1060 0.0015 -13 -2 1 0.1854 -0.2290 -13 -1 1 -0.5211 0.2928 -13 0 1 -0.1152 -0.1761 -13 1 1 0.2410 0.2616 -12 -13 1 -0.2179 0.2224 -12 -12 1 -0.0417 -0.5232 -12 -12 2 -0.1106 0.0824 -12 -12 3 -0.4446 0.3603 -12 -11 1 -0.4107 0.5470 -12 -11 2 -0.7855 0.0518 -12 -11 3 0.2982 -0.0800 -12 -11 4 0.0943 -0.0207 -12 -11 5 0.6417 0.1059 -12 -10 1 -0.3948 -0.5109 -12 -10 2 0.1840 -0.1166 -12 -10 3 0.4826 0.1908 -12 -10 4 -0.2509 0.1523 -12 -10 5 0.9926 0.2332 -12 -10 6 0.3746 0.0370 -12 -9 1 0.4423 0.4405 -12 -9 2 0.2609 0.3029 -12 -9 3 -0.2556 -0.1032 -12 -9 4 0.0394 0.0695 -12 -9 5 0.9584 -0.0111 -12 -9 6 0.3422 -0.1730 -12 -9 7 0.3579 -0.1097 -12 -8 1 0.5051 -0.2302 -12 -8 2 -0.4940 -0.3487 -12 -8 3 -0.2224 0.0462 -12 -8 4 -0.0210 0.0923 -12 -8 5 0.6970 -0.0664 -12 -8 6 0.0315 0.0120 -12 -8 7 -0.0464 -0.0621 -12 -7 1 -0.2082 0.1014 -12 -7 2 -0.6901 0.3667 -12 -7 3 -0.0251 -0.0385 -12 -7 4 -0.2638 -0.0638 -12 -7 5 0.8659 -0.0770 -12 -7 6 -0.2409 -0.0823 -12 -7 7 0.6808 -0.0873 -12 -6 1 -0.9681 0.1546 -12 -6 2 0.4487 -0.4302 -12 -6 3 0.0902 -0.1010 -12 -6 4 0.6517 0.0476 -12 -6 5 1.0879 -0.0343 -12 -6 6 -0.2172 0.0899 -12 -5 1 0.6543 -0.3390 -12 -5 2 1.1490 0.3173 -12 -5 3 0.7792 0.1625 -12 -5 4 1.0666 0.0037 -12 -4 1 1.5019 0.4516 -12 -4 2 0.7875 -0.1558 -12 -4 3 0.9103 -0.1977 -12 -3 1 1.0013 -0.5212 -12 -3 2 0.1934 0.0314 -12 -2 1 -0.1939 0.4897 -12 -2 2 0.1027 0.0789 -12 -1 1 -0.1918 -0.3048 -12 -1 2 0.4726 -0.2752 -12 -1 3 -1.5449 0.1504 -12 0 1 0.3042 0.1544 -12 0 2 -0.0414 0.2533 -12 0 3 -1.2958 -0.0510 -12 1 1 -0.2712 -0.0486 -12 1 2 0.4449 -0.2248 -12 1 3 -0.7747 -0.1199 -12 1 4 -0.3382 -0.1222 -12 2 1 0.2458 -0.0673 -12 2 2 0.1053 0.0840 -12 2 3 -0.8906 -0.1785 -12 3 1 -0.2054 0.0973 -11 -14 1 -0.4822 0.5715 -11 -13 1 -0.3777 -0.6439 -11 -13 2 -0.0171 -0.2222 -11 -13 3 0.3075 0.1782 -11 -13 4 0.0737 -0.0089 -11 -12 1 0.3191 0.3671 -11 -12 2 -0.0804 0.4616 -11 -12 3 0.2333 -0.1522 -11 -12 4 0.3935 -0.0969 -11 -12 5 0.0096 -0.0131 -11 -12 6 0.0980 -0.2757 -11 -11 1 0.2602 -0.2495 -11 -11 2 0.0116 -0.4562 -11 -11 3 0.2778 -0.1386 -11 -11 4 0.5632 0.1100 -11 -11 5 0.0920 -0.0096 -11 -11 6 0.0287 -0.0769 -11 -11 7 -0.1332 0.0363 -11 -10 1 0.0983 -0.0715 -11 -10 2 0.0234 0.4624 -11 -10 3 -0.2673 0.0480 -11 -10 4 1.0997 -0.0223 -11 -10 5 -0.0030 -0.1100 -11 -10 6 -0.1307 -0.1394 -11 -10 7 -0.4610 0.0056 -11 -10 8 -0.4583 0.0830 -11 -9 1 -0.2352 0.3214 -11 -9 2 -0.7280 -0.4354 -11 -9 3 0.3725 -0.2253 -11 -9 4 1.7251 0.0304 -11 -9 5 -0.3661 -0.0502 -11 -9 6 -0.2429 0.0635 -11 -9 7 -0.9974 0.1455 -11 -9 8 -0.8176 0.0984 -11 -9 9 -0.7831 0.1119 -11 -8 1 -0.4555 -0.5140 -11 -8 2 -0.2033 0.2907 -11 -8 3 1.5700 0.2567 -11 -8 4 1.0393 -0.0178 -11 -8 5 -0.5757 0.0178 -11 -8 6 -0.5748 0.0078 -11 -8 7 -1.0110 -0.0354 -11 -8 8 -0.5999 0.0238 -11 -8 9 -0.0713 0.0509 -11 -8 10 0.0271 -0.1068 -11 -7 1 0.0456 0.6770 -11 -7 2 0.8789 -0.1073 -11 -7 3 0.9827 -0.2976 -11 -7 4 0.4079 -0.0680 -11 -7 5 -0.3719 0.0055 -11 -7 6 -0.2849 0.0264 -11 -7 7 -0.3925 0.1082 -11 -7 8 -0.5703 0.0984 -11 -7 9 -0.1600 -0.0086 -11 -7 10 -0.8737 -0.0100 -11 -6 1 1.1306 -0.6927 -11 -6 2 0.4206 -0.0535 -11 -6 3 0.2220 0.2650 -11 -6 4 0.3176 0.0360 -11 -6 5 -0.6610 0.0946 -11 -6 6 0.3026 0.0393 -11 -6 7 -0.7483 -0.0412 -11 -6 8 -0.6131 -0.0675 -11 -6 9 0.2222 0.0105 -11 -6 10 0.2114 0.0074 -11 -5 1 0.9551 0.6189 -11 -5 2 -0.7173 0.2833 -11 -5 3 -0.1818 -0.2546 -11 -5 4 -1.0020 -0.1106 -11 -5 5 -0.0331 -0.0564 -11 -5 6 1.1013 -0.0902 -11 -5 7 -0.8950 0.0326 -11 -5 8 0.5490 0.1067 -11 -4 1 -0.2782 -0.4466 -11 -4 2 -1.0211 -0.4125 -11 -4 3 -1.3615 0.1338 -11 -4 4 -0.4702 0.0193 -11 -3 1 -1.2307 0.2063 -11 -3 2 -1.2093 0.5079 -11 -3 3 -1.0779 -0.0279 -11 -2 1 -1.6821 0.0907 -11 -2 2 -0.2033 -0.4250 -11 -2 3 -0.1818 -0.0761 -11 -1 1 0.3122 -0.2673 -11 -1 2 0.5148 0.3937 -11 -1 3 0.5325 0.1024 -11 -1 4 2.0322 -0.0748 -11 0 1 1.0140 0.4547 -11 0 2 0.3400 -0.2132 -11 0 3 0.9849 -0.2132 -11 0 4 0.9436 0.0444 -11 0 5 0.3281 -0.0984 -11 1 1 1.0046 -0.4216 -11 1 2 -0.0424 0.0503 -11 1 3 0.4667 0.1932 -11 1 4 0.1282 0.0042 -11 1 5 0.1111 0.0704 -11 1 6 0.0601 0.1568 -11 2 1 0.6831 0.5039 -11 2 2 -0.7347 0.0181 -11 2 3 0.3963 -0.0845 -11 2 4 -0.4031 0.0992 -11 2 5 0.0039 0.1069 -11 2 6 0.3951 -0.0748 -11 3 1 -0.2200 -0.3782 -11 3 2 -0.3300 -0.1326 -11 3 3 0.1857 0.2341 -11 3 4 -0.3514 -0.0197 -11 3 5 0.3251 -0.1108 -11 4 1 0.0308 0.2437 -11 4 2 0.0348 0.2555 -11 4 3 -0.0255 -0.2675 -11 5 1 -0.1306 0.0162 -10 -14 1 0.5040 -0.2220 -10 -14 2 0.8825 -0.4369 -10 -14 3 -0.0305 -0.2200 -10 -13 1 0.7431 -0.1751 -10 -13 2 0.7553 0.5090 -10 -13 3 -0.2992 0.1580 -10 -13 4 -0.5336 0.2151 -10 -13 5 -0.8789 -0.2042 -10 -13 6 0.6044 -0.1629 -10 -12 1 0.6114 0.4292 -10 -12 2 -0.0044 -0.3761 -10 -12 3 -0.6745 -0.2464 -10 -12 4 -0.5243 0.0610 -10 -12 5 -0.0771 -0.1695 -10 -12 6 0.5255 0.0849 -10 -12 7 -0.9913 0.1458 -10 -11 1 -0.5008 -0.5843 -10 -11 2 -0.3010 0.1827 -10 -11 3 -0.0840 0.4273 -10 -11 4 0.0655 0.0816 -10 -11 5 -0.1384 -0.0538 -10 -11 6 -0.5999 0.0550 -10 -11 7 -0.8162 0.0476 -10 -11 8 -0.0914 -0.1036 -10 -11 9 -0.1069 -0.2039 -10 -10 1 -0.7790 0.7740 -10 -10 2 0.0811 0.0088 -10 -10 3 0.7154 -0.2456 -10 -10 4 -0.2489 -0.1434 -10 -10 5 -0.9083 -0.0466 -10 -10 6 -0.6366 0.0493 -10 -10 7 -0.0323 0.0514 -10 -10 8 -0.1347 -0.0310 -10 -10 9 -0.4130 0.0587 -10 -10 10 -0.2088 -0.0525 -10 -9 1 -0.2487 -0.7572 -10 -9 2 0.6571 -0.2502 -10 -9 3 1.0890 0.3163 -10 -9 4 -1.4072 0.1234 -10 -9 5 -0.9154 0.0716 -10 -9 6 -0.5593 0.0099 -10 -9 7 0.0261 -0.0898 -10 -9 8 0.0069 -0.1097 -10 -9 9 0.6563 -0.0916 -10 -9 10 1.1093 -0.0909 -10 -9 11 0.1051 0.1204 -10 -8 1 0.1560 0.6016 -10 -8 2 1.3327 0.3862 -10 -8 3 -0.2419 -0.1679 -10 -8 4 -2.2726 -0.1739 -10 -8 5 -0.7394 -0.1131 -10 -8 6 -0.6622 -0.0946 -10 -8 7 0.8756 -0.0137 -10 -8 8 1.0967 0.0641 -10 -8 9 1.2570 0.0274 -10 -8 10 0.0340 0.0944 -10 -8 11 -0.7983 0.0615 -10 -7 1 0.4121 -0.4272 -10 -7 2 0.3575 -0.6027 -10 -7 3 -2.0582 0.0687 -10 -7 4 -1.5871 0.1071 -10 -7 5 -0.5749 0.0948 -10 -7 6 0.1286 0.1094 -10 -7 7 1.2795 0.0093 -10 -7 8 0.8959 -0.0537 -10 -7 9 0.3514 -0.0595 -10 -7 10 -0.1371 0.0224 -10 -7 11 -0.0975 -0.1293 -10 -7 12 -0.0068 -0.0872 -10 -6 1 -0.4792 0.0899 -10 -6 2 -1.4067 0.5853 -10 -6 3 -1.5560 0.0625 -10 -6 4 -0.6615 -0.0737 -10 -6 5 -0.0499 -0.0343 -10 -6 6 0.5027 -0.1152 -10 -6 7 0.4826 -0.0966 -10 -6 8 0.7356 0.0195 -10 -6 9 0.1620 0.0689 -10 -6 10 -0.1880 0.0145 -10 -6 11 -1.3655 0.0056 -10 -6 12 -0.2119 0.0469 -10 -5 1 -1.7948 0.2264 -10 -5 2 -0.6225 -0.5863 -10 -5 3 -0.5125 -0.1632 -10 -5 4 0.2616 0.0690 -10 -5 5 0.7221 0.0173 -10 -5 6 -0.5910 0.1149 -10 -5 7 0.1076 0.0659 -10 -5 8 0.4584 0.0202 -10 -5 9 -0.6681 -0.0476 -10 -5 10 -1.0591 0.0181 -10 -5 11 -1.1469 -0.0271 -10 -5 12 1.2856 -0.1468 -10 -4 1 -0.4988 -0.4810 -10 -4 2 0.1124 0.4369 -10 -4 3 0.0603 0.2673 -10 -4 4 1.2774 -0.0193 -10 -4 5 -0.4594 0.0563 -10 -4 6 -1.4163 -0.0365 -10 -4 7 0.4770 -0.1267 -10 -4 8 -0.3106 -0.0558 -10 -4 9 -0.7417 0.0374 -10 -4 10 -0.6376 0.0392 -10 -4 11 -0.1092 -0.0948 -10 -4 12 1.3502 0.0309 -10 -3 1 -0.4073 0.6888 -10 -3 2 -0.1425 -0.2164 -10 -3 3 1.1366 -0.3366 -10 -3 4 0.5650 -0.0056 -10 -3 8 -0.6880 0.0559 -10 -3 9 -0.3982 0.0014 -10 -3 10 -0.4390 -0.0074 -10 -2 1 0.5871 -0.6956 -10 -2 2 0.9781 0.0024 -10 -2 3 1.1834 0.2677 -10 -2 4 -0.4217 0.0524 -10 -1 1 2.3595 0.6707 -10 -1 2 0.1799 0.1695 -10 -1 3 -0.4104 -0.2493 -10 -1 4 -1.6945 -0.0372 -10 -1 5 -1.0650 -0.0422 -10 -1 6 0.1695 -0.0407 -10 -1 7 0.4369 0.0173 -10 0 1 0.1548 -0.5173 -10 0 2 -1.7791 -0.3228 -10 0 3 -1.4306 0.1740 -10 0 4 -0.9255 0.0552 -10 0 5 0.6743 0.0444 -10 0 6 0.5323 0.0712 -10 0 7 -0.6285 -0.0019 -10 0 8 -1.4977 0.0483 -10 0 9 -0.0105 -0.0271 -10 1 1 -2.0081 0.2501 -10 1 2 -1.4149 0.4057 -10 1 3 -0.3991 -0.1086 -10 1 4 0.2845 -0.0675 -10 1 5 0.5384 -0.0018 -10 1 6 -0.0411 -0.0893 -10 1 7 -0.9372 0.0183 -10 1 8 -1.1239 0.0281 -10 1 9 0.1950 -0.0753 -10 2 1 -1.9283 -0.1055 -10 2 2 -0.0217 -0.4287 -10 2 3 -0.2723 -0.0621 -10 2 4 0.3751 0.0954 -10 2 5 0.8654 -0.0212 -10 2 6 0.0478 -0.0039 -10 2 7 -1.0075 0.0455 -10 2 8 -0.8269 -0.0034 -10 2 9 0.1344 -0.0247 -10 3 1 -1.0166 -0.2118 -10 3 2 0.2823 0.3460 -10 3 3 -0.0011 0.0721 -10 3 4 1.2456 -0.0057 -10 3 5 0.3327 -0.0600 -10 3 6 -0.5255 -0.0167 -10 3 7 -0.7266 0.0616 -10 3 8 -0.5401 0.0547 -10 4 1 -0.5240 0.3803 -10 4 2 0.5996 -0.2344 -10 4 3 0.4451 -0.1782 -10 4 4 0.0701 0.1119 -10 4 5 -0.3632 0.1008 -10 4 6 0.3180 0.1593 -10 4 7 -0.4414 0.0528 -10 5 1 0.1286 -0.3337 -10 5 2 0.4827 0.0529 -10 5 3 -0.4516 0.3538 -10 5 4 -0.3140 0.3518 -10 5 5 0.8662 0.1516 -10 6 1 0.5131 0.4274 -10 6 2 -0.0575 0.3613 -9 -15 1 1.5224 0.4035 -9 -14 1 0.9199 -0.6696 -9 -14 2 -0.8639 -0.0266 -9 -14 3 -0.3632 0.4628 -9 -14 4 -0.5122 0.0884 -9 -14 5 -0.6008 -0.1024 -9 -13 1 0.0616 0.6861 -9 -13 2 -0.6739 0.0636 -9 -13 3 -0.1010 -0.1557 -9 -13 4 -0.4531 -0.3643 -9 -13 5 0.5564 -0.0852 -9 -13 6 0.4512 0.0616 -9 -13 7 0.0529 0.0681 -9 -12 1 -0.0781 -0.6466 -9 -12 2 0.0703 -0.3012 -9 -12 3 0.4280 0.2589 -9 -12 4 0.1641 0.0340 -9 -12 5 0.8967 0.2396 -9 -12 6 -0.4743 0.0525 -9 -12 7 0.0057 0.0877 -9 -12 8 0.5562 -0.1517 -9 -12 9 0.6472 -0.2116 -9 -11 1 0.1548 0.5405 -9 -11 2 0.4810 0.5378 -9 -11 3 0.4000 -0.1167 -9 -11 4 -0.0358 -0.2155 -9 -11 5 -0.0995 -0.0593 -9 -11 6 -0.5695 -0.1057 -9 -11 7 0.9040 -0.0083 -9 -11 8 0.9925 -0.0867 -9 -11 9 1.1225 0.2472 -9 -11 10 0.3480 0.0417 -9 -10 1 0.2639 -0.2707 -9 -10 2 0.4511 -0.5842 -9 -10 3 0.0574 -0.0535 -9 -10 4 -0.7922 0.1063 -9 -10 5 -0.1001 0.1091 -9 -10 6 0.6045 0.1162 -9 -10 7 0.9131 0.0230 -9 -10 8 0.6757 0.0028 -9 -10 9 0.8276 -0.0304 -9 -10 10 0.5238 -0.1753 -9 -10 11 0.5455 0.0698 -9 -9 1 0.4705 -0.0059 -9 -9 2 0.3912 0.6479 -9 -9 3 -1.1018 0.1421 -9 -9 4 -0.7948 -0.0920 -9 -9 5 0.7298 -0.0805 -9 -9 6 0.6500 -0.1048 -9 -9 7 0.5315 -0.0886 -9 -9 8 0.9574 0.0340 -9 -9 9 0.6426 0.0517 -9 -9 10 -0.1774 0.1295 -9 -9 11 -0.3222 0.0618 -9 -9 12 0.0830 -0.0754 -9 -8 1 -0.0172 0.3481 -9 -8 2 -0.7531 -0.5602 -9 -8 3 -1.8047 -0.2678 -9 -8 4 0.6909 0.0322 -9 -8 5 1.0322 0.0530 -9 -8 6 1.1206 0.1408 -9 -8 7 0.8093 0.1237 -9 -8 8 0.2078 0.0541 -9 -8 9 -0.9590 -0.0492 -9 -8 10 -0.7867 -0.0380 -9 -8 11 0.4053 -0.1274 -9 -8 12 0.2218 -0.0043 -9 -8 13 -0.3389 0.1226 -9 -7 1 -0.5623 -0.6520 -9 -7 2 -1.6603 0.4590 -9 -7 3 0.0398 0.3629 -9 -7 4 2.0887 0.0592 -9 -7 5 1.4136 0.0543 -9 -7 6 1.3150 -0.0738 -9 -7 7 -0.5589 -0.1336 -9 -7 8 -0.9580 -0.1098 -9 -7 9 -1.1142 0.0224 -9 -7 10 -0.1591 0.0225 -9 -7 11 0.1479 0.0180 -9 -7 12 -0.0642 0.1854 -9 -7 13 0.4265 0.1143 -9 -6 1 -0.8876 0.8602 -9 -6 2 -0.2408 -0.1574 -9 -6 3 2.3875 -0.4187 -9 -6 4 1.9804 -0.0264 -9 -6 5 1.1675 -0.0626 -9 -6 6 -0.2662 -0.0059 -9 -6 7 -1.1314 0.0815 -9 -6 8 -0.7329 0.0829 -9 -6 9 -0.9335 0.0411 -9 -6 10 -0.2613 -0.0603 -9 -6 11 0.9584 0.0396 -9 -6 12 1.3824 0.0226 -9 -6 13 0.2641 -0.0424 -9 -6 14 -0.2566 -0.0565 -9 -5 1 0.6364 -0.9224 -9 -5 2 1.6179 -0.1067 -9 -5 3 2.0374 0.3456 -9 -5 4 0.8069 0.1283 -9 -5 5 -0.2060 0.0854 -9 -5 6 -0.9693 0.0140 -9 -5 7 -0.3639 -0.0737 -9 -5 8 -0.6593 -0.0939 -9 -5 9 -0.0267 -0.0382 -9 -5 10 1.1487 -0.0010 -9 -5 11 2.1653 -0.0138 -9 -5 12 0.1058 0.0449 -9 -5 13 -0.9563 0.1090 -9 -5 14 -0.1315 -0.0215 -9 -4 1 1.0127 0.8100 -9 -4 2 0.3630 0.3150 -9 -4 3 0.8885 -0.3238 -9 -4 4 -0.2153 -0.0799 -9 -4 5 -0.6087 -0.0768 -9 -4 6 -0.1716 -0.0826 -9 -4 7 -0.0508 0.0406 -9 -4 8 0.3109 0.0432 -9 -4 9 1.3084 0.0691 -9 -4 10 1.0984 -0.0542 -9 -4 11 0.6430 0.0271 -9 -4 12 -1.1968 0.0904 -9 -4 13 -0.3250 -0.0303 -9 -4 14 -0.2126 -0.1348 -9 -3 1 -0.4906 -0.5793 -9 -3 2 0.7280 -0.5280 -9 -3 3 0.7606 0.1598 -9 -3 4 -0.4716 0.1358 -9 -3 5 -0.4156 0.0986 -9 -3 6 -0.1990 0.1119 -9 -3 7 0.4142 -0.0283 -9 -3 8 1.2443 -0.0626 -9 -3 9 0.8537 -0.0341 -9 -3 10 -0.0891 -0.0189 -9 -3 11 -0.1545 0.0326 -9 -3 12 -0.9190 -0.0571 -9 -3 13 -0.2157 0.0412 -9 -3 14 -0.3245 -0.0129 -9 -2 1 1.5673 0.3570 -9 -2 2 1.1833 0.5804 -9 -2 3 -0.7537 -0.0825 -9 -2 4 -0.9845 -0.0724 -9 -2 5 -0.6243 -0.0066 -9 -2 6 0.8589 -0.1179 -9 -2 7 1.0292 -0.0264 -9 -2 8 0.7169 0.0266 -9 -2 9 -0.2245 0.0699 -9 -2 10 -0.7148 -0.0137 -9 -2 11 -0.1393 -0.0248 -9 -2 12 -0.8993 0.0794 -9 -2 13 0.1930 0.1023 -9 -1 1 0.2231 0.0020 -9 -1 2 -1.4687 -0.6285 -9 -1 3 -1.5471 -0.0937 -9 -1 4 0.1308 0.0902 -9 -1 5 1.3056 0.0514 -9 -1 6 1.2708 0.1289 -9 -1 7 -0.7548 0.0320 -9 -1 8 -0.3282 -0.0222 -9 -1 9 -0.4909 -0.0070 -9 -1 10 -0.0137 -0.0462 -9 -1 11 0.2393 0.0936 -9 -1 12 -0.6272 0.0156 -9 -1 13 0.9293 -0.1507 -9 0 1 -2.9024 -0.2876 -9 0 2 -0.9085 0.4944 -9 0 3 0.8006 0.1341 -9 0 4 1.9984 -0.0272 -9 0 5 0.7629 0.0591 -9 0 6 -1.2763 -0.0977 -9 0 7 -1.5249 -0.0748 -9 0 8 0.7498 0.0251 -9 0 9 0.8213 0.0307 -9 0 10 0.5684 0.0473 -9 0 11 -0.2959 0.0342 -9 0 12 -0.5322 -0.1227 -9 0 13 0.7006 -0.1036 -9 1 1 -0.7607 0.5294 -9 1 2 1.7495 -0.3994 -9 1 3 1.5184 -0.2421 -9 1 4 0.5628 0.0380 -9 1 5 -0.9955 -0.0347 -9 1 6 -1.2494 0.0611 -9 1 7 0.1396 0.0954 -9 1 8 1.9289 0.0110 -9 1 9 0.3851 -0.0097 -9 1 10 -0.4152 0.0178 -9 1 11 -0.7620 0.0029 -9 1 12 -0.4559 -0.0818 -9 2 1 2.1650 -0.6226 -9 2 2 1.2194 0.1417 -9 2 3 0.2414 0.3073 -9 2 4 -0.0184 0.0050 -9 2 5 -0.6625 0.0748 -9 2 6 -0.5193 -0.0350 -9 2 7 0.5841 -0.0751 -9 2 8 0.8873 -0.0283 -9 2 9 -0.6976 0.0412 -9 2 10 -0.1285 0.0833 -9 2 11 -0.6180 -0.0436 -9 3 1 1.5889 0.6510 -9 3 2 0.0456 0.0553 -9 3 3 0.5037 -0.2019 -9 3 4 -0.3615 -0.0782 -9 3 5 -1.0648 -0.0880 -9 3 6 -0.1467 -0.0528 -9 3 7 0.0539 0.1016 -9 3 8 0.3904 0.0772 -9 3 9 0.0024 0.0613 -9 3 10 0.0825 -0.0809 -9 3 11 -0.5539 -0.2284 -9 4 1 0.9448 -0.5373 -9 4 2 0.2887 -0.2130 -9 4 3 -0.1251 0.1652 -9 4 4 -1.0471 -0.0091 -9 4 5 0.0140 0.0882 -9 4 6 0.1277 0.0247 -9 4 7 -0.1945 0.0002 -9 4 8 0.8653 -0.0593 -9 4 9 -0.4443 -0.1289 -9 5 1 1.2525 0.3088 -9 5 2 -0.3708 0.2918 -9 5 3 -0.3896 -0.1074 -9 5 4 0.3794 -0.0655 -9 5 5 0.4716 -0.1450 -9 5 6 -0.5794 -0.2394 -9 5 7 0.0447 -0.0399 -9 5 8 0.0352 -0.0542 -9 6 1 0.2624 -0.1836 -9 6 2 -0.4930 -0.4261 -9 6 3 0.6640 -0.1543 -9 6 4 0.5030 -0.2314 -9 6 5 -0.4199 -0.2108 -9 6 6 -0.4001 -0.0080 -9 7 1 -0.4278 -0.2799 -9 7 2 0.0977 0.0397 -9 7 3 0.5554 -0.2315 -8 -15 1 -0.4326 -0.8562 -8 -15 2 -1.1847 -0.2221 -8 -15 3 0.1176 0.0912 -8 -14 1 -1.2120 0.3503 -8 -14 2 -0.5759 0.6047 -8 -14 3 0.3299 -0.0944 -8 -14 4 0.4707 -0.0897 -8 -14 5 1.1183 -0.1079 -8 -14 6 0.2797 -0.1430 -8 -13 1 -1.1271 -0.1351 -8 -13 2 0.2302 -0.4877 -8 -13 3 0.4701 -0.1728 -8 -13 4 0.3880 0.1892 -8 -13 5 0.3614 0.1580 -8 -13 6 -0.0540 0.0478 -8 -13 7 0.1668 0.1095 -8 -13 8 -0.5618 -0.0765 -8 -12 1 -0.0388 -0.1071 -8 -12 2 0.0889 0.6181 -8 -12 3 -0.9450 0.1473 -8 -12 4 -0.3666 0.0596 -8 -12 5 0.0290 -0.1494 -8 -12 6 0.0632 -0.1410 -8 -12 7 0.0020 -0.1297 -8 -12 8 -0.1863 -0.1639 -8 -12 9 0.2653 0.1416 -8 -12 10 -0.4418 0.0996 -8 -11 1 -0.5224 0.4920 -8 -11 2 -1.5334 -0.5062 -8 -11 3 -1.1090 -0.3740 -8 -11 4 0.4162 0.0171 -8 -11 5 0.1369 -0.0354 -8 -11 6 0.4242 0.1656 -8 -11 7 0.1361 0.0405 -8 -11 8 -0.0580 0.1314 -8 -11 9 -1.0275 -0.0339 -8 -11 10 -1.6934 -0.2295 -8 -11 11 -0.3550 -0.0294 -8 -10 1 -1.0768 -0.7290 -8 -10 2 -0.4970 0.2950 -8 -10 3 -0.1518 0.3746 -8 -10 4 0.3840 0.0611 -8 -10 5 0.2367 0.0443 -8 -10 6 0.4450 -0.0320 -8 -10 7 -0.3980 -0.1845 -8 -10 8 -0.8284 -0.0878 -8 -10 9 -1.7195 -0.0914 -8 -10 10 -0.8265 0.1383 -8 -10 11 0.0729 0.0820 -8 -10 12 -0.3669 0.0200 -8 -9 1 0.2495 0.8789 -8 -9 2 -0.2040 -0.0628 -8 -9 3 -0.6187 -0.4686 -8 -9 4 0.9941 -0.1180 -8 -9 5 0.4217 -0.0197 -8 -9 6 0.0659 -0.0100 -8 -9 7 -0.4804 0.0911 -8 -9 8 -1.1523 0.1567 -8 -9 9 -1.3919 0.0858 -8 -9 10 -0.1684 -0.0469 -8 -9 11 0.0882 -0.1257 -8 -9 12 -0.4710 0.0208 -8 -9 13 -0.2525 0.0523 -8 -8 1 0.2925 -0.9776 -8 -8 2 -0.4684 -0.1943 -8 -8 3 1.1195 0.3646 -8 -8 4 1.5092 0.1813 -8 -8 5 -0.1928 0.1164 -8 -8 6 -0.1574 0.0299 -8 -8 7 -1.1480 -0.0296 -8 -8 8 -1.3849 -0.1122 -8 -8 9 -0.2031 -0.0792 -8 -8 10 0.7195 -0.0231 -8 -8 11 -0.2464 0.0475 -8 -8 12 -0.9089 0.0470 -8 -8 13 0.0890 0.0747 -8 -8 14 0.3112 0.0442 -8 -7 1 1.1090 0.8598 -8 -7 2 1.2290 0.5081 -8 -7 3 1.9744 -0.3142 -8 -7 4 -0.3415 -0.1731 -8 -7 5 -0.9928 -0.1152 -8 -7 6 -1.3066 -0.0963 -8 -7 7 -1.1002 0.0286 -8 -7 8 0.1734 0.1065 -8 -7 9 0.7585 0.1428 -8 -7 10 0.2517 -0.0261 -8 -7 11 -0.3331 -0.0224 -8 -7 12 0.3769 -0.0335 -8 -7 13 0.3846 -0.0289 -8 -7 14 -0.4379 -0.1162 -8 -7 15 -1.1249 -0.0751 -8 -6 1 1.7369 -0.5741 -8 -6 2 1.6427 -0.7055 -8 -6 3 -0.3034 0.1377 -8 -6 4 -2.1644 0.1590 -8 -6 5 -1.6658 0.0937 -8 -6 6 -0.9781 0.1173 -8 -6 7 0.7489 0.0277 -8 -6 8 0.4787 0.0019 -8 -6 9 0.4779 -0.1063 -8 -6 10 0.9050 -0.0631 -8 -6 11 0.8448 0.0215 -8 -6 12 -0.3679 -0.0414 -8 -6 13 -1.4335 -0.0172 -8 -6 14 -0.9099 -0.0200 -8 -6 15 -0.9255 0.0583 -8 -5 1 0.8765 0.2319 -8 -5 2 -0.3187 0.7772 -8 -5 3 -2.4277 0.0550 -8 -5 4 -2.0023 -0.1496 -8 -5 5 -0.7887 -0.0801 -8 -5 6 0.6409 -0.1581 -8 -5 7 0.8117 -0.0263 -8 -5 8 0.4348 0.0572 -8 -5 9 1.1865 0.0648 -8 -5 10 0.6881 0.0541 -8 -5 11 -1.2335 -0.0258 -8 -5 12 -2.0561 -0.0035 -8 -5 13 -0.6982 -0.0221 -8 -5 14 -0.0137 -0.0335 -8 -5 15 -0.0933 0.0144 -8 -4 1 -0.8140 0.1742 -8 -4 2 -1.0062 -0.7462 -8 -4 3 -1.4953 -0.1487 -8 -4 4 -0.4924 0.0748 -8 -4 5 -0.0716 0.0302 -8 -4 6 0.6603 0.1348 -8 -4 7 0.9280 0.0746 -8 -4 8 0.7944 0.0278 -8 -4 9 -0.4591 -0.0491 -8 -4 10 -1.5450 -0.0588 -8 -4 11 -1.8708 0.0073 -8 -4 12 -0.1625 -0.0010 -8 -4 13 0.3347 -0.0316 -8 -4 14 -0.0005 0.0212 -8 -4 15 0.4021 0.1046 -8 -3 1 0.8915 -0.5238 -8 -3 2 0.2001 0.6245 -8 -3 3 -1.0261 0.3166 -8 -3 4 -0.6682 -0.0588 -8 -3 5 -0.3254 0.0259 -8 -3 6 1.5804 -0.1584 -8 -3 7 1.0535 -0.1190 -8 -3 8 -1.1344 0.0315 -8 -3 9 -2.2293 0.0284 -8 -3 10 -1.1821 0.0681 -8 -3 11 -0.0098 0.0014 -8 -3 12 0.8361 0.0373 -8 -3 13 -0.1810 0.0149 -8 -3 14 0.2271 0.0307 -8 -3 15 0.2626 0.0378 -8 -2 1 0.6132 0.7992 -8 -2 2 -2.1909 -0.4375 -8 -2 3 -1.4933 -0.3918 -8 -2 4 -0.1684 0.0099 -8 -2 5 1.6579 -0.0622 -8 -2 6 1.7142 0.0301 -8 -2 7 -1.3522 0.1244 -8 -2 8 -2.3145 0.0691 -8 -2 9 -1.4814 0.0030 -8 -2 10 0.7618 -0.0525 -8 -2 11 0.9509 -0.0072 -8 -2 12 0.4879 0.0634 -8 -2 13 -0.3789 -0.0764 -8 -2 14 0.1892 0.0076 -8 -2 15 -0.0792 0.0115 -8 -1 1 -3.5959 -0.9820 -8 -1 2 -2.0949 0.0844 -8 -1 3 1.0623 0.4302 -8 -1 4 1.8505 0.0553 -8 -1 5 1.5267 0.0815 -8 -1 6 -1.6643 -0.0483 -8 -1 7 -2.0118 -0.1319 -8 -1 8 -0.7925 -0.0256 -8 -1 9 0.7381 -0.0253 -8 -1 10 1.9122 0.0043 -8 -1 11 -0.2466 0.0447 -8 -1 12 -0.0629 -0.0003 -8 -1 13 -0.5537 -0.0461 -8 -1 14 0.3836 0.1251 -8 -1 15 -0.1299 0.0877 -8 0 1 -1.4920 0.9359 -8 0 2 1.5355 0.1529 -8 0 3 2.2637 -0.3485 -8 0 4 0.6522 -0.0572 -8 0 5 -1.4998 -0.1189 -8 0 6 -2.0538 -0.0777 -8 0 7 0.5253 0.0802 -8 0 8 0.9217 0.0650 -8 0 9 1.2916 -0.0146 -8 0 10 -0.3121 -0.0292 -8 0 11 -1.3879 -0.0086 -8 0 12 0.7070 0.0031 -8 0 13 0.0968 0.0506 -8 0 14 0.8973 0.1254 -8 0 15 -0.6017 -0.0132 -8 1 1 2.1541 -0.7537 -8 1 2 1.4816 -0.4008 -8 1 3 0.3066 0.2925 -8 1 4 -1.1528 0.0757 -8 1 5 -1.4236 0.0830 -8 1 6 0.1074 0.1000 -8 1 7 1.4404 -0.0828 -8 1 8 0.0416 -0.0808 -8 1 9 -0.6189 -0.0919 -8 1 10 -1.0408 0.0066 -8 1 11 0.4676 0.0349 -8 1 12 1.8857 0.0388 -8 1 13 0.3867 0.0595 -8 1 14 -0.0443 0.0519 -8 2 1 0.9165 0.4875 -8 2 2 -0.4993 0.5618 -8 2 3 -0.6683 -0.1346 -8 2 4 -0.7804 -0.0598 -8 2 5 -0.3768 -0.0527 -8 2 6 0.5529 -0.1226 -8 2 7 0.3168 -0.0224 -8 2 8 -1.0412 0.0159 -8 2 9 0.3472 0.0355 -8 2 10 0.6467 0.0493 -8 2 11 1.4048 -0.0206 -8 2 12 1.1376 0.0135 -8 2 13 -1.2226 0.0495 -8 3 1 -1.2361 -0.1568 -8 3 2 -0.5401 -0.5541 -8 3 3 -0.3873 0.0249 -8 3 4 -0.3747 0.0737 -8 3 5 0.1976 0.0094 -8 3 6 0.1628 0.1702 -8 3 7 0.0185 0.0030 -8 3 8 0.4159 0.0005 -8 3 9 1.4011 -0.0586 -8 3 10 -0.0503 -0.0826 -8 3 11 0.5750 -0.0204 -8 3 12 -0.6613 0.1193 -8 3 13 -1.5008 0.1956 -8 4 1 -0.3960 -0.1271 -8 4 2 0.0433 0.5237 -8 4 3 -0.4899 0.1148 -8 4 4 0.2517 -0.0156 -8 4 5 0.3742 0.0325 -8 4 6 -0.2450 -0.0679 -8 4 7 1.0363 -0.1056 -8 4 8 0.3937 -0.0251 -8 4 9 0.1622 -0.0748 -8 4 10 -0.4836 0.0568 -8 4 11 0.3884 0.1912 -8 4 12 -0.4538 0.2970 -8 5 1 -0.0153 0.4007 -8 5 2 -0.5168 -0.3972 -8 5 3 -0.2775 -0.1396 -8 5 4 0.3906 0.0073 -8 5 5 -0.4023 -0.0965 -8 5 6 0.0904 0.0563 -8 5 7 0.9366 0.0320 -8 5 8 -0.5912 0.1068 -8 5 9 0.6570 0.0423 -8 5 10 0.2004 0.1602 -8 6 1 -1.1723 -0.6015 -8 6 2 -0.4078 0.1580 -8 6 3 -0.2723 0.2391 -8 6 4 -0.3178 -0.0058 -8 6 5 -0.3865 0.1067 -8 6 6 0.5667 0.1126 -8 6 7 0.3215 0.0957 -8 6 8 -0.0015 0.0665 -8 6 9 1.0633 -0.0440 -8 7 1 -0.7922 0.5379 -8 7 2 -0.0296 0.0821 -8 7 3 -0.7253 -0.1179 -8 7 4 -0.0452 0.1144 -8 7 5 0.0794 0.1282 -8 7 6 0.3348 0.1326 -8 7 7 0.0329 -0.0144 -8 8 1 0.1867 -0.3462 -8 8 2 -0.2348 -0.2464 -8 8 3 -0.3520 0.2234 -8 8 4 0.3736 0.2989 -7 -15 1 -0.6137 0.0152 -7 -15 2 0.2823 0.5122 -7 -15 3 0.2521 0.2858 -7 -15 4 0.3938 -0.0728 -7 -14 1 -0.3381 0.5760 -7 -14 2 0.5522 -0.4425 -7 -14 3 0.4183 -0.1992 -7 -14 4 0.2802 -0.1564 -7 -14 5 -1.1667 0.0199 -7 -14 6 -0.3186 0.1475 -7 -14 7 -0.3338 0.1084 -7 -13 1 0.4215 -0.6772 -7 -13 2 1.1275 0.2029 -7 -13 3 -0.0773 0.4646 -7 -13 4 -0.7813 0.0289 -7 -13 5 -0.7982 0.0398 -7 -13 6 0.4329 -0.0100 -7 -13 7 -0.2918 -0.0693 -7 -13 8 0.2442 -0.0962 -7 -13 9 -0.1877 -0.1112 -7 -12 1 1.3425 0.8723 -7 -12 2 -0.0652 0.0471 -7 -12 3 -0.8050 -0.3681 -7 -12 4 0.6255 -0.2367 -7 -12 5 0.5231 -0.0474 -7 -12 6 0.1324 0.0441 -7 -12 7 -0.3143 0.0612 -7 -12 8 0.2972 0.2307 -7 -12 9 -0.3992 0.1112 -7 -12 10 -0.3843 -0.1007 -7 -12 11 -0.1272 -0.0467 -7 -11 1 -0.1433 -0.8672 -7 -11 2 0.0894 -0.3658 -7 -11 3 1.5141 0.3194 -7 -11 4 1.3427 0.1700 -7 -11 5 -0.5278 0.1860 -7 -11 6 -0.4057 0.0178 -7 -11 7 -0.1647 -0.0370 -7 -11 8 -0.2395 -0.0641 -7 -11 9 -0.4949 -0.1884 -7 -11 10 0.7139 0.0776 -7 -11 11 1.0921 0.1800 -7 -11 12 0.3978 -0.0210 -7 -10 1 1.0385 0.6870 -7 -10 2 1.8486 0.5532 -7 -10 3 1.1262 -0.2119 -7 -10 4 -0.3194 -0.1880 -7 -10 5 -0.6296 -0.1069 -7 -10 6 -0.1173 -0.1761 -7 -10 7 -0.0921 0.0427 -7 -10 8 -0.0011 0.1282 -7 -10 9 1.0128 0.2082 -7 -10 10 1.6060 0.0758 -7 -10 11 0.2090 -0.0903 -7 -10 12 -0.1704 -0.0209 -7 -10 13 -0.2036 -0.0300 -7 -10 14 -0.1284 -0.3505 -7 -9 1 1.7513 -0.3832 -7 -9 2 0.3258 -0.7842 -7 -9 3 0.5468 0.0366 -7 -9 4 -0.0552 0.2089 -7 -9 5 -0.2204 0.1190 -7 -9 6 -0.2737 0.1114 -7 -9 7 -0.0137 0.0950 -7 -9 8 0.6868 -0.0305 -7 -9 9 1.7839 -0.1514 -7 -9 10 0.7317 -0.1194 -7 -9 11 -0.7118 0.0656 -7 -9 12 -0.0082 0.0222 -7 -9 13 0.0110 -0.1031 -7 -9 14 0.4412 -0.1463 -7 -8 1 0.3605 0.0834 -7 -8 2 0.3995 0.7664 -7 -8 3 0.9482 0.1598 -7 -8 4 -1.0885 -0.1121 -7 -8 5 -0.5110 -0.1212 -7 -8 6 -0.5676 -0.1871 -7 -8 7 0.4235 -0.1043 -7 -8 8 1.6196 -0.0254 -7 -8 9 1.3763 0.0936 -7 -8 10 -0.7073 0.1214 -7 -8 11 -0.8887 -0.0152 -7 -8 12 0.7823 -0.0317 -7 -8 13 0.7628 -0.0386 -7 -8 14 0.8141 -0.1129 -7 -8 15 0.1908 0.0206 -7 -7 1 -0.3601 0.4006 -7 -7 2 -0.1264 -0.7897 -7 -7 3 -1.3098 -0.2789 -7 -7 4 -1.4416 0.0603 -7 -7 5 0.2049 0.0172 -7 -7 6 0.1517 0.1265 -7 -7 7 1.6593 0.0806 -7 -7 8 0.9761 0.0394 -7 -7 9 -0.3676 -0.0718 -7 -7 10 -0.9590 -0.1034 -7 -7 11 0.4166 -0.0109 -7 -7 12 0.9659 0.0815 -7 -7 13 0.0336 -0.0650 -7 -7 14 0.0215 -0.0486 -7 -7 15 0.0872 0.1030 -7 -7 16 0.9619 0.0114 -7 -6 1 -2.3945 -0.7178 -7 -6 2 -1.9864 0.5425 -7 -6 3 -1.6393 0.4419 -7 -6 4 0.8239 0.0019 -7 -6 5 1.3829 0.0096 -7 -6 6 1.2062 -0.1561 -7 -6 7 0.4987 -0.1506 -7 -6 8 -0.7256 -0.0506 -7 -6 9 -0.0610 0.0104 -7 -6 10 0.0246 0.1171 -7 -6 11 -0.2037 0.0535 -7 -6 12 -0.8396 0.0136 -7 -6 13 -0.1219 -0.0829 -7 -6 14 0.6506 0.0364 -7 -6 15 1.4424 0.0449 -7 -6 16 1.1821 -0.0169 -7 -5 1 -2.9256 1.0071 -7 -5 2 -1.3928 -0.3200 -7 -5 3 1.0506 -0.4681 -7 -5 4 2.6515 -0.0292 -7 -5 5 1.2030 -0.0861 -7 -5 6 0.0207 0.0534 -7 -5 7 -0.8385 0.1564 -7 -5 8 0.1058 0.0672 -7 -5 9 0.0759 0.0066 -7 -5 10 -1.1602 -0.0808 -7 -5 11 -1.1690 -0.0391 -7 -5 12 0.1773 0.0065 -7 -5 13 1.3647 -0.0282 -7 -5 14 1.3226 0.0514 -7 -5 15 1.2465 0.0243 -7 -5 16 -0.7674 -0.0027 -7 -4 1 -0.5273 -1.1406 -7 -4 2 0.8875 -0.0269 -7 -4 3 2.3749 0.5098 -7 -4 4 1.1608 0.1211 -7 -4 5 -0.3577 0.0999 -7 -4 6 -0.0199 -0.0016 -7 -4 7 -0.0496 -0.1500 -7 -4 8 -0.4299 -0.0992 -7 -4 9 -1.0986 -0.0507 -7 -4 10 -0.4800 0.0403 -7 -4 11 0.9574 0.0809 -7 -4 12 1.4532 0.0214 -7 -4 13 0.8981 -0.0127 -7 -4 14 0.7050 -0.0022 -7 -4 15 -0.4315 0.0056 -7 -4 16 -1.2347 -0.1223 -7 -4 17 0.3025 -0.1640 -7 -3 1 0.2049 1.0657 -7 -3 2 0.0782 0.3291 -7 -3 3 0.5630 -0.4273 -7 -3 4 -0.2076 -0.0900 -7 -3 5 1.0424 -0.1386 -7 -3 6 0.6724 -0.0977 -7 -3 7 -1.5315 0.1121 -7 -3 8 -1.1067 0.0982 -7 -3 9 0.6193 0.0584 -7 -3 10 1.9517 -0.0100 -7 -3 11 1.7109 -0.0329 -7 -3 12 0.1836 -0.0411 -7 -3 13 0.0888 -0.0690 -7 -3 14 -0.0161 -0.0144 -7 -3 15 -0.8187 -0.0219 -7 -3 16 0.2851 -0.1010 -7 -3 17 0.6137 0.0044 -7 -2 1 -2.8853 -0.8620 -7 -2 2 -0.2159 -0.6610 -7 -2 3 1.3346 0.3069 -7 -2 4 1.6048 0.1853 -7 -2 5 1.2815 0.0998 -7 -2 6 -2.2277 0.1339 -7 -2 7 -1.5674 -0.0583 -7 -2 8 1.3837 -0.0764 -7 -2 9 2.7052 -0.0825 -7 -2 10 2.0624 -0.0469 -7 -2 11 -0.1528 0.0139 -7 -2 12 -0.9325 -0.0239 -7 -2 13 0.1186 0.0087 -7 -2 14 -0.0622 -0.0052 -7 -2 15 0.1225 0.0048 -7 -2 16 0.7751 -0.0391 -7 -2 17 -0.0109 -0.0079 -7 -1 1 -0.3176 0.4126 -7 -1 2 3.3527 0.7594 -7 -1 3 2.2445 -0.1025 -7 -1 4 0.5649 -0.0687 -7 -1 5 -2.2944 -0.0916 -7 -1 6 -2.0013 -0.2098 -7 -1 7 1.9825 0.0077 -7 -1 8 2.6627 0.0704 -7 -1 9 2.1078 0.0314 -7 -1 10 -0.7562 0.0329 -7 -1 11 -1.3496 -0.0123 -7 -1 12 -0.2402 -0.0173 -7 -1 13 0.8222 -0.0196 -7 -1 14 0.1921 -0.0483 -7 -1 15 0.1590 0.0199 -7 -1 16 0.4344 -0.0862 -7 0 1 3.9741 -0.0910 -7 0 2 2.8289 -0.8219 -7 0 3 -0.2921 -0.0430 -7 0 4 -2.2043 0.1362 -7 0 5 -2.0893 0.0046 -7 0 6 1.8347 0.1641 -7 0 7 2.6689 0.0613 -7 0 8 1.2973 -0.0218 -7 0 9 -0.5988 -0.0348 -7 0 10 -2.0451 -0.0300 -7 0 11 0.6435 -0.0385 -7 0 12 0.5770 -0.0227 -7 0 13 0.8889 0.0118 -7 0 14 -1.0976 0.0050 -7 0 15 -0.0612 0.0130 -7 0 16 0.5887 -0.0630 -7 1 1 2.0245 -0.3846 -7 1 2 -0.2205 0.6550 -7 1 3 -2.0684 0.1949 -7 1 4 -1.7464 -0.0154 -7 1 5 0.8756 0.0410 -7 1 6 2.6404 -0.1907 -7 1 7 0.9863 -0.0469 -7 1 8 -0.2229 0.0222 -7 1 9 -1.3561 0.0425 -7 1 10 0.0557 0.0433 -7 1 11 1.4280 -0.0293 -7 1 12 -0.4039 0.0470 -7 1 13 -0.8103 0.0125 -7 1 14 -2.0763 -0.0265 -7 1 15 1.4674 -0.0506 -7 1 16 0.4371 -0.1028 -7 2 1 -0.7152 0.5919 -7 2 2 -1.5413 -0.5104 -7 2 3 -1.2750 -0.2874 -7 2 4 0.4529 0.0570 -7 2 5 1.9499 -0.1082 -7 2 6 1.3677 0.0854 -7 2 7 -0.0469 0.1277 -7 2 8 -0.0661 0.0033 -7 2 9 -0.6057 0.0722 -7 2 10 0.2585 -0.0615 -7 2 11 -0.1010 -0.0373 -7 2 12 -1.9601 -0.0118 -7 2 13 -1.3071 -0.0194 -7 2 14 0.5705 -0.0098 -7 2 15 2.3797 -0.1015 -7 3 1 -1.1247 -0.7982 -7 3 2 -0.7279 0.2301 -7 3 3 0.5813 0.2771 -7 3 4 1.2547 -0.0094 -7 3 5 1.0157 0.1062 -7 3 6 0.2141 -0.0697 -7 3 7 0.0532 -0.0935 -7 3 8 -0.1317 0.0046 -7 3 9 -1.6090 -0.0267 -7 3 10 -0.2022 -0.0464 -7 3 11 -1.0436 0.0103 -7 3 12 -1.2626 0.0470 -7 3 13 1.4670 0.0537 -7 3 14 1.7266 -0.0943 -7 4 1 -0.1241 0.8038 -7 4 2 0.0665 -0.0354 -7 4 3 0.7566 -0.3514 -7 4 4 0.4222 -0.0022 -7 4 5 -0.1227 -0.1391 -7 4 6 0.1958 -0.0542 -7 4 7 -0.3625 0.1184 -7 4 8 -1.1268 -0.0276 -7 4 9 -1.4045 0.0374 -7 4 10 0.3428 0.0376 -7 4 11 -0.6571 0.0635 -7 4 12 0.8905 -0.0291 -7 4 13 1.2518 -0.1608 -7 4 14 -0.4075 -0.1353 -7 5 1 -0.6945 -0.7400 -7 5 2 -0.3169 -0.2148 -7 5 3 0.4718 0.2013 -7 5 4 -0.1487 0.0239 -7 5 5 -0.0841 0.1061 -7 5 6 0.2934 0.0755 -7 5 7 -1.1998 -0.0107 -7 5 8 -0.5916 -0.0264 -7 5 9 -0.7731 0.0284 -7 5 10 0.5244 0.0088 -7 5 11 -0.1423 -0.0950 -7 5 12 0.3088 -0.2707 -7 6 1 -0.9228 0.4830 -7 6 2 0.4078 0.3758 -7 6 3 0.6434 -0.1375 -7 6 4 -0.0308 0.0775 -7 6 5 0.4278 -0.0642 -7 6 6 -0.2608 -0.0565 -7 6 7 -1.3074 0.0830 -7 6 8 -0.1156 -0.0978 -7 6 9 -0.7103 0.0342 -7 6 10 0.7311 -0.1118 -7 6 11 -0.7335 -0.2563 -7 7 1 0.8367 -0.2097 -7 7 2 0.7965 -0.3600 -7 7 3 0.7324 0.1416 -7 7 4 0.1996 0.0217 -7 7 5 0.1180 0.0101 -7 7 6 -1.0252 0.1018 -7 7 7 -0.6851 -0.0898 -7 7 8 0.2567 -0.0926 -7 7 9 -0.3113 -0.0761 -7 8 1 0.9760 -0.0616 -7 8 2 0.2806 0.4125 -7 8 3 0.7989 0.1435 -7 8 4 -0.4667 0.0408 -7 8 5 -0.3014 -0.0882 -7 8 6 -0.5952 -0.2387 -7 8 7 0.2385 -0.0853 -7 9 1 -0.1325 0.2210 -7 9 2 0.2863 -0.0604 -7 9 3 0.1355 0.0783 -7 9 4 -0.7954 -0.2357 -7 9 5 0.3890 -0.3537 -6 -15 1 0.0207 0.8641 -6 -15 2 0.4706 0.0224 -6 -15 3 0.1785 -0.3184 -6 -15 4 0.0302 -0.0837 -6 -15 5 0.3381 0.0389 -6 -14 1 0.1540 -0.7306 -6 -14 2 0.3057 -0.2489 -6 -14 3 -0.0696 0.2121 -6 -14 4 -0.4156 0.2986 -6 -14 5 0.6226 0.1749 -6 -14 6 0.0789 0.0035 -6 -14 7 0.1464 0.0668 -6 -14 8 -0.3286 -0.2631 -6 -13 1 0.3515 0.5520 -6 -13 2 -0.5413 0.5792 -6 -13 3 -0.9207 -0.1997 -6 -13 4 0.0466 -0.0915 -6 -13 5 1.3060 -0.2022 -6 -13 6 -0.4083 -0.1231 -6 -13 7 0.2224 -0.0341 -6 -13 8 -0.7540 -0.0384 -6 -13 9 -0.0309 0.3550 -6 -13 10 -0.2792 -0.0570 -6 -12 1 -0.9900 -0.2925 -6 -12 2 -1.7115 -0.7439 -6 -12 3 0.2450 -0.0875 -6 -12 4 0.9582 0.1908 -6 -12 5 0.2951 0.0770 -6 -12 6 -0.8359 0.1321 -6 -12 7 0.0153 0.0691 -6 -12 8 -1.1902 -0.0200 -6 -12 9 0.2257 -0.1352 -6 -12 10 0.2487 -0.1844 -6 -12 11 0.9891 0.1977 -6 -12 12 -0.2631 -0.0415 -6 -11 1 -1.5671 -0.1536 -6 -11 2 -0.1631 0.6686 -6 -11 3 1.0060 0.2206 -6 -11 4 -0.7879 -0.0416 -6 -11 5 -0.3724 -0.1289 -6 -11 6 -0.3506 -0.1752 -6 -11 7 -0.1641 -0.0868 -6 -11 8 -0.4317 -0.0591 -6 -11 9 0.8759 0.1272 -6 -11 10 0.4837 0.1685 -6 -11 11 0.0284 -0.0012 -6 -11 12 -0.8276 -0.0559 -6 -11 13 0.0569 0.0370 -6 -10 1 0.0328 0.4438 -6 -10 2 -0.0821 -0.6520 -6 -10 3 -0.6658 -0.3088 -6 -10 4 -1.1751 0.0461 -6 -10 5 0.5134 -0.0006 -6 -10 6 -0.1666 0.1681 -6 -10 7 0.1289 0.1653 -6 -10 8 0.0455 0.0520 -6 -10 9 0.0663 -0.0815 -6 -10 10 -0.7178 -0.2000 -6 -10 11 -0.6997 -0.0399 -6 -10 12 -0.0518 0.0912 -6 -10 13 0.2075 -0.0458 -6 -10 14 -0.0519 0.1092 -6 -9 1 -0.7799 -0.8745 -6 -9 2 -0.9654 0.4166 -6 -9 3 -0.8558 0.4870 -6 -9 4 -0.5733 0.0793 -6 -9 5 0.2492 0.0347 -6 -9 6 -0.2108 -0.0937 -6 -9 7 0.2060 -0.1740 -6 -9 8 -0.4016 -0.1420 -6 -9 9 -1.0619 -0.0248 -6 -9 10 -1.2190 0.1267 -6 -9 11 0.1031 0.0829 -6 -9 12 0.6441 -0.0048 -6 -9 13 0.3241 0.0066 -6 -9 14 0.2629 0.1920 -6 -9 15 0.3590 -0.0064 -6 -8 1 -1.7943 0.9822 -6 -8 2 -0.7774 -0.1554 -6 -8 3 -1.3100 -0.4669 -6 -8 4 -0.4571 -0.0667 -6 -8 5 0.1171 -0.1219 -6 -8 6 0.2852 0.0324 -6 -8 7 0.1748 0.1731 -6 -8 8 -1.1014 0.1359 -6 -8 9 -1.8151 0.0389 -6 -8 10 -0.4645 -0.1292 -6 -8 11 1.3073 -0.0760 -6 -8 12 0.6416 0.0430 -6 -8 13 -0.0034 0.0575 -6 -8 14 -0.6253 0.0856 -6 -8 15 -0.7597 -0.0640 -6 -8 16 -1.0911 0.0197 -6 -7 1 -1.8057 -1.1570 -6 -7 2 -0.8132 -0.1881 -6 -7 3 -0.8016 0.4865 -6 -7 4 0.7993 0.1348 -6 -7 5 0.2966 0.1193 -6 -7 6 0.4290 0.0890 -6 -7 7 -1.0168 -0.0941 -6 -7 8 -1.7581 -0.1305 -6 -7 9 -0.7605 -0.1049 -6 -7 10 1.1586 0.0296 -6 -7 11 1.0842 0.1213 -6 -7 12 -0.5775 0.0015 -6 -7 13 -0.8104 -0.0020 -6 -7 14 -1.1816 0.0193 -6 -7 15 -0.3680 -0.0632 -6 -7 16 -0.3320 0.0209 -6 -7 17 -0.0640 0.0152 -6 -6 1 -0.2887 0.9593 -6 -6 2 0.5313 0.4794 -6 -6 3 1.3584 -0.4048 -6 -6 4 1.1057 -0.1426 -6 -6 5 -0.7324 -0.1248 -6 -6 6 -0.9893 -0.1068 -6 -6 7 -1.6570 0.1165 -6 -6 8 0.0995 0.1366 -6 -6 9 0.6598 0.0845 -6 -6 10 0.6200 -0.0363 -6 -6 11 -0.5219 -0.0815 -6 -6 12 -0.6962 -0.0803 -6 -6 13 -0.2348 0.0269 -6 -6 14 -0.0961 0.0232 -6 -6 15 0.1798 0.0044 -6 -6 16 -1.0271 0.0604 -6 -6 17 -0.4295 0.0165 -6 -5 1 2.2854 -0.7779 -6 -5 2 2.4948 -0.7673 -6 -5 3 1.8405 0.2451 -6 -5 4 -1.4721 0.1555 -6 -5 5 -2.2779 0.0797 -6 -5 6 -0.9474 0.2072 -6 -5 7 0.4196 0.0123 -6 -5 8 0.8969 -0.1200 -6 -5 9 -0.3523 -0.1511 -6 -5 10 -0.2539 -0.0403 -6 -5 11 -0.1806 0.0595 -6 -5 12 0.5370 0.0181 -6 -5 13 0.2844 0.0850 -6 -5 14 0.1012 0.0216 -6 -5 15 -1.1888 0.0184 -6 -5 16 -0.8952 -0.0472 -6 -5 17 1.1192 0.0049 -6 -5 18 0.9705 0.0794 -6 -4 1 3.0295 0.2952 -6 -4 2 1.9822 0.9172 -6 -4 3 -1.5135 -0.0905 -6 -4 4 -3.3313 -0.1821 -6 -4 5 -0.3086 -0.0818 -6 -4 6 0.8310 -0.2012 -6 -4 7 0.2972 -0.0297 -6 -4 8 -0.6612 0.0693 -6 -4 9 -0.2096 0.1066 -6 -4 10 0.5195 0.0888 -6 -4 11 0.4592 -0.0317 -6 -4 12 0.0977 -0.0281 -6 -4 13 -0.3699 -0.0027 -6 -4 14 -0.7945 -0.0266 -6 -4 15 -1.0017 -0.0177 -6 -4 16 1.3093 -0.0345 -6 -4 17 0.9171 0.1387 -6 -4 18 -0.3787 0.0044 -6 -3 1 0.8894 0.1037 -6 -3 2 -0.7212 -0.9305 -6 -3 3 -2.5865 -0.1404 -6 -3 4 -0.0293 0.1112 -6 -3 5 1.6034 -0.0198 -6 -3 6 -1.0554 0.2131 -6 -3 7 -1.1272 0.1307 -6 -3 8 -0.0122 -0.0196 -6 -3 9 1.0203 -0.0762 -6 -3 10 0.2169 -0.0959 -6 -3 11 -1.1026 -0.0179 -6 -3 12 -1.2618 -0.0140 -6 -3 13 -0.5484 0.0154 -6 -3 14 -0.4579 0.0426 -6 -3 15 0.9149 0.0182 -6 -3 16 1.0055 0.0730 -6 -3 17 -0.9876 0.0597 -6 -3 18 -0.4549 -0.0870 -6 -2 1 0.8968 -0.6040 -6 -2 2 -0.0427 0.7935 -6 -2 3 0.0582 0.3248 -6 -2 4 1.1376 -0.1021 -6 -2 5 -1.6219 0.0404 -6 -2 6 -2.1179 -0.1798 -6 -2 7 0.7277 -0.1111 -6 -2 8 0.7952 -0.0035 -6 -2 9 0.0995 0.0132 -6 -2 10 -2.2979 0.0608 -6 -2 11 -2.3876 0.0356 -6 -2 12 -0.4115 0.0076 -6 -2 13 0.3066 0.0223 -6 -2 14 0.4626 -0.0088 -6 -2 15 0.8535 0.0065 -6 -2 16 -1.0628 0.0315 -6 -2 17 -1.1714 -0.0277 -6 -2 18 0.0295 -0.0442 -6 -1 1 2.7866 0.8575 -6 -1 2 0.0458 -0.5356 -6 -1 3 -0.5867 -0.3727 -6 -1 4 -1.9247 0.0519 -6 -1 5 -2.2462 -0.1675 -6 -1 6 1.2543 0.0902 -6 -1 7 0.9276 0.2016 -6 -1 8 -0.9563 0.0204 -6 -1 9 -2.2830 -0.0026 -6 -1 10 -2.8176 -0.0452 -6 -1 11 -0.0830 0.0241 -6 -1 12 0.7685 -0.0273 -6 -1 13 0.1680 -0.0371 -6 -1 14 0.0666 0.0168 -6 -1 15 -0.4873 0.0305 -6 -1 16 -1.5254 0.0548 -6 -1 17 -0.4536 -0.0423 -6 -1 18 0.2046 -0.0516 -6 0 1 0.2525 -1.1159 -6 0 2 -1.9290 0.2496 -6 0 3 -2.2419 0.5468 -6 0 4 -1.7576 -0.0658 -6 0 5 1.3403 0.0953 -6 0 6 1.6315 0.0030 -6 0 7 -1.7162 -0.1335 -6 0 8 -2.2171 -0.0232 -6 0 9 -2.1264 -0.0312 -6 0 10 0.2516 0.0382 -6 0 11 0.7362 0.0555 -6 0 12 -0.0360 -0.0240 -6 0 13 -0.7064 0.0446 -6 0 14 -0.4272 0.0005 -6 0 15 -0.3987 -0.0114 -6 0 16 -0.7903 -0.0145 -6 0 17 0.0063 -0.0866 -6 1 1 -1.6527 1.0767 -6 1 2 -2.2892 0.1209 -6 1 3 -1.2206 -0.4164 -6 1 4 1.2105 -0.0190 -6 1 5 1.8326 -0.1533 -6 1 6 -1.1193 -0.0628 -6 1 7 -2.5154 0.1521 -6 1 8 -1.4712 0.0343 -6 1 9 -0.1732 0.0188 -6 1 10 0.9293 0.0028 -6 1 11 -0.5068 0.0172 -6 1 12 -0.2449 -0.0039 -6 1 13 -1.1877 -0.0451 -6 1 14 1.2326 -0.0842 -6 1 15 0.0844 -0.0157 -6 1 16 -0.6538 0.0358 -6 1 17 0.0253 0.0480 -6 2 1 -1.5470 -0.9737 -6 2 2 -1.0076 -0.3585 -6 2 3 1.3726 0.4325 -6 2 4 1.4808 0.0048 -6 2 5 -0.8207 0.0694 -6 2 6 -2.1926 0.1409 -6 2 7 -1.5466 -0.1443 -6 2 8 -0.7422 -0.0097 -6 2 9 0.3279 -0.0424 -6 2 10 0.6103 -0.0163 -6 2 11 -0.3824 0.0377 -6 2 12 -0.3232 -0.0475 -6 2 13 0.6352 0.0126 -6 2 14 2.3123 -0.0212 -6 2 15 -1.9944 0.0672 -6 2 16 -0.3126 0.0565 -6 2 17 0.1579 0.0750 -6 3 1 -0.6434 0.6654 -6 3 2 1.3401 0.5685 -6 3 3 1.3460 -0.2525 -6 3 4 -0.9712 -0.0425 -6 3 5 -2.0131 -0.0451 -6 3 6 -1.2078 -0.2065 -6 3 7 -0.8623 0.0654 -6 3 8 -0.4497 0.0898 -6 3 9 1.5220 -0.0160 -6 3 10 0.6310 0.0473 -6 3 11 -0.6853 0.0025 -6 3 12 0.9187 0.0670 -6 3 13 1.5019 -0.0092 -6 3 14 -0.7916 -0.0750 -6 3 15 -2.2075 -0.0051 -6 3 16 1.5307 0.0370 -6 4 1 0.8737 -0.3525 -6 4 2 1.2805 -0.7131 -6 4 3 -0.6062 0.1919 -6 4 4 -1.6853 0.0406 -6 4 5 -0.8354 -0.0129 -6 4 6 -0.2972 0.1976 -6 4 7 -0.3189 0.0175 -6 4 8 0.9367 -0.0072 -6 4 9 1.8694 0.0103 -6 4 10 -0.8184 -0.0324 -6 4 11 0.2982 0.0533 -6 4 12 1.0898 -0.0267 -6 4 13 -0.6546 -0.0888 -6 4 14 -1.1763 -0.0260 -6 4 15 0.3489 -0.0021 -6 5 1 0.8987 -0.0658 -6 5 2 0.3414 0.6623 -6 5 3 -0.8947 0.0144 -6 5 4 -0.5346 -0.0636 -6 5 5 0.2604 0.1152 -6 5 6 -0.0570 -0.1650 -6 5 7 0.6977 -0.0281 -6 5 8 0.9922 0.0573 -6 5 9 0.7979 -0.0221 -6 5 10 -0.4423 0.0070 -6 5 11 0.8496 -0.0207 -6 5 12 -0.4571 -0.0077 -6 5 13 -0.2266 0.0679 -6 5 14 -0.1160 -0.0480 -6 6 1 1.1607 0.3525 -6 6 2 0.1445 -0.5825 -6 6 3 -0.5330 -0.0638 -6 6 4 0.3150 0.0240 -6 6 5 0.1418 -0.1388 -6 6 6 -0.0081 0.1142 -6 6 7 1.0260 0.0297 -6 6 8 0.6657 -0.0081 -6 6 9 1.3762 -0.0151 -6 6 10 -0.5060 -0.1023 -6 6 11 -0.1908 0.0606 -6 6 12 -0.2414 0.1739 -6 6 13 0.1723 0.0173 -6 7 1 0.8405 -0.5956 -6 7 2 -0.6598 0.4349 -6 7 3 -0.4198 0.1321 -6 7 4 0.1737 -0.1941 -6 7 5 -0.3743 0.1724 -6 7 6 0.6346 -0.0967 -6 7 7 1.4568 -0.1501 -6 7 8 0.7656 0.0204 -6 7 9 0.5803 -0.1302 -6 7 10 -1.6560 0.1293 -6 7 11 0.1729 0.2982 -6 7 12 0.2516 0.1999 -6 8 1 -0.8807 0.7355 -6 8 2 -0.7697 -0.1656 -6 8 3 -0.4502 -0.3399 -6 8 4 0.0099 0.0406 -6 8 5 0.1110 -0.1957 -6 8 6 1.3706 -0.0955 -6 8 7 0.6147 0.0390 -6 8 8 -0.1639 0.0722 -6 8 9 -0.2433 0.2252 -6 8 10 -1.0172 0.3500 -6 9 1 -0.7759 -0.6620 -6 9 2 -0.0818 -0.0556 -6 9 3 -0.5373 0.1394 -6 9 4 0.6529 -0.2177 -6 9 5 0.2405 0.0724 -6 9 6 0.5321 0.1527 -6 9 7 -0.3406 0.1073 -6 9 8 0.0870 0.3778 -6 10 1 0.1900 0.5016 -6 10 2 -0.2374 0.2975 -6 10 3 -0.0229 -0.2970 -6 10 4 0.6319 0.0992 -6 10 5 -0.6910 0.1289 -5 -15 1 0.1782 -0.4388 -5 -15 2 -0.0599 -0.6086 -5 -15 3 -0.3803 -0.0261 -5 -15 4 0.0460 0.0760 -5 -15 5 -0.5645 0.2102 -5 -14 1 0.2792 -0.1910 -5 -14 2 -0.5836 0.5433 -5 -14 3 -0.2738 0.1448 -5 -14 4 0.2306 -0.1000 -5 -14 5 -0.7122 -0.1539 -5 -14 6 -0.4640 -0.2142 -5 -14 7 0.0973 -0.1140 -5 -14 8 0.4903 -0.1347 -5 -13 1 -0.3259 0.4023 -5 -13 2 -0.3266 -0.5789 -5 -13 3 0.8361 -0.3455 -5 -13 4 0.6029 -0.1115 -5 -13 5 -1.1980 0.0015 -5 -13 6 0.2821 0.1285 -5 -13 7 0.0693 0.0823 -5 -13 8 0.2371 0.1303 -5 -13 9 0.2842 -0.1515 -5 -13 10 0.4225 -0.1163 -5 -13 11 0.6619 -0.2560 -5 -12 1 0.4033 -0.7696 -5 -12 2 1.2952 0.2944 -5 -12 3 1.3191 0.4130 -5 -12 4 -0.3336 0.0183 -5 -12 5 -1.0429 0.1098 -5 -12 6 0.6537 -0.0770 -5 -12 7 -1.0016 -0.1460 -5 -12 8 1.0944 -0.1329 -5 -12 9 1.0505 -0.1763 -5 -12 10 0.7900 0.1925 -5 -12 11 -0.4497 -0.0052 -5 -12 12 -0.8153 0.0853 -5 -12 13 0.3069 -0.1883 -5 -11 1 1.7048 0.9616 -5 -11 2 1.4691 -0.0061 -5 -11 3 -0.1989 -0.4362 -5 -11 4 -0.6549 -0.1075 -5 -11 5 -0.5487 -0.0630 -5 -11 6 -0.0260 -0.0121 -5 -11 7 -0.2558 0.1329 -5 -11 8 2.2439 0.1331 -5 -11 9 0.2622 0.0420 -5 -11 10 -0.2502 -0.0528 -5 -11 11 -1.1386 -0.2035 -5 -11 12 0.2290 -0.0257 -5 -11 13 0.4640 -0.1225 -5 -11 14 0.3072 0.0517 -5 -10 1 1.1635 -0.9805 -5 -10 2 0.1650 -0.2437 -5 -10 3 -1.1240 0.4339 -5 -10 4 -0.1521 0.1568 -5 -10 5 -0.6283 0.1105 -5 -10 6 0.5561 0.0786 -5 -10 7 0.6851 -0.0800 -5 -10 8 0.9695 -0.1436 -5 -10 9 -0.5149 -0.1515 -5 -10 10 -0.1167 0.0138 -5 -10 11 -0.0031 0.0757 -5 -10 12 0.6876 0.0167 -5 -10 13 -0.0366 -0.0656 -5 -10 14 0.4272 -0.0198 -5 -10 15 -0.3994 0.0183 -5 -9 1 -0.0656 0.8396 -5 -9 2 -0.6217 0.6152 -5 -9 3 -0.9383 -0.3074 -5 -9 4 0.4405 -0.1796 -5 -9 5 0.0174 -0.1422 -5 -9 6 1.1877 -0.1436 -5 -9 7 -0.0642 0.0406 -5 -9 8 0.2436 0.1420 -5 -9 9 0.1658 0.1312 -5 -9 10 0.5968 0.0099 -5 -9 11 0.6922 -0.0790 -5 -9 12 -0.0442 -0.0997 -5 -9 13 -0.3416 -0.0546 -5 -9 14 -0.1456 -0.0331 -5 -9 15 -1.0104 0.0395 -5 -9 16 -0.0004 -0.1137 -5 -8 1 -0.2906 -0.5407 -5 -8 2 -0.0728 -0.8064 -5 -8 3 0.2162 0.1835 -5 -8 4 0.9610 0.1535 -5 -8 5 0.6129 0.0583 -5 -8 6 0.7704 0.1995 -5 -8 7 -0.5553 0.0398 -5 -8 8 0.5430 -0.0796 -5 -8 9 0.9572 -0.1633 -5 -8 10 1.1533 -0.0470 -5 -8 11 0.1410 0.0766 -5 -8 12 -1.0102 0.0067 -5 -8 13 -0.5305 0.0013 -5 -8 14 -0.3536 -0.0604 -5 -8 15 -0.3612 -0.0006 -5 -8 16 0.7192 -0.0938 -5 -8 17 0.3604 0.1366 -5 -7 1 1.4454 0.0646 -5 -7 2 0.9600 0.9737 -5 -7 3 0.8166 0.0569 -5 -7 4 1.0951 -0.2024 -5 -7 5 0.6240 -0.0402 -5 -7 6 -0.2265 -0.2041 -5 -7 7 -0.0871 -0.1066 -5 -7 8 1.6016 0.0626 -5 -7 9 1.3633 0.1379 -5 -7 10 0.0872 0.1275 -5 -7 11 -1.2468 -0.0278 -5 -7 12 -0.8244 -0.0506 -5 -7 13 0.2239 -0.0576 -5 -7 14 0.5902 -0.0558 -5 -7 15 0.5610 0.0710 -5 -7 16 0.8012 0.0316 -5 -7 17 0.2381 0.1276 -5 -7 18 -0.0465 -0.2045 -5 -6 1 2.0723 0.3503 -5 -6 2 0.9097 -0.8578 -5 -6 3 1.3868 -0.2300 -5 -6 4 0.1763 0.1410 -5 -6 5 -0.5748 -0.0071 -5 -6 6 0.0155 0.1573 -5 -6 7 1.8887 0.1469 -5 -6 8 1.4398 0.0182 -5 -6 9 -0.3501 -0.0964 -5 -6 10 -1.3163 -0.1052 -5 -6 11 -0.7029 0.0182 -5 -6 12 0.7268 0.0508 -5 -6 13 1.1660 0.0112 -5 -6 14 0.8934 0.0579 -5 -6 15 -0.1143 0.0702 -5 -6 16 0.2570 -0.0246 -5 -6 17 0.4514 -0.0538 -5 -6 18 -0.3410 -0.2264 -5 -5 1 0.9402 -0.8102 -5 -5 2 1.2762 0.7664 -5 -5 3 -0.6269 0.4433 -5 -5 4 -1.9468 -0.1082 -5 -5 5 0.6798 0.0595 -5 -5 6 2.1366 -0.1359 -5 -5 7 1.4952 -0.1742 -5 -5 8 -0.7786 -0.0430 -5 -5 9 -1.0306 0.0502 -5 -5 10 -0.5890 0.1387 -5 -5 11 0.9147 0.0654 -5 -5 12 1.3722 0.0104 -5 -5 13 0.7737 -0.0147 -5 -5 14 -0.5023 -0.0260 -5 -5 15 -0.7194 -0.0576 -5 -5 16 0.7446 -0.0793 -5 -5 17 -0.0682 -0.0342 -5 -5 18 -1.4173 -0.0760 -5 -5 19 -0.1926 0.1507 -5 -4 1 0.6395 1.1092 -5 -4 2 -1.6399 -0.4114 -5 -4 3 -3.0812 -0.5256 -5 -4 4 1.2121 0.0608 -5 -4 5 3.0450 -0.0733 -5 -4 6 0.6545 0.0553 -5 -4 7 -0.8691 0.1892 -5 -4 8 -0.5606 0.0771 -5 -4 9 0.1181 0.0062 -5 -4 10 0.5266 -0.0982 -5 -4 11 1.1493 -0.0401 -5 -4 12 0.2975 -0.0082 -5 -4 13 -0.3533 -0.0450 -5 -4 14 -1.0210 -0.0116 -5 -4 15 0.3276 -0.0243 -5 -4 16 0.0764 0.0502 -5 -4 17 -1.2817 0.0043 -5 -4 18 -0.5015 -0.0089 -5 -4 19 0.9473 0.1444 -5 -3 1 -1.3645 -1.2405 -5 -3 2 -3.5758 0.0900 -5 -3 3 1.2976 0.6405 -5 -3 4 3.9186 -0.0038 -5 -3 5 -0.3757 0.1204 -5 -3 6 -1.7150 0.0280 -5 -3 7 0.0310 -0.1692 -5 -3 8 1.3626 -0.0864 -5 -3 9 0.7006 -0.0677 -5 -3 10 0.2120 0.0373 -5 -3 11 -0.2000 0.0644 -5 -3 12 0.2096 -0.0029 -5 -3 13 0.2416 0.0283 -5 -3 14 0.0669 0.0179 -5 -3 15 0.1149 0.0179 -5 -3 16 -1.2826 0.0101 -5 -3 17 -0.2190 -0.0888 -5 -3 18 0.8173 0.0424 -5 -3 19 0.3481 0.0763 -5 -2 1 -2.7097 1.2065 -5 -2 2 -0.0800 0.3202 -5 -2 3 3.5243 -0.5632 -5 -2 4 -0.3809 -0.0539 -5 -2 5 -2.8173 -0.1007 -5 -2 6 0.5237 -0.1126 -5 -2 7 1.9604 0.1578 -5 -2 8 1.8359 0.0781 -5 -2 9 -0.3871 0.0351 -5 -2 10 -0.5913 0.0087 -5 -2 11 1.0420 -0.0296 -5 -2 12 1.9486 0.0231 -5 -2 13 0.4821 0.0037 -5 -2 14 -0.1328 0.0085 -5 -2 15 -1.1415 -0.0018 -5 -2 16 -0.4637 -0.0331 -5 -2 17 1.0714 -0.0104 -5 -2 18 0.7318 0.0675 -5 -2 19 -0.0375 0.0650 -5 -1 1 -2.0722 -1.0302 -5 -1 2 1.7900 -0.6191 -5 -1 3 -0.0267 0.5212 -5 -1 4 -2.3412 0.0875 -5 -1 5 0.5661 0.0214 -5 -1 6 2.4388 0.2153 -5 -1 7 1.5133 -0.0739 -5 -1 8 0.7103 -0.0722 -5 -1 9 -0.8804 -0.0655 -5 -1 10 1.7630 0.0111 -5 -1 11 2.4433 0.0370 -5 -1 12 0.8367 0.0103 -5 -1 13 -0.3616 0.0199 -5 -1 14 -0.5319 0.0339 -5 -1 15 -0.7392 0.0185 -5 -1 16 1.1710 -0.0126 -5 -1 17 1.2265 -0.0295 -5 -1 18 0.6172 0.0290 -5 -1 19 -0.3185 0.0602 -5 0 1 -0.3141 0.6159 -5 0 2 0.3364 0.9776 -5 0 3 -1.5746 -0.2722 -5 0 4 1.0377 -0.2010 -5 0 5 2.5826 -0.0039 -5 0 6 0.6583 -0.1870 -5 0 7 0.5013 0.0610 -5 0 8 0.4373 0.0577 -5 0 9 1.1178 0.0136 -5 0 10 2.2835 0.0605 -5 0 11 0.2446 -0.0619 -5 0 12 0.0570 0.0400 -5 0 13 -0.0713 -0.0124 -5 0 14 -0.0416 0.0238 -5 0 15 0.5105 0.0057 -5 0 16 1.6031 -0.0414 -5 0 17 0.5969 0.0275 -5 0 18 0.0088 0.0504 -5 0 19 -0.4507 0.0557 -5 1 1 -0.1888 -0.1295 -5 1 2 -1.0385 -0.9274 -5 1 3 0.9914 0.0833 -5 1 4 2.4748 0.1646 -5 1 5 0.2714 -0.0771 -5 1 6 -0.7133 0.2186 -5 1 7 1.1590 0.0435 -5 1 8 1.1451 -0.0973 -5 1 9 1.1962 -0.0172 -5 1 10 0.2182 -0.0697 -5 1 11 0.2584 0.0192 -5 1 12 0.3113 0.0255 -5 1 13 0.4020 -0.0368 -5 1 14 0.4006 0.0852 -5 1 15 0.3858 0.0145 -5 1 16 0.7664 0.0598 -5 1 17 -0.0898 -0.0053 -5 1 18 -0.1133 -0.0269 -5 2 1 -1.4124 -0.3385 -5 2 2 0.9924 0.9645 -5 2 3 1.8647 0.1587 -5 2 4 -0.0973 -0.2166 -5 2 5 -0.7613 0.0586 -5 2 6 0.5860 -0.1701 -5 2 7 1.7425 -0.0413 -5 2 8 0.5406 0.0477 -5 2 9 0.5948 -0.0224 -5 2 10 0.3444 0.0536 -5 2 11 0.2435 0.0201 -5 2 12 -0.0190 0.0050 -5 2 13 0.9416 0.0119 -5 2 14 -1.2493 0.0455 -5 2 15 0.3210 -0.0049 -5 2 16 0.7211 -0.0013 -5 2 17 -0.1662 -0.1041 -5 2 18 -0.0997 -0.0335 -5 3 1 0.5303 0.7281 -5 3 2 1.9271 -0.7084 -5 3 3 -0.5592 -0.2750 -5 3 4 -0.7309 0.1584 -5 3 5 0.9116 -0.1416 -5 3 6 1.2085 0.1376 -5 3 7 0.9772 0.1772 -5 3 8 0.7549 -0.0789 -5 3 9 0.6886 0.0158 -5 3 10 -0.7595 -0.0498 -5 3 11 -0.1825 0.0055 -5 3 12 0.7480 0.0101 -5 3 13 -0.6316 -0.0835 -5 3 14 -1.5144 0.0259 -5 3 15 2.2098 -0.0046 -5 3 16 -0.4227 0.0639 -5 3 17 -0.5494 -0.1302 -5 4 1 1.6462 -1.0254 -5 4 2 -0.0095 0.4725 -5 4 3 -1.2793 0.4740 -5 4 4 0.8589 -0.1323 -5 4 5 1.3377 0.1101 -5 4 6 0.4541 -0.0130 -5 4 7 1.1677 -0.1267 -5 4 8 0.7417 -0.0009 -5 4 9 -1.4038 -0.0904 -5 4 10 -0.7696 0.0279 -5 4 11 1.0945 0.0581 -5 4 12 0.0352 -0.0818 -5 4 13 -1.2985 -0.0091 -5 4 14 0.3963 0.0459 -5 4 15 0.9647 0.0922 -5 4 16 -1.6992 0.0009 -5 4 17 0.6120 -0.2365 -5 5 1 0.0075 1.0329 -5 5 2 -1.1956 -0.0688 -5 5 3 -0.1600 -0.4327 -5 5 4 1.4690 0.1457 -5 5 5 0.2158 -0.1491 -5 5 6 0.4610 -0.0278 -5 5 7 0.7756 0.1222 -5 5 8 -1.0488 -0.0692 -5 5 9 -1.5108 -0.0010 -5 5 10 1.0494 0.0865 -5 5 11 0.2921 -0.1017 -5 5 12 -0.6398 0.0099 -5 5 13 -0.9224 -0.0293 -5 5 14 0.1132 0.0573 -5 5 15 0.2206 0.1578 -5 5 16 0.2027 -0.0565 -5 6 1 -1.6309 -0.9690 -5 6 2 -0.7840 -0.1701 -5 6 3 0.9060 0.5038 -5 6 4 0.3943 -0.0523 -5 6 5 -0.3206 0.0420 -5 6 6 0.5138 0.1177 -5 6 7 -0.6962 -0.1417 -5 6 8 -1.0284 0.0162 -5 6 9 -0.6629 -0.0598 -5 6 10 0.3906 -0.0101 -5 6 11 -0.6269 0.0083 -5 6 12 -0.1942 0.0511 -5 6 13 -0.7414 -0.0518 -5 6 14 1.1694 0.2268 -5 6 15 1.0553 0.2302 -5 7 1 -1.7703 0.7251 -5 7 2 0.3760 0.4613 -5 7 3 0.7407 -0.3677 -5 7 4 -0.4273 0.0587 -5 7 5 0.1969 -0.0169 -5 7 6 -0.3605 -0.1658 -5 7 7 -1.2779 0.1186 -5 7 8 -0.6867 -0.0443 -5 7 9 -1.1631 0.0129 -5 7 10 0.4366 0.1890 -5 7 11 0.1829 -0.0185 -5 7 12 0.3646 -0.0516 -5 7 13 0.0176 -0.0338 -5 8 1 -0.6540 -0.3811 -5 8 2 1.0747 -0.6527 -5 8 3 0.2562 0.2848 -5 8 4 -0.3130 0.0443 -5 8 5 0.0530 -0.0801 -5 8 6 -1.3136 0.2203 -5 8 7 -0.8045 0.0330 -5 8 8 -0.3150 0.0393 -5 8 9 -0.5031 0.1146 -5 8 10 1.2279 -0.1105 -5 8 11 0.2626 -0.1913 -5 8 12 0.0017 -0.1620 -5 9 1 0.5943 -0.0161 -5 9 2 0.5117 0.6165 -5 9 3 -0.0688 -0.0925 -5 9 4 -0.2863 -0.0891 -5 9 5 -0.2215 0.1906 -5 9 6 -0.8963 -0.0768 -5 9 7 0.4415 0.1164 -5 9 8 -0.1007 -0.0972 -5 9 9 -0.1251 -0.2348 -5 9 10 0.8970 -0.1594 -5 10 1 0.1879 0.3762 -5 10 2 -0.2086 -0.5730 -5 10 3 0.3280 -0.1377 -5 10 4 -0.3134 0.1323 -5 10 5 0.2248 -0.1587 -5 10 6 0.0478 0.1131 -5 10 7 0.5640 0.0055 -5 10 8 -0.4742 -0.3180 -5 11 1 -0.1374 -0.5797 -5 11 2 0.4107 0.0592 -5 11 3 0.1942 0.0999 -5 11 4 -0.1827 -0.1373 -4 -15 1 0.5637 -0.6228 -4 -15 2 0.0493 0.3332 -4 -15 3 0.5020 0.2568 -4 -15 4 0.1917 0.0884 -4 -15 5 -0.0964 -0.2406 -4 -14 1 -0.1052 0.7516 -4 -14 2 0.1379 -0.0129 -4 -14 3 0.9036 -0.3201 -4 -14 4 0.0769 -0.1432 -4 -14 5 0.0253 -0.2482 -4 -14 6 0.7128 0.1365 -4 -14 7 0.6381 0.0745 -4 -14 8 -0.0718 0.1284 -4 -14 9 -0.7177 0.2490 -4 -13 1 0.0753 -0.7280 -4 -13 2 1.1833 -0.2615 -4 -13 3 0.6149 0.3821 -4 -13 4 -0.7296 0.1490 -4 -13 5 0.4873 0.1125 -4 -13 6 0.5604 0.1404 -4 -13 7 -0.2921 -0.0568 -4 -13 8 -0.3007 -0.0218 -4 -13 9 -0.2105 -0.0138 -4 -13 10 0.3091 -0.0750 -4 -13 11 -0.4434 0.1732 -4 -12 1 0.6793 0.6254 -4 -12 2 0.3523 0.5637 -4 -12 3 -1.0439 -0.1501 -4 -12 4 -0.5657 -0.1333 -4 -12 5 0.9193 -0.1203 -4 -12 6 -0.9083 -0.0866 -4 -12 7 0.4470 0.0645 -4 -12 8 0.8306 0.1248 -4 -12 9 -0.2023 0.1952 -4 -12 10 -0.7532 0.0664 -4 -12 11 -1.2712 0.1331 -4 -12 12 0.0854 -0.2220 -4 -12 13 0.4329 -0.0748 -4 -11 1 -1.1270 -0.3434 -4 -11 2 -1.2136 -0.7202 -4 -11 3 -0.7407 0.1204 -4 -11 4 0.4334 0.1670 -4 -11 5 0.4305 0.0576 -4 -11 6 -0.2285 0.2048 -4 -11 7 2.4622 0.0772 -4 -11 8 -0.5706 -0.0688 -4 -11 9 -1.4873 -0.0834 -4 -11 10 -1.3595 -0.0786 -4 -11 11 -0.0504 0.0734 -4 -11 12 0.9305 -0.0452 -4 -11 13 -0.3089 0.2364 -4 -11 14 -0.6539 -0.0080 -4 -11 15 -0.2586 -0.1734 -4 -10 1 -2.0253 -0.1079 -4 -10 2 -0.7567 0.8440 -4 -10 3 0.4858 0.1796 -4 -10 4 1.0529 -0.1965 -4 -10 5 1.4280 -0.0908 -4 -10 6 1.0174 -0.1521 -4 -10 7 0.6749 -0.0985 -4 -10 8 -2.5743 -0.0035 -4 -10 9 -0.8176 0.1206 -4 -10 10 -0.3440 0.1122 -4 -10 11 0.8739 0.0858 -4 -10 12 -0.1262 -0.0169 -4 -10 13 -0.7741 -0.0010 -4 -10 14 -0.5742 -0.0924 -4 -10 15 -0.0562 0.0300 -4 -10 16 0.3795 -0.0059 -4 -9 1 -1.2777 0.5141 -4 -9 2 -0.0296 -0.7025 -4 -9 3 1.9124 -0.3153 -4 -9 4 1.8608 0.0436 -4 -9 5 1.6164 -0.0090 -4 -9 6 -0.8744 0.1607 -4 -9 7 -1.2001 0.1482 -4 -9 8 -1.5224 -0.0000 -4 -9 9 0.2507 -0.0758 -4 -9 10 0.2118 -0.0630 -4 -9 11 0.1441 0.0305 -4 -9 12 -0.8754 -0.0201 -4 -9 13 -0.3933 0.0769 -4 -9 14 -0.2937 0.1094 -4 -9 15 0.8317 -0.0455 -4 -9 16 0.3040 -0.0690 -4 -9 17 -0.3494 0.1479 -4 -8 1 -0.0278 -0.8718 -4 -8 2 0.9881 0.5680 -4 -8 3 2.2342 0.5067 -4 -8 4 1.1833 -0.0786 -4 -8 5 0.1623 0.0252 -4 -8 6 -2.2130 -0.1112 -4 -8 7 -0.4777 -0.1554 -4 -8 8 -0.3805 -0.0811 -4 -8 9 0.3154 0.0419 -4 -8 10 -0.1516 0.1450 -4 -8 11 -0.9083 0.0441 -4 -8 12 -0.3522 0.0238 -4 -8 13 0.1778 0.0516 -4 -8 14 0.3638 -0.0339 -4 -8 15 1.0160 -0.0939 -4 -8 16 -0.1860 0.1123 -4 -8 17 0.1730 0.1275 -4 -8 18 0.3405 -0.0783 -4 -7 1 0.9967 1.1732 -4 -7 2 0.3833 -0.1550 -4 -7 3 1.9109 -0.5585 -4 -7 4 0.1943 -0.0398 -4 -7 5 -1.6922 -0.0897 -4 -7 6 -1.8138 0.0421 -4 -7 7 0.6438 0.2121 -4 -7 8 -0.4972 0.0611 -4 -7 9 -0.5606 -0.0083 -4 -7 10 -0.7794 -0.0878 -4 -7 11 -0.2545 -0.0406 -4 -7 12 0.9837 -0.0033 -4 -7 13 0.3327 -0.0233 -4 -7 14 0.1334 0.0534 -4 -7 15 0.1698 0.0270 -4 -7 16 -0.2812 0.1022 -4 -7 17 0.2116 -0.0896 -4 -7 18 -0.2151 -0.0203 -4 -6 1 0.1577 -1.1367 -4 -6 2 1.2593 -0.1740 -4 -6 3 0.7608 0.6077 -4 -6 4 -3.2591 0.0740 -4 -6 5 -1.9207 0.0793 -4 -6 6 0.6648 0.0499 -4 -6 7 0.3096 -0.1498 -4 -6 8 -1.8595 -0.1526 -4 -6 9 -0.7824 -0.0651 -4 -6 10 0.4869 0.0714 -4 -6 11 1.3360 0.0609 -4 -6 12 0.8674 -0.0258 -4 -6 13 -0.9145 0.0334 -4 -6 14 -0.9267 0.0110 -4 -6 15 -0.1284 -0.0568 -4 -6 16 0.0865 -0.0164 -4 -6 17 -0.3930 -0.1113 -4 -6 18 -0.5376 0.1136 -4 -6 19 -0.0343 0.0328 -4 -5 1 2.4121 1.0702 -4 -5 2 -0.0892 0.5341 -4 -5 3 -4.6732 -0.4892 -4 -5 4 -2.4212 -0.1348 -4 -5 5 1.9966 -0.1139 -4 -5 6 0.6299 -0.1252 -4 -5 7 -1.9692 0.1469 -4 -5 8 -1.4773 0.0792 -4 -5 9 0.7591 0.0519 -4 -5 10 1.6799 -0.0062 -4 -5 11 0.9733 -0.0826 -4 -5 12 -1.0273 -0.0332 -4 -5 13 -2.1571 -0.0473 -4 -5 14 -0.7041 -0.0322 -4 -5 15 0.6758 -0.0120 -4 -5 16 -0.0265 0.0014 -4 -5 17 -0.7906 0.0059 -4 -5 18 0.5637 0.1683 -4 -5 19 0.5905 0.0450 -4 -4 1 0.3925 -0.6993 -4 -4 2 -5.9782 -0.8540 -4 -4 3 -2.0304 0.3941 -4 -4 4 3.3782 0.1890 -4 -4 5 0.4732 0.0170 -4 -4 6 -2.2461 0.2115 -4 -4 7 -1.1710 -0.0706 -4 -4 8 0.4786 -0.1438 -4 -4 9 1.2609 -0.0756 -4 -4 10 0.8819 0.0037 -4 -4 11 -1.0543 0.0290 -4 -4 12 -1.9941 -0.0134 -4 -4 13 -1.1117 0.0046 -4 -4 14 0.8544 0.0445 -4 -4 15 0.7951 0.0135 -4 -4 16 -0.2653 0.0234 -4 -4 17 0.3211 0.0258 -4 -4 18 1.3444 0.0844 -4 -4 19 -0.3732 -0.1107 -4 -4 20 -0.1345 -0.2055 -4 -3 1 -6.9183 0.2948 -4 -3 2 -1.6099 1.0247 -4 -3 3 4.6758 -0.1327 -4 -3 4 0.1300 -0.2294 -4 -3 5 -3.4192 -0.0389 -4 -3 6 -0.4161 -0.2103 -4 -3 7 1.3639 0.0076 -4 -3 8 0.6470 0.0930 -4 -3 9 0.0767 0.0725 -4 -3 10 -1.2885 0.0718 -4 -3 11 -1.3238 -0.0412 -4 -3 12 -0.1271 0.0171 -4 -3 13 0.2648 -0.0004 -4 -3 14 0.7148 0.0066 -4 -3 15 -0.0819 0.0005 -4 -3 16 0.3383 -0.0357 -4 -3 17 0.7116 -0.0061 -4 -3 18 0.1236 -0.0097 -4 -3 19 -0.9778 -0.1051 -4 -3 20 0.2711 -0.0826 -4 -2 1 -3.5276 0.2075 -4 -2 2 5.9575 -1.0372 -4 -2 3 0.6914 -0.0713 -4 -2 4 -4.2879 0.2457 -4 -2 5 -0.4879 -0.0610 -4 -2 6 2.5996 0.2521 -4 -2 7 1.5338 0.0832 -4 -2 8 -1.0935 -0.1002 -4 -2 9 -2.0155 -0.0336 -4 -2 10 -1.2902 -0.0406 -4 -2 11 0.9038 0.0315 -4 -2 12 -0.1092 -0.0015 -4 -2 13 -0.7765 -0.0305 -4 -2 14 -0.3234 0.0206 -4 -2 15 0.0304 -0.0338 -4 -2 16 0.6729 -0.0329 -4 -2 17 0.0275 0.0044 -4 -2 18 -0.4156 -0.0039 -4 -2 19 -0.3908 -0.0189 -4 -2 20 0.3006 -0.0637 -4 -1 1 5.1074 -0.6489 -4 -1 2 2.5821 0.9663 -4 -1 3 -4.0267 0.3775 -4 -1 4 -0.8948 -0.2465 -4 -1 5 2.9239 0.0608 -4 -1 6 2.1294 -0.1499 -4 -1 7 -0.6549 -0.1283 -4 -1 8 -3.5241 0.0346 -4 -1 9 -1.5260 0.0174 -4 -1 10 0.5317 0.0696 -4 -1 11 -0.0082 -0.0137 -4 -1 12 -1.8772 -0.0555 -4 -1 13 -0.7595 -0.0047 -4 -1 14 -0.2175 -0.0172 -4 -1 15 0.6024 -0.0146 -4 -1 16 0.1939 -0.0490 -4 -1 17 -0.3111 0.0090 -4 -1 18 -0.7591 0.0279 -4 -1 19 -0.0708 0.0040 -4 -1 20 -0.0975 -0.0364 -4 0 1 3.9620 1.1104 -4 0 2 -3.4957 -0.5708 -4 0 3 -0.5855 -0.5444 -4 0 4 2.5582 0.1187 -4 0 5 1.6275 -0.0989 -4 0 6 -0.6354 0.1310 -4 0 7 -2.9203 0.1744 -4 0 8 -2.6586 -0.0994 -4 0 9 0.5841 0.0136 -4 0 10 -0.5049 -0.0550 -4 0 11 -1.2257 -0.0310 -4 0 12 -1.0954 -0.0258 -4 0 13 -0.2323 -0.0207 -4 0 14 -0.0239 0.0367 -4 0 15 0.4835 -0.0280 -4 0 16 -0.6875 -0.0381 -4 0 17 -0.7427 0.0380 -4 0 18 -0.7773 0.0154 -4 0 19 0.4470 0.0042 -4 0 20 -0.5213 -0.0523 -4 1 1 -2.0949 -1.1854 -4 1 2 -0.7965 0.2571 -4 1 3 3.2612 0.5753 -4 1 4 0.3797 -0.1444 -4 1 5 -1.1639 0.1049 -4 1 6 -1.6654 0.0240 -4 1 7 -1.8275 -0.2187 -4 1 8 -0.3340 0.0215 -4 1 9 0.1490 -0.0036 -4 1 10 -0.9592 0.0301 -4 1 11 -0.3096 0.0459 -4 1 12 -0.8479 -0.0767 -4 1 13 -0.2511 0.0630 -4 1 14 -0.0735 -0.0131 -4 1 15 -0.1083 -0.0373 -4 1 16 -0.9364 -0.0471 -4 1 17 -0.4514 -0.0069 -4 1 18 -0.1228 0.0133 -4 1 19 0.3518 -0.0093 -4 2 1 0.3620 1.2384 -4 2 2 3.3737 0.1636 -4 2 3 0.3222 -0.6542 -4 2 4 -1.9531 0.0160 -4 2 5 -0.8814 -0.0634 -4 2 6 -0.1140 -0.0337 -4 2 7 -0.7198 0.1968 -4 2 8 -0.0380 -0.0047 -4 2 9 -0.0298 0.0067 -4 2 10 -0.3284 0.0647 -4 2 11 -0.7245 -0.0967 -4 2 12 -0.7364 -0.0173 -4 2 13 -0.3088 -0.0003 -4 2 14 0.2982 -0.0368 -4 2 15 0.3354 0.0189 -4 2 16 -0.7395 -0.0589 -4 2 17 -0.3784 0.0733 -4 2 18 0.0991 -0.0133 -4 2 19 0.1647 0.0611 -4 3 1 4.0156 -0.9839 -4 3 2 0.2144 -0.4545 -4 3 3 -2.2925 0.5262 -4 3 4 -0.6603 0.0109 -4 3 5 0.3858 0.0339 -4 3 6 0.2485 0.1839 -4 3 7 -0.8253 -0.1735 -4 3 8 0.4773 -0.0120 -4 3 9 -0.5051 0.0156 -4 3 10 -0.8463 -0.0484 -4 3 11 -0.4754 0.0052 -4 3 12 -0.3446 -0.0213 -4 3 13 0.1931 0.0270 -4 3 14 1.6934 0.0500 -4 3 15 -0.6730 0.0267 -4 3 16 -1.1705 -0.0494 -4 3 17 0.0601 0.0380 -4 3 18 0.5633 -0.0155 -4 3 19 -0.1333 0.1233 -4 4 1 0.9944 0.6497 -4 4 2 -2.9144 0.8003 -4 4 3 -0.8206 -0.4384 -4 4 4 0.6857 -0.1147 -4 4 5 0.2356 -0.0030 -4 4 6 0.1379 -0.1712 -4 4 7 -0.4060 0.1316 -4 4 8 -0.4840 0.0218 -4 4 9 -1.3691 -0.0442 -4 4 10 0.1869 0.1022 -4 4 11 0.1082 -0.0338 -4 4 12 -0.2713 -0.0150 -4 4 13 1.0349 0.0385 -4 4 14 0.5527 -0.0211 -4 4 15 -1.6738 0.0091 -4 4 16 0.5987 -0.0707 -4 4 17 0.4349 0.1518 -4 4 18 0.1673 0.0169 -4 5 1 -2.1245 -0.2033 -4 5 2 -1.6810 -0.8249 -4 5 3 1.4632 0.2000 -4 5 4 0.0784 0.1172 -4 5 5 0.1132 -0.1029 -4 5 6 0.4042 0.2471 -4 5 7 -1.4889 -0.0707 -4 5 8 -1.3168 -0.0998 -4 5 9 0.2634 0.1256 -4 5 10 0.8466 -0.0904 -4 5 11 -0.3911 -0.0082 -4 5 12 -0.4535 -0.0097 -4 5 13 0.8161 -0.0006 -4 5 14 0.3385 0.0643 -4 5 15 0.1047 0.0185 -4 5 16 0.5340 0.0233 -4 5 17 -0.9408 0.0766 -4 6 1 -0.7246 -0.1737 -4 6 2 1.3944 0.8725 -4 6 3 1.0674 -0.0252 -4 6 4 -0.8492 -0.2396 -4 6 5 0.9298 0.1174 -4 6 6 -0.9746 -0.2068 -4 6 7 -1.8717 -0.0109 -4 6 8 0.3959 0.0721 -4 6 9 1.3284 -0.0387 -4 6 10 -0.0241 0.0086 -4 6 11 -0.6197 0.1331 -4 6 12 -0.0695 -0.0756 -4 6 13 1.8242 0.0997 -4 6 14 0.4104 -0.0200 -4 6 15 -0.9605 -0.1545 -4 6 16 -1.0000 -0.1153 -4 7 1 2.3222 0.5217 -4 7 2 1.4285 -0.6605 -4 7 3 -0.6166 -0.2018 -4 7 4 0.0602 0.1805 -4 7 5 -0.0838 -0.1799 -4 7 6 -1.7509 0.1494 -4 7 7 0.5497 0.0870 -4 7 8 1.4915 -0.1181 -4 7 9 0.7780 0.1766 -4 7 10 -0.6365 -0.0011 -4 7 11 0.0340 0.0083 -4 7 12 0.6074 -0.1590 -4 7 13 1.0403 0.0420 -4 7 14 -1.5694 -0.2708 -4 7 15 -1.0146 -0.2500 -4 8 1 2.1000 -0.7266 -4 8 2 -0.2539 0.4711 -4 8 3 -0.5956 0.3047 -4 8 4 0.1039 -0.1969 -4 8 5 -1.0654 0.1767 -4 8 6 0.7278 -0.0135 -4 8 7 1.7952 -0.1483 -4 8 8 0.2412 0.1127 -4 8 9 -0.2144 -0.0319 -4 8 10 -0.4187 -0.0874 -4 8 11 0.4767 -0.0109 -4 8 12 -0.1111 -0.1110 -4 8 13 -0.0820 0.0193 -4 8 14 -1.0364 -0.3824 -4 9 1 0.7156 0.8017 -4 9 2 -0.7287 -0.1424 -4 9 3 -0.0652 -0.3665 -4 9 4 0.0773 0.2475 -4 9 5 0.0015 -0.1208 -4 9 6 1.6862 -0.0357 -4 9 7 -0.3549 0.0856 -4 9 8 -0.9849 -0.1038 -4 9 9 0.1580 0.0630 -4 9 10 0.1970 0.0485 -4 9 11 0.1485 -0.0300 -4 9 12 -0.2214 -0.0366 -4 10 1 -0.0484 -0.7372 -4 10 2 -0.0377 -0.1021 -4 10 3 0.2135 0.4788 -4 10 4 -0.0839 -0.0980 -4 10 5 -0.0931 0.0473 -4 10 6 0.1662 0.2363 -4 10 7 -1.5644 -0.2191 -4 10 8 0.0786 0.1092 -4 10 9 0.5970 0.0442 -4 10 10 0.0038 -0.0733 -4 11 1 0.0364 0.4928 -4 11 2 0.0560 0.3981 -4 11 3 -0.6319 -0.1709 -4 11 4 -0.4060 0.0833 -4 11 5 -0.4810 0.2208 -4 11 6 -0.3761 -0.1292 -4 11 7 -0.7291 -0.1371 -4 12 1 -0.2378 -0.2422 -4 12 2 -0.6702 -0.2247 -4 12 3 -0.4921 0.2429 -3 -15 1 -0.4785 0.6075 -3 -15 2 -0.4016 0.3719 -3 -15 3 -0.6828 -0.0259 -3 -15 4 -0.9179 -0.0198 -3 -15 5 -0.3901 0.0138 -3 -14 1 -0.6184 -0.1637 -3 -14 2 -0.1393 -0.4682 -3 -14 3 -0.8816 0.1407 -3 -14 4 -1.1242 0.1389 -3 -14 5 -0.0229 0.3067 -3 -14 6 0.2398 0.1866 -3 -14 7 -0.3970 0.0474 -3 -14 8 -0.8605 0.0115 -3 -14 9 0.3482 0.0084 -3 -13 1 0.0838 -0.1279 -3 -13 2 0.0613 0.6380 -3 -13 3 -1.5365 0.1848 -3 -13 4 -0.8459 -0.0083 -3 -13 5 0.0967 0.0669 -3 -13 6 -0.5163 -0.2203 -3 -13 7 -0.3308 -0.0470 -3 -13 8 0.0241 0.0147 -3 -13 9 0.6264 0.0422 -3 -13 10 -0.3286 0.0642 -3 -13 11 -0.1998 0.1849 -3 -12 1 0.3245 0.4028 -3 -12 2 -0.8314 -0.4362 -3 -12 3 -1.1293 -0.2881 -3 -12 4 -0.0323 0.0698 -3 -12 5 -0.5640 0.0166 -3 -12 6 0.1301 0.1026 -3 -12 7 0.9111 0.1395 -3 -12 8 -0.4950 -0.0440 -3 -12 9 -0.7255 -0.1000 -3 -12 10 -0.9826 0.0004 -3 -12 11 0.5003 -0.1105 -3 -12 12 0.9770 -0.1318 -3 -12 13 0.1922 0.2330 -3 -11 1 -0.3619 -0.7157 -3 -11 2 -0.1975 0.3324 -3 -11 3 0.3444 0.3569 -3 -11 4 -0.2563 0.0368 -3 -11 5 -0.5620 0.0510 -3 -11 6 1.2638 -0.1282 -3 -11 7 -1.0634 -0.2231 -3 -11 8 -2.2682 -0.1251 -3 -11 9 -0.5718 0.0483 -3 -11 10 0.6860 0.1355 -3 -11 11 1.8912 -0.0592 -3 -11 12 0.1493 0.1345 -3 -11 13 -0.4311 0.0312 -3 -11 14 0.7575 -0.1517 -3 -11 15 -0.0620 0.1581 -3 -10 1 0.8949 0.8763 -3 -10 2 1.1669 -0.0325 -3 -10 3 0.4848 -0.4887 -3 -10 4 -0.8305 -0.0551 -3 -10 5 -0.9587 -0.0988 -3 -10 6 -1.0067 0.0056 -3 -10 7 -3.3368 0.1488 -3 -10 8 -0.0705 0.1000 -3 -10 9 1.5485 0.0202 -3 -10 10 1.8235 -0.0531 -3 -10 11 0.5109 -0.0602 -3 -10 12 -1.0413 0.0120 -3 -10 13 0.4635 -0.0834 -3 -10 14 0.9006 0.1340 -3 -10 15 0.0306 0.1778 -3 -10 16 0.0453 -0.0256 -3 -9 1 2.1106 -0.8584 -3 -9 2 1.2522 -0.2818 -3 -9 3 -0.4486 0.4021 -3 -9 4 -2.1840 0.1305 -3 -9 5 -3.0897 0.1392 -3 -9 6 -2.1755 0.0989 -3 -9 7 -0.6403 -0.1485 -3 -9 8 2.8593 -0.1402 -3 -9 9 1.3758 -0.0468 -3 -9 10 0.5294 0.0937 -3 -9 11 -1.0481 0.0093 -3 -9 12 -0.1347 0.0108 -3 -9 13 1.0433 0.0873 -3 -9 14 0.5816 0.0376 -3 -9 15 -0.0839 -0.0678 -3 -9 16 -0.4218 -0.0195 -3 -9 17 0.3551 0.0325 -3 -8 1 1.8380 0.7198 -3 -8 2 0.4899 0.5693 -3 -8 3 -1.9945 -0.3704 -3 -8 4 -3.2275 -0.1266 -3 -8 5 -3.3514 -0.0803 -3 -8 6 0.3067 -0.1105 -3 -8 7 1.8238 0.1028 -3 -8 8 2.1992 0.1108 -3 -8 9 -0.0717 0.0733 -3 -8 10 -0.5622 -0.0157 -3 -8 11 -0.5081 -0.0945 -3 -8 12 0.7651 0.0182 -3 -8 13 0.6954 -0.0454 -3 -8 14 0.3471 -0.0719 -3 -8 15 -0.5418 0.0384 -3 -8 16 -0.2841 0.0762 -3 -8 17 0.3191 -0.0286 -3 -8 18 -0.5008 -0.0516 -3 -7 1 0.3269 -0.4150 -3 -7 2 -0.0298 -0.8063 -3 -7 3 -3.1233 0.1586 -3 -7 4 -3.8577 0.1604 -3 -7 5 -1.3904 0.0739 -3 -7 6 3.0055 0.2537 -3 -7 7 1.4246 -0.0506 -3 -7 8 0.5766 -0.1593 -3 -7 9 -0.5714 -0.0852 -3 -7 10 -0.1574 0.0057 -3 -7 11 0.5055 0.0272 -3 -7 12 0.2330 -0.0123 -3 -7 13 0.0297 0.0122 -3 -7 14 -0.1826 0.0248 -3 -7 15 -0.5860 0.0267 -3 -7 16 0.0465 -0.0441 -3 -7 17 -0.2327 -0.0821 -3 -7 18 -0.4808 -0.0158 -3 -7 19 -0.1218 -0.1060 -3 -6 1 -0.4119 -0.0386 -3 -6 2 -1.6961 0.9112 -3 -6 3 -6.7349 -0.0501 -3 -6 4 -1.4872 -0.2051 -3 -6 5 3.8537 -0.0139 -3 -6 6 3.3116 -0.1980 -3 -6 7 -0.8885 -0.0500 -3 -6 8 -0.2341 0.1125 -3 -6 9 0.2240 0.1007 -3 -6 10 0.5595 0.0507 -3 -6 11 -0.0801 -0.0667 -3 -6 12 -1.2554 0.0133 -3 -6 13 -0.3504 0.0081 -3 -6 14 0.2212 -0.0542 -3 -6 15 0.2286 0.0000 -3 -6 16 -0.0741 -0.0707 -3 -6 17 -0.2347 -0.0098 -3 -6 18 0.2375 -0.0397 -3 -6 19 0.3851 0.0082 -3 -6 20 0.7378 0.1433 -3 -5 1 -4.1107 0.4280 -3 -5 2 -8.5053 -0.8649 -3 -5 3 -3.3406 -0.2638 -3 -5 4 7.6756 0.1738 -3 -5 5 4.4568 -0.0546 -3 -5 6 -1.1666 0.2741 -3 -5 7 -1.9860 0.1200 -3 -5 8 0.8814 -0.1017 -3 -5 9 0.9382 -0.0752 -3 -5 10 -0.2782 -0.0414 -3 -5 11 -1.7322 0.0339 -3 -5 12 -1.5029 0.0110 -3 -5 13 1.1098 -0.0048 -3 -5 14 1.3577 0.0359 -3 -5 15 0.2212 0.0124 -3 -5 16 -0.2865 -0.0305 -3 -5 17 0.7257 0.0581 -3 -5 18 0.4975 0.0251 -3 -5 19 0.3434 0.0650 -3 -5 20 0.2147 -0.1006 -3 -4 1 -13.9889 -0.8818 -3 -4 2 -3.3138 0.6896 -3 -4 3 9.9380 0.4241 -3 -4 4 6.6167 -0.2116 -3 -4 5 -2.6799 0.0839 -3 -4 6 -2.2319 -0.1188 -3 -4 7 0.3452 -0.2085 -3 -4 8 1.4197 0.0462 -3 -4 9 -0.1896 0.0760 -3 -4 10 -1.6823 0.0847 -3 -4 11 -1.4783 -0.0136 -3 -4 12 0.8072 -0.0219 -3 -4 13 2.2859 0.0675 -3 -4 14 0.4811 -0.0169 -3 -4 15 -0.4848 0.0050 -3 -4 16 0.1175 0.0153 -3 -4 17 0.8548 0.0481 -3 -4 18 -0.5640 -0.0475 -3 -4 19 0.1926 -0.0941 -3 -4 20 -0.4238 -0.0386 -3 -3 1 -4.9041 1.0267 -3 -3 2 13.5390 -0.3281 -3 -3 3 7.4831 -0.5987 -3 -3 4 -4.3021 0.0500 -3 -3 5 -2.6011 -0.0831 -3 -3 6 1.3695 0.0955 -3 -3 7 0.9620 0.2381 -3 -3 8 -0.1884 -0.0356 -3 -3 9 -1.6918 -0.0448 -3 -3 10 -0.9211 -0.0661 -3 -3 11 1.0543 -0.0142 -3 -3 12 1.5437 0.0128 -3 -3 13 0.3468 0.0003 -3 -3 14 -0.8207 -0.0144 -3 -3 15 -0.0978 0.0303 -3 -3 16 0.2858 -0.0102 -3 -3 17 0.1865 -0.0035 -3 -3 18 -0.6791 -0.0457 -3 -3 19 0.6495 0.0445 -3 -3 20 -0.5507 0.1508 -3 -3 21 0.6203 0.1085 -3 -2 1 17.6580 -1.2299 -3 -2 2 9.5083 0.0300 -3 -2 3 -6.2580 0.6015 -3 -2 4 -4.1291 -0.0988 -3 -2 5 2.7639 0.1127 -3 -2 6 1.6669 0.0582 -3 -2 7 -1.1788 -0.2587 -3 -2 8 -2.2293 -0.0696 -3 -2 9 -1.2703 0.0140 -3 -2 10 1.8861 0.0469 -3 -2 11 1.2686 0.0202 -3 -2 12 -0.5360 -0.0627 -3 -2 13 -0.5214 0.0430 -3 -2 14 0.0221 -0.0280 -3 -2 15 0.5733 -0.0067 -3 -2 16 0.2307 -0.0147 -3 -2 17 0.1671 0.0383 -3 -2 18 -0.2866 0.0486 -3 -2 19 0.5963 0.0416 -3 -2 20 -0.3941 0.0063 -3 -2 21 0.6421 -0.0914 -3 -1 1 13.7680 1.0310 -3 -1 2 -7.4561 0.4238 -3 -1 3 -5.7851 -0.6506 -3 -1 4 2.6841 -0.1032 -3 -1 5 2.8867 -0.0678 -3 -1 6 -1.5426 -0.1072 -3 -1 7 -3.9734 0.2015 -3 -1 8 -1.7103 0.0251 -3 -1 9 2.0303 -0.0089 -3 -1 10 2.6785 0.0067 -3 -1 11 -0.7900 -0.0810 -3 -1 12 -0.2990 0.0222 -3 -1 13 0.6041 0.0052 -3 -1 14 0.7563 -0.0351 -3 -1 15 0.6625 0.0063 -3 -1 16 0.2369 0.0305 -3 -1 17 -0.2604 0.0698 -3 -1 18 -0.0109 -0.0203 -3 -1 19 0.4277 -0.0477 -3 -1 20 -0.3915 -0.0692 -3 -1 21 0.4459 -0.0214 -3 0 1 -5.9581 -0.7944 -3 0 2 -6.4315 -0.6602 -3 0 3 2.6258 0.4103 -3 0 4 2.6290 0.0090 -3 0 5 -1.3984 0.0455 -3 0 6 -4.5743 0.2722 -3 0 7 -2.6342 -0.1975 -3 0 8 2.8475 -0.1039 -3 0 9 3.1942 0.0470 -3 0 10 0.3890 -0.0151 -3 0 11 -0.8634 0.0379 -3 0 12 1.0311 0.0047 -3 0 13 0.7841 0.0270 -3 0 14 0.9627 0.0000 -3 0 15 0.2680 -0.0253 -3 0 16 -0.2397 0.0394 -3 0 17 -0.3901 -0.0328 -3 0 18 0.8861 -0.0201 -3 0 19 -0.1961 -0.0441 -3 0 20 0.2098 -0.0102 -3 0 21 0.6582 0.0178 -3 1 1 -5.8077 0.4060 -3 1 2 3.8784 0.9296 -3 1 3 1.0929 -0.4126 -3 1 4 -1.6297 -0.2022 -3 1 5 -3.6613 0.1171 -3 1 6 -2.3754 -0.2275 -3 1 7 2.3071 0.0624 -3 1 8 3.6818 0.1240 -3 1 9 0.1869 -0.0293 -3 1 10 -0.5952 0.0610 -3 1 11 0.1221 -0.0328 -3 1 12 1.1858 0.0185 -3 1 13 0.8015 0.0263 -3 1 14 0.6280 -0.0813 -3 1 15 -0.3684 -0.0157 -3 1 16 -0.2284 0.0070 -3 1 17 0.3073 0.0253 -3 1 18 0.9956 0.0339 -3 1 19 -0.5406 -0.0245 -3 1 20 0.8589 0.0148 -3 2 1 3.3674 0.0809 -3 2 2 0.6413 -0.9681 -3 2 3 -3.6871 0.0665 -3 2 4 -1.3667 0.1913 -3 2 5 -1.3066 -0.0961 -3 2 6 1.2836 0.2659 -3 2 7 2.3875 -0.0107 -3 2 8 0.5247 -0.1731 -3 2 9 -1.0741 0.0712 -3 2 10 -0.1573 -0.0487 -3 2 11 0.3658 -0.0049 -3 2 12 1.2197 0.0217 -3 2 13 0.7082 -0.0236 -3 2 14 0.1061 0.0031 -3 2 15 -0.7791 0.0002 -3 2 16 -0.2103 0.0500 -3 2 17 0.6902 -0.0243 -3 2 18 0.6332 -0.0021 -3 2 19 -0.5180 0.0077 -3 2 20 0.3887 -0.0945 -3 3 1 -0.9775 -0.4612 -3 3 2 -4.8547 0.9389 -3 3 3 -0.7617 0.0936 -3 3 4 1.2227 -0.3638 -3 3 5 0.5335 0.1999 -3 3 6 0.3897 -0.1706 -3 3 7 0.2807 -0.1162 -3 3 8 -0.7820 0.1166 -3 3 9 -0.8737 -0.0439 -3 3 10 0.1457 -0.0065 -3 3 11 0.8588 0.0478 -3 3 12 1.3952 -0.0297 -3 3 13 0.2427 0.0584 -3 3 14 -1.2050 -0.0408 -3 3 15 -1.3066 -0.0407 -3 3 16 0.4689 -0.0297 -3 3 17 1.1460 -0.0551 -3 3 18 0.0798 0.1464 -3 3 19 -0.3769 -0.0380 -3 3 20 0.4586 -0.0445 -3 4 1 -5.4069 0.8329 -3 4 2 -0.9806 -0.6528 -3 4 3 2.8709 -0.3845 -3 4 4 1.0087 0.2270 -3 4 5 -0.5838 -0.1048 -3 4 6 -1.1093 0.1127 -3 4 7 -0.2782 0.1241 -3 4 8 -1.2006 -0.1858 -3 4 9 0.3520 0.0387 -3 4 10 1.0561 0.0306 -3 4 11 1.0926 -0.0444 -3 4 12 0.5094 0.0042 -3 4 13 -1.4001 -0.0154 -3 4 14 -1.6442 -0.0159 -3 4 15 0.3101 -0.0123 -3 4 16 1.1180 0.0365 -3 4 17 0.5418 0.0176 -3 4 18 -0.3345 0.0604 -3 4 19 0.0932 -0.0995 -3 5 1 -1.5794 -0.9094 -3 5 2 3.4026 0.4135 -3 5 3 1.5036 0.5110 -3 5 4 -0.8774 -0.3591 -3 5 5 -1.0651 0.1636 -3 5 6 -1.4633 -0.0146 -3 5 7 -0.3788 -0.2426 -3 5 8 0.3496 0.1162 -3 5 9 1.9426 0.0136 -3 5 10 0.6003 -0.0179 -3 5 11 -0.1483 0.0157 -3 5 12 -0.6536 0.0069 -3 5 13 -0.9736 0.0646 -3 5 14 0.1602 0.0541 -3 5 15 0.5331 -0.0507 -3 5 16 0.0245 -0.0483 -3 5 17 0.2342 -0.1860 -3 5 18 -0.2498 0.0874 -3 6 1 2.6852 0.9930 -3 6 2 2.1900 0.0260 -3 6 3 -1.7729 -0.6319 -3 6 4 -0.3688 0.0934 -3 6 5 -1.3742 0.0124 -3 6 6 -1.3392 -0.1003 -3 6 7 1.5804 0.2307 -3 6 8 1.8499 -0.0362 -3 6 9 0.9606 -0.0139 -3 6 10 -1.0210 0.1157 -3 6 11 -0.5911 -0.0960 -3 6 12 0.5068 0.0651 -3 6 13 -0.0522 -0.0147 -3 6 14 -0.4013 -0.0440 -3 6 15 -0.3706 -0.1340 -3 6 16 0.4264 -0.0718 -3 6 17 0.2503 0.0166 -3 7 1 1.2755 -0.7901 -3 7 2 -1.5190 -0.2385 -3 7 3 -1.4112 0.5272 -3 7 4 0.1427 -0.1142 -3 7 5 -1.9135 0.0155 -3 7 6 1.4803 0.1901 -3 7 7 2.5148 -0.1619 -3 7 8 0.2724 0.0519 -3 7 9 -1.0892 0.0234 -3 7 10 -0.9644 -0.0731 -3 7 11 0.7914 -0.0980 -3 7 12 0.7310 0.0684 -3 7 13 -1.2224 -0.0460 -3 7 14 -0.3800 0.0408 -3 7 15 0.5843 0.0403 -3 7 16 0.4639 0.1231 -3 8 1 -1.8300 0.5873 -3 8 2 -1.4016 0.5550 -3 8 3 0.0670 -0.4728 -3 8 4 -0.6492 -0.0942 -3 8 5 0.4765 0.1276 -3 8 6 2.4972 -0.1970 -3 8 7 -0.3459 0.1068 -3 8 8 -1.4974 0.0221 -3 8 9 -0.5676 -0.1385 -3 8 10 0.9821 0.0757 -3 8 11 0.5595 -0.0870 -3 8 12 -0.5126 0.1669 -3 8 13 -0.9917 -0.0500 -3 8 14 0.7238 0.2278 -3 8 15 0.4391 0.1459 -3 9 1 -1.4232 -0.2909 -3 9 2 -0.0417 -0.6127 -3 9 3 -0.0652 0.2503 -3 9 4 -0.1242 0.0484 -3 9 5 1.6645 -0.1346 -3 9 6 -0.4579 0.1598 -3 9 7 -1.5658 -0.0629 -3 9 8 0.3194 -0.0300 -3 9 9 1.4805 0.0398 -3 9 10 0.3827 -0.0773 -3 9 11 -1.0397 -0.0129 -3 9 12 -0.3374 0.1261 -3 9 13 -0.1405 0.0751 -3 9 14 0.8447 0.4114 -3 10 1 -0.8004 -0.0209 -3 10 2 -0.0453 0.7125 -3 10 3 -0.2426 -0.1558 -3 10 4 0.5217 -0.2783 -3 10 5 0.7426 0.2430 -3 10 6 -1.2993 -0.2141 -3 10 7 0.9939 -0.0363 -3 10 8 1.7072 0.0623 -3 10 9 0.2574 -0.1895 -3 10 10 -1.3050 0.0798 -3 10 11 -0.5556 0.0858 -3 10 12 0.4111 0.2406 -3 11 1 -0.3028 0.3490 -3 11 2 0.0050 -0.5017 -3 11 3 0.4390 -0.2114 -3 11 4 0.9909 0.2327 -3 11 5 0.4956 -0.1543 -3 11 6 0.0892 -0.1822 -3 11 7 1.7421 0.1183 -3 11 8 -0.0198 -0.0551 -3 11 9 -0.6748 0.1277 -3 11 10 -0.6398 0.1094 -3 12 1 0.4198 -0.4345 -3 12 2 0.4847 0.3615 -3 12 3 0.8905 0.0746 -3 12 4 0.8386 -0.1058 -3 12 5 0.4938 -0.0471 -3 12 6 0.2761 -0.0661 -3 12 7 0.4252 0.2072 -3 13 1 0.5117 0.8197 -2 -15 1 -0.0223 0.3600 -2 -15 2 -0.1384 -0.3459 -2 -15 3 0.6376 -0.2575 -2 -15 4 0.9199 -0.3201 -2 -14 1 0.0252 -0.3979 -2 -14 2 0.2741 0.2405 -2 -14 3 0.7779 0.0369 -2 -14 4 1.3049 -0.1811 -2 -14 5 1.1845 0.0203 -2 -14 6 0.0515 -0.0376 -2 -14 7 -0.5506 -0.1238 -2 -14 8 0.4385 -0.1929 -2 -13 1 0.5718 0.5757 -2 -13 2 -0.0711 0.0031 -2 -13 3 0.6959 -0.4214 -2 -13 4 1.4750 -0.1675 -2 -13 5 0.6367 -0.1971 -2 -13 6 0.0716 0.0230 -2 -13 7 0.2166 0.0866 -2 -13 8 0.6837 0.0219 -2 -13 9 -0.3847 -0.0733 -2 -13 10 -0.0006 -0.0207 -2 -13 11 -0.0275 -0.2358 -2 -12 1 0.1173 -0.4602 -2 -12 2 -0.7660 -0.1716 -2 -12 3 0.8928 0.2046 -2 -12 4 0.9397 -0.0795 -2 -12 5 0.6224 0.0416 -2 -12 6 0.8533 0.1465 -2 -12 7 -0.2988 -0.1301 -2 -12 8 -0.3064 -0.1892 -2 -12 9 -0.1894 -0.1000 -2 -12 10 1.3978 0.0304 -2 -12 11 0.9774 -0.1221 -2 -12 12 -0.1942 0.1412 -2 -12 13 -1.0386 0.0113 -2 -11 1 -0.6124 0.4772 -2 -11 2 0.0125 0.4393 -2 -11 3 0.6552 -0.2486 -2 -11 4 0.3912 -0.1904 -2 -11 5 0.9218 -0.0761 -2 -11 6 -0.0504 -0.1018 -2 -11 7 -1.0877 0.0334 -2 -11 8 1.1304 0.1050 -2 -11 9 1.9031 0.1330 -2 -11 10 1.8949 -0.0754 -2 -11 11 -0.9565 -0.1259 -2 -11 12 -1.6421 0.0223 -2 -11 13 0.0543 -0.1393 -2 -11 14 -0.2530 0.0646 -2 -11 15 -0.6640 0.0082 -2 -10 1 1.1238 -0.1520 -2 -10 2 0.2689 -0.5138 -2 -10 3 -0.6218 0.1158 -2 -10 4 -0.0626 0.0125 -2 -10 5 0.4367 0.0441 -2 -10 6 -0.0968 0.2424 -2 -10 7 1.9849 0.0225 -2 -10 8 3.3120 -0.1019 -2 -10 9 1.0591 -0.0869 -2 -10 10 -1.0524 -0.0819 -2 -10 11 -2.5340 0.0260 -2 -10 12 0.0519 -0.0229 -2 -10 13 0.7484 -0.0147 -2 -10 14 -0.9170 0.0213 -2 -10 15 0.1985 -0.1336 -2 -10 16 0.3033 -0.0445 -2 -10 17 0.2247 0.0724 -2 -9 1 0.5488 -0.0641 -2 -9 2 -1.5053 0.7215 -2 -9 3 -1.3130 0.0145 -2 -9 4 0.2978 -0.2230 -2 -9 5 1.6478 0.0478 -2 -9 6 3.0605 -0.1570 -2 -9 7 4.1614 -0.1084 -2 -9 8 0.5571 0.0688 -2 -9 9 -2.0612 0.1415 -2 -9 10 -2.3095 0.0405 -2 -9 11 -0.4898 -0.0892 -2 -9 12 1.3692 -0.0622 -2 -9 13 -0.3226 -0.0705 -2 -9 14 -0.5762 -0.0806 -2 -9 15 0.4577 -0.0580 -2 -9 16 0.0451 0.0512 -2 -9 17 0.0228 0.0756 -2 -9 18 -0.6135 -0.0945 -2 -8 1 -2.0153 0.4810 -2 -8 2 -2.0034 -0.5597 -2 -8 3 -0.0522 -0.2529 -2 -8 4 1.8236 0.0646 -2 -8 5 4.2391 -0.0538 -2 -8 6 4.0828 0.1705 -2 -8 7 1.1363 0.1132 -2 -8 8 -2.7577 -0.0393 -2 -8 9 -2.0359 -0.0324 -2 -8 10 -0.7887 -0.1180 -2 -8 11 0.9212 -0.0222 -2 -8 12 0.4156 0.0037 -2 -8 13 -0.5334 -0.0393 -2 -8 14 -0.0289 0.0121 -2 -8 15 -0.1008 0.0019 -2 -8 16 -0.0797 0.0659 -2 -8 17 -0.3838 -0.0530 -2 -8 18 -0.0806 -0.1708 -2 -8 19 0.4366 -0.1179 -2 -7 1 -2.3304 -0.6676 -2 -7 2 -1.3947 0.4860 -2 -7 3 1.2577 0.3580 -2 -7 4 3.9073 -0.2088 -2 -7 5 5.6056 0.1025 -2 -7 6 0.9740 -0.0785 -2 -7 7 -2.1563 -0.2308 -2 -7 8 -2.6272 0.0206 -2 -7 9 -0.5073 0.1093 -2 -7 10 0.1771 0.0559 -2 -7 11 0.5656 0.0228 -2 -7 12 0.0112 -0.0182 -2 -7 13 -0.0892 -0.0199 -2 -7 14 -0.2641 -0.0306 -2 -7 15 -0.2086 0.0095 -2 -7 16 0.2135 -0.0068 -2 -7 17 -0.0454 -0.0661 -2 -7 18 0.3668 -0.0796 -2 -7 19 0.0301 -0.0125 -2 -6 1 -1.8269 0.9271 -2 -6 2 -1.9961 -0.1191 -2 -6 3 5.4039 -0.5182 -2 -6 4 7.5747 0.0310 -2 -6 5 2.6833 -0.0445 -2 -6 6 -4.2784 0.0262 -2 -6 7 -2.9713 0.1901 -2 -6 8 -0.6198 0.0464 -2 -6 9 0.9621 -0.0034 -2 -6 10 0.3255 -0.0863 -2 -6 11 -0.0341 -0.0083 -2 -6 12 0.2394 -0.0028 -2 -6 13 0.2376 -0.0315 -2 -6 14 0.0215 0.0289 -2 -6 15 0.1407 0.0140 -2 -6 16 0.3648 0.0019 -2 -6 17 -0.0605 0.0522 -2 -6 18 -0.1201 0.0337 -2 -6 19 -0.0833 0.1439 -2 -6 20 0.1549 0.0700 -2 -5 1 -2.9552 -0.8723 -2 -5 2 4.9339 -0.0910 -2 -5 3 14.6520 0.5861 -2 -5 4 3.4393 -0.0703 -2 -5 5 -6.2881 0.1118 -2 -5 6 -6.2688 0.0848 -2 -5 7 0.2132 -0.2592 -2 -5 8 2.1693 -0.0766 -2 -5 9 0.9690 0.0525 -2 -5 10 -0.6122 0.0433 -2 -5 11 -0.0814 0.0400 -2 -5 12 1.3690 -0.0299 -2 -5 13 0.7827 0.0304 -2 -5 14 -0.2064 0.0100 -2 -5 15 -0.2818 -0.0165 -2 -5 16 0.0012 0.0488 -2 -5 17 -0.7797 0.0670 -2 -5 18 -0.4709 0.0520 -2 -5 19 -0.1246 -0.0551 -2 -5 20 -0.5531 -0.1769 -2 -5 21 -0.8617 -0.1172 -2 -4 1 10.0563 0.8013 -2 -4 2 20.8739 0.5773 -2 -4 3 8.1556 -0.5149 -2 -4 4 -11.7456 -0.1440 -2 -4 5 -8.4281 0.0219 -2 -4 6 -0.4283 -0.1881 -2 -4 7 3.8585 0.1435 -2 -4 8 1.5760 0.1225 -2 -4 9 -0.8367 0.0397 -2 -4 10 -0.3242 -0.0411 -2 -4 11 1.5184 -0.0629 -2 -4 12 1.7709 0.0255 -2 -4 13 -0.6472 -0.0182 -2 -4 14 -1.0570 -0.0051 -2 -4 15 -0.3450 -0.0172 -2 -4 16 -0.2966 0.0095 -2 -4 17 -1.1357 0.0272 -2 -4 18 0.0287 -0.0553 -2 -4 19 -0.4816 -0.1126 -2 -4 20 -0.5925 0.0442 -2 -4 21 0.1077 0.0506 -2 -3 1 33.0989 -0.5037 -2 -3 2 10.0029 -0.6568 -2 -3 3 -16.2206 0.3320 -2 -3 4 -13.0182 0.1185 -2 -3 5 1.8233 0.0175 -2 -3 6 4.2947 0.2366 -2 -3 7 1.9821 -0.1369 -2 -3 8 -1.2146 -0.1240 -2 -3 9 -0.4016 0.0375 -2 -3 10 1.6581 -0.0301 -2 -3 11 1.5657 0.0383 -2 -3 12 -0.4388 0.0013 -2 -3 13 -1.4037 -0.0152 -2 -3 14 0.0213 0.0184 -2 -3 15 -0.0074 -0.0728 -2 -3 16 -0.3779 0.0099 -2 -3 17 -0.7783 -0.0206 -2 -3 18 0.3608 -0.0307 -2 -3 19 -1.0211 0.0342 -2 -3 20 0.3147 0.0266 -2 -3 21 0.2042 -0.1337 -2 -2 1 13.7217 0.2229 -2 -2 2 -23.6152 1.0075 -2 -2 3 -17.1151 -0.2248 -2 -2 4 4.1815 -0.2282 -2 -2 5 7.1462 0.1289 -2 -2 6 0.9793 -0.2438 -2 -2 7 -2.0034 -0.0455 -2 -2 8 -0.9240 0.1852 -2 -2 9 2.4415 0.0276 -2 -2 10 1.9764 0.0087 -2 -2 11 -0.3706 -0.0332 -2 -2 12 -0.9376 0.0205 -2 -2 13 0.2180 -0.0037 -2 -2 14 0.4863 -0.0088 -2 -2 15 -0.3966 -0.0408 -2 -2 16 -0.2978 0.0097 -2 -2 17 -0.7074 0.0139 -2 -2 18 0.1271 0.0193 -2 -2 19 -0.9780 -0.0075 -2 -2 20 0.6138 -0.1044 -2 -2 21 -0.7649 -0.0093 -2 -1 1 -29.4893 0.5019 -2 -1 2 -21.4194 -0.9074 -2 -1 3 6.2015 -0.0906 -2 -1 4 10.2128 0.2578 -2 -1 5 0.6036 -0.0803 -2 -1 6 -3.5163 0.2001 -2 -1 7 -1.0519 0.0365 -2 -1 8 3.4593 -0.1268 -2 -1 9 3.8474 0.0395 -2 -1 10 -0.4048 -0.0291 -2 -1 11 -1.0800 0.0192 -2 -1 12 0.0052 0.0369 -2 -1 13 0.2273 -0.0132 -2 -1 14 -0.1912 0.0574 -2 -1 15 -0.5016 -0.0279 -2 -1 16 -0.6539 0.0565 -2 -1 17 -0.6588 -0.0119 -2 -1 18 0.2425 -0.0302 -2 -1 19 -0.9113 -0.0155 -2 -1 20 0.3929 -0.0069 -2 -1 21 -0.5065 0.1485 -2 0 1 -24.7755 -0.6519 -2 0 2 7.3867 0.8138 -2 0 3 10.7975 0.2139 -2 0 4 0.3633 -0.3033 -2 0 5 -4.1517 0.2435 -2 0 6 -0.6905 -0.1552 -2 0 7 5.1431 -0.2034 -2 0 8 4.9460 0.1698 -2 0 9 -0.1246 0.0353 -2 0 10 -2.6197 -0.0212 -2 0 11 -0.0939 0.0210 -2 0 12 -0.1457 0.0027 -2 0 13 -0.2287 0.0522 -2 0 14 -0.4384 0.0076 -2 0 15 -1.0432 0.0033 -2 0 16 -0.7743 -0.0075 -2 0 17 0.4387 -0.0248 -2 0 18 -0.1030 0.0545 -2 0 19 -0.6539 0.0277 -2 0 20 0.4962 0.0373 -2 0 21 -0.6617 -0.0016 -2 1 1 5.9637 1.1655 -2 1 2 9.1273 -0.5530 -2 1 3 -1.0409 -0.5880 -2 1 4 -3.3284 0.3995 -2 1 5 0.0622 -0.0378 -2 1 6 5.7660 -0.0102 -2 1 7 5.6750 0.1781 -2 1 8 -0.9390 -0.1108 -2 1 9 -3.2771 -0.0158 -2 1 10 -0.8836 -0.0088 -2 1 11 0.8036 -0.0291 -2 1 12 -0.5852 0.0446 -2 1 13 -0.4559 -0.0207 -2 1 14 -1.1494 0.0284 -2 1 15 -0.9690 -0.0005 -2 1 16 0.4360 0.0244 -2 1 17 0.8743 0.0879 -2 1 18 -1.0328 -0.0265 -2 1 19 -0.0817 -0.0107 -2 1 20 -0.5691 -0.0697 -2 1 21 -0.5536 0.0723 -2 2 1 5.9295 -0.9459 -2 2 2 -3.3430 0.0408 -2 2 3 -0.7708 0.6591 -2 2 4 0.7143 -0.1722 -2 2 5 4.6256 0.0864 -2 2 6 4.8365 0.0420 -2 2 7 -0.4944 -0.2828 -2 2 8 -3.7105 0.0782 -2 2 9 -0.8834 0.0602 -2 2 10 1.0201 -0.0644 -2 2 11 0.4583 0.0020 -2 2 12 -0.7814 0.0147 -2 2 13 -0.9607 0.0209 -2 2 14 -1.1191 0.0430 -2 2 15 0.0633 0.0046 -2 2 16 1.1350 0.0483 -2 2 17 0.1131 -0.0457 -2 2 18 -1.4116 -0.0269 -2 2 19 0.1424 0.0086 -2 2 20 -0.6058 -0.0125 -2 2 21 0.8676 0.2718 -2 3 1 -3.6727 1.0259 -2 3 2 0.9143 0.2284 -2 3 3 3.5094 -0.7520 -2 3 4 1.2538 0.1645 -2 3 5 2.9472 0.1116 -2 3 6 -0.0672 -0.1675 -2 3 7 -2.1723 0.1842 -2 3 8 -1.2720 0.0086 -2 3 9 1.3083 -0.0696 -2 3 10 1.2025 0.0281 -2 3 11 0.1462 -0.0479 -2 3 12 -1.3000 0.0824 -2 3 13 -1.2788 -0.0322 -2 3 14 -0.2567 0.0284 -2 3 15 1.0858 0.0032 -2 3 16 1.1620 -0.0051 -2 3 17 -0.6890 0.0754 -2 3 18 -0.8931 -0.0000 -2 3 19 0.5803 -0.0570 -2 3 20 -0.3700 0.0067 -2 3 21 0.2663 0.1356 -2 4 1 2.0556 -0.5127 -2 4 2 5.3190 -0.6432 -2 4 3 0.0639 0.5410 -2 4 4 -0.6084 0.1380 -2 4 5 0.3461 -0.0965 -2 4 6 -0.6107 0.1849 -2 4 7 -0.5132 -0.1910 -2 4 8 1.0641 -0.0164 -2 4 9 1.7972 0.1108 -2 4 10 0.4482 -0.0601 -2 4 11 -0.9694 0.0158 -2 4 12 -1.8756 0.0399 -2 4 13 0.0080 -0.0247 -2 4 14 1.1680 0.0737 -2 4 15 1.3668 -0.0268 -2 4 16 0.2357 0.0692 -2 4 17 -1.0627 -0.0094 -2 4 18 -0.2762 -0.1709 -2 4 19 -0.1611 -0.0299 -2 4 20 -0.7227 -0.0327 -2 5 1 4.9121 0.4384 -2 5 2 0.5046 0.7078 -2 5 3 -2.7035 -0.4966 -2 5 4 -0.0788 -0.1385 -2 5 5 0.1482 0.2012 -2 5 6 0.4836 -0.1604 -2 5 7 1.0923 0.0785 -2 5 8 1.8794 0.1068 -2 5 9 0.0571 -0.0531 -2 5 10 -0.9740 0.0265 -2 5 11 -1.3504 -0.0048 -2 5 12 -0.1844 0.0132 -2 5 13 1.5722 -0.0115 -2 5 14 0.5760 -0.0534 -2 5 15 0.2737 -0.0047 -2 5 16 -0.6268 -0.0409 -2 5 17 -0.8836 -0.0060 -2 5 18 -0.1947 -0.0285 -2 5 19 -0.2698 0.0455 -2 6 1 0.5493 0.1359 -2 6 2 -3.1177 -0.8748 -2 6 3 -0.7520 0.0796 -2 6 4 0.6096 0.4167 -2 6 5 0.1699 -0.1651 -2 6 6 2.0030 0.1761 -2 6 7 1.2453 -0.0772 -2 6 8 0.0207 -0.0924 -2 6 9 -1.6148 0.1231 -2 6 10 -0.7934 -0.1068 -2 6 11 0.1306 -0.0078 -2 6 12 0.9379 -0.0522 -2 6 13 0.3373 -0.0536 -2 6 14 -0.6942 -0.0062 -2 6 15 0.0274 0.0449 -2 6 16 -0.7022 0.0465 -2 6 17 -0.0405 0.1601 -2 6 18 0.4779 -0.0882 -2 6 19 0.0795 -0.0075 -2 7 1 -2.8202 -0.1701 -2 7 2 -1.7124 0.6809 -2 7 3 1.4024 0.0237 -2 7 4 -0.2252 -0.2903 -2 7 5 1.7436 0.1065 -2 7 6 1.7523 -0.0757 -2 7 7 -1.0055 -0.0946 -2 7 8 -1.2434 0.1334 -2 7 9 -1.3787 -0.1055 -2 7 10 0.6206 -0.0144 -2 7 11 0.7950 0.0302 -2 7 12 -0.2035 -0.0596 -2 7 13 -0.7220 0.0762 -2 7 14 -0.3966 -0.0554 -2 7 15 0.3044 0.1279 -2 7 16 -0.0830 0.0210 -2 7 17 0.9329 0.0757 -2 7 18 0.0804 -0.1063 -2 8 1 -1.1602 0.6725 -2 8 2 0.8897 -0.6372 -2 8 3 0.8514 -0.3336 -2 8 4 0.1545 0.3574 -2 8 5 2.0289 -0.0643 -2 8 6 -1.1486 0.0572 -2 8 7 -1.6587 0.0411 -2 8 8 -0.6306 -0.1364 -2 8 9 0.1768 0.1314 -2 8 10 1.0764 -0.0159 -2 8 11 -0.3896 -0.0263 -2 8 12 -0.8695 -0.0045 -2 8 13 -0.2660 -0.0444 -2 8 14 0.3795 0.0231 -2 8 15 0.5036 0.0756 -2 8 16 0.2444 -0.0442 -2 8 17 0.4639 0.1580 -2 9 1 1.0256 -0.5175 -2 9 2 0.6549 0.2733 -2 9 3 0.0980 0.4157 -2 9 4 0.9341 -0.1662 -2 9 5 -0.1583 0.0470 -2 9 6 -1.9891 0.0027 -2 9 7 -0.1077 -0.1081 -2 9 8 0.6829 0.1075 -2 9 9 0.1363 -0.0186 -2 9 10 -0.6839 -0.0989 -2 9 11 -0.4557 0.1011 -2 9 12 0.0244 -0.0722 -2 9 13 0.5068 0.1199 -2 9 14 0.3287 -0.1032 -2 9 15 -0.1314 -0.1104 -2 10 1 0.9984 0.8015 -2 10 2 0.3449 -0.0818 -2 10 3 0.7476 -0.4395 -2 10 4 0.3600 0.2023 -2 10 5 -1.8743 -0.0378 -2 10 6 -0.3907 -0.0421 -2 10 7 0.8702 0.1421 -2 10 8 -0.2866 -0.1762 -2 10 9 -1.6748 0.0993 -2 10 10 -0.0288 0.0518 -2 10 11 1.1109 0.0550 -2 10 12 0.1005 -0.0073 -2 10 13 -0.0781 -0.1983 -2 10 14 -0.4425 -0.3808 -2 11 1 1.2268 -0.4796 -2 11 2 0.7441 -0.2413 -2 11 3 0.1363 0.4236 -2 11 4 -1.3524 -0.0299 -2 11 5 -1.4899 -0.1520 -2 11 6 0.7939 0.2007 -2 11 7 -0.6602 -0.1214 -2 11 8 -1.3369 0.0084 -2 11 9 -0.4506 0.1024 -2 11 10 1.5937 -0.1379 -2 11 11 0.3384 0.0772 -2 11 12 -0.9110 -0.3934 -2 12 1 0.3664 0.4184 -2 12 2 -0.4429 0.2179 -2 12 3 -1.1266 -0.2299 -2 12 4 -1.0738 -0.0820 -2 12 5 -0.4252 -0.0088 -2 12 6 -0.1756 0.0657 -2 12 7 -1.1541 -0.0997 -2 12 8 0.1498 -0.1263 -2 12 9 0.4308 -0.0068 -2 13 1 -1.0875 -0.3287 -2 13 2 -0.7015 -0.4723 -2 13 3 -0.2799 0.3327 -2 13 4 -0.3924 -0.2024 -2 13 5 -0.6102 -0.0873 -1 -15 1 0.0515 -0.6701 -1 -14 1 0.4291 0.1734 -1 -14 2 0.5795 0.2055 -1 -14 3 -0.5814 -0.1621 -1 -14 4 -0.5985 0.2037 -1 -14 5 -0.8749 0.0407 -1 -14 6 -0.8053 -0.1896 -1 -14 7 0.1357 -0.1811 -1 -14 8 -0.2007 0.1036 -1 -13 1 0.3175 -0.0744 -1 -13 2 -0.0851 -0.3811 -1 -13 3 -0.6675 0.1633 -1 -13 4 -0.7401 0.1980 -1 -13 5 -0.9441 0.0389 -1 -13 6 -0.3921 0.0219 -1 -13 7 0.0594 -0.0234 -1 -13 8 -0.4540 0.1042 -1 -13 9 0.0291 0.0412 -1 -13 10 -0.3226 -0.1282 -1 -13 11 0.2669 -0.0002 -1 -12 1 -0.6530 -0.0143 -1 -12 2 -0.2237 0.3891 -1 -12 3 -0.7554 0.0038 -1 -12 4 -0.3738 -0.0562 -1 -12 5 -0.0974 0.0861 -1 -12 6 -0.4349 -0.1537 -1 -12 7 -0.4766 -0.0721 -1 -12 8 -0.4959 0.0864 -1 -12 9 0.4438 0.1626 -1 -12 10 -0.5306 0.0555 -1 -12 11 -1.0695 0.1355 -1 -12 12 -1.2683 0.0254 -1 -12 13 1.1734 -0.2055 -1 -11 1 -0.5120 0.3558 -1 -11 2 0.0949 -0.4409 -1 -11 3 -0.5842 -0.2208 -1 -11 4 0.4576 0.1947 -1 -11 5 0.1380 0.0093 -1 -11 6 -0.8674 0.0501 -1 -11 7 -0.1014 0.0499 -1 -11 8 -0.0633 0.0915 -1 -11 9 -0.3595 0.0473 -1 -11 10 -2.5487 -0.1102 -1 -11 11 -1.4209 0.0779 -1 -11 12 1.1998 -0.0150 -1 -11 13 1.6804 0.0946 -1 -11 14 -0.5177 0.0591 -1 -11 15 0.7523 -0.2626 -1 -10 1 -0.3877 -0.4208 -1 -10 2 -0.8994 0.1932 -1 -10 3 -0.2204 0.2277 -1 -10 4 0.9565 -0.0416 -1 -10 5 0.3022 0.0874 -1 -10 6 -0.2938 -0.0918 -1 -10 7 0.0426 -0.1762 -1 -10 8 -2.0581 0.0870 -1 -10 9 -2.6743 0.0143 -1 -10 10 -2.0902 0.0549 -1 -10 11 1.8239 0.1239 -1 -10 12 2.2072 -0.0002 -1 -10 13 -0.3799 0.0209 -1 -10 14 -0.1783 -0.1071 -1 -10 15 0.5168 -0.0051 -1 -10 16 -0.8749 0.0234 -1 -10 17 -0.6463 -0.2193 -1 -9 1 -2.7421 0.6460 -1 -9 2 -0.5566 -0.1097 -1 -9 3 1.1996 -0.4688 -1 -9 4 1.2233 0.1380 -1 -9 5 0.5343 0.0219 -1 -9 6 -0.8488 -0.0695 -1 -9 7 -2.8718 0.1122 -1 -9 8 -4.2252 0.0789 -1 -9 9 -1.2630 -0.0321 -1 -9 10 1.4541 -0.0368 -1 -9 11 2.7792 -0.0084 -1 -9 12 -0.1631 -0.0148 -1 -9 13 -0.8665 0.0864 -1 -9 14 0.4919 0.0703 -1 -9 15 -0.8543 0.0055 -1 -9 16 -0.9686 -0.0993 -1 -9 17 -0.3257 -0.1306 -1 -9 18 0.2264 -0.0256 -1 -8 1 -1.1817 -0.4701 -1 -8 2 2.1193 -0.2846 -1 -8 3 1.3473 0.3645 -1 -8 4 0.6284 0.1124 -1 -8 5 -0.9046 0.0687 -1 -8 6 -3.9673 0.0199 -1 -8 7 -4.7659 -0.1770 -1 -8 8 -1.7578 -0.0448 -1 -8 9 1.7707 -0.0138 -1 -8 10 2.2883 0.0237 -1 -8 11 0.8968 0.0886 -1 -8 12 -0.7488 0.0573 -1 -8 13 0.1032 0.1001 -1 -8 14 -0.4155 -0.0729 -1 -8 15 -1.2216 0.0018 -1 -8 16 -0.1250 -0.0147 -1 -8 17 0.2920 -0.0992 -1 -8 18 0.6492 0.0621 -1 -8 19 -0.1978 0.2365 -1 -7 1 2.4648 0.4770 -1 -7 2 2.6187 0.3955 -1 -7 3 0.3273 -0.4250 -1 -7 4 -0.6952 -0.0118 -1 -7 5 -4.7370 0.0934 -1 -7 6 -5.5689 -0.1656 -1 -7 7 -1.9953 0.0902 -1 -7 8 1.7446 0.1136 -1 -7 9 2.3534 -0.0182 -1 -7 10 1.4638 0.0006 -1 -7 11 0.1503 -0.0165 -1 -7 12 -0.3345 -0.0277 -1 -7 13 -0.5892 -0.0213 -1 -7 14 -1.0614 0.0205 -1 -7 15 -0.0099 0.1215 -1 -7 16 0.5360 -0.0618 -1 -7 17 0.3823 -0.0234 -1 -7 18 -0.0787 0.1338 -1 -7 19 -0.3759 0.2525 -1 -7 20 0.0885 0.1637 -1 -6 1 2.6158 -0.0824 -1 -6 2 3.1829 -0.6974 -1 -6 3 -0.5321 0.1539 -1 -6 4 -5.0522 0.2959 -1 -6 5 -8.1629 0.0280 -1 -6 6 -2.3192 0.1184 -1 -6 7 2.5060 -0.0792 -1 -6 8 3.4717 -0.1189 -1 -6 9 1.4066 -0.0501 -1 -6 10 -0.0109 -0.0070 -1 -6 11 -0.7983 -0.0012 -1 -6 12 -0.8366 0.0078 -1 -6 13 -0.7520 0.0653 -1 -6 14 0.0412 0.0500 -1 -6 15 0.8544 -0.0122 -1 -6 16 -0.1144 -0.0106 -1 -6 17 -0.3541 0.0009 -1 -6 18 -0.1045 0.0646 -1 -6 19 0.4919 0.1078 -1 -6 20 -0.0228 -0.0551 -1 -5 1 4.6484 0.0201 -1 -5 2 5.1071 0.6418 -1 -5 3 -8.3222 -0.1463 -1 -5 4 -11.7858 -0.1852 -1 -5 5 -5.4093 0.1045 -1 -5 6 4.6629 -0.2066 -1 -5 7 5.6723 -0.0258 -1 -5 8 1.9001 0.1270 -1 -5 9 -1.7082 -0.0085 -1 -5 10 -1.6560 0.0323 -1 -5 11 -0.6816 -0.0269 -1 -5 12 -0.1631 0.0216 -1 -5 13 -0.1426 -0.0282 -1 -5 14 0.2993 -0.0350 -1 -5 15 0.0540 0.0243 -1 -5 16 -0.8880 -0.0045 -1 -5 17 0.3858 -0.0763 -1 -5 18 0.9691 -0.0004 -1 -5 19 0.4173 -0.0401 -1 -5 20 -0.5247 -0.0418 -1 -5 21 0.3804 0.0787 -1 -4 1 8.8593 0.5457 -1 -4 2 -9.2140 -0.8185 -1 -4 3 -23.7101 -0.3212 -1 -4 4 -7.5902 0.3665 -1 -4 5 6.1912 -0.0098 -1 -4 6 9.8523 0.1316 -1 -4 7 2.7848 0.0946 -1 -4 8 -3.1964 -0.1234 -1 -4 9 -2.9120 -0.0222 -1 -4 10 -0.4693 -0.0149 -1 -4 11 0.2941 -0.0229 -1 -4 12 -0.5772 -0.0133 -1 -4 13 -0.5929 -0.0084 -1 -4 14 0.1339 0.0305 -1 -4 15 -0.1254 -0.0183 -1 -4 16 0.1054 0.0047 -1 -4 17 1.6238 -0.0461 -1 -4 18 0.5699 -0.0544 -1 -4 19 -0.2117 -0.0338 -1 -4 20 -0.0073 0.0770 -1 -4 21 0.9692 0.1380 -1 -3 1 -17.7344 -0.5304 -1 -3 2 -36.8989 0.4965 -1 -3 3 -15.2296 0.3329 -1 -3 4 14.3567 -0.1603 -1 -3 5 13.3489 0.1043 -1 -3 6 3.6896 -0.0978 -1 -3 7 -4.9401 -0.1716 -1 -3 8 -4.1306 0.1178 -1 -3 9 0.1445 -0.0067 -1 -3 10 0.3758 -0.0103 -1 -3 11 -0.8725 0.0002 -1 -3 12 -1.3286 0.0147 -1 -3 13 0.2530 0.0394 -1 -3 14 0.4756 -0.0632 -1 -3 15 0.2222 0.0576 -1 -3 16 0.7665 0.0335 -1 -3 17 1.2077 -0.0774 -1 -3 18 -0.4842 -0.0089 -1 -3 19 0.1989 0.0655 -1 -3 20 0.4158 0.0814 -1 -3 21 0.7256 0.0572 -1 -3 22 -0.5110 -0.0917 -1 -2 1 -56.0039 1.3883 -1 -2 2 -19.8319 -0.3542 -1 -2 3 22.0833 -0.6966 -1 -2 4 21.5054 0.2521 -1 -2 5 0.5003 0.0189 -1 -2 6 -7.3638 -0.0413 -1 -2 7 -5.1835 0.2064 -1 -2 8 1.1271 -0.0797 -1 -2 9 1.6554 -0.0611 -1 -2 10 -1.4469 0.0477 -1 -2 11 -1.9465 -0.0115 -1 -2 12 -0.3965 0.0166 -1 -2 13 0.6111 -0.0305 -1 -2 14 -0.0053 0.0140 -1 -2 15 0.4824 0.0720 -1 -2 16 0.4457 -0.0167 -1 -2 17 0.4407 0.0326 -1 -2 18 -0.6297 0.0509 -1 -2 19 1.0146 -0.0043 -1 -2 20 0.2967 -0.0317 -1 -2 21 0.8708 0.0493 -1 -2 22 -0.4905 -0.1196 -1 -1 1 -24.6509 -0.8524 -1 -1 2 30.9690 -0.3607 -1 -1 3 26.8345 0.5845 -1 -1 4 -1.9786 0.0010 -1 -1 5 -11.7418 0.0177 -1 -1 6 -5.0595 0.0429 -1 -1 7 2.4096 -0.1711 -1 -1 8 2.8892 0.0417 -1 -1 9 -1.9144 0.0867 -1 -1 10 -3.3993 -0.0294 -1 -1 11 -1.4677 -0.0186 -1 -1 12 0.1927 -0.0182 -1 -1 13 0.3202 0.0339 -1 -1 14 0.3948 -0.0241 -1 -1 15 0.3988 0.0267 -1 -1 16 -0.2025 0.0418 -1 -1 17 0.4584 -0.0153 -1 -1 18 -0.1362 -0.0333 -1 -1 19 1.4826 -0.0821 -1 -1 20 0.1703 0.0474 -1 -1 21 0.8598 0.0405 -1 -1 22 -0.8541 -0.1199 -1 0 2 29.0107 0.5169 -1 0 3 -5.1748 -0.6794 -1 0 4 -13.3954 0.0653 -1 0 5 -4.2819 0.1174 -1 0 6 3.6531 -0.1306 -1 0 7 2.6951 0.1972 -1 0 8 -3.4022 0.0328 -1 0 9 -5.0492 -0.1077 -1 0 10 -1.7160 0.0189 -1 0 11 -0.0035 -0.0204 -1 0 12 0.7312 0.0222 -1 0 13 0.7799 -0.0445 -1 0 14 0.1836 -0.0587 -1 0 15 -0.2092 0.0465 -1 0 16 0.3475 -0.0510 -1 0 17 0.7339 -0.0043 -1 0 18 0.0605 -0.0045 -1 0 19 1.3098 -0.0273 -1 0 20 -0.3458 0.0527 -1 0 21 0.5298 -0.0129 -1 0 22 -0.4310 -0.0203 -1 1 1 29.0714 0.0136 -1 1 2 -7.4905 -1.0168 -1 1 3 -12.2202 0.3948 -1 1 4 -2.2428 0.3088 -1 1 5 3.5251 -0.1152 -1 1 6 1.8719 0.1140 -1 1 7 -5.5124 -0.1547 -1 1 8 -6.2297 -0.0397 -1 1 9 -1.3376 0.0892 -1 1 10 1.2944 -0.0016 -1 1 11 0.3450 -0.0027 -1 1 12 0.9266 -0.0259 -1 1 13 0.2649 -0.0405 -1 1 14 -0.3439 -0.0164 -1 1 15 0.6623 -0.0115 -1 1 16 0.8568 0.0270 -1 1 17 -0.1138 -0.0016 -1 1 18 0.1711 -0.0367 -1 1 19 0.5882 -0.0250 -1 1 20 -0.1070 0.0360 -1 1 21 1.1784 0.0623 -1 1 22 0.0058 -0.1951 -1 2 1 -5.3433 -0.2843 -1 2 2 -8.8241 0.7391 -1 2 3 -0.1979 -0.1615 -1 2 4 1.9222 -0.2536 -1 2 5 0.5561 0.1403 -1 2 6 -5.1292 -0.1992 -1 2 7 -7.0188 0.1158 -1 2 8 -0.8372 0.1535 -1 2 9 2.2250 -0.1057 -1 2 10 1.0432 0.0294 -1 2 11 -0.1190 0.0170 -1 2 12 0.3015 0.0040 -1 2 13 -0.4040 -0.0036 -1 2 14 0.4071 -0.0645 -1 2 15 1.3560 0.0610 -1 2 16 0.0101 -0.0405 -1 2 17 -0.6517 -0.0378 -1 2 18 0.6534 0.0409 -1 2 19 0.3822 -0.0183 -1 2 20 0.9256 0.0539 -1 2 21 0.3203 -0.1074 -1 2 22 -0.6140 -0.2993 -1 3 1 -3.4858 0.4896 -1 3 2 1.7316 -0.7741 -1 3 3 -1.5158 -0.1518 -1 3 4 -0.5852 0.4463 -1 3 5 -3.1257 -0.1079 -1 3 6 -4.9968 0.0858 -1 3 7 -1.7611 0.0027 -1 3 8 2.5577 -0.1430 -1 3 9 1.6325 0.0950 -1 3 10 -0.3039 0.0102 -1 3 11 -1.0045 0.0521 -1 3 12 -0.6235 -0.0208 -1 3 13 0.3813 -0.0188 -1 3 14 1.3569 -0.0003 -1 3 15 0.9766 -0.0004 -1 3 16 -0.9506 -0.0513 -1 3 17 -0.3665 0.0559 -1 3 18 1.0017 -0.0280 -1 3 19 -0.0651 -0.0529 -1 3 20 0.4093 -0.0183 -1 3 21 -0.6422 -0.1154 -1 4 1 2.4024 -0.6421 -1 4 2 -3.5962 0.4294 -1 4 3 -2.9648 0.2886 -1 4 4 0.1307 -0.2840 -1 4 5 -2.6836 0.0648 -1 4 6 -1.4106 -0.1347 -1 4 7 1.1088 -0.0463 -1 4 8 2.1686 0.1966 -1 4 9 -0.5290 -0.0905 -1 4 10 -1.7964 0.0053 -1 4 11 -1.4330 0.0671 -1 4 12 0.6499 -0.0682 -1 4 13 1.5156 0.0829 -1 4 14 0.7802 -0.1025 -1 4 15 -0.2704 0.0044 -1 4 16 -1.4004 -0.0215 -1 4 17 0.3211 -0.0218 -1 4 18 0.4344 0.0111 -1 4 19 -0.4545 0.0143 -1 4 20 0.8199 0.0601 -1 4 21 -0.0075 -0.0082 -1 5 1 -3.6514 0.6182 -1 5 2 -4.3510 -0.3252 -1 5 3 1.5339 -0.4856 -1 5 4 -0.1724 0.3259 -1 5 5 -1.5600 0.0161 -1 5 6 0.8108 -0.0280 -1 5 7 1.3739 0.1186 -1 5 8 -0.4977 -0.1585 -1 5 9 -2.0798 0.0193 -1 5 10 -1.3578 0.0500 -1 5 11 0.2181 -0.0507 -1 5 12 1.5704 0.0182 -1 5 13 0.0475 -0.0157 -1 5 14 -0.1983 -0.0343 -1 5 15 -0.7644 0.0421 -1 5 16 -0.5695 -0.0338 -1 5 17 0.8161 0.0682 -1 5 18 0.1833 0.0708 -1 5 19 0.4231 0.0075 -1 5 20 0.7515 0.0764 -1 6 1 -3.5009 -0.6212 -1 6 2 0.7267 -0.0539 -1 6 3 1.7546 0.4918 -1 6 4 -1.6351 -0.1204 -1 6 5 0.7863 -0.0094 -1 6 6 1.0626 -0.0675 -1 6 7 -0.9897 -0.1097 -1 6 8 -1.8725 0.1921 -1 6 9 -0.8891 -0.0616 -1 6 10 -0.1462 -0.0819 -1 6 11 0.8290 0.0481 -1 6 12 0.2160 0.0039 -1 6 13 -0.6975 0.0885 -1 6 14 0.3818 0.0298 -1 6 15 -0.4134 -0.0579 -1 6 16 0.7100 0.0523 -1 6 17 0.6867 -0.0241 -1 6 18 -0.1169 0.0628 -1 6 19 0.0730 -0.0181 -1 6 20 0.1147 0.1352 -1 7 1 0.6253 0.4718 -1 7 2 1.9591 0.0965 -1 7 3 -0.4121 -0.5044 -1 7 4 0.0063 0.0707 -1 7 5 1.2944 0.1570 -1 7 6 -1.5996 -0.0951 -1 7 7 -1.3878 0.2525 -1 7 8 -0.8090 -0.1269 -1 7 9 0.0260 -0.0844 -1 7 10 0.4767 0.1089 -1 7 11 0.5099 -0.0466 -1 7 12 -0.4703 0.1137 -1 7 13 -0.0719 -0.0053 -1 7 14 0.8308 -0.0421 -1 7 15 0.2056 -0.0155 -1 7 16 0.8277 0.0398 -1 7 17 -0.8050 -0.0575 -1 7 18 -0.4745 0.0625 -1 7 19 0.3700 -0.0998 -1 8 1 1.8451 -0.4205 -1 8 2 0.5571 -0.4303 -1 8 3 -0.6162 0.3905 -1 8 4 0.9002 0.1377 -1 8 5 -1.1735 -0.0089 -1 8 6 -1.3912 0.0111 -1 8 7 -0.0676 -0.1273 -1 8 8 -0.2983 0.0571 -1 8 9 1.1059 0.0779 -1 8 10 0.4454 -0.1534 -1 8 11 -0.3726 0.0987 -1 8 12 -0.6295 -0.0176 -1 8 13 0.8040 0.0045 -1 8 14 1.0389 0.1142 -1 8 15 -0.2375 -0.0987 -1 8 16 -0.4503 0.0205 -1 8 17 -1.0986 -0.2188 -1 8 18 0.6689 -0.0786 -1 9 1 0.3810 0.0682 -1 9 2 -0.2798 0.4300 -1 9 3 -0.1653 -0.3086 -1 9 4 -0.0399 -0.1160 -1 9 5 -1.4978 0.0899 -1 9 6 0.2562 -0.1498 -1 9 7 0.3382 0.1456 -1 9 8 0.6101 0.0306 -1 9 9 0.6448 -0.1847 -1 9 10 -0.6669 0.1348 -1 9 11 -0.4742 0.0257 -1 9 12 0.2378 -0.0416 -1 9 13 1.2219 0.1395 -1 9 14 -0.2223 -0.1528 -1 9 15 -0.7248 -0.0877 -1 9 16 -0.3582 -0.0503 -1 10 1 -0.4896 -0.0285 -1 10 2 -0.1614 -0.5328 -1 10 3 -0.3702 0.0080 -1 10 4 -1.0496 0.1732 -1 10 5 -0.3119 -0.0514 -1 10 6 1.3270 0.0839 -1 10 7 0.5951 -0.1257 -1 10 8 -0.3013 0.0529 -1 10 9 -0.1551 0.0845 -1 10 10 0.0036 0.0108 -1 10 11 -0.0848 -0.0620 -1 10 12 0.3213 -0.0430 -1 10 13 0.3073 -0.0593 -1 10 14 -0.3779 0.0331 -1 10 15 0.0254 0.1610 -1 11 1 -0.9098 -0.2387 -1 11 2 -0.6958 0.3487 -1 11 3 -1.1772 -0.0558 -1 11 4 -0.2917 -0.1664 -1 11 5 1.6399 0.1794 -1 11 6 0.8646 -0.1518 -1 11 7 -0.4882 0.0406 -1 11 8 -0.4324 0.2436 -1 11 9 1.0024 -0.2301 -1 11 10 -0.2346 0.2040 -1 11 11 -0.6721 -0.1626 -1 11 12 0.4302 0.0015 -1 11 13 0.5700 0.3150 -1 12 1 -1.2138 0.2612 -1 12 2 -0.7536 -0.2862 -1 12 3 0.3282 -0.1500 -1 12 4 1.2693 0.2042 -1 12 5 0.7438 0.0837 -1 12 6 -0.5222 -0.0366 -1 12 7 0.2128 0.1185 -1 12 8 0.4677 0.0801 -1 12 9 0.4678 0.1337 -1 12 10 -1.0923 0.1117 -1 12 11 0.0441 -0.2149 -1 13 1 -0.0909 -0.2113 -1 13 2 0.8520 0.3427 -1 13 3 1.1474 0.0482 -1 13 4 -0.1959 -0.0194 -1 13 5 -0.3185 0.2640 -1 13 6 0.4211 -0.1285 -1 13 7 0.6289 0.2833 -1 13 8 -0.1656 0.2528 -1 14 1 1.1119 0.6811 -1 14 2 0.7794 -0.1073 -1 14 3 -0.1446 -0.4003 0 -14 1 0.2624 0.4104 0 -14 2 -1.0215 -0.4588 0 -14 3 -0.2250 -0.1112 0 -14 4 0.2433 0.1213 0 -14 5 -0.2539 0.0698 0 -14 6 0.4684 0.1395 0 -14 7 -0.4585 0.0256 0 -13 1 -0.3614 -0.1211 0 -13 2 -0.6328 0.0088 0 -13 3 0.4625 0.1760 0 -13 4 0.2351 -0.0551 0 -13 5 0.1114 0.0615 0 -13 6 0.0011 -0.0518 0 -13 7 -0.2546 -0.0257 0 -13 8 0.7023 -0.0523 0 -13 9 -0.1611 -0.1012 0 -13 10 -0.0659 0.0753 0 -13 11 0.2175 0.1828 0 -12 1 -0.7015 0.2906 0 -12 2 -0.2838 -0.1087 0 -12 3 1.2912 -0.3384 0 -12 4 0.6869 0.0812 0 -12 5 -0.2300 0.0456 0 -12 6 -0.5632 0.0693 0 -12 7 0.0116 0.1170 0 -12 8 0.5496 -0.0788 0 -12 9 -0.1290 -0.0360 0 -12 10 0.4893 0.0514 0 -12 11 0.6749 0.0472 0 -12 12 1.4241 -0.1152 0 -12 13 0.0942 0.1382 0 -11 1 -0.1312 -0.1990 0 -11 2 0.5531 -0.2983 0 -11 3 2.1262 0.2318 0 -11 4 0.0221 0.1345 0 -11 5 -1.1607 0.0593 0 -11 6 -0.8657 0.0348 0 -11 7 0.0559 -0.1104 0 -11 8 0.7548 -0.0319 0 -11 9 0.2050 -0.0246 0 -11 10 1.4444 0.0145 0 -11 11 2.0590 -0.0073 0 -11 12 1.0637 0.0628 0 -11 13 -1.8177 0.1947 0 -11 14 -0.6696 -0.1896 0 -11 15 -0.1671 0.0690 0 -10 1 0.2752 0.1074 0 -10 2 1.3916 0.2495 0 -10 3 1.7593 -0.1862 0 -10 4 -1.1094 -0.0439 0 -10 5 -1.7351 0.0392 0 -10 6 -0.7210 -0.0851 0 -10 7 0.1861 0.1791 0 -10 8 1.1222 0.0363 0 -10 9 1.4353 -0.0933 0 -10 10 3.0911 -0.0022 0 -10 11 1.1376 -0.0257 0 -10 12 -1.7499 0.0367 0 -10 13 -1.8720 -0.0631 0 -10 14 0.3289 -0.0001 0 -10 15 -0.3747 0.2850 0 -10 16 0.2492 0.0614 0 -10 17 0.6958 0.1436 0 -9 1 2.0168 0.1281 0 -9 2 2.0919 -0.4696 0 -9 3 0.0513 0.0585 0 -9 4 -1.8157 0.2203 0 -9 5 -1.5523 0.0058 0 -9 6 -0.2396 0.0988 0 -9 7 0.4642 0.0094 0 -9 8 2.6812 -0.1497 0 -9 9 2.8483 0.0032 0 -9 10 1.9262 0.0105 0 -9 11 -1.6911 -0.0398 0 -9 12 -1.8096 0.0244 0 -9 13 0.0566 0.0597 0 -9 14 0.0501 0.0792 0 -9 15 0.1223 0.0109 0 -9 16 1.5260 0.0433 0 -9 17 1.1185 0.2101 0 -9 18 0.4504 0.1829 0 -8 1 3.8858 -0.2424 0 -8 2 -0.2793 0.3013 0 -8 3 -1.6352 0.0652 0 -8 4 -1.2971 -0.1400 0 -8 5 -1.1005 -0.0097 0 -8 6 0.6916 -0.1176 0 -8 7 2.4102 0.0550 0 -8 8 4.1497 0.1332 0 -8 9 1.7053 0.0183 0 -8 10 -0.3208 -0.0371 0 -8 11 -1.8615 -0.0486 0 -8 12 -0.3703 0.0561 0 -8 13 -0.1590 -0.0728 0 -8 14 -0.2260 -0.0424 0 -8 15 1.6324 0.0847 0 -8 16 1.6652 0.0975 0 -8 17 0.5891 0.0920 0 -8 18 -0.1816 0.1013 0 -8 19 -0.4099 0.0226 0 -7 1 0.8611 0.4007 0 -7 2 -3.1113 -0.4167 0 -7 3 -1.1972 -0.2347 0 -7 4 -1.1925 0.2183 0 -7 5 0.5064 -0.0269 0 -7 6 4.0046 0.0911 0 -7 7 4.4947 0.1014 0 -7 8 2.8386 -0.0979 0 -7 9 -0.5918 -0.0420 0 -7 10 -1.5014 -0.0113 0 -7 11 -1.6090 -0.0184 0 -7 12 -0.7005 0.0028 0 -7 13 -0.2439 -0.0470 0 -7 14 1.4213 0.1364 0 -7 15 2.2477 -0.0135 0 -7 16 0.5802 -0.0663 0 -7 17 -0.3368 0.0250 0 -7 18 -0.5480 0.0807 0 -7 19 0.0770 -0.0515 0 -7 20 0.7215 -0.2482 0 -6 1 -2.5409 -0.4982 0 -6 2 -3.1879 0.0507 0 -6 3 -1.0206 0.3801 0 -6 4 0.0212 -0.0979 0 -6 5 5.5608 -0.0652 0 -6 6 6.5802 -0.1236 0 -6 7 3.0598 -0.0982 0 -6 8 -0.8753 0.1212 0 -6 9 -3.0191 0.0562 0 -6 10 -2.1804 0.0008 0 -6 11 -0.8143 0.0026 0 -6 12 0.5645 0.0348 0 -6 13 1.6623 0.0088 0 -6 14 1.9585 -0.0290 0 -6 15 0.2599 -0.1023 0 -6 16 -1.0029 -0.0075 0 -6 17 -0.3807 0.0196 0 -6 18 0.2225 0.0207 0 -6 19 0.2245 -0.1399 0 -6 20 0.0564 -0.2203 0 -6 21 -0.3451 -0.2015 0 -5 1 -1.6660 0.4738 0 -5 2 -4.9888 -0.0313 0 -5 3 -0.3119 -0.4073 0 -5 4 5.5408 0.0743 0 -5 5 10.1410 -0.0199 0 -5 6 4.8074 0.0089 0 -5 7 -1.4667 0.1979 0 -5 8 -4.8825 -0.0409 0 -5 9 -3.2047 -0.0291 0 -5 10 0.1456 0.0100 0 -5 11 2.0551 0.0104 0 -5 12 1.9626 -0.0205 0 -5 13 1.0191 -0.0506 0 -5 14 -0.5162 0.0230 0 -5 15 -1.4779 0.0053 0 -5 16 -0.0266 -0.0318 0 -5 17 0.7037 0.0325 0 -5 18 -0.1161 0.0041 0 -5 19 -0.6280 -0.1036 0 -5 20 0.0979 -0.1373 0 -5 21 0.1719 -0.0160 0 -4 1 -8.2240 -0.5308 0 -4 2 -8.1198 -0.3428 0 -4 3 10.3615 0.5076 0 -4 4 14.9877 0.1394 0 -4 5 9.6982 -0.0552 0 -4 6 -2.2597 -0.0118 0 -4 7 -7.4235 -0.1949 0 -4 8 -4.6920 0.0420 0 -4 9 0.9467 0.0865 0 -4 10 3.3372 -0.0508 0 -4 11 2.4133 0.0008 0 -4 12 0.1484 0.0000 0 -4 13 -0.8278 0.0770 0 -4 14 -1.1506 -0.0117 0 -4 15 -0.0471 -0.0244 0 -4 16 1.1517 0.0105 0 -4 17 -0.4594 0.0520 0 -4 18 -1.1467 -0.0430 0 -4 19 -0.3703 -0.0215 0 -4 20 0.6727 0.0808 0 -4 21 0.0592 0.1492 0 -4 22 -0.1994 0.0342 0 -3 1 -15.6613 0.2800 0 -3 2 14.0819 0.5035 0 -3 3 32.3381 -0.2883 0 -3 4 13.1261 -0.1313 0 -3 5 -4.2736 -0.0381 0 -3 6 -12.5194 -0.1268 0 -3 7 -6.3905 0.1727 0 -3 8 2.4992 0.0673 0 -3 9 4.2925 -0.1111 0 -3 10 2.4854 0.0140 0 -3 11 0.0244 0.0452 0 -3 12 -0.5872 0.0542 0 -3 13 -0.2249 -0.0504 0 -3 14 -0.1837 -0.0343 0 -3 15 0.5535 0.0468 0 -3 16 -0.0318 -0.0246 0 -3 17 -1.5388 0.0331 0 -3 18 -0.5809 0.0222 0 -3 19 0.3088 0.1280 0 -3 20 0.9197 0.0464 0 -3 21 -0.3670 -0.1199 0 -3 22 -0.5005 -0.1422 0 -2 1 24.1223 -0.1760 0 -2 2 51.2223 -0.9428 0 -2 3 22.9005 0.1703 0 -2 4 -14.8162 0.2778 0 -2 5 -17.9393 -0.0536 0 -2 6 -7.4061 0.0984 0 -2 7 5.3601 -0.1180 0 -2 8 6.7324 -0.0688 0 -2 9 1.2253 0.1182 0 -2 10 -0.4238 -0.0110 0 -2 11 -0.3700 -0.0020 0 -2 12 0.7960 -0.0337 0 -2 13 0.2496 -0.0228 0 -2 14 0.0027 0.0510 0 -2 15 -0.0546 -0.0579 0 -2 16 -0.7819 0.0155 0 -2 17 -1.1066 0.0430 0 -2 18 0.4683 -0.0013 0 -2 19 0.5367 -0.0405 0 -2 20 0.3985 -0.1110 0 -2 21 -1.4718 -0.0351 0 -2 22 -0.4669 0.0999 0 -1 1 70.7515 -1.0335 0 -1 2 27.7685 0.6075 0 -1 3 -22.9395 0.2085 0 -1 4 -26.1929 -0.1587 0 -1 5 -3.7547 -0.0181 0 -1 6 8.4621 -0.1594 0 -1 7 8.3328 0.0688 0 -1 8 0.4704 0.1653 0 -1 9 -2.4712 -0.1178 0 -1 10 0.1213 -0.0682 0 -1 11 1.6218 0.0367 0 -1 12 1.5303 0.0216 0 -1 13 0.1787 0.0186 0 -1 14 -0.2603 -0.0552 0 -1 15 -0.8217 -0.0095 0 -1 16 -0.3638 -0.0116 0 -1 17 -0.0949 -0.0544 0 -1 18 0.9616 -0.0475 0 -1 19 -0.5592 -0.0111 0 -1 20 -0.6667 0.0963 0 -1 21 -1.5884 0.0568 0 -1 22 0.5098 0.0622 0 -1 23 -0.0227 -0.0543 0 0 1 29.9722 0.6056 0 0 2 -31.0148 -0.5628 0 0 3 -28.0284 -0.2178 0 0 4 -0.0991 0.2637 0 0 5 12.0450 -0.1035 0 0 6 7.2909 0.0919 0 0 7 -1.0696 -0.0378 0 0 8 -2.7950 -0.1647 0 0 9 0.8597 0.0506 0 0 10 2.8291 0.0419 0 0 11 2.3530 0.0263 0 0 12 0.7729 -0.0071 0 0 13 -0.4773 -0.0350 0 0 14 -1.0069 0.0230 0 0 15 -0.3774 -0.0248 0 0 16 0.7469 -0.0459 0 0 17 0.0363 0.0467 0 0 18 0.1017 -0.0012 0 0 19 -1.6978 0.0702 0 0 20 -0.3049 -0.0126 0 0 21 -0.6436 -0.0577 0 0 22 0.6715 -0.0549 0 0 23 -0.6670 -0.0187 0 1 0 30.6522 0.4415 0 1 1 -34.5005 -1.3935 0 1 2 -26.9180 -0.1326 0 1 3 4.5445 0.5473 0 1 4 11.9547 -0.1568 0 1 5 5.9519 -0.0235 0 1 6 -2.5132 -0.1885 0 1 7 -2.3610 -0.0467 0 1 8 3.1543 0.2089 0 1 9 4.0902 -0.0330 0 1 10 2.0587 -0.0750 0 1 11 0.9974 0.0293 0 1 12 -0.4738 -0.0058 0 1 13 -1.0693 0.0501 0 1 14 -0.3561 0.0018 0 1 15 0.6748 -0.0124 0 1 16 0.5175 0.0321 0 1 17 -0.5551 0.0078 0 1 18 -0.5805 -0.0455 0 1 19 -1.3395 -0.0079 0 1 20 0.6478 -0.0558 0 1 21 -0.6083 -0.0096 0 1 22 -0.1634 -0.0011 0 2 0 -27.0858 -1.3846 0 2 1 -24.7626 -0.0090 0 2 2 6.2880 0.1879 0 2 3 9.3208 -0.2749 0 2 4 3.9068 0.1717 0 2 5 -0.7341 -0.1104 0 2 6 -2.2716 0.0324 0 2 7 4.2116 0.1572 0 2 8 5.2264 -0.2331 0 2 9 1.9744 0.0023 0 2 10 0.1380 0.0507 0 2 11 -0.1045 0.0097 0 2 12 -1.1973 0.0176 0 2 13 -0.2945 -0.0267 0 2 14 1.0313 0.0307 0 2 15 0.4261 -0.0092 0 2 16 -0.2502 -0.0262 0 2 17 -0.8195 -0.0043 0 2 18 -0.6804 -0.0511 0 2 19 -0.3448 0.0117 0 2 20 0.3347 -0.0044 0 2 21 -1.1740 0.0235 0 2 22 -0.2820 0.1190 0 3 0 -17.2276 0.0920 0 3 1 2.9049 -0.4453 0 3 2 5.1504 -0.4230 0 3 3 1.9808 0.5231 0 3 4 2.3196 -0.0341 0 3 5 -0.4721 -0.1102 0 3 6 1.7669 -0.0100 0 3 7 5.2211 -0.2397 0 3 8 2.2977 0.1764 0 3 9 0.0463 0.0727 0 3 10 -0.9233 -0.1067 0 3 11 -0.8398 0.0195 0 3 12 -0.0636 -0.0442 0 3 13 1.6095 0.0051 0 3 14 1.0479 0.0194 0 3 15 -1.1305 -0.0787 0 3 16 -0.8952 0.0413 0 3 17 -0.5240 -0.0369 0 3 18 -0.2317 -0.0181 0 3 19 0.0496 0.0322 0 3 20 -0.3372 0.0437 0 3 21 -0.5026 0.0743 0 3 22 0.1027 0.0879 0 4 0 -0.6134 -1.0222 0 4 1 0.3569 -0.2994 0 4 2 0.8182 0.2461 0 4 3 4.8150 -0.1292 0 4 4 1.0954 -0.0525 0 4 5 -0.3263 -0.0091 0 4 6 2.5052 -0.0669 0 4 7 3.2712 0.2419 0 4 8 0.0616 -0.0956 0 4 9 -1.3345 -0.1463 0 4 10 -1.1505 0.1094 0 4 11 0.7382 -0.0582 0 4 12 2.2162 0.0230 0 4 13 1.0874 -0.0617 0 4 14 -1.0180 -0.0206 0 4 15 -2.1138 -0.0027 0 4 16 0.2039 0.0298 0 4 17 0.2954 -0.0156 0 4 18 -0.2344 0.0117 0 4 19 0.2187 0.0332 0 4 20 -0.4171 0.0792 0 4 21 0.0216 -0.0161 0 4 22 0.0401 0.0779 0 5 0 -2.2810 -0.2668 0 5 1 0.3632 -0.1179 0 5 2 5.7866 -0.5075 0 5 3 1.9643 0.3515 0 5 4 -1.9982 0.1155 0 5 5 1.1204 -0.1055 0 5 6 2.5611 0.1232 0 5 7 0.6878 -0.2254 0 5 8 -1.8956 -0.0230 0 5 9 -0.9343 0.2106 0 5 10 0.7795 -0.0983 0 5 11 2.5807 -0.0058 0 5 12 1.2051 0.0027 0 5 13 -0.9288 -0.0819 0 5 14 -1.4524 0.0799 0 5 15 -0.6551 -0.0354 0 5 16 1.3560 0.0403 0 5 17 -0.3916 -0.0416 0 5 18 -0.4049 -0.0190 0 5 19 0.1044 0.0830 0 5 20 -0.5336 -0.0010 0 5 21 0.5272 -0.0625 0 6 0 0.9303 -0.6787 0 6 1 4.8220 -0.4702 0 6 2 2.8520 0.2262 0 6 3 -2.8980 0.0696 0 6 4 0.5889 -0.1380 0 6 5 2.4408 0.0190 0 6 6 -0.2111 -0.1296 0 6 7 -1.5736 0.1556 0 6 8 -0.7801 0.0865 0 6 9 0.8334 -0.1675 0 6 10 2.1537 0.0499 0 6 11 1.8040 0.0381 0 6 12 -0.5713 -0.0281 0 6 13 -0.7792 0.0097 0 6 14 -0.7589 -0.0436 0 6 15 0.4864 0.0179 0 6 16 0.3227 -0.0377 0 6 17 -1.1672 0.0121 0 6 18 -0.1425 0.0349 0 6 19 0.2128 0.0183 0 6 20 0.0763 -0.1348 0 7 0 4.5834 -0.5255 0 7 1 1.8851 0.0138 0 7 2 -1.6080 -0.3976 0 7 3 -0.8075 0.1337 0 7 4 2.8252 0.1886 0 7 5 -0.9224 -0.1755 0 7 6 -1.5736 0.1691 0 7 7 0.0573 -0.1153 0 7 8 0.7493 -0.1986 0 7 9 1.7583 0.2021 0 7 10 1.9818 -0.0338 0 7 11 -0.0888 -0.0210 0 7 12 -1.0963 0.0351 0 7 13 -0.3170 -0.0761 0 7 14 -0.2072 0.0478 0 7 15 0.4510 0.0332 0 7 16 -0.9892 -0.0720 0 7 17 -0.3846 0.0948 0 7 18 0.4947 -0.1750 0 7 19 0.2082 0.0082 0 7 20 -0.6802 -0.2135 0 8 0 1.6897 -0.4047 0 8 1 -1.8132 -0.5244 0 8 2 -0.6163 0.1545 0 8 3 1.5373 0.2031 0 8 4 0.0586 -0.1936 0 8 5 -1.7632 -0.0266 0 8 6 0.7817 -0.0913 0 8 7 0.7134 -0.0683 0 8 8 1.3529 0.1947 0 8 9 1.5546 -0.1400 0 8 10 -0.0993 -0.0086 0 8 11 -1.3480 0.0906 0 8 12 -0.1422 -0.0154 0 8 13 0.6032 0.0567 0 8 14 -0.1806 -0.0064 0 8 15 -0.3484 -0.0589 0 8 16 -0.7192 -0.0922 0 8 17 0.7628 0.0163 0 8 18 -0.1772 -0.0409 0 8 19 -0.7426 0.2269 0 9 0 -1.6494 -0.7414 0 9 1 -0.8160 0.1000 0 9 2 0.7146 -0.2358 0 9 3 0.3158 -0.0631 0 9 4 -1.0949 0.1812 0 9 5 0.5071 -0.1376 0 9 6 1.0277 0.0950 0 9 7 0.6554 0.0624 0 9 8 1.0261 -0.2203 0 9 9 -0.5183 0.1090 0 9 10 -0.8759 0.1122 0 9 11 0.0979 -0.1181 0 9 12 1.2859 0.1640 0 9 13 -0.1843 -0.1274 0 9 14 -0.8274 -0.0046 0 9 15 -0.1476 -0.0200 0 9 16 0.0727 -0.0272 0 9 17 0.4570 0.2558 0 9 18 -0.9190 0.1409 0 10 0 -1.3533 -0.2191 0 10 1 0.1123 -0.3617 0 10 2 -0.3139 -0.0582 0 10 3 -0.3312 0.3806 0 10 4 0.0424 -0.1159 0 10 5 1.3781 -0.0059 0 10 6 0.5058 0.0014 0 10 7 0.0454 -0.0668 0 10 8 -0.4642 0.1102 0 10 9 -0.4663 0.0425 0 10 10 0.6516 -0.1574 0 10 11 1.0084 0.0837 0 10 12 0.1902 0.0932 0 10 13 -1.1889 -0.1118 0 10 14 -0.0737 0.1727 0 10 15 0.0004 -0.1237 0 10 16 0.3906 0.1048 0 11 0 -1.3316 -0.6466 0 11 1 -0.0449 -0.0105 0 11 2 -0.3549 -0.0135 0 11 3 0.5193 -0.0759 0 11 4 0.9124 0.1268 0 11 5 0.7215 -0.0608 0 11 6 -0.4309 0.0412 0 11 7 -0.6105 0.2019 0 11 8 0.2437 -0.3116 0 11 9 0.5204 0.1135 0 11 10 0.6725 -0.0207 0 11 11 0.1552 0.0384 0 11 12 -0.5847 0.0813 0 11 13 -0.5796 -0.1663 0 11 14 0.0859 -0.0217 0 11 15 0.0759 -0.2153 0 12 0 -0.4332 -0.3153 0 12 1 0.6651 -0.2205 0 12 2 0.3475 -0.1959 0 12 3 0.6836 0.3041 0 12 4 -0.1356 -0.0169 0 12 5 -0.1608 -0.1162 0 12 6 0.0738 0.1366 0 12 7 0.1748 -0.2176 0 12 8 0.6885 -0.0573 0 12 9 -0.1988 0.2099 0 12 10 0.1968 -0.4286 0 12 11 -0.0812 0.2119 0 12 12 -0.4591 -0.2629 0 12 13 -0.4056 -0.2480 0 13 0 0.7966 -0.4959 0 13 1 0.6566 -0.1510 0 13 2 0.3572 -0.0533 0 13 3 -0.7093 -0.1167 0 13 4 -0.4388 -0.0121 0 13 5 1.0269 -0.1758 0 13 6 0.5738 -0.0017 0 13 7 -0.0557 -0.0407 0 13 8 0.0208 -0.1988 0 13 9 -0.5556 -0.1633 0 13 10 0.3596 -0.1772 0 14 0 1.0678 -0.4259 0 14 1 0.3661 -0.3070 0 14 2 -0.2351 -0.4268 0 14 3 -1.0612 0.2596 0 14 4 0.8091 -0.1811 0 14 5 0.9360 -0.2409 0 14 6 -0.1592 0.2329 1 -14 0 -0.4035 -0.2373 1 -14 1 -0.7998 -0.5264 1 -14 2 -0.0320 0.1109 1 -14 3 0.4286 0.4494 1 -14 4 -0.3734 -0.0427 1 -14 5 1.0428 -0.2032 1 -13 0 -1.5060 -0.3435 1 -13 1 -0.6533 -0.4608 1 -13 2 0.2534 0.2829 1 -13 3 0.1622 -0.0581 1 -13 4 0.0367 -0.1568 1 -13 5 0.5965 -0.2503 1 -13 6 -0.0621 -0.1511 1 -13 7 1.2183 0.3454 1 -13 8 0.1588 0.3040 1 -13 9 -0.3299 0.0684 1 -13 10 0.2133 -0.2813 1 -12 0 -1.2022 -0.5384 1 -12 1 0.0901 -0.1235 1 -12 2 0.9729 -0.1268 1 -12 3 0.1498 0.1068 1 -12 4 -0.7028 0.0579 1 -12 5 -0.3114 -0.0943 1 -12 6 0.8558 0.1145 1 -12 7 1.1913 0.0236 1 -12 8 -0.2332 -0.0446 1 -12 9 0.2000 -0.0512 1 -12 10 0.1096 -0.0607 1 -12 11 -0.5860 -0.0542 1 -12 12 -1.1213 -0.1730 1 -12 13 -0.5032 -0.0276 1 -11 0 0.0769 -0.1819 1 -11 1 0.8468 -0.4481 1 -11 2 1.1576 0.0788 1 -11 3 -1.4280 0.2025 1 -11 4 -1.4641 -0.1098 1 -11 5 0.1088 -0.0613 1 -11 6 1.3834 -0.1612 1 -11 7 1.0338 0.0148 1 -11 8 0.2779 0.1655 1 -11 9 0.1069 -0.0026 1 -11 10 -0.9420 -0.0805 1 -11 11 -1.7313 -0.1464 1 -11 12 -1.7657 -0.0022 1 -11 13 -0.0872 -0.1758 1 -11 14 0.3776 -0.1850 1 -11 15 0.7805 0.0548 1 -10 0 1.0088 -0.7794 1 -10 1 0.8786 -0.0944 1 -10 2 -0.1025 -0.0438 1 -10 3 -2.8045 -0.0077 1 -10 4 -0.6687 0.0715 1 -10 5 0.8774 -0.0912 1 -10 6 1.8666 0.0463 1 -10 7 1.3380 0.0774 1 -10 8 -0.0243 -0.1131 1 -10 9 -1.0020 -0.0856 1 -10 10 -2.5577 -0.0100 1 -10 11 -2.4155 0.0308 1 -10 12 -0.7063 -0.0449 1 -10 13 1.2788 -0.2081 1 -10 14 0.8214 0.1059 1 -10 15 0.6934 -0.0281 1 -10 16 -0.2254 -0.1879 1 -9 0 1.8787 -0.0867 1 -9 1 -0.4372 -0.3991 1 -9 2 -2.4918 -0.1363 1 -9 3 -2.2174 0.2943 1 -9 4 1.1576 -0.0333 1 -9 5 1.7402 -0.0897 1 -9 6 1.6759 -0.0851 1 -9 7 0.5471 -0.1467 1 -9 8 -1.3199 0.0815 1 -9 9 -2.1941 0.0715 1 -9 10 -2.9035 0.0241 1 -9 11 -0.7888 -0.0280 1 -9 12 0.8463 -0.0584 1 -9 13 1.1264 -0.0091 1 -9 14 0.4701 -0.0257 1 -9 15 0.4243 -0.2285 1 -9 16 -0.7662 -0.1144 1 -9 17 -1.0647 -0.0309 1 -9 18 -1.0364 0.0247 1 -8 0 0.4292 -0.9310 1 -8 1 -4.0632 -0.2890 1 -8 2 -2.6083 0.1100 1 -8 3 0.8457 -0.0288 1 -8 4 2.0183 -0.0060 1 -8 5 1.3891 -0.0812 1 -8 6 0.4615 0.0178 1 -8 7 -0.5031 0.1125 1 -8 8 -2.3449 -0.0434 1 -8 9 -2.0683 -0.0966 1 -8 10 -1.7842 -0.0101 1 -8 11 0.1939 0.0418 1 -8 12 0.3404 0.0224 1 -8 13 0.5830 -0.0680 1 -8 14 0.7580 -0.0470 1 -8 15 -0.2722 -0.0451 1 -8 16 -1.7245 -0.0307 1 -8 17 -1.4908 -0.0640 1 -8 18 -0.6608 -0.1307 1 -8 19 0.0659 -0.1999 1 -7 0 -3.7636 -0.2199 1 -7 1 -4.5838 -0.1935 1 -7 2 0.9586 -0.2842 1 -7 3 2.0033 0.2848 1 -7 4 1.5238 0.0724 1 -7 5 1.2004 -0.0383 1 -7 6 -0.9063 -0.0034 1 -7 7 -2.1598 -0.1958 1 -7 8 -3.4097 -0.0283 1 -7 9 -1.7726 0.0893 1 -7 10 -1.0689 0.0318 1 -7 11 0.5703 0.0448 1 -7 12 0.7871 -0.0676 1 -7 13 1.4186 0.0299 1 -7 14 0.4549 0.0287 1 -7 15 -1.9691 -0.0732 1 -7 16 -2.3873 -0.0817 1 -7 17 -1.0668 -0.0230 1 -7 18 0.0660 -0.0382 1 -7 19 0.2995 -0.1581 1 -7 20 -0.5899 -0.1527 1 -6 0 -4.4856 -0.7732 1 -6 1 -0.4110 -0.5351 1 -6 2 3.0530 0.2523 1 -6 3 1.5252 0.0813 1 -6 4 2.0334 -0.0836 1 -6 5 -0.7490 -0.0634 1 -6 6 -4.1604 -0.0641 1 -6 7 -4.6129 0.1570 1 -6 8 -3.5204 0.0566 1 -6 9 -0.0141 -0.0785 1 -6 10 1.2699 -0.0307 1 -6 11 2.0760 0.0090 1 -6 12 1.3787 -0.0178 1 -6 13 0.2026 0.0462 1 -6 14 -2.0916 -0.0361 1 -6 15 -3.0382 -0.0116 1 -6 16 -0.8395 -0.0037 1 -6 17 0.5734 0.0451 1 -6 18 0.4445 -0.0448 1 -6 19 -0.1201 -0.0578 1 -6 20 -0.7546 0.0225 1 -6 21 0.2257 0.1478 1 -5 0 0.8087 -0.5150 1 -5 1 1.9831 0.0888 1 -5 2 2.8612 -0.3009 1 -5 3 1.5269 0.0677 1 -5 4 0.2476 0.1369 1 -5 5 -5.3208 0.0005 1 -5 6 -6.6307 0.1511 1 -5 7 -4.8477 -0.1273 1 -5 8 -0.4251 -0.1448 1 -5 9 3.4333 0.0704 1 -5 10 3.1006 0.0130 1 -5 11 1.1414 0.0044 1 -5 12 -1.3111 -0.0413 1 -5 13 -2.6725 0.0380 1 -5 14 -2.1837 0.0329 1 -5 15 0.1115 0.0013 1 -5 16 1.5945 -0.0027 1 -5 17 0.2127 0.0160 1 -5 18 -0.2788 0.0142 1 -5 19 -0.0438 0.0347 1 -5 20 -0.2753 0.0531 1 -5 21 0.1701 0.2715 1 -5 22 -0.3910 0.1309 1 -4 0 0.8147 -0.4493 1 -4 1 0.6227 -0.7078 1 -4 2 6.3142 0.1058 1 -4 3 0.8523 0.2513 1 -4 4 -5.0818 -0.0980 1 -4 5 -10.2826 -0.0367 1 -4 6 -7.3277 -0.1504 1 -4 7 -1.5460 0.0174 1 -4 8 4.5194 0.1681 1 -4 9 4.8550 -0.0532 1 -4 10 1.0532 -0.0326 1 -4 11 -2.7508 -0.0018 1 -4 12 -3.3399 0.0138 1 -4 13 -1.1566 0.0253 1 -4 14 1.5692 -0.0177 1 -4 15 2.0187 -0.0038 1 -4 16 -0.0179 0.0044 1 -4 17 -0.9353 -0.0059 1 -4 18 0.3105 0.0307 1 -4 19 0.3375 0.0485 1 -4 20 -0.2397 0.1511 1 -4 21 -0.2602 0.0548 1 -4 22 -0.4521 -0.3566 1 -3 0 -1.3666 -0.9381 1 -3 1 12.6141 0.2598 1 -3 2 10.3470 -0.1634 1 -3 3 -11.6374 -0.1527 1 -3 4 -17.1610 0.0027 1 -3 5 -13.1552 -0.0489 1 -3 6 -0.9655 0.1501 1 -3 7 6.9972 0.0724 1 -3 8 6.7717 -0.1751 1 -3 9 1.0888 0.0309 1 -3 10 -3.7180 0.0635 1 -3 11 -4.1319 0.0046 1 -3 12 -0.5853 -0.0291 1 -3 13 1.8430 -0.0541 1 -3 14 1.9304 0.0520 1 -3 15 -0.0880 -0.0063 1 -3 16 -1.1938 0.0022 1 -3 17 0.0585 -0.0436 1 -3 18 0.7896 0.0296 1 -3 19 0.3447 0.0218 1 -3 20 -0.5819 -0.0721 1 -3 21 -1.0088 -0.2339 1 -3 22 -0.4228 -0.1368 1 -2 0 23.0778 0.0345 1 -2 1 20.3008 -0.7927 1 -2 2 -16.7463 -0.2055 1 -2 3 -36.5129 0.3132 1 -2 4 -17.3226 -0.0407 1 -2 5 1.5161 0.0730 1 -2 6 12.9291 -0.1028 1 -2 7 9.0771 -0.0991 1 -2 8 -0.8129 0.1449 1 -2 9 -5.1303 0.0268 1 -2 10 -4.6636 -0.0752 1 -2 11 -0.4501 0.0089 1 -2 12 1.8360 -0.0436 1 -2 13 1.0303 0.0482 1 -2 14 0.0033 0.0131 1 -2 15 -0.9241 -0.0010 1 -2 16 -0.3764 -0.0155 1 -2 17 0.7875 -0.0828 1 -2 18 0.6762 0.0095 1 -2 19 -0.1420 -0.0951 1 -2 20 -1.5024 -0.0255 1 -2 21 -0.4917 0.0413 1 -2 22 0.7171 0.1178 1 -2 23 0.6354 0.0475 1 -1 0 31.3705 -1.5635 1 -1 1 -25.4862 0.1862 1 -1 2 -53.6981 0.3944 1 -1 3 -25.4819 -0.1139 1 -1 4 11.0821 -0.0031 1 -1 5 17.0811 -0.1422 1 -1 6 9.8142 0.0152 1 -1 7 -3.3814 0.1779 1 -1 8 -7.9138 -0.1581 1 -1 9 -3.6974 -0.0705 1 -1 10 -0.3234 0.0931 1 -1 11 2.0428 0.0144 1 -1 12 0.3281 -0.0071 1 -1 13 -0.6570 -0.0201 1 -1 14 -0.7024 0.0055 1 -1 15 -0.3367 0.0278 1 -1 16 0.5062 -0.0528 1 -1 17 0.8329 0.0214 1 -1 18 -0.3593 -0.0067 1 -1 19 -0.7120 0.0245 1 -1 20 -0.6107 0.0998 1 -1 21 1.1757 -0.0177 1 -1 22 0.4970 -0.1120 1 -1 23 0.1191 -0.1281 1 0 0 -28.8147 0.5483 1 0 1 -67.8678 0.0926 1 0 2 -26.9208 -0.4391 1 0 3 17.5053 0.2097 1 0 4 21.4589 -0.1177 1 0 5 4.9145 0.0347 1 0 6 -5.8260 0.0445 1 0 7 -8.1781 -0.1730 1 0 8 -2.7317 0.0878 1 0 9 0.9025 0.1102 1 0 10 0.9628 -0.0617 1 0 11 0.0909 -0.0396 1 0 12 -1.3376 -0.0213 1 0 13 -0.9231 0.0007 1 0 14 -0.2957 0.0552 1 0 15 0.7514 -0.0072 1 0 16 0.4190 0.0694 1 0 17 -0.2190 0.0032 1 0 18 -1.0770 -0.0229 1 0 19 0.5431 0.0371 1 0 20 0.6069 -0.0244 1 0 21 1.0571 -0.0401 1 0 22 -0.5208 -0.0371 1 0 23 0.3685 0.0928 1 1 0 -70.1448 -0.9801 1 1 1 -26.6796 -0.5650 1 1 2 23.6075 0.5735 1 1 3 19.8804 0.0241 1 1 4 0.9561 0.0159 1 1 5 -8.6308 -0.0199 1 1 6 -6.7912 -0.1225 1 1 7 -0.5826 0.2416 1 1 8 0.8804 -0.0478 1 1 9 -0.3794 -0.1717 1 1 10 -0.7939 0.0483 1 1 11 -1.3945 0.0156 1 1 12 -0.9722 0.0170 1 1 13 -0.5524 -0.0129 1 1 14 0.5882 0.0157 1 1 15 0.7375 0.0190 1 1 16 -0.6992 0.0326 1 1 17 -0.8012 -0.0675 1 1 18 -0.4860 0.0264 1 1 19 1.7618 -0.0058 1 1 20 0.3811 0.0571 1 1 21 0.2631 0.0345 1 1 22 -0.7029 0.0205 1 1 23 0.8450 -0.0318 1 2 0 -25.2079 -0.2233 1 2 1 24.2891 0.8930 1 2 2 17.3076 -0.0039 1 2 3 -2.5472 0.0938 1 2 4 -6.8741 -0.0356 1 2 5 -6.6944 -0.1604 1 2 6 -0.2822 0.1821 1 2 7 1.1458 -0.1842 1 2 8 -1.6999 -0.0320 1 2 9 -1.5776 0.1736 1 2 10 -1.2205 -0.0047 1 2 11 -1.4680 -0.0372 1 2 12 -0.3827 -0.0414 1 2 13 0.1976 -0.0195 1 2 14 0.6790 0.0262 1 2 15 -0.4784 -0.0116 1 2 16 -1.5458 0.0335 1 2 17 -0.5029 -0.0280 1 2 18 0.7904 0.0410 1 2 19 1.9901 0.0121 1 2 20 -0.5760 0.0615 1 2 21 -0.1673 -0.0353 1 2 22 -0.0687 -0.0172 1 2 23 1.1346 -0.0709 1 3 0 16.9921 0.4774 1 3 1 14.8987 -0.3823 1 3 2 -3.0597 0.2446 1 3 3 -3.4139 0.0563 1 3 4 -5.1550 -0.1776 1 3 5 -3.8008 0.1335 1 3 6 1.2018 -0.1776 1 3 7 -0.8745 0.1610 1 3 8 -1.6907 0.2049 1 3 9 -1.7915 -0.2164 1 3 10 -1.7740 0.0184 1 3 11 -0.8399 -0.0128 1 3 12 0.9299 -0.0115 1 3 13 0.2677 0.0367 1 3 14 -1.2411 -0.0292 1 3 15 -1.4771 0.0541 1 3 16 -0.8404 -0.0006 1 3 17 1.1557 0.0054 1 3 18 1.3753 0.0417 1 3 19 0.6149 -0.0195 1 3 20 -1.1620 -0.0023 1 3 21 0.2961 -0.0274 1 3 22 0.6086 0.0579 1 3 23 0.5345 -0.0983 1 4 0 10.2149 -0.4450 1 4 1 0.1261 0.4336 1 4 2 -0.8391 0.2607 1 4 3 -3.3880 -0.0566 1 4 4 -6.4086 0.1403 1 4 5 -0.4833 -0.1532 1 4 6 1.9416 0.1152 1 4 7 -1.0757 0.0443 1 4 8 -2.4494 -0.2540 1 4 9 -2.6857 0.1526 1 4 10 -0.5076 0.0672 1 4 11 1.3572 -0.0497 1 4 12 0.5499 0.0118 1 4 13 -2.2261 -0.0151 1 4 14 -2.3285 0.0275 1 4 15 0.3809 0.0297 1 4 16 0.9235 0.0150 1 4 17 1.1980 0.0581 1 4 18 0.0868 -0.0540 1 4 19 -0.3380 0.0009 1 4 20 -0.3721 -0.0374 1 4 21 0.8253 0.0683 1 4 22 0.1507 -0.0528 1 5 0 3.2130 0.7290 1 5 1 1.2648 -0.1329 1 5 2 -2.8633 0.1833 1 5 3 -6.7078 0.0802 1 5 4 -1.3744 -0.1590 1 5 5 3.2540 0.0667 1 5 6 0.4266 -0.1036 1 5 7 -3.3198 -0.0830 1 5 8 -2.8167 0.2714 1 5 9 -0.2960 -0.0547 1 5 10 2.2449 -0.0933 1 5 11 0.8334 0.0467 1 5 12 -2.7516 -0.0580 1 5 13 -2.7925 0.0771 1 5 14 -0.0989 -0.0266 1 5 15 2.1272 0.0500 1 5 16 0.0176 0.0436 1 5 17 0.0725 -0.0382 1 5 18 -0.0138 0.0229 1 5 19 0.1805 -0.0166 1 5 20 0.5804 -0.0772 1 5 21 -0.1460 0.0349 1 5 22 -1.0314 -0.2012 1 6 0 2.9382 -0.4220 1 6 1 -2.2923 0.1003 1 6 2 -6.0979 0.3342 1 6 3 -1.2439 -0.1429 1 6 4 3.2963 0.1719 1 6 5 0.5843 -0.1153 1 6 6 -2.9796 -0.0186 1 6 7 -2.5250 0.1877 1 6 8 0.4062 -0.2056 1 6 9 2.4321 -0.0585 1 6 10 1.4041 0.1268 1 6 11 -2.9354 -0.0738 1 6 12 -3.4451 0.0362 1 6 13 -0.3095 -0.0081 1 6 14 1.6072 -0.0028 1 6 15 1.1287 0.0325 1 6 16 -0.9916 -0.0007 1 6 17 0.7368 0.0459 1 6 18 0.5918 -0.0018 1 6 19 0.4041 -0.1575 1 6 20 -0.3364 -0.0281 1 6 21 -1.5310 0.0841 1 7 0 -1.5406 0.5760 1 7 1 -4.5167 0.0969 1 7 2 -1.5833 0.1123 1 7 3 3.4471 0.1245 1 7 4 -0.1145 -0.1334 1 7 5 -2.6142 0.0181 1 7 6 -1.3033 0.0254 1 7 7 0.6096 -0.1913 1 7 8 2.0277 0.1357 1 7 9 1.2229 0.0421 1 7 10 -2.4696 -0.0846 1 7 11 -3.8434 0.0487 1 7 12 -0.3893 -0.0119 1 7 13 1.6966 -0.0108 1 7 14 1.2437 -0.0044 1 7 15 -0.5020 -0.0961 1 7 16 -0.2357 0.1562 1 7 17 1.1240 -0.1062 1 7 18 0.2155 0.0023 1 7 19 -0.5017 -0.0619 1 7 20 -0.6921 0.1776 1 8 0 -3.8273 -0.1805 1 8 1 -0.2649 -0.1104 1 8 2 2.4986 0.3006 1 8 3 0.5865 -0.1458 1 8 4 -3.3288 0.1423 1 8 5 -0.2411 0.0542 1 8 6 0.7344 -0.1571 1 8 7 0.8526 0.2095 1 8 8 0.6155 -0.0620 1 8 9 -1.8224 -0.1352 1 8 10 -3.0203 0.1789 1 8 11 -0.4602 -0.0287 1 8 12 1.9587 -0.0411 1 8 13 0.8444 -0.0362 1 8 14 -0.6115 -0.1285 1 8 15 -0.7769 0.0352 1 8 16 0.7702 0.0980 1 8 17 0.4097 -0.0947 1 8 18 -0.0392 0.2527 1 8 19 0.0008 -0.1007 1 8 20 0.8391 0.2160 1 9 0 -0.0142 0.2231 1 9 1 2.7810 0.2361 1 9 2 0.0134 0.0970 1 9 3 -2.4815 0.2058 1 9 4 -0.7799 -0.0368 1 9 5 1.5192 -0.0752 1 9 6 -0.1434 0.0819 1 9 7 -0.2771 -0.1145 1 9 8 -1.2203 0.0288 1 9 9 -1.7188 0.1545 1 9 10 -0.1693 -0.0818 1 9 11 1.3238 -0.0053 1 9 12 0.3527 -0.1001 1 9 13 -1.1212 -0.0064 1 9 14 -0.5653 -0.0485 1 9 15 0.3211 0.0177 1 9 16 0.9226 0.0814 1 9 17 0.0448 0.0269 1 9 18 0.5746 0.1022 1 10 0 1.6552 0.2451 1 10 1 -0.1005 -0.1834 1 10 2 -1.5593 0.2990 1 10 3 -0.2595 -0.1642 1 10 4 1.5312 -0.0349 1 10 5 0.0746 0.1304 1 10 6 -1.1824 -0.1517 1 10 7 -1.1237 0.1092 1 10 8 -0.9457 0.1112 1 10 9 0.2209 -0.2285 1 10 10 0.6698 0.0797 1 10 11 -0.2625 0.0054 1 10 12 -1.2168 -0.1318 1 10 13 -0.1259 0.1566 1 10 14 0.4218 -0.2845 1 10 15 0.6626 0.1506 1 10 16 0.4077 -0.0064 1 10 17 -0.2827 -0.0126 1 11 0 0.1683 -0.1194 1 11 1 -0.6318 0.1514 1 11 2 0.6152 0.0541 1 11 3 0.8917 0.0444 1 11 4 0.4155 0.0893 1 11 5 -1.1171 -0.1160 1 11 6 -1.2038 0.0545 1 11 7 -0.9633 -0.1348 1 11 8 0.1462 -0.0121 1 11 9 0.6558 0.0088 1 11 10 -0.4970 0.0425 1 11 11 -1.0818 -0.1127 1 11 12 0.0093 -0.0461 1 11 13 0.7515 0.0599 1 11 14 0.0690 -0.1132 1 11 15 0.3727 0.2560 1 11 16 -0.6012 -0.1445 1 12 0 0.7619 0.4154 1 12 1 -0.0748 -0.1117 1 12 2 0.6093 0.1901 1 12 3 -0.1994 -0.0492 1 12 4 0.0555 -0.1250 1 12 5 -0.6677 0.1395 1 12 6 -1.3005 -0.2247 1 12 7 -0.4370 -0.0310 1 12 8 0.3362 0.3069 1 12 9 -0.1318 -0.3572 1 12 10 -0.8899 0.1516 1 12 11 0.0688 -0.1220 1 12 12 0.6326 0.1046 1 12 13 0.0983 0.3713 1 12 14 -0.1514 -0.0906 1 13 0 0.1844 -0.1027 1 13 1 -0.3788 0.0107 1 13 2 0.1162 0.1254 1 13 3 -0.2250 0.0170 1 13 4 0.5393 0.1383 1 13 5 -1.2228 -0.0028 1 13 6 -1.2512 -0.0714 1 13 7 0.0250 0.1739 1 13 8 -0.4485 -0.0769 1 13 9 -0.0966 -0.1259 1 13 10 0.0597 0.3371 1 13 11 0.5299 -0.1381 1 14 0 -0.2064 0.4385 1 14 1 0.0875 0.0996 1 14 2 -0.7948 0.2828 1 14 3 -0.0668 0.0410 1 14 4 -0.0569 0.0156 1 14 5 -1.3162 0.3167 1 14 6 -0.3022 -0.1749 1 14 7 -0.3624 0.0805 1 14 8 -0.3070 0.1325 1 15 0 -0.1617 0.1680 1 15 1 -0.7280 0.0150 1 15 2 -1.1929 0.1140 2 -13 0 0.4404 -0.4388 2 -13 1 0.5068 0.2703 2 -13 2 0.5813 -0.0856 2 -13 3 0.2095 -0.0446 2 -13 4 0.4921 0.3056 2 -13 5 -1.3177 0.1859 2 -13 6 -0.1826 0.2962 2 -13 7 -0.2536 -0.1142 2 -13 8 -0.5101 -0.4195 2 -12 0 1.7541 0.4826 2 -12 1 1.0377 0.3585 2 -12 2 0.4629 -0.1085 2 -12 3 -0.8539 0.1460 2 -12 4 -0.5446 0.0240 2 -12 5 -0.2817 0.0968 2 -12 6 0.6421 -0.0416 2 -12 7 -0.9109 -0.3517 2 -12 8 -0.8057 -0.1387 2 -12 9 -0.5946 0.0765 2 -12 10 -0.4047 0.3533 2 -12 11 0.0659 0.0129 2 -12 12 0.6396 0.0707 2 -11 0 1.4286 -0.1365 2 -11 1 0.4732 -0.2058 2 -11 2 -0.7467 0.1565 2 -11 3 -1.0188 0.0019 2 -11 4 0.6187 0.0840 2 -11 5 0.8749 0.0119 2 -11 6 -0.0405 -0.0581 2 -11 7 -1.0862 0.0161 2 -11 8 -0.9411 -0.0422 2 -11 9 -0.8912 0.0035 2 -11 10 -0.2610 0.0226 2 -11 11 0.8744 0.0467 2 -11 12 1.3007 0.2346 2 -11 13 0.5519 0.0516 2 -11 14 0.8716 0.0733 2 -10 0 0.6661 0.1071 2 -10 1 0.0277 0.4658 2 -10 2 -1.2277 0.0910 2 -10 3 0.5778 0.0069 2 -10 4 1.3978 0.0197 2 -10 5 0.5570 -0.0455 2 -10 6 -0.6106 0.0312 2 -10 7 -1.1374 -0.1496 2 -10 8 -1.5708 -0.0624 2 -10 9 -0.9099 0.0842 2 -10 10 0.9453 0.0844 2 -10 11 2.4564 0.1438 2 -10 12 1.6933 -0.0099 2 -10 13 0.5378 0.0608 2 -10 14 0.4022 0.1139 2 -10 15 -1.0370 0.0046 2 -10 16 0.0711 -0.0996 2 -9 0 -0.5721 0.3169 2 -9 1 -1.0257 -0.2639 2 -9 2 0.0278 0.1019 2 -9 3 2.8131 0.0197 2 -9 4 0.6836 -0.0114 2 -9 5 -0.4933 0.0042 2 -9 6 -1.3368 -0.0406 2 -9 7 -1.6603 0.0756 2 -9 8 -1.1702 0.0421 2 -9 9 1.0079 -0.0347 2 -9 10 3.0660 -0.0225 2 -9 11 2.3817 -0.0129 2 -9 12 0.5823 0.0215 2 -9 13 -0.0606 0.1451 2 -9 14 -0.5392 -0.0236 2 -9 15 -1.1183 0.0046 2 -9 16 0.2398 0.1009 2 -9 17 0.0853 0.1863 2 -9 18 0.8806 -0.2167 2 -8 0 -2.4508 -0.2904 2 -8 1 0.8599 0.4408 2 -8 2 3.6817 0.2541 2 -8 3 2.2145 -0.0325 2 -8 4 -1.5761 -0.0110 2 -8 5 -1.3673 -0.0061 2 -8 6 -1.6038 0.0957 2 -8 7 -0.7907 -0.0634 2 -8 8 1.2788 -0.1250 2 -8 9 2.4468 0.0506 2 -8 10 2.2903 0.0104 2 -8 11 0.5588 0.0543 2 -8 12 0.3418 0.0180 2 -8 13 -0.1324 0.0131 2 -8 14 -0.7829 -0.0261 2 -8 15 -0.4737 0.0847 2 -8 16 0.5685 0.0869 2 -8 17 0.8604 -0.0617 2 -8 18 0.9651 -0.1598 2 -8 19 0.1717 0.1366 2 -7 0 0.3952 0.7393 2 -7 1 4.9919 -0.1402 2 -7 2 2.9234 -0.0019 2 -7 3 -0.9342 0.0251 2 -7 4 -1.8469 -0.0184 2 -7 5 -1.5678 0.0629 2 -7 6 -0.9659 -0.1049 2 -7 7 0.9842 0.0170 2 -7 8 2.5370 0.1522 2 -7 9 1.6763 -0.0193 2 -7 10 1.4751 -0.0446 2 -7 11 0.5889 -0.0225 2 -7 12 0.6080 -0.0271 2 -7 13 -0.7598 0.0494 2 -7 14 -1.0224 -0.0186 2 -7 15 -0.0284 0.0010 2 -7 16 1.3474 -0.0095 2 -7 17 1.7137 0.0351 2 -7 18 0.6823 0.0700 2 -7 19 -0.0124 0.0955 2 -7 20 0.3513 0.2677 2 -6 0 4.5790 -0.5856 2 -6 1 3.8150 0.2001 2 -6 2 -0.7545 0.4080 2 -6 3 -1.4064 -0.0166 2 -6 4 -2.0065 0.0014 2 -6 5 -1.8203 -0.0935 2 -6 6 0.7560 0.0600 2 -6 7 2.6592 0.0968 2 -6 8 3.4303 -0.1164 2 -6 9 1.9362 -0.0461 2 -6 10 1.2533 0.0520 2 -6 11 -0.3953 -0.0077 2 -6 12 -0.9215 0.0403 2 -6 13 -1.7533 -0.0054 2 -6 14 -0.4257 -0.0610 2 -6 15 1.9478 -0.0365 2 -6 16 2.6754 0.0683 2 -6 17 1.0631 0.0839 2 -6 18 -0.3504 -0.0115 2 -6 19 -0.0241 0.0671 2 -6 20 0.7887 0.1991 2 -6 21 0.1867 0.1551 2 -5 0 3.0925 0.8737 2 -5 1 -0.7983 0.2001 2 -5 2 -2.3944 -0.0907 2 -5 3 -1.7612 -0.0105 2 -5 4 -2.2114 -0.0746 2 -5 5 0.8258 0.0603 2 -5 6 3.3040 -0.0478 2 -5 7 4.5186 -0.1065 2 -5 8 3.8942 0.1194 2 -5 9 0.8575 0.0501 2 -5 10 -1.0685 -0.0087 2 -5 11 -2.4169 -0.0484 2 -5 12 -1.7267 0.0128 2 -5 13 -0.0339 0.0037 2 -5 14 2.5375 -0.0426 2 -5 15 2.9960 -0.0070 2 -5 16 0.3247 0.0529 2 -5 17 -0.9005 -0.0023 2 -5 18 -0.1963 -0.0179 2 -5 19 0.2888 -0.0179 2 -5 20 0.4115 0.0888 2 -5 21 -0.4632 0.1095 2 -5 22 0.2903 -0.1639 2 -4 0 -2.5622 -0.4995 2 -4 1 -1.5639 -0.2057 2 -4 2 -2.7993 0.4281 2 -4 3 -2.0217 0.0562 2 -4 4 0.1160 0.0430 2 -4 5 4.1623 -0.0898 2 -4 6 5.2235 -0.0972 2 -4 7 5.5945 0.1664 2 -4 8 2.1636 -0.0357 2 -4 9 -1.7558 -0.0837 2 -4 10 -3.4124 0.0309 2 -4 11 -2.2199 -0.0222 2 -4 12 1.0119 0.0672 2 -4 13 3.1215 -0.0114 2 -4 14 2.0106 -0.0361 2 -4 15 -0.8401 -0.0119 2 -4 16 -1.9052 0.0001 2 -4 17 0.1725 0.0175 2 -4 18 0.3200 -0.0742 2 -4 19 -0.0276 -0.0466 2 -4 20 0.0980 0.0571 2 -4 21 -0.1652 -0.1620 2 -4 22 0.8217 -0.2262 2 -3 0 0.9859 0.6172 2 -3 1 -0.6712 0.5514 2 -3 2 -7.9046 0.0359 2 -3 3 -1.5382 -0.0496 2 -3 4 4.6489 -0.0810 2 -3 5 9.2265 0.0008 2 -3 6 8.0149 0.0737 2 -3 7 3.9776 -0.0914 2 -3 8 -2.5201 0.0044 2 -3 9 -4.8722 0.0757 2 -3 10 -2.8380 -0.0254 2 -3 11 1.9359 -0.0183 2 -3 12 3.7187 -0.0035 2 -3 13 1.2540 -0.0016 2 -3 14 -2.0760 -0.0162 2 -3 15 -2.0583 -0.0034 2 -3 16 0.0315 0.0191 2 -3 17 1.0435 -0.0220 2 -3 18 -0.0867 -0.0683 2 -3 19 0.0318 0.0083 2 -3 20 -0.0670 -0.0662 2 -3 21 0.5985 -0.1063 2 -3 22 1.2761 0.2411 2 -3 23 0.1979 0.2859 2 -2 0 1.8838 0.0009 2 -2 1 -14.6895 -0.5050 2 -2 2 -10.7963 0.2835 2 -2 3 10.5227 0.0721 2 -2 4 15.9239 0.1843 2 -2 5 13.5602 0.0260 2 -2 6 3.7749 -0.1310 2 -2 7 -4.8897 0.0918 2 -2 8 -7.4010 0.0225 2 -2 9 -2.9302 -0.1270 2 -2 10 3.1140 0.0337 2 -2 11 5.0409 -0.0247 2 -2 12 0.9642 0.0236 2 -2 13 -2.3443 0.0133 2 -2 14 -2.0728 -0.0265 2 -2 15 0.1566 0.0212 2 -2 16 1.1242 -0.0398 2 -2 17 0.5794 0.0384 2 -2 18 -0.2521 0.0217 2 -2 19 -0.0907 0.0361 2 -2 20 0.5411 0.0119 2 -2 21 1.4900 0.1211 2 -2 22 0.5957 0.1584 2 -2 23 -0.2313 -0.2079 2 -1 0 -22.8465 -0.0814 2 -1 1 -18.7786 0.7324 2 -1 2 14.6146 0.2146 2 -1 3 30.3213 0.1006 2 -1 4 15.7960 -0.0405 2 -1 5 2.4778 -0.1685 2 -1 6 -8.6540 0.1454 2 -1 7 -9.4841 -0.0609 2 -1 8 -1.8252 -0.0629 2 -1 9 4.5036 0.0972 2 -1 10 6.2629 0.0294 2 -1 11 1.4277 -0.0655 2 -1 12 -2.6056 0.0151 2 -1 13 -1.7786 -0.0296 2 -1 14 0.0960 0.0217 2 -1 15 1.3004 -0.0243 2 -1 16 0.8563 0.0589 2 -1 17 -0.3104 0.0790 2 -1 18 -0.2734 -0.0138 2 -1 19 0.6373 0.0635 2 -1 20 1.0846 0.0095 2 -1 21 0.3733 -0.0004 2 -1 22 -0.2955 -0.1214 2 -1 23 -0.0780 -0.0678 2 0 0 -27.2705 0.7650 2 0 1 20.8022 -0.5097 2 0 2 40.8885 0.1262 2 0 3 19.5939 0.0115 2 0 4 -4.5214 -0.0211 2 0 5 -9.4375 0.2123 2 0 6 -8.6499 -0.0719 2 0 7 -0.2083 0.0281 2 0 8 5.9055 0.1101 2 0 9 5.3048 -0.1022 2 0 10 2.1334 -0.0199 2 0 11 -2.4029 0.0046 2 0 12 -1.7466 0.0253 2 0 13 0.0675 0.0340 2 0 14 1.2254 -0.0222 2 0 15 1.1533 0.0180 2 0 16 -0.3593 0.0302 2 0 17 -0.7231 -0.0669 2 0 18 0.8131 0.0269 2 0 19 0.8067 0.0197 2 0 20 0.2126 -0.0435 2 0 21 -0.5584 -0.0614 2 0 22 -0.1526 -0.0076 2 0 23 -0.1499 0.1148 2 1 0 19.7477 -0.8137 2 1 1 48.7238 0.5480 2 1 2 18.2326 0.4175 2 1 3 -8.2627 0.0127 2 1 4 -10.7458 0.1705 2 1 5 -3.8942 -0.2290 2 1 6 1.8205 0.0729 2 1 7 5.3918 0.0537 2 1 8 4.0065 -0.1431 2 1 9 1.4823 0.1025 2 1 10 -1.0992 0.0810 2 1 11 -1.6379 0.0029 2 1 12 -0.3471 0.0040 2 1 13 0.9345 -0.0157 2 1 14 1.4861 -0.0482 2 1 15 -0.1096 0.0021 2 1 16 -0.9383 -0.0717 2 1 17 0.0919 0.0304 2 1 18 1.6688 0.0183 2 1 19 0.2345 -0.0244 2 1 20 -0.4262 -0.0098 2 1 21 -1.1752 -0.0171 2 1 22 0.1674 0.0361 2 1 23 0.2121 0.0191 2 2 0 45.7207 1.1895 2 2 1 17.3038 0.0815 2 2 2 -11.7669 -0.1530 2 2 3 -7.5030 0.0573 2 2 4 -1.6453 -0.2817 2 2 5 3.1583 0.1251 2 2 6 4.8690 0.1040 2 2 7 2.6387 -0.0526 2 2 8 1.6340 0.1889 2 2 9 -0.3500 -0.0113 2 2 10 -1.6307 -0.0686 2 2 11 -0.2558 -0.0133 2 2 12 0.3462 -0.0237 2 2 13 1.9834 0.0422 2 2 14 0.3437 -0.0469 2 2 15 -0.9742 0.0298 2 2 16 -0.0281 -0.0229 2 2 17 1.4635 0.0294 2 2 18 1.9047 -0.0416 2 2 19 -1.2096 0.0511 2 2 20 -1.2563 0.0052 2 2 21 -0.6272 -0.0004 2 2 22 1.3643 -0.0050 2 2 23 -0.1157 0.0073 2 3 0 14.9879 -0.7240 2 3 1 -11.3527 -0.1227 2 3 2 -5.4684 0.4026 2 3 3 0.7125 -0.1185 2 3 4 0.3784 0.1599 2 3 5 5.1388 -0.0006 2 3 6 3.6720 -0.0447 2 3 7 1.4834 0.1728 2 3 8 0.0630 -0.1885 2 3 9 -1.9784 -0.0142 2 3 10 -0.4913 0.0529 2 3 11 1.7313 -0.0280 2 3 12 1.4724 0.0785 2 3 13 0.9388 -0.0028 2 3 14 -0.8462 0.0039 2 3 15 0.2947 0.0149 2 3 16 1.6997 -0.0517 2 3 17 1.6593 0.0440 2 3 18 -0.0679 0.0032 2 3 19 -2.3778 0.0640 2 3 20 0.0621 -0.0160 2 3 21 0.8688 0.0135 2 3 22 0.7470 -0.0925 2 3 23 -1.0933 -0.0650 2 4 0 -7.5193 0.5848 2 4 1 -5.2508 0.5571 2 4 2 0.4910 -0.1798 2 4 3 -1.4802 0.0489 2 4 4 3.9688 -0.2077 2 4 5 6.5307 -0.1014 2 4 6 1.3684 0.2086 2 4 7 -1.2170 -0.1508 2 4 8 -1.9829 0.0910 2 4 9 0.0133 0.1237 2 4 10 2.7757 -0.1280 2 4 11 2.4457 0.0389 2 4 12 -0.4112 -0.0114 2 4 13 -0.4211 0.0138 2 4 14 1.0083 0.0236 2 4 15 1.7352 -0.0334 2 4 16 1.5172 0.0534 2 4 17 -0.2347 -0.0204 2 4 18 -1.0895 0.0091 2 4 19 -0.8345 0.0266 2 4 20 1.4380 0.0261 2 4 21 0.1327 -0.0824 2 4 22 -0.5580 -0.1754 2 4 23 -0.3597 0.1805 2 5 0 -4.9736 -0.2744 2 5 1 -1.6766 -0.3806 2 5 2 -1.8976 0.1314 2 5 3 3.3632 -0.0553 2 5 4 7.4738 -0.0236 2 5 5 1.5716 0.1702 2 5 6 -3.2515 -0.0689 2 5 7 -1.9757 0.1121 2 5 8 1.3519 0.0096 2 5 9 3.6592 -0.1441 2 5 10 2.3621 0.0592 2 5 11 -1.2946 -0.0568 2 5 12 -1.4913 0.0424 2 5 13 1.7960 0.0240 2 5 14 2.7194 -0.0027 2 5 15 0.8239 0.0640 2 5 16 0.4311 -0.0644 2 5 17 -1.0072 -0.0364 2 5 18 -0.3087 0.0410 2 5 19 0.2153 -0.0096 2 5 20 0.4509 0.0193 2 5 21 -0.9824 -0.1951 2 5 22 0.3002 0.1504 2 6 0 -3.8865 -0.1298 2 6 1 -1.4604 0.6704 2 6 2 2.6824 -0.0326 2 6 3 6.6358 0.0999 2 6 4 1.3519 -0.0913 2 6 5 -4.0789 -0.1611 2 6 6 -1.9078 0.1405 2 6 7 2.3128 -0.0661 2 6 8 3.9920 -0.0420 2 6 9 1.5557 0.1781 2 6 10 -2.5618 -0.0906 2 6 11 -2.3549 -0.0031 2 6 12 2.3045 0.0439 2 6 13 3.6032 -0.0385 2 6 14 1.6859 0.0987 2 6 15 -0.7513 -0.0491 2 6 16 -0.1152 -0.0655 2 6 17 -1.1570 0.0539 2 6 18 0.1665 -0.0784 2 6 19 -0.2170 0.0312 2 6 20 -0.5950 -0.0122 2 6 21 0.4717 0.0005 2 6 22 1.6092 0.2990 2 7 0 -2.3011 0.3189 2 7 1 2.3609 -0.2581 2 7 2 4.8444 -0.0262 2 7 3 1.1007 -0.0180 2 7 4 -3.7047 -0.1748 2 7 5 -1.5648 0.1719 2 7 6 2.4901 -0.0216 2 7 7 3.2951 0.0457 2 7 8 0.9267 0.1298 2 7 9 -3.1889 -0.0833 2 7 10 -2.7479 0.0029 2 7 11 2.5973 0.0365 2 7 12 4.4751 -0.0553 2 7 13 1.3723 0.0900 2 7 14 -1.0171 -0.0477 2 7 15 -1.3974 0.0470 2 7 16 0.0599 -0.0390 2 7 17 -0.7021 0.0178 2 7 18 0.2130 -0.0940 2 7 19 -0.5345 0.0999 2 7 20 0.4864 -0.0059 2 7 21 1.4534 0.0519 2 8 0 1.5734 -0.5908 2 8 1 3.6635 0.4642 2 8 2 0.8343 0.1016 2 8 3 -3.5826 0.0648 2 8 4 -0.7608 0.0235 2 8 5 2.4270 -0.1725 2 8 6 2.4287 0.1068 2 8 7 0.3270 0.0195 2 8 8 -2.3701 -0.1057 2 8 9 -2.2784 0.1693 2 8 10 2.0759 -0.0330 2 8 11 4.2194 -0.0341 2 8 12 0.8714 0.0346 2 8 13 -1.8888 -0.0369 2 8 14 -1.1867 0.0334 2 8 15 0.4226 0.1115 2 8 16 0.3739 -0.1316 2 8 17 -0.4987 0.1524 2 8 18 -0.1374 -0.1943 2 8 19 0.0222 0.1299 2 8 20 0.2819 -0.1374 2 9 0 3.1284 0.5959 2 9 1 -0.1562 0.0597 2 9 2 -2.8656 -0.0785 2 9 3 -0.7100 -0.0228 2 9 4 3.4628 -0.2662 2 9 5 1.4067 0.1005 2 9 6 -0.3476 0.0618 2 9 7 -1.4136 -0.0808 2 9 8 -0.9116 0.1466 2 9 9 1.4017 -0.0352 2 9 10 2.6575 -0.0720 2 9 11 0.6722 0.0557 2 9 12 -1.9002 -0.0531 2 9 13 -0.6822 0.0236 2 9 14 1.0954 0.0427 2 9 15 0.7642 0.0199 2 9 16 -0.7450 0.0328 2 9 17 -0.6922 0.1045 2 9 18 -0.3392 -0.2687 2 9 19 -0.1570 0.0905 2 10 0 -0.1074 -0.6163 2 10 1 -2.3909 0.1221 2 10 2 0.2918 0.0884 2 10 3 3.1115 -0.0276 2 10 4 1.2390 0.1244 2 10 5 -1.7426 -0.1185 2 10 6 -0.9035 -0.0012 2 10 7 0.2531 0.0767 2 10 8 1.5477 -0.1564 2 10 9 1.7078 0.0832 2 10 10 0.2246 0.0066 2 10 11 -1.1035 -0.0515 2 10 12 -0.4163 0.1113 2 10 13 1.0630 -0.1856 2 10 14 0.5792 0.1234 2 10 15 -0.6021 0.0766 2 10 16 -1.2144 0.0981 2 10 17 -0.2394 0.0055 2 10 18 -0.0568 -0.3197 2 11 0 -0.8500 0.3683 2 11 1 0.5781 0.3386 2 11 2 2.0039 -0.0635 2 11 3 0.5464 0.1226 2 11 4 -1.9152 -0.2584 2 11 5 -0.8817 -0.0368 2 11 6 0.5119 0.1398 2 11 7 1.8278 -0.0891 2 11 8 2.0284 0.0387 2 11 9 0.2022 0.1130 2 11 10 -1.2304 -0.1413 2 11 11 -0.2522 0.1641 2 11 12 0.5689 -0.0764 2 11 13 0.1138 -0.1630 2 11 14 -0.0883 0.3192 2 11 15 -0.7242 -0.1922 2 11 16 -0.2920 0.2684 2 11 17 0.5407 -0.2527 2 12 0 0.3365 -0.2574 2 12 1 0.8251 -0.0890 2 12 2 -0.2328 0.1169 2 12 3 -0.7834 -0.0331 2 12 4 -0.6094 0.0765 2 12 5 0.1657 0.0261 2 12 6 0.9627 -0.0286 2 12 7 2.5699 0.1484 2 12 8 0.6619 -0.1390 2 12 9 -1.3722 0.1469 2 12 10 -0.5164 -0.0163 2 12 11 0.5863 0.0787 2 12 12 -0.2003 -0.0622 2 12 13 -0.0312 -0.1285 2 12 14 0.2928 0.0237 2 12 15 -0.2821 -0.1180 2 13 0 -0.2175 -0.0712 2 13 1 0.1831 0.4497 2 13 2 -0.6935 0.0590 2 13 3 0.2529 0.1442 2 13 4 -0.3016 -0.1060 2 13 5 0.2677 -0.1974 2 13 6 2.0204 0.2212 2 13 7 1.1005 -0.0779 2 13 8 -0.8584 -0.0399 2 13 9 -0.3207 0.3169 2 13 10 0.5765 -0.2417 2 13 11 -0.2003 0.2468 2 13 12 -0.4007 -0.3373 2 13 13 0.4263 -0.2615 2 14 0 0.0227 0.0937 2 14 1 -0.4488 -0.1081 2 14 2 -0.5575 -0.0628 2 14 3 0.7535 -0.0404 2 14 4 0.1424 -0.0607 2 14 5 1.4811 -0.0738 2 14 6 0.8031 0.0431 2 14 7 -0.5048 -0.0519 2 14 8 0.4118 0.0962 2 14 9 0.3103 0.1340 2 14 10 -0.1281 -0.1725 2 15 0 -0.2850 -0.6573 2 15 1 -0.9312 0.1268 2 15 2 0.9399 0.0597 2 15 3 1.1528 0.2069 2 15 4 0.6256 -0.2331 2 15 5 0.6220 -0.3464 3 -13 0 -0.1551 0.0121 3 -13 1 -0.0212 0.2414 3 -13 2 0.2263 0.1990 3 -13 3 0.2979 0.2973 3 -13 4 -0.9681 -0.2405 3 -13 5 0.1530 -0.4156 3 -12 0 -0.7678 0.3865 3 -12 1 -0.4161 -0.4606 3 -12 2 -0.8713 0.0580 3 -12 3 -0.0437 -0.0846 3 -12 4 -0.0031 -0.2788 3 -12 5 1.4548 -0.0684 3 -12 6 0.1759 0.0140 3 -12 7 -0.4981 0.3776 3 -12 8 -0.6547 0.2565 3 -12 9 0.4876 0.0569 3 -12 10 0.9143 -0.3145 3 -11 0 -1.4602 -0.6442 3 -11 1 -0.7075 0.2042 3 -11 2 -0.7668 0.3674 3 -11 3 0.9377 0.0231 3 -11 4 0.5768 -0.0524 3 -11 5 0.6319 -0.0902 3 -11 6 -0.9114 0.0806 3 -11 7 -0.7932 0.1252 3 -11 8 0.0862 -0.0339 3 -11 9 1.2906 -0.0270 3 -11 10 1.0032 -0.1774 3 -11 11 -0.0279 0.0525 3 -11 12 -0.5349 -0.1463 3 -11 13 0.2000 -0.1472 3 -10 0 -1.0931 0.6614 3 -10 1 -0.7061 0.1060 3 -10 2 -0.2863 -0.1542 3 -10 3 1.0669 -0.0164 3 -10 4 -0.2857 -0.1497 3 -10 5 -0.5440 0.0133 3 -10 6 -0.7493 0.0070 3 -10 7 -0.2011 0.1059 3 -10 8 0.8845 0.1438 3 -10 9 1.4795 -0.0337 3 -10 10 1.2048 -0.0727 3 -10 11 -0.5256 -0.0752 3 -10 12 -1.1342 -0.1977 3 -10 13 -0.7081 -0.0055 3 -10 14 -1.6017 0.0938 3 -10 15 0.0967 0.0582 3 -9 0 -1.1395 -0.6930 3 -9 1 -0.4548 -0.1180 3 -9 2 1.3012 0.3223 3 -9 3 -0.0410 0.1439 3 -9 4 -1.7025 -0.0535 3 -9 5 -0.4918 -0.0660 3 -9 6 0.2379 0.0136 3 -9 7 0.4039 0.1240 3 -9 8 1.7975 -0.0402 3 -9 9 1.6490 -0.0115 3 -9 10 -0.3191 0.0343 3 -9 11 -2.7432 -0.0318 3 -9 12 -1.6976 0.0085 3 -9 13 -0.8151 0.0187 3 -9 14 -0.6946 0.0049 3 -9 15 0.9840 -0.0519 3 -9 16 -0.2305 0.0825 3 -9 17 0.4040 0.0065 3 -8 0 0.6846 0.5128 3 -8 1 1.9127 0.4823 3 -8 2 0.3811 -0.0879 3 -8 3 -3.2098 -0.1047 3 -8 4 -1.1667 -0.1974 3 -8 5 0.6539 0.0055 3 -8 6 1.1212 0.0605 3 -8 7 1.6102 0.0126 3 -8 8 1.6037 0.1253 3 -8 9 -1.0720 0.0757 3 -8 10 -3.0861 0.0159 3 -8 11 -2.3626 -0.0243 3 -8 12 -0.4090 -0.0233 3 -8 13 -0.2373 -0.0458 3 -8 14 0.2906 -0.0182 3 -8 15 0.6201 0.0482 3 -8 16 -0.4307 0.0754 3 -8 17 0.2699 -0.0288 3 -8 18 -0.4993 0.2710 3 -8 19 0.0780 0.1753 3 -7 0 2.8726 -0.4201 3 -7 1 -0.2853 -0.4158 3 -7 2 -3.4668 0.1600 3 -7 3 -2.3822 0.1344 3 -7 4 0.8318 0.0398 3 -7 5 0.9853 -0.0222 3 -7 6 2.1977 -0.0512 3 -7 7 1.3413 0.0939 3 -7 8 -1.3346 0.0013 3 -7 9 -2.9357 -0.0541 3 -7 10 -2.2134 0.0443 3 -7 11 -0.4962 -0.0114 3 -7 12 -0.3766 0.0437 3 -7 13 0.0112 -0.0187 3 -7 14 0.3269 0.0371 3 -7 15 0.0044 0.0477 3 -7 16 -0.1443 0.0066 3 -7 17 -0.3382 0.0792 3 -7 18 -0.5856 0.0835 3 -7 19 -0.0205 -0.0831 3 -7 20 -0.2339 -0.1624 3 -6 0 -0.8109 0.0055 3 -6 1 -4.0424 0.7646 3 -6 2 -2.1692 0.1171 3 -6 3 0.2248 -0.0718 3 -6 4 0.8673 -0.2337 3 -6 5 1.9037 -0.1392 3 -6 6 2.1427 0.1031 3 -6 7 -0.7803 0.0069 3 -6 8 -2.7158 0.0081 3 -6 9 -2.1351 0.0709 3 -6 10 -1.4622 0.0034 3 -6 11 -0.5008 -0.0048 3 -6 12 -0.4460 0.0061 3 -6 13 0.7965 -0.0225 3 -6 14 0.6302 0.0260 3 -6 15 0.1700 0.0041 3 -6 16 -0.9248 0.0640 3 -6 17 -1.4949 -0.0122 3 -6 18 -0.2171 -0.0742 3 -6 19 0.0565 -0.0436 3 -6 20 -0.4417 -0.2084 3 -6 21 -0.6675 -0.2376 3 -5 0 -4.6170 0.2227 3 -5 1 -2.2987 -0.4792 3 -5 2 0.7319 -0.0945 3 -5 3 1.1321 0.0494 3 -5 4 2.2434 0.0067 3 -5 5 2.0386 0.1254 3 -5 6 -0.1683 0.0016 3 -5 7 -2.4654 0.0177 3 -5 8 -2.8357 -0.0087 3 -5 9 -2.0089 -0.0556 3 -5 10 -1.4473 -0.0337 3 -5 11 0.1640 -0.0005 3 -5 12 1.1330 0.0423 3 -5 13 2.0429 0.0079 3 -5 14 0.2681 -0.0135 3 -5 15 -1.7464 0.0319 3 -5 16 -2.1791 0.0014 3 -5 17 -0.4227 -0.0564 3 -5 18 0.6245 0.0200 3 -5 19 -0.3537 -0.0444 3 -5 20 -0.6383 -0.1556 3 -5 21 0.1876 -0.2081 3 -5 22 0.6780 -0.2434 3 -4 0 -1.9843 -0.6607 3 -4 1 1.4132 0.6614 3 -4 2 2.1028 0.3406 3 -4 3 2.9346 0.0386 3 -4 4 2.1997 -0.0951 3 -4 5 -1.0381 -0.2027 3 -4 6 -2.3540 0.0271 3 -4 7 -3.2915 0.0223 3 -4 8 -2.7141 -0.0039 3 -4 9 -1.9323 0.0787 3 -4 10 -0.1131 -0.0414 3 -4 11 2.2310 0.0400 3 -4 12 2.5297 0.0030 3 -4 13 0.5436 -0.0654 3 -4 14 -2.3896 0.0026 3 -4 15 -2.1714 -0.0056 3 -4 16 0.3547 0.0127 3 -4 17 0.9200 0.0305 3 -4 18 0.0651 0.0263 3 -4 19 -0.3997 -0.0080 3 -4 20 -0.0530 -0.0657 3 -4 21 0.8008 -0.1545 3 -4 22 -0.1080 0.1539 3 -3 0 2.6881 0.8191 3 -3 1 0.6947 -0.2096 3 -3 2 3.3690 -0.3024 3 -3 3 3.3270 -0.0450 3 -3 4 -0.3356 -0.1149 3 -3 5 -3.1627 0.1240 3 -3 6 -3.4551 0.1243 3 -3 7 -4.4269 0.0346 3 -3 8 -2.7230 0.0606 3 -3 9 -0.3560 -0.0721 3 -3 10 2.9994 -0.0542 3 -3 11 3.0183 0.0172 3 -3 12 0.0701 -0.0434 3 -3 13 -2.4797 0.0227 3 -3 14 -1.3974 0.0077 3 -3 15 1.0953 0.0103 3 -3 16 1.5680 0.0261 3 -3 17 -0.1112 -0.0197 3 -3 18 -0.1079 0.0718 3 -3 19 -0.3047 0.0778 3 -3 20 0.1317 -0.0258 3 -3 21 0.2893 0.0741 3 -3 22 -1.2309 0.3126 3 -3 23 -0.5397 -0.1061 3 -2 0 -2.0361 -1.1253 3 -2 1 0.7263 0.1851 3 -2 2 7.7090 0.3890 3 -2 3 1.7495 0.1484 3 -2 4 -2.9743 0.0520 3 -2 5 -5.7909 -0.1307 3 -2 6 -6.4756 -0.0487 3 -2 7 -5.0687 -0.0082 3 -2 8 0.5988 -0.0402 3 -2 9 4.0535 0.0667 3 -2 10 3.7903 0.0020 3 -2 11 -0.9774 0.0119 3 -2 12 -3.1534 0.0312 3 -2 13 -0.9699 -0.0139 3 -2 14 1.8267 0.0048 3 -2 15 1.5717 -0.0119 3 -2 16 0.1509 -0.0218 3 -2 17 -0.7420 0.0396 3 -2 18 -0.0776 0.1021 3 -2 19 -0.3510 0.0062 3 -2 20 -0.1366 -0.0331 3 -2 21 -1.2634 0.0874 3 -2 22 -1.2888 -0.0889 3 -2 23 0.1053 -0.2299 3 -1 0 -1.6903 0.9540 3 -1 1 11.3505 0.3364 3 -1 2 7.6269 -0.2615 3 -1 3 -6.2489 -0.0604 3 -1 4 -8.2574 -0.3141 3 -1 5 -9.3630 0.0069 3 -1 6 -6.2018 0.0960 3 -1 7 1.0564 0.0291 3 -1 8 6.2602 0.1108 3 -1 9 4.0301 -0.0015 3 -1 10 -1.6593 -0.0765 3 -1 11 -4.9816 0.0611 3 -1 12 -1.3943 -0.0477 3 -1 13 1.9896 0.0352 3 -1 14 1.8580 0.0224 3 -1 15 0.1421 -0.0180 3 -1 16 -1.0652 0.0146 3 -1 17 -0.6054 -0.0407 3 -1 18 0.3168 -0.0388 3 -1 19 -0.8216 -0.0644 3 -1 20 -1.3941 -0.0193 3 -1 21 -1.1962 -0.0597 3 -1 22 0.2195 -0.0885 3 -1 23 -0.1063 0.2608 3 0 0 15.7397 -0.8661 3 0 1 11.6830 -0.2973 3 0 2 -8.4952 0.2735 3 0 3 -15.3762 -0.0369 3 0 4 -8.4669 0.1183 3 0 5 -6.0088 0.0352 3 0 6 1.4896 -0.0990 3 0 7 6.9222 0.0222 3 0 8 3.7649 -0.0799 3 0 9 -2.2107 0.0267 3 0 10 -5.8439 0.0257 3 0 11 -2.6570 0.0225 3 0 12 1.8515 0.0191 3 0 13 2.0091 0.0378 3 0 14 0.7327 -0.0438 3 0 15 -1.2228 -0.0022 3 0 16 -1.2723 -0.0896 3 0 17 0.4934 -0.0684 3 0 18 -0.1437 -0.0087 3 0 19 -1.6013 0.0164 3 0 20 -0.8902 -0.0045 3 0 21 -0.1367 -0.0153 3 0 22 0.0940 0.1656 3 0 23 -0.1586 0.1559 3 0 24 0.4137 -0.1693 3 1 0 17.4404 0.5360 3 1 1 -12.0423 0.7868 3 1 2 -19.7196 -0.2753 3 1 3 -9.1589 -0.0075 3 1 4 -1.5838 -0.2195 3 1 5 0.3139 -0.1754 3 1 6 5.2223 0.0983 3 1 7 2.9769 -0.0314 3 1 8 -2.6213 0.1068 3 1 9 -5.0353 0.0302 3 1 10 -3.3002 -0.0868 3 1 11 1.0991 0.0479 3 1 12 2.1892 -0.0386 3 1 13 1.4331 -0.0489 3 1 14 -0.4614 0.0214 3 1 15 -1.9299 0.0011 3 1 16 -0.1174 0.0136 3 1 17 0.8525 0.0216 3 1 18 -0.7664 0.0037 3 1 19 -1.2280 0.0439 3 1 20 -0.9277 -0.0169 3 1 21 -0.0574 0.0475 3 1 22 0.8926 0.0179 3 1 23 0.4749 -0.0870 3 1 24 -0.2863 -0.1001 3 2 0 -9.0252 -0.0825 3 2 1 -23.4849 -0.7262 3 2 2 -6.4753 0.0522 3 2 3 -0.0776 -0.0661 3 2 4 -0.0016 -0.0580 3 2 5 1.6846 0.2284 3 2 6 1.9015 -0.0843 3 2 7 -1.5672 0.0142 3 2 8 -4.4283 -0.0650 3 2 9 -3.3666 -0.1131 3 2 10 0.5196 0.0512 3 2 11 2.0714 -0.0271 3 2 12 2.4562 0.0145 3 2 13 0.0364 0.0259 3 2 14 -1.8018 0.0669 3 2 15 -0.9408 0.0306 3 2 16 0.8709 0.0362 3 2 17 0.4627 -0.0677 3 2 18 -1.7780 0.0253 3 2 19 -1.6825 0.0039 3 2 20 -0.3396 -0.0426 3 2 21 1.7664 -0.0409 3 2 22 0.7362 -0.0646 3 2 23 -0.9041 0.0008 3 2 24 -0.4308 0.0259 3 3 0 -20.3276 -0.3420 3 3 1 -6.2378 0.8247 3 3 2 2.6638 -0.0488 3 3 3 -3.1694 -0.1643 3 3 4 0.4161 0.0230 3 3 5 1.6788 -0.2283 3 3 6 -0.9679 0.0020 3 3 7 -3.4946 -0.0292 3 3 8 -4.5276 0.0097 3 3 9 -0.0252 0.0864 3 3 10 3.1734 -0.0848 3 3 11 2.1268 0.0644 3 3 12 0.7312 0.0402 3 3 13 -2.5487 -0.0534 3 3 14 -0.5770 0.0378 3 3 15 0.1783 -0.0450 3 3 16 0.3229 0.0122 3 3 17 -1.2355 -0.0451 3 3 18 -2.5517 0.0242 3 3 19 0.1573 -0.0746 3 3 20 1.2913 -0.0443 3 3 21 1.0187 -0.0413 3 3 22 -1.3228 0.0294 3 3 23 -0.4300 0.0399 3 4 0 -5.3896 0.6916 3 4 1 2.3558 -0.6317 3 4 2 -2.6291 -0.3526 3 4 3 -1.1245 -0.0179 3 4 4 3.7668 -0.1357 3 4 5 -1.3896 0.2076 3 4 6 -4.5151 0.0469 3 4 7 -4.2115 -0.0009 3 4 8 -0.8891 0.0516 3 4 9 3.9039 -0.1893 3 4 10 2.6241 0.0572 3 4 11 -1.2877 0.0363 3 4 12 -2.0474 -0.0763 3 4 13 -1.1986 0.0205 3 4 14 0.8659 -0.0447 3 4 15 -0.6831 0.0200 3 4 16 -0.9736 0.0042 3 4 17 -1.9329 -0.0482 3 4 18 -0.8155 -0.0390 3 4 19 1.5233 -0.0472 3 4 20 -0.0729 -0.0130 3 4 21 -0.6176 -0.0116 3 4 22 -0.7255 0.0803 3 4 23 0.6305 -0.0289 3 5 0 1.4747 -0.9576 3 5 1 -1.2093 0.3360 3 5 2 0.3610 0.2822 3 5 3 3.6559 -0.1273 3 5 4 -1.3014 0.1733 3 5 5 -6.4419 -0.1081 3 5 6 -3.4366 -0.1193 3 5 7 0.5811 0.0196 3 5 8 2.9380 -0.0956 3 5 9 2.1965 0.0891 3 5 10 -2.3701 -0.0266 3 5 11 -3.1849 -0.0276 3 5 12 0.2297 0.0840 3 5 13 0.7679 -0.0555 3 5 14 -0.4206 -0.0015 3 5 15 -1.3776 0.0049 3 5 16 -2.0056 -0.0630 3 5 17 -1.2713 -0.0063 3 5 18 0.5172 -0.0541 3 5 19 0.7281 0.0339 3 5 20 -1.1700 -0.0757 3 5 21 0.1146 0.1157 3 5 22 0.2050 0.0299 3 5 23 -0.0082 -0.1983 3 6 0 1.1185 1.0292 3 6 1 0.8348 -0.0483 3 6 2 3.3228 -0.4230 3 6 3 -2.1477 -0.0867 3 6 4 -6.3578 -0.1447 3 6 5 -2.4643 -0.0028 3 6 6 2.2396 0.1023 3 6 7 2.5857 0.0105 3 6 8 0.0869 0.1096 3 6 9 -2.5838 -0.1233 3 6 10 -2.9028 -0.0574 3 6 11 1.1419 0.1593 3 6 12 1.8186 -0.0906 3 6 13 -0.8394 0.0325 3 6 14 -2.2266 -0.0141 3 6 15 -2.1378 -0.0717 3 6 16 -2.2321 0.0440 3 6 17 1.0390 -0.0569 3 6 18 1.0059 0.0259 3 6 19 -0.3855 -0.0032 3 6 20 -0.5612 0.0244 3 6 21 0.8332 0.2053 3 6 22 -0.5764 -0.2635 3 7 0 2.4007 -0.8706 3 7 1 0.9866 -0.3070 3 7 2 -1.1861 0.2522 3 7 3 -5.6704 -0.1086 3 7 4 -1.1439 0.1798 3 7 5 3.0277 0.0396 3 7 6 1.9645 -0.0995 3 7 7 -0.7376 0.0396 3 7 8 -3.1236 -0.1117 3 7 9 -1.3829 -0.0183 3 7 10 2.0555 0.0991 3 7 11 2.3645 -0.0799 3 7 12 -1.6235 0.0592 3 7 13 -3.0219 0.0090 3 7 14 -2.6394 -0.0908 3 7 15 -0.7530 0.0249 3 7 16 0.3460 0.0429 3 7 17 2.3707 -0.0792 3 7 18 -0.6681 0.0985 3 7 19 -0.6009 -0.0060 3 7 20 0.2975 0.1824 3 7 21 -0.1938 -0.0991 3 7 22 -0.9382 -0.3743 3 8 0 1.4433 0.6426 3 8 1 -1.4761 0.3806 3 8 2 -3.5421 -0.2713 3 8 3 -1.1583 -0.0869 3 8 4 3.3730 -0.0851 3 8 5 1.4025 -0.0960 3 8 6 -1.4438 0.0317 3 8 7 -2.4284 -0.0263 3 8 8 -0.8956 0.0907 3 8 9 2.8063 -0.0280 3 8 10 2.0862 -0.0893 3 8 11 -1.8888 0.0612 3 8 12 -3.6472 -0.0038 3 8 13 -1.5252 -0.1085 3 8 14 0.1802 0.0873 3 8 15 1.1245 -0.0167 3 8 16 0.5434 0.1044 3 8 17 0.5702 -0.1603 3 8 18 -1.2119 0.1825 3 8 19 0.2340 -0.0513 3 8 20 -0.0489 0.0689 3 8 21 -0.3075 -0.2789 3 9 0 -0.6067 -0.2765 3 9 1 -2.6943 -0.6355 3 9 2 -0.8704 0.0672 3 9 3 2.9162 -0.0981 3 9 4 0.8475 0.0900 3 9 5 -2.3349 0.1178 3 9 6 -2.1023 -0.1375 3 9 7 0.2065 0.1048 3 9 8 2.2539 -0.0514 3 9 9 1.6373 -0.1022 3 9 10 -1.7056 0.1063 3 9 11 -3.1355 -0.1265 3 9 12 -0.8091 0.0111 3 9 13 1.3029 0.0505 3 9 14 0.5299 0.0681 3 9 15 -0.4616 0.0222 3 9 16 -0.1023 0.0271 3 9 17 0.4727 -0.2190 3 9 18 -0.0589 0.1816 3 9 19 0.1795 -0.2220 3 9 20 0.2527 0.2228 3 10 0 -2.1597 -0.0294 3 10 1 -0.4134 0.5006 3 10 2 2.0473 -0.0527 3 10 3 0.3299 -0.0723 3 10 4 -3.3981 -0.0304 3 10 5 -1.7174 -0.1299 3 10 6 1.1317 0.0472 3 10 7 2.2632 0.0359 3 10 8 0.6601 0.0219 3 10 9 -1.6542 0.0246 3 10 10 -2.4522 -0.1090 3 10 11 -0.7669 0.0308 3 10 12 1.4701 0.0951 3 10 13 0.4759 -0.0094 3 10 14 -0.9019 0.1055 3 10 15 -0.3057 -0.0299 3 10 16 1.1173 -0.0550 3 10 17 0.7769 -0.2186 3 10 18 -0.0173 0.0811 3 10 19 -0.1414 0.0824 3 11 0 -0.6848 0.4263 3 11 1 1.5107 -0.5314 3 11 2 -0.1879 -0.1419 3 11 3 -3.0205 -0.1355 3 11 4 -1.3266 -0.0219 3 11 5 1.5489 0.2530 3 11 6 1.8718 -0.0641 3 11 7 0.4026 0.0511 3 11 8 -1.9447 0.0385 3 11 9 -2.6743 -0.1843 3 11 10 -0.7049 0.1688 3 11 11 1.1960 -0.0109 3 11 12 1.0351 -0.0378 3 11 13 -0.2472 0.2029 3 11 14 -0.2633 -0.0876 3 11 15 0.4706 0.1198 3 11 16 0.9445 -0.1673 3 11 17 -0.0988 -0.1918 3 12 0 0.2451 -0.5386 3 12 1 0.0199 0.2261 3 12 2 -1.6003 0.1108 3 12 3 -0.6584 -0.0923 3 12 4 1.2946 0.1430 3 12 5 0.4265 -0.1316 3 12 6 0.5897 -0.0754 3 12 7 -1.5004 0.0486 3 12 8 -2.8156 0.0115 3 12 9 -0.9309 -0.0010 3 12 10 1.5684 0.0600 3 12 11 1.0582 -0.1209 3 12 12 0.3645 0.2140 3 12 13 -0.0202 0.0746 3 12 14 -0.4455 -0.0339 3 12 15 0.1644 0.2376 3 12 16 0.1032 -0.4653 3 13 0 -0.3957 0.6431 3 13 1 -0.5338 -0.1141 3 13 2 0.1670 -0.2664 3 13 3 0.7475 -0.1404 3 13 4 -0.1811 -0.1857 3 13 5 -0.2092 0.0866 3 13 6 -0.2106 0.0192 3 13 7 -2.5248 0.0425 3 13 8 -0.5881 0.1182 3 13 9 1.3219 -0.2650 3 13 10 0.9726 0.1507 3 13 11 -0.2318 -0.0673 3 13 12 0.2153 0.1764 3 13 13 -0.3569 0.1424 3 13 14 -0.4551 -0.0397 3 14 0 -0.4521 -0.5873 3 14 1 0.0279 -0.1974 3 14 2 1.1657 0.1031 3 14 3 -0.0419 -0.1160 3 14 4 -0.4143 0.0909 3 14 5 -0.4857 0.0691 3 14 6 -1.5760 -0.1108 3 14 7 -0.4200 0.1242 3 14 8 1.2127 -0.0947 3 14 9 0.2606 -0.1627 3 14 10 -0.4254 0.1132 3 14 11 -0.1665 -0.1600 3 15 0 -0.3037 0.3912 3 15 1 0.7769 0.3618 3 15 2 0.9211 -0.0463 3 15 3 -0.6028 -0.1292 3 15 4 -0.6852 -0.0981 3 15 5 -1.4158 0.0782 3 15 6 -0.2529 -0.0403 3 15 7 0.9790 0.1069 4 -12 0 0.5975 -0.6190 4 -12 1 0.4523 -0.0294 4 -12 2 -0.1835 0.1353 4 -12 3 -0.6026 -0.0971 4 -12 4 0.2444 0.2038 4 -12 5 -0.2926 0.2785 4 -12 6 -0.6201 0.1325 4 -12 7 -0.6199 -0.1874 4 -12 8 1.0524 -0.4248 4 -11 0 0.7716 0.4440 4 -11 1 0.1008 0.5509 4 -11 2 0.0924 -0.2231 4 -11 3 -0.6357 -0.1591 4 -11 4 0.2279 -0.0465 4 -11 5 -0.9062 -0.0067 4 -11 6 -0.8306 -0.0421 4 -11 7 0.4682 -0.2354 4 -11 8 2.1279 -0.0048 4 -11 9 0.5195 0.1437 4 -11 10 -0.8329 0.2914 4 -11 11 -0.6992 0.0280 4 -11 12 0.4969 0.0615 4 -10 0 0.9641 -0.1195 4 -10 1 -0.0496 -0.5354 4 -10 2 0.4841 -0.1248 4 -10 3 -0.6402 -0.0343 4 -10 4 0.1499 0.0777 4 -10 5 -0.6422 0.0766 4 -10 6 0.3521 -0.0313 4 -10 7 1.3118 -0.0332 4 -10 8 1.0317 -0.0298 4 -10 9 -0.4883 -0.0152 4 -10 10 -1.2346 0.1318 4 -10 11 -0.7722 0.0366 4 -10 12 -0.1960 0.2002 4 -10 13 -0.4333 0.1300 4 -10 14 1.3391 -0.0018 4 -10 15 0.7483 -0.2553 4 -9 0 1.1527 -0.1343 4 -9 1 0.8817 0.5616 4 -9 2 0.4081 0.0464 4 -9 3 -1.5556 -0.2382 4 -9 4 0.6256 -0.0749 4 -9 5 0.5945 -0.1064 4 -9 6 0.5013 0.0529 4 -9 7 0.5386 -0.0433 4 -9 8 -0.1331 -0.0157 4 -9 9 -1.1412 0.0638 4 -9 10 -2.0285 0.0504 4 -9 11 -0.0622 0.0162 4 -9 12 1.1510 0.0391 4 -9 13 1.1214 -0.0154 4 -9 14 1.4167 -0.1384 4 -9 15 -0.6099 -0.1222 4 -9 16 0.1797 0.0167 4 -8 0 1.6830 0.4976 4 -8 1 0.4578 -0.5056 4 -8 2 -2.2674 -0.4021 4 -8 3 -0.8742 -0.1245 4 -8 4 2.1989 0.0980 4 -8 5 0.6558 0.1924 4 -8 6 0.0126 0.0881 4 -8 7 -0.2723 -0.0876 4 -8 8 -1.8173 -0.1001 4 -8 9 -1.6674 -0.1042 4 -8 10 -0.1037 -0.0459 4 -8 11 2.6742 -0.0405 4 -8 12 1.7195 0.0224 4 -8 13 0.5906 -0.0096 4 -8 14 0.0657 -0.0459 4 -8 15 -0.7390 0.0804 4 -8 16 0.8760 -0.0931 4 -8 17 -0.3669 -0.1285 4 -8 18 -0.0681 -0.2451 4 -7 0 -0.3558 -0.7052 4 -7 1 -2.1052 0.3532 4 -7 2 -1.5562 0.2709 4 -7 3 2.0900 -0.0741 4 -7 4 1.6092 0.0410 4 -7 5 0.3049 -0.0907 4 -7 6 -0.7360 -0.1024 4 -7 7 -2.2521 -0.0840 4 -7 8 -2.0296 -0.0269 4 -7 9 0.9740 0.0430 4 -7 10 2.6484 -0.0376 4 -7 11 2.3850 0.0045 4 -7 12 0.3744 -0.0100 4 -7 13 -0.1415 -0.0687 4 -7 14 -0.2253 0.0241 4 -7 15 0.2254 -0.0495 4 -7 16 0.7302 -0.1353 4 -7 17 -0.5854 -0.0709 4 -7 18 0.0292 -0.1940 4 -7 19 -0.4771 -0.0011 4 -6 0 -2.2473 1.0123 4 -6 1 -0.1955 -0.0911 4 -6 2 1.7165 -0.5421 4 -6 3 1.5941 -0.2358 4 -6 4 0.3210 -0.0462 4 -6 5 -0.1532 0.1310 4 -6 6 -2.6330 0.1721 4 -6 7 -2.1899 0.0734 4 -6 8 0.6157 -0.0344 4 -6 9 2.6388 -0.1132 4 -6 10 2.0189 -0.0510 4 -6 11 0.7138 0.0011 4 -6 12 0.2869 -0.0620 4 -6 13 -0.0453 0.0142 4 -6 14 0.2359 -0.0125 4 -6 15 0.2290 -0.0329 4 -6 16 -0.2114 0.0296 4 -6 17 -0.0380 -0.0574 4 -6 18 0.1712 -0.0362 4 -6 19 -0.1302 0.0681 4 -6 20 0.2631 0.1810 4 -5 0 0.6409 -0.9340 4 -5 1 2.7962 -0.1924 4 -5 2 1.3681 0.3043 4 -5 3 0.1272 0.0002 4 -5 4 -0.6220 0.1265 4 -5 5 -2.2347 0.0522 4 -5 6 -2.7444 -0.0673 4 -5 7 0.3597 -0.1124 4 -5 8 2.0362 -0.0786 4 -5 9 1.6456 0.0834 4 -5 10 1.0032 0.0409 4 -5 11 0.8178 0.0108 4 -5 12 0.7069 0.0258 4 -5 13 -0.7767 -0.0350 4 -5 14 -0.6924 -0.0285 4 -5 15 -0.4561 0.0576 4 -5 16 0.6456 -0.0050 4 -5 17 0.9499 -0.0205 4 -5 18 -0.2477 0.0068 4 -5 19 0.0959 0.0408 4 -5 20 0.2929 0.2389 4 -5 21 0.2681 0.1937 4 -4 0 3.5941 0.9681 4 -4 1 1.7215 0.4828 4 -4 2 0.1103 -0.4512 4 -4 3 -1.5381 -0.3156 4 -4 4 -3.3988 -0.1545 4 -4 5 -2.4841 -0.0354 4 -4 6 0.2533 0.1239 4 -4 7 2.4526 0.1215 4 -4 8 1.2188 0.1164 4 -4 9 0.9163 -0.0660 4 -4 10 1.4793 -0.0593 4 -4 11 0.6066 0.0483 4 -4 12 -1.2241 -0.0518 4 -4 13 -2.5107 -0.0109 4 -4 14 -0.3382 0.0472 4 -4 15 1.2618 0.0365 4 -4 16 1.2342 0.0135 4 -4 17 -0.0717 0.0016 4 -4 18 -0.5628 -0.0791 4 -4 19 0.2943 0.0623 4 -4 20 0.0147 0.1573 4 -4 21 -0.2936 0.1597 4 -4 22 -0.7548 0.1330 4 -3 0 1.1630 -0.5875 4 -3 1 -0.3471 -0.7450 4 -3 2 -1.1554 0.1187 4 -3 3 -4.4403 0.0184 4 -3 4 -2.9127 0.0922 4 -3 5 1.1078 0.1687 4 -3 6 2.2317 0.0148 4 -3 7 1.7096 -0.0665 4 -3 8 0.5658 -0.1734 4 -3 9 1.9589 -0.0526 4 -3 10 0.5053 0.0985 4 -3 11 -2.0129 0.0041 4 -3 12 -2.8083 0.0393 4 -3 13 -0.7156 0.0519 4 -3 14 1.7527 -0.0171 4 -3 15 0.8100 0.0275 4 -3 16 -0.5651 -0.0232 4 -3 17 -0.5010 -0.0521 4 -3 18 -0.4767 -0.0408 4 -3 19 -0.0063 0.0507 4 -3 20 -0.0855 -0.0344 4 -3 21 -0.4969 0.0328 4 -3 22 0.0448 -0.2642 4 -3 23 0.5705 -0.3449 4 -2 0 -1.6748 0.2763 4 -2 1 0.4358 0.9209 4 -2 2 -3.3253 -0.0905 4 -2 3 -3.4000 -0.2785 4 -2 4 0.8238 -0.1456 4 -2 5 1.5545 -0.1582 4 -2 6 0.6011 -0.0244 4 -2 7 2.0579 0.0273 4 -2 8 2.3416 0.0824 4 -2 9 1.1218 0.0338 4 -2 10 -2.7346 -0.0420 4 -2 11 -2.7901 0.0317 4 -2 12 -0.3371 0.0067 4 -2 13 1.6597 -0.0412 4 -2 14 0.4446 0.0145 4 -2 15 -1.0282 0.0118 4 -2 16 -0.8123 -0.0145 4 -2 17 -0.1897 0.0098 4 -2 18 -0.4562 -0.0392 4 -2 19 0.1868 -0.1281 4 -2 20 -0.1791 -0.1170 4 -2 21 0.4329 -0.0351 4 -2 22 1.5400 -0.2114 4 -2 23 0.2981 0.1795 4 -1 0 1.8492 0.3215 4 -1 1 -0.5843 -0.9020 4 -1 2 -4.4320 -0.2035 4 -1 3 0.2783 -0.0234 4 -1 4 0.0224 -0.0200 4 -1 5 -0.7632 0.1649 4 -1 6 2.5701 0.0867 4 -1 7 5.1700 0.0271 4 -1 8 1.1801 -0.1241 4 -1 9 -2.5544 -0.1127 4 -1 10 -3.6334 0.0744 4 -1 11 0.2615 -0.0381 4 -1 12 2.2764 -0.0118 4 -1 13 0.7356 0.0625 4 -1 14 -1.0400 0.0025 4 -1 15 -1.1300 -0.0075 4 -1 16 -0.3476 -0.0047 4 -1 17 0.3505 -0.0190 4 -1 18 -0.4293 -0.0526 4 -1 19 -0.0132 -0.0416 4 -1 20 0.9235 0.0726 4 -1 21 2.2723 0.0209 4 -1 22 0.7424 0.0741 4 -1 23 -0.7623 0.0646 4 0 0 1.2514 -0.6611 4 0 1 -4.9050 0.7809 4 0 2 -1.8760 0.2969 4 0 3 1.4075 -0.2020 4 0 4 -2.2306 -0.0467 4 0 5 2.4105 -0.1480 4 0 6 6.8283 -0.0437 4 0 7 2.7564 -0.0451 4 0 8 -3.4635 0.0380 4 0 9 -3.6162 0.0789 4 0 10 -0.1128 -0.0460 4 0 11 3.6512 -0.0558 4 0 12 1.7105 0.0735 4 0 13 -0.4705 -0.0603 4 0 14 -1.3326 -0.0191 4 0 15 -1.1245 0.0053 4 0 16 0.6814 0.0290 4 0 17 0.2360 0.0656 4 0 18 -0.6224 0.0995 4 0 19 1.2930 0.0745 4 0 20 2.0348 0.0022 4 0 21 1.0643 -0.0378 4 0 22 -0.5693 -0.0206 4 0 23 0.1620 -0.2866 4 0 24 0.3378 -0.1943 4 1 0 -6.3668 1.1351 4 1 1 -2.9438 -0.5068 4 1 2 2.5718 -0.5143 4 1 3 0.2335 -0.0985 4 1 4 -0.2622 -0.1310 4 1 5 6.8041 0.1501 4 1 6 4.1430 0.1087 4 1 7 -3.1304 0.0645 4 1 8 -3.9079 -0.0232 4 1 9 0.1055 -0.1617 4 1 10 3.7175 0.0377 4 1 11 2.9990 -0.0148 4 1 12 0.1050 -0.0498 4 1 13 -1.0196 -0.0013 4 1 14 -2.2196 0.0750 4 1 15 -0.1998 0.0357 4 1 16 1.1981 0.0375 4 1 17 -0.0402 0.0245 4 1 18 0.4872 0.0564 4 1 19 1.2636 -0.0935 4 1 20 0.7397 -0.0627 4 1 21 0.7257 -0.0245 4 1 22 0.2396 -0.0563 4 1 23 -0.1982 -0.0562 4 1 24 -0.6068 0.1439 4 2 0 -6.5062 -1.1645 4 2 1 5.0717 0.1138 4 2 2 1.7130 0.4647 4 2 3 -1.0619 -0.1338 4 2 4 3.6187 0.0836 4 2 5 5.8620 -0.0516 4 2 6 -0.9816 -0.0929 4 2 7 -4.0394 -0.0327 4 2 8 -0.3383 -0.0869 4 2 9 3.3069 0.1339 4 2 10 3.2368 0.0015 4 2 11 1.1536 -0.0795 4 2 12 -1.1695 0.0521 4 2 13 -2.6238 0.0270 4 2 14 -1.7388 -0.0174 4 2 15 1.2712 -0.0453 4 2 16 0.9885 -0.1004 4 2 17 0.0575 0.0055 4 2 18 0.1072 -0.0049 4 2 19 0.7174 -0.0480 4 2 20 1.5692 0.0762 4 2 21 0.9340 -0.0047 4 2 22 -1.0346 0.0682 4 2 23 -0.8360 0.0403 4 2 24 0.2318 0.0122 4 3 0 2.5507 1.2361 4 3 1 4.9623 0.1713 4 3 2 -3.1146 -0.5950 4 3 3 2.6668 -0.1354 4 3 4 6.1103 -0.1208 4 3 5 1.8081 0.0286 4 3 6 -3.2859 0.1735 4 3 7 -2.2834 0.0355 4 3 8 2.8893 0.0575 4 3 9 3.9817 -0.1079 4 3 10 1.4567 -0.0463 4 3 11 -0.9100 0.0681 4 3 12 -3.7991 -0.0833 4 3 13 -1.4663 -0.0226 4 3 14 0.2669 -0.0508 4 3 15 1.3031 -0.0201 4 3 16 0.2723 -0.0408 4 3 17 -0.2314 0.0719 4 3 18 0.8797 -0.0076 4 3 19 1.7007 0.0597 4 3 20 1.0223 0.0149 4 3 21 -0.9202 -0.0072 4 3 22 -1.1127 0.0333 4 3 23 0.4306 -0.0498 4 3 24 0.3001 0.0792 4 4 0 3.9584 -0.9288 4 4 1 -1.0690 -0.5762 4 4 2 0.6603 0.4071 4 4 3 7.6837 0.0695 4 4 4 1.7479 0.1260 4 4 5 -3.1244 0.1433 4 4 6 -2.4303 -0.1044 4 4 7 1.8391 -0.0601 4 4 8 5.6185 -0.1725 4 4 9 2.1387 0.0504 4 4 10 -2.2243 0.1081 4 4 11 -3.2866 -0.1081 4 4 12 -1.7984 0.0261 4 4 13 1.7617 0.0362 4 4 14 -0.3410 0.0116 4 4 15 0.7953 0.0220 4 4 16 -0.0469 -0.0286 4 4 17 0.7539 0.0277 4 4 18 1.8438 -0.0130 4 4 19 0.5051 0.0309 4 4 20 -0.1858 -0.0365 4 4 21 -0.7675 0.0222 4 4 22 0.2433 -0.0236 4 4 23 0.3446 0.1833 4 5 0 -0.5791 0.7124 4 5 1 1.7584 0.7799 4 5 2 5.6055 -0.2776 4 5 3 1.9742 -0.1531 4 5 4 -4.8797 -0.0988 4 5 5 -0.9981 -0.1266 4 5 6 3.2812 0.0871 4 5 7 4.9569 0.0030 4 5 8 3.1216 0.0706 4 5 9 -3.0385 0.0288 4 5 10 -3.6177 -0.1020 4 5 11 0.3090 0.1115 4 5 12 1.6368 0.0189 4 5 13 0.5391 -0.0337 4 5 14 -1.1173 0.0542 4 5 15 0.7354 -0.0602 4 5 16 0.2272 0.0179 4 5 17 2.1134 -0.0394 4 5 18 1.2566 0.0649 4 5 19 -0.5246 -0.0280 4 5 20 0.2755 0.0404 4 5 21 -0.0771 0.0023 4 5 22 0.2516 0.1110 4 5 23 -0.0556 0.3343 4 6 0 0.7174 -0.0994 4 6 1 4.4325 -0.9226 4 6 2 -0.0679 0.0405 4 6 3 -3.8753 0.1122 4 6 4 -0.4187 0.0167 4 6 5 5.2880 0.2505 4 6 6 4.0040 -0.0097 4 6 7 1.2954 -0.0170 4 6 8 -1.9278 -0.1076 4 6 9 -3.4143 -0.0960 4 6 10 1.2251 0.1864 4 6 11 2.5271 -0.0668 4 6 12 -0.3332 -0.0505 4 6 13 -0.9986 0.0619 4 6 14 -0.3036 -0.0192 4 6 15 0.8340 -0.0140 4 6 16 2.5052 -0.0254 4 6 17 2.2595 0.0089 4 6 18 -0.6294 0.0799 4 6 19 -0.5805 -0.0646 4 6 20 0.9912 0.1259 4 6 21 -0.3461 -0.1194 4 6 22 -0.0090 0.2463 4 6 23 0.0655 0.1174 4 7 0 0.8397 -0.2343 4 7 1 0.6794 0.8195 4 7 2 -3.5658 0.1430 4 7 3 1.3554 -0.1091 4 7 4 4.7113 -0.0142 4 7 5 2.7491 -0.1449 4 7 6 -0.4233 -0.0116 4 7 7 -1.9025 0.0078 4 7 8 -1.3868 -0.0167 4 7 9 0.7867 0.1010 4 7 10 2.1497 -0.0934 4 7 11 -0.7817 -0.0554 4 7 12 -1.2126 0.1059 4 7 13 0.1437 -0.0911 4 7 14 1.4000 0.0185 4 7 15 2.3948 -0.0293 4 7 16 2.9586 -0.0348 4 7 17 -1.2268 0.0846 4 7 18 -1.2947 -0.0575 4 7 19 0.9023 0.0608 4 7 20 0.7038 -0.0807 4 7 21 -0.6442 -0.1242 4 7 22 0.3240 0.3562 4 8 0 -0.9303 0.7231 4 8 1 -0.8737 -0.6162 4 8 2 0.0935 -0.2959 4 8 3 4.5571 0.0504 4 8 4 0.6641 -0.0966 4 8 5 -1.3202 0.1807 4 8 6 -1.2723 0.1083 4 8 7 -0.5945 0.0038 4 8 8 1.2727 -0.0417 4 8 9 0.2743 -0.1441 4 8 10 -1.0383 0.0576 4 8 11 -1.0930 0.0447 4 8 12 1.1071 -0.1117 4 8 13 1.7548 0.0320 4 8 14 2.1250 0.0224 4 8 15 1.1499 0.0026 4 8 16 0.1453 -0.0829 4 8 17 -2.2778 0.0384 4 8 18 1.0018 -0.0837 4 8 19 0.9154 0.0560 4 8 20 -0.0468 -0.2035 4 8 21 -0.1097 0.2457 4 9 0 -1.1983 -0.8563 4 9 1 0.2274 0.3904 4 9 2 2.2523 0.3464 4 9 3 0.9391 -0.0350 4 9 4 -2.3228 0.0850 4 9 5 -0.2452 -0.0679 4 9 6 0.7678 -0.0068 4 9 7 0.8716 -0.0421 4 9 8 -0.4215 -0.0673 4 9 9 -2.1982 0.1150 4 9 10 -0.4696 -0.0238 4 9 11 1.4322 -0.0579 4 9 12 2.2299 0.0371 4 9 13 0.9553 0.0424 4 9 14 0.2103 -0.0233 4 9 15 -0.1012 -0.0094 4 9 16 0.0074 -0.1919 4 9 17 -0.7076 0.1597 4 9 18 1.0602 -0.1727 4 9 19 -0.1079 0.2422 4 9 20 0.0052 -0.0622 4 10 0 -0.3104 1.0358 4 10 1 1.4702 -0.0245 4 10 2 0.7026 -0.4280 4 10 3 -1.7037 0.0056 4 10 4 -0.0018 -0.1075 4 10 5 2.3541 0.0598 4 10 6 1.1462 0.1468 4 10 7 -1.3764 -0.0478 4 10 8 -2.4775 0.0754 4 10 9 -0.7456 -0.1034 4 10 10 1.8045 -0.0091 4 10 11 2.2920 0.1333 4 10 12 0.8267 -0.1559 4 10 13 -0.5660 0.0653 4 10 14 -0.0027 -0.0301 4 10 15 0.5455 -0.0092 4 10 16 -0.2261 -0.0674 4 10 17 -0.7366 0.0729 4 10 18 0.1655 -0.0217 4 10 19 -0.0183 0.3591 4 11 0 1.6953 -0.8219 4 11 1 0.7316 -0.2739 4 11 2 -1.1684 0.3072 4 11 3 0.1310 0.0489 4 11 4 2.7091 0.1360 4 11 5 1.3863 -0.0225 4 11 6 -1.2616 -0.0321 4 11 7 -2.3780 -0.0409 4 11 8 -0.7893 -0.1036 4 11 9 1.7160 0.0633 4 11 10 2.4509 0.0771 4 11 11 1.1625 -0.0987 4 11 12 -0.6104 -0.0727 4 11 13 -0.4991 0.0702 4 11 14 0.0132 -0.0070 4 11 15 -0.0711 0.0546 4 11 16 -0.7680 -0.2338 4 11 17 -0.2256 0.0890 4 11 18 0.2288 0.1076 4 12 0 1.4055 0.5865 4 12 1 -0.9067 0.4787 4 12 2 -0.0236 -0.2604 4 12 3 2.1190 -0.0230 4 12 4 0.6772 -0.1352 4 12 5 -0.5452 -0.1212 4 12 6 -1.0383 0.1690 4 12 7 -0.6123 -0.0873 4 12 8 1.2190 0.0492 4 12 9 2.3801 0.0253 4 12 10 0.9424 -0.1169 4 12 11 -0.4349 0.0557 4 12 12 -0.8753 -0.1734 4 12 13 -0.5582 0.0115 4 12 14 -0.2297 0.0815 4 12 15 0.0873 -0.3015 4 12 16 -0.1033 -0.0815 4 13 0 0.2775 -0.1583 4 13 1 -0.1560 -0.5493 4 13 2 1.3074 0.0400 4 13 3 0.1359 0.0464 4 13 4 -0.9568 0.0309 4 13 5 0.7389 0.1554 4 13 6 -0.3001 0.0274 4 13 7 0.8500 -0.0325 4 13 8 1.5380 -0.1180 4 13 9 0.6722 0.0004 4 13 10 -0.9711 -0.0396 4 13 11 -0.5210 -0.0817 4 13 12 -0.3446 -0.1597 4 13 13 -0.1198 0.0347 4 13 14 0.3771 -0.1661 4 13 15 0.1684 -0.1869 4 14 0 0.8386 0.0251 4 14 1 0.6737 0.5460 4 14 2 -0.0275 0.0411 4 14 3 -1.1728 -0.0013 4 14 4 0.3062 0.0333 4 14 5 0.6480 -0.0959 4 14 6 0.1477 0.1056 4 14 7 1.5030 -0.1097 4 14 8 -0.1517 -0.0811 4 14 9 -0.7647 0.0785 4 14 10 -0.8580 -0.1901 4 14 11 0.5442 0.1788 4 14 12 0.1500 -0.2602 4 15 0 0.7144 0.6731 4 15 1 -0.0232 -0.3576 4 15 2 -0.8218 -0.1787 4 15 3 -0.3372 0.0251 4 15 4 0.3133 -0.0589 4 15 5 0.2885 0.0941 4 15 6 1.0826 0.1034 4 15 7 0.1782 -0.1066 4 15 8 -0.9222 -0.0153 4 15 9 -0.4350 0.0483 5 -11 0 -0.5149 0.3621 5 -11 1 -0.5601 -0.5536 5 -11 2 0.5051 -0.2910 5 -11 3 1.3141 0.0921 5 -11 4 0.4362 0.0223 5 -11 5 -0.2610 -0.0179 5 -11 6 0.3079 -0.0039 5 -11 7 1.3585 0.0890 5 -11 8 -0.9939 0.1795 5 -11 9 -1.4241 0.0684 5 -11 10 -0.9263 -0.2761 5 -10 0 -0.1961 -0.6640 5 -10 1 0.1182 0.1717 5 -10 2 0.4235 0.4058 5 -10 3 0.9567 0.1196 5 -10 4 -0.2463 -0.0210 5 -10 5 0.1021 -0.1340 5 -10 6 0.6252 -0.0746 5 -10 7 0.0681 0.0524 5 -10 8 -1.7292 0.0717 5 -10 9 -0.9947 0.0122 5 -10 10 -0.1639 -0.2302 5 -10 11 0.5002 -0.1291 5 -10 12 0.2129 -0.1562 5 -10 13 1.2890 -0.1257 5 -9 0 -0.6288 0.8647 5 -9 1 -0.3052 0.0563 5 -9 2 -0.6565 -0.3808 5 -9 3 1.0041 -0.0652 5 -9 4 -0.0658 -0.0964 5 -9 5 -0.0131 0.0412 5 -9 6 -0.0975 0.1493 5 -9 7 -0.3063 0.1588 5 -9 8 -0.9423 0.0380 5 -9 9 -0.5967 -0.1529 5 -9 10 0.7977 -0.1956 5 -9 11 1.2708 -0.1226 5 -9 12 0.7130 -0.1166 5 -9 13 -0.0246 -0.0191 5 -9 14 -1.6263 -0.0117 5 -9 15 -0.0427 0.1990 5 -8 0 -1.2277 -0.7538 5 -8 1 -1.3089 -0.4010 5 -8 2 -0.3071 0.3766 5 -8 3 2.0360 0.2681 5 -8 4 -0.3587 0.0581 5 -8 5 -0.0110 0.0526 5 -8 6 -0.1749 -0.1066 5 -8 7 -0.7544 -0.0925 5 -8 8 -0.3837 -0.0515 5 -8 9 0.7079 0.0770 5 -8 10 2.0289 0.0267 5 -8 11 0.2995 -0.0118 5 -8 12 -0.8271 0.0453 5 -8 13 -1.1654 -0.0344 5 -8 14 -0.7442 0.0312 5 -8 15 0.9022 0.0271 5 -8 16 -0.5492 -0.0374 5 -8 17 -0.1445 0.0962 5 -7 0 -1.1670 0.6529 5 -7 1 -0.8557 0.5914 5 -7 2 1.7063 -0.1944 5 -7 3 1.5747 -0.2035 5 -7 4 -0.5716 -0.1424 5 -7 5 -0.2213 -0.0968 5 -7 6 -1.3308 0.0062 5 -7 7 -0.1572 0.1902 5 -7 8 1.8768 0.2155 5 -7 9 1.5856 0.0130 5 -7 10 0.6113 -0.0855 5 -7 11 -1.7224 0.0176 5 -7 12 -1.2446 -0.0474 5 -7 13 -0.6053 -0.0141 5 -7 14 0.1028 0.0631 5 -7 15 0.1953 -0.0234 5 -7 16 -1.1827 0.0962 5 -7 17 0.4247 0.1021 5 -7 18 0.0650 0.1843 5 -7 19 0.6923 0.1208 5 -6 0 0.2051 -0.2371 5 -6 1 0.8473 -0.8593 5 -6 2 1.5654 0.0104 5 -6 3 -0.1270 0.2550 5 -6 4 -0.6002 0.1238 5 -6 5 -1.1654 0.1178 5 -6 6 -0.1560 0.0316 5 -6 7 2.3770 -0.0632 5 -6 8 2.3044 -0.1613 5 -6 9 -0.1531 -0.0364 5 -6 10 -1.3435 0.1082 5 -6 11 -1.7578 0.0278 5 -6 12 -0.4439 0.0265 5 -6 13 -0.0591 0.0933 5 -6 14 -0.3500 -0.0108 5 -6 15 -0.8437 0.0259 5 -6 16 -0.4823 0.0179 5 -6 17 0.9750 -0.0218 5 -6 18 0.1144 0.0458 5 -6 19 0.5798 -0.0758 5 -6 20 -0.5662 -0.1219 5 -5 0 1.6981 -0.0691 5 -5 1 0.4195 0.8051 5 -5 2 -0.3445 0.1727 5 -5 3 -0.8177 -0.1563 5 -5 4 -0.6521 -0.1277 5 -5 5 -0.0026 -0.1340 5 -5 6 2.7213 -0.1193 5 -5 7 2.5680 -0.0528 5 -5 8 0.1283 0.1610 5 -5 9 -1.7554 0.1211 5 -5 10 -1.0141 -0.0468 5 -5 11 -0.3933 -0.0078 5 -5 12 -0.4299 0.0051 5 -5 13 -0.5676 -0.0433 5 -5 14 -0.7479 -0.0265 5 -5 15 0.1515 0.0200 5 -5 16 0.6644 -0.0588 5 -5 17 0.2047 0.0090 5 -5 18 -0.1231 -0.0149 5 -5 19 0.0570 -0.0618 5 -5 20 -0.5101 -0.2266 5 -5 21 0.2554 -0.2736 5 -4 0 0.7052 0.6000 5 -4 1 -1.0337 -0.8194 5 -4 2 -1.1772 -0.4121 5 -4 3 -1.0672 0.1216 5 -4 4 0.7735 0.1270 5 -4 5 3.2258 0.1976 5 -4 6 3.4035 0.0469 5 -4 7 -0.3967 0.0060 5 -4 8 -1.8123 -0.1052 5 -4 9 -0.7097 -0.1829 5 -4 10 0.1923 0.0283 5 -4 11 -0.6870 0.0177 5 -4 12 -0.8580 -0.0386 5 -4 13 0.6982 0.0165 5 -4 14 0.9004 0.0194 5 -4 15 0.5083 0.0016 5 -4 16 -0.5158 -0.0236 5 -4 17 -0.4355 -0.0200 5 -4 18 0.2427 -0.0496 5 -4 19 -0.3069 -0.0743 5 -4 20 0.1250 -0.1955 5 -4 21 0.4634 -0.0755 5 -4 22 0.3012 -0.1293 5 -3 0 -1.0033 -0.8895 5 -3 1 -0.8779 0.5189 5 -3 2 -1.8060 0.5204 5 -3 3 0.8682 0.0343 5 -3 4 4.3857 0.0285 5 -3 5 3.4152 -0.0979 5 -3 6 -0.5667 -0.1617 5 -3 7 -2.7794 -0.1100 5 -3 8 0.0744 -0.0103 5 -3 9 0.4093 0.1198 5 -3 10 -0.5608 0.0305 5 -3 11 -0.2319 -0.0390 5 -3 12 1.5766 0.0191 5 -3 13 2.2580 -0.0396 5 -3 14 -0.2519 -0.0189 5 -3 15 -0.9508 -0.0218 5 -3 16 -0.1736 -0.0071 5 -3 17 0.1750 -0.0013 5 -3 18 0.2207 0.0505 5 -3 19 0.1313 -0.0443 5 -3 20 0.8925 -0.0461 5 -3 21 0.2668 -0.0138 5 -3 22 0.1290 0.0426 5 -2 0 -0.0742 1.2477 5 -2 1 -1.1733 -0.2352 5 -2 2 -0.2230 -0.6438 5 -2 3 4.5880 -0.0676 5 -2 4 2.6393 0.0105 5 -2 5 -1.4879 0.1530 5 -2 6 -1.7422 0.1461 5 -2 7 0.4710 0.0660 5 -2 8 1.3795 0.0070 5 -2 9 -1.1097 -0.1287 5 -2 10 0.2320 -0.0192 5 -2 11 1.9592 0.0293 5 -2 12 2.2019 -0.0279 5 -2 13 0.0022 -0.0210 5 -2 14 -1.3334 0.0121 5 -2 15 0.3928 -0.0028 5 -2 16 0.5778 0.0383 5 -2 17 -0.0930 0.0366 5 -2 18 0.6479 0.0440 5 -2 19 0.5543 -0.0495 5 -2 20 0.6335 0.1356 5 -2 21 -0.0957 0.1202 5 -2 22 -0.6314 0.2943 5 -2 23 -0.5663 0.1081 5 -1 0 -0.3188 -1.2223 5 -1 1 -1.0543 -0.2240 5 -1 2 3.1706 0.5746 5 -1 3 1.6063 0.1451 5 -1 4 -2.5281 0.1318 5 -1 5 0.1380 0.0599 5 -1 6 3.3170 -0.1188 5 -1 7 1.0830 -0.1111 5 -1 8 -1.4126 -0.0601 5 -1 9 -1.3362 0.0820 5 -1 10 1.7522 0.0663 5 -1 11 1.8400 -0.0248 5 -1 12 0.2201 0.0451 5 -1 13 -0.9436 -0.0208 5 -1 14 0.0571 -0.0338 5 -1 15 0.6704 -0.0241 5 -1 16 0.1890 0.0016 5 -1 17 0.1612 0.0507 5 -1 18 0.7339 0.0169 5 -1 19 0.5260 0.0798 5 -1 20 0.5017 0.1496 5 -1 21 -1.2743 -0.0094 5 -1 22 -1.6351 0.0172 5 -1 23 0.0328 -0.2431 5 0 0 -1.4657 1.1363 5 0 1 1.5112 0.5826 5 0 2 1.1509 -0.5571 5 0 3 -3.5216 -0.2701 5 0 4 1.5239 -0.0519 5 0 5 6.4237 0.0277 5 0 6 2.1744 0.1203 5 0 7 -3.7612 0.1062 5 0 8 -2.4008 0.0841 5 0 9 0.2621 -0.0760 5 0 10 2.3361 -0.0785 5 0 11 0.3588 0.0706 5 0 12 -1.0422 -0.0146 5 0 13 -0.5788 -0.0503 5 0 14 -0.3161 -0.0113 5 0 15 0.5813 -0.0188 5 0 16 0.5701 0.0285 5 0 17 0.2418 0.0139 5 0 18 0.9389 -0.0370 5 0 19 0.2743 -0.0097 5 0 20 -1.1492 -0.1297 5 0 21 -2.2463 -0.0671 5 0 22 -0.3476 0.0228 5 0 23 0.7050 0.1568 5 0 24 -0.3017 0.4350 5 1 0 0.2392 -0.7181 5 1 1 0.6224 -0.9029 5 1 2 -3.3973 0.1836 5 1 3 0.2497 0.2357 5 1 4 8.6565 0.2272 5 1 5 3.8738 0.1656 5 1 6 -4.6544 -0.0567 5 1 7 -4.6689 -0.0708 5 1 8 0.4534 -0.1349 5 1 9 1.9466 0.0072 5 1 10 1.1224 0.0733 5 1 11 -1.6322 0.0178 5 1 12 -1.3223 -0.0064 5 1 13 -1.3703 0.0350 5 1 14 -0.0485 -0.0309 5 1 15 1.8765 -0.0321 5 1 16 0.6689 -0.0797 5 1 17 0.5283 -0.0434 5 1 18 -0.0649 -0.0679 5 1 19 -1.3849 -0.0515 5 1 20 -1.2567 -0.0073 5 1 21 -0.4774 0.1179 5 1 22 0.4019 0.0973 5 1 23 -0.3647 0.1755 5 1 24 -0.3794 -0.0274 5 2 0 0.6618 0.3047 5 2 1 -3.2525 0.9380 5 2 2 -0.9233 -0.0984 5 2 3 7.4633 -0.1784 5 2 4 6.7361 -0.0368 5 2 5 -3.9211 -0.1314 5 2 6 -6.2193 0.0784 5 2 7 -0.4626 0.0506 5 2 8 2.5571 0.1115 5 2 9 0.9901 0.0206 5 2 10 -0.8818 -0.0875 5 2 11 -2.1926 0.0577 5 2 12 -2.0346 -0.0006 5 2 13 -1.0004 -0.0217 5 2 14 2.6110 -0.0246 5 2 15 2.3044 -0.0508 5 2 16 0.2807 0.0069 5 2 17 -0.7736 0.0723 5 2 18 -1.3742 -0.0127 5 2 19 -0.4018 0.0893 5 2 20 0.1348 -0.0144 5 2 21 -0.4430 -0.0187 5 2 22 -0.7177 -0.0437 5 2 23 -0.3737 -0.0283 5 2 24 0.3931 -0.0783 5 3 0 -0.4834 0.1536 5 3 1 -2.2046 -0.9841 5 3 2 6.1261 -0.1862 5 3 3 7.0267 0.2084 5 3 4 -1.4165 0.1731 5 3 5 -7.0553 0.2754 5 3 6 -2.4546 0.0325 5 3 7 2.7966 -0.0527 5 3 8 1.8903 -0.0725 5 3 9 -0.3176 -0.0925 5 3 10 -1.9544 0.1058 5 3 11 -3.3976 -0.0041 5 3 12 -0.7664 0.0095 5 3 13 2.4424 0.0493 5 3 14 3.6047 0.0499 5 3 15 0.7116 0.0218 5 3 16 -0.9433 0.0870 5 3 17 -1.4140 -0.0119 5 3 18 -0.0912 0.0199 5 3 19 0.1455 -0.0008 5 3 20 -0.5644 -0.1315 5 3 21 -1.2882 0.0320 5 3 22 -0.2462 -0.0496 5 3 23 0.7359 0.1164 5 3 24 0.5225 0.0589 5 4 0 0.1537 -0.5982 5 4 1 3.2395 0.8178 5 4 2 6.9195 0.3110 5 4 3 -1.4495 -0.0400 5 4 4 -6.3459 0.0798 5 4 5 -3.5758 -0.1926 5 4 6 2.0471 -0.0707 5 4 7 3.4612 0.0249 5 4 8 -0.0914 0.0674 5 4 9 -2.6285 0.1198 5 4 10 -3.6766 -0.0323 5 4 11 -1.1393 0.0257 5 4 12 3.6956 0.0759 5 4 13 2.3574 -0.0316 5 4 14 1.5861 0.0310 5 4 15 -0.7766 -0.0461 5 4 16 -0.8755 0.0336 5 4 17 -0.3357 -0.0322 5 4 18 -0.0489 0.0632 5 4 19 -0.7284 -0.0392 5 4 20 -1.0265 0.0673 5 4 21 -0.7099 0.0474 5 4 22 1.1005 0.0391 5 4 23 0.7111 0.1121 5 5 0 3.2700 0.9262 5 5 1 3.9806 -0.5910 5 5 2 -0.7425 -0.4972 5 5 3 -6.9801 0.0883 5 5 4 -2.0555 0.0044 5 5 5 2.0577 0.1879 5 5 6 2.6818 0.1455 5 5 7 0.2197 -0.0145 5 5 8 -4.2927 0.0235 5 5 9 -3.9429 -0.1034 5 5 10 -0.0375 0.0672 5 5 11 3.1607 0.0269 5 5 12 2.3773 -0.1087 5 5 13 -0.5911 0.0046 5 5 14 1.0435 -0.0446 5 5 15 -0.8877 0.0297 5 5 16 0.3634 0.0160 5 5 17 -0.4145 0.0327 5 5 18 -1.2032 0.0413 5 5 19 -0.8648 0.0466 5 5 20 -0.6144 0.0817 5 5 21 0.4700 -0.0229 5 5 22 0.9465 0.0696 5 5 23 -0.1349 -0.4468 5 6 0 3.3980 -1.1903 5 6 1 -1.8150 0.2498 5 6 2 -4.9384 0.5082 5 6 3 -1.9097 0.0437 5 6 4 3.6332 0.1790 5 6 5 0.6345 -0.0955 5 6 6 -1.5659 -0.1498 5 6 7 -3.9650 -0.0076 5 6 8 -4.4564 -0.0225 5 6 9 1.0726 0.1033 5 6 10 3.2092 -0.0003 5 6 11 0.6381 -0.0903 5 6 12 -0.7300 0.0499 5 6 13 -0.0911 -0.0305 5 6 14 1.1583 -0.0367 5 6 15 -0.1586 0.0362 5 6 16 0.2525 -0.0561 5 6 17 -2.3241 0.1356 5 6 18 -1.3134 -0.0562 5 6 19 0.3203 0.1454 5 6 20 -0.1849 -0.0858 5 6 21 0.3140 0.0537 5 6 22 0.1925 -0.2576 5 6 23 -0.0669 -0.5446 5 7 0 -0.1288 1.1309 5 7 1 -4.2730 0.1682 5 7 2 -0.1644 -0.5534 5 7 3 2.5629 -0.0139 5 7 4 0.0966 -0.0781 5 7 5 -3.5935 -0.0109 5 7 6 -3.0923 0.2131 5 7 7 -2.7466 -0.0103 5 7 8 0.7199 0.0316 5 7 9 3.2458 -0.0393 5 7 10 -0.0520 -0.0409 5 7 11 -1.4109 0.1325 5 7 12 0.1433 -0.0804 5 7 13 0.6985 -0.0170 5 7 14 0.4815 -0.0285 5 7 15 -0.3381 0.0056 5 7 16 -2.2107 0.0947 5 7 17 -2.1271 0.0461 5 7 18 0.8778 -0.0264 5 7 19 0.3903 0.0769 5 7 20 -0.9982 -0.1639 5 7 21 0.4258 0.1263 5 7 22 0.1794 -0.4595 5 8 0 -1.1581 -0.9900 5 8 1 -1.1486 -0.4298 5 8 2 2.9354 0.4201 5 8 3 -1.2720 0.1380 5 8 4 -2.9563 0.1673 5 8 5 -1.9758 0.1035 5 8 6 -0.9781 -0.1290 5 8 7 0.8366 -0.0763 5 8 8 1.8178 -0.0259 5 8 9 0.4660 0.0764 5 8 10 -0.9798 0.0843 5 8 11 0.0208 -0.0339 5 8 12 0.3505 0.0108 5 8 13 -0.1288 0.0568 5 8 14 -0.7952 -0.0372 5 8 15 -1.1835 0.0996 5 8 16 -2.3561 -0.0018 5 8 17 0.6840 -0.0234 5 8 18 0.5686 0.0711 5 8 19 -0.9813 -0.0863 5 8 20 -0.2820 0.0613 5 8 21 0.5081 -0.0261 5 8 22 -0.2432 -0.4329 5 9 0 0.2155 0.6414 5 9 1 0.8898 0.7185 5 9 2 0.3621 -0.2496 5 9 3 -2.8893 -0.0850 5 9 4 0.1591 -0.0588 5 9 5 0.0292 -0.1553 5 9 6 0.1070 0.0920 5 9 7 0.7847 0.0652 5 9 8 0.0727 0.0694 5 9 9 0.8711 0.0306 5 9 10 0.3468 -0.0875 5 9 11 -0.1029 0.0982 5 9 12 -0.8255 0.0344 5 9 13 -1.0700 -0.0039 5 9 14 -0.8771 0.0659 5 9 15 -0.5768 -0.1045 5 9 16 -1.2312 0.0341 5 9 17 0.9205 -0.0008 5 9 18 -0.9869 0.1210 5 9 19 -0.1660 -0.1176 5 9 20 0.1896 0.0685 5 9 21 -0.1555 -0.3544 5 10 0 0.9611 -0.2555 5 10 1 -0.0169 -0.7843 5 10 2 -0.8788 0.0945 5 10 3 -0.0113 0.1151 5 10 4 1.2991 0.0555 5 10 5 -0.9195 0.1965 5 10 6 -0.7123 -0.0151 5 10 7 0.0468 -0.0046 5 10 8 1.4149 -0.1036 5 10 9 1.9106 -0.0376 5 10 10 -0.4259 0.0629 5 10 11 -1.2000 -0.0265 5 10 12 -1.4509 0.0690 5 10 13 -0.7268 0.0730 5 10 14 -0.2546 -0.0778 5 10 15 -0.6693 -0.1512 5 10 16 -0.7786 0.0765 5 10 17 0.5428 -0.0741 5 10 18 -0.6420 0.2192 5 10 19 0.3942 -0.3190 5 10 20 -0.0693 0.0467 5 11 0 -0.1643 -0.2352 5 11 1 -0.7726 0.7530 5 11 2 0.2351 0.1125 5 11 3 0.8626 -0.0709 5 11 4 -0.7389 0.0380 5 11 5 -1.7784 -0.1100 5 11 6 -0.3704 -0.0214 5 11 7 1.3175 -0.0163 5 11 8 2.0338 -0.0564 5 11 9 0.2622 0.1054 5 11 10 -1.5571 -0.0650 5 11 11 -1.4252 0.0317 5 11 12 -0.9334 0.1383 5 11 13 -0.4544 -0.1535 5 11 14 -0.3681 -0.0573 5 11 15 -0.2933 -0.2310 5 11 16 0.2879 0.0403 5 11 17 0.2174 0.1072 5 11 18 -0.3828 0.1502 5 12 0 -1.3027 0.5144 5 12 1 -0.1061 -0.5322 5 12 2 0.6930 -0.2249 5 12 3 -0.8024 0.1237 5 12 4 -1.7319 -0.0214 5 12 5 -0.4896 0.2091 5 12 6 0.5637 -0.0499 5 12 7 1.0644 0.0088 5 12 8 0.3472 0.0060 5 12 9 -1.2182 0.0041 5 12 10 -1.1135 0.0289 5 12 11 -0.7013 -0.0810 5 12 12 -0.6266 0.0419 5 12 13 -0.4981 -0.0556 5 12 14 0.3062 -0.1215 5 12 15 0.4359 -0.1886 5 12 16 0.2167 0.3060 5 12 17 -0.5363 0.1772 5 13 0 -0.7606 -0.7208 5 13 1 0.6174 0.2929 5 13 2 -0.6328 0.3603 5 13 3 -1.9220 0.0253 5 13 4 -0.0713 0.1345 5 13 5 0.3035 -0.0430 5 13 6 0.0429 -0.0950 5 13 7 -0.1305 0.0825 5 13 8 -0.6372 -0.0712 5 13 9 -0.8368 0.1025 5 13 10 -0.0704 -0.1025 5 13 11 -0.4107 0.0328 5 13 12 -0.4571 0.2617 5 13 13 -0.0344 -0.2343 5 13 14 0.4690 -0.0258 5 13 15 0.0277 0.1512 5 14 0 -0.2995 0.7482 5 14 1 -0.2365 -0.0302 5 14 2 -1.6317 -0.2963 5 14 3 -0.3179 0.0408 5 14 4 1.0143 -0.0604 5 14 5 -0.4414 0.0806 5 14 6 -0.0879 0.0443 5 14 7 -0.6242 -0.0520 5 14 8 -0.3042 0.0542 5 14 9 -0.3816 0.0005 5 14 10 0.3898 0.1602 5 14 11 -0.1076 0.1677 5 14 12 -0.2855 -0.0873 5 14 13 -0.1552 -0.0779 5 15 0 -0.7692 -0.8007 5 15 1 -0.4103 -0.3215 5 15 2 -0.3562 0.2379 5 15 3 0.7859 0.0144 5 15 4 0.0396 0.1161 5 15 5 -0.2989 0.0791 5 15 6 0.0648 -0.1373 5 15 7 -0.6051 0.0529 5 15 8 -0.0795 0.0160 5 15 9 -0.1536 0.1359 5 15 10 1.0202 0.1651 6 -11 1 0.8231 -0.1184 6 -11 2 0.1030 0.4060 6 -11 3 -0.6981 0.1307 6 -11 4 -1.0863 -0.1115 6 -11 5 -0.2768 0.0863 6 -10 0 -0.2436 0.3986 6 -10 1 -0.1130 0.5902 6 -10 2 -0.7675 -0.0571 6 -10 3 -0.7457 -0.3635 6 -10 4 -0.2833 -0.1952 6 -10 5 0.3009 0.1289 6 -10 6 -0.0369 0.2146 6 -10 7 -0.8670 0.1800 6 -10 8 0.8564 0.0573 6 -10 9 0.4564 -0.1525 6 -10 10 0.6113 -0.0516 6 -10 11 0.0567 0.1819 6 -9 0 -0.9570 -0.1233 6 -9 1 -0.1781 -0.5850 6 -9 2 0.4211 -0.1370 6 -9 3 0.0063 0.0528 6 -9 4 -0.3023 0.2294 6 -9 5 -0.0915 0.3083 6 -9 6 0.0779 0.1616 6 -9 7 -0.2705 -0.0598 6 -9 8 0.2866 -0.3139 6 -9 9 0.3049 -0.1835 6 -9 10 0.6680 0.2149 6 -9 11 -0.0719 0.3086 6 -9 12 -0.4379 0.2755 6 -9 13 -1.1858 0.0757 6 -9 14 0.7515 0.0989 6 -8 0 0.2320 -0.3187 6 -8 1 0.8706 0.6464 6 -8 2 0.9582 0.2908 6 -8 3 -0.7250 -0.1323 6 -8 4 0.0437 -0.0736 6 -8 5 -0.1480 -0.0758 6 -8 6 -0.8286 -0.0314 6 -8 7 -0.5446 -0.0721 6 -8 8 0.8380 0.0229 6 -8 9 1.0204 0.1353 6 -8 10 -0.2962 0.0693 6 -8 11 -0.7066 0.1113 6 -8 12 -0.7074 0.0508 6 -8 13 -0.0328 -0.0106 6 -8 14 0.9697 0.0758 6 -8 15 -0.3069 0.0064 6 -8 16 0.2851 0.0761 6 -7 0 0.6274 0.5435 6 -7 1 0.5776 -0.3863 6 -7 2 0.3112 -0.4451 6 -7 3 -0.5075 -0.0586 6 -7 4 0.0348 0.1198 6 -7 5 -1.9252 0.2012 6 -7 6 -0.3152 0.1619 6 -7 7 1.4792 0.0436 6 -7 8 0.9244 -0.1334 6 -7 9 -0.3590 -0.2397 6 -7 10 -1.4591 -0.0450 6 -7 11 -0.4362 0.1035 6 -7 12 -0.3347 0.0242 6 -7 13 0.5977 0.1297 6 -7 14 0.5982 0.0882 6 -7 15 -0.0037 0.0467 6 -7 16 0.9959 -0.0184 6 -7 17 -0.2340 -0.1279 6 -7 18 -0.0309 -0.0234 6 -6 0 -0.3252 -0.8520 6 -6 1 0.4139 0.2681 6 -6 2 -0.0239 0.4892 6 -6 3 -0.4695 0.1407 6 -6 4 -1.1615 0.0142 6 -6 5 -0.8928 -0.1087 6 -6 6 1.8989 -0.0959 6 -6 7 0.5926 -0.0854 6 -6 8 -1.2998 -0.0650 6 -6 9 -1.4021 0.0705 6 -6 10 -1.1684 0.0738 6 -6 11 0.4547 0.0072 6 -6 12 0.4824 0.0196 6 -6 13 0.7980 0.0227 6 -6 14 0.2580 -0.0427 6 -6 15 0.6144 -0.0241 6 -6 16 1.1400 -0.0552 6 -6 17 -0.7914 0.0233 6 -6 18 -0.1135 0.0615 6 -6 19 -0.6901 0.0950 6 -5 0 -0.4041 0.9343 6 -5 1 0.1332 0.1121 6 -5 2 -0.6978 -0.4849 6 -5 3 -0.6512 -0.1874 6 -5 4 -0.4838 -0.0502 6 -5 5 0.9971 0.1292 6 -5 6 0.4864 0.2117 6 -5 7 -1.9544 0.1536 6 -5 8 -2.2367 0.0301 6 -5 9 -0.6576 -0.1283 6 -5 10 0.3965 -0.0921 6 -5 11 1.0839 -0.0253 6 -5 12 0.2173 -0.0108 6 -5 13 0.1005 -0.0146 6 -5 14 0.6984 0.0572 6 -5 15 1.1019 0.0493 6 -5 16 0.0613 0.0632 6 -5 17 -1.1962 0.0376 6 -5 18 0.1672 0.0417 6 -5 19 -0.4498 0.1079 6 -5 20 0.6879 0.1578 6 -4 0 -0.9152 -0.9650 6 -4 1 -0.8244 -0.3620 6 -4 2 -1.1945 0.4160 6 -4 3 0.1878 0.2810 6 -4 4 1.0589 0.2111 6 -4 5 0.3629 0.0172 6 -4 6 -2.6725 -0.1125 6 -4 7 -3.0541 -0.0698 6 -4 8 -0.6635 -0.0843 6 -4 9 1.3340 0.0524 6 -4 10 0.5213 0.0931 6 -4 11 -0.0466 0.0041 6 -4 12 -0.1177 0.0332 6 -4 13 0.2980 0.0196 6 -4 14 0.4926 0.0760 6 -4 15 -0.2650 -0.0230 6 -4 16 -0.3193 -0.0126 6 -4 17 0.0525 -0.0557 6 -4 18 0.2680 0.0747 6 -4 19 -0.1797 0.1830 6 -4 20 0.7212 0.3052 6 -4 21 -0.2824 0.1771 6 -3 0 -1.5720 0.7346 6 -3 1 -1.6956 0.6836 6 -3 2 -0.1076 -0.2845 6 -3 3 2.1823 -0.2074 6 -3 4 0.2965 -0.1710 6 -3 5 -3.1841 -0.1367 6 -3 6 -3.9167 0.1626 6 -3 7 0.1106 0.1678 6 -3 8 1.6554 0.1004 6 -3 9 0.3971 0.0217 6 -3 10 -0.8128 -0.0389 6 -3 11 -0.3164 0.0037 6 -3 12 -0.2891 -0.0203 6 -3 13 -1.0707 0.0013 6 -3 14 -0.6233 0.0148 6 -3 15 0.4394 -0.0378 6 -3 16 0.7099 0.0243 6 -3 17 -0.0046 -0.0181 6 -3 18 -0.2254 0.0936 6 -3 19 0.3342 0.1152 6 -3 20 -0.1717 0.0901 6 -3 21 -1.0230 -0.1171 6 -3 22 -0.3481 -0.0755 6 -2 0 -1.9222 -0.4560 6 -2 1 -0.7438 -0.8621 6 -2 2 2.7624 0.0780 6 -2 3 0.4762 0.2372 6 -2 4 -3.5866 0.1798 6 -2 5 -2.9542 0.1952 6 -2 6 0.7380 -0.0317 6 -2 7 2.1189 -0.1411 6 -2 8 -1.0421 -0.1168 6 -2 9 -1.2072 0.0406 6 -2 10 -0.8599 0.0913 6 -2 11 -0.9041 0.0059 6 -2 12 -1.5200 -0.0131 6 -2 13 -1.2665 0.0140 6 -2 14 0.9812 -0.0144 6 -2 15 0.7996 0.0267 6 -2 16 -0.5332 -0.0485 6 -2 17 -0.1108 -0.0583 6 -2 18 0.1100 -0.0468 6 -2 19 0.0511 -0.0205 6 -2 20 -1.2290 -0.0302 6 -2 21 -0.6050 -0.0752 6 -2 22 0.4494 -0.1250 6 -2 23 0.6260 -0.2670 6 -1 0 -0.6060 0.0226 6 -1 1 2.7429 0.9671 6 -1 2 1.0875 0.1066 6 -1 3 -3.9083 -0.1534 6 -1 4 -1.2622 -0.0796 6 -1 5 2.2730 -0.2716 6 -1 6 0.8083 -0.0553 6 -1 7 -2.5077 0.1016 6 -1 8 -2.8418 0.1125 6 -1 9 -0.2934 0.0980 6 -1 10 -0.7413 -0.0578 6 -1 11 -0.8964 -0.0101 6 -1 12 -0.9055 -0.0538 6 -1 13 0.2396 -0.0215 6 -1 14 0.6185 0.0051 6 -1 15 -0.7915 -0.0289 6 -1 16 -0.2589 -0.0284 6 -1 17 0.6235 -0.0191 6 -1 18 -0.2245 -0.1005 6 -1 19 -0.5518 0.0084 6 -1 20 -1.3445 -0.0901 6 -1 21 0.3209 -0.0770 6 -1 22 1.0432 -0.1346 6 -1 23 0.4346 0.0849 6 0 0 3.1234 0.4456 6 0 1 1.4369 -0.8562 6 0 2 -3.8032 -0.3511 6 0 3 -0.6731 0.1738 6 0 4 3.9743 0.0855 6 0 5 -0.2457 0.2315 6 0 6 -5.3347 0.1560 6 0 7 -3.5638 -0.0916 6 0 8 -0.1667 -0.1448 6 0 9 1.3140 -0.0464 6 0 10 0.0518 0.0309 6 0 11 -0.4916 0.0137 6 0 12 -0.2365 -0.0291 6 0 13 -0.1429 0.0611 6 0 14 -0.2647 -0.0306 6 0 15 0.0344 0.0395 6 0 16 0.5842 0.0525 6 0 17 0.1908 -0.0765 6 0 18 -0.9816 -0.0263 6 0 19 -1.0139 -0.0108 6 0 20 -0.4642 -0.0336 6 0 21 1.5354 0.1090 6 0 22 1.0147 0.0576 6 0 23 -0.1921 0.0658 6 1 0 1.4343 -0.7900 6 1 1 -3.3768 0.6477 6 1 2 -0.6503 0.4954 6 1 3 5.2997 0.0279 6 1 4 -0.1947 0.0601 6 1 5 -7.4143 -0.1617 6 1 6 -5.3607 -0.1716 6 1 7 1.2307 -0.0462 6 1 8 2.3692 0.0835 6 1 9 1.6143 0.1162 6 1 10 -0.6280 0.0095 6 1 11 -0.5348 0.0125 6 1 12 -0.1835 0.0206 6 1 13 -0.1671 -0.0218 6 1 14 1.3112 0.0123 6 1 15 0.6541 0.0597 6 1 16 -0.0213 0.0041 6 1 17 -1.2566 0.0424 6 1 18 -1.4848 0.0674 6 1 19 0.2137 -0.0036 6 1 20 1.1059 0.0946 6 1 21 1.3097 0.0442 6 1 22 -0.3012 -0.0342 6 1 23 -0.5882 -0.2096 6 1 24 0.2827 -0.2730 6 2 0 -1.8086 1.0704 6 2 1 0.0169 -0.3563 6 2 2 5.7078 -0.5681 6 2 3 1.1355 0.0386 6 2 4 -8.6434 -0.0354 6 2 5 -6.9295 0.1575 6 2 6 1.0741 0.2092 6 2 7 4.1863 0.0141 6 2 8 1.3247 -0.0527 6 2 9 0.0814 -0.0794 6 2 10 -1.1938 0.0511 6 2 11 -0.3069 0.0015 6 2 12 0.2504 -0.0155 6 2 13 2.1106 0.0563 6 2 14 1.8732 0.0360 6 2 15 -1.0299 -0.0056 6 2 16 -1.8449 0.0907 6 2 17 -1.9077 0.0311 6 2 18 0.5906 -0.0198 6 2 19 1.4087 -0.0349 6 2 20 0.5904 0.0061 6 2 21 -0.2650 0.0139 6 2 22 -0.8185 0.0219 6 2 23 0.4304 -0.0831 6 2 24 0.8221 0.1293 6 3 0 1.3773 -1.2259 6 3 1 5.1115 -0.0205 6 3 2 1.5718 0.5780 6 3 3 -7.9139 0.1725 6 3 4 -8.3267 0.1587 6 3 5 0.5103 -0.0037 6 3 6 4.7736 -0.2468 6 3 7 1.9187 -0.1089 6 3 8 -0.5480 -0.0237 6 3 9 -0.8492 0.1256 6 3 10 -1.6150 0.0288 6 3 11 0.8495 -0.0123 6 3 12 2.8986 0.0707 6 3 13 2.4778 -0.0092 6 3 14 -1.5559 -0.0787 6 3 15 -3.1038 -0.0156 6 3 16 -1.9057 -0.0069 6 3 17 0.5155 -0.0584 6 3 18 1.6693 0.0221 6 3 19 0.4270 -0.0427 6 3 20 -0.5233 0.0793 6 3 21 -0.6980 0.0344 6 3 22 0.7320 0.0512 6 3 23 1.0951 0.0747 6 3 24 -0.1602 -0.0633 6 4 0 3.2724 1.1218 6 4 1 1.1337 0.3308 6 4 2 -6.8436 -0.4908 6 4 3 -7.6231 -0.0663 6 4 4 -0.3620 -0.1512 6 4 5 4.7021 -0.0829 6 4 6 2.5482 0.1419 6 4 7 -0.8379 0.0565 6 4 8 -1.3913 0.0070 6 4 9 -1.9592 -0.0217 6 4 10 0.4403 -0.0262 6 4 11 4.2970 0.0406 6 4 12 1.9064 -0.1110 6 4 13 -1.7982 -0.0127 6 4 14 -3.8339 -0.0678 6 4 15 -1.7223 0.0210 6 4 16 0.3411 -0.0259 6 4 17 1.5854 0.0417 6 4 18 0.3157 -0.0189 6 4 19 -0.3671 -0.0412 6 4 20 -0.8037 0.0099 6 4 21 1.1127 -0.0881 6 4 22 1.3353 0.1672 6 4 23 -0.7207 -0.1856 6 4 24 -1.0658 -0.1491 6 5 0 -0.3850 -0.9090 6 5 1 -4.8964 -0.6963 6 5 2 -6.6048 0.3962 6 5 3 0.0495 0.1684 6 5 4 3.7492 0.1245 6 5 5 2.4527 0.1635 6 5 6 -0.3585 -0.1903 6 5 7 -2.0713 -0.1338 6 5 8 -1.6566 -0.0571 6 5 9 0.8792 0.0607 6 5 10 4.3918 0.0359 6 5 11 2.2550 -0.0808 6 5 12 -2.9597 0.0332 6 5 13 -2.6902 0.0585 6 5 14 -2.0122 -0.0360 6 5 15 0.5935 0.0566 6 5 16 0.6977 -0.0706 6 5 17 0.2122 0.0018 6 5 18 -0.5082 -0.0917 6 5 19 0.1005 0.0162 6 5 20 0.7128 -0.0986 6 5 21 1.6337 0.0381 6 5 22 -0.9783 -0.0705 6 5 23 -1.2297 -0.2407 6 6 0 -3.9796 0.5223 6 6 1 -4.3194 0.8079 6 6 2 -0.6008 -0.1743 6 6 3 3.6542 -0.1216 6 6 4 1.0764 -0.0678 6 6 5 0.0141 -0.2237 6 6 6 -1.1012 0.0347 6 6 7 -1.3926 0.0920 6 6 8 2.1454 0.0284 6 6 9 4.1886 0.0459 6 6 10 1.6237 -0.0389 6 6 11 -2.2511 0.0721 6 6 12 -2.7087 -0.0053 6 6 13 -0.3741 -0.0333 6 6 14 -0.6498 0.0584 6 6 15 0.8586 -0.0506 6 6 16 -0.7452 0.0500 6 6 17 -0.1080 -0.0299 6 6 18 0.9993 0.0472 6 6 19 0.9993 -0.0521 6 6 20 0.3640 -0.0973 6 6 21 -0.2189 -0.0501 6 6 22 -1.1305 -0.2273 6 6 23 0.0281 0.5054 6 7 0 -3.5443 -0.0621 6 7 1 -0.1401 -0.9559 6 7 2 2.1886 0.0362 6 7 3 1.0168 0.1496 6 7 4 -0.9518 0.0194 6 7 5 0.6863 0.2727 6 7 6 -0.2536 -0.0290 6 7 7 2.2469 -0.1202 6 7 8 4.1466 -0.0399 6 7 9 0.7296 0.0252 6 7 10 -2.0676 0.0723 6 7 11 -1.3757 -0.0777 6 7 12 -0.3042 -0.0093 6 7 13 0.2710 0.0861 6 7 14 -0.3048 0.0179 6 7 15 0.0882 0.0511 6 7 16 -0.5901 0.1011 6 7 17 1.7982 -0.1251 6 7 18 1.2791 0.0865 6 7 19 -0.7100 -0.2361 6 7 20 -0.1699 0.0988 6 7 21 -0.0427 -0.1813 6 7 22 -0.3131 0.2390 6 8 0 -1.2102 -0.3237 6 8 1 2.2509 0.7790 6 8 2 0.0889 0.1937 6 8 3 -0.8531 -0.1598 6 8 4 0.7914 0.0577 6 8 5 1.1739 -0.1911 6 8 6 1.3970 -0.1279 6 8 7 3.1650 0.0804 6 8 8 0.4711 0.0197 6 8 9 -1.8532 0.0412 6 8 10 -1.0653 -0.0453 6 8 11 0.5104 0.0097 6 8 12 0.3067 0.0803 6 8 13 0.2283 -0.1044 6 8 14 0.1594 0.0817 6 8 15 -0.0935 -0.0011 6 8 16 0.9625 -0.0334 6 8 17 1.4395 -0.0362 6 8 18 -0.4999 0.0239 6 8 19 -0.3272 -0.0580 6 8 20 0.7584 0.1747 6 8 21 -0.5050 -0.1893 6 8 22 -0.1193 0.4758 6 9 0 0.5891 0.6978 6 9 1 0.8916 -0.6720 6 9 2 -1.7292 -0.3898 6 9 3 1.0507 0.0648 6 9 4 1.0559 -0.0804 6 9 5 0.3206 0.1925 6 9 6 1.6988 0.1143 6 9 7 0.5617 -0.0891 6 9 8 -1.0157 -0.0546 6 9 9 -1.0527 -0.0430 6 9 10 -0.1990 0.0749 6 9 11 0.8307 -0.0560 6 9 12 0.1988 -0.1177 6 9 13 0.5922 0.0220 6 9 14 0.5242 0.0187 6 9 15 -0.1734 -0.0701 6 9 16 1.3663 0.0948 6 9 17 0.1120 0.0154 6 9 18 0.4164 0.0033 6 9 19 0.6650 0.0801 6 9 20 -0.2890 -0.0268 6 9 21 -0.4351 0.0088 6 10 0 -0.5556 -0.8909 6 10 1 -0.4476 0.2791 6 10 2 -0.0855 0.3876 6 10 3 1.2196 -0.0454 6 10 4 -0.9805 0.1397 6 10 5 0.3836 -0.0300 6 10 6 1.0679 -0.2114 6 10 7 -0.3502 -0.0399 6 10 8 -0.5724 0.0298 6 10 9 -1.4079 0.0316 6 10 10 0.0048 -0.0009 6 10 11 0.7912 -0.0864 6 10 12 0.4756 0.0918 6 10 13 0.9581 -0.0420 6 10 14 0.2164 -0.0957 6 10 15 0.1904 0.1246 6 10 16 1.5612 0.0157 6 10 17 0.0213 0.0751 6 10 18 1.1281 -0.0187 6 10 19 -0.2395 0.1313 6 10 20 -0.4808 -0.1130 6 11 0 -0.7239 0.9831 6 11 1 0.9049 -0.0388 6 11 2 -0.0740 -0.4345 6 11 3 -0.8402 0.0345 6 11 4 -0.5412 -0.1277 6 11 5 1.3136 -0.0048 6 11 6 0.3974 0.0999 6 11 7 -0.5353 -0.0001 6 11 8 -1.1857 0.0763 6 11 9 -1.2473 -0.0398 6 11 10 0.9730 0.0864 6 11 11 0.9539 0.0023 6 11 12 0.5362 -0.0796 6 11 13 0.5740 -0.0086 6 11 14 0.5098 0.0472 6 11 15 1.0586 0.1517 6 11 16 0.8170 0.0154 6 11 17 -0.2135 0.2255 6 11 18 0.8313 -0.0906 6 11 19 -0.4564 0.0887 6 12 0 1.0053 -0.8129 6 12 1 0.1960 -0.3064 6 12 2 -1.4811 0.4104 6 12 3 -0.1999 -0.0248 6 12 4 1.3275 0.0823 6 12 5 0.9356 0.0819 6 12 6 -0.2145 -0.1014 6 12 7 -0.6660 0.0167 6 12 8 -0.9975 0.0369 6 12 9 0.4456 0.0167 6 12 10 1.4097 -0.0040 6 12 11 0.1018 -0.0823 6 12 12 -0.0431 0.1325 6 12 13 0.9741 0.1396 6 12 14 1.2619 0.0349 6 12 15 0.5654 0.2247 6 12 16 -0.3528 0.0489 6 12 17 0.1429 0.1378 6 13 0 0.5363 0.5688 6 13 1 -1.0591 0.4766 6 13 2 -0.5965 -0.2574 6 13 3 1.5838 -0.1241 6 13 4 1.6365 -0.0329 6 13 5 0.1749 -0.1323 6 13 6 -0.2598 0.1252 6 13 7 -0.5169 -0.0854 6 13 8 0.1120 0.0623 6 13 9 1.1410 -0.0754 6 13 10 0.0219 0.0343 6 13 11 -0.4027 0.2414 6 13 12 0.6526 -0.0495 6 13 13 1.5646 0.1367 6 13 14 0.5957 0.1220 6 13 15 -0.3249 0.1526 6 13 16 -0.3057 -0.0861 6 14 0 0.0324 -0.3286 6 14 1 -0.5704 -0.6357 6 14 2 0.8300 0.0789 6 14 3 2.0577 -0.0028 6 14 4 0.6383 0.0187 6 14 5 -0.3999 0.1212 6 14 6 -0.3481 -0.1186 6 14 7 -0.0209 -0.0915 6 14 8 0.3446 0.0758 6 14 9 0.3334 -0.0399 6 14 10 -0.0840 0.2483 6 14 11 0.4910 -0.1778 6 14 12 0.7102 -0.0867 6 14 13 0.6782 0.3735 6 15 0 0.2875 -0.2858 6 15 1 0.0877 0.5632 6 15 2 1.0000 0.0456 6 15 3 0.7575 -0.0934 6 15 4 -0.5604 0.0859 6 15 5 -0.1873 -0.1811 6 15 6 -0.0006 -0.0179 6 15 7 0.0108 0.0041 6 15 8 -0.1482 -0.0082 6 15 9 0.8598 0.0924 6 15 10 0.1824 -0.1188 7 -10 0 -0.0692 0.3063 7 -10 1 -0.1893 -0.1811 7 -10 2 0.6398 -0.4100 7 -10 3 0.5836 -0.1192 7 -10 4 0.2850 0.2984 7 -10 5 -0.3404 0.2084 7 -10 6 -0.6412 -0.0965 7 -10 7 0.5173 -0.2389 7 -9 0 0.9913 -0.3200 7 -9 1 1.0146 0.0684 7 -9 2 0.8243 0.1380 7 -9 3 -0.7464 0.2752 7 -9 4 -0.5960 0.2109 7 -9 5 -0.1159 -0.2069 7 -9 6 0.0718 -0.3829 7 -9 7 -0.0177 -0.3754 7 -9 8 -0.8135 -0.1341 7 -9 9 0.6311 0.2558 7 -9 10 0.2005 0.2819 7 -9 11 0.2034 0.0015 7 -9 12 -0.6604 -0.3155 7 -8 0 1.6391 0.6391 7 -8 1 0.0678 0.0437 7 -8 2 -0.8896 -0.3072 7 -8 3 -0.8479 -0.1341 7 -8 4 0.1187 -0.1421 7 -8 5 -0.1720 -0.0164 7 -8 6 0.1749 0.0067 7 -8 7 0.7608 -0.0363 7 -8 8 0.3422 0.1005 7 -8 9 0.0660 0.0885 7 -8 10 -0.4054 -0.0294 7 -8 11 -0.2527 -0.1666 7 -8 12 -0.3109 -0.2617 7 -8 13 0.5400 -0.0944 7 -8 14 -0.2885 0.0002 7 -8 15 0.1800 -0.1303 7 -7 0 -0.1825 -0.5327 7 -7 1 -1.0043 -0.3567 7 -7 2 -0.0622 0.1503 7 -7 3 0.2148 0.1541 7 -7 4 -0.8321 0.2568 7 -7 5 0.4968 0.1101 7 -7 6 1.8217 -0.1910 7 -7 7 0.4712 -0.2296 7 -7 8 -1.0658 -0.0768 7 -7 9 -0.8774 0.0964 7 -7 10 0.0634 0.1798 7 -7 11 -0.2241 -0.0229 7 -7 12 0.4624 -0.0560 7 -7 13 0.5458 -0.0731 7 -7 14 -0.0465 -0.1577 7 -7 15 -0.2192 -0.1833 7 -7 16 -1.2465 -0.1036 7 -7 17 -0.2258 0.0101 7 -6 0 -0.4877 0.5023 7 -6 1 0.5227 0.4465 7 -6 2 0.6914 -0.1412 7 -6 3 -0.9967 -0.1257 7 -6 4 -0.5573 -0.1049 7 -6 5 2.2368 -0.1673 7 -6 6 0.3419 0.0312 7 -6 7 -1.2973 0.0680 7 -6 8 -0.8279 0.1199 7 -6 9 0.0699 0.0956 7 -6 10 0.9102 0.0524 7 -6 11 0.3177 -0.0807 7 -6 12 0.7594 -0.0541 7 -6 13 -0.5252 -0.1365 7 -6 14 -0.5566 -0.0814 7 -6 15 -0.6374 -0.0408 7 -6 16 -1.0447 0.0103 7 -6 17 0.3991 0.0622 7 -6 18 0.0524 -0.0682 7 -5 0 0.9963 -0.2239 7 -5 1 0.3881 -0.7026 7 -5 2 -0.7591 -0.0250 7 -5 3 -0.9588 0.1063 7 -5 4 1.2160 0.1461 7 -5 5 1.1869 0.2515 7 -5 6 -1.2419 0.0170 7 -5 7 -0.4551 -0.2479 7 -5 8 0.4701 -0.1642 7 -5 9 1.1654 0.0277 7 -5 10 1.2614 0.1134 7 -5 11 -0.1842 0.0285 7 -5 12 -0.4728 0.0544 7 -5 13 -0.8811 -0.0181 7 -5 14 0.1585 0.0099 7 -5 15 -0.4309 -0.0491 7 -5 16 -0.6859 -0.0816 7 -5 17 0.8553 -0.0760 7 -5 18 -0.1332 -0.1612 7 -5 19 0.3629 -0.1413 7 -5 20 -0.1927 -0.1199 7 -4 0 0.0752 -0.1145 7 -4 1 -1.2527 0.6702 7 -4 2 0.0732 0.1482 7 -4 3 1.3866 -0.1052 7 -4 4 1.3301 -0.0338 7 -4 5 -0.8938 -0.2375 7 -4 6 -1.1228 -0.2078 7 -4 7 1.0723 -0.0097 7 -4 8 2.0475 0.1545 7 -4 9 1.2277 0.1149 7 -4 10 0.0114 -0.0090 7 -4 11 -0.9213 0.0327 7 -4 12 -0.2746 -0.0259 7 -4 13 0.2712 -0.0432 7 -4 14 0.3973 -0.0384 7 -4 15 -0.2099 -0.0698 7 -4 16 -0.0232 -0.0606 7 -4 17 0.3855 0.0011 7 -4 18 -0.9118 -0.0325 7 -4 19 0.5537 -0.0780 7 -4 20 -0.2261 -0.2594 7 -4 21 -0.3309 -0.3345 7 -3 0 -0.9119 0.4658 7 -3 1 0.5959 -0.6846 7 -3 2 3.1711 -0.3353 7 -3 3 1.2286 0.0627 7 -3 4 -1.3511 -0.0073 7 -3 5 -1.7681 0.1889 7 -3 6 1.3854 0.1769 7 -3 7 2.9518 -0.0491 7 -3 8 1.3007 -0.1754 7 -3 9 -0.5521 -0.1086 7 -3 10 -0.4546 0.0235 7 -3 11 -0.0410 0.0184 7 -3 12 0.8725 -0.0294 7 -3 13 0.9586 0.0705 7 -3 14 0.6515 -0.0259 7 -3 15 -0.0779 0.0360 7 -3 16 -0.7695 -0.0348 7 -3 17 -0.5221 0.0221 7 -3 18 -0.1992 -0.0657 7 -3 19 0.8695 -0.1675 7 -3 20 -0.7012 -0.2407 7 -3 21 -0.0347 -0.0522 7 -2 0 1.3864 -0.7555 7 -2 1 3.9362 0.4218 7 -2 2 1.8108 0.4889 7 -2 3 -2.2883 -0.0049 7 -2 4 -1.5361 0.0807 7 -2 5 1.3133 -0.0953 7 -2 6 2.9003 -0.2700 7 -2 7 0.4672 -0.1297 7 -2 8 -0.5798 0.0812 7 -2 9 -0.2176 0.1448 7 -2 10 0.8074 -0.0121 7 -2 11 1.6376 -0.0149 7 -2 12 1.5855 0.0286 7 -2 13 0.9117 -0.0261 7 -2 14 -0.1241 -0.0108 7 -2 15 -1.1371 0.0250 7 -2 16 -0.4150 -0.0535 7 -2 17 0.2557 0.0787 7 -2 18 0.3499 -0.0204 7 -2 19 -0.2298 0.0329 7 -2 20 -0.5713 0.0253 7 -2 21 0.9659 0.0986 7 -2 22 0.4404 0.1008 7 -1 0 4.1934 1.0223 7 -1 1 1.7592 -0.1962 7 -1 2 -3.0696 -0.5465 7 -1 3 -1.3521 -0.0561 7 -1 4 1.9319 -0.0830 7 -1 5 1.4144 0.0408 7 -1 6 -0.5195 0.2237 7 -1 7 -0.8000 0.1084 7 -1 8 1.3883 -0.0081 7 -1 9 1.4225 -0.1363 7 -1 10 2.2706 -0.0388 7 -1 11 1.7539 0.0145 7 -1 12 0.3117 -0.0358 7 -1 13 -0.2098 0.0186 7 -1 14 -0.7705 0.0679 7 -1 15 0.0261 0.0262 7 -1 16 0.7779 0.0932 7 -1 17 -0.2302 0.0637 7 -1 18 -0.2970 0.0636 7 -1 19 -0.7991 0.0971 7 -1 20 0.9065 0.0052 7 -1 21 1.0753 0.0311 7 -1 22 -0.6183 0.0003 7 -1 23 -0.8368 -0.0256 7 0 0 0.8386 -1.0635 7 0 1 -3.9581 -0.2114 7 0 2 -1.6946 0.5217 7 0 3 3.2549 0.1088 7 0 4 0.7810 0.1347 7 0 5 -2.1594 0.1160 7 0 6 -0.3254 -0.2308 7 0 7 2.6004 -0.2020 7 0 8 3.0650 0.0089 7 0 9 1.5779 0.0784 7 0 10 1.0876 0.0745 7 0 11 -0.3568 -0.0241 7 0 12 -0.5500 0.0641 7 0 13 -0.0505 -0.0047 7 0 14 0.4198 0.0158 7 0 15 0.9487 0.0608 7 0 16 -0.0750 0.0038 7 0 17 -1.1524 -0.0193 7 0 18 -0.3653 0.0895 7 0 19 0.3700 0.0051 7 0 20 1.7836 0.0275 7 0 21 -0.5411 -0.0422 7 0 22 -1.2738 -0.0505 7 0 23 -0.3321 -0.0278 7 1 0 -4.3349 1.0023 7 1 1 -1.4682 0.4708 7 1 2 4.1119 -0.4756 7 1 3 1.2656 -0.1596 7 1 4 -3.6800 -0.0893 7 1 5 -0.6862 -0.1730 7 1 6 4.2738 0.0543 7 1 7 3.8209 0.1799 7 1 8 1.5041 0.0830 7 1 9 -0.5671 -0.0784 7 1 10 -0.9249 -0.0183 7 1 11 -0.5257 0.0053 7 1 12 -0.0785 -0.0390 7 1 13 0.9921 -0.0744 7 1 14 0.8712 0.0665 7 1 15 -0.0535 -0.0250 7 1 16 -1.5316 -0.0397 7 1 17 -1.0393 0.0298 7 1 18 1.2625 -0.0141 7 1 19 1.2562 -0.0372 7 1 20 0.2412 -0.0345 7 1 21 -1.6173 -0.0404 7 1 22 -0.4954 0.0435 7 1 23 0.3155 -0.0103 7 2 0 -0.7864 -0.7037 7 2 1 3.9203 -0.8134 7 2 2 0.8761 0.3074 7 2 3 -4.8400 0.2067 7 2 4 -1.2025 0.0573 7 2 5 5.2173 0.1809 7 2 6 5.1840 -0.0977 7 2 7 0.5093 -0.1897 7 2 8 -0.8241 -0.1310 7 2 9 -1.7026 0.0331 7 2 10 -0.6288 0.0549 7 2 11 0.2327 -0.0567 7 2 12 0.8594 -0.0041 7 2 13 1.3030 0.0071 7 2 14 -1.0525 -0.0353 7 2 15 -1.7525 -0.0520 7 2 16 -1.4049 -0.0027 7 2 17 1.6499 -0.0509 7 2 18 1.9696 -0.0438 7 2 19 -0.1841 -0.0119 7 2 20 -0.6899 0.0109 7 2 21 -0.9487 0.0499 7 2 22 0.4408 -0.1154 7 2 23 0.4560 0.0145 7 3 0 1.6700 0.3599 7 3 1 -0.3403 0.9486 7 3 2 -5.4621 -0.0242 7 3 3 -1.4825 -0.2331 7 3 4 6.1252 -0.0728 7 3 5 5.5931 -0.2895 7 3 6 0.5078 -0.1112 7 3 7 -1.8699 0.0885 7 3 8 -0.6663 0.1091 7 3 9 -1.3713 0.0231 7 3 10 0.6442 -0.0806 7 3 11 1.3947 0.0169 7 3 12 0.5174 -0.0326 7 3 13 -1.5911 -0.0798 7 3 14 -2.5730 -0.0268 7 3 15 -0.2058 0.0450 7 3 16 1.6629 -0.0130 7 3 17 2.5618 0.0201 7 3 18 -0.1396 0.0246 7 3 19 -0.7946 -0.0256 7 3 20 -0.7433 -0.0385 7 3 21 0.0819 -0.1134 7 3 22 0.9098 0.0051 7 3 23 -0.3915 0.0637 7 3 24 -0.4378 -0.2259 7 4 0 -2.2687 0.1878 7 4 1 -4.6479 -0.9292 7 4 2 -1.5347 -0.1026 7 4 3 6.1427 0.1315 7 4 4 5.8005 -0.0288 7 4 5 0.1270 0.1730 7 4 6 -1.9126 0.0843 7 4 7 -0.6127 -0.0959 7 4 8 -0.4594 -0.0690 7 4 9 0.0360 -0.0567 7 4 10 2.4072 0.0378 7 4 11 -0.1598 -0.0498 7 4 12 -2.6688 -0.0005 7 4 13 -2.1188 0.0279 7 4 14 0.8836 0.0580 7 4 15 2.5573 0.0355 7 4 16 1.8619 -0.0174 7 4 17 0.0697 0.0470 7 4 18 -1.2256 -0.0506 7 4 19 -0.8252 -0.0348 7 4 20 0.3125 -0.0527 7 4 21 1.3649 0.1385 7 4 22 -0.5203 0.0344 7 4 23 -0.9768 -0.3124 7 5 0 -3.6931 -0.5460 7 5 1 -0.9869 0.8203 7 5 2 4.8860 0.3731 7 5 3 5.4202 -0.1575 7 5 4 0.3244 0.0531 7 5 5 -1.7412 -0.2062 7 5 6 -0.5740 -0.1791 7 5 7 -0.2032 0.0438 7 5 8 0.2733 0.0939 7 5 9 2.2109 0.0469 7 5 10 0.2424 -0.0361 7 5 11 -3.5813 -0.0027 7 5 12 -1.6643 0.0741 7 5 13 1.7227 -0.0986 7 5 14 3.0882 0.0686 7 5 15 1.3571 -0.0629 7 5 16 -0.2372 0.0434 7 5 17 -1.2303 0.0336 7 5 18 -0.4528 0.0530 7 5 19 0.4173 0.0391 7 5 20 1.5408 0.0245 7 5 21 -0.6005 0.0515 7 5 22 -1.4431 -0.3400 7 5 23 0.3134 0.1804 7 6 0 -0.5262 0.8873 7 6 1 3.2118 -0.5011 7 6 2 4.3617 -0.4450 7 6 3 0.9092 0.0829 7 6 4 -0.9036 -0.1190 7 6 5 -0.5875 0.0668 7 6 6 -0.6521 0.1842 7 6 7 0.3903 -0.0122 7 6 8 1.8362 -0.0186 7 6 9 0.1542 -0.0628 7 6 10 -3.2810 -0.0112 7 6 11 -2.1930 -0.0511 7 6 12 2.0089 -0.0726 7 6 13 2.7447 0.0175 7 6 14 1.7522 0.0752 7 6 15 -0.5214 -0.0268 7 6 16 -0.9012 0.0709 7 6 17 -0.0793 -0.0022 7 6 18 0.8050 0.0451 7 6 19 0.0076 -0.1351 7 6 20 -0.2045 -0.0262 7 6 21 -1.3111 -0.1158 7 6 22 0.4416 0.2025 7 6 23 0.5109 0.4550 7 7 0 1.8215 -1.0586 7 7 1 2.9113 0.2364 7 7 2 1.6317 0.5237 7 7 3 -0.1208 -0.0439 7 7 4 -0.1751 0.0757 7 7 5 -1.3283 -0.0495 7 7 6 -0.0076 -0.2221 7 7 7 1.6502 -0.0443 7 7 8 -0.3857 0.0432 7 7 9 -3.0890 0.0100 7 7 10 -2.0624 -0.0628 7 7 11 1.0019 -0.0288 7 7 12 2.7815 0.0922 7 7 13 1.3023 -0.0241 7 7 14 0.2058 -0.0321 7 7 15 -1.4178 -0.0209 7 7 16 0.1064 -0.1242 7 7 17 0.8074 0.0207 7 7 18 -0.9401 -0.1461 7 7 19 -0.9131 -0.0024 7 7 20 0.4342 0.0163 7 7 21 0.1445 0.1007 7 7 22 0.6273 0.4136 7 8 0 2.3237 1.0511 7 8 1 1.7156 0.1395 7 8 2 0.4072 -0.5312 7 8 3 -0.0078 -0.0081 7 8 4 -1.0487 -0.1422 7 8 5 -0.7911 -0.1060 7 8 6 1.6738 0.1604 7 8 7 -0.6182 0.0143 7 8 8 -2.9698 0.0321 7 8 9 -2.1051 -0.0355 7 8 10 0.9123 0.0010 7 8 11 1.7418 0.0438 7 8 12 1.2943 -0.1483 7 8 13 -0.5179 -0.0441 7 8 14 -1.0816 0.0151 7 8 15 -0.8859 -0.0446 7 8 16 0.9609 -0.0690 7 8 17 -0.5763 0.0440 7 8 18 -1.3578 -0.1665 7 8 19 1.0116 0.1479 7 8 20 0.4369 -0.2238 7 8 21 -0.0117 0.2385 7 8 22 0.1833 -0.0340 7 9 0 2.0289 -0.8744 7 9 1 0.0023 -0.4155 7 9 2 0.1779 0.4260 7 9 3 -0.1216 0.0612 7 9 4 -1.0534 0.0594 7 9 5 1.1376 0.1267 7 9 6 0.1508 -0.1666 7 9 7 -2.8142 -0.0625 7 9 8 -1.7944 0.0661 7 9 9 0.1495 -0.0022 7 9 10 2.0265 -0.0276 7 9 11 0.1629 -0.0868 7 9 12 -0.5570 0.0381 7 9 13 -1.3986 0.1389 7 9 14 -0.8539 -0.0525 7 9 15 0.4291 0.0310 7 9 16 0.1956 -0.1046 7 9 17 -0.8176 -0.0344 7 9 18 0.0152 -0.1162 7 9 19 0.4292 -0.0154 7 9 20 -0.6349 -0.2251 7 9 21 0.4606 0.2807 7 10 0 0.3455 0.6390 7 10 1 -0.0927 0.6327 7 10 2 0.7921 -0.2774 7 10 3 -0.6732 -0.0907 7 10 4 0.0514 -0.0125 7 10 5 1.0114 -0.2229 7 10 6 -2.0149 0.0847 7 10 7 -1.6076 0.0902 7 10 8 0.0325 -0.0124 7 10 9 1.4199 -0.0091 7 10 10 1.1923 -0.0087 7 10 11 -1.5419 0.1548 7 10 12 -0.7437 0.0371 7 10 13 -0.8909 -0.0681 7 10 14 -0.0192 -0.0496 7 10 15 0.4469 -0.0264 7 10 16 -0.8480 -0.0530 7 10 17 -0.1666 0.1004 7 10 18 -0.5458 -0.0591 7 10 19 -0.5305 -0.1635 7 10 20 0.0085 -0.0828 7 11 0 1.1629 -0.2471 7 11 1 -0.0574 -0.7127 7 11 2 -0.1321 0.1220 7 11 3 -0.2211 0.0778 7 11 4 0.9199 0.0034 7 11 5 -0.7024 0.1717 7 11 6 -1.6946 -0.0202 7 11 7 0.5347 -0.1207 7 11 8 0.8837 -0.0171 7 11 9 1.5607 0.0841 7 11 10 -0.4347 -0.0066 7 11 11 -1.7795 -0.0184 7 11 12 -0.2271 -0.0881 7 11 13 -0.3632 -0.0285 7 11 14 0.2022 -0.0133 7 11 15 -0.4087 0.0245 7 11 16 -1.2094 0.2463 7 11 17 0.0211 0.0403 7 11 18 -1.0084 -0.2611 7 11 19 -0.0460 -0.3058 7 12 0 0.2886 -0.1062 7 12 1 -1.5160 0.7018 7 12 2 0.8352 -0.0167 7 12 3 1.0143 -0.1335 7 12 4 -0.3154 0.1345 7 12 5 -1.3662 -0.2500 7 12 6 0.0635 -0.0925 7 12 7 0.9627 0.0029 7 12 8 0.7619 0.0333 7 12 9 0.7230 0.0259 7 12 10 -1.6557 -0.1973 7 12 11 -1.1958 0.1106 7 12 12 0.4128 -0.0671 7 12 13 0.2963 -0.0758 7 12 14 -0.2362 0.0326 7 12 15 -1.3503 0.0415 7 12 16 -0.8061 0.2424 7 12 17 0.1505 -0.3776 7 13 0 -1.3273 0.4179 7 13 1 -0.0390 -0.5805 7 13 2 1.9196 -0.2469 7 13 3 -0.2152 0.1652 7 13 4 -1.4311 -0.1335 7 13 5 -0.6468 0.0189 7 13 6 0.0688 0.0151 7 13 7 0.3749 -0.0274 7 13 8 0.7899 0.0583 7 13 9 -0.3997 -0.0949 7 13 10 -1.4982 -0.0098 7 13 11 0.1279 -0.0428 7 13 12 0.9280 -0.1859 7 13 13 -0.1861 0.0094 7 13 14 -1.3450 -0.1454 7 13 15 -1.1027 -0.0218 7 13 16 0.1206 0.0440 7 14 0 -0.6903 -0.6322 7 14 1 0.7135 0.3615 7 14 2 0.4579 0.2827 7 14 3 -1.1404 -0.0540 7 14 4 -1.3872 0.0811 7 14 5 -0.5846 -0.0763 7 14 6 -0.0838 -0.1099 7 14 7 0.7970 0.1558 7 14 8 0.4630 -0.0760 7 14 9 -0.6211 0.0516 7 14 10 -0.2790 -0.1857 7 14 11 0.2029 -0.1991 7 14 12 -0.0131 0.0968 7 14 13 -1.0126 -0.2802 7 15 0 -0.5384 0.9154 7 15 1 -0.0441 0.0415 7 15 2 -0.1491 -0.3093 7 15 3 -1.0391 0.1472 7 15 4 -0.8631 -0.1167 7 15 5 0.2091 -0.0389 7 15 6 0.2751 0.1039 7 15 7 0.4874 -0.0088 7 15 8 0.2472 0.0486 7 15 9 -0.2519 -0.0025 7 15 10 -0.4657 -0.3551 8 -9 0 0.0618 0.2604 8 -9 1 -0.2002 -0.0662 8 -9 2 -0.9169 -0.0489 8 -9 3 -0.3028 0.1336 8 -9 4 0.5583 -0.1376 8 -9 5 0.8714 -0.2894 8 -9 6 0.3701 -0.0775 8 -9 7 -0.0351 0.2825 8 -9 8 1.3043 0.4350 8 -8 0 -1.1511 -0.3428 8 -8 1 -0.9032 -0.4349 8 -8 2 -0.5114 0.1149 8 -8 3 1.0976 0.0827 8 -8 4 0.6913 0.0387 8 -8 5 0.5164 0.1198 8 -8 6 0.1300 0.0975 8 -8 7 0.1054 0.1179 8 -8 8 0.4374 0.0538 8 -8 9 -0.6312 -0.0089 8 -8 10 -0.2688 -0.0463 8 -8 11 -0.6391 -0.1559 8 -8 12 0.5692 0.0465 8 -7 0 -1.7326 -0.0148 8 -7 1 0.4131 0.5048 8 -7 2 0.6517 0.1212 8 -7 3 0.4832 -0.0077 8 -7 4 -0.0248 0.0267 8 -7 5 0.5272 -0.2218 8 -7 6 -0.7266 -0.2315 8 -7 7 -0.6742 0.0441 8 -7 8 0.1769 0.2402 8 -7 9 0.2644 0.1741 8 -7 10 0.0455 -0.0964 8 -7 11 0.1069 -0.1117 8 -7 12 0.8045 0.1036 8 -7 13 0.0435 0.1145 8 -7 14 -0.2957 -0.0936 8 -7 15 -0.2075 0.2603 8 -6 0 -0.1084 0.3879 8 -6 1 1.3402 -0.4423 8 -6 2 -0.8054 -0.2812 8 -6 3 -0.5537 0.0841 8 -6 4 0.6233 -0.0893 8 -6 5 -0.2899 0.0040 8 -6 6 -0.9899 0.1105 8 -6 7 0.3931 0.1450 8 -6 8 0.7422 -0.0379 8 -6 9 0.5018 -0.1232 8 -6 10 -0.2064 -0.1142 8 -6 11 0.2752 0.0055 8 -6 12 -0.0445 0.0237 8 -6 13 0.1979 0.0762 8 -6 14 0.3349 0.1138 8 -6 15 0.6873 0.1755 8 -6 16 0.8411 -0.0254 8 -6 17 -0.0374 0.1254 8 -5 0 0.3517 -0.5992 8 -5 1 -0.6725 0.2609 8 -5 2 -1.3992 0.3776 8 -5 3 1.1690 0.0179 8 -5 4 0.8061 0.0076 8 -5 5 -0.9883 -0.0221 8 -5 6 0.0291 -0.2526 8 -5 7 0.3927 -0.1204 8 -5 8 0.5293 0.0341 8 -5 9 0.3922 0.1919 8 -5 10 -0.5926 -0.0121 8 -5 11 0.0391 -0.0276 8 -5 12 -0.0106 -0.0593 8 -5 13 1.2390 0.0228 8 -5 14 0.4322 -0.0334 8 -5 15 0.1162 -0.0109 8 -5 16 -0.0310 0.1028 8 -5 17 -0.5132 0.1122 8 -5 18 0.1212 0.0750 8 -5 19 -0.2414 0.2385 8 -4 0 -1.2909 0.8107 8 -4 1 -0.1887 -0.0265 8 -4 2 1.4805 -0.4353 8 -4 3 1.2805 -0.0573 8 -4 4 -1.3739 -0.0352 8 -4 5 -1.2855 -0.0751 8 -4 6 0.7142 0.0714 8 -4 7 0.9255 0.2298 8 -4 8 0.6815 0.0677 8 -4 9 -0.5352 -0.1092 8 -4 10 -1.0027 -0.1347 8 -4 11 -0.0369 -0.0324 8 -4 12 0.2973 -0.0993 8 -4 13 0.9926 0.0286 8 -4 14 -0.5156 -0.0040 8 -4 15 -0.6738 0.0912 8 -4 16 -0.5058 0.0972 8 -4 17 -0.5809 0.0065 8 -4 18 0.7806 0.1662 8 -4 19 0.0868 0.1017 8 -4 20 0.0694 0.0832 8 -3 0 0.4435 -0.8062 8 -3 1 2.5955 -0.2802 8 -3 2 0.2039 0.4373 8 -3 3 -2.3261 0.1784 8 -3 4 -2.0384 0.0386 8 -3 5 0.9260 0.0388 8 -3 6 2.2788 -0.0766 8 -3 7 0.4491 -0.1656 8 -3 8 -1.1637 -0.1107 8 -3 9 -1.3731 0.0904 8 -3 10 -0.8590 0.1128 8 -3 11 0.1970 -0.0460 8 -3 12 0.2758 0.0122 8 -3 13 -0.2250 0.0136 8 -3 14 -1.5056 -0.0560 8 -3 15 -0.9793 -0.0440 8 -3 16 0.1679 -0.0251 8 -3 17 0.4548 0.0610 8 -3 18 1.1617 0.1388 8 -3 19 -0.9512 0.0732 8 -3 20 -0.4409 0.2178 8 -3 21 0.0001 0.1306 8 -2 0 2.4745 0.6690 8 -2 1 -0.3146 0.5447 8 -2 2 -4.0006 -0.2971 8 -2 3 -1.8809 -0.2170 8 -2 4 1.0442 -0.1190 8 -2 5 2.5854 -0.1465 8 -2 6 0.5659 0.0096 8 -2 7 -1.6457 0.1367 8 -2 8 -1.5030 0.1982 8 -2 9 -0.6360 0.0161 8 -2 10 0.0796 -0.0828 8 -2 11 0.0180 -0.0639 8 -2 12 -1.5258 -0.0208 8 -2 13 -1.7067 -0.0958 8 -2 14 -1.0124 0.0006 8 -2 15 0.7494 -0.0220 8 -2 16 0.9996 0.0993 8 -2 17 0.0795 0.0378 8 -2 18 -0.1505 0.0639 8 -2 19 -1.4516 0.0427 8 -2 20 0.7425 -0.0128 8 -2 21 0.4549 -0.0638 8 -1 0 -1.0713 -0.4779 8 -1 1 -4.8026 -0.7527 8 -1 2 -2.3016 0.1161 8 -1 3 1.9889 0.2202 8 -1 4 1.8769 0.0757 8 -1 5 0.5674 0.1482 8 -1 6 -1.2793 -0.0147 8 -1 7 -0.8205 -0.0902 8 -1 8 -0.5052 -0.1234 8 -1 9 0.1496 -0.0620 8 -1 10 -0.5288 0.0709 8 -1 11 -2.5971 -0.0237 8 -1 12 -2.3577 0.0018 8 -1 13 -0.0912 0.0606 8 -1 14 1.0656 0.0355 8 -1 15 0.9410 -0.0399 8 -1 16 -0.5653 -0.0221 8 -1 17 -0.3638 -0.1162 8 -1 18 -0.5009 -0.0107 8 -1 19 0.1757 -0.1307 8 -1 20 1.4375 -0.0194 8 -1 21 -0.7759 0.0547 8 -1 22 -0.5524 -0.0023 8 0 0 -4.9746 0.0761 8 0 1 -2.1419 0.8263 8 0 2 2.9485 0.0709 8 0 3 1.9428 -0.1503 8 0 4 -0.7238 -0.0564 8 0 5 -0.6148 -0.2549 8 0 6 -0.1434 -0.1324 8 0 7 0.0650 0.0912 8 0 8 -0.8110 0.1070 8 0 9 -0.8535 0.0897 8 0 10 -2.7404 -0.0443 8 0 11 -2.3645 -0.0441 8 0 12 0.3540 0.0207 8 0 13 1.2665 -0.0137 8 0 14 0.4441 -0.0719 8 0 15 -0.6593 -0.0515 8 0 16 -0.8252 -0.0622 8 0 17 0.2155 -0.0317 8 0 18 0.1042 -0.0487 8 0 19 1.3871 -0.0264 8 0 20 -0.5726 0.0895 8 0 21 -1.3953 -0.0198 8 0 22 0.6255 0.0765 8 0 23 1.0811 0.1120 8 1 0 -0.9490 0.2994 8 1 1 3.3358 -0.8411 8 1 2 1.7254 -0.2321 8 1 3 -2.3630 0.1883 8 1 4 -0.8045 -0.0131 8 1 5 1.1797 0.1402 8 1 6 0.0301 0.1400 8 1 7 -1.2630 -0.0284 8 1 8 -1.8363 -0.1149 8 1 9 -1.8189 -0.0602 8 1 10 -1.7668 -0.0241 8 1 11 0.2349 0.0055 8 1 12 1.2036 -0.0311 8 1 13 0.2639 0.0254 8 1 14 -0.7481 0.0077 8 1 15 -1.1992 0.0195 8 1 16 -0.2963 -0.0124 8 1 17 1.1607 -0.0189 8 1 18 0.6731 -0.0480 8 1 19 -0.0566 0.0330 8 1 20 -1.8020 0.0203 8 1 21 0.5019 0.0844 8 1 22 1.2439 -0.0294 8 1 23 0.6345 -0.2003 8 2 0 2.6163 -0.7301 8 2 1 0.3101 0.6059 8 2 2 -3.0684 0.4610 8 2 3 -0.6519 -0.0918 8 2 4 2.6551 0.0562 8 2 5 0.1380 -0.1532 8 2 6 -2.4951 -0.2321 8 2 7 -1.7563 -0.0217 8 2 8 -1.5067 0.0890 8 2 9 -0.9998 0.1270 8 2 10 0.0902 -0.0082 8 2 11 0.8363 -0.0076 8 2 12 0.5747 0.0034 8 2 13 -1.1250 0.0309 8 2 14 -1.5029 -0.0250 8 2 15 -0.6116 0.0080 8 2 16 1.7981 0.0111 8 2 17 1.5131 0.0119 8 2 18 -1.0824 -0.0216 8 2 19 -0.9869 0.0296 8 2 20 -0.5859 0.0996 8 2 21 1.0869 -0.0602 8 2 22 0.3581 -0.1926 8 2 23 0.2039 0.0899 8 3 0 -0.6082 0.8883 8 3 1 -2.5892 -0.3754 8 3 2 0.6256 -0.5512 8 3 3 3.7297 0.0430 8 3 4 0.0109 -0.0590 8 3 5 -3.4567 -0.0057 8 3 6 -2.1466 0.2004 8 3 7 -0.2317 0.0936 8 3 8 -1.3792 0.0335 8 3 9 -0.0361 -0.0395 8 3 10 0.9310 -0.0269 8 3 11 0.1335 -0.0109 8 3 12 -0.8172 -0.0161 8 3 13 -1.7583 0.0000 8 3 14 0.2989 0.0011 8 3 15 1.6761 0.0600 8 3 16 1.9131 0.0427 8 3 17 -1.3877 -0.0056 8 3 18 -1.6757 -0.0673 8 3 19 -0.3001 0.0452 8 3 20 -0.0294 0.0125 8 3 21 1.0157 -0.0110 8 3 22 0.0566 0.1565 8 3 23 0.4287 -0.0458 8 4 0 -0.4092 -1.1319 8 4 1 1.2791 0.0145 8 4 2 4.2780 0.5327 8 4 3 0.0818 0.0436 8 4 4 -4.0885 0.0773 8 4 5 -2.0046 0.0215 8 4 6 0.0471 -0.1868 8 4 7 -0.5968 -0.0481 8 4 8 -1.2909 0.0431 8 4 9 1.3551 0.0568 8 4 10 0.0723 0.0232 8 4 11 -1.3143 -0.0123 8 4 12 -0.4597 0.0231 8 4 13 0.6622 -0.0410 8 4 14 1.8259 0.0211 8 4 15 0.2803 -0.0223 8 4 16 -0.9073 0.0164 8 4 17 -2.1426 -0.0242 8 4 18 -0.1978 -0.0383 8 4 19 0.4418 0.0506 8 4 20 1.1733 0.0663 8 4 21 0.2446 0.1381 8 4 22 -0.6168 -0.2190 8 4 23 0.4029 -0.0969 8 5 0 2.0952 0.9807 8 5 1 3.2694 0.3174 8 5 2 1.0424 -0.5576 8 5 3 -3.8472 -0.0860 8 5 4 -2.1893 -0.0897 8 5 5 0.4718 -0.1481 8 5 6 -0.5239 0.1365 8 5 7 -1.1251 0.1333 8 5 8 0.4602 0.0402 8 5 9 0.9027 0.0016 8 5 10 -1.6492 -0.0401 8 5 11 -0.2715 -0.0001 8 5 12 1.6712 -0.0900 8 5 13 0.9153 0.0155 8 5 14 -0.6025 -0.0031 8 5 15 -1.5895 -0.0107 8 5 16 -1.0950 0.0819 8 5 17 -0.4923 -0.0506 8 5 18 1.1795 -0.0344 8 5 19 1.1571 -0.0505 8 5 20 -0.1182 0.0308 8 5 21 -1.5351 -0.1348 8 5 22 -0.0025 -0.0109 8 5 23 0.5106 0.4677 8 6 0 2.6100 -0.8515 8 6 1 0.9845 -0.6011 8 6 2 -2.1990 0.3493 8 6 3 -2.4811 0.1321 8 6 4 0.2530 0.0341 8 6 5 -0.2528 0.1462 8 6 6 -1.1475 -0.0849 8 6 7 0.3328 -0.0842 8 6 8 0.7583 -0.0020 8 6 9 -1.0178 0.0003 8 6 10 -0.8267 -0.0089 8 6 11 1.7004 -0.0015 8 6 12 1.1649 0.0237 8 6 13 -1.2033 0.1099 8 6 14 -1.7872 -0.0846 8 6 15 -1.2304 0.0330 8 6 16 -0.1234 -0.0689 8 6 17 0.9819 -0.0411 8 6 18 0.7115 -0.0832 8 6 19 -0.3478 -0.0229 8 6 20 -1.2220 0.0690 8 6 21 -0.1119 0.0669 8 6 22 0.8143 0.3860 8 6 23 0.4424 -0.2554 8 7 0 0.8719 0.4665 8 7 1 -1.0679 0.7828 8 7 2 -1.5041 -0.2199 8 7 3 -0.9332 -0.1596 8 7 4 -0.4713 -0.0080 8 7 5 -0.8388 -0.2163 8 7 6 0.3585 0.0322 8 7 7 0.5673 0.1083 8 7 8 -0.9237 0.0519 8 7 9 -0.6715 0.0260 8 7 10 1.2829 0.0106 8 7 11 1.6401 0.0532 8 7 12 -0.7610 -0.0279 8 7 13 -2.0929 0.0020 8 7 14 -1.8137 -0.0717 8 7 15 -0.3371 0.0090 8 7 16 1.3703 0.0211 8 7 17 0.2561 0.0690 8 7 18 -0.6683 -0.0021 8 7 19 0.2851 0.1117 8 7 20 -0.0730 0.0270 8 7 21 0.4355 0.1817 8 7 22 -0.0037 -0.1400 8 8 0 0.0362 -0.1132 8 8 1 -0.8331 -0.8157 8 8 2 -1.4045 0.0200 8 8 3 -1.7862 0.1559 8 8 4 -0.4107 -0.0030 8 8 5 0.8161 0.1992 8 8 6 0.2252 0.0302 8 8 7 -1.3112 -0.0360 8 8 8 -0.6064 0.0198 8 8 9 1.7018 -0.0292 8 8 10 1.6698 -0.0012 8 8 11 0.0145 -0.0586 8 8 12 -2.1851 0.0161 8 8 13 -1.8757 0.1136 8 8 14 -0.5034 0.0135 8 8 15 1.9434 0.0756 8 8 16 0.8983 0.0653 8 8 17 -1.3120 -0.0427 8 8 18 0.7483 0.1019 8 8 19 0.4971 -0.0286 8 8 20 -0.7051 0.1551 8 8 21 -0.0601 0.1135 8 8 22 -0.3726 -0.3305 8 9 0 -0.5979 -0.3206 8 9 1 -1.7584 0.7358 8 9 2 -1.8704 0.1452 8 9 3 -1.1314 -0.1267 8 9 4 1.2604 0.1477 8 9 5 0.1674 -0.1808 8 9 6 -1.9473 -0.0791 8 9 7 -0.5405 0.1109 8 9 8 1.8198 -0.0623 8 9 9 2.5003 0.0154 8 9 10 -0.1925 0.0161 8 9 11 -1.3767 0.0459 8 9 12 -1.8427 0.0874 8 9 13 0.4266 -0.0237 8 9 14 1.7937 0.0008 8 9 15 1.4516 -0.0593 8 9 16 -1.1792 -0.0010 8 9 17 -0.3981 0.0045 8 9 18 1.1043 0.2126 8 9 19 -1.1227 0.0371 8 9 20 -0.1191 0.3599 8 9 21 0.0351 -0.1606 8 10 0 -1.4467 0.5013 8 10 1 -1.3809 -0.5845 8 10 2 -0.9217 -0.2746 8 10 3 -0.1803 0.1996 8 10 4 0.8472 -0.0794 8 10 5 -1.9627 0.0700 8 10 6 -0.5729 0.1033 8 10 7 2.1318 -0.0817 8 10 8 2.1495 0.0030 8 10 9 0.6594 0.0640 8 10 10 -2.2203 -0.0093 8 10 11 -0.6358 -0.0787 8 10 12 0.5122 -0.0836 8 10 13 2.2332 -0.0417 8 10 14 0.6831 0.0018 8 10 15 -0.6920 -0.0084 8 10 16 -0.5133 0.1527 8 10 17 0.5235 -0.0166 8 10 18 0.0007 0.0861 8 10 19 -0.6975 -0.0366 8 10 20 0.8306 0.2546 8 11 0 -0.8946 -0.8256 8 11 1 -0.5570 0.3037 8 11 2 -0.4755 0.3845 8 11 3 0.0658 -0.0716 8 11 4 -0.4033 0.0905 8 11 5 -1.0401 -0.0633 8 11 6 2.3758 -0.1770 8 11 7 1.5221 0.0994 8 11 8 0.1085 0.0289 8 11 9 -1.5816 -0.0637 8 11 10 -1.8810 -0.0779 8 11 11 1.8265 -0.0331 8 11 12 1.5572 0.0587 8 11 13 0.8790 -0.0273 8 11 14 -0.8799 0.0712 8 11 15 -0.2109 0.0514 8 11 16 0.6618 -0.1212 8 11 17 0.0068 -0.4085 8 11 18 0.0212 -0.1244 8 11 19 0.1782 0.2235 8 12 0 -1.2689 0.7298 8 12 1 0.4716 -0.0868 8 12 2 0.0688 -0.3915 8 12 3 -0.3951 0.1109 8 12 4 -0.4253 -0.1318 8 12 5 1.1490 -0.0289 8 12 6 1.7554 0.1734 8 12 7 -0.9127 0.0514 8 12 8 -0.9450 -0.0266 8 12 9 -1.7607 -0.0741 8 12 10 0.4491 0.1208 8 12 11 2.5173 0.0510 8 12 12 0.3116 -0.0069 8 12 13 -0.1940 -0.0039 8 12 14 -0.7073 -0.0498 8 12 15 0.3012 -0.1624 8 12 16 0.6663 -0.5035 8 12 17 -0.1338 -0.3489 8 13 0 -0.4348 -0.7868 8 13 1 1.4767 -0.1536 8 13 2 -0.6983 0.4006 8 13 3 -0.4876 -0.0195 8 13 4 0.6793 0.0491 8 13 5 1.0039 0.2086 8 13 6 -0.1073 -0.0928 8 13 7 -0.8797 0.0903 8 13 8 -0.4988 -0.0697 8 13 9 -0.8046 -0.0089 8 13 10 1.3525 0.1924 8 13 11 1.1088 -0.0567 8 13 12 -0.3506 0.1557 8 13 13 -0.5201 -0.1989 8 13 14 -0.5011 -0.1413 8 13 15 0.7342 -0.0802 8 13 16 0.5211 -0.4252 8 14 0 0.6650 0.6122 8 14 1 0.7865 0.4584 8 14 2 -0.6763 -0.2979 8 14 3 0.4707 0.0136 8 14 4 0.5971 0.0631 8 14 5 0.1846 -0.1098 8 14 6 0.1528 0.0873 8 14 7 -0.1190 0.0015 8 14 8 -0.5520 -0.0652 8 14 9 -0.4340 0.1519 8 14 10 0.7146 0.0705 8 14 11 0.2806 0.1478 8 14 12 -0.4094 -0.0037 8 14 13 -0.3407 -0.2095 8 15 0 0.9488 -0.2062 8 15 1 0.5120 -0.5680 8 15 2 0.1783 0.1199 8 15 3 0.2480 0.0408 8 15 4 0.3279 -0.0741 8 15 5 0.1984 0.1177 8 15 6 0.3178 -0.0337 8 15 7 -0.3420 0.0113 8 15 8 -0.6251 0.1262 8 15 9 -0.2351 -0.0894 8 15 10 0.3577 0.1629 9 -8 1 0.1208 0.3700 9 -8 2 0.2478 0.3620 9 -8 3 -0.0318 -0.0070 9 -8 4 -0.3659 -0.1738 9 -8 5 -0.7085 -0.0387 9 -8 6 -0.3371 0.1410 9 -8 7 -0.2416 -0.1152 9 -8 8 -1.0275 -0.2175 9 -7 0 0.9903 0.5240 9 -7 1 0.3254 0.0864 9 -7 2 0.0509 -0.2760 9 -7 3 -0.7095 -0.1609 9 -7 4 -0.0455 -0.0773 9 -7 5 -0.5768 0.0584 9 -7 6 0.0446 0.0753 9 -7 7 0.1323 0.0856 9 -7 8 -0.3218 0.1802 9 -7 9 -0.1292 -0.0929 9 -7 10 -0.4705 -0.3152 9 -7 11 0.5398 0.0057 9 -7 12 -0.1458 0.1555 9 -6 0 1.7679 -0.4992 9 -6 1 -0.5238 -0.2798 9 -6 2 -0.4131 0.2103 9 -6 3 -0.0618 0.2128 9 -6 4 0.5384 0.1129 9 -6 5 -0.1874 0.0347 9 -6 6 0.7127 0.0114 9 -6 7 -0.2743 -0.0030 9 -6 8 -0.5265 -0.0891 9 -6 9 -0.5739 -0.1075 9 -6 10 -0.3405 0.0281 9 -6 11 0.3362 0.0850 9 -6 12 -0.1075 -0.0409 9 -6 13 -0.3744 -0.1217 9 -6 14 -0.3422 0.2086 9 -6 15 -0.9650 -0.2977 9 -5 0 0.8622 0.3271 9 -5 1 -1.0309 0.3919 9 -5 2 0.9956 -0.0340 9 -5 3 0.5298 -0.1421 9 -5 4 -0.1283 -0.0887 9 -5 5 -0.0770 -0.0906 9 -5 6 0.0633 0.0554 9 -5 7 -0.3486 0.0478 9 -5 8 0.0849 0.1892 9 -5 9 -0.8958 0.0802 9 -5 10 -0.2034 -0.0951 9 -5 11 0.0176 -0.1220 9 -5 12 -0.2769 -0.0273 9 -5 13 -1.2161 0.0120 9 -5 14 -1.0579 0.0567 9 -5 15 -0.9329 -0.0592 9 -5 16 0.4093 0.1978 9 -5 17 0.7619 -0.2785 9 -4 0 0.5897 -0.2563 9 -4 1 0.7401 -0.4922 9 -4 2 0.7353 -0.0304 9 -4 3 -1.4347 0.1239 9 -4 4 -0.4135 0.1362 9 -4 5 0.7852 0.0983 9 -4 6 0.5225 0.0461 9 -4 7 0.1384 -0.0589 9 -4 8 -1.1460 0.0166 9 -4 9 -1.5416 -0.1202 9 -4 10 -0.0867 0.0049 9 -4 11 -0.3619 0.0415 9 -4 12 0.0057 0.1035 9 -4 13 -0.7964 0.0431 9 -4 14 -0.2781 0.0918 9 -4 15 0.0666 0.0181 9 -4 16 1.0842 -0.1418 9 -4 17 0.6638 -0.1484 9 -4 18 -0.2321 0.0713 9 -3 0 1.5456 -0.0872 9 -3 1 -0.4562 0.5664 9 -3 2 -1.8117 0.1277 9 -3 3 -0.6115 -0.0747 9 -3 4 1.6611 -0.0886 9 -3 5 1.3787 -0.1537 9 -3 6 -0.6517 -0.0663 9 -3 7 -1.8627 0.0245 9 -3 8 -1.7867 0.1602 9 -3 9 -0.3882 0.1081 9 -3 10 0.6751 0.0458 9 -3 11 0.7508 -0.0554 9 -3 12 0.9149 0.0051 9 -3 13 -0.5448 -0.0415 9 -3 14 0.1724 0.0446 9 -3 15 1.0008 -0.0356 9 -3 16 0.9979 0.0232 9 -3 17 0.1165 0.1403 9 -3 18 -0.6069 -0.1077 9 -3 19 0.3323 -0.1586 9 -3 20 0.1728 -0.1872 9 -2 0 -0.7936 0.3243 9 -2 1 -2.5018 -0.4891 9 -2 2 0.2461 -0.2742 9 -2 3 1.9966 0.0264 9 -2 4 1.4329 0.0384 9 -2 5 -0.6714 0.1982 9 -2 6 -2.5596 0.1218 9 -2 7 -1.4239 0.0309 9 -2 8 0.1092 -0.0279 9 -2 9 1.0089 -0.0833 9 -2 10 1.5040 -0.0905 9 -2 11 0.6175 0.0067 9 -2 12 0.2192 0.0197 9 -2 13 0.1474 0.0534 9 -2 14 1.6167 0.1080 9 -2 15 0.9983 0.0717 9 -2 16 -0.5761 0.0434 9 -2 17 -0.2499 -0.0658 9 -2 18 -0.1696 -0.1584 9 -2 19 1.4734 -0.1108 9 -2 20 0.5639 -0.1875 9 -2 21 0.0598 0.1333 9 -1 0 -2.8827 -0.5820 9 -1 1 0.3075 0.3906 9 -1 2 3.4461 0.3626 9 -1 3 1.3089 0.0131 9 -1 4 -0.6149 0.0797 9 -1 5 -2.2328 -0.1055 9 -1 6 -1.4812 -0.1698 9 -1 7 0.4830 -0.0354 9 -1 8 0.9286 0.0189 9 -1 9 1.0334 0.0995 9 -1 10 0.2554 0.0368 9 -1 11 -0.0340 0.0578 9 -1 12 1.7495 -0.0261 9 -1 13 1.8111 0.0359 9 -1 14 0.8882 -0.0175 9 -1 15 -1.0996 -0.0212 9 -1 16 -0.5830 -0.0661 9 -1 17 0.5262 0.0255 9 -1 18 0.4974 0.0004 9 -1 19 1.7160 -0.0093 9 -1 20 -0.8847 0.0456 9 -1 21 -0.6336 0.0260 9 0 0 0.2807 0.7817 9 0 1 4.3198 -0.1705 9 0 2 2.4778 -0.4335 9 0 3 -1.6783 -0.0485 9 0 4 -1.8574 -0.0997 9 0 5 -1.1923 0.0392 9 0 6 0.5419 0.2114 9 0 7 0.5741 0.0765 9 0 8 0.4453 0.0266 9 0 9 -0.1420 -0.0207 9 0 10 0.0888 -0.0708 9 0 11 2.2673 -0.0204 9 0 12 2.6458 -0.0387 9 0 13 0.0785 0.0072 9 0 14 -1.0402 0.0049 9 0 15 -0.6743 0.0610 9 0 16 0.5593 0.0170 9 0 17 0.0578 0.0561 9 0 18 0.9214 0.0053 9 0 19 0.1815 0.0514 9 0 20 -1.6319 -0.1229 9 0 21 0.7237 -0.1608 9 0 22 0.5935 -0.0212 9 1 0 3.8114 -0.9185 9 1 1 2.2795 -0.1363 9 1 2 -1.9644 0.4325 9 1 3 -1.8975 0.0538 9 1 4 0.2361 0.1130 9 1 5 0.1921 0.0666 9 1 6 0.3936 -0.1630 9 1 7 0.0109 -0.0967 9 1 8 0.1170 0.0082 9 1 9 -0.0096 0.0119 9 1 10 2.0968 0.0416 9 1 11 2.6801 0.0561 9 1 12 0.2067 0.0139 9 1 13 -1.3610 0.0034 9 1 14 -0.3597 0.0529 9 1 15 0.4084 -0.0476 9 1 16 0.4667 -0.0745 9 1 17 0.0604 0.0054 9 1 18 0.5897 0.0574 9 1 19 -1.0719 -0.0333 9 1 20 0.3161 -0.0914 9 1 21 1.0870 0.0229 9 1 22 -0.3707 -0.0470 9 2 0 0.7932 0.7356 9 2 1 -1.4592 0.3895 9 2 2 -0.5376 -0.3955 9 2 3 1.4366 -0.1097 9 2 4 -0.4620 -0.1091 9 2 5 -0.7007 -0.1913 9 2 6 0.9562 0.1543 9 2 7 0.4097 0.1419 9 2 8 0.0094 0.0602 9 2 9 1.1594 0.0095 9 2 10 2.5717 0.0149 9 2 11 0.6932 -0.0374 9 2 12 -1.1500 -0.0567 9 2 13 -0.5843 0.0064 9 2 14 0.7647 -0.0127 9 2 15 1.1877 -0.0612 9 2 16 0.3982 0.0395 9 2 17 -0.6936 0.0216 9 2 18 0.0058 0.0200 9 2 19 -0.1286 0.0010 9 2 20 1.1201 0.0210 9 2 21 -0.2116 -0.0958 9 2 22 -0.3872 0.1171 9 2 23 -0.6308 0.2752 9 3 0 -0.2277 -0.6203 9 3 1 1.0279 -0.5942 9 3 2 1.5522 0.2618 9 3 3 -1.4878 0.1374 9 3 4 -2.0275 -0.0013 9 3 5 1.8954 0.2081 9 3 6 1.6596 0.0070 9 3 7 -0.7443 -0.1226 9 3 8 0.4926 -0.0043 9 3 9 2.3952 -0.0308 9 3 10 1.3609 -0.0214 9 3 11 -0.5510 -0.0186 9 3 12 -0.7719 0.0584 9 3 13 0.7616 0.0241 9 3 14 1.5956 0.0282 9 3 15 0.7835 0.0430 9 3 16 -1.3573 -0.0369 9 3 17 -0.7351 -0.0747 9 3 18 0.9705 0.0370 9 3 19 0.3906 0.0452 9 3 20 0.8500 -0.0429 9 3 21 -0.4009 0.0407 9 3 22 -0.1159 0.1254 9 3 23 -0.7860 -0.1086 9 4 0 1.0782 0.3408 9 4 1 0.7903 0.7659 9 4 2 -2.2114 -0.1224 9 4 3 -2.5618 -0.1639 9 4 4 1.9403 -0.0097 9 4 5 2.2707 -0.1880 9 4 6 -0.7519 -0.0071 9 4 7 -0.4932 0.1330 9 4 8 2.6352 0.0490 9 4 9 1.9249 -0.0126 9 4 10 -0.5077 0.0053 9 4 11 -0.4970 0.0517 9 4 12 0.0994 -0.0220 9 4 13 1.4591 0.0228 9 4 14 0.4617 0.0440 9 4 15 -0.7898 -0.0274 9 4 16 -1.3542 -0.0411 9 4 17 1.0004 -0.0008 9 4 18 1.1346 0.0522 9 4 19 0.5433 -0.0272 9 4 20 -0.0013 0.0292 9 4 21 -1.1854 -0.0220 9 4 22 -0.2458 -0.0969 9 4 23 -0.8805 0.1454 9 5 0 -0.6264 0.0715 9 5 1 -1.5864 -0.8194 9 5 2 -2.7349 -0.0751 9 5 3 1.0437 0.1836 9 5 4 2.2121 -0.0447 9 5 5 -0.7716 0.2156 9 5 6 -0.4482 0.1406 9 5 7 1.7840 -0.0667 9 5 8 2.6181 -0.0322 9 5 9 -0.7462 -0.0298 9 5 10 -1.2207 -0.0141 9 5 11 0.4894 -0.0114 9 5 12 0.5183 0.0159 9 5 13 0.6097 0.1078 9 5 14 -0.7678 -0.0229 9 5 15 -0.4561 0.0536 9 5 16 -0.1667 -0.0210 9 5 17 1.7010 -0.0311 9 5 18 0.4390 -0.0353 9 5 19 -0.5419 0.0100 9 5 20 -1.4659 0.0928 9 5 21 -0.2870 -0.0600 9 5 22 0.5023 0.2061 9 5 23 -0.0552 -0.0498 9 6 0 -1.3248 -0.3897 9 6 1 -1.9140 0.6766 9 6 2 -0.5113 0.2606 9 6 3 1.8043 -0.1427 9 6 4 -0.2057 0.0833 9 6 5 -1.0238 -0.0942 9 6 6 1.3649 -0.1240 9 6 7 2.0406 0.0766 9 6 8 -0.0330 0.0299 9 6 9 -2.1456 -0.0067 9 6 10 0.3031 0.0168 9 6 11 1.2165 0.0363 9 6 12 -0.2944 0.0564 9 6 13 -0.2461 -0.0133 9 6 14 -0.5815 -0.0079 9 6 15 0.2276 0.0162 9 6 16 0.8584 -0.0454 9 6 17 1.2251 0.0190 9 6 18 -1.0400 0.0065 9 6 19 -0.8661 0.1258 9 6 20 -0.2747 0.0142 9 6 21 0.9380 0.0832 9 6 22 0.3191 -0.0309 9 7 0 -1.3770 0.7354 9 7 1 -0.5166 -0.5328 9 7 2 0.4534 -0.3788 9 7 3 0.3582 0.1197 9 7 4 -1.0368 -0.1005 9 7 5 0.5060 0.0951 9 7 6 2.1086 0.1721 9 7 7 0.0846 0.0168 9 7 8 -1.7050 -0.0129 9 7 9 -0.2984 -0.0079 9 7 10 1.4577 -0.0227 9 7 11 -0.0779 -0.0403 9 7 12 -1.0417 0.0325 9 7 13 0.0259 -0.0064 9 7 14 0.2461 0.0193 9 7 15 1.5996 -0.0054 9 7 16 0.9081 0.0522 9 7 17 -0.4585 -0.0273 9 7 18 -0.6308 -0.0011 9 7 19 0.0840 -0.0308 9 7 20 0.0532 0.0352 9 7 21 0.4044 0.1284 9 7 22 -0.3493 -0.3093 9 8 0 -0.2762 -0.8440 9 8 1 -0.0557 0.1790 9 8 2 -0.7094 0.4549 9 8 3 0.2228 -0.0882 9 8 4 0.4878 0.0915 9 8 5 1.9077 0.0317 9 8 6 0.3006 -0.1541 9 8 7 -1.2772 0.0636 9 8 8 0.0991 -0.0265 9 8 9 0.9988 -0.0265 9 8 10 0.0235 -0.0012 9 8 11 -0.9915 0.0439 9 8 12 -0.2312 0.0739 9 8 13 0.8898 -0.0784 9 8 14 1.7984 0.0112 9 8 15 1.2949 -0.0611 9 8 16 -1.1941 -0.0390 9 8 17 -0.2103 -0.0673 9 8 18 0.1613 -0.0240 9 8 19 -0.3698 0.0723 9 8 20 0.2681 0.1823 9 8 21 0.0199 -0.1773 9 9 0 -0.4046 0.8990 9 9 1 -0.9276 0.0251 9 9 2 0.2452 -0.4501 9 9 3 2.1357 0.0446 9 9 4 1.2957 -0.0854 9 9 5 0.4050 -0.0810 9 9 6 -0.7434 0.1713 9 9 7 0.8246 0.0037 9 9 8 0.9498 -0.0137 9 9 9 -0.5261 0.0745 9 9 10 -0.6807 -0.0045 9 9 11 -0.5237 -0.0413 9 9 12 0.8903 -0.0591 9 9 13 1.6446 -0.0043 9 9 14 1.0039 -0.0111 9 9 15 -1.4440 -0.0689 9 9 16 -0.8868 0.0211 9 9 17 1.1125 0.0464 9 9 18 -0.4636 0.0586 9 9 19 0.3655 0.0661 9 9 20 0.4307 -0.2821 9 9 21 -0.2722 -0.2826 9 10 0 -0.6983 -0.7584 9 10 1 0.5728 -0.3488 9 10 2 1.9014 0.4218 9 10 3 2.0878 0.0198 9 10 4 -0.2242 -0.0143 9 10 5 0.2109 0.1332 9 10 6 1.2433 -0.1191 9 10 7 0.7337 0.0095 9 10 8 -0.9436 0.0687 9 10 9 -1.2334 -0.0739 9 10 10 -0.0911 -0.0444 9 10 11 0.3994 0.0125 9 10 12 1.7103 0.1254 9 10 13 -0.2399 0.0284 9 10 14 -1.2959 -0.0223 9 10 15 -0.8949 0.0707 9 10 16 1.1178 -0.0091 9 10 17 0.5015 0.0935 9 10 18 -0.6207 -0.1120 9 10 19 1.0039 -0.1132 9 10 20 -0.2643 -0.2621 9 11 0 0.3167 0.5264 9 11 1 1.6575 0.5077 9 11 2 1.2911 -0.2788 9 11 3 0.6040 -0.0624 9 11 4 -0.3076 -0.0015 9 11 5 1.9219 -0.1607 9 11 6 0.1260 0.1186 9 11 7 -1.5272 0.0323 9 11 8 -1.0888 -0.0530 9 11 9 -0.4628 0.0822 9 11 10 1.5374 0.1109 9 11 11 0.9605 0.0769 9 11 12 -0.4115 -0.0547 9 11 13 -2.3160 -0.0128 9 11 14 0.0915 0.1063 9 11 15 0.7524 0.0625 9 11 16 0.4641 0.0074 9 11 17 -0.4700 0.1669 9 11 18 -0.0491 0.0762 9 11 19 0.8804 0.2097 9 12 0 1.1005 -0.2303 9 12 1 0.9882 -0.5824 9 12 2 0.0541 0.1498 9 12 3 0.1427 0.1563 9 12 4 0.7879 -0.0440 9 12 5 0.8196 0.1610 9 12 6 -2.1238 -0.0468 9 12 7 -0.7493 -0.0592 9 12 8 -0.0232 0.1647 9 12 9 1.1453 0.0264 9 12 10 2.0260 -0.0529 9 12 11 -1.4348 -0.1256 9 12 12 -1.6982 -0.0386 9 12 13 -0.5543 0.1835 9 12 14 1.1444 0.1614 9 12 15 -0.0361 0.1963 9 12 16 -0.2236 0.2157 9 12 17 0.0117 0.5095 9 13 0 1.3852 0.0517 9 13 1 -0.0481 0.5419 9 13 2 -0.1957 0.0486 9 13 3 0.3859 -0.0161 9 13 4 0.1567 0.0747 9 13 5 -0.8394 -0.2569 9 13 6 -1.1635 0.0192 9 13 7 0.7029 0.1320 9 13 8 0.4993 -0.0760 9 13 9 1.5092 -0.0499 9 13 10 -0.1431 -0.0956 9 13 11 -1.8073 0.0112 9 13 12 0.0772 0.0202 9 13 13 0.0613 0.1921 9 13 14 0.3948 0.3663 9 13 15 -0.0447 0.2502 9 14 0 1.2979 0.3726 9 14 1 -0.7037 -0.6053 9 14 2 -0.1120 -0.0022 9 14 3 -0.3460 0.1247 9 14 4 -0.5609 -0.2640 9 14 5 -0.2643 0.0351 9 14 6 0.1558 0.2188 9 14 7 0.7719 -0.1089 9 14 8 0.1850 0.0346 9 14 9 0.5445 -0.0982 9 14 10 -0.4394 -0.1147 9 14 11 -0.1825 0.0123 9 14 12 0.0686 -0.0821 9 14 13 -0.0845 0.4439 9 15 0 0.0837 -0.6256 9 15 1 -0.9153 0.1775 9 15 2 -0.2959 0.2933 9 15 3 -0.5578 -0.2162 9 15 4 -0.0046 0.1062 9 15 5 0.3689 0.0776 9 15 6 0.3230 0.0279 9 15 7 0.1619 0.0069 9 15 8 -0.1646 -0.1737 9 15 9 0.5601 -0.1986 9 15 10 -0.0505 0.0541 10 -7 3 0.0734 -0.0837 10 -7 4 0.0506 0.3309 10 -7 5 0.4575 0.1791 10 -7 6 0.1248 -0.2453 10 -7 7 -0.1380 0.0384 10 -6 0 -0.7619 -0.0644 10 -6 1 -0.0552 -0.0069 10 -6 2 -0.0456 0.0440 10 -6 3 0.4507 0.1739 10 -6 4 -0.3795 -0.0222 10 -6 5 0.2260 -0.3685 10 -6 6 -0.3039 -0.0929 10 -6 7 0.0685 0.2017 10 -6 8 0.2482 -0.0917 10 -6 9 0.1213 -0.1260 10 -6 10 1.0265 0.1975 10 -6 11 0.2558 0.1865 10 -6 12 -0.3660 -0.1190 10 -5 0 -1.2457 0.0083 10 -5 1 0.3999 -0.3242 10 -5 2 -0.1341 -0.0643 10 -5 3 -0.1953 -0.0848 10 -5 4 -0.5895 -0.1234 10 -5 5 0.4824 0.0761 10 -5 6 -0.0810 0.1887 10 -5 7 0.4055 0.0507 10 -5 8 -0.6614 -0.1088 10 -5 9 0.2177 -0.1115 10 -5 10 1.2364 -0.0041 10 -5 11 0.0572 0.0294 10 -5 12 -0.2595 0.0755 10 -5 13 0.5095 0.2288 10 -5 14 0.6409 -0.2506 10 -5 15 1.5818 0.2421 10 -4 0 -0.9006 -0.3596 10 -4 1 0.1356 0.1898 10 -4 2 -1.0438 0.1377 10 -4 3 0.2933 0.0895 10 -4 4 0.5530 0.1348 10 -4 5 0.3148 -0.0969 10 -4 6 -0.5808 -0.1958 10 -4 7 -0.9721 0.0366 10 -4 8 -0.7137 -0.0037 10 -4 9 1.9116 -0.0436 10 -4 10 1.2980 0.0742 10 -4 11 0.3542 0.0785 10 -4 12 0.4120 0.0434 10 -4 13 0.7090 -0.0168 10 -4 14 0.3501 -0.1564 10 -4 15 0.8553 0.0664 10 -4 16 -0.8229 -0.2547 10 -4 17 -0.8761 0.3327 10 -3 0 -1.0994 0.5370 10 -3 1 -0.4559 -0.1324 10 -3 2 0.2275 -0.1746 10 -3 3 1.1601 0.0583 10 -3 4 -0.2945 -0.1532 10 -3 5 -1.0123 -0.0889 10 -3 6 -1.0987 0.1723 10 -3 7 -0.0454 0.2281 10 -3 8 1.9837 -0.0791 10 -3 9 2.2891 -0.0558 10 -3 10 0.3112 -0.0750 10 -3 11 0.2344 -0.0927 10 -3 12 -0.6511 -0.0128 10 -3 13 -0.4757 0.0480 10 -3 14 -0.0811 -0.0013 10 -3 15 0.1540 -0.0024 10 -3 16 -1.1046 0.0430 10 -3 17 0.0280 0.1231 10 -3 18 0.5072 -0.2704 10 -2 0 -0.8531 -0.5726 10 -2 1 0.7181 -0.0978 10 -2 2 0.6792 0.3015 10 -2 3 -0.3878 0.0226 10 -2 4 -0.7938 0.1021 10 -2 5 -0.7177 0.0918 10 -2 6 0.5699 -0.0797 10 -2 7 2.0167 -0.1165 10 -2 8 1.7385 -0.0693 10 -2 9 0.3340 0.0132 10 -2 10 -0.7607 -0.0528 10 -2 11 -0.8562 0.0685 10 -2 12 -1.4368 0.0929 10 -2 13 0.1004 0.0508 10 -2 14 0.1213 -0.0760 10 -2 15 -0.8050 -0.0530 10 -2 16 -0.5296 -0.0097 10 -2 17 0.5420 -0.1285 10 -2 18 -0.0834 -0.0520 10 -2 19 -1.3055 0.0914 10 -1 0 0.6418 0.5484 10 -1 1 1.4271 0.2834 10 -1 2 -0.4363 -0.2753 10 -1 3 -0.8687 -0.0315 10 -1 4 -0.6119 -0.0412 10 -1 5 0.1113 -0.2023 10 -1 6 2.0174 0.0229 10 -1 7 1.1244 0.1532 10 -1 8 0.0178 0.1122 10 -1 9 -0.3961 -0.0427 10 -1 10 -1.1684 0.0014 10 -1 11 -0.5609 -0.0431 10 -1 12 -0.3733 -0.0396 10 -1 13 0.1896 0.0048 10 -1 14 -1.2697 -0.0325 10 -1 15 -1.0517 0.0097 10 -1 16 0.3913 -0.0051 10 -1 17 -0.0146 -0.0130 10 -1 18 -0.2741 0.0107 10 -1 19 -1.5986 0.0230 10 -1 20 -0.5508 0.2210 10 0 0 2.4143 -0.4164 10 0 1 0.5042 -0.5291 10 0 2 -2.6147 0.1982 10 0 3 -1.4374 0.1352 10 0 4 0.1243 0.0138 10 0 5 1.7846 0.1420 10 0 6 1.3024 0.0303 10 0 7 -0.3478 -0.0632 10 0 8 0.1108 -0.0797 10 0 9 -0.3200 -0.0526 10 0 10 -0.3836 -0.0098 10 0 11 0.3186 -0.0580 10 0 12 -1.1617 0.1494 10 0 13 -1.3034 0.0598 10 0 14 -1.2802 0.0013 10 0 15 0.1301 -0.0590 10 0 16 0.2446 -0.0237 10 0 17 0.1634 -0.0197 10 0 18 -0.0827 -0.0501 10 0 19 -1.7391 0.0677 10 0 20 0.6277 0.1329 10 0 21 0.4060 0.0647 10 1 0 0.6835 0.1403 10 1 1 -3.0603 0.6365 10 1 2 -2.8340 0.0093 10 1 3 1.1210 -0.1026 10 1 4 1.3780 0.0127 10 1 5 0.9776 -0.2009 10 1 6 -0.1872 -0.0674 10 1 7 0.0412 0.0826 10 1 8 0.2674 0.0658 10 1 9 0.0970 0.0355 10 1 10 0.3168 0.0106 10 1 11 -1.2673 0.0348 10 1 12 -2.5242 0.0115 10 1 13 -0.3130 -0.0669 10 1 14 0.2879 -0.0529 10 1 15 0.2538 -0.0399 10 1 16 0.0460 0.0973 10 1 17 0.6859 0.0346 10 1 18 -0.6743 0.0318 10 1 19 -0.5742 0.0965 10 1 20 0.8551 0.1076 10 1 21 -0.6551 0.0455 10 2 0 -2.2972 0.1506 10 2 1 -1.9411 -0.6008 10 2 2 0.8209 -0.0730 10 2 3 0.7673 0.1526 10 2 4 -0.2888 -0.0739 10 2 5 0.8816 0.1670 10 2 6 -0.0612 0.1466 10 2 7 -0.3562 -0.0322 10 2 8 0.1170 -0.0259 10 2 9 0.7166 -0.0221 10 2 10 -1.1353 -0.0480 10 2 11 -2.6681 -0.0893 10 2 12 -0.7527 0.0119 10 2 13 1.3898 0.0703 10 2 14 0.0687 0.0144 10 2 15 -0.5147 0.1060 10 2 16 -0.0708 0.0540 10 2 17 0.6295 -0.0163 10 2 18 -0.6586 -0.0140 10 2 19 -0.1196 0.0414 10 2 20 -0.4405 -0.0289 10 2 21 -0.2863 -0.0695 10 2 22 0.1350 -0.0245 10 3 0 -0.9701 -0.4200 10 3 1 0.0980 0.5735 10 3 2 -0.6605 0.3059 10 3 3 -0.7249 -0.1105 10 3 4 2.0628 0.0891 10 3 5 0.5379 -0.0511 10 3 6 -2.0516 -0.1938 10 3 7 -0.3908 0.0697 10 3 8 1.1835 0.0466 10 3 9 -0.2538 -0.0095 10 3 10 -2.6085 -0.0455 10 3 11 -1.3826 0.0518 10 3 12 0.6854 0.0855 10 3 13 0.7793 -0.0313 10 3 14 -0.8657 -0.0034 10 3 15 -0.9102 0.0002 10 3 16 0.2512 -0.0487 10 3 17 0.5167 -0.0025 10 3 18 -1.0685 0.0062 10 3 19 -0.2273 0.0472 10 3 20 -0.4327 -0.0741 10 3 21 0.0987 -0.0158 10 3 22 -0.3665 -0.1372 10 4 0 -1.0937 0.6905 10 4 1 -1.1828 -0.3681 10 4 2 -0.2736 -0.3466 10 4 3 2.7237 0.1072 10 4 4 1.1644 -0.0843 10 4 5 -2.9830 0.0183 10 4 6 -1.1251 0.1771 10 4 7 1.5675 0.0798 10 4 8 0.5302 -0.0701 10 4 9 -2.3636 -0.0243 10 4 10 -2.2662 -0.0199 10 4 11 -0.2985 -0.0279 10 4 12 0.8879 -0.0659 10 4 13 0.3267 -0.0132 10 4 14 -1.2597 0.0159 10 4 15 -0.8180 -0.0005 10 4 16 0.4922 0.0262 10 4 17 -0.0700 -0.0100 10 4 18 -0.6802 0.0183 10 4 19 -0.1274 -0.0038 10 4 20 -0.8156 -0.0387 10 4 21 0.2337 -0.0638 10 4 22 0.0819 -0.1056 10 5 0 -0.7408 -0.8348 10 5 1 0.0885 0.1109 10 5 2 2.5964 0.4829 10 5 3 1.5466 -0.0575 10 5 4 -2.4668 0.0735 10 5 5 -1.2565 0.0598 10 5 6 1.2824 -0.1693 10 5 7 0.9849 -0.0246 10 5 8 -1.8867 -0.0217 10 5 9 -3.0064 -0.0224 10 5 10 -0.2737 -0.0360 10 5 11 1.0571 -0.0216 10 5 12 1.1985 0.0694 10 5 13 -0.9498 -0.0100 10 5 14 -1.5772 0.0046 10 5 15 -0.2147 -0.0164 10 5 16 1.2055 -0.0332 10 5 17 0.0631 -0.0461 10 5 18 -0.6757 0.0018 10 5 19 -0.7817 0.0642 10 5 20 0.1667 -0.0145 10 5 21 1.0129 -0.0854 10 5 22 0.2235 -0.0803 10 6 0 0.4417 0.8371 10 6 1 1.3976 0.1529 10 6 2 1.9547 -0.4209 10 6 3 -1.1502 -0.0007 10 6 4 -1.3141 -0.0395 10 6 5 1.1677 -0.1409 10 6 6 0.8345 0.1371 10 6 7 -0.7971 0.0609 10 6 8 -3.0769 -0.0446 10 6 9 -0.1625 0.0035 10 6 10 2.3056 0.0032 10 6 11 0.4398 -0.0171 10 6 12 -0.5130 0.0106 10 6 13 -1.6132 -0.0745 10 6 14 0.1531 0.0071 10 6 15 1.3722 -0.0465 10 6 16 1.3398 0.0128 10 6 17 -1.3136 -0.0393 10 6 18 -0.6966 0.0709 10 6 19 0.1107 0.0303 10 6 20 0.9335 -0.1038 10 6 21 0.2783 -0.0396 10 6 22 -0.0102 -0.1856 10 7 0 0.7066 -0.7259 10 7 1 1.1894 -0.3909 10 7 2 -0.0044 0.4219 10 7 3 -0.9118 0.0627 10 7 4 0.7008 0.0085 10 7 5 1.5568 0.1608 10 7 6 -0.7632 -0.0725 10 7 7 -2.2035 -0.0821 10 7 8 -0.3132 0.0243 10 7 9 2.8875 -0.0413 10 7 10 0.4580 -0.0430 10 7 11 -1.5475 -0.0028 10 7 12 0.0012 0.0667 10 7 13 0.2333 -0.0664 10 7 14 1.7151 0.0019 10 7 15 0.6553 -0.0047 10 7 16 -0.8649 0.0118 10 7 17 -1.5032 -0.0097 10 7 18 0.4821 0.0147 10 7 19 -0.0167 -0.0464 10 7 20 0.7149 0.0624 10 7 21 -0.0364 -0.1772 10 8 0 0.4181 0.4651 10 8 1 -0.3998 0.6591 10 8 2 0.0971 -0.2527 10 8 3 0.6685 -0.1033 10 8 4 1.4686 0.0605 10 8 5 -0.4666 -0.1855 10 8 6 -2.5813 0.0579 10 8 7 0.2714 0.0494 10 8 8 2.4614 -0.0389 10 8 9 0.5184 -0.0130 10 8 10 -1.5102 0.0219 10 8 11 -0.1566 0.0425 10 8 12 1.1184 -0.0334 10 8 13 0.6092 -0.0598 10 8 14 0.5431 0.0157 10 8 15 -1.5373 0.0260 10 8 16 -1.0290 0.0468 10 8 17 -0.2512 0.0049 10 8 18 0.2465 0.0256 10 8 19 0.2642 0.0741 10 8 20 0.6538 -0.1650 10 8 21 -0.6252 -0.3846 10 9 0 -0.6570 -0.1745 10 9 1 -0.0222 -0.6460 10 9 2 1.4639 0.0933 10 9 3 0.5228 0.1852 10 9 4 -0.3992 -0.0834 10 9 5 -2.7016 0.1619 10 9 6 -0.0562 0.0158 10 9 7 2.0139 -0.1387 10 9 8 0.0769 0.0473 10 9 9 -1.1125 -0.0323 10 9 10 -0.4469 -0.0353 10 9 11 0.2931 0.0028 10 9 12 0.7064 0.0447 10 9 13 -0.0266 0.0209 10 9 14 -1.1673 -0.0274 10 9 15 -1.2596 0.0676 10 9 16 0.1189 0.0004 10 9 17 -0.3013 0.0868 10 9 18 0.4507 0.0113 10 9 19 0.1169 -0.2350 10 9 20 -0.5870 -0.2252 10 10 0 -0.1638 -0.1719 10 10 1 1.1220 0.7214 10 10 2 0.5966 0.1028 10 10 3 -1.3263 -0.1673 10 10 4 -1.7501 0.0548 10 10 5 -0.9404 -0.1545 10 10 6 1.0891 -0.0697 10 10 7 -0.6861 0.0458 10 10 8 -0.5238 -0.0250 10 10 9 -0.4231 0.0299 10 10 10 -0.4285 0.0365 10 10 11 0.5981 0.0840 10 10 12 0.0553 -0.0364 10 10 13 -1.0304 -0.1145 10 10 14 -0.8009 -0.0077 10 10 15 0.2295 -0.0128 10 10 16 -0.2026 0.0681 10 10 17 -0.4634 0.0333 10 10 18 0.2766 -0.2558 10 10 19 -0.7617 -0.0941 10 11 0 1.0636 0.4899 10 11 1 0.1588 -0.4509 10 11 2 -1.2672 -0.2004 10 11 3 -1.8007 0.1054 10 11 4 -0.1514 -0.1714 10 11 5 -0.3626 0.1032 10 11 6 -1.1186 0.1163 10 11 7 -0.4590 -0.1042 10 11 8 0.3303 0.1430 10 11 9 -0.5248 0.0098 10 11 10 0.2605 -0.1271 10 11 11 -0.0429 -0.0481 10 11 12 -1.3413 -0.1181 10 11 13 0.3565 0.0665 10 11 14 0.4374 -0.0398 10 11 15 -0.0751 -0.0763 10 11 16 -0.8520 -0.0217 10 11 17 -0.2078 -0.2629 10 11 18 0.3092 -0.0620 10 12 0 0.6565 -0.5506 10 12 1 -1.5698 0.3214 10 12 2 -1.1394 0.3810 10 12 3 -0.0137 -0.2079 10 12 4 0.1806 0.0749 10 12 5 -1.9514 0.0340 10 12 6 -0.4387 -0.1263 10 12 7 0.6189 0.1052 10 12 8 -0.1674 -0.0972 10 12 9 0.2891 -0.1966 10 12 10 -0.6825 0.0641 10 12 11 -1.0652 0.0814 10 12 12 0.4579 0.0652 10 12 13 1.5116 -0.0462 10 12 14 -0.6774 -0.2596 10 12 15 -0.3730 -0.2954 10 12 16 -0.3743 -0.2730 10 12 17 0.3708 -0.2164 10 13 0 -0.4210 0.6722 10 13 1 -1.2798 0.0441 10 13 2 0.2391 -0.2308 10 13 3 0.0316 -0.0971 10 13 4 -1.0034 -0.1345 10 13 5 -0.9895 0.0073 10 13 6 0.7784 0.1583 10 13 7 0.0197 -0.2003 10 13 8 0.1624 -0.1355 10 13 9 -0.3174 0.2557 10 13 10 -1.3618 0.1709 10 13 11 0.8268 -0.0282 10 13 12 0.7505 -0.1361 10 13 13 -0.1223 -0.2589 10 13 14 -0.6324 -0.3987 10 13 15 0.3719 -0.4267 10 14 0 -0.8415 -0.6508 10 14 1 -0.6320 0.0162 10 14 2 0.1289 0.1633 10 14 3 -0.3564 -0.3301 10 14 4 -0.0364 0.1256 10 14 5 0.1777 0.3005 10 14 6 0.3637 -0.2387 10 14 7 -0.3295 -0.1623 10 14 8 -0.2279 0.1330 10 14 9 -0.7518 0.1722 10 14 10 0.0150 0.0523 10 14 11 0.5127 -0.1393 10 14 12 -0.5655 -0.1198 10 15 1 0.2057 0.4171 10 15 2 0.2741 -0.4590 10 15 3 0.2495 0.0860 10 15 4 0.2844 0.2458 10 15 5 -0.1270 -0.1485 10 15 6 -0.1872 -0.2393 10 15 7 -0.8488 -0.0826 10 15 8 -0.1098 0.1074 11 -5 0 0.6951 -0.3527 11 -5 1 -0.1664 0.3675 11 -5 2 0.1100 0.3671 11 -5 3 -0.3047 -0.1644 11 -5 4 0.6755 -0.1741 11 -5 5 -0.1504 0.3477 11 -5 6 -0.2589 0.2169 11 -5 7 -0.6727 -0.3438 11 -5 8 0.1101 -0.1911 11 -5 9 0.8757 0.2048 11 -5 10 -0.5363 0.1003 11 -5 11 -0.8085 -0.1959 11 -4 0 0.3172 0.5189 11 -4 1 -0.6010 0.3319 11 -4 2 0.4012 -0.1984 11 -4 3 0.1106 -0.0999 11 -4 4 0.0650 -0.0393 11 -4 5 -1.2130 0.0191 11 -4 6 -0.3800 -0.0831 11 -4 7 0.2029 -0.0085 11 -4 8 1.8350 0.1167 11 -4 9 0.3065 0.1113 11 -4 10 -1.6382 -0.0968 11 -4 11 -0.8033 -0.0700 11 -4 12 -0.2453 0.0438 11 -4 13 -0.6071 -0.2838 11 -4 14 0.1111 0.2269 11 -3 0 0.2773 -0.2207 11 -3 1 -0.1288 -0.3645 11 -3 2 0.1524 0.1489 11 -3 3 -1.0330 0.0112 11 -3 4 -0.4291 -0.0808 11 -3 5 -0.1115 0.1264 11 -3 6 0.8853 0.1313 11 -3 7 1.3911 -0.0684 11 -3 8 0.5421 -0.1424 11 -3 9 -2.2872 -0.0366 11 -3 10 -1.4753 -0.0839 11 -3 11 -0.1459 0.0987 11 -3 12 0.0504 0.0251 11 -3 13 0.1897 -0.0069 11 -3 14 0.4523 0.1299 11 -3 15 -0.6211 -0.2495 11 -3 16 0.7766 0.2371 11 -2 0 0.2979 0.0164 11 -2 1 -0.6971 0.4481 11 -2 2 -0.6883 0.0010 11 -2 3 -0.0271 -0.1693 11 -2 4 0.7141 0.0195 11 -2 5 0.2552 -0.0309 11 -2 6 0.7058 -0.1027 11 -2 7 -0.1498 -0.0987 11 -2 8 -1.9113 0.0924 11 -2 9 -1.4784 0.0242 11 -2 10 0.7735 0.0283 11 -2 11 0.5077 0.0942 11 -2 12 0.7572 -0.0778 11 -2 13 0.5082 -0.0473 11 -2 14 -0.1941 -0.1249 11 -2 15 -0.3288 0.0054 11 -2 16 0.9921 0.1014 11 -2 17 -0.5434 -0.2255 11 -2 18 -0.8276 0.2682 11 -1 0 -0.2533 0.1785 11 -1 1 -0.3427 -0.4662 11 -1 2 0.0905 -0.1279 11 -1 3 0.2295 0.1183 11 -1 4 -0.1990 -0.0320 11 -1 5 0.5076 0.0380 11 -1 6 -0.0948 0.0828 11 -1 7 -1.5211 0.0522 11 -1 8 -0.6488 -0.0654 11 -1 9 0.7069 -0.0872 11 -1 10 0.8812 -0.0021 11 -1 11 0.1624 -0.0705 11 -1 12 0.8627 -0.0071 11 -1 13 -0.3933 0.0117 11 -1 14 -0.6796 0.0184 11 -1 15 0.5424 0.0526 11 -1 16 0.7591 -0.1390 11 -1 17 -0.2784 0.0216 11 -1 18 0.1235 0.1665 11 -1 19 0.9934 0.0443 11 0 0 0.1053 -0.4037 11 0 1 -1.0378 0.3522 11 0 2 -0.6336 0.2936 11 0 3 0.5046 -0.0818 11 0 4 1.2701 -0.0050 11 0 5 0.5607 -0.0161 11 0 6 -1.6465 -0.0796 11 0 7 -0.4964 -0.0839 11 0 8 0.5632 -0.0279 11 0 9 -0.1333 0.0822 11 0 10 0.2058 -0.0361 11 0 11 -0.0667 0.0789 11 0 12 0.2103 0.0392 11 0 13 -0.7436 -0.0754 11 0 14 0.5126 -0.0727 11 0 15 1.4397 -0.0924 11 0 16 0.7891 0.0317 11 0 17 0.1109 0.1029 11 0 18 -0.5098 0.0943 11 0 19 0.8181 0.0801 11 0 20 0.4642 -0.2597 11 1 0 -1.6470 0.5554 11 1 1 -1.4367 -0.1668 11 1 2 2.0650 -0.3379 11 1 3 1.9412 0.0192 11 1 4 0.4085 -0.0458 11 1 5 -1.2320 0.0374 11 1 6 -1.0415 0.0839 11 1 7 0.3927 0.0387 11 1 8 -0.5966 0.0557 11 1 9 -0.3601 -0.0386 11 1 10 0.0032 -0.0331 11 1 11 -0.8142 0.0139 11 1 12 0.8353 -0.1256 11 1 13 0.6622 -0.0137 11 1 14 1.1681 0.0049 11 1 15 0.8081 0.0969 11 1 16 0.2133 0.0286 11 1 17 -0.6247 -0.0007 11 1 18 -0.6169 0.1217 11 1 19 0.8743 -0.1786 11 1 20 -0.4607 -0.2956 11 2 0 -0.9762 -0.6606 11 2 1 1.8209 0.0164 11 2 2 2.3383 0.3510 11 2 3 -0.5292 0.0204 11 2 4 -0.0694 0.0434 11 2 5 -0.7091 0.0642 11 2 6 -0.5821 -0.1173 11 2 7 -0.1459 -0.0203 11 2 8 -0.2501 -0.0384 11 2 9 -0.1218 -0.0307 11 2 10 -0.9641 0.0149 11 2 11 0.4941 0.0067 11 2 12 2.3616 0.0622 11 2 13 0.0137 0.0316 11 2 14 -0.0564 -0.0041 11 2 15 0.1785 -0.0626 11 2 16 0.2854 -0.0951 11 2 17 -0.8040 0.0778 11 2 18 -0.6207 -0.0369 11 2 19 0.0716 -0.2113 11 2 20 -0.0063 0.0097 11 2 21 0.6701 0.1111 11 3 0 1.1357 0.6833 11 3 1 1.3808 0.2598 11 3 2 0.0616 -0.3413 11 3 3 0.4763 -0.0684 11 3 4 0.1522 -0.0492 11 3 5 -1.7465 -0.1008 11 3 6 0.1380 0.1052 11 3 7 1.0551 0.0427 11 3 8 0.0309 -0.0308 11 3 9 -1.0184 0.0094 11 3 10 -0.0545 0.0164 11 3 11 1.9848 0.0267 11 3 12 1.0757 -0.0495 11 3 13 -1.1153 -0.0699 11 3 14 0.1789 -0.0227 11 3 15 0.6589 -0.0434 11 3 16 0.0096 0.0566 11 3 17 -1.5332 -0.0121 11 3 18 -0.0188 0.0012 11 3 19 0.8806 0.0015 11 3 20 0.6228 0.0296 11 3 21 -0.0863 0.0225 11 4 0 1.1993 -0.5026 11 4 1 0.6958 -0.4240 11 4 2 0.9931 0.2588 11 4 3 -0.0451 0.0603 11 4 4 -2.3130 0.0211 11 4 5 0.0655 0.1360 11 4 6 2.1325 -0.0325 11 4 7 0.7726 -0.1244 11 4 8 -1.0778 -0.0130 11 4 9 -0.8168 -0.0527 11 4 10 1.2510 0.0002 11 4 11 1.7945 -0.0020 11 4 12 0.5042 0.0224 11 4 13 -0.9380 0.0540 11 4 14 0.1427 0.0115 11 4 15 0.2365 -0.0271 11 4 16 -0.3650 -0.0882 11 4 17 -0.1542 0.0236 11 4 18 1.2966 0.0926 11 4 19 0.1904 -0.0884 11 4 20 0.0382 0.0221 11 4 21 0.0152 0.0426 11 5 0 1.0232 0.2807 11 5 1 0.9873 0.5812 11 5 2 -0.2174 -0.1571 11 5 3 -2.5083 -0.1144 11 5 4 -0.5444 0.0413 11 5 5 2.2348 -0.1855 11 5 6 1.2549 0.0401 11 5 7 -0.4390 0.0278 11 5 8 -1.7772 -0.0225 11 5 9 0.7090 -0.0134 11 5 10 2.4804 0.0842 11 5 11 1.5268 0.0652 11 5 12 -0.9230 -0.0035 11 5 13 -1.8567 -0.0435 11 5 14 0.5524 -0.0757 11 5 15 1.1192 -0.0662 11 5 16 0.6228 -0.0007 11 5 17 0.0696 0.0980 11 5 18 -0.2289 -0.0276 11 5 19 -0.1511 0.0465 11 5 20 0.6283 0.0428 11 5 21 0.0399 -0.0348 11 6 0 0.2917 -0.0696 11 6 1 0.3194 -0.5990 11 6 2 -2.3336 0.0360 11 6 3 -1.3539 0.1630 11 6 4 1.6141 -0.0706 11 6 5 1.2642 0.1572 11 6 6 0.1529 0.0640 11 6 7 -2.0014 -0.1343 11 6 8 -0.2829 0.0322 11 6 9 3.2103 -0.0025 11 6 10 1.1412 -0.0082 11 6 11 -1.0005 -0.0153 11 6 12 -2.1840 -0.0430 11 6 13 0.0100 0.0062 11 6 14 1.9948 -0.0137 11 6 15 0.6499 0.0561 11 6 16 -1.2211 -0.0380 11 6 17 -0.9885 0.0073 11 6 18 0.2075 0.0681 11 6 19 0.6949 0.0660 11 6 20 0.0921 -0.0757 11 6 21 -0.1906 -0.0039 11 7 0 -0.0211 -0.2964 11 7 1 -1.2338 0.6368 11 7 2 -1.5427 0.1242 11 7 3 1.0074 -0.1628 11 7 4 1.1301 0.0894 11 7 5 -0.5548 -0.1472 11 7 6 -1.3280 -0.1222 11 7 7 -0.6111 0.1014 11 7 8 2.9535 -0.0241 11 7 9 0.7048 -0.0713 11 7 10 -2.1613 0.0060 11 7 11 -0.7387 0.1189 11 7 12 -0.5050 -0.0363 11 7 13 1.1576 -0.0023 11 7 14 -0.0814 -0.0203 11 7 15 -1.5785 -0.0060 11 7 16 -1.2459 -0.0521 11 7 17 0.8446 0.0827 11 7 18 0.3918 0.0209 11 7 19 0.2734 0.0433 11 7 20 -0.2078 -0.0210 11 7 21 -0.1855 -0.0416 11 8 0 -0.6422 0.4878 11 8 1 -0.5320 -0.4798 11 8 2 0.8565 -0.3024 11 8 3 0.4830 0.1577 11 8 4 -0.8826 -0.1168 11 8 5 -1.5766 0.0069 11 8 6 0.9808 0.1597 11 8 7 2.0973 -0.0645 11 8 8 -0.1345 -0.0664 11 8 9 -2.7093 0.0045 11 8 10 -0.4732 0.0187 11 8 11 0.6433 0.0499 11 8 12 -0.7683 -0.1501 11 8 13 -0.1895 0.0500 11 8 14 -1.5057 -0.0191 11 8 15 -0.3236 0.0735 11 8 16 0.5308 -0.0247 11 8 17 0.7444 -0.0218 11 8 18 -0.1306 0.0269 11 8 19 0.4203 0.0372 11 8 20 -0.8816 -0.0879 11 9 0 0.0275 -0.6905 11 9 1 0.9487 0.2171 11 9 2 0.1826 0.3771 11 9 3 -0.7445 -0.1194 11 9 4 -1.1480 0.0784 11 9 5 1.0387 -0.0205 11 9 6 2.5587 -0.1697 11 9 7 -1.2102 0.0328 11 9 8 -2.4301 -0.0048 11 9 9 -0.2227 -0.0511 11 9 10 0.7880 0.0159 11 9 11 -0.0358 0.0241 11 9 12 -0.9410 -0.0573 11 9 13 -0.3183 0.0602 11 9 14 -0.3211 -0.0039 11 9 15 0.7312 0.0049 11 9 16 0.2408 -0.0685 11 9 17 0.7558 0.0085 11 9 18 0.1070 -0.0883 11 9 19 -0.4106 -0.0037 11 10 0 0.5298 0.7312 11 10 1 0.3789 -0.0207 11 10 2 -0.4330 -0.3867 11 10 3 -0.4001 0.0690 11 10 4 0.3194 -0.0543 11 10 5 2.1926 -0.1167 11 10 6 -0.6276 0.1529 11 10 7 -1.5149 0.0311 11 10 8 0.1923 0.0117 11 10 9 0.7226 -0.0155 11 10 10 0.4943 -0.0361 11 10 11 0.0772 -0.0270 11 10 12 -0.7157 -0.0673 11 10 13 0.4625 0.0596 11 10 14 0.4288 -0.0313 11 10 15 0.2977 0.0338 11 10 16 0.8288 0.0589 11 10 17 0.7710 -0.2131 11 10 18 -0.5804 -0.0511 11 10 19 0.0862 0.2803 11 11 0 0.1368 -0.6500 11 11 1 -0.4097 -0.2522 11 11 2 -0.2598 0.3807 11 11 3 0.6298 -0.0225 11 11 4 1.0896 0.0734 11 11 5 0.1211 0.1671 11 11 6 -0.5911 -0.1476 11 11 7 1.2222 0.0946 11 11 8 0.1133 -0.0062 11 11 9 1.0356 -0.2295 11 11 10 0.5091 0.0483 11 11 11 -0.3869 -0.0370 11 11 12 0.5422 0.0616 11 11 13 0.9587 0.0404 11 11 14 -0.1162 -0.0129 11 11 15 0.3639 0.1418 11 11 16 0.9219 -0.1045 11 11 17 -0.0547 -0.0700 11 12 0 -1.1129 0.4386 11 12 1 -0.2861 0.5088 11 12 2 0.9460 -0.3025 11 12 3 0.9477 -0.0119 11 12 4 -0.5958 0.1433 11 12 5 -0.0395 -0.2770 11 12 6 1.6289 0.0133 11 12 7 0.8238 0.1250 11 12 8 0.5234 -0.1659 11 12 9 1.1898 0.1500 11 12 10 -0.5570 0.0285 11 12 11 0.7248 -0.1966 11 12 12 1.0481 0.0746 11 12 13 -0.6146 -0.0196 11 12 14 -0.0841 0.1717 11 12 15 0.4297 0.1739 11 12 16 0.4732 0.1466 11 13 0 -1.1815 -0.1197 11 13 1 0.9402 -0.4750 11 13 2 0.5015 -0.1108 11 13 3 -0.6630 0.1259 11 13 4 -0.2321 -0.0985 11 13 5 1.7350 0.0362 11 13 6 1.3256 0.0486 11 13 7 0.4748 0.0828 11 13 8 0.8222 0.2061 11 13 9 -0.3416 -0.0799 11 13 10 0.1475 -0.4353 11 13 11 0.7164 -0.0769 11 13 12 -0.5131 0.2261 11 13 13 -0.3960 0.2200 11 13 14 0.6627 0.3587 11 14 0 -0.5593 -0.1446 11 14 1 0.6207 0.2088 11 14 2 -0.4956 -0.1884 11 14 3 0.2713 0.1567 11 14 4 1.0844 0.1855 11 14 5 0.9046 -0.1402 11 14 6 0.3415 0.0133 11 14 7 0.2161 0.2277 11 14 8 -0.0103 -0.0766 11 14 9 -0.1866 -0.3321 11 14 10 0.4041 -0.1693 11 14 11 -0.2721 0.2044 12 -4 2 -0.0762 -0.3365 12 -4 3 0.5292 0.1042 12 -4 4 -0.4478 0.3975 12 -4 5 0.3964 -0.0931 12 -4 6 0.5858 -0.3021 12 -4 7 0.6462 0.2065 12 -4 8 -0.0993 0.2729 12 -4 9 -1.0191 -0.2103 12 -4 10 -0.0668 -0.2618 12 -3 0 0.1401 -0.4092 12 -3 1 0.5842 0.0954 12 -3 2 0.2504 0.2793 12 -3 3 0.9790 0.1662 12 -3 4 0.4850 -0.0361 12 -3 5 0.9005 -0.2778 12 -3 6 0.1032 0.0875 12 -3 7 -0.1604 0.1092 12 -3 8 -1.1583 -0.1042 12 -3 9 -0.1713 -0.1919 12 -3 10 1.2658 0.2283 12 -3 11 0.6560 0.1742 12 -3 12 -0.0230 -0.1775 12 -3 13 0.1514 0.2309 12 -2 0 0.2365 0.2914 12 -2 1 0.9406 0.0911 12 -2 2 1.3110 -0.1991 12 -2 3 1.3783 -0.1002 12 -2 4 -0.1743 -0.1224 12 -2 5 0.0425 0.0835 12 -2 6 -0.1374 0.1330 12 -2 7 -0.5832 -0.0201 12 -2 8 -0.0164 0.0094 12 -2 9 1.4858 0.0215 12 -2 10 0.3538 0.1335 12 -2 11 -0.8782 -0.1815 12 -2 12 -0.8615 0.0768 12 -2 13 -0.4273 0.0261 12 -2 14 -0.1470 -0.1646 12 -2 15 0.9450 0.3748 12 -1 0 1.0291 -0.3989 12 -1 1 1.1967 -0.0855 12 -1 2 0.7434 0.1188 12 -1 3 0.1644 0.0929 12 -1 4 0.0045 0.0823 12 -1 5 0.4650 0.0190 12 -1 6 -0.6258 -0.0897 12 -1 7 -0.0060 0.0024 12 -1 8 1.1471 0.0073 12 -1 9 -0.1765 -0.0092 12 -1 10 -1.7700 -0.0224 12 -1 11 -0.7207 0.0732 12 -1 12 -0.3508 0.1933 12 -1 13 0.0440 -0.1263 12 -1 14 0.7439 0.1387 12 -1 15 0.9025 -0.0243 12 -1 16 -0.6785 -0.1259 12 -1 17 -0.0263 0.3470 12 0 0 0.5728 0.2787 12 0 1 -0.2578 0.2243 12 0 2 0.9052 -0.1298 12 0 3 0.9543 -0.0282 12 0 4 -0.0107 -0.1172 12 0 5 -1.2019 -0.0962 12 0 6 -0.4955 0.0698 12 0 7 1.1635 0.0772 12 0 8 -0.2523 0.0600 12 0 9 -1.4879 -0.0185 12 0 10 -0.5648 0.0558 12 0 11 0.6802 0.0734 12 0 12 -0.1215 -0.0672 12 0 13 0.4943 -0.0063 12 0 14 0.9221 0.0336 12 0 15 0.0783 -0.0458 12 0 16 -1.0136 0.2638 12 0 17 -0.5270 0.0327 12 0 18 -0.0478 -0.1779 12 1 0 -0.5031 -0.3055 12 1 1 1.2087 -0.2834 12 1 2 1.3374 0.1133 12 1 3 -0.8094 0.0374 12 1 4 -1.5936 0.0283 12 1 5 -0.7327 0.0872 12 1 6 1.0685 -0.0322 12 1 7 0.4042 -0.0073 12 1 8 -0.7984 -0.0075 12 1 9 0.0573 -0.0648 12 1 10 0.3904 0.0019 12 1 11 1.0141 -0.0453 12 1 12 -0.0051 0.0982 12 1 13 0.3455 0.0400 12 1 14 -0.0450 -0.0076 12 1 15 -0.9500 0.1045 12 1 16 -1.0989 0.0294 12 1 17 -0.2825 -0.0814 12 1 18 0.5398 -0.1813 12 1 19 -0.1639 -0.1862 12 2 0 0.8966 0.1609 12 2 1 1.2178 0.4028 12 2 2 -1.2942 -0.0363 12 2 3 -0.9712 -0.0931 12 2 4 -0.5084 -0.0154 12 2 5 0.0515 -0.1851 12 2 6 0.9132 0.0093 12 2 7 0.1172 0.0407 12 2 8 0.1874 -0.0205 12 2 9 0.1065 -0.0008 12 2 10 0.6212 -0.0038 12 2 11 1.4275 0.0426 12 2 12 -0.9426 0.0034 12 2 13 -0.4419 -0.0764 12 2 14 -0.6075 0.0340 12 2 15 -0.6984 0.0120 12 2 16 -0.3430 0.0555 12 2 17 -0.0250 -0.1122 12 2 18 0.4634 -0.2764 12 2 19 0.1727 0.1923 12 3 0 0.8838 0.0912 12 3 1 -0.2780 -0.4771 12 3 2 -0.8725 -0.0603 12 3 3 -0.0955 0.0136 12 3 4 -1.1198 -0.0238 12 3 5 0.7081 0.1080 12 3 6 1.1432 0.0361 12 3 7 -0.3317 -0.1015 12 3 8 -0.3535 0.0285 12 3 9 -0.0665 -0.0230 12 3 10 1.4015 -0.0687 12 3 11 0.3310 -0.0377 12 3 12 -1.6318 -0.0041 12 3 13 -0.0122 0.0901 12 3 14 -0.5023 0.0211 12 3 15 -0.2404 0.0499 12 3 16 -0.4117 -0.0810 12 3 17 0.4697 -0.1936 12 3 18 1.2846 0.0842 12 3 19 0.3649 0.1773 12 3 20 -0.0552 -0.1307 12 4 0 0.3417 -0.3240 12 4 1 -0.5038 0.3805 12 4 2 -0.7857 0.1094 12 4 3 -1.0586 -0.0986 12 4 4 0.3425 0.0974 12 4 5 1.4657 -0.1449 12 4 6 -0.4585 -0.1149 12 4 7 -1.2299 0.0730 12 4 8 -0.4969 -0.0006 12 4 9 0.5882 -0.0439 12 4 10 1.3174 0.0176 12 4 11 -0.5348 0.0915 12 4 12 -1.3295 0.0344 12 4 13 -0.1812 -0.0282 12 4 14 -0.3785 -0.0521 12 4 15 0.2568 -0.0414 12 4 16 0.4012 -0.0449 12 4 17 1.3544 0.1528 12 4 18 -0.0419 -0.0074 12 4 19 -0.8571 -0.1081 12 4 20 -0.1251 -0.0443 12 5 0 -0.6126 0.4531 12 5 1 -0.7346 -0.2911 12 5 2 -0.9236 -0.2619 12 5 3 0.2812 0.0850 12 5 4 1.5009 -0.1257 12 5 5 -0.1611 0.0691 12 5 6 -1.0491 0.1425 12 5 7 -1.5863 -0.0705 12 5 8 0.1058 -0.0511 12 5 9 1.7692 0.0873 12 5 10 0.5471 0.0243 12 5 11 -1.7201 -0.0623 12 5 12 -1.5779 -0.0956 12 5 13 0.7333 0.0375 12 5 14 0.8556 0.0427 12 5 15 0.6857 0.0782 12 5 16 -0.0049 0.1179 12 5 17 -0.4650 -0.0639 12 5 18 -0.9642 -0.0872 12 5 19 0.2668 0.0693 12 5 20 0.3525 -0.0834 12 6 0 0.0465 -0.5599 12 6 1 -0.7216 0.1412 12 6 2 0.1565 0.2775 12 6 3 1.6851 -0.1022 12 6 4 0.6147 0.0722 12 6 5 -0.6971 0.0573 12 6 6 -1.8147 -0.2279 12 6 7 -0.8676 0.0108 12 6 8 2.8042 0.0253 12 6 9 0.8227 0.0110 12 6 10 -1.9409 -0.0487 12 6 11 -1.9581 0.0146 12 6 12 0.5055 0.0951 12 6 13 2.2994 0.0475 12 6 14 0.1647 0.0244 12 6 15 -0.7632 -0.0216 12 6 16 -0.9180 -0.0595 12 6 17 0.1059 0.0281 12 6 18 0.4706 0.1673 12 6 19 0.2398 -0.1507 12 6 20 -0.2336 -0.1800 12 7 0 0.3334 0.6443 12 7 1 -0.2936 0.0458 12 7 2 2.1187 -0.3636 12 7 3 0.7378 0.0244 12 7 4 -0.8951 -0.1011 12 7 5 -0.9556 -0.0845 12 7 6 -0.6143 0.1591 12 7 7 2.6872 0.0184 12 7 8 1.0696 -0.0907 12 7 9 -2.7529 0.0724 12 7 10 -1.2239 0.0736 12 7 11 0.3161 0.0120 12 7 12 2.1750 -0.0843 12 7 13 1.0185 -0.0710 12 7 14 -1.2005 0.0223 12 7 15 -0.2841 -0.0137 12 7 16 0.6618 0.1597 12 7 17 0.5700 0.0917 12 7 18 -0.2231 -0.0806 12 7 19 -0.2258 -0.2536 12 7 20 -0.0512 -0.0145 12 8 0 0.1981 -0.4851 12 8 1 1.3987 -0.2891 12 8 2 0.5745 0.3088 12 8 3 -1.3685 -0.0335 12 8 4 -0.2572 -0.0172 12 8 5 1.1443 0.2564 12 8 6 1.2426 -0.1146 12 8 7 0.1318 -0.1095 12 8 8 -2.7644 0.0471 12 8 9 -0.5403 0.0062 12 8 10 1.3384 0.0402 12 8 11 0.9822 -0.1239 12 8 12 1.7997 0.0314 12 8 13 -0.3977 0.0396 12 8 14 -0.1264 0.0915 12 8 15 0.7076 0.0262 12 8 16 0.2116 0.0079 12 8 17 -0.3532 -0.1212 12 8 18 0.1821 -0.0689 12 8 19 -0.0113 -0.0963 12 9 0 0.3335 0.4036 12 9 1 0.2457 0.3855 12 9 2 -1.1670 -0.2418 12 9 3 -0.0163 -0.0463 12 9 4 0.9919 0.0245 12 9 5 0.8554 -0.1090 12 9 6 -1.8502 0.0190 12 9 7 -1.6766 0.0808 12 9 8 0.3670 -0.0661 12 9 9 1.6939 0.0821 12 9 10 0.7550 0.1307 12 9 11 0.6071 -0.0563 12 9 12 0.8687 0.0919 12 9 13 -0.4295 -0.1243 12 9 14 0.4798 0.0141 12 9 15 -0.2961 -0.0917 12 9 16 0.1781 0.0243 12 9 17 0.2067 -0.0358 12 9 18 0.0954 0.0349 12 10 0 -0.2478 -0.1564 12 10 1 -0.2621 -0.5493 12 10 2 -0.3810 0.1510 12 10 3 -0.0519 0.0394 12 10 4 -0.0148 -0.1573 12 10 5 -1.2385 0.2842 12 10 6 -1.4450 0.0117 12 10 7 1.3289 -0.0426 12 10 8 0.9131 0.0539 12 10 9 0.0725 0.0786 12 10 10 0.0843 0.0120 12 10 11 -0.0795 -0.1105 12 10 12 0.7553 -0.0019 12 10 13 -0.3813 -0.1265 12 10 14 -0.4606 0.1129 12 10 15 -0.0414 0.0723 12 10 16 0.5274 0.0061 12 10 17 -0.7102 -0.0499 12 11 0 -0.0071 -0.0820 12 11 1 -0.1351 0.5272 12 11 2 -0.4937 -0.0602 12 11 3 -0.3428 -0.2446 12 11 4 -0.6014 0.1738 12 11 5 -0.7902 -0.0859 12 11 6 1.0364 -0.0578 12 11 7 0.0961 0.1490 12 11 8 -0.5705 -0.1650 12 11 9 -0.5065 0.0682 12 11 10 -0.4826 -0.0134 12 11 11 0.3420 -0.0232 12 11 12 0.4204 0.1100 12 11 13 -1.8945 -0.0148 12 11 14 -0.3466 0.1831 12 11 15 0.4932 -0.0766 12 11 16 -0.6917 -0.1227 12 12 0 0.1482 0.4244 12 12 1 0.2216 -0.5614 12 12 2 -0.1443 -0.3435 12 12 3 -0.7159 0.1517 12 12 4 -0.4919 -0.2020 12 12 5 0.9473 0.0265 12 12 6 0.1531 0.3104 12 12 7 -1.4023 -0.1636 12 12 8 -0.4107 -0.0357 12 12 9 -1.6094 0.0739 12 12 10 0.1330 -0.1479 12 12 11 0.1008 0.2802 12 12 12 -1.6113 0.1022 12 12 13 -1.2309 -0.0219 12 12 14 0.7755 -0.0335 12 12 15 -0.0817 -0.2339 12 13 0 0.7571 -0.5893 12 13 1 0.0917 -0.1379 12 13 2 -0.5443 0.2563 12 13 3 -0.1758 -0.1120 12 13 4 1.0188 0.0404 12 13 5 0.4102 0.3104 12 13 6 -1.5964 0.0132 12 13 7 -1.1577 -0.2043 12 13 8 -1.3307 -0.0957 12 13 9 -1.1022 -0.1513 12 13 10 0.5836 0.3077 12 13 11 -1.1356 0.4158 12 13 12 -0.5481 -0.1698 12 14 3 0.7150 0.0756 12 14 4 -0.1524 0.0506 12 14 5 -1.1475 0.0581 12 14 6 -1.3949 -0.1248 12 14 7 -0.6969 -0.2836 12 14 8 -0.8899 0.0233 13 -2 2 -0.9031 -0.1394 13 -2 3 -1.8503 -0.2108 13 -2 4 -0.8123 0.2431 13 -2 5 -0.4342 0.4446 13 -2 6 -0.0032 -0.2061 13 -2 7 -0.3419 -0.2884 13 -2 8 -0.0675 0.0901 13 -2 9 -0.0524 0.3076 13 -2 10 -0.5227 -0.2644 13 -2 11 -0.0275 -0.1351 13 -1 0 -0.6278 0.0668 13 -1 1 -1.2066 0.0806 13 -1 2 -1.3939 0.0781 13 -1 3 -1.3812 0.1596 13 -1 4 -0.4204 0.1571 13 -1 5 -0.7992 -0.2918 13 -1 6 -0.3502 -0.1634 13 -1 7 0.2967 0.2098 13 -1 8 -0.1301 0.0848 13 -1 9 -0.2097 -0.1126 13 -1 10 0.7475 -0.0854 13 -1 11 1.1052 0.2602 13 -1 12 0.7726 -0.2959 13 -1 13 0.1981 -0.0717 13 -1 14 -0.0385 0.2182 13 0 0 -1.4914 0.1115 13 0 1 -0.1690 -0.1064 13 0 2 -0.6775 0.1308 13 0 3 -1.5645 -0.0816 13 0 4 -0.9265 -0.1406 13 0 5 -0.3378 0.0890 13 0 6 1.0328 0.2310 13 0 7 0.2025 -0.0135 13 0 8 -0.5008 -0.1723 13 0 9 1.1497 0.0114 13 0 10 1.5311 0.0578 13 0 11 0.1909 -0.1667 13 0 12 -0.1748 -0.1520 13 0 13 -0.3219 0.2247 13 0 14 -0.4057 -0.2004 13 0 15 -0.8999 0.0458 13 1 0 0.0141 -0.0368 13 1 1 0.4527 0.2610 13 1 2 -1.8392 0.0350 13 1 3 -0.9266 -0.0809 13 1 4 0.5897 0.1673 13 1 5 0.6466 -0.0206 13 1 6 0.4965 -0.1226 13 1 7 -0.7245 -0.0147 13 1 8 0.4665 0.0347 13 1 9 1.3041 -0.0055 13 1 10 0.2456 -0.1217 13 1 11 -0.9724 0.0828 13 1 12 -0.5871 0.0730 13 1 13 -0.1441 -0.1727 13 1 14 -0.0312 -0.0535 13 1 15 -0.2964 0.1482 13 1 16 0.3673 -0.2501 13 1 17 0.1762 -0.0951 13 2 0 0.4081 0.3619 13 2 1 -0.7228 -0.1879 13 2 2 -0.4761 -0.1216 13 2 3 0.7492 0.0957 13 2 4 -0.0719 -0.1243 13 2 5 -0.0033 -0.0482 13 2 6 0.0980 0.1467 13 2 7 -0.4430 0.1141 13 2 8 0.4334 -0.0720 13 2 9 0.1588 -0.0794 13 2 10 -0.3903 0.0876 13 2 11 -1.4830 0.0471 13 2 12 -0.0706 -0.1895 13 2 13 0.4456 0.0395 13 2 14 0.0492 0.1271 13 2 15 0.2837 -0.0913 13 2 16 0.4422 -0.1681 13 2 17 0.1224 0.0119 13 3 0 0.2258 -0.4049 13 3 1 -0.3040 0.0901 13 3 2 0.0296 0.1719 13 3 3 -0.7055 -0.0403 13 3 4 0.0987 0.0417 13 3 5 0.8141 0.0794 13 3 6 -0.6376 -0.0670 13 3 7 -0.5801 0.0325 13 3 8 0.1816 -0.0331 13 3 9 0.1349 0.0354 13 3 10 -0.6850 0.0230 13 3 11 -1.2159 -0.0172 13 3 12 0.7075 0.1127 13 3 13 -0.0590 0.0343 13 3 14 0.5087 -0.1031 13 3 15 0.9741 -0.1004 13 3 16 0.2034 -0.0196 13 3 17 0.2139 0.2842 13 3 18 -0.2063 0.2887 13 4 0 -0.4273 0.4337 13 4 1 -1.1499 0.0786 13 4 2 -0.4933 -0.2480 13 4 3 0.4999 0.1288 13 4 4 1.1030 -0.0927 13 4 5 -0.5813 -0.0886 13 4 6 -0.8959 0.1190 13 4 7 0.4264 0.1058 13 4 8 0.2891 -0.0347 13 4 9 0.3015 0.0043 13 4 10 -0.9249 0.0511 13 4 11 -0.6811 0.0431 13 4 12 0.3819 -0.0684 13 4 13 0.2268 -0.1056 13 4 14 1.6168 0.0645 13 4 15 0.4165 0.0254 13 4 16 -0.3434 0.1951 13 4 17 -0.6782 0.1307 13 4 18 -0.8741 -0.1656 13 5 0 -1.0151 -0.3378 13 5 1 -0.3408 -0.2411 13 5 2 0.7400 0.2586 13 5 3 0.9493 0.0212 13 5 4 -0.4408 -0.0477 13 5 5 -0.4514 0.1680 13 5 6 -0.0416 -0.0869 13 5 7 0.4646 -0.0396 13 5 8 0.7262 0.0228 13 5 9 0.1403 0.0051 13 5 10 -1.4092 -0.0058 13 5 11 -0.2846 -0.0878 13 5 12 0.8458 0.0829 13 5 13 0.9312 0.0790 13 5 14 0.6096 0.0126 13 5 15 -0.9391 -0.0442 13 5 16 -0.8782 -0.0233 13 5 17 -0.7721 -0.1199 13 5 18 0.4857 0.0520 13 6 0 0.2041 0.2518 13 6 1 0.3119 0.3311 13 6 2 0.5739 -0.1468 13 6 3 -0.2339 -0.0418 13 6 4 -0.6968 0.0410 13 6 5 -0.1967 -0.2010 13 6 6 -0.3072 0.0028 13 6 7 1.7356 0.1295 13 6 8 0.2714 0.0147 13 6 9 -1.5626 -0.0002 13 6 10 -0.8679 0.0145 13 6 11 0.8546 0.0563 13 6 12 0.9759 0.0103 13 6 13 -0.3712 -0.1744 13 6 14 -0.7000 -0.0389 13 6 15 -0.8059 -0.0372 13 6 16 -0.0189 0.0525 13 6 17 0.2685 0.1276 13 6 18 0.5199 -0.0587 13 7 0 -0.4721 -0.0579 13 7 1 0.4568 -0.4374 13 7 2 -0.7566 0.1021 13 7 3 -1.1937 0.0549 13 7 4 -0.1193 -0.0754 13 7 5 -0.0477 0.1300 13 7 6 1.0359 0.0581 13 7 7 0.3302 -0.0521 13 7 8 -2.6036 0.0912 13 7 9 -0.4830 -0.0265 13 7 10 1.1148 -0.0229 13 7 11 1.0051 -0.0813 13 7 12 -0.2496 -0.0810 13 7 13 -1.5677 0.1058 13 7 14 -0.2162 0.1281 13 7 15 0.1136 0.0635 13 7 16 0.2682 0.0020 13 7 17 -0.1828 -0.1783 13 7 18 0.2090 -0.2385 13 8 0 -0.4361 -0.1562 13 8 1 -0.2712 0.4239 13 8 2 -1.9736 0.0297 13 8 3 0.5158 -0.1092 13 8 4 0.7168 0.1912 13 8 5 -0.5304 -0.1842 13 8 6 -0.7118 -0.0724 13 8 7 -2.2890 0.1487 13 8 8 -0.0073 -0.0347 13 8 9 2.1447 -0.0435 13 8 10 0.8079 0.0781 13 8 11 -0.1122 0.0816 13 8 12 -1.9699 0.1175 13 8 13 -1.2958 0.0751 13 8 14 0.7456 -0.0457 13 8 15 0.1233 -0.0617 13 8 16 -0.0058 -0.1989 13 8 17 0.1335 -0.0336 13 8 18 0.4383 0.1422 13 9 0 0.1456 0.2428 13 9 1 -0.9736 -0.3319 13 9 2 0.1117 -0.0839 13 9 3 0.9575 0.1525 13 9 4 -0.9842 -0.1152 13 9 5 -1.6624 -0.0194 13 9 6 -0.4593 0.2116 13 9 7 0.6723 -0.1290 13 9 8 2.1150 0.0258 13 9 9 0.5537 0.2029 13 9 10 -0.4860 -0.0017 13 9 11 -1.5176 -0.0348 13 9 12 -2.0578 -0.1581 13 9 13 0.6209 0.0572 13 9 14 0.7918 0.0815 13 9 15 0.1484 0.0661 13 9 16 0.1470 -0.0339 13 9 17 -0.1226 0.1490 13 10 0 0.6727 -0.5050 13 10 1 -0.2545 0.3430 13 10 2 0.4231 0.2399 13 10 3 -0.5172 -0.1648 13 10 4 -0.3685 0.2336 13 10 5 0.2358 -0.0466 13 10 6 1.6761 -0.1662 13 10 7 0.5014 0.0088 13 10 8 0.1971 0.1248 13 10 9 -0.1603 -0.1231 13 10 10 -0.8824 -0.2167 13 10 11 -0.9223 0.0281 13 10 12 -0.2664 0.0984 13 10 13 0.8739 0.3727 13 10 14 0.2359 0.0735 13 10 15 0.4329 -0.0601 13 10 16 -0.5594 -0.1883 13 11 0 0.5314 0.4912 13 11 1 -0.1732 0.0160 13 11 2 0.2790 -0.3450 13 11 3 0.3336 0.3051 13 11 4 0.8894 -0.0186 13 11 5 0.9943 -0.3206 13 11 6 0.2340 0.2350 13 11 7 -0.6520 -0.1248 13 11 8 0.7085 -0.1158 13 11 9 0.0330 -0.1074 13 11 10 -0.0948 0.0912 13 11 11 0.3096 0.3446 13 11 12 -0.8387 0.0683 13 11 13 0.8012 0.0568 13 11 14 0.9820 -0.2616 13 11 15 0.1287 -0.1948 13 12 0 0.1893 -0.5638 13 12 1 0.0247 -0.1975 13 12 2 0.2244 0.4623 13 12 3 0.5044 0.1154 13 12 4 1.0268 -0.1408 13 12 5 0.1132 0.2315 13 12 6 -0.7384 -0.1046 13 12 7 0.6278 -0.2843 13 12 8 0.3830 0.1302 13 12 9 0.6494 -0.0113 13 12 10 0.7628 0.3226 13 12 11 -0.5479 0.0171 13 12 12 -0.0772 -0.3406 13 12 13 2.3200 -0.0868 13 13 3 0.7562 0.0227 13 13 4 0.2275 0.1872 13 13 5 -0.9894 -0.1510 13 13 6 0.0743 -0.3339 13 13 7 0.7411 0.0721 13 13 8 0.5076 0.1310 13 13 9 1.8161 0.1227 14 0 3 0.9715 -0.2164 14 0 4 1.2498 -0.0669 14 0 5 1.2984 0.3110 14 0 6 0.1708 0.0414 14 0 7 -0.5007 -0.3096 14 0 8 0.0330 -0.0930 14 0 9 -0.5094 0.2126 14 0 10 -0.7975 0.0438 14 0 11 -0.4431 -0.1935 14 1 1 -1.0023 -0.0866 14 1 2 0.5843 -0.2576 14 1 3 1.7232 0.1004 14 1 4 0.3622 -0.0219 14 1 5 0.1616 -0.1064 14 1 6 -0.4218 -0.0742 14 1 7 0.0857 0.0965 14 1 8 0.0870 0.0827 14 1 9 -1.0738 -0.1227 14 1 10 -0.6248 0.0589 14 1 11 0.0915 0.2209 14 1 12 0.3575 -0.0387 14 1 13 0.5285 -0.1898 14 2 1 -0.3786 -0.1577 14 2 2 1.2362 0.1629 14 2 3 -0.5002 -0.0715 14 2 4 -0.6642 -0.1749 14 2 5 1.2001 0.1705 14 2 6 0.1417 0.2010 14 2 7 0.2139 -0.1108 14 2 8 -0.4856 -0.2388 14 2 9 -0.6213 0.0881 14 2 10 0.0838 0.2466 14 2 11 0.7886 -0.1450 14 2 12 0.6816 -0.0185 14 2 13 -0.3486 0.2515 14 2 14 -0.6987 0.0072 14 2 15 0.1783 -0.2126 14 3 1 -0.2866 0.2421 14 3 2 -0.5326 -0.1379 14 3 3 -0.4985 -0.0875 14 3 4 1.4536 0.1021 14 3 5 0.9050 0.0591 14 3 6 -0.6468 -0.0161 14 3 7 0.4371 -0.1858 14 3 8 -0.1559 0.0786 14 3 9 0.1240 0.1273 14 3 10 0.5570 -0.0728 14 3 11 1.0181 0.0238 14 3 12 -0.4370 0.1575 14 3 13 -0.6670 -0.0872 14 3 14 0.2850 -0.1428 14 3 15 -0.2133 0.0757 14 4 0 -1.0046 -0.0435 14 4 1 -0.2717 -0.3204 14 4 2 0.5609 0.1426 14 4 3 0.9414 0.0591 14 4 4 0.4655 -0.0508 14 4 5 -0.4413 0.0857 14 4 6 0.3545 0.0608 14 4 7 0.5397 -0.0718 14 4 8 -0.0812 0.0164 14 4 9 0.4059 -0.0912 14 4 10 0.6364 0.0736 14 4 11 0.2591 0.0476 14 4 12 -0.7005 -0.0649 14 4 13 0.4733 0.0388 14 4 14 -0.4224 0.0110 14 4 15 -1.4740 0.0410 14 4 16 -0.2856 -0.0535 14 5 0 0.0347 -0.1741 14 5 1 1.1648 0.3657 14 5 2 0.6931 0.1083 14 5 3 -0.3523 -0.1972 14 5 4 -0.1445 0.1268 14 5 5 0.0796 -0.0253 14 5 6 0.3842 0.0071 14 5 7 0.0695 -0.0416 14 5 8 0.4606 -0.0308 14 5 9 0.1911 0.0776 14 5 10 0.3401 0.0615 14 5 11 -0.2562 0.0146 14 5 12 -0.1702 0.0546 14 5 13 0.0119 -0.0396 14 5 14 -1.4153 -0.1572 14 5 15 -0.5310 0.0028 14 5 16 0.6189 -0.0591 14 6 0 0.6522 0.2666 14 6 1 0.4464 -0.2055 14 6 2 -0.4314 -0.1407 14 6 3 -0.5770 0.0866 14 6 4 0.4475 -0.0058 14 6 5 -0.2449 0.0530 14 6 6 0.7971 0.1634 14 6 7 0.3296 -0.0875 14 6 8 -0.0347 0.0749 14 6 9 -0.1528 0.0546 14 6 10 0.1996 -0.0370 14 6 11 -0.3642 0.0013 14 6 12 0.1887 -0.1304 14 6 13 -0.0401 0.0505 14 6 14 -0.3419 0.0753 14 6 15 0.4873 0.1033 14 6 16 0.5116 0.0205 14 7 0 -0.0471 -0.3886 14 7 1 -0.3519 0.1841 14 7 2 -0.4854 0.2050 14 7 3 0.6637 -0.0567 14 7 4 0.5617 0.1319 14 7 5 -0.0392 0.0645 14 7 6 0.8953 -0.0611 14 7 7 -0.7278 0.0272 14 7 8 0.4624 -0.0070 14 7 9 0.5983 -0.0737 14 7 10 0.0108 0.0020 14 7 11 0.0972 0.0035 14 7 12 0.4603 0.1250 14 7 13 0.3579 0.1904 14 7 14 0.0749 -0.1429 14 7 15 0.1272 -0.1072 14 7 16 0.0652 -0.1318 14 8 0 0.3732 0.4002 14 8 1 -0.5313 0.0501 14 8 2 1.1792 -0.2261 14 8 3 0.8744 0.1541 14 8 4 -0.6683 -0.0757 14 8 5 0.2841 -0.0125 14 8 6 0.5806 0.1803 14 8 7 0.7700 -0.1290 14 8 8 1.6842 -0.1133 14 8 9 -0.2282 0.1812 14 8 10 -0.4481 0.0483 14 8 11 -0.0045 -0.0651 14 8 12 0.3683 -0.0799 14 8 13 0.9187 -0.1807 14 8 14 -0.1016 -0.1535 14 8 15 -0.1296 -0.0285 14 8 16 0.0902 0.1032 14 9 0 0.3059 -0.3351 14 9 1 0.1378 -0.0993 14 9 2 1.0371 0.2475 14 9 3 -0.9608 -0.0587 14 9 4 0.1403 -0.0104 14 9 5 1.7469 0.2841 14 9 6 1.1510 -0.2592 14 9 7 1.1937 -0.1381 14 9 8 -0.3400 0.2424 14 9 9 -1.0584 0.0273 14 9 10 -0.5652 -0.3099 14 9 11 0.2379 -0.2704 14 9 12 1.5022 0.0209 14 9 13 0.7740 0.1175 14 9 14 -0.9193 0.0051 14 9 15 -0.4126 -0.1240 14 10 0 -0.5696 0.3186 14 10 1 0.1728 0.2527 14 10 2 -0.1531 -0.2578 14 10 3 0.1930 0.0586 14 10 4 1.3866 0.0395 14 10 5 0.9187 -0.2133 14 10 6 -0.3249 -0.0676 14 10 7 -0.2287 0.2554 14 10 8 -0.7294 -0.0719 14 10 9 -0.5827 -0.2217 14 10 10 -0.2156 -0.0706 14 10 11 1.1656 0.1438 14 10 12 0.9953 0.2110 14 10 13 -0.8526 -0.2190 14 10 14 -0.9774 -0.3620 14 11 2 -0.1386 0.1976 14 11 3 0.4632 0.0151 14 11 4 -0.1255 -0.3515 14 11 5 -0.4862 0.3140 14 11 6 -0.7855 0.0982 14 11 7 0.4042 -0.0704 14 11 8 -0.6670 -0.0593 14 11 9 -0.6907 0.1873 14 11 10 0.3309 0.2138 14 11 11 0.1939 -0.1713 14 11 12 -0.1317 -0.3426 14 12 8 -1.1129 0.1277 15 3 4 0.6639 0.1244 15 3 5 -1.5169 -0.0542 15 3 6 -0.3711 -0.2090 15 3 7 -0.3230 0.0656 15 3 8 0.2135 0.2311 15 3 9 0.1327 -0.0785 15 3 10 -0.3348 -0.1812 15 4 4 -0.6797 0.0212 15 4 5 -0.9935 -0.0427 15 4 6 0.1793 -0.0815 15 4 7 -0.7467 0.1244 15 4 8 0.0627 -0.1178 15 4 9 -0.3256 -0.0187 15 4 10 -0.7323 0.0482 15 4 11 -0.6283 -0.0543 15 4 12 0.7378 -0.1215 15 5 3 0.1021 0.0196 15 5 4 -0.7435 -0.0141 15 5 5 -0.2611 -0.0228 15 5 6 -0.2280 -0.0120 15 5 7 -0.4610 -0.0326 15 5 8 -0.0171 -0.0134 15 5 9 -0.8216 0.1024 15 5 10 -1.0484 -0.1239 15 5 11 -0.0166 -0.0526 15 5 12 1.1351 -0.0972 15 5 13 0.2141 -0.0838 15 6 3 0.1849 0.0276 15 6 4 -0.4649 -0.0460 15 6 5 0.2898 0.0656 15 6 6 -0.3532 -0.1943 15 6 7 -0.3956 0.0420 15 6 8 -0.7810 0.0223 15 6 9 -0.9351 -0.1354 15 6 10 -0.4455 -0.1042 15 6 11 1.2052 -0.0335 15 6 12 0.8069 0.0156 15 6 13 -0.2715 0.0780 15 7 2 0.3768 -0.1507 15 7 3 0.4589 -0.0399 15 7 4 -0.6729 -0.0599 15 7 5 0.3039 -0.1561 15 7 6 -0.9569 -0.0413 15 7 7 -0.3854 0.0780 15 7 8 -0.6554 -0.1572 15 7 9 -0.1972 -0.0376 15 7 10 0.4834 0.0192 15 7 11 0.7817 0.0500 15 7 12 -0.8285 0.0664 15 7 13 -0.7506 -0.2379 15 8 3 -0.8511 -0.0506 15 8 4 -0.3449 -0.1421 15 8 5 0.4448 0.1094 15 8 6 -1.0889 -0.1123 15 8 7 -0.0276 -0.0861 15 8 8 -0.7583 0.1042 15 8 9 -0.1181 0.0236 15 8 10 0.0137 -0.1210 15 8 11 -0.6544 -0.0507 15 8 12 -0.9425 -0.0753 15 9 4 0.7362 0.1519 15 9 5 -0.8765 -0.2397 15 9 6 -1.1968 -0.1484 15 9 7 -0.4318 0.3101 15 9 8 -0.8706 0.0462 15 9 9 -0.1378 -0.2786 15 9 10 -0.2487 -0.0932 15 9 11 -0.4494 0.2410 0 0 0 0.0 0.0 ; _shelx_fab_checksum 21143 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_007a-22007 _database_code_depnum_ccdc_archive 'CCDC 2226344' loop_ _audit_author_name _audit_author_address 'Brandon Mercado' ;Yale University United States of America ; _audit_update_record ; 2022-12-13 deposited with the CCDC. 2024-02-06 downloaded from the CCDC. ; _audit_creation_method SHELXL-2014/7 _shelx_SHELXL_version_number 2014/7 _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C41 H62 Fe N4 Si2' _chemical_formula_weight 722.97 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 11.9946(2) _cell_length_b 19.7217(3) _cell_length_c 17.1523(3) _cell_angle_alpha 90 _cell_angle_beta 95.2570(10) _cell_angle_gamma 90 _cell_volume 4040.38(12) _cell_formula_units_Z 4 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 65353 _cell_measurement_theta_min 2.2420 _cell_measurement_theta_max 66.7920 _exptl_crystal_description Plate _exptl_crystal_colour Black _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.189 _exptl_crystal_F_000 1560 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.020 _exptl_absorpt_coefficient_mu 3.798 _shelx_estimated_absorpt_T_min 0.517 _shelx_estimated_absorpt_T_max 0.928 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.79405 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 126800 _diffrn_reflns_av_unetI/netI 0.0168 _diffrn_reflns_av_R_equivalents 0.0574 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 3.423 _diffrn_reflns_theta_max 66.601 _diffrn_reflns_theta_full 66.601 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 7123 _reflns_number_gt 6762 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0342P)^2^+2.2267P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7123 _refine_ls_number_parameters 447 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0313 _refine_ls_R_factor_gt 0.0295 _refine_ls_wR_factor_ref 0.0744 _refine_ls_wR_factor_gt 0.0733 _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_restrained_S_all 1.037 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.53522(2) 0.30813(2) 0.26502(2) 0.01514(7) Uani 1 1 d . . . . . Si24 Si 0.25317(3) 0.18775(2) 0.20501(3) 0.02126(10) Uani 1 1 d . . . . . Si14 Si 0.45862(4) 0.15714(2) 0.12982(3) 0.02272(10) Uani 1 1 d . . . . . N1 N 0.46309(10) 0.22209(6) 0.27547(7) 0.0205(3) Uani 1 1 d . . . . . N2 N 0.39907(11) 0.18666(6) 0.21188(8) 0.0219(3) Uani 1 1 d . . . . . N11 N 0.48303(10) 0.39983(6) 0.29494(7) 0.0162(2) Uani 1 1 d . . . . . N21 N 0.69657(10) 0.33392(6) 0.26950(7) 0.0166(3) Uani 1 1 d . . . . . C11 C 0.50777(13) 0.51050(8) 0.36073(10) 0.0246(3) Uani 1 1 d . . . . . H11A H 0.4589 0.5312 0.3183 0.037 Uiso 1 1 calc R U . . . H11B H 0.5702 0.5412 0.3761 0.037 Uiso 1 1 calc R U . . . H11C H 0.4649 0.5022 0.4058 0.037 Uiso 1 1 calc R U . . . C21 C 0.55282(12) 0.44413(7) 0.33291(9) 0.0182(3) Uani 1 1 d . . . . . C31 C 0.66863(12) 0.43350(8) 0.34722(9) 0.0201(3) Uani 1 1 d . . . . . H31 H 0.7065 0.4635 0.3840 0.024 Uiso 1 1 calc R U . . . C41 C 0.73639(12) 0.38487(7) 0.31497(9) 0.0183(3) Uani 1 1 d . . . . . C51 C 0.86119(12) 0.39287(8) 0.33456(10) 0.0241(3) Uani 1 1 d . . . . . H51A H 0.8843 0.3681 0.3829 0.036 Uiso 1 1 calc R U . . . H51B H 0.8794 0.4410 0.3417 0.036 Uiso 1 1 calc R U . . . H51C H 0.9008 0.3746 0.2917 0.036 Uiso 1 1 calc R U . . . C12 C 0.36825(12) 0.41915(7) 0.27429(8) 0.0161(3) Uani 1 1 d . . . . . C62 C 0.33768(12) 0.43825(7) 0.19605(9) 0.0174(3) Uani 1 1 d . . . . . C52 C 0.22686(12) 0.45741(7) 0.17537(9) 0.0201(3) Uani 1 1 d . . . . . H52 H 0.2053 0.4720 0.1234 0.024 Uiso 1 1 calc R U . . . C42 C 0.14810(12) 0.45557(8) 0.22902(9) 0.0220(3) Uani 1 1 d . . . . . H42 H 0.0731 0.4690 0.2140 0.026 Uiso 1 1 calc R U . . . C32 C 0.17855(12) 0.43408(8) 0.30485(9) 0.0207(3) Uani 1 1 d . . . . . H32 H 0.1233 0.4319 0.3411 0.025 Uiso 1 1 calc R U . . . C22 C 0.28854(12) 0.41554(7) 0.32919(9) 0.0184(3) Uani 1 1 d . . . . . C102 C 0.42260(12) 0.43739(8) 0.13560(9) 0.0200(3) Uani 1 1 d . . . . . H102 H 0.4756 0.3993 0.1500 0.024 Uiso 1 1 calc R U . . . C112 C 0.49220(14) 0.50226(8) 0.13774(10) 0.0262(3) Uani 1 1 d . . . . . H11D H 0.5467 0.4994 0.0986 0.039 Uiso 1 1 calc R U . . . H11E H 0.5318 0.5078 0.1899 0.039 Uiso 1 1 calc R U . . . H11F H 0.4428 0.5412 0.1261 0.039 Uiso 1 1 calc R U . . . C122 C 0.37022(14) 0.42320(9) 0.05251(9) 0.0272(4) Uani 1 1 d . . . . . H12A H 0.3234 0.4617 0.0340 0.041 Uiso 1 1 calc R U . . . H12B H 0.3241 0.3822 0.0526 0.041 Uiso 1 1 calc R U . . . H12C H 0.4296 0.4166 0.0176 0.041 Uiso 1 1 calc R U . . . C72 C 0.31549(13) 0.38740(8) 0.41126(9) 0.0220(3) Uani 1 1 d . . . . . H72 H 0.3987 0.3866 0.4227 0.026 Uiso 1 1 calc R U . . . C82 C 0.26635(15) 0.43029(10) 0.47434(10) 0.0323(4) Uani 1 1 d . . . . . H82A H 0.2944 0.4768 0.4721 0.048 Uiso 1 1 calc R U . . . H82B H 0.2887 0.4110 0.5261 0.048 Uiso 1 1 calc R U . . . H82C H 0.1845 0.4305 0.4652 0.048 Uiso 1 1 calc R U . . . C92 C 0.27262(15) 0.31424(8) 0.41415(10) 0.0281(4) Uani 1 1 d . . . . . H92A H 0.1917 0.3135 0.3996 0.042 Uiso 1 1 calc R U . . . H92B H 0.2883 0.2963 0.4673 0.042 Uiso 1 1 calc R U . . . H92C H 0.3105 0.2862 0.3774 0.042 Uiso 1 1 calc R U . . . C13 C 0.77183(12) 0.29527(7) 0.22556(9) 0.0171(3) Uani 1 1 d . . . . . C63 C 0.79010(12) 0.31783(8) 0.14983(9) 0.0189(3) Uani 1 1 d . . . . . C53 C 0.85783(12) 0.27901(8) 0.10568(9) 0.0227(3) Uani 1 1 d . . . . . H53 H 0.8728 0.2942 0.0551 0.027 Uiso 1 1 calc R U . . . C43 C 0.90382(13) 0.21851(8) 0.13435(10) 0.0244(3) Uani 1 1 d . . . . . H43 H 0.9490 0.1922 0.1032 0.029 Uiso 1 1 calc R U . . . C33 C 0.88393(13) 0.19652(8) 0.20813(10) 0.0229(3) Uani 1 1 d . . . . . H33 H 0.9149 0.1546 0.2269 0.027 Uiso 1 1 calc R U . . . C23 C 0.81940(12) 0.23445(8) 0.25571(9) 0.0194(3) Uani 1 1 d . . . . . C103 C 0.73691(13) 0.38270(8) 0.11533(9) 0.0222(3) Uani 1 1 d . . . . . H103 H 0.6676 0.3915 0.1420 0.027 Uiso 1 1 calc R U . . . C113 C 0.81475(15) 0.44377(8) 0.13068(11) 0.0314(4) Uani 1 1 d . . . . . H11G H 0.8288 0.4511 0.1872 0.047 Uiso 1 1 calc R U . . . H11H H 0.7794 0.4842 0.1061 0.047 Uiso 1 1 calc R U . . . H11I H 0.8858 0.4350 0.1085 0.047 Uiso 1 1 calc R U . . . C123 C 0.70247(15) 0.37710(9) 0.02724(10) 0.0312(4) Uani 1 1 d . . . . . H12D H 0.7696 0.3762 -0.0013 0.047 Uiso 1 1 calc R U . . . H12E H 0.6561 0.4162 0.0101 0.047 Uiso 1 1 calc R U . . . H12F H 0.6596 0.3353 0.0166 0.047 Uiso 1 1 calc R U . . . C73 C 0.80444(13) 0.20930(8) 0.33774(9) 0.0228(3) Uani 1 1 d . . . . . H73 H 0.7497 0.2399 0.3609 0.027 Uiso 1 1 calc R U . . . C83 C 0.91520(15) 0.21211(10) 0.39049(10) 0.0333(4) Uani 1 1 d . . . . . H83A H 0.9674 0.1786 0.3725 0.050 Uiso 1 1 calc R U . . . H83B H 0.9009 0.2020 0.4446 0.050 Uiso 1 1 calc R U . . . H83C H 0.9478 0.2575 0.3879 0.050 Uiso 1 1 calc R U . . . C93 C 0.75739(14) 0.13736(8) 0.33725(11) 0.0301(4) Uani 1 1 d . . . . . H93A H 0.6886 0.1352 0.3018 0.045 Uiso 1 1 calc R U . . . H93B H 0.7408 0.1250 0.3903 0.045 Uiso 1 1 calc R U . . . H93C H 0.8126 0.1057 0.3193 0.045 Uiso 1 1 calc R U . . . C1 C 0.48514(12) 0.18552(8) 0.34479(9) 0.0199(3) Uani 1 1 d . . . . . C2 C 0.53476(13) 0.22100(9) 0.41076(9) 0.0247(3) Uani 1 1 d . . . . . H2 H 0.5470 0.2684 0.4072 0.030 Uiso 1 1 calc R U . . . C3 C 0.56560(14) 0.18785(10) 0.48024(10) 0.0316(4) Uani 1 1 d . . . . . H3 H 0.6009 0.2124 0.5233 0.038 Uiso 1 1 calc R U . . . C4 C 0.54550(14) 0.11913(10) 0.48774(11) 0.0344(4) Uani 1 1 d . . . . . H4 H 0.5670 0.0963 0.5355 0.041 Uiso 1 1 calc R U . . . C5 C 0.49342(13) 0.08428(9) 0.42434(11) 0.0310(4) Uani 1 1 d . . . . . H5 H 0.4780 0.0373 0.4294 0.037 Uiso 1 1 calc R U . . . C6 C 0.46331(13) 0.11664(8) 0.35363(10) 0.0260(4) Uani 1 1 d . . . . . H6 H 0.4276 0.0917 0.3110 0.031 Uiso 1 1 calc R U . . . C24 C 0.22926(14) 0.13232(9) 0.11622(10) 0.0293(4) Uani 1 1 d . . . . . H24A H 0.2280 0.0840 0.1320 0.035 Uiso 1 1 calc R U . . . H24B H 0.1565 0.1434 0.0870 0.035 Uiso 1 1 calc R U . . . C14 C 0.32611(14) 0.14504(10) 0.06405(10) 0.0328(4) Uani 1 1 d . . . . . H14A H 0.3103 0.1860 0.0315 0.039 Uiso 1 1 calc R U . . . H14B H 0.3339 0.1059 0.0289 0.039 Uiso 1 1 calc R U . . . C64 C 0.19796(14) 0.27532(8) 0.18912(10) 0.0270(4) Uani 1 1 d . . . . . H64A H 0.2221 0.3034 0.2347 0.040 Uiso 1 1 calc R U . . . H64B H 0.1160 0.2740 0.1820 0.040 Uiso 1 1 calc R U . . . H64C H 0.2267 0.2946 0.1423 0.040 Uiso 1 1 calc R U . . . C54 C 0.19332(14) 0.15018(9) 0.29160(10) 0.0292(4) Uani 1 1 d . . . . . H54A H 0.2140 0.1022 0.2961 0.044 Uiso 1 1 calc R U . . . H54B H 0.1116 0.1543 0.2853 0.044 Uiso 1 1 calc R U . . . H54C H 0.2228 0.1743 0.3391 0.044 Uiso 1 1 calc R U . . . C44 C 0.55324(15) 0.22113(9) 0.09158(10) 0.0318(4) Uani 1 1 d . . . . . H44A H 0.5169 0.2657 0.0901 0.048 Uiso 1 1 calc R U . . . H44B H 0.5696 0.2084 0.0386 0.048 Uiso 1 1 calc R U . . . H44C H 0.6232 0.2231 0.1258 0.048 Uiso 1 1 calc R U . . . C34 C 0.53865(17) 0.07686(9) 0.14627(12) 0.0370(4) Uani 1 1 d . . . . . H34A H 0.6030 0.0846 0.1847 0.056 Uiso 1 1 calc R U . . . H34B H 0.5650 0.0616 0.0968 0.056 Uiso 1 1 calc R U . . . H34C H 0.4901 0.0421 0.1660 0.056 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.01355(12) 0.01268(12) 0.01935(13) -0.00066(9) 0.00232(9) -0.00058(8) Si24 0.0184(2) 0.0185(2) 0.0270(2) -0.00227(16) 0.00266(17) -0.00325(15) Si14 0.0222(2) 0.0212(2) 0.0254(2) -0.00165(17) 0.00612(17) -0.00534(17) N1 0.0203(6) 0.0198(6) 0.0212(7) -0.0015(5) 0.0013(5) -0.0034(5) N2 0.0198(6) 0.0212(7) 0.0246(7) -0.0042(5) 0.0016(5) -0.0045(5) N11 0.0144(6) 0.0167(6) 0.0172(6) -0.0003(5) 0.0008(5) 0.0007(5) N21 0.0153(6) 0.0166(6) 0.0182(6) -0.0004(5) 0.0026(5) 0.0015(5) C11 0.0223(8) 0.0213(8) 0.0298(9) -0.0077(7) -0.0002(6) 0.0013(6) C21 0.0209(7) 0.0171(7) 0.0167(7) -0.0020(6) 0.0016(6) 0.0002(6) C31 0.0190(7) 0.0197(7) 0.0208(8) -0.0053(6) -0.0015(6) -0.0013(6) C41 0.0171(7) 0.0188(7) 0.0187(7) 0.0014(6) 0.0005(6) -0.0014(6) C51 0.0159(7) 0.0262(8) 0.0299(9) -0.0057(7) 0.0003(6) -0.0022(6) C12 0.0159(7) 0.0116(7) 0.0204(7) -0.0023(6) -0.0001(6) 0.0009(5) C62 0.0191(7) 0.0121(7) 0.0208(8) -0.0013(6) 0.0007(6) -0.0015(6) C52 0.0220(8) 0.0163(7) 0.0213(8) 0.0018(6) -0.0024(6) 0.0007(6) C42 0.0173(7) 0.0180(7) 0.0299(9) -0.0004(6) -0.0017(6) 0.0029(6) C32 0.0175(7) 0.0199(8) 0.0250(8) -0.0022(6) 0.0044(6) 0.0014(6) C22 0.0185(7) 0.0166(7) 0.0200(8) -0.0034(6) 0.0010(6) 0.0004(6) C102 0.0217(7) 0.0187(7) 0.0198(8) 0.0027(6) 0.0023(6) 0.0009(6) C112 0.0269(8) 0.0266(8) 0.0256(8) 0.0023(7) 0.0047(7) -0.0053(7) C122 0.0320(9) 0.0299(9) 0.0200(8) -0.0003(7) 0.0038(7) -0.0045(7) C72 0.0190(7) 0.0289(8) 0.0183(8) -0.0002(6) 0.0025(6) 0.0037(6) C82 0.0330(9) 0.0421(10) 0.0221(8) -0.0048(8) 0.0042(7) 0.0055(8) C92 0.0306(9) 0.0303(9) 0.0234(9) 0.0060(7) 0.0031(7) 0.0026(7) C13 0.0115(7) 0.0187(7) 0.0212(8) -0.0035(6) 0.0024(6) -0.0017(6) C63 0.0152(7) 0.0209(7) 0.0206(8) -0.0011(6) 0.0009(6) -0.0030(6) C53 0.0189(7) 0.0288(8) 0.0208(8) -0.0022(6) 0.0045(6) -0.0038(6) C43 0.0184(7) 0.0282(8) 0.0272(9) -0.0074(7) 0.0056(6) 0.0018(6) C33 0.0180(7) 0.0220(8) 0.0286(9) -0.0015(6) 0.0017(6) 0.0028(6) C23 0.0135(7) 0.0207(8) 0.0241(8) -0.0009(6) 0.0021(6) -0.0004(6) C103 0.0208(7) 0.0227(8) 0.0234(8) 0.0034(6) 0.0041(6) 0.0003(6) C113 0.0358(9) 0.0230(9) 0.0352(10) 0.0021(7) 0.0018(8) -0.0024(7) C123 0.0353(9) 0.0298(9) 0.0278(9) 0.0075(7) -0.0013(7) -0.0039(7) C73 0.0215(8) 0.0224(8) 0.0254(8) 0.0039(7) 0.0065(6) 0.0052(6) C83 0.0344(10) 0.0384(10) 0.0263(9) 0.0067(8) -0.0008(7) 0.0011(8) C93 0.0269(8) 0.0253(9) 0.0396(10) 0.0059(7) 0.0110(7) 0.0028(7) C1 0.0139(7) 0.0238(8) 0.0229(8) 0.0023(6) 0.0059(6) 0.0023(6) C2 0.0200(8) 0.0293(9) 0.0256(8) 0.0014(7) 0.0056(6) 0.0015(7) C3 0.0193(8) 0.0522(12) 0.0236(9) 0.0014(8) 0.0039(7) 0.0057(7) C4 0.0227(8) 0.0502(11) 0.0311(10) 0.0174(8) 0.0071(7) 0.0072(8) C5 0.0218(8) 0.0310(9) 0.0413(10) 0.0133(8) 0.0084(7) 0.0032(7) C6 0.0200(8) 0.0252(8) 0.0334(9) 0.0034(7) 0.0056(7) 0.0010(6) C24 0.0239(8) 0.0284(9) 0.0358(10) -0.0083(7) 0.0036(7) -0.0072(7) C14 0.0309(9) 0.0407(10) 0.0272(9) -0.0091(8) 0.0045(7) -0.0110(8) C64 0.0255(8) 0.0244(8) 0.0299(9) 0.0001(7) -0.0030(7) -0.0027(7) C54 0.0223(8) 0.0287(9) 0.0370(10) 0.0052(7) 0.0050(7) -0.0003(7) C44 0.0322(9) 0.0358(10) 0.0280(9) 0.0002(8) 0.0051(7) -0.0110(8) C34 0.0454(11) 0.0286(9) 0.0399(11) -0.0021(8) 0.0186(9) 0.0043(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 1.9205(13) . ? Fe1 N21 1.9957(12) . ? Fe1 N11 1.9962(12) . ? Si24 N2 1.7433(13) . ? Si24 C64 1.8607(17) . ? Si24 C54 1.8618(17) . ? Si24 C24 1.8753(17) . ? Si14 N2 1.7363(14) . ? Si14 C44 1.8567(17) . ? Si14 C34 1.8596(19) . ? Si14 C14 1.8780(18) . ? N1 C1 1.395(2) . ? N1 N2 1.4540(18) . ? N11 C21 1.3373(19) . ? N11 C12 1.4411(18) . ? N21 C41 1.3332(19) . ? N21 C13 1.4452(19) . ? C11 C21 1.510(2) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C21 C31 1.404(2) . ? C31 C41 1.403(2) . ? C31 H31 0.9500 . ? C41 C51 1.512(2) . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C12 C22 1.404(2) . ? C12 C62 1.410(2) . ? C62 C52 1.396(2) . ? C62 C102 1.519(2) . ? C52 C42 1.378(2) . ? C52 H52 0.9500 . ? C42 C32 1.385(2) . ? C42 H42 0.9500 . ? C32 C22 1.396(2) . ? C32 H32 0.9500 . ? C22 C72 1.520(2) . ? C102 C112 1.526(2) . ? C102 C122 1.530(2) . ? C102 H102 1.0000 . ? C112 H11D 0.9800 . ? C112 H11E 0.9800 . ? C112 H11F 0.9800 . ? C122 H12A 0.9800 . ? C122 H12B 0.9800 . ? C122 H12C 0.9800 . ? C72 C82 1.533(2) . ? C72 C92 1.534(2) . ? C72 H72 1.0000 . ? C82 H82A 0.9800 . ? C82 H82B 0.9800 . ? C82 H82C 0.9800 . ? C92 H92A 0.9800 . ? C92 H92B 0.9800 . ? C92 H92C 0.9800 . ? C13 C23 1.406(2) . ? C13 C63 1.409(2) . ? C63 C53 1.390(2) . ? C63 C103 1.525(2) . ? C53 C43 1.386(2) . ? C53 H53 0.9500 . ? C43 C33 1.379(2) . ? C43 H43 0.9500 . ? C33 C23 1.393(2) . ? C33 H33 0.9500 . ? C23 C73 1.518(2) . ? C103 C113 1.532(2) . ? C103 C123 1.533(2) . ? C103 H103 1.0000 . ? C113 H11G 0.9800 . ? C113 H11H 0.9800 . ? C113 H11I 0.9800 . ? C123 H12D 0.9800 . ? C123 H12E 0.9800 . ? C123 H12F 0.9800 . ? C73 C93 1.527(2) . ? C73 C83 1.538(2) . ? C73 H73 1.0000 . ? C83 H83A 0.9800 . ? C83 H83B 0.9800 . ? C83 H83C 0.9800 . ? C93 H93A 0.9800 . ? C93 H93B 0.9800 . ? C93 H93C 0.9800 . ? C1 C6 1.394(2) . ? C1 C2 1.415(2) . ? C2 C3 1.380(2) . ? C2 H2 0.9500 . ? C3 C4 1.385(3) . ? C3 H3 0.9500 . ? C4 C5 1.386(3) . ? C4 H4 0.9500 . ? C5 C6 1.389(2) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C24 C14 1.550(2) . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C64 H64A 0.9800 . ? C64 H64B 0.9800 . ? C64 H64C 0.9800 . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N21 131.69(5) . . ? N1 Fe1 N11 128.46(5) . . ? N21 Fe1 N11 94.88(5) . . ? N2 Si24 C64 111.29(7) . . ? N2 Si24 C54 113.53(7) . . ? C64 Si24 C54 109.16(8) . . ? N2 Si24 C24 97.22(7) . . ? C64 Si24 C24 113.34(8) . . ? C54 Si24 C24 111.99(8) . . ? N2 Si14 C44 111.63(7) . . ? N2 Si14 C34 114.04(8) . . ? C44 Si14 C34 107.97(9) . . ? N2 Si14 C14 98.11(7) . . ? C44 Si14 C14 112.66(8) . . ? C34 Si14 C14 112.31(9) . . ? C1 N1 N2 115.89(12) . . ? C1 N1 Fe1 118.98(10) . . ? N2 N1 Fe1 124.48(9) . . ? N1 N2 Si14 122.76(10) . . ? N1 N2 Si24 120.18(10) . . ? Si14 N2 Si24 115.74(7) . . ? C21 N11 C12 119.23(12) . . ? C21 N11 Fe1 121.34(10) . . ? C12 N11 Fe1 119.43(9) . . ? C41 N21 C13 119.68(12) . . ? C41 N21 Fe1 120.58(10) . . ? C13 N21 Fe1 119.69(9) . . ? C21 C11 H11A 109.5 . . ? C21 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C21 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N11 C21 C31 123.56(13) . . ? N11 C21 C11 119.61(13) . . ? C31 C21 C11 116.82(13) . . ? C41 C31 C21 129.24(14) . . ? C41 C31 H31 115.4 . . ? C21 C31 H31 115.4 . . ? N21 C41 C31 123.80(13) . . ? N21 C41 C51 120.19(13) . . ? C31 C41 C51 116.01(13) . . ? C41 C51 H51A 109.5 . . ? C41 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C41 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C22 C12 C62 121.23(13) . . ? C22 C12 N11 121.05(13) . . ? C62 C12 N11 117.64(13) . . ? C52 C62 C12 118.21(14) . . ? C52 C62 C102 120.80(13) . . ? C12 C62 C102 120.98(13) . . ? C42 C52 C62 121.21(14) . . ? C42 C52 H52 119.4 . . ? C62 C52 H52 119.4 . . ? C52 C42 C32 119.80(14) . . ? C52 C42 H42 120.1 . . ? C32 C42 H42 120.1 . . ? C42 C32 C22 121.47(14) . . ? C42 C32 H32 119.3 . . ? C22 C32 H32 119.3 . . ? C32 C22 C12 117.98(14) . . ? C32 C22 C72 119.19(13) . . ? C12 C22 C72 122.66(13) . . ? C62 C102 C112 111.95(13) . . ? C62 C102 C122 113.22(13) . . ? C112 C102 C122 110.66(13) . . ? C62 C102 H102 106.9 . . ? C112 C102 H102 106.9 . . ? C122 C102 H102 106.9 . . ? C102 C112 H11D 109.5 . . ? C102 C112 H11E 109.5 . . ? H11D C112 H11E 109.5 . . ? C102 C112 H11F 109.5 . . ? H11D C112 H11F 109.5 . . ? H11E C112 H11F 109.5 . . ? C102 C122 H12A 109.5 . . ? C102 C122 H12B 109.5 . . ? H12A C122 H12B 109.5 . . ? C102 C122 H12C 109.5 . . ? H12A C122 H12C 109.5 . . ? H12B C122 H12C 109.5 . . ? C22 C72 C82 112.91(13) . . ? C22 C72 C92 109.26(13) . . ? C82 C72 C92 110.15(14) . . ? C22 C72 H72 108.1 . . ? C82 C72 H72 108.1 . . ? C92 C72 H72 108.1 . . ? C72 C82 H82A 109.5 . . ? C72 C82 H82B 109.5 . . ? H82A C82 H82B 109.5 . . ? C72 C82 H82C 109.5 . . ? H82A C82 H82C 109.5 . . ? H82B C82 H82C 109.5 . . ? C72 C92 H92A 109.5 . . ? C72 C92 H92B 109.5 . . ? H92A C92 H92B 109.5 . . ? C72 C92 H92C 109.5 . . ? H92A C92 H92C 109.5 . . ? H92B C92 H92C 109.5 . . ? C23 C13 C63 121.08(14) . . ? C23 C13 N21 120.66(13) . . ? C63 C13 N21 118.13(13) . . ? C53 C63 C13 118.44(14) . . ? C53 C63 C103 119.69(14) . . ? C13 C63 C103 121.86(13) . . ? C43 C53 C63 120.97(15) . . ? C43 C53 H53 119.5 . . ? C63 C53 H53 119.5 . . ? C33 C43 C53 119.98(14) . . ? C33 C43 H43 120.0 . . ? C53 C43 H43 120.0 . . ? C43 C33 C23 121.39(15) . . ? C43 C33 H33 119.3 . . ? C23 C33 H33 119.3 . . ? C33 C23 C13 118.11(14) . . ? C33 C23 C73 119.13(14) . . ? C13 C23 C73 122.76(13) . . ? C63 C103 C113 111.48(13) . . ? C63 C103 C123 112.79(13) . . ? C113 C103 C123 109.32(13) . . ? C63 C103 H103 107.7 . . ? C113 C103 H103 107.7 . . ? C123 C103 H103 107.7 . . ? C103 C113 H11G 109.5 . . ? C103 C113 H11H 109.5 . . ? H11G C113 H11H 109.5 . . ? C103 C113 H11I 109.5 . . ? H11G C113 H11I 109.5 . . ? H11H C113 H11I 109.5 . . ? C103 C123 H12D 109.5 . . ? C103 C123 H12E 109.5 . . ? H12D C123 H12E 109.5 . . ? C103 C123 H12F 109.5 . . ? H12D C123 H12F 109.5 . . ? H12E C123 H12F 109.5 . . ? C23 C73 C93 111.94(14) . . ? C23 C73 C83 111.37(13) . . ? C93 C73 C83 109.61(14) . . ? C23 C73 H73 107.9 . . ? C93 C73 H73 107.9 . . ? C83 C73 H73 107.9 . . ? C73 C83 H83A 109.5 . . ? C73 C83 H83B 109.5 . . ? H83A C83 H83B 109.5 . . ? C73 C83 H83C 109.5 . . ? H83A C83 H83C 109.5 . . ? H83B C83 H83C 109.5 . . ? C73 C93 H93A 109.5 . . ? C73 C93 H93B 109.5 . . ? H93A C93 H93B 109.5 . . ? C73 C93 H93C 109.5 . . ? H93A C93 H93C 109.5 . . ? H93B C93 H93C 109.5 . . ? C6 C1 N1 125.00(15) . . ? C6 C1 C2 117.67(15) . . ? N1 C1 C2 117.33(14) . . ? C3 C2 C1 121.09(16) . . ? C3 C2 H2 119.5 . . ? C1 C2 H2 119.5 . . ? C2 C3 C4 120.59(17) . . ? C2 C3 H3 119.7 . . ? C4 C3 H3 119.7 . . ? C3 C4 C5 118.84(16) . . ? C3 C4 H4 120.6 . . ? C5 C4 H4 120.6 . . ? C4 C5 C6 121.31(17) . . ? C4 C5 H5 119.3 . . ? C6 C5 H5 119.3 . . ? C5 C6 C1 120.43(16) . . ? C5 C6 H6 119.8 . . ? C1 C6 H6 119.8 . . ? C14 C24 Si24 107.90(11) . . ? C14 C24 H24A 110.1 . . ? Si24 C24 H24A 110.1 . . ? C14 C24 H24B 110.1 . . ? Si24 C24 H24B 110.1 . . ? H24A C24 H24B 108.4 . . ? C24 C14 Si14 108.16(12) . . ? C24 C14 H14A 110.1 . . ? Si14 C14 H14A 110.1 . . ? C24 C14 H14B 110.1 . . ? Si14 C14 H14B 110.1 . . ? H14A C14 H14B 108.4 . . ? Si24 C64 H64A 109.5 . . ? Si24 C64 H64B 109.5 . . ? H64A C64 H64B 109.5 . . ? Si24 C64 H64C 109.5 . . ? H64A C64 H64C 109.5 . . ? H64B C64 H64C 109.5 . . ? Si24 C54 H54A 109.5 . . ? Si24 C54 H54B 109.5 . . ? H54A C54 H54B 109.5 . . ? Si24 C54 H54C 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? Si14 C44 H44A 109.5 . . ? Si14 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? Si14 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? Si14 C34 H34A 109.5 . . ? Si14 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? Si14 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N1 N2 Si14 -107.02(13) . . . . ? Fe1 N1 N2 Si14 63.62(14) . . . . ? C1 N1 N2 Si24 86.70(14) . . . . ? Fe1 N1 N2 Si24 -102.66(11) . . . . ? C44 Si14 N2 N1 -44.34(14) . . . . ? C34 Si14 N2 N1 78.37(13) . . . . ? C14 Si14 N2 N1 -162.72(12) . . . . ? C44 Si14 N2 Si24 122.50(9) . . . . ? C34 Si14 N2 Si24 -114.79(10) . . . . ? C14 Si14 N2 Si24 4.13(10) . . . . ? C64 Si24 N2 N1 63.27(13) . . . . ? C54 Si24 N2 N1 -60.35(13) . . . . ? C24 Si24 N2 N1 -178.17(11) . . . . ? C64 Si24 N2 Si14 -103.93(9) . . . . ? C54 Si24 N2 Si14 132.44(9) . . . . ? C24 Si24 N2 Si14 14.62(10) . . . . ? C12 N11 C21 C31 -172.00(14) . . . . ? Fe1 N11 C21 C31 7.1(2) . . . . ? C12 N11 C21 C11 6.3(2) . . . . ? Fe1 N11 C21 C11 -174.62(11) . . . . ? N11 C21 C31 C41 13.0(3) . . . . ? C11 C21 C31 C41 -165.34(16) . . . . ? C13 N21 C41 C31 166.74(14) . . . . ? Fe1 N21 C41 C31 -15.8(2) . . . . ? C13 N21 C41 C51 -13.2(2) . . . . ? Fe1 N21 C41 C51 164.22(11) . . . . ? C21 C31 C41 N21 -7.9(3) . . . . ? C21 C31 C41 C51 172.04(15) . . . . ? C21 N11 C12 C22 -81.47(17) . . . . ? Fe1 N11 C12 C22 99.40(14) . . . . ? C21 N11 C12 C62 101.89(16) . . . . ? Fe1 N11 C12 C62 -77.25(14) . . . . ? C22 C12 C62 C52 3.7(2) . . . . ? N11 C12 C62 C52 -179.68(12) . . . . ? C22 C12 C62 C102 -175.75(13) . . . . ? N11 C12 C62 C102 0.9(2) . . . . ? C12 C62 C52 C42 -2.2(2) . . . . ? C102 C62 C52 C42 177.20(14) . . . . ? C62 C52 C42 C32 -0.3(2) . . . . ? C52 C42 C32 C22 1.5(2) . . . . ? C42 C32 C22 C12 -0.1(2) . . . . ? C42 C32 C22 C72 -175.50(14) . . . . ? C62 C12 C22 C32 -2.5(2) . . . . ? N11 C12 C22 C32 -179.06(13) . . . . ? C62 C12 C22 C72 172.70(13) . . . . ? N11 C12 C22 C72 -3.8(2) . . . . ? C52 C62 C102 C112 96.76(16) . . . . ? C12 C62 C102 C112 -83.84(17) . . . . ? C52 C62 C102 C122 -29.2(2) . . . . ? C12 C62 C102 C122 150.23(14) . . . . ? C32 C22 C72 C82 -48.08(19) . . . . ? C12 C22 C72 C82 136.75(15) . . . . ? C32 C22 C72 C92 74.86(17) . . . . ? C12 C22 C72 C92 -100.31(16) . . . . ? C41 N21 C13 C23 94.88(17) . . . . ? Fe1 N21 C13 C23 -82.58(15) . . . . ? C41 N21 C13 C63 -89.27(17) . . . . ? Fe1 N21 C13 C63 93.27(14) . . . . ? C23 C13 C63 C53 -0.9(2) . . . . ? N21 C13 C63 C53 -176.75(13) . . . . ? C23 C13 C63 C103 178.44(13) . . . . ? N21 C13 C63 C103 2.6(2) . . . . ? C13 C63 C53 C43 1.8(2) . . . . ? C103 C63 C53 C43 -177.52(14) . . . . ? C63 C53 C43 C33 -0.9(2) . . . . ? C53 C43 C33 C23 -1.0(2) . . . . ? C43 C33 C23 C13 1.9(2) . . . . ? C43 C33 C23 C73 -177.35(14) . . . . ? C63 C13 C23 C33 -0.9(2) . . . . ? N21 C13 C23 C33 174.82(13) . . . . ? C63 C13 C23 C73 178.29(14) . . . . ? N21 C13 C23 C73 -6.0(2) . . . . ? C53 C63 C103 C113 -87.72(17) . . . . ? C13 C63 C103 C113 92.93(17) . . . . ? C53 C63 C103 C123 35.72(19) . . . . ? C13 C63 C103 C123 -143.63(15) . . . . ? C33 C23 C73 C93 -55.48(19) . . . . ? C13 C23 C73 C93 125.33(15) . . . . ? C33 C23 C73 C83 67.62(19) . . . . ? C13 C23 C73 C83 -111.56(16) . . . . ? N2 N1 C1 C6 8.6(2) . . . . ? Fe1 N1 C1 C6 -162.59(12) . . . . ? N2 N1 C1 C2 -172.26(12) . . . . ? Fe1 N1 C1 C2 16.56(18) . . . . ? C6 C1 C2 C3 3.2(2) . . . . ? N1 C1 C2 C3 -176.01(14) . . . . ? C1 C2 C3 C4 -2.0(2) . . . . ? C2 C3 C4 C5 -0.3(2) . . . . ? C3 C4 C5 C6 1.2(3) . . . . ? C4 C5 C6 C1 0.1(2) . . . . ? N1 C1 C6 C5 176.91(14) . . . . ? C2 C1 C6 C5 -2.2(2) . . . . ? N2 Si24 C24 C14 -32.27(13) . . . . ? C64 Si24 C24 C14 84.68(14) . . . . ? C54 Si24 C24 C14 -151.29(12) . . . . ? Si24 C24 C14 Si14 37.68(15) . . . . ? N2 Si14 C14 C24 -26.31(13) . . . . ? C44 Si14 C14 C24 -143.89(12) . . . . ? C34 Si14 C14 C24 93.91(14) . . . . ? _refine_diff_density_max 0.379 _refine_diff_density_min -0.318 _refine_diff_density_rms 0.040 _shelx_res_file ; 007a-22007.res created by SHELXL-2014/7 TITL 007a-22007 CELL 1.54184 11.9946 19.7217 17.1523 90 95.257 90 ZERR 4 0.0002 0.0003 0.0003 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Fe N Si UNIT 164 248 4 16 8 L.S. 30 TEMP -180 SIZE 0.20 0.20 0.02 CONF MORE -1 BOND $H ACTA WGHT 0.034200 2.226700 FVAR 0.41853 FE1 3 0.535219 0.308131 0.265020 11.00000 0.01355 0.01268 = 0.01935 -0.00066 0.00232 -0.00058 SI24 5 0.253174 0.187753 0.205006 11.00000 0.01837 0.01852 = 0.02700 -0.00227 0.00266 -0.00325 SI14 5 0.458619 0.157140 0.129815 11.00000 0.02223 0.02125 = 0.02541 -0.00165 0.00612 -0.00534 N1 4 0.463091 0.222091 0.275471 11.00000 0.02027 0.01979 = 0.02122 -0.00154 0.00132 -0.00336 N2 4 0.399073 0.186657 0.211881 11.00000 0.01978 0.02117 = 0.02460 -0.00419 0.00161 -0.00451 N11 4 0.483032 0.399833 0.294937 11.00000 0.01445 0.01667 = 0.01721 -0.00031 0.00079 0.00066 N21 4 0.696567 0.333924 0.269500 11.00000 0.01525 0.01659 = 0.01825 -0.00038 0.00259 0.00148 C11 1 0.507771 0.510503 0.360731 11.00000 0.02231 0.02133 = 0.02980 -0.00771 -0.00022 0.00130 AFIX 137 H11A 2 0.458929 0.531194 0.318338 11.00000 -1.50000 H11B 2 0.570220 0.541168 0.376140 11.00000 -1.50000 H11C 2 0.464927 0.502219 0.405772 11.00000 -1.50000 AFIX 0 C21 1 0.552824 0.444134 0.332907 11.00000 0.02088 0.01713 = 0.01667 -0.00201 0.00161 0.00025 C31 1 0.668625 0.433505 0.347220 11.00000 0.01905 0.01974 = 0.02084 -0.00529 -0.00153 -0.00127 AFIX 43 H31 2 0.706522 0.463528 0.383994 11.00000 -1.20000 AFIX 0 C41 1 0.736391 0.384867 0.314967 11.00000 0.01706 0.01879 = 0.01873 0.00140 0.00053 -0.00140 C51 1 0.861189 0.392866 0.334555 11.00000 0.01587 0.02615 = 0.02988 -0.00566 0.00033 -0.00215 AFIX 137 H51A 2 0.884269 0.368149 0.382922 11.00000 -1.50000 H51B 2 0.879359 0.441039 0.341747 11.00000 -1.50000 H51C 2 0.900822 0.374593 0.291693 11.00000 -1.50000 AFIX 0 C12 1 0.368250 0.419153 0.274292 11.00000 0.01592 0.01163 = 0.02036 -0.00229 -0.00006 0.00092 C62 1 0.337683 0.438246 0.196054 11.00000 0.01911 0.01215 = 0.02082 -0.00129 0.00069 -0.00152 C52 1 0.226861 0.457407 0.175374 11.00000 0.02200 0.01634 = 0.02129 0.00178 -0.00238 0.00069 AFIX 43 H52 2 0.205346 0.471979 0.123375 11.00000 -1.20000 AFIX 0 C42 1 0.148095 0.455569 0.229015 11.00000 0.01730 0.01800 = 0.02988 -0.00037 -0.00172 0.00286 AFIX 43 H42 2 0.073131 0.469002 0.214011 11.00000 -1.20000 AFIX 0 C32 1 0.178555 0.434083 0.304846 11.00000 0.01752 0.01991 = 0.02500 -0.00217 0.00443 0.00139 AFIX 43 H32 2 0.123349 0.431916 0.341103 11.00000 -1.20000 AFIX 0 C22 1 0.288545 0.415541 0.329191 11.00000 0.01853 0.01659 = 0.02004 -0.00340 0.00095 0.00041 C102 1 0.422604 0.437389 0.135600 11.00000 0.02170 0.01867 = 0.01983 0.00273 0.00226 0.00093 AFIX 13 H102 2 0.475556 0.399299 0.150008 11.00000 -1.20000 AFIX 0 C112 1 0.492202 0.502264 0.137739 11.00000 0.02688 0.02665 = 0.02563 0.00232 0.00470 -0.00531 AFIX 137 H11D 2 0.546663 0.499441 0.098618 11.00000 -1.50000 H11E 2 0.531842 0.507768 0.189901 11.00000 -1.50000 H11F 2 0.442788 0.541238 0.126070 11.00000 -1.50000 AFIX 0 C122 1 0.370220 0.423197 0.052509 11.00000 0.03196 0.02990 = 0.02004 -0.00032 0.00380 -0.00450 AFIX 137 H12A 2 0.323427 0.461735 0.034047 11.00000 -1.50000 H12B 2 0.324052 0.382204 0.052603 11.00000 -1.50000 H12C 2 0.429623 0.416559 0.017650 11.00000 -1.50000 AFIX 0 C72 1 0.315489 0.387400 0.411261 11.00000 0.01905 0.02892 = 0.01829 -0.00019 0.00253 0.00367 AFIX 13 H72 2 0.398740 0.386640 0.422716 11.00000 -1.20000 AFIX 0 C82 1 0.266349 0.430290 0.474343 11.00000 0.03300 0.04206 = 0.02206 -0.00483 0.00416 0.00548 AFIX 137 H82A 2 0.294418 0.476850 0.472081 11.00000 -1.50000 H82B 2 0.288726 0.410981 0.526062 11.00000 -1.50000 H82C 2 0.184491 0.430456 0.465207 11.00000 -1.50000 AFIX 0 C92 1 0.272624 0.314239 0.414146 11.00000 0.03056 0.03032 = 0.02344 0.00601 0.00312 0.00264 AFIX 137 H92A 2 0.191705 0.313471 0.399555 11.00000 -1.50000 H92B 2 0.288320 0.296292 0.467297 11.00000 -1.50000 H92C 2 0.310464 0.286218 0.377429 11.00000 -1.50000 AFIX 0 C13 1 0.771828 0.295269 0.225564 11.00000 0.01149 0.01872 = 0.02117 -0.00350 0.00243 -0.00165 C63 1 0.790097 0.317834 0.149832 11.00000 0.01520 0.02086 = 0.02060 -0.00114 0.00091 -0.00298 C53 1 0.857827 0.279011 0.105682 11.00000 0.01892 0.02879 = 0.02077 -0.00216 0.00453 -0.00385 AFIX 43 H53 2 0.872798 0.294180 0.055118 11.00000 -1.20000 AFIX 0 C43 1 0.903821 0.218512 0.134348 11.00000 0.01843 0.02817 = 0.02715 -0.00737 0.00558 0.00179 AFIX 43 H43 2 0.949043 0.192192 0.103185 11.00000 -1.20000 AFIX 0 C33 1 0.883930 0.196518 0.208132 11.00000 0.01797 0.02201 = 0.02863 -0.00146 0.00174 0.00278 AFIX 43 H33 2 0.914890 0.154618 0.226904 11.00000 -1.20000 AFIX 0 C23 1 0.819400 0.234446 0.255712 11.00000 0.01346 0.02071 = 0.02414 -0.00090 0.00210 -0.00038 C103 1 0.736905 0.382695 0.115330 11.00000 0.02082 0.02273 = 0.02341 0.00344 0.00409 0.00030 AFIX 13 H103 2 0.667634 0.391502 0.142031 11.00000 -1.20000 AFIX 0 C113 1 0.814755 0.443771 0.130678 11.00000 0.03585 0.02304 = 0.03515 0.00211 0.00182 -0.00241 AFIX 137 H11G 2 0.828829 0.451118 0.187231 11.00000 -1.50000 H11H 2 0.779420 0.484217 0.106136 11.00000 -1.50000 H11I 2 0.885814 0.435048 0.108486 11.00000 -1.50000 AFIX 0 C123 1 0.702469 0.377097 0.027242 11.00000 0.03527 0.02978 = 0.02780 0.00746 -0.00135 -0.00395 AFIX 137 H12D 2 0.769627 0.376223 -0.001263 11.00000 -1.50000 H12E 2 0.656148 0.416212 0.010085 11.00000 -1.50000 H12F 2 0.659623 0.335278 0.016607 11.00000 -1.50000 AFIX 0 C73 1 0.804441 0.209297 0.337742 11.00000 0.02152 0.02237 = 0.02543 0.00390 0.00647 0.00524 AFIX 13 H73 2 0.749741 0.239917 0.360855 11.00000 -1.20000 AFIX 0 C83 1 0.915199 0.212107 0.390489 11.00000 0.03442 0.03841 = 0.02633 0.00675 -0.00076 0.00111 AFIX 137 H83A 2 0.967440 0.178573 0.372520 11.00000 -1.50000 H83B 2 0.900907 0.202015 0.444625 11.00000 -1.50000 H83C 2 0.947814 0.257524 0.387927 11.00000 -1.50000 AFIX 0 C93 1 0.757386 0.137363 0.337252 11.00000 0.02691 0.02526 = 0.03957 0.00593 0.01101 0.00281 AFIX 137 H93A 2 0.688562 0.135230 0.301833 11.00000 -1.50000 H93B 2 0.740769 0.124963 0.390291 11.00000 -1.50000 H93C 2 0.812618 0.105717 0.319316 11.00000 -1.50000 AFIX 0 C1 1 0.485136 0.185520 0.344788 11.00000 0.01390 0.02376 = 0.02286 0.00235 0.00588 0.00232 C2 1 0.534757 0.221001 0.410762 11.00000 0.01997 0.02928 = 0.02558 0.00136 0.00562 0.00149 AFIX 43 H2 2 0.547048 0.268440 0.407173 11.00000 -1.20000 AFIX 0 C3 1 0.565601 0.187848 0.480238 11.00000 0.01930 0.05217 = 0.02363 0.00142 0.00388 0.00573 AFIX 43 H3 2 0.600946 0.212392 0.523313 11.00000 -1.20000 AFIX 0 C4 1 0.545503 0.119133 0.487742 11.00000 0.02266 0.05023 = 0.03109 0.01738 0.00714 0.00724 AFIX 43 H4 2 0.567039 0.096275 0.535512 11.00000 -1.20000 AFIX 0 C5 1 0.493415 0.084276 0.424345 11.00000 0.02180 0.03100 = 0.04132 0.01327 0.00840 0.00323 AFIX 43 H5 2 0.478003 0.037308 0.429360 11.00000 -1.20000 AFIX 0 C6 1 0.463305 0.116642 0.353635 11.00000 0.02001 0.02521 = 0.03338 0.00342 0.00560 0.00098 AFIX 43 H6 2 0.427603 0.091693 0.311016 11.00000 -1.20000 AFIX 0 C24 1 0.229261 0.132318 0.116216 11.00000 0.02389 0.02835 = 0.03576 -0.00832 0.00363 -0.00722 AFIX 23 H24A 2 0.228001 0.084049 0.131961 11.00000 -1.20000 H24B 2 0.156536 0.143440 0.086997 11.00000 -1.20000 AFIX 0 C14 1 0.326112 0.145043 0.064055 11.00000 0.03089 0.04074 = 0.02722 -0.00908 0.00446 -0.01099 AFIX 23 H14A 2 0.310326 0.185960 0.031465 11.00000 -1.20000 H14B 2 0.333916 0.105870 0.028874 11.00000 -1.20000 AFIX 0 C64 1 0.197957 0.275319 0.189117 11.00000 0.02554 0.02441 = 0.02990 0.00013 -0.00301 -0.00271 AFIX 137 H64A 2 0.222089 0.303443 0.234668 11.00000 -1.50000 H64B 2 0.115978 0.274011 0.182043 11.00000 -1.50000 H64C 2 0.226721 0.294624 0.142272 11.00000 -1.50000 AFIX 0 C54 1 0.193320 0.150178 0.291603 11.00000 0.02231 0.02865 = 0.03702 0.00518 0.00504 -0.00030 AFIX 137 H54A 2 0.214042 0.102175 0.296072 11.00000 -1.50000 H54B 2 0.111573 0.154326 0.285267 11.00000 -1.50000 H54C 2 0.222839 0.174253 0.339053 11.00000 -1.50000 AFIX 0 C44 1 0.553239 0.221132 0.091580 11.00000 0.03217 0.03575 = 0.02795 0.00025 0.00507 -0.01099 AFIX 137 H44A 2 0.516898 0.265676 0.090142 11.00000 -1.50000 H44B 2 0.569563 0.208355 0.038595 11.00000 -1.50000 H44C 2 0.623200 0.223140 0.125823 11.00000 -1.50000 AFIX 0 C34 1 0.538647 0.076859 0.146268 11.00000 0.04539 0.02860 = 0.03987 -0.00211 0.01864 0.00431 AFIX 137 H34A 2 0.603027 0.084603 0.184676 11.00000 -1.50000 H34B 2 0.565000 0.061579 0.096781 11.00000 -1.50000 H34C 2 0.490087 0.042089 0.166019 11.00000 -1.50000 AFIX 0 HKLF 4 REM 007a-22007 REM R1 = 0.0295 for 6762 Fo > 4sig(Fo) and 0.0313 for all 7123 data REM 447 parameters refined using 0 restraints END WGHT 0.0339 2.2020 REM Highest difference peak 0.379, deepest hole -0.318, 1-sigma level 0.040 Q1 1 0.4014 0.2033 0.1616 11.00000 0.05 0.38 Q2 1 0.4603 0.2543 0.1956 11.00000 0.05 0.35 Q3 1 0.2482 0.2012 0.1519 11.00000 0.05 0.32 Q4 1 0.4222 0.1478 0.0818 11.00000 0.05 0.31 Q5 1 0.2144 0.1452 0.2452 11.00000 0.05 0.31 Q6 1 0.5693 0.2681 0.4243 11.00000 0.05 0.27 Q7 1 0.7687 0.3478 0.1327 11.00000 0.05 0.25 Q8 1 0.7665 0.3013 0.1791 11.00000 0.05 0.24 Q9 1 0.7420 0.3102 0.2470 11.00000 0.05 0.22 Q10 1 0.3247 0.4085 0.3007 11.00000 0.05 0.22 Q11 1 0.3990 0.4320 0.0987 11.00000 0.05 0.21 Q12 1 0.3028 0.4025 0.3689 11.00000 0.05 0.21 Q13 1 0.3006 0.3532 0.4138 11.00000 0.05 0.21 Q14 1 0.7092 0.4782 0.3565 11.00000 0.05 0.20 Q15 1 0.2803 0.4368 0.1843 11.00000 0.05 0.20 Q16 1 0.3814 0.4393 0.1639 11.00000 0.05 0.19 Q17 1 0.5292 0.2393 0.3520 11.00000 0.05 0.19 Q18 1 0.2431 0.4213 0.3161 11.00000 0.05 0.19 Q19 1 0.8109 0.2934 0.1232 11.00000 0.05 0.19 Q20 1 0.8178 0.2242 0.2968 11.00000 0.05 0.19 ; _shelx_res_checksum 86321