############################################################################## # # # This CIF contains the data in a paper accepted for publication in # # Acta Crystallographica Section E. It conforms to the requirements of # # Notes for Authors for Acta Crystallographica Section E, and has been # # peer reviewed under the auspices of the IUCr Commission on Journals. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the journal # # article from which it was obtained. # # # ############################################################################## data_I _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _journal_date_recd_electronic 2024-05-10 _journal_date_accepted 2024-07-01 _journal_name_full 'Acta Crystallographica, Section E' _journal_year 2024 _journal_volume 80 _journal_issue 1 _journal_page_first 0 _journal_page_last 0 _journal_paper_category GO _journal_paper_doi 10.1107/S205698902400642X _journal_coeditor_code OX2006 _publ_contact_author_name 'Yukiyasu Kashiwagi' _publ_contact_author_address ; Osaka Research Institute of Industrial Science and Technology, 1-6-50 Morinomiya, Joto-ku, Osaka 536-8553, Japan ; _publ_contact_author_email 'kasiwagi@orist.jp' _publ_contact_author_fax ? _publ_contact_author_phone '+81-6-6963-8025' _publ_section_title ; Crystal structure of the 1:1 co-crystal 4-(dimethylamino)pyridin-1-ium 8-hydroxyquinoline-5-sulfonate--N,N-dimethylpyridin-4-amine ; loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Isobe, Mami' . ; Department of Chemistry and Bioengineering, Graduate School of Engineering, Osaka Metropolitan University, 3-3-138 Sugimoto, Sumiyoshi-ku, Osaka 558-8585, Japan ; 'Kashiwagi, Yukiyasu' . ; Osaka Research Institute of Industrial Science and Technology, 1-6-50 Morinomiya, Joto-ku, Osaka 536-8553, Japan ; 'Kubono, Koji' . ; Osaka Kyoiku University, 4-698-1 Asahigaoka, Kashiwara, Osaka 582-8582, Japan ; _publ_section_synopsis ; The asymmetric unit of the title compound consists of two independent ion pairs of 4-(dimethylamino)pyridin-1-ium quinolin-8-ol-5-sulfonate (HDMAP^+^\\cdotHqSA^-^) and neutral N,N-dimethylpyridin-4-amine (DMAP), forming a 1:1:1 cation:anion:neutral molecule co-crystal. The compound has a layered structure, including cation layers of HDMAP^+^ with DMAP and anion layers of HqSA^-^ in the crystal. The cation and anion layers are linked by intermolecular C---H...O hydrogen bonds and C---H...\p interactions. ; _chemical_name_systematic ; 4-(Dimethylamino)pyridin-1-ium 8-hydroxyquinoline-5-sulfonate; N,N-dimethylpyridin-4-amine ; _chemical_formula_moiety 'C7 H11 N2 +, C9 H6 N O4 S -, C7 H10 N2' _chemical_formula_sum 'C23 H27 N5 O4 S' _chemical_formula_iupac 'C7 H11 N2 +, C9 H6 N O4 S -, C7 H10 N2' _chemical_formula_weight 469.55 _chemical_melting_point ? _chemical_absolute_configuration ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P c' _space_group_name_Hall 'P -2yc' loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' _cell_length_a 8.00032(10) _cell_length_b 15.14469(18) _cell_length_c 18.9141(2) _cell_angle_alpha 90 _cell_angle_beta 100.6050(12) _cell_angle_gamma 90 _cell_volume 2252.53(5) _cell_formula_units_Z 4 _cell_measurement_reflns_used 11719 _cell_measurement_theta_min 3.7490 _cell_measurement_theta_max 76.8410 _cell_measurement_temperature 100 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.302 _exptl_crystal_size_min 0.112 _exptl_crystal_density_diffrn 1.385 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 992 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 0 -1 0.0333 0 0 1 0.0788 1 1 0 0.1185 1 1 2 0.1009 0 -1 -1 0.1244 -2 1 2 0.0858 0 2 -1 0.1767 0 -10 0 0.1691 4 -4 -8 0.1589 _exptl_absorpt_coefficient_mu 1.622 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2023) ; _exptl_absorpt_correction_T_min 0.73086 _exptl_absorpt_correction_T_max 1.00000 _diffrn_ambient_temperature 100 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_monochromator mirror _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_reflns_number 16358 _diffrn_reflns_av_R_equivalents 0.0300 _diffrn_reflns_av_unetI/netI 0.0350 _diffrn_reflns_theta_min 3.765 _diffrn_reflns_theta_max 77.159 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.934 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_limit_l_max 23 _diffrn_radiation_probe x-ray _refine_special_details ; Refined as a 2-component inversion twin. 1. Twinned data refinement Scales: 0.522(18) 0.478(18) 2. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 3. Restrained distances H18-N18 0.86 with sigma of 0.02 H14-N14 0.86 with sigma of 0.02 4.a Aromatic/amide H refined with riding coordinates: C35(H35), C23(H23), C27(H27), C26(H26), C49(H49), C31(H31), C28(H28), C61(H61), C54(H54), C36(H36), C60(H60), C50(H50), C22(H22), C40(H40), C53(H53), C37(H37), C42(H42), C47(H47), C64(H64), C63(H63), C46(H46), C43(H43), C39(H39), C32(H32), C56(H56), C57(H57) 4.b Idealised Me refined as rotating group: C52(H52A,H52B,H52C), C44(H44A,H44B,H44C), C58(H58A,H58B,H58C), C66(H66A,H66B, H66C), C51(H51A,H51B,H51C), C45(H45A,H45B,H45C), C65(H65A,H65B,H65C), C59(H59A, H59B,H59C) ; _reflns_number_total 6813 _reflns_number_gt 6608 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0336 _refine_ls_R_factor_gt 0.0325 _refine_ls_wR_factor_gt 0.0838 _refine_ls_wR_factor_ref 0.0848 _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_restrained_S_all 1.038 _refine_ls_number_reflns 6813 _refine_ls_number_parameters 620 _refine_ls_number_restraints 4 _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0463P)^2^+0.5548P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.297 _refine_diff_density_min -0.393 _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Refined as an inversion twin ; _refine_ls_abs_structure_Flack 0.478(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; CrysAlisPro 1.171.42.90a (Rigaku OD, 2023) ; _computing_cell_refinement ; CrysAlisPro 1.171.42.90a (Rigaku OD, 2023) ; _computing_data_reduction ; CrysAlisPro 1.171.42.90a (Rigaku OD, 2023) ; _computing_structure_solution ; SHELXT2018/2 (Sheldrick, 2015a) ; _computing_structure_refinement ; SHELXL2018/3 (Sheldrick, 2015b) ; _computing_molecular_graphics ; Olex2 1.5 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 1.5 (Dolomanov et al., 2009) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S S1 0.17772(8) 0.49921(4) 0.37557(4) 0.01431(15) Uani d 1 . . S S2 0.88938(8) 0.99725(4) 0.36763(4) 0.01686(16) Uani d 1 . . O O5 0.0868(3) 0.46728(13) 0.43037(11) 0.0198(4) Uani d 1 . . O O10 0.3080(3) 0.75413(13) 0.36853(12) 0.0189(4) Uani d 1 . . O O4 0.2618(3) 0.58342(12) 0.39552(12) 0.0222(4) Uani d 1 . . O O7 1.0147(3) 0.97468(16) 0.43079(12) 0.0274(5) Uani d 1 . . O O6 0.7498(3) 0.25632(14) 0.35776(12) 0.0191(4) Uani d 1 . . N N11 0.4365(3) 0.18427(15) 0.35601(13) 0.0168(5) Uani d 1 . . O O3 0.0728(3) 0.49865(13) 0.30454(12) 0.0251(5) Uani d 1 . . N N14 0.0994(3) 0.57921(17) 0.61872(14) 0.0228(5) Uani d 1 . . O O9 0.9547(3) 0.98318(15) 0.30206(12) 0.0253(5) Uani d 1 . . N N18 1.0806(4) 1.06837(18) 0.62048(15) 0.0283(6) Uani d 1 . . N N12 0.6186(3) 0.68257(14) 0.36322(13) 0.0153(5) Uani d 1 . . N N17 1.3114(3) 1.31360(18) 0.63022(14) 0.0268(6) Uani d 1 . . N N13 0.3275(3) 0.82252(17) 0.60874(14) 0.0248(6) Uani d 1 . . C C25 0.3141(4) 0.33136(18) 0.36637(15) 0.0132(5) Uani d 1 . . N N16 -0.3146(4) 0.16966(18) 0.60144(14) 0.0300(6) Uani d 1 . . N N15 -0.0827(3) 0.41978(17) 0.61461(14) 0.0258(6) Uani d 1 . . C C30 0.4422(3) 0.80852(18) 0.36639(15) 0.0152(6) Uani d 1 . . N N20 0.6851(4) 0.65381(18) 0.61189(15) 0.0297(6) Uani d 1 . . C C29 0.4524(4) 0.27401(18) 0.36172(15) 0.0141(5) Uani d 1 . . N N19 0.9083(4) 0.90581(18) 0.61654(15) 0.0271(6) Uani d 1 . . C C35 0.9054(4) 0.79031(19) 0.36300(15) 0.0157(5) Uani d 1 . . H H35 1.003375 0.825760 0.363038 0.019 Uiso calc 1 . . O O8 0.8170(3) 1.08342(14) 0.37345(18) 0.0427(7) Uani d 1 . . C C48 -0.2420(4) 0.25088(19) 0.60531(16) 0.0222(6) Uani d 1 . . C C23 0.5063(4) 0.45581(18) 0.37350(16) 0.0165(6) Uani d 1 . . H H23 0.525964 0.517580 0.378068 0.020 Uiso calc 1 . . C C24 0.3458(4) 0.42408(18) 0.37218(15) 0.0156(6) Uani d 1 . . C C27 0.1385(4) 0.20164(19) 0.35746(16) 0.0195(6) Uani d 1 . . H H27 0.031056 0.173969 0.355266 0.023 Uiso calc 1 . . C C26 0.1533(4) 0.29119(19) 0.36372(15) 0.0162(6) Uani d 1 . . H H26 0.056312 0.326366 0.366290 0.019 Uiso calc 1 . . C C34 0.7451(3) 0.82997(18) 0.36388(15) 0.0137(5) Uani d 1 . . C C49 -0.2102(4) 0.29987(19) 0.66961(16) 0.0224(6) Uani d 1 . . H H49 -0.243039 0.277078 0.711817 0.027 Uiso calc 1 . . C C31 0.4187(4) 0.89824(19) 0.36710(17) 0.0192(6) Uani d 1 . . H H31 0.309000 0.921934 0.367659 0.023 Uiso calc 1 . . C C38 0.6054(4) 0.77244(17) 0.36430(15) 0.0130(5) Uani d 1 . . C C28 0.2840(4) 0.15080(18) 0.35428(16) 0.0197(6) Uani d 1 . . H H28 0.271473 0.088498 0.350666 0.024 Uiso calc 1 . . C C33 0.7176(4) 0.92240(18) 0.36554(15) 0.0152(5) Uani d 1 . . C C61 0.8018(4) 0.7746(2) 0.55202(16) 0.0215(6) Uani d 1 . . H H61 0.781003 0.744043 0.507393 0.026 Uiso calc 1 . . C C54 1.1908(4) 1.1940(2) 0.68862(16) 0.0220(6) Uani d 1 . . H H54 1.212304 1.223795 0.733567 0.026 Uiso calc 1 . . C C36 0.9166(4) 0.70039(19) 0.36211(16) 0.0184(6) Uani d 1 . . H H36 1.022730 0.672608 0.361413 0.022 Uiso calc 1 . . C C62 0.7562(4) 0.7356(2) 0.61344(17) 0.0237(6) Uani d 1 . . C C60 0.8763(4) 0.8566(2) 0.55657(17) 0.0257(7) Uani d 1 . . H H60 0.907308 0.880142 0.514258 0.031 Uiso calc 1 . . C C50 -0.1315(4) 0.3809(2) 0.67126(17) 0.0247(6) Uani d 1 . . H H50 -0.110204 0.411581 0.715822 0.030 Uiso calc 1 . . C C22 0.6432(4) 0.39925(19) 0.36825(17) 0.0193(6) Uani d 1 . . H H22 0.753237 0.423009 0.368649 0.023 Uiso calc 1 . . C C40 0.2142(4) 0.7096(2) 0.67653(16) 0.0209(6) Uani d 1 . . H H40 0.240263 0.743534 0.719363 0.025 Uiso calc 1 . . C C53 1.1159(4) 1.1131(2) 0.68335(18) 0.0257(7) Uani d 1 . . H H53 1.087382 1.087116 0.725275 0.031 Uiso calc 1 . . C C37 0.7696(4) 0.64896(18) 0.36221(17) 0.0183(6) Uani d 1 . . H H37 0.780438 0.586507 0.361522 0.022 Uiso calc 1 . . C C42 0.2165(4) 0.6872(2) 0.55097(16) 0.0229(6) Uani d 1 . . H H42 0.243782 0.705189 0.506333 0.027 Uiso calc 1 . . C C41 0.2560(4) 0.74334(19) 0.61167(16) 0.0200(6) Uani d 1 . . C C21 0.6173(4) 0.30979(18) 0.36257(15) 0.0145(5) Uani d 1 . . C C47 -0.1930(4) 0.2920(2) 0.54526(16) 0.0237(6) Uani d 1 . . H H47 -0.212812 0.263269 0.499838 0.028 Uiso calc 1 . . C C64 0.8639(4) 0.8686(2) 0.67528(18) 0.0296(7) Uani d 1 . . H H64 0.885457 0.901387 0.718843 0.036 Uiso calc 1 . . C C55 1.2371(4) 1.23419(19) 0.62685(16) 0.0218(6) Uani d 1 . . C C52 -0.3516(5) 0.1263(2) 0.66566(19) 0.0318(7) Uani d 1 . . H H52A -0.246320 0.120190 0.701170 0.048 Uiso calc 1 . . H H52B -0.399916 0.067773 0.652889 0.048 Uiso calc 1 . . H H52C -0.433271 0.161935 0.686096 0.048 Uiso calc 1 . . C C63 0.7900(4) 0.7873(2) 0.67674(17) 0.0282(7) Uani d 1 . . H H63 0.761539 0.765609 0.720146 0.034 Uiso calc 1 . . C C44 0.3650(5) 0.8790(2) 0.67269(19) 0.0302(7) Uani d 1 . . H H44A 0.258673 0.894730 0.688314 0.045 Uiso calc 1 . . H H44B 0.422323 0.932840 0.661072 0.045 Uiso calc 1 . . H H44C 0.439097 0.847174 0.711421 0.045 Uiso calc 1 . . C C46 -0.1165(4) 0.3737(2) 0.55256(17) 0.0250(6) Uani d 1 . . H H46 -0.085302 0.399369 0.511048 0.030 Uiso calc 1 . . C C43 0.1398(4) 0.6079(2) 0.55592(17) 0.0238(6) Uani d 1 . . H H43 0.113795 0.571602 0.514381 0.029 Uiso calc 1 . . C C39 0.1381(4) 0.6302(2) 0.67832(17) 0.0230(6) Uani d 1 . . H H39 0.111083 0.609654 0.722336 0.028 Uiso calc 1 . . C C32 0.5578(4) 0.95491(19) 0.36698(17) 0.0202(6) Uani d 1 . . H H32 0.541065 1.016967 0.367926 0.024 Uiso calc 1 . . C C56 1.2007(4) 1.1840(2) 0.56237(17) 0.0252(6) Uani d 1 . . H H56 1.230849 1.206924 0.519661 0.030 Uiso calc 1 . . C C58 1.3420(5) 1.3650(2) 0.69703(19) 0.0322(7) Uani d 1 . . H H58A 1.233475 1.377047 0.712141 0.048 Uiso calc 1 . . H H58B 1.397149 1.420969 0.688945 0.048 Uiso calc 1 . . H H58C 1.415965 1.331447 0.734677 0.048 Uiso calc 1 . . C C57 1.1241(4) 1.1046(2) 0.56067(18) 0.0292(7) Uani d 1 . . H H57 1.100001 1.073059 0.516531 0.035 Uiso calc 1 . . C C66 0.6549(5) 0.6125(2) 0.6777(2) 0.0355(8) Uani d 1 . . H H66A 0.761279 0.610761 0.712932 0.053 Uiso calc 1 . . H H66B 0.613111 0.552185 0.667276 0.053 Uiso calc 1 . . H H66C 0.569870 0.646643 0.697307 0.053 Uiso calc 1 . . C C51 -0.3476(5) 0.1193(2) 0.53443(18) 0.0345(8) Uani d 1 . . H H51A -0.429289 0.151412 0.498551 0.052 Uiso calc 1 . . H H51B -0.394504 0.061445 0.543216 0.052 Uiso calc 1 . . H H51C -0.241090 0.111422 0.516567 0.052 Uiso calc 1 . . C C45 0.3605(5) 0.8585(2) 0.54079(18) 0.0316(7) Uani d 1 . . H H45A 0.434078 0.817948 0.520221 0.047 Uiso calc 1 . . H H45B 0.416725 0.916003 0.549571 0.047 Uiso calc 1 . . H H45C 0.252586 0.865738 0.507093 0.047 Uiso calc 1 . . C C65 0.6452(5) 0.6043(2) 0.54515(19) 0.0320(7) Uani d 1 . . H H65A 0.569908 0.639435 0.509079 0.048 Uiso calc 1 . . H H65B 0.588361 0.549017 0.553627 0.048 Uiso calc 1 . . H H65C 0.750475 0.591031 0.527717 0.048 Uiso calc 1 . . C C59 1.3515(5) 1.3552(2) 0.5656(2) 0.0355(8) Uani d 1 . . H H59A 1.429459 1.317305 0.545016 0.053 Uiso calc 1 . . H H59B 1.405242 1.412637 0.578214 0.053 Uiso calc 1 . . H H59C 1.246532 1.363609 0.530309 0.053 Uiso calc 1 . . H H14 0.047(5) 0.5262(17) 0.616(2) 0.029(9) Uiso d 1 . . H H10 0.336(6) 0.697(3) 0.372(2) 0.037(11) Uiso d 1 . . H H18 1.027(6) 1.016(2) 0.618(3) 0.057(15) Uiso d 1 . . H H6 0.714(6) 0.204(3) 0.357(2) 0.039(12) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0135(3) 0.0121(3) 0.0179(3) 0.0021(2) 0.0043(2) 0.0012(2) S2 0.0140(3) 0.0113(3) 0.0270(4) -0.0012(2) 0.0083(3) -0.0004(2) O5 0.0221(10) 0.0170(9) 0.0228(11) 0.0007(8) 0.0104(8) -0.0003(8) O10 0.0124(10) 0.0129(10) 0.0327(12) -0.0020(8) 0.0079(8) 0.0022(8) O4 0.0193(10) 0.0115(9) 0.0376(12) 0.0007(8) 0.0100(9) -0.0005(8) O7 0.0270(12) 0.0331(11) 0.0216(11) -0.0145(10) 0.0027(9) -0.0034(9) O6 0.0117(10) 0.0142(10) 0.0321(12) 0.0006(8) 0.0054(8) 0.0000(8) N11 0.0166(11) 0.0136(11) 0.0202(12) 0.0000(9) 0.0030(9) 0.0005(9) O3 0.0270(12) 0.0286(12) 0.0185(11) 0.0128(9) 0.0012(9) 0.0007(8) N14 0.0237(13) 0.0207(12) 0.0239(14) -0.0030(10) 0.0041(10) -0.0013(10) O9 0.0251(11) 0.0316(11) 0.0205(11) -0.0083(9) 0.0076(9) 0.0026(9) N18 0.0251(14) 0.0240(14) 0.0335(16) 0.0010(11) -0.0006(11) -0.0050(11) N12 0.0142(11) 0.0127(11) 0.0188(12) -0.0001(9) 0.0029(9) -0.0001(9) N17 0.0303(14) 0.0248(13) 0.0229(13) -0.0001(11) -0.0010(11) 0.0038(10) N13 0.0297(14) 0.0218(13) 0.0231(14) -0.0044(10) 0.0052(11) 0.0012(10) C25 0.0125(12) 0.0147(13) 0.0128(12) -0.0001(10) 0.0035(10) 0.0009(10) N16 0.0447(17) 0.0249(13) 0.0179(13) -0.0064(12) -0.0008(12) -0.0001(10) N15 0.0263(14) 0.0231(13) 0.0275(14) -0.0001(11) 0.0036(11) -0.0002(10) C30 0.0120(13) 0.0159(13) 0.0178(14) -0.0007(11) 0.0029(10) 0.0012(11) N20 0.0382(16) 0.0294(14) 0.0225(14) -0.0068(12) 0.0081(12) 0.0030(10) C29 0.0135(13) 0.0158(13) 0.0132(13) 0.0016(10) 0.0029(10) 0.0012(10) N19 0.0289(15) 0.0246(13) 0.0264(14) -0.0010(11) 0.0014(11) -0.0038(10) C35 0.0134(13) 0.0174(13) 0.0165(14) -0.0010(11) 0.0035(10) 0.0008(10) O8 0.0219(12) 0.0115(10) 0.100(2) -0.0016(9) 0.0251(13) -0.0010(12) C48 0.0210(15) 0.0243(15) 0.0199(15) 0.0037(12) -0.0001(12) 0.0005(12) C23 0.0158(12) 0.0119(13) 0.0220(14) -0.0004(11) 0.0037(11) 0.0004(10) C24 0.0167(14) 0.0138(13) 0.0167(14) 0.0028(11) 0.0039(11) 0.0014(10) C27 0.0133(13) 0.0160(13) 0.0295(16) -0.0032(11) 0.0045(11) 0.0022(11) C26 0.0157(14) 0.0149(13) 0.0190(14) 0.0032(10) 0.0057(11) -0.0009(10) C34 0.0128(13) 0.0163(13) 0.0119(12) -0.0005(11) 0.0023(10) -0.0003(10) C49 0.0241(15) 0.0249(15) 0.0182(14) 0.0009(12) 0.0039(11) 0.0013(11) C31 0.0110(14) 0.0170(13) 0.0308(17) 0.0032(11) 0.0070(11) 0.0025(11) C38 0.0131(13) 0.0130(12) 0.0129(12) -0.0002(10) 0.0026(10) 0.0004(10) C28 0.0178(14) 0.0130(13) 0.0274(16) -0.0008(10) 0.0017(12) 0.0014(11) C33 0.0144(13) 0.0148(13) 0.0172(14) -0.0010(11) 0.0048(10) 0.0006(10) C61 0.0237(15) 0.0239(15) 0.0160(14) -0.0009(12) 0.0015(11) -0.0010(11) C54 0.0199(14) 0.0267(15) 0.0185(14) 0.0022(12) 0.0016(11) -0.0023(11) C36 0.0139(14) 0.0169(13) 0.0248(15) 0.0034(11) 0.0050(11) 0.0003(11) C62 0.0217(15) 0.0281(15) 0.0212(15) 0.0027(12) 0.0039(12) 0.0021(12) C60 0.0259(16) 0.0286(16) 0.0219(15) 0.0012(13) 0.0028(12) 0.0012(13) C50 0.0241(15) 0.0269(15) 0.0218(15) 0.0011(12) 0.0006(12) -0.0047(12) C22 0.0143(14) 0.0179(14) 0.0272(16) -0.0007(11) 0.0075(12) -0.0005(11) C40 0.0195(14) 0.0254(15) 0.0172(14) 0.0003(11) 0.0021(11) -0.0011(11) C53 0.0211(15) 0.0280(16) 0.0270(17) 0.0036(12) 0.0019(12) 0.0001(12) C37 0.0158(13) 0.0102(12) 0.0295(16) 0.0012(10) 0.0054(11) 0.0003(11) C42 0.0231(15) 0.0290(16) 0.0176(14) 0.0013(12) 0.0064(11) 0.0005(12) C41 0.0191(14) 0.0202(14) 0.0206(15) 0.0024(11) 0.0030(11) 0.0029(11) C21 0.0129(13) 0.0157(13) 0.0154(13) 0.0024(11) 0.0038(10) 0.0006(11) C47 0.0239(15) 0.0266(15) 0.0198(15) 0.0037(12) 0.0020(11) -0.0034(11) C64 0.0304(17) 0.0340(17) 0.0237(16) 0.0047(14) 0.0033(13) -0.0076(13) C55 0.0187(14) 0.0223(14) 0.0229(16) 0.0049(11) -0.0001(12) -0.0012(11) C52 0.0371(19) 0.0279(17) 0.0296(18) -0.0070(14) 0.0044(14) 0.0041(13) C63 0.0316(17) 0.0341(17) 0.0196(16) 0.0034(14) 0.0070(13) -0.0004(13) C44 0.0347(18) 0.0234(15) 0.0319(18) -0.0074(13) 0.0052(14) -0.0007(13) C46 0.0219(15) 0.0311(16) 0.0218(15) 0.0003(13) 0.0034(12) 0.0040(12) C43 0.0228(15) 0.0260(15) 0.0222(15) -0.0002(12) 0.0035(12) -0.0037(12) C39 0.0256(16) 0.0233(15) 0.0205(15) 0.0013(12) 0.0053(12) 0.0007(12) C32 0.0200(14) 0.0115(13) 0.0309(17) 0.0023(11) 0.0096(12) 0.0016(11) C56 0.0258(16) 0.0296(16) 0.0194(15) 0.0044(13) 0.0023(12) -0.0015(12) C58 0.0369(19) 0.0261(16) 0.0303(18) -0.0032(14) -0.0025(14) -0.0027(13) C57 0.0275(16) 0.0318(17) 0.0254(16) 0.0057(13) -0.0024(13) -0.0090(13) C66 0.038(2) 0.0373(19) 0.0331(19) -0.0040(15) 0.0117(15) 0.0101(15) C51 0.042(2) 0.0318(18) 0.0269(18) -0.0040(15) -0.0022(15) -0.0051(14) C45 0.0344(18) 0.0333(17) 0.0287(18) -0.0062(14) 0.0100(14) 0.0082(13) C65 0.0346(19) 0.0261(16) 0.0348(19) -0.0073(13) 0.0054(15) -0.0003(13) C59 0.0352(19) 0.0381(19) 0.0317(19) -0.0014(15) 0.0023(14) 0.0119(15) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag S1 O5 . 1.455(2) ? S1 O4 . 1.459(2) ? S1 O3 . 1.447(2) ? S1 C24 . 1.772(3) ? S2 O7 . 1.452(2) ? S2 O9 . 1.448(2) ? S2 O8 . 1.440(2) ? S2 C33 . 1.776(3) ? O10 C30 . 1.359(3) ? O10 H10 . 0.90(4) ? O6 C21 . 1.350(3) ? O6 H6 . 0.84(4) ? N11 C29 . 1.367(4) ? N11 C28 . 1.316(4) ? N14 C43 . 1.358(4) ? N14 C39 . 1.354(4) ? N14 H14 . 0.90(2) ? N18 C53 . 1.353(4) ? N18 C57 . 1.359(5) ? N18 H18 . 0.90(2) ? N12 C38 . 1.366(3) ? N12 C37 . 1.315(4) ? N17 C55 . 1.338(4) ? N17 C58 . 1.466(4) ? N17 C59 . 1.462(4) ? N13 C41 . 1.334(4) ? N13 C44 . 1.467(4) ? N13 C45 . 1.464(4) ? C25 C29 . 1.422(4) ? C25 C24 . 1.428(4) ? C25 C26 . 1.415(4) ? N16 C48 . 1.356(4) ? N16 C52 . 1.458(4) ? N16 C51 . 1.461(4) ? N15 C50 . 1.342(4) ? N15 C46 . 1.350(4) ? C30 C31 . 1.372(4) ? C30 C38 . 1.423(4) ? N20 C62 . 1.362(4) ? N20 C66 . 1.453(4) ? N20 C65 . 1.452(4) ? C29 C21 . 1.424(4) ? N19 C60 . 1.342(4) ? N19 C64 . 1.350(4) ? C35 H35 . 0.9500 ? C35 C34 . 1.419(4) ? C35 C36 . 1.365(4) ? C48 C49 . 1.407(4) ? C48 C47 . 1.413(4) ? C23 H23 . 0.9500 ? C23 C24 . 1.367(4) ? C23 C22 . 1.408(4) ? C27 H27 . 0.9500 ? C27 C26 . 1.365(4) ? C27 C28 . 1.407(4) ? C26 H26 . 0.9500 ? C34 C38 . 1.419(4) ? C34 C33 . 1.418(4) ? C49 H49 . 0.9500 ? C49 C50 . 1.377(4) ? C31 H31 . 0.9500 ? C31 C32 . 1.406(4) ? C28 H28 . 0.9500 ? C33 C32 . 1.375(4) ? C61 H61 . 0.9500 ? C61 C62 . 1.409(4) ? C61 C60 . 1.373(4) ? C54 H54 . 0.9500 ? C54 C53 . 1.359(4) ? C54 C55 . 1.426(4) ? C36 H36 . 0.9500 ? C36 C37 . 1.410(4) ? C62 C63 . 1.414(4) ? C60 H60 . 0.9500 ? C50 H50 . 0.9500 ? C22 H22 . 0.9500 ? C22 C21 . 1.372(4) ? C40 H40 . 0.9500 ? C40 C41 . 1.425(4) ? C40 C39 . 1.351(4) ? C53 H53 . 0.9500 ? C37 H37 . 0.9500 ? C42 H42 . 0.9500 ? C42 C41 . 1.417(4) ? C42 C43 . 1.360(4) ? C47 H47 . 0.9500 ? C47 C46 . 1.375(4) ? C64 H64 . 0.9500 ? C64 C63 . 1.369(5) ? C55 C56 . 1.421(4) ? C52 H52A . 0.9800 ? C52 H52B . 0.9800 ? C52 H52C . 0.9800 ? C63 H63 . 0.9500 ? C44 H44A . 0.9800 ? C44 H44B . 0.9800 ? C44 H44C . 0.9800 ? C46 H46 . 0.9500 ? C43 H43 . 0.9500 ? C39 H39 . 0.9500 ? C32 H32 . 0.9500 ? C56 H56 . 0.9500 ? C56 C57 . 1.348(5) ? C58 H58A . 0.9800 ? C58 H58B . 0.9800 ? C58 H58C . 0.9800 ? C57 H57 . 0.9500 ? C66 H66A . 0.9800 ? C66 H66B . 0.9800 ? C66 H66C . 0.9800 ? C51 H51A . 0.9800 ? C51 H51B . 0.9800 ? C51 H51C . 0.9800 ? C45 H45A . 0.9800 ? C45 H45B . 0.9800 ? C45 H45C . 0.9800 ? C65 H65A . 0.9800 ? C65 H65B . 0.9800 ? C65 H65C . 0.9800 ? C59 H59A . 0.9800 ? C59 H59B . 0.9800 ? C59 H59C . 0.9800 ? loop_ _geom_contact_atom_site_label_1 _geom_contact_atom_site_label_2 _geom_contact_distance _geom_contact_site_symmetry_1 _geom_contact_site_symmetry_2 _geom_contact_publ_flag N14 H14 0.84 1_555 ? no loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O5 S1 O4 . . 111.94(13) ? O5 S1 C24 . . 107.15(12) ? O4 S1 C24 . . 104.71(13) ? O3 S1 O5 . . 112.26(14) ? O3 S1 O4 . . 113.97(13) ? O3 S1 C24 . . 106.09(13) ? O7 S2 C33 . . 106.42(13) ? O9 S2 O7 . . 111.50(14) ? O9 S2 C33 . . 106.67(13) ? O8 S2 O7 . . 112.15(17) ? O8 S2 O9 . . 114.36(16) ? O8 S2 C33 . . 105.04(14) ? C30 O10 H10 . . 114(3) ? C21 O6 H6 . . 107(3) ? C28 N11 C29 . . 117.2(2) ? C43 N14 H14 . . 115(2) ? C39 N14 C43 . . 119.4(3) ? C39 N14 H14 . . 125(2) ? C53 N18 C57 . . 119.1(3) ? C53 N18 H18 . . 121(3) ? C57 N18 H18 . . 120(3) ? C37 N12 C38 . . 117.4(2) ? C55 N17 C58 . . 121.4(3) ? C55 N17 C59 . . 120.8(3) ? C59 N17 C58 . . 117.6(3) ? C41 N13 C44 . . 120.9(3) ? C41 N13 C45 . . 121.3(3) ? C45 N13 C44 . . 117.7(3) ? C29 C25 C24 . . 118.4(2) ? C26 C25 C29 . . 116.6(2) ? C26 C25 C24 . . 125.0(2) ? C48 N16 C52 . . 120.9(3) ? C48 N16 C51 . . 121.8(3) ? C52 N16 C51 . . 117.1(3) ? C50 N15 C46 . . 115.2(3) ? O10 C30 C31 . . 119.3(2) ? O10 C30 C38 . . 120.1(2) ? C31 C30 C38 . . 120.6(2) ? C62 N20 C66 . . 120.6(3) ? C62 N20 C65 . . 120.8(3) ? C65 N20 C66 . . 118.5(3) ? N11 C29 C25 . . 123.4(3) ? N11 C29 C21 . . 116.8(2) ? C25 C29 C21 . . 119.8(2) ? C60 N19 C64 . . 115.2(3) ? C34 C35 H35 . . 120.5 ? C36 C35 H35 . . 120.5 ? C36 C35 C34 . . 118.9(3) ? N16 C48 C49 . . 122.2(3) ? N16 C48 C47 . . 122.4(3) ? C49 C48 C47 . . 115.4(3) ? C24 C23 H23 . . 119.2 ? C24 C23 C22 . . 121.7(2) ? C22 C23 H23 . . 119.2 ? C25 C24 S1 . . 120.6(2) ? C23 C24 S1 . . 119.4(2) ? C23 C24 C25 . . 120.0(2) ? C26 C27 H27 . . 120.4 ? C26 C27 C28 . . 119.2(3) ? C28 C27 H27 . . 120.4 ? C25 C26 H26 . . 120.2 ? C27 C26 C25 . . 119.6(3) ? C27 C26 H26 . . 120.2 ? C35 C34 C38 . . 117.1(2) ? C33 C34 C35 . . 124.2(2) ? C33 C34 C38 . . 118.7(2) ? C48 C49 H49 . . 120.0 ? C50 C49 C48 . . 119.9(3) ? C50 C49 H49 . . 120.0 ? C30 C31 H31 . . 120.2 ? C30 C31 C32 . . 119.7(3) ? C32 C31 H31 . . 120.2 ? N12 C38 C30 . . 117.2(2) ? N12 C38 C34 . . 123.3(3) ? C34 C38 C30 . . 119.5(2) ? N11 C28 C27 . . 124.0(3) ? N11 C28 H28 . . 118.0 ? C27 C28 H28 . . 118.0 ? C34 C33 S2 . . 120.5(2) ? C32 C33 S2 . . 119.3(2) ? C32 C33 C34 . . 120.2(3) ? C62 C61 H61 . . 119.9 ? C60 C61 H61 . . 119.9 ? C60 C61 C62 . . 120.1(3) ? C53 C54 H54 . . 119.9 ? C53 C54 C55 . . 120.2(3) ? C55 C54 H54 . . 119.9 ? C35 C36 H36 . . 120.2 ? C35 C36 C37 . . 119.6(3) ? C37 C36 H36 . . 120.2 ? N20 C62 C61 . . 122.2(3) ? N20 C62 C63 . . 122.4(3) ? C61 C62 C63 . . 115.4(3) ? N19 C60 C61 . . 124.6(3) ? N19 C60 H60 . . 117.7 ? C61 C60 H60 . . 117.7 ? N15 C50 C49 . . 124.9(3) ? N15 C50 H50 . . 117.6 ? C49 C50 H50 . . 117.6 ? C23 C22 H22 . . 120.1 ? C21 C22 C23 . . 119.9(3) ? C21 C22 H22 . . 120.1 ? C41 C40 H40 . . 119.3 ? C39 C40 H40 . . 119.3 ? C39 C40 C41 . . 121.3(3) ? N18 C53 C54 . . 122.3(3) ? N18 C53 H53 . . 118.9 ? C54 C53 H53 . . 118.9 ? N12 C37 C36 . . 123.7(2) ? N12 C37 H37 . . 118.2 ? C36 C37 H37 . . 118.2 ? C41 C42 H42 . . 119.6 ? C43 C42 H42 . . 119.6 ? C43 C42 C41 . . 120.7(3) ? N13 C41 C40 . . 121.9(3) ? N13 C41 C42 . . 122.6(3) ? C42 C41 C40 . . 115.4(3) ? O6 C21 C29 . . 120.6(2) ? O6 C21 C22 . . 119.3(3) ? C22 C21 C29 . . 120.2(3) ? C48 C47 H47 . . 120.0 ? C46 C47 C48 . . 120.0(3) ? C46 C47 H47 . . 120.0 ? N19 C64 H64 . . 117.6 ? N19 C64 C63 . . 124.9(3) ? C63 C64 H64 . . 117.6 ? N17 C55 C54 . . 121.7(3) ? N17 C55 C56 . . 122.7(3) ? C56 C55 C54 . . 115.6(3) ? N16 C52 H52A . . 109.5 ? N16 C52 H52B . . 109.5 ? N16 C52 H52C . . 109.5 ? H52A C52 H52B . . 109.5 ? H52A C52 H52C . . 109.5 ? H52B C52 H52C . . 109.5 ? C62 C63 H63 . . 120.1 ? C64 C63 C62 . . 119.8(3) ? C64 C63 H63 . . 120.1 ? N13 C44 H44A . . 109.5 ? N13 C44 H44B . . 109.5 ? N13 C44 H44C . . 109.5 ? H44A C44 H44B . . 109.5 ? H44A C44 H44C . . 109.5 ? H44B C44 H44C . . 109.5 ? N15 C46 C47 . . 124.5(3) ? N15 C46 H46 . . 117.7 ? C47 C46 H46 . . 117.7 ? N14 C43 C42 . . 121.7(3) ? N14 C43 H43 . . 119.1 ? C42 C43 H43 . . 119.1 ? N14 C39 H39 . . 119.3 ? C40 C39 N14 . . 121.4(3) ? C40 C39 H39 . . 119.3 ? C31 C32 H32 . . 119.3 ? C33 C32 C31 . . 121.4(2) ? C33 C32 H32 . . 119.3 ? C55 C56 H56 . . 119.4 ? C57 C56 C55 . . 121.2(3) ? C57 C56 H56 . . 119.4 ? N17 C58 H58A . . 109.5 ? N17 C58 H58B . . 109.5 ? N17 C58 H58C . . 109.5 ? H58A C58 H58B . . 109.5 ? H58A C58 H58C . . 109.5 ? H58B C58 H58C . . 109.5 ? N18 C57 H57 . . 119.2 ? C56 C57 N18 . . 121.7(3) ? C56 C57 H57 . . 119.2 ? N20 C66 H66A . . 109.5 ? N20 C66 H66B . . 109.5 ? N20 C66 H66C . . 109.5 ? H66A C66 H66B . . 109.5 ? H66A C66 H66C . . 109.5 ? H66B C66 H66C . . 109.5 ? N16 C51 H51A . . 109.5 ? N16 C51 H51B . . 109.5 ? N16 C51 H51C . . 109.5 ? H51A C51 H51B . . 109.5 ? H51A C51 H51C . . 109.5 ? H51B C51 H51C . . 109.5 ? N13 C45 H45A . . 109.5 ? N13 C45 H45B . . 109.5 ? N13 C45 H45C . . 109.5 ? H45A C45 H45B . . 109.5 ? H45A C45 H45C . . 109.5 ? H45B C45 H45C . . 109.5 ? N20 C65 H65A . . 109.5 ? N20 C65 H65B . . 109.5 ? N20 C65 H65C . . 109.5 ? H65A C65 H65B . . 109.5 ? H65A C65 H65C . . 109.5 ? H65B C65 H65C . . 109.5 ? N17 C59 H59A . . 109.5 ? N17 C59 H59B . . 109.5 ? N17 C59 H59C . . 109.5 ? H59A C59 H59B . . 109.5 ? H59A C59 H59C . . 109.5 ? H59B C59 H59C . . 109.5 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag S2 C33 C32 C31 . . . . -178.5(2) ? O5 S1 C24 C25 . . . . 50.1(3) ? O5 S1 C24 C23 . . . . -131.4(2) ? O10 C30 C31 C32 . . . . 178.2(3) ? O10 C30 C38 N12 . . . . 1.2(4) ? O10 C30 C38 C34 . . . . -178.4(2) ? O4 S1 C24 C25 . . . . 169.1(2) ? O4 S1 C24 C23 . . . . -12.4(3) ? O7 S2 C33 C34 . . . . -57.5(3) ? O7 S2 C33 C32 . . . . 121.2(3) ? N11 C29 C21 O6 . . . . 0.1(4) ? N11 C29 C21 C22 . . . . -179.9(3) ? O3 S1 C24 C25 . . . . -70.0(3) ? O3 S1 C24 C23 . . . . 108.5(2) ? O9 S2 C33 C34 . . . . 61.6(3) ? O9 S2 C33 C32 . . . . -119.6(3) ? N17 C55 C56 C57 . . . . -179.3(3) ? C25 C29 C21 O6 . . . . -179.6(3) ? C25 C29 C21 C22 . . . . 0.4(4) ? N16 C48 C49 C50 . . . . 178.0(3) ? N16 C48 C47 C46 . . . . -178.6(3) ? C30 C31 C32 C33 . . . . 0.6(5) ? N20 C62 C63 C64 . . . . 179.1(3) ? C29 N11 C28 C27 . . . . 0.4(4) ? C29 C25 C24 S1 . . . . 178.2(2) ? C29 C25 C24 C23 . . . . -0.3(4) ? C29 C25 C26 C27 . . . . 0.4(4) ? N19 C64 C63 C62 . . . . 0.4(5) ? C35 C34 C38 N12 . . . . -0.7(4) ? C35 C34 C38 C30 . . . . 179.0(3) ? C35 C34 C33 S2 . . . . -0.7(4) ? C35 C34 C33 C32 . . . . -179.4(3) ? C35 C36 C37 N12 . . . . -0.1(5) ? O8 S2 C33 C34 . . . . -176.6(2) ? O8 S2 C33 C32 . . . . 2.1(3) ? C48 C49 C50 N15 . . . . 1.2(5) ? C48 C47 C46 N15 . . . . 0.1(5) ? C23 C22 C21 O6 . . . . -179.8(3) ? C23 C22 C21 C29 . . . . 0.2(4) ? C24 C25 C29 N11 . . . . 180.0(3) ? C24 C25 C29 C21 . . . . -0.3(4) ? C24 C25 C26 C27 . . . . 179.4(3) ? C24 C23 C22 C21 . . . . -0.8(4) ? C26 C25 C29 N11 . . . . -0.9(4) ? C26 C25 C29 C21 . . . . 178.7(3) ? C26 C25 C24 S1 . . . . -0.8(4) ? C26 C25 C24 C23 . . . . -179.3(3) ? C26 C27 C28 N11 . . . . -0.9(5) ? C34 C35 C36 C37 . . . . -0.1(4) ? C34 C33 C32 C31 . . . . 0.2(5) ? C49 C48 C47 C46 . . . . 1.3(4) ? C31 C30 C38 N12 . . . . -179.6(3) ? C31 C30 C38 C34 . . . . 0.8(4) ? C38 N12 C37 C36 . . . . -0.1(4) ? C38 C30 C31 C32 . . . . -1.1(4) ? C38 C34 C33 S2 . . . . 178.2(2) ? C38 C34 C33 C32 . . . . -0.5(4) ? C28 N11 C29 C25 . . . . 0.5(4) ? C28 N11 C29 C21 . . . . -179.2(3) ? C28 C27 C26 C25 . . . . 0.5(4) ? C33 C34 C38 N12 . . . . -179.6(3) ? C33 C34 C38 C30 . . . . 0.0(4) ? C61 C62 C63 C64 . . . . -0.7(5) ? C54 C55 C56 C57 . . . . 1.3(4) ? C36 C35 C34 C38 . . . . 0.5(4) ? C36 C35 C34 C33 . . . . 179.4(3) ? C62 C61 C60 N19 . . . . -1.2(5) ? C60 N19 C64 C63 . . . . -0.5(5) ? C60 C61 C62 N20 . . . . -178.7(3) ? C60 C61 C62 C63 . . . . 1.1(5) ? C50 N15 C46 C47 . . . . -0.9(5) ? C22 C23 C24 S1 . . . . -177.6(2) ? C22 C23 C24 C25 . . . . 0.9(4) ? C53 N18 C57 C56 . . . . -0.4(5) ? C53 C54 C55 N17 . . . . -179.8(3) ? C53 C54 C55 C56 . . . . -0.4(4) ? C37 N12 C38 C30 . . . . -179.2(3) ? C37 N12 C38 C34 . . . . 0.5(4) ? C41 C40 C39 N14 . . . . 0.4(5) ? C41 C42 C43 N14 . . . . -0.4(5) ? C47 C48 C49 C50 . . . . -1.9(4) ? C64 N19 C60 C61 . . . . 0.9(5) ? C55 C54 C53 N18 . . . . -0.8(5) ? C55 C56 C57 N18 . . . . -0.9(5) ? C52 N16 C48 C49 . . . . -4.7(5) ? C52 N16 C48 C47 . . . . 175.2(3) ? C44 N13 C41 C40 . . . . -0.5(5) ? C44 N13 C41 C42 . . . . 179.4(3) ? C46 N15 C50 C49 . . . . 0.3(5) ? C43 N14 C39 C40 . . . . 0.8(5) ? C43 C42 C41 N13 . . . . -178.4(3) ? C43 C42 C41 C40 . . . . 1.6(4) ? C39 N14 C43 C42 . . . . -0.8(5) ? C39 C40 C41 N13 . . . . 178.4(3) ? C39 C40 C41 C42 . . . . -1.6(4) ? C58 N17 C55 C54 . . . . -2.7(4) ? C58 N17 C55 C56 . . . . 177.9(3) ? C57 N18 C53 C54 . . . . 1.2(5) ? C66 N20 C62 C61 . . . . 174.1(3) ? C66 N20 C62 C63 . . . . -5.7(5) ? C51 N16 C48 C49 . . . . 179.8(3) ? C51 N16 C48 C47 . . . . -0.3(5) ? C45 N13 C41 C40 . . . . -176.3(3) ? C45 N13 C41 C42 . . . . 3.7(5) ? C65 N20 C62 C61 . . . . -3.0(5) ? C65 N20 C62 C63 . . . . 177.2(3) ? C59 N17 C55 C54 . . . . -177.4(3) ? C59 N17 C55 C56 . . . . 3.2(5) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_D _geom_hbond_site_symmetry_H _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O6 H6 O8 . . 1_545 0.84(5) 2.00(5) 2.679(3) 137(4) yes O6 H6 N11 . . . 0.84(5) 2.24(5) 2.728(3) 117(4) yes O10 H10 O4 . . 1_555 0.89(5) 1.90(5) 2.674(3) 144(4) yes O10 H10 N12 . . . 0.89(5) 2.31(5) 2.730(3) 109(4) yes N14 H14 N15 . . 1_555 0.90(3) 1.91(3) 2.814(4) 174(3) yes N18 H18 N19 . . 1_555 0.90(3) 1.92(4) 2.816(4) 177(7) yes C27 H27 O6 . . 1_455 0.95 2.58 3.219(4) 125 yes C27 H27 O8 . . 1_445 0.95 2.27 3.194(4) 164 yes C36 H36 O4 . . 1_655 0.95 2.33 3.244(4) 160 yes C36 H36 O10 . . 1_655 0.95 2.58 3.216(4) 125 yes C39 H39 O3 . . 2_565 0.95 2.32 3.200(4) 154 yes C43 H43 O5 . . . 0.95 2.22 3.160(4) 169 yes C46 H46 O5 . . . 0.95 2.46 3.373(4) 161 yes C50 H50 O3 . . 2_565 0.95 2.43 3.292(4) 151 yes C53 H53 O9 . . 2_575 0.95 2.22 3.146(4) 164 yes C54 H54 O10 . . 2_675 0.95 2.55 3.450(4) 158 yes C57 H57 O7 . . . 0.95 2.22 3.143(4) 165 yes C60 H60 O7 . . . 0.95 2.40 3.325(4) 163 yes C64 H64 O9 . . 2_575 0.95 2.35 3.267(4) 162 yes C40 H40 Cg1 . . 2_565 0.95 2.63 3.498(3) 153 yes C49 H49 Cg2 . . 2_465 0.95 2.87 3.754(3) 156 yes C61 H61 Cg2 . . 1_555 0.95 2.70 3.571(3) 152 yes _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _shelx_hkl_file ; 0 0 2 296.01 7.93 0 0 3 0.10 0.17 0 0 5 -0.05 0.26 0 0 6 9999.00 253.65 0 0 7 0.15 0.32 0 0 8 1801.92 47.30 0 0 9 0.60 0.45 0 0 9 -0.10 0.40 0 0 9 0.24 0.40 0 0 10 2384.35 63.23 0 0 10 2416.49 63.18 0 0 10 2401.60 62.80 0 0 10 2364.43 63.17 0 0 11 0.71 0.49 0 0 11 0.63 0.55 0 0 11 0.32 0.50 0 0 11 0.13 0.30 0 0 11 0.48 0.53 0 0 12 4526.10 112.40 0 0 12 4225.03 113.24 0 0 12 4388.23 113.02 0 0 12 4317.88 112.57 0 0 12 4214.93 113.19 0 0 12 4326.03 113.19 0 0 13 -0.13 0.38 0 0 13 0.20 0.60 0 0 13 -0.19 0.53 0 0 13 0.41 0.75 0 0 13 0.33 0.47 0 0 13 0.40 0.57 0 0 13 -0.60 0.79 0 0 14 242.01 9.89 0 0 14 244.17 9.14 0 0 14 230.84 9.69 0 0 14 258.70 9.18 0 0 15 0.25 0.71 0 0 15 -0.18 0.82 0 0 15 0.24 0.65 0 0 15 0.19 0.50 0 0 16 4022.86 105.80 0 0 16 3790.36 105.46 0 0 16 3977.05 104.30 0 0 16 4121.20 105.44 0 0 17 -0.27 0.90 0 0 17 0.27 0.60 0 0 17 -0.25 0.79 0 0 17 -0.20 0.94 0 0 18 79.49 5.14 0 0 18 73.84 4.85 0 0 18 72.08 4.36 0 0 19 -0.36 0.70 0 0 19 0.21 0.56 0 0 19 0.91 0.95 0 0 20 640.42 19.29 0 0 20 599.31 19.37 0 0 21 -0.16 0.43 0 0 21 0.17 0.54 0 0 22 155.12 5.96 0 -1 1 5.65 0.37 0 -1 1 6.06 0.31 0 -1 2 9.72 0.61 0 1 2 9.94 0.45 0 -1 2 9.51 0.55 0 -1 3 6.75 0.60 0 1 3 6.79 0.47 0 1 4 33.30 1.40 0 1 5 20.36 1.15 0 -1 6 117.26 4.19 0 1 6 113.02 3.91 0 -1 7 41.33 2.27 0 1 7 41.57 2.04 0 1 8 42.97 2.24 0 -1 8 44.29 2.44 0 -1 9 26.69 2.02 0 1 9 27.78 1.84 0 -1 9 23.95 1.96 0 1 9 27.88 2.07 0 -1 10 45.66 3.00 0 -1 10 48.43 3.04 0 -1 10 55.52 3.20 0 1 10 60.29 3.02 0 -1 10 57.27 3.11 0 1 10 52.17 2.80 0 -1 11 11.16 1.52 0 -1 11 9.79 1.41 0 -1 11 9.99 1.42 0 1 11 8.25 1.13 0 1 11 9.50 1.21 0 -1 11 8.47 1.23 0 1 12 93.78 4.44 0 -1 12 93.75 4.75 0 -1 12 95.72 4.84 0 -1 12 100.11 5.10 0 -1 12 95.35 4.96 0 1 12 112.83 4.86 0 -1 12 92.76 4.89 0 -1 13 90.84 4.92 0 -1 13 95.59 5.17 0 -1 13 90.21 4.38 0 -1 13 90.04 5.11 0 -1 13 101.06 4.64 0 1 13 95.53 4.68 0 1 13 94.78 4.56 0 -1 13 98.05 4.93 0 1 14 31.86 2.73 0 -1 14 34.69 3.04 0 -1 14 29.61 2.35 0 -1 14 33.74 3.06 0 -1 14 33.19 2.79 0 1 14 29.65 2.49 0 -1 14 31.55 2.55 0 1 14 32.33 2.63 0 -1 15 19.55 2.44 0 -1 15 21.47 2.58 0 1 15 23.45 2.43 0 -1 15 20.01 2.22 0 -1 15 18.34 2.05 0 1 15 24.87 2.41 0 -1 16 53.89 4.25 0 -1 16 43.07 3.75 0 -1 16 56.57 3.75 0 1 16 54.20 3.77 0 1 16 44.80 3.57 0 1 17 108.24 5.77 0 -1 17 103.16 6.05 0 1 17 97.46 5.89 0 -1 17 97.23 5.92 0 -1 17 99.88 5.79 0 -1 17 103.66 5.33 0 1 17 106.64 5.50 0 -1 18 28.99 3.05 0 1 18 33.55 2.98 0 -1 18 34.50 3.17 0 1 18 36.23 2.96 0 -1 18 32.88 2.81 0 -1 19 5.66 1.17 0 1 19 4.77 1.11 0 -1 19 8.18 1.52 0 1 19 6.39 1.38 0 -1 20 12.94 1.85 0 1 20 12.36 1.72 0 -1 21 5.92 1.19 0 1 21 7.32 1.21 0 -1 22 11.13 1.30 0 -2 0 859.32 21.95 0 -2 0 857.72 21.89 0 -2 1 124.62 3.72 0 -2 1 131.99 3.64 0 -2 2 1215.82 31.80 0 -2 2 1242.84 31.65 0 2 3 195.97 5.23 0 -2 3 193.88 5.84 0 2 4 448.95 11.89 0 -2 4 455.82 12.56 0 -2 5 28.36 1.66 0 2 5 29.69 1.30 0 2 6 720.16 19.12 0 2 7 35.98 1.75 0 2 8 509.92 14.25 0 -2 9 16.78 1.60 0 2 9 19.11 1.67 0 -2 9 17.28 1.39 0 2 9 18.26 1.38 0 -2 9 22.01 1.81 0 -2 9 18.98 1.68 0 2 9 16.18 1.58 0 2 10 325.90 10.53 0 -2 10 313.76 10.47 0 -2 10 307.60 10.44 0 2 10 307.21 10.42 0 -2 10 296.85 9.72 0 -2 10 322.77 10.50 0 2 10 328.54 10.53 0 2 10 310.90 9.70 0 -2 10 335.48 10.65 0 2 10 314.43 10.14 0 2 11 123.59 5.55 0 -2 11 116.18 5.45 0 2 11 126.66 5.58 0 -2 11 127.64 5.64 0 -2 11 121.98 4.93 0 2 11 136.67 5.53 0 -2 11 121.84 5.49 0 2 11 126.41 5.55 0 2 11 116.50 4.80 0 -2 11 127.58 5.59 0 2 11 118.49 5.17 0 -2 12 273.28 10.08 0 2 12 282.65 9.28 0 2 12 282.84 9.95 0 -2 12 274.88 9.95 0 2 12 284.87 10.04 0 -2 12 291.14 10.36 0 2 12 285.42 10.31 0 2 12 282.14 10.14 0 -2 12 282.73 10.18 0 2 12 294.43 10.33 0 2 12 264.82 9.70 0 -2 13 49.55 3.49 0 2 13 60.74 3.65 0 2 13 45.68 3.40 0 -2 13 50.87 3.49 0 2 13 47.95 3.56 0 -2 13 49.57 3.60 0 -2 13 49.00 3.14 0 2 13 57.84 3.49 0 2 13 52.91 3.65 0 -2 13 47.50 3.49 0 2 13 50.33 3.58 0 -2 14 192.61 8.30 0 2 14 206.23 8.32 0 2 14 202.39 8.50 0 -2 14 200.37 8.48 0 2 14 203.87 8.46 0 2 14 208.33 8.72 0 -2 14 207.37 8.70 0 2 14 192.81 7.99 0 -2 14 195.79 7.72 0 -2 14 198.62 7.68 0 -2 15 102.47 5.69 0 2 15 118.97 6.13 0 2 15 120.89 5.94 0 2 15 108.84 5.99 0 -2 15 102.61 5.86 0 -2 15 115.88 6.19 0 2 15 114.55 6.18 0 -2 15 121.03 5.52 0 2 15 110.53 5.60 0 -2 15 101.69 5.14 0 2 16 212.11 9.00 0 2 16 218.08 9.37 0 -2 16 216.09 9.33 0 -2 16 203.22 8.72 0 2 16 198.18 8.99 0 -2 16 212.66 9.20 0 -2 16 189.90 8.00 0 2 16 189.17 8.32 0 2 16 220.65 8.92 0 2 17 88.79 5.31 0 -2 17 81.63 5.38 0 2 17 97.73 5.70 0 -2 17 92.37 4.86 0 2 17 82.93 4.83 0 -2 17 87.54 5.50 0 2 17 73.84 5.13 0 -2 17 89.73 5.34 0 2 17 82.90 5.01 0 -2 18 92.25 5.54 0 2 18 88.11 5.39 0 2 18 84.46 5.05 0 -2 18 84.30 4.66 0 2 18 80.76 4.72 0 2 18 88.89 5.31 0 -2 18 99.56 5.53 0 2 19 39.99 3.23 0 -2 19 37.42 2.84 0 2 19 40.09 3.00 0 -2 19 43.05 3.40 0 2 19 45.39 3.49 0 -2 20 125.37 5.98 0 2 20 113.81 5.76 0 2 20 120.60 5.74 0 -2 21 39.21 2.85 0 -2 22 100.76 4.44 0 -3 0 0.20 0.14 0 -3 0 0.12 0.14 0 3 1 2.34 0.17 0 -3 1 2.55 0.19 0 -3 -1 2.69 0.19 0 -3 1 3.20 0.35 0 -3 1 3.26 0.40 0 -3 -1 2.63 0.18 0 -3 2 9.58 0.69 0 -3 2 8.90 0.73 0 -3 3 9.66 0.84 0 -3 4 4.37 0.63 0 -3 5 7.26 0.86 0 3 5 7.78 0.50 0 -3 6 4.52 0.75 0 3 6 4.35 0.44 0 -3 7 9.01 1.12 0 3 7 8.29 0.70 0 3 8 4.36 0.57 0 -3 8 3.24 0.70 0 -3 9 35.31 2.36 0 3 9 30.97 2.25 0 3 9 35.09 2.27 0 3 9 33.88 1.81 0 -3 9 29.80 2.19 0 3 9 33.97 2.30 0 3 9 31.62 2.19 0 -3 9 33.73 2.02 0 -3 9 33.34 2.26 0 3 9 32.58 2.21 0 -3 10 47.01 2.99 0 3 10 53.87 3.12 0 3 10 54.79 3.05 0 3 10 48.32 2.39 0 -3 10 43.56 2.86 0 3 10 44.53 2.93 0 3 10 50.17 2.99 0 -3 10 50.28 2.68 0 -3 10 46.15 2.92 0 3 10 53.10 3.08 0 3 11 5.37 1.04 0 -3 11 2.88 0.79 0 -3 11 5.12 1.07 0 3 11 3.53 0.89 0 3 11 3.31 0.80 0 -3 11 4.29 0.84 0 -3 11 2.96 0.80 0 3 11 4.22 0.98 0 3 11 6.03 1.07 0 -3 12 13.37 1.75 0 3 12 13.58 1.76 0 -3 12 13.17 1.56 0 3 12 12.38 1.65 0 -3 12 14.19 1.50 0 3 12 14.66 1.74 0 3 12 12.84 1.71 0 -3 12 13.54 1.73 0 -3 12 11.45 1.60 0 3 12 10.25 1.57 0 3 12 11.46 1.51 0 3 12 15.29 1.85 0 -3 12 14.55 1.81 0 3 12 14.83 1.78 0 3 13 10.51 1.57 0 -3 13 7.62 1.39 0 3 13 14.26 1.84 0 3 13 10.64 1.57 0 3 13 11.36 1.59 0 3 13 9.13 1.53 0 -3 13 8.09 1.49 0 3 13 12.11 1.75 0 -3 13 10.99 1.54 0 -3 13 9.11 1.51 0 -3 14 42.57 3.46 0 3 14 47.35 3.49 0 -3 14 45.68 3.55 0 3 14 48.30 3.64 0 3 14 55.12 3.84 0 3 14 55.82 3.67 0 -3 14 46.87 3.24 0 3 14 44.26 3.58 0 -3 14 53.61 3.84 0 -3 15 14.84 2.07 0 3 15 17.84 2.19 0 3 15 15.31 2.19 0 -3 15 14.69 2.06 0 3 15 18.20 2.30 0 3 15 17.35 2.25 0 3 15 15.06 1.99 0 -3 15 16.61 1.92 0 -3 15 18.35 2.00 0 -3 15 17.66 2.31 0 3 16 16.19 2.12 0 3 16 15.27 2.05 0 -3 16 14.36 1.90 0 -3 16 17.70 2.33 0 -3 16 15.89 2.22 0 3 16 15.07 2.18 0 3 16 15.24 2.23 0 -3 16 17.20 2.24 0 3 16 16.44 2.17 0 3 17 19.23 2.35 0 3 17 18.41 2.27 0 -3 17 17.20 2.33 0 3 17 18.83 2.38 0 -3 17 20.97 2.47 0 -3 17 22.36 2.68 0 3 17 19.87 2.49 0 3 17 17.47 2.13 0 -3 17 24.21 2.33 0 -3 18 18.79 2.00 0 3 18 12.06 1.76 0 -3 18 15.13 2.11 0 3 18 15.81 2.13 0 3 18 11.59 1.80 0 -3 18 14.34 1.90 0 -3 19 7.26 1.23 0 -3 19 7.30 1.50 0 3 19 6.42 1.32 0 3 19 7.19 1.41 0 -3 19 7.63 1.43 0 3 20 10.43 1.55 0 -3 20 10.11 1.61 0 -3 20 13.38 1.69 0 -3 21 33.60 2.53 0 3 -21 33.52 2.37 0 -3 21 30.22 2.35 0 -4 0 66.16 2.16 0 -4 1 181.91 5.46 0 -4 -1 188.42 5.00 0 4 2 3760.00 94.18 0 -4 2 3702.01 94.22 0 -4 2 3639.97 94.85 0 -4 3 159.64 4.63 0 4 3 152.06 4.57 0 -4 3 164.38 5.19 0 4 4 527.98 14.06 0 -4 4 511.96 14.07 0 -4 4 526.83 14.66 0 -4 5 10.11 0.88 0 4 5 9.59 0.85 0 -4 6 233.97 7.38 0 4 6 236.88 7.34 0 -4 6 244.70 7.88 0 4 7 127.47 4.68 0 -4 7 119.71 4.64 0 4 8 734.57 20.11 0 -4 8 745.39 20.18 0 -4 8 760.37 20.72 0 4 8 678.26 20.21 0 -4 8 696.43 19.76 0 4 8 690.81 20.16 0 4 9 72.03 3.66 0 -4 9 72.42 3.31 0 4 9 72.32 3.67 0 4 9 64.72 3.49 0 -4 9 67.24 3.58 0 4 9 70.42 3.55 0 -4 9 77.70 3.72 0 4 9 71.74 3.57 0 -4 9 79.52 3.99 0 -4 10 7.67 1.03 0 4 10 7.87 1.19 0 4 10 7.08 1.19 0 -4 10 6.42 1.09 0 4 10 7.47 1.17 0 4 10 7.23 1.13 0 -4 10 6.35 1.08 0 4 10 8.25 1.18 0 -4 11 57.84 3.08 0 4 11 57.07 3.51 0 4 11 48.36 3.30 0 4 11 56.05 3.43 0 -4 11 56.04 3.29 0 -4 11 55.23 3.37 0 4 11 56.50 3.37 0 4 11 57.22 3.48 0 -4 11 50.40 3.32 0 4 12 192.14 7.75 0 4 12 192.88 7.76 0 4 12 195.09 7.83 0 -4 12 188.31 7.09 0 4 12 194.83 7.79 0 -4 12 196.18 7.89 0 4 12 185.52 7.70 0 -4 12 187.85 7.41 0 4 12 182.17 7.57 0 -4 12 188.13 7.72 0 4 13 104.68 5.36 0 -4 13 96.09 5.20 0 4 13 97.07 5.21 0 4 13 107.88 5.46 0 -4 13 96.46 4.67 0 4 13 97.80 5.25 0 -4 13 95.84 5.28 0 4 13 93.50 5.13 0 -4 13 104.90 5.56 0 -4 13 108.04 5.13 0 -4 14 465.38 15.92 0 4 14 476.16 15.95 0 4 14 462.66 15.87 0 4 14 479.23 15.95 0 -4 14 485.25 16.11 0 4 14 481.66 16.06 0 4 14 469.43 15.81 0 -4 14 480.01 16.22 0 -4 14 499.01 15.57 0 -4 15 21.60 2.50 0 4 15 29.22 2.83 0 4 15 23.44 2.60 0 4 15 25.78 2.64 0 -4 15 23.83 2.67 0 4 15 23.94 2.59 0 4 15 29.67 2.78 0 -4 15 18.02 2.39 0 -4 15 26.76 2.46 0 4 16 87.27 5.30 0 -4 16 87.75 5.33 0 4 16 91.59 5.30 0 -4 16 86.11 5.34 0 4 16 84.21 5.22 0 -4 16 93.02 4.90 0 -4 16 100.29 4.97 0 4 16 86.92 5.05 0 -4 16 86.96 5.36 0 4 16 90.36 5.24 0 4 17 10.65 1.68 0 -4 17 11.40 1.60 0 -4 17 11.80 1.88 0 4 17 7.48 1.55 0 4 17 12.59 1.96 0 -4 17 6.66 1.44 0 4 17 11.91 1.85 0 -4 17 12.78 1.94 0 4 17 11.93 1.85 0 -4 18 211.77 8.11 0 4 18 199.61 8.60 0 -4 18 225.43 9.02 0 4 18 204.50 8.75 0 -4 19 2.59 0.78 0 -4 19 2.41 0.97 0 4 19 1.00 0.67 0 -4 19 2.26 0.85 0 -4 20 23.76 2.25 0 4 -20 25.36 2.23 0 -4 20 22.92 2.17 0 -4 21 4.51 0.94 0 4 -21 4.00 0.84 0 -4 21 3.84 0.87 0 -4 22 13.23 1.29 0 -5 0 0.06 0.13 0 -5 1 1.14 0.29 0 -5 -1 0.93 0.17 0 -5 2 2.28 0.44 0 -5 -2 1.91 0.18 0 -5 3 1.92 0.29 0 5 3 1.83 0.27 0 -5 3 1.57 0.44 0 -5 4 4.29 0.51 0 5 4 4.30 0.48 0 -5 4 4.15 0.71 0 -5 5 22.83 1.35 0 5 5 22.83 1.31 0 -5 5 25.00 1.74 0 -5 6 66.53 2.85 0 5 6 65.52 2.77 0 -5 6 66.01 3.27 0 -5 7 37.76 2.13 0 5 7 38.84 2.12 0 -5 7 36.84 2.45 0 5 7 34.23 2.25 0 5 8 77.50 3.54 0 -5 8 78.91 3.57 0 -5 8 84.09 4.10 0 5 8 79.04 3.84 0 5 8 75.13 3.72 0 5 9 5.08 0.98 0 -5 9 6.31 0.96 0 5 9 7.79 1.11 0 5 9 7.91 1.17 0 5 9 6.67 1.03 0 -5 9 4.77 0.89 0 -5 9 6.55 1.04 0 5 9 6.27 0.97 0 -5 9 6.88 1.19 0 -5 10 17.89 1.62 0 5 10 13.17 1.60 0 5 10 13.22 1.56 0 5 10 13.08 1.64 0 5 10 14.19 1.59 0 -5 10 13.29 1.56 0 -5 10 13.88 1.52 0 5 10 15.54 1.61 0 -5 10 16.17 1.84 0 -5 11 22.76 2.30 0 5 11 18.82 1.90 0 5 11 23.98 2.17 0 5 11 23.83 2.26 0 5 11 22.01 2.10 0 -5 11 21.21 2.07 0 5 11 22.06 2.20 0 -5 11 22.50 1.93 0 5 11 23.28 2.09 0 -5 11 24.82 2.17 0 5 12 20.64 2.05 0 5 12 18.99 2.04 0 5 12 18.19 1.95 0 -5 12 17.95 1.95 0 5 12 16.56 1.90 0 5 12 19.67 2.16 0 -5 12 14.56 1.61 0 5 12 17.82 2.00 0 -5 12 18.86 2.06 0 5 12 14.51 1.91 0 -5 13 4.32 1.12 0 5 13 3.64 1.04 0 -5 13 3.21 0.95 0 5 13 4.16 1.08 0 -5 13 4.54 1.08 0 5 13 3.83 1.05 0 5 13 4.33 1.13 0 5 13 3.57 1.06 0 -5 13 3.52 0.99 0 -5 14 34.38 2.99 0 5 14 32.26 2.92 0 5 14 29.54 2.85 0 5 14 39.36 3.17 0 5 14 29.10 2.79 0 -5 14 29.23 2.80 0 5 14 30.59 2.85 0 -5 14 35.29 2.86 0 5 15 4.24 1.21 0 -5 15 8.09 1.45 0 5 15 6.97 1.43 0 -5 15 6.52 1.39 0 5 15 3.87 1.13 0 -5 15 7.15 1.43 0 5 15 7.67 1.47 0 -5 15 5.10 1.34 0 -5 16 3.54 1.04 0 -5 16 1.65 0.86 0 5 16 2.30 0.93 0 5 16 2.30 0.87 0 5 16 4.22 1.22 0 -5 16 3.14 1.10 0 -5 16 3.61 1.07 0 5 16 3.65 1.12 0 -5 17 6.35 1.32 0 5 17 5.10 1.28 0 -5 17 4.47 1.03 0 -5 18 8.62 1.55 0 5 18 11.73 1.71 0 -5 18 13.46 1.62 0 -5 19 1.07 0.62 0 -5 19 1.64 0.78 0 5 -19 2.17 0.77 0 -5 20 29.46 2.36 0 5 -20 27.18 2.24 0 -5 20 27.00 2.28 0 -5 21 0.92 0.52 0 5 -21 0.41 0.47 0 -5 21 1.37 0.53 0 -6 0 25.98 1.22 0 -6 1 560.78 15.18 0 -6 2 622.09 17.04 0 -6 -3 284.57 7.71 0 -6 3 319.31 8.96 0 -6 4 57.93 2.18 0 6 4 60.61 2.16 0 -6 5 47.01 2.62 0 -6 5 47.45 2.08 0 6 5 48.60 2.03 0 -6 6 80.29 3.88 0 6 6 85.16 3.23 0 -6 6 83.25 3.30 0 -6 7 50.94 3.03 0 -6 7 48.51 2.49 0 6 7 50.10 2.45 0 -6 8 73.16 3.49 0 6 8 73.38 3.43 0 6 -8 86.40 3.50 0 -6 8 82.30 4.17 0 -6 9 7.59 1.26 0 -6 9 7.00 1.04 0 6 9 8.47 1.09 0 -6 9 6.34 1.02 0 -6 9 8.62 1.17 0 6 9 6.12 0.96 0 6 9 8.12 1.12 0 -6 10 142.81 5.98 0 6 10 151.26 6.03 0 6 10 165.45 6.33 0 -6 10 147.09 5.83 0 -6 10 146.81 6.12 0 6 10 152.56 6.13 0 -6 10 145.39 6.17 0 -6 10 152.10 6.74 0 6 10 148.43 6.08 0 6 11 50.70 3.21 0 -6 11 50.84 3.23 0 6 11 53.90 3.33 0 -6 11 49.67 3.03 0 6 11 49.77 3.46 0 6 11 42.69 3.16 0 6 11 54.57 3.38 0 -6 11 56.46 3.46 0 -6 11 54.22 3.41 0 6 11 52.81 3.32 0 -6 11 57.02 3.82 0 6 12 18.42 2.01 0 6 12 18.00 2.01 0 6 12 15.87 1.86 0 6 12 15.78 2.01 0 -6 12 17.28 1.78 0 -6 12 15.63 2.12 0 -6 12 17.33 1.94 0 6 12 14.61 1.78 0 -6 12 12.20 1.67 0 6 13 114.74 5.68 0 6 13 118.34 5.87 0 6 13 113.47 5.67 0 -6 13 119.90 5.84 0 -6 13 117.11 5.36 0 6 13 110.56 5.58 0 -6 13 115.34 5.70 0 -6 13 127.90 6.44 0 -6 14 227.63 8.44 0 6 14 219.00 8.86 0 -6 14 208.57 8.80 0 6 14 226.97 9.08 0 -6 14 227.11 9.03 0 6 14 214.88 8.82 0 -6 15 32.91 2.87 0 6 15 30.34 2.80 0 -6 15 29.96 2.82 0 6 15 32.76 2.97 0 -6 15 39.66 3.18 0 6 16 48.41 3.61 0 -6 16 57.91 3.78 0 -6 17 105.91 5.09 0 -6 17 100.40 5.33 0 6 -17 103.53 5.53 0 -6 18 144.26 5.94 0 6 -18 131.98 6.35 0 -6 18 143.00 6.35 0 -6 19 30.99 2.48 0 -6 19 26.65 2.28 0 6 -19 23.78 2.24 0 6 -20 1.37 0.59 0 -6 20 0.28 0.47 0 6 -20 1.32 0.55 0 -6 20 1.26 0.60 0 6 -21 1.62 0.58 0 -6 21 2.31 0.64 0 -7 0 15.60 0.93 0 -7 1 80.85 3.00 0 -7 2 45.58 2.20 0 -7 3 4.57 0.75 0 7 -3 5.18 0.89 0 7 -4 0.77 0.45 0 -7 4 0.10 0.33 0 7 -4 -0.29 0.38 0 7 -4 0.29 0.40 0 7 -4 0.37 0.41 0 7 -5 28.54 2.21 0 7 -5 28.60 1.90 0 -7 5 30.13 2.08 0 7 -5 28.30 1.90 0 7 -5 24.52 2.02 0 7 -6 5.23 0.98 0 -7 6 4.57 0.88 0 7 -6 4.65 0.81 0 -7 6 4.09 0.58 0 7 6 4.73 0.59 0 7 -6 5.17 0.85 0 7 -6 3.72 0.82 0 -7 7 4.67 0.96 0 7 -7 5.24 0.86 0 7 -7 5.22 1.10 0 -7 7 4.78 0.72 0 7 7 4.43 0.65 0 7 -8 20.36 1.66 0 -7 8 22.99 2.13 0 7 8 20.92 1.57 0 -7 8 19.68 1.60 0 7 -8 21.70 2.14 0 -7 9 0.89 0.54 0 7 9 0.56 0.49 0 7 -9 0.58 0.55 0 7 9 0.50 0.40 0 7 9 0.34 0.30 0 -7 9 0.62 0.39 0 7 -9 0.52 0.39 0 -7 9 0.56 0.53 0 7 10 21.28 1.86 0 -7 10 21.05 1.90 0 -7 10 26.01 2.49 0 -7 10 23.15 1.98 0 7 10 24.40 2.14 0 -7 10 23.27 2.17 0 -7 11 1.22 0.72 0 7 11 1.17 0.71 0 -7 11 1.18 0.69 0 -7 11 0.22 0.50 0 7 11 0.17 0.45 0 7 11 0.76 0.48 0 -7 11 1.12 0.53 0 7 11 0.31 0.35 0 7 12 23.24 2.25 0 -7 12 24.00 2.39 0 7 12 19.33 2.14 0 -7 12 21.26 2.06 0 -7 12 19.68 2.36 0 7 12 20.41 2.01 0 7 12 21.77 2.10 0 7 13 6.78 1.40 0 -7 13 8.51 1.64 0 -7 13 10.29 1.64 0 -7 13 7.97 1.40 0 7 13 7.39 1.29 0 7 -13 7.59 1.50 0 -7 13 7.56 1.29 0 -7 14 2.85 1.08 0 -7 14 2.71 0.95 0 7 -14 4.32 1.16 0 -7 15 7.35 1.57 0 7 -15 7.58 1.50 0 -7 16 69.92 4.18 0 7 -16 70.80 4.54 0 -7 17 18.76 2.00 0 7 -17 17.58 2.10 0 -7 17 17.37 1.86 0 7 -18 0.18 0.49 0 7 -18 0.78 0.65 0 -7 18 0.15 0.52 0 -7 19 0.76 0.57 0 7 -19 -0.15 0.43 0 7 -19 0.33 0.52 0 -7 19 0.13 0.44 0 -7 20 6.02 0.97 0 7 -20 5.11 0.95 0 -7 20 4.97 0.76 0 7 -20 5.31 0.87 0 8 0 199.73 7.07 0 8 0 191.32 6.90 0 8 1 55.35 2.93 0 8 -1 57.65 3.10 0 8 1 53.96 2.81 0 8 -1 57.99 2.96 0 8 -1 55.38 3.11 0 -8 1 60.58 2.42 0 8 -1 58.34 3.01 0 8 1 55.62 2.91 0 8 -2 37.56 2.46 0 8 2 35.88 2.22 0 8 -2 33.49 2.22 0 8 2 35.23 2.19 0 8 -2 38.19 2.29 0 8 2 32.04 2.05 0 8 -2 32.41 2.33 0 -8 2 32.02 1.84 0 8 -3 69.86 3.64 0 8 3 68.36 3.31 0 8 -3 66.12 3.33 0 8 3 69.13 3.26 0 8 3 71.03 3.22 0 8 -3 64.30 3.26 0 8 -3 69.54 3.67 0 -8 3 73.58 3.23 0 8 -4 57.97 3.28 0 8 4 53.29 2.78 0 8 -4 52.96 2.91 0 8 4 51.56 2.70 0 8 -4 57.47 3.34 0 -8 4 59.03 3.00 0 8 -4 54.17 2.94 0 -8 5 36.61 2.46 0 8 -5 37.92 2.71 0 8 -5 37.43 2.41 0 8 -5 44.39 2.92 0 8 5 41.08 2.34 0 8 -5 43.68 2.56 0 -8 6 74.43 3.86 0 8 -6 70.36 4.00 0 8 -6 75.31 3.63 0 8 -6 77.71 4.20 0 8 -6 76.58 3.64 0 8 -7 288.02 10.48 0 8 -7 302.64 10.72 0 -8 7 308.98 10.38 0 8 -7 285.85 9.56 0 -8 8 240.99 9.05 0 -8 8 236.62 8.60 0 8 -8 245.61 9.34 0 8 -8 246.35 9.45 0 8 8 242.24 8.44 0 8 -8 230.65 8.10 0 -8 9 165.12 7.31 0 -8 9 172.66 6.92 0 8 -9 155.93 7.37 0 8 -9 179.92 7.72 0 8 9 175.72 6.78 0 8 -9 165.08 6.22 0 -8 10 69.95 3.74 0 -8 10 59.91 4.08 0 8 -10 67.76 4.48 0 8 -10 68.58 4.51 0 8 10 67.60 3.84 0 -8 10 66.02 3.90 0 -8 11 21.37 2.07 0 -8 11 20.76 2.43 0 8 -11 20.29 2.48 0 8 -11 22.59 2.60 0 8 11 25.05 2.35 0 -8 11 28.71 2.50 0 -8 12 13.84 1.67 0 -8 12 12.96 1.77 0 8 -12 11.92 1.89 0 8 12 13.86 1.78 0 -8 12 13.21 1.98 0 -8 13 56.29 3.44 0 -8 13 52.33 4.05 0 8 -13 48.98 3.89 0 8 -13 46.36 3.86 0 8 13 47.22 3.43 0 -8 13 49.43 3.53 0 -8 14 80.01 5.14 0 -8 14 78.52 4.24 0 8 -14 71.34 4.77 0 8 -14 64.73 4.63 0 -8 14 78.33 4.59 0 -8 15 4.59 1.07 0 -8 15 3.21 1.05 0 8 -15 4.48 1.19 0 8 -15 3.38 1.06 0 8 -16 36.33 3.18 0 8 -16 40.86 3.29 0 -8 16 38.14 2.79 0 -8 17 26.48 2.22 0 8 -17 28.18 2.58 0 -8 17 27.34 2.21 0 8 -17 28.26 2.64 0 8 -18 20.99 2.07 0 8 -18 19.67 2.03 0 8 -19 11.10 1.31 0 -8 19 13.04 1.43 0 8 -20 9.45 1.14 0 -8 20 12.95 1.26 0 9 0 9.03 1.27 0 9 0 5.91 1.05 0 9 -1 18.23 1.66 0 9 1 19.93 1.69 0 9 -1 21.03 1.91 0 9 1 19.63 1.74 0 9 -1 17.20 1.68 0 9 1 16.61 1.63 0 9 -1 17.76 1.75 0 9 2 5.63 0.96 0 9 -2 6.80 1.11 0 -9 2 6.52 0.79 0 9 -2 8.84 1.25 0 9 -2 7.03 1.05 0 9 2 9.99 1.19 0 9 2 6.10 1.00 0 9 -2 7.02 1.10 0 9 -3 46.86 2.84 0 9 3 46.26 2.74 0 9 -3 45.81 2.78 0 -9 3 46.96 2.51 0 9 -3 50.95 3.18 0 9 -3 41.71 2.89 0 9 3 47.72 2.70 0 9 -4 24.59 1.99 0 9 4 19.33 1.71 0 9 -4 18.68 1.77 0 9 4 21.71 1.75 0 9 -4 21.56 2.06 0 -9 4 21.43 1.76 0 9 -4 25.15 2.23 0 9 -5 5.17 1.08 0 9 -5 7.18 1.21 0 9 -5 4.40 0.88 0 9 -5 6.16 1.07 0 -9 5 5.41 0.97 0 9 -6 3.38 0.78 0 9 -6 5.53 1.15 0 -9 6 2.67 0.85 0 9 -6 3.10 0.92 0 9 -6 3.54 0.86 0 9 -7 4.32 1.08 0 9 7 4.16 0.74 0 9 -7 3.38 0.85 0 9 -7 2.71 0.75 0 9 7 3.97 0.85 0 -9 7 2.94 0.80 0 -9 7 4.38 1.03 0 9 -7 3.29 0.97 0 9 -8 6.20 1.28 0 9 -8 8.31 1.23 0 9 8 5.66 0.85 0 -9 8 7.25 1.22 0 9 8 6.19 1.07 0 9 -8 7.52 1.15 0 9 -8 6.63 1.39 0 -9 8 6.72 1.30 0 9 9 2.02 0.76 0 9 -9 0.47 0.58 0 -9 9 0.67 0.53 0 9 -9 1.31 0.56 0 9 -9 0.93 0.61 0 -9 9 0.63 0.66 0 9 10 22.25 2.13 0 9 -10 23.52 2.60 0 9 -10 23.64 2.61 0 -9 10 22.61 2.47 0 -9 10 24.49 2.29 0 9 -10 17.62 1.70 0 -9 10 19.27 1.97 0 9 -11 4.89 1.32 0 -9 11 3.58 1.06 0 -9 11 4.28 1.20 0 9 -11 5.36 1.34 0 -9 11 5.35 1.16 0 9 11 5.08 1.12 0 9 -12 1.57 0.83 0 -9 12 1.57 0.88 0 9 12 1.27 0.75 0 -9 12 1.24 0.83 0 9 -12 2.06 0.93 0 -9 12 0.99 0.73 0 -9 13 13.51 2.07 0 9 -13 17.94 2.35 0 9 -13 16.77 2.32 0 -9 13 16.36 2.06 0 -9 13 19.52 1.99 0 9 -14 22.50 2.56 0 -9 14 21.66 2.11 0 9 -14 18.31 2.38 0 -9 14 23.20 2.38 0 -9 15 8.79 1.54 0 9 -15 9.66 1.62 0 9 -15 6.90 1.45 0 9 -16 2.62 0.90 0 9 -16 1.04 0.62 0 9 -17 7.93 1.31 0 9 -17 8.61 1.39 0 9 -18 15.13 1.61 0 9 -18 12.70 1.53 0 9 -19 4.01 0.76 0 -9 19 4.78 0.83 0 10 0 632.76 18.76 0 10 -1 306.69 10.35 0 10 1 279.26 9.76 0 10 -1 283.27 10.07 0 10 1 282.84 10.01 0 10 1 299.51 9.76 0 10 -1 283.90 9.92 0 10 1 292.26 9.83 0 10 -1 270.59 9.61 0 10 -2 251.58 9.09 0 10 2 240.69 8.52 0 10 -2 235.66 8.58 0 10 2 227.08 8.67 0 10 -2 240.50 8.83 0 10 2 237.59 8.36 0 10 2 245.50 8.53 0 10 -2 250.52 8.91 0 10 -2 222.68 8.39 0 10 -3 53.61 3.50 0 10 3 52.93 3.08 0 10 -3 57.48 3.36 0 10 3 57.38 3.23 0 10 -3 57.07 3.31 0 10 3 51.98 3.31 0 10 -3 51.81 3.34 0 10 -3 50.67 3.34 0 10 4 176.55 6.47 0 10 -4 177.68 7.32 0 10 -4 178.37 7.12 0 10 4 182.44 7.01 0 10 -4 169.00 6.76 0 -10 4 168.58 6.34 0 10 -4 168.06 7.26 0 10 5 75.03 3.71 0 10 -5 75.86 4.45 0 10 -5 79.46 4.26 0 10 5 77.75 4.08 0 10 -5 78.63 4.08 0 -10 5 88.61 4.16 0 10 -5 79.17 4.55 0 10 -6 508.15 15.89 0 10 6 459.93 14.05 0 10 -6 488.53 15.64 0 10 6 460.20 14.52 0 10 -6 486.56 15.03 0 10 -6 461.86 14.65 0 -10 6 465.71 14.86 0 -10 6 454.37 14.55 0 10 6 478.11 14.33 0 10 -7 68.85 4.38 0 10 -7 71.89 3.78 0 -10 7 69.74 3.82 0 10 7 60.98 3.22 0 10 -7 69.85 4.32 0 10 7 60.57 3.47 0 10 -7 62.43 3.73 0 -10 7 67.50 3.99 0 10 -8 43.14 2.81 0 -10 8 40.04 3.15 0 10 8 35.41 2.30 0 10 8 42.14 2.84 0 10 -8 38.67 3.34 0 10 -8 41.90 3.41 0 10 -8 43.09 2.93 0 -10 8 41.96 2.99 0 10 9 44.55 3.03 0 10 -9 43.14 3.63 0 10 -9 41.12 3.50 0 10 -9 43.75 2.81 0 -10 9 40.69 3.28 0 -10 9 46.58 3.22 0 10 -9 45.22 2.96 0 10 10 316.38 10.75 0 10 -10 304.93 11.90 0 10 -10 299.50 11.86 0 -10 10 298.93 11.45 0 -10 10 295.64 10.46 0 -10 10 302.49 10.86 0 10 -10 310.21 10.11 0 10 -11 13.79 2.08 0 -10 11 10.17 1.53 0 10 -11 9.22 1.78 0 -10 11 11.74 1.84 0 10 11 12.06 1.66 0 -10 11 12.13 1.78 0 10 -12 98.10 5.74 0 -10 12 88.57 5.03 0 10 -12 94.07 5.68 0 10 12 109.96 5.20 0 -10 12 101.18 4.90 0 10 -13 7.79 1.66 0 -10 13 6.60 1.21 0 10 -13 6.38 1.42 0 -10 13 4.42 1.13 0 -10 14 83.99 4.65 0 -10 14 90.13 4.39 0 10 -14 75.51 4.87 0 10 -14 83.06 4.97 0 10 -15 29.08 2.80 0 10 -15 25.14 2.53 0 10 -16 124.46 5.89 0 10 -16 133.17 5.96 0 10 -17 12.46 1.51 0 10 -17 12.16 1.48 0 10 -18 23.27 1.79 0 11 0 0.32 0.43 0 11 -1 4.59 1.10 0 11 1 4.75 1.09 0 11 -1 4.48 0.98 0 11 1 6.32 1.10 0 11 1 5.48 1.06 0 11 -2 2.78 0.88 0 11 2 3.63 1.05 0 11 -2 2.57 0.89 0 11 -2 4.27 1.05 0 11 2 4.20 0.91 0 11 -2 3.54 0.93 0 11 -3 10.10 1.53 0 11 3 11.93 1.60 0 11 3 10.48 1.36 0 11 -3 11.57 1.66 0 11 -3 14.37 1.82 0 11 3 9.77 1.35 0 11 -3 12.78 1.59 0 11 -4 5.22 1.14 0 11 4 4.08 0.87 0 11 -4 4.22 1.05 0 11 4 5.38 1.11 0 11 -4 5.39 1.25 0 11 -4 3.64 0.95 0 11 -5 2.04 0.82 0 11 -5 1.32 0.68 0 11 5 1.67 0.73 0 11 5 0.80 0.52 0 11 -5 0.73 0.64 0 11 -5 0.87 0.72 0 11 -6 2.82 0.93 0 -11 6 4.81 1.01 0 11 6 4.28 1.00 0 11 -6 3.62 1.03 0 11 6 4.45 0.86 0 11 -6 3.46 0.94 0 11 -6 4.08 1.14 0 11 -7 7.62 1.53 0 11 -7 8.90 1.39 0 -11 7 8.35 1.29 0 11 7 13.37 1.51 0 11 -7 8.93 1.61 0 11 7 9.14 1.18 0 11 7 11.30 1.40 0 11 -7 10.10 1.48 0 11 -8 130.35 6.73 0 11 -8 126.48 5.66 0 -11 8 127.78 5.84 0 11 -8 138.47 6.01 0 11 8 132.90 5.67 0 11 -8 145.71 6.99 0 11 8 126.60 5.12 0 11 9 1.72 0.81 0 -11 9 2.47 0.89 0 11 9 2.63 0.65 0 11 -9 2.56 0.81 0 11 -9 1.28 0.85 0 -11 9 3.88 1.01 0 11 -9 2.77 1.13 0 11 -9 3.15 0.83 0 11 -10 6.32 1.05 0 11 -10 9.04 1.75 0 -11 10 5.81 1.17 0 -11 10 6.91 1.27 0 11 -10 5.18 1.38 0 11 10 4.65 1.13 0 11 -11 2.80 1.15 0 -11 11 3.20 0.89 0 11 -11 4.16 1.23 0 11 11 5.52 1.14 0 -11 11 4.80 1.11 0 -11 12 100.00 5.08 0 11 -12 91.42 5.54 0 11 -12 94.60 5.53 0 -11 12 100.26 4.77 0 11 -13 6.54 1.43 0 11 -13 4.31 1.15 0 -11 13 6.85 1.17 0 -11 13 5.35 1.15 0 -11 14 15.45 1.65 0 11 -14 17.51 2.05 0 11 -14 15.07 2.00 0 11 -15 1.94 0.73 0 11 -15 0.72 0.58 0 11 -16 3.08 0.84 0 11 -16 4.37 0.95 0 11 -17 0.11 0.32 0 11 -19 1.29 0.36 0 12 0 239.59 8.97 0 12 1 3.27 1.00 0 12 -1 3.21 1.02 0 12 1 4.24 1.04 0 12 -1 4.25 1.13 0 12 1 4.63 1.16 0 12 -2 318.70 11.32 0 12 -2 324.13 11.44 0 12 2 323.42 10.97 0 12 2 333.26 11.72 0 12 -2 337.26 11.85 0 12 -3 54.48 3.56 0 12 -3 51.84 3.57 0 12 3 54.51 3.30 0 12 3 60.70 3.84 0 12 -3 54.38 3.74 0 12 -3 53.84 3.84 0 12 -4 794.91 24.00 0 12 -4 800.15 24.37 0 12 4 818.09 23.48 0 12 -4 804.07 24.40 0 12 4 828.42 24.27 0 12 -4 864.38 25.00 0 12 -5 303.22 10.72 0 12 -5 286.52 11.04 0 12 5 293.83 10.09 0 12 -5 324.54 11.23 0 12 5 311.07 10.81 0 12 -5 300.89 11.44 0 12 -6 70.66 4.10 0 12 6 76.62 4.19 0 12 -6 74.20 4.39 0 12 -6 75.14 4.62 0 12 6 72.77 3.73 0 12 -6 68.88 4.61 0 12 -7 239.41 8.64 0 -12 7 215.03 8.24 0 12 -7 229.81 8.76 0 12 7 226.40 8.34 0 12 -7 220.93 9.48 0 12 7 223.23 7.82 0 12 -7 213.99 9.21 0 12 -8 1071.52 31.69 0 12 -8 1025.74 31.40 0 12 8 1044.92 29.62 0 12 -8 1082.42 30.14 0 -12 8 1074.71 30.12 0 12 8 1051.19 29.13 0 12 -8 1119.33 30.54 0 12 -9 198.48 8.83 0 12 -9 206.16 7.63 0 12 9 201.89 7.48 0 -12 9 205.72 7.88 0 -12 9 201.08 7.67 0 12 -9 184.73 8.59 0 12 9 191.56 6.77 0 12 -10 53.60 4.08 0 -12 10 55.70 3.54 0 12 -10 62.62 4.39 0 -12 10 57.56 3.42 0 12 10 54.96 3.31 0 -12 11 56.97 3.32 0 12 -11 59.99 4.21 0 -12 11 52.02 3.42 0 12 -11 55.37 4.03 0 -12 12 302.17 9.82 0 12 -12 260.34 10.65 0 -12 12 293.33 10.15 0 12 -12 274.50 10.77 0 -12 13 31.54 2.28 0 12 -13 26.23 2.58 0 12 -13 30.53 2.71 0 12 -14 55.15 3.52 0 12 -14 54.03 3.46 0 12 -15 5.71 1.03 0 12 -15 7.50 1.18 0 12 -16 33.62 2.21 0 12 -18 38.61 1.95 0 13 0 0.18 0.75 0 13 -1 12.20 1.67 0 13 1 10.03 1.65 0 13 1 9.85 1.49 0 13 -2 6.25 1.29 0 13 -2 5.83 1.26 0 13 2 3.44 0.92 0 13 -2 4.48 1.18 0 13 2 6.09 1.39 0 13 -3 1.90 0.78 0 13 -3 1.54 0.67 0 13 -3 0.21 0.60 0 13 3 1.43 0.66 0 13 3 2.45 0.87 0 13 -4 3.95 1.05 0 13 4 5.28 1.22 0 13 4 6.72 1.12 0 13 -4 6.45 1.35 0 13 -4 8.17 1.41 0 13 -5 5.93 1.26 0 13 5 6.78 1.12 0 13 -5 5.08 1.30 0 13 5 4.61 1.18 0 13 -5 5.21 1.31 0 13 -5 7.68 1.43 0 13 -6 16.36 2.21 0 13 -6 20.46 2.25 0 13 -6 17.66 2.00 0 13 -6 15.46 2.03 0 13 6 16.11 1.64 0 13 6 13.19 1.72 0 13 -7 1.11 0.80 0 13 -7 1.31 0.75 0 13 7 2.58 0.73 0 13 -7 1.46 0.88 0 -13 8 10.25 1.39 0 13 8 10.54 1.23 0 13 -8 12.15 1.85 0 -13 8 8.05 1.33 0 13 -8 7.79 1.54 0 13 -9 28.37 2.79 0 -13 9 28.90 2.34 0 -13 9 27.14 2.28 0 13 -9 31.99 3.00 0 13 -10 85.18 4.99 0 -13 10 84.65 4.22 0 13 -10 90.72 5.23 0 -13 10 96.20 4.53 0 -13 11 11.69 1.38 0 13 -11 10.78 1.67 0 13 -11 13.93 1.85 0 -13 12 0.60 0.48 0 13 -12 0.19 0.50 0 13 -12 0.55 0.58 0 -13 13 14.73 1.42 0 13 -13 13.16 1.66 0 13 -13 14.43 1.66 0 13 -14 23.68 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2.95 0.75 0 15 -6 2.02 0.72 0 -15 6 3.23 0.76 0 15 6 2.20 0.63 0 15 -7 3.27 0.90 0 -15 7 2.14 0.63 0 15 -8 1.39 0.66 0 -15 8 1.15 0.51 0 -15 9 4.58 0.77 0 15 -10 16.70 1.48 0 15 -11 1.45 0.48 0 15 -12 16.41 1.16 0 16 0 143.48 5.90 0 16 1 46.90 2.87 0 16 -1 43.46 2.90 0 16 2 25.58 2.03 0 16 -3 81.82 4.26 0 16 3 90.62 4.08 0 16 4 82.89 3.78 0 16 -4 83.63 4.22 0 16 -5 12.09 1.47 0 16 -6 103.80 4.69 0 16 -7 63.48 3.32 0 16 -8 39.29 2.40 0 16 -9 35.26 2.11 0 16 -10 74.04 3.09 0 16 -11 0.93 0.33 0 17 0 5.38 0.96 0 17 -1 21.59 1.79 0 17 1 19.37 1.62 0 17 2 13.03 1.30 0 17 3 7.33 0.96 0 17 -4 5.99 0.99 0 17 -5 0.78 0.53 0 17 -6 0.61 0.42 0 17 -7 0.45 0.40 0 17 -8 0.30 0.32 0 17 -9 2.07 0.44 0 18 0 0.88 0.40 0 18 1 9.00 0.95 0 18 -1 8.33 0.95 0 18 -4 5.07 0.75 0 18 -5 7.71 0.85 0 18 -6 29.08 1.60 0 18 -7 0.69 0.28 0 19 -1 1.13 0.30 0 19 -2 0.79 0.28 -1 0 22 24.10 2.03 -1 0 21 0.62 0.58 -1 0 21 0.52 0.53 -1 0 20 92.48 4.91 -1 0 20 94.46 5.10 -1 0 19 -0.21 0.85 -1 0 19 -0.22 0.66 -1 0 18 111.17 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0 4 228.14 6.90 1 0 5 2.27 0.58 1 0 6 1325.40 35.20 1 0 7 2.03 0.66 1 0 7 2.44 0.69 1 0 8 602.64 17.55 1 0 8 607.15 17.33 1 0 9 0.78 0.54 1 0 9 0.52 0.41 1 0 9 0.85 0.58 1 0 10 328.16 10.86 1 0 10 341.38 10.32 1 0 10 322.14 10.99 1 0 11 1.05 0.56 1 0 11 1.68 0.79 1 0 11 0.58 0.53 1 0 12 150.30 5.73 1 0 12 134.34 5.96 1 0 12 136.80 6.41 1 0 12 129.72 6.23 1 0 12 138.67 6.29 1 0 13 1.04 0.91 1 0 13 1.17 0.64 1 0 13 2.38 0.92 1 0 13 1.42 0.80 1 0 13 0.42 0.70 1 0 13 0.22 0.72 1 0 14 18.54 2.30 1 0 14 19.07 1.96 1 0 14 19.02 2.36 1 0 14 17.39 2.01 1 0 14 19.83 2.36 1 0 14 17.45 2.25 1 0 15 9.44 1.92 1 0 15 3.12 0.99 1 0 15 7.34 1.48 1 0 15 6.39 1.89 1 0 15 3.27 1.30 1 0 15 12.83 2.09 1 0 16 24.67 2.79 1 0 16 21.29 2.68 1 0 16 22.90 2.71 1 0 16 21.02 2.20 1 0 16 23.52 2.42 1 0 16 24.53 2.40 1 0 17 0.69 0.65 1 0 17 1.06 0.80 1 0 17 1.26 0.87 1 0 17 0.53 0.84 1 0 17 0.53 0.93 1 0 18 8.41 1.45 1 0 18 7.26 1.51 1 0 18 10.23 1.86 1 0 19 0.38 0.57 1 0 19 0.88 0.76 1 0 19 1.16 0.84 1 0 20 35.46 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1.87 1 10 -15 15.37 1.86 1 10 -14 37.01 3.37 1 10 -14 44.43 3.37 -1 -10 14 49.14 3.41 -1 10 14 42.35 3.12 1 10 -13 11.55 1.97 1 10 -13 11.74 1.81 -1 -10 13 12.92 1.54 -1 -10 13 14.30 1.90 -1 10 13 13.47 1.81 1 10 -12 95.46 5.95 1 10 -12 108.10 5.79 -1 -10 12 108.67 4.94 -1 -10 12 114.13 5.58 -1 10 12 102.65 5.27 -1 -10 11 3.08 0.85 1 10 -11 3.72 1.24 -1 10 11 4.37 1.15 1 10 -11 5.79 1.49 -1 -10 11 4.23 1.11 1 10 -10 138.52 7.26 -1 10 10 146.78 5.55 -1 -10 10 142.05 5.87 1 10 -10 132.61 6.73 -1 -10 10 136.94 6.35 -1 10 10 147.38 6.36 1 10 -9 46.69 3.50 1 10 -9 42.75 2.94 -1 10 9 48.14 2.73 -1 -10 9 38.28 2.65 -1 10 9 43.04 3.04 -1 -10 9 42.45 3.10 1 10 -9 47.63 3.86 1 10 -8 23.26 2.41 -1 10 8 24.89 1.94 1 10 -8 22.66 2.57 -1 10 8 22.67 2.11 -1 -10 8 21.69 1.91 1 10 -8 22.09 2.14 -1 -10 8 23.74 2.23 -1 10 7 25.20 2.14 -1 10 7 26.72 2.08 1 10 -7 26.73 2.71 -1 10 7 26.04 2.02 1 10 -7 25.56 2.31 1 10 -7 22.97 2.40 1 10 -7 27.88 2.23 -1 -10 7 21.20 2.12 -1 -10 6 133.46 5.70 1 10 -6 133.62 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2.08 1 -10 10 19.74 2.45 -1 10 -10 18.30 2.30 1 -10 10 22.14 2.21 -1 10 -11 11.12 1.85 1 -10 11 8.56 1.60 -1 10 -11 12.34 2.10 1 -10 11 13.67 1.83 1 -10 11 12.95 1.71 -1 10 -12 33.64 3.28 1 -10 12 31.13 3.07 -1 10 -12 25.39 2.73 1 -10 12 33.61 2.67 -1 10 -13 6.14 1.33 1 -10 13 4.65 1.09 -1 10 -14 13.03 1.78 -1 10 -14 12.95 1.92 1 -10 14 14.22 1.66 -1 10 -15 2.41 0.90 -1 10 -16 17.18 1.91 -1 10 -17 26.02 2.12 -1 10 -18 4.44 0.79 -1 10 -19 0.06 0.25 1 11 -18 10.28 1.17 1 11 -17 11.87 1.44 1 11 -16 2.26 0.78 -1 -11 16 3.59 0.92 1 11 -16 2.97 0.71 1 11 -15 2.04 0.89 -1 -11 15 3.87 1.04 1 11 -15 3.19 0.87 1 11 -14 12.18 1.82 -1 -11 14 12.96 1.71 1 11 -14 10.75 1.57 -1 -11 13 8.14 1.25 1 11 -13 7.40 1.47 -1 11 13 8.33 1.50 -1 -11 13 7.91 1.43 1 11 -13 6.59 1.58 -1 -11 12 84.09 4.56 -1 -11 12 76.71 3.90 -1 11 12 75.30 4.25 1 11 -12 74.30 4.62 -1 -11 11 48.56 3.42 -1 11 11 57.24 3.61 -1 -11 11 55.15 3.20 1 11 -11 50.39 3.80 1 11 -11 48.79 4.09 -1 -11 10 10.57 1.59 -1 -11 10 12.30 1.47 -1 11 10 13.44 1.42 1 11 -10 11.66 1.49 -1 11 10 10.48 1.55 1 11 -10 8.22 1.72 1 11 -10 8.34 1.60 -1 -11 9 105.48 4.77 -1 11 9 108.86 4.60 1 11 -9 97.38 4.87 1 11 -9 103.46 6.07 1 11 -9 103.54 5.66 -1 11 9 102.15 5.06 -1 -11 9 103.31 5.22 -1 -11 8 318.97 10.57 -1 11 8 333.93 11.09 -1 11 8 330.42 10.53 1 11 -8 324.01 12.39 -1 -11 8 307.35 11.07 1 11 -8 302.42 11.77 1 11 -8 336.59 11.31 -1 11 7 64.04 3.73 1 11 -7 68.40 4.53 1 11 -7 66.62 4.27 -1 -11 7 60.46 3.72 -1 11 7 65.34 3.48 1 11 -7 66.45 3.97 1 11 -6 7.29 1.43 -1 -11 6 6.36 1.21 1 11 -6 4.20 1.06 -1 11 6 7.30 1.21 -1 11 6 5.02 0.99 1 11 -6 8.25 1.43 -1 11 6 6.62 1.09 -1 11 5 23.93 2.06 1 11 -5 16.64 2.05 1 11 -5 27.61 2.73 1 11 -5 25.51 2.53 -1 -11 5 21.32 1.98 -1 11 5 24.98 2.20 -1 11 5 21.86 1.94 -1 11 5 21.46 2.15 -1 11 5 22.77 2.03 -1 11 4 248.46 8.93 -1 11 4 270.00 9.20 1 11 -4 272.47 9.53 1 11 -4 256.91 9.96 1 11 -4 269.00 9.94 -1 11 4 243.32 9.01 -1 11 4 269.03 9.62 -1 11 4 272.37 9.47 1 11 -3 5.28 1.46 -1 11 3 6.41 1.14 -1 11 3 2.78 0.89 -1 11 3 6.82 1.13 -1 11 3 5.24 1.07 -1 11 3 8.12 1.39 1 11 -2 175.05 7.39 -1 11 2 172.77 6.83 -1 11 2 167.86 7.09 -1 11 2 173.96 6.93 -1 11 1 18.07 1.86 -1 11 1 19.03 2.07 1 11 -1 14.20 1.86 -1 11 1 17.21 1.84 -1 11 1 16.79 1.91 -1 11 0 84.57 4.34 1 11 0 78.12 4.41 -1 11 0 80.73 4.11 -1 11 -1 24.90 2.41 -1 11 -1 19.01 2.43 1 11 1 21.71 2.18 -1 11 -1 25.17 2.26 -1 11 -1 23.43 2.23 -1 11 -2 140.58 6.00 -1 11 -2 145.76 6.33 -1 11 -2 139.24 6.18 -1 11 -2 152.02 6.55 -1 11 -3 32.67 2.63 -1 11 -3 32.25 2.73 -1 11 -3 31.52 2.64 -1 11 -3 28.72 2.55 -1 11 -4 117.33 5.52 -1 11 -4 133.36 5.97 1 11 4 108.52 4.87 1 11 4 113.03 5.55 -1 11 -4 126.94 5.65 -1 11 -4 119.29 5.60 -1 11 -5 10.81 1.56 1 11 5 11.76 1.61 1 11 5 13.72 1.44 -1 11 -5 15.15 1.80 -1 11 -5 16.62 1.96 -1 11 -5 14.44 1.77 -1 11 -6 55.79 4.01 1 11 6 48.13 2.76 1 11 6 49.06 3.23 -1 11 -6 48.31 3.46 -1 11 -6 51.49 3.34 -1 11 -6 49.91 3.32 -1 11 -7 14.93 1.85 1 11 7 16.60 1.76 1 -11 7 13.69 1.90 1 -11 7 19.64 2.06 -1 11 -8 201.69 7.80 -1 11 -8 212.34 8.62 1 -11 8 189.29 8.30 1 -11 8 205.81 7.95 -1 11 -8 195.85 9.07 -1 11 -9 13.13 1.94 -1 11 -9 14.61 1.66 -1 11 -9 11.97 2.01 1 -11 9 14.63 2.01 1 -11 9 12.25 1.68 -1 11 -10 35.15 3.37 -1 11 -10 32.14 2.99 1 -11 10 35.07 2.80 -1 11 -10 29.17 2.31 1 -11 10 31.60 2.62 1 -11 10 31.88 2.99 1 -11 11 5.78 1.24 -1 11 -11 6.35 1.53 -1 11 -11 6.97 1.43 -1 11 -11 4.27 0.86 1 -11 12 160.61 6.59 -1 11 -12 151.91 7.45 -1 11 -12 148.75 6.96 1 -11 13 6.58 1.18 -1 11 -13 6.36 1.37 -1 11 -13 5.65 1.18 1 -11 14 45.66 2.87 -1 11 -14 39.11 3.15 -1 11 -15 1.72 0.73 -1 11 -16 30.77 2.33 -1 11 -17 0.22 0.38 -1 11 -18 41.90 2.15 1 12 -17 5.23 0.82 1 12 -16 26.11 2.10 1 12 -15 3.58 0.79 1 12 -15 3.33 0.86 -1 -12 15 5.28 1.03 1 12 -14 65.79 3.71 1 12 -14 62.49 4.01 -1 -12 14 66.66 3.71 -1 -12 13 9.50 1.47 1 12 -13 8.50 1.39 -1 12 13 8.52 1.36 1 12 -13 12.28 1.82 -1 -12 12 206.77 7.55 1 12 -12 221.44 8.77 -1 12 12 239.70 8.35 -1 -12 12 217.69 8.38 1 12 -12 204.10 9.14 -1 -12 11 20.94 1.84 1 12 -11 19.96 2.57 -1 12 11 21.57 2.11 1 12 -11 16.39 2.12 -1 -12 11 23.78 2.27 -1 -12 10 4.77 1.08 -1 12 10 4.30 0.82 1 12 -10 5.50 1.06 -1 -12 10 5.71 1.02 1 12 -10 4.95 1.18 -1 12 10 4.77 1.08 1 12 -10 4.26 1.34 1 12 -9 16.62 2.34 -1 12 9 21.55 2.07 1 12 -9 17.82 2.21 1 12 -9 18.95 1.99 -1 12 9 20.21 1.78 -1 -12 9 20.68 1.87 -1 -12 9 21.08 2.13 -1 12 8 280.77 9.23 1 12 -8 274.79 11.00 1 12 -8 275.63 10.60 1 12 -8 284.11 10.00 -1 -12 8 268.42 9.70 -1 -12 8 253.90 9.07 -1 12 8 258.81 9.49 -1 12 7 27.88 2.23 1 12 -7 29.76 2.98 1 12 -7 33.65 3.02 1 12 -7 35.03 2.89 -1 -12 7 30.12 2.49 -1 -12 7 31.31 2.29 -1 12 7 34.77 2.60 -1 12 6 12.45 1.53 1 12 -6 15.70 2.08 1 12 -6 18.96 2.19 -1 12 6 16.53 1.71 -1 -12 6 14.81 1.67 1 12 -6 16.94 2.25 -1 12 5 20.65 1.97 -1 12 5 15.54 1.68 1 12 -5 18.67 2.19 1 12 -5 21.66 2.39 1 12 -5 17.81 2.14 -1 12 4 50.90 3.05 1 12 -4 51.17 3.69 -1 12 4 53.83 3.31 -1 12 4 46.44 3.39 1 12 -4 55.40 3.77 -1 12 4 50.97 3.38 -1 12 4 47.79 3.12 1 12 -3 17.58 2.09 -1 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12 116.81 5.96 2 -5 12 113.84 5.64 -2 5 -12 112.05 5.84 -2 -5 -12 112.85 5.86 2 -5 12 110.42 8.39 2 -5 13 0.26 0.69 2 -5 13 0.50 0.67 2 5 13 0.55 0.52 2 5 13 -0.43 0.89 2 -5 13 -0.66 0.99 2 5 13 -0.23 0.68 2 5 13 -0.22 0.87 2 -5 13 -0.67 0.94 -2 5 -13 0.23 0.51 -2 -5 -13 -0.23 0.57 2 -5 13 -0.40 0.77 2 -5 14 141.25 6.66 2 -5 14 143.27 6.31 2 5 14 142.04 6.45 2 -5 14 163.99 7.36 2 5 14 143.76 6.96 2 5 14 157.47 7.24 2 -5 14 145.39 7.02 2 5 14 142.01 6.91 -2 -5 -14 139.51 7.01 -2 5 -14 148.81 7.14 2 -5 14 148.97 7.43 2 -5 15 26.83 2.90 2 -5 15 35.16 3.12 2 5 15 29.24 2.83 -2 -5 -15 30.72 2.94 -2 5 -15 24.59 2.67 2 -5 15 29.76 2.94 2 5 15 20.92 2.52 2 -5 15 28.56 2.65 2 5 15 32.28 3.02 2 -5 16 89.14 5.12 2 5 16 96.41 5.25 2 -5 17 1.22 0.79 2 5 17 1.58 0.77 2 -5 18 31.28 2.61 2 -5 19 0.40 0.48 -2 5 -19 0.79 0.61 2 -5 20 8.73 1.05 -2 5 -20 8.81 1.17 -2 -6 22 2.04 0.49 -2 -6 21 11.53 1.29 -2 -6 21 7.95 1.07 -2 -6 21 7.34 0.99 2 6 -21 8.52 1.28 -2 -6 20 1.36 0.64 -2 -6 20 1.26 0.58 -2 -6 20 0.54 0.47 2 6 -20 0.53 0.59 -2 -6 19 4.88 1.05 -2 -6 19 4.76 1.00 -2 -6 19 4.13 0.97 2 6 -19 4.56 1.15 -2 -6 18 30.17 2.54 -2 -6 18 24.92 2.33 -2 -6 18 28.12 2.52 -2 -6 17 30.47 2.64 -2 -6 17 28.47 2.55 -2 6 16 7.50 1.43 -2 -6 16 7.15 1.36 2 6 -16 7.77 1.47 -2 6 16 7.92 1.36 2 6 -15 10.84 1.69 2 -6 -15 10.52 1.82 -2 6 15 9.93 1.63 -2 -6 15 8.08 1.39 -2 6 15 7.75 1.35 -2 -6 15 7.87 1.43 -2 6 15 10.29 1.49 -2 6 14 76.99 4.96 2 6 -14 74.75 4.27 2 6 -14 74.32 4.54 2 -6 -14 73.51 4.73 -2 6 14 69.16 4.18 -2 -6 14 73.18 4.27 -2 6 14 81.99 4.55 -2 -6 14 83.07 4.61 2 6 -13 8.20 1.34 2 -6 -13 8.15 1.50 2 6 -13 7.88 1.42 -2 -6 13 10.96 1.63 -2 6 13 8.33 1.43 -2 6 13 6.74 1.46 -2 6 13 9.37 1.42 -2 -6 13 7.57 5.16 -2 -6 12 4.47 0.96 -2 6 12 2.78 0.81 -2 6 12 4.35 1.01 2 -6 -12 1.94 0.78 2 6 -12 3.17 0.86 2 6 -12 3.41 0.91 -2 6 12 3.15 1.06 -2 6 12 4.52 1.06 -2 6 11 6.49 1.08 -2 6 11 5.44 1.06 -2 -6 11 5.20 0.88 2 6 -11 3.20 0.87 -2 6 11 5.01 1.07 2 6 -11 5.75 1.16 2 -6 -11 4.70 1.08 -2 6 11 5.55 1.23 -2 -6 10 51.08 2.71 -2 6 10 45.41 3.30 2 6 -10 53.66 3.19 2 -6 -10 49.02 3.12 2 6 -10 52.80 3.20 -2 6 10 50.55 3.16 -2 -6 9 216.61 7.89 -2 -6 9 208.06 7.01 -2 -6 9 212.18 7.83 2 6 -9 210.49 7.65 2 -6 -9 215.26 7.69 -2 6 9 206.54 8.04 2 6 -9 215.04 7.75 -2 -6 8 11.17 1.08 2 -6 -8 12.21 1.31 2 6 -8 11.48 1.30 2 6 -8 13.22 1.43 -2 -6 8 12.98 1.45 -2 -6 7 113.17 4.82 2 -6 -7 116.79 4.62 2 6 -7 121.20 4.68 2 6 -7 115.71 4.78 2 6 -7 119.13 5.34 2 6 -6 26.81 2.16 2 -6 -6 27.39 1.76 2 6 -6 25.13 1.71 -2 -6 6 28.59 1.97 2 6 -5 87.90 3.48 2 -6 -5 85.49 3.43 2 6 -5 84.71 4.09 -2 -6 5 85.75 3.77 2 6 -4 92.13 3.42 2 -6 -4 89.22 3.38 -2 -6 4 84.08 3.69 2 6 -4 90.70 4.14 -2 6 3 18.80 1.15 -2 -6 3 18.46 1.16 2 -6 -3 18.78 1.20 2 6 -3 19.73 1.25 -2 -6 2 383.97 10.72 -2 6 2 376.95 10.70 2 6 -2 387.96 10.77 2 -6 -2 397.92 10.77 -2 6 1 535.66 14.65 -2 -6 1 539.40 14.67 2 6 -1 535.71 14.64 2 -6 -1 560.44 14.66 2 6 0 141.56 4.55 2 -6 0 150.20 4.57 2 6 1 150.49 4.84 2 -6 1 152.83 4.85 2 6 2 371.86 10.28 2 -6 2 356.01 10.25 2 6 2 339.64 10.77 -2 6 -2 356.54 10.89 -2 6 -3 51.81 2.93 -2 6 -3 51.26 2.70 2 6 3 53.52 2.42 2 -6 3 53.39 2.44 -2 6 -4 31.83 2.06 2 -6 4 32.73 1.91 2 6 4 30.96 1.86 -2 6 -4 31.82 1.91 -2 -6 -4 32.56 1.92 -2 6 -5 9.47 1.10 2 6 5 10.28 1.10 2 -6 5 10.21 1.12 -2 6 -5 11.71 1.17 -2 -6 -5 10.46 1.14 2 6 6 17.17 1.54 2 -6 6 18.57 1.59 2 -6 6 15.53 1.76 -2 -6 -6 19.34 1.62 -2 6 -6 20.79 1.69 -2 6 -6 18.50 1.54 2 -6 7 430.42 14.02 -2 6 -7 411.40 12.58 -2 6 -7 427.51 13.16 -2 -6 -7 430.46 13.15 2 -6 8 37.59 3.00 2 -6 8 36.49 2.62 2 6 8 37.06 2.67 -2 -6 -8 36.52 2.62 -2 6 -8 36.62 2.61 -2 -6 -9 133.25 6.01 -2 6 -9 136.38 6.01 2 -6 9 145.43 6.75 2 6 9 144.97 6.17 2 -6 10 130.33 6.51 -2 -6 -10 123.81 5.82 -2 6 -10 123.08 5.80 2 6 10 117.92 5.54 2 -6 10 123.71 5.70 2 6 10 124.80 5.85 2 -6 11 18.11 2.33 2 6 11 20.18 2.21 2 6 11 23.31 2.27 2 -6 11 20.24 2.18 -2 -6 -11 25.67 2.45 -2 6 -11 20.24 2.17 2 -6 12 1.82 0.94 2 -6 12 -0.17 0.65 2 6 12 2.15 0.85 2 -6 12 0.81 0.73 2 6 12 1.68 0.87 2 6 12 0.20 0.68 2 -6 12 1.41 0.84 -2 6 -12 0.84 0.66 -2 -6 -12 0.22 0.53 2 -6 13 12.02 1.87 2 6 13 11.02 1.78 -2 -6 -13 12.20 1.81 -2 6 -13 13.57 1.92 2 6 13 14.02 1.97 2 -6 13 16.38 2.10 2 6 13 11.95 1.82 2 -6 13 15.56 1.80 2 -6 14 27.74 2.69 2 6 14 24.30 2.49 2 6 14 24.06 2.53 2 -6 14 18.84 2.22 2 6 14 19.24 2.20 2 -6 14 21.98 2.23 2 -6 14 25.00 2.30 -2 6 -14 20.66 2.33 2 -6 15 64.92 4.00 2 -6 15 77.47 4.61 2 6 15 73.49 4.43 2 6 15 79.07 4.67 2 -6 16 16.29 1.98 2 6 16 16.24 1.99 2 -6 16 15.17 1.74 2 -6 17 20.80 2.11 -2 6 -17 22.06 2.33 -2 6 -18 17.02 1.59 -2 6 -18 14.78 1.83 2 -6 19 12.12 1.35 -2 6 -19 10.17 1.35 -2 -7 21 2.41 0.57 -2 -7 21 2.07 0.58 2 7 -21 2.82 0.73 -2 -7 20 43.04 2.53 -2 -7 20 43.38 2.65 2 7 -20 37.46 2.78 -2 -7 20 41.97 2.65 2 7 -19 4.78 1.08 -2 -7 19 5.11 0.99 -2 -7 19 5.50 1.09 -2 -7 19 5.38 1.00 2 7 -18 36.89 3.18 -2 -7 18 40.95 2.98 -2 -7 18 42.45 2.95 -2 -7 18 42.43 2.92 -2 -7 17 9.07 1.42 -2 -7 17 9.62 1.51 2 7 -17 7.76 1.54 -2 7 16 209.19 8.36 2 7 -16 187.95 8.83 -2 -7 16 206.01 8.27 -2 -7 15 8.03 1.51 -2 7 15 6.98 1.41 -2 7 14 30.67 2.53 -2 7 14 31.29 2.77 2 7 -14 31.14 2.65 -2 7 13 4.22 1.15 -2 7 13 4.05 1.00 2 7 -13 5.91 1.15 2 7 -13 4.29 1.00 -2 7 12 127.99 5.67 2 7 -12 140.11 6.13 2 7 -12 121.38 5.77 -2 -7 11 0.97 0.51 2 7 -11 0.87 0.58 2 7 -11 0.16 0.54 2 -7 -11 0.33 0.70 -2 -7 11 0.18 0.70 -2 7 11 0.74 0.51 -2 -7 10 44.51 2.56 -2 -7 10 47.75 3.16 2 7 -10 46.20 3.57 2 7 -10 43.88 3.00 -2 7 10 42.11 2.75 2 -7 -10 43.41 2.84 2 7 -10 41.08 2.79 -2 7 9 2.44 0.64 -2 7 9 2.70 0.80 2 7 -9 2.05 0.90 -2 -7 9 1.40 0.68 2 7 -9 2.29 0.78 -2 -7 9 1.50 0.57 2 -7 -9 1.81 0.58 2 7 -9 1.82 0.57 -2 -7 8 42.65 2.78 -2 7 8 39.52 2.66 2 7 -8 37.21 2.97 2 7 -8 44.33 2.80 -2 -7 8 42.16 2.27 -2 7 8 35.33 2.20 2 -7 -8 37.12 2.36 2 7 -8 38.40 2.40 -2 -7 8 39.66 2.71 2 -7 -7 27.96 1.89 2 7 -7 31.54 2.00 2 7 -7 32.07 2.28 2 7 -7 33.01 2.64 -2 -7 7 31.26 2.27 -2 7 7 27.33 1.96 2 7 -6 121.82 5.11 2 7 -6 136.08 5.79 2 7 -6 128.53 4.64 2 -7 -6 125.47 4.61 -2 -7 6 129.56 5.16 -2 7 6 121.88 4.92 2 7 -5 11.24 1.28 -2 7 5 14.03 1.25 2 7 -5 13.18 1.07 -2 7 5 14.93 1.42 2 7 -5 11.49 1.47 -2 -7 5 12.76 1.37 -2 -7 4 251.72 7.98 2 7 -4 239.03 7.18 2 7 -4 234.74 8.05 2 7 -4 252.64 8.71 -2 7 4 234.36 8.06 -2 -7 3 17.34 1.41 2 7 -3 17.50 1.05 2 7 -3 17.18 1.51 -2 7 3 15.44 1.47 2 7 -3 17.52 1.71 2 7 -2 182.92 5.45 2 7 -2 200.98 7.07 -2 7 2 184.39 6.66 -2 -7 2 186.77 6.24 2 7 -1 31.88 2.27 -2 7 1 31.88 1.37 -2 7 0 390.38 10.68 2 7 0 399.65 12.18 -2 7 0 401.37 12.13 2 7 0 385.83 10.75 -2 7 0 415.67 12.21 2 7 1 19.38 1.66 -2 7 -1 18.47 1.62 2 7 1 18.51 1.08 -2 7 -1 17.17 1.63 2 7 2 178.49 6.40 -2 7 -2 174.77 6.62 2 7 2 170.60 5.40 -2 7 -2 177.84 6.43 -2 7 -3 5.21 0.97 2 7 3 4.40 0.60 -2 7 -3 4.87 0.89 -2 7 -4 121.91 5.39 2 -7 4 114.41 4.33 2 -7 4 128.69 5.38 2 7 4 118.93 4.36 -2 7 -4 125.99 5.00 2 -7 5 3.08 0.82 2 7 5 3.23 0.62 -2 7 -5 4.18 0.79 -2 7 -5 2.80 0.83 -2 7 -5 3.43 0.63 -2 7 -5 2.23 0.67 2 -7 6 31.41 2.59 -2 7 -6 27.86 2.12 -2 7 -6 31.03 2.59 -2 -7 -6 26.03 1.91 -2 7 -6 27.06 1.95 -2 7 -6 29.21 2.10 -2 7 -7 139.69 5.34 2 7 7 133.63 5.57 2 -7 7 125.01 5.58 -2 7 -7 135.09 5.42 -2 -7 -7 127.02 5.31 -2 7 -7 132.71 5.62 2 -7 7 141.10 6.36 2 7 8 132.10 5.63 2 -7 8 132.31 6.35 -2 -7 -8 122.43 5.37 -2 7 -8 119.58 5.34 -2 7 -8 133.02 5.76 2 -7 9 2.75 0.98 -2 7 -9 5.30 1.01 2 7 9 4.96 0.95 2 7 9 5.01 1.04 2 7 10 59.82 3.73 2 -7 10 62.78 4.32 2 7 10 57.27 3.50 -2 7 -10 58.26 3.66 2 7 10 63.63 3.63 2 7 11 42.25 3.21 2 7 11 45.91 3.32 2 -7 11 46.49 3.78 2 -7 11 40.28 3.03 2 7 11 41.33 3.00 -2 7 -11 40.26 3.07 2 7 11 37.58 2.87 2 7 12 113.94 5.77 2 -7 12 121.61 6.55 2 -7 12 120.28 5.73 2 7 12 113.60 5.53 -2 7 -12 111.58 5.69 2 7 12 112.78 5.57 2 -7 13 0.27 0.66 2 7 13 0.35 0.46 2 -7 13 -0.19 0.91 2 7 13 -0.38 0.84 2 7 13 0.41 0.55 2 7 14 103.67 5.47 -2 7 -14 101.06 5.40 2 -7 14 115.94 6.33 2 -7 14 105.04 5.39 2 -7 15 0.36 0.58 -2 7 -15 0.47 0.62 -2 7 -16 36.44 3.11 -2 7 -17 1.33 0.74 -2 7 -18 24.53 1.88 -2 7 -18 23.91 2.17 -2 7 -19 2.61 0.68 -2 7 -19 1.64 0.42 2 -7 19 2.05 0.59 -2 -8 20 2.36 0.63 -2 -8 20 1.49 0.52 2 8 -20 2.60 0.73 -2 -8 19 1.82 0.55 2 8 -19 2.56 0.84 -2 -8 19 3.56 0.79 -2 -8 19 2.92 0.76 2 8 -18 3.63 1.02 -2 -8 18 3.98 0.97 -2 -8 18 5.84 1.11 -2 -8 18 5.18 0.97 -2 -8 17 84.71 4.49 -2 -8 17 79.24 4.16 2 8 -17 73.25 4.72 2 8 -16 10.73 1.84 2 8 -15 4.76 1.31 2 8 -14 22.95 2.27 2 8 -14 24.22 2.78 2 8 -13 13.72 1.77 2 8 -13 12.00 2.06 -2 -8 13 13.61 1.93 -2 -8 12 49.68 3.59 2 8 -12 53.69 4.14 2 8 -12 60.41 3.80 -2 -8 11 9.28 1.52 2 8 -11 7.76 1.38 -2 -8 11 8.20 1.14 -2 8 11 7.42 1.39 2 8 -11 8.20 1.64 -2 8 10 36.66 2.82 -2 -8 10 35.60 2.33 2 8 -10 41.65 3.00 2 8 -10 30.38 3.02 -2 -8 10 39.94 3.00 -2 8 10 41.34 2.51 -2 8 9 47.98 3.13 2 8 -9 40.87 3.36 -2 -8 9 42.66 2.50 -2 -8 9 44.07 3.10 2 8 -9 45.84 3.11 -2 8 9 47.15 2.71 2 8 -8 142.58 6.63 -2 8 8 137.91 5.33 2 8 -8 134.56 5.85 -2 -8 8 138.14 5.91 -2 8 8 131.86 5.24 -2 8 8 134.07 5.79 -2 8 7 15.29 1.63 -2 -8 7 13.54 1.53 -2 8 7 14.43 1.44 -2 8 7 12.30 1.33 -2 -8 7 13.47 1.55 2 8 -7 11.80 1.69 2 8 -7 13.71 1.58 -2 8 6 42.00 2.59 -2 8 6 37.49 2.27 2 8 -6 44.74 3.15 -2 -8 6 42.91 2.70 2 8 -6 46.48 2.85 -2 8 5 6.28 1.00 2 8 -5 7.37 1.25 -2 8 5 4.74 0.81 2 8 -5 8.42 1.16 -2 -8 5 5.49 0.94 -2 8 4 68.01 3.52 -2 -8 4 66.01 3.25 -2 8 4 67.90 3.31 2 8 -4 69.23 3.53 2 8 -4 67.29 3.86 2 8 -3 2.97 0.80 2 8 -3 2.25 0.62 -2 8 3 1.81 0.64 -2 -8 3 3.49 0.67 2 8 -2 8.03 1.21 -2 8 2 7.61 1.10 -2 -8 2 9.29 1.05 -2 -8 1 167.95 5.70 2 8 -1 162.03 6.48 -2 8 1 172.29 6.42 2 -8 -1 166.25 5.72 -2 -8 0 61.28 2.71 -2 8 0 60.67 3.33 2 -8 0 63.23 3.05 -2 8 0 64.87 3.41 2 8 0 58.92 3.30 -2 8 -1 23.89 2.03 2 -8 1 23.43 1.86 -2 8 -1 26.95 2.09 2 8 1 22.75 1.91 2 -8 2 0.66 0.47 2 8 2 0.52 0.43 -2 8 -2 1.20 0.52 -2 8 -2 1.06 0.58 2 -8 3 2.03 0.69 -2 8 -3 4.52 0.93 -2 8 -3 4.00 0.90 2 -8 4 150.63 6.23 -2 8 -4 143.64 5.64 -2 8 -4 140.88 5.80 -2 8 -4 151.83 6.44 -2 8 -5 46.18 3.24 -2 8 -5 39.91 2.63 2 -8 5 40.95 2.96 -2 8 -5 41.23 2.66 2 8 5 41.45 3.02 -2 8 -6 27.64 2.62 -2 8 -6 30.53 2.34 2 -8 6 30.35 2.66 2 8 6 30.35 2.62 -2 8 -6 30.05 2.24 -2 8 -7 44.10 2.73 -2 8 -7 43.23 3.38 2 -8 7 40.47 3.24 -2 8 -7 39.13 2.81 2 8 7 44.29 3.29 2 8 7 40.97 2.70 2 8 8 354.76 11.56 -2 8 -8 339.81 11.82 2 -8 8 348.52 12.66 -2 8 -8 357.09 11.26 2 8 8 355.16 12.42 2 8 9 73.15 4.51 2 8 9 80.87 4.22 -2 8 -9 76.60 4.36 2 -8 9 82.15 5.00 2 8 10 20.71 2.31 2 8 10 20.40 2.07 -2 8 -10 22.06 1.96 -2 8 -10 21.15 2.24 2 -8 10 20.09 2.47 2 8 11 19.05 2.13 2 8 11 17.07 1.94 2 -8 11 19.33 2.44 -2 8 -11 15.79 1.99 -2 8 -12 103.34 5.42 2 8 12 100.53 5.18 2 8 12 110.12 5.35 -2 8 -12 102.40 6.00 2 -8 12 100.82 6.00 2 8 13 18.17 2.03 -2 8 -13 12.66 1.75 -2 8 -13 14.30 2.18 2 -8 13 13.83 2.12 -2 8 -14 44.26 3.62 -2 8 -15 42.26 3.43 -2 8 -16 15.66 1.98 -2 8 -17 0.34 0.45 -2 8 -18 11.56 1.40 -2 8 -18 10.41 1.16 -2 8 -19 2.09 0.42 2 9 -20 36.05 2.29 2 9 -19 22.66 2.01 -2 -9 19 22.25 1.77 -2 -9 19 21.25 1.53 2 9 -18 67.73 4.09 -2 -9 18 74.71 3.52 -2 -9 18 75.38 3.86 -2 -9 17 14.94 1.55 2 9 -17 14.12 1.92 2 9 -16 77.13 4.84 -2 -9 15 18.17 2.08 2 9 -15 13.00 2.02 2 9 -14 130.40 7.08 2 9 -14 134.36 6.16 -2 -9 14 150.71 6.73 -2 9 14 150.87 6.71 2 9 -13 16.91 2.41 2 9 -13 17.34 1.97 -2 -9 13 17.14 2.12 -2 9 13 17.85 2.15 2 9 -12 46.03 3.96 -2 9 12 57.45 3.71 -2 -9 12 54.20 3.73 2 9 -12 42.82 3.25 -2 9 11 31.53 2.66 -2 -9 11 28.53 2.12 2 9 -11 23.23 2.81 -2 -9 11 26.92 2.64 2 9 -11 24.24 2.41 2 9 -10 202.95 8.17 -2 9 10 211.24 7.42 -2 -9 10 203.56 7.20 2 9 -10 203.09 9.12 -2 9 10 205.52 8.13 -2 -9 10 200.22 8.23 2 9 -9 101.09 5.11 -2 -9 9 102.90 5.14 -2 9 9 96.97 4.97 -2 9 9 107.11 4.57 2 9 -9 101.93 5.81 2 9 -8 63.47 3.81 -2 -9 8 65.34 3.77 -2 9 8 61.24 3.30 -2 9 8 64.91 3.75 -2 9 8 56.97 3.19 2 9 -8 66.14 4.38 2 9 -7 52.85 3.32 2 9 -7 48.47 3.62 -2 -9 7 49.39 3.22 -2 9 7 52.11 2.97 -2 9 7 45.64 2.58 -2 9 7 46.49 2.87 -2 9 7 53.21 3.25 -2 9 6 169.66 6.84 -2 9 6 174.94 6.35 -2 9 6 188.47 6.67 2 9 -6 173.78 6.94 -2 -9 6 175.61 6.89 -2 9 6 167.26 6.63 2 9 -6 180.53 7.71 2 9 -5 21.03 2.21 -2 9 5 20.94 1.76 -2 9 5 18.80 1.71 -2 -9 5 19.46 1.75 2 9 -5 20.86 1.97 -2 -9 5 23.23 1.98 -2 9 5 19.88 1.87 -2 9 5 18.70 1.88 -2 -9 4 250.19 8.72 -2 9 4 267.69 9.30 2 9 -4 273.85 9.39 2 9 -4 283.91 10.08 -2 9 4 265.91 8.95 2 9 -3 0.52 0.58 -2 9 3 1.03 0.63 -2 9 3 2.11 0.67 -2 9 3 3.13 0.75 -2 -9 3 1.80 0.58 2 9 -2 242.29 8.60 -2 9 2 219.10 8.13 -2 -9 2 216.50 7.28 -2 9 2 217.10 7.89 -2 9 2 219.34 7.75 2 9 -1 1.73 0.82 -2 9 1 1.13 0.57 -2 9 1 1.96 0.60 -2 9 1 2.94 0.79 -2 9 0 318.97 10.36 -2 9 0 321.28 10.91 -2 9 0 318.10 10.82 2 9 0 333.79 10.97 -2 9 -1 39.36 2.79 2 9 1 40.70 2.75 2 -9 1 35.07 2.33 -2 9 -1 38.07 2.70 -2 9 -2 123.45 5.65 -2 9 -2 118.42 4.86 2 9 2 121.93 5.41 2 9 2 124.37 5.77 2 -9 2 123.08 5.26 -2 9 -2 132.54 5.57 -2 9 -3 14.13 1.78 -2 9 -3 17.34 1.58 2 9 3 17.01 1.96 2 -9 3 16.69 1.76 -2 9 -3 13.91 1.64 -2 9 -4 173.71 7.37 -2 9 -4 176.53 6.64 2 9 4 170.72 7.35 2 -9 4 167.03 7.03 -2 9 -4 180.28 6.94 -2 9 -5 1.65 0.77 -2 9 -5 1.85 0.62 2 9 5 2.58 0.85 2 -9 5 1.87 0.77 -2 9 -5 1.35 0.64 -2 9 -6 64.45 4.15 -2 9 -6 52.81 3.30 2 9 6 48.46 3.59 2 -9 6 55.98 3.76 -2 9 -6 55.40 3.32 -2 9 -7 1.45 0.80 2 9 7 3.83 1.09 -2 9 -7 2.48 0.78 2 -9 7 3.66 1.06 -2 9 -7 2.34 0.73 -2 9 -8 136.03 6.14 2 9 8 138.25 6.63 -2 9 -8 135.18 5.71 -2 9 -8 139.48 6.00 2 -9 8 141.47 6.81 2 -9 9 63.74 4.37 2 9 9 60.50 4.07 -2 9 -9 60.78 3.57 -2 9 -9 58.58 3.83 -2 9 -10 98.53 4.73 2 -9 10 113.78 6.06 -2 9 -10 95.23 5.14 2 9 10 93.65 5.26 2 -9 10 100.98 5.15 2 -9 11 7.75 1.39 2 -9 11 5.42 1.41 -2 9 -11 5.99 1.23 2 9 11 8.68 1.47 -2 9 -11 8.15 1.21 2 -9 12 161.74 7.80 -2 9 -12 139.98 6.70 2 -9 12 176.06 7.00 -2 9 -12 151.98 7.72 2 -9 13 3.24 0.91 -2 9 -13 2.29 0.96 2 -9 14 61.98 3.64 -2 9 -14 60.70 4.24 -2 9 -15 3.95 1.09 -2 9 -16 109.20 5.32 -2 9 -17 26.67 2.04 -2 9 -17 20.67 1.95 -2 9 -18 14.63 1.26 -2 9 -18 14.86 1.43 -2 -10 19 53.93 2.70 -2 -10 18 24.96 1.93 -2 -10 17 20.70 1.95 2 10 -16 61.39 4.11 -2 -10 16 63.28 3.74 -2 -10 15 117.55 5.60 -2 10 15 118.97 5.55 2 10 -15 104.06 5.94 -2 -10 14 5.37 1.28 -2 10 14 3.32 1.05 2 10 -14 5.74 1.11 2 10 -14 6.46 1.47 2 10 -13 48.25 4.07 -2 -10 13 57.82 3.80 2 10 -13 46.40 3.30 -2 10 13 52.23 3.56 2 10 -12 134.80 7.13 -2 -10 12 141.25 6.45 -2 10 12 139.68 6.34 -2 10 11 89.71 4.79 2 10 -11 82.17 4.67 -2 -10 11 86.07 4.82 2 10 -10 68.11 3.88 2 10 -10 75.63 5.10 -2 10 10 82.57 3.93 2 10 -10 74.69 4.41 -2 10 10 77.27 4.42 -2 -10 10 81.29 4.56 2 10 -9 192.89 8.89 -2 -10 9 198.54 7.94 -2 10 9 195.31 7.81 2 10 -9 181.79 7.79 -2 10 9 191.86 7.12 2 10 -9 197.22 7.60 2 10 -8 113.77 6.17 -2 -10 8 114.90 5.42 2 10 -8 102.88 5.29 -2 10 8 112.21 5.33 -2 10 8 106.26 4.78 -2 10 8 109.36 4.84 2 10 -7 180.67 8.18 -2 10 7 187.01 6.98 -2 10 7 188.16 6.68 2 10 -7 182.88 7.51 -2 10 7 175.90 6.96 -2 -10 7 188.10 7.41 -2 10 7 189.39 7.45 -2 10 6 152.78 6.34 -2 -10 6 136.74 6.11 -2 10 6 143.56 5.74 2 10 -6 152.32 6.51 -2 10 6 149.01 5.98 -2 10 6 152.98 6.20 2 10 -6 149.83 7.04 -2 10 5 161.30 6.69 -2 10 5 172.18 6.57 -2 10 5 165.43 6.75 2 10 -5 167.47 7.45 -2 -10 5 164.45 6.64 2 10 -5 173.29 7.00 -2 10 5 170.50 6.47 -2 10 4 10.38 1.43 -2 10 4 10.87 1.45 -2 -10 4 14.65 1.55 -2 10 4 11.91 1.44 2 10 -4 11.51 1.71 -2 10 3 43.02 2.83 2 10 -3 39.35 3.07 -2 10 3 43.10 2.98 2 10 -2 16.68 1.97 -2 10 2 17.81 1.90 -2 10 2 18.27 1.75 -2 10 2 16.02 1.75 2 10 -1 7.34 1.39 -2 10 1 10.75 1.44 -2 10 1 12.96 1.47 -2 10 1 6.36 1.10 -2 10 0 30.54 2.49 -2 10 0 30.08 2.09 2 10 0 35.85 2.72 -2 10 0 32.42 2.37 -2 10 0 33.09 2.50 -2 10 0 31.89 2.58 -2 10 -1 79.90 4.42 -2 10 -1 76.78 3.93 -2 10 -1 71.49 3.55 2 10 1 84.55 4.38 -2 10 -1 85.69 4.37 -2 10 -1 80.63 4.33 -2 10 -2 12.03 1.57 -2 10 -2 10.57 1.24 -2 10 -2 11.52 1.54 -2 10 -2 9.34 1.42 -2 10 -2 9.77 1.50 2 10 2 7.68 1.41 2 10 3 69.81 4.33 -2 10 -3 65.26 3.49 -2 10 -3 71.90 4.02 -2 10 -3 75.69 4.36 -2 10 -3 68.63 4.00 -2 10 -4 302.35 10.79 -2 10 -4 311.56 10.71 2 10 4 292.56 11.22 -2 10 -4 300.87 10.17 2 -10 4 309.18 10.79 -2 10 -4 319.03 11.36 -2 10 -5 278.19 10.14 -2 10 -5 278.00 9.96 2 10 5 282.98 10.78 -2 10 -5 275.62 9.70 2 -10 5 282.98 10.36 -2 10 -5 294.78 10.91 -2 10 -6 144.21 6.32 -2 10 -6 145.23 6.11 2 10 6 129.58 6.63 -2 10 -6 141.12 6.09 2 -10 6 139.62 6.57 -2 10 -6 142.81 7.03 -2 10 -7 425.61 13.92 -2 10 -7 454.99 13.79 2 10 7 406.58 14.57 -2 10 -7 417.43 13.81 2 -10 7 418.51 14.56 -2 10 -7 425.66 15.18 2 10 8 331.80 12.50 -2 10 -8 348.74 11.77 -2 10 -8 331.81 11.77 2 -10 8 344.95 12.61 -2 10 -8 366.17 11.58 -2 10 -9 170.13 7.22 2 -10 9 172.48 7.89 2 10 9 161.71 7.52 -2 10 -9 176.20 6.99 2 10 10 41.34 3.26 2 -10 10 42.37 3.54 -2 10 -10 36.93 3.00 -2 10 -10 43.81 2.93 2 -10 10 43.35 3.20 2 -10 11 157.56 6.68 2 10 11 148.99 6.67 2 -10 11 158.32 7.51 -2 10 -11 145.00 5.99 -2 10 -12 20.18 2.51 2 -10 12 24.48 2.27 -2 10 -13 36.56 3.25 2 -10 13 38.54 2.79 -2 10 -14 36.35 3.07 2 -10 14 44.24 2.88 -2 10 -15 18.03 2.01 -2 10 -16 14.31 1.58 -2 10 -16 13.74 1.61 -2 10 -17 20.15 1.63 -2 10 -17 16.60 1.57 -2 10 -18 12.62 1.03 -2 -11 18 105.63 4.20 -2 -11 17 45.54 2.73 -2 -11 16 114.59 5.09 -2 11 15 70.80 3.90 -2 -11 15 73.11 4.01 -2 11 14 138.74 6.05 -2 -11 14 131.02 6.04 -2 11 13 139.65 6.18 -2 -11 13 149.26 6.38 -2 11 12 344.27 11.85 -2 -11 12 348.97 12.03 2 11 -12 326.27 11.64 -2 11 11 42.08 3.16 2 11 -11 46.61 3.32 -2 -11 11 48.17 3.42 2 11 -10 75.38 4.01 -2 11 10 69.16 4.20 -2 11 10 75.46 3.78 2 11 -10 65.86 4.85 2 11 -10 69.12 4.23 -2 -11 10 75.91 4.38 2 11 -9 168.00 6.96 -2 11 9 165.80 6.47 2 11 -9 165.28 7.23 2 11 -9 154.67 7.86 -2 -11 9 170.26 7.20 -2 11 9 171.63 7.16 2 11 -8 549.20 17.29 -2 11 8 584.52 16.70 -2 11 8 540.98 16.52 2 11 -8 535.98 17.42 2 11 -8 540.21 18.52 -2 -11 8 542.14 17.25 -2 11 8 555.43 17.24 -2 11 7 70.09 3.72 -2 11 7 64.23 3.67 2 11 -7 68.89 4.16 -2 11 7 71.28 4.01 -2 11 7 66.11 3.44 -2 -11 7 66.27 3.95 2 11 -7 62.91 4.50 2 11 -6 257.64 10.31 -2 11 6 251.80 9.18 -2 11 6 266.63 9.40 -2 11 6 252.18 8.78 -2 -11 6 243.61 9.19 -2 11 6 260.83 9.07 -2 11 5 86.62 4.35 -2 11 5 88.52 4.31 -2 11 5 89.64 4.56 -2 11 5 87.29 4.56 -2 -11 5 90.34 4.48 2 11 -5 84.15 5.05 -2 11 4 432.90 13.56 -2 11 4 422.62 13.67 -2 11 4 417.53 13.90 -2 -11 4 410.21 13.35 2 11 -4 453.17 14.80 -2 11 3 173.09 6.88 -2 11 3 176.06 7.22 -2 11 3 163.87 6.77 2 11 -3 168.55 7.45 -2 11 2 478.01 15.16 2 11 -2 477.77 15.68 -2 11 2 493.38 15.04 -2 11 2 466.52 15.40 -2 11 1 215.03 8.26 2 11 -1 215.19 8.51 -2 11 1 207.48 7.93 -2 11 1 216.00 7.85 -2 11 0 298.31 10.61 -2 11 0 296.89 10.22 2 11 0 304.80 10.77 -2 11 0 290.24 10.23 -2 11 -1 101.07 5.25 -2 11 -1 102.43 4.98 -2 11 -1 90.74 4.24 2 11 1 96.82 5.09 -2 11 -1 100.77 4.76 -2 11 -1 96.57 5.04 -2 11 -2 295.85 10.60 -2 11 -2 293.52 10.24 -2 11 -2 258.36 10.01 -2 11 -2 264.13 9.12 -2 11 -2 264.41 9.58 -2 11 -2 292.43 10.30 -2 11 -3 187.60 7.99 -2 11 -3 192.62 7.86 -2 11 -3 176.60 6.81 -2 11 -3 193.81 7.74 -2 11 -3 179.75 7.18 -2 11 -3 190.41 7.79 -2 11 -4 189.99 7.13 -2 11 -4 197.35 7.75 -2 11 -4 184.49 7.78 2 11 4 182.57 6.69 -2 11 -4 194.53 8.30 2 11 5 33.13 3.05 -2 11 -5 27.15 2.49 -2 11 -5 33.12 2.75 -2 11 -5 27.47 2.28 -2 11 -5 27.33 2.77 2 11 6 159.89 7.64 -2 11 -6 174.95 7.04 -2 11 -6 173.84 7.21 -2 11 -6 171.73 7.94 -2 11 -6 157.39 6.64 -2 11 -7 63.95 3.74 -2 11 -7 67.20 3.84 -2 11 -7 60.05 4.43 2 -11 7 61.43 4.15 2 11 7 61.56 3.57 2 11 7 57.63 4.21 -2 11 -7 68.34 3.98 -2 11 -8 100.06 4.89 -2 11 -8 86.46 4.21 -2 11 -8 85.56 4.56 2 11 8 96.36 5.36 2 -11 8 90.58 5.23 -2 11 -9 22.25 2.11 2 -11 9 21.98 2.49 2 -11 10 156.48 6.73 -2 11 -10 153.49 6.30 2 -11 11 34.16 2.72 -2 11 -11 37.48 2.50 2 -11 12 77.00 4.12 -2 11 -12 71.53 4.65 2 -11 13 31.04 2.37 -2 11 -13 29.02 2.73 2 -11 14 96.03 4.36 -2 11 -14 91.00 4.82 -2 11 -15 58.96 3.36 -2 11 -15 54.61 3.31 -2 11 -16 23.72 1.85 -2 11 -16 25.93 1.97 -2 11 -17 12.34 1.10 -2 -12 16 10.71 1.26 -2 -12 15 9.84 1.33 -2 12 14 48.86 3.04 -2 -12 14 46.56 3.05 -2 12 13 16.10 1.79 -2 -12 13 17.23 1.88 -2 12 12 41.94 3.07 -2 -12 12 41.55 3.05 -2 12 11 29.05 2.51 -2 -12 11 32.92 2.70 -2 12 10 11.09 1.44 -2 12 10 15.85 1.91 2 12 -10 12.97 1.61 -2 -12 10 15.95 1.91 -2 12 9 16.00 1.66 -2 12 9 15.51 1.91 2 12 -9 14.75 1.78 -2 -12 9 14.64 1.85 -2 12 8 345.67 11.07 -2 -12 8 318.03 11.45 -2 12 8 338.99 11.57 2 12 -8 332.69 11.68 2 12 -7 149.71 6.79 -2 12 7 146.46 6.09 -2 -12 7 156.34 6.51 -2 12 7 145.70 6.37 -2 12 7 145.46 6.17 -2 12 6 50.53 3.15 -2 -12 6 49.86 3.27 -2 12 6 44.61 3.14 -2 12 6 48.38 3.02 -2 12 6 50.04 3.28 -2 12 5 13.23 1.57 -2 12 5 9.11 1.46 -2 -12 5 9.41 1.38 -2 12 5 12.31 1.55 -2 12 5 10.30 1.52 -2 12 4 413.81 14.02 -2 12 4 423.08 13.67 -2 12 4 433.41 13.69 -2 12 3 21.75 2.28 -2 12 3 23.46 2.15 -2 12 3 21.66 2.15 -2 12 2 290.17 9.96 -2 12 2 269.55 9.59 2 12 -2 247.15 9.95 -2 12 2 264.26 10.01 -2 12 2 258.04 9.36 -2 12 1 2.63 0.83 -2 12 1 4.29 1.04 -2 12 1 4.63 1.18 2 12 -1 3.03 1.09 -2 12 0 170.81 7.48 2 12 0 185.45 7.78 -2 12 0 178.70 7.24 -2 12 0 189.19 7.23 -2 12 -1 9.75 1.66 -2 12 -1 11.04 1.50 -2 12 -1 11.32 1.55 -2 12 -2 378.64 12.48 -2 12 -2 337.80 12.35 -2 12 -2 362.14 12.50 -2 12 -2 380.91 12.94 -2 12 -2 337.43 11.88 -2 12 -3 56.03 3.77 -2 12 -3 54.43 3.76 -2 12 -3 54.08 3.66 -2 12 -3 55.78 3.93 2 12 3 53.47 3.07 -2 12 -3 51.87 3.33 -2 12 -4 217.44 8.67 -2 12 -4 203.82 8.35 -2 12 -4 218.86 8.38 -2 12 -4 195.65 8.64 2 12 4 199.79 7.25 -2 12 -4 203.04 7.87 -2 12 -5 34.92 3.03 -2 12 -5 32.21 2.79 -2 12 -5 30.92 3.08 -2 12 -5 37.21 2.91 2 12 5 32.91 2.76 -2 12 -5 28.81 2.40 -2 12 -6 142.16 6.03 2 12 6 146.05 6.32 -2 12 -6 146.14 6.57 -2 12 -6 154.21 6.55 -2 12 -6 144.50 7.27 -2 12 -7 52.81 3.16 -2 12 -7 54.05 4.16 2 12 7 50.45 3.18 -2 12 -7 56.25 3.59 -2 12 -8 338.07 11.15 -2 12 -8 303.02 10.33 2 -12 9 53.18 3.44 -2 12 -9 53.47 3.27 -2 12 -9 46.44 2.76 -2 12 -10 57.73 3.31 2 -12 10 62.54 3.69 -2 12 -11 7.80 1.07 2 -12 11 8.03 1.32 2 -12 12 180.77 6.71 -2 12 -12 152.35 7.12 2 -12 13 1.12 0.60 -2 12 -13 2.29 0.77 -2 12 -14 79.20 4.03 2 -12 14 80.73 3.64 -2 12 -14 74.11 3.95 -2 12 -15 1.28 0.52 -2 12 -15 0.93 0.45 -2 12 -16 30.86 1.85 2 13 -16 28.03 1.90 -2 -13 15 1.74 0.58 2 13 -15 0.13 0.41 -2 -13 14 22.51 1.87 -2 13 13 0.38 0.52 -2 -13 13 0.54 0.56 -2 -13 12 32.75 2.47 -2 13 12 32.72 2.42 -2 -13 11 9.44 1.48 -2 13 11 11.03 1.45 2 13 -10 77.99 3.93 -2 13 10 75.33 4.04 -2 -13 10 73.30 4.02 2 13 -9 10.62 1.50 -2 13 9 12.53 1.45 -2 13 9 12.48 1.62 -2 -13 9 10.73 1.51 2 13 -8 5.30 1.17 -2 13 8 6.49 1.11 -2 -13 8 7.95 1.31 -2 13 8 7.10 1.27 -2 13 7 28.96 2.44 -2 -13 7 31.97 2.52 2 13 -7 36.10 2.96 -2 13 7 29.76 2.34 -2 13 6 94.35 4.66 -2 13 6 100.53 4.68 2 13 -6 98.36 5.29 -2 -13 6 88.85 4.53 -2 13 5 14.14 1.68 2 13 -5 15.36 2.07 -2 13 5 12.63 1.60 -2 13 5 15.15 1.86 -2 13 5 12.18 1.53 2 13 -4 60.13 4.16 -2 13 4 68.74 4.09 -2 13 4 58.36 3.51 -2 13 4 62.11 3.67 -2 13 3 4.86 1.06 2 13 -3 4.85 1.34 -2 13 3 4.56 1.18 -2 13 3 4.61 1.03 -2 13 2 29.08 2.36 -2 13 2 29.04 2.48 -2 13 2 29.43 2.55 -2 13 2 26.27 2.55 -2 13 1 -0.38 0.57 -2 13 1 0.51 0.62 -2 13 1 0.41 0.75 -2 13 1 1.05 0.56 -2 13 0 57.56 3.51 -2 13 0 51.68 3.60 -2 13 -1 3.44 0.90 -2 13 -1 3.87 0.92 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-4 5 18.32 1.76 -4 4 5 22.91 1.90 4 -4 -4 75.04 3.79 4 4 -4 71.77 3.78 -4 4 4 69.80 3.63 -4 -4 4 70.60 3.62 4 -4 -3 172.63 6.55 4 4 -3 172.59 6.61 4 -4 -2 1195.88 32.46 4 4 -2 1176.26 32.46 4 4 -1 679.86 19.72 4 -4 -1 688.17 19.77 4 -4 0 754.50 21.47 4 4 0 753.75 21.49 4 4 1 524.95 15.98 4 -4 1 552.71 16.08 4 4 2 1739.29 46.08 4 -4 2 1703.51 46.04 4 4 3 756.77 22.07 4 -4 3 784.69 22.13 4 4 3 742.91 21.79 4 -4 3 755.14 21.86 4 4 4 37.55 2.69 4 -4 4 33.95 2.64 4 4 4 33.35 2.51 4 -4 4 33.79 2.53 4 4 5 63.18 3.80 4 -4 5 74.93 4.13 4 4 5 69.28 3.83 4 -4 5 65.57 3.79 -4 4 -5 62.96 3.81 4 4 6 138.83 6.32 4 -4 6 142.28 6.42 -4 4 -6 142.20 6.29 4 4 6 144.50 6.27 4 -4 6 145.02 6.27 4 -4 7 37.53 2.96 4 4 7 41.11 3.05 4 -4 7 35.29 2.75 -4 4 -7 39.66 2.97 -4 -4 -7 36.99 3.10 -4 4 -7 37.04 3.10 4 4 7 38.20 3.04 4 -4 7 42.30 3.20 4 -4 7 32.35 2.31 4 -4 8 292.79 10.60 -4 -4 -8 299.63 11.32 -4 4 -8 299.78 11.34 4 4 8 301.60 11.13 4 -4 8 299.31 11.16 -4 4 -8 310.06 10.91 4 -4 8 291.13 9.83 4 -4 9 19.97 1.83 -4 4 -9 16.41 1.94 4 -4 9 16.98 2.01 4 -4 9 18.46 2.30 4 4 9 19.11 2.30 -4 -4 -9 16.99 2.25 -4 4 -9 22.96 2.52 4 4 10 67.82 4.62 4 -4 10 74.19 3.83 -4 4 -10 75.94 4.37 4 4 10 69.56 4.58 4 -4 10 64.86 4.49 4 -4 10 76.77 5.07 -4 -4 -10 75.36 4.93 -4 4 -10 70.60 4.79 4 -4 10 78.18 4.47 4 -4 11 1.14 0.62 -4 4 -11 1.13 0.68 4 -4 11 1.92 0.95 -4 -4 -11 2.10 0.95 -4 4 -11 0.26 0.69 4 4 11 3.16 1.15 4 -4 11 2.67 0.92 4 -4 12 30.56 2.35 4 -4 12 34.06 3.33 -4 -4 -12 32.15 3.18 -4 4 -12 29.23 3.02 4 4 12 31.92 3.11 4 -4 12 38.00 3.05 -4 4 -12 30.68 2.59 4 4 13 32.70 3.04 4 -4 13 36.00 3.19 4 4 13 37.66 3.31 4 -4 13 37.97 3.05 -4 4 -13 36.88 2.73 4 4 14 166.38 7.44 4 -4 14 152.84 6.80 4 4 14 146.22 6.95 4 -4 14 154.98 7.14 4 4 15 21.32 2.32 4 4 15 21.68 2.31 4 -4 15 28.38 2.58 4 4 16 134.98 6.17 4 -4 16 133.61 6.03 4 4 16 131.71 5.96 4 -4 17 32.27 2.41 4 4 17 28.44 2.26 -4 4 -17 27.03 2.26 -4 4 -18 117.08 4.76 -4 -5 22 2.32 0.55 -4 -5 21 13.14 1.37 -4 -5 20 0.14 0.45 4 5 -20 0.92 0.49 -4 -5 19 19.13 1.90 4 5 -19 15.38 1.76 4 5 -18 21.92 2.24 -4 -5 18 25.98 2.39 -4 5 18 23.63 2.26 -4 -5 18 27.00 2.38 -4 -5 18 23.65 2.05 -4 5 17 16.96 1.99 -4 -5 17 20.50 2.20 -4 -5 17 20.23 2.17 4 5 -17 16.57 2.06 -4 5 17 19.33 2.01 -4 -5 17 16.66 1.86 -4 -5 16 17.39 2.07 -4 -5 16 19.16 2.03 -4 5 16 14.41 1.97 -4 5 16 17.02 2.09 4 5 -16 16.72 2.11 -4 5 16 20.21 2.14 -4 -5 16 12.88 1.83 -4 5 15 69.36 4.54 4 5 -15 59.09 4.23 -4 -5 15 68.08 4.09 4 -5 -15 62.04 4.65 -4 5 15 64.52 4.20 -4 -5 15 67.13 4.22 -4 5 15 70.12 4.35 -4 5 15 67.54 4.03 4 5 -15 54.05 4.25 4 5 -14 6.83 1.70 4 -5 -14 8.96 1.87 -4 5 14 6.16 1.39 -4 -5 14 7.39 1.56 -4 5 14 10.93 1.68 4 5 -14 11.60 1.80 -4 5 14 12.04 1.83 -4 -5 14 9.42 1.62 -4 5 14 11.42 1.65 4 -5 -13 2.29 0.96 4 5 -13 3.43 1.10 -4 5 13 4.51 1.20 -4 -5 13 3.25 0.88 4 5 -13 2.94 0.99 -4 5 13 3.19 1.08 -4 5 13 3.13 1.02 -4 -5 13 2.48 0.98 -4 -5 12 24.66 2.41 4 -5 -12 23.29 2.59 4 5 -12 23.34 2.56 -4 5 12 24.52 2.47 -4 -5 12 23.48 2.19 -4 5 12 22.51 2.38 -4 -5 12 25.35 2.47 4 5 -12 21.13 2.37 -4 5 12 19.80 2.31 -4 5 12 25.71 2.43 -4 -5 11 91.48 4.91 -4 5 11 88.16 4.55 -4 -5 11 84.83 4.66 -4 5 11 80.09 4.58 4 5 -11 84.55 4.80 -4 5 11 78.86 4.63 -4 -5 11 81.65 4.48 4 -5 -11 86.63 5.03 4 5 -11 81.11 4.85 -4 -5 10 27.91 2.53 -4 5 10 23.30 2.19 -4 5 10 27.91 2.44 -4 -5 10 24.89 2.33 4 5 -10 24.18 2.37 -4 5 10 24.71 2.33 4 -5 -10 22.91 2.40 4 5 -10 25.35 2.51 -4 -5 10 23.73 2.25 -4 -5 9 80.37 4.43 -4 5 9 79.04 4.27 -4 -5 9 82.08 4.33 -4 5 9 83.12 4.26 4 -5 -9 81.03 4.52 4 5 -9 80.25 4.55 4 5 -9 80.22 4.39 -4 5 9 75.50 4.14 -4 -5 9 79.52 4.28 4 5 -8 36.94 2.73 -4 5 8 35.01 2.61 -4 -5 8 38.95 2.87 -4 -5 8 34.61 2.67 4 5 -8 44.32 3.05 4 -5 -8 40.96 2.94 4 5 -7 58.45 3.49 4 5 -7 60.59 3.63 4 -5 -7 68.42 3.76 -4 5 7 64.45 3.54 -4 -5 7 64.79 3.55 4 5 -6 9.03 1.25 -4 5 6 8.92 1.26 -4 -5 6 9.09 1.24 4 -5 -6 9.65 1.32 4 5 -6 10.59 1.44 4 5 -5 45.78 2.85 -4 5 5 49.44 2.92 -4 -5 5 51.55 2.97 4 -5 -5 50.58 3.07 4 5 -5 53.38 3.12 4 5 -4 9.65 1.21 -4 5 4 10.65 1.32 -4 -5 4 12.05 1.40 4 -5 -4 10.13 1.29 4 5 -4 11.46 1.36 4 5 -3 28.96 2.02 4 -5 -3 23.17 1.94 4 5 -3 24.29 2.02 4 5 -2 48.90 2.74 4 -5 -2 59.34 3.16 4 5 -2 55.39 3.09 4 5 -1 2.26 0.65 4 -5 -1 2.58 0.73 4 5 -1 1.24 0.60 4 -5 0 66.32 3.44 4 5 0 75.43 3.63 4 5 0 65.80 3.14 4 5 1 45.78 2.75 4 -5 1 45.29 2.73 -4 5 -2 10.72 1.28 4 -5 2 14.54 1.56 4 5 2 13.99 1.46 4 -5 2 11.28 1.35 -4 5 -3 55.36 3.45 4 5 3 53.40 3.17 4 -5 3 56.89 3.23 4 5 3 51.90 3.19 4 -5 3 55.69 3.33 -4 5 -3 49.58 2.99 4 -5 4 94.32 4.67 4 5 4 93.02 4.64 -4 5 -4 88.38 4.73 4 5 4 98.33 4.62 4 -5 4 98.09 4.63 4 5 5 97.39 4.81 4 -5 5 96.68 4.86 -4 5 -5 85.80 4.73 4 5 5 93.73 4.62 4 -5 5 87.46 4.55 4 -5 6 149.32 6.37 4 5 6 144.24 6.27 4 -5 6 142.91 6.41 4 5 6 137.07 6.34 -4 5 -6 152.49 5.97 -4 5 -6 138.36 6.46 4 -5 7 95.36 4.68 -4 5 -7 104.32 5.33 4 -5 7 99.82 5.22 4 5 7 90.56 5.01 4 -5 8 130.68 6.42 4 5 8 132.49 6.38 4 -5 8 126.47 5.50 4 -5 8 134.03 5.89 -4 5 -8 142.74 6.52 4 5 9 45.89 3.56 -4 5 -9 40.26 3.24 4 -5 9 41.27 3.03 4 5 9 41.94 3.36 4 -5 9 46.38 3.59 4 -5 9 44.00 3.78 4 -5 9 42.99 2.84 -4 5 -9 44.34 3.60 4 -5 10 55.06 3.60 4 -5 10 60.00 3.42 4 5 10 55.45 4.07 -4 -5 -10 54.47 4.15 -4 5 -10 55.33 4.17 4 5 11 24.71 2.66 4 -5 11 24.43 2.33 4 -5 11 22.88 2.09 -4 5 -11 26.20 2.83 -4 5 -11 28.38 2.58 -4 5 -12 24.48 2.38 -4 5 -12 22.31 2.58 4 -5 12 21.21 1.96 4 -5 12 21.63 2.69 4 5 12 25.87 2.70 4 -5 12 19.84 2.13 4 5 13 3.18 1.07 4 -5 13 2.82 0.83 4 5 13 1.68 0.87 4 -5 13 4.70 1.21 -4 5 -13 3.46 0.90 4 5 14 13.81 1.94 4 -5 14 14.18 1.87 4 5 14 10.19 1.57 -4 5 -14 11.89 1.49 4 5 15 4.40 1.06 4 -5 15 6.28 1.23 4 5 15 7.20 1.27 4 5 16 23.21 2.17 -4 5 -16 22.31 2.15 4 -5 16 20.27 1.95 -4 5 -17 9.15 1.24 4 -5 17 9.50 1.18 -4 -6 20 23.48 1.89 4 6 -20 21.33 1.79 -4 -6 19 2.61 0.79 4 6 -19 2.60 0.75 -4 -6 18 60.90 3.40 4 6 -18 52.00 3.55 -4 -6 18 57.60 3.51 -4 -6 18 61.76 3.43 -4 -6 17 29.26 2.53 4 6 -17 24.98 2.56 -4 -6 17 24.02 2.23 -4 -6 17 27.68 2.36 -4 6 17 26.98 2.41 4 6 -16 56.31 3.97 -4 6 16 54.50 3.59 -4 -6 16 58.45 3.64 -4 6 16 54.33 3.60 -4 -6 16 58.37 3.70 4 6 -15 6.80 1.50 -4 -6 15 6.75 1.34 -4 6 15 8.91 1.54 -4 6 15 6.37 1.33 -4 -6 15 6.35 1.36 -4 6 15 8.17 1.45 -4 6 14 60.91 3.98 -4 6 14 58.06 3.76 -4 -6 14 60.43 3.85 -4 -6 14 52.27 3.72 4 6 -14 55.86 4.07 4 -6 -14 52.04 4.08 4 6 -14 48.30 3.87 -4 6 14 62.00 3.90 -4 6 13 6.42 1.41 -4 6 13 9.44 1.51 -4 -6 13 7.73 1.38 4 6 -13 7.99 1.52 -4 -6 13 10.16 1.61 4 -6 -13 6.88 1.44 4 6 -13 6.46 1.38 -4 6 13 5.95 1.32 -4 6 12 143.67 6.55 -4 6 12 150.12 6.61 4 6 -12 150.44 7.02 -4 -6 12 143.66 6.57 4 6 -12 141.35 6.80 4 -6 -12 136.75 6.79 -4 -6 12 144.83 6.86 -4 6 11 0.92 0.64 -4 -6 11 0.73 0.64 -4 6 11 0.53 0.64 -4 -6 11 0.38 0.57 4 6 -11 1.52 0.79 -4 6 11 0.56 0.53 4 -6 -11 0.21 0.56 4 6 -11 1.05 0.70 -4 -6 11 1.25 0.81 -4 -6 10 111.16 5.39 -4 6 10 110.62 5.38 4 6 -10 111.95 5.74 -4 6 10 119.79 5.60 -4 6 10 110.15 4.83 4 -6 -10 124.31 5.84 4 6 -10 112.30 5.62 -4 -6 10 122.64 5.86 4 6 -9 13.70 1.82 4 6 -9 14.96 1.82 4 -6 -9 14.92 1.83 -4 6 9 13.55 1.70 -4 -6 9 13.62 1.79 -4 -6 9 14.57 1.72 -4 6 9 15.97 1.76 4 6 -8 224.72 8.77 -4 -6 8 248.41 9.01 4 -6 -8 233.64 8.72 4 6 -8 230.10 8.73 -4 6 8 236.73 8.72 -4 6 8 222.48 8.33 4 6 -7 25.92 2.32 -4 -6 7 27.34 2.34 4 -6 -7 28.65 2.34 4 6 -7 23.89 2.17 -4 6 7 24.47 2.18 -4 -6 7 25.31 2.28 -4 -6 6 242.16 8.46 4 6 -6 248.39 8.90 -4 -6 6 235.04 8.74 -4 6 6 250.00 8.51 4 -6 -6 239.35 8.62 4 6 -6 247.02 8.73 -4 6 6 235.71 8.18 -4 -6 5 38.10 2.46 -4 6 5 33.22 2.35 4 6 -5 38.58 2.70 4 -6 -5 38.36 2.57 4 6 -5 36.73 2.52 -4 6 5 36.25 2.30 -4 6 4 205.77 7.30 -4 -6 4 195.25 7.20 4 6 -4 205.71 7.48 4 -6 -4 196.95 7.26 4 6 -4 207.91 7.41 -4 6 3 71.23 3.63 -4 -6 3 78.72 3.76 4 6 -3 71.36 3.70 4 -6 -3 72.97 3.68 4 6 -3 82.43 3.83 4 6 -2 198.10 7.16 4 -6 -2 201.16 7.20 4 6 -2 207.11 7.26 4 6 -1 151.63 5.74 4 -6 -1 144.80 5.71 4 6 -1 150.40 5.79 4 6 0 211.55 7.44 4 6 0 218.34 7.61 4 -6 0 220.68 7.60 -4 6 -1 17.43 1.62 4 -6 1 20.58 1.74 4 6 1 23.53 1.86 -4 6 -1 20.00 2.01 -4 6 -2 99.67 4.65 4 -6 2 97.64 4.54 4 6 2 108.53 4.71 4 6 2 110.10 4.85 4 -6 2 108.24 4.81 -4 6 -2 109.83 5.25 -4 6 -3 24.51 2.14 4 6 3 23.66 2.01 4 -6 3 24.21 2.02 4 -6 3 28.74 2.31 4 6 3 25.51 2.12 -4 6 -3 26.75 2.44 -4 6 -4 179.88 7.25 -4 6 -4 179.70 7.59 4 6 4 185.62 7.05 4 -6 4 180.60 7.01 4 6 4 188.33 7.25 4 -6 4 182.01 7.21 -4 6 -5 4.38 1.15 -4 6 -5 3.25 0.88 4 6 5 4.05 0.96 4 -6 5 3.07 0.86 4 6 5 3.14 0.84 4 -6 5 2.97 0.85 -4 6 -5 1.44 0.72 -4 6 -6 119.48 6.05 -4 6 -6 128.84 5.52 4 6 6 125.40 5.80 4 -6 6 127.59 5.87 -4 6 -7 4.29 1.08 -4 6 -7 2.93 0.85 4 6 7 2.48 0.86 4 -6 7 2.51 0.87 -4 6 -8 97.75 5.37 4 6 8 92.06 5.04 4 -6 8 97.97 5.18 4 -6 8 91.52 5.67 4 6 9 33.72 3.05 -4 6 -9 31.29 2.89 4 6 9 32.66 2.88 4 -6 9 36.52 7.72 4 -6 9 31.40 3.22 4 -6 9 32.37 2.48 4 6 10 102.62 5.64 -4 6 -10 108.21 5.69 4 -6 10 114.49 6.44 4 -6 10 99.41 4.83 4 6 11 22.80 2.53 -4 6 -11 18.31 2.20 4 -6 11 21.60 2.72 4 -6 11 21.72 2.01 4 6 12 17.37 2.19 4 -6 12 18.12 1.83 4 6 12 18.56 2.15 4 -6 12 18.70 2.18 -4 6 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9.43 1.34 -4 7 2 8.56 1.32 4 7 -2 10.03 1.45 -4 7 2 9.48 1.14 -4 7 2 10.41 1.22 -4 -7 2 8.66 1.12 4 7 -2 7.14 1.08 4 -7 -2 9.28 1.18 4 7 -2 8.38 1.26 4 7 -1 47.55 2.74 4 -7 -1 52.54 2.81 4 7 -1 53.43 3.07 4 7 -1 44.65 3.22 -4 7 1 47.84 2.69 -4 7 0 4.40 0.82 4 7 0 4.59 1.01 4 -7 0 3.98 0.78 -4 7 0 4.50 1.00 4 7 0 5.37 0.97 4 7 0 4.33 0.81 4 -7 0 3.64 0.76 -4 7 0 4.30 0.77 4 7 1 30.99 2.67 4 7 1 29.62 2.19 4 -7 1 32.28 2.24 -4 7 -1 33.25 2.36 -4 7 -1 32.21 2.05 4 -7 2 11.51 1.36 4 7 2 13.62 1.46 4 7 2 8.27 1.44 -4 7 -2 10.76 1.39 4 7 3 4.12 0.86 4 -7 3 4.93 0.94 4 7 3 5.03 0.92 -4 7 -3 4.78 1.08 -4 7 -3 5.11 1.12 -4 7 -3 5.41 1.07 -4 7 -4 58.20 3.97 -4 7 -4 66.74 3.74 4 7 4 64.69 3.49 4 -7 4 60.55 3.53 4 7 4 61.88 3.52 -4 7 -4 64.18 3.84 -4 7 -5 0.96 0.68 -4 7 -5 -0.20 0.52 4 7 5 0.48 0.51 -4 7 -5 1.49 0.74 4 7 6 71.45 4.01 -4 7 -6 76.47 4.03 -4 7 -6 70.15 4.46 -4 7 -6 64.30 4.23 -4 7 -7 31.15 2.94 4 7 7 31.47 2.61 4 -7 7 28.34 3.03 -4 7 -7 33.57 2.56 -4 7 -7 31.08 2.91 -4 7 -8 79.07 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22.41 2.62 -4 8 13 28.86 2.49 -4 8 13 28.94 2.63 4 8 -12 2.69 1.07 -4 8 12 4.58 1.11 -4 8 12 2.59 1.00 -4 8 11 76.70 4.33 -4 8 11 87.95 4.78 -4 -8 11 78.89 4.67 4 8 -11 72.61 4.79 -4 8 10 266.88 9.41 4 8 -10 289.64 10.95 -4 8 10 273.36 9.96 -4 8 10 285.63 10.43 -4 -8 10 274.26 10.52 -4 -8 10 296.02 10.63 4 8 -9 107.38 5.85 -4 -8 9 114.24 5.80 -4 8 9 127.75 5.90 -4 8 9 117.66 5.25 -4 -8 9 112.26 5.68 4 8 -8 66.27 4.22 -4 -8 8 62.60 3.97 -4 8 8 67.99 4.08 -4 -8 8 65.21 3.98 -4 8 8 59.33 3.63 -4 -8 7 46.66 3.31 -4 8 7 52.68 3.38 4 8 -7 48.34 3.56 -4 -8 7 48.24 3.33 -4 8 7 47.07 3.37 -4 8 7 45.69 2.74 -4 8 7 52.17 3.12 -4 8 6 376.64 11.77 4 8 -6 364.78 12.58 -4 -8 6 349.94 12.15 -4 -8 6 368.31 12.30 -4 8 6 350.63 12.22 -4 8 5 103.20 4.63 4 8 -5 106.15 5.21 -4 -8 5 105.09 5.00 -4 8 5 101.50 5.12 -4 -8 5 94.04 4.85 4 8 -4 18.40 1.96 -4 8 4 13.45 1.48 -4 8 4 14.89 1.85 -4 -8 4 14.64 1.72 -4 8 3 64.57 3.37 4 8 -3 59.30 3.85 4 8 -3 60.66 3.66 -4 8 3 65.72 3.98 -4 8 3 63.29 3.73 -4 8 2 8.60 1.17 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10 -14 129.99 4.96 -4 10 -14 119.72 5.01 -4 10 -15 1.61 0.42 4 11 -17 1.96 0.56 -4 -11 17 0.90 0.45 -4 -11 17 1.58 0.57 4 11 -16 48.38 2.92 -4 -11 16 53.74 2.91 4 11 -15 5.61 1.07 -4 -11 15 5.94 1.12 4 11 -14 50.07 3.35 -4 -11 14 47.43 3.10 4 11 -13 2.18 0.84 -4 -11 13 1.84 0.77 -4 -11 12 46.78 3.25 4 11 -12 41.96 3.33 4 11 -11 14.12 1.60 -4 -11 11 14.45 1.83 4 11 -11 10.95 1.75 -4 11 10 31.73 2.74 -4 -11 10 25.92 2.48 4 11 -10 29.53 2.84 -4 11 9 31.70 2.42 -4 11 9 27.56 2.64 -4 -11 9 32.87 2.76 4 11 -9 32.52 2.98 -4 11 8 42.56 2.99 4 11 -8 43.46 3.49 -4 11 8 49.49 3.46 -4 -11 8 43.38 3.21 -4 11 7 12.96 1.75 -4 -11 7 10.58 1.59 -4 11 7 13.85 1.66 4 11 -7 12.15 1.86 -4 11 7 14.02 1.88 -4 11 6 60.12 3.46 -4 11 6 63.43 4.11 4 11 -6 72.68 4.45 -4 11 6 68.07 4.17 -4 -11 6 65.48 3.97 -4 11 6 69.43 3.84 -4 11 5 6.27 1.35 -4 11 5 5.28 1.10 -4 11 5 4.77 1.04 -4 11 5 2.30 1.01 4 11 -5 4.97 1.16 -4 -11 5 6.05 1.19 -4 11 4 42.95 3.06 -4 11 4 45.06 3.34 -4 -11 4 41.22 3.00 -4 11 4 44.84 2.99 -4 11 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1.07 0.77 -5 3 14 0.95 0.75 -5 -3 14 1.81 0.93 -5 -3 14 1.17 0.81 -5 3 14 1.15 0.90 5 -3 -14 1.15 0.82 5 3 -14 1.68 0.98 -5 3 14 1.24 0.75 -5 -3 14 0.89 0.67 -5 -3 14 1.37 0.75 -5 -3 13 42.02 3.48 -5 3 13 39.98 3.40 -5 3 13 37.78 2.81 -5 3 13 40.93 3.11 -5 -3 13 42.10 3.02 -5 -3 13 38.49 3.12 5 -3 -13 41.26 3.75 5 3 -13 39.53 3.63 -5 -3 13 42.84 3.37 -5 -3 13 44.50 3.09 -5 3 12 169.34 7.52 -5 -3 12 166.43 7.47 -5 3 12 151.25 6.41 -5 -3 12 161.97 6.96 5 -3 -12 160.55 7.88 5 3 -12 150.33 7.63 -5 -3 12 158.05 6.57 -5 3 12 151.32 6.73 -5 -3 12 157.39 6.68 -5 -3 12 150.88 7.01 -5 -3 11 11.54 1.55 -5 -3 11 11.52 1.63 -5 -3 11 9.44 1.69 -5 3 11 11.62 1.76 5 -3 -11 15.38 2.20 5 3 -11 12.39 1.90 -5 -3 11 12.91 1.79 -5 3 11 9.55 1.40 -5 3 11 11.24 1.45 -5 -3 10 138.22 6.52 -5 3 10 145.40 6.61 -5 -3 10 139.95 6.12 -5 3 10 133.76 5.82 5 -3 -10 137.68 6.88 5 3 -10 133.27 6.83 -5 3 10 137.11 5.84 -5 3 10 136.06 5.59 -5 -3 10 143.60 6.56 5 -3 -9 16.05 2.14 5 3 -9 15.09 2.09 -5 3 9 15.06 1.68 -5 -3 9 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3.63 5 3 3 2.97 1.00 5 -3 3 2.38 0.89 -5 3 -3 2.62 0.77 5 3 3 4.34 1.11 5 -3 3 2.89 0.94 5 3 4 119.22 5.87 5 -3 4 121.82 5.91 -5 3 -4 105.79 5.23 5 3 4 112.47 5.62 5 -3 4 110.41 5.54 5 3 5 6.78 1.41 5 -3 5 5.50 1.33 -5 3 -5 6.74 1.24 5 -3 5 6.78 1.35 5 3 5 7.37 1.39 5 3 6 193.93 8.36 5 -3 6 189.96 8.31 -5 3 -6 182.76 7.52 5 3 6 191.58 8.10 5 -3 6 188.12 8.08 5 3 7 7.21 1.54 5 -3 7 6.29 1.41 5 3 7 7.05 1.48 5 -3 7 7.95 1.58 -5 3 -7 7.41 1.28 -5 3 -8 132.45 6.05 5 -3 8 149.63 6.78 5 3 8 141.17 7.07 5 -3 8 138.62 7.04 5 -3 9 11.68 1.77 5 3 9 11.71 1.93 5 -3 9 10.02 1.81 -5 3 -9 10.02 1.45 5 3 10 39.80 3.54 5 -3 10 43.28 3.75 5 -3 10 42.72 3.80 5 -3 10 47.99 3.53 5 -3 11 8.26 1.49 5 -3 12 22.42 2.36 5 -3 13 30.50 2.62 5 3 13 26.48 2.64 5 -3 13 28.28 2.74 5 -3 14 20.60 2.04 5 3 14 22.77 2.30 5 -3 14 20.00 2.18 5 3 15 0.81 0.54 5 -3 15 1.81 0.70 5 -3 16 26.38 2.11 5 3 16 26.05 2.07 -5 -4 20 3.35 0.76 -5 -4 19 1.66 0.64 -5 4 19 1.40 0.67 -5 -4 19 0.99 0.60 -5 -4 18 135.04 5.87 -5 4 18 138.63 6.05 -5 -4 18 136.89 6.07 -5 -4 17 27.02 2.52 -5 4 17 30.26 2.66 -5 -4 17 23.67 2.25 -5 4 17 28.53 2.59 -5 4 17 26.40 2.15 -5 -4 16 36.40 2.68 -5 -4 16 37.90 2.83 -5 4 16 30.81 2.82 -5 -4 16 35.82 3.02 -5 4 16 31.25 2.85 -5 4 16 32.77 2.54 -5 -4 15 4.09 1.09 -5 -4 15 2.93 0.98 -5 4 15 5.11 1.30 -5 -4 15 6.20 1.39 -5 4 15 3.89 1.19 -5 4 15 4.55 1.06 5 -4 -14 299.02 12.08 5 4 -14 300.42 12.02 -5 4 14 307.63 10.56 -5 -4 14 309.99 10.75 -5 4 14 276.03 10.83 -5 4 14 297.21 11.33 -5 -4 14 295.34 10.75 -5 4 14 305.86 11.42 -5 -4 14 307.35 11.52 -5 -4 14 297.24 11.29 -5 -4 14 313.05 10.83 5 -4 -13 81.04 5.42 5 4 -13 84.23 5.39 -5 4 13 86.26 4.56 -5 -4 13 88.42 4.65 -5 4 13 78.37 4.66 -5 4 13 83.81 4.95 -5 -4 13 89.61 4.76 -5 4 13 101.69 5.38 -5 -4 13 91.67 5.20 -5 -4 13 89.06 5.09 -5 -4 13 90.09 4.80 5 -4 -12 7.44 1.59 5 4 -12 6.47 1.45 -5 -4 12 7.20 1.41 -5 -4 12 6.14 1.37 -5 4 12 5.18 1.34 -5 4 12 5.26 1.18 -5 -4 12 5.98 1.24 -5 -4 12 8.69 1.43 -5 4 12 7.37 1.30 5 -4 -11 14.11 2.18 5 4 -11 16.66 2.30 -5 4 11 18.10 2.25 -5 -4 11 20.16 2.07 -5 -4 11 17.99 2.22 -5 4 11 17.31 1.91 -5 -4 11 17.03 2.11 -5 4 11 19.74 2.00 -5 -4 11 20.10 2.12 -5 -4 10 72.45 4.21 5 -4 -10 73.69 4.76 5 4 -10 74.30 4.74 -5 -4 10 76.47 4.15 -5 4 10 75.23 4.10 -5 4 10 79.04 4.55 -5 -4 10 80.96 4.66 -5 -4 9 41.72 3.06 5 -4 -9 42.51 3.39 5 4 -9 44.48 3.51 -5 4 9 42.78 2.98 -5 4 9 44.67 3.27 -5 -4 9 47.37 3.37 -5 -4 8 156.53 6.85 -5 4 8 158.11 6.84 5 -4 -8 161.69 7.14 5 4 -8 156.06 7.11 -5 4 8 166.98 6.93 -5 -4 8 153.85 6.80 -5 4 8 144.13 6.30 -5 -4 8 144.73 6.44 -5 -4 7 43.27 3.18 -5 4 7 44.14 3.19 5 -4 -7 48.37 3.39 5 4 -7 40.54 3.18 -5 4 7 45.11 3.16 -5 -4 7 39.38 3.04 -5 4 6 81.10 4.48 -5 -4 6 83.59 4.57 5 -4 -6 87.86 4.73 5 4 -6 82.03 4.66 -5 -4 6 89.78 4.63 -5 4 6 83.18 4.53 -5 -4 5 13.64 1.74 -5 4 5 12.88 1.71 5 -4 -5 11.49 1.61 5 4 -5 16.45 1.89 -5 4 5 15.00 1.74 -5 -4 5 13.80 1.75 -5 -4 4 84.36 4.62 -5 4 4 90.55 4.72 5 -4 -4 91.25 4.66 5 4 -4 82.11 4.53 -5 4 4 87.53 4.58 -5 -4 4 90.01 4.63 5 -4 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5 4 8 20.91 2.46 5 -4 8 21.80 2.53 5 -4 8 17.30 1.62 5 4 9 8.62 1.63 5 -4 9 7.20 1.57 5 -4 9 7.29 1.67 5 -4 9 7.91 1.11 -5 4 -9 7.68 1.31 5 -4 9 4.98 1.14 5 -4 10 8.62 1.75 5 4 10 7.33 1.54 5 -4 10 6.91 1.54 -5 4 -10 8.19 1.34 5 4 10 9.64 1.82 5 -4 10 7.31 1.39 -5 4 -11 7.50 1.22 5 4 11 8.64 1.62 5 -4 11 5.17 1.16 5 4 12 2.72 1.09 5 -4 12 3.06 0.89 5 4 13 2.71 1.00 5 -4 13 2.12 0.75 5 4 13 1.17 0.86 5 -4 13 2.37 1.01 5 4 14 5.93 1.23 -5 4 -14 5.63 1.09 5 4 14 5.33 1.24 5 -4 14 5.05 1.11 5 -4 15 24.14 2.11 5 4 15 23.31 2.06 5 4 15 24.40 2.18 5 -4 16 0.34 0.38 -5 -5 20 6.72 0.93 -5 -5 19 5.07 0.91 -5 -5 19 5.19 1.01 -5 -5 18 48.16 3.08 -5 -5 18 55.13 3.24 -5 5 17 5.39 1.05 -5 -5 17 4.14 1.04 -5 -5 17 3.80 0.92 -5 5 17 6.02 1.21 -5 -5 17 4.86 1.12 5 5 -17 4.75 1.01 -5 5 16 5.45 1.13 5 5 -16 5.33 1.10 -5 -5 16 6.21 1.15 -5 5 16 7.76 1.36 -5 -5 16 5.37 1.18 -5 5 16 7.39 1.40 -5 -5 16 7.46 1.26 -5 -5 15 24.84 2.31 -5 5 15 31.14 2.76 -5 5 15 25.43 2.49 -5 -5 15 21.92 2.34 5 5 -15 23.72 2.35 -5 5 15 27.57 2.40 -5 -5 15 22.61 2.26 -5 -5 14 91.01 4.73 5 5 -14 82.45 4.75 5 -5 -14 83.62 5.42 5 5 -14 84.35 5.36 -5 5 14 97.39 4.87 -5 -5 14 96.91 4.99 -5 5 14 97.53 5.28 -5 -5 13 43.22 3.23 -5 -5 13 39.48 3.22 -5 5 13 43.23 3.33 5 5 -13 38.22 3.03 -5 -5 13 38.16 3.26 5 -5 -13 37.30 3.46 5 5 -13 33.36 3.24 -5 5 13 39.60 2.99 -5 5 13 39.92 3.27 -5 -5 13 34.13 2.70 -5 -5 12 77.52 4.65 -5 5 12 76.35 4.59 5 5 -12 76.58 4.44 5 -5 -12 79.12 5.04 5 5 -12 72.93 4.84 -5 5 12 79.04 4.37 -5 -5 12 69.92 3.98 -5 5 12 76.10 4.58 -5 -5 12 74.77 4.38 -5 5 11 48.02 3.29 5 5 -11 42.88 3.19 5 -5 -11 41.91 3.59 5 5 -11 47.80 3.75 -5 -5 11 49.95 3.44 -5 5 11 51.51 3.58 -5 -5 11 49.86 3.56 -5 5 10 244.86 9.18 -5 5 10 258.09 9.54 -5 -5 10 249.30 9.51 5 -5 -10 238.92 9.82 5 5 -10 226.38 9.65 -5 -5 10 242.92 9.35 -5 -5 10 254.63 9.74 -5 -5 9 57.82 4.00 -5 5 9 62.62 3.77 -5 -5 9 62.17 3.84 -5 -5 9 60.76 3.87 -5 5 9 61.89 3.90 5 -5 -9 56.50 3.94 5 5 -9 64.51 4.21 -5 -5 8 251.78 9.41 -5 5 8 255.62 9.40 -5 -5 8 241.94 9.27 5 -5 -8 249.52 9.66 5 5 -8 238.79 9.60 -5 5 8 253.92 9.21 5 -5 -7 88.09 4.87 5 5 -7 91.16 4.95 -5 5 7 92.11 4.81 -5 -5 7 89.72 4.80 -5 5 7 101.49 4.99 -5 -5 7 91.73 4.78 5 -5 -6 203.68 8.16 5 5 -6 200.21 8.14 -5 5 6 205.93 8.06 -5 -5 6 201.32 8.04 -5 5 6 210.73 8.09 -5 -5 6 202.12 8.01 5 -5 -5 30.31 2.58 5 5 -5 35.63 2.81 -5 5 5 28.96 2.52 -5 -5 5 30.41 2.62 -5 5 5 30.38 2.53 -5 -5 5 36.04 2.73 5 -5 -4 86.82 4.61 5 5 -4 90.22 4.72 -5 5 4 92.19 4.73 -5 -5 4 89.12 4.66 -5 -5 4 97.19 4.84 -5 5 4 92.99 4.75 -5 -5 3 14.97 1.85 5 -5 -3 16.20 1.92 5 5 -3 13.12 1.75 -5 5 3 15.16 1.92 -5 5 3 16.86 1.86 5 5 -3 16.27 1.81 -5 -5 2 80.48 4.45 -5 5 2 81.77 4.48 5 5 -2 86.24 4.46 5 -5 -2 83.49 4.39 5 5 -2 85.80 4.45 5 -5 -1 4.28 1.11 5 5 -1 4.33 1.09 -5 5 1 5.23 1.11 -5 -5 1 1.96 0.98 -5 5 1 4.72 1.18 -5 5 0 82.03 4.44 5 5 0 78.66 4.28 5 -5 0 80.56 4.29 -5 -5 0 79.20 4.45 -5 5 0 78.73 4.40 -5 5 -1 50.26 3.41 5 5 1 54.86 3.42 5 -5 1 53.03 3.33 -5 -5 -1 47.84 3.41 -5 5 -1 45.30 3.32 -5 5 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5 12 42.55 3.33 -5 5 -13 14.14 1.75 5 -5 13 15.27 1.82 5 5 13 13.52 1.72 5 5 13 14.73 1.88 5 -5 14 28.37 2.35 5 5 14 34.69 2.68 5 -5 15 25.89 2.00 5 5 15 24.42 2.08 -5 -6 19 1.59 0.58 -5 -6 18 15.03 1.53 -5 -6 18 20.37 1.83 -5 6 17 2.32 0.82 -5 -6 17 2.23 0.70 -5 -6 17 2.65 0.81 -5 -6 17 2.10 0.72 5 6 -17 3.00 0.80 -5 6 16 13.99 1.65 -5 -6 16 13.07 1.60 -5 -6 16 10.85 1.53 -5 -6 16 10.86 1.53 -5 6 16 11.88 1.67 5 6 -16 11.04 1.55 -5 6 15 5.26 1.10 -5 -6 15 7.16 1.31 -5 -6 15 6.94 1.22 5 6 -15 5.86 1.16 -5 6 15 5.40 1.18 -5 -6 15 4.70 1.04 -5 6 15 5.18 1.26 -5 6 14 44.48 3.36 -5 6 14 47.34 3.33 -5 -6 14 49.73 3.35 -5 6 14 46.96 3.26 -5 -6 14 40.31 3.13 5 6 -14 38.12 3.10 -5 -6 13 10.87 1.71 -5 6 13 10.88 1.73 5 6 -13 6.95 1.45 5 6 -13 10.13 1.59 -5 6 13 10.00 1.55 -5 6 12 27.03 2.62 -5 -6 12 28.56 2.70 -5 -6 12 28.51 2.88 -5 -6 12 29.41 2.67 5 -6 -12 32.68 3.06 5 6 -12 34.38 3.09 5 6 -12 29.48 2.67 -5 6 12 31.12 2.66 -5 6 12 33.05 2.88 5 6 -11 16.03 1.95 -5 -6 11 13.59 1.87 -5 -6 11 16.01 1.96 -5 6 11 15.81 1.97 5 -6 -11 13.11 2.01 5 6 -11 15.14 2.06 -5 -6 11 19.09 2.27 -5 6 11 12.94 1.52 -5 6 11 14.82 1.82 5 6 -10 15.46 1.90 -5 -6 10 17.62 2.08 -5 -6 10 16.03 2.06 -5 6 10 17.07 1.94 5 -6 -10 14.51 1.96 5 6 -10 15.05 2.00 -5 6 10 15.77 1.91 -5 -6 10 17.28 2.03 -5 6 9 24.06 2.32 -5 -6 9 20.20 2.18 5 6 -9 22.37 2.18 -5 -6 9 24.38 2.50 -5 6 9 23.29 2.27 5 -6 -9 23.43 2.39 5 6 -9 26.36 2.55 -5 6 8 51.28 3.41 -5 -6 8 55.57 3.54 -5 6 8 53.84 3.53 5 -6 -8 55.10 3.67 5 6 -8 50.29 3.54 -5 -6 8 53.89 3.78 5 6 -8 50.82 3.33 -5 6 7 11.02 1.51 -5 -6 7 9.69 1.47 5 6 -7 9.02 1.32 5 -6 -7 10.27 1.54 5 6 -7 13.16 1.73 -5 -6 7 13.02 1.64 -5 -6 7 11.28 1.60 5 -6 -6 17.24 1.89 5 6 -6 15.92 1.90 -5 6 6 14.83 1.75 -5 -6 6 14.50 1.73 -5 6 6 16.65 1.82 -5 -6 6 19.74 1.97 5 6 -5 0.52 0.43 5 -6 -5 0.52 0.49 -5 6 5 0.66 0.44 -5 -6 5 0.67 0.63 -5 -6 5 1.01 0.53 -5 6 5 1.16 0.62 -5 -6 4 32.10 2.53 -5 6 4 26.72 2.33 5 6 -4 25.51 2.37 -5 6 4 23.42 2.19 -5 -6 4 21.31 2.10 5 -6 -4 23.87 2.23 5 6 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9.85 1.51 5 6 5 10.06 1.56 5 -6 5 8.99 1.58 -5 6 -6 8.01 1.35 5 6 6 6.13 1.43 5 -6 6 11.39 8.42 -5 6 -6 7.63 1.43 -5 6 -6 8.40 1.33 5 -6 7 6.66 1.12 -5 6 -7 4.04 1.02 5 6 7 4.31 1.11 5 -6 7 6.68 1.37 -5 6 -7 5.20 1.08 -5 6 -7 7.40 1.44 -5 6 -8 20.27 2.28 5 -6 8 23.91 2.01 5 6 8 20.11 2.33 5 -6 8 22.76 2.45 5 -6 8 18.57 2.58 -5 6 -8 24.08 2.49 -5 6 -9 21.81 2.32 5 -6 9 23.02 1.97 -5 6 -9 19.00 2.24 5 6 9 25.16 2.65 5 -6 9 19.65 2.61 5 6 10 7.89 1.59 -5 6 -10 7.06 1.39 5 -6 10 8.06 1.16 -5 6 -10 6.82 1.29 5 6 11 19.78 2.27 -5 6 -11 15.59 1.79 -5 6 -11 17.46 2.03 5 -6 12 19.67 2.06 5 6 12 21.91 2.27 -5 6 -12 19.92 1.93 -5 6 -12 23.27 2.27 5 6 13 1.34 0.67 5 -6 13 1.33 0.66 -5 6 -13 2.44 0.77 -5 6 -13 0.80 0.56 5 6 13 1.39 0.78 5 6 14 0.30 0.52 5 -6 14 0.60 0.49 5 6 15 11.74 1.33 -5 -7 19 10.76 1.14 -5 -7 18 9.19 1.14 -5 -7 18 8.82 1.15 -5 -7 17 30.38 2.29 -5 -7 17 28.17 2.21 5 7 -17 27.83 2.21 -5 7 17 34.09 2.37 -5 7 16 34.57 2.58 -5 -7 16 31.12 2.42 -5 -7 16 38.15 2.74 5 7 -16 32.39 2.56 -5 -7 16 33.95 2.36 -5 7 15 21.32 2.15 -5 -7 15 24.62 2.21 -5 7 15 25.91 2.33 -5 -7 15 20.54 1.92 -5 -7 15 21.18 2.17 5 7 -15 21.32 2.17 -5 -7 14 37.27 2.94 -5 7 14 32.08 2.67 5 7 -14 28.12 2.63 -5 7 14 37.20 2.90 -5 -7 14 34.72 2.61 5 7 -13 7.31 1.38 -5 7 13 8.83 1.50 -5 -7 13 7.16 1.23 -5 7 13 6.53 1.32 -5 -7 13 8.92 1.54 -5 7 12 101.38 5.26 -5 7 12 110.71 5.39 -5 -7 12 103.36 5.39 -5 -7 12 96.24 5.50 5 7 -12 92.20 5.19 -5 -7 11 58.70 4.07 -5 7 11 63.44 3.90 -5 7 11 61.76 3.90 -5 -7 11 54.76 3.58 -5 7 11 52.17 3.49 -5 7 11 54.56 3.21 5 7 -11 50.59 3.61 5 7 -10 201.74 8.14 -5 7 10 198.34 7.72 -5 7 10 194.68 8.00 -5 -7 10 188.31 8.31 -5 7 10 189.86 7.44 -5 7 9 81.01 4.57 -5 7 9 79.52 4.32 -5 7 9 79.65 4.28 -5 -7 9 81.60 4.82 -5 -7 9 74.53 4.49 5 7 -9 76.38 4.44 5 7 -9 78.87 4.49 -5 -7 8 168.94 7.32 5 7 -8 169.61 7.11 -5 7 8 170.62 7.31 5 7 -8 161.75 7.02 -5 -7 8 174.83 7.54 -5 -7 7 65.77 4.07 5 7 -7 63.10 3.77 -5 7 7 65.18 3.99 5 7 -7 62.31 3.79 -5 -7 7 61.23 4.03 -5 -7 6 268.58 10.10 5 7 -6 265.19 9.72 5 7 -6 283.70 9.77 -5 7 5 118.95 5.22 5 7 -5 110.06 5.18 5 7 -5 106.46 5.00 -5 7 4 67.53 3.76 5 7 -4 71.68 4.25 5 7 -4 65.58 3.79 5 7 -4 67.15 3.63 -5 7 3 61.18 3.28 -5 7 3 58.46 3.52 5 7 -3 61.37 3.93 5 7 -3 56.70 3.50 5 7 -3 61.68 3.40 -5 7 2 101.62 4.43 -5 7 2 99.62 4.79 5 7 -2 107.48 5.39 5 7 -2 95.83 4.69 5 7 -2 92.56 4.41 5 7 -1 74.28 3.99 -5 7 1 68.45 3.95 5 7 -1 81.61 4.65 -5 7 1 73.43 3.57 5 7 0 97.06 4.65 5 7 0 98.42 5.30 5 7 0 95.77 4.78 -5 7 0 99.42 4.20 5 7 1 34.08 3.05 -5 7 -1 39.80 3.15 5 7 1 40.62 2.94 5 7 1 39.82 2.78 5 7 2 130.82 6.50 5 7 2 132.14 5.71 -5 7 -2 123.82 6.22 5 7 2 125.73 5.79 5 7 3 5.24 1.10 -5 7 -3 3.59 1.07 -5 7 -3 4.85 1.04 5 7 3 4.65 1.11 -5 7 -3 7.56 1.49 5 7 4 228.90 8.43 -5 7 -4 218.13 8.56 -5 7 -4 225.35 9.14 -5 7 -4 225.28 8.54 -5 7 -4 209.19 8.22 5 7 4 209.97 8.44 -5 7 -5 18.88 2.27 -5 7 -5 16.23 1.88 -5 7 -5 15.43 1.86 5 7 5 14.34 1.82 -5 7 -6 207.08 7.96 -5 7 -6 202.66 8.26 -5 7 -6 213.40 8.88 -5 7 -7 6.27 1.40 5 -7 7 9.01 1.77 5 -7 7 9.16 1.37 -5 7 -7 7.30 1.37 -5 7 -7 10.68 1.50 5 7 8 112.04 5.95 -5 7 -8 117.77 5.97 -5 7 -8 117.06 5.84 5 -7 8 116.09 6.56 5 -7 8 115.33 5.15 -5 7 -9 5.16 1.26 5 7 9 4.55 1.20 5 -7 9 5.11 0.97 -5 7 -9 2.68 0.93 5 7 10 97.14 5.24 -5 7 -10 91.93 5.07 5 -7 10 88.56 4.65 -5 7 -10 104.50 5.22 5 7 10 109.07 5.79 5 -7 10 96.89 4.39 -5 7 -11 2.60 0.88 -5 7 -11 1.52 0.74 5 7 11 0.19 0.54 5 7 11 1.04 0.81 -5 7 -12 21.73 2.00 5 7 12 19.74 2.08 5 7 12 23.85 2.26 -5 7 -13 5.61 0.95 5 7 13 4.89 0.97 5 7 13 6.10 1.11 -5 7 -14 14.48 1.18 -5 -8 18 5.86 0.92 -5 -8 18 5.57 0.85 -5 8 17 2.26 0.73 -5 -8 17 1.66 0.58 5 8 -17 1.30 0.52 -5 -8 17 0.12 0.49 -5 8 16 41.96 2.75 5 8 -16 37.12 2.67 -5 -8 16 40.33 2.67 -5 -8 16 43.73 2.86 5 8 -15 25.82 2.33 -5 8 15 29.71 2.43 -5 -8 15 30.90 2.54 -5 8 14 1.38 0.73 -5 8 14 1.43 0.77 5 8 -14 1.31 0.68 -5 -8 14 0.91 0.71 -5 8 13 7.67 1.39 -5 8 13 5.63 1.13 5 8 -13 6.30 1.27 -5 8 12 4.94 1.15 -5 8 12 3.74 1.00 5 8 -12 4.89 1.14 -5 -8 11 19.09 2.27 -5 8 11 19.27 2.16 -5 8 11 19.77 2.11 5 8 -11 19.02 2.18 5 8 -10 160.17 7.15 -5 8 10 171.91 7.30 -5 -8 10 156.07 7.30 -5 8 10 156.22 6.52 -5 -8 10 176.68 7.48 5 8 -9 82.24 4.72 -5 8 9 93.64 5.00 -5 -8 9 87.53 5.03 -5 8 9 89.91 4.64 -5 -8 9 85.88 4.90 5 8 -8 140.11 6.38 -5 8 8 139.31 6.54 -5 -8 8 132.11 6.49 -5 8 8 143.89 6.38 -5 -8 8 148.05 6.64 -5 8 7 40.74 3.14 -5 -8 7 36.19 3.00 -5 8 7 33.68 2.88 -5 -8 7 29.96 2.78 5 8 -7 36.47 2.84 -5 -8 6 283.05 10.61 -5 -8 6 279.65 10.57 -5 8 6 316.53 11.10 5 8 -6 290.50 10.33 -5 -8 5 58.24 3.73 5 8 -5 53.42 3.41 -5 8 5 54.99 3.87 -5 -8 5 53.91 3.62 -5 8 4 33.02 2.91 5 8 -4 30.44 2.42 -5 8 4 27.03 2.23 5 8 -3 16.99 2.11 5 8 -3 16.08 1.73 -5 8 3 15.81 1.65 -5 8 2 48.34 2.89 5 8 -2 45.60 3.50 -5 8 1 5.32 1.17 -5 8 1 4.33 1.17 -5 8 1 4.62 0.88 5 8 -1 3.93 1.14 -5 8 0 32.70 2.84 -5 8 0 29.82 2.16 5 8 0 33.95 3.00 5 8 1 35.90 3.15 -5 8 -1 36.80 3.00 -5 8 -2 1.09 0.76 5 8 2 2.80 1.10 -5 8 -2 3.83 1.04 -5 8 -3 12.06 1.83 -5 8 -3 10.49 1.59 5 8 3 14.97 2.13 -5 8 -4 7.96 1.29 -5 8 -4 7.73 1.61 -5 8 -4 6.75 1.37 5 8 4 7.99 1.63 -5 8 -5 61.68 3.83 -5 8 -5 60.13 4.23 -5 8 -5 67.94 3.91 5 8 5 57.30 4.34 -5 8 -6 49.89 3.73 -5 8 -6 49.14 3.27 5 -8 6 44.92 3.83 -5 8 -6 48.39 3.40 -5 8 -7 59.94 4.07 -5 8 -7 54.61 3.68 5 -8 7 54.90 4.23 -5 8 -7 57.16 3.39 5 8 7 50.87 3.69 5 8 8 61.87 4.01 -5 8 -8 57.21 3.86 -5 8 -8 72.30 4.37 5 8 8 65.52 4.57 5 -8 8 60.95 3.48 -5 8 -9 4.45 1.14 5 8 9 3.83 1.21 -5 8 -9 4.45 1.09 5 -8 9 4.96 0.96 5 8 9 5.75 1.25 -5 8 -10 26.70 2.46 -5 8 -10 34.49 2.77 5 -8 10 31.47 2.25 5 8 10 30.09 2.81 5 8 10 26.92 2.46 5 8 11 46.43 3.38 -5 8 -11 50.39 2.84 -5 8 -11 52.78 3.30 5 8 12 8.98 1.36 -5 8 -12 6.75 1.14 -5 8 -13 0.63 0.50 -5 -9 18 26.49 1.69 -5 9 17 5.61 0.91 -5 -9 17 5.82 0.87 -5 -9 17 6.10 0.94 5 9 -16 28.90 2.16 -5 -9 16 29.53 2.12 -5 9 16 31.21 2.25 -5 -9 16 34.67 2.39 5 9 -15 7.72 1.17 -5 9 15 11.17 1.43 -5 9 14 50.23 3.22 5 9 -14 49.15 3.26 -5 9 13 1.04 0.78 5 9 -13 0.74 0.59 -5 9 12 81.20 4.46 5 9 -12 75.82 4.41 -5 -9 12 80.39 4.59 -5 9 11 5.16 1.19 5 9 -11 5.98 1.24 -5 -9 11 6.59 1.37 5 9 -10 75.55 4.47 -5 9 10 73.51 4.12 -5 9 10 73.94 3.95 -5 9 10 86.09 4.66 -5 -9 10 74.56 4.46 -5 9 9 49.47 3.20 -5 -9 9 42.81 3.41 -5 9 9 45.05 3.36 5 9 -9 45.11 3.31 -5 -9 9 42.62 3.29 -5 9 8 184.47 7.55 -5 -9 8 174.03 7.64 -5 9 8 188.61 7.85 5 9 -8 177.52 7.54 -5 -9 8 182.86 7.72 -5 9 7 62.22 4.00 -5 -9 7 68.25 4.16 -5 9 7 69.02 4.27 5 9 -7 66.43 4.01 -5 9 7 59.15 3.35 -5 -9 7 67.35 4.11 -5 -9 6 52.40 3.62 -5 9 6 55.12 3.79 -5 9 6 52.55 3.75 5 9 -6 55.50 3.55 -5 -9 6 56.96 3.74 -5 9 5 25.49 2.61 5 9 -5 22.53 2.18 -5 -9 5 20.50 2.17 -5 -9 5 22.41 2.29 -5 -9 4 106.04 5.35 -5 9 4 109.30 5.79 -5 9 4 121.72 5.15 -5 -9 4 92.82 5.04 5 9 -4 107.46 5.13 -5 -9 3 59.48 3.79 -5 -9 3 61.49 3.85 5 9 -3 65.56 3.79 -5 9 3 65.85 3.58 -5 9 2 56.53 3.23 5 9 -2 56.19 3.99 -5 9 1 72.67 4.40 -5 9 1 68.43 3.58 -5 9 1 65.26 4.33 5 9 -1 75.57 4.70 -5 9 0 52.57 3.78 -5 9 0 55.10 3.05 -5 9 0 50.39 3.75 5 9 0 50.56 3.84 -5 9 -1 47.37 3.64 5 9 1 56.95 4.06 -5 9 -1 49.88 3.58 -5 9 -1 51.74 2.88 5 9 2 115.72 6.19 -5 9 -2 110.41 5.65 5 9 3 20.12 2.48 -5 9 -3 23.46 2.35 -5 9 -4 62.62 3.78 5 9 4 72.65 4.79 5 -9 4 62.37 4.39 -5 9 -4 69.76 4.49 -5 9 -4 70.91 4.12 -5 9 -5 0.71 0.56 5 9 5 0.26 0.78 -5 9 -5 0.68 0.72 -5 9 -5 1.92 0.84 5 -9 5 1.20 0.68 -5 9 -6 102.13 5.65 5 9 6 107.55 5.35 -5 9 -6 113.20 5.19 -5 9 -6 106.69 5.29 -5 9 -7 13.51 1.92 -5 9 -7 16.06 1.69 5 9 8 106.56 5.82 -5 9 -8 97.88 5.26 5 -9 8 92.75 4.51 5 9 9 1.56 0.78 5 -9 9 0.53 0.55 -5 9 -9 0.38 0.54 -5 9 -10 28.54 2.20 -5 9 -10 28.60 2.48 5 9 10 33.48 2.84 5 -9 10 33.18 2.24 5 9 11 29.58 2.48 -5 9 -11 31.03 2.38 5 9 12 38.03 2.61 -5 9 -12 44.41 2.64 -5 9 -13 20.80 1.56 -5 -10 18 3.01 0.52 -5 -10 17 32.23 1.96 -5 10 16 0.64 0.51 -5 -10 16 0.76 0.41 5 10 -16 0.97 0.44 5 10 -15 13.03 1.40 -5 10 15 16.30 1.63 5 10 -14 0.72 0.58 -5 10 14 0.14 0.52 -5 -10 14 -0.15 0.57 5 10 -13 6.78 1.18 -5 10 13 7.03 1.24 -5 -10 13 7.49 1.29 5 10 -12 11.72 1.57 -5 10 12 14.61 1.77 -5 -10 12 9.44 1.49 5 10 -11 5.71 1.22 -5 10 11 4.91 1.19 -5 -10 11 5.22 1.20 -5 10 10 24.64 2.43 -5 -10 10 27.09 2.51 5 10 -10 25.83 2.44 -5 -10 9 77.93 4.38 5 10 -9 71.87 4.22 -5 10 9 71.94 4.30 -5 10 9 64.68 3.77 5 10 -8 4.15 1.04 -5 10 8 5.83 1.28 -5 10 8 5.49 1.17 -5 -10 8 4.99 1.21 -5 10 7 3.50 1.03 -5 -10 7 1.52 0.74 -5 -10 7 3.90 1.06 5 10 -7 2.40 0.83 -5 10 7 1.85 0.88 5 10 -6 51.45 3.45 -5 -10 6 44.65 3.29 -5 -10 6 57.12 3.63 -5 10 6 46.39 3.02 -5 10 6 61.64 3.92 -5 -10 5 164.94 6.94 -5 10 5 145.99 6.37 -5 10 5 150.17 7.16 5 10 -5 163.71 6.80 -5 -10 4 0.37 0.52 -5 10 4 0.60 0.64 5 10 -4 0.70 0.74 -5 10 3 38.21 2.64 -5 -10 3 35.27 2.82 -5 10 2 15.38 1.63 -5 -10 2 14.56 1.81 -5 -10 1 56.86 3.65 -5 10 1 56.52 4.00 5 10 -1 60.34 4.20 -5 10 1 59.51 3.30 -5 10 0 36.95 2.50 -5 -10 0 37.86 2.90 5 10 0 37.04 3.28 -5 10 0 38.85 3.18 -5 10 -1 51.20 2.93 -5 10 -1 58.92 3.95 5 10 1 53.32 4.03 -5 10 -1 54.05 3.75 -5 -10 -1 56.31 3.57 5 10 2 33.61 3.14 -5 10 -2 33.72 2.85 -5 10 -2 32.78 2.94 5 10 3 10.48 1.83 -5 10 -3 14.16 1.80 5 10 4 37.60 3.37 -5 10 -4 35.77 2.82 -5 10 -5 14.72 1.74 -5 10 -5 12.70 1.87 -5 10 -6 97.13 4.62 -5 10 -6 92.46 5.20 5 10 7 17.98 2.35 5 -10 7 22.21 2.03 -5 10 -7 23.09 1.95 5 10 8 6.25 1.41 -5 10 -8 7.58 1.35 5 -10 8 6.10 1.06 -5 10 -8 7.94 1.23 5 10 9 2.60 0.92 -5 10 -9 1.55 0.73 -5 10 -9 1.31 0.59 5 -10 9 2.69 0.71 -5 10 -10 32.45 2.19 5 -10 10 36.44 2.27 5 10 10 40.91 2.90 -5 10 -10 38.61 2.69 5 10 11 19.43 1.86 -5 10 -11 21.76 1.85 -5 10 -12 5.79 0.89 -5 10 -13 6.91 0.79 -5 11 16 39.17 2.15 -5 -11 16 39.04 2.18 -5 -11 15 6.09 0.82 -5 11 15 6.56 0.98 -5 -11 15 9.20 1.14 5 11 -15 6.13 0.85 -5 -11 14 80.52 3.81 -5 11 14 79.76 3.74 5 11 -13 2.29 0.68 -5 11 13 3.08 0.87 -5 -11 13 4.70 1.01 -5 11 12 70.16 3.80 -5 -11 12 68.05 3.79 5 11 -12 59.23 3.52 -5 11 11 26.83 2.39 5 11 -11 21.11 2.08 -5 -11 11 23.90 2.19 5 11 -10 94.78 4.81 -5 -11 10 96.66 4.84 5 11 -9 25.49 2.34 -5 -11 9 23.31 2.28 5 11 -8 93.60 4.79 -5 11 8 89.51 4.57 -5 -11 8 88.95 4.73 5 11 -7 12.96 1.69 -5 11 7 13.16 1.74 -5 -11 7 10.26 1.51 -5 -11 6 98.97 5.00 -5 11 6 93.86 5.13 5 11 -6 102.15 5.06 -5 11 5 9.63 1.38 -5 11 5 7.85 1.55 5 11 -5 10.19 1.52 -5 -11 5 9.83 1.48 5 11 -4 66.41 3.94 -5 11 4 75.07 4.40 -5 11 4 71.07 4.45 -5 11 4 75.67 3.88 -5 -11 4 68.82 4.01 -5 11 4 62.49 3.79 -5 11 3 7.15 1.31 -5 11 3 6.51 1.12 -5 11 3 6.92 1.46 -5 -11 3 4.68 1.11 -5 11 2 99.23 4.56 -5 11 2 89.44 4.95 -5 -11 2 97.26 4.86 -5 -11 1 6.59 1.21 -5 11 1 7.67 1.16 -5 11 1 9.27 1.64 -5 -11 0 85.06 4.42 -5 11 0 77.87 4.76 -5 11 0 89.11 4.08 -5 11 -1 6.97 1.31 -5 11 -1 6.40 1.01 -5 11 -1 5.79 1.28 -5 11 -2 86.26 4.78 -5 11 -2 74.52 3.56 5 11 2 74.84 4.82 -5 11 -2 80.12 4.49 5 11 3 13.01 2.03 -5 11 -3 12.48 1.79 -5 11 -3 14.35 1.79 5 11 4 64.31 4.39 -5 11 -4 66.63 3.85 -5 11 -5 14.89 1.69 -5 11 -6 71.39 4.08 -5 11 -6 83.31 3.99 5 11 7 30.38 2.78 -5 11 -7 28.15 2.31 -5 11 -7 32.04 2.69 5 -11 7 30.39 2.28 -5 11 -7 31.26 2.14 5 -11 8 69.86 3.48 -5 11 -8 61.88 3.43 -5 11 -8 70.56 3.90 5 11 8 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36.64 2.54 -8 -4 4 41.85 3.22 -8 4 4 36.96 3.08 -8 -4 3 1.44 1.03 -8 4 3 0.82 0.94 8 4 -2 8.91 1.55 8 -4 -2 7.35 1.37 -8 -4 2 5.36 1.32 -8 4 2 4.50 1.29 8 4 -1 2.93 1.02 8 -4 -1 1.72 0.79 -8 -4 1 3.07 1.09 -8 4 1 1.22 0.98 8 4 0 37.99 3.02 8 -4 0 43.93 3.21 8 4 0 38.52 2.70 -8 -4 0 40.93 3.22 -8 4 0 38.71 3.14 8 4 1 8.06 1.42 8 -4 1 6.83 1.32 8 4 1 8.15 1.29 -8 -4 -1 7.93 1.50 -8 4 -1 6.71 1.47 8 4 2 9.07 1.42 8 -4 2 5.73 1.20 -8 4 -2 6.33 1.27 -8 -4 -2 5.57 1.20 8 4 2 7.43 1.23 8 4 3 10.91 1.51 8 -4 3 10.44 1.51 -8 4 -3 10.20 1.32 8 4 3 10.39 1.46 -8 4 -3 14.65 1.83 -8 -4 -3 11.76 1.65 -8 -4 -4 14.34 1.75 -8 4 -4 17.66 1.95 -8 4 -4 13.85 1.40 8 4 4 16.08 1.78 -8 -4 -5 29.24 2.40 -8 4 -5 29.10 2.39 8 4 5 28.63 2.38 -8 -4 -6 110.26 4.98 -8 4 -6 108.31 4.95 8 4 6 118.81 5.09 -8 -4 -7 74.30 3.64 8 4 7 78.88 3.81 -8 -4 -8 100.86 4.13 8 4 8 102.02 4.29 -8 -4 -9 36.34 1.90 8 4 9 35.30 2.07 -8 -5 15 19.38 1.27 -8 5 15 23.66 1.63 -8 5 14 27.41 1.96 -8 -5 14 24.33 1.66 -8 5 13 21.77 1.87 -8 -5 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4.21 8 -5 2 78.50 4.18 8 5 2 74.64 4.09 -8 -5 -3 32.89 2.55 -8 5 -3 33.09 2.29 8 5 3 32.16 2.51 -8 -5 -4 49.65 3.03 8 5 4 48.67 3.06 -8 -5 -5 62.43 3.37 8 5 5 61.29 3.48 -8 -5 -6 42.50 2.60 8 5 6 47.64 2.85 8 5 6 42.69 2.82 8 5 7 22.34 1.80 8 5 7 21.66 1.83 -8 -5 -7 20.45 1.57 -8 -5 -8 29.29 1.68 8 5 8 35.59 2.13 8 5 9 14.82 1.20 -8 6 15 22.20 1.42 -8 6 14 101.99 4.03 -8 -6 13 7.27 0.84 -8 6 13 7.51 1.06 -8 -6 12 44.92 2.52 -8 6 12 45.56 2.69 -8 -6 12 40.45 2.27 -8 -6 11 2.84 0.80 -8 -6 11 3.28 0.74 -8 6 11 3.61 0.93 -8 -6 10 143.34 5.59 -8 -6 10 133.80 5.36 -8 6 10 129.45 4.88 -8 6 9 10.96 1.40 -8 -6 9 9.95 1.34 -8 6 9 12.67 1.28 -8 -6 9 9.70 1.31 -8 -6 8 80.75 4.04 -8 -6 8 82.19 4.18 -8 6 8 77.19 4.13 -8 6 8 84.34 3.77 -8 -6 7 35.16 2.57 -8 6 7 39.58 2.47 -8 -6 7 38.03 2.75 -8 -6 6 58.79 3.41 -8 6 6 54.17 3.12 -8 6 5 9.70 1.30 -8 -6 5 8.50 1.39 8 -6 -5 6.35 1.31 -8 6 4 25.72 2.14 -8 -6 4 25.70 2.27 -8 -6 4 26.60 2.36 8 -6 -4 26.31 2.26 8 -6 -3 2.82 1.03 -8 -6 3 2.49 0.99 8 -6 -2 46.47 3.03 -8 -6 2 43.05 3.00 -8 6 1 47.38 3.14 -8 -6 1 38.57 2.77 8 -6 -1 38.69 2.74 8 6 0 41.58 2.74 -8 -6 0 48.17 3.01 8 -6 0 40.72 2.76 -8 6 0 46.76 3.10 8 6 1 67.93 3.68 -8 -6 -1 69.14 3.72 8 -6 1 63.53 3.53 -8 6 -1 68.75 3.76 -8 6 -2 84.47 4.10 8 6 2 89.78 4.33 -8 -6 -2 85.62 4.16 -8 6 -3 33.88 2.26 8 6 3 35.12 2.57 -8 -6 -3 37.11 2.45 8 6 4 80.48 4.00 -8 -6 -4 76.92 3.65 8 6 5 10.05 1.33 8 6 5 10.09 1.29 -8 -6 -5 10.34 1.13 8 6 6 41.86 2.57 -8 -6 -6 35.91 2.00 8 6 6 44.03 2.59 8 6 7 32.83 2.11 8 6 8 43.88 2.28 -8 -7 13 15.12 1.21 -8 -7 12 61.14 2.92 -8 7 12 59.89 2.96 -8 -7 11 2.18 0.70 -8 7 11 3.78 0.80 -8 7 11 4.12 0.67 -8 7 10 43.88 2.66 -8 -7 10 43.59 2.63 -8 7 10 39.69 2.21 -8 -7 9 10.67 1.33 -8 7 9 11.20 1.18 -8 7 8 45.75 2.60 -8 7 8 44.12 2.83 -8 7 7 7.07 1.03 -8 7 7 6.16 1.15 -8 7 6 85.34 4.49 -8 7 6 89.83 4.14 -8 -7 6 93.95 4.55 -8 7 5 15.01 1.81 -8 7 5 15.70 1.63 -8 -7 5 16.10 1.78 -8 7 4 88.42 4.24 -8 -7 4 87.22 4.42 -8 7 3 34.19 2.73 -8 7 3 36.80 2.56 -8 -7 3 35.32 2.68 -8 7 2 81.48 4.34 -8 -7 2 80.11 4.20 -8 7 1 7.23 1.33 -8 7 0 143.14 5.95 -8 7 -1 25.56 2.13 8 7 1 28.50 2.18 -8 7 -2 58.29 3.15 8 7 2 62.31 3.38 -8 7 -3 4.16 0.78 8 7 3 4.18 0.89 8 7 4 82.79 3.98 8 7 4 83.31 3.93 8 7 5 3.43 0.78 8 7 5 4.56 0.84 8 7 6 44.04 2.48 8 7 7 2.50 0.56 -8 -8 13 30.93 1.65 -8 -8 12 132.04 4.72 -8 -8 11 16.72 1.43 -8 8 11 15.41 1.13 -8 8 10 71.65 3.06 -8 8 9 5.05 0.82 -8 8 8 62.12 3.23 -8 8 8 66.52 3.13 -8 -8 8 62.01 3.30 -8 8 7 4.97 1.01 -8 8 7 6.10 0.98 -8 -8 7 5.79 1.04 -8 8 6 60.55 3.44 -8 8 6 66.31 3.30 -8 -8 6 61.40 3.41 -8 8 5 5.26 0.94 -8 -8 5 4.87 1.00 -8 8 5 4.76 1.07 -8 8 4 37.01 2.45 -8 -8 4 36.20 2.54 -8 8 3 1.29 0.62 -8 -8 3 0.84 0.65 -8 8 3 0.61 0.66 -8 8 2 55.42 3.27 -8 -8 2 57.50 3.22 -8 8 2 46.44 2.88 -8 8 1 37.76 2.65 -8 -8 1 40.81 2.66 -8 8 0 125.84 5.25 -8 -8 0 125.26 5.25 -8 8 -1 51.81 2.91 -8 -8 -1 52.04 2.93 -8 8 -2 151.27 5.44 -8 -8 -2 137.06 5.42 -8 -8 -3 57.09 2.80 -8 -8 -4 50.49 2.40 -8 -9 12 14.87 1.10 -8 9 10 42.02 2.04 -8 9 9 16.32 1.31 -8 -9 9 17.92 1.51 -8 9 8 48.39 2.46 -8 -9 8 46.63 2.62 -8 9 7 8.41 1.09 -8 9 7 10.31 1.11 -8 -9 7 8.15 1.10 -8 9 6 28.71 2.11 -8 9 6 32.83 2.08 -8 -9 6 29.39 2.09 -8 9 5 0.63 0.55 -8 -9 5 0.71 0.52 -8 9 5 1.51 0.59 -8 9 4 60.03 3.06 -8 -9 4 56.79 3.08 -8 9 3 2.75 0.71 -8 -9 3 4.50 0.87 -8 9 3 3.12 0.85 -8 9 2 41.33 2.56 -8 9 2 48.50 2.82 -8 -9 2 43.52 2.60 -8 9 1 1.92 0.69 -8 -9 1 4.00 0.81 -8 9 1 3.53 0.80 -8 9 0 62.43 3.17 -8 -9 0 62.22 3.07 -8 9 -1 14.93 1.36 -8 -9 -1 14.77 1.34 -8 -9 -2 54.03 2.53 -8 -9 -3 7.42 0.72 -8 -10 11 2.58 0.43 -8 -10 10 51.32 2.30 -8 -10 9 7.79 0.88 -8 10 9 8.04 0.79 -8 -10 8 40.58 2.14 -8 10 8 36.51 1.94 -8 -10 7 8.53 0.98 -8 10 7 7.82 0.88 -8 10 6 33.21 2.04 -8 10 6 32.77 1.96 -8 -10 6 36.34 2.09 -8 10 5 3.94 0.77 -8 -10 5 4.95 0.79 -8 10 5 4.41 0.75 -8 -10 4 24.91 1.73 -8 10 4 23.70 1.69 -8 10 3 9.18 1.13 -8 -10 3 11.93 1.18 -8 10 3 10.55 1.14 -8 10 2 17.06 1.48 -8 -10 2 17.46 1.41 -8 10 2 17.08 1.44 -8 10 1 24.07 1.70 -8 10 1 19.40 1.54 -8 -10 1 21.12 1.50 -8 10 0 51.34 2.67 -8 -10 0 58.96 2.51 -8 10 -1 7.06 0.88 -8 10 -2 13.42 1.15 -8 10 -3 12.19 1.02 -8 10 -4 22.19 1.28 -8 11 7 8.19 0.78 -8 -11 7 10.31 0.87 -8 11 6 1.44 0.39 -8 -11 6 2.13 0.44 -8 11 5 1.89 0.47 -8 -11 5 1.98 0.44 -8 11 4 4.46 0.67 -8 -11 4 3.49 0.54 -8 -11 3 0.99 0.33 -8 11 3 0.86 0.38 -8 11 2 6.82 0.81 -8 11 1 1.67 0.44 -8 11 0 4.09 0.61 -8 11 -1 2.62 0.47 -9 0 14 25.63 1.60 -9 0 13 -0.14 0.34 -9 0 12 12.06 1.31 -9 0 12 10.46 1.10 -9 0 11 0.20 0.45 -9 0 11 0.13 0.49 -9 0 10 5.09 0.92 -9 0 10 5.60 1.09 -9 0 9 -0.15 0.53 -9 0 8 7.53 1.32 -9 0 7 -0.16 0.58 -9 0 6 31.71 2.59 -9 0 5 -0.34 0.96 9 0 -4 33.20 2.65 -9 0 4 26.95 2.45 -9 0 3 -0.34 0.98 9 0 -2 83.83 4.44 -9 0 2 81.15 4.40 9 0 -1 -0.33 0.64 -9 0 1 0.17 0.65 9 0 0 113.67 5.28 -9 0 0 113.43 5.29 9 0 1 0.30 0.48 -9 0 -1 0.47 0.63 9 0 2 118.65 5.22 -9 0 -2 116.74 5.21 -9 0 -3 0.13 0.49 -9 0 -4 20.04 1.74 -9 0 -5 0.21 0.34 -9 0 -6 9.04 0.96 -9 -1 14 40.83 2.00 -9 1 14 32.57 1.72 -9 -1 13 1.64 0.41 -9 1 13 1.33 0.48 -9 -1 12 25.57 1.88 -9 -1 12 22.49 1.49 -9 1 12 23.37 1.70 -9 -1 11 0.12 0.52 -9 -1 11 1.94 0.56 -9 1 11 1.81 0.62 -9 -1 10 24.27 2.07 -9 -1 10 22.69 1.74 -9 1 10 25.95 1.97 -9 -1 9 1.00 0.69 -9 -1 9 1.08 0.59 -9 -1 8 67.44 3.73 -9 -1 7 0.63 0.67 -9 -1 6 61.45 3.70 -9 -1 5 0.33 0.90 -9 -1 4 84.72 4.55 9 -1 -4 89.97 4.61 -9 -1 3 -0.34 1.02 9 -1 -3 1.00 0.85 -9 -1 2 93.47 4.79 9 -1 -2 96.22 4.78 -9 -1 1 4.97 1.16 9 -1 -1 3.70 0.95 -9 -1 0 56.98 3.49 9 -1 0 59.15 3.51 -9 -1 -1 3.53 0.93 9 -1 1 3.73 0.90 -9 -1 -2 69.97 3.70 9 -1 2 62.29 3.52 -9 -1 -3 0.79 0.59 9 1 4 28.00 2.01 -9 -1 -4 30.27 2.13 -9 -1 -5 0.50 0.45 -9 -1 -6 30.73 1.83 -9 2 14 3.60 0.57 -9 2 14 3.73 0.55 -9 -2 14 3.90 0.58 -9 2 13 5.19 0.75 -9 2 12 4.47 0.78 -9 2 12 4.29 0.78 -9 -2 12 5.07 0.87 -9 -2 11 6.39 0.76 -9 2 11 6.47 1.03 -9 2 11 6.49 1.01 -9 -2 11 4.96 0.89 -9 -2 10 9.66 0.99 -9 2 10 9.00 1.20 -9 2 10 12.16 1.39 -9 -2 10 10.26 1.34 -9 -2 9 19.61 1.51 -9 2 9 21.04 1.91 -9 -2 9 21.50 1.92 -9 -2 8 10.67 1.15 -9 2 8 9.27 1.35 -9 -2 8 10.92 1.44 -9 2 7 8.04 1.27 -9 -2 7 6.75 1.23 -9 2 6 1.39 0.78 -9 -2 6 2.96 0.91 -9 2 5 18.85 2.00 -9 -2 5 15.01 1.84 -9 -2 5 17.31 1.62 9 2 -5 19.41 1.98 9 -2 -5 17.33 1.91 -9 2 4 0.32 0.77 -9 -2 4 1.13 0.87 9 2 -4 -0.32 0.90 9 -2 -4 0.79 0.90 -9 -2 3 26.75 2.38 -9 2 3 29.26 2.47 9 2 -3 29.80 2.49 9 -2 -3 29.66 2.47 -9 -2 2 9.34 1.46 -9 2 2 11.50 1.56 9 2 -2 10.14 1.49 9 -2 -2 10.75 1.51 -9 -2 1 20.35 2.06 -9 2 1 23.76 2.16 9 2 -1 18.74 1.92 9 -2 -1 23.92 2.12 -9 -2 0 22.78 2.06 -9 2 0 21.82 2.02 9 2 0 20.22 1.95 9 -2 0 20.04 1.94 -9 -2 -1 13.69 1.56 -9 2 -1 11.98 1.47 9 -2 1 11.37 1.42 9 2 1 10.12 1.38 -9 -2 -2 5.15 0.97 -9 2 -2 5.65 1.02 -9 -2 -3 11.49 1.34 -9 2 -3 13.99 1.46 9 2 4 4.67 0.84 -9 -2 -4 5.43 0.89 -9 2 -4 5.84 0.91 -9 -2 -5 5.54 0.80 -9 2 -5 6.62 0.87 -9 -2 -6 0.07 0.26 -9 2 -6 0.21 0.27 -9 3 14 20.29 1.24 -9 -3 13 -0.13 0.37 -9 3 13 0.30 0.34 -9 -3 12 23.42 1.65 -9 3 12 24.67 1.71 -9 3 11 9.57 1.14 -9 -3 11 10.35 1.20 -9 3 11 11.25 1.26 -9 3 10 73.90 3.57 -9 -3 10 75.04 3.59 -9 3 10 78.44 3.66 -9 3 9 28.69 2.12 -9 -3 9 27.97 2.13 -9 3 8 30.03 2.24 -9 -3 8 30.50 2.28 -9 -3 7 37.13 2.59 -9 3 7 37.56 2.56 9 3 -6 96.45 4.74 9 -3 -6 107.68 4.93 -9 -3 6 111.34 4.58 -9 3 6 108.88 4.89 -9 -3 6 108.31 4.91 9 3 -5 21.79 2.09 9 -3 -5 24.43 2.20 -9 -3 5 25.34 1.99 -9 3 5 23.51 2.16 -9 -3 5 26.57 2.26 9 3 -4 65.98 3.66 9 -3 -4 64.40 3.58 -9 -3 4 56.93 3.20 -9 3 4 58.64 3.48 -9 -3 4 54.45 3.40 9 3 -3 4.88 1.19 9 -3 -3 4.06 1.22 -9 3 3 7.22 1.33 -9 -3 3 7.45 1.35 9 3 -2 64.92 3.68 9 -3 -2 65.32 3.64 -9 -3 2 64.42 3.67 -9 3 2 67.97 3.72 9 3 -1 3.13 0.93 9 -3 -1 1.39 0.75 -9 -3 1 2.31 0.87 -9 3 1 4.71 1.02 9 3 0 74.65 3.81 9 -3 0 75.05 3.80 -9 -3 0 72.63 3.81 -9 3 0 75.58 3.85 -9 3 -1 0.20 0.43 -9 -3 -1 0.26 0.49 -9 3 -1 0.39 0.50 9 -3 1 0.63 0.58 9 3 1 0.65 0.50 -9 -3 -2 36.19 2.43 -9 3 -2 40.01 2.53 -9 -3 -3 0.43 0.48 -9 3 -3 1.61 0.55 -9 -3 -4 24.80 1.75 -9 3 -4 26.32 1.77 -9 -3 -5 0.37 0.31 -9 4 13 1.65 0.46 -9 4 12 10.12 1.05 -9 -4 12 9.06 0.88 -9 -4 11 10.99 1.09 -9 4 11 10.99 1.16 -9 -4 10 34.46 2.13 -9 4 10 39.47 2.33 -9 -4 9 22.50 1.75 -9 -4 8 18.59 1.65 -9 -4 7 47.55 2.79 9 4 -7 46.49 2.75 9 -4 -7 43.81 2.70 -9 -4 7 44.67 2.53 -9 -4 6 10.45 1.24 -9 4 6 12.68 1.41 -9 -4 6 11.10 1.33 9 4 -6 9.66 1.33 9 -4 -6 10.37 1.38 9 4 -5 26.86 2.19 9 -4 -5 29.98 2.30 -9 4 5 31.45 2.26 -9 -4 5 30.46 2.26 -9 -4 5 32.24 2.20 9 4 -4 12.17 1.50 9 -4 -4 13.23 1.55 -9 4 4 13.89 1.53 -9 -4 4 12.74 1.51 -9 -4 4 13.72 1.45 9 4 -3 6.26 1.19 9 -4 -3 7.64 1.25 -9 4 3 7.04 1.20 -9 -4 3 6.50 1.14 -9 -4 3 10.07 1.27 -9 4 2 15.85 1.58 -9 -4 2 11.69 1.41 9 4 -2 10.78 1.39 9 -4 -2 13.00 1.50 9 4 -1 1.49 0.80 9 -4 -1 2.42 0.82 -9 4 1 1.85 0.68 -9 -4 0 10.12 1.27 9 4 0 15.18 1.50 9 -4 0 11.51 1.34 -9 4 0 12.41 1.30 -9 -4 -1 3.78 0.76 -9 4 -1 3.19 0.66 -9 -4 -2 7.55 1.00 -9 -4 -3 7.94 0.95 -9 -4 -4 0.28 0.32 -9 -5 10 77.93 3.11 -9 -5 9 2.58 0.58 -9 5 8 194.08 6.82 -9 -5 8 214.24 6.86 -9 -5 8 202.14 6.74 -9 5 7 25.22 1.88 -9 -5 7 24.90 1.77 -9 -5 7 24.25 1.80 9 -5 -6 115.93 4.82 -9 5 6 126.68 5.07 -9 -5 6 126.71 4.84 -9 -5 6 131.58 4.99 9 -5 -5 1.15 0.98 -9 -5 5 2.69 0.79 -9 5 4 185.27 6.91 9 -5 -4 198.34 6.74 -9 -5 4 191.67 6.67 -9 -5 4 190.00 6.82 9 -5 -3 2.91 0.97 -9 -5 3 4.60 0.90 -9 5 2 162.47 5.88 9 -5 -2 143.37 5.49 -9 -5 2 150.82 5.58 -9 5 1 0.64 0.48 -9 -5 1 1.38 0.61 -9 5 0 120.58 4.66 -9 -5 0 122.69 4.65 -9 -5 -1 5.73 0.81 -9 -5 -2 100.28 3.72 -9 6 11 0.74 0.35 -9 6 10 1.50 0.48 -9 -6 9 9.23 0.96 -9 6 9 9.60 1.06 -9 -6 8 0.08 0.33 -9 -6 7 23.64 1.66 -9 6 7 20.22 1.59 -9 -6 6 25.32 1.74 -9 6 6 24.31 1.77 -9 -6 5 4.44 0.74 -9 6 4 18.08 1.57 -9 -6 4 14.31 1.19 -9 -6 3 0.31 0.43 -9 6 3 0.64 0.48 -9 -6 3 -0.55 0.66 -9 -6 2 28.09 1.96 -9 6 2 30.95 2.02 -9 -6 1 6.38 0.92 -9 6 1 6.13 0.87 -9 -6 0 29.60 1.92 -9 -6 -1 12.34 1.16 -9 -6 -2 3.83 0.65 -9 -6 -3 5.86 0.69 -9 -7 9 11.12 0.94 -9 -7 8 46.16 2.23 -9 -7 5 32.14 1.94 -9 -7 4 32.71 1.94 -9 7 4 27.89 1.86 -9 -7 3 30.20 1.89 -9 -7 2 39.59 2.17 -9 -7 1 11.99 1.14 -9 -7 0 25.82 1.60 -9 -7 -1 19.64 1.30 -9 -8 6 43.54 2.07 -9 -8 5 4.49 0.63 -9 -8 4 31.18 1.74 -9 -8 3 5.45 0.69 -9 -8 2 55.54 2.41 -9 -8 1 11.23 0.92 -10 0 7 0.27 0.32 -10 0 6 1.57 0.44 -10 0 5 0.15 0.30 -10 0 4 0.15 0.30 -10 0 3 0.22 0.33 -10 0 2 2.89 0.53 -10 0 1 0.81 0.33 -10 1 7 25.36 1.53 -10 -1 7 31.70 1.67 -10 1 6 38.89 1.99 -10 -1 6 38.68 2.01 -10 -1 5 17.49 1.34 -10 -1 4 14.48 1.22 -10 -1 3 17.91 1.33 -10 -1 2 23.05 1.45 -10 2 5 9.92 0.96 -10 -2 5 8.88 0.94 -10 2 4 106.65 3.82 -10 -2 4 110.11 3.87 -10 -2 3 6.80 0.83 0 0 0 0.00 0.00 TITL 230329_mi_01_14_01_autored in P2/c REM P2/c (#13 in standard setting) CELL 1.54184 8.000324 15.144691 18.914070 90.0000 100.6050 90.0000 ZERR 4.00 0.000096 0.000180 0.000224 0.0000 0.0012 0.0000 LATT 1 SYMM -x, y,-z+1/2 SFAC C H N O S UNIT 92.00 108.00 20.00 16.00 4.00 SIZE 0.11 0.30 0.40 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 81358 _shelx_res_file ; TITL 230329_mi_01_14_01_autored_a.res in Pc 230329_mi_01_14_01_autored.res created by SHELXL-2018/3 at 14:53:45 on 24-Oct-2023 REM Old TITL 230329_mi_01_14_01_autored in P2/c REM SHELXT solution in Pc: R1 0.080, Rweak 0.016, Alpha 0.004 REM 1.202 for 175 systematic absences, Orientation as input REM Flack x = 0.490 ( 0.009 ) from 2204 Parsons' quotients REM Formula found by SHELXT: C50 N13 O8 S2 CELL 1.54184 8.000324 15.144691 18.91407 90 100.605 90 ZERR 4 0.000096 0.00018 0.000224 0 0.0012 0 LATT -1 SYMM +X,-Y,0.5+Z SFAC C H N O S UNIT 92 108 20 16 4 DFIX 0.86 H18 N18 DFIX 0.86 H14 N14 L.S. 10 PLAN 1 TEMP -173.15 CONF MORE -1 BOND $H fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 REM REM REM WGHT 0.046300 0.554800 BASF 0.47755 FVAR 0.38636 S1 5 0.177723 0.499207 0.375570 11.00000 0.01346 0.01210 = 0.01791 0.00117 0.00430 0.00213 S2 5 0.889377 0.997247 0.367632 11.00000 0.01402 0.01129 = 0.02699 -0.00044 0.00834 -0.00125 O5 4 0.086758 0.467277 0.430375 11.00000 0.02209 0.01701 = 0.02284 -0.00032 0.01042 0.00074 O10 4 0.308037 0.754131 0.368535 11.00000 0.01244 0.01292 = 0.03274 0.00220 0.00792 -0.00202 O4 4 0.261788 0.583418 0.395518 11.00000 0.01933 0.01146 = 0.03755 -0.00045 0.00997 0.00070 O7 4 1.014747 0.974682 0.430788 11.00000 0.02701 0.03310 = 0.02156 -0.00339 0.00274 -0.01454 O6 4 0.749797 0.256316 0.357756 11.00000 0.01168 0.01416 = 0.03210 -0.00003 0.00540 0.00056 N11 3 0.436542 0.184269 0.356009 11.00000 0.01655 0.01364 = 0.02017 0.00052 0.00303 0.00005 O3 4 0.072781 0.498651 0.304536 11.00000 0.02704 0.02856 = 0.01849 0.00074 0.00121 0.01276 N14 3 0.099395 0.579209 0.618722 11.00000 0.02374 0.02072 = 0.02388 -0.00129 0.00410 -0.00298 O9 4 0.954712 0.983182 0.302059 11.00000 0.02512 0.03156 = 0.02053 0.00262 0.00762 -0.00829 N18 3 1.080601 1.068373 0.620483 11.00000 0.02512 0.02400 = 0.03347 -0.00498 -0.00059 0.00100 N12 3 0.618615 0.682574 0.363216 11.00000 0.01424 0.01270 = 0.01878 -0.00007 0.00288 -0.00012 N17 3 1.311383 1.313601 0.630219 11.00000 0.03033 0.02482 = 0.02289 0.00375 -0.00102 -0.00014 N13 3 0.327536 0.822524 0.608740 11.00000 0.02966 0.02183 = 0.02307 0.00123 0.00518 -0.00440 C25 1 0.314058 0.331357 0.366367 11.00000 0.01249 0.01472 = 0.01276 0.00085 0.00350 -0.00011 N16 3 -0.314594 0.169662 0.601445 11.00000 0.04468 0.02489 = 0.01793 -0.00009 -0.00076 -0.00641 N15 3 -0.082681 0.419776 0.614608 11.00000 0.02627 0.02314 = 0.02753 -0.00016 0.00364 -0.00006 C30 1 0.442167 0.808521 0.366393 11.00000 0.01204 0.01593 = 0.01775 0.00125 0.00290 -0.00066 N20 3 0.685112 0.653813 0.611886 11.00000 0.03817 0.02943 = 0.02251 0.00305 0.00811 -0.00676 C29 1 0.452360 0.274006 0.361724 11.00000 0.01351 0.01580 = 0.01325 0.00122 0.00287 0.00160 N19 3 0.908325 0.905805 0.616537 11.00000 0.02887 0.02456 = 0.02641 -0.00377 0.00136 -0.00097 C35 1 0.905400 0.790305 0.363001 11.00000 0.01338 0.01740 = 0.01652 0.00082 0.00353 -0.00101 AFIX 43 H35 2 1.003375 0.825760 0.363038 11.00000 -1.20000 AFIX 0 O8 4 0.816980 1.083422 0.373453 11.00000 0.02186 0.01147 = 0.10019 -0.00102 0.02513 -0.00156 C48 1 -0.242041 0.250882 0.605313 11.00000 0.02105 0.02432 = 0.01988 0.00047 -0.00008 0.00369 C23 1 0.506274 0.455806 0.373498 11.00000 0.01577 0.01190 = 0.02199 0.00044 0.00372 -0.00039 AFIX 43 H23 2 0.525964 0.517580 0.378068 11.00000 -1.20000 AFIX 0 C24 1 0.345791 0.424081 0.372181 11.00000 0.01666 0.01378 = 0.01667 0.00138 0.00392 0.00281 C27 1 0.138453 0.201641 0.357456 11.00000 0.01332 0.01595 = 0.02953 0.00218 0.00449 -0.00316 AFIX 43 H27 2 0.031056 0.173969 0.355266 11.00000 -1.20000 AFIX 0 C26 1 0.153328 0.291188 0.363720 11.00000 0.01568 0.01492 = 0.01900 -0.00092 0.00565 0.00320 AFIX 43 H26 2 0.056312 0.326366 0.366290 11.00000 -1.20000 AFIX 0 C34 1 0.745144 0.829972 0.363877 11.00000 0.01284 0.01629 = 0.01191 -0.00029 0.00231 -0.00050 C49 1 -0.210244 0.299873 0.669607 11.00000 0.02414 0.02491 = 0.01817 0.00128 0.00389 0.00092 AFIX 43 H49 2 -0.243039 0.277078 0.711817 11.00000 -1.20000 AFIX 0 C31 1 0.418693 0.898236 0.367097 11.00000 0.01097 0.01703 = 0.03082 0.00252 0.00700 0.00319 AFIX 43 H31 2 0.309000 0.921934 0.367659 11.00000 -1.20000 AFIX 0 C38 1 0.605369 0.772440 0.364305 11.00000 0.01315 0.01300 = 0.01291 0.00040 0.00265 -0.00016 C28 1 0.284016 0.150800 0.354280 11.00000 0.01777 0.01296 = 0.02743 0.00142 0.00174 -0.00084 AFIX 43 H28 2 0.271473 0.088498 0.350666 11.00000 -1.20000 AFIX 0 C33 1 0.717572 0.922398 0.365540 11.00000 0.01435 0.01479 = 0.01725 0.00061 0.00476 -0.00104 C61 1 0.801819 0.774584 0.552023 11.00000 0.02365 0.02391 = 0.01599 -0.00099 0.00151 -0.00094 AFIX 43 H61 2 0.781003 0.744043 0.507393 11.00000 -1.20000 AFIX 0 C54 1 1.190790 1.193982 0.688615 11.00000 0.01987 0.02675 = 0.01851 -0.00229 0.00157 0.00221 AFIX 43 H54 2 1.212304 1.223795 0.733567 11.00000 -1.20000 AFIX 0 C36 1 0.916579 0.700390 0.362105 11.00000 0.01390 0.01688 = 0.02484 0.00027 0.00504 0.00335 AFIX 43 H36 2 1.022730 0.672608 0.361413 11.00000 -1.20000 AFIX 0 C62 1 0.756223 0.735645 0.613437 11.00000 0.02167 0.02812 = 0.02117 0.00211 0.00393 0.00270 C60 1 0.876278 0.856584 0.556570 11.00000 0.02594 0.02856 = 0.02186 0.00122 0.00279 0.00118 AFIX 43 H60 2 0.907308 0.880142 0.514258 11.00000 -1.20000 AFIX 0 C50 1 -0.131528 0.380903 0.671257 11.00000 0.02409 0.02685 = 0.02176 -0.00468 0.00057 0.00107 AFIX 43 H50 2 -0.110204 0.411581 0.715822 11.00000 -1.20000 AFIX 0 C22 1 0.643171 0.399249 0.368252 11.00000 0.01430 0.01789 = 0.02715 -0.00048 0.00751 -0.00075 AFIX 43 H22 2 0.753237 0.423009 0.368649 11.00000 -1.20000 AFIX 0 C40 1 0.214156 0.709556 0.676529 11.00000 0.01954 0.02536 = 0.01723 -0.00111 0.00209 0.00028 AFIX 43 H40 2 0.240263 0.743534 0.719363 11.00000 -1.20000 AFIX 0 C53 1 1.115910 1.113116 0.683352 11.00000 0.02107 0.02803 = 0.02702 0.00006 0.00195 0.00359 AFIX 43 H53 2 1.087382 1.087116 0.725275 11.00000 -1.20000 AFIX 0 C37 1 0.769646 0.648956 0.362213 11.00000 0.01578 0.01021 = 0.02948 0.00035 0.00536 0.00122 AFIX 43 H37 2 0.780438 0.586507 0.361522 11.00000 -1.20000 AFIX 0 C42 1 0.216468 0.687219 0.550970 11.00000 0.02306 0.02899 = 0.01756 0.00052 0.00639 0.00131 AFIX 43 H42 2 0.243782 0.705189 0.506333 11.00000 -1.20000 AFIX 0 C41 1 0.256044 0.743337 0.611667 11.00000 0.01906 0.02015 = 0.02056 0.00293 0.00295 0.00236 C21 1 0.617330 0.309791 0.362569 11.00000 0.01292 0.01565 = 0.01537 0.00060 0.00382 0.00240 C47 1 -0.192971 0.292014 0.545257 11.00000 0.02389 0.02661 = 0.01981 -0.00338 0.00198 0.00367 AFIX 43 H47 2 -0.212812 0.263269 0.499838 11.00000 -1.20000 AFIX 0 C64 1 0.863863 0.868635 0.675276 11.00000 0.03040 0.03405 = 0.02374 -0.00761 0.00328 0.00469 AFIX 43 H64 2 0.885457 0.901387 0.718843 11.00000 -1.20000 AFIX 0 C55 1 1.237143 1.234193 0.626849 11.00000 0.01866 0.02231 = 0.02290 -0.00117 -0.00006 0.00487 C52 1 -0.351554 0.126340 0.665662 11.00000 0.03712 0.02789 = 0.02957 0.00410 0.00436 -0.00699 AFIX 137 H52A 2 -0.246320 0.120190 0.701170 11.00000 -1.50000 H52B 2 -0.399916 0.067773 0.652889 11.00000 -1.50000 H52C 2 -0.433271 0.161935 0.686096 11.00000 -1.50000 AFIX 0 C63 1 0.790007 0.787293 0.676742 11.00000 0.03158 0.03411 = 0.01963 -0.00042 0.00699 0.00342 AFIX 43 H63 2 0.761539 0.765609 0.720146 11.00000 -1.20000 AFIX 0 C44 1 0.365017 0.879002 0.672692 11.00000 0.03473 0.02345 = 0.03194 -0.00071 0.00523 -0.00742 AFIX 137 H44A 2 0.258673 0.894730 0.688314 11.00000 -1.50000 H44B 2 0.422323 0.932840 0.661072 11.00000 -1.50000 H44C 2 0.439097 0.847174 0.711421 11.00000 -1.50000 AFIX 0 C46 1 -0.116496 0.373652 0.552558 11.00000 0.02193 0.03108 = 0.02175 0.00402 0.00336 0.00034 AFIX 43 H46 2 -0.085302 0.399369 0.511048 11.00000 -1.20000 AFIX 0 C43 1 0.139788 0.607895 0.555920 11.00000 0.02283 0.02598 = 0.02224 -0.00372 0.00349 -0.00017 AFIX 43 H43 2 0.113795 0.571602 0.514381 11.00000 -1.20000 AFIX 0 C39 1 0.138058 0.630172 0.678316 11.00000 0.02563 0.02330 = 0.02054 0.00069 0.00525 0.00127 AFIX 43 H39 2 0.111083 0.609654 0.722336 11.00000 -1.20000 AFIX 0 C32 1 0.557811 0.954908 0.366985 11.00000 0.01997 0.01149 = 0.03095 0.00159 0.00961 0.00235 AFIX 43 H32 2 0.541065 1.016967 0.367926 11.00000 -1.20000 AFIX 0 C56 1 1.200705 1.184038 0.562369 11.00000 0.02582 0.02956 = 0.01939 -0.00154 0.00234 0.00443 AFIX 43 H56 2 1.230849 1.206924 0.519661 11.00000 -1.20000 AFIX 0 C58 1 1.342034 1.365030 0.697035 11.00000 0.03694 0.02615 = 0.03028 -0.00273 -0.00253 -0.00318 AFIX 137 H58A 2 1.233475 1.377047 0.712141 11.00000 -1.50000 H58B 2 1.397149 1.420969 0.688945 11.00000 -1.50000 H58C 2 1.415965 1.331447 0.734677 11.00000 -1.50000 AFIX 0 C57 1 1.124134 1.104562 0.560669 11.00000 0.02751 0.03184 = 0.02537 -0.00898 -0.00237 0.00565 AFIX 43 H57 2 1.100001 1.073059 0.516531 11.00000 -1.20000 AFIX 0 C66 1 0.654883 0.612488 0.677706 11.00000 0.03792 0.03735 = 0.03308 0.01015 0.01168 -0.00398 AFIX 137 H66A 2 0.761279 0.610761 0.712932 11.00000 -1.50000 H66B 2 0.613111 0.552185 0.667276 11.00000 -1.50000 H66C 2 0.569870 0.646643 0.697307 11.00000 -1.50000 AFIX 0 C51 1 -0.347583 0.119345 0.534431 11.00000 0.04164 0.03184 = 0.02688 -0.00506 -0.00215 -0.00405 AFIX 137 H51A 2 -0.429289 0.151412 0.498551 11.00000 -1.50000 H51B 2 -0.394504 0.061445 0.543216 11.00000 -1.50000 H51C 2 -0.241090 0.111422 0.516567 11.00000 -1.50000 AFIX 0 C45 1 0.360451 0.858529 0.540791 11.00000 0.03437 0.03327 = 0.02871 0.00825 0.00999 -0.00617 AFIX 137 H45A 2 0.434078 0.817948 0.520221 11.00000 -1.50000 H45B 2 0.416725 0.916003 0.549571 11.00000 -1.50000 H45C 2 0.252586 0.865738 0.507093 11.00000 -1.50000 AFIX 0 C65 1 0.645221 0.604298 0.545152 11.00000 0.03458 0.02613 = 0.03479 -0.00031 0.00540 -0.00735 AFIX 137 H65A 2 0.569908 0.639435 0.509079 11.00000 -1.50000 H65B 2 0.588361 0.549017 0.553627 11.00000 -1.50000 H65C 2 0.750475 0.591031 0.527717 11.00000 -1.50000 AFIX 0 C59 1 1.351457 1.355218 0.565615 11.00000 0.03522 0.03806 = 0.03169 0.01193 0.00232 -0.00140 AFIX 137 H59A 2 1.429459 1.317305 0.545016 11.00000 -1.50000 H59B 2 1.405242 1.412637 0.578214 11.00000 -1.50000 H59C 2 1.246532 1.363609 0.530309 11.00000 -1.50000 AFIX 0 H14 2 0.046694 0.526222 0.616364 11.00000 0.02937 H10 2 0.335753 0.696656 0.371907 11.00000 0.03718 H18 2 1.026617 1.016145 0.618003 11.00000 0.05658 H6 2 0.714143 0.203903 0.356738 11.00000 0.03922 HKLF 4 REM 230329_mi_01_14_01_autored_a.res in Pc REM wR2 = 0.0848, GooF = S = 1.038, Restrained GooF = 1.038 for all data REM R1 = 0.0325 for 6608 Fo > 4sig(Fo) and 0.0336 for all 6813 data REM 620 parameters refined using 4 restraints END WGHT 0.0463 0.5548 REM Highest difference peak 0.297, deepest hole -0.393, 1-sigma level 0.046 Q1 1 0.7682 1.0903 0.3307 11.00000 0.05 0.30 ; _shelx_res_checksum 38723