data_BiCuSeCl2 _audit_creation_method 'SHELXL-2019/2' _shelx_SHELXL_version_number '2019/2' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'Bi Cl2 Cu Se' _chemical_formula_sum 'Bi Cl2 Cu Se' _chemical_formula_weight 422.38 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Cl' 'Cl' 0.1420 0.1501 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3307 1.2021 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Se' 'Se' -0.0190 2.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Bi' 'Bi' -3.3368 10.1080 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_H-M_alt 'P n m a' _space_group_name_Hall '-P 2ac 2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' _cell_length_a 8.78415(6) _cell_length_b 3.99803(3) _cell_length_c 13.13998(9) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 461.467(6) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 6525 _cell_measurement_theta_min 2.25 _cell_measurement_theta_max 35.51 _exptl_crystal_description 'platelet' _exptl_crystal_colour 'black' _exptl_crystal_density_diffrn 6.080 _exptl_crystal_F_000 720 _exptl_crystal_size_max 0.350 _exptl_crystal_size_mid 0.250 _exptl_crystal_size_min 0.050 _exptl_absorpt_coefficient_mu 47.290 _shelx_estimated_absorpt_T_min 0.021 _shelx_estimated_absorpt_T_max 0.201 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.34269824407931376 _exptl_absorpt_correction_T_max 1.0 _exptl_absorpt_process_details ; DIALS 3.8 Scaling & analysis of unmerged intensities, absorption correction using spherical harmonics ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.6889 _diffrn_source Synchrotron _diffrn_source_details 'Allan et al. (2017)' _diffrn_source_type 'Diamond Light Source Beamline I19-1' _diffrn_measurement_device 'Fixed \c 3-circle diffractometer' _diffrn_measurement_device_type 'Fluid Film Devices' _diffrn_measurement_method 'shutterless scans' _diffrn_measurement_specimen_support 'MiTeGen MicroMount' _diffrn_radiation_monochromator 'Silicon 111' _diffrn_reflns_number 9843 _diffrn_reflns_av_unetI/netI 0.0147 _diffrn_reflns_av_R_equivalents 0.0261 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_theta_min 2.704 _diffrn_reflns_theta_max 34.986 _diffrn_reflns_theta_full 24.415 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 1240 _reflns_number_gt 1215 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'GDA - generic data acquisition software' _computing_cell_refinement 'DIALS 3.8 (Winter, G. et al., 2018)' _computing_data_reduction ; DIALS 3.8 (Winter, G. et al., 2018) dials.scale (Beilsten-Edmands, J. et al., 2020) XIA2 3.8.6 (Winter, G., 2010) ; _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0048P)^2^+0.9603P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1240 _refine_ls_number_parameters 31 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0119 _refine_ls_R_factor_gt 0.0114 _refine_ls_wR_factor_ref 0.0256 _refine_ls_wR_factor_gt 0.0254 _refine_ls_goodness_of_fit_ref 1.168 _refine_ls_restrained_S_all 1.168 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.27145(2) 0.250000 0.94748(2) 0.00532(3) Uani 1 2 d S T P . . Se1 Se 0.23941(3) 0.750000 0.80575(2) 0.00496(4) Uani 1 2 d S T P . . Cu1 Cu 0.45965(4) 0.750000 0.69957(3) 0.01027(6) Uani 1 2 d S T P . . Cl1 Cl 0.43403(7) 1.250000 0.59546(4) 0.00634(9) Uani 1 2 d S T P . . Cl2 Cl 0.55935(7) 0.250000 0.89837(4) 0.00722(9) Uani 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.00565(4) 0.00600(4) 0.00430(4) 0.000 0.00018(2) 0.000 Se1 0.00491(9) 0.00628(10) 0.00369(9) 0.000 0.00039(7) 0.000 Cu1 0.00868(14) 0.01284(15) 0.00930(13) 0.000 0.00347(10) 0.000 Cl1 0.0059(2) 0.0076(2) 0.0055(2) 0.000 0.00011(17) 0.000 Cl2 0.0050(2) 0.0101(2) 0.0065(2) 0.000 0.00036(17) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Cl2 2.6100(6) . ? Bi1 Se1 2.74661(18) 1_545 ? Bi1 Se1 2.74661(18) . ? Bi1 Cl1 3.0172(6) 6_547 ? Se1 Cu1 2.3852(4) . ? Se1 Cu1 2.4585(4) 6_557 ? Cu1 Cl1 2.4327(4) . ? Cu1 Cl1 2.4327(4) 1_545 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl2 Bi1 Se1 86.079(11) . 1_545 ? Cl2 Bi1 Se1 86.079(11) . . ? Se1 Bi1 Se1 93.407(8) 1_545 . ? Cl2 Bi1 Cl1 154.905(18) . 6_547 ? Se1 Bi1 Cl1 76.851(9) 1_545 6_547 ? Se1 Bi1 Cl1 76.852(9) . 6_547 ? Cu1 Se1 Cu1 142.574(12) . 6_557 ? Cu1 Se1 Bi1 108.271(9) . . ? Cu1 Se1 Bi1 96.990(9) 6_557 . ? Cu1 Se1 Bi1 108.271(9) . 1_565 ? Cu1 Se1 Bi1 96.990(9) 6_557 1_565 ? Bi1 Se1 Bi1 93.406(8) . 1_565 ? Se1 Cu1 Cl1 104.709(17) . . ? Se1 Cu1 Cl1 104.709(17) . 1_545 ? Cl1 Cu1 Cl1 110.51(3) . 1_545 ? Se1 Cu1 Se1 145.832(16) . 6_657 ? Cl1 Cu1 Se1 94.385(17) . 6_657 ? Cl1 Cu1 Se1 94.386(17) 1_545 6_657 ? Cu1 Cl1 Cu1 110.51(3) 1_565 . ? Cu1 Cl1 Bi1 90.820(17) 1_565 6_667 ? Cu1 Cl1 Bi1 90.820(17) . 6_667 ? _refine_diff_density_max 0.911 _refine_diff_density_min -1.685 _refine_diff_density_rms 0.228 _shelx_res_file ; TITL BiCuSeCl2 in Pnma BiCuSeCl2.res created by SHELXL-2019/2 at 19:00:35 on 16-Jan-2024 CELL 0.68890 8.78415 3.99803 13.13998 90.000 90.000 90.000 ZERR 4.000 0.00006 0.00003 0.00009 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, -Z SYMM 1/2+X, 1/2-Y, 1/2-Z SFAC Cl Cu Se Bi DISP $Cl 0.1420 0.1501 610.90 DISP $Cu 0.3307 1.2021 4755.30 DISP $Se -0.0190 2.1234 8370.53 DISP $Bi -3.3368 10.1080 40209.46 UNIT 8 4 4 4 SIZE 0.05 0.25 0.35 TEMP 27 OMIT -2 70 LIST 4 L.S. 10 BOND ACTA FMAP 2 PLAN 10 WGHT 0.004800 0.960300 FVAR 0.19937 BI1 4 0.271452 0.250000 0.947484 10.50000 0.00565 0.00600 = 0.00430 0.00000 0.00018 0.00000 SE1 3 0.239412 0.750000 0.805748 10.50000 0.00491 0.00628 = 0.00369 0.00000 0.00039 0.00000 CU1 2 0.459646 0.750000 0.699573 10.50000 0.00868 0.01284 = 0.00930 0.00000 0.00347 0.00000 CL1 1 0.434031 1.250000 0.595460 10.50000 0.00595 0.00763 = 0.00545 0.00000 0.00011 0.00000 CL2 1 0.559348 0.250000 0.898367 10.50000 0.00500 0.01013 = 0.00652 0.00000 0.00036 0.00000 HKLF 4 REM BiCuSeCl2 in Pnma REM wR2 = 0.0256, GooF = S = 1.170, Restrained GooF = 1.170 for all data REM R1 = 0.0114 for 1215 Fo > 4sig(Fo) and 0.0119 for all 1240 data REM 31 parameters refined using 0 restraints END WGHT 0.0048 0.9602 REM Highest difference peak 0.911, deepest hole -1.685, 1-sigma level 0.228 Q1 1 0.2783 0.0709 0.9500 11.00000 0.05 0.91 Q2 1 0.4760 0.8778 0.7236 11.00000 0.05 0.84 Q3 1 0.4265 0.2500 0.7991 10.50000 0.05 0.76 Q4 1 0.2634 0.1832 1.0301 11.00000 0.05 0.71 Q5 1 0.2864 0.0085 1.0611 11.00000 0.05 0.68 Q6 1 0.2730 1.0038 0.8333 11.00000 0.05 0.64 Q7 1 0.2130 0.1260 0.8960 11.00000 0.05 0.63 Q8 1 0.2228 0.0036 1.0263 11.00000 0.05 0.63 Q9 1 0.2224 0.9964 0.8710 11.00000 0.05 0.61 Q10 1 0.4680 0.9939 0.6801 11.00000 0.05 0.61 ; _shelx_res_checksum 30982 _shelx_hkl_file ; -7 1 5 804.38 26.44 -5 2 3 441.97 14.70 -2 4 -7 37.22 2.04 -4 -3 2 29.53 2.23 -5 -2 4 388.79 14.22 0 -3 -3 3260.62 99.10 0 3 -6 0.07 0.48 3 -2 -10 112.05 5.09 2 2 -8 1527.06 49.03 -8 1 5 286.37 10.79 -6 -1 5 939.70 31.07 -6 -3 3 935.70 31.60 -4 -1 4 94.32 4.47 2 -1 -4 3.75 0.69 2 1 -5 2455.74 76.15 3 1 -9 857.59 28.91 -6 0 5 940.42 30.70 -5 1 4 326.39 11.47 3 0 -7 343.67 12.55 -3 -3 1 1167.84 36.88 -4 3 0 1003.15 31.10 3 -1 -7 180.79 7.26 -7 -1 5 831.14 28.10 3 1 -8 157.61 7.15 -7 0 5 101.71 5.09 -6 -2 4 5.03 1.29 1 -3 -5 92.10 3.56 2 -2 -5 152.59 5.78 4 0 -13 125.12 6.60 4 0 -14 10.89 1.93 -10 0 5 864.57 29.44 -6 2 3 339.67 11.74 -4 2 2 140.33 5.25 -9 -1 5 66.55 4.56 -8 -1 5 287.86 11.72 -4 -2 3 679.21 22.58 2 2 -7 100.22 5.06 -8 0 5 970.84 32.14 -3 -1 3 2215.55 68.56 4 -1 -12 443.17 16.14 4 0 -11 295.70 11.88 -6 1 4 37.41 2.43 1 3 -8 5.92 1.30 3 -2 -8 12.74 1.38 -7 -2 4 6.33 1.56 -3 0 3 28.29 1.79 -5 -3 2 352.75 13.10 -3 3 -1 1188.83 36.39 3 0 -6 3483.50 107.67 4 -1 -11 810.12 27.24 -5 -1 4 334.38 12.20 -7 2 3 498.61 16.74 1 2 -4 683.03 22.09 3 1 -7 181.48 7.79 4 0 -10 183.37 8.19 -5 0 4 529.09 17.87 -4 1 3 2281.52 70.42 -4 -4 -1 14.73 1.44 4 -1 -10 39.99 2.94 -7 1 4 381.94 13.51 4 1 -12 428.15 16.76 3 2 -10 119.11 6.51 -8 1 4 106.53 5.07 -3 -2 2 3037.55 93.53 0 3 -5 1478.87 46.17 2 1 -4 4.34 0.79 4 0 -9 346.80 13.23 4 1 -11 785.29 27.55 -5 -2 3 439.74 15.61 -6 -3 2 499.85 18.12 2 2 -6 21.78 2.01 2 -3 -7 628.32 20.33 -6 -1 4 42.21 2.96 -3 2 1 350.50 11.37 -3 -4 -2 1233.37 38.49 3 -2 -7 233.30 8.70 4 -1 -9 611.60 20.98 -2 0 2 1318.80 40.85 -1 -1 1 1624.64 49.81 1 3 -7 226.17 8.90 -10 0 4 1.37 1.16 -6 0 4 6.26 1.12 3 2 -9 145.34 7.22 4 1 -10 41.52 3.47 -9 -1 4 749.38 26.24 -4 -3 1 64.40 3.47 2 0 -3 88.64 3.80 -7 -1 4 393.09 14.57 -5 2 2 134.38 5.22 1 1 -2 307.83 10.15 -9 0 4 100.17 5.34 -8 -1 4 98.28 5.44 3 1 -6 113.69 5.46 -7 0 4 6.70 1.25 4 0 -8 2618.25 82.19 -8 0 4 175.35 7.63 3 0 -5 65.58 3.53 -4 -1 3 2220.63 69.01 -5 3 0 0.52 0.42 -5 1 3 648.74 21.16 -2 -2 1 83.64 3.45 4 -1 -8 797.40 26.55 2 -1 -3 915.27 28.85 3 -1 -5 2016.45 62.87 -8 -2 3 1119.74 37.71 -7 -2 3 503.95 18.37 -3 1 2 41.23 2.05 0 2 -2 266.78 8.63 3 2 -8 26.73 2.60 5 0 -13 5.05 1.56 -4 0 3 976.97 31.10 -1 0 1 1.27 0.25 2 -2 -4 293.74 9.97 -6 2 2 188.85 7.06 5 0 -12 460.82 17.44 -6 1 3 1482.89 46.66 -5 -3 1 278.52 10.68 3 -2 -6 2351.37 72.91 -7 2 2 921.06 29.53 -4 -2 2 133.52 5.66 -1 4 -7 15.02 1.28 4 0 -7 31.45 2.59 4 -2 -9 243.84 9.36 -8 1 3 55.51 3.28 2 2 -5 159.23 6.59 4 1 -8 775.22 26.68 -7 1 3 957.92 30.97 -3 -3 0 0.36 0.51 -1 -2 0 1.39 0.33 -10 0 3 587.95 20.88 -5 -1 3 653.87 21.79 5 -1 -11 1322.61 43.08 2 -3 -6 26.63 1.64 4 -1 -7 124.02 5.70 -2 2 0 1634.02 49.89 -9 -1 3 73.64 4.74 -5 0 3 570.27 18.98 -6 -3 1 1.41 1.11 3 1 -5 2064.19 64.80 3 2 -7 231.95 9.65 2 3 -8 41.16 3.13 5 0 -10 88.47 5.21 -9 0 3 359.92 13.59 -8 -1 3 53.21 3.73 -6 -1 3 1480.56 47.20 4 2 -10 146.81 7.81 5 -1 -10 28.41 2.54 -7 -1 3 947.04 31.38 -4 -4 -2 88.86 4.10 5 1 -11 1190.88 40.37 -5 -2 2 135.00 5.98 4 -2 -8 1845.08 58.01 -8 0 3 1382.71 44.49 -6 0 3 392.94 13.83 -3 -1 2 43.32 2.31 -4 2 1 63.75 2.78 2 1 -3 961.58 30.51 3 0 -4 630.26 20.88 4 1 -7 120.73 6.12 1 2 -3 246.08 8.49 5 0 -9 590.69 21.09 -8 -2 2 17.94 2.37 4 0 -6 24.59 2.21 -6 -2 2 186.07 7.96 -4 1 2 21.09 1.46 -7 -2 2 901.13 30.39 4 2 -9 252.43 11.11 5 1 -10 25.83 2.93 0 3 -4 0.10 0.39 5 -1 -9 1060.75 34.93 -3 0 2 4501.82 137.45 3 -1 -4 623.97 20.47 -2 1 1 17.95 1.01 1 0 -1 2.08 0.31 -10 0 2 27.80 2.68 -4 -3 0 1001.26 32.16 -2 -3 -1 11.18 0.93 6 0 -13 530.09 20.01 3 2 -6 2407.56 75.65 2 3 -7 616.07 21.19 -3 -2 1 337.41 11.52 -5 2 1 492.42 16.09 3 -2 -5 31.14 1.99 5 0 -8 720.25 24.95 5 1 -9 1065.79 36.18 -9 -1 2 369.12 14.38 -8 1 2 162.01 6.78 6 0 -12 259.82 11.40 -5 1 2 587.41 19.20 4 -2 -7 25.73 2.02 -4 -1 2 23.31 1.73 -7 2 1 572.50 18.91 4 2 -8 1826.92 59.12 -9 0 2 193.86 8.36 -7 1 2 595.09 19.90 -6 2 1 185.33 6.91 4 1 -6 3.36 1.09 5 -1 -8 42.27 3.10 -5 -3 0 1.40 0.84 2 2 -4 312.58 11.07 1 3 -5 94.54 4.17 -3 -4 -3 21.53 1.48 6 0 -11 69.09 4.75 3 1 -4 638.82 21.30 -6 -3 0 385.77 14.40 2 0 -2 1270.62 39.50 -8 0 2 24.84 2.28 -5 3 -1 296.84 9.90 1 -2 -2 1065.52 32.67 4 0 -5 539.66 18.64 5 1 -8 39.93 3.45 -7 -1 2 581.10 20.16 -5 -1 2 572.12 19.19 -8 -2 1 12.34 2.02 -6 -1 2 851.48 28.02 -4 -2 1 58.35 3.11 5 0 -7 143.95 6.89 -10 0 1 48.42 3.52 2 -3 -5 1222.91 38.00 3 3 -8 75.76 4.76 -5 0 2 141.36 5.75 -9 1 1 161.33 6.92 -7 -2 1 582.69 20.58 4 2 -7 32.14 2.98 6 -1 -10 845.27 28.72 -6 0 2 237.50 8.99 0 4 -7 0.30 0.56 5 -1 -7 271.86 10.64 2 3 -6 28.77 2.28 -6 -2 1 188.86 7.97 2 -2 -3 63.23 2.66 3 2 -5 34.99 2.59 -9 -1 1 158.45 7.62 -4 -4 -3 320.55 11.37 3 0 -3 30.91 2.02 4 -2 -6 16.14 1.56 6 1 -10 813.93 29.12 6 0 -9 1.58 1.15 5 1 -7 268.62 11.27 5 2 -9 451.18 17.88 -8 1 1 62.90 3.50 -3 -3 -1 1214.72 38.11 1 -1 -1 1664.84 50.77 4 1 -5 1609.17 51.37 5 -2 -8 509.45 17.64 -9 0 1 818.65 27.56 6 -1 -9 125.29 6.28 -3 1 1 2259.91 69.29 -3 2 0 0.38 0.31 -1 -3 -2 115.46 3.94 5 0 -6 1409.96 45.62 7 0 -12 13.19 2.35 6 1 -9 115.00 6.76 -7 1 1 291.02 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1.49 7 4 -9 332.17 12.65 7 4 -10 24.82 2.51 7 5 -9 125.21 6.18 3 1 -17 488.16 17.65 4 1 -14 4.31 1.52 7 4 -7 87.11 4.90 7 5 -8 48.84 3.50 6 6 -3 112.99 6.22 1 0 -16 327.49 12.03 6 3 -15 108.01 5.63 7 4 -11 381.29 14.17 7 5 -7 3.76 1.66 5 2 -2 136.59 6.00 6 2 -9 1.74 1.32 6 4 -1 82.30 5.00 7 4 -6 580.94 20.37 7 4 -12 3.13 1.47 6 5 -1 1.87 1.62 6 2 -8 847.89 28.01 6 2 -10 33.43 2.79 6 2 -11 59.11 3.74 7 4 -5 37.08 3.13 7 4 -13 18.01 2.30 7 5 -5 213.79 9.25 4 2 -19 51.66 3.91 6 3 -2 505.25 17.86 6 3 -16 78.34 4.64 2 0 -14 9.23 1.64 4 1 -3 2239.46 69.43 4 2 1 56.01 3.14 6 2 -6 92.67 4.68 2 0 -4 504.29 16.23 4 3 3 1159.63 37.32 5 3 1 274.16 10.69 7 3 -8 92.18 4.89 7 3 -9 212.48 8.79 3 1 -18 0.53 1.75 5 2 -17 154.17 7.32 7 3 -7 4.01 1.57 7 3 -11 299.15 11.55 7 4 -4 12.05 2.06 7 5 -4 169.96 7.93 6 2 -13 435.01 15.77 5 1 -9 1024.24 33.09 6 2 -5 761.18 25.28 6 3 -17 339.61 13.05 7 3 -12 92.05 5.02 4 4 4 80.85 4.59 6 5 0 214.13 9.73 5 1 -8 41.53 2.82 7 3 -6 679.28 23.12 6 4 0 1229.86 40.54 5 1 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45.64 3.18 3 0 -6 3414.94 104.74 7 2 -9 542.91 18.76 7 2 -11 649.37 22.11 5 1 -15 106.91 5.44 4 2 2 131.32 5.47 7 2 -8 11.46 1.87 7 5 -1 118.56 6.48 8 5 -5 114.14 5.97 4 1 -18 63.75 4.28 6 2 -17 84.58 4.93 7 2 -12 9.92 1.73 7 4 -1 360.53 13.93 8 4 -5 490.98 17.64 7 2 -7 133.86 6.10 8 3 -9 145.80 6.62 5 1 -4 336.15 11.93 8 3 -8 819.80 27.36 8 3 -11 151.32 6.84 3 0 -14 1610.69 50.87 2 1 2 278.68 9.11 7 2 -13 26.50 2.62 8 3 -12 365.03 13.51 8 5 -4 35.41 3.20 5 2 -20 4.88 1.91 7 2 -6 1113.49 36.03 4 3 4 50.05 2.97 7 3 -2 389.25 14.37 8 3 -7 149.93 6.75 8 4 -4 92.50 5.17 -1 -1 -9 2067.30 62.87 4 1 -1 150.07 5.93 5 1 -16 96.23 5.16 8 3 -13 238.02 9.61 7 2 -14 670.51 22.94 3 0 -5 65.12 3.07 6 2 -18 65.26 4.27 8 3 -6 44.22 3.24 6 1 -9 119.84 5.48 8 3 -14 4.63 1.67 -1 -1 -11 2183.02 66.56 6 1 -11 223.71 8.83 7 2 -5 88.19 4.60 6 4 2 108.04 5.86 7 5 0 0.46 1.78 8 5 -3 31.91 3.16 3 0 -15 47.47 3.16 6 1 -8 461.28 15.96 7 2 -15 0.82 1.60 6 3 1 0.97 1.33 7 4 0 1.35 1.73 8 4 -3 676.88 23.46 5 1 -3 666.96 21.97 6 1 -7 8.48 1.50 6 1 -13 132.81 6.11 9 4 -9 383.92 14.05 9 4 -10 16.80 2.14 5 2 1 467.15 16.05 7 3 -1 211.00 8.85 4 0 -10 197.96 7.60 6 2 -1 192.63 7.86 6 2 -19 5.60 1.87 7 2 -4 14.61 1.91 5 3 3 428.25 15.11 9 4 -8 1.34 1.29 4 0 -9 350.82 12.23 4 0 -11 301.40 10.85 8 3 -4 69.10 4.19 8 5 -2 99.69 5.70 6 1 -6 133.30 5.80 5 4 4 181.75 7.82 9 4 -7 205.03 8.58 3 0 -16 238.75 9.30 4 0 -12 941.34 30.39 8 4 -2 13.17 2.18 4 0 -8 2785.33 85.94 9 4 -6 69.78 4.23 3 0 -4 641.82 20.63 5 1 -18 54.18 3.80 7 2 -17 294.54 11.49 -1 -1 -12 16.02 0.96 4 0 -13 132.65 5.76 6 1 -15 139.54 6.42 8 2 -9 209.28 8.47 8 2 -10 248.74 9.70 8 2 -11 362.87 13.26 7 2 -3 487.61 16.99 8 2 -12 168.07 7.26 9 5 -5 25.06 2.69 5 1 -2 605.27 20.04 8 3 -3 44.98 3.25 9 3 -10 30.22 2.63 9 3 -11 63.00 3.80 8 2 -13 228.11 9.15 9 3 -9 25.62 2.40 9 3 -12 210.86 8.58 9 4 -5 8.43 1.69 8 5 -1 20.39 2.82 2 0 -2 1190.22 36.84 9 3 -8 137.15 6.27 4 0 -14 13.18 1.79 4 1 0 1781.98 55.36 3 2 4 442.58 14.32 8 2 -7 99.88 4.94 9 3 -13 1.04 1.27 6 1 -16 108.19 5.50 7 2 -18 65.80 4.15 6 3 2 459.49 16.30 6 4 3 209.21 8.95 8 4 -1 2.82 1.79 9 5 -4 318.07 12.42 3 0 -17 21.49 2.25 4 2 3 662.30 21.42 8 2 -14 6.51 1.62 9 3 -7 45.18 3.21 6 2 0 2244.53 70.13 -2 -1 -7 1239.79 37.86 4 0 -6 26.06 1.91 5 1 -19 305.38 11.90 8 2 -6 32.05 2.62 6 1 -4 40.74 2.71 0 2 6 232.83 7.25 8 2 -15 297.51 11.36 8 3 -2 131.98 6.30 9 3 -6 564.46 19.50 7 1 -11 467.48 16.26 7 1 -9 326.24 11.86 7 1 -12 115.68 5.45 9 5 -3 36.80 3.23 7 1 -8 133.41 5.85 8 5 0 794.68 27.55 7 1 -13 44.43 3.11 9 3 -5 48.13 3.35 9 4 -3 201.57 8.69 5 2 2 124.00 5.31 8 4 0 103.03 5.66 10 4 -8 113.81 5.50 3 0 -3 29.83 1.78 7 1 -7 2.34 1.20 7 1 -14 781.43 26.00 7 4 2 448.77 16.52 4 0 -5 594.90 19.44 -1 1 4 144.60 4.75 5 1 -1 448.71 15.21 7 3 1 206.87 8.64 4 0 -16 442.62 15.53 5 0 -10 64.48 3.43 5 0 -11 418.93 14.48 2 2 5 149.64 4.95 10 4 -7 186.46 7.87 6 1 -3 1516.22 47.81 6 1 -18 226.71 9.33 8 2 -4 152.18 6.65 8 2 -17 294.63 11.32 4 3 5 1002.85 31.70 8 3 -1 43.23 3.23 9 3 -4 535.66 18.69 9 5 -2 160.26 7.59 5 0 -9 568.92 18.93 5 3 4 216.21 8.25 7 1 -6 1116.82 35.83 7 1 -15 125.78 5.90 9 4 -2 100.59 5.48 10 4 -6 1.85 1.33 7 2 -1 567.34 19.40 9 2 -10 25.99 2.40 9 2 -11 472.09 16.50 5 0 -8 722.21 23.55 5 0 -13 5.54 1.48 9 2 -9 579.21 19.74 9 2 -12 0.90 1.33 6 2 1 167.66 6.90 10 3 -10 379.68 13.69 9 2 -13 35.59 2.76 10 3 -9 58.34 3.59 0 -1 -11 1158.28 35.71 7 1 -16 214.60 8.75 6 3 3 935.04 30.52 10 4 -5 477.80 17.02 0 -1 -10 1.30 0.51 4 0 -17 220.68 8.82 5 0 -14 1013.83 32.77 6 1 -19 12.45 2.20 8 2 -3 1137.45 36.77 9 2 -14 77.27 4.27 9 3 -3 61.95 3.91 10 3 -8 478.59 16.75 5 0 -7 134.90 5.59 9 2 -7 305.35 11.35 6 4 4 4.21 1.51 9 5 -1 59.34 4.27 8 4 1 3.08 1.62 10 3 -7 70.64 4.05 0 -1 -12 0.31 0.61 4 0 -4 270.86 9.54 6 1 -2 842.90 27.38 9 2 -15 22.01 2.35 9 4 -1 445.63 16.41 3 1 2 41.73 1.97 3 3 6 82.00 3.20 8 3 0 1547.98 49.66 10 4 -4 0.73 1.48 8 1 -11 194.15 7.84 9 2 -6 90.20 4.58 8 1 -10 158.10 6.67 8 1 -12 518.54 17.83 8 1 -9 210.21 8.29 7 3 2 374.63 13.72 7 4 3 254.29 10.30 0 -1 -9 807.38 24.92 5 0 -6 1582.17 49.56 7 1 -4 420.00 14.67 8 1 -13 338.86 12.38 7 2 0 0.19 1.08 9 3 -2 256.39 10.23 8 1 -8 1214.49 38.86 8 2 -2 17.64 2.05 5 1 0 0.52 0.65 9 2 -5 7.85 1.67 7 1 -18 28.72 2.82 8 1 -14 4.31 1.54 10 3 -5 47.94 3.26 10 4 -3 337.62 12.88 0 -1 -13 203.15 6.87 8 1 -7 218.09 8.53 6 0 -11 70.89 3.74 8 1 -15 73.80 4.16 -2 -1 -8 68.40 2.37 6 0 -10 39.10 2.67 6 0 -9 1.34 1.09 5 0 -5 177.20 6.88 6 0 -13 540.68 18.36 9 2 -4 72.69 4.09 10 2 -10 106.50 5.09 10 2 -11 120.07 5.56 10 3 -4 46.65 3.35 8 4 2 12.15 2.22 10 5 -2 172.21 7.92 7 1 -3 985.79 31.87 8 1 -6 58.76 3.46 4 2 4 176.23 6.33 6 2 2 184.03 7.29 10 2 -12 56.34 3.42 8 3 1 40.80 3.13 4 0 -3 992.56 31.40 5 0 -17 181.09 7.63 6 1 -1 2.16 0.98 8 1 -16 197.88 8.17 10 2 -9 62.75 3.68 10 2 -13 451.21 15.84 10 4 -2 7.93 1.91 6 0 -8 1114.05 35.56 6 0 -14 67.42 3.80 1 -1 -11 2119.74 65.09 8 2 -1 11.16 1.75 10 2 -8 190.04 7.77 10 2 -14 11.11 1.76 11 3 -9 38.50 2.81 1 -1 -10 1.31 0.64 11 3 -8 28.46 2.42 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66.59 7 -3 -8 89.93 4.80 8 -3 -6 44.72 3.27 9 -2 2 155.48 6.62 11 -3 -6 723.87 25.08 12 -3 -8 484.74 17.70 10 -2 2 19.60 2.09 12 -1 5 1.25 1.37 7 -3 -7 9.26 1.70 9 -3 -5 48.49 3.52 9 1 9 31.77 2.40 10 -3 -5 46.98 3.57 12 -3 -7 4.11 1.77 5 -2 0 0.49 0.78 5 -1 4 322.26 10.82 11 -2 2 0.39 1.16 13 -2 1 335.22 12.96 2 -2 -7 98.14 3.60 3 -1 2 41.74 1.91 6 -2 1 167.73 6.47 11 -3 -5 5.73 1.73 13 0 7 194.17 8.18 1 0 2 1671.68 50.82 8 -3 -5 193.34 8.20 11 1 9 64.52 3.78 12 -3 -6 40.80 3.39 3 -2 -3 26.40 1.55 6 0 7 554.86 17.97 7 -3 -6 709.54 23.85 8 1 9 204.88 7.70 9 -3 -4 507.60 18.08 10 -3 -4 38.88 3.21 12 -2 2 1.26 1.35 13 -1 5 135.88 6.38 4 -2 -1 57.97 2.70 10 0 8 263.94 9.84 -1 0 -3 435.25 13.41 6 -3 -9 77.16 4.19 9 0 8 5.21 1.24 10 -1 6 51.30 3.16 11 -3 -4 161.49 7.54 0 -1 -5 3175.33 96.21 6 -3 -8 324.86 11.90 6 -3 -10 525.37 18.10 6 -1 5 894.21 28.35 8 -3 -4 66.46 4.00 11 0 8 15.86 2.01 11 -1 6 1093.48 35.37 6 -3 -7 11.82 1.73 10 -3 -3 236.84 9.81 10 -2 3 482.93 16.84 12 -3 -4 51.43 3.80 13 -2 2 49.28 3.62 14 0 7 54.50 3.66 8 -1 6 55.79 3.06 8 0 8 455.30 15.33 9 -3 -3 54.32 3.66 9 -2 3 305.16 11.20 11 -3 -3 80.12 4.82 11 -2 3 544.88 18.94 5 1 8 41.64 2.04 7 1 9 336.18 11.49 12 -1 6 51.84 3.41 12 0 8 0.31 1.30 6 -3 -6 85.20 4.31 7 -3 -4 287.67 10.80 8 -3 -3 39.72 2.99 8 -2 3 1049.26 33.62 12 -3 -3 0.68 1.44 12 -2 3 552.58 19.36 3 0 5 59.84 2.36 4 0 6 27.08 1.51 5 -2 1 471.63 15.53 6 -2 2 188.21 7.06 10 -3 -2 304.04 11.85 7 -1 6 1044.42 33.09 9 -3 -2 252.17 10.04 11 -3 -2 482.80 17.53 13 -1 6 436.85 15.69 7 0 8 14.81 1.47 13 0 8 76.60 4.37 13 -2 3 173.14 7.71 4 -2 0 3567.58 109.07 7 -3 -3 592.23 20.04 7 -2 3 468.63 15.79 12 -3 -2 159.95 7.50 8 -3 -2 132.83 6.07 2 -2 -5 164.70 5.63 4 2 8 1946.88 59.33 5 0 7 133.32 4.99 10 -2 4 1.47 1.16 11 -2 4 111.99 5.40 4 -1 4 92.68 3.67 9 -2 4 79.21 4.09 10 -1 7 115.16 5.23 5 -3 -9 734.49 24.03 5 -1 5 47.11 2.39 6 -3 -4 29.60 2.28 11 -3 -1 36.48 3.02 11 -1 7 55.80 3.39 9 -1 7 56.87 3.21 12 -2 4 1.48 1.44 0 1 2 0.78 0.18 1 -1 -1 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22.08 13 -1 8 152.86 6.73 5 -2 3 423.27 14.05 5 -1 6 981.42 30.85 6 -2 4 5.80 1.11 8 -3 1 44.95 2.98 4 -1 5 1687.43 52.03 5 -3 -3 438.08 14.80 6 -3 -1 3.66 1.18 7 1 10 23.78 1.86 10 -3 2 307.43 11.60 11 -3 2 490.77 17.41 11 -2 6 162.95 6.94 11 0 10 2.41 1.31 8 -1 8 1164.01 36.93 10 0 10 141.34 6.08 12 -3 2 161.62 7.29 12 -2 6 1.45 1.38 2 -2 -3 62.68 2.53 12 0 10 1.98 1.43 3 -2 0 0.60 0.56 4 -3 -8 476.39 15.80 7 -2 5 81.24 3.84 9 -3 2 257.74 9.88 9 -2 6 88.84 4.30 4 -3 -7 85.46 3.83 4 0 7 29.88 1.62 6 -1 7 7.49 1.13 4 -3 -9 380.57 12.88 4 -2 2 127.17 4.87 13 -2 6 5.97 1.44 4 1 8 829.28 25.73 4 -3 -6 5.21 1.04 7 -3 1 207.76 8.03 5 -3 -2 341.44 11.82 3 -1 4 688.20 21.61 4 -3 -10 37.41 2.28 6 -3 0 373.35 12.93 8 -3 2 125.41 5.59 8 -2 6 34.46 2.41 11 -3 3 88.78 4.76 11 -1 9 66.33 3.73 10 -3 3 237.66 9.37 10 -1 9 98.31 4.69 11 -4 -7 56.88 3.97 12 -1 9 0.79 1.29 3 0 6 3532.73 107.57 4 -3 -5 996.81 31.55 7 -1 8 124.80 5.17 10 -4 -7 182.53 8.21 10 -4 -8 111.92 5.95 11 -4 -6 88.33 5.11 8 0 10 307.74 10.93 10 -4 -6 0.89 1.39 3 1 7 195.14 6.30 11 -4 -5 116.46 6.05 11 -2 7 78.78 4.20 6 0 9 0.86 0.87 9 -3 3 58.17 3.44 9 -1 9 30.38 2.27 10 -4 -5 449.99 16.52 10 -2 7 287.65 10.62 12 -2 7 163.37 7.00 13 -1 9 70.76 4.01 6 -2 5 747.02 24.05 9 -4 -7 204.92 8.84 9 -4 -8 1.59 1.64 1 -1 0 0.73 0.27 2 -2 -2 834.72 25.98 4 -3 -4 53.17 2.77 5 -2 4 385.94 12.94 11 -4 -4 62.29 4.15 5 -3 -1 279.12 9.90 10 -4 -4 1.24 1.46 7 -2 6 1066.91 33.91 9 -4 -5 7.12 1.76 9 -2 7 310.04 11.20 11 -3 4 177.11 7.53 3 -2 1 353.91 11.62 6 -3 1 2.24 0.97 8 -3 3 41.82 2.75 11 -4 -3 336.51 13.02 12 -3 4 47.12 3.33 8 -1 9 198.61 7.59 9 -4 -4 43.60 3.31 10 -4 -3 292.40 11.54 10 -3 4 44.39 3.01 1 2 4 797.95 24.48 8 -4 -7 73.51 4.39 8 -4 -8 234.02 9.61 11 0 11 625.71 21.12 0 -1 -10 0.58 0.34 4 -3 -3 1262.80 39.58 5 -1 7 279.48 9.62 6 1 10 865.65 27.34 10 0 11 142.27 6.15 11 -4 -2 0.37 1.41 7 0 10 48.77 2.78 8 -4 -5 489.77 17.37 9 -4 -3 179.01 7.82 6 -1 8 435.68 14.54 10 -4 -2 6.82 1.72 11 -2 8 14.87 1.86 11 -1 10 31.55 2.50 12 -1 10 257.00 9.84 8 -4 -4 90.98 4.85 12 -2 8 0.36 1.14 7 -3 3 545.62 18.27 10 -2 8 204.05 8.03 10 -1 10 547.11 18.53 11 -4 -1 298.58 11.72 6 -3 2 508.08 16.99 9 -4 -2 98.58 5.16 11 -3 5 3.36 1.28 12 -3 5 0.39 1.29 13 -1 10 16.02 1.97 4 -3 -2 25.17 1.78 10 -4 -1 21.98 2.41 10 -3 5 46.67 3.06 2 -2 -1 76.13 2.99 2 -1 3 970.05 29.98 6 -2 6 110.36 4.68 7 -1 9 321.67 11.26 8 -4 -3 591.33 20.36 5 -2 5 122.88 4.93 7 -4 -7 81.39 4.48 9 -2 8 4.12 1.17 7 -4 -8 2.85 1.47 9 -1 10 43.93 2.82 2 0 5 239.80 7.70 7 -4 -5 44.48 3.16 7 -2 7 132.97 5.48 9 -4 -1 434.16 15.62 11 -4 0 0.12 1.33 3 -2 2 2964.87 90.70 3 -1 5 2071.50 63.53 9 -3 5 47.68 3.01 5 -3 1 274.32 9.71 8 -4 -2 15.61 1.99 10 -4 0 363.89 13.55 7 -4 -4 11.79 1.77 7 1 11 491.34 16.24 1 0 3 428.49 13.21 4 -2 4 166.03 6.10 5 0 9 603.77 19.37 8 0 11 472.92 16.02 4 -3 -1 62.31 3.03 7 -3 4 280.13 10.16 12 -3 6 39.21 2.87 8 -2 8 400.52 13.84 9 -4 0 5.57 1.46 11 -4 1 309.45 11.90 11 -3 6 796.10 26.40 0 -1 -9 683.20 20.96 6 -3 3 909.87 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1131.86 35.42 4 -2 5 422.10 13.94 9 -4 2 94.57 4.78 11 -4 3 323.35 12.20 12 -2 10 2.33 1.28 8 -2 9 202.84 7.82 11 -2 10 1.96 1.32 1 -2 -6 2821.37 85.82 4 -3 1 64.67 3.12 5 -3 3 425.56 14.33 7 -4 0 2.03 1.11 10 -4 3 315.00 11.83 1 -2 -7 64.30 2.28 2 -1 4 3.14 0.54 5 1 10 28.13 1.62 9 -3 7 38.87 2.65 10 -2 10 101.39 4.81 1 -2 -5 239.67 7.70 6 -4 -2 113.56 5.15 0 -1 -4 0.69 0.12 0 -1 -8 0.52 0.24 2 1 6 54.70 1.84 2 -2 1 82.38 3.25 3 -3 -2 34.51 2.02 8 -1 11 217.74 8.29 12 -1 12 250.06 9.64 4 1 9 662.61 20.66 9 -4 3 191.48 7.84 11 -3 8 25.72 2.25 11 -1 12 53.21 3.31 7 -3 6 748.03 24.40 8 0 12 215.04 8.21 9 -2 10 27.63 2.28 6 -4 -1 81.27 4.10 6 -2 8 895.13 28.65 6 1 11 225.94 7.91 7 -4 1 342.13 12.31 1 -2 -4 744.34 23.03 5 -2 7 109.18 4.57 8 -3 7 151.64 6.30 10 -4 4 0.76 1.27 10 -3 8 451.41 15.68 7 -2 9 548.97 18.30 10 -1 12 275.26 10.31 3 -3 -1 1171.05 36.64 3 -2 4 441.15 14.38 4 -3 2 24.95 1.82 5 -4 -6 686.73 22.67 5 -3 4 222.29 8.14 5 -1 9 1079.96 34.01 5 -4 -5 54.57 3.18 5 0 10 67.33 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21.28 1 -1 3 2301.37 70.22 2 -3 -2 130.00 4.93 3 -2 6 2386.49 73.40 4 -3 5 1069.43 33.82 6 -3 8 318.91 11.31 6 0 12 274.79 9.71 7 -3 9 231.30 8.73 8 -5 0 763.72 25.63 11 -2 13 2.70 1.35 7 -5 -4 170.46 7.41 7 -5 -5 217.84 8.95 8 -1 13 338.30 12.15 4 -4 -1 15.05 1.61 8 -3 10 131.92 5.73 9 -5 2 160.09 7.03 10 -3 11 60.83 3.47 1 -2 0 0.64 0.50 3 -3 3 1161.34 36.45 4 -2 8 1867.37 57.91 4 0 10 175.66 6.26 5 -3 7 161.24 6.37 8 -2 12 172.37 7.02 2 -2 4 323.20 10.73 2 2 5 165.15 5.27 5 1 11 1258.42 38.98 7 -5 -2 192.07 8.02 7 -4 6 567.72 19.11 8 -4 7 71.21 3.80 2 -3 -1 12.70 1.17 2 -1 6 53.86 2.35 3 -1 8 171.71 6.18 7 0 13 26.51 2.17 8 -5 1 19.91 2.14 10 -2 13 461.77 16.08 5 -4 3 211.60 8.05 9 -4 8 2.78 1.27 0 -1 -6 0.07 0.13 4 -4 0 1714.31 53.61 6 -4 5 427.94 14.76 7 -5 -1 129.23 5.97 9 -5 3 33.85 2.75 9 -3 11 62.21 3.51 8 -5 2 95.99 4.88 4 -3 6 5.29 1.05 5 -1 11 1273.31 40.03 6 -1 12 101.86 4.58 7 -5 0 -0.09 1.16 9 -2 13 35.24 2.64 2 -3 0 53.95 2.60 9 -1 14 479.31 16.65 4 -4 1 16.85 1.69 6 -3 9 76.76 3.81 6 -2 11 63.98 3.41 7 -3 10 13.19 1.63 0 -1 -2 0.45 0.17 1 -2 1 1.72 0.50 3 -3 4 326.52 11.18 5 -4 4 184.29 7.19 5 -2 10 52.43 2.91 8 -4 8 235.76 9.03 3 -2 7 237.87 8.38 4 1 10 42.71 1.87 7 -5 1 112.70 5.37 7 -2 12 10.03 1.60 2 0 7 145.05 4.94 4 -1 10 41.66 2.32 5 -3 8 30.53 2.21 8 -5 3 24.25 2.31 8 -3 11 146.79 6.24 6 -5 -4 15.87 2.05 6 -4 6 54.97 3.14 9 -4 9 408.59 14.39 6 -5 -5 322.38 12.04 4 -4 2 87.95 4.12 6 -5 -2 231.65 9.13 2 -2 5 163.34 5.93 3 0 9 196.40 6.71 4 -2 9 264.28 9.38 7 -5 2 199.60 8.08 6 -5 -1 3.26 1.44 8 -2 13 231.81 8.92 1 -1 4 146.16 5.02 8 -5 4 31.88 2.53 9 -3 12 199.12 7.92 10 -2 14 13.60 1.86 5 -4 5 58.45 3.24 8 -1 14 3.48 1.44 4 -3 7 84.13 3.90 7 -4 8 4.24 1.34 3 -3 5 1120.26 35.30 6 -5 0 221.02 8.73 8 -4 9 115.50 5.27 3 -4 -3 22.13 1.83 3 -4 -4 288.14 10.21 7 -5 3 256.06 9.82 1 -2 2 1105.60 34.29 3 -4 -2 1332.20 41.92 4 -4 3 314.56 11.12 6 -4 7 239.96 9.01 7 -3 11 320.07 11.54 2 -3 2 131.12 5.08 2 -1 7 1282.49 39.70 3 -1 9 848.94 26.79 9 -4 10 14.34 1.84 5 -3 9 739.10 24.08 5 0 12 480.19 15.79 6 -5 1 1.89 1.26 6 0 13 532.78 17.63 3 -4 -1 157.76 6.22 8 -3 12 362.23 12.92 0 -1 -1 104.80 3.42 3 -4 -6 1242.60 39.15 3 -2 8 13.77 1.38 5 -4 6 684.25 22.50 5 -2 11 358.10 12.45 2 -3 -9 195.09 6.51 5 -1 12 89.02 4.08 6 -1 13 138.49 5.79 7 -5 4 157.82 6.70 7 -2 13 22.29 2.11 3 -4 0 0.11 0.90 4 -4 4 87.21 4.11 6 -5 2 225.34 8.81 2 -2 6 19.67 1.49 4 0 11 292.09 9.87 7 -4 9 346.31 12.38 2 -3 3 651.26 20.95 4 -3 8 470.18 15.79 8 -4 10 147.71 6.28 9 -3 13 1.59 1.28 4 -2 10 160.94 6.28 5 -5 -2 164.75 6.95 5 -5 -3 239.65 9.31 5 -5 -4 121.17 5.62 6 -4 8 477.49 16.32 7 -1 14 817.46 26.74 8 -5 6 26.58 2.36 1 -2 3 247.25 8.34 3 -4 1 161.58 6.37 3 -4 -7 101.96 4.39 4 -1 11 794.42 25.40 5 -5 -1 143.38 6.24 5 -5 -5 6.23 1.53 6 -5 3 470.01 16.30 8 -2 14 9.96 1.71 1 0 5 390.09 12.18 6 -3 11 153.44 6.35 10 -2 15 313.60 11.63 7 -3 12 100.16 4.75 5 -5 0 -0.05 1.14 5 -4 7 72.36 3.73 4 -4 5 220.03 8.26 5 -3 10 21.35 1.88 1 -1 5 157.82 5.44 3 -4 2 1345.87 42.39 6 -5 4 13.77 1.78 8 -1 15 78.68 4.23 2 -3 4 2.42 0.90 7 -4 10 25.14 2.21 0 -1 0 0.19 0.21 7 -5 6 383.34 13.64 9 -2 15 19.80 2.15 3 -3 7 148.32 5.86 3 -2 9 164.05 6.26 6 -4 9 0.99 1.05 6 -2 13 461.02 15.82 2 -2 7 102.68 4.19 2 -1 8 67.05 2.90 5 -5 2 160.31 6.71 2 0 8 2109.27 64.52 3 -1 10 16.69 1.44 3 1 9 860.31 26.46 4 -4 6 18.33 1.74 7 -2 14 670.21 22.34 9 -3 14 387.78 13.79 1 -3 -2 115.86 4.44 1 -3 -3 1146.25 35.66 3 0 10 153.12 5.46 5 -4 8 288.75 10.49 1 -3 -1 866.80 27.29 4 -2 11 226.71 8.37 1 -3 -4 47.88 2.23 5 -5 3 242.06 9.23 6 -3 12 87.68 4.29 7 -5 7 4.58 1.35 2 -3 5 1478.79 46.14 5 -1 13 14.22 1.63 6 -1 14 7.70 1.53 7 -3 13 32.02 2.48 1 -3 0 0.13 0.65 5 -3 11 898.84 29.06 8 -2 15 307.10 11.35 3 -4 4 276.78 9.94 7 -4 11 408.66 14.31 5 0 13 4.81 1.11 6 -5 6 41.52 2.84 6 -4 10 29.15 2.27 3 -3 8 88.94 4.04 4 -5 -2 21.42 2.12 4 -5 -3 597.89 20.16 7 -1 15 130.33 5.80 8 -4 12 106.07 4.95 8 -3 14 3.26 1.38 1 -3 -5 105.46 3.96 4 -5 -1 17.76 1.99 4 -4 7 26.24 2.06 4 -1 12 434.58 14.56 5 -5 4 129.04 5.66 0 -1 1 112.35 3.79 4 -5 0 396.07 13.95 4 -3 10 44.06 2.69 0 0 -4 58.14 2.01 2 -4 -2 378.24 12.91 5 -4 9 269.71 9.91 7 -5 8 57.19 3.35 1 -2 5 244.47 8.39 1 -1 6 412.29 13.25 2 -4 -1 29.89 2.11 2 -4 -3 44.92 2.57 3 -2 10 124.07 5.09 2 -2 8 1706.83 52.94 7 -6 -1 170.49 7.41 2 -4 0 897.06 28.70 2 -4 -4 162.95 6.26 4 -5 -5 520.27 17.80 6 -2 14 61.47 3.48 9 -2 16 34.44 2.65 2 1 7 1225.64 37.33 5 -5 5 6.86 1.45 5 -2 13 6.03 1.37 6 -5 7 7.61 1.49 1 -3 2 121.93 4.80 2 -4 1 29.77 2.10 4 -5 2 23.02 2.09 6 -3 13 105.65 4.93 4 1 11 783.91 24.37 6 -4 11 46.35 2.96 7 -4 12 4.25 1.35 2 -1 9 329.47 11.00 4 -2 12 729.97 23.76 5 -3 12 72.78 3.78 7 -3 14 603.38 20.32 2 -4 -5 77.88 3.58 2 -4 2 373.50 12.84 3 -4 6 1186.17 37.64 3 -3 9 560.83 18.56 4 -5 3 582.70 19.59 5 -4 10 30.03 2.29 5 -5 6 279.16 10.30 0 -2 -2 293.85 9.44 1 -3 3 1148.58 36.02 6 -5 8 188.11 7.51 8 -3 15 60.02 3.50 0 0 -3 0.66 0.17 1 0 6 3821.59 116.22 4 -3 11 518.84 17.45 8 -2 16 199.38 8.07 1 -2 6 3004.55 92.08 2 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13 254.79 9.56 2 -2 10 1430.22 44.80 3 -5 3 508.26 17.29 1 -3 -7 225.55 7.42 4 0 13 121.86 4.81 5 -6 0 0.33 1.19 5 -6 -1 139.21 6.26 5 -4 12 229.03 8.73 0 -2 3 0.25 0.51 3 -2 12 13.09 1.48 4 -5 7 60.17 3.31 5 -6 1 137.47 6.11 5 -5 9 397.39 13.90 2 -4 6 13.67 1.47 12 3 3 1.73 1.83 4 2 5 384.89 12.59 4 1 4 101.38 3.70 10 2 4 0.00 0.63 4 6 3 146.41 5.74 0 1 2 0.80 0.21 3 4 5 8.83 1.09 10 1 3 347.07 11.67 0 6 1 -0.07 0.97 -1 6 0 0.62 0.99 -3 2 0 0.77 0.28 -4 3 -1 60.30 2.30 -5 3 -3 412.01 12.82 2 5 4 1.29 1.07 3 6 3 14.57 1.55 9 4 5 7.05 1.32 1 6 2 244.64 8.79 2 3 5 1348.11 41.86 6 5 5 312.85 10.89 8 1 4 105.87 4.17 1 2 4 718.58 22.49 11 4 4 54.91 2.94 5 5 5 9.03 1.37 -1 3 3 1127.56 34.95 -1 5 2 42.42 2.38 -2 1 0 83.71 2.67 3 2 5 33.77 1.79 7 5 5 206.76 7.66 -2 3 2 132.21 4.71 2 4 5 81.49 3.56 4 5 5 521.92 17.21 3 -1 -1 2133.48 64.81 -4 4 -1 15.86 1.23 6 3 6 80.68 3.62 -1 4 3 83.05 3.47 5 3 6 590.38 19.09 8 5 5 111.70 4.72 2 6 3 21.88 1.82 7 3 6 709.39 22.84 5 4 6 733.08 23.56 6 4 6 56.98 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8.21 1.25 5 4 7 72.43 3.42 7 4 7 84.71 3.86 10 3 6 40.29 2.51 3 5 6 52.58 2.79 5 1 5 49.15 2.22 1 5 5 47.13 2.58 2 1 4 4.04 0.59 5 3 7 166.60 6.24 7 3 7 2.94 1.06 10 1 4 47.83 2.53 -1 4 4 373.00 12.33 0 6 3 0.27 1.03 -1 6 2 247.56 8.86 6 0 3 378.28 11.93 -2 2 2 824.88 25.45 3 6 5 2.22 1.04 1 0 1 1.69 0.14 -1 3 4 48.88 2.27 4 4 7 25.39 1.85 8 4 7 73.91 3.55 0 4 5 0.74 0.81 -2 4 3 37.48 2.02 -4 4 0 1635.65 50.41 -3 5 1 590.06 19.08 1 6 4 191.34 7.13 3 2 6 2487.65 76.26 9 2 6 100.10 4.30 4 3 7 88.92 3.80 8 3 7 147.16 5.82 12 3 5 0.81 1.15 -2 6 1 10.78 1.45 5 0 3 578.26 17.92 8 1 5 282.56 9.59 11 2 5 208.83 7.81 -2 3 3 652.23 20.51 1 2 5 243.26 8.13 6 5 7 8.31 1.31 2 5 6 13.76 1.47 9 4 7 199.02 7.45 11 4 6 86.96 4.00 5 5 7 79.78 3.68 7 5 7 4.50 1.15 -4 3 0 931.89 28.74 3 4 7 116.80 4.73 1 4 6 1458.36 45.38 2 6 5 39.93 2.37 9 3 7 40.75 2.53 11 3 6 746.98 24.28 -3 4 2 1367.47 42.37 4 5 7 62.73 3.12 -1 5 4 12.19 1.38 1 3 6 189.68 6.73 -2 5 3 336.77 11.40 6 2 7 453.19 14.89 10 4 7 175.74 6.77 0 6 4 12.58 1.48 -1 6 3 29.37 2.08 -3 3 2 33.58 1.65 6 4 8 497.75 16.49 3 5 7 94.15 4.09 3 6 6 542.96 17.88 7 2 7 136.77 5.32 2 4 7 45.71 2.47 1 5 6 66.15 3.18 10 3 7 74.29 3.65 5 4 8 281.84 9.87 1 6 5 20.19 1.73 3 1 5 2126.65 65.05 -2 6 2 165.96 6.38 8 4 8 242.94 8.79 4 0 3 948.38 29.07 8 2 7 97.81 4.21 7 3 8 95.06 4.16 2 3 7 706.73 22.50 -5 3 -2 320.12 10.03 4 4 8 1033.01 32.66 -1 4 5 78.33 3.37 4 -1 -1 136.32 4.31 4 2 7 31.42 1.85 -3 5 2 21.50 1.68 0 1 3 7836.22 237.68 -3 2 1 326.71 10.26 6 5 8 197.20 7.34 7 5 8 55.74 2.94 -4 2 -1 56.64 1.91 8 3 8 818.49 26.29 -2 4 4 163.25 5.94 5 5 8 19.80 1.67 2 5 7 342.78 11.70 2 6 6 9.73 1.35 9 4 8 4.29 1.20 2 0 2 1199.18 36.51 4 3 8 492.15 16.13 -4 4 1 17.58 1.31 4 5 8 235.01 8.46 9 2 7 318.03 11.04 11 2 6 156.31 6.22 -1 3 5 105.07 4.05 3 4 8 9.24 1.30 6 1 6 125.09 4.68 10 1 5 63.66 3.08 11 3 7 33.62 2.35 -1 5 5 47.94 2.59 7 1 6 1060.37 33.13 -1 1 2 297.54 9.31 0 2 5 0.03 0.58 9 3 8 126.45 5.26 0 5 6 0.96 1.03 3 2 7 244.33 8.37 0 6 5 0.60 1.03 -1 6 4 176.74 6.69 5 1 6 976.13 30.41 -2 3 4 2.98 0.73 10 4 8 107.66 4.68 -2 5 4 1.70 0.97 3 6 7 49.15 2.68 -3 4 3 19.99 1.46 3 5 8 41.69 2.40 9 0 3 323.84 10.49 1 5 7 130.15 5.18 1 6 6 695.51 22.52 8 1 6 52.48 2.60 1 2 6 2690.39 82.29 1 3 7 254.31 8.75 6 4 9 3.61 1.15 -2 6 3 20.81 1.81 5 4 9 264.42 9.37 2 4 8 992.30 31.35 10 2 7 277.71 9.91 2 1 5 2631.37 80.27 10 3 8 477.75 16.07 8 4 9 114.25 4.86 -2 2 3 64.26 2.47 6 5 9 34.81 2.26 2 6 7 17.23 1.66 6 2 8 844.72 26.83 7 2 8 8.96 1.25 -3 5 3 483.79 15.90 -4 3 1 63.13 2.47 5 5 9 397.52 13.46 2 5 8 27.72 1.97 7 3 9 234.56 8.50 -1 4 6 1510.35 46.91 5 3 9 752.47 24.14 9 4 9 377.65 12.96 0 4 7 0.27 0.88 8 2 8 409.48 13.79 8 3 9 145.21 5.81 2 3 8 48.93 2.52 -3 3 3 1183.19 36.56 4 5 9 177.51 6.71 -2 4 5 82.22 3.50 3 4 9 101.81 4.31 0 6 6 67.65 3.31 -1 6 5 20.29 1.78 4 2 8 2037.21 62.81 -1 5 6 66.48 3.20 11 3 8 25.01 2.10 0 5 7 13.74 1.43 10 4 9 36.28 2.36 1 6 7 5.52 1.29 9 2 8 4.84 1.32 11 2 7 69.47 3.60 9 3 9 25.95 2.07 -4 4 2 86.89 3.51 3 5 9 305.51 10.61 -2 5 5 678.32 21.85 -2 6 4 76.31 3.64 1 5 8 1.06 1.00 3 1 6 108.45 4.00 0 3 7 14.93 1.30 -1 3 6 196.74 6.91 7 0 4 6.38 0.75 6 4 10 27.09 2.02 7 4 10 26.71 2.02 -3 4 4 281.83 9.55 2 6 8 469.59 15.64 3 3 9 574.66 18.65 5 4 10 28.49 2.03 2 4 9 3.19 1.07 6 5 10 283.69 10.00 5 -1 -1 417.92 12.86 3 2 8 15.60 1.35 8 4 10 157.24 6.19 10 1 6 49.88 2.69 10 3 9 59.15 3.23 1 3 8 8.14 1.12 -2 3 5 1397.94 43.22 5 0 4 527.46 16.46 6 1 7 14.01 1.25 0 2 6 245.60 8.25 2 5 9 119.80 4.90 -1 0 -2 1518.78 46.16 7 1 7 5.83 1.05 10 2 8 204.81 7.73 8 0 4 175.97 6.01 1 2 7 68.55 2.93 6 3 10 537.66 17.73 7 3 10 15.37 1.61 4 5 10 35.07 2.24 0 6 7 0.06 0.94 5 1 7 272.21 9.17 0 4 8 1656.35 51.47 -1 4 7 19.28 1.55 -1 6 6 660.44 21.49 8 1 7 215.48 7.69 6 2 9 1.64 0.95 7 2 9 552.43 18.12 -3 2 2 2916.83 88.73 5 3 10 22.82 1.84 -5 3 -1 266.14 8.43 8 3 10 134.58 5.55 -1 5 7 139.40 5.48 1 6 8 113.52 4.75 0 1 4 0.13 0.34 5 2 9 465.52 15.33 2 3 9 237.38 8.38 3 4 10 75.89 3.54 -2 4 6 12.79 1.34 0 5 8 0.53 0.95 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3360.18 101.97 3 4 11 80.56 3.73 3 5 11 354.90 12.17 6 2 10 34.35 2.21 -2 4 7 50.38 2.63 -2 5 7 340.34 11.65 6 1 8 420.83 13.85 7 1 8 130.69 5.10 1 2 8 386.37 12.71 2 3 10 112.82 4.62 1 4 10 53.09 2.81 1 5 10 -0.02 0.96 -1 2 6 2929.84 89.51 11 3 10 21.94 2.04 5 2 10 54.12 2.85 4 3 11 514.49 17.00 5 1 8 39.58 2.13 8 2 10 238.47 8.73 9 3 11 65.60 3.49 6 4 12 145.48 5.84 7 4 12 2.89 1.17 8 1 8 1199.02 37.65 5 4 12 234.83 8.57 8 4 12 109.55 4.77 -4 5 4 22.83 1.85 6 0 5 920.18 28.52 2 2 9 8.76 1.15 2 4 11 5.88 1.24 -4 4 4 93.40 3.83 2 5 11 181.44 6.84 0 6 9 0.81 0.99 7 0 5 100.59 3.76 4 2 10 159.70 6.06 -3 3 5 1129.94 35.12 -3 5 6 57.10 2.97 -1 6 8 112.95 4.80 9 2 10 25.97 2.13 -3 4 6 1225.54 38.33 4 5 12 149.94 5.90 2 0 3 87.26 2.94 1 1 6 417.08 13.33 3 3 11 679.21 21.98 0 3 9 415.67 13.79 -4 3 3 1235.12 38.14 4 4 12 411.90 13.96 4 1 8 788.40 24.87 -3 2 3 28.67 1.38 10 3 11 57.52 3.27 -1 3 8 9.39 1.18 -5 3 0 1.33 0.51 -2 6 7 20.76 1.93 9 1 8 178.11 6.77 -2 2 5 166.09 5.74 1 3 10 1.93 1.00 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