#============================================================================== data_global #============================================================================== _publ_contact_author 'Harry L. Anderson' _publ_contact_author_email harry.anderson@chem.ox.ac.uk loop_ _publ_author_name _publ_author_address 'Chen, Qiang' ; Chemistry Research Laboratory, University of Oxford, Mansfield Road, Oxford OX1 3TA. UK. ; 'Lodi, Alessandro' ; Department of Materials University of Oxford Parks Road Oxford OX1 3PH (UK) ; 'Zhang, Heng' ; Max Planck Institute for Polymer Research, Ackermannweg 10, Mainz D-55128, Germany. ; 'Gee, Alex' ; Department of Materials University of Oxford Parks Road Oxford OX1 3PH (UK) ; 'Wang, Hai' ; Max Planck Institute for Polymer Research, Ackermannweg 10, 55128 Mainz, Germany ; 'Kong, Fanmiao' ; Department of Materials University of Oxford Parks Road Oxford OX1 3PH (UK) ; 'Clarke, Michael' ; School of Physics & Astronomy, University of Nottingham, Nottingham, NG7 2RD (UK). ; 'Edmondson, Matt' ; School of Physics & Astronomy, University of Nottingham, Nottingham, NG7 2RD (UK). ; 'Hart, Jack' ; School of Physics & Astronomy, University of Nottingham, Nottingham, NG7 2RD (UK). ; 'O'Shea, James' ; School of Physics & Astronomy, University of Nottingham, Nottingham, NG7 2RD (UK). ; 'Stawski, Wojciech' ; Chemistry Research Laboratory, University of Oxford, Mansfield Road, Oxford OX1 3TA. UK. ; 'Baugh, Jonathan' ; Institute of Quantum Computing, University of Waterloo, 200 University Ave., N2L 3G1 Waterloo, ON. Canada. ; 'Narita, Akimitsu' ; Max Planck Institute for Polymer Research, Ackermannweg 10, 55128 Mainz, Germany ; 'Saywell, Alex' ; School of Physics & Astronomy, University of Nottingham, Nottingham, NG7 2RD (UK). ; 'Bonn, Mischa' ; Max Planck Institute for Polymer Research, Ackermannweg 10, 55128 Mainz, Germany ; 'M\"ullen, Klaus' ; Max Planck Institute for Polymer Research, Ackermannweg 10, 55128 Mainz, Germany ; 'Bogani, Lapo' ; Department of Materials University of Oxford Parks Road Oxford OX1 3PH (UK) ; 'Anderson, Harry L.' ; Chemistry Research Laboratory, University of Oxford, Mansfield Road, Oxford OX1 3TA. UK. ; _publ_requested_journal 'Nature Chemistry' _journal_volume '?' _journal_page_first '?' _journal_page_last '?' _journal_year '2023' _ccdc_journal_depnumber '?' _publ_section_title ; Porphyrin-Fused Graphene Nanoribbons Synthesised in Solution ; #============================================================================== data_12 #============================================================================== _audit_creation_date 2022-12-04 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _shelx_SHELXL_version_number '2018/3' loop_ _audit_author_name _audit_author_email _audit_author_address 'Stawski, W.' wojciech.stawski@chem.ox.ac.uk ; University of Oxford Department of Chemistry 12 Mansfield Rd Oxford OX1 3TA ; _oxford_structure_analysis_title '039wps22' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. Spek, A. L. (2015). Acta Cryst. C71, 9-18. Spek, A. L. (2002). PLATON. A Multipurpose Crystallographic Tool. Utrecht University, The Netherlands. ; _chemical_name_common ? _chemical_name_systematic . _chemical_formula_moiety 'C48 H48 B Cl O2' _chemical_formula_sum 'C48 H48 B Cl O2' _chemical_formula_weight 703.12 _chemical_melting_point ? _chemical_oxdiff_formula 'C48 H48 B1 Cl1 O2' _chemical_oxdiff_usercomment 'Qiang, better crystal, thicker' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'B' 'B' 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 13 _space_group_name_H-M_alt 'P 1 2/c 1' _space_group_name_Hall '-P 2yc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' _cell_length_a 27.0823(9) _cell_length_b 6.1137(2) _cell_length_c 24.9379(7) _cell_angle_alpha 90 _cell_angle_beta 105.412(3) _cell_angle_gamma 90 _cell_volume 3980.6(2) _cell_formula_units_Z 4 _cell_measurement_reflns_used 8022 _cell_measurement_temperature 150.01(10) _cell_measurement_theta_max 76.2340 _cell_measurement_theta_min 4.2540 _shelx_estimated_absorpt_T_max 0.989 _shelx_estimated_absorpt_T_min 0.625 _exptl_absorpt_coefficient_mu 1.129 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71870 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.57a (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.173 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description needle _exptl_crystal_F_000 1496 _exptl_crystal_preparation 'As described in the manuscript.' _exptl_crystal_recrystallization_method 'Slow evaporation of a solution in a mixture of dichloromethane and methanol.' _exptl_crystal_size_max 0.46 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.01 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0520 _diffrn_reflns_av_unetI/netI 0.0425 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 33 _diffrn_reflns_limit_h_min -31 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -7 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 32789 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 70.075 _diffrn_reflns_theta_min 3.616 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.5035 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -18.00 28.00 1.00 7.50 -- -41.27 37.00 -60.00 46 2 \w -5.00 20.00 1.00 7.50 -- -41.27 19.00-120.00 25 3 \w 3.00 32.00 1.00 7.50 -- -41.27 19.00-150.00 29 4 \w -21.00 18.00 1.00 7.50 -- -41.27 37.00 0.00 39 5 \w -4.00 33.00 1.00 7.50 -- -41.27 19.00 90.00 37 6 \w -12.00 14.00 1.00 7.50 -- -41.27 37.00 -30.00 26 7 \w -19.00 25.00 1.00 7.50 -- -41.27 37.00-120.00 44 8 \w 48.00 89.00 1.00 7.50 -- 41.27-125.00 -60.00 41 9 \w 37.00 107.00 1.00 30.00 -- 111.00-111.00 0.00 70 10 \w 107.00 170.00 1.00 30.00 -- 111.00 77.00 -30.00 63 11 \w 41.00 72.00 1.00 30.00 -- 111.00 -45.00-120.00 31 12 \w 63.00 107.00 1.00 30.00 -- 111.00 -94.00 60.00 44 13 \w 40.00 66.00 1.00 30.00 -- 111.00 -45.00 -90.00 26 14 \w 41.00 70.00 1.00 30.00 -- 111.00 -45.00 30.00 29 15 \w 47.00 98.00 1.00 30.00 -- 111.00-111.00 -60.00 51 16 \w 150.00 177.00 1.00 30.00 -- 111.00 61.00 0.00 27 17 \w 86.00 131.00 1.00 30.00 -- 111.00 61.00 0.00 45 18 \w 72.00 105.00 1.00 30.00 -- 111.00-111.00-180.00 33 19 \w 37.00 62.00 1.00 30.00 -- 111.00-111.00-180.00 25 20 \w 38.00 87.00 1.00 30.00 -- 111.00 -77.00-150.00 49 21 \w 65.00 94.00 1.00 30.00 -- 111.00-111.00 -30.00 29 22 \w 44.00 71.00 1.00 30.00 -- 111.00 -61.00-150.00 27 23 \w 50.00 84.00 1.00 30.00 -- 111.00-111.00 150.00 34 24 \w 24.00 175.00 1.00 30.00 -- 111.00 0.00 -30.00 151 25 \w -4.00 25.00 1.00 7.50 -- -41.27 19.00 60.00 29 26 \w -8.00 25.00 1.00 7.50 -- -41.27 37.00 120.00 33 27 \w -48.00 -13.00 1.00 7.50 -- -41.27 -19.00 90.00 35 28 \w -81.00 -53.00 1.00 7.50 -- -41.27 -19.00 90.00 28 29 \w 43.00 88.00 1.00 7.50 -- 41.27-125.00-120.00 45 30 \w 28.00 82.00 1.00 7.50 -- 41.27-125.00 90.00 54 31 \w 36.00 103.00 1.00 30.00 -- 111.00-111.00-150.00 67 32 \w 40.00 66.00 1.00 30.00 -- 111.00 -45.00-150.00 26 33 \w 45.00 72.00 1.00 30.00 -- 111.00 -45.00 0.00 27 34 \w 79.00 109.00 1.00 30.00 -- 111.00-111.00 30.00 30 35 \w 42.00 69.00 1.00 30.00 -- 111.00-111.00 -90.00 27 36 \w 84.00 109.00 1.00 30.00 -- 111.00-111.00 -90.00 25 37 \w 88.00 130.00 1.00 30.00 -- 111.00 45.00 60.00 42 38 \w 140.00 168.00 1.00 30.00 -- 111.00 45.00 60.00 28 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0573049000 _diffrn_orient_matrix_UB_12 -0.0088248000 _diffrn_orient_matrix_UB_13 -0.0019621000 _diffrn_orient_matrix_UB_21 0.0036979000 _diffrn_orient_matrix_UB_22 0.2310592000 _diffrn_orient_matrix_UB_23 0.0253957000 _diffrn_orient_matrix_UB_31 -0.0135639000 _diffrn_orient_matrix_UB_32 0.1001254000 _diffrn_orient_matrix_UB_33 -0.0588012000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 5578 _reflns_number_total 7584 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.42.57a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.57a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.57a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _refine_diff_density_max 0.247 _refine_diff_density_min -0.216 _refine_diff_density_rms 0.041 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 586 _refine_ls_number_reflns 7584 _refine_ls_number_restraints 651 _refine_ls_R_factor_all 0.0674 _refine_ls_R_factor_gt 0.0453 _refine_ls_restrained_S_all 1.050 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0656P)^2^+0.3502P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1132 _refine_ls_wR_factor_ref 0.1281 _refine_special_details ; Two tBu groups are disordered and were modelled using similar distance (SADI) and ADP (SIMU, RIGU) restraints. One of the phenyl rings is disordered too and was modelled similarly, additionally using FLAT command on both components of disorder. Small residual electron density in voids (6 electrons per cell in total) was accounted for, using solvent mask (SQUEEZE, Platon). G Alert points out short contacts between hydrogen atoms from disordered components, these were chcecked carefully. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C6A-C7A \\sim C7A-C8A \\sim C8A-C6A \\sim C6B-C7B \\sim C7B-C8B \\sim C8B-C6B with sigma of 0.02 C7B-C5 \\sim C7A-C5 \\sim C6B-C5 \\sim C6A-C5 \\sim C8B-C5 \\sim C8A-C5 with sigma of 0.01 C35-C6A \\sim C35-C6B \\sim C35-C7A \\sim C35-C7B \\sim C35-C8A \\sim C35-C8B with sigma of 0.02 C14-C1B \\sim C14-C1A with sigma of 0.02 C14-C10A \\sim C14-C10B \\sim C9A-C11A \\sim C9B-C11B \\sim C10A-C12A \\sim C10B-C12B \\sim C11A-C11B \\sim C12A-C14 \\sim C12B-C14 \\sim C13-C9A \\sim C13-C9B with sigma of 0.02 C10A-C1A \\sim C10B-C1B with sigma of 0.02 C2A-C3A \\sim C3A-C4A \\sim C4A-C2A \\sim C2B-C3B \\sim C3B-C4B \\sim C4B-C2B with sigma of 0.02 C14-C13 \\sim C13-C12A \\sim C13-C12B \\sim C12A-C11A \\sim C12B-C11B \\sim C11A-C10A \\sim C11B-C10B \\sim C9A-C10A \\sim C9B-C10B \\sim C9A-C14 \\sim C9B-C14 with sigma of 0.01 C2B-C1B \\sim C3A-C1A \\sim C3B-C1B \\sim C4A-C1A \\sim C4B-C1B \\sim C2A-C1A with sigma of 0.01 C9A-C2A \\sim C9A-C3A \\sim C9A-C4A \\sim C9B-C2B \\sim C9B-C3B \\sim C9B-C4B with sigma of 0.02 3. Restrained planarity C9B, C10B, C11B, C12B, C13, C14 with sigma of 0.1 C9A, C10A, C11A, C12A, C13, C14 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints C1B \\sim C1A \\sim C3A \\sim C2B \\sim C2A \\sim C4B \\sim C4A \\sim C3B: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A C12A \\sim C12B \\sim C11A \\sim C11B \\sim C10A \\sim C10B \\sim C9A \\sim C9B \\sim C13 \\sim C14: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A C8A \\sim C7B \\sim C7A \\sim C6B \\sim C6A \\sim C8B \\sim C5: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A C1B \\sim C1A \\sim C4A \\sim C4B \\sim C2A \\sim C2B \\sim C3A \\sim C3B: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A 5. Rigid body (RIGU) restrains C12A, C11A, C9A, C10A, C13, C14 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C12B, C11B, C10B, C9B, C13, C14 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C8B, C8A, C7B, C7A, C6B, C6A, C5 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C1B, C4B, C3B, C2B with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C1A, C2A, C4A, C3A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Sof(C1A)=Sof(C2A)=Sof(H2AA)=Sof(H2AB)=Sof(H2AC)=Sof(C3A)=Sof(H3AA)=Sof(H3AB)= Sof(H3AC)=Sof(C4A)=Sof(H4AA)=Sof(H4AB)=Sof(H4AC)=Sof(C9B)=Sof(C10B)=Sof(H10B)= Sof(C11B)=Sof(H11B)=Sof(C12B)=Sof(H12B)=Sof(H14A)=1-FVAR(1) Sof(C1B)=Sof(C2B)=Sof(H2BA)=Sof(H2BB)=Sof(H2BC)=Sof(C4B)=Sof(H4BA)=Sof(H4BB)= Sof(H4BC)=Sof(C3B)=Sof(H3BA)=Sof(H3BB)=Sof(H3BC)=Sof(C9A)=Sof(C10A)=Sof(H10A)= Sof(C11A)=Sof(H11A)=Sof(C12A)=Sof(H12A)=Sof(H14)=FVAR(1) Sof(C6B)=Sof(H6BA)=Sof(H6BB)=Sof(H6BC)=Sof(C7B)=Sof(H7BA)=Sof(H7BB)=Sof(H7BC)= Sof(C8B)=Sof(H8BA)=Sof(H8BB)=Sof(H8BC)=1-FVAR(2) Sof(C6A)=Sof(H6AA)=Sof(H6AB)=Sof(H6AC)=Sof(C7A)=Sof(H7AA)=Sof(H7AB)=Sof(H7AC)= Sof(C8A)=Sof(H8AA)=Sof(H8AB)=Sof(H8AC)=FVAR(2) 7.a Aromatic/amide H refined with riding coordinates: C10A(H10A), C11A(H11A), C12A(H12A), C10B(H10B), C11B(H11B), C12B(H12B), C14(H14), C14(H14A), C16(H16), C19(H19), C20(H20), C23(H23), C24(H24), C31(H31), C32(H32), C33(H33), C34(H34), C36(H36), C38(H38), C39(H39), C41(H41), C42(H42) 7.b Idealised Me refined as rotating group: C2A(H2AA,H2AB,H2AC), C3A(H3AA,H3AB,H3AC), C4A(H4AA,H4AB,H4AC), C2B(H2BA,H2BB, H2BC), C4B(H4BA,H4BB,H4BC), C3B(H3BA,H3BB,H3BC), C6A(H6AA,H6AB,H6AC), C7A(H7AA, H7AB,H7AC), C8A(H8AA,H8AB,H8AC), C44(H44A,H44B,H44C), C45(H45A,H45B,H45C), C47(H47A,H47B,H47C), C48(H48A,H48B,H48C), C6B(H6BA,H6BB,H6BC), C7B(H7BA,H7BB, H7BC), C8B(H8BA,H8BB,H8BC) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group B1 B 0.54476(8) 0.0734(3) 0.13945(8) 0.0285(4) Uani 1 1 d . . . . . C1A C 0.9358(3) 0.8857(15) 0.0660(4) 0.064(2) Uani 0.346(4) 1 d D U P A 1 C2A C 0.8961(3) 1.0278(16) 0.0261(4) 0.075(2) Uani 0.346(4) 1 d D U P A 1 H2AA H 0.886444 1.150090 0.046625 0.113 Uiso 0.346(4) 1 calc R U P A 1 H2AB H 0.865719 0.939728 0.009215 0.113 Uiso 0.346(4) 1 calc R U P A 1 H2AC H 0.910665 1.084729 -0.003115 0.113 Uiso 0.346(4) 1 calc R U P A 1 C3A C 0.9830(3) 1.0230(18) 0.0931(4) 0.087(3) Uani 0.346(4) 1 d D U P A 1 H3AA H 0.998654 1.076138 0.064352 0.131 Uiso 0.346(4) 1 calc R U P A 1 H3AB H 1.007716 0.933224 0.119888 0.131 Uiso 0.346(4) 1 calc R U P A 1 H3AC H 0.972739 1.147941 0.112299 0.131 Uiso 0.346(4) 1 calc R U P A 1 C4A C 0.9514(4) 0.7008(14) 0.0319(3) 0.082(2) Uani 0.346(4) 1 d D U P A 1 H4AA H 0.961241 0.763444 0.000098 0.123 Uiso 0.346(4) 1 calc R U P A 1 H4AB H 0.922345 0.601156 0.018487 0.123 Uiso 0.346(4) 1 calc R U P A 1 H4AC H 0.980369 0.619887 0.055403 0.123 Uiso 0.346(4) 1 calc R U P A 1 C1B C 0.93741(18) 0.9157(9) 0.0722(2) 0.0627(14) Uani 0.654(4) 1 d D U P A 2 C2B C 0.9363(2) 1.1611(8) 0.0835(2) 0.0939(17) Uani 0.654(4) 1 d D U P A 2 H2BA H 0.951762 1.240556 0.057896 0.141 Uiso 0.654(4) 1 calc R U P A 2 H2BB H 0.955677 1.191221 0.121915 0.141 Uiso 0.654(4) 1 calc R U P A 2 H2BC H 0.900754 1.208938 0.077905 0.141 Uiso 0.654(4) 1 calc R U P A 2 C4B C 0.9058(2) 0.8632(13) 0.01317(17) 0.097(2) Uani 0.654(4) 1 d D U P A 2 H4BA H 0.871162 0.922810 0.007379 0.146 Uiso 0.654(4) 1 calc R U P A 2 H4BB H 0.903802 0.704202 0.007956 0.146 Uiso 0.654(4) 1 calc R U P A 2 H4BC H 0.922041 0.928701 -0.013695 0.146 Uiso 0.654(4) 1 calc R U P A 2 C3B C 0.99316(17) 0.8493(10) 0.0770(2) 0.0866(16) Uani 0.654(4) 1 d D U P A 2 H3BA H 1.004916 0.919780 0.047367 0.130 Uiso 0.654(4) 1 calc R U P A 2 H3BB H 0.995219 0.690055 0.073607 0.130 Uiso 0.654(4) 1 calc R U P A 2 H3BC H 1.014888 0.895555 0.113283 0.130 Uiso 0.654(4) 1 calc R U P A 2 C5 C 0.74003(8) -0.4236(3) 0.45939(7) 0.0385(4) Uani 1 1 d D U . . . C6A C 0.79444(10) -0.5156(4) 0.46699(10) 0.0521(7) Uani 0.891(3) 1 d D U P B 1 H6AA H 0.805335 -0.592316 0.502700 0.078 Uiso 0.891(3) 1 calc R U P B 1 H6AB H 0.818176 -0.395218 0.466374 0.078 Uiso 0.891(3) 1 calc R U P B 1 H6AC H 0.794418 -0.617871 0.436714 0.078 Uiso 0.891(3) 1 calc R U P B 1 C7A C 0.70468(10) -0.6177(4) 0.46214(9) 0.0469(6) Uani 0.891(3) 1 d D U P B 1 H7AA H 0.704859 -0.720911 0.432125 0.070 Uiso 0.891(3) 1 calc R U P B 1 H7AB H 0.669730 -0.564359 0.457938 0.070 Uiso 0.891(3) 1 calc R U P B 1 H7AC H 0.716915 -0.691573 0.498111 0.070 Uiso 0.891(3) 1 calc R U P B 1 C8A C 0.73844(13) -0.2655(4) 0.50535(9) 0.0574(8) Uani 0.891(3) 1 d D U P B 1 H8AA H 0.747530 -0.342349 0.541115 0.086 Uiso 0.891(3) 1 calc R U P B 1 H8AB H 0.703858 -0.204699 0.498697 0.086 Uiso 0.891(3) 1 calc R U P B 1 H8AC H 0.762914 -0.146704 0.506081 0.086 Uiso 0.891(3) 1 calc R U P B 1 C9A C 0.91521(15) 0.7942(13) 0.1136(3) 0.0514(13) Uani 0.654(4) 1 d D U P A 1 C10A C 0.9476(2) 0.7057(11) 0.1622(3) 0.0630(16) Uani 0.654(4) 1 d D U P A 1 H10A H 0.983683 0.712519 0.167661 0.076 Uiso 0.654(4) 1 calc R U P A 1 C11A C 0.9283(3) 0.6090(10) 0.2024(2) 0.0634(16) Uani 0.654(4) 1 d D U P A 1 H11A H 0.951026 0.548515 0.234695 0.076 Uiso 0.654(4) 1 calc R U P A 1 C12A C 0.8759(2) 0.5995(11) 0.1958(2) 0.0510(16) Uani 0.654(4) 1 d D U P A 1 H12A H 0.862938 0.534418 0.223893 0.061 Uiso 0.654(4) 1 calc R U P A 1 C9B C 0.9156(2) 0.785(2) 0.1140(5) 0.052(2) Uani 0.346(4) 1 d D U P A 2 C10B C 0.9466(4) 0.652(2) 0.1547(5) 0.057(2) Uani 0.346(4) 1 d D U P A 2 H10B H 0.981957 0.638532 0.156720 0.069 Uiso 0.346(4) 1 calc R U P A 2 C11B C 0.9264(5) 0.5385(19) 0.1921(5) 0.058(2) Uani 0.346(4) 1 d D U P A 2 H11B H 0.948162 0.453647 0.220772 0.070 Uiso 0.346(4) 1 calc R U P A 2 C12B C 0.8741(4) 0.550(2) 0.1875(5) 0.051(2) Uani 0.346(4) 1 d D U P A 2 H12B H 0.860012 0.463874 0.211561 0.061 Uiso 0.346(4) 1 calc R U P A 2 C13 C 0.84209(8) 0.6852(3) 0.14806(7) 0.0393(4) Uani 1 1 d D U . . . C14 C 0.86315(7) 0.7897(3) 0.10927(8) 0.0404(4) Uani 1 1 d D U . . . H14 H 0.840621 0.861015 0.078486 0.049 Uiso 0.654(4) 1 calc R U P A 1 H14A H 0.841121 0.865474 0.078941 0.049 Uiso 0.346(4) 1 calc R U P A 2 C15 C 0.78598(7) 0.6824(3) 0.14077(6) 0.0316(4) Uani 1 1 d . . . . . C16 C 0.76238(7) 0.5076(3) 0.15966(6) 0.0297(4) Uani 1 1 d . . . . . H16 H 0.783123 0.390151 0.177911 0.036 Uiso 1 1 calc R U . . . C17 C 0.70934(7) 0.4967(3) 0.15300(6) 0.0271(3) Uani 1 1 d . . . . . C18 C 0.67873(7) 0.6602(3) 0.11899(6) 0.0285(3) Uani 1 1 d . . . . . C19 C 0.70285(7) 0.8426(3) 0.10243(7) 0.0320(4) Uani 1 1 d . . . . . H19 H 0.682433 0.958198 0.082721 0.038 Uiso 1 1 calc R U . . . C20 C 0.75496(7) 0.8568(3) 0.11408(7) 0.0325(4) Uani 1 1 d . . . . . H20 H 0.770375 0.984809 0.104156 0.039 Uiso 1 1 calc R U . . . C21 C 0.68303(7) 0.3248(3) 0.17659(6) 0.0262(3) Uani 1 1 d . . . . . C22 C 0.62958(7) 0.2920(3) 0.15099(6) 0.0276(3) Uani 1 1 d . . . . . C23 C 0.60190(7) 0.4490(3) 0.11104(6) 0.0302(4) Uani 1 1 d . . . . . H23 H 0.566856 0.423215 0.092882 0.036 Uiso 1 1 calc R U . . . C24 C 0.62460(7) 0.6312(3) 0.09893(6) 0.0308(4) Uani 1 1 d . . . . . H24 H 0.604404 0.741961 0.076760 0.037 Uiso 1 1 calc R U . . . C25 C 0.70674(6) 0.2015(3) 0.22493(6) 0.0253(3) Uani 1 1 d . . . . . C26 C 0.67869(6) 0.0383(3) 0.24480(6) 0.0256(3) Uani 1 1 d . . . . . C27 C 0.62908(7) -0.0193(3) 0.21113(6) 0.0271(3) Uani 1 1 d . . . . . C28 C 0.60367(7) 0.1144(3) 0.16634(6) 0.0285(3) Uani 1 1 d . . . . . C29 C 0.69628(7) -0.0757(3) 0.29880(6) 0.0267(3) Uani 1 1 d . . . . . C30 C 0.67013(7) -0.2683(3) 0.30801(6) 0.0276(3) Uani 1 1 d . . . . . C31 C 0.62603(7) -0.3436(3) 0.26668(7) 0.0302(4) Uani 1 1 d . . . . . H31 H 0.611575 -0.482313 0.270644 0.036 Uiso 1 1 calc R U . . . C32 C 0.60503(7) -0.2177(3) 0.22217(7) 0.0292(3) Uani 1 1 d . . . . . H32 H 0.573463 -0.261162 0.197384 0.035 Uiso 1 1 calc R U . . . C33 C 0.73543(7) -0.0020(3) 0.34460(7) 0.0319(4) Uani 1 1 d . . . . . H33 H 0.753112 0.129099 0.341061 0.038 Uiso 1 1 calc R U . . . C34 C 0.74888(7) -0.1141(3) 0.39434(7) 0.0342(4) Uani 1 1 d . . . . . H34 H 0.775838 -0.058434 0.423762 0.041 Uiso 1 1 calc R U . . . C35 C 0.72413(7) -0.3078(3) 0.40307(7) 0.0323(4) Uani 1 1 d D . . . . C36 C 0.68522(7) -0.3809(3) 0.35913(7) 0.0299(4) Uani 1 1 d . . . . . H36 H 0.667897 -0.512216 0.363417 0.036 Uiso 1 1 calc R U . . . C37 C 0.76095(7) 0.2441(3) 0.25609(6) 0.0270(3) Uani 1 1 d . . . . . C38 C 0.77479(7) 0.4403(3) 0.28452(7) 0.0308(4) Uani 1 1 d . . . . . H38 H 0.749761 0.551608 0.281833 0.037 Uiso 1 1 calc R U . . . C39 C 0.82431(8) 0.4764(3) 0.31661(7) 0.0396(4) Uani 1 1 d . . . . . H39 H 0.833205 0.609548 0.336447 0.048 Uiso 1 1 calc R U . . . C40 C 0.86052(8) 0.3147(4) 0.31919(8) 0.0454(5) Uani 1 1 d . . . . . C41 C 0.84848(8) 0.1205(4) 0.29026(8) 0.0438(5) Uani 1 1 d . . . . . H41 H 0.874054 0.012641 0.291741 0.053 Uiso 1 1 calc R U . . . C42 C 0.79852(7) 0.0856(3) 0.25905(7) 0.0334(4) Uani 1 1 d . . . . . H42 H 0.789798 -0.048188 0.239442 0.040 Uiso 1 1 calc R U . . . C43 C 0.46731(7) 0.0343(3) 0.07656(7) 0.0340(4) Uani 1 1 d . . . . . C44 C 0.45292(8) 0.2618(3) 0.05303(8) 0.0422(4) Uani 1 1 d . . . . . H44A H 0.464136 0.280400 0.019045 0.063 Uiso 1 1 calc R U . . . H44B H 0.469661 0.371591 0.080514 0.063 Uiso 1 1 calc R U . . . H44C H 0.415687 0.280186 0.044372 0.063 Uiso 1 1 calc R U . . . C45 C 0.44055(8) -0.1370(4) 0.03523(8) 0.0445(5) Uani 1 1 d . . . . . H45A H 0.403829 -0.136160 0.032788 0.067 Uiso 1 1 calc R U . . . H45B H 0.454813 -0.281468 0.047513 0.067 Uiso 1 1 calc R U . . . H45C H 0.445653 -0.104362 -0.001401 0.067 Uiso 1 1 calc R U . . . C46 C 0.46167(7) 0.0055(3) 0.13673(8) 0.0360(4) Uani 1 1 d . . . . . C47 C 0.45999(8) -0.2334(3) 0.15343(8) 0.0414(4) Uani 1 1 d . . . . . H47A H 0.426358 -0.295176 0.135064 0.062 Uiso 1 1 calc R U . . . H47B H 0.465877 -0.243505 0.193860 0.062 Uiso 1 1 calc R U . . . H47C H 0.486667 -0.315297 0.142114 0.062 Uiso 1 1 calc R U . . . C48 C 0.41828(8) 0.1310(4) 0.15012(10) 0.0482(5) Uani 1 1 d . . . . . H48A H 0.422000 0.287166 0.143221 0.072 Uiso 1 1 calc R U . . . H48B H 0.419238 0.108770 0.189296 0.072 Uiso 1 1 calc R U . . . H48C H 0.385506 0.078374 0.126500 0.072 Uiso 1 1 calc R U . . . Cl1 Cl 0.92314(3) 0.36179(15) 0.35845(3) 0.0824(2) Uani 1 1 d . . . . . O1 O 0.52298(5) 0.0145(2) 0.08539(5) 0.0318(3) Uani 1 1 d . . . . . O2 O 0.51029(5) 0.0937(2) 0.17017(5) 0.0350(3) Uani 1 1 d . . . . . C6B C 0.7471(7) -0.6662(12) 0.4580(6) 0.044(3) Uani 0.109(3) 1 d D U P B 2 H6BA H 0.777355 -0.699029 0.444974 0.066 Uiso 0.109(3) 1 calc R U P B 2 H6BB H 0.716753 -0.732238 0.432628 0.066 Uiso 0.109(3) 1 calc R U P B 2 H6BC H 0.751656 -0.726233 0.495434 0.066 Uiso 0.109(3) 1 calc R U P B 2 C7B C 0.6989(5) -0.370(3) 0.4911(6) 0.051(4) Uani 0.109(3) 1 d D U P B 2 H7BA H 0.708997 -0.436501 0.528221 0.077 Uiso 0.109(3) 1 calc R U P B 2 H7BB H 0.665662 -0.429317 0.470364 0.077 Uiso 0.109(3) 1 calc R U P B 2 H7BC H 0.696173 -0.211296 0.494692 0.077 Uiso 0.109(3) 1 calc R U P B 2 C8B C 0.7893(5) -0.321(3) 0.4986(5) 0.054(4) Uani 0.109(3) 1 d D U P B 2 H8BA H 0.798648 -0.402129 0.533817 0.081 Uiso 0.109(3) 1 calc R U P B 2 H8BB H 0.782890 -0.167938 0.505824 0.081 Uiso 0.109(3) 1 calc R U P B 2 H8BC H 0.817480 -0.330106 0.480791 0.081 Uiso 0.109(3) 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 B1 0.0312(10) 0.0268(9) 0.0288(8) 0.0032(7) 0.0100(8) 0.0024(7) C1A 0.055(4) 0.083(5) 0.064(4) 0.019(4) 0.031(4) -0.017(4) C2A 0.067(4) 0.094(6) 0.075(5) 0.033(4) 0.035(4) -0.015(4) C3A 0.071(5) 0.108(6) 0.087(5) 0.017(5) 0.028(4) -0.034(5) C4A 0.082(5) 0.104(5) 0.076(4) 0.018(4) 0.049(4) -0.008(4) C1B 0.048(2) 0.080(3) 0.065(3) 0.017(2) 0.023(2) -0.017(2) C2B 0.089(4) 0.081(3) 0.123(4) 0.034(3) 0.048(3) -0.014(3) C4B 0.083(3) 0.160(6) 0.057(2) 0.016(3) 0.034(2) -0.042(4) C3B 0.068(3) 0.107(4) 0.101(3) 0.031(3) 0.050(3) -0.007(3) C5 0.0458(11) 0.0391(10) 0.0303(8) 0.0095(7) 0.0094(8) 0.0026(8) C6A 0.0510(15) 0.0561(15) 0.0433(12) 0.0183(11) 0.0024(11) 0.0092(12) C7A 0.0633(16) 0.0447(12) 0.0321(10) 0.0127(9) 0.0117(10) -0.0034(11) C8A 0.100(2) 0.0461(13) 0.0267(10) 0.0033(9) 0.0179(12) 0.0033(14) C9A 0.040(2) 0.063(3) 0.053(2) 0.009(2) 0.015(2) -0.009(2) C10A 0.036(2) 0.087(4) 0.065(2) 0.019(2) 0.0113(18) -0.010(2) C11A 0.0391(19) 0.091(4) 0.055(2) 0.018(3) 0.0026(18) -0.004(3) C12A 0.0377(19) 0.075(3) 0.039(2) 0.017(2) 0.0081(16) -0.005(2) C9B 0.040(3) 0.065(4) 0.053(4) 0.011(4) 0.019(4) -0.010(4) C10B 0.036(3) 0.076(4) 0.063(4) 0.015(3) 0.018(3) -0.006(3) C11B 0.038(3) 0.077(5) 0.057(4) 0.021(4) 0.009(3) -0.006(4) C12B 0.038(3) 0.072(5) 0.044(4) 0.019(4) 0.013(3) -0.008(3) C13 0.0375(10) 0.0478(10) 0.0337(8) 0.0036(8) 0.0113(8) -0.0052(8) C14 0.0400(10) 0.0454(10) 0.0373(9) 0.0045(8) 0.0127(8) -0.0084(9) C15 0.0370(10) 0.0376(9) 0.0218(7) 0.0007(6) 0.0105(7) -0.0022(8) C16 0.0338(9) 0.0345(9) 0.0222(7) 0.0026(6) 0.0097(7) 0.0035(7) C17 0.0325(9) 0.0290(8) 0.0214(7) -0.0008(6) 0.0101(6) 0.0018(7) C18 0.0366(9) 0.0284(8) 0.0223(7) 0.0008(6) 0.0110(6) 0.0031(7) C19 0.0420(10) 0.0292(8) 0.0258(7) 0.0017(6) 0.0108(7) 0.0030(7) C20 0.0415(10) 0.0314(8) 0.0267(7) 0.0020(6) 0.0131(7) -0.0039(7) C21 0.0311(9) 0.0256(7) 0.0238(7) 0.0008(6) 0.0107(6) 0.0034(6) C22 0.0314(9) 0.0293(8) 0.0235(7) -0.0004(6) 0.0097(6) 0.0033(7) C23 0.0300(9) 0.0358(9) 0.0241(7) 0.0028(7) 0.0058(6) 0.0031(7) C24 0.0351(9) 0.0323(8) 0.0243(7) 0.0045(6) 0.0066(7) 0.0069(7) C25 0.0282(8) 0.0247(7) 0.0243(7) -0.0003(6) 0.0089(6) 0.0036(6) C26 0.0294(9) 0.0256(7) 0.0234(7) -0.0008(6) 0.0098(6) 0.0042(6) C27 0.0293(9) 0.0296(8) 0.0245(7) 0.0007(6) 0.0107(6) 0.0017(7) C28 0.0302(9) 0.0309(8) 0.0252(7) -0.0015(6) 0.0088(6) 0.0029(7) C29 0.0297(9) 0.0275(8) 0.0251(7) 0.0023(6) 0.0109(6) 0.0050(7) C30 0.0303(9) 0.0282(8) 0.0268(7) 0.0021(6) 0.0119(7) 0.0048(7) C31 0.0323(9) 0.0278(8) 0.0339(8) 0.0016(6) 0.0148(7) -0.0012(7) C32 0.0290(9) 0.0318(8) 0.0273(7) -0.0008(6) 0.0084(7) -0.0014(7) C33 0.0378(10) 0.0306(8) 0.0276(8) 0.0035(6) 0.0097(7) -0.0013(7) C34 0.0398(10) 0.0369(9) 0.0245(7) 0.0024(7) 0.0062(7) -0.0003(8) C35 0.0393(10) 0.0329(9) 0.0273(8) 0.0044(7) 0.0135(7) 0.0072(7) C36 0.0331(9) 0.0283(8) 0.0320(8) 0.0054(6) 0.0152(7) 0.0032(7) C37 0.0296(9) 0.0309(8) 0.0227(7) 0.0060(6) 0.0108(6) 0.0019(7) C38 0.0341(9) 0.0331(8) 0.0273(7) 0.0034(7) 0.0122(7) -0.0002(7) C39 0.0426(11) 0.0431(10) 0.0317(8) 0.0025(8) 0.0072(8) -0.0090(9) C40 0.0290(10) 0.0608(13) 0.0404(9) 0.0132(9) -0.0011(8) -0.0048(9) C41 0.0340(10) 0.0516(12) 0.0453(10) 0.0139(9) 0.0095(8) 0.0111(9) C42 0.0348(10) 0.0338(9) 0.0325(8) 0.0057(7) 0.0107(7) 0.0058(7) C43 0.0282(9) 0.0354(9) 0.0373(9) 0.0051(7) 0.0066(7) 0.0009(7) C44 0.0359(10) 0.0401(10) 0.0475(10) 0.0087(8) 0.0060(8) 0.0049(8) C45 0.0430(12) 0.0447(11) 0.0419(10) 0.0023(8) 0.0043(9) -0.0058(9) C46 0.0301(10) 0.0385(10) 0.0403(9) 0.0021(7) 0.0108(8) -0.0007(8) C47 0.0384(11) 0.0407(10) 0.0469(10) 0.0072(8) 0.0143(9) -0.0015(8) C48 0.0384(11) 0.0497(12) 0.0629(12) 0.0042(10) 0.0249(10) 0.0053(9) Cl1 0.0396(3) 0.1025(6) 0.0848(5) 0.0133(4) -0.0191(3) -0.0113(4) O1 0.0287(6) 0.0366(6) 0.0302(6) 0.0011(5) 0.0078(5) 0.0017(5) O2 0.0323(7) 0.0403(7) 0.0345(6) -0.0019(5) 0.0129(5) -0.0008(5) C6B 0.052(8) 0.056(6) 0.027(6) 0.011(6) 0.013(6) 0.004(6) C7B 0.063(7) 0.061(8) 0.033(7) 0.017(7) 0.017(6) 0.007(7) C8B 0.057(7) 0.057(8) 0.042(7) 0.027(6) 0.002(6) -0.003(7) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag B1 C28 1.578(3) . ? B1 O1 1.369(2) . ? B1 O2 1.361(2) . ? C1A C2A 1.528(7) . ? C1A C3A 1.526(7) . ? C1A C4A 1.539(7) . ? C1A C9A 1.544(10) . ? C2A H2AA 0.9800 . ? C2A H2AB 0.9800 . ? C2A H2AC 0.9800 . ? C3A H3AA 0.9800 . ? C3A H3AB 0.9800 . ? C3A H3AC 0.9800 . ? C4A H4AA 0.9800 . ? C4A H4AB 0.9800 . ? C4A H4AC 0.9800 . ? C1B C2B 1.528(6) . ? C1B C4B 1.527(5) . ? C1B C3B 1.537(5) . ? C1B C9B 1.550(8) . ? C2B H2BA 0.9800 . ? C2B H2BB 0.9800 . ? C2B H2BC 0.9800 . ? C4B H4BA 0.9800 . ? C4B H4BB 0.9800 . ? C4B H4BC 0.9800 . ? C3B H3BA 0.9800 . ? C3B H3BB 0.9800 . ? C3B H3BC 0.9800 . ? C5 C6A 1.541(3) . ? C5 C7A 1.538(3) . ? C5 C8A 1.508(3) . ? C5 C35 1.529(2) . ? C5 C6B 1.497(7) . ? C5 C7B 1.563(7) . ? C5 C8B 1.561(7) . ? C6A H6AA 0.9800 . ? C6A H6AB 0.9800 . ? C6A H6AC 0.9800 . ? C7A H7AA 0.9800 . ? C7A H7AB 0.9800 . ? C7A H7AC 0.9800 . ? C8A H8AA 0.9800 . ? C8A H8AB 0.9800 . ? C8A H8AC 0.9800 . ? C9A C10A 1.404(5) . ? C9A C14 1.386(4) . ? C10A H10A 0.9500 . ? C10A C11A 1.380(5) . ? C11A H11A 0.9500 . ? C11A C12A 1.385(5) . ? C12A H12A 0.9500 . ? C12A C13 1.397(4) . ? C9B C10B 1.395(6) . ? C9B C14 1.393(6) . ? C10B H10B 0.9500 . ? C10B C11B 1.387(6) . ? C11B H11B 0.9500 . ? C11B C12B 1.391(6) . ? C12B H12B 0.9500 . ? C12B C13 1.398(6) . ? C13 C14 1.401(2) . ? C13 C15 1.482(3) . ? C14 H14 0.9500 . ? C14 H14A 0.9500 . ? C15 C16 1.390(2) . ? C15 C20 1.410(3) . ? C16 H16 0.9500 . ? C16 C17 1.403(3) . ? C17 C18 1.426(2) . ? C17 C21 1.477(2) . ? C18 C19 1.409(2) . ? C18 C24 1.428(3) . ? C19 H19 0.9500 . ? C19 C20 1.366(3) . ? C20 H20 0.9500 . ? C21 C22 1.432(2) . ? C21 C25 1.422(2) . ? C22 C23 1.442(2) . ? C22 C28 1.400(2) . ? C23 H23 0.9500 . ? C23 C24 1.345(3) . ? C24 H24 0.9500 . ? C25 C26 1.421(2) . ? C25 C37 1.490(2) . ? C26 C27 1.426(2) . ? C26 C29 1.479(2) . ? C27 C28 1.407(2) . ? C27 C32 1.438(2) . ? C29 C30 1.424(2) . ? C29 C33 1.410(2) . ? C30 C31 1.431(2) . ? C30 C36 1.410(2) . ? C31 H31 0.9500 . ? C31 C32 1.346(2) . ? C32 H32 0.9500 . ? C33 H33 0.9500 . ? C33 C34 1.379(2) . ? C34 H34 0.9500 . ? C34 C35 1.406(3) . ? C35 C36 1.377(3) . ? C36 H36 0.9500 . ? C37 C38 1.393(2) . ? C37 C42 1.393(2) . ? C38 H38 0.9500 . ? C38 C39 1.384(3) . ? C39 H39 0.9500 . ? C39 C40 1.382(3) . ? C40 C41 1.382(3) . ? C40 Cl1 1.742(2) . ? C41 H41 0.9500 . ? C41 C42 1.387(3) . ? C42 H42 0.9500 . ? C43 C44 1.519(3) . ? C43 C45 1.513(3) . ? C43 C46 1.558(3) . ? C43 O1 1.469(2) . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C46 C47 1.523(3) . ? C46 C48 1.513(3) . ? C46 O2 1.462(2) . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C48 H48A 0.9800 . ? C48 H48B 0.9800 . ? C48 H48C 0.9800 . ? C6B H6BA 0.9800 . ? C6B H6BB 0.9800 . ? C6B H6BC 0.9800 . ? C7B H7BA 0.9800 . ? C7B H7BB 0.9800 . ? C7B H7BC 0.9800 . ? C8B H8BA 0.9800 . ? C8B H8BB 0.9800 . ? C8B H8BC 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 B1 C28 125.68(15) . . ? O2 B1 C28 120.89(15) . . ? O2 B1 O1 113.43(17) . . ? C2A C1A C4A 107.8(7) . . ? C2A C1A C9A 111.7(6) . . ? C3A C1A C2A 109.7(7) . . ? C3A C1A C4A 109.2(7) . . ? C3A C1A C9A 106.9(6) . . ? C4A C1A C9A 111.5(6) . . ? C1A C2A H2AA 109.5 . . ? C1A C2A H2AB 109.5 . . ? C1A C2A H2AC 109.5 . . ? H2AA C2A H2AB 109.5 . . ? H2AA C2A H2AC 109.5 . . ? H2AB C2A H2AC 109.5 . . ? C1A C3A H3AA 109.5 . . ? C1A C3A H3AB 109.5 . . ? C1A C3A H3AC 109.5 . . ? H3AA C3A H3AB 109.5 . . ? H3AA C3A H3AC 109.5 . . ? H3AB C3A H3AC 109.5 . . ? C1A C4A H4AA 109.5 . . ? C1A C4A H4AB 109.5 . . ? C1A C4A H4AC 109.5 . . ? H4AA C4A H4AB 109.5 . . ? H4AA C4A H4AC 109.5 . . ? H4AB C4A H4AC 109.5 . . ? C2B C1B C3B 108.2(4) . . ? C2B C1B C9B 110.5(6) . . ? C4B C1B C2B 110.6(5) . . ? C4B C1B C3B 108.0(5) . . ? C4B C1B C9B 108.9(6) . . ? C3B C1B C9B 110.7(4) . . ? C1B C2B H2BA 109.5 . . ? C1B C2B H2BB 109.5 . . ? C1B C2B H2BC 109.5 . . ? H2BA C2B H2BB 109.5 . . ? H2BA C2B H2BC 109.5 . . ? H2BB C2B H2BC 109.5 . . ? C1B C4B H4BA 109.5 . . ? C1B C4B H4BB 109.5 . . ? C1B C4B H4BC 109.5 . . ? H4BA C4B H4BB 109.5 . . ? H4BA C4B H4BC 109.5 . . ? H4BB C4B H4BC 109.5 . . ? C1B C3B H3BA 109.5 . . ? C1B C3B H3BB 109.5 . . ? C1B C3B H3BC 109.5 . . ? H3BA C3B H3BB 109.5 . . ? H3BA C3B H3BC 109.5 . . ? H3BB C3B H3BC 109.5 . . ? C7A C5 C6A 107.39(18) . . ? C8A C5 C6A 111.1(2) . . ? C8A C5 C7A 108.48(18) . . ? C8A C5 C35 110.09(16) . . ? C35 C5 C6A 107.97(16) . . ? C35 C5 C7A 111.81(16) . . ? C35 C5 C7B 107.7(5) . . ? C35 C5 C8B 112.1(6) . . ? C6B C5 C35 116.3(5) . . ? C6B C5 C7B 109.3(7) . . ? C6B C5 C8B 108.5(7) . . ? C8B C5 C7B 101.9(7) . . ? C5 C6A H6AA 109.5 . . ? C5 C6A H6AB 109.5 . . ? C5 C6A H6AC 109.5 . . ? H6AA C6A H6AB 109.5 . . ? H6AA C6A H6AC 109.5 . . ? H6AB C6A H6AC 109.5 . . ? C5 C7A H7AA 109.5 . . ? C5 C7A H7AB 109.5 . . ? C5 C7A H7AC 109.5 . . ? H7AA C7A H7AB 109.5 . . ? H7AA C7A H7AC 109.5 . . ? H7AB C7A H7AC 109.5 . . ? C5 C8A H8AA 109.5 . . ? C5 C8A H8AB 109.5 . . ? C5 C8A H8AC 109.5 . . ? H8AA C8A H8AB 109.5 . . ? H8AA C8A H8AC 109.5 . . ? H8AB C8A H8AC 109.5 . . ? C10A C9A C1A 122.2(5) . . ? C14 C9A C1A 121.1(4) . . ? C14 C9A C10A 116.7(4) . . ? C9A C10A H10A 119.3 . . ? C11A C10A C9A 121.4(5) . . ? C11A C10A H10A 119.3 . . ? C10A C11A H11A 119.8 . . ? C10A C11A C12A 120.5(5) . . ? C12A C11A H11A 119.8 . . ? C11A C12A H12A 119.9 . . ? C11A C12A C13 120.2(5) . . ? C13 C12A H12A 119.9 . . ? C10B C9B C1B 121.8(6) . . ? C14 C9B C1B 119.7(6) . . ? C14 C9B C10B 118.4(7) . . ? C9B C10B H10B 119.5 . . ? C11B C10B C9B 120.9(7) . . ? C11B C10B H10B 119.5 . . ? C10B C11B H11B 120.2 . . ? C10B C11B C12B 119.6(8) . . ? C12B C11B H11B 120.2 . . ? C11B C12B H12B 119.5 . . ? C11B C12B C13 121.0(8) . . ? C13 C12B H12B 119.5 . . ? C12A C13 C14 117.7(3) . . ? C12A C13 C15 121.3(3) . . ? C12B C13 C14 117.8(5) . . ? C12B C13 C15 120.3(5) . . ? C14 C13 C15 120.87(17) . . ? C9A C14 C13 123.2(3) . . ? C9A C14 H14 118.4 . . ? C9B C14 C13 121.7(4) . . ? C9B C14 H14A 119.2 . . ? C13 C14 H14 118.4 . . ? C13 C14 H14A 119.2 . . ? C16 C15 C13 121.07(17) . . ? C16 C15 C20 118.13(17) . . ? C20 C15 C13 120.80(16) . . ? C15 C16 H16 118.5 . . ? C15 C16 C17 123.02(16) . . ? C17 C16 H16 118.5 . . ? C16 C17 C18 116.89(15) . . ? C16 C17 C21 125.04(15) . . ? C18 C17 C21 118.03(15) . . ? C17 C18 C24 120.12(16) . . ? C19 C18 C17 119.20(17) . . ? C19 C18 C24 120.54(16) . . ? C18 C19 H19 119.3 . . ? C20 C19 C18 121.44(17) . . ? C20 C19 H19 119.3 . . ? C15 C20 H20 119.9 . . ? C19 C20 C15 120.29(16) . . ? C19 C20 H20 119.9 . . ? C22 C21 C17 117.35(14) . . ? C25 C21 C17 123.89(15) . . ? C25 C21 C22 118.63(15) . . ? C21 C22 C23 119.55(15) . . ? C28 C22 C21 120.46(15) . . ? C28 C22 C23 119.93(16) . . ? C22 C23 H23 119.3 . . ? C24 C23 C22 121.46(17) . . ? C24 C23 H23 119.3 . . ? C18 C24 H24 119.6 . . ? C23 C24 C18 120.78(16) . . ? C23 C24 H24 119.6 . . ? C21 C25 C37 120.65(15) . . ? C26 C25 C21 120.33(15) . . ? C26 C25 C37 119.01(14) . . ? C25 C26 C27 118.39(14) . . ? C25 C26 C29 125.18(15) . . ? C27 C26 C29 116.41(15) . . ? C26 C27 C32 119.96(15) . . ? C28 C27 C26 120.60(15) . . ? C28 C27 C32 119.42(16) . . ? C22 C28 B1 122.06(15) . . ? C22 C28 C27 119.51(16) . . ? C27 C28 B1 118.08(15) . . ? C30 C29 C26 118.90(15) . . ? C33 C29 C26 125.31(15) . . ? C33 C29 C30 115.65(14) . . ? C29 C30 C31 120.39(15) . . ? C36 C30 C29 120.82(16) . . ? C36 C30 C31 118.68(16) . . ? C30 C31 H31 120.0 . . ? C32 C31 C30 119.92(16) . . ? C32 C31 H31 120.0 . . ? C27 C32 H32 119.1 . . ? C31 C32 C27 121.78(16) . . ? C31 C32 H32 119.1 . . ? C29 C33 H33 118.9 . . ? C34 C33 C29 122.15(17) . . ? C34 C33 H33 118.9 . . ? C33 C34 H34 118.8 . . ? C33 C34 C35 122.35(17) . . ? C35 C34 H34 118.8 . . ? C34 C35 C5 120.19(17) . . ? C36 C35 C5 123.35(17) . . ? C36 C35 C34 116.45(15) . . ? C30 C36 H36 118.8 . . ? C35 C36 C30 122.50(16) . . ? C35 C36 H36 118.8 . . ? C38 C37 C25 120.70(15) . . ? C42 C37 C25 120.70(16) . . ? C42 C37 C38 118.57(17) . . ? C37 C38 H38 119.4 . . ? C39 C38 C37 121.29(17) . . ? C39 C38 H38 119.4 . . ? C38 C39 H39 120.7 . . ? C40 C39 C38 118.67(18) . . ? C40 C39 H39 120.7 . . ? C39 C40 C41 121.58(18) . . ? C39 C40 Cl1 118.74(18) . . ? C41 C40 Cl1 119.65(18) . . ? C40 C41 H41 120.5 . . ? C40 C41 C42 119.01(19) . . ? C42 C41 H41 120.5 . . ? C37 C42 H42 119.6 . . ? C41 C42 C37 120.84(18) . . ? C41 C42 H42 119.6 . . ? C44 C43 C46 113.24(16) . . ? C45 C43 C44 110.09(16) . . ? C45 C43 C46 115.21(16) . . ? O1 C43 C44 106.33(15) . . ? O1 C43 C45 109.37(16) . . ? O1 C43 C46 101.86(13) . . ? C43 C44 H44A 109.5 . . ? C43 C44 H44B 109.5 . . ? C43 C44 H44C 109.5 . . ? H44A C44 H44B 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? C43 C45 H45A 109.5 . . ? C43 C45 H45B 109.5 . . ? C43 C45 H45C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C47 C46 C43 112.94(16) . . ? C48 C46 C43 115.83(16) . . ? C48 C46 C47 110.16(16) . . ? O2 C46 C43 101.75(14) . . ? O2 C46 C47 106.60(15) . . ? O2 C46 C48 108.76(16) . . ? C46 C47 H47A 109.5 . . ? C46 C47 H47B 109.5 . . ? C46 C47 H47C 109.5 . . ? H47A C47 H47B 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C46 C48 H48A 109.5 . . ? C46 C48 H48B 109.5 . . ? C46 C48 H48C 109.5 . . ? H48A C48 H48B 109.5 . . ? H48A C48 H48C 109.5 . . ? H48B C48 H48C 109.5 . . ? B1 O1 C43 106.41(13) . . ? B1 O2 C46 107.08(14) . . ? C5 C6B H6BA 109.5 . . ? C5 C6B H6BB 109.5 . . ? C5 C6B H6BC 109.5 . . ? H6BA C6B H6BB 109.5 . . ? H6BA C6B H6BC 109.5 . . ? H6BB C6B H6BC 109.5 . . ? C5 C7B H7BA 109.5 . . ? C5 C7B H7BB 109.5 . . ? C5 C7B H7BC 109.5 . . ? H7BA C7B H7BB 109.5 . . ? H7BA C7B H7BC 109.5 . . ? H7BB C7B H7BC 109.5 . . ? C5 C8B H8BA 109.5 . . ? C5 C8B H8BB 109.5 . . ? C5 C8B H8BC 109.5 . . ? H8BA C8B H8BB 109.5 . . ? H8BA C8B H8BC 109.5 . . ? H8BB C8B H8BC 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1A C9A C10A C11A -174.8(7) . . . . ? C1A C9A C14 C13 172.1(5) . . . . ? C2A C1A C9A C10A -164.0(7) . . . . ? C2A C1A C9A C14 18.0(10) . . . . ? C3A C1A C9A C10A -44.1(9) . . . . ? C3A C1A C9A C14 138.0(8) . . . . ? C4A C1A C9A C10A 75.3(9) . . . . ? C4A C1A C9A C14 -102.7(8) . . . . ? C1B C9B C10B C11B 179.3(12) . . . . ? C1B C9B C14 C13 -176.1(7) . . . . ? C2B C1B C9B C10B -111.6(10) . . . . ? C2B C1B C9B C14 72.4(12) . . . . ? C4B C1B C9B C10B 126.8(10) . . . . ? C4B C1B C9B C14 -49.2(13) . . . . ? C3B C1B C9B C10B 8.2(13) . . . . ? C3B C1B C9B C14 -167.8(9) . . . . ? C5 C35 C36 C30 178.10(16) . . . . ? C6A C5 C35 C34 -68.0(2) . . . . ? C6A C5 C35 C36 113.3(2) . . . . ? C7A C5 C35 C34 174.09(18) . . . . ? C7A C5 C35 C36 -4.7(3) . . . . ? C8A C5 C35 C34 53.4(3) . . . . ? C8A C5 C35 C36 -125.3(2) . . . . ? C9A C10A C11A C12A -0.8(9) . . . . ? C10A C9A C14 C13 -6.0(8) . . . . ? C10A C11A C12A C13 0.9(9) . . . . ? C11A C12A C13 C14 -3.3(8) . . . . ? C11A C12A C13 C15 -178.3(4) . . . . ? C12A C13 C14 C9A 6.1(6) . . . . ? C12A C13 C15 C16 -36.5(5) . . . . ? C12A C13 C15 C20 144.0(4) . . . . ? C9B C10B C11B C12B 3.1(13) . . . . ? C10B C9B C14 C13 7.7(13) . . . . ? C10B C11B C12B C13 -4.4(17) . . . . ? C11B C12B C13 C14 7.2(15) . . . . ? C11B C12B C13 C15 175.3(9) . . . . ? C12B C13 C14 C9B -8.9(11) . . . . ? C12B C13 C15 C16 -19.1(8) . . . . ? C12B C13 C15 C20 161.3(8) . . . . ? C13 C15 C16 C17 -179.12(15) . . . . ? C13 C15 C20 C19 173.19(16) . . . . ? C14 C9A C10A C11A 3.2(9) . . . . ? C14 C9B C10B C11B -4.6(13) . . . . ? C14 C13 C15 C16 148.67(18) . . . . ? C14 C13 C15 C20 -30.9(3) . . . . ? C15 C13 C14 C9A -178.9(5) . . . . ? C15 C13 C14 C9B -177.0(8) . . . . ? C15 C16 C17 C18 8.3(2) . . . . ? C15 C16 C17 C21 -174.28(15) . . . . ? C16 C15 C20 C19 -6.4(2) . . . . ? C16 C17 C18 C19 -11.2(2) . . . . ? C16 C17 C18 C24 164.50(15) . . . . ? C16 C17 C21 C22 -158.62(15) . . . . ? C16 C17 C21 C25 25.6(2) . . . . ? C17 C18 C19 C20 5.8(2) . . . . ? C17 C18 C24 C23 -1.0(2) . . . . ? C17 C21 C22 C23 -11.1(2) . . . . ? C17 C21 C22 C28 171.76(14) . . . . ? C17 C21 C25 C26 -179.78(14) . . . . ? C17 C21 C25 C37 1.4(2) . . . . ? C18 C17 C21 C22 18.8(2) . . . . ? C18 C17 C21 C25 -156.92(15) . . . . ? C18 C19 C20 C15 3.2(2) . . . . ? C19 C18 C24 C23 174.71(15) . . . . ? C20 C15 C16 C17 0.5(2) . . . . ? C21 C17 C18 C19 171.12(14) . . . . ? C21 C17 C18 C24 -13.1(2) . . . . ? C21 C22 C23 C24 -2.9(2) . . . . ? C21 C22 C28 B1 179.60(14) . . . . ? C21 C22 C28 C27 6.5(2) . . . . ? C21 C25 C26 C27 8.6(2) . . . . ? C21 C25 C26 C29 -170.03(14) . . . . ? C21 C25 C37 C38 67.3(2) . . . . ? C21 C25 C37 C42 -114.98(17) . . . . ? C22 C21 C25 C26 4.5(2) . . . . ? C22 C21 C25 C37 -174.33(14) . . . . ? C22 C23 C24 C18 9.3(2) . . . . ? C23 C22 C28 B1 2.5(2) . . . . ? C23 C22 C28 C27 -170.59(15) . . . . ? C24 C18 C19 C20 -169.89(16) . . . . ? C25 C21 C22 C23 164.83(14) . . . . ? C25 C21 C22 C28 -12.3(2) . . . . ? C25 C26 C27 C28 -14.6(2) . . . . ? C25 C26 C27 C32 164.23(14) . . . . ? C25 C26 C29 C30 -165.80(15) . . . . ? C25 C26 C29 C33 18.7(3) . . . . ? C25 C37 C38 C39 175.71(15) . . . . ? C25 C37 C42 C41 -176.80(16) . . . . ? C26 C25 C37 C38 -111.56(17) . . . . ? C26 C25 C37 C42 66.1(2) . . . . ? C26 C27 C28 B1 -166.28(14) . . . . ? C26 C27 C28 C22 7.1(2) . . . . ? C26 C27 C32 C31 5.8(2) . . . . ? C26 C29 C30 C31 -3.1(2) . . . . ? C26 C29 C30 C36 -179.27(15) . . . . ? C26 C29 C33 C34 178.16(16) . . . . ? C27 C26 C29 C30 15.6(2) . . . . ? C27 C26 C29 C33 -159.95(16) . . . . ? C28 B1 O1 C43 -169.82(16) . . . . ? C28 B1 O2 C46 -169.38(15) . . . . ? C28 C22 C23 C24 174.21(15) . . . . ? C28 C27 C32 C31 -175.35(16) . . . . ? C29 C26 C27 C28 164.14(14) . . . . ? C29 C26 C27 C32 -17.1(2) . . . . ? C29 C30 C31 C32 -8.8(2) . . . . ? C29 C30 C36 C35 2.5(3) . . . . ? C29 C33 C34 C35 -0.8(3) . . . . ? C30 C29 C33 C34 2.5(3) . . . . ? C30 C31 C32 C27 7.5(3) . . . . ? C31 C30 C36 C35 -173.71(16) . . . . ? C32 C27 C28 B1 14.9(2) . . . . ? C32 C27 C28 C22 -171.72(15) . . . . ? C33 C29 C30 C31 172.87(15) . . . . ? C33 C29 C30 C36 -3.3(2) . . . . ? C33 C34 C35 C5 -179.02(17) . . . . ? C33 C34 C35 C36 -0.2(3) . . . . ? C34 C35 C36 C30 -0.7(3) . . . . ? C36 C30 C31 C32 167.51(16) . . . . ? C37 C25 C26 C27 -172.55(14) . . . . ? C37 C25 C26 C29 8.9(2) . . . . ? C37 C38 C39 C40 1.3(3) . . . . ? C38 C37 C42 C41 0.9(2) . . . . ? C38 C39 C40 C41 0.6(3) . . . . ? C38 C39 C40 Cl1 178.77(14) . . . . ? C39 C40 C41 C42 -1.6(3) . . . . ? C40 C41 C42 C37 0.8(3) . . . . ? C42 C37 C38 C39 -2.0(2) . . . . ? C43 C46 O2 B1 -24.94(18) . . . . ? C44 C43 C46 C47 162.38(17) . . . . ? C44 C43 C46 C48 34.0(2) . . . . ? C44 C43 C46 O2 -83.74(18) . . . . ? C44 C43 O1 B1 93.69(16) . . . . ? C45 C43 C46 C47 34.4(2) . . . . ? C45 C43 C46 C48 -94.0(2) . . . . ? C45 C43 C46 O2 148.29(16) . . . . ? C45 C43 O1 B1 -147.47(15) . . . . ? C46 C43 O1 B1 -25.11(17) . . . . ? C47 C46 O2 B1 93.57(17) . . . . ? C48 C46 O2 B1 -147.67(16) . . . . ? Cl1 C40 C41 C42 -179.80(15) . . . . ? O1 B1 C28 C22 67.9(2) . . . . ? O1 B1 C28 C27 -118.88(18) . . . . ? O1 B1 O2 C46 10.2(2) . . . . ? O1 C43 C46 C47 -83.86(18) . . . . ? O1 C43 C46 C48 147.77(16) . . . . ? O1 C43 C46 O2 30.02(17) . . . . ? O2 B1 C28 C22 -112.55(19) . . . . ? O2 B1 C28 C27 60.6(2) . . . . ? O2 B1 O1 C43 10.63(19) . . . . ? C6B C5 C35 C34 -134.1(7) . . . . ? C6B C5 C35 C36 47.2(8) . . . . ? C7B C5 C35 C34 102.9(8) . . . . ? C7B C5 C35 C36 -75.9(8) . . . . ? C8B C5 C35 C34 -8.4(8) . . . . ? C8B C5 C35 C36 172.9(8) . . . . ? _shelx_res_file ; TITL 039wps22_ws_a.res in P2/c 039wps22_sq.res created by SHELXL-2018/3 at 01:32:54 on 04-Dec-2022 REM Old TITL 039wps22_ws_a.res in P2/c REM SHELXT solution in P2/c: R1 0.191, Rweak 0.010, Alpha 0.030 REM 0.296 for 795 systematic absences, Orientation as input REM Formula found by SHELXT: C44 B O2 Cl CELL 1.54184 27.0823 6.1137 24.9379 90 105.412 90 ZERR 4 0.0009 0.0002 0.0007 0 0.003 0 LATT 1 SYMM -X,+Y,0.5-Z SFAC C H B Cl O UNIT 192 192 4 4 8 SADI C6A C7A C7A C8A C8A C6A C6B C7B C7B C8B C8B C6B FLAT C9B C10B C11B C12B C13 C14 FLAT C9A C10A C11A C12A C13 C14 SIMU 0.01 0.02 2 C1B C1A C3A C2B C2A C4B C4A C3B SIMU 0.01 0.02 2 C12A C12B C11A C11B C10A C10B C9A C9B C13 C14 RIGU C12A C11A C9A C10A C13 C14 SADI 0.01 C7B C5 C7A C5 C6B C5 C6A C5 C8B C5 C8A C5 RIGU C12B C11B C10B C9B C13 C14 SADI C35 C6A C35 C6B C35 C7A C35 C7B C35 C8A C35 C8B SIMU 0.01 0.02 2 C8A C7B C7A C6B C6A C8B C5 RIGU C8B C8A C7B C7A C6B C6A C5 RIGU C1B C4B C3B C2B RIGU C1A C2A C4A C3A SIMU 0.01 0.02 2 C1B C1A C4A C4B C2A C2B C3A C3B SADI C14 C1B C14 C1A SADI C14 C10A C14 C10B C9A C11A C9B C11B C10A C12A C10B C12B C11A C11B C12A = C14 C12B C14 C13 C9A C13 C9B SADI C10A C1A C10B C1B SADI C2A C3A C3A C4A C4A C2A C2B C3B C3B C4B C4B C2B SADI 0.01 C14 C13 C13 C12A C13 C12B C12A C11A C12B C11B C11A C10A C11B C10B = C9A C10A C9B C10B C9A C14 C9B C14 SADI 0.01 C2B C1B C3A C1A C3B C1B C4A C1A C4B C1B C2A C1A SADI C9A C2A C9A C3A C9A C4A C9B C2B C9B C3B C9B C4B L.S. 40 0 2 PLAN 8 SIZE 0.46 0.06 0.01 TEMP -123.14(10) CONF BOND MORE -1 BOND $H ABIN fmap 2 53 acta SHEL 99 0.82 REM REM REM WGHT 0.065600 0.350200 FVAR 0.33522 0.65357 0.89051 B1 3 0.544765 0.073367 0.139454 11.00000 0.03119 0.02679 = 0.02880 0.00318 0.00996 0.00237 PART 1 C1A 1 0.935848 0.885710 0.066014 -21.00000 0.05507 0.08334 = 0.06397 0.01941 0.03143 -0.01736 C2A 1 0.896107 1.027801 0.026108 -21.00000 0.06664 0.09409 = 0.07483 0.03320 0.03467 -0.01530 AFIX 137 H2AA 2 0.886444 1.150090 0.046625 -21.00000 -1.50000 H2AB 2 0.865719 0.939728 0.009215 -21.00000 -1.50000 H2AC 2 0.910665 1.084729 -0.003115 -21.00000 -1.50000 AFIX 0 C3A 1 0.982956 1.023045 0.093059 -21.00000 0.07146 0.10753 = 0.08722 0.01737 0.02801 -0.03374 AFIX 137 H3AA 2 0.998654 1.076138 0.064352 -21.00000 -1.50000 H3AB 2 1.007716 0.933224 0.119888 -21.00000 -1.50000 H3AC 2 0.972739 1.147941 0.112299 -21.00000 -1.50000 AFIX 0 C4A 1 0.951359 0.700753 0.031903 -21.00000 0.08150 0.10364 = 0.07620 0.01804 0.04878 -0.00787 AFIX 137 H4AA 2 0.961241 0.763444 0.000098 -21.00000 -1.50000 H4AB 2 0.922345 0.601156 0.018487 -21.00000 -1.50000 H4AC 2 0.980369 0.619887 0.055403 -21.00000 -1.50000 AFIX 0 PART 2 C1B 1 0.937407 0.915736 0.072159 21.00000 0.04773 0.08029 = 0.06465 0.01664 0.02273 -0.01686 C2B 1 0.936301 1.161123 0.083485 21.00000 0.08863 0.08149 = 0.12285 0.03371 0.04759 -0.01438 AFIX 137 H2BA 2 0.951762 1.240556 0.057896 21.00000 -1.50000 H2BB 2 0.955677 1.191221 0.121915 21.00000 -1.50000 H2BC 2 0.900754 1.208938 0.077905 21.00000 -1.50000 AFIX 0 C4B 1 0.905770 0.863153 0.013167 21.00000 0.08306 0.15986 = 0.05696 0.01637 0.03354 -0.04247 AFIX 137 H4BA 2 0.871162 0.922810 0.007379 21.00000 -1.50000 H4BB 2 0.903802 0.704202 0.007956 21.00000 -1.50000 H4BC 2 0.922041 0.928701 -0.013695 21.00000 -1.50000 AFIX 0 C3B 1 0.993157 0.849260 0.077047 21.00000 0.06820 0.10655 = 0.10103 0.03054 0.05020 -0.00749 AFIX 137 H3BA 2 1.004916 0.919780 0.047367 21.00000 -1.50000 H3BB 2 0.995219 0.690055 0.073607 21.00000 -1.50000 H3BC 2 1.014888 0.895555 0.113283 21.00000 -1.50000 AFIX 0 PART 0 C5 1 0.740030 -0.423556 0.459394 11.00000 0.04575 0.03915 = 0.03034 0.00951 0.00944 0.00256 PART 1 C6A 1 0.794444 -0.515624 0.466987 31.00000 0.05103 0.05610 = 0.04328 0.01835 0.00244 0.00918 AFIX 137 H6AA 2 0.805335 -0.592316 0.502700 31.00000 -1.50000 H6AB 2 0.818176 -0.395218 0.466374 31.00000 -1.50000 H6AC 2 0.794418 -0.617871 0.436714 31.00000 -1.50000 AFIX 0 C7A 1 0.704677 -0.617708 0.462141 31.00000 0.06331 0.04475 = 0.03211 0.01265 0.01170 -0.00339 AFIX 137 H7AA 2 0.704859 -0.720911 0.432125 31.00000 -1.50000 H7AB 2 0.669730 -0.564359 0.457938 31.00000 -1.50000 H7AC 2 0.716915 -0.691573 0.498111 31.00000 -1.50000 AFIX 0 C8A 1 0.738444 -0.265485 0.505346 31.00000 0.10013 0.04611 = 0.02668 0.00332 0.01790 0.00329 AFIX 137 H8AA 2 0.747530 -0.342349 0.541115 31.00000 -1.50000 H8AB 2 0.703858 -0.204699 0.498697 31.00000 -1.50000 H8AC 2 0.762914 -0.146704 0.506081 31.00000 -1.50000 AFIX 0 C9A 1 0.915209 0.794232 0.113577 21.00000 0.04017 0.06310 = 0.05254 0.00945 0.01504 -0.00918 C10A 1 0.947643 0.705712 0.162234 21.00000 0.03600 0.08691 = 0.06482 0.01876 0.01133 -0.01035 AFIX 43 H10A 2 0.983683 0.712519 0.167661 21.00000 -1.20000 AFIX 0 C11A 1 0.928276 0.608989 0.202358 21.00000 0.03911 0.09094 = 0.05450 0.01837 0.00260 -0.00413 AFIX 43 H11A 2 0.951026 0.548515 0.234695 21.00000 -1.20000 AFIX 0 C12A 1 0.875906 0.599467 0.195815 21.00000 0.03773 0.07461 = 0.03944 0.01702 0.00808 -0.00512 AFIX 43 H12A 2 0.862938 0.534418 0.223893 21.00000 -1.20000 AFIX 0 PART 2 C9B 1 0.915579 0.785385 0.114030 -21.00000 0.03972 0.06528 = 0.05329 0.01063 0.01855 -0.01041 C10B 1 0.946555 0.651915 0.154673 -21.00000 0.03575 0.07550 = 0.06312 0.01532 0.01765 -0.00648 AFIX 43 H10B 2 0.981957 0.638532 0.156720 -21.00000 -1.20000 AFIX 0 C11B 1 0.926406 0.538477 0.192135 -21.00000 0.03837 0.07723 = 0.05660 0.02102 0.00921 -0.00592 AFIX 43 H11B 2 0.948162 0.453647 0.220772 -21.00000 -1.20000 AFIX 0 C12B 1 0.874141 0.549644 0.187528 -21.00000 0.03758 0.07233 = 0.04372 0.01942 0.01325 -0.00796 AFIX 43 H12B 2 0.860012 0.463874 0.211561 -21.00000 -1.20000 AFIX 0 PART 0 C13 1 0.842086 0.685209 0.148057 11.00000 0.03752 0.04778 = 0.03366 0.00360 0.01132 -0.00518 C14 1 0.863148 0.789719 0.109266 11.00000 0.04001 0.04538 = 0.03730 0.00448 0.01265 -0.00836 PART 1 AFIX 43 H14 2 0.840621 0.861015 0.078486 21.00000 -1.20000 AFIX 43 PART 2 H14A 2 0.841121 0.865474 0.078941 -21.00000 -1.20000 AFIX 0 PART 0 C15 1 0.785977 0.682423 0.140771 11.00000 0.03700 0.03761 = 0.02184 0.00072 0.01054 -0.00216 C16 1 0.762382 0.507606 0.159656 11.00000 0.03379 0.03447 = 0.02221 0.00264 0.00968 0.00348 AFIX 43 H16 2 0.783123 0.390151 0.177911 11.00000 -1.20000 AFIX 0 C17 1 0.709344 0.496651 0.152996 11.00000 0.03248 0.02898 = 0.02144 -0.00075 0.01011 0.00176 C18 1 0.678728 0.660178 0.118987 11.00000 0.03659 0.02838 = 0.02226 0.00076 0.01102 0.00310 C19 1 0.702853 0.842580 0.102425 11.00000 0.04196 0.02919 = 0.02575 0.00168 0.01076 0.00300 AFIX 43 H19 2 0.682433 0.958198 0.082721 11.00000 -1.20000 AFIX 0 C20 1 0.754961 0.856838 0.114077 11.00000 0.04151 0.03140 = 0.02674 0.00195 0.01310 -0.00387 AFIX 43 H20 2 0.770375 0.984809 0.104156 11.00000 -1.20000 AFIX 0 C21 1 0.683026 0.324766 0.176585 11.00000 0.03109 0.02560 = 0.02377 0.00080 0.01069 0.00335 C22 1 0.629580 0.292043 0.150986 11.00000 0.03137 0.02934 = 0.02355 -0.00036 0.00970 0.00334 C23 1 0.601904 0.449030 0.111044 11.00000 0.02998 0.03578 = 0.02411 0.00277 0.00576 0.00309 AFIX 43 H23 2 0.566856 0.423215 0.092882 11.00000 -1.20000 AFIX 0 C24 1 0.624604 0.631216 0.098925 11.00000 0.03513 0.03232 = 0.02429 0.00452 0.00659 0.00689 AFIX 43 H24 2 0.604404 0.741961 0.076760 11.00000 -1.20000 AFIX 0 C25 1 0.706741 0.201526 0.224933 11.00000 0.02822 0.02467 = 0.02428 -0.00029 0.00892 0.00360 C26 1 0.678693 0.038301 0.244796 11.00000 0.02936 0.02560 = 0.02338 -0.00085 0.00981 0.00416 C27 1 0.629080 -0.019305 0.211126 11.00000 0.02925 0.02958 = 0.02454 0.00068 0.01072 0.00171 C28 1 0.603669 0.114441 0.166345 11.00000 0.03022 0.03091 = 0.02516 -0.00154 0.00885 0.00293 C29 1 0.696280 -0.075737 0.298805 11.00000 0.02968 0.02746 = 0.02511 0.00225 0.01092 0.00504 C30 1 0.670131 -0.268308 0.308009 11.00000 0.03028 0.02824 = 0.02685 0.00208 0.01190 0.00476 C31 1 0.626029 -0.343620 0.266683 11.00000 0.03228 0.02782 = 0.03391 0.00163 0.01478 -0.00120 AFIX 43 H31 2 0.611575 -0.482313 0.270644 11.00000 -1.20000 AFIX 0 C32 1 0.605028 -0.217715 0.222168 11.00000 0.02903 0.03181 = 0.02735 -0.00085 0.00843 -0.00144 AFIX 43 H32 2 0.573463 -0.261162 0.197384 11.00000 -1.20000 AFIX 0 C33 1 0.735427 -0.002049 0.344596 11.00000 0.03783 0.03064 = 0.02764 0.00349 0.00967 -0.00134 AFIX 43 H33 2 0.753112 0.129099 0.341061 11.00000 -1.20000 AFIX 0 C34 1 0.748881 -0.114095 0.394337 11.00000 0.03977 0.03694 = 0.02453 0.00242 0.00619 -0.00034 AFIX 43 H34 2 0.775838 -0.058434 0.423762 11.00000 -1.20000 AFIX 0 C35 1 0.724133 -0.307805 0.403075 11.00000 0.03927 0.03287 = 0.02734 0.00435 0.01349 0.00724 C36 1 0.685224 -0.380934 0.359130 11.00000 0.03306 0.02835 = 0.03200 0.00539 0.01522 0.00325 AFIX 43 H36 2 0.667897 -0.512216 0.363417 11.00000 -1.20000 AFIX 0 C37 1 0.760947 0.244150 0.256086 11.00000 0.02955 0.03090 = 0.02266 0.00596 0.01079 0.00190 C38 1 0.774789 0.440348 0.284517 11.00000 0.03410 0.03315 = 0.02733 0.00337 0.01221 -0.00017 AFIX 43 H38 2 0.749761 0.551608 0.281833 11.00000 -1.20000 AFIX 0 C39 1 0.824306 0.476366 0.316606 11.00000 0.04258 0.04306 = 0.03167 0.00250 0.00715 -0.00899 AFIX 43 H39 2 0.833205 0.609548 0.336447 11.00000 -1.20000 AFIX 0 C40 1 0.860524 0.314694 0.319193 11.00000 0.02900 0.06076 = 0.04039 0.01318 -0.00111 -0.00484 C41 1 0.848481 0.120526 0.290262 11.00000 0.03399 0.05163 = 0.04526 0.01389 0.00949 0.01106 AFIX 43 H41 2 0.874054 0.012641 0.291741 11.00000 -1.20000 AFIX 0 C42 1 0.798519 0.085591 0.259053 11.00000 0.03476 0.03375 = 0.03253 0.00571 0.01065 0.00580 AFIX 43 H42 2 0.789798 -0.048188 0.239442 11.00000 -1.20000 AFIX 0 C43 1 0.467314 0.034329 0.076556 11.00000 0.02818 0.03540 = 0.03733 0.00505 0.00664 0.00093 C44 1 0.452922 0.261819 0.053034 11.00000 0.03589 0.04013 = 0.04755 0.00872 0.00597 0.00485 AFIX 137 H44A 2 0.464136 0.280400 0.019045 11.00000 -1.50000 H44B 2 0.469661 0.371591 0.080514 11.00000 -1.50000 H44C 2 0.415687 0.280186 0.044372 11.00000 -1.50000 AFIX 0 C45 1 0.440546 -0.136996 0.035226 11.00000 0.04297 0.04465 = 0.04191 0.00231 0.00430 -0.00578 AFIX 137 H45A 2 0.403829 -0.136160 0.032788 11.00000 -1.50000 H45B 2 0.454813 -0.281468 0.047513 11.00000 -1.50000 H45C 2 0.445653 -0.104362 -0.001401 11.00000 -1.50000 AFIX 0 C46 1 0.461672 0.005475 0.136726 11.00000 0.03011 0.03849 = 0.04031 0.00205 0.01084 -0.00070 C47 1 0.459994 -0.233411 0.153429 11.00000 0.03844 0.04066 = 0.04686 0.00716 0.01433 -0.00146 AFIX 137 H47A 2 0.426358 -0.295176 0.135064 11.00000 -1.50000 H47B 2 0.465877 -0.243505 0.193860 11.00000 -1.50000 H47C 2 0.486667 -0.315297 0.142114 11.00000 -1.50000 AFIX 0 C48 1 0.418282 0.131005 0.150116 11.00000 0.03843 0.04970 = 0.06289 0.00425 0.02487 0.00532 AFIX 137 H48A 2 0.422000 0.287166 0.143221 11.00000 -1.50000 H48B 2 0.419238 0.108770 0.189296 11.00000 -1.50000 H48C 2 0.385506 0.078374 0.126500 11.00000 -1.50000 AFIX 0 CL1 4 0.923138 0.361794 0.358452 11.00000 0.03964 0.10249 = 0.08482 0.01327 -0.01908 -0.01134 O1 5 0.522976 0.014460 0.085388 11.00000 0.02870 0.03665 = 0.03019 0.00112 0.00783 0.00166 O2 5 0.510294 0.093710 0.170165 11.00000 0.03232 0.04033 = 0.03450 -0.00191 0.01289 -0.00076 PART 2 C6B 1 0.747055 -0.666225 0.457986 -31.00000 0.05179 0.05594 = 0.02676 0.01070 0.01341 0.00407 AFIX 137 H6BA 2 0.777355 -0.699029 0.444974 -31.00000 -1.50000 H6BB 2 0.716753 -0.732238 0.432628 -31.00000 -1.50000 H6BC 2 0.751656 -0.726233 0.495434 -31.00000 -1.50000 AFIX 0 C7B 1 0.698877 -0.370190 0.491128 -31.00000 0.06295 0.06061 = 0.03312 0.01725 0.01681 0.00726 AFIX 137 H7BA 2 0.708997 -0.436501 0.528221 -31.00000 -1.50000 H7BB 2 0.665662 -0.429317 0.470364 -31.00000 -1.50000 H7BC 2 0.696173 -0.211296 0.494692 -31.00000 -1.50000 AFIX 0 C8B 1 0.789350 -0.321432 0.498604 -31.00000 0.05705 0.05734 = 0.04163 0.02686 0.00156 -0.00345 AFIX 137 H8BA 2 0.798648 -0.402129 0.533817 -31.00000 -1.50000 H8BB 2 0.782890 -0.167938 0.505824 -31.00000 -1.50000 H8BC 2 0.817480 -0.330106 0.480791 -31.00000 -1.50000 AFIX 0 HKLF 4 REM 039wps22_ws_a.res in P2/c REM wR2 = 0.1281, GooF = S = 1.033, Restrained GooF = 1.050 for all data REM R1 = 0.0453 for 5578 Fo > 4sig(Fo) and 0.0674 for all 7584 data REM 586 parameters refined using 651 restraints END WGHT 0.0656 0.3525 REM Highest difference peak 0.247, deepest hole -0.216, 1-sigma level 0.041 Q1 1 0.5821 0.1045 0.1534 11.00000 0.05 0.25 Q2 1 0.7455 -0.5952 0.4607 11.00000 0.05 0.23 Q3 1 0.6197 0.0270 0.1829 11.00000 0.05 0.21 Q4 1 0.6539 -0.0087 0.2239 11.00000 0.05 0.21 Q5 1 0.7004 0.4257 0.1625 11.00000 0.05 0.19 Q6 1 0.7366 0.2233 0.2422 11.00000 0.05 0.18 Q7 1 0.6993 0.2223 0.2021 11.00000 0.05 0.18 Q8 1 0.6189 0.3584 0.1361 11.00000 0.05 0.17 ; _shelx_res_checksum 42789 _shelx_hkl_file ; 0 0 -3 -0.72 1.02 0 0 -3 0.64 1.50 0 0 -3 2.16 2.00 0 0 -3 0.80 1.27 0 0 -4 5144.10 31.83 0 0 -4 5264.99 22.01 0 0 -4 5214.38 36.08 0 0 -4 5104.37 37.92 0 0 -4 5021.49 42.94 0 0 -5 -1.87 1.66 0 0 -5 -0.42 0.91 0 0 -5 0.56 2.54 0 0 -5 3.02 3.12 0 0 -6 860.97 16.33 0 0 -6 830.28 10.75 0 0 -6 830.03 19.55 0 0 -7 0.07 2.05 0 0 -7 -1.08 1.01 0 0 -7 2.49 4.03 0 0 -7 -0.63 3.43 0 0 -8 340.22 12.12 0 0 -8 355.95 8.08 0 0 -8 362.37 17.31 0 0 -9 1.00 2.22 0 0 -9 3.48 4.77 0 0 -9 0.66 0.86 0 0 -10 220.80 4.59 0 0 -10 237.10 11.28 0 0 -10 255.90 12.88 0 0 -10 260.31 17.09 0 0 -10 237.58 7.17 0 0 -11 0.35 2.16 0 0 -11 -0.04 3.46 0 0 -11 0.98 0.86 0 0 -11 0.09 5.31 0 0 -12 60.08 7.65 0 0 -12 62.73 10.67 0 0 -13 0.59 4.24 0 0 -13 3.13 5.60 0 0 -14 8.23 4.43 0 0 -14 7.23 5.85 0 0 -15 1.93 4.61 0 0 -15 -2.79 5.65 0 0 -16 406.17 21.75 0 0 -16 370.54 27.87 0 0 -17 -1.35 3.41 0 0 -17 4.72 5.88 0 0 -18 10.59 2.28 0 0 -18 7.62 2.83 0 0 -18 10.14 4.76 0 0 -18 11.38 3.20 0 0 -18 6.35 2.48 0 0 -18 12.45 7.90 0 0 -18 7.41 2.48 0 0 -19 1.84 2.27 0 0 -19 -2.24 3.10 0 0 -19 -4.23 4.05 0 0 -19 -0.14 1.95 0 0 -19 -0.44 1.90 0 0 -19 2.16 3.01 0 0 -19 -0.46 1.96 0 0 -19 -1.72 2.53 0 0 -20 247.09 13.68 0 0 -20 247.24 12.42 0 0 -20 219.41 9.59 0 0 -20 247.45 19.71 0 0 -20 242.55 13.25 0 0 -20 220.48 11.21 0 0 -20 238.42 9.23 0 0 -20 245.60 11.67 0 0 -21 -2.71 2.32 0 0 -21 7.99 3.92 0 0 -21 0.60 3.13 0 0 -21 3.35 2.35 0 0 -21 3.22 3.00 0 0 -21 1.55 3.15 0 0 -22 2.03 2.07 0 0 -22 1.24 3.74 0 0 -22 6.41 2.74 0 0 -22 3.96 2.68 0 0 -22 -3.56 2.27 0 0 -22 3.46 3.22 0 0 -23 3.60 3.63 0 0 -23 0.10 3.30 0 0 -23 1.19 1.85 0 0 -23 -4.11 2.74 0 0 -24 16.94 4.77 0 0 -24 7.51 4.26 0 0 -24 11.80 2.27 0 0 -24 9.97 3.00 0 0 -25 -2.81 3.73 0 0 -25 1.79 1.92 0 0 -25 -0.41 2.50 0 0 -26 27.51 3.85 0 0 -26 35.21 5.50 0 0 -26 34.90 3.35 0 0 -26 25.06 3.68 0 0 -27 -4.31 2.86 0 0 -27 1.49 2.34 0 0 -27 -0.53 1.49 0 0 -28 123.55 6.44 0 0 -28 103.05 4.36 0 0 -29 -1.71 1.67 0 0 -29 1.38 1.80 0 0 -30 3.89 1.31 0 0 -30 1.28 1.39 0 -1 0 171.36 6.18 0 -1 0 153.60 6.11 0 -1 -1 121.36 6.04 0 -1 1 124.24 4.47 0 1 -1 108.56 5.17 0 -1 1 106.88 5.00 0 1 -1 107.13 4.98 0 -1 2 14.19 1.25 0 -1 -2 14.43 3.48 0 -1 2 8.86 1.74 0 1 -2 10.24 2.19 0 1 -2 7.80 2.83 0 1 -2 7.08 2.30 0 -1 3 1430.48 15.84 0 1 -3 1434.27 17.38 0 -1 -3 1416.91 14.40 0 1 -3 1431.61 23.29 0 1 -3 1454.14 24.22 0 1 -4 42.54 3.20 0 -1 4 41.68 2.70 0 -1 -4 23.50 4.34 0 -1 -4 24.17 4.62 0 -1 -4 43.26 3.51 0 1 -4 42.72 5.69 0 -1 5 35.57 2.37 0 1 -5 37.15 1.67 0 -1 -5 44.61 5.22 0 -1 -5 39.10 5.51 0 1 -5 39.02 2.15 0 -1 -5 34.38 3.99 0 1 -5 28.69 5.11 0 -1 6 1929.49 14.20 0 -1 -6 1838.43 34.23 0 -1 -6 1837.00 28.52 0 1 -6 1913.20 36.91 0 -1 -6 1838.51 31.20 0 1 -7 861.49 26.78 0 -1 -7 819.73 21.24 0 1 -7 847.59 23.95 0 1 -7 817.92 20.33 0 -1 -7 835.92 24.51 0 -1 -7 844.22 22.53 0 -1 -8 4.03 4.40 0 1 -8 6.33 4.17 0 1 -8 5.89 5.18 0 -1 -8 2.16 2.90 0 1 -8 4.21 3.15 0 -1 -9 176.34 11.59 0 -1 -9 177.43 12.00 0 1 -9 182.92 14.64 0 1 -9 190.56 13.46 0 1 -9 188.17 11.15 0 -1 -10 187.76 12.37 0 -1 -10 190.01 13.29 0 1 -10 181.33 16.00 0 1 -10 185.56 13.94 0 1 -10 202.96 12.38 0 -1 -11 1190.92 31.66 0 -1 -11 1182.92 34.59 0 1 -11 1244.20 40.97 0 1 -11 1300.61 36.82 0 1 -11 1229.24 31.09 0 -1 -12 422.41 19.92 0 1 -12 457.25 23.15 0 1 -12 426.25 25.80 0 -1 -12 412.08 21.88 0 1 -12 444.50 19.88 0 -1 -13 -0.14 3.71 0 -1 -13 -0.49 3.93 0 1 -13 -0.89 4.64 0 1 -13 -0.09 5.54 0 1 -13 0.55 3.90 0 -1 -14 40.60 7.08 0 1 -14 35.67 9.55 0 -1 -14 30.94 7.24 0 1 -14 49.12 7.72 0 -1 -15 -4.94 4.92 0 1 -15 7.36 7.70 0 -1 -15 -1.67 4.40 0 1 -15 3.69 4.04 0 -1 -16 5.75 4.03 0 1 -16 4.04 7.24 0 -1 -16 -2.47 5.48 0 1 -16 0.76 4.06 0 -1 -16 -1.65 4.30 0 1 -17 24.87 8.72 0 -1 -17 39.75 7.94 0 1 -17 40.99 8.68 0 1 -18 -2.27 1.64 0 -1 -18 1.63 2.57 0 -1 -18 3.90 3.27 0 1 -18 -0.10 1.82 0 1 -18 0.75 4.07 0 -1 -18 2.13 2.27 0 -1 -18 1.31 2.17 0 1 -18 -0.90 2.33 0 1 -18 -1.50 1.67 0 -1 -18 -2.52 1.64 0 1 -18 1.72 2.07 0 1 -18 -0.68 2.30 0 -1 -18 -0.90 3.38 0 -1 -19 7.85 3.53 0 1 -19 11.77 2.75 0 -1 -19 5.41 3.31 0 1 -19 8.56 4.92 0 1 -19 9.66 2.66 0 -1 -19 9.04 3.18 0 -1 -19 12.06 2.97 0 1 -19 8.19 3.68 0 -1 -19 10.55 2.55 0 1 -19 8.82 2.82 0 -1 -19 9.73 2.97 0 1 -19 13.46 3.40 0 1 -19 9.09 3.45 0 -1 -19 11.95 3.75 0 1 -19 8.53 2.97 0 -1 -20 7.22 3.23 0 1 -20 9.35 2.50 0 1 -20 11.59 2.62 0 -1 -20 10.33 2.48 0 -1 -20 9.03 3.58 0 -1 -20 8.70 2.79 0 1 -20 7.46 3.34 0 -1 -20 16.03 6.23 0 1 -20 12.08 5.21 0 1 -20 14.85 3.47 0 -1 -20 15.27 3.90 0 1 -20 11.17 3.19 0 1 -20 13.93 3.62 0 -1 -20 14.64 4.13 0 1 -20 10.31 3.62 0 -1 -21 44.34 6.28 0 1 -21 48.91 4.46 0 1 -21 43.67 4.79 0 1 -21 53.13 4.85 0 1 -21 38.12 5.56 0 -1 -21 46.65 6.73 0 1 -21 51.33 6.10 0 -1 -21 47.41 6.18 0 1 -21 46.39 6.52 0 -1 -21 43.83 5.33 0 -1 -21 49.19 5.60 0 1 -21 44.57 5.38 0 -1 -21 50.67 4.85 0 -1 -22 63.43 5.18 0 1 -22 77.83 6.73 0 -1 -22 75.01 6.76 0 1 -22 70.39 5.62 0 1 -22 66.43 5.83 0 1 -22 75.52 7.08 0 -1 -22 79.14 5.60 0 -1 -22 65.11 6.33 0 1 -22 71.50 7.99 0 1 -22 74.08 5.38 0 -1 -22 71.64 7.68 0 -1 -22 70.33 7.98 0 1 -22 68.32 7.13 0 -1 -23 -0.98 3.10 0 1 -23 0.73 1.96 0 1 -23 -4.11 2.62 0 1 -23 0.40 1.91 0 1 -23 7.26 3.93 0 -1 -23 -3.38 3.78 0 1 -23 -0.72 3.34 0 1 -23 3.49 4.16 0 -1 -23 0.63 2.30 0 -1 -23 1.95 2.67 0 1 -23 0.58 2.53 0 -1 -24 60.60 5.10 0 1 -24 63.06 6.68 0 1 -24 58.07 4.86 0 -1 -24 53.68 7.17 0 1 -24 53.64 5.17 0 1 -24 70.11 7.89 0 1 -24 57.18 5.99 0 1 -24 56.82 5.18 0 1 -24 60.80 5.40 0 1 -25 92.49 5.87 0 1 -25 100.51 5.96 0 1 -25 86.80 7.07 0 -1 -25 82.39 6.21 0 -1 -25 97.47 5.28 0 1 -25 92.42 5.40 0 -1 -25 101.26 9.00 0 -1 -26 23.39 3.57 0 1 -26 20.58 3.51 0 1 -26 18.50 2.67 0 1 -26 29.11 4.31 0 -1 -26 29.21 3.08 0 1 -26 21.73 2.76 0 -1 -26 22.15 4.97 0 -1 -27 0.93 2.53 0 1 -27 3.65 2.23 0 -1 -27 4.41 1.58 0 1 -27 4.82 1.72 0 1 -27 6.50 1.51 0 -1 -27 0.52 2.16 0 1 -27 5.32 2.74 0 1 -28 -1.36 2.12 0 -1 -28 -2.22 2.08 0 1 -28 0.56 1.74 0 -1 -28 0.51 1.89 0 -1 -28 0.22 1.05 0 1 -29 11.54 2.29 0 -1 -29 8.03 1.75 0 -1 -30 0.42 1.29 0 2 0 1.45 3.28 0 -2 0 1.65 2.46 0 2 -1 350.70 13.08 0 2 1 349.15 13.21 0 -2 1 311.04 11.21 0 -2 -1 310.90 13.01 0 2 2 48.16 5.40 0 2 -2 55.28 5.66 0 2 -2 50.04 6.00 0 -2 -2 40.35 5.85 0 2 -3 650.94 18.88 0 2 -3 624.90 19.87 0 -2 -3 656.68 20.98 0 2 -3 650.79 17.13 0 -2 -3 678.89 21.62 0 2 -4 4.08 3.81 0 2 -4 3.51 3.56 0 -2 -4 2.53 4.11 0 2 -4 0.04 2.74 0 -2 -4 5.99 4.08 0 2 -5 63.19 7.70 0 2 -5 66.96 8.03 0 -2 -5 62.01 7.99 0 2 -5 57.40 5.38 0 2 -5 58.76 4.66 0 -2 -5 67.59 8.37 0 -2 -6 26.32 6.58 0 2 -6 18.72 5.88 0 2 -6 15.54 5.39 0 2 -6 24.13 2.91 0 -2 -6 17.59 5.61 0 -2 -7 -1.87 4.73 0 2 -7 -3.69 5.45 0 2 -7 0.68 4.44 0 2 -7 0.21 0.84 0 2 -8 219.50 16.75 0 2 -8 219.00 15.44 0 -2 -8 216.72 14.85 0 2 -9 49.34 8.88 0 2 -9 45.83 8.88 0 -2 -9 39.20 7.60 0 -2 -10 -0.04 4.65 0 2 -10 7.10 5.94 0 2 -10 0.65 5.78 0 2 10 5.62 3.20 0 -2 -11 339.31 20.29 0 2 -11 339.25 23.74 0 2 -11 328.47 20.84 0 2 11 343.80 14.55 0 2 -12 6.24 4.92 0 2 -12 1.49 5.49 0 -2 -12 3.34 5.02 0 -2 -13 7.99 5.43 0 2 -13 7.74 7.12 0 2 -13 8.86 5.68 0 2 -13 6.20 4.64 0 -2 -14 9.72 5.27 0 2 -14 6.99 7.10 0 2 -14 5.09 4.73 0 2 -14 5.71 3.93 0 2 -15 53.86 10.22 0 2 -15 46.89 11.05 0 -2 -15 64.22 10.41 0 -2 -16 44.89 5.49 0 2 -16 47.63 4.08 0 2 -16 46.64 4.83 0 -2 -16 41.04 5.11 0 -2 -16 43.60 8.54 0 2 -17 8.57 3.10 0 2 -17 5.74 2.03 0 2 -17 7.66 2.31 0 2 -17 4.65 1.88 0 -2 -17 9.31 3.61 0 2 -17 8.22 2.26 0 -2 -17 8.23 3.17 0 2 -17 4.66 2.90 0 -2 -17 9.10 1.91 0 2 -17 10.86 3.74 0 -2 -17 13.00 3.60 0 -2 -17 2.69 1.73 0 2 -17 10.00 3.33 0 -2 -18 109.86 7.49 0 2 -18 107.41 8.49 0 2 -18 116.85 6.79 0 2 -18 101.03 6.78 0 -2 -18 116.81 14.21 0 -2 -18 105.59 9.25 0 -2 -18 123.06 9.47 0 2 -18 106.65 6.47 0 2 -18 115.10 7.56 0 2 -18 113.27 7.90 0 2 -18 102.96 8.80 0 -2 -18 111.87 8.55 0 -2 -18 106.15 5.83 0 -2 -19 25.75 3.09 0 2 -19 24.48 3.39 0 -2 -19 25.58 5.14 0 -2 -19 25.74 4.37 0 2 -19 20.61 4.53 0 2 -19 27.58 3.88 0 2 -19 29.51 4.06 0 -2 -19 41.54 8.82 0 -2 -19 19.21 4.42 0 2 -19 28.79 4.63 0 2 -19 24.95 3.68 0 -2 -19 20.80 3.44 0 2 -19 26.88 4.79 0 2 -19 24.29 3.48 0 2 -20 14.78 3.02 0 -2 -20 15.03 4.50 0 2 -20 13.86 4.15 0 -2 -20 11.53 3.60 0 2 -20 14.94 3.09 0 2 -20 11.72 3.24 0 -2 -20 14.85 4.37 0 2 -20 15.63 4.11 0 -2 -20 16.61 3.23 0 2 -20 11.26 3.46 0 2 -20 8.42 3.19 0 2 -20 9.75 2.54 0 -2 -21 3.51 3.58 0 2 -21 1.05 1.94 0 2 -21 -1.64 3.24 0 -2 -21 3.46 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-2 -26 0.90 1.15 0 2 -26 3.28 2.66 0 -2 -26 0.40 2.17 0 -2 -27 1.03 1.36 0 -2 -27 -0.65 1.91 0 -2 -28 0.80 1.59 0 2 -28 5.87 2.07 0 -2 -29 1.61 1.46 0 3 0 496.79 19.79 0 -3 0 456.51 19.01 0 3 0 474.98 18.79 0 3 -1 343.57 16.34 0 3 1 345.91 16.49 0 -3 -1 309.89 16.48 0 -3 1 312.17 15.22 0 3 -1 322.15 16.11 0 3 2 9.55 4.07 0 3 -2 12.67 4.01 0 -3 2 13.01 3.48 0 -3 -2 18.15 5.02 0 3 -2 16.15 4.49 0 3 3 -0.65 4.20 0 3 -3 2.70 3.47 0 -3 3 0.83 2.50 0 -3 -3 0.83 3.58 0 3 -3 2.08 3.60 0 3 4 171.60 12.14 0 3 -4 181.72 11.87 0 -3 -4 149.68 13.15 0 -3 4 157.14 9.20 0 3 -4 155.61 12.66 0 3 -5 336.02 18.96 0 -3 -5 384.46 20.50 0 3 5 322.86 16.57 0 3 -5 337.32 15.78 0 3 -5 401.51 15.67 0 3 -6 12.80 5.59 0 -3 -6 16.13 6.38 0 3 6 11.80 4.53 0 3 -6 10.31 2.39 0 3 7 2.03 3.80 0 -3 -7 2.90 5.46 0 3 -7 2.52 3.97 0 3 8 25.92 5.41 0 -3 -8 19.23 7.57 0 3 -8 21.50 6.85 0 3 9 22.74 5.25 0 -3 -9 25.76 7.79 0 3 -9 20.51 7.12 0 3 10 117.38 10.40 0 -3 -10 138.56 14.87 0 3 -10 139.09 14.97 0 3 11 49.51 6.92 0 -3 -11 64.67 10.81 0 3 -11 51.73 9.41 0 3 12 40.90 6.24 0 3 -12 45.88 10.21 0 -3 -12 44.24 9.43 0 3 -13 3.08 4.75 0 -3 -13 11.32 6.10 0 3 -14 164.92 18.41 0 -3 -14 177.86 10.12 0 3 -14 181.07 10.52 0 3 -14 184.46 9.19 0 3 -14 164.85 6.99 0 -3 -14 175.31 10.40 0 3 -14 184.56 9.25 0 -3 -14 168.42 7.75 0 3 -14 167.55 8.69 0 -3 -14 179.08 18.47 0 3 -15 9.54 2.90 0 3 -15 11.61 3.39 0 3 -15 16.06 3.28 0 -3 -15 11.32 2.88 0 3 -15 8.28 2.94 0 3 -15 10.19 2.52 0 3 15 10.54 2.35 0 3 -15 9.34 2.13 0 -3 -15 11.69 3.06 0 3 -15 11.22 2.66 0 -3 -15 9.80 2.32 0 3 -15 9.34 5.71 0 -3 -15 15.32 6.27 0 3 -16 13.28 2.99 0 -3 -16 11.93 5.28 0 -3 -16 12.21 3.55 0 3 -16 11.39 2.39 0 -3 -16 7.55 2.75 0 3 -16 15.39 3.44 0 3 -16 11.86 3.57 0 -3 -16 15.73 3.87 0 3 -16 10.23 2.68 0 3 -16 13.05 2.99 0 -3 -16 12.70 2.43 0 3 -16 13.00 3.04 0 3 -17 6.51 2.89 0 -3 -17 4.50 4.72 0 3 -17 4.25 1.66 0 -3 -17 4.02 2.73 0 -3 -17 5.84 2.68 0 3 -17 8.03 2.72 0 3 -17 6.65 2.80 0 -3 -17 11.24 3.95 0 3 -17 1.79 2.57 0 3 -17 1.19 2.45 0 -3 -17 7.18 2.25 0 3 -17 4.66 2.83 0 3 -18 260.08 13.22 0 3 -18 248.69 9.23 0 -3 -18 239.61 12.80 0 -3 -18 243.89 13.24 0 3 -18 256.61 11.59 0 3 -18 260.89 11.30 0 3 -18 253.64 12.77 0 -3 -18 250.53 13.10 0 3 -18 242.35 11.37 0 3 -18 263.46 12.03 0 -3 -18 240.59 9.67 0 3 -19 4.68 2.19 0 -3 -19 6.58 3.69 0 3 -19 4.15 2.61 0 -3 -19 1.72 2.44 0 3 -19 4.41 3.05 0 -3 -19 5.25 1.96 0 3 -19 5.22 2.88 0 3 -19 5.31 2.44 0 3 -19 -0.63 3.07 0 3 -19 2.98 2.65 0 -3 -19 2.53 3.23 0 -3 -20 11.95 4.08 0 -3 -20 15.20 3.66 0 3 -20 17.33 3.86 0 3 -20 12.56 3.40 0 3 -20 15.68 4.03 0 -3 -20 13.75 2.56 0 3 -20 11.08 2.96 0 3 -20 9.63 3.49 0 3 -20 16.79 4.49 0 -3 -20 14.72 4.25 0 -3 -21 23.12 5.20 0 -3 -21 17.34 4.35 0 3 -21 28.89 4.45 0 3 -21 23.32 3.97 0 3 -21 20.70 4.11 0 3 -21 21.79 4.64 0 -3 -21 18.27 4.63 0 3 -21 25.00 4.71 0 3 -21 20.61 3.61 0 -3 -22 64.17 6.59 0 -3 -22 62.46 6.90 0 3 -22 70.54 6.15 0 3 -22 56.10 4.58 0 3 -22 68.46 6.08 0 3 -22 64.70 6.51 0 3 -22 67.32 6.74 0 -3 -22 59.45 6.60 0 3 -22 76.44 6.21 0 3 -23 4.46 2.92 0 3 -23 10.33 3.37 0 3 -23 6.94 2.01 0 3 -23 8.57 2.92 0 3 -23 5.17 3.12 0 -3 -23 1.01 2.90 0 -3 -23 2.84 2.59 0 3 -24 4.91 2.63 0 -3 -24 0.55 2.07 0 3 -24 3.45 2.75 0 3 -24 0.66 1.52 0 3 -24 2.58 2.58 0 -3 -24 3.31 2.37 0 3 -24 5.15 2.27 0 -3 -25 -0.11 1.55 0 3 -25 -1.15 1.88 0 -3 -25 -1.56 2.00 0 -3 -26 22.26 1.89 0 -3 -26 19.50 2.44 0 -3 -27 -4.44 1.63 0 -3 -28 1.20 1.20 0 -4 0 6.97 4.75 0 4 0 0.32 5.12 0 -4 -1 11.67 4.55 0 4 1 5.07 3.56 0 4 -1 12.12 4.85 0 4 -2 28.37 6.42 0 -4 -2 13.50 4.37 0 4 -2 21.21 5.91 0 4 2 17.14 4.69 0 4 -3 9.38 4.73 0 -4 -3 9.55 4.85 0 4 3 9.18 4.00 0 4 -3 8.05 4.19 0 -4 -4 76.72 11.13 0 4 -4 71.00 8.28 0 4 -4 92.09 11.08 0 4 -4 84.21 9.92 0 4 4 75.82 9.95 0 -4 -5 7.77 4.55 0 4 -5 3.75 2.71 0 4 -5 15.61 5.48 0 4 5 11.17 4.61 0 4 6 -2.68 4.46 0 4 -6 4.59 4.48 0 -4 -6 -0.48 4.33 0 4 7 29.87 6.44 0 4 -7 49.21 9.92 0 -4 -7 46.17 8.53 0 4 8 13.55 5.19 0 -4 -8 14.44 5.46 0 4 -8 18.88 6.35 0 4 9 16.16 2.64 0 4 -9 11.22 1.91 0 4 -9 18.59 3.25 0 -4 -9 17.00 6.98 0 4 -9 14.41 2.10 0 4 -9 16.06 6.00 0 4 9 13.94 4.73 0 4 10 0.84 1.62 0 4 -10 -0.56 1.33 0 4 -10 2.09 2.10 0 -4 -10 1.80 5.27 0 4 -10 5.48 2.63 0 -4 -10 1.48 2.18 0 4 -10 2.84 1.23 0 4 -10 -7.03 4.95 0 4 10 -0.83 3.85 0 4 11 84.92 5.78 0 4 -11 82.28 5.09 0 4 -11 81.29 5.08 0 4 -11 83.78 7.22 0 -4 -11 71.30 12.70 0 4 -11 82.12 6.36 0 -4 -11 82.11 6.99 0 4 -11 79.94 4.80 0 4 -11 79.81 12.42 0 4 11 76.78 9.65 0 4 -12 62.72 4.63 0 -4 -12 62.79 6.15 0 4 -12 58.89 4.37 0 4 -12 61.33 6.38 0 4 -12 63.39 5.96 0 4 -12 66.60 11.72 0 -4 -12 77.37 13.67 0 4 -12 56.42 3.99 0 4 12 64.83 5.29 0 4 -13 58.38 4.42 0 4 -13 64.01 12.04 0 4 -13 59.20 6.34 0 4 -13 55.71 5.49 0 -4 -13 58.13 6.34 0 4 13 58.06 5.01 0 -4 -13 60.43 11.94 0 4 -13 53.45 5.47 0 4 14 31.53 3.82 0 4 -14 30.77 3.55 0 -4 -14 28.48 4.38 0 4 -14 37.72 5.05 0 4 -14 31.47 4.70 0 -4 -14 35.18 4.16 0 4 -14 25.52 4.67 0 -4 -14 30.81 4.85 0 4 15 28.97 3.56 0 -4 -15 26.56 4.40 0 4 -15 25.70 3.19 0 4 -15 29.20 4.55 0 4 -15 33.54 4.28 0 4 -15 28.16 4.34 0 -4 -15 31.37 4.02 0 4 -15 23.56 4.55 0 -4 -15 21.81 4.34 0 4 16 -3.10 1.81 0 -4 -16 0.20 2.40 0 4 -16 0.64 1.73 0 4 -16 0.03 2.61 0 4 -16 0.68 1.87 0 4 -16 -1.95 3.06 0 -4 -16 -1.22 2.05 0 4 -16 -0.37 2.59 0 -4 -16 -4.11 2.95 0 4 17 3.44 1.85 0 4 -17 1.79 1.77 0 -4 -17 -1.14 2.75 0 4 -17 3.33 3.54 0 4 -17 3.76 2.12 0 4 -17 4.04 3.09 0 -4 -17 5.86 3.35 0 -4 -17 3.10 2.48 0 4 -17 3.69 2.91 0 4 -18 0.12 2.91 0 -4 -18 3.34 2.12 0 -4 -18 1.61 2.65 0 -4 -18 -0.98 2.88 0 4 -18 3.89 2.87 0 4 18 1.90 1.50 0 4 -18 6.58 2.12 0 4 -18 4.59 2.68 0 4 -18 -0.22 1.92 0 -4 -19 -2.23 3.13 0 -4 -19 1.90 1.77 0 4 -19 1.05 2.46 0 4 -19 0.25 1.68 0 4 -19 -0.26 2.78 0 4 -19 4.09 2.05 0 4 -20 4.83 2.40 0 4 -20 2.64 2.98 0 -4 -20 6.16 2.34 0 4 -20 8.95 3.04 0 -4 -20 2.13 2.95 0 4 -21 5.51 2.00 0 4 -21 4.02 2.21 0 -4 -21 0.20 2.94 0 4 -21 3.44 3.26 0 4 -22 1.91 1.84 0 4 -22 2.27 2.47 0 4 -22 -1.95 2.49 0 -4 -23 0.32 1.91 0 4 -23 -1.88 1.69 0 -4 -23 0.48 2.10 0 4 -24 3.00 1.42 0 -4 -24 1.01 1.69 0 -4 -24 -0.85 1.59 0 -4 -25 0.80 1.25 0 -4 -25 -0.98 1.31 0 -4 -26 -2.39 1.16 0 5 0 61.33 4.86 0 5 0 61.85 9.74 0 5 0 67.92 10.25 0 5 0 60.99 4.51 0 5 0 61.56 4.68 0 5 -1 34.84 6.87 0 5 -1 48.20 4.33 0 -5 -1 35.07 3.68 0 5 1 32.10 6.84 0 5 -1 38.42 3.62 0 5 1 39.96 3.96 0 5 -1 36.16 3.74 0 5 1 35.65 3.53 0 5 -2 3.59 3.28 0 5 -2 12.80 2.32 0 5 2 10.65 2.12 0 5 -2 15.32 2.74 0 -5 -2 9.59 2.11 0 5 2 14.94 2.72 0 5 2 12.37 4.80 0 5 -3 68.81 5.12 0 -5 -3 57.32 4.79 0 5 3 63.80 4.88 0 5 3 54.87 9.06 0 5 -3 60.90 4.76 0 5 3 53.05 4.43 0 5 -4 20.46 2.91 0 5 4 16.71 2.54 0 -5 -4 17.80 2.94 0 5 -4 20.96 3.10 0 5 4 21.55 3.20 0 5 4 17.49 6.06 0 -5 -5 53.11 4.87 0 5 -5 56.48 4.51 0 5 5 53.65 4.21 0 -5 -5 60.24 10.61 0 5 -5 66.41 5.10 0 5 5 56.91 9.42 0 5 5 63.01 5.04 0 5 -6 231.44 8.88 0 5 6 209.88 8.07 0 -5 -6 214.87 20.30 0 5 -6 228.31 9.14 0 5 6 242.03 18.79 0 5 6 229.38 9.61 0 5 -7 280.69 9.70 0 -5 -7 291.20 23.89 0 5 -7 287.04 10.20 0 5 7 288.26 10.59 0 5 -8 31.44 3.81 0 5 8 24.90 3.81 0 5 -8 33.99 4.13 0 5 -9 50.85 4.17 0 5 9 48.84 4.80 0 5 -9 42.36 4.82 0 5 -10 17.88 3.38 0 5 -10 22.04 2.96 0 5 -10 19.26 3.52 0 5 -10 21.73 2.92 0 5 10 21.60 3.37 0 5 -11 4.34 2.49 0 5 -11 4.31 2.31 0 5 -11 4.00 1.59 0 5 11 2.90 2.27 0 5 -11 2.23 1.71 0 5 12 62.76 5.30 0 -5 -12 58.77 5.75 0 -5 -12 55.89 5.40 0 5 -12 57.00 5.79 0 5 -12 60.16 4.34 0 5 -12 61.02 5.63 0 5 -12 53.02 4.19 0 5 -13 24.05 3.03 0 -5 -13 25.93 3.96 0 -5 -13 23.32 3.60 0 5 -13 26.13 4.26 0 5 -13 22.31 2.55 0 5 -13 22.66 3.97 0 5 13 27.07 3.73 0 5 -14 13.92 2.45 0 -5 -14 13.17 3.20 0 -5 -14 14.12 3.26 0 5 -14 13.52 3.56 0 5 -14 13.41 1.94 0 5 -14 12.22 2.98 0 5 14 15.09 3.00 0 -5 -15 14.23 3.16 0 -5 -15 14.69 2.99 0 5 -15 12.84 2.44 0 5 -15 9.31 3.29 0 5 -15 12.32 3.23 0 5 15 16.25 2.90 0 -5 -16 4.07 2.44 0 -5 -16 3.36 2.44 0 5 -16 3.22 1.65 0 5 -16 6.83 3.08 0 5 16 3.70 1.81 0 5 -16 2.27 2.56 0 5 17 -1.00 1.59 0 5 -17 -1.01 1.58 0 -5 -17 1.78 2.30 0 -5 -17 -1.49 2.06 0 5 -17 4.85 2.89 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4.17 1.79 0 6 -11 3.26 2.06 0 6 11 2.52 2.23 0 -6 -12 6.29 2.05 0 6 -12 8.70 1.89 0 6 -12 6.63 1.64 0 6 -12 4.76 1.91 0 6 12 6.94 2.30 0 6 -13 1.45 1.29 0 -6 -13 5.37 2.27 0 6 -13 5.51 2.16 0 6 13 3.51 1.89 0 6 -14 -2.62 1.37 0 6 -14 1.14 1.89 0 -6 -14 2.12 1.82 0 6 14 2.21 1.71 0 6 -15 6.88 2.21 0 -6 -15 4.93 1.77 0 6 15 5.41 1.67 0 6 -15 2.28 0.93 0 -6 -16 26.67 2.74 0 6 -16 18.29 2.41 0 -6 -16 21.87 2.51 0 6 16 25.25 2.38 0 -6 -17 19.33 2.14 0 6 -17 13.52 2.00 0 6 17 17.50 1.82 0 -6 -17 16.87 2.11 0 6 -18 0.41 1.10 0 -6 -18 0.56 0.90 0 7 0 -0.74 1.15 0 7 -1 0.78 1.19 0 7 1 -1.63 1.14 0 7 2 29.57 2.43 0 7 2 29.36 2.61 0 7 -2 30.20 2.82 0 7 3 0.85 1.05 0 7 -3 1.35 1.31 0 7 -4 3.12 1.29 0 7 4 5.13 1.45 0 7 -4 2.77 1.47 0 7 -5 1.67 1.08 0 7 -5 -0.57 1.26 0 7 5 -0.49 1.16 0 -7 -6 0.76 1.02 0 7 6 0.91 1.28 0 7 -6 2.48 1.11 0 -7 -7 1.43 1.00 0 7 7 -0.19 1.19 0 7 -7 2.57 1.00 0 7 8 10.96 1.84 0 -7 -8 10.35 1.50 0 7 9 17.46 2.05 0 -7 -9 16.10 1.75 0 7 10 9.66 1.58 0 -7 -10 8.37 1.32 0 7 11 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5.34 32 0 -9 3.30 1.98 32 0 -9 -0.22 2.32 32 0 -8 18.11 2.86 32 0 -8 17.13 3.34 32 0 -7 0.32 1.96 32 0 -7 2.45 2.63 32 0 -6 57.73 4.67 32 0 -6 56.26 5.23 32 0 -5 -1.81 2.00 32 0 -5 1.48 2.22 32 0 -4 2.08 2.02 32 0 -4 1.47 2.28 32 0 -3 1.44 1.96 32 0 -3 -0.40 2.09 32 0 -2 21.07 3.07 32 0 -2 21.43 3.44 32 0 -1 3.72 2.06 32 0 -1 1.06 1.92 32 0 0 37.72 3.50 32 0 0 35.16 3.52 32 0 1 -0.99 1.51 32 0 1 -2.19 1.77 32 0 2 8.34 1.85 32 0 2 4.56 1.64 32 1 -17 1.72 1.29 32 1 -16 8.99 1.72 32 -1 -16 12.85 2.02 32 1 -16 15.40 2.30 -32 1 15 2.64 1.02 32 1 -15 3.37 1.63 32 -1 -15 0.10 1.36 -32 1 14 1.39 1.13 32 1 -14 -1.86 1.87 32 -1 -14 -2.24 1.62 32 1 -14 1.49 1.70 32 1 -13 -0.14 1.67 32 -1 -13 -2.04 1.66 32 1 -13 2.44 2.06 32 1 -12 -1.14 1.79 32 -1 -12 0.66 1.67 32 1 -12 -0.22 2.06 32 -1 -11 -0.17 1.66 32 1 -11 0.98 2.08 32 -1 -10 -0.03 1.69 32 1 -10 -0.16 2.20 32 -1 -9 9.87 2.38 32 1 -9 8.89 2.60 32 -1 -8 0.22 2.24 32 -1 -8 1.90 1.96 32 1 -8 -4.37 2.40 32 -1 -7 4.68 2.45 32 1 -7 0.86 2.19 32 -1 -7 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-2 -0.22 1.34 33 0 -15 -0.41 1.29 33 0 -14 22.36 2.68 33 0 -13 -1.66 1.66 33 0 -12 6.12 2.06 33 0 -11 -2.06 1.93 33 0 -10 16.08 2.73 33 0 -9 -1.84 1.87 33 0 -8 57.17 4.51 33 0 -7 2.38 1.37 33 0 -7 0.08 1.90 33 0 -6 11.43 2.07 33 0 -6 10.80 2.50 33 0 -5 -2.04 1.60 33 0 -5 1.62 1.97 33 0 -4 14.19 2.24 33 0 -4 18.99 2.75 33 0 -3 -3.23 1.63 33 0 -3 2.12 1.68 33 0 -2 1.66 1.44 33 0 -2 5.68 1.93 33 0 -1 1.77 1.36 33 1 -14 1.60 1.34 -33 1 13 0.58 0.86 33 1 -13 0.32 1.35 -33 1 12 4.39 1.26 33 -1 -12 2.71 1.26 33 1 -12 5.34 1.77 33 1 -12 3.16 1.43 33 -1 -11 0.28 1.18 33 1 -11 -1.40 1.65 33 1 -11 -1.27 1.52 33 -1 -10 0.79 1.27 33 1 -10 2.28 1.79 33 -1 -9 2.91 1.55 33 1 -9 3.20 1.97 33 -1 -8 13.65 2.10 33 1 -8 12.61 2.51 33 -1 -7 4.34 1.46 33 1 -7 7.43 2.28 33 -1 -6 7.25 1.69 33 1 -6 12.02 2.54 33 -1 -6 12.66 2.39 33 1 -5 0.10 1.75 33 -1 -5 2.18 1.67 33 1 -4 3.54 1.89 33 -1 -4 -0.33 1.67 33 1 -3 1.80 1.56 33 -1 -3 6.38 1.89 33 1 -2 0.58 1.40 33 -1 -2 2.30 1.54 34 0 -10 7.71 1.73 34 0 -9 -1.83 1.44 34 0 -8 -1.45 1.35 34 0 -7 -2.33 1.47 0 0 0 0.00 0.00 TITL 039wps22_WS in P2/c REM P2/c (#13 in standard setting) CELL 1.54184 27.082265 6.113699 24.937874 90.0000 105.4116 90.0000 ZERR 4.00 0.000915 0.000165 0.000671 0.0000 0.0032 0.0000 LATT 1 SYMM -x, y,-z+1/2 SFAC C H B O Cl UNIT 192.00 192.00 4.00 8.00 4.00 REM CrysAlisPro recorded range (K): Min=150.0; max=150.0; aver:150.0 TEMP -123 TREF HKLF 4 END ; _shelx_hkl_checksum 21746 _shelx_fab_file ; 3 0 0 -0.10 0.00 4 0 0 3.01 0.00 5 0 0 -0.76 0.00 6 0 0 2.69 0.00 7 0 0 -0.29 0.00 8 0 0 2.05 0.00 9 0 0 -0.79 0.00 10 0 0 0.91 0.00 11 0 0 -0.93 0.00 12 0 0 0.84 0.00 13 0 0 -0.35 0.00 14 0 0 0.94 0.00 15 0 0 -0.33 0.00 16 0 0 0.56 0.00 17 0 0 -0.51 0.00 18 0 0 0.42 0.00 19 0 0 -0.47 0.00 20 0 0 0.29 0.00 21 0 0 -0.59 0.00 22 0 0 0.08 0.00 23 0 0 -0.53 0.00 24 0 0 0.17 0.00 25 0 0 -0.26 0.00 26 0 0 0.18 0.00 27 0 0 -0.29 0.00 28 0 0 -0.04 0.00 29 0 0 -0.34 0.00 30 0 0 -0.06 0.00 31 0 0 -0.18 0.00 0 1 0 1.99 0.00 1 1 0 4.66 0.00 2 1 0 0.94 0.00 3 1 0 2.95 0.00 4 1 0 -0.24 0.00 5 1 0 2.14 0.00 6 1 0 -0.14 0.00 7 1 0 1.86 0.00 8 1 0 -0.32 0.00 9 1 0 0.96 0.00 10 1 0 -0.74 0.00 11 1 0 0.56 0.00 12 1 0 -0.40 0.00 13 1 0 0.77 0.00 14 1 0 -0.15 0.00 15 1 0 0.56 0.00 16 1 0 -0.35 0.00 17 1 0 0.31 0.00 18 1 0 -0.32 0.00 19 1 0 0.34 0.00 20 1 0 -0.24 0.00 21 1 0 0.20 0.00 22 1 0 -0.32 0.00 23 1 0 0.05 0.00 24 1 0 -0.28 0.00 25 1 0 0.03 0.00 26 1 0 -0.22 0.00 27 1 0 -0.04 0.00 28 1 0 -0.22 0.00 29 1 0 -0.06 0.00 30 1 0 -0.14 0.00 31 1 0 -0.01 0.00 0 2 0 1.34 0.00 1 2 0 0.83 0.00 2 2 0 1.18 0.00 3 2 0 0.62 0.00 4 2 0 0.97 0.00 5 2 0 0.48 0.00 6 2 0 0.78 0.00 7 2 0 0.25 0.00 8 2 0 0.43 0.00 9 2 0 -0.06 0.00 10 2 0 0.18 0.00 11 2 0 -0.11 0.00 12 2 0 0.23 0.00 13 2 0 0.00 0.00 14 2 0 0.23 0.00 15 2 0 -0.03 0.00 16 2 0 0.11 0.00 17 2 0 -0.06 0.00 18 2 0 0.10 0.00 19 2 0 0.08 0.00 20 2 0 0.19 0.00 21 2 0 0.19 0.00 22 2 0 0.13 0.00 23 2 0 0.08 0.00 24 2 0 -0.11 0.00 25 2 0 -0.12 0.00 26 2 0 -0.23 0.00 27 2 0 -0.08 0.00 28 2 0 -0.08 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23 0.00 0.00 -19 4 23 0.06 0.00 13 0 24 -0.03 0.00 11 2 24 -0.08 0.00 -22 3 24 0.01 0.00 8 3 24 -0.23 0.00 -17 4 24 0.24 0.00 3 4 24 0.01 0.00 -25 1 25 -0.17 0.00 9 2 25 -0.08 0.00 6 3 25 -0.15 0.00 -14 4 25 0.11 0.00 -1 4 25 0.01 0.00 0 4 25 0.16 0.00 -22 2 26 -0.05 0.00 7 2 26 0.19 0.00 -18 3 26 -0.07 0.00 3 3 26 -0.03 0.00 -22 1 27 0.06 0.00 -20 2 27 -0.03 0.00 -15 3 27 -0.09 0.00 0 3 27 -0.07 0.00 -21 0 28 0.03 0.00 -20 1 28 0.05 0.00 4 1 28 -0.11 0.00 1 2 28 0.03 0.00 -10 3 28 0.09 0.00 -9 3 28 -0.14 0.00 -8 3 28 0.03 0.00 -7 3 28 -0.10 0.00 -6 3 28 0.04 0.00 -17 1 29 0.07 0.00 1 1 29 0.04 0.00 -14 2 29 0.10 0.00 -13 2 29 -0.12 0.00 -4 2 29 0.15 0.00 -3 2 29 -0.17 0.00 -15 0 30 0.09 0.00 -14 0 30 -0.07 0.00 -3 0 30 -0.09 0.00 -13 1 30 -0.05 0.00 -12 1 30 0.05 0.00 -5 1 30 -0.34 0.00 -4 1 30 -0.12 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 90622) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.069 0.250 38 2 ' ' 2 0.000 -0.070 0.750 37 2 ' ' 3 0.121 0.111 0.604 11 0 ' ' 4 0.879 0.111 0.896 10 0 ' ' 5 0.500 0.417 0.250 15 1 ' ' 6 0.500 0.582 0.750 15 1 ' ' 7 0.121 0.889 0.104 11 0 ' ' 8 0.879 0.889 0.396 10 0 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 0 0 1.692 2 0 0 3.386 0 0 2 3.677 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL 039wps22 P 1 2/c 1 R = 0.05 CELL 27.0823 6.1137 24.9379 90.00 105.41 90.00 SPGR P2/c # Solvent Accessible Volume = 148 # Electrons Found in S.A.V. = 6 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.500 0.406 0.248 ! 1.18 eA-3 ) ; _shelx_fab_checksum 99339 _platon_squeeze_details ? _platon_squeeze_special_details ? loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.069 0.250 38 2 ' ' 2 0.000 -0.070 0.750 37 2 ' ' 3 0.121 0.111 0.604 11 0 ' ' 4 0.879 0.111 0.896 10 0 ' ' 5 0.500 0.417 0.250 15 1 ' ' 6 0.500 0.582 0.750 15 1 ' ' 7 0.121 0.889 0.104 11 0 ' ' 8 0.879 0.889 0.396 10 0 ' ' _platon_squeeze_void_probe_radius 1.20 loop_ _hkl_oxdiff_h _hkl_oxdiff_k _hkl_oxdiff_l _hkl_oxdiff_f2 _hkl_oxdiff_sig _hkl_oxdiff_ba 0 0 -3 -71.6116 102.090 1 0 0 -3 63.9630 149.571 30 0 0 -3 215.567 199.819 29 0 0 -3 79.5327 126.632 6 0 0 -4 514461. 3183.51 1 0 0 -4 526551. 2201.55 7 0 0 -4 521490. 3608.81 6 0 0 -4 510488. 3792.66 30 0 0 -4 502199. 4294.66 29 0 0 -5 -187.327 166.195 1 0 0 -5 -42.1242 91.4344 7 0 0 -5 56.0159 254.516 30 0 0 -5 301.964 312.446 29 0 0 -6 86105.6 1633.28 1 0 0 -6 83036.0 1075.22 7 0 0 -6 83011.0 1954.91 30 0 0 -7 7.27749 205.071 1 0 0 -7 -107.709 101.485 7 0 0 -7 248.620 402.840 29 0 0 -7 -63.3404 343.148 30 0 0 -8 34025.5 1212.27 1 0 0 -8 35598.5 808.329 7 0 0 -8 36240.2 1731.47 29 0 0 -9 99.8439 222.093 1 0 0 -9 348.443 477.402 29 0 0 -9 65.6969 86.0250 7 0 0 -10 22081.9 459.175 2 0 0 -10 23712.6 1128.47 1 0 0 -10 25592.2 1288.04 8 0 0 -10 26033.7 1708.97 29 0 0 -10 23760.1 717.066 7 0 0 -11 35.3264 216.469 1 0 0 -11 -3.71225 345.568 8 0 0 -11 98.1016 86.3724 7 0 0 -11 9.43130 530.811 29 0 0 -12 6008.47 765.414 8 0 0 -12 6273.24 1067.46 29 0 0 -13 59.0076 424.266 8 0 0 -13 313.309 560.257 29 0 0 -14 822.648 442.873 8 0 0 -14 722.849 584.897 29 0 0 -15 192.626 461.236 8 0 0 -15 -278.899 565.173 29 0 0 -16 40620.6 2175.47 8 0 0 -16 37057.2 2787.44 29 0 0 -17 -134.601 340.853 8 0 0 -17 471.919 588.364 29 0 0 -18 1059.09 228.511 15 0 0 -18 762.077 282.991 31 0 0 -18 1013.68 476.076 8 0 0 -18 1137.95 319.776 18 0 0 -18 635.104 248.036 20 0 0 -18 1245.60 790.566 29 0 0 -18 741.430 247.645 35 0 0 -19 184.251 226.993 18 0 0 -19 -223.711 309.949 20 0 0 -19 -422.629 405.182 8 0 0 -19 -14.3115 194.550 9 0 0 -19 -43.7846 190.435 35 0 0 -19 216.190 301.036 31 0 0 -19 -46.4499 196.114 15 0 0 -19 -171.883 253.240 22 0 0 -20 24711.3 1367.66 20 0 0 -20 24726.1 1241.77 22 0 0 -20 21943.1 959.229 9 0 0 -20 24747.6 1971.57 8 0 0 -20 24257.6 1324.64 31 0 0 -20 22050.1 1121.49 18 0 0 -20 23843.9 923.527 15 0 0 -20 24562.7 1166.91 35 0 0 -21 -270.722 231.593 9 0 0 -21 799.558 391.550 18 0 0 -21 59.6747 312.620 20 0 0 -21 334.713 234.591 15 0 0 -21 322.369 300.426 22 0 0 -21 155.111 315.067 31 0 0 -22 203.412 207.450 9 0 0 -22 123.577 373.890 20 0 0 -22 640.896 274.058 15 0 0 -22 395.846 267.835 22 0 0 -22 -355.825 226.808 21 0 0 -22 346.332 322.035 31 0 0 -23 359.716 362.968 31 0 0 -23 9.89870 330.173 20 0 0 -23 118.854 184.963 21 0 0 -23 -411.153 274.139 15 0 0 -24 1693.99 476.876 31 0 0 -24 751.327 426.529 20 0 0 -24 1179.92 226.780 21 0 0 -24 997.418 299.537 15 0 0 -25 -281.249 373.325 20 0 0 -25 179.436 192.031 21 0 0 -25 -41.0219 250.066 15 0 0 -26 2750.79 385.529 36 0 0 -26 3521.11 550.217 20 0 0 -26 3490.27 334.568 21 0 0 -26 2505.93 368.515 15 0 0 -27 -431.119 286.239 36 0 0 -27 148.965 233.824 15 0 0 -27 -53.3808 149.180 21 0 0 -28 12356.1 644.232 36 0 0 -28 10306.3 436.428 21 0 0 -29 -170.730 167.459 36 0 0 -29 137.800 179.690 15 0 0 -30 388.861 130.973 36 0 0 -30 128.496 139.333 15 0 -1 0 17138.1 618.071 6 0 -1 0 15361.5 611.010 28 0 -1 -1 12136.8 604.145 6 0 -1 1 12425.7 446.724 6 0 1 -1 10857.0 517.330 26 0 -1 1 10689.5 499.839 28 0 1 -1 10713.7 498.123 29 0 -1 2 1418.95 124.933 6 0 -1 -2 1443.06 348.352 6 0 -1 2 886.174 173.628 28 0 1 -2 1024.41 219.066 26 0 1 -2 780.090 283.302 30 0 1 -2 708.418 230.303 29 0 -1 3 143062. 1584.60 28 0 1 -3 143441. 1738.62 26 0 -1 -3 141705. 1440.17 29 0 1 -3 143175. 2329.44 30 0 1 -3 145428. 2421.86 29 0 1 -4 4253.94 320.346 26 0 -1 4 4168.34 269.864 28 0 -1 -4 2350.12 434.237 1 0 -1 -4 2416.87 462.200 6 0 -1 -4 4325.99 350.735 29 0 1 -4 4272.59 569.486 29 0 -1 5 3557.73 236.562 28 0 1 -5 3715.13 166.661 25 0 -1 -5 4461.10 521.749 1 0 -1 -5 3910.75 551.550 6 0 1 -5 3902.53 214.603 5 0 -1 -5 3437.87 398.644 29 0 1 -5 2869.00 511.098 29 0 -1 6 192968. 1420.26 28 0 -1 -6 183861. 3423.80 6 0 -1 -6 183718. 2852.56 29 0 1 -6 191339. 3691.51 29 0 -1 -6 183869. 3119.95 1 0 1 -7 86157.2 2678.49 29 0 -1 -7 81981.4 2124.20 29 0 1 -7 84767.5 2395.35 30 0 1 -7 81800.1 2033.59 8 0 -1 -7 83599.8 2450.76 6 0 -1 -7 84430.4 2252.95 1 0 -1 -8 403.239 440.016 1 0 1 -8 633.452 417.525 30 0 1 -8 588.922 517.852 29 0 -1 -8 216.114 289.720 29 0 1 -8 421.200 315.437 8 0 -1 -9 17635.7 1159.05 1 0 -1 -9 17744.8 1200.31 29 0 1 -9 18294.2 1463.71 29 0 1 -9 19058.0 1346.17 30 0 1 -9 18818.6 1115.47 8 0 -1 -10 18777.5 1237.04 1 0 -1 -10 19002.9 1329.20 29 0 1 -10 18134.6 1599.76 29 0 1 -10 18557.5 1394.35 30 0 1 -10 20297.9 1238.02 8 0 -1 -11 119104. 3166.24 1 0 -1 -11 118304. 3459.16 29 0 1 -11 124432. 4097.86 29 0 1 -11 130074. 3682.05 30 0 1 -11 122936. 3109.70 8 0 -1 -12 42245.5 1991.76 1 0 1 -12 45729.2 2315.39 30 0 1 -12 42629.2 2580.74 29 0 -1 -12 41212.1 2188.29 29 0 1 -12 44454.7 1988.08 8 0 -1 -13 -13.5384 371.233 1 0 -1 -13 -48.6524 392.640 29 0 1 -13 -88.6205 464.273 30 0 1 -13 -8.85003 553.674 29 0 1 -13 55.1725 389.594 8 0 -1 -14 4060.04 708.522 1 0 1 -14 3567.23 954.696 29 0 -1 -14 3094.04 724.339 29 0 1 -14 4912.20 772.410 8 0 -1 -15 -493.872 492.313 1 0 1 -15 735.681 770.022 29 0 -1 -15 -167.260 439.918 29 0 1 -15 368.933 404.008 8 0 -1 -16 574.938 402.560 1 0 1 -16 404.041 723.802 29 0 -1 -16 -247.258 547.821 29 0 1 -16 76.3406 406.417 8 0 -1 -16 -164.548 430.475 8 0 1 -17 2487.27 872.118 29 0 -1 -17 3975.25 794.058 8 0 1 -17 4099.80 868.345 8 0 1 -18 -227.052 164.427 21 0 -1 -18 163.300 257.380 22 0 -1 -18 390.420 326.564 8 0 1 -18 -9.91894 181.907 9 0 1 -18 75.1777 407.156 8 0 -1 -18 213.341 227.102 31 0 -1 -18 130.784 217.279 32 0 1 -18 -89.7610 233.066 31 0 1 -18 -149.552 166.580 15 0 -1 -18 -252.476 163.568 35 0 1 -18 172.323 207.373 20 0 1 -18 -68.2439 229.697 18 0 -1 -18 -89.8958 337.575 20 0 -1 -19 784.713 353.313 22 0 1 -19 1177.53 275.236 21 0 -1 -19 540.741 331.282 8 0 1 -19 856.173 492.034 8 0 1 -19 965.785 265.705 9 0 -1 -19 903.965 318.393 31 0 -1 -19 1206.44 297.129 32 0 1 -19 818.881 368.023 31 0 -1 -19 1054.90 254.945 15 0 1 -19 881.655 281.599 15 0 -1 -19 972.661 297.470 35 0 1 -19 1345.98 339.670 34 0 1 -19 908.616 345.215 18 0 -1 -19 1195.14 375.311 20 0 1 -19 853.324 297.192 20 0 -1 -20 722.398 323.022 22 0 1 -20 934.810 250.362 21 0 1 -20 1158.97 262.225 15 0 -1 -20 1033.33 248.087 15 0 -1 -20 903.055 357.617 31 0 -1 -20 870.266 279.107 32 0 1 -20 745.652 333.882 31 0 -1 -20 1603.46 623.509 8 0 1 -20 1208.58 520.827 8 0 1 -20 1484.98 347.016 9 0 -1 -20 1526.94 389.726 35 0 1 -20 1117.55 319.340 34 0 1 -20 1392.79 361.730 20 0 -1 -20 1464.57 413.437 20 0 1 -20 1031.21 361.762 18 0 -1 -21 4434.39 627.840 22 0 1 -21 4891.13 445.770 21 0 1 -21 4367.73 479.092 9 0 1 -21 5313.57 485.122 15 0 1 -21 3812.05 556.518 20 0 -1 -21 4665.56 673.040 20 0 1 -21 5133.58 609.668 18 0 -1 -21 4741.63 618.363 31 0 1 -21 4639.21 652.279 31 0 -1 -21 4383.69 533.534 32 0 -1 -21 4919.13 559.656 35 0 1 -21 4457.54 538.486 34 0 -1 -21 5067.13 484.835 15 0 -1 -22 6343.15 517.644 11 0 1 -22 7784.15 673.371 34 0 -1 -22 7502.14 676.200 35 0 1 -22 7039.52 562.351 15 0 1 -22 6643.25 583.373 9 0 1 -22 7553.15 708.065 18 0 -1 -22 7914.76 559.644 15 0 -1 -22 6511.69 632.997 32 0 1 -22 7150.58 799.352 31 0 1 -22 7409.05 538.058 21 0 -1 -22 7164.74 767.929 22 0 -1 -22 7033.62 798.397 20 0 1 -22 6832.89 712.804 20 0 -1 -23 -97.7393 309.914 22 0 1 -23 73.3649 195.528 21 0 1 -23 -411.071 262.451 9 0 1 -23 39.5100 191.391 34 0 1 -23 726.093 393.221 18 0 -1 -23 -337.919 378.405 20 0 1 -23 -71.8024 333.972 20 0 1 -23 348.896 416.476 31 0 -1 -23 63.4419 229.682 32 0 -1 -23 194.654 266.801 15 0 1 -23 57.9560 252.560 15 0 -1 -24 6060.51 510.397 15 0 1 -24 6306.76 667.568 20 0 1 -24 5807.76 485.604 21 0 -1 -24 5368.57 717.558 20 0 1 -24 5364.19 517.008 15 0 1 -24 7011.95 789.253 31 0 1 -24 5718.43 599.365 36 0 1 -24 5682.52 518.282 9 0 1 -24 6080.52 539.562 34 0 1 -25 9249.91 587.432 9 0 1 -25 10052.2 596.337 15 0 1 -25 8680.38 706.678 36 0 -1 -25 8239.40 620.850 15 0 -1 -25 9748.01 528.122 21 0 1 -25 9243.29 540.294 21 0 -1 -25 10127.5 899.782 20 0 -1 -26 2339.24 357.028 15 0 1 -26 2058.06 351.180 15 0 1 -26 1849.89 266.727 9 0 1 -26 2910.97 430.945 36 0 -1 -26 2920.92 308.194 21 0 1 -26 2173.26 276.229 21 0 -1 -26 2215.50 497.078 20 0 -1 -27 93.2823 253.146 15 0 1 -27 364.629 223.441 15 0 -1 -27 440.731 158.160 21 0 1 -27 481.818 172.329 21 0 1 -27 650.324 151.273 9 0 -1 -27 52.0793 216.399 36 0 1 -27 532.385 274.406 36 0 1 -28 -136.093 212.038 36 0 -1 -28 -222.028 207.738 36 0 1 -28 55.7111 174.319 15 0 -1 -28 50.6330 189.340 15 0 -1 -28 21.6360 105.175 21 0 1 -29 1153.76 228.781 36 0 -1 -29 803.499 175.076 36 0 -1 -30 41.7402 129.349 15 0 2 0 145.338 328.079 26 0 -2 0 165.074 246.345 6 0 2 -1 35073.5 1307.86 26 0 2 1 34918.1 1321.29 26 0 -2 1 31107.4 1121.57 6 0 -2 -1 31093.1 1301.60 6 0 2 2 4816.77 540.042 26 0 2 -2 5528.56 566.071 26 0 2 -2 5004.71 600.189 30 0 -2 -2 4035.18 585.493 6 0 2 -3 65100.7 1888.32 29 0 2 -3 62496.2 1986.94 30 0 -2 -3 65674.1 2097.96 1 0 2 -3 65085.7 1712.79 26 0 -2 -3 67895.4 2162.60 6 0 2 -4 408.436 380.907 30 0 2 -4 351.295 356.209 29 0 -2 -4 252.643 411.048 1 0 2 -4 3.57199 274.264 26 0 -2 -4 599.267 407.553 6 0 2 -5 6319.43 770.247 30 0 2 -5 6696.67 802.981 29 0 -2 -5 6201.34 799.252 1 0 2 -5 5740.47 537.613 26 0 2 -5 5876.15 466.255 5 0 -2 -5 6759.58 837.396 6 0 -2 -6 2632.35 658.130 1 0 2 -6 1872.46 588.204 30 0 2 -6 1553.96 539.243 29 0 2 -6 2413.08 291.435 5 0 -2 -6 1759.61 560.647 6 0 -2 -7 -186.959 473.478 1 0 2 -7 -369.465 544.970 29 0 2 -7 68.1291 443.965 30 0 2 -7 21.0859 83.9267 5 0 2 -8 21952.0 1674.97 29 0 2 -8 21902.1 1543.89 30 0 -2 -8 21673.9 1485.32 1 0 2 -9 4934.90 887.825 30 0 2 -9 4583.37 888.082 29 0 -2 -9 3920.34 759.651 1 0 -2 -10 -4.36883 465.085 1 0 2 -10 709.863 593.980 30 0 2 -10 65.3670 577.715 29 0 2 10 562.103 319.991 26 0 -2 -11 33933.9 2029.28 1 0 2 -11 33928.0 2374.53 29 0 2 -11 32850.0 2084.57 30 0 2 11 34383.0 1455.01 26 0 2 -12 624.261 492.424 29 0 2 -12 149.042 549.115 30 0 -2 -12 334.070 502.035 1 0 -2 -13 798.621 543.260 1 0 2 -13 774.297 711.965 29 0 2 -13 886.533 568.017 30 0 2 -13 620.393 463.684 8 0 -2 -14 972.554 526.587 1 0 2 -14 699.079 709.816 29 0 2 -14 509.389 473.301 30 0 2 -14 570.794 392.636 8 0 2 -15 5386.16 1022.55 30 0 2 -15 4689.75 1105.60 29 0 -2 -15 6422.76 1041.48 1 0 -2 -16 4489.57 549.335 22 0 2 -16 4763.10 408.006 21 0 2 -16 4664.53 483.413 9 0 -2 -16 4104.26 510.911 32 0 -2 -16 4360.37 853.609 1 0 2 -17 856.804 310.455 9 0 2 -17 573.947 203.093 15 0 2 -17 765.972 231.413 12 0 2 -17 465.428 187.874 23 0 -2 -17 931.327 361.182 22 0 2 -17 821.719 225.551 21 0 -2 -17 823.222 317.490 20 0 2 -17 466.080 289.750 18 0 -2 -17 910.128 190.829 38 0 2 -17 1086.21 373.742 31 0 -2 -17 1299.66 359.886 32 0 -2 -17 269.444 172.653 35 0 2 -17 1000.38 333.297 34 0 -2 -18 10987.4 748.690 35 0 2 -18 10742.5 848.839 34 0 2 -18 11686.0 678.592 15 0 2 -18 10104.1 677.952 12 0 -2 -18 11682.1 1421.46 1 0 -2 -18 10560.3 925.023 20 0 -2 -18 12307.4 947.240 22 0 2 -18 10666.3 647.157 21 0 2 -18 11510.7 755.665 9 0 2 -18 11328.6 790.570 18 0 2 -18 10296.6 880.391 31 0 -2 -18 11188.2 855.177 32 0 -2 -18 10616.3 582.731 38 0 -2 -19 2575.24 309.387 38 0 2 -19 2447.77 339.002 21 0 -2 -19 2557.80 513.704 22 0 -2 -19 2574.49 436.903 32 0 2 -19 2060.84 453.528 31 0 2 -19 2758.20 387.797 15 0 2 -19 2951.23 406.202 9 0 -2 -19 4154.91 881.837 8 0 -2 -19 1921.19 442.033 20 0 2 -19 2878.93 462.971 18 0 2 -19 2495.10 367.978 36 0 -2 -19 2080.21 344.391 35 0 2 -19 2688.27 478.645 34 0 2 -19 2429.30 348.515 12 0 2 -20 1478.61 302.117 21 0 -2 -20 1503.32 450.243 22 0 2 -20 1385.99 414.814 31 0 -2 -20 1152.96 359.561 32 0 2 -20 1493.80 308.713 15 0 2 -20 1171.64 324.232 9 0 -2 -20 1485.58 436.909 20 0 2 -20 1563.43 411.185 18 0 -2 -20 1661.28 323.111 35 0 2 -20 1126.47 345.563 36 0 2 -20 842.553 319.468 34 0 2 -20 975.144 254.223 12 0 -2 -21 351.050 358.329 22 0 2 -21 105.100 193.779 21 0 2 -21 -164.515 323.841 31 0 -2 -21 345.585 314.419 32 0 2 -21 394.384 248.891 15 0 2 -21 -3.94559 264.856 9 0 2 -21 795.664 377.945 18 0 -2 -21 -329.233 412.226 20 0 2 -21 -21.4952 328.561 36 0 2 -21 419.611 284.494 34 0 -2 -21 241.854 243.555 35 0 2 -21 227.538 174.945 12 0 -2 -22 2474.62 554.265 22 0 2 -22 2359.62 342.359 21 0 2 -22 3108.48 615.063 31 0 -2 -22 2872.75 490.689 32 0 2 -22 3275.98 436.629 15 0 -2 -22 2385.27 373.029 15 0 2 -22 2239.38 406.127 9 0 2 -22 3114.36 497.631 18 0 -2 -22 2547.86 525.520 20 0 2 -22 2382.14 422.240 36 0 2 -22 2875.71 463.061 34 0 -2 -22 2499.94 397.271 35 0 2 -22 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894.943 6 -4 3 -2 3193.10 563.489 5 -4 -3 -2 2330.12 646.687 6 -4 3 -2 2667.07 644.055 30 -4 3 -3 111.015 305.009 5 -4 -3 -3 72.2801 421.637 6 -4 3 -3 465.841 438.645 30 -4 -3 -4 -288.000 462.050 6 -4 3 -4 227.488 270.675 5 -4 3 -4 -74.7050 469.655 30 -4 3 -5 7961.63 767.503 5 -4 -3 -5 6805.15 1073.56 6 -4 3 -5 7871.85 1095.78 30 -4 -3 -6 -79.4925 587.029 1 -4 -3 -6 726.739 477.905 6 -4 3 -6 1067.19 321.997 5 -4 3 -6 1121.09 569.213 30 -4 -3 -7 9856.51 1224.01 1 -4 -3 -7 9647.02 1286.06 6 -4 3 -7 10793.1 836.090 5 -4 3 -7 11096.9 1327.89 30 -4 -3 -8 6643.21 1086.18 1 -4 -3 -8 6904.44 1103.46 6 -4 3 -8 6459.57 1025.20 30 -4 -3 -9 7600.72 1155.85 1 -4 -3 -9 6913.88 1179.44 6 -4 3 -9 7944.12 1204.43 30 -4 -3 -10 656.038 560.026 1 -4 3 -10 274.377 597.584 30 -4 -3 -11 4595.78 965.705 1 -4 3 -11 4547.36 996.668 30 -4 -3 -12 6963.61 522.433 38 -4 3 -12 6469.35 577.266 36 -4 3 -12 5725.06 454.383 21 4 3 12 5264.76 817.508 26 -4 3 -12 6786.16 1246.11 30 -4 -3 -12 6452.21 620.768 32 -4 3 -12 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523.456 32 4 4 -23 6010.33 453.382 12 4 4 -23 5687.85 444.229 18 4 4 -22 58.3635 218.974 18 4 -4 -22 -143.275 214.055 22 4 -4 -22 230.608 273.676 32 4 4 -22 374.502 211.226 31 4 4 -22 -230.478 257.274 12 4 -4 -22 92.1650 118.102 38 4 4 -21 2387.26 376.452 18 4 4 -21 2316.71 378.974 31 4 -4 -21 1706.25 403.814 32 4 -4 -21 2156.51 398.339 22 4 4 -21 1396.30 279.000 12 4 -4 -21 2023.94 270.270 38 4 4 -20 5254.84 508.031 12 4 -4 -20 5132.95 541.293 22 4 4 -20 5579.40 509.024 18 4 4 -20 5705.25 625.958 34 4 -4 -20 5862.51 647.886 32 4 4 -20 5591.16 528.763 31 4 4 -20 5229.07 441.022 23 4 -4 -20 5691.99 451.188 38 -4 4 19 -129.670 157.294 24 4 -4 -19 158.861 182.013 38 4 4 -19 -231.676 227.148 18 4 -4 -19 -175.733 254.248 22 4 4 -19 -117.908 191.115 23 4 -4 -19 68.5308 295.823 32 4 4 -19 245.186 299.894 12 4 4 -19 148.785 335.187 34 -4 4 18 1005.30 231.634 24 4 -4 -18 1027.58 250.390 38 4 4 -18 966.277 323.591 18 4 4 -18 1027.59 330.340 12 4 4 -18 606.308 345.106 34 4 4 -18 1058.38 271.669 23 4 -4 -18 195.113 251.413 22 4 -4 -18 950.732 368.453 32 4 -4 -17 368.110 286.271 22 4 4 -17 174.658 189.375 23 4 -4 -17 7.63993 289.425 32 -4 4 17 149.984 153.299 24 4 4 -17 371.372 246.975 12 4 4 -17 203.351 296.411 34 4 -4 -17 454.846 221.421 38 -4 4 16 2826.98 347.970 24 4 4 -16 3151.40 358.573 23 4 4 -16 2581.07 485.691 34 4 4 -16 3211.80 461.662 12 4 -4 -16 2921.11 460.272 22 -4 4 15 678.345 239.601 24 4 -4 -15 622.429 258.619 22 4 4 -15 986.821 261.959 23 4 4 -15 940.024 318.174 12 4 4 -15 876.064 324.553 34 -4 4 14 6540.06 524.553 24 4 4 -14 7368.28 513.472 23 4 -4 -14 7396.19 648.699 22 -4 4 14 5651.31 971.749 5 4 4 -14 6504.31 664.592 34 4 4 -14 6449.65 616.961 12 4 4 -14 6457.18 436.999 14 4 4 -13 1200.07 323.693 12 -4 4 13 1111.77 241.938 24 4 4 -13 1134.41 237.077 23 4 -4 -13 2105.22 825.577 1 4 4 -13 1112.48 266.395 19 4 4 -13 1165.51 208.774 14 4 -4 -13 1042.98 285.402 16 4 4 -13 1443.64 364.412 34 -4 4 13 1229.73 479.913 5 4 -4 -12 35295.2 1213.07 37 4 4 -12 34077.9 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4 4 109.462 318.156 26 4 -4 -3 589.291 404.267 1 4 4 -3 696.701 434.994 26 -4 4 3 599.690 455.353 5 4 4 -2 6057.33 883.254 26 -4 4 2 6897.83 951.158 5 -4 4 1 382.865 410.353 30 4 4 -1 22.0124 407.035 26 -4 4 1 -362.790 468.910 5 -4 4 0 7492.06 1063.01 30 -4 4 0 10105.7 1144.67 5 4 4 0 9489.87 1106.73 26 -4 4 -1 2783.34 725.701 30 -4 -4 -1 2281.09 600.264 1 -4 4 -1 1895.32 585.864 5 4 4 1 1684.97 531.047 26 -4 4 -2 3854.07 864.803 30 -4 -4 -2 2693.43 694.216 1 -4 4 -2 3309.49 667.393 5 4 4 2 3406.79 747.131 26 -4 4 -3 5607.03 1003.76 30 -4 -4 -3 4928.08 882.701 1 -4 4 -3 6540.26 896.986 5 4 4 3 5875.63 939.394 26 -4 4 -4 1315.21 481.651 30 -4 -4 -4 2026.26 582.556 1 -4 4 -4 2894.13 548.332 5 4 4 4 3151.78 737.056 26 -4 4 -5 120.527 434.975 30 -4 -4 -5 183.670 572.239 1 -4 4 -5 1066.19 348.130 5 4 4 5 62.6757 363.207 26 -4 4 -6 -225.986 405.139 30 -4 -4 -6 28.3192 430.001 1 4 4 6 415.407 455.746 26 -4 4 -7 284.215 127.079 33 -4 4 -7 139.380 452.249 30 -4 -4 -7 793.043 664.868 1 4 4 7 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273.156 32 -4 4 -17 37.4296 300.201 9 -4 4 -17 -93.4048 313.666 34 -4 -4 -17 -12.4552 202.562 38 -4 4 -17 295.215 278.382 12 4 4 17 -1.71880 133.657 24 -4 4 -18 2217.95 486.955 34 -4 4 -18 2007.89 346.165 12 -4 -4 -18 2097.15 333.221 38 -4 4 -18 1885.03 389.911 9 -4 4 -19 173.242 204.009 12 -4 4 -19 88.8558 289.725 9 -4 4 -19 156.871 268.417 34 -4 -4 -20 -207.689 254.269 11 -4 4 -20 122.020 246.732 9 -4 4 -20 195.095 207.230 12 -4 4 -20 -296.466 245.201 34 -4 -4 -20 184.404 194.737 15 -4 -4 -21 1643.91 326.733 11 -4 4 -21 1444.51 250.273 12 -4 4 -21 1685.39 349.061 34 -4 -4 -21 578.633 208.306 15 -4 -4 -22 431.552 209.615 11 -4 4 -22 -148.141 163.146 12 -4 4 -22 482.870 253.372 34 -4 -4 -22 0.28237 153.802 15 -4 4 -23 359.728 123.845 12 -4 -4 -23 228.439 167.499 11 -4 4 -23 567.362 224.665 34 -4 -4 -23 107.992 138.852 15 -4 -4 -24 -211.908 112.532 15 -4 -4 -24 1811.02 221.248 11 4 -5 -24 38.5674 109.790 15 4 -5 -23 133.576 147.208 15 4 -5 -23 566.556 148.076 11 4 5 -22 275.954 169.475 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1831.65 391.838 22 8 -3 -25 1978.25 320.149 35 8 3 -25 1936.54 365.998 31 8 -3 -25 1979.40 384.927 32 8 -3 -25 1991.39 369.295 20 8 3 -25 2431.40 364.332 18 8 -3 -25 1798.66 298.130 15 8 3 -24 861.498 321.514 18 8 -3 -24 766.025 298.083 20 8 -3 -24 701.264 283.367 35 8 -3 -24 625.793 341.598 32 8 3 -24 528.207 322.895 31 8 -3 -24 618.627 362.983 22 8 -3 -23 1956.20 382.360 20 8 3 -23 1899.31 384.955 18 8 -3 -23 1707.21 333.466 35 8 -3 -23 1821.70 389.836 32 8 3 -23 2659.99 477.357 31 8 -3 -23 2229.87 466.691 22 8 3 -23 3519.51 447.751 12 8 -3 -22 -263.342 321.718 20 8 3 -22 59.1159 325.238 18 8 3 -22 192.133 325.219 31 8 3 -22 150.067 255.742 12 8 -3 -22 -20.6242 340.024 22 8 -3 -22 346.391 275.903 35 8 -3 -21 3505.02 557.932 22 8 -3 -21 3936.42 549.718 20 8 3 -21 5162.88 591.961 18 8 3 -21 4484.38 449.318 23 8 3 -21 3987.64 551.582 31 8 -3 -21 4265.96 529.598 35 8 3 -21 3825.13 470.596 12 8 -3 -20 6.33840 317.529 16 8 3 -20 701.401 322.983 31 8 3 -20 928.993 265.755 23 8 -3 -20 258.228 296.417 22 8 3 -20 295.943 268.030 12 8 -3 -20 324.956 248.658 20 8 3 -19 13070.2 702.450 23 8 -3 -19 12667.5 637.326 38 8 -3 -19 11502.6 943.211 16 8 3 -19 12032.4 909.251 31 8 3 -19 11748.6 780.674 12 8 -3 -19 11834.5 888.618 20 8 -3 -18 4796.99 576.804 20 8 3 -18 4455.74 585.207 34 8 -3 -18 4672.77 610.870 16 8 3 -18 4747.32 593.578 31 8 3 -18 4687.05 503.469 12 8 3 -18 5512.42 469.396 23 -8 3 17 3224.32 370.572 24 8 3 -17 3749.57 392.866 23 8 3 -17 3521.11 468.404 19 8 -3 -17 3519.65 520.888 20 8 -3 -17 2254.95 565.885 7 8 -3 -17 2963.19 478.149 16 8 3 -17 1788.78 733.680 29 8 3 -17 3384.04 487.995 31 8 3 -17 3645.08 524.354 34 8 3 -17 3070.03 436.914 12 8 3 -16 26505.8 1287.99 34 8 -3 -16 25507.9 1299.49 16 8 3 -16 27004.5 1279.34 31 8 3 -16 26458.6 2450.61 29 -8 3 16 27022.0 997.487 24 8 3 -16 26400.1 936.795 23 8 -3 -16 25890.8 1249.76 20 8 -3 -16 26117.3 1801.43 7 8 3 -16 25348.7 1125.22 12 8 3 -16 26397.8 1170.26 19 8 3 -15 1957.10 414.009 34 8 -3 -15 1430.49 369.050 16 8 3 -15 1689.63 385.468 31 8 3 -15 2639.42 753.062 29 8 3 -15 1572.73 327.699 12 -8 3 15 1666.64 265.590 24 8 3 -15 1741.97 263.625 23 8 -3 -15 1382.72 232.676 37 8 3 -15 1777.99 351.535 19 -8 3 15 747.218 364.299 5 8 -3 -15 759.120 429.499 7 8 3 -14 9089.78 1371.35 29 8 3 -14 8173.87 689.114 31 8 -3 -14 7534.08 519.646 37 -8 3 14 7683.99 541.939 24 8 3 -14 8433.20 641.253 19 8 3 -14 8718.93 628.326 12 -8 3 14 8450.20 1073.14 5 8 3 -14 8391.84 722.171 34 8 -3 -14 7831.66 694.512 16 8 3 -14 8599.19 517.592 23 8 3 -13 3727.33 852.918 29 -8 3 13 4408.52 853.041 5 8 3 -12 6097.37 1007.55 29 -8 3 12 6341.61 923.608 5 8 3 -11 214.468 286.362 29 -8 3 11 185.076 309.486 5 -8 -3 10 8031.02 926.103 28 8 3 -10 8442.59 1144.62 29 -8 3 10 7673.73 1018.26 5 -8 -3 9 12244.3 1109.85 28 8 3 -9 11078.7 903.274 26 8 3 -9 12010.6 1293.28 29 -8 3 9 13305.0 1286.32 5 8 3 -8 31686.0 1552.97 26 -8 -3 8 31298.4 1790.43 28 8 3 -8 32292.5 2065.58 29 -8 3 8 31292.2 1933.20 5 8 3 -7 1868.32 465.441 26 -8 -3 7 1094.92 442.928 28 8 3 -7 823.967 374.772 29 -8 3 7 1790.66 560.739 5 -8 -3 6 783.026 430.132 28 8 3 -6 398.368 360.087 29 -8 3 6 160.238 385.903 5 -8 3 5 1254.03 516.580 5 -8 -3 5 1765.92 551.253 28 -8 3 4 24626.5 1620.59 5 -8 -3 4 24144.7 1670.66 28 -8 3 3 5646.12 808.128 5 -8 -3 3 5686.40 881.095 28 -8 -3 2 10089.9 1006.53 4 -8 3 2 9963.46 1093.24 5 -8 -3 2 9454.99 1116.20 28 -8 3 1 1132.71 506.197 5 -8 -3 1 1188.21 385.303 4 -8 -3 1 1640.06 591.677 28 -8 3 0 623.251 384.748 5 -8 -3 0 965.697 417.461 4 -8 -3 0 440.564 440.808 28 -8 -3 -1 14661.0 1335.85 28 -8 -3 -1 16676.1 1449.40 4 -8 3 -1 15852.1 1277.46 5 -8 -3 -2 817.456 404.843 28 -8 3 -2 872.464 395.536 5 -8 -3 -3 10290.3 1176.63 28 -8 3 -3 10205.3 1306.96 30 -8 3 -3 11464.2 1050.00 5 -8 -3 -3 11638.1 1368.30 6 -8 -3 -4 5928.96 897.628 28 -8 3 -4 7659.96 859.890 25 -8 3 -4 6314.68 1110.25 30 -8 3 -4 6569.62 807.471 5 -8 -3 -4 5810.31 1109.09 6 -8 3 -5 743.745 311.350 25 -8 -3 -5 784.545 433.793 28 -8 3 -5 999.283 651.566 30 -8 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45.8681 164.223 11 -8 3 -23 71.4282 196.774 34 -8 -3 -23 -94.3837 126.900 15 -8 3 -23 64.7782 181.553 9 -8 -3 -24 1074.59 195.460 11 -8 3 -24 757.502 184.965 34 -8 3 -24 810.518 182.223 9 8 -4 -27 27.1029 107.217 15 8 -4 -26 354.826 179.582 32 8 4 -26 317.967 143.890 18 8 -4 -26 26.1529 148.655 15 8 -4 -26 495.732 131.148 11 8 -4 -25 1153.62 264.586 32 8 4 -25 1526.00 238.634 18 8 -4 -25 893.142 156.977 35 8 -4 -24 764.949 253.220 32 8 4 -24 1500.30 252.201 31 8 -4 -24 893.876 185.746 35 8 4 -24 1571.09 282.354 18 8 -4 -24 823.669 233.264 22 8 4 -23 1578.10 297.623 18 8 -4 -23 1624.32 259.156 35 8 4 -23 1606.43 281.846 31 8 -4 -23 1849.66 378.951 32 8 -4 -23 1080.62 276.500 22 8 -4 -22 290.842 110.108 38 8 4 -22 160.981 224.548 18 8 -4 -22 253.791 206.556 35 8 4 -22 -300.022 219.430 31 8 -4 -22 138.657 271.156 32 8 -4 -22 151.798 270.790 22 8 -4 -21 -547.123 333.187 22 8 -4 -21 -85.4696 140.824 38 8 4 -21 -302.077 318.316 18 8 -4 -21 -28.4516 170.680 35 8 -4 -21 -299.577 341.411 32 8 4 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253.645 222.668 19 8 -4 -15 352.366 220.053 16 -8 4 15 322.276 175.143 24 8 4 -15 504.498 248.906 12 8 -4 -15 76.0634 206.974 37 8 4 -15 224.963 181.365 23 8 4 -14 23351.4 1095.09 19 8 -4 -14 22324.1 1171.54 16 8 4 -14 24144.0 903.088 23 -8 4 14 22345.3 961.593 24 8 4 -14 22030.7 1074.43 12 8 -4 -14 24466.9 1006.86 37 -8 4 13 16.4134 185.491 24 8 4 -13 370.103 240.199 19 8 -4 -13 -258.808 270.437 16 8 4 -13 155.988 181.490 23 8 4 -13 -53.1321 179.536 12 -8 4 13 319.682 460.762 5 8 -4 -13 -57.0441 209.378 37 8 4 -12 -20.5720 176.008 19 8 -4 -12 64.8968 186.773 16 -8 4 12 159.640 172.992 24 8 -4 -12 -19.5174 201.920 37 8 4 -12 401.150 247.448 12 -8 4 12 68.7019 409.407 5 -8 4 11 2941.27 844.752 5 8 4 -11 4010.62 463.447 19 8 -4 -11 2992.43 427.280 16 8 -4 -11 4130.74 442.486 37 8 4 -11 3898.30 448.064 12 -8 4 11 4253.36 438.552 24 8 4 -11 4158.17 386.718 14 8 4 -10 13879.9 812.639 19 8 -4 -10 14671.4 780.960 37 8 4 -10 14413.7 693.437 14 8 4 -10 14503.0 797.847 12 -8 4 10 14663.1 763.799 24 -8 4 10 14835.1 1561.18 5 -8 4 9 1100.96 514.358 5 8 -4 -9 1262.48 284.491 37 8 4 -9 1345.82 242.564 14 -8 4 9 1432.60 297.952 24 8 4 -9 1499.12 279.612 12 8 4 -8 629.360 175.084 14 -8 4 8 463.739 433.860 5 8 -4 -8 853.010 242.070 37 -8 4 8 789.557 216.775 24 8 4 -8 656.356 315.200 26 -8 4 7 5362.76 974.395 5 -8 4 7 5734.12 481.219 24 -8 -4 7 5737.69 917.087 28 8 4 -7 5199.68 815.956 26 8 4 -7 5727.61 424.450 14 8 -4 -7 5429.50 469.683 37 8 4 -6 1920.13 268.594 14 -8 -4 6 1889.27 583.240 28 8 4 -6 1763.06 458.228 26 -8 4 6 1363.76 581.526 5 8 -4 -6 1565.82 264.201 37 8 4 -5 9141.50 1076.34 26 -8 -4 5 9658.25 1186.36 28 -8 4 5 8048.33 1101.80 5 -8 -4 4 43.6144 376.137 28 8 4 -4 360.656 489.905 26 -8 4 4 421.854 453.754 5 -8 -4 3 7102.11 1055.42 28 8 4 -3 6015.03 954.136 26 -8 4 3 7014.31 1048.00 5 -8 -4 2 1764.01 609.219 28 8 4 -2 1298.96 599.177 26 -8 4 2 2129.63 642.382 5 8 4 -1 705.716 491.767 26 -8 4 1 -35.3497 374.438 5 -8 4 0 3812.49 745.897 5 -8 -4 0 3538.78 774.356 6 -8 4 0 3223.07 770.301 30 -8 4 -1 1672.54 599.842 5 -8 -4 -1 836.061 478.818 6 -8 4 -1 964.491 435.910 30 -8 4 -2 900.200 376.991 5 -8 -4 -2 749.351 551.117 6 -8 4 -2 971.866 623.519 30 -8 4 -3 812.238 456.754 5 -8 -4 -3 418.708 564.761 6 8 4 3 200.980 136.613 24 -8 4 -3 -123.365 563.773 30 -8 -4 -4 867.867 193.396 38 -8 4 -4 1493.21 513.697 5 8 4 4 898.459 210.727 24 -8 -4 -5 86.6961 599.457 1 -8 -4 -5 254.939 131.240 38 -8 -4 -5 -565.761 503.282 6 8 4 5 310.766 182.816 24 -8 4 -6 7592.22 1298.72 30 -8 -4 -6 8839.42 1398.40 6 -8 -4 -6 8622.14 575.581 38 8 4 6 8221.07 567.407 24 -8 -4 -6 9573.86 1412.36 1 -8 4 -7 7989.42 1394.11 30 -8 -4 -7 8156.21 1369.94 6 -8 -4 -7 7106.13 519.041 38 8 4 7 7181.89 553.279 24 -8 -4 -7 8299.47 1369.26 1 -8 4 -8 4705.04 459.057 9 -8 -4 -8 4966.84 1176.04 6 -8 -4 -8 6007.45 1202.12 1 -8 4 -8 5821.62 1183.34 30 8 4 8 4872.83 461.995 24 -8 -4 -8 4082.87 418.782 38 8 4 9 2228.84 347.492 24 -8 -4 -9 2521.77 345.197 38 -8 -4 -9 1684.31 678.089 1 -8 4 -9 2252.23 858.466 30 8 4 9 2134.64 676.276 26 -8 4 -9 2281.77 309.659 33 -8 4 -9 3231.30 410.417 9 -8 4 -10 -42.9011 139.311 33 8 4 10 74.6343 174.515 24 -8 -4 -10 406.442 233.869 38 -8 4 -10 112.733 193.555 9 -8 4 -11 88.5937 125.980 33 -8 -4 -11 83.6692 184.948 38 8 4 11 72.1346 176.691 24 -8 4 -11 115.113 225.260 9 -8 -4 -12 265.887 224.303 38 -8 4 -12 102.476 121.607 33 8 4 12 313.153 182.213 24 -8 4 -12 44.7956 210.868 9 -8 -4 -13 1158.70 297.877 38 -8 4 -13 1066.33 380.830 34 8 4 13 1238.86 285.272 24 -8 4 -13 367.424 243.446 9 -8 4 -14 2327.24 375.957 9 -8 -4 -14 3111.74 456.455 11 -8 4 -14 3102.55 499.427 34 8 4 14 2632.53 344.829 24 -8 -4 -14 2731.91 387.277 38 -8 4 -15 -25.3024 271.206 34 -8 4 -15 -246.861 253.063 9 8 4 15 -48.2284 150.757 24 -8 -4 -15 200.905 240.075 11 8 4 16 473.099 195.000 24 -8 -4 -16 195.064 256.114 11 -8 4 -16 327.911 281.923 34 -8 -4 -16 333.408 193.528 15 -8 4 -16 84.5397 232.852 9 -8 4 -16 240.479 233.639 12 -8 4 -17 -84.4008 296.812 34 -8 -4 -17 174.470 167.424 15 -8 4 -17 42.9069 246.537 9 -8 -4 -17 -81.4022 269.450 11 -8 4 -17 21.4336 216.394 12 -8 4 -18 1853.45 370.536 34 -8 4 -18 2036.93 361.143 9 -8 4 -18 1160.42 254.854 12 -8 -4 -18 2021.27 382.075 11 -8 -4 -19 -7.60879 127.471 15 -8 4 -19 385.973 186.412 12 -8 -4 -19 583.063 261.814 11 -8 4 -19 617.881 260.996 34 -8 4 -19 620.417 247.357 9 -8 -4 -20 732.624 243.242 11 -8 4 -20 746.844 178.880 12 -8 4 -20 696.438 264.041 34 -8 4 -20 636.530 236.533 9 -8 4 -21 1116.43 249.523 34 -8 -4 -21 1137.88 223.879 11 -8 4 -22 137.487 142.167 34 -8 -4 -22 147.008 98.7508 13 -8 -4 -22 297.666 152.549 11 8 -5 -24 25.2623 110.828 15 8 -5 -23 123.481 126.984 32 8 -5 -22 180.243 157.521 32 8 -5 -22 147.563 86.5439 38 8 5 -22 139.408 114.990 18 8 -5 -21 -80.4680 174.800 32 8 -5 -21 47.8898 99.8310 38 8 5 -21 11.5436 133.149 18 8 -5 -20 -9.39909 117.516 38 -8 5 20 -101.620 108.097 24 8 5 -20 141.086 152.091 23 8 -5 -20 -52.1573 182.375 32 8 5 -20 -17.2459 160.287 18 8 5 -19 1757.08 276.526 18 8 -5 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385.066 24 -10 4 -12 2635.04 291.496 33 -10 4 -12 2463.36 376.930 9 -10 -4 -13 2371.02 409.465 11 -10 4 -13 2054.18 362.500 9 10 4 13 2180.19 322.443 24 -10 -4 -14 429.872 273.866 11 -10 4 -14 52.2876 213.671 9 -10 4 -14 -56.2706 274.671 34 10 4 14 149.755 144.657 24 -10 -4 -15 227.455 246.659 11 -10 4 -15 -217.786 232.032 9 -10 4 -15 98.6010 257.889 34 10 4 15 152.579 157.572 24 -10 4 -16 1851.66 386.352 34 -10 -4 -16 2000.71 370.797 11 -10 4 -16 2028.40 318.518 12 -10 4 -16 2426.90 360.817 9 -10 4 -17 144.262 247.476 34 -10 4 -17 693.787 223.850 12 -10 -4 -17 155.694 246.767 11 -10 4 -17 391.971 210.967 9 -10 -4 -18 639.777 262.202 11 -10 4 -18 -118.827 159.669 12 -10 4 -18 59.1596 186.783 9 -10 4 -18 101.524 240.059 34 -10 -4 -19 242.778 198.341 11 -10 4 -19 -36.0317 130.279 12 -10 4 -19 -58.0057 170.498 9 -10 4 -19 142.186 206.444 34 -10 -4 -20 89.3647 158.971 11 -10 4 -20 73.2117 101.793 12 -10 4 -20 328.304 183.483 34 -10 -4 -21 962.208 155.238 13 -10 -4 -21 999.965 185.368 11 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5 -14 1769.17 303.452 12 -10 5 14 1820.51 317.183 24 10 5 -14 1733.84 286.980 23 10 5 -14 1758.70 327.525 19 10 -5 -13 160.526 194.189 37 10 5 -13 35.6663 183.077 12 -10 5 13 105.693 219.350 24 10 5 -13 157.873 209.360 23 10 5 -13 -12.3703 186.118 19 10 5 -12 56.8178 160.539 12 -10 5 12 67.4377 204.780 24 10 -5 -12 -4.96928 201.470 37 10 5 -12 126.622 202.475 19 10 5 -11 594.755 207.677 12 10 5 -11 485.353 227.889 19 10 -5 -11 462.041 234.257 37 -10 5 11 543.851 251.726 24 10 5 -10 2259.56 371.922 19 10 -5 -10 2488.97 379.188 37 -10 5 10 2408.70 364.080 24 10 5 -9 166.150 206.947 19 -10 5 9 -89.9229 216.897 24 10 -5 -9 102.886 203.349 37 -10 5 8 8126.82 605.159 24 10 -5 -8 8377.96 638.824 37 -10 5 7 3897.02 431.552 24 -10 5 7 3747.48 352.818 33 10 -5 -7 4193.69 460.353 37 -10 5 6 1001.53 270.874 24 -10 5 6 613.552 197.108 33 10 -5 -6 1012.73 299.339 37 -10 5 5 176.909 170.971 24 -10 5 5 206.123 166.857 33 10 -5 -5 290.537 195.566 37 -10 5 4 874.666 257.743 24 10 5 -4 832.998 201.735 24 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2549.30 335.153 38 10 5 6 2084.53 354.584 24 -10 -5 -7 852.268 232.848 38 -10 5 -7 719.855 227.668 33 10 5 7 873.238 283.475 24 -10 5 -8 11874.8 651.173 33 -10 -5 -8 11448.6 659.974 38 10 5 8 12656.9 721.342 24 -10 -5 -9 1156.90 269.792 38 -10 5 -9 1046.87 238.384 33 10 5 9 1064.79 280.125 24 -10 -5 -10 482.053 196.640 11 -10 5 -10 160.388 104.804 14 10 5 10 552.329 234.676 24 -10 5 -10 348.188 168.311 33 10 5 11 67.8533 190.751 24 -10 5 -11 217.051 201.917 34 -10 5 -11 -71.3703 142.180 33 -10 -5 -11 -331.869 200.754 11 10 5 12 3165.64 371.492 24 -10 5 -12 3161.53 281.170 33 -10 5 -12 2984.48 377.677 34 -10 -5 -12 3028.75 363.254 11 10 5 13 871.408 233.446 24 -10 5 -13 920.459 243.229 34 -10 5 -13 747.273 141.180 33 -10 -5 -13 1041.93 239.094 11 10 5 14 409.037 160.852 24 -10 5 -14 2.82804 146.023 34 -10 -5 -14 197.139 173.800 11 -10 5 -14 -17.6046 210.577 12 10 5 15 183.688 129.687 24 -10 5 -15 660.708 207.612 34 -10 5 -15 132.638 183.769 12 -10 -5 -15 377.287 198.399 11 10 5 16 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5 5 1235.22 303.096 24 -11 5 4 3577.94 390.849 33 11 -5 -4 3441.20 447.009 37 11 5 -4 3468.39 350.434 24 -11 5 4 3880.77 422.666 24 11 -5 -3 1555.73 326.571 37 -11 5 3 1630.78 287.000 24 11 5 -3 1766.65 298.524 24 -11 5 3 1640.63 300.261 33 11 -5 -2 498.467 282.675 37 -11 5 2 334.141 192.388 24 11 5 -2 663.891 212.134 24 -11 5 2 274.739 165.298 33 11 -5 -1 -50.8731 206.873 37 -11 5 1 109.364 143.234 24 11 5 -1 193.760 173.156 24 -11 5 1 96.5779 188.490 33 -11 5 0 3089.12 406.084 33 11 -5 0 2557.33 394.244 37 -11 5 0 3289.96 331.396 24 11 5 0 3367.63 390.658 24 11 -5 1 30.3495 197.195 37 11 5 1 7.54577 172.354 24 -11 5 -1 -86.2705 172.727 33 11 -5 2 1036.18 270.155 37 11 5 2 1118.82 282.046 24 -11 5 -2 816.251 264.348 33 11 -5 3 133.462 165.022 37 11 5 3 60.3287 199.529 24 -11 5 -3 40.6100 185.576 33 11 -5 4 -64.5314 157.192 37 -11 -5 -4 -212.106 149.535 38 11 5 4 341.917 237.391 24 -11 5 -4 208.366 216.224 33 11 -5 5 1883.88 299.843 37 -11 -5 -5 2245.22 305.505 38 11 5 5 1880.42 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641.650 273.842 9 -13 -3 -16 90.3647 211.145 9 -13 -3 -17 -346.058 289.193 11 -13 3 -17 -298.716 242.350 9 -13 -3 -17 39.9563 195.016 9 -13 -3 -18 1474.36 306.633 13 -13 -3 -18 853.801 313.045 11 -13 3 -18 990.056 267.979 9 -13 -3 -18 876.287 232.373 9 -13 3 -19 296.888 257.092 34 -13 -3 -19 117.962 165.220 13 -13 -3 -19 231.776 217.182 11 -13 -3 -19 134.310 158.360 9 -13 3 -19 76.6952 183.243 9 -13 3 -20 1524.22 290.577 34 -13 -3 -20 2127.99 220.215 9 -13 -3 -20 2449.14 258.802 13 -13 3 -20 2223.27 279.918 9 -13 3 -21 213.532 171.699 34 -13 -3 -21 345.040 137.297 13 -13 3 -21 459.408 162.031 9 -13 3 -22 4489.35 298.996 34 -13 3 -22 4789.25 268.407 9 13 -4 -26 309.927 133.966 32 13 4 -26 657.136 145.924 18 13 4 -25 866.328 195.436 18 13 4 -25 424.790 138.388 31 13 -4 -25 627.967 196.013 32 13 -4 -25 557.723 151.308 35 13 -4 -25 373.249 158.392 22 13 4 -24 816.009 220.503 18 13 -4 -24 0.23887 132.424 15 13 -4 -24 345.679 166.007 35 13 -4 -24 499.138 199.045 22 13 4 -24 944.159 205.115 31 13 -4 -24 523.835 218.189 32 13 -4 -23 3063.86 338.609 35 13 4 -23 3660.14 381.499 18 13 -4 -23 3053.80 381.230 22 13 -4 -23 3515.60 422.781 32 13 4 -23 3918.72 378.014 31 13 -4 -22 2213.85 325.006 35 13 4 -22 2023.33 332.162 18 13 4 -22 2963.17 352.025 31 13 -4 -22 2756.53 388.034 22 13 4 -21 233.629 215.135 31 13 -4 -21 266.198 239.800 22 13 4 -21 162.752 167.982 23 13 -4 -20 48.5838 137.314 38 13 4 -20 293.232 257.328 31 13 -4 -20 -208.628 304.436 16 13 4 -20 232.201 185.074 23 13 -4 -20 140.896 225.906 22 -13 4 20 230.342 134.036 24 13 -4 -19 2422.21 435.286 16 13 4 -19 3024.85 397.312 31 -13 4 19 2592.00 306.694 24 13 4 -19 2308.67 298.654 23 13 -4 -18 1173.05 367.518 16 13 4 -18 1443.56 373.063 19 13 4 -18 1878.90 301.077 23 13 4 -18 2086.05 399.763 31 -13 4 18 1523.73 264.891 24 13 -4 -17 1473.29 396.081 16 13 4 -17 1512.68 340.529 19 13 4 -17 1879.29 297.474 23 13 4 -17 1117.99 319.406 31 -13 4 17 1628.58 286.047 24 -13 4 16 1733.70 319.472 24 13 4 -16 2068.74 378.737 19 13 -4 -16 1888.19 293.040 37 13 4 -16 1624.10 279.008 23 13 4 -16 1981.20 391.299 31 13 4 -16 2377.96 404.049 12 13 -4 -16 1995.98 445.313 16 -13 4 15 114.194 204.295 24 13 4 -15 -30.9781 164.594 23 13 4 -15 338.450 294.393 19 13 -4 -15 -88.1453 212.179 37 13 4 -15 363.501 274.037 31 13 4 -15 597.113 297.901 12 13 -4 -15 236.235 293.424 16 -13 4 14 437.498 203.413 24 13 4 -14 345.115 173.972 23 13 -4 -14 404.937 198.853 37 13 -4 -14 34.1045 245.511 16 13 4 -14 195.039 192.146 31 13 4 -14 916.213 311.745 12 13 4 -14 419.573 244.105 19 13 -4 -13 5728.43 504.429 37 13 4 -13 6228.56 581.420 31 13 4 -13 6161.69 463.351 23 -13 4 13 6507.50 547.500 24 13 4 -13 6706.70 596.926 12 13 4 -13 7116.72 648.554 19 13 -4 -13 5752.97 617.269 16 -13 4 12 1550.99 306.643 24 13 4 -12 1423.14 311.618 12 13 4 -12 1277.44 314.037 19 13 -4 -12 1592.79 322.701 37 13 -4 -12 1360.91 372.726 16 13 4 -11 198.805 225.561 12 13 -4 -11 17.7053 170.556 37 -13 4 11 -36.8306 197.538 24 13 4 -10 1557.89 328.058 12 13 -4 -10 1759.47 311.932 37 -13 4 10 1655.80 563.157 5 -13 4 10 1825.33 321.781 24 -13 4 9 2528.54 774.760 5 13 -4 -9 1586.67 326.949 37 -13 -4 9 2814.39 733.321 28 -13 4 9 2050.86 345.786 24 -13 4 8 777.047 442.280 5 13 -4 -8 1420.31 293.100 37 -13 -4 8 1474.30 738.222 28 -13 4 8 1543.30 286.392 24 -13 4 7 854.210 238.075 24 13 -4 -7 547.460 194.249 37 13 4 -7 262.625 323.121 26 -13 4 6 -405.183 486.587 5 13 4 -6 -386.455 200.951 24 -13 4 6 60.4477 173.205 24 13 -4 -6 -1.77818 173.428 37 -13 -4 6 177.885 437.955 28 13 4 -6 520.092 462.233 26 -13 4 5 502.403 503.065 5 13 4 -5 66.4612 132.001 24 -13 4 5 -52.6560 152.939 24 13 -4 -5 69.7898 190.467 37 -13 -4 5 480.442 478.553 28 13 4 -5 624.496 400.608 26 -13 4 4 7423.63 1133.35 5 13 4 -4 5523.50 461.961 24 -13 4 4 6080.42 510.361 24 13 -4 -4 6235.72 562.654 37 -13 -4 4 7417.79 1178.45 28 13 4 -3 435.833 155.731 24 -13 4 3 416.643 182.651 24 -13 4 3 783.666 537.306 5 -13 -4 3 466.269 529.772 28 -13 4 2 136.959 165.227 24 13 4 -2 12.9051 151.634 24 -13 -4 2 -621.016 400.022 6 -13 4 2 234.906 334.771 5 -13 -4 2 -7.53706 412.717 28 -13 4 1 487.631 210.214 24 13 4 -1 352.361 177.614 24 -13 -4 1 970.657 542.332 6 -13 -4 1 571.629 502.742 28 -13 4 1 585.970 477.434 25 -13 4 0 422.638 189.681 24 13 4 0 352.634 187.403 24 -13 -4 0 699.696 712.307 6 -13 4 0 323.172 540.106 30 -13 4 0 -24.6104 596.190 25 -13 -4 0 1341.56 723.334 28 13 4 1 193.287 189.035 24 -13 -4 -1 1194.46 705.777 6 -13 4 -1 109.885 501.351 30 -13 -4 -1 -115.260 501.555 28 -13 4 -1 -632.061 595.293 25 13 4 2 509.047 240.858 24 -13 4 -2 -466.167 606.276 30 -13 4 -2 -454.891 611.798 25 -13 4 -3 9500.28 1445.42 30 -13 -4 -3 11853.1 1689.95 6 13 4 3 12098.3 715.406 24 13 4 4 18588.0 882.579 24 13 4 5 13161.7 762.941 24 13 4 6 6036.98 543.473 24 -13 -4 -7 5.75920 180.579 11 13 4 7 6.72409 197.369 24 -13 -4 -8 3223.80 420.373 11 13 4 8 2754.95 394.004 24 -13 -4 -9 1099.19 288.141 11 13 4 9 881.394 273.146 24 -13 -4 -10 1606.08 349.120 11 -13 4 -10 1024.19 211.332 33 13 4 10 1483.58 301.072 24 -13 -4 -11 2581.12 399.501 11 13 4 11 2528.44 363.401 24 -13 4 -11 1866.10 251.225 33 -13 -4 -12 983.101 303.386 11 13 4 12 570.168 216.866 24 -13 4 -12 1082.59 267.020 9 -13 4 -12 963.969 191.030 33 -13 -4 -13 346.816 246.821 11 13 4 13 294.135 184.123 24 -13 4 -13 442.389 209.217 9 -13 -4 -14 251.061 242.151 11 13 4 14 57.4651 132.652 24 -13 4 -14 -8.44557 232.901 34 -13 4 -14 456.652 206.005 9 -13 4 -15 446.266 207.953 12 -13 -4 -15 375.907 230.080 11 -13 4 -15 123.442 234.332 34 -13 -4 -15 785.628 239.607 9 -13 4 -15 495.205 182.544 9 -13 4 -16 677.353 194.188 9 -13 4 -16 915.855 206.004 12 -13 -4 -16 653.630 221.447 11 -13 4 -16 969.817 248.417 34 -13 -4 -16 1009.71 191.802 9 -13 4 -17 457.825 197.335 34 -13 4 -17 474.708 174.499 9 -13 4 -17 493.412 154.665 12 -13 -4 -17 496.298 200.947 11 -13 -4 -18 107.881 173.697 11 -13 -4 -18 252.969 155.011 13 -13 4 -18 43.0023 94.4770 12 -13 4 -18 77.7022 159.051 34 -13 -4 -19 763.078 153.157 13 -13 4 -19 798.261 181.492 34 13 -5 -23 -10.4976 88.9046 15 13 5 -22 -215.663 136.191 18 13 -5 -22 213.054 141.940 32 13 5 -21 344.022 163.653 18 -13 5 21 54.0895 68.3674 24 13 -5 -21 336.850 176.461 32 13 -5 -21 282.832 120.730 35 13 5 -20 39.4027 177.324 18 13 -5 -20 42.3256 157.877 32 -13 5 20 121.269 94.6986 24 13 5 -20 267.455 141.139 23 13 -5 -20 -78.6876 135.669 35 13 -5 -20 -84.6486 87.0754 38 13 -5 -19 152.174 167.612 32 13 5 -19 140.954 137.918 23 13 -5 -19 447.799 148.538 38 -13 5 19 288.710 135.934 24 13 -5 -18 -78.4020 193.872 32 -13 5 18 -130.714 148.559 24 13 5 -18 195.011 159.890 23 -13 5 17 1156.41 233.734 24 13 5 -17 1124.07 230.957 23 -13 5 16 3338.07 350.118 24 13 5 -16 3234.70 329.472 23 13 5 -16 3147.86 385.392 19 -13 5 15 469.566 241.726 24 13 5 -15 462.321 242.084 19 13 5 -15 563.496 217.685 23 13 -5 -14 404.902 229.408 37 -13 5 14 -65.0160 193.500 24 13 5 -14 -76.8852 202.803 19 13 5 -14 68.3252 166.829 23 13 -5 -13 1321.05 272.146 37 -13 5 13 1527.24 295.114 24 13 5 -13 1400.60 326.325 19 13 5 -13 1350.30 253.542 23 13 -5 -12 795.155 260.587 37 -13 5 12 794.020 243.349 24 13 5 -12 754.249 250.174 19 13 5 -12 611.120 195.167 23 -13 5 11 289.511 225.737 24 13 5 -11 536.216 255.534 19 13 -5 -11 389.337 224.641 37 -13 5 10 1447.63 312.262 24 13 5 -10 1384.36 334.193 19 13 -5 -10 1209.12 294.035 37 -13 5 9 4083.98 445.686 24 13 -5 -9 4772.97 483.526 37 13 -5 -8 1699.00 334.965 37 -13 5 8 1420.55 293.966 24 -13 5 8 1489.81 238.998 33 -13 5 7 9138.50 628.557 24 13 -5 -7 8582.23 647.920 37 -13 5 7 8203.60 520.637 33 -13 5 6 321.034 233.650 24 -13 5 6 125.758 138.522 33 13 -5 -6 108.333 229.269 37 -13 5 5 1436.62 266.267 33 13 -5 -5 1152.27 323.795 37 -13 5 5 1552.87 315.647 24 13 5 -5 1149.24 221.527 24 -13 5 4 1016.48 249.386 33 -13 5 4 1331.57 261.062 24 13 5 -4 624.241 195.633 24 13 -5 -4 884.382 278.674 37 13 5 -3 2469.97 333.538 24 -13 5 3 2969.06 365.119 24 13 -5 -3 2885.07 417.935 37 -13 5 3 3381.60 388.772 33 -13 5 2 473.807 197.568 33 13 -5 -2 528.395 252.530 37 -13 5 2 841.496 225.501 24 13 5 -2 499.459 208.318 24 -13 5 1 2750.46 369.431 33 13 -5 -1 2124.18 375.223 37 -13 5 1 2696.47 315.523 24 13 5 -1 2769.68 353.621 24 13 5 0 1806.65 317.221 24 -13 5 0 2052.90 317.826 33 13 -5 0 1836.15 353.914 37 13 5 1 -40.2748 188.781 24 -13 5 -1 -25.7256 199.708 33 13 -5 1 60.3419 193.571 37 13 5 2 109.414 190.367 24 -13 5 -2 32.3958 190.889 33 13 -5 2 205.745 233.332 37 13 5 3 117.113 196.456 24 -13 5 -3 82.5305 194.135 33 13 -5 3 94.7666 183.917 37 13 5 4 341.050 233.527 24 -13 5 -4 168.994 188.408 33 13 -5 4 429.347 214.620 37 13 5 5 1555.89 342.631 24 13 -5 5 1052.71 260.476 37 -13 5 -5 963.029 256.103 33 -13 5 -6 6920.55 517.585 33 13 5 6 7347.69 555.568 24 13 -5 6 5934.17 484.672 37 13 5 7 1158.52 302.160 24 13 -5 7 950.050 225.050 37 -13 5 -7 971.362 242.500 33 13 5 8 1902.07 329.771 24 -13 5 -8 1423.70 249.801 33 -13 5 -9 736.757 154.970 14 -13 5 -9 467.348 169.726 33 13 5 9 358.276 235.458 24 -13 5 -10 176.089 133.967 33 13 5 10 345.024 196.055 24 -13 -5 -11 183.066 126.472 11 -13 5 -11 430.870 139.157 33 13 5 11 315.919 176.164 24 -13 -5 -12 92.1253 136.991 11 -13 5 -12 177.182 89.7015 33 -13 -5 -13 1134.25 199.312 11 -13 5 -13 1333.79 253.845 12 -13 5 -13 1266.16 210.028 34 13 5 13 1257.91 200.831 24 -13 5 -14 122.387 161.557 12 -13 -5 -14 12.9065 112.551 11 -13 5 -14 129.118 107.947 34 13 5 14 65.8446 92.8567 24 -13 5 -15 146.982 136.868 12 -13 -5 -16 1623.47 178.482 13 -13 5 -16 1423.72 163.843 12 13 6 -18 419.057 96.9623 23 13 6 -17 165.141 97.7690 23 -13 6 17 120.214 89.5532 24 13 -6 -17 28.3599 86.4949 38 13 6 -16 525.386 137.834 18 13 6 -16 740.744 142.954 23 13 -6 -16 869.852 158.117 38 -13 6 16 742.671 153.257 24 13 6 -15 -10.7171 113.113 23 -13 6 15 38.4755 118.371 24 13 6 -14 138.835 131.276 23 -13 6 14 78.0487 134.886 24 13 6 -13 17.0334 127.405 23 -13 6 13 -32.8663 146.787 24 13 6 -12 60.6856 134.260 23 13 6 -12 20.5622 151.253 19 -13 6 12 34.0226 158.522 24 13 -6 -11 1650.22 256.522 37 -13 6 11 1989.16 278.229 24 13 6 -11 1396.60 213.513 23 13 6 -11 1242.97 219.148 19 13 -6 -10 236.039 193.382 37 -13 6 10 -49.8764 91.0526 14 13 6 -10 150.704 157.939 23 13 6 -10 399.450 179.512 19 -13 6 10 176.341 173.446 24 13 -6 -9 14.0032 181.907 37 13 6 -9 235.506 169.997 19 -13 6 9 278.643 190.366 24 13 -6 -8 478.186 206.455 37 13 6 -8 340.993 173.309 19 -13 6 8 490.813 178.839 24 13 -6 -7 550.559 232.038 37 13 6 -7 487.389 178.429 19 -13 6 7 838.316 225.063 24 13 -6 -6 -2.67995 209.748 37 -13 6 6 56.4521 101.961 33 13 6 -6 83.7165 159.376 19 -13 6 6 118.066 156.090 24 13 -6 -5 995.603 255.566 37 -13 6 5 812.779 199.689 24 -13 6 5 836.216 167.502 33 13 6 -5 1550.35 269.948 19 13 6 -4 2016.58 225.685 24 -13 6 4 1773.67 237.529 24 -13 6 4 1778.21 248.613 33 13 -6 -4 2078.22 323.094 37 13 6 -3 561.249 162.301 24 -13 6 3 689.271 170.215 24 -13 6 3 852.042 207.878 33 13 -6 -3 614.773 224.067 37 13 6 -2 272.876 156.299 24 -13 6 2 158.569 132.283 24 -13 6 2 230.070 182.431 33 13 -6 -2 59.9082 174.690 37 -13 6 1 484.105 197.936 33 13 6 -1 496.322 183.651 24 13 -6 -1 529.273 189.691 37 -13 6 0 445.294 179.973 33 13 6 0 674.838 180.979 24 13 -6 0 160.568 158.783 37 -13 6 -1 556.692 200.524 33 13 6 1 385.899 182.260 24 13 -6 1 592.287 187.629 37 -13 6 -2 275.922 191.254 33 13 6 2 178.231 178.080 24 13 -6 2 0.37330 120.825 37 -13 6 -3 96.1993 185.672 33 13 -6 3 -11.1915 113.025 37 13 6 3 304.324 185.318 24 13 -6 4 -99.2966 110.675 37 -13 6 -4 47.1669 129.777 14 13 6 4 -116.170 173.584 24 -13 6 -4 -4.52231 166.130 33 -13 6 -5 440.801 150.399 14 13 6 5 92.5962 156.915 24 -13 6 -5 217.985 164.181 33 -13 6 -6 8.66189 98.3484 14 13 6 6 133.532 166.141 24 -13 6 -6 111.577 147.693 33 -13 6 -7 731.638 132.087 14 13 6 7 598.071 187.978 24 -13 6 -7 744.620 177.222 33 -13 6 -8 -127.275 81.9976 14 -13 6 -8 48.8838 104.771 33 13 6 8 85.5865 138.828 24 -13 6 -9 1270.71 212.555 12 13 6 9 1546.15 211.771 24 -13 6 -10 114.421 132.501 12 13 6 10 35.5990 107.652 24 -13 6 -11 1115.60 172.406 12 13 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374.234 10 22 2 -7 1939.67 316.346 24 22 -2 -6 1874.54 474.116 17 22 2 -6 1782.96 429.007 10 22 -2 -6 1323.57 332.113 10 22 2 -6 1425.83 301.964 24 22 -2 -5 7438.49 776.959 17 22 -2 -5 8599.42 755.483 10 22 2 -5 7943.22 608.751 24 22 -2 -4 11447.5 928.380 17 22 -2 -4 12012.4 889.777 10 22 2 -4 13804.0 780.722 24 22 -2 -3 37753.6 1642.22 17 22 -2 -3 35496.3 1498.23 10 22 2 -3 37056.9 1244.81 24 22 -2 -2 10667.5 890.596 17 22 -2 -2 10257.9 812.618 10 22 2 -2 9300.49 662.800 24 22 2 -1 3513.39 459.307 17 22 -2 -1 3573.61 558.704 17 22 -2 -1 4235.71 541.531 10 22 2 -1 3953.99 459.005 24 22 -2 0 2203.08 461.956 17 22 2 0 2428.17 368.834 24 -22 -2 -1 3300.13 348.831 13 22 -2 1 2872.89 495.701 17 22 2 1 2948.56 391.031 24 22 -2 2 860.668 341.841 17 -22 -2 -2 1495.64 273.819 13 22 2 2 973.720 273.622 24 22 -2 3 441.201 294.588 17 -22 -2 -3 380.078 187.297 13 22 2 3 309.095 242.458 24 22 -2 4 299.581 320.826 17 -22 -2 -4 605.219 214.608 13 22 2 4 512.311 237.875 24 22 -2 5 608.931 326.039 17 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3 -14 692.285 152.520 34 22 -4 -22 -70.4486 123.490 35 22 4 -22 303.885 120.204 18 22 -4 -21 2109.84 255.925 16 22 4 -21 1810.39 218.643 18 22 4 -21 1333.83 192.258 31 22 4 -20 -107.802 157.975 31 -22 4 20 -123.022 87.7812 24 22 -4 -20 17.4854 157.234 16 22 -4 -20 168.975 149.791 22 22 -4 -19 20.3899 171.805 16 22 4 -19 1.89410 148.612 31 -22 4 19 -10.1674 105.424 24 22 -4 -18 4052.74 405.782 16 22 4 -18 4108.03 400.274 31 -22 4 18 3828.74 301.973 24 -22 4 17 67.9789 145.092 24 22 -4 -17 186.712 185.748 16 22 4 -17 -64.8514 180.529 19 22 4 -17 153.034 189.762 31 22 -4 -16 1132.54 296.706 16 -22 4 16 1182.03 239.299 24 22 4 -16 805.447 253.942 19 22 4 -16 1161.70 276.656 31 22 4 -15 -19.1984 199.740 31 -22 4 15 401.125 217.078 24 22 -4 -15 415.619 246.449 16 22 -4 -15 1.80891 128.091 37 22 4 -15 299.123 204.275 19 22 4 -14 8082.07 581.003 19 -22 4 14 8523.06 554.617 24 22 -4 -14 8577.79 655.989 16 22 4 -14 9000.98 645.395 31 22 -4 -14 8518.30 470.188 37 -22 4 13 303.509 225.459 24 22 4 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471.844 160.516 24 22 4 0 2081.64 345.873 24 22 4 1 809.953 279.363 24 22 4 2 632.700 279.120 24 22 4 3 732.213 238.066 24 22 4 4 4688.99 432.124 24 22 4 5 129.565 186.445 24 22 4 6 387.049 186.119 24 22 4 7 164.711 169.741 24 -22 4 -7 251.164 142.675 33 -22 4 -8 334.073 120.019 33 22 4 8 416.760 153.645 24 -22 -4 -8 20.3956 85.8586 13 -22 -4 -9 1057.56 149.011 13 -22 4 -9 624.133 111.712 33 22 4 9 684.145 152.294 24 22 -4 10 904.757 123.809 37 -22 -4 -10 1976.02 251.849 9 -22 -4 -11 -8.59110 118.602 9 -22 5 17 117.659 75.4918 24 -22 5 16 701.095 129.397 24 22 5 -15 -56.1689 136.102 19 -22 5 15 -16.8993 116.971 24 22 5 -14 -146.972 163.284 19 -22 5 14 -198.766 142.769 24 -22 5 13 5183.50 342.030 24 22 5 -13 4984.47 386.872 19 22 -5 -13 5230.54 310.365 37 -22 5 12 765.484 184.492 24 22 5 -12 1366.95 255.022 19 22 -5 -12 1139.73 184.332 37 -22 5 11 92.6604 149.528 24 22 5 -11 56.6486 172.681 19 22 -5 -11 143.655 138.420 37 -22 5 10 550.754 192.531 24 22 5 -10 955.984 252.940 19 22 -5 -10 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37 22 5 1 -1.13873 150.424 24 -22 5 -1 106.920 132.231 33 22 -5 1 162.596 144.130 37 22 5 2 -70.2435 140.088 24 -22 5 -2 -32.8131 131.837 33 22 -5 2 -81.3638 129.531 37 -22 5 -3 35.5753 124.776 33 22 -5 3 -71.2665 113.984 37 22 5 3 116.299 137.457 24 -22 5 -4 222.352 114.630 33 22 -5 4 159.101 106.329 37 22 5 4 209.104 145.043 24 -22 5 -5 62.7265 89.9944 33 22 -5 5 108.890 95.2171 37 22 5 5 195.849 111.977 24 22 5 6 101.528 86.4624 24 -22 5 -6 167.170 83.6721 33 23 0 -27 317.308 193.215 20 23 0 -26 182.550 226.501 20 23 0 -25 -611.624 322.876 20 23 0 -25 -97.0199 136.299 31 23 0 -24 5059.70 539.268 20 23 0 -24 4881.06 429.965 31 23 0 -23 62.0900 177.037 31 23 0 -23 54.1131 280.305 10 23 0 -22 9787.77 682.874 31 23 0 -22 10967.9 802.654 10 23 0 -21 -273.148 239.051 31 23 0 -21 -128.980 196.661 16 23 0 -21 199.677 331.329 10 23 0 -20 4936.11 561.780 31 23 0 -20 4635.01 629.203 10 23 0 -20 5189.16 499.247 16 23 0 -19 80.5269 230.499 31 23 0 -19 -513.518 368.514 10 23 0 -18 2477.41 448.934 31 23 0 -18 3192.50 556.180 10 23 0 -17 -273.059 294.023 31 23 0 -17 -11.2517 323.103 10 23 0 -16 1011.82 441.233 10 23 0 -15 -71.7113 348.148 10 23 0 -14 7390.64 712.046 17 23 0 -14 7579.95 801.119 10 23 0 -13 -116.801 254.329 17 23 0 -13 -14.1222 317.751 10 23 0 -12 -31.0803 256.584 17 23 0 -12 -53.8686 349.216 10 23 0 -11 -16.3150 311.194 10 23 0 -11 -238.980 225.513 24 23 0 -11 -25.6365 273.146 17 23 0 -10 19621.5 1249.51 10 23 0 -10 17423.4 851.571 24 23 0 -10 18168.7 1112.97 17 23 0 -9 -405.505 327.930 10 23 0 -9 269.845 297.951 17 23 0 -9 107.676 199.796 24 23 0 -8 17747.5 873.785 24 -23 0 8 17638.0 1710.58 27 23 0 -8 20875.2 1279.25 10 23 0 -8 19483.8 1155.37 17 23 0 -8 20083.1 1742.63 3 23 0 -7 27.4470 180.688 24 -23 0 7 -981.133 438.659 27 23 0 -7 25.4654 285.272 10 23 0 -7 268.286 325.827 17 23 0 -7 -863.352 442.529 3 23 0 -6 3271.16 417.431 24 -23 0 6 3890.92 929.280 27 23 0 -6 4227.17 644.960 10 23 0 -6 3704.05 757.076 3 23 0 -6 4405.64 608.192 17 -23 0 5 497.020 591.476 27 23 0 -5 97.6370 272.700 17 23 0 -5 19.6598 279.736 3 23 0 -5 47.3598 198.409 24 -23 0 4 -729.745 537.773 27 23 0 -4 -386.451 319.658 17 23 0 -4 223.083 293.201 3 23 0 -4 205.271 196.446 24 -23 0 3 -809.833 640.154 27 23 0 -3 -193.816 273.048 17 23 0 -3 -503.520 442.594 3 23 0 -3 80.7269 189.101 24 23 0 -2 -73.4106 337.998 3 23 0 -2 53.3551 267.452 17 23 0 -2 366.693 227.872 24 23 0 -1 -322.082 320.991 17 23 0 -1 -53.9668 200.045 24 23 0 0 2657.76 384.509 24 23 0 1 -136.098 171.759 24 23 0 2 23666.7 981.190 24 23 0 3 65.8550 187.279 24 23 0 4 112.856 152.682 24 -23 0 -4 634.310 237.882 9 23 0 5 -141.651 174.365 24 -23 0 -5 304.643 221.354 9 23 0 6 1779.51 268.010 24 -23 0 -6 1530.96 319.651 9 -23 0 -7 51.2834 185.761 9 -23 0 -8 1024.52 266.680 9 -23 0 -9 -176.202 219.158 9 -23 0 -10 5169.91 461.347 9 -23 0 -11 -453.244 245.762 9 -23 0 -12 2395.45 321.575 9 -23 0 -13 93.8813 185.030 9 -23 0 -14 74.6611 163.793 9 -23 0 -15 153.176 148.639 9 23 0 16 271.796 181.347 17 -23 0 -16 204.418 114.949 9 23 -1 -27 113.396 162.736 20 23 1 -27 249.877 127.800 31 23 1 -26 2068.55 258.593 20 23 -1 -26 2485.02 352.211 20 23 1 -26 1794.87 264.480 31 23 1 -25 370.231 221.280 31 23 -1 -25 610.285 173.487 16 23 1 -25 909.453 252.726 20 23 -1 -25 651.420 296.602 20 23 -1 -25 456.152 132.765 35 23 1 -24 228.214 229.942 31 23 -1 -24 -14.4812 178.176 16 23 1 -24 -479.136 306.633 20 23 -1 -24 52.0374 271.220 20 23 -1 -24 140.960 126.651 35 23 -1 -23 -25.9612 190.990 16 23 -1 -23 97.0011 156.735 35 23 1 -23 369.341 269.563 31 23 1 -23 -627.792 296.489 20 23 -1 -23 -175.225 346.949 20 23 -1 -23 -277.704 279.294 10 23 1 -23 230.620 269.024 10 23 -1 -22 2870.39 322.099 35 23 -1 -22 2748.54 389.402 16 23 -1 -22 2845.87 448.956 10 23 1 -22 2466.32 416.955 10 23 1 -22 2445.45 430.663 31 23 1 -21 671.844 318.662 31 23 -1 -21 704.935 216.410 35 23 -1 -21 1003.94 291.735 16 23 -1 -21 940.117 359.656 10 23 1 -21 441.380 305.163 10 23 -1 -20 783.772 317.191 16 23 -1 -20 397.241 309.216 10 23 1 -20 618.979 280.154 10 23 1 -20 366.063 298.835 31 23 -1 -19 592.956 298.685 10 23 1 -19 979.391 360.575 10 23 1 -19 1335.68 404.091 31 23 -1 -18 312.473 305.552 10 23 1 -18 352.989 328.928 10 23 1 -18 85.4039 312.393 31 23 -1 -17 2859.54 528.671 10 23 1 -17 2440.41 505.379 10 23 1 -17 2228.33 514.756 31 23 -1 -16 10437.3 889.833 10 23 1 -16 11991.9 939.008 10 23 -1 -15 -32.0983 326.092 10 23 1 -15 361.148 341.906 10 23 -1 -14 1985.84 443.911 10 23 1 -14 2061.12 478.079 10 23 -1 -14 1828.85 418.085 17 23 1 -13 124.166 152.386 24 23 1 -13 -188.479 330.006 10 23 -1 -13 -146.311 331.592 10 23 -1 -13 379.295 355.565 17 23 1 -12 7109.11 533.518 24 23 1 -12 6553.15 769.387 10 23 -1 -12 7006.40 774.950 10 23 -1 -12 6551.00 705.408 17 23 1 -11 -82.6014 206.216 24 23 -1 -11 367.954 327.901 10 23 1 -11 97.4046 300.196 10 23 -1 -11 -64.4960 309.552 17 23 1 -10 6810.69 548.562 24 23 1 -10 7262.44 766.362 10 23 -1 -10 6677.80 753.379 10 23 1 -10 6724.04 618.226 17 23 -1 -10 7174.87 756.443 17 23 1 -9 9582.02 638.717 24 23 -1 -9 9786.79 874.818 10 23 1 -9 10016.4 901.528 10 23 -1 -9 9972.82 866.217 17 23 1 -9 8885.50 723.988 17 23 1 -8 41.6942 172.338 24 23 -1 -8 -21.5760 298.492 10 23 1 -8 -11.1056 342.053 10 23 -1 -8 294.237 335.802 17 23 1 -8 309.522 256.929 17 23 1 -7 8224.49 598.510 24 23 -1 -7 7584.61 778.207 10 23 1 -7 8817.77 877.522 10 23 -1 -7 9450.63 871.180 17 23 1 -7 9255.78 760.196 17 23 1 -6 -174.768 191.291 24 23 -1 -6 101.409 271.249 17 23 1 -6 311.705 288.721 17 23 1 -6 -69.8325 324.543 10 23 -1 -6 -93.7518 300.960 10 23 -1 -5 6787.37 587.665 24 23 1 -5 6907.01 568.309 24 -23 1 5 6074.42 998.300 27 23 -1 -5 7489.03 785.005 17 23 1 -5 6429.75 648.236 17 23 -1 -5 6508.91 727.488 10 23 -1 -4 89.4767 200.155 24 23 1 -4 112.954 190.238 24 -23 1 4 553.742 592.025 27 23 -1 -4 218.072 298.041 10 23 1 -4 39.7927 268.686 17 23 -1 -4 -190.385 326.733 17 23 1 -3 1640.27 375.870 17 23 -1 -3 2063.54 491.278 17 23 -1 -3 1495.02 307.371 24 23 1 -3 1380.14 318.908 24 23 -1 -2 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1405.63 333.912 9 -23 1 -10 1684.57 283.692 9 -23 1 -11 454.085 181.238 9 -23 -1 -11 440.409 234.242 9 -23 1 -12 2302.52 285.265 9 -23 -1 -12 2596.85 351.051 9 23 -1 13 330.738 250.171 17 -23 1 -13 -142.552 151.460 9 -23 -1 -13 84.5322 202.158 9 23 -1 14 379.547 217.360 17 -23 1 -14 81.7547 123.408 9 -23 -1 -14 378.757 194.118 9 23 -1 15 116.365 142.476 17 -23 1 -15 170.812 117.126 9 -23 -1 -15 385.234 161.176 9 -23 -1 -16 890.195 162.506 9 23 -2 -26 1719.52 229.702 20 23 2 -26 1582.90 224.088 31 23 -2 -26 1650.86 235.869 22 23 -2 -25 3415.93 271.780 35 23 -2 -25 3989.71 335.970 16 23 2 -25 3890.79 367.648 31 23 -2 -25 3678.58 356.274 20 23 -2 -24 410.042 153.855 35 23 -2 -24 2.14770 181.276 16 23 -2 -24 145.798 203.558 20 23 2 -24 410.879 235.154 31 23 -2 -23 110.778 177.475 35 23 -2 -23 -79.5651 230.661 16 23 -2 -23 105.081 211.193 20 23 2 -23 369.365 260.658 31 23 -2 -22 660.364 230.861 35 23 -2 -22 371.036 273.608 20 23 2 -22 178.439 278.661 31 23 -2 -22 109.749 232.077 16 23 2 -22 146.716 130.232 18 23 2 -21 4994.48 454.728 10 23 -2 -21 5031.64 508.869 10 23 -2 -21 5349.59 547.946 16 23 2 -21 5017.05 399.653 18 23 2 -21 5310.01 570.528 31 23 2 -20 3811.11 535.123 31 23 -2 -20 3831.49 470.858 10 23 2 -20 3980.49 443.094 10 23 -2 -20 3729.30 509.044 16 23 2 -19 623.592 358.742 31 23 -2 -19 1069.16 327.169 10 23 2 -19 431.126 241.465 10 -23 2 19 253.034 136.927 24 23 2 -18 1541.40 432.041 31 23 -2 -18 1658.33 358.379 10 23 2 -18 2286.94 376.376 10 -23 2 18 1835.00 279.794 24 -23 2 17 3081.15 360.698 24 23 2 -17 4268.06 601.265 31 23 2 -17 3662.22 414.447 19 23 -2 -17 3602.04 511.283 10 23 2 -17 3460.65 455.067 10 23 2 -16 472.397 386.232 31 -23 2 16 149.410 180.306 24 23 2 -16 398.927 195.208 19 23 -2 -16 300.965 293.363 10 23 2 -16 321.533 275.276 10 23 2 -15 2921.82 379.449 19 23 -2 -15 3031.26 484.282 10 23 2 -15 2904.47 487.012 10 23 2 -14 1905.17 328.531 19 23 -2 -14 1928.80 400.612 10 23 2 -14 1650.10 388.430 10 23 2 -13 -13.9474 175.431 19 23 2 -13 -23.4548 130.119 24 23 -2 -13 -446.111 275.563 10 23 2 -13 -64.3624 255.244 10 23 2 -12 476.349 225.752 19 23 2 -12 159.291 255.912 10 23 -2 -12 550.539 303.492 10 23 -2 -12 825.552 397.795 17 23 2 -12 510.203 198.459 24 23 2 -11 944.862 357.418 10 23 -2 -11 1167.32 374.253 10 23 -2 -11 1129.61 421.572 17 23 2 -11 853.969 239.036 24 23 2 -10 906.316 344.248 10 23 -2 -10 635.330 275.180 10 23 -2 -10 1418.31 423.735 17 23 2 -10 1105.43 262.364 24 23 -2 -9 969.501 328.886 10 23 2 -9 837.638 311.872 10 23 -2 -9 1004.81 380.671 17 23 2 -9 985.291 239.034 24 23 -2 -8 1221.84 298.693 10 23 2 -8 1381.96 419.987 10 23 -2 -8 1057.83 405.121 17 23 2 -8 1005.28 252.033 24 23 -2 -7 1759.62 421.004 10 23 2 -7 1025.59 386.199 10 23 -2 -7 1589.27 458.652 17 23 2 -7 1667.04 312.605 24 23 -2 -6 -8.69113 244.694 10 23 2 -6 75.8271 291.992 10 23 -2 -6 -143.185 297.583 17 23 2 -6 216.985 192.556 24 23 -2 -5 846.376 297.746 10 23 2 -5 971.024 407.986 10 23 -2 -5 579.891 361.744 17 23 2 -5 786.015 263.514 24 23 -2 -4 5095.85 595.052 10 23 -2 -4 5792.81 713.819 17 23 2 -4 5944.70 540.324 24 23 -2 -3 1219.79 343.190 10 23 -2 -3 1089.51 389.597 17 23 2 -3 1270.36 308.179 24 23 -2 -2 -222.046 266.613 10 23 -2 -2 -6.51859 311.712 17 23 2 -2 54.8686 201.846 24 23 -2 -1 13565.3 933.344 10 23 -2 -1 13458.8 1002.74 17 23 2 -1 12848.6 857.239 17 23 2 -1 13551.7 775.122 24 23 -2 0 1356.44 349.711 10 23 2 0 1202.39 305.167 17 23 -2 0 1387.16 415.118 17 23 2 0 1395.34 312.082 24 23 -2 1 1226.40 394.690 17 23 2 1 1286.24 301.091 24 23 -2 2 -4.47021 295.957 17 -23 -2 -2 21.1188 143.392 13 23 2 2 -27.6381 198.600 24 23 -2 3 -27.1816 291.213 17 -23 -2 -3 300.534 166.665 13 23 2 3 294.182 198.077 24 23 -2 4 1644.48 403.119 17 -23 -2 -4 1931.85 308.575 13 23 2 4 1409.21 318.526 24 23 -2 5 2384.19 466.193 17 -23 -2 -5 2048.57 298.129 13 23 2 5 2245.45 350.962 24 23 -2 6 187.318 276.015 17 -23 -2 -6 54.3217 200.158 13 23 2 6 -88.2505 169.458 24 -23 -2 -7 5757.78 468.540 13 23 -2 7 6097.50 651.678 17 23 2 7 6378.54 484.507 24 23 2 8 3881.68 367.104 24 -23 -2 -8 3646.51 372.023 13 23 -2 8 3383.84 467.860 17 23 2 9 112.448 118.663 24 23 -2 9 247.855 256.794 17 -23 -2 -9 131.808 181.535 13 23 -2 10 -224.923 265.507 17 -23 -2 -10 177.101 251.318 9 -23 -2 -10 431.025 233.849 13 23 -2 11 5433.40 467.138 17 -23 -2 -11 6249.48 444.300 13 -23 -2 -11 6630.13 511.481 9 -23 -2 -12 514.757 186.602 13 23 -2 12 1139.59 255.364 17 -23 -2 -12 448.144 230.008 9 -23 -2 -13 -18.2254 177.823 9 -23 -2 -14 -44.0853 152.464 9 -23 -2 -15 1555.71 193.241 9 23 3 -24 1101.22 210.342 31 23 -3 -24 1457.11 221.207 22 23 -3 -24 1414.63 187.652 35 23 -3 -23 490.809 176.724 35 23 3 -23 206.393 120.662 18 23 -3 -23 439.235 194.849 16 23 3 -23 268.613 179.270 31 23 -3 -22 -61.2527 129.054 20 23 -3 -22 64.3229 194.531 16 23 3 -22 -148.481 141.323 18 23 3 -22 27.8810 195.188 31 23 -3 -21 292.842 180.766 20 23 -3 -21 -110.279 228.019 16 23 3 -21 124.940 221.787 31 23 -3 -20 1185.42 328.573 16 23 3 -20 810.268 283.009 31 -23 3 20 848.171 165.641 24 23 -3 -20 818.022 225.266 20 23 -3 -19 2782.11 454.181 16 -23 3 19 2029.56 245.675 24 23 3 -19 2663.14 423.962 31 23 -3 -19 2534.32 367.418 20 -23 3 18 2716.48 307.151 24 23 -3 -18 3141.14 487.817 16 23 3 -18 2979.56 367.333 19 23 3 -18 2862.76 452.509 31 23 3 -17 30.8540 173.568 19 23 3 -17 163.486 284.387 31 -23 3 17 225.313 175.835 24 23 3 -16 115.885 209.221 19 23 3 -16 282.343 299.193 31 -23 3 16 85.5173 182.073 24 23 3 -15 402.697 213.718 19 23 3 -15 846.271 368.003 31 -23 3 15 769.264 251.109 24 23 3 -14 2694.39 379.621 19 23 3 -14 2752.31 486.671 31 -23 3 14 2636.80 383.587 24 23 -3 -13 195.126 145.905 37 23 3 -13 -4.86697 225.209 19 -23 3 13 115.039 205.421 24 23 -3 -12 3130.96 339.244 37 -23 3 12 2929.62 404.993 24 23 3 -12 3139.32 431.514 19 23 3 -11 808.077 216.171 24 23 -3 -11 989.757 214.159 37 -23 3 11 1258.97 309.642 24 23 3 -10 3557.88 370.663 24 23 -3 -10 3097.02 359.328 37 23 -3 -10 3283.56 537.807 17 -23 3 10 3256.38 422.840 24 23 -3 -9 1051.05 388.615 17 23 -3 -9 835.051 239.886 37 23 3 -9 785.197 234.890 24 23 -3 -8 1170.40 281.302 37 23 3 -8 1600.17 366.643 10 23 3 -8 1724.65 305.009 24 23 -3 -8 1436.87 423.751 17 23 3 -7 407.858 227.468 10 23 3 -7 820.959 249.838 24 23 -3 -7 554.337 330.081 17 23 3 -6 318.599 236.101 10 23 3 -6 61.1433 176.013 24 23 -3 -6 452.885 330.104 17 23 3 -5 812.380 307.210 10 23 3 -5 1305.74 300.811 24 23 -3 -5 1224.28 350.474 17 23 3 -4 102.239 239.709 10 23 3 -4 -31.7621 211.744 24 23 -3 -4 -205.681 321.786 17 23 3 -3 1908.45 416.378 10 23 3 -3 1767.08 342.372 24 23 -3 -3 1586.34 402.626 17 23 3 -2 19.8043 259.835 10 23 -3 -2 -235.668 289.297 17 23 3 -2 -166.556 212.181 24 23 -3 -1 5433.35 614.398 17 23 3 -1 5698.48 530.194 24 23 -3 0 2013.93 425.085 17 23 3 0 2594.45 401.202 24 -23 3 -1 3401.48 341.916 24 23 -3 1 3226.39 494.523 17 23 3 1 3233.05 430.019 24 23 -3 2 2669.96 455.981 17 23 3 2 2764.32 402.224 24 23 -3 3 8455.88 700.618 17 23 3 3 9406.06 635.175 24 -23 -3 -4 622.032 164.551 13 23 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197.081 31 23 4 -16 142.344 170.534 19 23 -4 -16 544.524 246.353 16 -23 4 16 468.445 175.571 24 23 4 -16 296.382 181.208 31 23 4 -15 720.657 237.288 31 23 -4 -15 484.104 239.756 16 23 -4 -15 753.292 145.664 37 -23 4 15 612.954 206.357 24 23 4 -15 462.530 217.023 19 23 4 -14 1439.34 308.093 31 23 -4 -14 1563.62 205.008 37 23 4 -14 1588.22 303.060 19 -23 4 14 1287.06 267.033 24 23 -4 -14 1890.14 346.927 16 23 4 -13 7424.32 558.019 19 23 4 -13 7411.44 584.625 31 23 -4 -13 7594.62 441.943 37 -23 4 13 7104.34 500.866 24 23 4 -12 759.373 261.110 19 23 -4 -12 978.913 207.399 37 -23 4 12 726.515 244.053 24 23 4 -12 660.756 258.719 31 23 4 -11 29.8133 238.627 19 23 -4 -11 156.430 175.294 37 -23 4 11 -64.7896 211.479 24 23 4 -11 -143.050 228.586 31 23 -4 -10 1020.68 249.015 37 -23 4 10 596.964 253.610 24 23 4 -10 1390.96 364.408 31 23 -4 -9 1857.47 298.347 37 -23 4 9 2136.53 325.413 24 23 4 -9 1776.66 238.618 24 23 -4 -8 2608.48 345.262 37 -23 4 8 2633.51 369.957 24 23 4 -8 2868.02 307.702 24 23 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23 5 -14 1157.60 195.249 19 23 5 -13 -95.3023 141.460 19 -23 5 13 -29.2532 119.335 24 23 -5 -13 -5.15607 88.2191 37 23 5 -12 465.449 172.435 19 -23 5 12 379.628 150.320 24 23 -5 -12 372.690 118.263 37 23 5 -11 770.528 216.583 19 -23 5 11 779.880 174.100 24 23 -5 -11 754.392 157.482 37 23 5 -10 1105.48 228.027 19 -23 5 10 1134.20 201.636 24 23 -5 -10 1282.45 189.021 37 23 5 -9 1015.58 232.588 19 -23 5 9 873.040 182.646 24 23 -5 -9 782.823 175.688 37 -23 5 8 119.839 137.315 24 23 -5 -8 -7.81131 135.202 37 23 5 -8 154.974 187.055 19 -23 5 8 -10.2996 65.4739 33 23 5 -7 512.810 206.942 19 23 5 -7 -15.4523 69.0990 24 23 -5 -7 542.168 180.139 37 -23 5 7 383.453 111.519 33 -23 5 7 557.849 149.405 24 23 5 -6 82.5194 93.3050 24 -23 5 6 208.306 120.153 24 23 -5 -6 -51.4186 148.840 37 -23 5 6 253.716 115.514 33 -23 5 5 1309.51 181.587 33 23 -5 -5 1356.39 230.956 37 23 5 -5 1201.27 174.497 24 -23 5 5 1273.83 173.574 24 -23 5 4 3717.40 244.137 24 23 5 -4 4089.28 298.670 24 -23 5 4 3457.09 274.978 33 23 -5 -4 3842.41 336.844 37 23 5 -3 1627.96 209.103 24 -23 5 3 1603.21 210.956 33 23 -5 -3 2165.36 276.435 37 23 5 -2 200.320 134.327 24 -23 5 2 -19.7844 117.888 33 23 -5 -2 197.526 163.390 37 23 5 -1 1993.90 235.144 24 23 -5 -1 2377.03 265.633 37 -23 5 1 2010.24 229.060 33 23 5 0 3306.67 280.593 24 -23 5 0 3020.27 263.334 33 23 -5 0 3115.03 286.990 37 23 5 1 6.71671 123.583 24 -23 5 -1 27.0542 111.911 33 23 -5 1 176.626 135.381 37 -23 5 -2 83.3154 108.671 33 23 -5 2 -120.247 115.170 37 23 5 2 64.6400 116.764 24 -23 5 -3 293.891 108.888 33 23 -5 3 337.249 114.456 37 23 5 3 577.364 145.168 24 -23 5 -4 64.7981 82.6089 33 23 5 4 89.6462 105.914 24 24 0 -27 319.401 166.121 20 24 0 -26 4514.63 396.987 20 24 0 -25 -419.506 274.122 20 24 0 -25 -184.521 136.555 31 24 0 -24 15209.0 676.389 31 24 0 -24 16635.8 854.366 20 24 0 -23 -186.647 271.318 10 24 0 -23 -150.878 169.674 31 24 0 -22 2924.83 496.567 10 24 0 -22 2500.59 362.003 31 24 0 -21 -111.135 322.962 10 24 0 -21 -383.903 249.373 31 24 0 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0 -5 53.0608 197.094 24 24 0 -4 19534.1 1186.53 17 24 0 -4 18492.3 926.857 24 24 0 -3 -12.8651 319.513 17 24 0 -3 39.1242 196.218 24 24 0 -2 57.9633 295.320 17 24 0 -2 386.817 250.874 24 24 0 -1 233.777 354.762 17 24 0 -1 226.852 215.345 24 24 0 0 8505.49 802.469 17 24 0 0 8655.33 647.020 24 24 0 1 -860.548 421.593 17 24 0 1 -233.926 204.452 24 24 0 2 2457.90 357.072 24 24 0 3 -76.9664 180.439 24 24 0 4 230.517 160.867 24 -24 0 -5 86.4151 172.413 9 24 0 5 -105.111 167.397 24 -24 0 -6 31.3411 187.291 9 -24 0 -7 55.6598 169.015 9 -24 0 -8 2555.51 349.731 9 -24 0 -9 130.812 190.433 9 -24 0 -10 24.1680 175.413 9 -24 0 -11 198.774 181.240 9 -24 0 -12 6222.94 432.427 9 -24 0 -13 -154.639 157.933 9 -24 0 -14 2046.28 231.139 9 24 0 14 2268.80 345.225 17 24 0 15 392.511 195.149 17 24 -1 -27 374.595 155.924 20 24 -1 -26 1188.77 207.600 22 24 1 -26 898.002 180.315 31 24 -1 -26 1558.81 257.403 20 24 1 -25 3169.22 317.920 20 24 1 -25 2763.78 320.978 31 24 -1 -25 3154.62 375.154 20 24 1 -24 331.304 213.617 31 24 -1 -24 258.117 166.583 16 24 -1 -24 358.997 264.291 20 24 1 -23 175.713 213.559 31 24 -1 -23 5.60405 268.613 20 24 -1 -23 -23.1532 171.872 16 24 1 -23 527.976 255.182 10 24 1 -22 -76.4888 247.693 31 24 -1 -22 167.401 217.277 16 24 -1 -22 -80.5458 136.738 35 24 -1 -22 5.04722 267.659 10 24 1 -22 -66.9880 252.514 10 24 -1 -21 484.826 332.013 10 24 1 -21 721.536 311.221 10 24 -1 -21 501.162 265.415 16 24 -1 -21 602.008 188.098 35 24 1 -21 439.253 279.788 31 24 -1 -20 -39.5951 229.152 16 24 -1 -20 -207.937 333.694 10 24 1 -20 600.432 344.639 10 24 1 -20 -128.176 261.726 31 24 -1 -19 234.425 310.624 10 24 1 -19 -105.514 271.476 10 24 1 -19 -586.338 365.672 31 24 -1 -18 2759.94 509.444 10 24 1 -18 2613.89 481.475 10 24 1 -18 1641.13 406.074 31 -24 1 18 2506.33 310.033 24 24 -1 -17 57.1564 287.172 10 24 1 -17 273.798 341.757 10 24 1 -17 -189.404 337.842 31 24 1 -16 7109.41 758.499 10 24 -1 -16 6068.67 687.156 10 24 1 -15 12029.7 923.448 10 24 -1 -15 11065.8 926.944 10 24 -1 -14 308.530 300.714 10 24 1 -14 339.071 372.017 10 24 -1 -14 219.088 301.269 17 24 -1 -13 5487.23 697.912 10 24 1 -13 5043.68 659.270 10 24 -1 -13 6180.74 694.413 17 24 1 -13 5381.68 461.284 24 24 -1 -12 11741.8 955.105 10 24 1 -12 13953.3 1045.16 10 24 -1 -12 12482.3 963.045 17 24 1 -12 12317.0 691.673 24 24 -1 -11 13479.9 1030.15 10 24 1 -11 14170.9 1066.42 10 24 -1 -11 13940.9 1005.06 17 24 1 -11 13698.5 745.501 24 24 -1 -10 366.819 346.474 10 24 1 -10 416.082 341.592 10 24 -1 -10 190.794 311.675 17 24 1 -10 453.261 211.598 17 24 1 -10 305.341 187.722 24 24 -1 -9 12351.4 980.757 10 24 1 -9 12489.5 1020.21 10 24 -1 -9 14192.9 1037.84 17 24 1 -9 12817.5 863.286 17 24 1 -9 12425.4 729.666 24 24 -1 -8 7103.14 772.098 10 24 1 -8 7686.44 838.437 10 24 1 -8 7705.91 706.591 17 24 -1 -8 6807.58 759.011 17 24 1 -8 6822.49 553.765 24 24 -1 -7 -230.061 325.512 10 24 1 -7 106.699 332.242 10 24 -1 -7 281.904 355.445 17 24 1 -7 -184.251 280.813 17 24 1 -7 228.521 222.767 24 24 1 -6 3117.12 560.265 10 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4 -1 179.140 200.270 24 24 4 0 -176.535 200.994 24 24 4 1 43.3245 180.274 24 24 4 2 1541.98 280.486 24 24 4 3 1424.20 257.972 24 24 4 4 2359.06 283.322 24 24 4 5 129.939 152.500 24 -24 4 -6 4960.10 288.565 33 24 4 6 5295.21 347.692 24 24 4 7 449.445 127.484 24 24 -4 7 357.821 124.913 37 -24 4 -7 586.588 112.838 33 -24 -4 -8 3247.59 263.135 9 -24 5 14 677.682 123.206 24 24 5 -14 875.441 153.181 19 -24 5 13 413.121 120.959 24 24 5 -13 402.223 138.028 19 -24 5 12 901.916 157.716 24 24 5 -12 523.038 145.629 19 24 -5 -12 755.820 116.895 37 -24 5 11 149.040 115.837 24 24 -5 -11 277.894 104.996 37 24 5 -11 75.2491 130.948 19 24 -5 -10 3419.89 244.516 37 24 5 -10 3346.26 296.961 19 -24 5 10 3623.15 262.700 24 24 -5 -9 724.434 147.316 37 24 5 -9 429.797 166.506 19 -24 5 9 653.506 149.137 24 24 -5 -8 1724.14 203.897 37 -24 5 8 1444.58 180.993 24 24 5 -8 1435.27 233.290 19 24 -5 -7 828.290 179.310 37 24 5 -7 640.518 189.381 19 -24 5 7 762.398 112.883 33 -24 5 7 792.317 137.544 24 -24 5 6 671.170 131.077 24 24 5 -6 604.805 111.825 24 -24 5 6 689.787 123.098 33 24 -5 -6 629.541 165.150 37 24 5 -6 551.585 185.833 19 24 5 -5 815.914 135.828 24 24 -5 -5 751.438 168.770 37 -24 5 5 881.165 138.599 33 -24 5 5 821.202 126.696 24 24 -5 -4 2411.67 249.988 37 24 5 -4 2245.34 204.661 24 -24 5 4 2518.75 212.142 33 24 -5 -3 353.924 142.901 37 24 5 -3 394.922 121.965 24 -24 5 3 475.084 129.748 33 24 -5 -2 1014.88 183.861 37 24 5 -2 1094.35 161.646 24 -24 5 2 1058.48 157.868 33 24 -5 -1 289.824 139.489 37 24 5 -1 88.8254 108.589 24 -24 5 1 144.098 107.958 33 24 -5 0 -51.6690 104.810 37 24 5 0 95.1894 109.952 24 -24 5 0 35.1854 92.3280 33 24 -5 1 120.545 110.498 37 24 5 1 -10.0969 98.0197 24 -24 5 -1 159.139 95.5625 33 24 -5 2 440.097 109.987 37 -24 5 -2 354.041 107.363 33 24 5 2 130.550 92.3866 24 25 0 -26 614.259 194.870 20 25 0 -25 -388.722 237.867 20 25 0 -24 2413.02 354.946 20 25 0 -24 2395.97 255.997 31 25 0 -23 -772.381 320.507 20 25 0 -23 -217.225 150.917 31 25 0 -23 -174.371 255.532 10 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342.546 10 25 0 -6 1479.25 332.577 24 25 0 -6 1608.47 433.747 17 25 0 -6 1247.25 471.203 10 25 0 -5 -87.0622 230.096 24 25 0 -5 348.091 323.759 17 25 0 -5 35.2707 348.264 10 25 0 -4 2490.59 372.543 24 25 0 -4 3364.91 555.770 17 25 0 -3 179.794 232.190 24 25 0 -3 -0.91968 308.992 17 25 0 -2 20110.2 940.013 24 25 0 -2 20203.6 1202.03 17 25 0 -1 75.0443 192.073 24 25 0 -1 10.0743 334.959 17 25 0 0 1360.24 302.341 24 25 0 0 1125.12 405.521 17 25 0 1 12.4193 189.873 24 25 0 1 -142.819 319.443 17 25 0 2 4005.85 424.419 24 25 0 2 4306.19 622.944 17 25 0 3 143.272 174.877 24 25 0 3 -596.713 388.088 17 25 0 4 6105.59 470.618 24 25 0 5 39.4999 143.599 24 -25 0 -6 6719.81 497.832 9 -25 0 -7 185.637 186.524 9 -25 0 -8 5632.44 440.519 9 -25 0 -9 -34.3984 158.753 9 -25 0 -10 -83.7540 150.288 9 25 0 11 290.042 313.986 17 -25 0 -11 101.106 149.675 9 25 0 12 2379.67 377.716 17 -25 0 -12 1379.67 200.181 9 25 0 13 -279.100 235.927 17 -25 0 -13 130.799 126.070 9 25 0 14 -95.4773 167.469 17 25 -1 -26 1141.29 206.347 20 25 -1 -25 358.114 202.096 20 25 1 -25 140.964 140.576 31 25 1 -24 3742.17 371.241 31 25 1 -24 3364.96 321.903 20 25 -1 -24 4432.65 436.609 20 25 -1 -24 3924.95 312.098 16 25 -1 -23 148.709 155.906 16 25 1 -23 623.933 257.556 10 25 1 -23 731.607 251.922 31 25 1 -23 -206.616 229.510 20 25 -1 -23 438.240 258.436 20 25 -1 -22 5265.59 522.694 10 25 1 -22 4401.74 463.537 10 25 1 -22 4385.71 481.071 31 25 -1 -22 4560.42 443.162 16 25 1 -21 1336.86 310.892 31 25 -1 -21 1677.04 321.966 16 25 -1 -21 1825.25 390.293 10 25 1 -21 1741.39 375.137 10 25 1 -20 711.678 287.023 31 25 -1 -20 1799.28 361.831 16 25 -1 -20 1125.51 363.779 10 25 1 -20 1946.88 401.413 10 25 1 -19 1288.07 374.086 31 25 -1 -19 687.564 310.028 10 25 1 -19 1025.33 376.086 10 25 1 -18 -82.7275 311.298 31 -25 1 18 311.826 163.532 24 25 -1 -18 648.621 361.290 10 25 1 -18 310.659 303.116 10 25 -1 -17 -259.154 298.946 10 25 1 -17 288.100 305.205 10 25 1 -17 -405.711 325.151 31 25 -1 -16 -110.232 300.914 10 25 1 -16 23.7380 297.303 10 25 -1 -15 440.217 380.632 10 25 1 -15 568.371 371.422 10 25 -1 -14 2354.90 503.918 10 25 1 -14 2192.09 500.675 10 25 -1 -13 10356.5 880.325 10 25 1 -13 11481.7 960.674 10 25 -1 -13 10767.4 880.762 17 25 1 -12 612.248 393.149 10 25 -1 -12 361.332 347.503 10 25 -1 -12 -61.1236 337.032 17 25 1 -12 392.715 218.097 24 25 -1 -11 8303.13 809.605 10 25 1 -11 8892.75 867.431 10 25 -1 -11 9091.33 819.588 17 25 1 -11 9174.73 628.336 24 25 -1 -10 49.3738 338.997 10 25 1 -10 -537.781 472.097 10 25 1 -10 218.944 254.437 17 25 -1 -10 104.673 319.892 17 25 1 -10 5.87656 185.774 24 25 -1 -9 1385.26 437.706 10 25 1 -9 1396.38 439.329 10 25 -1 -9 1131.40 417.568 17 25 1 -9 1931.10 392.019 17 25 1 -9 1232.36 284.041 24 25 -1 -8 -101.678 351.647 10 25 1 -8 -41.7431 365.786 10 25 -1 -8 7.50451 321.581 17 25 1 -8 355.440 254.952 17 25 1 -8 -49.0907 194.608 24 25 -1 -7 1620.96 450.856 10 25 1 -7 2112.88 508.494 10 25 -1 -7 2286.35 509.390 17 25 1 -7 2222.81 423.354 17 25 1 -7 2078.90 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503.248 329.646 10 29 0 -16 11571.8 688.289 31 29 0 -16 13006.3 839.390 10 29 0 -15 425.293 332.268 10 29 0 -15 -385.028 223.404 31 29 0 -14 1342.74 414.794 10 29 0 -13 -75.1628 354.876 10 29 0 -12 647.056 404.179 10 29 0 -12 466.095 254.810 17 29 0 -11 -128.999 354.112 10 29 0 -11 143.580 272.968 17 29 0 -10 653.024 397.613 10 29 0 -10 463.261 302.013 17 29 0 -9 34.1291 343.418 10 29 0 -9 -393.172 334.006 17 29 0 -8 -340.473 386.243 10 29 0 -8 -105.002 295.784 17 29 0 -7 -81.0667 338.873 10 29 0 -7 291.004 311.651 17 29 0 -6 6416.67 712.563 10 29 0 -6 6580.89 666.217 17 29 0 -5 190.468 344.732 10 29 0 -5 -370.332 312.107 17 29 0 -4 245.794 333.169 10 29 0 -4 400.470 281.686 17 29 0 -3 -5.71641 323.475 10 29 0 -3 -161.913 306.058 17 29 0 -2 6301.17 697.012 10 29 0 -2 6709.15 678.380 17 29 0 -1 -440.769 387.866 10 29 0 -1 -101.601 316.883 17 29 0 0 523.695 350.130 10 29 0 0 134.299 297.332 17 29 0 1 233.254 284.530 10 29 0 1 90.1637 287.728 17 29 0 2 1891.85 419.356 10 29 0 2 1725.21 411.901 17 29 0 3 69.2218 257.570 10 29 0 3 75.9459 312.623 17 29 0 4 69.6337 240.626 10 29 0 4 -134.077 268.369 17 29 0 5 44.0543 222.600 10 29 0 5 -20.2433 245.972 17 29 0 6 2115.34 337.028 10 29 0 6 1915.72 328.982 17 29 0 7 142.983 198.203 10 29 0 7 10.4527 212.703 17 29 0 8 264.303 167.762 10 29 0 8 60.2245 188.289 17 29 -1 -22 2349.73 267.167 20 29 1 -21 -421.755 188.276 20 29 -1 -21 -265.230 167.627 10 29 1 -21 129.827 150.889 10 29 1 -21 126.790 139.874 31 29 -1 -20 997.652 192.577 16 29 1 -20 807.729 219.830 31 29 -1 -20 760.933 217.915 10 29 1 -20 630.053 206.851 10 29 1 -19 232.179 179.308 31 29 -1 -19 545.792 190.131 16 29 -1 -19 685.948 220.560 10 29 1 -19 389.032 215.549 10 29 1 -18 36.4696 197.076 31 -29 1 18 -179.461 108.629 24 29 -1 -18 -52.9938 226.481 10 29 1 -18 130.434 232.744 10 29 1 -17 2014.78 357.898 31 -29 1 17 1984.40 234.167 24 29 -1 -17 1964.21 351.121 10 29 1 -17 2938.43 412.464 10 29 1 -16 154.060 248.206 31 29 -1 -16 -172.937 242.033 10 29 1 -16 123.666 240.302 10 29 1 -15 3421.60 469.466 31 29 -1 -15 4084.87 496.996 10 29 1 -15 4203.46 500.642 10 29 -1 -14 185.539 276.341 10 29 1 -14 -298.397 334.648 10 29 -1 -13 -75.5317 272.646 10 29 1 -13 496.436 353.408 10 29 -1 -12 150.857 275.692 10 29 1 -12 -54.2511 332.734 10 29 -1 -12 417.689 289.779 17 29 1 -11 -102.422 338.202 10 29 -1 -11 412.911 319.668 10 29 -1 -11 354.413 336.684 17 29 1 -10 149.706 325.680 10 29 -1 -10 -223.712 277.057 10 29 -1 -10 -22.6085 308.820 17 29 -1 -9 399.947 311.011 10 29 1 -9 -85.1300 350.320 10 29 1 -9 -333.549 208.775 17 29 -1 -9 288.447 327.078 17 29 -1 -8 1569.77 387.665 10 29 1 -8 1995.30 473.188 10 29 1 -8 1855.57 324.491 17 29 -1 -8 2148.38 460.877 17 29 1 -8 1700.95 318.145 24 29 -1 -7 904.847 333.059 10 29 1 -7 1577.42 459.666 10 29 1 -7 1075.23 289.466 17 29 -1 -7 1449.45 432.589 17 29 1 -7 1058.11 288.208 24 29 -1 -6 -165.372 264.055 10 29 1 -6 -473.815 421.316 10 29 -1 -6 230.482 326.856 17 29 1 -6 222.770 206.440 17 29 1 -6 270.439 269.470 24 29 -1 -5 396.581 275.403 10 29 1 -5 823.446 399.979 10 29 -1 -5 645.832 372.764 17 29 1 -5 1232.85 310.573 17 29 1 -5 915.842 278.393 24 29 -1 -4 2014.31 435.588 10 29 1 -4 1921.92 487.482 10 29 -1 -4 2205.05 447.145 17 29 1 -4 1895.90 362.371 17 29 1 -4 1992.24 347.160 24 29 -1 -3 53.9062 254.448 10 29 1 -3 -116.385 348.643 10 29 -1 -3 583.618 356.571 17 29 1 -3 451.349 251.053 17 29 1 -3 34.9657 208.070 24 29 -1 -2 375.340 294.494 10 29 1 -2 61.9680 334.556 10 29 -1 -2 -173.152 328.420 17 29 1 -2 291.687 257.309 17 29 1 -2 -8.74156 192.377 24 29 1 -1 186.823 359.398 10 29 -1 -1 197.609 243.294 10 29 -1 -1 241.772 348.716 17 29 1 -1 -158.747 242.285 17 29 1 -1 -33.3198 189.548 24 29 1 0 477.155 377.771 10 29 -1 0 -18.7125 241.149 10 29 -1 0 478.371 321.297 17 29 1 0 -61.9076 224.291 17 29 1 0 107.895 178.773 24 29 1 1 2893.15 484.922 10 29 -1 1 2771.95 401.232 10 29 -1 1 3152.75 500.843 17 29 1 1 2805.82 406.769 17 29 1 1 3041.18 331.418 24 29 1 2 1821.62 426.322 10 29 -1 2 1982.27 353.335 10 29 -1 2 2098.23 415.762 17 29 1 2 1844.13 355.555 17 29 1 2 1744.79 253.391 24 29 1 3 1031.48 347.810 10 29 -1 3 1263.01 276.414 10 29 -1 3 1022.04 312.368 17 29 1 3 1011.13 288.017 17 29 1 4 1258.08 360.093 10 29 -1 4 976.524 244.293 10 29 -1 4 754.948 315.382 17 29 1 4 935.066 263.447 17 29 1 5 459.156 275.554 10 29 -1 5 270.143 171.603 10 29 -1 5 499.131 245.639 17 29 1 5 428.446 236.213 17 29 1 6 1568.87 309.678 10 29 -1 6 931.384 194.465 10 29 -1 6 1140.77 275.210 17 29 1 6 1271.03 263.150 17 29 1 7 3649.30 382.471 10 29 1 7 3312.89 318.527 17 29 -1 7 3214.09 331.046 17 29 1 8 4736.41 366.792 10 29 -1 8 4301.78 332.132 17 29 -2 -20 1254.97 203.879 16 29 2 -20 1273.32 219.855 31 29 -2 -20 1069.71 183.230 20 29 -2 -19 1000.93 217.839 16 29 2 -19 1069.30 238.803 31 29 2 -18 1563.12 277.312 31 -29 2 18 1403.93 164.409 24 29 -2 -18 1723.29 275.601 16 29 -2 -18 1621.02 215.581 10 29 2 -18 1774.44 228.372 10 29 2 -17 662.579 262.327 31 29 -2 -17 34.6519 128.831 10 29 2 -17 692.545 195.452 10 -29 2 17 561.440 148.823 24 29 2 -16 173.015 230.519 31 29 -2 -16 9.22670 138.234 10 29 2 -16 254.029 180.843 10 -29 2 16 130.707 134.907 24 29 2 -15 406.649 292.203 31 29 2 -15 -75.0269 175.074 10 -29 2 15 142.098 139.466 24 29 2 -14 15.9234 259.288 31 -29 2 14 -283.236 167.054 24 29 -2 -14 -174.711 179.124 10 29 2 -14 -169.960 209.817 10 -29 2 13 569.114 203.424 24 29 -2 -13 912.332 216.145 10 29 2 -13 948.217 260.709 10 29 -2 -12 814.582 246.110 10 29 2 -12 1182.78 286.703 10 29 -2 -11 327.662 189.307 10 29 2 -11 308.573 244.291 10 29 -2 -10 642.410 235.344 10 29 2 -10 238.000 245.750 10 29 2 -10 464.285 189.843 24 29 -2 -10 556.115 312.875 17 29 2 -9 292.822 250.855 10 29 -2 -9 398.082 202.759 10 29 2 -9 574.104 204.791 24 29 -2 -9 481.979 315.311 17 29 2 -8 4836.19 547.371 10 29 -2 -8 4619.45 458.266 10 29 2 -8 5325.59 425.276 24 29 -2 -8 4735.57 546.381 17 29 2 -7 -70.5761 276.055 10 29 -2 -7 413.257 223.484 10 29 2 -7 504.371 235.273 24 29 -2 -7 404.171 316.301 17 29 2 -6 1521.41 367.610 10 29 -2 -6 1561.94 292.018 10 29 2 -6 1846.23 297.079 24 29 -2 -6 1595.71 392.030 17 29 2 -5 162.313 264.916 10 29 -2 -5 -40.1372 186.956 10 29 2 -5 208.720 207.051 24 29 -2 -5 -29.3081 291.338 17 29 2 -4 610.519 309.354 10 29 2 -4 835.121 231.119 24 29 -2 -4 889.988 350.133 17 29 2 -3 608.729 303.599 10 29 2 -3 656.592 237.245 24 29 -2 -3 417.982 305.937 17 29 2 -2 -38.8586 252.341 10 29 2 -2 295.011 196.438 24 29 -2 -2 214.892 254.927 17 29 2 -1 484.334 266.053 10 29 2 -1 434.364 212.392 24 29 -2 -1 499.284 285.401 17 29 2 0 240.434 249.295 10 29 2 0 237.444 178.705 24 29 -2 0 325.543 288.994 17 29 2 1 1314.72 328.732 10 29 2 1 1151.67 230.630 24 29 -2 1 1666.39 343.467 17 29 2 2 -118.230 227.341 10 29 2 2 -226.450 152.501 24 29 -2 2 302.247 237.718 17 29 2 3 2035.95 342.453 10 29 2 3 2044.24 234.169 24 29 -2 3 1992.81 316.408 17 29 2 4 511.524 220.905 10 29 2 4 145.611 102.875 24 29 -2 4 279.318 183.487 17 29 -2 5 1138.36 215.931 17 29 2 5 1344.43 240.805 10 29 2 6 427.286 171.725 10 29 -3 -17 241.125 152.121 16 29 3 -17 230.509 145.636 31 29 3 -16 145.741 153.026 31 -29 3 16 78.8924 93.1692 24 -29 3 15 302.473 130.481 24 29 -3 -15 478.107 197.168 16 29 3 -14 -179.685 198.211 31 -29 3 14 67.5933 121.120 24 29 3 -13 562.970 223.570 31 -29 3 13 407.651 146.645 24 29 3 -12 56.6415 197.425 31 -29 3 12 175.168 159.547 24 29 3 -11 384.489 249.046 31 -29 3 11 -19.2200 143.069 24 -29 3 10 2084.01 267.847 24 29 3 -10 1755.70 194.924 24 -29 3 9 32.4362 143.755 24 29 3 -9 -41.9096 115.392 24 -29 3 8 250.532 168.445 24 29 -3 -8 177.517 106.813 37 29 3 -8 -169.565 138.805 24 -29 3 7 79.3244 137.257 24 29 -3 -7 39.9974 103.407 37 29 3 -7 148.483 139.113 24 -29 3 6 747.977 178.517 24 29 3 -6 926.747 196.843 24 29 -3 -6 670.977 159.417 37 -29 3 5 -116.981 118.605 24 29 3 -5 199.862 140.053 10 29 3 -5 44.3547 148.150 24 29 -3 -5 -6.03295 118.797 37 29 3 -4 751.613 188.703 24 -29 3 4 491.193 140.118 24 29 -3 -4 656.219 212.975 17 29 3 -4 588.477 170.678 10 29 -3 -4 543.252 159.471 37 29 3 -3 -138.018 142.150 24 -29 3 3 -156.449 105.787 24 29 -3 -3 47.8065 179.740 17 29 3 -3 -218.461 128.709 10 29 -3 -3 121.464 129.438 37 29 3 -2 250.935 156.538 24 -29 3 2 80.7135 79.9329 24 29 -3 -2 277.495 175.333 17 29 3 -2 3.80894 118.690 10 29 -3 -2 536.271 164.936 37 29 -3 -1 1526.54 235.915 17 29 -3 -1 1301.39 202.776 37 29 3 -1 1731.56 233.118 24 29 -3 0 475.357 158.994 17 29 3 0 726.763 172.166 24 29 3 1 4319.13 303.116 24 29 3 2 1274.15 177.585 24 29 -3 3 107.816 109.727 37 30 0 -21 -344.944 189.761 20 30 0 -21 224.798 152.953 10 30 0 -20 928.434 230.580 10 30 0 -19 7.98091 198.088 10 30 0 -18 5773.72 481.616 10 30 0 -18 3748.66 305.420 31 30 0 -17 -227.629 247.788 10 -30 0 17 -1.92989 89.6047 24 30 0 -17 39.3958 124.951 31 30 0 -16 3015.97 342.447 31 30 0 -16 3549.19 454.885 10 30 0 -15 39.9088 271.562 10 30 0 -15 160.457 171.174 31 30 0 -14 1467.35 353.651 10 30 0 -14 1432.28 283.064 31 30 0 -13 185.035 316.953 10 30 0 -12 -330.619 317.720 10 30 0 -11 -193.622 295.703 10 30 0 -11 5.57586 218.557 17 30 0 -10 1745.76 433.223 10 30 0 -10 1280.03 295.711 17 30 0 -9 266.322 333.395 10 30 0 -9 -56.9444 248.426 17 30 0 -8 -268.575 319.403 10 30 0 -8 118.272 261.832 17 30 0 -7 158.374 310.308 10 30 0 -7 394.022 266.593 17 30 0 -6 424.869 359.243 10 30 0 -6 754.001 308.905 17 30 0 -5 -215.455 313.880 10 30 0 -5 255.714 270.718 17 30 0 -4 -286.186 310.553 10 30 0 -4 366.393 290.516 17 30 0 -3 -89.5880 290.228 10 30 0 -3 -215.696 266.630 17 30 0 -2 990.731 342.630 10 30 0 -2 848.774 303.149 17 30 0 -1 70.6389 279.921 10 30 0 -1 -262.471 300.529 17 30 0 0 693.621 309.927 10 30 0 0 693.528 299.721 17 30 0 1 -18.2881 254.069 10 30 0 1 228.381 277.328 17 30 0 2 3119.21 436.372 10 30 0 2 3648.40 448.910 17 30 0 3 -231.304 248.320 10 30 0 3 65.3401 232.573 17 30 0 4 11317.6 660.116 10 30 0 4 10682.8 633.864 17 30 0 5 -65.1017 190.426 10 30 0 5 -134.341 207.516 17 30 0 6 101.688 151.445 10 30 0 6 63.1588 176.116 17 30 0 7 57.5840 153.505 17 30 -1 -21 -110.895 128.054 20 30 -1 -20 58.2680 147.893 10 30 1 -20 -26.5128 139.514 10 30 1 -20 178.442 124.507 31 30 1 -19 128.582 144.971 31 30 -1 -19 128.396 110.917 16 30 -1 -19 252.502 173.275 10 30 1 -19 447.187 202.553 10 -30 1 18 537.718 108.733 24 30 -1 -18 1052.92 217.378 16 30 1 -18 364.170 161.890 31 30 -1 -18 486.571 199.719 10 30 1 -18 756.400 241.835 10 30 1 -17 403.113 212.644 31 -30 1 17 308.351 121.290 24 30 -1 -17 395.919 219.775 10 30 1 -17 825.366 274.419 10 30 1 -16 520.109 220.331 31 -30 1 16 602.997 166.774 24 30 -1 -16 751.930 255.820 10 30 1 -16 701.433 263.684 10 30 -1 -15 215.725 213.342 10 30 1 -15 -54.2941 230.152 10 30 1 -15 246.017 230.448 31 30 -1 -14 2214.37 378.108 10 30 1 -14 2260.84 396.413 10 30 1 -14 2136.93 390.829 31 30 -1 -13 607.635 277.116 10 30 1 -13 -86.4362 284.536 10 30 -1 -12 191.201 235.689 10 30 1 -12 7.06285 276.081 10 30 -1 -11 1062.91 331.067 10 30 1 -11 802.506 322.106 10 30 -1 -11 933.572 323.023 17 30 1 -10 278.770 302.588 10 30 -1 -10 415.228 274.209 10 30 -1 -10 144.366 266.361 17 30 1 -9 2889.72 475.220 10 30 -1 -9 3043.41 451.058 10 30 -1 -9 3040.34 452.763 17 30 -1 -8 133.626 241.847 10 30 1 -8 99.0077 309.455 10 30 1 -8 19.6893 167.078 17 30 -1 -8 120.354 294.462 17 30 -1 -7 4098.66 497.547 10 30 1 -7 3815.99 539.093 10 30 1 -7 3577.81 392.722 17 30 -1 -7 3889.47 527.346 17 30 1 -6 2478.04 337.042 24 30 -1 -6 2628.80 427.709 10 30 1 -6 2742.44 491.886 10 30 1 -6 3003.42 367.852 17 30 -1 -6 2181.08 435.777 17 30 1 -5 182.837 202.616 24 30 -1 -5 181.925 232.613 10 30 1 -5 37.7986 327.673 10 30 -1 -5 288.431 313.143 17 30 1 -5 143.268 184.445 17 30 1 -4 157.035 196.008 24 30 -1 -4 -49.3048 244.055 10 30 1 -4 71.1266 298.983 10 30 -1 -4 -216.911 293.786 17 30 1 -4 84.8947 195.636 17 30 1 -3 3201.05 357.648 24 30 -1 -3 3551.79 443.438 10 30 1 -3 3305.56 506.583 10 30 1 -3 3761.77 418.464 17 30 -1 -3 4217.82 528.283 17 30 1 -2 1911.58 296.814 24 30 -1 -2 1813.92 339.227 10 30 1 -2 1560.09 409.418 10 30 -1 -2 1917.67 406.594 17 30 1 -2 2137.37 349.140 17 30 1 -1 168.841 171.818 24 30 -1 -1 -146.521 263.854 17 30 1 -1 95.2272 203.450 17 30 -1 -1 50.7783 203.758 10 30 1 -1 101.926 274.019 10 30 -1 0 633.965 310.085 17 30 1 0 668.910 228.686 17 30 -1 0 714.618 245.840 10 30 1 0 427.048 299.385 10 30 -1 1 165.525 274.894 17 30 1 1 395.504 235.978 17 30 -1 1 147.260 190.434 10 30 1 1 73.0915 254.457 10 30 -1 2 1150.29 307.837 17 30 1 2 760.465 249.895 17 30 -1 2 881.415 223.166 10 30 1 2 630.816 280.621 10 30 -1 3 850.294 278.533 17 30 1 3 667.600 226.219 17 30 -1 3 1212.48 242.832 10 30 1 3 1027.69 295.669 10 30 -1 4 -48.6851 201.030 17 30 1 4 393.253 191.416 17 30 -1 4 235.379 139.718 10 30 1 4 491.235 271.395 10 30 -1 5 217.732 198.005 17 30 1 5 339.537 164.900 17 30 1 5 77.1964 194.193 10 30 -1 6 997.470 202.298 17 30 1 6 1025.95 212.461 10 30 2 -19 1154.83 198.405 31 30 -2 -19 737.081 160.081 16 30 2 -18 722.918 190.114 31 30 -2 -18 689.643 190.299 16 30 2 -17 1137.19 239.531 31 30 2 -17 766.793 162.764 10 -30 2 17 551.964 126.507 24 30 -2 -17 1350.97 252.921 16 -30 2 16 210.926 122.783 24 30 -2 -16 -96.8098 112.093 10 30 2 -16 449.526 174.999 10 30 2 -16 85.4104 195.669 31 -30 2 15 -53.3349 122.895 24 30 -2 -15 211.618 131.421 10 30 2 -15 370.924 224.771 31 -30 2 14 570.448 170.122 24 30 -2 -14 406.505 152.318 10 30 2 -14 712.350 216.286 10 30 2 -14 666.217 257.305 31 -30 2 13 90.3125 145.191 24 30 -2 -13 -585.495 180.225 10 30 2 -13 -315.400 199.968 10 30 2 -13 161.456 233.517 31 -30 2 12 126.619 156.200 24 30 -2 -12 -360.572 166.717 10 30 2 -12 -5.58764 190.200 10 -30 2 11 -33.2911 163.878 24 30 -2 -11 27.7392 147.074 10 30 2 -11 -379.275 226.978 10 30 -2 -10 2048.43 285.064 10 30 2 -10 1609.58 315.627 10 30 -2 -9 1197.45 342.532 17 30 -2 -9 1016.06 212.624 10 30 2 -9 1156.76 299.572 10 30 -2 -8 1435.64 345.381 17 30 2 -8 1647.89 332.287 10 30 -2 -8 1129.98 229.452 10 30 2 -8 1390.89 259.706 24 30 -2 -7 -17.4882 250.348 17 30 2 -7 60.3980 222.430 10 30 -2 -7 -396.809 171.029 10 30 2 -7 -17.8170 158.388 24 30 -2 -6 43.3296 257.321 17 30 2 -6 -57.3639 220.837 10 30 2 -6 -61.7467 159.386 24 30 -2 -5 178.995 108.700 37 30 2 -5 573.415 215.068 24 30 -2 -5 131.402 250.583 17 30 2 -5 -6.10273 216.788 10 30 2 -4 352.003 178.842 24 30 -2 -4 539.710 270.901 17 30 2 -4 502.803 273.417 10 30 2 -3 83.2018 160.066 24 30 -2 -3 336.212 251.198 17 30 2 -3 183.318 230.582 10 30 2 -2 106.279 154.483 24 30 2 -2 224.243 235.623 10 30 -2 -2 208.528 257.616 17 30 2 -1 117.227 151.389 24 30 2 -1 179.112 223.271 10 -30 2 1 313.132 102.146 24 30 -2 -1 -93.8096 219.419 17 30 2 0 620.268 168.104 24 30 -2 0 864.228 249.821 17 30 2 0 722.121 260.716 10 30 2 1 1025.07 182.861 24 30 -2 1 996.020 246.873 17 30 2 1 874.995 239.704 10 30 2 2 536.044 137.208 24 30 2 2 803.671 235.125 10 30 -2 2 878.901 218.459 17 30 2 3 605.109 195.641 10 30 -2 3 618.284 193.094 17 30 2 4 299.960 151.022 10 -30 3 15 15.1543 77.5471 24 30 -3 -15 37.7147 129.358 16 30 3 -15 -5.89021 128.142 31 -30 3 14 251.605 113.415 24 30 -3 -14 289.333 153.441 16 30 3 -14 358.155 165.257 31 -30 3 13 102.145 101.858 24 30 3 -13 126.042 160.564 31 -30 3 12 1076.96 175.864 24 30 3 -12 937.545 220.815 31 -30 3 11 -157.800 131.631 24 30 3 -11 133.388 180.012 31 -30 3 10 176.142 130.543 24 30 3 -10 55.1964 194.747 31 -30 3 9 12.7676 121.338 24 -30 3 8 163.626 134.829 24 30 3 -8 104.101 110.050 24 -30 3 7 1782.56 212.372 24 30 3 -7 1833.49 205.844 24 -30 3 6 684.133 147.642 24 30 -3 -6 660.614 117.842 37 30 3 -6 854.741 161.213 24 -30 3 5 882.320 148.138 24 30 -3 -5 845.020 138.169 37 30 3 -5 847.672 165.767 24 -30 3 4 62.0593 85.6491 24 30 -3 -4 -149.309 99.3442 37 30 3 -4 31.8194 117.478 24 30 -3 -3 665.224 134.508 37 30 3 -3 943.506 173.876 24 30 -3 -2 210.974 105.070 37 30 3 -2 -26.4930 116.386 24 30 -3 -1 607.545 126.244 37 30 3 -1 797.286 155.494 24 30 -3 0 125.209 88.8443 37 30 3 0 353.816 117.086 24 31 0 -20 6259.01 368.135 10 31 0 -19 -230.040 153.318 10 31 0 -18 718.380 213.171 10 31 0 -17 -15.6242 198.388 10 31 0 -16 2303.05 341.474 10 31 0 -16 1880.73 229.830 31 31 0 -15 -208.009 243.971 10 31 0 -15 350.237 169.439 31 31 0 -14 207.955 248.387 10 31 0 -14 -165.629 169.734 31 31 0 -13 -470.627 300.875 10 31 0 -13 -286.412 182.910 31 31 0 -12 -17.0297 257.115 10 31 0 -11 -223.163 269.189 10 31 0 -10 4539.49 525.115 10 31 0 -10 4423.66 439.563 17 31 0 -9 -271.575 278.588 10 31 0 -9 -124.020 195.750 17 31 0 -8 243.106 293.766 10 31 0 -8 656.489 242.752 17 31 0 -7 289.853 288.999 10 31 0 -7 226.496 227.783 17 31 0 -6 45.6257 268.647 10 31 0 -6 71.5015 225.612 17 31 0 -5 266.038 305.568 10 31 0 -5 -168.326 259.637 17 31 0 -4 -3.73524 288.165 10 31 0 -4 780.265 282.621 17 31 0 -3 -137.513 293.416 10 31 0 -3 59.5212 259.231 17 31 0 -2 2365.44 395.010 10 31 0 -2 1892.91 333.812 17 31 0 -1 -122.114 267.736 10 31 0 -1 220.785 239.281 17 31 0 0 1270.01 296.972 10 31 0 0 1550.62 326.317 17 31 0 1 52.4140 217.030 10 31 0 1 -148.369 219.671 17 31 0 2 831.259 253.375 10 31 0 2 590.622 223.356 17 31 0 3 -166.625 199.638 10 31 0 3 -142.713 202.674 17 31 0 4 1626.03 243.535 10 31 0 4 1933.35 268.558 17 31 0 5 -131.755 136.660 17 31 -1 -19 1154.46 183.225 10 31 1 -19 1183.06 186.133 10 31 1 -18 101.876 125.259 31 31 -1 -18 -10.8568 133.240 10 31 1 -18 57.2487 159.783 10 -31 1 17 2988.62 211.374 24 31 1 -17 3059.26 305.576 31 31 -1 -17 3421.71 321.893 10 31 1 -17 3890.89 356.894 10 31 -1 -17 3350.97 301.344 16 31 -1 -16 949.639 221.622 10 31 1 -16 1336.99 268.596 10 31 1 -16 1150.03 233.956 31 -31 1 16 949.480 158.177 24 31 -1 -15 692.932 220.714 10 31 1 -15 909.228 253.432 10 31 1 -15 577.019 215.880 31 -31 1 15 964.480 175.091 24 31 1 -14 197.029 209.820 31 31 -1 -14 736.177 234.205 10 31 1 -14 900.023 276.480 10 31 1 -13 -86.8117 211.741 31 31 -1 -13 171.627 199.158 10 31 1 -13 122.150 242.448 10 31 -1 -12 1267.28 294.043 10 31 1 -12 1027.34 295.456 10 31 -1 -11 167.897 203.294 10 31 1 -11 472.494 271.184 10 31 -1 -10 1307.93 328.050 17 31 -1 -10 1265.93 294.156 10 31 1 -10 1823.69 369.289 10 31 -1 -9 1159.11 330.716 17 31 1 -9 1097.92 332.741 10 31 -1 -9 764.462 271.039 10 31 -1 -8 -53.9000 261.891 17 31 1 -8 51.0379 274.410 10 31 -1 -8 -378.140 220.608 10 31 1 -7 93.4734 142.976 17 31 1 -7 199.529 275.153 10 31 -1 -7 20.2712 200.632 10 31 1 -6 159.494 152.324 17 31 -1 -6 407.932 278.984 17 31 -1 -6 33.6544 214.017 10 31 1 -6 98.9950 279.240 10 31 1 -5 721.590 202.425 17 31 -1 -5 1313.18 342.336 17 31 -1 -5 1039.07 290.023 10 31 1 -5 1170.57 340.863 10 31 1 -4 148.589 161.186 17 31 -1 -4 -1.09253 251.134 17 31 -1 -4 89.1763 223.136 10 31 1 -4 191.476 292.673 10 31 -1 -3 112.624 249.233 17 31 1 -3 274.559 175.990 17 31 -1 -3 -154.430 192.986 10 31 1 -3 141.339 258.301 10 31 -1 -2 440.384 265.961 17 31 1 -2 112.403 164.968 17 31 -1 -2 293.577 203.006 10 31 1 -2 490.669 302.870 10 31 -1 -1 -3.96087 234.046 17 31 1 -1 -54.5512 156.833 17 31 -1 -1 -270.166 204.620 10 31 1 -1 -133.206 231.396 10 31 -1 0 382.507 250.986 17 31 1 0 247.850 176.096 17 31 -1 0 22.9985 166.532 10 31 1 0 336.783 239.408 10 31 -1 1 307.747 222.532 17 31 1 1 529.043 191.623 17 31 -1 1 -26.4489 150.859 10 31 1 1 -138.136 234.229 10 31 -1 2 291.191 196.528 17 31 1 2 14.2709 136.737 17 31 -1 2 -382.779 148.740 10 31 1 2 161.957 208.518 10 31 -1 3 300.044 183.031 17 31 1 3 -172.436 128.419 17 31 1 3 47.8783 184.961 10 31 -1 4 1810.57 245.430 17 31 1 4 1630.54 246.431 10 31 2 -17 468.561 143.999 31 31 -2 -17 274.933 139.588 16 31 2 -16 -35.3232 153.062 31 31 -2 -16 174.065 153.981 16 -31 2 16 -115.665 84.2278 24 31 2 -15 304.751 192.377 31 -31 2 15 105.467 109.470 24 31 2 -14 -46.0028 172.411 31 -31 2 14 16.5140 118.578 24 31 2 -13 154.907 159.377 10 31 2 -13 295.061 220.420 31 -31 2 13 -3.04639 121.367 24 31 2 -12 313.278 154.800 10 31 2 -12 736.694 264.658 31 -31 2 12 400.809 156.447 24 -31 2 11 86.0441 139.747 24 31 2 -11 -170.950 200.787 10 -31 2 10 45.1742 142.501 24 31 2 -10 -81.6900 174.976 10 -31 2 9 -254.160 165.175 24 31 2 -9 157.536 193.232 10 -31 2 8 -52.8060 152.439 24 31 2 -8 385.763 223.980 10 31 -2 -7 917.312 263.352 17 31 2 -7 1075.18 247.925 10 31 2 -6 22.2195 138.666 24 31 -2 -6 170.323 222.359 17 31 2 -6 88.9039 189.018 10 -31 2 5 -249.909 143.759 24 31 2 -5 162.997 160.962 24 31 -2 -5 0.91108 209.215 17 31 2 -5 -197.350 205.416 10 31 -2 -4 506.930 113.519 37 -31 2 4 1248.41 189.797 24 31 2 -4 1248.46 211.791 24 31 -2 -4 1161.42 271.826 17 31 2 -4 1091.24 250.512 10 31 -2 -3 1535.61 174.268 37 31 2 -3 1807.74 233.529 24 -31 2 3 1389.74 185.484 24 31 2 -3 1852.99 285.645 10 31 -2 -2 1632.73 287.649 17 31 2 -2 1105.72 193.655 24 -31 2 2 1081.88 151.624 24 31 2 -2 1289.27 264.591 10 31 -2 -1 1676.35 273.936 17 31 2 -1 1944.87 217.165 24 31 2 -1 2300.88 308.025 10 31 -2 0 -231.945 165.346 17 31 2 0 151.066 172.075 10 31 -2 1 415.261 156.244 17 31 2 1 892.704 201.132 10 -31 3 12 252.866 103.858 24 -31 3 11 -52.2983 92.0732 24 31 3 -11 82.5908 127.193 31 -31 3 10 80.7124 98.1935 24 31 3 -10 -62.1482 126.439 31 -31 3 9 352.317 108.750 24 31 3 -9 640.239 179.539 31 -31 3 8 53.6460 87.4247 24 31 3 -8 201.169 149.505 31 -31 3 7 203.940 88.4810 24 32 0 -18 3187.50 274.211 10 32 0 -17 -121.243 164.029 10 32 0 -16 999.341 217.045 10 32 0 -15 -15.1445 177.117 10 32 0 -14 2769.14 357.407 10 32 0 -13 -258.622 146.970 31 32 0 -13 -89.7171 211.976 10 32 0 -12 924.781 189.597 31 32 0 -12 758.505 265.718 10 32 0 -11 -152.991 233.169 10 32 0 -10 5729.49 533.562 10 32 0 -9 330.215 198.237 17 32 0 -9 -21.5131 232.381 10 32 0 -8 1811.19 285.668 17 32 0 -8 1713.48 334.468 10 32 0 -7 32.4476 195.703 17 32 0 -7 244.821 262.796 10 32 0 -6 5773.18 467.078 17 32 0 -6 5626.70 523.382 10 32 0 -5 -180.865 200.285 17 32 0 -5 148.323 221.944 10 32 0 -4 208.091 201.890 17 32 0 -4 147.360 227.873 10 32 0 -3 144.033 195.761 17 32 0 -3 -39.8609 209.096 10 32 0 -2 2107.54 307.320 17 32 0 -2 2143.23 344.039 10 32 0 -1 371.747 205.669 17 32 0 -1 106.149 191.744 10 32 0 0 3772.39 350.364 17 32 0 0 3516.79 351.785 10 32 0 1 -99.4218 151.300 17 32 0 1 -219.051 176.777 10 32 0 2 833.716 184.811 17 32 0 2 455.974 164.460 10 32 1 -17 172.027 128.517 10 32 1 -16 899.088 171.886 31 32 -1 -16 1285.37 202.086 10 32 1 -16 1539.85 230.452 10 -32 1 15 264.000 101.739 24 32 1 -15 336.803 162.906 31 32 -1 -15 9.92228 135.595 10 -32 1 14 139.198 112.527 24 32 1 -14 -186.384 187.139 31 32 -1 -14 -223.701 161.986 10 32 1 -14 149.407 170.462 10 32 1 -13 -14.0212 167.444 31 32 -1 -13 -203.709 166.320 10 32 1 -13 243.891 205.720 10 32 1 -12 -114.476 178.987 31 32 -1 -12 65.5626 166.866 10 32 1 -12 -21.8526 206.184 10 32 -1 -11 -16.8545 165.769 10 32 1 -11 97.6327 208.052 10 32 -1 -10 -3.38123 169.024 10 32 1 -10 -15.6826 219.632 10 32 -1 -9 987.058 238.071 10 32 1 -9 889.212 259.706 10 32 -1 -8 22.2843 223.958 17 32 -1 -8 190.150 195.834 10 32 1 -8 -437.285 240.251 10 32 -1 -7 467.917 245.077 17 32 1 -7 86.1807 218.857 10 32 -1 -7 139.257 171.225 10 32 -1 -6 -130.828 231.251 17 32 1 -6 50.6035 228.671 10 32 -1 -6 305.809 190.888 10 32 -1 -5 402.980 238.950 17 32 1 -5 101.308 222.246 10 32 -1 -5 57.3761 156.547 10 32 1 -4 61.0197 107.499 17 32 -1 -4 743.668 247.384 17 32 1 -4 568.575 252.990 10 32 -1 -4 445.523 181.810 10 32 1 -3 99.1334 107.928 17 32 -1 -3 127.164 199.033 17 32 -1 -3 309.207 168.844 10 32 1 -3 242.226 220.521 10 32 1 -2 529.333 140.452 17 32 -1 -2 1024.50 265.607 17 32 -1 -2 549.261 173.039 10 32 1 -2 590.829 242.219 10 32 -1 -1 3748.07 369.583 17 32 -1 -1 2946.86 273.911 10 32 1 -1 3774.29 381.359 10 32 -1 0 72.8753 175.810 17 32 1 0 143.894 181.251 10 32 -1 1 1331.19 222.493 17 32 1 1 1106.21 222.663 10 32 2 -14 -5.45571 127.559 31 -32 2 14 -40.2245 87.5606 24 32 2 -13 1345.29 216.001 31 -32 2 13 1382.19 174.945 24 32 2 -12 500.223 186.464 31 -32 2 12 292.843 123.526 24 32 2 -11 -105.627 177.255 31 -32 2 11 -130.398 128.520 24 32 2 -11 -189.724 127.591 10 -32 2 10 2389.10 240.379 24 32 2 -10 2209.44 240.799 10 -32 2 9 3913.59 289.032 24 32 2 -9 3861.59 318.057 10 -32 2 8 1251.44 191.398 24 32 2 -8 812.354 181.880 10 -32 2 7 2729.31 243.120 24 32 2 -7 2093.78 256.169 10 -32 2 6 659.546 142.419 24 32 2 -6 680.369 173.750 10 -32 2 5 1202.87 159.487 24 32 -2 -5 1337.56 243.704 17 32 2 -5 976.178 193.413 10 -32 2 4 301.314 99.9961 24 32 -2 -4 332.883 175.723 17 32 2 -4 230.546 156.121 10 32 -2 -3 502.216 175.560 17 32 2 -3 553.971 162.367 10 32 -2 -2 -22.0358 134.048 17 33 0 -15 -40.9076 129.234 10 33 0 -14 2236.37 267.922 10 33 0 -13 -166.242 166.232 10 33 0 -12 612.163 205.804 10 33 0 -11 -206.007 193.217 10 33 0 -10 1608.57 272.750 10 33 0 -9 -184.435 186.818 10 33 0 -8 5717.73 450.830 10 33 0 -7 238.365 136.789 17 33 0 -7 8.19537 190.401 10 33 0 -6 1143.13 207.518 17 33 0 -6 1080.33 250.197 10 33 0 -5 -203.829 160.514 17 33 0 -5 162.328 197.386 10 33 0 -4 1419.57 224.081 17 33 0 -4 1899.40 274.949 10 33 0 -3 -322.828 163.086 17 33 0 -3 211.706 167.951 10 33 0 -2 166.273 144.083 17 33 0 -2 568.279 192.644 10 33 0 -1 176.688 136.480 10 33 1 -14 159.613 134.126 10 -33 1 13 57.8445 85.6397 24 33 1 -13 32.1948 134.558 10 -33 1 12 438.759 125.549 24 33 -1 -12 270.660 126.029 10 33 1 -12 533.630 176.950 10 33 1 -12 315.851 142.607 31 33 -1 -11 28.2609 118.194 10 33 1 -11 -140.225 165.472 10 33 1 -11 -126.911 152.037 31 33 -1 -10 78.8018 127.430 10 33 1 -10 228.042 179.201 10 33 -1 -9 290.734 154.937 10 33 1 -9 320.275 196.852 10 33 -1 -8 1364.85 209.670 10 33 1 -8 1261.49 250.687 10 33 -1 -7 433.701 145.791 10 33 1 -7 742.939 228.426 10 33 -1 -6 724.728 168.889 10 33 1 -6 1201.82 253.946 10 33 -1 -6 1265.90 238.749 17 33 1 -5 10.2025 175.407 10 33 -1 -5 217.905 166.551 17 33 1 -4 353.575 188.565 10 33 -1 -4 -32.9780 167.438 17 33 1 -3 179.632 155.868 10 33 -1 -3 637.987 188.594 17 33 1 -2 57.9655 139.537 10 33 -1 -2 230.491 153.789 17 34 0 -10 770.651 172.700 10 34 0 -9 -183.205 143.537 10 34 0 -8 -145.056 134.772 10 34 0 -7 -232.621 147.293 10 _ins_header ; TITL 039wps22_WS in P2/c REM P2/c (#13 in standard setting) CELL 1.54184 27.082265 6.113699 24.937874 90.0000 105.4116 90.0000 ZERR 4.00 0.000915 0.000165 0.000671 0.0000 0.0032 0.0000 LATT 1 SYMM -x, y,-z+1/2 SFAC C H B O Cl UNIT 192.00 192.00 4.00 8.00 4.00 REM CrysAlisPro recorded range (K): Min=150.0; max=150.0; aver:150.0 TEMP -123 TREF HKLF 4 END ; _olex2_exptl_crystal_mounting_method 'Fomblin YR-1800 oil, MiTeGen 200 micron loop.' _olex2_submission_original_sample_id 039wps22 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.633 _oxdiff_exptl_absorpt_empirical_full_min 0.619