data_1 #============================================================================== # PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic 2024-03-26 _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code AW5090 _journal_coeditor_notes ; ? ; _journal_paper_category FA _journal_techeditor_code ? _iucr_compatibility_tag ACTA95 _journal_techeditor_notes ; ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 3.3(H2 O)' _chemical_formula_sum 'C36 H38.60 Cl2 Cu N8 O11.30' _chemical_formula_weight 898.59 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.8398(6) _cell_length_b 9.9196(8) _cell_length_c 12.8239(10) _cell_angle_alpha 97.633(6) _cell_angle_beta 93.948(6) _cell_angle_gamma 107.385(7) _cell_volume 1056.59(14) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4296 _cell_measurement_theta_min 4.1960 _cell_measurement_theta_max 29.0940 _exptl_crystal_description block _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.412 _exptl_crystal_F_000 464 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.15 _exptl_absorpt_coefficient_mu 0.710 _shelx_estimated_absorpt_T_min 0.843 _shelx_estimated_absorpt_T_max 0.901 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.838 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 7899 _diffrn_reflns_av_unetI/netI 0.0369 _diffrn_reflns_av_R_equivalents 0.0260 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 3.068 _diffrn_reflns_theta_max 24.997 _diffrn_reflns_theta_full 24.997 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measured_fraction_theta_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_point_group_measured_fraction_full 0.994 _reflns_number_total 3692 _reflns_number_gt 3323 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0898P)^2^+2.5027P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3692 _refine_ls_number_parameters 283 _refine_ls_number_restraints 19 _refine_ls_R_factor_all 0.0619 _refine_ls_R_factor_gt 0.0565 _refine_ls_wR_factor_ref 0.1672 _refine_ls_wR_factor_gt 0.1615 _refine_ls_goodness_of_fit_ref 1.110 _refine_ls_restrained_S_all 1.117 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.0141(2) Uani 1 2 d S . P . . N1A N 0.2544(4) 0.3929(3) -0.0718(3) 0.0182(7) Uani 1 1 d D . . . . H1A H 0.261(5) 0.4794(17) -0.069(4) 0.027 Uiso 1 1 d D U . . . C2A C 0.1320(4) 0.3015(4) -0.0354(3) 0.0182(8) Uani 1 1 d . . . . . H2A H 0.0443 0.3255 -0.0084 0.022 Uiso 1 1 calc R U . . . N3A N 0.1508(4) 0.1730(3) -0.0425(2) 0.0158(6) Uani 1 1 d . . . . . C4A C 0.2929(4) 0.1841(4) -0.0853(3) 0.0169(7) Uani 1 1 d . . . . . H4A H 0.3369 0.1081 -0.0999 0.020 Uiso 1 1 calc R U . . . C5A C 0.3604(4) 0.3213(4) -0.1032(3) 0.0161(7) Uani 1 1 d . . . . . C6A C 0.5095(4) 0.3868(4) -0.1462(3) 0.0168(7) Uani 1 1 d . . . . . C7A C 0.5389(5) 0.5155(4) -0.1861(3) 0.0249(9) Uani 1 1 d . . . . . H7A H 0.4604 0.5634 -0.1856 0.030 Uiso 1 1 calc R U . . . C8A C 0.6809(5) 0.5739(4) -0.2263(4) 0.0301(10) Uani 1 1 d . . . . . H8A H 0.7003 0.6624 -0.2519 0.036 Uiso 1 1 calc R U . . . C9A C 0.7961(5) 0.5033(4) -0.2294(3) 0.0271(9) Uani 1 1 d . . . . . H9A H 0.8929 0.5426 -0.2582 0.032 Uiso 1 1 calc R U . . . C10A C 0.7681(5) 0.3757(4) -0.1902(3) 0.0238(8) Uani 1 1 d . . . . . H10A H 0.8460 0.3272 -0.1921 0.029 Uiso 1 1 calc R U . . . C11A C 0.6261(5) 0.3179(4) -0.1480(3) 0.0198(8) Uani 1 1 d . . . . . H11A H 0.6085 0.2310 -0.1203 0.024 Uiso 1 1 calc R U . . . N1B N -0.3739(4) -0.0806(3) -0.2365(3) 0.0197(7) Uani 1 1 d D . . . . H1B H -0.4731(13) -0.103(5) -0.242(4) 0.030 Uiso 1 1 d D U . . . C2B C -0.3095(4) -0.0665(4) -0.1371(3) 0.0186(8) Uani 1 1 d . . . . . H2B H -0.3689 -0.0903 -0.0795 0.022 Uiso 1 1 calc R U . . . N3B N -0.1521(4) -0.0150(3) -0.1289(2) 0.0166(6) Uani 1 1 d . . . . . C4B C -0.1152(5) 0.0046(4) -0.2297(3) 0.0210(8) Uani 1 1 d . . . . . H4B H -0.0104 0.0416 -0.2486 0.025 Uiso 1 1 calc R U . . . C5B C -0.2521(5) -0.0370(4) -0.2985(3) 0.0212(8) Uani 1 1 d . . . . . C6B C -0.2824(5) -0.0466(5) -0.4140(3) 0.0281(9) Uani 1 1 d . . . . . C7B C -0.4178(6) -0.1482(5) -0.4710(4) 0.0385(11) Uani 1 1 d . . . . . H7B H -0.4911 -0.2114 -0.4349 0.046 Uiso 1 1 calc R U . . . C8B C -0.4463(7) -0.1579(6) -0.5798(4) 0.0470(14) Uani 1 1 d . . . . . H8B H -0.5388 -0.2273 -0.6182 0.056 Uiso 1 1 calc R U . . . C9B C -0.3403(7) -0.0669(7) -0.6316(4) 0.0497(15) Uani 1 1 d . . . . . H9B H -0.3596 -0.0733 -0.7061 0.060 Uiso 1 1 calc R U . . . C10B C -0.2067(7) 0.0332(8) -0.5768(4) 0.0558(16) Uani 1 1 d . . . . . H10B H -0.1341 0.0960 -0.6136 0.067 Uiso 1 1 calc R U . . . C11B C -0.1767(6) 0.0436(7) -0.4675(4) 0.0445(13) Uani 1 1 d . . . . . H11B H -0.0835 0.1129 -0.4299 0.053 Uiso 1 1 calc R U . . . Cl Cl 0.22971(10) -0.22173(9) -0.13429(7) 0.0176(2) Uani 1 1 d . . . . . O1 O 0.1021(3) -0.1595(3) -0.1400(2) 0.0241(6) Uani 1 1 d . . . . . O2 O 0.2815(4) -0.2450(3) -0.2376(2) 0.0324(7) Uani 1 1 d . . . . . O3 O 0.3620(3) -0.1267(3) -0.0618(2) 0.0258(6) Uani 1 1 d . . . . . O4 O 0.1729(3) -0.3566(3) -0.0967(2) 0.0273(7) Uani 1 1 d . . . . . O5 O 0.1278(4) 0.3709(4) 0.6721(3) 0.0465(9) Uani 1 1 d D . . . . H5A H 0.173(6) 0.399(6) 0.616(2) 0.070 Uiso 1 1 d D U . . . H5B H 0.169(6) 0.445(4) 0.718(3) 0.070 Uiso 1 1 d D U . . . O6A O 0.099(2) 0.3508(16) 0.4575(13) 0.075(3) Uani 0.3 1 d D U P . . O6B O 0.2741(18) 0.4773(14) 0.4891(12) 0.075(3) Uani 0.35 1 d . U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0148(3) 0.0139(3) 0.0131(3) 0.0031(2) -0.0003(2) 0.0038(2) N1A 0.0202(16) 0.0126(15) 0.0237(16) 0.0031(13) 0.0033(13) 0.0077(13) C2A 0.0185(18) 0.0183(18) 0.0183(18) 0.0036(14) 0.0008(14) 0.0063(15) N3A 0.0190(15) 0.0153(15) 0.0130(15) 0.0021(12) 0.0007(12) 0.0054(12) C4A 0.0194(18) 0.0174(18) 0.0155(17) 0.0019(14) 0.0015(14) 0.0086(14) C5A 0.0182(18) 0.0152(17) 0.0153(17) 0.0004(14) -0.0016(14) 0.0073(14) C6A 0.0184(18) 0.0163(18) 0.0134(17) -0.0016(14) -0.0006(14) 0.0043(14) C7A 0.023(2) 0.0204(19) 0.034(2) 0.0061(17) 0.0053(17) 0.0093(16) C8A 0.029(2) 0.023(2) 0.040(2) 0.0119(18) 0.0086(19) 0.0063(17) C9A 0.020(2) 0.029(2) 0.028(2) 0.0007(17) 0.0045(16) 0.0031(17) C10A 0.0181(19) 0.028(2) 0.024(2) -0.0010(16) -0.0020(16) 0.0093(16) C11A 0.0244(19) 0.0177(18) 0.0168(18) -0.0001(14) -0.0024(15) 0.0082(15) N1B 0.0143(15) 0.0232(16) 0.0208(17) 0.0002(13) -0.0024(13) 0.0071(13) C2B 0.0192(18) 0.0209(18) 0.0171(18) 0.0035(15) 0.0029(15) 0.0080(15) N3B 0.0187(15) 0.0162(15) 0.0158(15) 0.0021(12) 0.0011(12) 0.0072(12) C4B 0.0214(19) 0.030(2) 0.0148(18) 0.0066(15) 0.0020(15) 0.0112(16) C5B 0.026(2) 0.026(2) 0.0156(19) 0.0019(15) 0.0019(15) 0.0144(16) C6B 0.034(2) 0.044(3) 0.016(2) 0.0036(17) -0.0006(17) 0.027(2) C7B 0.050(3) 0.040(3) 0.025(2) -0.003(2) -0.011(2) 0.021(2) C8B 0.066(4) 0.057(3) 0.022(2) -0.007(2) -0.012(2) 0.035(3) C9B 0.064(4) 0.086(4) 0.017(2) -0.003(2) -0.003(2) 0.056(3) C10B 0.050(3) 0.105(5) 0.028(3) 0.026(3) 0.014(2) 0.040(3) C11B 0.032(3) 0.080(4) 0.023(2) 0.015(2) 0.0013(19) 0.018(3) Cl 0.0170(4) 0.0143(4) 0.0222(5) 0.0017(3) 0.0017(3) 0.0064(3) O1 0.0200(13) 0.0202(14) 0.0355(16) 0.0053(12) 0.0013(12) 0.0113(11) O2 0.0301(16) 0.0406(18) 0.0251(15) -0.0008(13) 0.0067(13) 0.0106(14) O3 0.0187(13) 0.0233(14) 0.0318(16) -0.0039(12) -0.0028(12) 0.0062(11) O4 0.0230(14) 0.0190(14) 0.0440(18) 0.0125(12) 0.0050(13) 0.0092(11) O5 0.045(2) 0.048(2) 0.0366(19) -0.0190(16) -0.0064(16) 0.0122(17) O6A 0.096(6) 0.057(4) 0.084(5) 0.037(4) 0.033(5) 0.028(4) O6B 0.096(6) 0.057(4) 0.084(5) 0.037(4) 0.033(5) 0.028(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 2.000(3) . ? Cu N3A 2.000(3) 2 ? Cu N3B 2.018(3) 2 ? Cu N3B 2.018(3) . ? N1A C2A 1.345(5) . ? N1A C5A 1.385(5) . ? N1A H1A 0.839(10) . ? C2A N3A 1.326(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.385(5) . ? C4A C5A 1.370(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.465(5) . ? C6A C11A 1.396(5) . ? C6A C7A 1.398(5) . ? C7A C8A 1.383(6) . ? C7A H7A 0.9500 . ? C8A C9A 1.398(6) . ? C8A H8A 0.9500 . ? C9A C10A 1.384(6) . ? C9A H9A 0.9500 . ? C10A C11A 1.394(6) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.331(5) . ? N1B C5B 1.382(5) . ? N1B H1B 0.833(10) . ? C2B N3B 1.322(5) . ? C2B H2B 0.9500 . ? N3B C4B 1.380(5) . ? C4B C5B 1.367(5) . ? C4B H4B 0.9500 . ? C5B C6B 1.472(5) . ? C6B C11B 1.377(7) . ? C6B C7B 1.395(7) . ? C7B C8B 1.386(7) . ? C7B H7B 0.9500 . ? C8B C9B 1.369(9) . ? C8B H8B 0.9500 . ? C9B C10B 1.369(9) . ? C9B H9B 0.9500 . ? C10B C11B 1.393(7) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O1 1.441(3) . ? Cl O3 1.441(3) . ? Cl O4 1.441(3) . ? Cl O2 1.443(3) . ? O5 H5A 0.885(15) . ? O5 H5B 0.847(14) . ? O6A O6B 1.66(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 . 2 ? N3A Cu N3B 90.99(12) . 2 ? N3A Cu N3B 89.01(12) 2 2 ? N3A Cu N3B 89.01(12) . . ? N3A Cu N3B 90.99(12) 2 . ? N3B Cu N3B 180.0 2 . ? C2A N1A C5A 108.7(3) . . ? C2A N1A H1A 121(3) . . ? C5A N1A H1A 130(3) . . ? N3A C2A N1A 110.4(3) . . ? N3A C2A H2A 124.8 . . ? N1A C2A H2A 124.8 . . ? C2A N3A C4A 106.2(3) . . ? C2A N3A Cu 125.8(3) . . ? C4A N3A Cu 128.0(2) . . ? C5A C4A N3A 109.7(3) . . ? C5A C4A H4A 125.1 . . ? N3A C4A H4A 125.1 . . ? C4A C5A N1A 104.9(3) . . ? C4A C5A C6A 130.7(3) . . ? N1A C5A C6A 124.5(3) . . ? C11A C6A C7A 118.8(3) . . ? C11A C6A C5A 119.0(3) . . ? C7A C6A C5A 122.3(3) . . ? C8A C7A C6A 120.6(4) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C7A C8A C9A 120.3(4) . . ? C7A C8A H8A 119.9 . . ? C9A C8A H8A 119.9 . . ? C10A C9A C8A 119.5(4) . . ? C10A C9A H9A 120.2 . . ? C8A C9A H9A 120.2 . . ? C9A C10A C11A 120.3(4) . . ? C9A C10A H10A 119.9 . . ? C11A C10A H10A 119.9 . . ? C10A C11A C6A 120.5(4) . . ? C10A C11A H11A 119.7 . . ? C6A C11A H11A 119.7 . . ? C2B N1B C5B 108.4(3) . . ? C2B N1B H1B 113(3) . . ? C5B N1B H1B 138(3) . . ? N3B C2B N1B 111.2(3) . . ? N3B C2B H2B 124.4 . . ? N1B C2B H2B 124.4 . . ? C2B N3B C4B 105.7(3) . . ? C2B N3B Cu 126.1(3) . . ? C4B N3B Cu 127.6(2) . . ? C5B C4B N3B 109.8(3) . . ? C5B C4B H4B 125.1 . . ? N3B C4B H4B 125.1 . . ? C4B C5B N1B 104.9(3) . . ? C4B C5B C6B 132.9(4) . . ? N1B C5B C6B 122.2(4) . . ? C11B C6B C7B 119.0(4) . . ? C11B C6B C5B 120.5(4) . . ? C7B C6B C5B 120.5(4) . . ? C8B C7B C6B 120.6(5) . . ? C8B C7B H7B 119.7 . . ? C6B C7B H7B 119.7 . . ? C9B C8B C7B 119.5(5) . . ? C9B C8B H8B 120.2 . . ? C7B C8B H8B 120.2 . . ? C10B C9B C8B 120.6(4) . . ? C10B C9B H9B 119.7 . . ? C8B C9B H9B 119.7 . . ? C9B C10B C11B 120.4(6) . . ? C9B C10B H10B 119.8 . . ? C11B C10B H10B 119.8 . . ? C6B C11B C10B 119.9(5) . . ? C6B C11B H11B 120.1 . . ? C10B C11B H11B 120.1 . . ? O1 Cl O3 109.46(17) . . ? O1 Cl O4 108.85(16) . . ? O3 Cl O4 109.49(17) . . ? O1 Cl O2 110.20(18) . . ? O3 Cl O2 109.37(17) . . ? O4 Cl O2 109.44(18) . . ? H5A O5 H5B 101(4) . . ? _refine_diff_density_max 1.523 _refine_diff_density_min -0.480 _refine_diff_density_rms 0.114 # start Validation Reply Form _vrf_PLAT420_1 ; RESPONSE: The solvent water molecule O5 is located in a disordered solvent area. One of its H-atoms (H5A) is H-bonded to the disordered water molecule O6A; the second one (H5B) forms a very weak bifurcated hydrogen bond with two oxygen atoms of a neighboring perchlorate ion. ; _vrf_PLAT042_1 ; RESPONSE: The missing (not located in a difference Fourier map) H-atoms of the highly disordered crystallization water molecules O6A and O6B (modelled with partial occupancies) have been included in the sum and moiety formula and the Mr, Dx and F(000) have been modified accordingly. These modifications account for the differences detected in the relevant data items. ; _vrf_PLAT094_1 ; RESPONSE: The maximum residual density is located in the region of the disordered solvent water molecules O6A/O6B. ; _vrf_PLAT971_1 ; RESPONSE: Due to the disorder in the area of crystallization water molecules O6A/O6B. ; _vrf_FORMU01_1 ; RESPONSE: See response for PLAT042 Alert. ; # end Validation Reply Form _shelx_res_file ; 1.res created by SHELXL-2014/7 TITL EL104B in P-1 CELL 0.71073 8.8398 9.9196 12.8239 97.633 93.948 107.385 ZERR 1 0.0006 0.0008 0.0010 0.006 0.006 0.007 LATT 1 SFAC C H N O CL CU UNIT 36 38.6 8 11.3 2 1 MERG 2 FMAP 2 SIZE 0.15 0.16 0.25 TEMP -173 OMIT -2 50 OMIT 0 1 1 OMIT 0 1 2 OMIT -1 -1 2 OMIT 0 -1 3 OMIT -1 0 2 OMIT -1 -1 4 OMIT -1 1 2 OMIT 0 -2 1 OMIT -1 -1 3 OMIT 0 -3 1 OMIT -1 -2 3 OMIT -1 1 3 OMIT -1 0 3 OMIT -1 2 4 OMIT 0 2 0 OMIT 0 1 3 ACTA LIST 4 MORE -3 PLAN 10 BOND $H HTAB L.S. 15 WGHT 0.089800 2.502720 FVAR 5.45565 CU 6 0.000000 0.000000 0.000000 10.50000 0.01478 0.01390 = 0.01305 0.00305 -0.00033 0.00382 DFIX 0.84 0.01 N1A H1A N1B H1B N1A 3 0.254425 0.392933 -0.071804 11.00000 0.02019 0.01256 = 0.02375 0.00310 0.00327 0.00767 H1A 2 0.260863 0.479446 -0.069463 11.00000 -1.50000 C2A 1 0.131960 0.301480 -0.035423 11.00000 0.01850 0.01834 = 0.01826 0.00361 0.00079 0.00627 AFIX 43 H2A 2 0.044314 0.325527 -0.008423 11.00000 -1.20000 AFIX 0 N3A 3 0.150761 0.172993 -0.042542 11.00000 0.01899 0.01529 = 0.01302 0.00207 0.00073 0.00538 C4A 1 0.292905 0.184122 -0.085260 11.00000 0.01940 0.01737 = 0.01554 0.00193 0.00148 0.00858 AFIX 43 H4A 2 0.336939 0.108145 -0.099882 11.00000 -1.20000 AFIX 0 C5A 1 0.360383 0.321291 -0.103234 11.00000 0.01818 0.01521 = 0.01529 0.00043 -0.00157 0.00733 C6A 1 0.509531 0.386780 -0.146183 11.00000 0.01837 0.01629 = 0.01345 -0.00157 -0.00057 0.00433 C7A 1 0.538860 0.515536 -0.186086 11.00000 0.02338 0.02041 = 0.03351 0.00613 0.00526 0.00932 AFIX 43 H7A 2 0.460433 0.563392 -0.185578 11.00000 -1.20000 AFIX 0 C8A 1 0.680948 0.573916 -0.226292 11.00000 0.02853 0.02284 = 0.04032 0.01194 0.00858 0.00627 AFIX 43 H8A 2 0.700348 0.662414 -0.251918 11.00000 -1.20000 AFIX 0 C9A 1 0.796125 0.503293 -0.229389 11.00000 0.02019 0.02880 = 0.02832 0.00067 0.00453 0.00312 AFIX 43 H9A 2 0.892912 0.542618 -0.258154 11.00000 -1.20000 AFIX 0 C10A 1 0.768128 0.375654 -0.190241 11.00000 0.01814 0.02847 = 0.02388 -0.00102 -0.00200 0.00928 AFIX 43 H10A 2 0.845997 0.327188 -0.192143 11.00000 -1.20000 AFIX 0 C11A 1 0.626116 0.317910 -0.148026 11.00000 0.02444 0.01767 = 0.01677 -0.00009 -0.00245 0.00821 AFIX 43 H11A 2 0.608533 0.231020 -0.120296 11.00000 -1.20000 AFIX 0 N1B 3 -0.373865 -0.080623 -0.236465 11.00000 0.01427 0.02325 = 0.02076 0.00017 -0.00239 0.00715 H1B 2 -0.473072 -0.103140 -0.242022 11.00000 -1.50000 C2B 1 -0.309463 -0.066502 -0.137114 11.00000 0.01923 0.02094 = 0.01706 0.00351 0.00289 0.00798 AFIX 43 H2B 2 -0.368891 -0.090328 -0.079541 11.00000 -1.20000 AFIX 0 N3B 3 -0.152121 -0.015040 -0.128924 11.00000 0.01873 0.01619 = 0.01580 0.00214 0.00106 0.00717 C4B 1 -0.115242 0.004644 -0.229747 11.00000 0.02142 0.02988 = 0.01475 0.00660 0.00202 0.01123 AFIX 43 H4B 2 -0.010440 0.041628 -0.248588 11.00000 -1.20000 AFIX 0 C5B 1 -0.252109 -0.037046 -0.298494 11.00000 0.02584 0.02597 = 0.01558 0.00193 0.00189 0.01444 C6B 1 -0.282373 -0.046609 -0.413980 11.00000 0.03372 0.04377 = 0.01574 0.00358 -0.00055 0.02671 C7B 1 -0.417752 -0.148243 -0.471005 11.00000 0.04986 0.04034 = 0.02534 -0.00321 -0.01091 0.02108 AFIX 43 H7B 2 -0.491073 -0.211418 -0.434924 11.00000 -1.20000 AFIX 0 C8B 1 -0.446304 -0.157929 -0.579809 11.00000 0.06556 0.05726 = 0.02210 -0.00683 -0.01171 0.03455 AFIX 43 H8B 2 -0.538813 -0.227257 -0.618188 11.00000 -1.20000 AFIX 0 C9B 1 -0.340295 -0.066918 -0.631558 11.00000 0.06391 0.08578 = 0.01711 -0.00280 -0.00325 0.05631 AFIX 43 H9B 2 -0.359576 -0.073304 -0.706126 11.00000 -1.20000 AFIX 0 C10B 1 -0.206745 0.033217 -0.576819 11.00000 0.05040 0.10537 = 0.02835 0.02633 0.01432 0.04040 AFIX 43 H10B 2 -0.134133 0.095960 -0.613581 11.00000 -1.20000 AFIX 0 C11B 1 -0.176697 0.043646 -0.467503 11.00000 0.03212 0.08049 = 0.02312 0.01459 0.00131 0.01847 AFIX 43 H11B 2 -0.083460 0.112902 -0.429924 11.00000 -1.20000 AFIX 0 CL 5 0.229712 -0.221727 -0.134287 11.00000 0.01697 0.01428 = 0.02217 0.00172 0.00175 0.00641 O1 4 0.102088 -0.159468 -0.140008 11.00000 0.01998 0.02023 = 0.03554 0.00528 0.00128 0.01129 O2 4 0.281479 -0.245024 -0.237597 11.00000 0.03012 0.04056 = 0.02512 -0.00081 0.00672 0.01056 O3 4 0.361957 -0.126728 -0.061837 11.00000 0.01869 0.02334 = 0.03184 -0.00391 -0.00285 0.00620 O4 4 0.172932 -0.356559 -0.096726 11.00000 0.02304 0.01901 = 0.04402 0.01254 0.00496 0.00918 DFIX 0.84 0.015 O5 H5A O5 H5B DANG 1.32 H5A H5B DFIX 1.87 0.05 H5A O6A EQIV $1 X, 1+Y, 1+Z DFIX 2.85 0.02 H5B O4_$1 O5 4 0.127843 0.370943 0.672148 11.00000 0.04468 0.04782 = 0.03661 -0.01896 -0.00640 0.01223 H5A 2 0.172787 0.398798 0.615781 11.00000 -1.50000 H5B 2 0.169282 0.444751 0.718498 11.00000 -1.50000 ISOR 0.005 O6A O6B EADP O6A O6B O6A 4 0.099077 0.350796 0.457532 10.30000 0.09644 0.05732 = 0.08371 0.03706 0.03328 0.02810 O6B 4 0.274145 0.477252 0.489113 10.35000 0.09644 0.05732 = 0.08371 0.03706 0.03328 0.02810 HKLF 4 REM EL104B in P-1 REM R1 = 0.0565 for 3323 Fo > 4sig(Fo) and 0.0619 for all 3692 data REM 283 parameters refined using 19 restraints END WGHT 0.0888 2.6909 REM Instructions for potential hydrogen bonds EQIV $2 x, y+1, z HTAB N1A O4_$2 EQIV $3 -x, -y, -z HTAB C2A O4_$3 HTAB C4A O3 EQIV $4 x-1, y, z HTAB N1B O2_$4 HTAB C2B O3_$4 HTAB C2B O3_$3 HTAB O5 O6A HTAB O5 O6B REM Highest difference peak 1.523, deepest hole -0.480, 1-sigma level 0.114 Q1 1 0.2124 0.4365 0.5555 11.00000 0.05 1.52 Q2 1 0.0000 0.5000 0.5000 10.50000 0.05 1.51 Q3 1 0.3525 0.4983 0.5375 11.00000 0.05 1.28 Q4 1 0.1464 0.5464 0.5150 11.00000 0.05 1.06 Q5 1 0.2661 0.4533 0.4641 11.00000 0.05 0.85 Q6 1 -0.1872 0.1229 -0.5589 11.00000 0.05 0.53 Q7 1 -0.1588 0.1346 -0.4424 11.00000 0.05 0.50 Q8 1 -0.2789 0.0144 -0.6192 11.00000 0.05 0.43 Q9 1 -0.1829 0.0158 -0.5827 11.00000 0.05 0.40 Q10 1 0.4485 0.3608 -0.1314 11.00000 0.05 0.39 ; _shelx_res_checksum 34591 _shelx_hkl_file ; 0 0 3 158659. 3159.64 5 0 0 3 158015. 3168.64 4 0 0 -3 161770. 3151.72 5 0 0 4 3489.56 223.644 4 0 0 4 2570.72 189.188 5 0 0 -4 3123.66 203.782 5 0 0 -5 273.271 87.0762 5 0 0 5 241.658 72.9958 5 0 0 5 401.174 102.325 4 0 0 6 1931.73 206.718 4 0 0 6 1933.96 196.292 5 0 0 -6 1950.91 221.808 5 0 0 -7 18863.7 738.786 5 0 0 7 17439.9 693.896 5 0 0 7 17512.7 698.410 4 0 0 -8 38840.9 1278.85 5 0 0 8 38155.7 1210.48 4 0 0 8 41277.2 1245.48 5 0 0 9 28433.9 1047.34 5 0 0 9 28744.1 1045.62 4 0 0 -9 29484.0 1161.39 5 0 0 -10 1878.85 339.370 5 0 0 10 2315.48 291.674 4 0 0 -11 13180.0 857.802 5 0 0 11 13457.9 740.872 4 0 0 12 267.964 139.469 4 0 0 -12 16.5484 234.744 5 0 0 -13 11372.3 845.255 5 0 0 13 12069.6 766.769 4 0 0 14 10059.0 720.520 4 0 0 -14 8825.41 761.680 5 0 0 15 4905.07 530.467 4 0 0 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85.4438 103.962 3 3 -6 -4 118.899 70.5662 1 -3 6 4 180.448 92.4142 1 3 -6 -3 4436.71 339.867 1 -3 6 3 6115.40 426.975 1 3 -6 -3 5409.07 421.141 3 3 -6 -2 12821.9 594.930 1 -3 6 2 13394.3 639.937 1 3 -6 -2 13080.7 633.599 3 3 -6 -1 314.836 105.062 3 -3 6 1 242.664 104.100 1 3 -6 -1 231.120 82.9140 1 -3 6 0 160.130 85.5926 5 3 -6 0 230.887 84.9241 3 3 -6 0 100.167 67.5297 1 -3 6 0 265.370 110.136 1 3 -6 1 30049.2 934.925 3 -3 6 -1 29375.4 1027.93 1 -3 6 -2 16284.8 734.801 1 3 -6 2 15815.5 590.939 3 -3 6 -3 4762.01 392.458 1 -3 6 -3 3281.72 282.891 3 3 -6 3 4043.31 264.432 3 -3 6 -4 6163.74 466.569 1 3 -6 4 6052.67 307.220 3 -3 6 -4 5967.56 324.735 3 -3 6 -5 213.121 56.1925 3 -3 6 -5 332.295 80.1327 2 -3 6 -5 275.466 121.954 1 -3 6 -5 447.388 128.398 5 -3 6 -6 22965.3 740.331 2 -3 6 -6 25901.1 913.701 5 -3 6 -6 25099.8 703.689 3 -3 6 -6 27224.7 1129.37 1 -3 6 -7 26187.1 937.016 5 -3 6 -7 27465.6 736.983 3 -3 6 -7 26671.3 780.232 2 -3 6 -8 20605.5 604.557 3 -3 6 -8 20711.9 634.836 2 -3 6 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8633.37 777.617 5 8 4 -7 6544.75 664.496 5 8 4 -6 1788.95 370.612 5 8 4 -5 339.506 184.072 5 8 4 -5 179.442 103.672 2 8 4 -4 82.0965 113.816 5 8 4 -4-36.9084 99.7637 2 8 4 -3 147.098 133.771 5 8 4 -3-20.1049 105.143 2 8 4 -2 2231.84 356.837 5 8 4 -2 2948.49 392.330 2 8 4 -1 7403.47 637.403 2 8 4 -1 7854.73 654.009 5 8 4 0 6974.08 633.051 2 8 4 0 5983.14 564.304 5 8 4 1 7360.67 662.321 2 8 4 1 6747.66 589.497 5 8 4 2 5609.78 592.447 2 8 4 2 4468.40 469.096 5 8 4 3 576.312 201.686 2 8 4 4-145.948 132.083 2 8 5 -7 565.457 234.414 5 8 5 -6-16.2066 109.120 5 8 5 -5 69.8288 105.913 5 8 5 -5 0.63735 89.2401 2 8 5 -4 1137.60 293.807 5 8 5 -4 995.151 236.428 2 8 5 -3 1225.79 302.911 5 8 5 -3 1491.38 285.741 2 8 5 -2 1549.65 306.723 5 8 5 -2 1542.36 292.924 2 8 5 -1 8527.12 709.729 2 8 5 -1 7026.70 657.358 5 8 5 0 5009.39 556.379 2 8 5 0 4078.94 494.610 5 8 5 1-36.0674 75.4402 5 8 5 1 157.964 157.771 2 8 5 2-53.5532 142.656 2 8 6 -5 1382.62 313.062 5 8 6 -5 1157.69 252.163 2 8 6 -4 3664.90 447.962 2 8 6 -4 3868.20 537.539 5 8 6 -3 3268.05 430.508 2 8 6 -3 3983.92 536.044 5 8 6 -2 1293.19 300.940 5 8 6 -2 1324.89 279.464 2 8 6 -1 659.595 234.186 5 8 6 -1 148.683 117.888 2 8 6 0-12.1251 107.548 5 8 6 1 486.239 186.666 5 8 7 -3-30.0924 79.7472 2 -9 11 2 5283.26 691.849 1 -9 11 1-138.782 159.260 1 9 -10 -6 30.3279 103.331 3 9 -10 -5 1450.46 296.394 3 -9 10 5 1431.74 374.662 1 9 -10 -4 1455.23 292.626 3 -9 10 4 1988.64 414.112 1 -9 10 3 869.207 295.633 1 -9 10 2-177.392 187.800 1 -9 10 1 204.326 165.406 1 -9 10 0 523.096 251.803 1 -9 10 -1 3285.57 553.253 1 -9 10 -2 4459.02 634.990 1 -9 10 -3 3277.42 539.327 1 9 -9 -7 6276.90 705.194 3 -9 9 7 5877.38 748.044 1 -9 9 6 3411.38 556.235 1 9 -9 -6 4130.96 551.229 3 9 -9 -5 1076.13 286.652 3 -9 9 5 1647.88 385.857 1 9 -9 -4 12.7723 131.388 3 -9 9 4-171.569 171.155 1 9 -9 -3-41.2011 89.5610 3 -9 9 3 271.081 179.292 1 -9 9 2 333.340 204.516 1 9 -9 -2 98.3110 92.0042 3 -9 9 1 5094.89 659.686 1 -9 9 0 10436.4 942.494 1 -9 9 -1 2567.77 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295.256 213.291 1 9 -5 -2 203.794 136.575 5 -9 5 2-151.760 190.043 1 9 -5 -1 653.405 178.927 5 -9 5 1 594.944 239.663 1 -9 5 0 7042.70 729.243 1 9 -5 0 6762.32 472.455 5 -9 5 -1 339.253 178.266 1 -9 5 -2 1387.75 325.618 1 -9 5 -3 342.208 218.242 1 -9 5 -4 4183.12 554.115 1 -9 5 -5 1120.14 328.801 1 -9 5 -6 666.452 252.334 1 -9 5 -7 5254.08 652.465 1 -9 5 -8 1240.47 339.199 1 -9 5 -9 1787.77 409.073 1 9 -4 -10 1797.94 455.667 5 9 -4 -9 4082.09 652.031 5 9 -4 -8 6214.71 766.106 5 9 -4 -7 1546.05 383.920 5 9 -4 -6 99.5788 158.167 5 -9 4 6 491.089 247.068 1 9 -4 -5 166.954 151.572 5 -9 4 5 221.152 147.187 1 -9 4 4 7034.63 760.517 1 9 -4 -4 5867.26 652.772 5 9 -4 -3 7276.82 695.000 5 -9 4 3 6891.19 744.143 1 9 -4 -2 9083.28 748.396 5 -9 4 2 8573.30 809.814 1 9 -4 -1 34136.6 1451.96 5 -9 4 1 31745.8 1618.88 1 -9 4 0 21944.0 1314.77 1 9 -4 0 21470.1 994.282 5 9 -4 1 845.976 167.070 5 -9 4 -1 896.438 273.731 1 -9 4 -2-80.8411 149.710 1 -9 4 -3 632.601 227.710 1 -9 4 -4 260.318 192.219 1 -9 4 -5-76.0790 155.057 1 -9 4 -6 193.350 131.746 1 -9 4 -7 1813.83 389.488 1 -9 4 -8 7680.47 790.387 1 -9 4 -9 10055.2 938.242 1 9 -3 -10 10606.2 1019.19 5 9 -3 -9 6661.38 769.926 5 9 -3 -8 699.461 263.549 5 9 -3 -7 501.304 197.998 5 9 -3 -6-107.667 163.152 5 -9 3 6 188.484 141.896 1 9 -3 -5-20.1693 129.226 5 -9 3 5 49.8619 157.430 1 -9 3 4 8205.35 805.035 1 9 -3 -4 7904.88 675.917 5 -9 3 3 23313.0 1372.66 1 9 -3 -3 22691.3 1150.52 5 9 -3 -2 7258.72 612.941 5 -9 3 2 7284.16 739.040 1 9 -3 -1 7958.95 622.630 5 -9 3 1 6812.34 710.570 1 9 -3 0 525.333 154.268 5 -9 3 0 1301.86 319.736 1 9 -3 1 1743.02 262.040 5 -9 3 -1 1004.83 283.348 1 -9 3 -2 22.6660 115.792 1 -9 3 -3 8211.05 766.922 1 -9 3 -4 14870.9 1047.58 1 -9 3 -5 6715.12 701.556 1 -9 3 -6 3534.19 511.909 1 -9 3 -7-134.654 157.172 1 -9 3 -8 664.148 246.258 1 9 -3 8 715.802 230.403 2 9 -3 9 287.980 172.124 2 -9 3 -9 195.446 157.150 1 9 -3 10 184.968 132.514 2 -9 3 -10 140.244 136.953 1 9 -2 -10 4380.34 599.316 5 9 -2 -9 2357.78 414.702 5 9 -2 -8 5233.70 596.613 5 9 -2 -7 167.087 154.671 5 9 -2 -6 1889.09 330.747 5 -9 2 5 23729.1 1422.85 1 9 -2 -5 23831.6 1174.38 5 -9 2 4 20087.7 1283.43 1 9 -2 -4 21749.0 1063.36 5 -9 2 3 3265.36 500.347 1 9 -2 -3 2862.34 357.910 5 -9 2 2 2605.01 461.025 1 9 -2 -2 2979.14 351.804 5 9 -2 -1 26.9347 74.4854 5 -9 2 1 283.300 208.196 1 -9 2 0 65.2531 136.852 1 9 -2 0 134.076 99.2459 5 9 -2 1-23.2429 73.6883 5 -9 2 -1 72.6078 123.244 1 -9 2 -2-2.69781 155.133 1 -9 2 -3 6974.30 703.760 1 -9 2 -4 21443.3 1265.14 1 9 -2 4 21893.4 1163.23 2 -9 2 -5 17383.4 1136.98 1 9 -2 5 17962.4 1053.43 2 -9 2 -6 1241.64 314.916 1 9 -2 6 604.841 189.399 2 -9 2 -7 106.353 122.843 1 9 -2 7 113.037 114.992 2 -9 2 -8-136.688 140.283 1 9 -2 8 161.799 142.048 2 -9 2 -9 749.733 253.264 1 9 -2 9 1397.83 303.413 2 -9 2 -10 131.717 141.747 1 9 -2 10 213.010 126.575 4 9 -1 -10 2144.86 391.007 5 9 -1 -9 661.361 229.377 5 9 -1 -8 683.457 223.515 5 9 -1 -7 394.833 172.654 5 9 -1 -6 9923.43 741.692 5 9 -1 -5 17011.4 959.607 5 -9 1 4 7228.04 748.499 1 9 -1 -4 7155.99 582.770 5 9 -1 -3 269.992 136.164 5 -9 1 3 9.49503 140.054 1 -9 1 2 200.203 184.161 1 9 -1 -2 325.071 107.579 5 9 -1 -1 4297.72 402.326 5 -9 1 1 4443.88 563.039 1 -9 1 0 1911.79 379.124 1 9 -1 0 1992.63 263.012 5 -9 1 -1 4822.04 574.229 1 9 -1 1 4664.96 375.884 5 9 -1 2 25983.4 1253.49 2 -9 1 -2 24608.7 1351.36 1 9 -1 3 28945.8 1347.41 2 -9 1 -3 26920.6 1428.14 1 -9 1 -4 94.9114 130.100 1 9 -1 4 418.299 185.548 2 -9 1 -5 2403.90 412.025 1 9 -1 5 3160.82 438.448 2 -9 1 -6 597.500 214.004 1 9 -1 6 855.345 259.491 2 -9 1 -7 5041.59 608.108 1 9 -1 7 5477.74 591.938 2 -9 1 -8 10726.8 884.022 1 9 -1 8 10967.7 869.962 2 -9 1 -9 12104.6 955.299 1 9 -1 9 11034.1 789.767 4 9 0 -10 175.181 127.715 5 9 0 -9 621.257 229.173 5 9 0 -8 5830.52 618.417 5 9 0 -7 3474.41 454.934 5 9 0 -6 4261.11 492.384 5 9 0 -5 869.255 228.355 5 9 0 -4 774.903 214.501 5 -9 0 3 1940.17 381.940 1 9 0 -3 2044.51 308.507 5 9 0 -2 206.843 128.594 5 -9 0 2-29.4973 129.754 1 -9 0 1 3263.71 466.540 1 9 0 -1 3268.70 361.827 5 9 0 0 6852.51 615.211 2 9 0 0 6116.15 474.836 5 -9 0 0 6588.89 677.015 1 9 0 1 4835.39 518.967 2 9 0 1 4641.55 391.650 5 -9 0 -1 4717.84 566.829 1 -9 0 -2 989.837 260.928 1 9 0 2 1195.99 269.346 2 9 0 3 4762.57 529.581 2 -9 0 -3 4770.77 570.022 1 9 0 4 2903.71 426.031 2 -9 0 -4 3707.44 497.291 1 9 0 5 10160.2 806.043 2 -9 0 -5 9548.79 806.999 1 9 0 6 10689.8 841.390 2 -9 0 -6 9999.11 838.827 1 9 0 7 6163.04 653.714 2 -9 0 -7 5726.39 636.795 1 9 1 -9 5066.58 593.511 5 9 1 -8 8170.08 729.610 5 9 1 -7 3025.07 434.982 5 9 1 -6 164.714 133.119 5 9 1 -5-166.895 123.154 5 9 1 -4 58.6742 101.982 5 9 1 -3 503.124 178.181 5 -9 -1 2 9413.76 823.757 1 9 1 -2 9896.21 686.085 5 -9 -1 1 15619.4 1056.06 1 9 1 -1 12856.7 859.332 2 9 1 -1 14168.4 805.908 5 9 1 0 1534.02 245.151 5 -9 -1 0 1410.22 326.449 1 9 1 0 1629.43 310.527 2 9 1 1 216.590 139.836 2 -9 -1 -1 536.287 210.698 1 -9 -1 -2 221.117 165.492 1 9 1 2 207.837 119.425 2 -9 -1 -3 691.095 234.090 1 9 1 3 369.321 176.460 2 -9 -1 -4 738.442 226.365 1 9 1 4 871.796 255.504 2 9 1 5 4166.70 527.846 2 -9 -1 -5 3219.29 460.004 1 9 2 -9 1820.96 361.924 5 9 2 -8 180.531 118.761 5 9 2 -7 436.913 181.357 5 9 2 -6 1469.47 322.992 5 9 2 -5-135.528 127.079 5 9 2 -4 9512.02 736.495 5 9 2 -3 19481.8 1052.56 5 9 2 -2 11724.4 814.936 2 9 2 -2 11331.6 769.228 5 9 2 -1 9596.51 744.826 2 9 2 -1 9028.46 662.789 5 -9 -2 0 1556.93 326.531 1 9 2 0 1979.51 302.595 5 9 2 0 1864.49 332.467 2 9 2 1 689.409 226.382 2 -9 -2 -1 718.995 215.601 1 -9 -2 -2 112.960 111.465 1 9 2 2 288.986 188.222 2 9 2 3 1536.85 324.914 2 9 2 4 2420.90 401.502 2 9 3 -8-26.7049 102.553 5 9 3 -7-37.7294 118.537 5 9 3 -6 2015.33 373.471 5 9 3 -5 17347.6 1068.31 5 9 3 -4 9860.50 772.773 5 9 3 -3 3681.23 456.917 2 9 3 -3 4022.88 488.259 5 9 3 -2 1000.62 243.538 5 9 3 -2 1505.40 293.413 2 9 3 -1 480.335 178.724 5 9 3 -1 364.834 165.101 2 9 3 0 234.649 109.930 5 9 3 0 215.959 150.672 2 9 3 1 1751.67 344.666 2 9 3 2 5275.94 589.293 2 9 4 -6 4423.15 553.066 5 9 4 -5 4993.56 585.955 5 9 4 -4 730.766 236.711 5 9 4 -4 747.029 203.089 2 9 4 -3-351.890 164.638 5 9 4 -3-49.7621 106.475 2 9 4 -2 459.863 179.362 5 9 4 -2 302.606 164.306 2 9 4 -1 619.925 195.733 5 9 4 -1 1117.22 268.793 2 9 4 0 1488.45 326.909 2 9 5 -4 323.259 163.589 5 9 5 -4 173.806 120.761 2 9 5 -3 599.544 205.269 5 9 5 -3 439.245 182.095 2 9 5 -2 1157.41 270.785 5 9 5 -2 972.156 261.472 2 9 5 -1 2409.25 397.232 5 10 -9 -6 1309.49 348.585 3 10 -9 -5 3111.81 480.848 3 -10 8 4 3321.87 572.386 1 -10 8 3 270.139 196.340 1 -10 8 2 273.317 222.403 1 -10 8 1 3209.78 548.690 1 -10 8 0 7026.18 809.733 1 -10 8 -1 2005.07 437.455 1 -10 8 -2 1811.82 439.538 1 10 -7 -7 1374.55 313.329 5 10 -7 -6 3929.51 508.692 5 10 -7 -5 1330.45 289.548 5 -10 7 5 839.704 310.709 1 10 -7 -4 344.707 149.507 5 -10 7 4 517.183 258.850 1 -10 7 3 975.933 322.148 1 -10 7 2 1013.77 331.472 1 -10 7 1 8475.39 877.620 1 -10 7 0 2587.18 493.664 1 -10 7 -1 92.3299 164.177 1 -10 7 -2 744.613 279.814 1 -10 7 -3 1863.51 399.279 1 -10 7 -4 1656.99 390.532 1 10 -6 -8 82.0369 129.590 5 10 -6 -7 3096.62 490.475 5 10 -6 -6 1706.92 355.279 5 -10 6 6 1465.81 370.426 1 10 -6 -5 77.4907 109.040 5 -10 6 5 83.2015 180.351 1 -10 6 4 5998.67 745.934 1 10 -6 -4 6068.99 582.360 5 10 -6 -3 7876.87 634.097 5 -10 6 3 7396.06 821.336 1 10 -6 -2 4518.90 452.423 5 -10 6 2 4690.31 642.063 1 -10 6 1 978.052 307.242 1 -10 6 0 243.267 154.495 1 -10 6 -1 1920.19 413.772 1 -10 6 -2 179.032 195.714 1 -10 6 -3 3319.16 546.161 1 -10 6 -4 4419.19 625.963 1 -10 6 -5 2410.24 471.875 1 10 -5 -8-239.968 192.822 5 10 -5 -7-348.805 270.641 5 -10 5 6 5771.90 754.414 1 10 -5 -6 5321.81 684.517 5 -10 5 5 14617.8 1177.35 1 10 -5 -5 11294.4 971.414 5 -10 5 4 6466.62 768.826 1 10 -5 -4 6373.32 674.417 5 10 -5 -3 166.116 125.936 5 -10 5 3 272.042 226.661 1 10 -5 -2 1849.03 312.023 5 -10 5 2 1383.30 356.252 1 -10 5 1 2003.20 435.342 1 -10 5 0 201.648 227.965 1 -10 5 -1-268.128 185.821 1 -10 5 -2 604.185 242.864 1 -10 5 -3 9272.00 897.462 1 -10 5 -4 8354.79 846.484 1 -10 5 -5 2091.64 439.199 1 -10 5 -6-19.3425 116.207 1 10 -4 -8-21.5843 100.068 5 10 -4 -7-353.554 227.575 5 10 -4 -6 4003.72 605.932 5 -10 4 6 4692.70 687.028 1 -10 4 5 7411.94 829.951 1 10 -4 -5 5189.34 663.108 5 10 -4 -4 2320.80 428.338 5 -10 4 4 2821.01 517.069 1 10 -4 -3 2204.01 403.644 5 -10 4 3 2342.18 477.410 1 10 -4 -2-58.9825 171.865 5 -10 4 2 220.631 172.077 1 10 -4 -1 2620.29 385.181 5 -10 4 1 2066.69 427.765 1 -10 4 0 8859.00 867.864 1 -10 4 -1 13813.7 1087.07 1 -10 4 -2 24134.6 1464.10 1 -10 4 -3 22605.6 1416.91 1 -10 4 -4 774.014 285.165 1 -10 4 -5 123.045 189.979 1 -10 4 -6 26.7755 143.929 1 -10 4 -7-326.029 198.480 1 10 -3 -9-31.0679 172.196 5 10 -3 -8 1371.31 363.333 5 10 -3 -7 3219.12 506.586 5 10 -3 -6 5386.77 643.254 5 10 -3 -5-1.83092 160.935 5 -10 3 5 270.306 202.208 1 10 -3 -4-112.761 185.063 5 -10 3 4-1.13085 196.265 1 -10 3 3-86.2393 171.265 1 10 -3 -3-30.4150 123.423 5 10 -3 -2 13547.9 912.038 5 -10 3 2 14181.8 1108.90 1 10 -3 -1 4266.70 484.646 5 -10 3 1 4774.30 637.617 1 -10 3 0 4064.95 579.423 1 -10 3 -1 2813.75 483.275 1 -10 3 -2 1352.42 331.689 1 -10 3 -3 2406.37 447.414 1 -10 3 -4 278.174 192.973 1 -10 3 -5 2358.17 449.628 1 -10 3 -6 5415.76 685.955 1 -10 3 -7 8404.71 850.690 1 -10 3 -8 2432.05 463.712 1 10 -2 -9 1802.56 386.470 5 10 -2 -8 220.022 145.995 5 10 -2 -7-40.5842 118.473 5 10 -2 -6 226.798 152.264 5 10 -2 -5 2699.01 398.080 5 -10 2 5 2419.08 471.774 1 -10 2 4 12334.5 1053.42 1 10 -2 -4 12327.5 834.794 5 -10 2 3 3100.52 528.635 1 10 -2 -3 3155.13 406.282 5 -10 2 2 21906.5 1387.33 1 10 -2 -2 23491.2 1109.26 5 10 -2 -1 3344.14 376.645 5 -10 2 1 4254.91 601.367 1 -10 2 0 744.666 278.410 1 -10 2 -1-56.7715 142.272 1 -10 2 -2 69.5581 116.101 1 -10 2 -3 812.780 276.983 1 -10 2 -4 798.493 280.656 1 -10 2 -5 8129.23 816.440 1 -10 2 -6 2060.87 430.180 1 -10 2 -7 400.238 241.328 1 -10 2 -8 531.479 222.596 1 10 -1 -9 690.401 238.804 5 10 -1 -8-67.8163 68.2610 5 10 -1 -7 483.230 176.029 5 10 -1 -6 362.972 176.444 5 10 -1 -5 975.795 249.141 5 -10 1 4 9148.67 899.408 1 10 -1 -4 8353.40 665.332 5 -10 1 3 3360.19 554.149 1 10 -1 -3 3545.86 417.402 5 -10 1 2 6041.87 715.258 1 10 -1 -2 6063.58 527.517 5 -10 1 1-43.5606 119.735 1 -10 1 0 1228.34 327.128 1 -10 1 -1 2472.31 446.010 1 -10 1 -2 3321.23 518.502 1 10 -1 3 5234.77 577.230 2 -10 1 -3 4524.67 598.598 1 10 -1 4 3466.57 480.780 2 -10 1 -4 3050.40 500.893 1 -10 1 -5 6575.25 734.038 1 -10 1 -6 2072.54 418.309 1 -10 1 -7 363.011 131.032 1 10 0 -8 487.213 167.028 5 10 0 -7 336.058 190.193 5 10 0 -6 7673.59 686.525 5 10 0 -5 16226.4 992.287 5 10 0 -4 6690.98 604.480 5 10 0 -3 306.118 118.420 5 -10 0 3 352.326 198.435 1 10 0 -2 50.6599 86.8399 5 -10 0 2-294.320 179.669 1 -10 0 1 130.870 146.097 1 -10 0 0 282.652 172.309 1 -10 0 -1 995.806 293.136 1 10 0 1 1121.36 281.166 2 -10 0 -2 1365.69 338.559 1 10 0 2 424.357 216.104 2 -10 0 -3 1365.64 339.422 1 10 0 3 1190.00 282.311 2 -10 0 -4 864.150 258.593 1 -10 0 -5 43.3559 101.272 1 10 1 -8 3431.81 494.141 5 10 1 -7 7271.27 698.461 5 10 1 -6 3429.45 464.291 5 10 1 -5 1302.95 289.699 5 10 1 -4-170.736 122.237 5 10 1 -3-251.568 139.660 5 10 1 -2 1541.12 281.277 5 -10 -1 1 2361.07 447.129 1 -10 -1 0 2097.19 417.886 1 10 1 0 2837.42 430.751 2 -10 -1 -1 3161.27 494.597 1 10 1 1 3845.51 504.880 2 -10 -1 -2 1153.22 301.006 1 10 2 -7 2658.10 431.842 5 10 2 -6 89.5701 129.070 5 10 2 -5 44.0413 107.213 5 10 2 -4-55.3402 113.917 5 10 2 -3 1053.70 258.297 5 10 2 -2 3250.29 421.434 5 10 2 -1 5794.06 612.816 2 10 3 -5 3663.94 498.858 5 10 3 -4 5192.83 580.113 5 10 3 -3 5271.81 575.230 5 11 -7 -6 2541.87 412.181 5 11 -7 -5 631.224 209.167 5 11 -6 -6 2317.51 410.684 5 11 -6 -5 208.096 134.034 5 11 -6 -4 1575.70 309.511 5 11 -5 -7 968.044 346.478 5 11 -5 -6 14.6669 112.861 5 11 -5 -5 879.811 279.634 5 11 -5 -4 6005.45 670.053 5 -11 5 1 436.264 285.521 1 -11 5 0 623.153 274.222 1 -11 5 -1 306.709 208.000 1 11 -4 -7 534.975 202.131 5 11 -4 -6 2430.74 490.547 5 11 -4 -5 4276.32 631.520 5 11 -4 -4 5239.61 658.282 5 -11 4 3 244.732 205.134 1 -11 4 2 895.196 309.843 1 -11 4 1 153.518 161.631 1 -11 4 0 242.067 165.262 1 -11 4 -1 153.464 190.122 1 -11 4 -2 1260.87 380.026 1 -11 4 -3 4766.48 658.605 1 11 -3 -7 194.119 136.131 5 11 -3 -6 625.611 234.358 5 11 -3 -5 3637.64 540.919 5 11 -3 -4 819.839 250.304 5 -11 3 3 108.078 187.228 1 -11 3 2 229.440 193.419 1 -11 3 1 369.115 231.653 1 -11 3 0 1368.79 386.557 1 -11 3 -1 4258.63 638.175 1 -11 3 -2 3171.08 535.638 1 -11 3 -3 1435.14 369.956 1 -11 3 -4 1373.01 391.799 1 11 -2 -7 2480.04 434.660 5 11 -2 -6 2003.28 386.240 5 11 -2 -5 122.892 115.301 5 11 -2 -4 738.606 206.646 5 -11 2 4 218.111 188.029 1 -11 2 3 413.548 248.960 1 -11 2 2 3872.34 615.367 1 -11 2 1 7283.01 822.357 1 -11 2 0 5585.46 728.322 1 -11 2 -1 937.906 291.728 1 -11 2 -2 1457.83 387.562 1 -11 2 -3 773.653 285.982 1 -11 2 -4 2815.01 510.102 1 -11 2 -5 1103.97 328.744 1 11 -1 -7 135.848 117.760 5 11 -1 -6 170.533 115.798 5 11 -1 -5-12.0576 81.2216 5 11 -1 -4 850.150 231.817 5 -11 1 3 4071.15 637.636 1 -11 1 2 1203.22 341.450 1 -11 1 1-223.758 204.095 1 -11 1 0 1360.73 358.749 1 -11 1 -1 640.786 276.241 1 -11 1 -2 355.738 194.484 1 -11 1 -3 1415.79 376.243 1 -11 1 -4 6318.42 746.441 1 11 0 -6 193.561 168.070 5 11 0 -5 1319.02 295.308 5 -11 0 2 5260.03 694.187 1 -11 0 1 775.339 280.805 1 -11 0 0 438.461 234.016 1 -11 0 -1 59.2112 111.267 1 -11 0 -2 672.652 267.894 1 11 1 -5 8201.28 739.366 5 -11 -1 0 1950.80 426.981 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 66380 data_2 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C H4 O)' _chemical_formula_sum 'C38 H40 Cl2 Cu N8 O10' _chemical_formula_weight 903.22 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3557(7) _cell_length_b 9.8380(10) _cell_length_c 13.0238(10) _cell_angle_alpha 75.710(8) _cell_angle_beta 89.649(6) _cell_angle_gamma 69.657(8) _cell_volume 1084.99(17) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 8876 _cell_measurement_theta_min 3.1232 _cell_measurement_theta_max 28.8126 _exptl_crystal_description prism _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.382 _exptl_crystal_F_000 467 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.20 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.13 _exptl_absorpt_coefficient_mu 0.689 _shelx_estimated_absorpt_T_min 0.874 _shelx_estimated_absorpt_T_max 0.916 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.896 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 15902 _diffrn_reflns_av_unetI/netI 0.0255 _diffrn_reflns_av_R_equivalents 0.0348 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 3.129 _diffrn_reflns_theta_max 24.997 _diffrn_reflns_theta_full 24.997 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 0.995 _reflns_number_total 3791 _reflns_number_gt 3516 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0915P)^2^+2.8379P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3791 _refine_ls_number_parameters 334 _refine_ls_number_restraints 82 _refine_ls_R_factor_all 0.0688 _refine_ls_R_factor_gt 0.0651 _refine_ls_wR_factor_ref 0.1722 _refine_ls_wR_factor_gt 0.1685 _refine_ls_goodness_of_fit_ref 1.050 _refine_ls_restrained_S_all 1.111 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.0244(2) Uani 1 2 d S . P . . N1A N 0.2751(4) -0.3818(3) -0.0779(2) 0.0286(7) Uani 1 1 d D . . . . H1A H 0.285(5) -0.469(3) -0.085(4) 0.043 Uiso 1 1 d D U . . . C2A C 0.1511(4) -0.2971(4) -0.0415(3) 0.0288(8) Uani 1 1 d . . . . . H2A H 0.0653 -0.3249 -0.0213 0.035 Uiso 1 1 calc R U . . . N3A N 0.1644(3) -0.1685(3) -0.0374(2) 0.0250(6) Uani 1 1 d . . . . . C4A C 0.3046(4) -0.1738(4) -0.0718(3) 0.0251(7) Uani 1 1 d . . . . . H4A H 0.3458 -0.0970 -0.0767 0.030 Uiso 1 1 calc R U . . . C5A C 0.3766(4) -0.3063(4) -0.0982(3) 0.0249(7) Uani 1 1 d . . . . . C6A C 0.5236(4) -0.3638(4) -0.1405(3) 0.0295(8) Uani 1 1 d . . . . . C7A C 0.5616(5) -0.4865(4) -0.1835(3) 0.0378(9) Uani 1 1 d . . . . . H7A H 0.4904 -0.5351 -0.1860 0.045 Uiso 1 1 calc R U . . . C8A C 0.7026(6) -0.5382(5) -0.2227(4) 0.0473(11) Uani 1 1 d . . . . . H8A H 0.7273 -0.6222 -0.2519 0.057 Uiso 1 1 calc R U . . . C9A C 0.8067(6) -0.4703(6) -0.2199(4) 0.0542(13) Uani 1 1 d . . . . . H9A H 0.9032 -0.5067 -0.2472 0.065 Uiso 1 1 calc R U . . . C10A C 0.7710(6) -0.3475(6) -0.1769(4) 0.0561(13) Uani 1 1 d . . . . . H10A H 0.8432 -0.3000 -0.1749 0.067 Uiso 1 1 calc R U . . . C11A C 0.6310(5) -0.2944(5) -0.1373(4) 0.0432(10) Uani 1 1 d . . . . . H11A H 0.6073 -0.2106 -0.1079 0.052 Uiso 1 1 calc R U . . . N1B N 0.2795(4) -0.1090(5) 0.2767(3) 0.0461(9) Uani 1 1 d D . . . . H1B H 0.370(3) -0.129(7) 0.304(4) 0.069 Uiso 1 1 d D U . . . C2B C 0.2518(5) -0.0680(5) 0.1700(3) 0.0414(10) Uani 1 1 d . . . . . H2B H 0.3250 -0.0550 0.1213 0.050 Uiso 1 1 calc R U . . . N3B N 0.1095(4) -0.0484(3) 0.1424(2) 0.0284(7) Uani 1 1 d . . . . . C4B C 0.0435(4) -0.0801(4) 0.2355(3) 0.0343(9) Uani 1 1 d D . . . . H4B H -0.0596 -0.0750 0.2401 0.041 Uiso 1 1 calc R U . . . C5B C 0.1487(5) -0.1202(5) 0.3209(3) 0.0422(11) Uani 1 1 d D . . . . C6B C 0.1625(17) -0.1359(14) 0.4335(5) 0.043(5) Uani 0.357(18) 1 d DG . P A 1 C7B C 0.2580(18) -0.1080(15) 0.5006(8) 0.056(5) Uani 0.357(18) 1 d G . P A 1 H7B H 0.3277 -0.0610 0.4715 0.067 Uiso 0.357(18) 1 calc R U P A 1 C8B C 0.2514(19) -0.1489(16) 0.6100(7) 0.068(6) Uani 0.357(18) 1 d G . P A 1 H8B H 0.3166 -0.1299 0.6559 0.082 Uiso 0.357(18) 1 calc R U P A 1 C9B C 0.1494(19) -0.2177(17) 0.6525(5) 0.052(6) Uani 0.357(18) 1 d G . P A 1 H9B H 0.1450 -0.2457 0.7274 0.062 Uiso 0.357(18) 1 calc R U P A 1 C10B C 0.0540(16) -0.2456(17) 0.5855(8) 0.062(5) Uani 0.357(18) 1 d G U P A 1 H10B H -0.0157 -0.2926 0.6145 0.074 Uiso 0.357(18) 1 calc R U P A 1 C11B C 0.0605(15) -0.2047(15) 0.4760(7) 0.053(5) Uani 0.357(18) 1 d G . P A 1 H11B H -0.0047 -0.2237 0.4302 0.064 Uiso 0.357(18) 1 calc R U P A 1 C6C C 0.1275(8) -0.1807(9) 0.4350(3) 0.032(2) Uani 0.643(18) 1 d DG . P A 2 C7C C 0.2057(8) -0.1521(8) 0.5128(4) 0.043(2) Uani 0.643(18) 1 d G . P A 2 H7C H 0.2708 -0.0961 0.4929 0.051 Uiso 0.643(18) 1 calc R U P A 2 C8C C 0.1887(8) -0.2056(10) 0.6196(3) 0.051(4) Uani 0.643(18) 1 d G . P A 2 H8C H 0.2421 -0.1861 0.6728 0.061 Uiso 0.643(18) 1 calc R U P A 2 C9C C 0.0935(8) -0.2875(12) 0.6487(3) 0.064(3) Uani 0.643(18) 1 d G . P A 2 H9C H 0.0818 -0.3241 0.7217 0.076 Uiso 0.643(18) 1 calc R U P A 2 C10C C 0.0153(8) -0.3161(12) 0.5709(5) 0.078(3) Uani 0.643(18) 1 d G U P A 2 H10C H -0.0498 -0.3721 0.5908 0.094 Uiso 0.643(18) 1 calc R U P A 2 C11C C 0.0323(8) -0.2627(11) 0.4641(4) 0.059(3) Uani 0.643(18) 1 d G U P A 2 H11C H -0.0211 -0.2822 0.4110 0.070 Uiso 0.643(18) 1 calc R U P A 2 Cl Cl 0.23884(13) 0.24685(13) -0.13218(8) 0.0438(3) Uani 1 1 d D U . . . O1 O 0.1628(4) 0.1711(4) -0.0620(3) 0.0501(8) Uani 1 1 d . . . . . O2A O 0.239(2) 0.2079(19) -0.2377(15) 0.044(4) Uani 0.3 1 d . U P B 1 O3A O 0.3777(16) 0.261(2) -0.1141(11) 0.068(4) Uani 0.3 1 d . U P B 1 O4A O 0.1474(16) 0.3971(12) -0.1072(13) 0.061(4) Uani 0.3 1 d D U P B 1 O2B O 0.1839(9) 0.2611(12) -0.2371(8) 0.072(3) Uani 0.7 1 d . U P B 2 O3B O 0.4006(6) 0.1590(7) -0.1004(5) 0.0598(15) Uani 0.7 1 d . . P B 2 O4B O 0.2095(10) 0.3943(8) -0.1380(7) 0.079(2) Uani 0.7 1 d . U P B 2 O5 O 0.5622(7) 0.8036(8) 0.3920(5) 0.127(2) Uani 1 1 d D U . . . H5 H 0.621(12) 0.820(11) 0.340(7) 0.191 Uiso 1 1 d D U . . . C12A C 0.6285(17) 0.6510(15) 0.4651(12) 0.127(2) Uani 0.65 1 d D U P C 1 H12A H 0.7399 0.6129 0.4628 0.191 Uiso 0.65 1 calc R U P C 1 H12B H 0.5856 0.5838 0.4431 0.191 Uiso 0.65 1 calc R U P C 1 H12C H 0.6040 0.6553 0.5377 0.191 Uiso 0.65 1 calc R U P C 1 C12B C 0.657(3) 0.730(4) 0.4822(19) 0.127(2) Uani 0.35 1 d D U P C 2 H12D H 0.7297 0.7810 0.4871 0.191 Uiso 0.35 1 calc R U P C 2 H12E H 0.7138 0.6265 0.4805 0.191 Uiso 0.35 1 calc R U P C 2 H12F H 0.5972 0.7309 0.5441 0.191 Uiso 0.35 1 calc R U P C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0246(3) 0.0307(4) 0.0176(3) -0.0071(2) -0.0007(2) -0.0089(3) N1A 0.0394(18) 0.0243(15) 0.0243(15) -0.0063(12) -0.0001(13) -0.0141(14) C2A 0.0340(19) 0.0348(19) 0.0217(17) -0.0058(15) -0.0001(14) -0.0181(16) N3A 0.0304(16) 0.0261(15) 0.0185(14) -0.0047(11) -0.0022(12) -0.0107(13) C4A 0.0280(18) 0.0227(17) 0.0243(17) -0.0047(13) -0.0013(14) -0.0096(14) C5A 0.0309(18) 0.0231(16) 0.0185(16) -0.0011(13) -0.0041(13) -0.0099(14) C6A 0.0340(19) 0.0234(17) 0.0234(18) -0.0029(14) -0.0018(14) -0.0031(15) C7A 0.043(2) 0.0283(19) 0.035(2) -0.0085(16) -0.0013(17) -0.0039(17) C8A 0.051(3) 0.035(2) 0.041(2) -0.0131(19) 0.002(2) 0.004(2) C9A 0.041(3) 0.061(3) 0.045(3) -0.016(2) 0.011(2) 0.002(2) C10A 0.041(3) 0.069(3) 0.062(3) -0.023(3) 0.013(2) -0.021(2) C11A 0.038(2) 0.048(2) 0.048(3) -0.020(2) 0.0102(19) -0.016(2) N1B 0.040(2) 0.058(2) 0.0356(19) -0.0170(17) -0.0169(16) -0.0081(18) C2B 0.036(2) 0.060(3) 0.033(2) -0.0135(19) -0.0038(17) -0.021(2) N3B 0.0289(16) 0.0347(17) 0.0206(15) -0.0100(12) -0.0016(12) -0.0084(13) C4B 0.0302(19) 0.040(2) 0.0202(18) -0.0072(15) -0.0007(15) 0.0016(16) C5B 0.039(2) 0.046(2) 0.026(2) -0.0150(18) -0.0052(17) 0.0081(19) C6B 0.045(9) 0.030(8) 0.047(10) -0.015(6) -0.007(7) -0.003(6) C7B 0.086(13) 0.065(10) 0.035(7) -0.015(7) -0.012(7) -0.047(9) C8B 0.094(15) 0.059(10) 0.048(9) -0.015(8) -0.022(9) -0.022(10) C9B 0.067(12) 0.066(11) 0.013(7) 0.003(7) -0.006(8) -0.020(9) C10B 0.069(8) 0.065(8) 0.039(7) -0.008(6) 0.005(6) -0.012(6) C11B 0.073(13) 0.052(9) 0.020(7) -0.007(7) -0.011(7) -0.006(9) C6C 0.033(4) 0.038(5) 0.014(4) -0.009(3) -0.007(3) 0.002(4) C7C 0.043(5) 0.054(5) 0.029(4) -0.016(3) -0.013(3) -0.011(3) C8C 0.058(6) 0.066(7) 0.017(4) -0.008(4) -0.006(4) -0.012(5) C9C 0.060(5) 0.103(8) 0.017(4) 0.000(4) -0.005(3) -0.025(5) C10C 0.085(6) 0.117(8) 0.040(4) 0.001(4) -0.002(4) -0.061(6) C11C 0.067(5) 0.086(6) 0.030(4) -0.006(4) -0.002(3) -0.043(5) Cl 0.0465(6) 0.0568(7) 0.0348(5) -0.0016(5) 0.0004(4) -0.0335(5) O1 0.064(2) 0.0514(19) 0.0496(19) -0.0175(15) 0.0183(16) -0.0350(17) O2A 0.067(11) 0.058(8) 0.036(7) -0.032(7) 0.021(8) -0.043(8) O3A 0.048(7) 0.111(10) 0.052(7) -0.015(7) 0.010(5) -0.042(8) O4A 0.075(7) 0.061(7) 0.061(7) 0.007(5) -0.016(5) -0.056(6) O2B 0.051(5) 0.126(8) 0.037(3) -0.016(5) 0.001(3) -0.031(5) O3B 0.024(2) 0.069(4) 0.096(4) -0.045(4) 0.012(2) -0.012(3) O4B 0.094(5) 0.056(4) 0.091(6) 0.004(3) -0.033(4) -0.048(4) O5 0.092(3) 0.155(4) 0.114(4) -0.028(3) -0.052(3) -0.022(3) C12A 0.092(3) 0.155(4) 0.114(4) -0.028(3) -0.052(3) -0.022(3) C12B 0.092(3) 0.155(4) 0.114(4) -0.028(3) -0.052(3) -0.022(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3B 1.991(3) 2 ? Cu N3B 1.991(3) . ? Cu N3A 1.992(3) . ? Cu N3A 1.992(3) 2 ? N1A C2A 1.335(5) . ? N1A C5A 1.383(5) . ? N1A H1A 0.857(10) . ? C2A N3A 1.327(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.371(5) . ? C4A C5A 1.370(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.456(5) . ? C6A C7A 1.390(5) . ? C6A C11A 1.403(6) . ? C7A C8A 1.383(6) . ? C7A H7A 0.9500 . ? C8A C9A 1.365(8) . ? C8A H8A 0.9500 . ? C9A C10A 1.391(8) . ? C9A H9A 0.9500 . ? C10A C11A 1.380(7) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.348(6) . ? N1B C5B 1.376(6) . ? N1B H1B 0.857(10) . ? C2B N3B 1.315(5) . ? C2B H2B 0.9500 . ? N3B C4B 1.374(5) . ? C4B C5B 1.375(4) . ? C4B H4B 0.9500 . ? C5B C6B 1.438(6) . ? C5B C6C 1.498(5) . ? C6B C7B 1.3900 . ? C6B C11B 1.3900 . ? C7B C8B 1.3900 . ? C7B H7B 0.9500 . ? C8B C9B 1.3900 . ? C8B H8B 0.9500 . ? C9B C10B 1.3900 . ? C9B H9B 0.9500 . ? C10B C11B 1.3900 . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? C6C C7C 1.3900 . ? C6C C11C 1.3900 . ? C7C C8C 1.3900 . ? C7C H7C 0.9500 . ? C8C C9C 1.3900 . ? C8C H8C 0.9500 . ? C9C C10C 1.3900 . ? C9C H9C 0.9500 . ? C10C C11C 1.3900 . ? C10C H10C 0.9500 . ? C11C H11C 0.9500 . ? Cl O4B 1.362(7) . ? Cl O3A 1.384(13) . ? Cl O1 1.386(3) . ? Cl O2B 1.420(10) . ? Cl O3B 1.459(5) . ? Cl O2A 1.515(17) . ? Cl O4A 1.542(9) . ? O5 C12B 1.357(16) . ? O5 C12A 1.483(11) . ? O5 H5 0.89(2) . ? C12A H12A 0.9800 . ? C12A H12B 0.9800 . ? C12A H12C 0.9800 . ? C12B H12D 0.9800 . ? C12B H12E 0.9800 . ? C12B H12F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Cu N3B 180.0 2 . ? N3B Cu N3A 89.00(12) 2 . ? N3B Cu N3A 91.01(12) . . ? N3B Cu N3A 91.00(12) 2 2 ? N3B Cu N3A 89.00(12) . 2 ? N3A Cu N3A 180.00(14) . 2 ? C2A N1A C5A 108.7(3) . . ? C2A N1A H1A 122(3) . . ? C5A N1A H1A 129(3) . . ? N3A C2A N1A 110.5(3) . . ? N3A C2A H2A 124.7 . . ? N1A C2A H2A 124.7 . . ? C2A N3A C4A 106.2(3) . . ? C2A N3A Cu 124.6(3) . . ? C4A N3A Cu 129.1(2) . . ? C5A C4A N3A 110.0(3) . . ? C5A C4A H4A 125.0 . . ? N3A C4A H4A 125.0 . . ? C4A C5A N1A 104.5(3) . . ? C4A C5A C6A 131.3(3) . . ? N1A C5A C6A 124.1(3) . . ? C7A C6A C11A 118.8(4) . . ? C7A C6A C5A 121.9(4) . . ? C11A C6A C5A 119.3(3) . . ? C8A C7A C6A 120.3(4) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C9A C8A C7A 120.9(4) . . ? C9A C8A H8A 119.5 . . ? C7A C8A H8A 119.5 . . ? C8A C9A C10A 119.7(4) . . ? C8A C9A H9A 120.2 . . ? C10A C9A H9A 120.2 . . ? C11A C10A C9A 120.3(5) . . ? C11A C10A H10A 119.8 . . ? C9A C10A H10A 119.8 . . ? C10A C11A C6A 120.1(4) . . ? C10A C11A H11A 120.0 . . ? C6A C11A H11A 120.0 . . ? C2B N1B C5B 108.4(3) . . ? C2B N1B H1B 119(4) . . ? C5B N1B H1B 132(4) . . ? N3B C2B N1B 110.8(4) . . ? N3B C2B H2B 124.6 . . ? N1B C2B H2B 124.6 . . ? C2B N3B C4B 106.2(3) . . ? C2B N3B Cu 131.1(3) . . ? C4B N3B Cu 122.5(2) . . ? N3B C4B C5B 109.9(3) . . ? N3B C4B H4B 125.1 . . ? C5B C4B H4B 125.1 . . ? C4B C5B N1B 104.7(3) . . ? C4B C5B C6B 142.8(7) . . ? N1B C5B C6B 110.5(7) . . ? C4B C5B C6C 126.2(4) . . ? N1B C5B C6C 128.7(4) . . ? C7B C6B C11B 120.0 . . ? C7B C6B C5B 134.1(8) . . ? C11B C6B C5B 105.7(7) . . ? C6B C7B C8B 120.0 . . ? C6B C7B H7B 120.0 . . ? C8B C7B H7B 120.0 . . ? C9B C8B C7B 120.0 . . ? C9B C8B H8B 120.0 . . ? C7B C8B H8B 120.0 . . ? C8B C9B C10B 120.0 . . ? C8B C9B H9B 120.0 . . ? C10B C9B H9B 120.0 . . ? C11B C10B C9B 120.0 . . ? C11B C10B H10B 120.0 . . ? C9B C10B H10B 120.0 . . ? C10B C11B C6B 120.0 . . ? C10B C11B H11B 120.0 . . ? C6B C11B H11B 120.0 . . ? C7C C6C C11C 120.0 . . ? C7C C6C C5B 118.1(4) . . ? C11C C6C C5B 121.9(4) . . ? C6C C7C C8C 120.0 . . ? C6C C7C H7C 120.0 . . ? C8C C7C H7C 120.0 . . ? C9C C8C C7C 120.0 . . ? C9C C8C H8C 120.0 . . ? C7C C8C H8C 120.0 . . ? C10C C9C C8C 120.0 . . ? C10C C9C H9C 120.0 . . ? C8C C9C H9C 120.0 . . ? C11C C10C C9C 120.0 . . ? C11C C10C H10C 120.0 . . ? C9C C10C H10C 120.0 . . ? C10C C11C C6C 120.0 . . ? C10C C11C H11C 120.0 . . ? C6C C11C H11C 120.0 . . ? O4B Cl O1 118.5(5) . . ? O3A Cl O1 128.5(6) . . ? O4B Cl O2B 99.4(6) . . ? O1 Cl O2B 107.9(5) . . ? O4B Cl O3B 110.4(4) . . ? O1 Cl O3B 104.2(3) . . ? O2B Cl O3B 117.1(4) . . ? O3A Cl O2A 107.6(9) . . ? O1 Cl O2A 109.6(6) . . ? O3A Cl O4A 92.6(10) . . ? O1 Cl O4A 91.9(6) . . ? O2A Cl O4A 127.6(10) . . ? C12B O5 H5 106(9) . . ? C12A O5 H5 113(7) . . ? O5 C12A H12A 109.5 . . ? O5 C12A H12B 109.5 . . ? H12A C12A H12B 109.5 . . ? O5 C12A H12C 109.5 . . ? H12A C12A H12C 109.5 . . ? H12B C12A H12C 109.5 . . ? O5 C12B H12D 109.5 . . ? O5 C12B H12E 109.5 . . ? H12D C12B H12E 109.5 . . ? O5 C12B H12F 109.5 . . ? H12D C12B H12F 109.5 . . ? H12E C12B H12F 109.5 . . ? _refine_diff_density_max 1.390 _refine_diff_density_min -0.961 _refine_diff_density_rms 0.102 # start Validation Reply Form _vrf_PLAT301_2 ; RESPONSE: The structure exhibits significant disorder affecting: i) the phenyl ring of one ligand (modelled over two orientations with a 65:35 domain ratio), ii) the O2, O3 and O4 atoms of the coordinated perchlorate ion (30:70), and iii) the methanol solvent molecule (atom C12, 65:35), as calculated after detailed refinement. ; _vrf_PLAT933_2 ; RESPONSE: Those discordant reflections with a high error/esd value have been removed from the refinement. ; # end Validation Reply Form _shelx_res_file ; 2.res created by SHELXL-2014/7 TITL EL22A in P-1 CELL 0.71073 9.3557 9.8380 13.0238 75.710 89.649 69.657 ZERR 1 0.0007 0.0010 0.0010 0.008 0.006 0.008 LATT 1 SFAC C H N O CL CU UNIT 38 40 8 10 2 1 MERG 2 FMAP 2 OMIT -2 50 OMIT 1 3 4 OMIT -3 3 3 OMIT 2 0 1 OMIT 3 0 9 OMIT -1 1 4 OMIT 0 1 4 OMIT 3 0 0 OMIT -1 2 0 OMIT 2 2 2 OMIT 0 0 2 SIZE 0.20 0.17 0.13 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND $H HTAB L.S. 10 WGHT 0.091500 2.837900 FVAR 5.02973 0.35655 CU 6 0.000000 0.000000 0.000000 10.50000 0.02463 0.03066 = 0.01761 -0.00714 -0.00074 -0.00895 DFIX 0.86 0.01 N1A H1A N1B H1B N1A 3 0.275072 -0.381838 -0.077919 11.00000 0.03940 0.02427 = 0.02432 -0.00634 -0.00014 -0.01414 H1A 2 0.285085 -0.468813 -0.085169 11.00000 -1.50000 C2A 1 0.151116 -0.297073 -0.041499 11.00000 0.03399 0.03477 = 0.02167 -0.00576 -0.00009 -0.01811 AFIX 43 H2A 2 0.065350 -0.324901 -0.021322 11.00000 -1.20000 AFIX 0 N3A 3 0.164405 -0.168479 -0.037408 11.00000 0.03039 0.02607 = 0.01853 -0.00467 -0.00220 -0.01071 C4A 1 0.304599 -0.173843 -0.071814 11.00000 0.02797 0.02266 = 0.02434 -0.00472 -0.00128 -0.00956 AFIX 43 H4A 2 0.345779 -0.097002 -0.076672 11.00000 -1.20000 AFIX 0 C5A 1 0.376561 -0.306308 -0.098157 11.00000 0.03093 0.02309 = 0.01847 -0.00107 -0.00409 -0.00991 C6A 1 0.523614 -0.363811 -0.140466 11.00000 0.03396 0.02341 = 0.02340 -0.00289 -0.00178 -0.00313 C7A 1 0.561557 -0.486528 -0.183476 11.00000 0.04293 0.02830 = 0.03511 -0.00852 -0.00132 -0.00387 AFIX 43 H7A 2 0.490358 -0.535112 -0.185967 11.00000 -1.20000 AFIX 0 C8A 1 0.702576 -0.538242 -0.222680 11.00000 0.05089 0.03527 = 0.04126 -0.01306 0.00160 0.00441 AFIX 43 H8A 2 0.727270 -0.622202 -0.251940 11.00000 -1.20000 AFIX 0 C9A 1 0.806747 -0.470281 -0.219900 11.00000 0.04075 0.06084 = 0.04532 -0.01562 0.01102 0.00193 AFIX 43 H9A 2 0.903181 -0.506659 -0.247168 11.00000 -1.20000 AFIX 0 C10A 1 0.770953 -0.347511 -0.176938 11.00000 0.04066 0.06940 = 0.06245 -0.02269 0.01299 -0.02104 AFIX 43 H10A 2 0.843239 -0.300024 -0.174857 11.00000 -1.20000 AFIX 0 C11A 1 0.630983 -0.294352 -0.137328 11.00000 0.03837 0.04758 = 0.04815 -0.01997 0.01021 -0.01594 AFIX 43 H11A 2 0.607254 -0.210622 -0.107892 11.00000 -1.20000 AFIX 0 N1B 3 0.279457 -0.109044 0.276702 11.00000 0.04015 0.05789 = 0.03562 -0.01703 -0.01689 -0.00814 H1B 2 0.369873 -0.128645 0.303964 11.00000 -1.50000 C2B 1 0.251758 -0.068023 0.169984 11.00000 0.03585 0.05984 = 0.03250 -0.01354 -0.00385 -0.02071 AFIX 43 H2B 2 0.324973 -0.055032 0.121337 11.00000 -1.20000 AFIX 0 N3B 3 0.109533 -0.048427 0.142367 11.00000 0.02895 0.03471 = 0.02063 -0.01000 -0.00162 -0.00843 dfix 1.40 0.007 c4b c5b C4B 1 0.043471 -0.080052 0.235476 11.00000 0.03017 0.04035 = 0.02022 -0.00717 -0.00074 0.00164 AFIX 43 H4B 2 -0.059555 -0.074970 0.240122 11.00000 -1.20000 AFIX 0 C5B 1 0.148718 -0.120152 0.320923 11.00000 0.03931 0.04572 = 0.02581 -0.01498 -0.00523 0.00810 DFIX 1.5 0.01 C5B C6B DFIX 1.45 0.007 C5B C6C ISOR 0.01 C10B C10C C11C PART 1 AFIX 66 C6B 1 0.162531 -0.135891 0.433533 21.00000 0.04513 0.02967 = 0.04684 -0.01504 -0.00682 -0.00257 C7B 1 0.257960 -0.108022 0.500554 21.00000 0.08599 0.06474 = 0.03471 -0.01520 -0.01204 -0.04693 AFIX 43 H7B 2 0.327660 -0.061002 0.471526 21.00000 -1.20000 AFIX 65 C8B 1 0.251410 -0.148949 0.610049 21.00000 0.09357 0.05910 = 0.04838 -0.01480 -0.02227 -0.02194 AFIX 43 H8B 2 0.316633 -0.129901 0.655855 21.00000 -1.20000 AFIX 65 C9B 1 0.149430 -0.217746 0.652523 21.00000 0.06679 0.06560 = 0.01291 0.00298 -0.00639 -0.02014 AFIX 43 H9B 2 0.144954 -0.245718 0.727358 21.00000 -1.20000 AFIX 65 C10B 1 0.053999 -0.245617 0.585503 21.00000 0.06863 0.06532 = 0.03859 -0.00762 0.00482 -0.01200 AFIX 43 H10B 2 -0.015699 -0.292637 0.614533 21.00000 -1.20000 AFIX 65 C11B 1 0.060548 -0.204690 0.476009 21.00000 0.07307 0.05200 = 0.02014 -0.00720 -0.01068 -0.00575 AFIX 43 H11B 2 -0.004674 -0.223739 0.430203 21.00000 -1.20000 AFIX 66 PART 2 C6C 1 0.127544 -0.180682 0.435041 -21.00000 0.03267 0.03788 = 0.01384 -0.00864 -0.00695 0.00174 C7C 1 0.205737 -0.152146 0.512811 -21.00000 0.04317 0.05449 = 0.02884 -0.01561 -0.01323 -0.01129 AFIX 43 H7C 2 0.270822 -0.096124 0.492949 -21.00000 -1.20000 AFIX 65 C8C 1 0.188699 -0.205580 0.619642 -21.00000 0.05827 0.06638 = 0.01733 -0.00791 -0.00596 -0.01159 AFIX 43 H8C 2 0.242141 -0.186077 0.672794 -21.00000 -1.20000 AFIX 65 C9C 1 0.093469 -0.287550 0.648705 -21.00000 0.06003 0.10259 = 0.01701 -0.00027 -0.00496 -0.02549 AFIX 43 H9C 2 0.081825 -0.324069 0.721720 -21.00000 -1.20000 AFIX 65 C10C 1 0.015275 -0.316086 0.570936 -21.00000 0.08518 0.11712 = 0.04035 0.00107 -0.00215 -0.06054 AFIX 43 H10C 2 -0.049810 -0.372109 0.590800 -21.00000 -1.20000 AFIX 65 C11C 1 0.032312 -0.262653 0.464105 -21.00000 0.06736 0.08627 = 0.03000 -0.00595 -0.00162 -0.04273 AFIX 43 H11C 2 -0.021130 -0.282156 0.410953 -21.00000 -1.20000 AFIX 0 PART 0 ISOR 0.007 CL O4B O3A ISOR 0.010 O2B O2A ISOR 0.004 O4A DFIX 1.50 0.01 CL O4A CL 5 0.238845 0.246846 -0.132179 11.00000 0.04647 0.05676 = 0.03479 -0.00160 0.00042 -0.03350 O1 4 0.162810 0.171092 -0.061964 11.00000 0.06359 0.05138 = 0.04960 -0.01752 0.01828 -0.03499 PART 1 O2A 4 0.238829 0.207860 -0.237671 10.30000 0.06728 0.05764 = 0.03590 -0.03178 0.02094 -0.04334 O3A 4 0.377706 0.261479 -0.114125 10.30000 0.04768 0.11111 = 0.05237 -0.01454 0.00995 -0.04177 O4A 4 0.147438 0.397146 -0.107162 10.30000 0.07488 0.06076 = 0.06060 0.00726 -0.01571 -0.05641 PART 2 O2B 4 0.183947 0.261081 -0.237109 10.70000 0.05136 0.12572 = 0.03672 -0.01620 0.00071 -0.03135 O3B 4 0.400554 0.158967 -0.100446 10.70000 0.02393 0.06899 = 0.09572 -0.04492 0.01204 -0.01187 O4B 4 0.209483 0.394274 -0.137984 10.70000 0.09420 0.05579 = 0.09057 0.00428 -0.03338 -0.04761 PART 0 DFIX 1.40 0.015 O5 C12A DFIX 1.42 0.02 O5 C12B EADP O5 C12A C12B ISOR 0.007 O5 C12A C12B EQIV $1 1-x, 1-y, -z DFIX 0.84 0.025 O5 H5 DFIX 1.80 0.03 H5 O2A_$1 O5 4 0.562156 0.803550 0.391996 11.00000 0.09189 0.15458 = 0.11409 -0.02751 -0.05194 -0.02222 H5 2 0.621186 0.820026 0.340433 11.00000 -1.50000 PART 1 C12A 1 0.628532 0.650958 0.465098 10.65000 0.09189 0.15458 = 0.11409 -0.02751 -0.05194 -0.02222 AFIX 137 H12A 2 0.739883 0.612937 0.462767 10.65000 -1.50000 H12B 2 0.585582 0.583757 0.443087 10.65000 -1.50000 H12C 2 0.603995 0.655340 0.537747 10.65000 -1.50000 AFIX 0 PART 2 C12B 1 0.657326 0.730419 0.482186 10.35000 0.09189 0.15458 = 0.11409 -0.02751 -0.05194 -0.02222 AFIX 137 H12D 2 0.729682 0.780987 0.487131 10.35000 -1.50000 H12E 2 0.713839 0.626492 0.480512 10.35000 -1.50000 H12F 2 0.597208 0.730947 0.544069 10.35000 -1.50000 AFIX 0 HKLF 4 REM EL22A in P-1 REM R1 = 0.0651 for 3516 Fo > 4sig(Fo) and 0.0688 for all 3791 data REM 334 parameters refined using 82 restraints END WGHT 0.0910 2.8479 REM Instructions for potential hydrogen bonds EQIV $2 x, y-1, z HTAB N1A O3A_$2 HTAB N1A O4A_$2 HTAB N1A O4B_$2 EQIV $3 -x, -y, -z HTAB C2A O1_$3 HTAB C4A O1 HTAB N1B O5_$2 EQIV $4 -x+1, -y, -z HTAB C2B O3B_$4 HTAB C4B O2A_$3 HTAB C4B O2B_$3 HTAB O5 O2A_$1 HTAB O5 O2B_$1 REM Highest difference peak 1.390, deepest hole -0.961, 1-sigma level 0.102 Q1 1 0.5470 0.5382 0.4706 11.00000 0.05 1.39 Q2 1 0.5812 0.9235 0.4400 11.00000 0.05 1.37 Q3 1 0.5165 -0.0681 0.6259 11.00000 0.05 1.26 Q4 1 0.5696 0.8800 0.3609 11.00000 0.05 0.86 Q5 1 0.0991 0.4231 -0.0975 11.00000 0.05 0.82 Q6 1 0.1992 0.3229 -0.1220 11.00000 0.05 0.82 Q7 1 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545.358 9 -2 -8 6 7641.99 432.323 8 -2 -8 6 7828.26 428.328 4 -2 -8 6 6895.10 410.272 2 -2 -8 6 7945.41 422.074 1 -2 -8 7 1806.71 213.792 8 -2 -8 7 1975.26 208.768 1 -2 -8 7 1980.10 220.697 4 -2 -8 7 1557.82 204.684 2 -2 -8 8 14.2151 58.5470 1 -2 -8 8 42.8881 60.9177 2 -2 -8 9-48.3726 67.8215 2 -2 -8 10 375.488 125.272 2 -2 -7 -16 871.224 167.400 6 -2 -7 -16 1118.65 198.506 1 -2 -7 -15 1447.78 204.024 6 -2 -7 -15 1413.83 223.304 1 -2 -7 -14-73.0722 60.6332 6 -2 -7 -14-131.520 97.9048 1 -2 -7 -13 619.411 121.399 6 -2 -7 -13 393.353 107.854 1 -2 -7 -12 48.2644 54.4462 6 -2 -7 -12-23.8344 67.2945 1 -2 -7 -11 7300.94 389.822 6 -2 -7 -11 6847.43 428.159 1 -2 -7 -10 6153.40 336.318 6 -2 -7 -10 6164.69 392.898 1 -2 -7 -9 17835.8 593.736 6 -2 -7 -9 17355.1 685.372 1 -2 -7 -8 25082.8 827.724 1 -2 -7 -8 24102.7 760.776 9 -2 -7 -7 14521.8 583.557 1 -2 -7 -7 14397.5 554.738 9 -2 -7 -6 1569.54 180.096 1 -2 -7 -6 1606.36 172.829 9 -2 -7 -5 2157.42 202.129 1 -2 -7 -5 2095.06 198.048 9 -2 -7 -4 861.612 128.517 1 -2 -7 -4 879.911 138.182 9 -2 -7 -3 5281.17 303.843 1 -2 -7 -3 5533.41 335.688 9 -2 -7 -2 23615.3 722.938 1 -2 -7 -2 23299.3 778.798 9 -2 -7 -1 27095.5 783.594 1 -2 -7 -1 26603.7 864.129 9 -2 -7 0 6954.49 342.478 1 -2 -7 0 7491.38 354.834 8 -2 -7 0 7616.63 412.042 9 -2 -7 1 461.596 92.2774 8 -2 -7 1 221.669 92.4389 9 -2 -7 1 375.655 81.5792 4 -2 -7 1 330.610 82.3048 1 -2 -7 2 106.957 57.7029 8 -2 -7 2 186.216 64.2609 4 -2 -7 2 191.609 78.4708 9 -2 -7 2 130.601 58.0568 1 -2 -7 3 26.3234 36.2842 1 -2 -7 3 164.436 61.2479 8 -2 -7 3-12.8663 44.8861 4 -2 -7 3 113.985 62.4753 2 -2 -7 3 73.4416 54.8355 9 -2 -7 4 685.680 121.136 8 -2 -7 4 669.026 116.306 4 -2 -7 4 492.767 101.108 2 -2 -7 4 515.815 97.7124 1 -2 -7 4 636.488 129.811 9 -2 -7 5 5344.04 330.644 8 -2 -7 5 5431.93 329.848 4 -2 -7 5 5621.98 339.155 2 -2 -7 5 5618.25 319.252 1 -2 -7 5 5699.00 375.393 9 -2 -7 6 11599.7 520.578 4 -2 -7 6 11870.9 493.179 1 -2 -7 6 11652.5 524.641 8 -2 -7 6 11683.7 531.001 2 -2 -7 7 5133.94 314.585 1 -2 -7 7 5232.73 396.449 7 -2 -7 7 5256.81 354.926 8 -2 -7 7 5389.17 355.946 4 -2 -7 7 5294.11 357.987 2 -2 -7 8 59.0544 69.6608 2 -2 -7 8-66.4023 113.274 7 -2 -7 8 9.93936 46.9338 1 -2 -7 9 1408.59 166.671 1 -2 -7 9 1098.66 191.595 7 -2 -7 9 1378.23 197.632 2 -2 -7 10 583.478 139.850 2 -2 -7 10 444.234 133.044 7 -2 -7 11 165.838 112.266 7 -2 -7 11 372.170 130.559 2 -2 -6 -17 55.3444 64.2107 6 -2 -6 -17 571.768 146.676 1 -2 -6 -16 866.982 164.000 6 -2 -6 -16 839.956 179.592 1 -2 -6 -15 2223.33 248.325 6 -2 -6 -15 2369.41 281.053 1 -2 -6 -14 5000.41 359.667 6 -2 -6 -14 5449.80 413.722 1 -2 -6 -13 2167.66 222.120 6 -2 -6 -13 2004.27 243.923 1 -2 -6 -12 440.907 109.447 6 -2 -6 -12 676.860 139.675 1 -2 -6 -11 2864.30 238.323 6 -2 -6 -11 2975.40 278.268 1 -2 -6 -10 1403.61 185.372 1 -2 -6 -10 1480.80 158.865 6 -2 -6 -9 4269.05 263.011 6 -2 -6 -9 4129.08 302.724 1 -2 -6 -8 32780.9 974.700 1 -2 -6 -7 55254.9 1255.27 6 -2 -6 -7 58432.3 1413.65 1 -2 -6 -7 58530.3 1326.38 9 -2 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44.9169 1 -2 -5 6 7697.37 387.126 8 -2 -5 6 7838.16 329.083 1 -2 -5 6 7212.57 373.819 4 -2 -5 6 6811.97 363.961 2 -2 -5 6 7292.06 399.462 7 -2 -5 7 7720.19 408.833 8 -2 -5 7 6805.60 320.173 1 -2 -5 7 7675.95 403.107 4 -2 -5 7 7604.58 417.798 7 -2 -5 7 7885.77 409.947 2 -2 -5 8 7545.14 344.193 1 -2 -5 8 7608.72 436.708 7 -2 -5 8 7292.55 419.097 2 -2 -5 9 1750.92 209.855 2 -2 -5 9 1503.86 203.396 7 -2 -5 9 1431.84 150.522 1 -2 -5 10 2005.80 240.667 7 -2 -5 10 1674.13 215.777 2 -2 -5 11 1380.30 206.081 2 -2 -5 11 1425.06 219.427 7 -2 -5 12 744.970 173.741 7 -2 -5 12 934.146 169.349 2 -2 -5 13 102.039 92.0698 7 -2 -5 13-7.86748 68.1140 2 -2 -4 -17 2330.58 287.495 6 -2 -4 -17 2279.87 297.568 1 -2 -4 -16 335.301 121.262 6 -2 -4 -16 211.393 102.271 1 -2 -4 -15 1053.04 196.910 1 -2 -4 -15 1290.79 195.615 6 -2 -4 -14 5756.36 389.236 6 -2 -4 -14 4901.57 391.943 1 -2 -4 -13 4748.39 337.694 6 -2 -4 -13 4790.02 369.201 1 -2 -4 -12 8250.98 435.946 6 -2 -4 -12 8222.49 478.165 1 -2 -4 -11 2221.99 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5 3976.57 253.257 7 -2 -4 5 3757.45 241.539 2 -2 -4 6 2774.87 217.959 8 -2 -4 6 2700.11 166.274 1 -2 -4 6 2888.72 221.399 4 -2 -4 6 2480.30 203.248 2 -2 -4 6 2831.14 221.400 7 -2 -4 7 47.3867 38.9254 8 -2 -4 7 67.1474 50.1459 7 -2 -4 7 84.8951 39.3939 1 -2 -4 7 136.113 58.0908 2 -2 -4 8 105.871 58.2209 7 -2 -4 8 87.0662 45.3792 1 -2 -4 8 150.742 71.8324 2 -2 -4 9-3.98907 60.2900 7 -2 -4 9 90.0001 83.3118 2 -2 -4 10 139.958 61.3523 7 -2 -4 10 169.755 93.9934 2 -2 -4 11 7840.14 478.075 7 -2 -4 11 7807.52 481.595 2 -2 -4 12 6296.08 444.953 7 -2 -4 12 6379.71 451.620 2 -2 -4 13 2905.91 310.381 7 -2 -4 13 2580.06 297.780 2 -2 -4 14 638.570 162.931 7 -2 -3 -17 2799.60 325.727 1 -2 -3 -16 4061.41 367.041 6 -2 -3 -16 3677.81 367.127 1 -2 -3 -15 1906.10 243.146 6 -2 -3 -15 2238.31 278.553 1 -2 -3 -14 4086.49 332.065 6 -2 -3 -14 4256.42 364.977 1 -2 -3 -13 1795.78 226.399 1 -2 -3 -13 1669.17 208.662 6 -2 -3 -12 917.170 157.563 1 -2 -3 -12 553.719 115.391 6 -2 -3 -11 2317.38 210.400 6 -2 -3 -11 2167.45 234.322 1 -2 -3 -10 26358.8 878.605 1 -2 -3 -10 26014.4 794.299 6 -2 -3 -9 18334.6 671.045 1 -2 -3 -9 17047.9 574.732 6 -2 -3 -8 2397.65 211.948 1 -2 -3 -7 576.711 100.850 1 -2 -3 -7 557.224 79.2919 6 -2 -3 -6 147.398 57.5223 1 -2 -3 -6 108.720 38.4220 6 -2 -3 -5 3492.55 167.466 6 -2 -3 -5 3979.59 193.452 5 -2 -3 -5 3608.14 225.275 1 -2 -3 -4 31408.2 689.605 6 -2 -3 -4 35528.5 838.185 1 -2 -3 -4 32962.1 759.305 5 -2 -3 -3 41220.3 815.550 6 -2 -3 -3 44761.9 971.451 1 -2 -3 -2 17330.4 448.609 1 -2 -3 -2 14951.3 306.393 6 -2 -3 -1 21088.6 518.283 1 -2 -3 0 30991.7 611.701 6 -2 -3 0 31868.4 682.879 1 -2 -3 1 2549.07 116.124 6 -2 -3 1 2785.97 133.680 1 -2 -3 1 2185.81 152.750 2 -2 -3 2 3288.99 138.842 1 -2 -3 2 3125.94 147.350 6 -2 -3 2 3216.44 159.419 5 -2 -3 2 3088.71 179.004 2 -2 -3 3 7369.08 234.275 1 -2 -3 3 7737.41 277.819 6 -2 -3 3 7904.49 310.754 2 -2 -3 3 7558.27 261.939 5 -2 -3 3 7783.49 302.591 7 -2 -3 4 28655.1 637.264 1 -2 -3 4 27910.6 740.189 2 -2 -3 4 28318.4 660.203 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91.8420 7 1 1 9 110.787 41.2673 10 1 1 10 8970.97 402.363 7 1 1 10 8989.78 278.748 5 1 1 11 9816.07 455.536 7 1 1 11 8738.32 304.010 5 1 1 12 1763.54 203.567 7 1 1 12 1792.94 147.267 10 1 1 13 2076.45 231.171 7 1 1 14 1043.17 177.736 7 1 1 15 94.1108 71.8951 7 1 1 16 648.447 161.672 7 1 2 -14 428.550 135.662 6 1 2 -13 707.177 156.641 6 1 2 -12 755.394 152.865 6 1 2 -12 486.699 111.455 1 1 2 -11 4005.71 302.008 1 1 2 -11 4128.68 319.794 6 1 2 -10 11902.6 523.493 1 1 2 -10 11478.2 531.091 6 1 2 -9 19481.9 683.922 1 1 2 -9 21323.0 717.500 6 1 2 -8 23716.8 739.290 1 1 2 -8 26956.9 789.789 6 1 2 -8 24125.8 617.648 9 1 2 -7 9476.02 400.523 1 1 2 -7 9917.75 414.780 6 1 2 -7 9828.06 329.825 9 1 2 -6 28694.5 680.335 1 1 2 -6 27773.8 765.170 1 1 2 -6 27159.2 664.708 5 1 2 -6 27948.9 687.491 9 1 2 -5 1955.57 117.253 1 1 2 -5 2252.44 123.479 5 1 2 -5 1462.28 117.024 10 1 2 -5 2048.87 128.860 9 1 2 -4 7636.58 286.700 8 1 2 -4 7238.12 287.187 7 1 2 -4 7178.15 278.831 4 1 2 -4 7275.82 234.112 1 1 2 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682.833 9 1 2 6 34237.1 698.938 3 1 2 7 112859. 2118.01 5 1 2 7 110259. 2029.24 3 1 2 8 27871.2 790.251 7 1 2 8 29771.9 600.865 3 1 2 8 25925.2 653.246 5 1 2 9 2308.89 195.072 7 1 2 9 2237.41 137.455 5 1 2 10 2100.79 197.677 7 1 2 10 1878.52 131.254 5 1 2 11 896.667 134.618 7 1 2 11 721.619 107.210 10 1 2 11 847.996 89.4265 5 1 2 12 7080.66 404.369 7 1 2 12 5379.37 312.266 10 1 2 13 9324.05 498.668 7 1 2 14 5149.79 379.247 7 1 2 15 983.865 178.402 7 1 2 16 1761.01 243.498 7 1 2 17 20.0476 80.0172 7 1 3 -14 2602.77 303.416 6 1 3 -13 1704.56 239.657 6 1 3 -12 628.689 133.241 1 1 3 -12 606.879 141.327 6 1 3 -11 557.348 129.745 6 1 3 -11 702.474 139.396 1 1 3 -10 175.627 74.0976 6 1 3 -10 162.604 73.5723 1 1 3 -9 5587.46 351.711 1 1 3 -9 6037.93 358.802 6 1 3 -8 18961.0 674.030 1 1 3 -8 19175.4 667.345 6 1 3 -7 28537.3 810.176 6 1 3 -7 25526.5 697.847 5 1 3 -6 8431.84 364.620 6 1 3 -6 6932.19 293.574 5 1 3 -5 7442.00 305.563 9 1 3 -5 7592.15 325.769 6 1 3 -5 7134.47 286.120 5 1 3 -5 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53.8559 6 1 6 0 89.9320 32.5775 2 1 6 0 51.7776 60.4545 5 1 6 1 5401.70 243.694 6 1 6 1 5794.25 318.078 5 1 6 1 4742.31 189.693 2 1 6 2 24883.4 635.022 6 1 6 2 23027.2 552.456 2 1 6 2 24349.6 745.398 5 1 6 3 21364.2 681.914 5 1 6 4 30398.8 858.008 5 1 6 5 49047.0 1205.47 5 1 6 6 20196.2 650.340 5 1 6 7 13167.0 495.758 5 1 6 8 2242.16 191.711 5 1 6 9 1549.17 164.824 5 1 6 10 405.346 87.6171 5 1 6 11 3776.35 298.676 7 1 6 11 3496.87 242.607 5 1 6 12 615.250 106.394 5 1 6 12 573.595 120.845 7 1 6 13 3211.37 296.462 7 1 6 14 4173.33 346.144 7 1 6 15 4646.69 376.615 7 1 6 16 846.592 162.870 7 1 6 17 20.4919 70.9680 7 1 7 -10 476.921 134.423 6 1 7 -9 2243.73 257.882 6 1 7 -8 1895.09 235.747 6 1 7 -8 1715.49 218.373 5 1 7 -7 4635.02 346.300 6 1 7 -7 4108.62 327.956 5 1 7 -6 3314.86 283.284 6 1 7 -6 3414.17 295.022 5 1 7 -5 1813.03 196.666 6 1 7 -5 1948.95 218.529 5 1 7 -4-4.00699 50.9952 6 1 7 -4 60.8610 51.1084 5 1 7 -3 110.578 51.5243 6 1 7 -3 78.6740 51.7953 5 1 7 -2 2060.87 181.077 6 1 7 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2 117.341 94.3329 5 1 10 3 2474.18 227.449 6 1 10 3 2616.61 290.948 5 1 10 4 3021.01 312.799 5 1 10 5 2208.36 267.068 5 1 10 6 4577.88 376.506 5 1 10 7 1285.38 196.892 5 1 10 8 457.995 115.689 5 1 10 9 653.673 152.348 5 1 10 10 1937.80 241.403 5 1 10 11 1048.48 175.552 5 1 10 12 1043.43 174.411 5 1 10 14 1210.62 213.362 7 1 11 -4-44.9358 75.3444 6 1 11 -3 758.581 158.124 6 1 11 -3 87.0590 96.4326 5 1 11 -2 814.282 156.055 6 1 11 -2 530.303 153.312 5 1 11 -1 1564.31 241.822 5 1 11 -1 1787.59 219.214 6 1 11 0 1286.66 225.540 5 1 11 0 1215.65 175.845 6 1 11 1 848.238 181.847 5 1 11 1 620.548 130.059 6 1 11 2 1070.10 164.665 6 1 11 2 934.734 197.460 5 1 11 3 2765.82 328.403 5 1 11 4 2030.93 274.960 5 1 11 5 403.318 118.160 5 1 11 6 8.41278 76.1491 5 1 11 7 992.355 196.341 5 1 11 8 323.510 133.951 5 1 11 9 96.0619 89.6062 5 1 11 10 242.740 108.809 5 1 11 11 1108.70 201.552 5 1 11 12 968.187 187.430 5 2 -10 -11 997.399 187.682 1 2 -10 -10 645.400 159.185 9 2 -10 -10 373.266 121.714 1 2 -10 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50611.1 1035.06 5 2 2 2 177.993 41.4236 5 2 2 2 161.042 20.6804 6 2 2 3 18458.3 418.887 6 2 2 3 18868.4 473.997 5 2 2 4 23744.1 526.171 6 2 2 4 24244.3 555.802 5 2 2 5 1755.53 119.787 5 2 2 5 1829.29 120.322 6 2 2 6 3190.90 169.545 5 2 2 6 2845.57 116.157 9 2 2 7 2196.63 145.749 5 2 2 7 1752.55 79.1555 9 2 2 8 11433.4 383.308 5 2 2 9 11200.0 394.756 5 2 2 9 12839.6 512.915 7 2 2 10 3492.91 262.538 7 2 2 10 3351.79 197.051 5 2 2 11 1441.99 180.742 7 2 2 11 699.967 99.6794 10 2 2 11 1497.91 137.623 5 2 2 12 1633.70 203.257 7 2 2 12 1867.74 154.144 5 2 2 13 5158.11 374.580 7 2 2 14 1416.80 205.971 7 2 2 15 333.340 107.375 7 2 2 16 5107.87 429.997 7 2 3 -14 4663.94 397.342 6 2 3 -13 10083.9 572.735 6 2 3 -12 5575.24 401.263 6 2 3 -11 108.723 47.4207 1 2 3 -11 213.058 89.1039 6 2 3 -10 3057.37 240.940 1 2 3 -10 3007.45 268.974 6 2 3 -9 2393.01 203.174 1 2 3 -9 2197.33 215.568 6 2 3 -8 13147.1 496.443 1 2 3 -8 14976.7 564.027 6 2 3 -7 28726.6 802.981 1 2 3 -7 29187.2 717.193 5 2 3 -6 10638.2 330.765 1 2 3 -6 11858.3 436.342 6 2 3 -6 10602.9 348.219 5 2 3 -5 6357.59 226.132 1 2 3 -5 6303.90 289.322 6 2 3 -5 6372.31 247.967 5 2 3 -4 27137.5 617.952 1 2 3 -4 29422.8 712.912 6 2 3 -4 26911.6 656.904 5 2 3 -4 28383.6 715.480 9 2 3 -3 7463.75 270.823 6 2 3 -3 7221.53 231.335 1 2 3 -3 7237.70 263.720 5 2 3 -3 7947.62 294.621 10 2 3 -3 7997.25 305.040 9 2 3 -2 3339.55 180.727 7 2 3 -2 3393.66 152.433 6 2 3 -2 3216.02 138.479 1 2 3 -2 3478.69 178.991 2 2 3 -2 3105.30 161.820 5 2 3 -2 3088.17 171.805 10 2 3 -2 3410.77 186.798 9 2 3 -2 3648.37 190.501 8 2 3 -1 2287.99 152.759 7 2 3 -1 2935.61 122.081 6 2 3 -1 2224.41 120.693 1 2 3 -1 2701.46 155.688 2 2 3 -1 3021.73 162.322 5 2 3 -1 2497.69 160.678 9 2 3 0 32111.0 620.147 6 2 3 0 30186.5 693.674 1 2 3 0 32085.5 724.936 2 2 3 0 31123.3 723.829 5 2 3 0 32355.4 752.029 9 2 3 1 20877.6 534.735 1 2 3 1 21743.6 544.555 5 2 3 1 22637.5 561.726 9 2 3 2 17512.8 468.090 5 2 3 2 17253.2 465.121 9 2 3 3 44259.1 960.411 5 2 3 3 43961.0 946.082 9 2 3 4 33341.5 807.561 5 2 3 4 37742.6 795.809 9 2 3 5 3736.56 189.898 5 2 3 5 3339.45 156.287 9 2 3 6 161.205 45.9588 5 2 3 6 94.4336 27.7860 9 2 3 7 522.369 72.6582 5 2 3 7 381.887 32.6612 3 2 3 7 510.966 52.2331 9 2 3 8 2327.54 193.912 7 2 3 8 1470.51 60.5507 3 2 3 8 2229.36 155.072 5 2 3 8 1776.28 88.9052 9 2 3 9 18877.5 643.213 7 2 3 9 17047.7 523.884 5 2 3 10 26572.8 837.851 7 2 3 10 25437.3 694.893 5 2 3 11 2622.49 243.076 7 2 3 11 2688.52 184.743 5 2 3 12 664.660 93.7286 5 2 3 12 609.929 124.112 7 2 3 12 240.649 85.8696 10 2 3 13 1797.41 219.780 7 2 3 14 3971.59 346.292 7 2 3 15 1969.71 249.300 7 2 3 16 3866.91 364.217 7 2 4 -13 2612.76 293.679 6 2 4 -12 6682.87 460.061 6 2 4 -11 8029.15 476.750 6 2 4 -10-24.3765 44.9177 1 2 4 -10 73.9806 57.2187 6 2 4 -9 87.5103 51.3153 1 2 4 -9 185.207 74.0571 6 2 4 -8 155.380 63.3556 6 2 4 -8 129.520 45.9568 5 2 4 -7 1.06528 28.7556 5 2 4 -7 69.0404 51.1614 6 2 4 -6 2890.69 210.967 6 2 4 -6 2794.32 183.331 5 2 4 -5 4174.77 241.847 6 2 4 -5 3853.45 215.750 5 2 4 -4 28429.6 688.883 1 2 4 -4 30422.0 764.001 6 2 4 -4 29099.2 747.302 5 2 4 -3 39304.2 887.217 6 2 4 -3 37080.5 843.707 1 2 4 -3 37878.5 907.096 5 2 4 -2 15147.8 416.728 6 2 4 -2 13763.4 402.247 1 2 4 -2 14613.8 454.828 5 2 4 -1 9508.60 281.855 6 2 4 -1 8494.41 297.431 1 2 4 -1 8849.66 309.728 2 2 4 -1 9377.02 343.057 5 2 4 0 47728.7 941.822 6 2 4 0 45019.4 1019.85 1 2 4 0 48618.7 1023.32 2 2 4 0 48151.0 1067.28 5 2 4 1 28683.4 595.615 6 2 4 1 28894.4 712.946 1 2 4 1 31281.3 742.505 5 2 4 2 34413.5 827.867 5 2 4 2 34242.3 830.704 9 2 4 3 1401.36 125.786 5 2 4 3 1222.20 111.239 9 2 4 4 24447.0 638.101 5 2 4 4 23057.4 612.031 9 2 4 5 2377.24 166.600 5 2 4 5 2407.80 151.655 9 2 4 6 23111.7 630.522 5 2 4 6 22503.0 583.481 9 2 4 7 387.429 74.4569 5 2 4 7 292.811 52.3906 9 2 4 8 8425.52 393.618 7 2 4 8 7964.00 328.087 5 2 4 8 7223.64 260.065 9 2 4 9 2464.33 219.329 7 2 4 9 1771.25 96.2086 3 2 4 9 2242.32 168.677 5 2 4 9 1851.97 113.505 9 2 4 10 12964.7 533.106 7 2 4 10 12737.6 435.666 5 2 4 11 2248.33 226.238 7 2 4 11 2690.27 189.249 5 2 4 12 8221.99 460.027 7 2 4 12 8054.10 353.457 5 2 4 13 4434.35 348.130 7 2 4 14 5915.32 417.374 7 2 4 15 1303.17 202.441 7 2 4 16 333.376 128.823 7 2 4 17 2555.34 301.134 7 2 5 -13 92.5935 78.5954 6 2 5 -12 602.204 141.873 6 2 5 -11 1256.16 194.608 6 2 5 -10 1829.85 219.573 1 2 5 -10 1814.00 226.286 6 2 5 -9 1414.09 189.252 6 2 5 -8 7863.48 425.553 6 2 5 -8 7269.76 363.525 5 2 5 -7 7774.17 401.314 6 2 5 -7 7745.42 367.284 5 2 5 -6 7996.89 387.147 6 2 5 -6 7372.38 352.717 5 2 5 -5-61.9010 45.3641 6 2 5 -5 49.8309 42.3744 5 2 5 -4 716.928 99.6731 6 2 5 -4 620.065 97.3151 5 2 5 -3 12384.2 418.369 6 2 5 -3 11378.4 434.157 5 2 5 -2 20084.2 542.024 6 2 5 -2 18463.7 592.967 5 2 5 -1 17072.6 462.886 6 2 5 -1 16075.1 536.966 5 2 5 -1 17499.7 490.407 2 2 5 0 1165.15 99.0455 6 2 5 0 888.479 93.6321 2 2 5 0 1552.21 161.805 5 2 5 1 344.593 77.3782 5 2 5 1 255.182 46.5812 2 2 5 1 147.680 36.8203 6 2 5 2 874.027 70.3874 6 2 5 2 808.916 106.711 5 2 5 3 1689.04 147.109 5 2 5 4 16828.3 539.022 5 2 5 5 15002.3 501.781 5 2 5 6 16156.3 527.049 5 2 5 7 13698.4 477.947 5 2 5 8 625.375 102.042 5 2 5 9 146.674 51.5516 5 2 5 9 91.8108 56.3755 7 2 5 9 219.706 54.2798 9 2 5 10 6719.00 390.713 7 2 5 10 6417.31 319.453 5 2 5 11 7072.40 415.354 7 2 5 11 6785.72 332.226 5 2 5 12 2325.04 240.622 7 2 5 12 2261.19 186.377 5 2 5 13 3801.64 324.439 7 2 5 14 8778.47 522.283 7 2 5 15 3359.76 328.853 7 2 5 16 262.237 89.1161 7 2 5 17 311.055 131.095 7 2 6 -12 190.765 111.850 6 2 6 -11 789.574 160.694 6 2 6 -10 3129.17 302.089 6 2 6 -9 6516.70 419.290 6 2 6 -8 10774.3 522.518 6 2 6 -8 9754.83 471.959 5 2 6 -7 7166.40 404.936 6 2 6 -7 6209.66 364.015 5 2 6 -6 308.761 90.8666 5 2 6 -6 425.654 100.318 6 2 6 -5 573.943 102.777 6 2 6 -5 589.599 103.271 5 2 6 -4 2751.97 207.362 6 2 6 -4 2930.70 230.340 5 2 6 -3 491.771 84.1608 6 2 6 -3 503.640 97.4270 5 2 6 -2 1263.72 123.390 6 2 6 -2 986.589 134.313 5 2 6 -1 9647.37 346.216 6 2 6 -1 9134.19 413.150 5 2 6 0 13199.3 404.607 6 2 6 0 14034.5 422.912 2 2 6 0 13538.7 516.474 5 2 6 1 8966.82 298.401 6 2 6 1 8270.76 307.542 2 2 6 1 8157.09 392.414 5 2 6 2 1369.35 102.818 6 2 6 2 1379.87 114.287 2 2 6 2 1334.09 151.908 5 2 6 3 2223.99 194.054 5 2 6 4 1789.07 168.824 5 2 6 5 15408.8 545.998 5 2 6 6 28530.9 816.726 5 2 6 7 56359.5 1336.81 5 2 6 8 33185.4 908.689 5 2 6 9 4194.63 269.870 5 2 6 10 1338.51 152.282 5 2 6 11 2978.61 273.306 7 2 6 11 2768.43 220.708 5 2 6 12 457.500 94.0276 5 2 6 12 451.611 119.414 7 2 6 13 1840.89 228.689 7 2 6 14 5160.28 396.227 7 2 6 15 2080.68 262.856 7 2 6 16 947.097 183.605 7 2 7 -11 445.608 135.934 6 2 7 -10 641.334 152.860 6 2 7 -9 1401.51 204.301 6 2 7 -8 67.5106 67.6609 6 2 7 -8-56.4148 49.8125 5 2 7 -7 5382.30 362.066 6 2 7 -7 5539.77 368.590 5 2 7 -6 11353.5 515.557 6 2 7 -6 10539.8 515.239 5 2 7 -5 5776.29 345.074 6 2 7 -5 5248.14 350.815 5 2 7 -4 621.249 115.884 6 2 7 -4 653.903 125.278 5 2 7 -3 56.1630 48.3575 6 2 7 -3 51.8032 49.2216 5 2 7 -2 113.938 48.6088 6 2 7 -2 106.472 51.1392 5 2 7 -1 228.194 58.2782 6 2 7 -1 195.784 65.8878 5 2 7 0 6415.61 281.664 6 2 7 0 6685.78 370.387 5 2 7 1 25996.9 665.618 6 2 7 1 24746.7 808.881 5 2 7 2 21632.4 587.119 6 2 7 2 22345.7 590.944 2 2 7 2 21646.9 731.989 5 2 7 3 4934.25 231.729 2 2 7 3 5318.24 323.822 5 2 7 4 753.617 133.789 5 2 7 5 2122.18 201.860 5 2 7 6 1389.73 165.180 5 2 7 7 13953.2 555.752 5 2 7 8 23584.2 769.788 5 2 7 9 17284.5 632.559 5 2 7 10 5222.39 322.419 5 2 7 11 6934.79 381.082 5 2 7 12 124.687 65.8160 5 2 7 12 72.7567 63.9141 7 2 7 13 402.261 120.779 7 2 7 14 347.252 131.909 7 2 7 15 1004.89 188.154 7 2 7 16 968.665 182.091 7 2 8 -10 361.681 137.867 6 2 8 -9 238.913 106.715 6 2 8 -8 52.2101 79.3529 6 2 8 -8 43.8122 66.3052 5 2 8 -7 1852.89 222.998 6 2 8 -7 1364.64 197.808 5 2 8 -6 7935.74 442.427 6 2 8 -6 7198.03 451.252 5 2 8 -5 9291.35 463.139 6 2 8 -5 7739.89 464.421 5 2 8 -4 10837.7 490.384 6 2 8 -4 9988.24 527.009 5 2 8 -3 3189.34 244.633 6 2 8 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565.411 5 2 9 0 3031.34 225.663 6 2 9 0 2757.04 278.180 5 2 9 1 1790.48 167.442 6 2 9 1 1555.55 206.290 5 2 9 2 3368.86 227.399 6 2 9 2 2840.49 277.858 5 2 9 3 766.671 149.377 5 2 9 4 321.151 99.0095 5 2 9 5 251.252 97.8059 5 2 9 6 745.261 139.194 5 2 9 7 0.96067 49.5817 5 2 9 8 305.932 92.5770 5 2 9 9-30.9823 83.5351 5 2 9 10-93.9270 83.0852 5 2 9 11 2510.82 255.003 5 2 9 12 6586.95 424.443 5 2 9 13 3556.57 345.935 7 2 9 14 2552.19 304.937 7 2 9 15 3014.30 332.020 7 2 10 -7-164.822 117.420 6 2 10 -7 248.706 112.557 5 2 10 -6 411.913 112.581 6 2 10 -6 344.742 126.729 5 2 10 -5 2983.11 289.995 6 2 10 -5 3115.90 338.868 5 2 10 -4 1787.58 222.143 6 2 10 -4 1761.39 251.528 5 2 10 -3 1078.37 166.872 6 2 10 -3 1166.08 202.090 5 2 10 -2 602.500 124.241 6 2 10 -2 440.117 129.329 5 2 10 -1 1400.31 169.172 6 2 10 -1 1507.58 229.809 5 2 10 0 1931.56 194.163 6 2 10 0 2231.98 268.459 5 2 10 1 1726.91 180.363 6 2 10 1 1753.01 240.860 5 2 10 2 778.711 123.460 6 2 10 2 795.096 172.404 5 2 10 3 139.710 82.5046 5 2 10 4 61.5490 61.1690 5 2 10 5 143.060 87.0273 5 2 10 6 1086.62 186.878 5 2 10 7 1480.13 211.626 5 2 10 8 3116.93 300.629 5 2 10 9 2571.68 282.619 5 2 10 10 662.386 149.495 5 2 10 11 404.413 114.894 5 2 10 12 1655.20 222.252 5 2 10 14 460.383 132.458 7 2 11 -5 589.843 168.895 5 2 11 -4 179.556 127.721 5 2 11 -3 42.8193 86.3556 5 2 11 -2-100.806 96.2072 5 2 11 -1 298.420 138.435 5 2 11 0 1352.41 215.258 5 2 11 1 1123.43 204.221 5 2 11 2 1945.47 268.207 5 2 11 3 1655.95 248.964 5 2 11 4 222.585 93.2767 5 2 11 5 192.055 92.3330 5 2 11 6 1837.16 256.446 5 2 11 7 3056.06 326.371 5 2 11 8 2453.46 290.558 5 2 11 9 1464.17 222.214 5 2 11 10 355.329 118.792 5 2 11 11-85.8234 70.8039 5 2 11 12-224.707 95.8997 5 2 12 2 1353.77 237.531 5 2 12 3 2084.50 296.260 5 2 12 4 677.090 174.079 5 2 12 5 148.946 103.031 5 2 12 6 157.903 104.963 5 2 12 7 343.774 116.087 5 2 12 8 972.188 197.326 5 2 12 9 1945.98 271.499 5 3 -10 -10 472.354 146.784 9 3 -10 -9-35.6759 83.7114 1 3 -10 -9-354.051 129.130 9 3 -10 -8 538.906 143.387 1 3 -10 -8 487.674 143.265 9 3 -10 -7 1607.72 235.550 1 3 -10 -7 1660.76 268.265 9 3 -10 -6 1050.49 184.295 1 3 -10 -6 1026.73 216.746 9 3 -10 -5 906.619 185.318 1 3 -10 -5 1564.94 258.508 9 3 -10 -4 762.428 171.122 1 3 -10 -4 1027.01 214.208 9 3 -10 -3 445.666 138.267 1 3 -10 -3 845.119 204.265 9 3 -10 -2 198.619 101.606 1 3 -10 -2-117.485 105.936 9 3 -9 -12-76.5975 73.0658 1 3 -9 -11 1708.89 242.262 9 3 -9 -11 1718.54 231.480 1 3 -9 -10 1669.46 228.397 1 3 -9 -10 1543.63 240.389 9 3 -9 -9 1339.20 202.921 1 3 -9 -9 1363.00 225.708 9 3 -9 -8 41.6531 67.3544 1 3 -9 -8 179.517 96.1741 9 3 -9 -7-23.1200 64.8774 1 3 -9 -7-25.8138 79.6790 9 3 -9 -6 181.895 82.4434 1 3 -9 -6 302.536 130.019 9 3 -9 -5 698.343 137.802 1 3 -9 -5 554.969 148.656 9 3 -9 -4 2964.41 294.696 1 3 -9 -4 3242.47 347.933 9 3 -9 -3 930.269 172.475 1 3 -9 -3 933.546 184.200 9 3 -9 -2 2349.55 265.716 1 3 -9 -2 2348.56 302.350 9 3 -9 -1 1053.06 180.875 1 3 -9 -1 889.151 201.188 9 3 -9 0 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25.6927 59.6287 9 3 -6 -3 11982.2 505.074 1 3 -6 -3 12148.4 586.914 9 3 -6 -2 36.8396 57.3914 1 3 -6 -2-57.1364 58.3398 9 3 -6 -1 1120.71 153.621 1 3 -6 -1 1045.74 176.363 9 3 -6 0 297.367 92.5502 1 3 -6 0 293.734 111.675 9 3 -6 1 8125.45 423.963 1 3 -6 1 8022.96 429.502 7 3 -6 1 6980.41 443.809 9 3 -6 2 13983.1 592.875 1 3 -6 2 14167.9 607.419 7 3 -6 2 13706.6 645.566 9 3 -6 3 6429.11 391.947 1 3 -6 3 5939.11 390.922 7 3 -6 3 6690.41 439.039 9 3 -6 4 55.3269 68.2884 7 3 -6 4 6.17999 53.8758 1 3 -6 4-9.45975 59.8692 9 3 -6 5 634.314 147.541 7 3 -6 5 399.103 108.086 1 3 -6 5 395.242 115.843 9 3 -6 6 539.077 143.931 7 3 -6 6 363.117 117.625 1 3 -6 6 420.035 130.018 9 3 -6 7 12.4828 68.4266 7 3 -6 7 44.6752 59.8789 1 3 -6 7 50.3673 57.1265 9 3 -6 8 374.262 143.285 7 3 -6 8 592.286 145.560 1 3 -6 8 554.618 133.310 9 3 -6 9 4604.87 386.791 1 3 -6 9 4022.72 400.466 7 3 -5 -15 1041.49 199.011 6 3 -5 -14 94.1372 80.5588 6 3 -5 -13 307.306 114.907 6 3 -5 -12 4353.14 358.094 6 3 -5 -12 4604.37 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6606.52 399.254 7 3 -5 4 6510.93 407.770 9 3 -5 5 2475.66 235.836 1 3 -5 5 2240.01 239.845 7 3 -5 5 2483.74 252.488 9 3 -5 6 3007.88 265.123 1 3 -5 6 2994.96 288.323 7 3 -5 6 3347.19 293.715 9 3 -5 7 16.6405 68.1995 7 3 -5 7 101.722 69.9436 1 3 -5 7 30.8791 68.2251 9 3 -5 8 64.2419 68.4208 7 3 -5 8-69.7364 77.5820 1 3 -5 8 33.8433 52.3803 9 3 -5 9 3316.44 344.443 7 3 -5 9 3403.07 278.176 2 3 -5 9 3290.15 311.649 1 3 -5 10 5546.37 463.573 7 3 -5 10 5696.22 384.613 2 3 -5 11 5722.72 403.891 2 3 -4 -15 137.288 89.7915 6 3 -4 -14-30.0956 90.0262 6 3 -4 -13 60.5794 82.5067 6 3 -4 -12 2550.79 270.150 6 3 -4 -12 2418.06 201.695 1 3 -4 -11 15.0529 38.7435 1 3 -4 -11-74.4344 70.1323 6 3 -4 -11-27.6817 49.8353 9 3 -4 -10 202.139 76.2320 9 3 -4 -10 63.8919 36.0840 1 3 -4 -9 5129.84 282.948 1 3 -4 -9 5104.49 308.481 9 3 -4 -8 8520.47 363.018 1 3 -4 -8 8403.49 414.591 9 3 -4 -7 21981.5 740.286 9 3 -4 -7 22399.1 656.098 1 3 -4 -6 7695.53 333.068 1 3 -4 -6 6936.25 382.350 9 3 -4 -5 3826.39 281.716 9 3 -4 -5 4460.81 248.441 1 3 -4 -4 4618.56 254.401 1 3 -4 -4 4850.69 314.933 9 3 -4 -3 9471.28 376.300 1 3 -4 -3 7736.47 420.546 9 3 -4 -2 28170.2 634.696 8 3 -4 -2 31665.0 801.008 1 3 -4 -1 4159.52 125.387 8 3 -4 -1 5229.46 270.320 1 3 -4 -1 3945.50 125.157 4 3 -4 -1 4272.31 129.653 2 3 -4 0 421.576 75.6309 7 3 -4 0 361.819 78.2867 1 3 -4 1 99.1019 44.9271 7 3 -4 1 12.7975 56.1102 1 3 -4 1 17.5184 45.4660 9 3 -4 2 1293.80 143.766 1 3 -4 2 1391.07 151.759 7 3 -4 2 1226.17 157.779 9 3 -4 3 1025.90 141.008 1 3 -4 3 920.234 149.007 9 3 -4 3 828.193 133.703 7 3 -4 4 7547.65 380.913 1 3 -4 4 7070.28 389.952 7 3 -4 4 7079.62 403.254 9 3 -4 5 3627.12 271.387 1 3 -4 5 3606.47 286.476 7 3 -4 5 3214.61 266.493 9 3 -4 6 25325.8 819.594 1 3 -4 6 24271.8 861.609 7 3 -4 6 24731.4 835.050 9 3 -4 7 9063.82 469.695 1 3 -4 7 9637.04 521.444 7 3 -4 7 10174.9 492.299 9 3 -4 8 44.1409 68.7472 7 3 -4 8 73.5762 54.9959 1 3 -4 8 59.5637 60.6752 9 3 -4 9 442.872 134.835 7 3 -4 9 285.257 82.2165 9 3 -4 9 180.505 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373.021 4 3 -3 -1 17841.5 414.547 2 3 -3 -1 17093.7 376.237 8 3 -3 0 101757. 2052.30 1 3 -3 0 100432. 2016.88 7 3 -3 1 1260.72 134.877 1 3 -3 1 910.173 111.450 7 3 -3 2 9962.31 397.829 1 3 -3 2 9446.64 392.173 7 3 -3 2 9876.88 450.279 9 3 -3 3 12369.8 464.742 1 3 -3 3 11874.0 470.110 7 3 -3 3 12698.6 523.495 9 3 -3 4 8288.65 380.462 1 3 -3 4 9156.51 415.346 7 3 -3 4 8653.52 422.467 9 3 -3 5 412.568 94.1387 7 3 -3 5 313.562 71.6283 1 3 -3 5 428.992 93.6555 9 3 -3 6 4885.00 307.620 1 3 -3 6 4660.50 323.534 7 3 -3 6 4202.59 287.461 9 3 -3 7 20591.4 716.196 1 3 -3 7 20486.2 758.225 7 3 -3 7 20156.1 690.698 9 3 -3 8 933.962 158.939 7 3 -3 8 900.945 128.902 9 3 -3 8 809.176 131.846 1 3 -3 9 1440.44 204.851 7 3 -3 9 1411.08 162.985 9 3 -3 10 162.580 71.0312 7 3 -3 11 2642.25 305.080 7 3 -3 12 2491.34 308.783 7 3 -2 -15 216.967 109.586 6 3 -2 -14 1172.58 202.442 6 3 -2 -13 4268.16 357.642 6 3 -2 -12 12691.5 613.377 6 3 -2 -12 12093.0 444.091 1 3 -2 -11 7355.50 433.743 6 3 -2 -11 7277.87 316.980 1 3 -2 -10-26.2027 41.5901 1 3 -2 -10-12.0606 54.7739 6 3 -2 -10 16.9685 29.4016 9 3 -2 -9 355.588 29.0432 5 3 -2 -9 476.046 70.6105 1 3 -2 -9 425.039 98.4631 6 3 -2 -9 510.757 83.9030 9 3 -2 -8 6380.39 259.321 1 3 -2 -8 6174.89 193.658 5 3 -2 -8 6263.38 304.063 9 3 -2 -7 74.5731 27.0001 5 3 -2 -7 78.0846 35.5916 1 3 -2 -6 17360.8 469.107 1 3 -2 -6 16870.4 449.071 5 3 -2 -5 22083.4 547.556 1 3 -2 -5 21141.1 548.941 5 3 -2 -4 36669.4 872.072 8 3 -2 -4 36491.5 864.284 4 3 -2 -4 37001.5 824.264 1 3 -2 -4 36583.5 847.755 5 3 -2 -4 37836.2 812.978 2 3 -2 -3 33325.3 768.276 8 3 -2 -3 33158.4 762.391 4 3 -2 -3 33270.2 766.154 1 3 -2 -3 34654.5 811.589 5 3 -2 -3 34875.9 736.062 2 3 -2 -2 2747.10 133.343 8 3 -2 -2 2833.68 134.436 4 3 -2 -2 3118.39 164.746 1 3 -2 -2 2831.99 133.729 2 3 -2 -1 4641.04 152.220 8 3 -2 -1 4373.88 149.795 4 3 -2 -1 5538.40 232.017 1 3 -2 -1 4716.26 191.940 7 3 -2 0 47500.7 1037.48 1 3 -2 0 45661.4 994.996 7 3 -2 1 27182.9 688.565 1 3 -2 1 25008.3 657.868 7 3 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242.679 2 3 -1 -3 148.378 39.8473 8 3 -1 -3 184.472 41.6601 4 3 -1 -3 179.127 32.6650 1 3 -1 -3 161.717 35.8095 2 3 -1 -3 154.476 36.9734 5 3 -1 -2 1280.89 91.0705 8 3 -1 -2 1353.61 93.1141 4 3 -1 -2 1440.17 93.0073 1 3 -1 -2 1623.70 122.748 6 3 -1 -2 1247.71 102.947 5 3 -1 -2 1418.00 100.745 2 3 -1 -1 4204.97 156.968 8 3 -1 -1 4649.98 185.487 1 3 -1 -1 4196.54 156.033 4 3 -1 -1 4443.45 148.840 7 3 -1 -1 4385.79 204.020 6 3 -1 -1 4340.15 213.648 5 3 -1 0 6296.69 236.259 1 3 -1 0 5319.12 197.558 7 3 -1 0 5354.84 237.850 6 3 -1 1 22794.6 586.452 1 3 -1 1 23413.0 569.171 7 3 -1 1 23739.2 603.405 6 3 -1 2 30138.0 731.586 1 3 -1 2 29545.3 723.046 7 3 -1 3 39794.9 905.930 1 3 -1 3 38448.8 901.180 7 3 -1 4 28788.1 760.605 1 3 -1 4 29254.4 771.866 7 3 -1 4 29171.5 781.077 9 3 -1 5 4435.54 259.255 7 3 -1 5 4813.09 260.645 9 3 -1 5 4384.02 250.490 1 3 -1 6 537.017 96.2773 7 3 -1 6 560.161 88.5867 9 3 -1 7 915.037 132.774 7 3 -1 7 758.274 100.249 9 3 -1 8 5536.44 346.410 7 3 -1 8 5258.28 263.329 9 3 -1 9 11168.6 530.660 7 3 -1 9 11065.5 394.865 9 3 -1 10 7369.47 448.405 7 3 -1 11 2178.13 252.842 7 3 -1 12 8168.93 514.677 7 3 -1 13 2649.97 309.207 7 3 -1 14 1403.53 235.739 7 3 0 -15 1571.41 241.798 6 3 0 -14 858.166 168.371 6 3 0 -13 869.386 168.458 6 3 0 -12-48.7796 73.1566 6 3 0 -11 12224.0 570.882 6 3 0 -11 12132.7 407.923 1 3 0 -10 29592.4 925.973 6 3 0 -10 28005.6 699.626 1 3 0 -9 34601.7 982.640 6 3 0 -9 32612.0 750.711 1 3 0 -9 32135.5 722.100 1 3 0 -8 10415.1 360.822 7 3 0 -8 10320.6 451.990 6 3 0 -8 10249.8 306.672 1 3 0 -7 2381.35 141.015 7 3 0 -7 2507.97 199.208 6 3 0 -7 2386.18 114.087 1 3 0 -6 13097.0 358.889 7 3 0 -6 13453.7 317.365 1 3 0 -5 3956.07 141.678 7 3 0 -5 3852.75 121.788 1 3 0 -5 3576.64 129.663 5 3 0 -5 3703.85 123.136 5 3 0 -4 8691.90 209.429 7 3 0 -4 8920.20 210.635 1 3 0 -3 17542.4 484.741 8 3 0 -3 17121.5 368.903 1 3 0 -3 18359.9 490.418 4 3 0 -2 108004. 1946.25 8 3 0 -2 96051.2 1839.79 1 3 0 -2 98342.8 1930.14 4 3 0 -2 102882. 1949.45 6 3 0 -2 105176. 2009.02 10 3 0 -1 6313.64 195.479 1 3 0 -1 6171.17 162.201 7 3 0 -1 6295.23 217.019 4 3 0 -1 6237.23 231.553 6 3 0 -1 7827.11 274.805 10 3 0 -1 6722.84 224.151 8 3 0 0 6018.53 208.373 1 3 0 0 6265.88 192.559 7 3 0 0 6293.90 226.233 6 3 0 0 7806.85 256.128 10 3 0 1 894.913 89.4702 1 3 0 1 824.146 74.7255 7 3 0 1 901.144 82.6661 6 3 0 1 715.823 70.9393 10 3 0 2 3767.53 178.809 7 3 0 2 3996.22 183.247 6 3 0 2 4519.27 157.440 10 3 0 2 4022.24 187.683 1 3 0 3 294.497 58.5237 7 3 0 3 178.582 43.3394 6 3 0 3 297.437 34.8513 10 3 0 4 34187.8 843.531 7 3 0 6 10018.7 362.548 9 3 0 7 6383.75 334.835 7 3 0 7 6352.65 274.588 9 3 0 8 3359.19 186.428 9 3 0 8 3395.73 256.793 7 3 0 9 4261.21 302.893 7 3 0 9 2986.15 164.485 9 3 0 10 3882.08 306.954 7 3 0 11 18267.0 744.750 7 3 0 12 30442.0 1049.33 7 3 0 12 29110.6 858.592 5 3 0 13 12548.8 658.793 7 3 0 14 3470.05 349.642 7 3 1 -15 3007.80 325.659 6 3 1 -14 2437.27 286.460 6 3 1 -13 118.850 92.0157 6 3 1 -12 266.028 90.0089 6 3 1 -11 1079.01 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856.447 7 3 1 1 41114.6 855.176 3 3 1 1 40330.6 828.558 6 3 1 1 41548.1 853.710 10 3 1 2 8015.15 273.501 7 3 1 2 7588.18 238.952 6 3 1 2 7821.89 233.462 10 3 1 3 9327.39 324.969 7 3 1 3 9709.57 294.854 6 3 1 3 9186.99 253.060 10 3 1 4 14154.9 409.043 6 3 1 8 42158.0 885.493 7 3 1 8 41957.4 616.238 9 3 1 8 44199.6 771.901 5 3 1 9 40896.2 1112.81 7 3 1 9 41558.9 796.015 10 3 1 9 36491.7 822.776 9 3 1 9 37946.8 974.480 5 3 1 10 4972.09 336.844 7 3 1 10 5220.77 284.620 5 3 1 11 5112.87 359.552 7 3 1 11 5525.88 302.019 5 3 1 12 4682.56 359.875 7 3 1 12 4901.23 290.516 5 3 1 13 1783.34 231.090 7 3 1 14 478.360 128.387 7 3 1 15 1977.63 270.938 7 3 2 -14 2266.00 282.197 6 3 2 -13 4256.64 368.149 6 3 2 -12 2067.64 237.919 6 3 2 -11 3465.08 294.997 6 3 2 -10 2140.01 222.327 6 3 2 -10 1907.88 148.238 1 3 2 -9 12.6990 23.6597 1 3 2 -9-6.03989 54.0260 6 3 2 -8 5643.85 200.043 1 3 2 -8 6348.06 338.446 6 3 2 -8 5964.77 236.477 1 3 2 -7 14940.0 356.900 1 3 2 -7 16478.6 552.347 6 3 2 -7 14200.6 342.964 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30.8149 34.7669 5 3 3 8 1.99094 41.3853 7 3 3 8 18.4730 16.8247 9 3 3 9 5294.73 325.304 7 3 3 9 4737.93 258.852 5 3 3 9 4020.94 155.654 9 3 3 10 9011.70 458.160 7 3 3 10 8761.50 376.084 5 3 3 11 1055.41 160.798 7 3 3 11 1227.09 140.661 5 3 3 12 7937.13 463.201 7 3 3 12 7470.00 359.597 5 3 3 13 6047.64 417.743 7 3 3 14 79.1849 75.0588 7 3 3 15 211.653 102.259 7 3 3 16 246.196 111.232 7 3 4 -13 371.022 131.008 6 3 4 -12 2597.57 281.100 6 3 4 -11 6804.04 433.689 6 3 4 -10 8918.61 482.659 6 3 4 -9 15338.4 544.959 1 3 4 -9 16740.2 651.134 6 3 4 -8 6453.05 317.945 1 3 4 -8 6426.39 359.473 6 3 4 -8 6469.31 281.024 5 3 4 -7 1206.06 150.739 6 3 4 -7 1083.54 112.409 5 3 4 -6 119.220 37.3317 1 3 4 -6 115.037 55.1938 6 3 4 -6 87.0113 41.1619 5 3 4 -5 4558.86 249.342 6 3 4 -5 4471.38 189.573 1 3 4 -5 4564.47 224.982 5 3 4 -4 6440.82 279.286 6 3 4 -4 6435.27 230.633 1 3 4 -4 6475.35 274.075 5 3 4 -3 2115.86 139.136 6 3 4 -3 1989.30 118.092 1 3 4 -3 2121.55 148.023 5 3 4 -2 70086.1 1372.21 6 3 4 -2 68040.3 1369.96 1 3 4 -2 67597.9 1437.48 5 3 4 -1 56360.2 1090.40 6 3 4 -1 53777.4 1145.89 1 3 4 -1 54695.6 1201.90 5 3 4 0 50199.3 957.072 6 3 4 0 49834.1 1082.05 1 3 4 0 51732.6 1123.91 5 3 4 1 4889.98 233.316 1 3 4 1 5819.77 261.307 5 3 4 2 9873.61 360.622 5 3 4 3 29888.2 765.061 5 3 4 4 7367.98 310.180 5 3 4 5 30528.2 790.659 5 3 4 5 30206.5 747.186 9 3 4 6 39825.8 962.578 5 3 4 6 38155.0 891.628 9 3 4 7 7392.45 325.518 5 3 4 7 7157.84 273.718 9 3 4 8 790.387 128.286 7 3 4 8 890.483 115.568 5 3 4 8 680.782 74.1328 9 3 4 9 89.7528 46.5293 5 3 4 9 43.1540 55.8779 7 3 4 9 95.2985 29.7725 9 3 4 10 1581.27 187.003 7 3 4 10 1445.30 150.014 5 3 4 11 832.434 117.005 5 3 4 11 976.204 153.223 7 3 4 12 953.192 126.179 5 3 4 12 668.098 134.243 7 3 4 13 6289.77 429.618 7 3 4 13 5939.06 325.148 5 3 4 14 2319.94 269.267 7 3 4 15 2309.80 274.880 7 3 4 16 424.677 142.082 7 3 5 -13 1209.57 208.016 6 3 5 -12 273.195 114.426 6 3 5 -11-100.023 85.5726 6 3 5 -10 580.537 132.823 6 3 5 -9 8297.01 454.823 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1379.70 228.470 6 3 6 -11 173.363 91.0466 6 3 6 -10-34.6920 71.6252 6 3 6 -9-26.9212 86.9710 6 3 6 -8 8603.22 456.629 6 3 6 -8 8064.92 401.812 5 3 6 -7 19691.3 698.257 6 3 6 -7 18269.0 652.657 5 3 6 -6 22104.6 723.038 6 3 6 -6 20649.8 699.322 5 3 6 -5 16571.2 572.906 6 3 6 -5 15326.3 569.587 5 3 6 -4 585.232 104.803 6 3 6 -4 501.759 103.273 5 3 6 -3 3014.45 196.322 6 3 6 -3 3427.37 243.128 5 3 6 -2 2080.31 147.430 6 3 6 -2 2051.98 184.022 5 3 6 -1 362.809 82.8133 5 3 6 -1 443.205 63.1962 6 3 6 0 3238.71 158.482 6 3 6 0 4153.10 265.132 5 3 6 1 10459.2 295.021 6 3 6 1 10396.6 433.775 5 3 6 2 2054.31 176.779 5 3 6 3 1740.50 168.398 5 3 6 4 708.016 114.542 5 3 6 5 4948.62 288.998 5 3 6 6 1468.74 162.609 5 3 6 7 5577.88 311.774 5 3 6 8 14381.6 539.416 5 3 6 9 21701.3 704.637 5 3 6 10 18868.7 731.968 7 3 6 10 17462.5 625.050 5 3 6 11 3341.05 296.514 7 3 6 11 3122.15 243.353 5 3 6 12 330.494 94.0400 5 3 6 12 218.116 82.3169 7 3 6 13 2294.06 260.669 7 3 6 13 1882.21 193.870 5 3 6 14 5619.38 427.252 7 3 6 15 1888.04 256.295 7 3 6 16 3890.43 375.299 7 3 7 -11 1954.78 259.312 6 3 7 -10 299.195 116.331 6 3 7 -9 25.8301 75.2721 6 3 7 -8 935.528 157.497 6 3 7 -8 850.191 139.629 5 3 7 -7 1914.28 205.921 6 3 7 -7 1359.60 173.591 5 3 7 -6-11.3090 60.2762 6 3 7 -6 143.896 71.7837 5 3 7 -5 4583.01 289.328 6 3 7 -5 3908.91 289.695 5 3 7 -4 701.891 113.646 6 3 7 -4 690.416 123.423 5 3 7 -3 4983.73 272.338 6 3 7 -3 5189.56 326.265 5 3 7 -2 1.35329 34.3697 6 3 7 -2 71.6562 61.1357 5 3 7 -1 285.065 83.9885 5 3 7 -1 199.606 50.2795 6 3 7 0 790.176 129.103 5 3 7 0 991.299 96.3546 6 3 7 1 8455.09 288.764 6 3 7 1 8586.70 421.742 5 3 7 2 9478.74 303.928 6 3 7 2 9957.03 450.885 5 3 7 3 4728.59 303.339 5 3 7 4 6859.10 369.526 5 3 7 5 3414.52 257.784 5 3 7 6 6297.57 356.009 5 3 7 7 2355.10 214.135 5 3 7 8 497.387 105.735 5 3 7 9 4593.44 304.908 5 3 7 10 16340.1 623.308 5 3 7 11 19426.3 778.387 7 3 7 11 17109.6 658.341 5 3 7 12 3309.67 313.024 7 3 7 12 3170.84 262.137 5 3 7 13 2871.30 302.287 7 3 7 13 2445.83 233.001 5 3 7 14 4943.35 406.780 7 3 7 15 406.751 115.075 7 3 7 16 43.3553 69.2105 7 3 8 -10 353.151 115.354 6 3 8 -9 98.3074 69.0222 6 3 8 -8-77.8054 81.0913 6 3 8 -7 14.1694 58.9563 6 3 8 -7-61.4968 60.0607 5 3 8 -6 146.723 79.6808 6 3 8 -6-6.35055 60.2737 5 3 8 -5 287.239 82.2604 6 3 8 -5 142.486 78.9377 5 3 8 -4 3723.02 261.581 6 3 8 -4 3186.08 283.996 5 3 8 -3 15534.4 556.016 6 3 8 -3 14543.1 630.398 5 3 8 -2 33625.1 884.767 6 3 8 -2 31858.9 1007.32 5 3 8 -1 14378.7 487.742 6 3 8 -1 14919.0 621.049 5 3 8 0 1551.27 135.558 6 3 8 0 1765.96 210.323 5 3 8 1 4223.76 212.592 6 3 8 1 4276.01 316.213 5 3 8 2 286.761 102.560 5 3 8 2 189.074 52.1473 6 3 8 3 1820.23 204.941 5 3 8 4 13511.6 581.626 5 3 8 5 19297.2 713.318 5 3 8 6 9290.62 470.109 5 3 8 7 9507.91 477.433 5 3 8 8 1769.34 201.344 5 3 8 9 34.8904 58.2014 5 3 8 10 746.139 135.520 5 3 8 11 4479.22 326.337 5 3 8 12 863.715 148.856 5 3 8 12 1133.46 190.182 7 3 8 13 475.555 114.917 5 3 8 13 309.331 107.788 7 3 8 14 1000.82 190.139 7 3 8 15 258.215 100.284 7 3 9 -9 1311.50 206.674 6 3 9 -8 3469.10 323.838 6 3 9 -7 4749.42 362.511 6 3 9 -7 4516.78 375.666 5 3 9 -6 4320.62 333.470 6 3 9 -6 4102.05 352.116 5 3 9 -5 929.202 155.447 6 3 9 -5 761.816 157.039 5 3 9 -4 839.014 140.581 6 3 9 -4 857.483 165.046 5 3 9 -3 133.284 69.4444 6 3 9 -3 139.513 74.6690 5 3 9 -2 96.4270 63.7977 6 3 9 -2 73.6049 82.2403 5 3 9 -1 1396.18 145.653 6 3 9 -1 1141.65 175.948 5 3 9 0 7883.48 345.870 6 3 9 0 7215.10 447.855 5 3 9 1 13575.2 466.559 6 3 9 1 13207.6 624.911 5 3 9 2 9893.96 375.986 6 3 9 2 9703.93 520.080 5 3 9 3 2337.02 251.425 5 3 9 4 140.753 73.6747 5 3 9 5 2131.68 232.365 5 3 9 6 3213.93 287.094 5 3 9 7 8605.51 485.411 5 3 9 8 2290.21 250.613 5 3 9 9 11.9913 60.5241 5 3 9 10 362.812 102.125 5 3 9 11 19.3006 56.3303 5 3 9 12 77.8990 59.5900 5 3 9 13 174.322 72.2997 5 3 9 13 17.5275 59.1951 7 3 9 14 2102.90 284.420 7 3 10 -6 2808.64 310.179 5 3 10 -5 123.855 79.3273 6 3 10 -5 170.045 106.184 5 3 10 -4 520.168 112.345 6 3 10 -4 810.396 170.289 5 3 10 -3 871.960 141.173 6 3 10 -3 1106.84 189.866 5 3 10 -2 297.214 83.8132 6 3 10 -2 151.599 85.7739 5 3 10 -1 5310.27 409.498 5 3 10 0 7410.38 493.250 5 3 10 1 5436.13 411.266 5 3 10 2 3522.68 326.915 5 3 10 3 1880.59 240.591 5 3 10 4 604.097 149.693 5 3 10 5-4.77258 60.4196 5 3 10 6 267.863 102.683 5 3 10 7 213.629 85.5572 5 3 10 8 2748.54 285.093 5 3 10 9 932.005 175.970 5 3 10 10 51.0447 59.1594 5 3 10 11 451.410 119.232 5 3 10 12 485.885 135.255 5 3 10 13 137.090 80.3956 5 3 11 -5 1171.79 226.025 5 3 11 -4 1484.35 243.711 5 3 11 -3 1658.50 252.546 5 3 11 -2 176.463 103.089 5 3 11 -1-150.954 102.114 5 3 11 0 182.983 117.138 5 3 11 1 283.612 118.363 5 3 11 2 945.318 188.724 5 3 11 3 686.917 153.646 5 3 11 4 705.271 160.453 5 3 11 5 436.441 133.326 5 3 11 6 1093.05 197.702 5 3 11 7 465.105 148.664 5 3 11 8 1932.57 263.237 5 3 11 9 2521.64 292.723 5 3 11 10 1200.14 207.833 5 3 11 11 1174.34 208.429 5 3 11 12 708.196 162.840 5 3 11 13 56.6103 69.0645 5 3 12 0 81.7335 83.2190 5 3 12 1 128.209 92.7193 5 3 12 2 539.513 163.059 5 3 12 3 2187.65 300.922 5 3 12 4 2017.79 282.830 5 3 12 5 664.516 165.677 5 3 12 6-24.1784 72.2210 5 3 12 7-185.009 100.644 5 3 12 8-61.9865 74.3526 5 3 12 9 493.181 144.318 5 4 -9 -11 18.1981 80.5504 1 4 -9 -10 207.027 87.4539 1 4 -9 -10 230.963 104.658 9 4 -9 -9 6.80865 75.5651 1 4 -9 -9 48.8799 79.5901 9 4 -9 -8 523.999 130.403 1 4 -9 -8 949.868 199.738 9 4 -9 -7 1306.05 207.192 1 4 -9 -7 1373.66 237.461 9 4 -9 -6 528.430 142.433 1 4 -9 -6 440.371 145.585 9 4 -9 -5 435.296 126.985 1 4 -9 -5 455.610 173.353 9 4 -9 -4 230.411 98.3696 1 4 -9 -4 354.699 135.016 9 4 -9 -3 38.8783 68.8684 1 4 -9 -3 318.403 135.392 9 4 -9 -2 714.904 158.334 1 4 -9 -2 513.389 161.483 9 4 -9 -1 144.884 98.6208 1 4 -9 -1 256.122 105.133 9 4 -9 0 486.835 150.349 1 4 -9 0 578.549 158.315 9 4 -8 -11 1.37016 54.9318 1 4 -8 -11-88.3991 84.3138 9 4 -8 -10-74.3400 74.1141 1 4 -8 -10 49.5996 80.2156 9 4 -8 -9 1189.75 183.906 1 4 -8 -9 1127.32 201.184 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568.947 6 4 4 6 22928.6 521.021 3 4 4 6 24185.7 695.059 5 4 4 7 26609.5 789.368 7 4 4 7 25185.2 714.214 5 4 4 8 14357.9 584.815 7 4 4 8 14388.5 523.740 5 4 4 9 8472.24 444.443 7 4 4 9 7890.55 380.245 5 4 4 10 370.923 84.9498 5 4 4 10 357.250 97.3389 7 4 4 11 1049.93 139.932 5 4 4 11 943.612 158.633 7 4 4 12 4977.93 380.804 7 4 4 12 5192.63 317.785 5 4 4 13 3011.76 298.033 7 4 4 13 3034.88 244.928 5 4 4 14 233.037 111.962 7 4 4 15 735.462 152.118 7 4 5 -13 2682.45 307.187 6 4 5 -12 2485.05 281.399 6 4 5 -11 425.210 127.559 6 4 5 -10 345.360 105.478 6 4 5 -9 3720.39 293.209 6 4 5 -8 7831.78 415.011 6 4 5 -8 7695.03 339.164 5 4 5 -7 7777.80 389.780 6 4 5 -7 7690.17 341.075 5 4 5 -6 17760.9 597.905 6 4 5 -6 17106.6 553.287 5 4 5 -5 3968.06 238.577 6 4 5 -5 3749.30 183.005 1 4 5 -5 3962.36 238.060 5 4 5 -4 4519.66 237.616 6 4 5 -4 4444.70 202.395 1 4 5 -4 4495.59 251.786 5 4 5 -3 329.957 67.7930 5 4 5 -3 249.356 49.7697 6 4 5 -3 279.016 48.8761 1 4 5 -2 3310.82 163.567 6 4 5 -2 2926.89 169.566 1 4 5 -2 2955.61 200.502 5 4 5 -1 249.710 58.8068 5 4 5 -1 223.104 36.1850 6 4 5 -1 213.729 52.7300 1 4 5 0 31634.7 640.821 6 4 5 0 33926.9 856.046 5 4 5 1 37704.6 955.304 5 4 5 2 25436.4 725.816 5 4 5 3 4824.21 270.580 5 4 5 4 5886.01 305.464 5 4 5 5 11109.8 441.291 5 4 5 6 969.746 125.708 5 4 5 7 2409.83 135.379 3 4 5 7 2446.17 200.688 5 4 5 8 10499.1 483.379 7 4 5 8 8241.10 255.535 3 4 5 8 9859.32 424.386 5 4 5 9 21818.3 778.398 7 4 5 9 20110.1 683.197 5 4 5 10 2029.64 227.100 7 4 5 10 2488.45 217.371 5 4 5 11 2455.71 253.872 7 4 5 11 2207.51 208.977 5 4 5 12 38.6987 64.3241 5 4 5 12-56.4126 66.1560 7 4 5 13 801.519 132.569 5 4 5 13 1161.98 194.284 7 4 5 14 58.9233 76.0133 7 4 5 15 1562.81 238.901 7 4 6 -12 4054.45 370.767 6 4 6 -11 2721.84 293.809 6 4 6 -10 1122.57 178.990 6 4 6 -9 623.990 134.092 6 4 6 -8 213.147 82.9108 6 4 6 -7 2641.56 227.686 6 4 6 -7 2489.76 207.809 5 4 6 -6 5300.80 309.857 6 4 6 -6 4557.91 282.238 5 4 6 -5 6876.17 337.326 6 4 6 -5 6570.70 339.999 5 4 6 -4 20400.9 611.523 6 4 6 -4 19387.4 648.822 5 4 6 -3 28925.5 734.976 6 4 6 -3 27498.1 810.428 5 4 6 -2 17636.8 488.664 6 4 6 -2 16710.4 584.723 5 4 6 -1 563.947 102.322 5 4 6 -1 753.049 72.2915 6 4 6 0 455.609 89.8266 5 4 6 0 392.731 44.7935 6 4 6 1 3690.98 120.194 6 4 6 1 4517.60 269.908 5 4 6 2 4497.18 275.460 5 4 6 3 39.8748 49.8598 5 4 6 4 818.327 121.382 5 4 6 5 1714.48 175.021 5 4 6 6 3606.93 256.259 5 4 6 7 1625.73 173.492 5 4 6 8-2.06379 43.7702 5 4 6 9 607.823 114.958 5 4 6 10 7280.24 438.601 7 4 6 10 6541.07 372.533 5 4 6 11 592.435 113.356 5 4 6 11 627.086 140.456 7 4 6 12 6154.89 431.747 7 4 6 12 6162.21 366.579 5 4 6 13 6957.98 474.336 7 4 6 13 6473.21 387.370 5 4 6 14 2295.34 274.952 7 4 6 15 548.949 153.550 7 4 7 -11 2463.02 284.182 6 4 7 -10 3655.70 328.407 6 4 7 -9 4499.58 350.271 6 4 7 -8 1674.37 202.698 6 4 7 -7 316.292 97.8370 6 4 7 -7 248.824 79.2626 5 4 7 -6 9.09426 46.8960 6 4 7 -6 10.3877 47.0495 5 4 7 -5 1428.36 155.865 6 4 7 -5 1176.73 153.469 5 4 7 -4 3413.84 227.373 6 4 7 -4 3105.46 249.023 5 4 7 -3 12335.5 435.923 6 4 7 -3 11090.9 498.583 5 4 7 -2 17856.7 520.300 6 4 7 -2 16876.5 630.974 5 4 7 -1 2039.56 136.366 6 4 7 -1 1797.93 189.593 5 4 7 0 2178.03 123.459 6 4 7 0 1984.98 195.389 5 4 7 1 4468.72 166.559 6 4 7 1 4749.73 301.647 5 4 7 2 474.314 105.808 5 4 7 3 2474.56 218.052 5 4 7 4 17207.0 629.486 5 4 7 5 18582.0 668.221 5 4 7 6 13570.8 556.431 5 4 7 7 111.462 68.0543 5 4 7 8 806.755 136.620 5 4 7 9 265.172 90.9531 5 4 7 10 6199.22 375.566 5 4 7 11 3473.59 323.591 7 4 7 11 3475.04 278.853 5 4 7 12 4410.75 372.603 7 4 7 12 4123.65 309.722 5 4 7 13 12624.7 663.120 7 4 7 13 11571.0 547.657 5 4 7 14 10264.7 613.299 7 4 7 15 2284.25 288.396 7 4 8 -10-18.1341 73.4014 6 4 8 -9 619.664 150.835 6 4 8 -8 1473.13 201.514 6 4 8 -7 637.850 131.204 6 4 8 -7 418.388 108.617 5 4 8 -6 5.26862 54.5048 6 4 8 -6-87.9724 64.6900 5 4 8 -5 1489.77 167.740 6 4 8 -5 1782.63 205.979 5 4 8 -4 2753.47 215.709 6 4 8 -4 2642.83 248.207 5 4 8 -3 157.801 60.1528 6 4 8 -3-10.8056 45.4325 5 4 8 -2 7066.70 313.941 6 4 8 -2 6308.25 391.613 5 4 8 -1 18364.1 536.365 6 4 8 -1 19629.0 719.462 5 4 8 0 15807.1 454.514 6 4 8 0 16184.9 646.365 5 4 8 1 19950.8 510.886 6 4 8 1 20854.5 744.884 5 4 8 2 10821.4 512.147 5 4 8 3 1331.94 177.440 5 4 8 4 5601.50 356.279 5 4 8 5 1204.61 166.828 5 4 8 6 5062.32 339.420 5 4 8 7 23066.1 807.002 5 4 8 8 12486.7 564.573 5 4 8 9 2409.10 240.164 5 4 8 10 1294.49 179.414 5 4 8 11 1662.68 203.445 5 4 8 12 328.100 86.2511 5 4 8 12 204.074 92.7370 7 4 8 13 3790.46 365.260 7 4 8 13 3096.42 281.856 5 4 8 14 6859.11 506.070 7 4 9 -9 54.1087 78.2542 6 4 9 -8 377.857 116.771 6 4 9 -7 1808.00 221.653 6 4 9 -6 3819.50 300.005 6 4 9 -6 3552.61 317.814 5 4 9 -5 2600.46 236.992 6 4 9 -5 2374.34 257.765 5 4 9 -4 987.247 140.646 6 4 9 -4 748.147 141.018 5 4 9 -3 142.616 59.0867 6 4 9 -3-31.4842 63.8832 5 4 9 -2 932.127 123.141 6 4 9 -2 586.295 136.953 5 4 9 -1 8873.19 356.212 6 4 9 -1 8777.16 497.252 5 4 9 0 9348.65 513.079 5 4 9 1 5458.86 384.962 5 4 9 2 1859.01 227.184 5 4 9 3 864.850 160.794 5 4 9 4 932.367 153.630 5 4 9 5 1642.54 209.413 5 4 9 6 991.235 172.608 5 4 9 7 6478.75 414.974 5 4 9 8 7158.22 438.920 5 4 9 9 4951.12 369.457 5 4 9 10 3633.76 316.456 5 4 9 11 462.954 120.316 5 4 9 12 185.159 95.0825 5 4 9 13 97.0575 57.4558 5 4 9 13 5.53751 75.8032 7 4 9 14 552.921 160.220 7 4 10 -6 1894.35 252.631 5 4 10 -5 1897.61 247.514 5 4 10 -4 3397.32 333.290 5 4 10 -3 1187.81 196.690 5 4 10 -2 24.8178 65.2678 5 4 10 -1 285.246 101.947 5 4 10 0 1766.32 226.895 5 4 10 1 28.5623 74.0187 5 4 10 2 4330.68 363.790 5 4 10 3 10700.0 579.510 5 4 10 4 9875.19 550.043 5 4 10 5 3312.77 318.524 5 4 10 6 1201.96 191.830 5 4 10 7 827.223 172.599 5 4 10 8 295.206 94.3049 5 4 10 9 177.280 96.6036 5 4 10 10 552.128 130.993 5 4 10 11 818.644 160.298 5 4 10 12 349.933 116.428 5 4 10 13-76.6764 105.563 5 4 10 13-46.4564 90.3431 7 4 11 -5 70.0080 97.9344 5 4 11 -4 80.8272 93.2804 5 4 11 -3-20.8061 84.1507 5 4 11 -2 181.457 97.8344 5 4 11 -1 817.015 173.621 5 4 11 0 1468.95 233.441 5 4 11 1 1042.78 203.128 5 4 11 2 570.947 158.648 5 4 11 3 593.714 160.491 5 4 11 4 2065.25 263.734 5 4 11 5 401.566 132.261 5 4 11 6 511.208 141.127 5 4 11 7 147.510 79.3590 5 4 11 8 846.675 176.981 5 4 11 9 979.533 191.232 5 4 11 10 1018.16 188.033 5 4 11 11 1492.52 232.055 5 4 11 12 966.257 188.408 5 4 11 13 178.672 85.7033 5 4 12 -1 1630.53 254.364 5 4 12 0 881.880 201.836 5 4 12 1-84.2254 87.4677 5 4 12 2-241.624 114.844 5 4 12 3 84.1976 78.2416 5 4 12 4 159.879 102.715 5 4 12 5 756.397 187.327 5 4 12 6 2293.74 304.129 5 4 12 7 1857.64 281.673 5 4 12 8 508.360 143.675 5 5 -9 -9 196.830 91.8743 1 5 -9 -8 504.969 138.379 1 5 -9 -7 75.2885 66.2103 1 5 -9 -6 89.6725 85.3339 1 5 -9 -5 147.601 102.922 1 5 -9 -4-90.6706 97.2286 1 5 -8 -11 368.873 123.546 9 5 -8 -10 120.174 88.7527 1 5 -8 -10-102.057 84.4039 9 5 -8 -9 142.805 85.6565 1 5 -8 -9-79.9666 96.7084 9 5 -8 -8 24.3198 70.2674 1 5 -8 -8 150.492 86.8625 9 5 -8 -7 136.024 77.6124 1 5 -8 -7-71.3057 79.2497 9 5 -8 -6 1172.21 182.969 1 5 -8 -6 1005.83 213.787 9 5 -8 -5 2391.71 268.177 1 5 -8 -5 2448.86 316.823 9 5 -8 -4 1069.41 183.612 1 5 -8 -4 1030.85 221.288 9 5 -8 -3 64.7255 68.8314 1 5 -8 -3-26.7960 90.5950 9 5 -8 -2 343.485 125.856 1 5 -8 -2 191.162 118.539 9 5 -8 -1 253.956 95.7601 1 5 -8 -1 181.247 110.563 9 5 -8 0 680.223 162.499 1 5 -8 0 947.393 203.776 9 5 -8 1 724.440 168.320 1 5 -8 1 665.786 177.912 9 5 -8 2 1850.56 288.275 9 5 -7 -11 2248.25 277.339 9 5 -7 -10 122.688 70.7246 1 5 -7 -10 121.679 101.127 9 5 -7 -9 77.4216 68.9107 1 5 -7 -9-86.7422 90.8624 9 5 -7 -8 1396.18 185.878 1 5 -7 -8 1148.10 203.051 9 5 -7 -7 501.745 114.802 1 5 -7 -7 489.615 148.018 9 5 -7 -6 148.231 76.6350 1 5 -7 -6 6.76611 86.8544 9 5 -7 -5 2901.68 270.151 1 5 -7 -5 2178.80 287.088 9 5 -7 -4 9900.09 513.618 1 5 -7 -4 8391.57 565.009 9 5 -7 -3 2016.33 229.121 1 5 -7 -3 1862.65 262.404 9 5 -7 -2 2060.95 238.078 1 5 -7 -2 1710.15 258.160 9 5 -7 -1-0.34084 66.8362 1 5 -7 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1-68.5316 75.7329 7 5 -6 1 126.744 80.6396 1 5 -6 1-77.2443 87.6134 9 5 -6 2 1701.47 214.336 1 5 -6 2 1411.43 195.439 7 5 -6 2 1093.58 202.576 9 5 -6 3-9.41017 53.9474 7 5 -6 3 135.673 91.7196 1 5 -6 4 90.6424 83.3597 7 5 -6 4 163.265 90.6658 1 5 -6 4 25.8719 68.3561 9 5 -6 5 1961.33 241.597 1 5 -6 5 1697.16 243.667 7 5 -6 5 1820.38 250.174 9 5 -6 6 2061.29 260.907 1 5 -6 6 1468.74 231.735 7 5 -6 6 1798.51 261.220 9 5 -6 7 1202.11 212.943 7 5 -6 7 1126.40 209.252 9 5 -5 -13 901.474 188.292 6 5 -5 -11 2045.39 243.225 9 5 -5 -10 1727.61 179.197 1 5 -5 -10 1812.19 230.633 9 5 -5 -9 1359.04 157.985 1 5 -5 -9 1175.06 191.870 9 5 -5 -8 9215.51 425.659 1 5 -5 -8 9287.46 543.273 9 5 -5 -7 6801.51 359.296 1 5 -5 -7 7026.15 467.119 9 5 -5 -6 1590.05 173.761 1 5 -5 -6 1547.41 215.540 9 5 -5 -5 134.864 63.7127 1 5 -5 -5 70.9689 77.1435 9 5 -5 -4 3181.16 246.559 1 5 -5 -4 2163.44 262.486 9 5 -5 -3 2953.90 238.026 1 5 -5 -3 2617.14 283.316 9 5 -5 -2 109.093 60.7186 1 5 -5 -2 75.6396 75.4850 9 5 -5 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215.144 6 7 5 -6 1878.45 177.231 6 7 5 -6 1814.52 165.383 5 7 5 -5 4063.90 249.072 6 7 5 -5 3872.74 250.710 5 7 5 -4 1568.33 142.440 6 7 5 -4 1673.46 168.228 5 7 5 -3 679.178 107.904 5 7 5 -3 619.689 84.2086 6 7 5 -2 15922.5 455.381 6 7 5 -2 14677.7 555.767 5 7 5 -1 17101.4 451.265 6 7 5 -1 17217.7 609.971 5 7 5 0 7699.36 237.290 6 7 5 0 7626.54 382.735 5 7 5 1 6426.12 185.843 6 7 5 1 7363.59 377.688 5 7 5 2 1701.02 68.2376 6 7 5 2 2756.70 230.098 5 7 5 3 4092.14 286.907 5 7 5 4-2.83252 51.3716 5 7 5 5 3892.93 293.610 5 7 5 6 4574.88 327.191 7 7 5 6 4174.82 309.002 5 7 5 7 2741.27 260.373 7 7 5 7 2704.10 252.472 5 7 5 8 4705.39 354.522 7 7 5 8 4904.44 349.243 5 7 5 9 3810.12 328.123 7 7 5 9 4192.75 328.802 5 7 5 10 1728.17 226.062 7 7 5 10 1778.60 219.048 5 7 5 11 469.446 128.750 5 7 5 11 422.168 132.700 7 7 5 12 755.282 152.296 5 7 5 12 700.509 167.550 7 7 5 13 3750.23 370.434 7 7 5 13 3438.31 320.327 5 7 5 14 5626.11 415.276 5 7 6 -12 442.389 139.290 6 7 6 -11 328.088 110.878 6 7 6 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420.915 5 7 7 -2 146.607 72.2200 5 7 7 -1 187.615 81.2449 5 7 7 0 1828.32 202.359 5 7 7 1 4546.01 316.431 5 7 7 2 13944.9 594.346 5 7 7 3 18810.6 716.526 5 7 7 4 13688.2 600.860 5 7 7 5 5393.06 365.842 5 7 7 6 322.600 99.1180 5 7 7 7 768.365 147.565 5 7 7 8 83.5694 74.9425 5 7 7 9 2675.36 288.694 7 7 7 9 2966.11 287.899 5 7 7 10 5631.25 431.145 7 7 7 10 5591.28 404.306 5 7 7 11 1142.25 185.891 5 7 7 11 1419.28 222.983 7 7 7 12-103.962 105.984 5 7 7 12-115.600 99.6534 7 7 7 13 50.4332 85.5670 5 7 7 14 21.9369 73.2348 5 7 8 -5 324.377 100.858 5 7 8 -4 2754.07 254.153 5 7 8 -3 11308.6 537.502 5 7 8 -2 10553.1 518.405 5 7 8 -1 5083.62 351.519 5 7 8 0 429.831 112.739 5 7 8 1 939.194 155.973 5 7 8 2 918.246 152.273 5 7 8 3-61.6769 63.2655 5 7 8 4 4490.08 341.636 5 7 8 5 2167.45 242.643 5 7 8 6 4713.84 358.059 5 7 8 7 145.396 71.2564 5 7 8 8 1948.17 236.384 5 7 8 9-216.775 97.2814 5 7 8 10 2819.77 313.460 7 7 8 10 3399.76 320.103 5 7 8 11 7952.93 547.309 7 7 8 11 8213.10 515.292 5 7 8 12 6053.37 488.710 7 7 8 12 6344.79 457.631 5 7 8 13 3647.31 351.811 5 7 8 14 835.856 181.357 5 7 9 -5 129.447 71.8851 5 7 9 -4 75.3113 65.3686 5 7 9 -3 978.620 170.112 5 7 9 -2 4133.95 338.159 5 7 9 -1 1240.89 181.878 5 7 9 0 1378.69 198.318 5 7 9 1 75.6957 61.9354 5 7 9 2 996.844 171.793 5 7 9 3 1070.60 173.082 5 7 9 4-33.1989 75.9441 5 7 9 5 752.862 154.575 5 7 9 6 8090.71 497.921 5 7 9 7 8973.90 528.036 5 7 9 8 4021.42 353.082 5 7 9 9 2010.67 257.053 5 7 9 10 1328.05 210.763 5 7 9 11 1866.68 249.043 5 7 9 11 1711.85 260.713 7 7 9 12 1077.39 193.421 5 7 9 13 708.073 161.411 5 7 10 -4 283.291 119.549 5 7 10 -3 265.742 104.204 5 7 10 -2 6.54074 59.6763 5 7 10 -1 90.7805 83.0579 5 7 10 0 3369.87 326.401 5 7 10 1 3354.24 323.629 5 7 10 2 2719.34 291.037 5 7 10 3 1734.49 237.145 5 7 10 4 646.310 161.545 5 7 10 5 307.753 128.831 5 7 10 6 812.000 172.418 5 7 10 7 1452.05 213.685 5 7 10 8 968.570 186.294 5 7 10 9 38.2840 65.2142 5 7 10 10 820.362 178.273 5 7 10 11 1528.41 235.888 5 7 11 -4 1011.44 190.154 5 7 11 -3 564.797 143.183 5 7 11 -2 277.978 108.328 5 7 11 -1-117.495 83.8289 5 7 11 0-34.7283 79.6533 5 7 11 1 347.277 120.247 5 7 11 2 1517.53 235.039 5 7 11 3 3806.84 367.016 5 7 11 4 3548.15 357.508 5 7 11 5 1744.10 254.505 5 7 11 6 129.528 86.7831 5 7 11 7 60.5382 78.6185 5 7 11 8 214.372 117.214 5 8 -6 -5 140.615 73.7851 1 8 -6 -4 1001.96 174.215 1 8 -6 -3 2580.94 279.609 1 8 -6 -2 127.129 106.705 1 8 -6 -1 105.124 91.1482 1 8 -5 -10-51.6548 87.9748 9 8 -5 -9 933.900 212.639 9 8 -5 -8 975.076 221.194 9 8 -5 -7 1962.88 304.524 9 8 -5 -6 737.038 203.398 9 8 -5 -5 1.51220 61.3331 1 8 -5 -5 89.7487 133.383 9 8 -5 -4 33.9174 53.7256 1 8 -5 -4 129.427 103.060 9 8 -5 -3 742.998 147.462 1 8 -5 -3 1322.96 255.384 9 8 -5 -2 1340.86 194.069 1 8 -5 -2 1441.61 257.828 9 8 -5 -1 385.855 114.759 1 8 -5 -1 424.612 151.913 9 8 -5 0 783.598 158.111 1 8 -5 0 927.738 223.135 9 8 -5 1 947.160 168.312 1 8 -5 1 1140.33 233.884 9 8 -5 2-35.5655 62.1435 1 8 -5 2 142.514 96.4482 9 8 -4 -11 19.8779 86.8826 9 8 -4 -10 40.8597 93.1233 9 8 -4 -9 1372.65 247.317 9 8 -4 -8 3054.38 364.315 9 8 -4 -7 2989.08 353.071 9 8 -4 -6 1124.23 221.401 9 8 -4 -5 140.862 64.3394 1 8 -4 -5-68.2289 118.889 9 8 -4 -4 68.9455 56.3370 1 8 -4 -4 23.8101 90.7950 9 8 -4 -3 1776.87 206.048 1 8 -4 -3 1624.26 281.791 9 8 -4 -2 4674.28 336.461 1 8 -4 -2 5054.21 463.988 9 8 -4 -1 789.231 148.560 1 8 -4 -1 1314.19 236.022 9 8 -4 0 469.889 111.262 1 8 -4 0 1013.04 213.161 9 8 -4 1 2885.96 283.162 1 8 -4 1 3396.71 380.888 9 8 -4 2 781.920 150.460 1 8 -4 2 786.795 182.197 9 8 -4 3 318.268 112.078 1 8 -4 3 471.883 154.016 9 8 -4 4 507.928 132.132 1 8 -4 4 826.837 194.798 9 8 -4 5 1448.29 260.200 9 8 -4 6 948.214 186.016 7 8 -4 6 744.879 189.100 9 8 -3 -11 495.369 150.649 9 8 -3 -10 287.300 136.588 9 8 -3 -9-62.9558 81.2973 9 8 -3 -8 937.917 201.864 9 8 -3 -7 1597.74 254.859 9 8 -3 -6 5307.42 452.945 9 8 -3 -5 3140.47 344.180 9 8 -3 -4 1226.63 151.263 1 8 -3 -4 974.600 206.436 9 8 -3 -3 117.063 70.4213 1 8 -3 -3-118.576 121.094 9 8 -3 -2 3646.27 274.379 1 8 -3 -2 3655.95 373.057 9 8 -3 -1 2442.44 224.983 1 8 -3 -1 3191.30 350.403 9 8 -3 0 5449.14 355.628 1 8 -3 0 5937.75 481.398 9 8 -3 1 7387.19 431.543 1 8 -3 1 8216.83 571.017 9 8 -3 2 3881.07 315.278 1 8 -3 2 4508.78 420.894 9 8 -3 3-25.3567 80.7366 1 8 -3 3-208.961 107.958 9 8 -3 4-13.9488 62.0058 7 8 -3 4-48.3021 70.3719 1 8 -3 4 12.8533 69.6715 9 8 -3 5 443.519 124.397 7 8 -3 5 511.617 149.449 9 8 -3 6 324.215 120.226 7 8 -3 6 389.611 132.259 9 8 -3 7 164.459 86.2444 7 8 -3 7 320.516 120.735 9 8 -3 8 1174.12 214.941 7 8 -2 -11 1434.44 233.448 6 8 -2 -11 1116.66 213.907 9 8 -2 -4 2488.81 192.917 1 8 -2 -3 3983.69 258.209 1 8 -2 -2 11205.8 473.547 1 8 -2 -1 5847.09 337.619 1 8 -2 0 322.879 82.6810 1 8 -2 1 496.954 108.028 1 8 -2 1 464.497 132.783 9 8 -2 2 1557.65 179.390 7 8 -2 2 1842.44 258.036 9 8 -2 2 1711.30 199.924 1 8 -2 3 361.206 92.1041 7 8 -2 3 151.504 99.3843 9 8 -2 3 278.035 88.7262 1 8 -2 4 102.754 68.6495 7 8 -2 4-27.8802 70.8741 9 8 -2 5 176.892 77.3378 7 8 -2 5 170.074 102.377 9 8 -2 6 394.713 112.865 7 8 -2 6 541.192 140.273 9 8 -2 7 111.626 78.6504 7 8 -2 7 115.290 96.3639 9 8 -2 8 521.288 142.868 7 8 -2 9-118.025 94.5788 7 8 -1 -12 1126.21 216.413 6 8 -1 -11 1662.82 240.715 6 8 -1 -10 3062.24 318.195 6 8 -1 -4 1693.24 147.309 1 8 -1 -3 1601.59 151.245 1 8 -1 -2 601.270 95.8365 1 8 -1 -1 2498.33 201.660 1 8 -1 0-33.1733 64.1567 1 8 -1 1 49.4014 39.0953 7 8 -1 1-15.5976 66.7117 1 8 -1 2 368.525 83.0079 7 8 -1 3 512.148 101.999 7 8 -1 4 1685.51 197.086 7 8 -1 4 2039.39 260.703 9 8 -1 5 4396.69 332.440 7 8 -1 5 4635.88 396.898 9 8 -1 6 6718.14 431.427 7 8 -1 6 7113.32 497.362 9 8 -1 7 38.7625 73.2651 7 8 -1 7 272.213 103.557 9 8 -1 8 237.119 101.071 7 8 -1 8 419.002 123.509 9 8 -1 9 867.681 179.276 7 8 0 -12 355.793 124.932 6 8 0 -11 1271.24 212.632 6 8 0 -10 1706.18 229.493 6 8 0 -9 2531.27 277.698 6 8 0 -6 1184.86 135.373 5 8 0 0 7374.59 305.125 7 8 0 1 6506.00 307.093 7 8 0 2 12630.3 482.569 7 8 0 3 3495.28 251.040 7 8 0 4 106.891 67.8371 7 8 0 5 138.483 74.1270 7 8 0 6 12534.9 585.210 7 8 0 7 11683.7 590.263 7 8 0 7 13349.1 670.088 9 8 0 8 4320.80 360.891 7 8 0 8 4801.35 392.231 9 8 0 9 1844.28 256.522 7 8 0 10 73.1217 77.2010 7 8 1 -12 350.857 126.124 6 8 1 -11-335.942 118.561 6 8 1 -10 75.1427 54.6199 6 8 1 -9 211.245 90.4782 6 8 1 -8 419.551 111.479 6 8 1 -6 8946.83 388.264 5 8 1 -5 9220.23 404.994 5 8 1 -4 1870.94 179.250 5 8 1 -3 1553.20 165.640 5 8 1 -2 116.984 66.4743 5 8 1 -1 7018.11 260.076 7 8 1 0 20658.9 572.476 7 8 1 1 6121.41 288.988 7 8 1 2 3025.85 212.722 7 8 1 3 2972.10 221.776 7 8 1 4 1546.12 170.497 7 8 1 5 932.404 139.875 7 8 1 6 3017.57 266.110 7 8 1 7 9668.40 508.197 7 8 1 8 1797.86 227.082 7 8 1 8 2298.33 253.459 5 8 1 9 3202.78 313.259 7 8 1 9 3573.97 322.625 5 8 1 10 620.471 149.450 5 8 1 10 585.697 156.034 7 8 1 11 39.3376 90.7779 5 8 1 11 136.220 99.8482 7 8 2 -12 2650.29 303.204 6 8 2 -11 2433.89 280.446 6 8 2 -10 726.761 155.748 6 8 2 -9-9.53037 55.6188 6 8 2 -8 258.084 97.7323 6 8 2 -7 701.721 132.603 6 8 2 -6 10778.9 505.112 6 8 2 -6 11882.8 446.392 5 8 2 -5 16553.0 567.243 5 8 2 -4 22212.9 699.984 5 8 2 -3 10385.3 448.080 5 8 2 -2-16.7208 45.8956 5 8 2 -2 14.7944 22.2460 7 8 2 -1 4511.78 213.040 7 8 2 -1 4174.29 284.157 5 8 2 0 822.669 97.9665 7 8 2 0 612.262 112.135 5 8 2 1 355.617 95.6114 5 8 2 1 380.832 73.7234 7 8 2 2 8196.50 367.968 7 8 2 2 7993.63 424.163 5 8 2 3 38386.8 1020.25 7 8 2 3 37974.6 1100.44 5 8 2 4 9914.16 450.536 7 8 2 4 9826.56 489.702 5 8 2 5 1403.80 184.979 5 8 2 5 1139.49 153.597 7 8 2 6 265.441 96.9625 5 8 2 6 476.023 104.746 7 8 2 7 552.073 125.042 5 8 2 7 685.063 140.692 7 8 2 8 590.162 143.924 5 8 2 8 842.892 163.158 7 8 2 9 244.592 99.2881 5 8 2 9 309.934 104.648 7 8 2 10 2065.12 259.882 7 8 2 10 2080.71 251.799 5 8 2 11 1274.31 207.471 5 8 2 11 1097.52 189.097 7 8 2 12 2197.75 278.853 5 8 3 -12 2212.96 272.995 6 8 3 -11 2631.98 287.135 6 8 3 -10 3413.07 313.949 6 8 3 -9 1387.42 192.689 6 8 3 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120.139 6 8 4 -9 1618.88 206.482 6 8 4 -8 2423.88 236.517 6 8 4 -7 2151.27 215.113 6 8 4 -6 607.422 104.050 5 8 4 -6 658.671 118.595 6 8 4 -5 44.8315 41.2215 5 8 4 -5 56.9192 39.6102 6 8 4 -4 353.769 82.9251 5 8 4 -4 286.743 73.9790 6 8 4 -3 10413.8 403.227 6 8 4 -3 10099.3 444.168 5 8 4 -2 22457.2 640.434 6 8 4 -2 22888.6 739.618 5 8 4 -1 23265.8 757.516 5 8 4 0 8300.31 417.664 5 8 4 1 3030.69 248.105 5 8 4 2 5.47745 68.8039 5 8 4 2-3.99211 43.8984 7 8 4 3 2748.27 225.924 7 8 4 3 2785.87 246.739 5 8 4 4 120.865 59.5281 5 8 4 4 90.7103 59.7041 7 8 4 5 331.784 97.3167 5 8 4 5 304.609 88.2087 7 8 4 6 3150.30 271.950 7 8 4 6 3375.17 290.461 5 8 4 7 10205.7 522.913 7 8 4 7 9832.30 522.239 5 8 4 8 14584.6 661.919 7 8 4 8 13590.7 637.739 5 8 4 9 1528.66 213.439 5 8 4 9 1712.11 228.571 7 8 4 10-96.5203 78.9651 5 8 4 10 147.538 86.7230 7 8 4 11 293.992 108.269 5 8 4 11 397.201 129.067 7 8 4 12 9.70906 65.5468 5 8 4 12 61.9377 79.9415 7 8 4 13 1836.60 248.804 5 8 5 -12 382.738 145.168 6 8 5 -11 115.114 75.1799 6 8 5 -10 220.995 90.2310 6 8 5 -9 1061.08 162.720 6 8 5 -8 2083.90 216.982 6 8 5 -7 1517.53 177.144 6 8 5 -6 4377.22 286.458 6 8 5 -5 9854.13 423.645 6 8 5 -5 9505.97 429.697 5 8 5 -4 3625.80 231.801 6 8 5 -4 3628.91 258.512 5 8 5 -3 193.391 68.2388 5 8 5 -3 289.099 64.5377 6 8 5 -2 1849.96 140.299 6 8 5 -2 2014.28 195.898 5 8 5 -1 939.925 135.603 5 8 5 -1 895.637 88.4781 6 8 5 0 1809.42 192.011 5 8 5 1 11382.6 514.097 5 8 5 2 11114.3 515.236 5 8 5 3 3266.27 271.330 5 8 5 4 7370.00 405.464 7 8 5 4 7118.07 416.604 5 8 5 5-25.9539 71.2347 5 8 5 5-72.5267 70.9914 7 8 5 6 9.73992 65.6960 5 8 5 6 35.8677 59.8095 7 8 5 7 218.114 97.3517 5 8 5 7 422.258 126.532 7 8 5 8 7118.06 456.243 7 8 5 8 7093.35 448.345 5 8 5 9 9164.02 534.449 7 8 5 9 9439.63 529.411 5 8 5 10 928.676 173.930 5 8 5 10 1062.83 192.380 7 8 5 11 940.986 169.854 5 8 5 11 1196.63 214.460 7 8 5 12 58.1246 79.4820 5 8 5 12 387.755 150.201 7 8 5 13 223.975 114.032 5 8 6 -5 3522.79 267.523 5 8 6 -4 2940.12 243.939 5 8 6 -3 242.261 72.8587 5 8 6 -2 1290.18 162.943 5 8 6 -1 4501.48 311.444 5 8 6 0 144.301 69.3124 5 8 6 1 4946.06 334.849 5 8 6 2 13663.7 590.968 5 8 6 3 14643.3 622.273 5 8 6 4 6068.67 389.896 5 8 6 5 5402.28 370.907 5 8 6 6 138.236 80.5296 5 8 6 6 45.8262 71.6465 7 8 6 7 136.227 73.8911 5 8 6 7 86.4417 60.5387 7 8 6 8 3240.28 307.226 7 8 6 8 3327.63 307.419 5 8 6 9 11776.0 624.278 7 8 6 9 11303.8 591.010 5 8 6 10 4381.96 382.362 7 8 6 10 3999.73 349.225 5 8 6 11 3776.54 364.422 7 8 6 11 2989.36 307.669 5 8 6 12 3195.02 350.403 7 8 6 12 3243.97 326.962 5 8 6 13 391.717 138.483 5 8 7 -5 53.6926 57.6462 5 8 7 -4 2226.78 221.172 5 8 7 -3 8312.93 443.917 5 8 7 -2 4364.65 316.158 5 8 7 -1 1992.54 214.247 5 8 7 0-14.4080 70.0999 5 8 7 1 19.1399 59.3930 5 8 7 2 2026.72 223.888 5 8 7 3 4177.80 326.120 5 8 7 4 8867.43 491.806 5 8 7 5 25182.9 906.062 5 8 7 6 7929.47 474.547 5 8 7 7 957.826 172.967 5 8 7 8 367.806 117.444 5 8 7 8 280.100 106.950 7 8 7 9 1408.59 211.640 5 8 7 9 1849.95 253.377 7 8 7 10 2589.59 303.722 7 8 7 10 2914.32 298.482 5 8 7 11 715.535 164.968 5 8 7 11 472.960 147.532 7 8 7 12 1063.68 190.991 5 8 7 13 543.508 161.466 5 8 8 -5-57.8106 55.3759 5 8 8 -4 921.029 156.576 5 8 8 -3 3931.57 311.558 5 8 8 -2 8111.08 458.676 5 8 8 -1 7455.90 444.373 5 8 8 0 1922.76 226.385 5 8 8 1 1268.71 187.395 5 8 8 2 2590.58 265.155 5 8 8 3 1120.89 173.043 5 8 8 4 950.861 170.905 5 8 8 5 1379.41 211.027 5 8 8 6 3435.44 317.003 5 8 8 7 1309.35 200.154 5 8 8 8 92.8209 77.1653 5 8 8 9 28.9001 61.8938 5 8 8 9-12.9847 75.9714 7 8 8 10 176.038 109.027 5 8 8 10-65.0246 72.3982 7 8 8 11 388.768 126.609 5 8 8 11 264.984 115.502 7 8 8 12-52.4877 90.7465 5 8 9 -4 1572.67 206.093 5 8 9 -3 98.6015 70.5360 5 8 9 -2 381.840 105.385 5 8 9 -1 1501.41 207.452 5 8 9 0 2722.04 277.717 5 8 9 1 2928.98 287.294 5 8 9 2 2137.59 250.404 5 8 9 3 380.815 109.879 5 8 9 4 387.412 128.087 5 8 9 5 1713.27 234.255 5 8 9 6 113.355 92.2505 5 8 9 7 516.208 143.772 5 8 9 8 557.536 151.384 5 8 9 9 3334.90 335.489 5 8 9 10 3801.50 385.844 7 8 9 10 3330.93 344.680 5 8 9 11 2382.79 294.226 5 8 10 -4 1518.15 216.733 5 8 10 -3 1177.83 196.904 5 8 10 -2 549.625 135.864 5 8 10 -1-4.35755 70.3771 5 8 10 0-10.7022 77.8548 5 8 10 1 27.8742 58.9038 5 8 10 2 1796.75 241.689 5 8 10 3 4363.78 376.468 5 8 10 4 4996.09 408.181 5 8 10 5 596.550 147.478 5 8 10 6 32.1577 68.1535 5 8 10 7 110.024 96.8404 5 8 10 8-39.7885 87.7643 5 8 10 9 3313.02 348.329 5 8 11 -3 2109.74 270.706 5 8 11 -2 2524.86 300.337 5 8 11 -1 716.346 154.660 5 8 11 0 143.192 106.333 5 8 11 1-36.9922 74.1990 5 8 11 2 68.0694 82.6294 5 8 11 3 23.4335 85.6227 5 8 11 4 1738.52 245.572 5 8 11 5 2049.37 272.053 5 8 11 6 2566.47 312.089 5 9 -5 -3 1750.56 220.417 1 9 -5 -2 620.565 140.570 1 9 -5 -1 529.224 141.055 1 9 -5 0 753.548 162.906 1 9 -4 -7 1374.55 260.633 9 9 -4 -6 524.661 198.724 9 9 -4 -5 154.777 106.538 9 9 -4 -4 344.073 146.345 9 9 -4 -3 698.993 129.519 1 9 -4 -3 669.069 177.013 9 9 -4 -2 193.522 67.6087 1 9 -4 -2 535.037 194.661 9 9 -4 -1-30.5142 56.0201 1 9 -4 -1 28.8524 82.6768 9 9 -4 0 1623.01 216.820 1 9 -4 0 1953.33 309.326 9 9 -4 1 2880.01 295.203 1 9 -4 2 430.377 113.887 1 9 -3 -10 490.175 167.742 9 9 -3 -9 781.761 194.172 9 9 -3 -8 344.746 149.155 9 9 -3 -7 766.054 195.055 9 9 -3 -6 966.778 211.783 9 9 -3 -5 402.841 150.993 9 9 -3 -4 592.327 159.642 9 9 -3 -3 1270.44 164.713 1 9 -3 -3 795.073 196.731 9 9 -3 -2 1833.01 203.887 1 9 -3 -2 1994.18 303.231 9 9 -3 -1 433.660 114.308 1 9 -3 -1 221.223 119.238 9 9 -3 0 241.112 95.0730 1 9 -3 0 552.843 163.754 9 9 -3 1 1936.19 224.685 1 9 -3 1 1854.94 285.584 9 9 -3 2 311.410 94.9421 1 9 -3 2 281.640 134.697 9 9 -3 3 4067.72 430.766 9 9 -3 3 3858.58 340.857 1 9 -3 4 4450.42 452.645 9 9 -3 5 2655.03 351.526 9 9 -3 6 630.239 172.638 9 9 -2 -10 1422.37 254.481 9 9 -2 -2 4806.62 312.866 1 9 -2 -1 1281.48 161.984 1 9 -2 0 706.375 123.657 1 9 -2 0 884.409 193.124 9 9 -2 1 4956.82 456.883 9 9 -2 1 5102.29 352.614 1 9 -2 2 2567.97 326.488 9 9 -2 3 656.676 187.781 9 9 -2 4 2349.14 311.639 9 9 -2 5 2175.99 303.363 9 9 -2 6 657.881 168.287 9 9 -2 7-60.7958 90.6382 7 9 -2 7-12.0115 72.2153 9 9 -1 -10 922.425 177.271 6 9 -1 4 114.802 85.4827 9 9 -1 5-43.4003 60.3773 7 9 -1 5-60.4296 116.150 9 9 -1 6 609.368 141.290 7 9 -1 6 541.159 156.352 9 9 -1 7 1811.40 244.766 7 9 -1 7 1440.98 248.551 9 9 -1 8 3326.66 337.084 7 9 0 -11 43.1442 76.7226 6 9 0 -10 111.778 94.2090 6 9 0 -9 361.438 119.811 6 9 0 -5 2028.36 201.145 5 9 0 3 143.144 76.2605 7 9 0 4-33.6876 45.0443 7 9 0 5 4022.88 314.945 7 9 0 6 5444.83 385.784 7 9 0 6 5462.67 445.223 9 9 0 7 3085.60 301.309 7 9 0 7 3138.62 338.661 9 9 0 8 1963.53 257.239 7 9 0 9 991.106 188.739 7 9 1 -11 943.004 185.635 6 9 1 -10 205.523 105.572 6 9 1 -9 122.076 76.9803 6 9 1 -8 282.361 105.765 6 9 1 -5 6385.70 359.342 5 9 1 -4 2268.54 216.696 5 9 1 -3 463.979 98.4344 5 9 1 -2 1062.26 150.029 5 9 1 -1 2155.13 219.724 5 9 1 2 7025.40 347.278 7 9 1 3 12418.7 508.351 7 9 1 4 4255.09 297.737 7 9 1 5 424.991 97.4550 7 9 1 6 23.4690 68.4120 7 9 1 7 79.7632 80.0345 5 9 1 7 28.3684 69.2451 7 9 1 8 2720.48 290.027 7 9 1 8 3065.06 323.823 9 9 1 8 2881.10 310.613 5 9 1 9 5410.08 426.408 7 9 1 9 4960.48 408.811 5 9 1 10 3484.92 353.329 7 9 2 -11 841.658 177.986 6 9 2 -10 436.318 118.857 6 9 2 -9 562.582 133.066 6 9 2 -8 675.686 138.361 6 9 2 -7 400.574 110.861 6 9 2 -5 1991.38 192.883 5 9 2 -4 5316.36 328.955 5 9 2 -3 4835.18 319.932 5 9 2 -2 7058.53 397.473 5 9 2 -1 6095.63 370.246 5 9 2 0 5271.88 348.950 5 9 2 1 1576.39 150.789 7 9 2 1 1554.22 193.637 5 9 2 2-32.7500 77.4380 5 9 2 2 33.7698 43.8656 7 9 2 3 168.457 77.5805 5 9 2 3 129.094 56.1620 7 9 2 4 61.7543 68.7000 5 9 2 4 7.02309 43.4020 7 9 2 5 2227.40 225.659 7 9 2 5 2042.03 237.651 5 9 2 6 11602.3 553.043 7 9 2 6 11574.6 595.620 5 9 2 7 2870.85 275.877 7 9 2 7 3041.15 302.742 5 9 2 8 527.401 136.658 5 9 2 8 381.487 118.768 7 9 2 9 1552.33 227.198 5 9 2 9 1147.68 195.037 7 9 2 10 200.870 99.6099 5 9 2 10 141.637 77.3820 7 9 3 -11-43.3421 67.3180 6 9 3 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244.012 5 9 4 -4 507.896 99.1442 5 9 4 -4 714.922 110.308 6 9 4 -3 154.997 68.0113 5 9 4 -3 117.098 45.4287 6 9 4 -2 777.638 134.660 5 9 4 -1 1791.16 160.286 7 9 4 -1 1770.82 198.466 5 9 4 0 16332.9 560.515 7 9 4 0 15942.6 643.984 5 9 4 1 19327.9 640.354 7 9 4 1 17587.1 699.562 5 9 4 2 20560.4 686.707 7 9 4 2 19663.0 754.082 5 9 4 3 6087.16 353.515 7 9 4 3 5493.04 377.861 5 9 4 4 2351.05 223.489 7 9 4 4 2010.75 232.321 5 9 4 5 1222.29 185.852 5 9 4 5 1394.94 178.566 7 9 4 6 684.094 145.762 5 9 4 6 576.624 123.962 7 9 4 7 1157.75 183.511 5 9 4 7 1251.15 185.511 7 9 4 8 734.142 152.126 5 9 4 8 858.785 165.168 7 9 4 9 1483.45 216.125 5 9 4 9 1448.98 217.641 7 9 4 10 2725.26 310.755 7 9 4 10 2994.66 309.807 5 9 4 11 652.181 160.017 5 9 4 11 871.012 181.466 7 9 5 -5 9583.53 451.521 5 9 5 -4 11039.2 498.029 5 9 5 -3 1233.90 165.419 5 9 5 -2-2.70843 51.0640 5 9 5 -1 237.880 81.4892 5 9 5 0 1191.88 168.581 5 9 5 1 3343.64 281.744 5 9 5 2 1578.92 178.186 7 9 5 2 1748.69 206.160 5 9 5 3 2664.42 240.141 7 9 5 3 2676.43 262.811 5 9 5 4 4759.69 331.816 7 9 5 4 5327.22 377.508 5 9 5 5 161.877 93.7558 5 9 5 5 54.7362 54.0611 7 9 5 6 264.517 98.9702 5 9 5 6 427.196 111.115 7 9 5 7 1016.33 180.285 5 9 5 7 1109.80 177.889 7 9 5 8 1257.08 203.870 5 9 5 8 1332.88 199.242 7 9 5 9 1839.50 242.348 5 9 5 9 1740.48 239.459 7 9 5 10 2007.06 260.796 5 9 5 10 1878.31 254.335 7 9 5 11 1255.95 210.381 5 9 5 11 1465.73 236.071 7 9 6 -5 922.287 140.952 5 9 6 -4 5466.99 354.504 5 9 6 -3 4516.80 318.230 5 9 6 -2 2056.03 218.462 5 9 6 -1 378.638 101.238 5 9 6 0 220.337 77.5428 5 9 6 1-22.6111 58.8904 5 9 6 2 1251.24 178.609 5 9 6 3 258.460 105.713 5 9 6 4 3129.04 281.847 7 9 6 4 3065.38 287.349 5 9 6 5 9353.46 507.949 7 9 6 5 9650.15 530.516 5 9 6 6 5160.70 378.956 7 9 6 6 4429.50 358.210 5 9 6 7 1732.49 227.094 5 9 6 7 1483.64 216.960 7 9 6 8 794.757 162.995 5 9 6 8 912.407 166.306 7 9 6 9 222.051 94.5976 5 9 6 9 253.419 112.818 7 9 6 10 1270.00 206.682 5 9 6 10 824.911 182.476 7 9 6 11 2698.01 308.443 5 9 7 -4 23.5334 55.7366 5 9 7 -3 1314.79 179.177 5 9 7 -2 2043.20 227.251 5 9 7 -1 1760.72 214.540 5 9 7 0 939.433 159.674 5 9 7 1 905.708 164.353 5 9 7 2 151.096 78.1075 5 9 7 3 1.73459 62.2495 5 9 7 4 191.634 96.2816 5 9 7 5 2733.95 285.548 5 9 7 6 4627.05 370.529 7 9 7 6 4849.44 384.204 5 9 7 7 4909.08 392.517 7 9 7 7 4917.75 392.740 5 9 7 8 10428.6 603.374 7 9 7 8 10510.7 594.416 5 9 7 9 3666.42 357.193 7 9 7 9 3381.58 336.349 5 9 7 10 1444.17 221.414 5 9 7 10 1291.09 220.036 7 9 8 -4 533.451 125.381 5 9 8 -3-29.4993 56.8833 5 9 8 -2-48.6623 68.7884 5 9 8 -1 890.649 158.389 5 9 8 0 3658.21 321.412 5 9 8 1 10499.0 561.021 5 9 8 2 7711.25 479.123 5 9 8 3 2051.95 244.675 5 9 8 4-28.0092 78.5367 5 9 8 5 174.035 91.6990 5 9 8 6 1119.54 196.826 5 9 8 7 2010.26 260.559 5 9 8 8 7748.40 527.766 7 9 8 8 7703.46 517.627 5 9 8 9 2910.45 330.290 7 9 8 9 3265.42 334.676 5 9 8 10 292.808 102.122 5 9 8 10 92.8046 85.6336 7 9 9 -4 3802.50 329.537 5 9 9 -3 2555.40 274.384 5 9 9 -2 558.623 125.412 5 9 9 -1 0.37451 67.4354 5 9 9 0 209.099 89.7518 5 9 9 1 3106.84 306.718 5 9 9 2 5628.96 423.572 5 9 9 3 9149.83 549.702 5 9 9 4 1818.76 245.248 5 9 9 5 395.159 129.782 5 9 9 6 1128.26 200.744 5 9 9 7 1014.31 189.648 5 9 9 8-128.734 98.3219 5 9 9 9 1902.03 271.905 7 9 10 -3 2807.96 300.904 5 9 10 -2 1355.30 213.790 5 9 10 -1 235.322 99.8147 5 9 10 0 100.808 80.9095 5 9 10 1 34.8241 91.5759 5 9 10 2 353.996 133.877 5 9 10 3 1660.07 242.343 5 9 10 4 2452.18 290.894 5 9 10 5 3328.90 344.921 5 9 10 6 2174.76 283.519 5 9 11 -2 1275.21 215.431 5 9 11 -1 1109.03 206.222 5 9 11 0 858.578 194.737 5 9 11 1 272.107 113.621 5 9 11 2 314.455 112.117 5 10 -3 0 325.335 108.808 1 10 -2 -3 476.794 164.060 9 10 -2 -2 1907.51 304.025 9 10 -2 -1 510.195 175.467 9 10 -2 0 1968.34 305.813 9 10 -2 1 1840.06 302.308 9 10 -2 2 196.410 97.9966 9 10 -2 3 428.245 147.876 9 10 -1 3 1136.51 232.449 9 10 -1 4-188.644 108.306 9 10 -1 5-96.0536 70.4383 9 10 -1 6 174.508 109.233 9 10 0 -9 48.7258 83.5948 6 10 0 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1150.31 171.884 7 10 2 7 974.732 189.671 5 10 2 7 1127.53 183.568 7 10 2 8 322.461 107.590 7 10 2 9 1089.11 193.580 7 10 3 -10 203.231 95.7281 6 10 3 -9-51.8703 63.4234 6 10 3 -8 590.715 137.502 6 10 3 -7 3755.92 314.433 6 10 3 -6 6757.07 411.227 6 10 3 -5 3635.96 292.385 6 10 3 -4 341.410 96.6426 5 10 3 -3 69.1161 67.4251 5 10 3 -2 393.655 103.130 5 10 3 -1 1526.32 198.808 5 10 3 0 2118.49 237.400 5 10 3 1 1656.95 215.854 5 10 3 2 2399.27 257.809 5 10 3 3 4157.42 345.554 5 10 3 4 157.347 86.5708 5 10 3 4 195.827 76.0467 7 10 3 5 149.060 85.7037 5 10 3 5 268.916 89.9916 7 10 3 6 1401.54 223.021 5 10 3 6 1312.38 187.561 7 10 3 7 3654.29 328.510 7 10 3 7 3940.57 362.727 5 10 3 8 7386.65 481.334 7 10 3 8 7087.74 500.129 5 10 3 9 4863.41 407.573 7 10 4 -4 1665.20 191.683 5 10 4 -3 461.728 108.749 5 10 4 -2 168.981 69.3633 5 10 4 -1 76.2365 68.9302 5 10 4 0 168.512 76.1492 5 10 4 1 1072.62 171.775 5 10 4 2 3122.09 298.521 5 10 4 3 11241.4 505.050 7 10 4 3 10521.3 564.538 5 10 4 4 5968.40 373.402 7 10 4 4 5355.79 401.998 5 10 4 5 4084.29 324.833 7 10 4 5 4315.60 362.823 5 10 4 6 1781.34 239.004 5 10 4 6 1428.66 198.460 7 10 4 7 137.386 82.2962 5 10 4 7 71.6349 74.1066 7 10 4 8 1674.87 241.277 5 10 4 8 2021.27 255.108 7 10 4 9 1374.28 225.204 7 10 5 -4 2100.72 216.526 5 10 5 -3 3488.54 290.249 5 10 5 -2 2224.82 232.201 5 10 5 -1 3984.65 318.437 5 10 5 0 2244.49 242.676 5 10 5 1 759.668 140.465 5 10 5 2 433.360 123.678 5 10 5 2 308.623 87.1056 7 10 5 3 628.590 140.423 5 10 5 3 722.623 128.504 7 10 5 4 4401.38 327.514 7 10 5 4 4192.59 354.764 5 10 5 5 2531.06 259.557 7 10 5 5 2235.78 261.501 5 10 5 6 2640.14 271.253 7 10 5 6 2876.71 302.612 5 10 5 7-53.2694 96.3152 5 10 5 7 123.971 87.7698 7 10 5 8 183.676 95.5188 5 10 5 8 193.711 95.1379 7 10 5 9 89.2601 68.1509 7 10 6 -4-0.90987 55.6104 5 10 6 -3 717.668 143.095 5 10 6 -2 4884.27 354.576 5 10 6 -1 4794.59 358.379 5 10 6 0 4675.08 358.075 5 10 6 1 245.315 89.4496 5 10 6 2-11.3736 58.2103 5 10 6 2-4.01998 64.1645 7 10 6 3 502.349 124.984 5 10 6 3 388.374 104.978 7 10 6 4-44.3829 81.6727 5 10 6 4-57.2694 78.3189 7 10 6 5 173.569 94.5415 5 10 6 5-12.0868 69.5734 7 10 6 6 1238.18 209.083 5 10 6 6 776.292 156.150 7 10 6 7 2504.78 278.445 7 10 6 7 2491.52 291.075 5 10 6 8 571.292 149.162 5 10 6 8 453.214 121.501 7 10 6 9 1283.48 211.507 7 10 7 -4 572.471 134.263 5 10 7 -3 185.320 66.2610 5 10 7 -2 213.431 91.9152 5 10 7 -1 197.804 94.1221 5 10 7 0 4667.10 367.640 5 10 7 1 4038.74 345.335 5 10 7 2 2199.88 257.857 5 10 7 3 93.7822 99.3538 5 10 7 4 79.0414 79.8161 5 10 7 5 323.841 107.419 5 10 7 5 210.553 99.8970 7 10 7 6-0.83267 71.3964 5 10 7 6-8.25372 96.6731 7 10 7 7 2734.48 300.101 7 10 7 7 2927.56 321.365 5 10 7 8 3380.58 341.774 7 10 7 8 2575.78 300.394 5 10 7 9 2023.36 269.464 7 10 8 -3 423.202 122.742 5 10 8 -2 117.243 64.9590 5 10 8 -1 110.796 77.5091 5 10 8 0 16.7745 64.4187 5 10 8 1 3078.03 307.165 5 10 8 2 3686.66 340.104 5 10 8 3 3967.63 359.778 5 10 8 4 4050.19 364.943 5 10 8 5 826.673 172.942 5 10 8 6 35.5194 74.1162 5 10 8 6 87.3574 86.4672 7 10 8 7 41.1290 79.1687 5 10 8 7-64.4851 112.507 7 10 8 8 1929.96 269.184 7 10 9 -3 2229.67 255.268 5 10 9 -2 1470.88 210.897 5 10 9 -1 397.238 115.017 5 10 9 0 41.7332 74.3239 5 10 9 1 881.150 176.367 5 10 9 2 640.963 151.403 5 10 9 3 1978.25 265.831 5 10 9 4 5122.62 425.732 5 10 9 5 6044.46 466.689 5 10 10 -2 986.206 183.133 5 10 10 -1 1434.24 222.379 5 10 10 0 390.136 131.063 5 10 10 1 579.155 148.907 5 10 10 2 192.972 100.843 5 10 10 3-76.0190 76.7954 5 11 0 -4 555.953 144.225 5 11 0 -3 1284.08 198.688 5 11 0 -2 1393.83 208.915 5 11 1 -8 618.184 157.654 6 11 1 -4 633.421 138.611 5 11 1 -3 2075.29 243.467 5 11 1 -2 2440.91 267.520 5 11 1 -1 1536.58 218.138 5 11 1 0 258.858 85.8729 5 11 1 1 0.79909 76.7047 5 11 1 2 59.4732 69.7094 5 11 1 3 111.914 84.9987 5 11 2 -4 130.728 62.3333 5 11 2 -3 120.181 78.6667 5 11 2 -2 363.093 106.435 5 11 2 -1 1565.00 212.776 5 11 2 0 3205.22 310.713 5 11 2 1 3335.78 326.613 5 11 2 2 2192.97 267.065 5 11 2 3 462.992 134.202 5 11 2 4 141.653 100.347 5 11 3 -4 864.795 154.220 5 11 3 -3 1049.67 167.336 5 11 3 -2 806.446 154.739 5 11 3 -1 576.686 137.379 5 11 3 0 902.766 166.321 5 11 3 1 1847.88 239.268 5 11 3 2 2745.15 296.560 5 11 3 3 3024.58 314.078 5 11 3 4 770.173 161.380 5 11 3 5-53.3009 79.3950 5 11 4 -3 2534.94 261.425 5 11 4 -2 707.387 142.956 5 11 4 -1 643.576 140.455 5 11 4 0 346.132 111.101 5 11 4 1 41.5344 67.6943 5 11 4 2 63.1676 73.4152 5 11 4 3 483.227 138.175 5 11 4 4 1537.42 226.977 5 11 4 5 2613.60 304.017 5 11 4 7 974.684 171.656 7 11 4 8 2075.56 263.453 7 11 5 -3 671.436 137.475 5 11 5 -2 3250.47 300.850 5 11 5 -1 4660.79 363.694 5 11 5 0 1874.97 234.333 5 11 5 1 463.168 113.381 5 11 5 2 186.980 91.1037 5 11 5 3 248.922 105.655 5 11 5 4 1685.36 236.383 5 11 5 5 3392.90 340.962 5 11 5 6 4007.89 347.431 7 11 5 7 2701.06 288.513 7 11 5 8 1296.34 211.338 7 11 6 -3 127.652 79.2051 5 11 6 -2 53.9749 70.2410 5 11 6 -1 582.360 142.850 5 11 6 0 1935.49 239.634 5 11 6 1 4588.54 376.570 5 11 6 2 2497.91 282.143 5 11 6 3 1596.25 224.787 5 11 6 4-33.5543 78.0098 5 11 6 5-14.1128 88.5798 5 11 6 5 11.1743 59.6671 7 11 6 6-29.4707 75.7376 7 11 6 7 978.657 181.377 7 11 6 8 700.338 160.460 7 11 7 -3 58.0045 72.1170 5 11 7 -2-14.3569 76.6803 5 11 7 -1 121.561 78.8359 5 11 7 0 805.690 156.088 5 11 7 1 893.586 179.609 5 11 7 2 2334.50 276.346 5 11 7 3 2069.56 265.919 5 11 7 4 985.831 180.425 5 11 7 4 1084.06 180.560 7 11 7 5-44.7605 84.4235 5 11 7 5 67.7072 75.8307 7 11 7 6 129.078 83.4209 7 11 7 7-165.581 118.295 7 11 7 8-57.2242 105.162 7 11 8 -2 2843.75 302.334 5 11 8 -1 604.928 146.849 5 11 8 0 237.674 118.701 5 11 8 1 11.5019 96.9689 5 11 8 2 180.143 99.7661 5 11 8 3 255.694 107.646 5 11 8 4 3150.20 318.466 7 11 8 5 2733.31 308.681 7 11 8 6 2334.13 286.455 7 11 8 7 192.975 104.537 7 11 9 -2 2063.74 263.484 5 11 9 -1 1190.39 208.089 5 11 9 0 1352.92 219.693 5 11 9 1 409.168 130.386 5 11 9 6 2379.23 301.741 7 12 1 -3-35.2996 67.9565 5 12 1 -2 85.1247 84.0143 5 12 1 -1 1693.73 246.885 5 12 2 -3-16.5764 65.3950 5 12 2 -2 199.974 102.014 5 12 2 -1 386.739 126.073 5 12 2 0 184.594 91.3411 5 12 3 -3 278.699 123.433 5 12 3 -2 264.968 107.487 5 12 3 -1 43.8132 90.4533 5 12 3 0 685.107 169.912 5 12 3 1 80.6225 75.3685 5 12 4 -2 1421.89 216.187 5 12 4 -1 1831.44 239.316 5 12 4 0 1499.65 228.162 5 12 4 1 274.355 108.155 5 12 5 -2-54.2488 88.2454 5 12 5 -1 1103.67 188.853 5 12 5 0 1437.83 224.686 5 12 5 1 4218.93 381.075 5 12 6 -2 461.186 130.898 5 12 6 -1 818.768 172.211 5 12 6 0 1750.30 240.997 5 12 6 1 3225.63 329.221 5 12 7 -2 1559.44 229.570 5 12 7 -1 285.136 122.534 5 12 7 0-39.6528 84.3700 5 12 8 -1 489.185 144.207 5 ; _shelx_hkl_checksum 2289 data_3 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C2 H6 O)' _chemical_formula_sum 'C40 H44 Cl2 Cu N8 O10' _chemical_formula_weight 931.27 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3377(3) _cell_length_b 9.7888(4) _cell_length_c 12.9870(6) _cell_angle_alpha 103.114(5) _cell_angle_beta 90.344(5) _cell_angle_gamma 109.408(4) _cell_volume 1086.13(8) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 6342 _cell_measurement_theta_min 2.8983 _cell_measurement_theta_max 28.8212 _exptl_crystal_description prism _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.424 _exptl_crystal_F_000 483 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.17 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.10 _exptl_absorpt_coefficient_mu 0.691 _shelx_estimated_absorpt_T_min 0.892 _shelx_estimated_absorpt_T_max 0.934 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.890 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 12262 _diffrn_reflns_av_unetI/netI 0.0267 _diffrn_reflns_av_R_equivalents 0.0270 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 2.905 _diffrn_reflns_theta_max 24.999 _diffrn_reflns_theta_full 24.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 3812 _reflns_number_gt 3397 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0851P)^2^+2.6183P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3812 _refine_ls_number_parameters 365 _refine_ls_number_restraints 423 _refine_ls_R_factor_all 0.0725 _refine_ls_R_factor_gt 0.0661 _refine_ls_wR_factor_ref 0.1758 _refine_ls_wR_factor_gt 0.1697 _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_restrained_S_all 1.262 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.5000 0.0294(2) Uani 1 2 d S . P . . Cl Cl 0.23383(15) -0.24826(17) 0.36963(9) 0.0597(4) Uani 1 1 d D . . . . O1 O 0.1642(5) -0.1719(4) 0.4419(3) 0.0610(9) Uani 1 1 d D U . . . O2A O 0.2214(14) -0.1930(10) 0.2702(7) 0.060(3) Uani 0.44 1 d D U P A 1 O3A O 0.3902(10) -0.2390(16) 0.3890(8) 0.089(3) Uani 0.44 1 d D U P A 1 O4A O 0.2077(11) -0.3924(10) 0.3429(7) 0.058(2) Uani 0.44 1 d D U P A 1 O2B O 0.1766(10) -0.2726(12) 0.2643(6) 0.081(3) Uani 0.56 1 d D U P A 2 O3B O 0.3923(7) -0.1525(7) 0.4034(7) 0.0557(18) Uani 0.56 1 d D U P A 2 O4B O 0.1582(12) -0.4023(8) 0.3912(7) 0.090(3) Uani 0.56 1 d D U P A 2 N1A N 0.2757(4) 0.3830(4) 0.4230(3) 0.0391(8) Uani 1 1 d D . . . . H1A H 0.292(6) 0.473(2) 0.420(4) 0.059 Uiso 1 1 d D U . . . C2A C 0.1504(5) 0.2980(4) 0.4580(3) 0.0362(9) Uani 1 1 d . . . . . H2A H 0.0652 0.3272 0.4780 0.043 Uiso 1 1 calc R U . . . N3A N 0.1621(4) 0.1678(3) 0.4607(2) 0.0321(7) Uani 1 1 d . . . . . C4A C 0.3022(4) 0.1722(4) 0.4261(3) 0.0332(8) Uani 1 1 d . . . . . H4A H 0.3426 0.0938 0.4202 0.040 Uiso 1 1 calc R U . . . C5A C 0.3750(5) 0.3052(4) 0.4014(3) 0.0329(8) Uani 1 1 d . . . . . C6A C 0.5224(5) 0.3622(4) 0.3594(3) 0.0385(9) Uani 1 1 d . . . . . C7A C 0.5624(6) 0.4887(5) 0.3198(4) 0.0495(11) Uani 1 1 d . . . . . H7A H 0.4931 0.5412 0.3201 0.059 Uiso 1 1 calc R U . . . C8A C 0.7019(7) 0.5392(5) 0.2798(4) 0.0604(14) Uani 1 1 d . . . . . H8A H 0.7276 0.6256 0.2524 0.073 Uiso 1 1 calc R U . . . C9A C 0.8034(7) 0.4652(6) 0.2796(4) 0.0655(16) Uani 1 1 d . . . . . H9A H 0.8992 0.5001 0.2520 0.079 Uiso 1 1 calc R U . . . C10A C 0.7659(6) 0.3395(7) 0.3197(5) 0.0644(14) Uani 1 1 d . . . . . H10A H 0.8365 0.2886 0.3202 0.077 Uiso 1 1 calc R U . . . C11A C 0.6259(6) 0.2878(6) 0.3591(4) 0.0510(11) Uani 1 1 d . . . . . H11A H 0.6003 0.2010 0.3861 0.061 Uiso 1 1 calc R U . . . N1B N -0.2872(5) -0.1037(5) 0.2275(3) 0.0561(11) Uani 1 1 d D . . . . H1B H -0.377(3) -0.126(7) 0.198(5) 0.084 Uiso 1 1 d D U . . . C2B C -0.2556(6) -0.0664(6) 0.3331(4) 0.0513(12) Uani 1 1 d . . . . . H2B H -0.3274 -0.0557 0.3831 0.062 Uiso 1 1 calc R U . . . N3B N -0.1120(4) -0.0466(3) 0.3587(2) 0.0336(7) Uani 1 1 d . . . . . C4B C -0.0497(5) -0.0731(5) 0.2637(3) 0.0419(10) Uani 1 1 d . . . . . H4B H 0.0534 -0.0664 0.2566 0.050 Uiso 1 1 calc R U . . . C5B C -0.1573(6) -0.1103(5) 0.1815(3) 0.0511(12) Uani 1 1 d D . . . . C6B C -0.1358(14) -0.1748(13) 0.0644(4) 0.051(3) Uani 0.45 1 d DG U P B 1 C7B C -0.2193(12) -0.1513(12) -0.0147(6) 0.064(3) Uani 0.45 1 d G U P B 1 H7B H -0.2888 -0.0993 0.0038 0.076 Uiso 0.45 1 calc R U P B 1 C8B C -0.2012(12) -0.2038(13) -0.1208(5) 0.063(3) Uani 0.45 1 d G U P B 1 H8B H -0.2583 -0.1878 -0.1748 0.076 Uiso 0.45 1 calc R U P B 1 C9B C -0.0996(12) -0.2798(13) -0.1479(5) 0.074(3) Uani 0.45 1 d G U P B 1 H9B H -0.0873 -0.3157 -0.2204 0.089 Uiso 0.45 1 calc R U P B 1 C10B C -0.0161(12) -0.3033(14) -0.0688(7) 0.093(4) Uani 0.45 1 d G U P B 1 H10B H 0.0534 -0.3552 -0.0873 0.112 Uiso 0.45 1 calc R U P B 1 C11B C -0.0342(14) -0.2508(14) 0.0373(6) 0.079(4) Uani 0.45 1 d G U P B 1 H11B H 0.0229 -0.2668 0.0914 0.095 Uiso 0.45 1 calc R U P B 1 C6C C -0.1628(12) -0.1333(10) 0.0683(3) 0.052(3) Uani 0.55 1 d DG U P B 2 C7C C -0.2657(10) -0.1092(10) 0.0029(5) 0.060(3) Uani 0.55 1 d G U P B 2 H7C H -0.3389 -0.0676 0.0330 0.072 Uiso 0.55 1 calc R U P B 2 C8C C -0.2614(9) -0.1461(9) -0.1066(5) 0.066(3) Uani 0.55 1 d G U P B 2 H8C H -0.3317 -0.1296 -0.1513 0.079 Uiso 0.55 1 calc R U P B 2 C9C C -0.1543(9) -0.2070(9) -0.1507(3) 0.058(3) Uani 0.55 1 d G U P B 2 H9C H -0.1514 -0.2322 -0.2256 0.069 Uiso 0.55 1 calc R U P B 2 C10C C -0.0515(9) -0.2311(8) -0.0853(5) 0.066(3) Uani 0.55 1 d G U P B 2 H10C H 0.0217 -0.2728 -0.1154 0.079 Uiso 0.55 1 calc R U P B 2 C11C C -0.0557(10) -0.1943(9) 0.0242(4) 0.058(2) Uani 0.55 1 d G U P B 2 H11C H 0.0146 -0.2107 0.0689 0.069 Uiso 0.55 1 calc R U P B 2 O5 O 0.4253(7) 0.8213(7) 0.1209(5) 0.1168(19) Uani 1 1 d D U . . . H5A H 0.370(11) 0.838(8) 0.170(8) 0.175 Uiso 0.5 1 d D U P C 1 H5B H 0.353(9) 0.826(17) 0.158(6) 0.175 Uiso 0.5 1 d D U P D 2 C12A C 0.350(2) 0.7459(19) 0.0205(10) 0.112(5) Uani 0.5 1 d D U P E 1 H12A H 0.4240 0.7419 -0.0333 0.134 Uiso 0.5 1 calc R U P E 1 H12B H 0.2824 0.7965 -0.0003 0.134 Uiso 0.5 1 calc R U P E 1 C13A C 0.259(3) 0.5930(19) 0.0296(16) 0.135(7) Uani 0.5 1 d D U P E 1 H13A H 0.2030 0.5342 -0.0391 0.202 Uiso 0.5 1 calc R U P E 1 H13B H 0.3274 0.5448 0.0505 0.202 Uiso 0.5 1 calc R U P E 1 H13C H 0.1866 0.5991 0.0833 0.202 Uiso 0.5 1 calc R U P E 1 C12B C 0.3667(16) 0.6783(14) 0.0444(12) 0.094(4) Uani 0.5 1 d D U P E 2 H12C H 0.3906 0.6959 -0.0267 0.113 Uiso 0.5 1 calc R U P E 2 H12D H 0.2543 0.6419 0.0442 0.113 Uiso 0.5 1 calc R U P E 2 C13B C 0.421(2) 0.5568(19) 0.0575(17) 0.130(6) Uani 0.5 1 d D U P E 2 H13D H 0.3715 0.4676 0.0002 0.195 Uiso 0.5 1 calc R U P E 2 H13E H 0.5313 0.5882 0.0548 0.195 Uiso 0.5 1 calc R U P E 2 H13F H 0.3944 0.5339 0.1261 0.195 Uiso 0.5 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0354(4) 0.0299(4) 0.0218(4) 0.0025(3) -0.0043(3) 0.0123(3) Cl 0.0557(7) 0.0900(10) 0.0389(6) -0.0057(6) -0.0042(5) 0.0466(7) O1 0.086(3) 0.053(2) 0.057(2) 0.0113(17) 0.0102(19) 0.0419(19) O2A 0.095(7) 0.055(5) 0.040(4) 0.014(4) -0.009(5) 0.036(5) O3A 0.064(5) 0.178(9) 0.058(5) 0.031(7) 0.015(4) 0.083(6) O4A 0.074(5) 0.074(6) 0.037(5) 0.018(4) 0.011(4) 0.035(4) O2B 0.058(5) 0.135(8) 0.037(4) 0.003(5) -0.007(3) 0.028(5) O3B 0.044(3) 0.047(3) 0.091(5) 0.030(3) 0.011(3) 0.027(3) O4B 0.147(7) 0.056(4) 0.072(5) -0.015(4) -0.047(5) 0.064(4) N1A 0.064(2) 0.0261(16) 0.0272(17) 0.0031(14) -0.0042(16) 0.0183(16) C2A 0.053(2) 0.033(2) 0.0233(19) 0.0034(16) -0.0034(17) 0.0183(18) N3A 0.0440(19) 0.0262(16) 0.0237(16) 0.0001(12) -0.0078(13) 0.0130(14) C4A 0.036(2) 0.0244(18) 0.035(2) 0.0016(15) -0.0088(16) 0.0089(15) C5A 0.043(2) 0.0248(18) 0.0251(18) 0.0010(15) -0.0111(16) 0.0082(16) C6A 0.047(2) 0.0261(19) 0.030(2) 0.0001(16) -0.0111(17) 0.0001(17) C7A 0.062(3) 0.030(2) 0.043(3) 0.0051(19) -0.005(2) 0.002(2) C8A 0.074(4) 0.036(2) 0.050(3) 0.009(2) -0.002(3) -0.009(2) C9A 0.061(3) 0.061(3) 0.050(3) 0.011(3) 0.005(2) -0.010(3) C10A 0.056(3) 0.072(4) 0.062(3) 0.020(3) 0.005(3) 0.016(3) C11A 0.052(3) 0.048(3) 0.052(3) 0.019(2) 0.004(2) 0.012(2) N1B 0.061(3) 0.061(3) 0.042(2) 0.0096(19) -0.025(2) 0.018(2) C2B 0.058(3) 0.063(3) 0.036(2) -0.001(2) -0.013(2) 0.034(2) N3B 0.0427(19) 0.0309(16) 0.0262(16) 0.0052(13) -0.0046(14) 0.0126(14) C4B 0.046(2) 0.039(2) 0.025(2) 0.0081(17) -0.0022(17) -0.0064(18) C5B 0.056(3) 0.047(3) 0.030(2) 0.0150(19) -0.010(2) -0.012(2) C6B 0.059(7) 0.051(7) 0.017(5) 0.009(4) -0.011(4) -0.014(5) C7B 0.077(7) 0.069(7) 0.026(5) 0.005(5) -0.006(5) 0.005(5) C8B 0.075(7) 0.072(7) 0.022(5) 0.006(5) -0.005(5) 0.003(5) C9B 0.075(7) 0.100(8) 0.024(5) 0.002(6) -0.003(5) 0.008(6) C10B 0.101(8) 0.126(9) 0.041(6) 0.001(7) -0.001(6) 0.038(7) C11B 0.090(7) 0.103(9) 0.030(5) 0.006(6) 0.000(5) 0.023(6) C6C 0.064(6) 0.039(5) 0.031(4) 0.007(3) -0.006(4) -0.008(4) C7C 0.085(7) 0.054(5) 0.029(4) 0.007(4) -0.012(4) 0.013(4) C8C 0.089(7) 0.058(6) 0.036(5) 0.011(4) -0.019(5) 0.008(5) C9C 0.077(6) 0.057(5) 0.019(4) 0.006(4) -0.006(4) -0.001(5) C10C 0.086(6) 0.069(6) 0.022(4) 0.009(4) 0.004(4) 0.003(5) C11C 0.085(6) 0.055(5) 0.022(4) 0.017(4) -0.006(4) 0.004(5) O5 0.094(4) 0.149(4) 0.092(3) 0.021(3) -0.039(3) 0.028(3) C12A 0.104(9) 0.131(8) 0.090(7) 0.031(6) -0.019(6) 0.024(7) C13A 0.165(13) 0.112(9) 0.100(11) 0.009(7) 0.020(10) 0.022(8) C12B 0.055(6) 0.121(7) 0.078(7) 0.018(6) 0.001(5) 0.000(5) C13B 0.097(10) 0.121(9) 0.134(13) 0.015(8) -0.029(9) 0.002(7) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3B 1.987(3) 2_556 ? Cu N3B 1.987(3) . ? Cu N3A 1.997(3) 2_556 ? Cu N3A 1.997(3) . ? Cl O4A 1.311(9) . ? Cl O1 1.369(3) . ? Cl O2B 1.405(7) . ? Cl O3A 1.449(8) . ? Cl O3B 1.465(6) . ? Cl O2A 1.527(8) . ? Cl O4B 1.529(8) . ? N1A C2A 1.341(6) . ? N1A C5A 1.376(5) . ? N1A H1A 0.858(10) . ? C2A N3A 1.323(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.376(5) . ? C4A C5A 1.365(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.463(6) . ? C6A C7A 1.386(6) . ? C6A C11A 1.389(7) . ? C7A C8A 1.381(8) . ? C7A H7A 0.9500 . ? C8A C9A 1.370(9) . ? C8A H8A 0.9500 . ? C9A C10A 1.384(8) . ? C9A H9A 0.9500 . ? C10A C11A 1.384(7) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.341(6) . ? N1B C5B 1.369(7) . ? N1B H1B 0.858(10) . ? C2B N3B 1.318(6) . ? C2B H2B 0.9500 . ? N3B C4B 1.375(5) . ? C4B C5B 1.360(6) . ? C4B H4B 0.9500 . ? C5B C6C 1.434(5) . ? C5B C6B 1.551(6) . ? C6B C7B 1.3900 . ? C6B C11B 1.3900 . ? C7B C8B 1.3900 . ? C7B H7B 0.9500 . ? C8B C9B 1.3900 . ? C8B H8B 0.9500 . ? C9B C10B 1.3900 . ? C9B H9B 0.9500 . ? C10B C11B 1.3900 . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? C6C C7C 1.3900 . ? C6C C11C 1.3900 . ? C7C C8C 1.3900 . ? C7C H7C 0.9500 . ? C8C C9C 1.3900 . ? C8C H8C 0.9500 . ? C9C C10C 1.3900 . ? C9C H9C 0.9500 . ? C10C C11C 1.3900 . ? C10C H10C 0.9500 . ? C11C H11C 0.9500 . ? O5 C12A 1.396(9) . ? O5 C12B 1.449(9) . ? O5 H5A 0.841(10) . ? O5 H5B 0.841(11) . ? C12A C13A 1.487(10) . ? C12A H12A 0.9900 . ? C12A H12B 0.9900 . ? C13A H13A 0.9800 . ? C13A H13B 0.9800 . ? C13A H13C 0.9800 . ? C12B C13B 1.478(10) . ? C12B H12C 0.9900 . ? C12B H12D 0.9900 . ? C13B H13D 0.9800 . ? C13B H13E 0.9800 . ? C13B H13F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Cu N3B 180.0 2_556 . ? N3B Cu N3A 89.29(13) 2_556 2_556 ? N3B Cu N3A 90.71(13) . 2_556 ? N3B Cu N3A 90.71(13) 2_556 . ? N3B Cu N3A 89.29(13) . . ? N3A Cu N3A 180.0 2_556 . ? O4A Cl O1 128.1(4) . . ? O1 Cl O2B 113.1(4) . . ? O4A Cl O3A 83.6(6) . . ? O1 Cl O3A 122.2(5) . . ? O1 Cl O3B 98.5(3) . . ? O2B Cl O3B 119.1(5) . . ? O4A Cl O2A 109.6(5) . . ? O1 Cl O2A 103.5(4) . . ? O3A Cl O2A 108.4(6) . . ? O1 Cl O4B 97.6(4) . . ? O2B Cl O4B 101.5(5) . . ? O3B Cl O4B 125.0(4) . . ? C2A N1A C5A 108.9(3) . . ? C2A N1A H1A 124(4) . . ? C5A N1A H1A 127(4) . . ? N3A C2A N1A 110.5(4) . . ? N3A C2A H2A 124.8 . . ? N1A C2A H2A 124.8 . . ? C2A N3A C4A 105.7(3) . . ? C2A N3A Cu 125.3(3) . . ? C4A N3A Cu 128.9(2) . . ? C5A C4A N3A 110.4(3) . . ? C5A C4A H4A 124.8 . . ? N3A C4A H4A 124.8 . . ? C4A C5A N1A 104.4(4) . . ? C4A C5A C6A 131.5(4) . . ? N1A C5A C6A 124.1(3) . . ? C7A C6A C11A 118.8(4) . . ? C7A C6A C5A 122.0(4) . . ? C11A C6A C5A 119.2(4) . . ? C8A C7A C6A 120.7(5) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C9A C8A C7A 120.3(5) . . ? C9A C8A H8A 119.9 . . ? C7A C8A H8A 119.9 . . ? C8A C9A C10A 119.8(5) . . ? C8A C9A H9A 120.1 . . ? C10A C9A H9A 120.1 . . ? C9A C10A C11A 120.1(6) . . ? C9A C10A H10A 119.9 . . ? C11A C10A H10A 119.9 . . ? C10A C11A C6A 120.3(5) . . ? C10A C11A H11A 119.9 . . ? C6A C11A H11A 119.9 . . ? C2B N1B C5B 107.9(4) . . ? C2B N1B H1B 123(5) . . ? C5B N1B H1B 129(5) . . ? N3B C2B N1B 111.3(5) . . ? N3B C2B H2B 124.4 . . ? N1B C2B H2B 124.4 . . ? C2B N3B C4B 105.4(4) . . ? C2B N3B Cu 130.4(3) . . ? C4B N3B Cu 124.1(3) . . ? C5B C4B N3B 110.1(4) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 105.4(4) . . ? C4B C5B C6C 137.5(6) . . ? N1B C5B C6C 116.6(5) . . ? C4B C5B C6B 124.0(6) . . ? N1B C5B C6B 129.6(6) . . ? C7B C6B C11B 120.0 . . ? C7B C6B C5B 117.9(6) . . ? C11B C6B C5B 122.1(6) . . ? C8B C7B C6B 120.0 . . ? C8B C7B H7B 120.0 . . ? C6B C7B H7B 120.0 . . ? C7B C8B C9B 120.0 . . ? C7B C8B H8B 120.0 . . ? C9B C8B H8B 120.0 . . ? C8B C9B C10B 120.0 . . ? C8B C9B H9B 120.0 . . ? C10B C9B H9B 120.0 . . ? C9B C10B C11B 120.0 . . ? C9B C10B H10B 120.0 . . ? C11B C10B H10B 120.0 . . ? C10B C11B C6B 120.0 . . ? C10B C11B H11B 120.0 . . ? C6B C11B H11B 120.0 . . ? C7C C6C C11C 120.0 . . ? C7C C6C C5B 127.2(5) . . ? C11C C6C C5B 112.7(5) . . ? C6C C7C C8C 120.0 . . ? C6C C7C H7C 120.0 . . ? C8C C7C H7C 120.0 . . ? C9C C8C C7C 120.0 . . ? C9C C8C H8C 120.0 . . ? C7C C8C H8C 120.0 . . ? C8C C9C C10C 120.0 . . ? C8C C9C H9C 120.0 . . ? C10C C9C H9C 120.0 . . ? C11C C10C C9C 120.0 . . ? C11C C10C H10C 120.0 . . ? C9C C10C H10C 120.0 . . ? C10C C11C C6C 120.0 . . ? C10C C11C H11C 120.0 . . ? C6C C11C H11C 120.0 . . ? C12A O5 H5A 116(9) . . ? C12B O5 H5B 105(10) . . ? O5 C12A C13A 105.7(13) . . ? O5 C12A H12A 110.6 . . ? C13A C12A H12A 110.6 . . ? O5 C12A H12B 110.6 . . ? C13A C12A H12B 110.6 . . ? H12A C12A H12B 108.7 . . ? C12A C13A H13A 109.5 . . ? C12A C13A H13B 109.5 . . ? H13A C13A H13B 109.5 . . ? C12A C13A H13C 109.5 . . ? H13A C13A H13C 109.5 . . ? H13B C13A H13C 109.5 . . ? O5 C12B C13B 118.7(13) . . ? O5 C12B H12C 107.6 . . ? C13B C12B H12C 107.6 . . ? O5 C12B H12D 107.6 . . ? C13B C12B H12D 107.6 . . ? H12C C12B H12D 107.1 . . ? C12B C13B H13D 109.5 . . ? C12B C13B H13E 109.5 . . ? H13D C13B H13E 109.5 . . ? C12B C13B H13F 109.5 . . ? H13D C13B H13F 109.5 . . ? H13E C13B H13F 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N1A H1A O4A 0.858(10) 2.15(4) 2.877(10) 143(5) 1_565 N1A H1A O4B 0.858(10) 2.09(4) 2.777(8) 136(5) 1_565 C2A H2A O1 0.95 2.56 3.196(6) 124.3 2_556 C4A H4A O1 0.95 2.66 3.238(5) 119.7 . C4A H4A O3B 0.95 2.57 3.501(7) 167.9 . N1B H1B O5 0.858(10) 1.944(14) 2.801(6) 176(6) 1_445 C2B H2B O3A 0.95 2.66 3.346(12) 129.1 1_455 C2B H2B O3B 0.95 2.51 3.301(8) 141.0 1_455 C4B H4B O2A 0.95 2.33 3.132(12) 142.2 . O5 H5A O2A 0.841(10) 1.91(2) 2.719(13) 162(8) 1_565 O5 H5B O2B 0.841(11) 2.26(6) 3.018(11) 150(11) 1_565 _refine_diff_density_max 1.118 _refine_diff_density_min -1.330 _refine_diff_density_rms 0.085 # start Validation Reply Form _vrf_PLAT230_3 ; RESPONSE: The structure exhibits significant disorder affecting i) the phenyl ring of one ligand (modelled over two orientations with a 55:45 domain ratio), ii) the O2, O3 and O4 atoms of the coordinated perchlorate ion (56:44), and iii) the ethanol solvent molecule (atoms C12 and C13, 50:50), as calculated after detailed refinement. ; # end Validation Reply Form _shelx_res_file ; 03.res created by SHELXL-2014/7 TITL EL24A in P-1 CELL 0.71073 9.3377 9.7888 12.9870 103.114 90.344 109.408 ZERR 1 0.0003 0.0004 0.0006 0.005 0.005 0.004 LATT 1 SFAC C H N O CL CU UNIT 40 44 8 10 2 1 MERG 2 FMAP 2 OMIT -2 50 OMIT 1 0 1 OMIT 4 -1 1 OMIT 2 0 1 SIZE 0.17 0.12 0.10 TEMP -173 LIST 4 ACTA PLAN 10 MORE -3 BOND $H HTAB HTAB N1A O4A_$1 HTAB N1A O4B_$1 EQIV $2 -x, -y, -z+1 HTAB C2A O1_$2 HTAB C4A O1 HTAB C4A O3B EQIV $3 x-1, y-1, z HTAB N1B O5_$3 EQIV $4 x-1, y, z HTAB C2B O3A_$4 HTAB C2B O3B_$4 HTAB C4B O2A HTAB O5 O2A_$1 HTAB O5 O2B_$1 L.S. 15 WGHT 0.085100 2.618300 FVAR 3.98115 1.42096 CU 6 0.000000 0.000000 0.500000 10.50000 0.03541 0.02987 = 0.02181 0.00254 -0.00433 0.01225 DFIX 21 Cl O1 Cl O2A Cl O3A Cl O4A Cl O2B Cl O3B Cl O4B DFIX 21.633 O1 O2A O1 O3A O1 O4A O2A O3A O2A O4A O3A O4A DFIX 21.633 O1 O2B O1 O3B O1 O4B O2B O3B O2B O4B O3B O4B SIMU 0.015 0.03 3 $O ISOR 0.006 O4B CL 5 0.233826 -0.248261 0.369633 11.00000 0.05575 0.09003 = 0.03890 -0.00569 -0.00423 0.04657 O1 4 0.164189 -0.171934 0.441852 11.00000 0.08621 0.05279 = 0.05710 0.01126 0.01024 0.04191 PART 1 O2A 4 0.221375 -0.193013 0.270154 10.44000 0.09463 0.05470 = 0.04006 0.01415 -0.00861 0.03647 O3A 4 0.390188 -0.239027 0.389012 10.44000 0.06353 0.17797 = 0.05772 0.03111 0.01535 0.08280 O4A 4 0.207695 -0.392440 0.342911 10.44000 0.07372 0.07442 = 0.03689 0.01839 0.01054 0.03492 PART 2 O2B 4 0.176640 -0.272601 0.264262 10.56000 0.05765 0.13526 = 0.03716 0.00286 -0.00690 0.02847 O3B 4 0.392311 -0.152488 0.403389 10.56000 0.04430 0.04704 = 0.09144 0.02987 0.01050 0.02740 O4B 4 0.158240 -0.402331 0.391218 10.56000 0.14746 0.05620 = 0.07150 -0.01544 -0.04737 0.06370 PART 0 DFIX 0.86 0.01 N1A H1A N1A 3 0.275681 0.382952 0.422991 11.00000 0.06446 0.02605 = 0.02722 0.00310 -0.00422 0.01835 H1A 2 0.291547 0.473415 0.420000 11.00000 -1.50000 C2A 1 0.150444 0.298002 0.457978 11.00000 0.05278 0.03346 = 0.02334 0.00341 -0.00345 0.01833 AFIX 43 H2A 2 0.065241 0.327215 0.478037 11.00000 -1.20000 AFIX 0 N3A 3 0.162115 0.167780 0.460660 11.00000 0.04400 0.02620 = 0.02368 0.00007 -0.00785 0.01300 C4A 1 0.302224 0.172243 0.426051 11.00000 0.03604 0.02444 = 0.03494 0.00156 -0.00884 0.00886 AFIX 43 H4A 2 0.342570 0.093849 0.420162 11.00000 -1.20000 AFIX 0 C5A 1 0.375045 0.305225 0.401378 11.00000 0.04336 0.02480 = 0.02506 0.00103 -0.01106 0.00822 C6A 1 0.522439 0.362231 0.359386 11.00000 0.04654 0.02606 = 0.02989 0.00011 -0.01113 0.00012 C7A 1 0.562430 0.488709 0.319752 11.00000 0.06215 0.03036 = 0.04335 0.00513 -0.00537 0.00209 AFIX 43 H7A 2 0.493145 0.541191 0.320061 11.00000 -1.20000 AFIX 0 C8A 1 0.701916 0.539191 0.279832 11.00000 0.07375 0.03555 = 0.05010 0.00920 -0.00183 -0.00871 AFIX 43 H8A 2 0.727644 0.625587 0.252406 11.00000 -1.20000 AFIX 0 C9A 1 0.803414 0.465216 0.279600 11.00000 0.06056 0.06068 = 0.04985 0.01050 0.00496 -0.01011 AFIX 43 H9A 2 0.899246 0.500136 0.251979 11.00000 -1.20000 AFIX 0 C10A 1 0.765936 0.339508 0.319709 11.00000 0.05566 0.07228 = 0.06235 0.01957 0.00535 0.01596 AFIX 43 H10A 2 0.836541 0.288618 0.320197 11.00000 -1.20000 AFIX 0 C11A 1 0.625851 0.287761 0.359108 11.00000 0.05175 0.04847 = 0.05243 0.01932 0.00360 0.01212 AFIX 43 H11A 2 0.600283 0.200978 0.386073 11.00000 -1.20000 AFIX 0 DFIX 0.86 0.01 N1B H1B N1B 3 -0.287200 -0.103709 0.227498 11.00000 0.06060 0.06143 = 0.04176 0.00955 -0.02499 0.01767 H1B 2 -0.377324 -0.126497 0.198058 11.00000 -1.50000 C2B 1 -0.255591 -0.066418 0.333149 11.00000 0.05766 0.06348 = 0.03619 -0.00083 -0.01263 0.03418 AFIX 43 H2B 2 -0.327411 -0.055695 0.383087 11.00000 -1.20000 AFIX 0 N3B 3 -0.112040 -0.046572 0.358747 11.00000 0.04268 0.03093 = 0.02617 0.00523 -0.00462 0.01256 C4B 1 -0.049727 -0.073069 0.263744 11.00000 0.04595 0.03880 = 0.02483 0.00807 -0.00221 -0.00638 AFIX 43 H4B 2 0.053428 -0.066353 0.256600 11.00000 -1.20000 AFIX 0 C5B 1 -0.157289 -0.110276 0.181548 11.00000 0.05614 0.04675 = 0.03040 0.01495 -0.01012 -0.01157 DELU 0.02 C6B > C11C SIMU 0.02 C6B > C11C DFIX 0.3 0.02 C6C C6B DFIX 1.49 0.01 C5B C6B C5B C6C PART 1 AFIX 66 C6B 1 -0.135800 -0.174750 0.064399 10.45000 0.05916 0.05075 = 0.01659 0.00875 -0.01094 -0.01426 C7B 1 -0.219328 -0.151271 -0.014665 10.45000 0.07713 0.06890 = 0.02590 0.00456 -0.00575 0.00549 AFIX 43 H7B 2 -0.288779 -0.099324 0.003843 10.45000 -1.20000 AFIX 65 C8B 1 -0.201237 -0.203799 -0.120811 10.45000 0.07499 0.07226 = 0.02220 0.00598 -0.00535 0.00315 AFIX 43 H8B 2 -0.258324 -0.187752 -0.174847 10.45000 -1.20000 AFIX 65 C9B 1 -0.099619 -0.279806 -0.147892 10.45000 0.07546 0.10002 = 0.02355 0.00206 -0.00269 0.00829 AFIX 43 H9B 2 -0.087255 -0.315706 -0.220438 10.45000 -1.20000 AFIX 65 C10B 1 -0.016090 -0.303286 -0.068829 10.45000 0.10091 0.12595 = 0.04149 0.00060 -0.00118 0.03840 AFIX 43 H10B 2 0.053361 -0.355233 -0.087339 10.45000 -1.20000 AFIX 65 C11B 1 -0.034180 -0.250759 0.037316 10.45000 0.09048 0.10299 = 0.03024 0.00646 0.00034 0.02250 AFIX 43 H11B 2 0.022908 -0.266806 0.091353 10.45000 -1.20000 AFIX 66 PART 2 C6C 1 -0.162781 -0.133347 0.068320 10.55000 0.06411 0.03943 = 0.03121 0.00733 -0.00615 -0.00775 C7C 1 -0.265652 -0.109250 0.002892 10.55000 0.08497 0.05437 = 0.02923 0.00679 -0.01181 0.01276 AFIX 43 H7C 2 -0.338850 -0.067607 0.033029 10.55000 -1.20000 AFIX 65 C8C 1 -0.261423 -0.146082 -0.106630 10.55000 0.08886 0.05812 = 0.03640 0.01077 -0.01946 0.00791 AFIX 43 H8C 2 -0.331731 -0.129612 -0.151346 10.55000 -1.20000 AFIX 65 C9C 1 -0.154324 -0.207011 -0.150725 10.55000 0.07724 0.05727 = 0.01891 0.00591 -0.00575 -0.00080 AFIX 43 H9C 2 -0.151434 -0.232184 -0.225578 10.55000 -1.20000 AFIX 65 C10C 1 -0.051452 -0.231109 -0.085298 10.55000 0.08607 0.06898 = 0.02248 0.00919 0.00448 0.00251 AFIX 43 H10C 2 0.021745 -0.272752 -0.115436 10.55000 -1.20000 AFIX 65 C11C 1 -0.055679 -0.194277 0.024224 10.55000 0.08457 0.05483 = 0.02205 0.01732 -0.00557 0.00429 AFIX 43 H11C 2 0.014629 -0.210747 0.068940 10.55000 -1.20000 AFIX 0 PART 0 RIGU O5 > C13B ISOR 0.01 O5 > C13B EQIV $1 X, 1+Y, Z DFIX 0.84 0.01 O5 H5A O5 H5B DFIX 1.90 0.02 H5A O2A_$1 H5B O2A_$1 DFIX 0.2 H5A H5B O5 4 0.425293 0.821288 0.120943 11.00000 0.09409 0.14934 = 0.09199 0.02110 -0.03947 0.02837 PART 1 H5A 2 0.369884 0.837762 0.169655 10.50000 -1.50000 PART 2 H5B 2 0.352959 0.825593 0.158377 10.50000 -1.50000 PART 0 DFIX 1.41 0.01 O5 C12A DFIX 1.39 0.01 O5 C12B DFIX 1.49 0.01 C12A C13A C12B C13B PART 1 C12A 1 0.349835 0.745885 0.020492 10.50000 0.10436 0.13116 = 0.09017 0.03118 -0.01852 0.02439 AFIX 23 H12A 2 0.424002 0.741888 -0.033272 10.50000 -1.20000 H12B 2 0.282412 0.796489 -0.000253 10.50000 -1.20000 AFIX 0 C13A 1 0.258947 0.592955 0.029569 10.50000 0.16462 0.11204 = 0.09971 0.00933 0.01986 0.02222 AFIX 33 H13A 2 0.202965 0.534197 -0.039058 10.50000 -1.50000 H13B 2 0.327394 0.544803 0.050456 10.50000 -1.50000 H13C 2 0.186598 0.599098 0.083290 10.50000 -1.50000 AFIX 0 PART 2 C12B 1 0.366743 0.678339 0.044357 10.50000 0.05541 0.12128 = 0.07845 0.01759 0.00065 -0.00042 AFIX 23 H12C 2 0.390583 0.695879 -0.026720 10.50000 -1.20000 H12D 2 0.254320 0.641870 0.044223 10.50000 -1.20000 AFIX 0 C13B 1 0.420503 0.556751 0.057460 10.50000 0.09701 0.12121 = 0.13440 0.01468 -0.02930 0.00166 AFIX 33 H13D 2 0.371452 0.467555 0.000215 10.50000 -1.50000 H13E 2 0.531322 0.588190 0.054774 10.50000 -1.50000 H13F 2 0.394371 0.533907 0.126075 10.50000 -1.50000 AFIX 0 HKLF 4 REM EL24A in P-1 REM R1 = 0.0661 for 3397 Fo > 4sig(Fo) and 0.0725 for all 3812 data REM 365 parameters refined using 423 restraints END WGHT 0.0854 2.8816 REM Instructions for potential hydrogen bonds HTAB N1A O4A_$1 HTAB N1A O4B_$1 HTAB C2A O1_$2 HTAB C4A O3B HTAB N1B O5_$3 HTAB C2B O3B_$4 HTAB C4B O2A HTAB C4B O2B HTAB O5 O2A_$1 HTAB O5 O2B_$1 REM Highest difference peak 1.118, deepest hole -1.330, 1-sigma level 0.085 Q1 1 0.3601 -0.3031 0.3817 11.00000 0.05 1.12 Q2 1 0.1008 -0.4203 0.3993 11.00000 0.05 1.02 Q3 1 0.4047 0.9105 0.0694 11.00000 0.05 0.94 Q4 1 0.2101 -0.3401 0.3654 11.00000 0.05 0.80 Q5 1 -0.5036 -0.0639 -0.1331 11.00000 0.05 0.65 Q6 1 0.3625 0.6196 0.0420 11.00000 0.05 0.54 Q7 1 -0.0550 -0.0003 0.4269 11.00000 0.05 0.47 Q8 1 0.4497 0.8945 0.1435 11.00000 0.05 0.45 Q9 1 0.1677 -0.3616 0.4656 11.00000 0.05 0.44 Q10 1 -0.2033 -0.1875 -0.0130 11.00000 0.05 0.39 ; _shelx_res_checksum 77919 _shelx_hkl_file ; 0 0 2 27696.3 465.969 1 0 0 -2 26842.3 448.061 7 0 0 -2 27793.2 433.745 2 0 0 3 54507.8 875.605 1 0 0 -3 51962.3 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86.3255 1 0 1 -14 656.678 118.773 7 0 -1 14 394.230 111.079 1 0 1 -13 171.020 60.7059 7 0 1 -13 109.797 47.8047 2 0 -1 13 103.504 72.8412 1 0 1 -12 330.972 65.2929 2 0 1 -12 244.254 70.7340 7 0 -1 12 349.478 93.3862 1 0 -1 11 1488.40 158.714 1 0 1 -11 1740.50 127.354 2 0 1 -11 1589.63 142.455 7 0 1 -10 5347.97 247.428 7 0 -1 10 4947.47 267.980 1 0 1 -10 5453.39 221.108 2 0 -1 9 6890.52 300.873 1 0 1 -9 6984.57 270.820 7 0 1 -9 6866.20 243.097 2 0 1 -8 2624.56 138.468 2 0 -1 8 2762.32 173.971 1 0 1 -8 2820.72 156.754 7 0 1 -7 2066.01 114.697 2 0 -1 7 2007.68 139.986 1 0 1 -7 2045.23 123.737 7 0 -1 6 5996.57 210.784 8 0 1 -6 6239.54 209.206 7 0 -1 6 6362.75 207.014 2 0 1 -6 6137.63 195.851 2 0 -1 5 1763.43 101.281 8 0 1 -5 1727.52 92.5203 2 0 1 -5 1863.09 99.8495 7 0 -1 5 1957.15 99.4563 2 0 1 -4 187.347 32.6042 2 0 -1 4 153.096 32.9454 8 0 1 -4 193.773 33.9042 7 0 -1 3 40011.3 649.305 8 0 1 -3 38420.0 650.886 2 0 1 -3 38661.6 644.004 7 0 1 -2 20948.1 380.939 2 0 -1 2 22434.3 379.959 5 0 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28.1232 2 0 1 11 42.7419 54.6627 1 0 1 12 5314.77 319.306 1 0 -1 -12 5726.89 288.299 7 0 -1 -13 2866.71 214.252 7 0 1 13 3294.52 260.362 1 0 1 14 1171.55 169.967 1 0 1 15 1341.19 194.318 1 0 -2 16 287.609 111.007 1 0 2 -16 196.631 88.1035 5 0 -2 15 81.9837 82.5932 1 0 -2 14 1933.51 214.638 1 0 2 -14 1869.88 158.942 2 0 2 -14 1918.95 182.367 7 0 2 -13 3551.05 211.495 2 0 2 -13 3561.63 234.320 7 0 -2 13 3408.99 262.602 1 0 2 -12 6058.60 269.345 2 0 -2 12 5706.06 320.748 1 0 2 -12 5694.74 282.824 7 0 -2 11 1521.86 161.335 1 0 2 -11 1776.13 150.389 7 0 2 -11 1818.78 140.659 2 0 2 -10 6732.33 264.432 2 0 -2 10 6948.68 318.492 1 0 2 -10 6733.35 280.635 7 0 2 -9 871.623 93.1620 2 0 2 -9 1027.49 104.877 7 0 -2 9 816.678 99.2163 8 0 -2 8 427.074 70.2951 8 0 2 -8 375.414 62.9210 7 0 2 -8 527.127 69.7642 2 0 2 -7 2722.08 143.342 2 0 -2 7 3142.19 158.879 8 0 2 -7 2732.29 146.394 7 0 2 -6 5965.99 212.438 2 0 -2 6 6148.29 213.486 8 0 2 -6 6029.87 207.189 7 0 2 -5 30236.3 592.762 2 0 2 -5 31014.3 581.224 7 0 -2 5 30635.0 586.698 8 0 -2 4 73325.1 1161.93 7 0 -2 4 74585.1 1173.95 8 0 2 -4 72068.5 1186.23 2 0 2 -4 71250.9 1158.52 7 0 -2 3 5037.26 139.638 7 0 2 -3 5023.09 140.536 7 0 -2 3 5247.93 154.083 8 0 -2 3 5598.21 160.343 5 0 2 -3 5005.30 161.006 2 0 -2 2 182.768 21.2647 7 0 -2 2 202.664 28.2832 5 0 2 -2 216.389 32.6972 2 0 -2 2 223.673 25.5078 4 0 2 -2 170.355 21.8819 7 0 -2 2 180.424 29.1376 8 0 2 -1 104274. 1510.94 1 0 2 -1 101240. 1513.80 2 0 -2 1 104126. 1510.87 8 0 2 -1 101245. 1449.20 7 0 -2 1 96361.0 1446.13 7 0 2 0 40936.0 656.087 2 0 2 0 41911.9 680.741 1 0 -2 0 41037.6 673.287 8 0 -2 0 40493.2 660.105 2 0 2 1 38295.4 642.113 1 0 -2 -1 38536.8 631.215 8 0 2 1 37241.9 580.611 2 0 -2 -1 36416.2 554.247 7 0 2 1 35860.4 552.656 7 0 2 2 39965.6 626.328 2 0 2 2 41373.4 725.757 1 0 2 2 41143.1 640.729 7 0 -2 -2 40240.8 653.744 6 0 -2 -2 40911.5 640.509 7 0 2 3 1971.76 79.5797 6 0 2 3 1577.72 50.1768 2 0 2 3 1825.91 112.567 1 0 -2 -3 1956.99 81.4249 7 0 2 3 1989.36 81.3904 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237.547 1 0 3 -14 2913.75 224.191 7 0 3 -13 3674.80 225.567 2 0 -3 13 3511.49 265.671 1 0 3 -13 3536.56 238.340 5 0 3 -13 3408.05 230.585 7 0 3 -12 4135.23 231.055 2 0 3 -12 4091.18 242.479 5 0 3 -12 3796.29 235.474 7 0 -3 12 4054.35 271.813 1 0 -3 12 3638.83 237.656 8 0 3 -11 274.404 71.9403 5 0 3 -11 388.470 78.6078 2 0 -3 11 375.757 85.4216 8 0 3 -11 433.008 81.7833 7 0 3 -10 659.604 90.7258 7 0 3 -10 640.636 90.7562 5 0 3 -10 654.424 90.5410 2 0 -3 10 597.208 95.1011 8 0 3 -9 3387.51 188.187 2 0 -3 9 3814.99 201.251 8 0 3 -9 3353.45 191.500 5 0 3 -9 3410.00 187.837 7 0 3 -8 18877.1 488.972 2 0 -3 8 20129.0 497.469 8 0 3 -8 19912.8 487.581 7 0 -3 7 43190.4 829.269 8 0 3 -7 41920.9 840.112 2 0 3 -7 44106.0 827.011 7 0 3 -6 22194.2 516.426 2 0 -3 6 23502.1 508.037 8 0 3 -6 23616.2 498.241 7 0 3 -5 2033.81 106.452 7 0 3 -5 1792.72 116.876 2 0 -3 5 2057.98 114.117 8 0 -3 5 2027.33 103.803 7 0 -3 4 49.8181 29.6883 8 0 -3 4 21.4849 19.1696 4 0 3 -4 44.5219 25.8724 7 0 -3 4 72.7186 22.0792 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11664.4 356.909 8 0 -4 -6 5949.03 209.386 7 0 4 6 5931.54 282.175 1 0 4 7 4887.39 267.546 1 0 -4 -7 5149.02 206.041 7 0 4 8 5814.07 308.044 1 0 4 9 4864.46 294.680 1 0 4 10 1135.41 155.843 1 0 4 11 685.608 129.887 1 0 4 12 203.261 95.8045 1 0 4 13 100.589 90.1442 1 0 5 -17 837.302 142.227 2 0 -5 16 1033.16 175.382 1 0 5 -16 785.678 132.264 2 0 -5 15 2118.84 213.788 8 0 5 -15 2249.80 214.159 5 0 -5 15 1918.92 223.157 1 0 5 -15 1708.63 184.773 2 0 5 -14 2062.56 196.004 5 0 -5 14 2079.09 203.565 8 0 5 -14 2300.93 203.956 2 0 5 -13 1630.75 164.303 7 0 5 -13 1603.04 168.412 5 0 -5 13 1678.05 173.332 8 0 5 -13 1850.79 179.272 2 0 5 -12 51.7151 58.6078 7 0 5 -12-28.5836 61.7161 5 0 5 -12 38.3057 56.9341 2 0 -5 12-37.8296 64.7825 8 0 5 -11 3040.04 213.429 2 0 5 -11 2973.06 207.510 5 0 -5 11 2549.42 192.707 8 0 5 -11 3144.61 207.279 7 0 5 -10 1382.74 139.091 5 0 5 -10 1703.93 153.908 2 0 -5 10 1753.78 150.220 8 0 5 -10 1560.06 139.063 7 0 5 -9 8429.99 331.077 5 0 5 -9 8530.81 315.615 7 0 -5 9 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242.222 18.8485 7 0 5 2 359.933 47.7772 2 0 5 2 342.966 71.6718 1 0 5 3 1929.00 75.4469 7 0 5 3 2250.18 101.515 2 0 -5 -3 2374.31 153.221 8 0 5 3 2166.55 158.201 1 0 5 4 1447.58 76.5687 7 0 5 4 1295.00 130.077 1 0 5 4 1419.64 72.1227 2 0 -5 -4 1384.88 123.189 8 0 5 5 5668.89 279.940 1 0 -5 -5 6209.51 267.970 8 0 5 5 6026.82 188.863 7 0 5 5 5062.53 124.336 2 0 5 5 5317.29 131.579 2 0 -5 -6 4179.95 229.295 8 0 5 6 4398.04 252.824 1 0 -5 -7 1692.77 152.883 8 0 5 7 1976.19 177.348 1 0 -5 -8 373.517 84.4352 8 0 5 8 427.721 102.763 1 0 -5 -9 254.082 86.7796 8 0 5 9 136.327 77.1083 1 0 5 10 99.8444 79.8264 1 0 -5 -10-27.3238 57.9705 8 0 -5 -11 736.755 127.497 8 0 5 11 722.635 141.741 1 0 5 12 2684.22 264.227 1 0 -5 -12 2960.90 245.787 8 0 6 -16 135.549 78.7066 2 0 -6 16 45.4817 72.7275 8 0 6 -15 109.494 81.3228 5 0 -6 15 87.5835 67.1630 8 0 6 -15 27.3717 62.9307 2 0 -6 14 23.6840 68.4770 8 0 6 -14 166.696 79.1897 2 0 6 -14 127.698 71.6940 5 0 -6 13 192.376 78.0083 8 0 6 -13 262.786 88.3814 2 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260.334 1 0 -6 0 6023.25 246.865 8 0 6 1 5322.29 203.745 2 0 -6 -1 6085.32 253.438 8 0 6 1 5695.48 254.497 1 0 6 2 3082.00 191.341 1 0 6 2 2689.59 133.263 2 0 -6 -2 3050.07 183.833 8 0 -6 -3 6042.94 264.259 8 0 6 3 5960.47 276.202 1 0 6 3 5948.58 185.880 2 0 -6 -4 10215.6 368.534 8 0 6 4 9900.47 244.521 2 0 6 4 9640.78 379.216 1 0 -6 -5 7726.85 325.119 8 0 6 5 7958.52 351.218 1 0 -6 -6 1289.45 137.669 8 0 6 6 1121.19 138.666 1 0 -6 -7 66.5490 57.0926 8 0 6 7 29.8408 64.0288 1 0 -6 -8 480.966 97.3948 8 0 6 8 508.221 113.216 1 0 -6 -9 153.181 73.7099 8 0 6 9 292.486 100.774 1 0 6 10 623.372 137.144 1 0 -6 -10 518.618 115.586 8 0 -6 -11 674.992 127.644 8 0 6 11 738.090 150.167 1 0 -7 15 639.454 132.934 8 0 7 -15 491.033 115.021 2 0 7 -14 375.266 101.964 2 0 -7 14 379.566 102.562 8 0 -7 13-32.0496 64.4602 8 0 7 -13-62.5175 87.2456 2 0 -7 12-56.3617 69.1534 8 0 7 -12 53.6870 64.7857 2 0 -7 11 191.645 73.9619 8 0 7 -11 194.572 82.2624 2 0 7 -10 1438.86 158.110 2 0 -7 10 1935.83 172.221 8 0 7 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117.903 1 0 -8 2 1137.38 126.050 8 0 8 -2 1159.24 112.822 4 0 8 -1 369.954 85.3239 1 0 8 -1 427.157 74.5233 2 0 -8 1 393.659 87.2102 8 0 8 -1 386.594 71.8079 4 0 -8 0 643.850 98.4367 8 0 8 0 692.274 86.3566 2 0 8 0 453.237 89.5182 1 0 -8 -1 611.921 101.077 8 0 8 1 763.892 90.2867 2 0 8 1 536.302 96.3371 1 0 8 2 341.981 91.3477 1 0 -8 -2 343.574 82.7540 8 0 8 2 424.212 66.2387 2 0 -8 -3 260.911 80.9617 8 0 8 3 224.402 85.5545 1 0 8 4 1406.77 166.978 1 0 -8 -4 1472.67 156.926 8 0 -8 -5 2072.28 187.810 8 0 8 5 2067.74 201.071 1 0 8 6 2929.31 242.656 1 0 -8 -6 3033.11 232.824 8 0 -8 -7 2867.34 236.636 8 0 8 7 2840.09 248.279 1 0 -8 -8 833.954 140.911 8 0 8 8 517.067 122.499 1 0 -9 13-23.0156 77.9607 8 0 9 -13-68.5087 71.3786 2 0 9 -12 666.435 137.432 2 0 -9 12 782.611 136.480 8 0 -9 11 646.099 124.096 8 0 9 -11 627.913 122.072 2 0 9 -10 2710.15 231.604 2 0 -9 10 2820.16 230.157 8 0 -9 9 2459.73 213.926 8 0 9 -9 2047.76 200.237 2 0 9 -8 1726.99 183.257 2 0 -9 8 1989.63 189.013 8 0 -9 7 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73.6324 1 0 -10 -4 43.7082 76.0770 8 0 11 -9 93.8572 73.3786 2 0 -11 9 219.634 89.3028 8 0 -11 8 262.173 96.2107 8 0 11 -8 306.323 96.9394 2 0 -11 7-3.91687 66.8351 8 0 11 -7-128.426 78.5004 2 0 -11 6-4.84247 62.5705 8 0 11 -6 9.52435 65.2406 2 0 11 -5 303.960 89.4992 2 0 -11 5 256.202 92.5653 8 0 11 -4 1782.52 191.539 2 0 -11 4 1861.62 195.332 8 0 -11 3 600.394 122.186 8 0 11 -3 378.293 99.7072 2 0 -11 2 132.019 79.3819 8 0 11 -2-61.9051 57.1251 2 0 11 -2 94.3877 73.2091 1 0 11 -1 43.4992 62.4612 4 0 11 -1-0.32341 61.7338 1 0 -11 1 152.505 74.4579 8 0 11 0 424.985 94.4625 4 0 11 0 476.577 108.654 1 0 -11 0 248.472 94.8121 8 0 -11 -1 484.122 115.807 8 0 11 1 607.962 126.573 1 0 11 1 477.091 108.488 4 0 12 -6 823.300 148.405 2 0 12 -5 1111.63 164.363 2 0 12 -4 1308.64 167.454 2 -1 12 2 390.853 115.139 4 -1 12 1 483.441 120.504 4 -1 12 0 520.194 118.533 4 -1 12 -1 445.391 105.136 4 1 -12 3 219.779 85.1066 8 -1 12 -4 253.989 80.6545 2 1 -12 4 425.038 108.437 8 -1 12 -5 176.375 91.6029 2 1 -12 5 146.375 76.7827 8 -1 12 -6 381.061 103.783 2 1 -12 6 541.255 123.135 8 -1 12 -7 1159.32 167.634 2 -1 11 2 721.204 135.430 1 1 -11 -2 796.159 135.675 8 1 -11 -1 761.729 135.986 8 -1 11 1 854.722 141.544 1 -1 11 1 862.038 135.440 4 1 -11 0 397.381 106.395 8 -1 11 0 600.514 121.477 1 -1 11 0 399.246 96.6975 4 1 -11 1 269.402 93.8556 8 -1 11 -1 211.113 81.0196 1 -1 11 -1 190.505 73.1037 4 -1 11 -2 882.847 130.087 4 1 -11 2 884.343 137.369 8 -1 11 -2 1082.06 147.870 1 -1 11 -2 846.230 118.696 2 -1 11 -3 2389.92 202.297 2 -1 11 -3 2281.17 209.446 1 1 -11 3 2800.77 231.028 8 -1 11 -3 2459.16 207.248 4 1 -11 4 1773.18 187.202 8 -1 11 -4 1316.96 148.173 4 -1 11 -4 1431.02 162.921 2 1 -11 5 179.772 83.9704 8 -1 11 -5 271.435 86.5898 2 -1 11 -5 123.585 51.0715 4 -1 11 -6 235.634 83.0200 2 1 -11 6 194.683 85.4442 8 -1 11 -7 35.5027 56.8239 2 1 -11 7 258.018 84.9292 8 -1 11 -8 14.0391 66.8230 2 1 -11 8 106.110 75.3600 8 1 -11 9 78.4246 77.8846 8 -1 11 -9 42.7964 68.9883 2 1 -11 10 416.897 109.665 8 -1 11 -10 129.413 75.8422 2 1 -11 11 440.661 121.404 8 1 -10 -5 615.061 122.914 8 -1 10 5 562.373 125.792 1 -1 10 4 696.432 139.357 1 1 -10 -4 873.038 137.217 8 1 -10 -3 1085.27 150.082 8 -1 10 3 669.609 133.023 1 1 -10 -2 317.687 98.6740 8 -1 10 2 74.0021 73.9583 1 1 -10 -1-28.5268 72.8540 8 -1 10 1-47.4457 75.8568 1 -1 10 0-63.8602 74.0063 1 -1 10 0 63.9587 63.0674 4 1 -10 0 13.9982 55.7639 8 1 -10 1 10.2905 64.3602 8 -1 10 -1 9.18656 44.3016 4 -1 10 -1 37.7257 58.1548 1 -1 10 -1-49.1591 48.1733 2 -1 10 -2 733.912 113.853 4 -1 10 -2 932.675 133.945 1 -1 10 -2 912.188 117.622 2 1 -10 2 969.982 131.321 8 -1 10 -3 1630.45 164.488 1 -1 10 -3 1663.48 160.849 2 1 -10 3 2120.32 186.147 8 -1 10 -3 1661.66 160.613 4 1 -10 4 1155.34 143.130 8 -1 10 -4 1033.65 134.705 2 -1 10 -4 1010.42 126.834 4 -1 10 -5 755.241 109.854 4 -1 10 -5 837.332 124.027 2 -1 10 -6 1873.30 184.520 2 1 -10 6 1879.54 183.582 8 1 -10 7 513.490 102.941 8 -1 10 -7 628.676 120.016 2 1 -10 8 267.517 79.1335 8 -1 10 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4 -1 9 -3 195.952 63.7569 2 -1 9 -4 403.559 87.1720 2 1 -9 4 498.791 95.6380 8 -1 9 -4 536.356 86.7087 4 1 -9 5 364.412 85.1356 8 -1 9 -5 237.743 65.3179 4 -1 9 -5 218.367 68.9397 2 1 -9 6 11.0675 52.9187 8 -1 9 -6 74.0544 64.0779 2 1 -9 7 1201.68 147.189 8 -1 9 -7 1041.54 134.237 2 1 -9 8 3882.90 249.467 8 -1 9 -8 3222.55 238.501 2 1 -9 9 4149.65 264.413 8 -1 9 -9 4388.69 280.436 2 -1 9 -10 3517.96 263.069 2 1 -9 10 4269.52 273.475 8 1 -9 11 745.099 123.397 8 -1 9 -11 897.422 144.418 2 -1 9 -12 1427.89 179.070 2 1 -9 12 1354.76 166.726 8 1 -9 13-6.08847 68.3028 8 -1 9 -13 83.3790 76.9538 2 1 -9 14 135.241 72.0732 8 -1 8 9 457.506 127.526 1 1 -8 -9 400.114 106.424 8 1 -8 -8 187.986 78.2164 8 -1 8 8 223.218 94.1020 1 1 -8 -7 2185.01 205.278 8 -1 8 7 2090.30 211.094 1 1 -8 -6 2372.82 205.626 8 -1 8 6 2353.07 216.204 1 1 -8 -5 4515.64 272.267 8 -1 8 5 4608.93 290.556 1 -1 8 4 2930.93 226.944 1 1 -8 -4 2829.11 211.326 8 -1 8 3 1312.46 151.598 1 1 -8 -3 1445.75 150.034 8 -1 8 2 1304.80 147.879 1 1 -8 -2 1480.17 148.278 8 -1 8 2 1268.06 95.7148 2 -1 8 1 605.433 74.3123 2 1 -8 -1 684.206 101.888 8 -1 8 1 642.460 108.257 1 -1 8 0 326.649 64.4782 2 1 -8 0 519.227 89.6745 8 -1 8 0 440.023 89.9988 1 1 -8 1 3257.31 203.567 8 -1 8 -1 3111.46 179.036 2 -1 8 -1 3023.47 196.929 1 -1 8 -1 3061.18 192.820 4 -1 8 -2 8523.75 332.223 1 -1 8 -2 8435.05 324.323 4 1 -8 2 9292.51 342.226 8 -1 8 -2 8919.97 328.928 2 -1 8 -3 3703.95 206.646 4 -1 8 -3 3701.13 213.052 1 1 -8 3 3779.72 213.483 8 -1 8 -3 3827.23 215.830 2 -1 8 -4 367.423 78.4187 2 1 -8 4 390.657 75.1710 8 -1 8 -4 369.040 70.8921 4 1 -8 5 41.6655 48.7760 8 -1 8 -5 89.5360 63.1261 2 -1 8 -5 84.9118 44.3621 4 -1 8 -6 68.9781 56.0976 2 1 -8 6 47.0301 52.0386 8 1 -8 7 308.584 77.6546 8 -1 8 -7 328.956 81.0323 2 -1 8 -8 502.758 94.2398 2 1 -8 8 608.470 100.512 8 -1 8 -9 2058.22 184.577 2 1 -8 9 1752.20 163.748 8 1 -8 10 1622.55 161.379 8 -1 8 -10 1428.71 165.710 2 1 -8 11 296.887 81.0977 8 -1 8 -11 361.648 103.828 2 -1 8 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71.2971 2 -1 6 11 1986.00 222.511 1 1 -6 -11 1441.30 177.482 8 1 -6 -10 1004.09 147.186 8 -1 6 10 1127.89 164.408 1 1 -6 -9 43.6052 58.9734 8 -1 6 9 35.1903 75.7435 1 -1 6 8 70.9688 68.8345 1 1 -6 -8 156.599 45.2837 7 1 -6 -8 165.413 68.2709 8 1 -6 -7 41.2466 33.7247 7 1 -6 -7 0.70111 55.9507 8 -1 6 7 126.774 70.6940 1 -1 6 6 23.9886 64.7668 1 1 -6 -6 4.49292 47.1157 8 1 -6 -6 2.15880 29.0022 7 1 -6 -5 58.9709 51.1820 8 -1 6 5 82.4687 61.2071 1 1 -6 -5 60.1269 26.2016 7 -1 6 4 19.9102 12.4198 2 1 -6 -4 24.9519 19.6514 7 -1 6 4 1.58270 18.3554 7 -1 6 4 56.9940 50.2705 1 1 -6 -4 1.99225 40.6415 8 1 -6 -3 3801.44 113.518 7 1 -6 -3 4431.50 219.139 8 -1 6 3 3757.39 127.474 2 -1 6 3 3953.38 219.147 1 -1 6 3 3537.17 113.911 7 1 -6 -2 6695.66 263.405 8 -1 6 2 6279.82 266.554 1 -1 6 2 6068.28 183.817 2 1 -6 -2 6198.08 196.995 2 1 -6 -2 5115.80 117.866 7 1 -6 -1 2673.30 133.066 2 -1 6 1 2682.75 167.957 1 -1 6 1 2496.15 122.639 2 1 -6 -1 2272.66 148.687 8 -1 6 0 117.178 39.3920 2 -1 6 0 70.9019 50.1324 1 1 -6 0 112.758 46.2073 8 1 -6 1 10740.0 323.202 8 1 -6 1 9388.98 218.957 3 -1 6 -1 9769.03 316.510 1 -1 6 -1 9941.53 295.921 2 -1 6 -2 15759.8 408.592 1 -1 6 -2 15864.8 402.612 2 1 -6 2 14440.7 270.610 3 1 -6 2 16535.8 412.024 8 1 -6 2 14705.8 265.758 7 1 -6 3 7882.12 269.564 8 1 -6 3 7512.71 179.609 7 -1 6 -3 7128.77 263.440 2 -1 6 -3 7408.55 265.271 1 -1 6 -4 18969.8 491.980 2 1 -6 4 19279.5 390.162 7 1 -6 4 20679.5 492.474 8 1 -6 5 22002.4 528.328 8 -1 6 -5 20669.6 534.914 2 1 -6 6 12509.2 376.946 8 -1 6 -6 12544.5 397.099 2 -1 6 -7 3922.10 106.955 3 -1 6 -7 4903.27 238.573 2 1 -6 7 4767.19 221.448 8 1 -6 8 2242.70 157.624 8 -1 6 -8 2037.90 89.8184 3 -1 6 -8 1938.96 160.063 2 -1 6 -9 2337.41 182.583 2 1 -6 9 2470.56 172.855 8 -1 6 -10-33.7713 56.9201 2 1 -6 10-17.3172 55.3022 8 1 -6 11 1800.80 162.968 8 -1 6 -11 2050.36 177.113 5 -1 6 -11 2034.23 182.297 2 -1 6 -12 52.6014 56.8597 5 -1 6 -12 119.765 77.6735 2 1 -6 12 50.8673 57.7304 8 1 -6 13 951.160 137.581 8 -1 6 -13 1506.21 166.670 2 -1 6 -13 1173.06 149.078 5 -1 6 -14 1946.34 197.717 2 -1 6 -14 2040.65 200.751 5 1 -6 14 2078.30 203.440 8 1 -6 15 1260.00 169.772 8 -1 6 -15 1653.54 183.990 2 -1 6 -15 2033.84 206.279 5 -1 6 -16 376.534 101.935 2 1 -6 16 221.933 102.098 1 -1 6 -17 27.7622 64.6142 2 -1 5 12 3402.67 291.068 1 -1 5 11 4686.85 328.481 1 1 -5 -11 5093.81 264.896 7 -1 5 10 2597.14 236.300 1 1 -5 -10 3056.77 191.486 7 -1 5 9 12.5364 68.7153 1 1 -5 -9 3.34647 45.9562 7 1 -5 -8 253.410 58.3092 7 -1 5 8 225.287 82.1162 1 1 -5 -7 873.338 86.0007 7 -1 5 7 780.384 119.034 1 1 -5 -6 4918.39 188.112 7 1 -5 -6 4768.73 239.762 8 -1 5 6 5023.52 267.054 1 1 -5 -5 7274.69 215.993 7 1 -5 -5 7106.72 284.699 8 -1 5 5 6853.18 211.780 7 -1 5 5 7003.22 304.859 1 -1 5 4 1631.20 50.9864 2 1 -5 -4 2111.70 96.2294 7 -1 5 4 2268.13 163.516 1 -1 5 4 2081.45 95.6280 7 1 -5 -4 2268.76 150.633 8 -1 5 3 1044.00 109.706 1 -1 5 3 1015.87 54.1359 2 -1 5 3 977.474 58.5207 7 1 -5 -3 961.241 99.8969 8 1 -5 -3 935.302 56.0200 7 1 -5 -2 170.912 20.9191 7 1 -5 -2 197.588 51.0769 8 -1 5 2 148.429 52.6011 1 -1 5 2 125.061 20.2334 7 -1 5 2 161.969 30.2343 2 1 -5 -2 180.004 30.7382 2 1 -5 -1 1986.98 100.708 2 -1 5 1 2142.69 101.410 2 1 -5 -1 1826.51 54.3696 7 1 -5 -1 2081.06 128.337 8 -1 5 1 2094.34 135.310 1 -1 5 0 3125.83 133.570 2 1 -5 0 3187.49 138.737 2 -1 5 0 3118.31 158.565 1 1 -5 0 3432.28 160.008 8 -1 5 -1 52415.8 905.389 4 1 -5 1 46241.0 739.276 7 -1 5 -1 52740.1 877.074 2 -1 5 -1 52663.5 904.938 1 1 -5 1 46005.5 742.188 7 1 -5 1 52788.4 890.097 2 1 -5 1 51138.1 779.637 3 1 -5 1 52653.6 900.083 8 1 -5 2 13027.0 246.715 7 1 -5 2 13407.0 337.694 8 -1 5 -2 12898.5 336.481 1 -1 5 -2 13436.8 345.519 4 1 -5 2 11799.4 226.278 3 -1 5 -2 13260.7 339.642 2 -1 5 -3 80.0492 35.1498 4 1 -5 3 128.535 24.1625 7 1 -5 3 121.825 40.8895 8 -1 5 -3 120.052 42.8022 2 1 -5 4 6837.96 233.389 8 -1 5 -4 6554.28 244.017 2 1 -5 4 6432.90 189.517 7 -1 5 -5 6823.72 140.878 3 -1 5 -5 8324.91 281.226 2 1 -5 5 8597.09 264.858 8 -1 5 -6 14318.9 280.886 3 1 -5 6 14743.7 389.472 8 -1 5 -6 14617.9 416.197 2 -1 5 -7 2652.73 170.220 2 1 -5 7 2775.81 157.842 8 -1 5 -8 938.405 108.725 2 1 -5 8 1030.90 101.568 8 -1 5 -8 1020.15 107.491 5 -1 5 -9 1510.17 136.222 5 -1 5 -9 1547.99 140.938 2 1 -5 9 1399.22 124.996 8 1 -5 10 694.247 98.8684 8 -1 5 -10 502.764 87.8865 2 -1 5 -10 603.304 93.9265 5 1 -5 11 5124.83 267.180 8 -1 5 -11 5195.76 272.745 5 -1 5 -11 5679.48 287.689 2 -1 5 -12 519.722 99.4289 5 1 -5 12 650.010 108.018 8 -1 5 -12 714.635 110.386 2 -1 5 -13 785.371 120.384 2 1 -5 13 640.914 113.144 8 -1 5 -13 1017.02 136.260 5 -1 5 -14 1038.68 145.008 5 1 -5 14 1204.22 157.653 8 -1 5 -14 868.823 129.513 2 -1 5 -15 372.422 104.358 5 -1 5 -15 277.598 87.6395 2 1 -5 15 254.626 110.290 1 1 -5 16 152.325 106.937 1 -1 5 -16 92.9008 73.7125 5 -1 5 -16-5.93917 57.0233 2 -1 5 -17 1276.36 166.201 2 1 -4 -13 1864.92 180.133 7 -1 4 13 2111.44 232.330 1 -1 4 12 752.400 146.856 1 1 -4 -12 798.663 116.965 7 -1 4 11 70.6355 71.2889 1 -1 4 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23.9070 15.7708 2 -1 4 1 49.3638 14.2263 7 1 -4 -1 66.8924 12.9517 7 1 -4 0 29062.0 474.828 7 1 -4 0 32384.0 591.671 8 -1 4 0 31977.4 600.572 1 -1 4 0 31698.3 556.057 2 1 -4 0 31672.2 564.798 2 1 -4 1 55237.8 867.171 3 -1 4 -1 55955.0 956.032 1 -1 4 -1 55361.8 944.450 2 1 -4 1 58243.0 958.354 2 1 -4 1 56657.4 950.429 8 1 -4 1 57661.2 970.578 1 1 -4 2 1443.42 86.7257 8 1 -4 2 1264.74 84.2522 1 1 -4 2 1131.63 43.9460 3 -1 4 -2 1191.25 85.2340 4 -1 4 -2 1376.53 86.2442 1 -1 4 -2 1249.81 85.6606 2 1 -4 2 1215.25 86.3052 2 1 -4 2 1389.55 62.5969 7 1 -4 3 37.2679 18.5265 7 1 -4 3 44.4773 28.4187 8 1 -4 3 28.6385 20.4031 4 -1 4 -3 39.9495 31.5887 2 -1 4 -3 74.3808 32.2901 4 -1 4 -3 38.0363 9.81264 3 1 -4 3 45.5782 25.9514 1 -1 4 -4 235.549 22.6953 3 1 -4 4 216.542 35.9672 7 -1 4 -4 247.218 50.9128 2 1 -4 4 236.028 44.1863 8 1 -4 4 259.975 43.9620 4 -1 4 -5 7151.82 249.918 2 1 -4 5 7405.22 233.685 8 1 -4 6 2084.02 122.535 8 -1 4 -6 1682.86 124.349 2 -1 4 -7 127.368 48.5328 2 1 -4 7 171.912 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0 95.6276 58.3211 2 -1 -8 0 55.8526 52.2908 8 1 8 0-13.3323 64.0124 1 1 8 1 59.3681 57.7105 1 1 8 1 11.5571 45.1179 2 -1 -8 -1 55.9746 55.6516 8 -1 -8 -2 1399.23 150.122 8 1 8 2 1497.08 126.602 2 1 8 2 1462.38 162.330 1 1 8 3 1367.76 161.793 1 -1 -8 -3 1750.05 169.757 8 -1 -8 -4 227.423 80.5087 8 1 8 4 35.8736 66.2416 1 1 8 5 126.389 74.4461 1 -1 -8 -5 78.0812 65.6509 8 -1 -8 -6 164.790 76.9073 8 1 8 6 126.725 79.6645 1 -1 -8 -7 493.616 119.200 8 1 8 7 490.450 122.600 1 -1 -8 -8 1113.94 160.078 8 1 8 8 1369.37 184.645 1 1 9 -12 467.963 122.307 2 -1 -9 12 524.962 122.281 8 -1 -9 11 821.093 139.058 8 1 9 -11 841.908 140.868 2 -1 -9 10 307.454 98.6701 8 1 9 -10 631.589 123.996 2 -1 -9 9 14.7436 56.0697 8 1 9 -9 207.348 84.9344 2 1 9 -8 867.341 136.332 2 -1 -9 8 837.909 134.002 8 1 9 -7 2698.12 226.099 2 -1 -9 7 2144.07 198.972 8 1 9 -6 4162.54 278.035 2 -1 -9 6 4543.62 276.704 8 1 9 -5 1666.79 175.616 2 -1 -9 5 1243.17 146.391 8 1 9 -4 1547.00 128.203 4 -1 -9 4 1788.93 175.353 8 1 9 -4 2165.73 192.707 2 1 9 -3 1960.17 183.041 2 -1 -9 3 1743.21 170.525 8 1 9 -3 1728.53 143.231 4 1 9 -3 1716.99 172.272 1 -1 -9 2 1237.05 149.517 8 1 9 -2 1209.08 123.581 4 1 9 -2 1090.80 139.089 1 1 9 -2 1484.90 157.492 2 1 9 -1 2146.38 192.754 1 1 9 -1 2512.60 195.928 2 1 9 -1 2328.26 173.934 4 -1 -9 1 2396.99 202.996 8 1 9 0 1808.82 159.224 2 1 9 0 1553.31 173.536 1 -1 -9 0 1653.26 171.695 8 -1 -9 -1 745.088 123.806 8 1 9 1 746.510 102.521 2 1 9 1 610.783 120.624 1 -1 -9 -2 186.476 73.8971 8 1 9 2 113.097 68.9058 1 -1 -9 -3 105.930 66.4925 8 1 9 3 140.879 80.5956 1 1 9 4 203.071 89.1130 1 -1 -9 -4 253.575 90.8949 8 1 9 5-36.0595 73.7579 1 -1 -9 -5 101.762 76.3245 8 1 9 6-6.70698 85.2354 1 -1 -9 -6 220.194 86.8448 8 -1 -10 10 9.96188 68.5105 8 1 10 -10 43.1217 62.7764 2 1 10 -9 158.735 85.5721 2 -1 -10 9 221.907 88.4202 8 1 10 -8 429.306 109.126 2 -1 -10 8 666.015 123.978 8 -1 -10 7 366.515 97.1998 8 1 10 -7 340.374 93.9748 2 -1 -10 6 43.6092 72.7853 8 1 10 -6-1.30743 68.2765 2 -1 -10 5 191.841 77.4992 8 1 10 -5 408.742 101.790 2 -1 -10 4 1714.51 181.670 8 1 10 -4 1721.54 184.648 2 1 10 -3 639.640 115.637 2 -1 -10 3 589.736 118.753 8 -1 -10 2 150.170 81.9359 8 1 10 -2 344.627 90.7848 2 1 10 -2 192.288 83.3612 1 -1 -10 1 309.282 94.0518 8 1 10 -1 354.404 88.4072 2 1 10 -1 318.716 94.3675 1 1 10 0 1606.95 161.601 4 -1 -10 0 1292.64 166.876 8 1 10 0 1267.31 167.976 1 -1 -10 -1 2857.57 239.020 8 1 10 1 2683.53 238.168 1 -1 -10 -2 2702.65 233.870 8 1 10 2 2559.12 236.256 1 -1 -10 -3 706.157 133.080 8 1 10 3 773.194 143.031 1 1 11 -8 93.2603 76.5504 2 -1 -11 7 121.173 73.1806 8 1 11 -7 58.1448 66.1622 2 1 11 -6 36.7055 55.2040 2 -1 -11 6-60.6738 72.6471 8 -1 -11 5 33.7362 62.9970 8 1 11 -5 337.011 99.9609 2 1 11 -4 468.444 113.051 2 -1 -11 4 482.853 117.162 8 -1 -11 3 250.600 85.9610 8 1 11 -3 408.426 99.1705 2 -1 -11 2 483.206 122.566 8 1 11 -2 579.288 132.672 1 1 12 -5-73.5599 65.6106 2 1 12 -4 541.199 124.069 2 -2 12 2 102.708 71.0342 4 -2 12 1 1.47575 62.5755 4 -2 12 0 487.073 113.661 4 2 -12 0 391.286 101.115 8 -2 12 -1 747.798 134.341 4 2 -12 1 602.609 121.804 8 -2 12 -1 808.054 146.994 1 2 -12 2 646.843 131.096 8 -2 12 -2 689.945 125.141 1 -2 12 -2 516.692 116.181 4 -2 12 -3 786.418 139.238 4 2 -12 3 722.090 135.260 8 2 -12 4 78.8612 64.5723 8 -2 12 -4 161.167 81.2670 4 -2 12 -5-15.4834 58.3506 2 -2 12 -5-20.7319 49.7229 4 2 -12 5-109.196 80.9091 8 2 -12 6 18.5047 61.4145 8 -2 12 -6-79.3266 70.1957 2 -2 12 -7 466.941 112.673 2 2 -12 7 593.080 120.527 8 -2 12 -8 861.627 141.902 2 2 -12 8 1029.95 157.303 8 2 -12 9 1191.11 172.648 8 2 -11 -3 16.5464 65.3069 8 -2 11 3-11.6931 83.4357 1 2 -11 -2 184.974 80.3056 8 -2 11 2 149.704 77.1536 1 -2 11 2 211.701 83.1432 4 2 -11 -1 391.348 102.593 8 -2 11 1 515.010 114.057 4 -2 11 1 350.688 97.7587 1 -2 11 0 502.426 107.084 4 2 -11 0 472.464 110.413 8 -2 11 0 413.233 103.462 1 -2 11 -1 365.282 94.4550 1 -2 11 -1 446.956 103.201 4 2 -11 1 384.777 96.8839 8 -2 11 -2 1137.87 152.076 4 2 -11 2 1197.04 151.683 8 -2 11 -2 1353.18 164.615 1 -2 11 -2 1177.10 134.855 2 -2 11 -3 1249.84 156.905 4 2 -11 3 1110.64 146.510 8 -2 11 -3 1382.62 161.105 1 -2 11 -3 1054.24 135.142 2 -2 11 -4 156.866 67.6820 2 2 -11 4 212.375 83.3827 8 -2 11 -4 93.9283 60.7223 4 2 -11 5 398.732 95.4403 8 -2 11 -5 304.741 85.0884 2 -2 11 -5 292.825 80.8448 4 2 -11 6 1655.52 180.019 8 -2 11 -6 1244.18 158.739 2 2 -11 7 2192.73 204.556 8 -2 11 -7 2031.97 204.662 2 2 -11 8 570.113 117.477 8 -2 11 -8 935.637 143.838 2 2 -11 9 510.353 115.199 8 -2 11 -9 392.815 105.420 2 -2 11 -10 30.1964 64.6136 2 2 -11 10 248.952 89.5879 8 2 -11 11 35.0192 61.9445 8 2 -11 12-36.7105 73.5766 8 -2 10 6 261.459 94.5110 1 2 -10 -6 335.850 98.0120 8 2 -10 -5 2560.06 227.007 8 -2 10 5 2669.22 243.150 1 -2 10 4 1876.76 204.820 1 2 -10 -4 1839.32 194.411 8 2 -10 -3 1406.24 168.921 8 -2 10 3 1253.88 166.397 1 -2 10 2 364.821 100.727 1 2 -10 -2 586.856 114.135 8 -2 10 1 546.223 109.516 4 2 -10 -1 378.588 92.7135 8 -2 10 1 310.151 92.5372 1 -2 10 0 674.883 115.767 4 -2 10 0 570.110 107.126 1 2 -10 0 567.808 104.501 8 -2 10 -1 1297.47 150.569 4 -2 10 -1 1046.12 134.380 1 2 -10 1 1162.83 139.807 8 -2 10 -1 1043.23 115.756 2 -2 10 -2 999.203 129.864 4 -2 10 -2 1023.57 118.284 2 2 -10 2 901.133 124.841 8 -2 10 -2 1066.92 136.575 1 2 -10 3 313.860 84.5972 8 -2 10 -3 280.706 79.9131 1 -2 10 -3 282.456 77.0257 2 -2 10 -3 223.875 72.5898 4 2 -10 4 11.0513 51.3314 8 -2 10 -4-16.9505 49.0273 2 -2 10 -4 20.4906 46.5082 4 -2 10 -5 214.580 75.1399 4 2 -10 5 142.070 66.2765 8 -2 10 -5 213.458 80.2260 2 -2 10 -6 712.434 120.487 2 2 -10 6 790.943 119.153 8 -2 10 -7 617.381 111.401 2 2 -10 7 553.403 104.144 8 -2 10 -8 820.532 131.995 2 2 -10 8 913.576 130.053 8 -2 10 -9 1336.57 166.081 2 2 -10 9 1205.67 153.938 8 -2 10 -10 374.153 102.072 2 2 -10 10 612.349 115.187 8 -2 10 -11 508.514 114.751 2 2 -10 11 540.071 119.182 8 -2 10 -12 906.182 147.163 2 2 -10 12 685.763 121.231 8 2 -10 13 131.627 77.8166 8 -2 9 7 1267.06 177.818 1 2 -9 -7 1133.19 160.531 8 -2 9 6 74.5073 78.9016 1 2 -9 -6 79.1203 75.6685 8 2 -9 -5 10.4644 54.1791 8 -2 9 5 182.234 94.5363 1 2 -9 -4 138.698 65.3862 8 -2 9 4 278.087 91.6259 1 2 -9 -3 2112.04 185.633 8 -2 9 3 2005.83 190.990 1 2 -9 -2 6936.96 331.406 8 -2 9 2 7016.22 345.767 1 -2 9 1 5516.80 222.573 2 2 -9 -1 5922.96 299.690 8 -2 9 1 5998.43 310.305 1 -2 9 0 2549.13 197.581 4 -2 9 0 2475.41 154.765 2 2 -9 0 2532.31 191.000 8 -2 9 0 2584.78 198.466 1 -2 9 -1 2740.32 201.673 4 -2 9 -1 2616.88 193.136 1 -2 9 -1 2661.18 169.432 2 2 -9 1 2808.47 199.465 8 -2 9 -2 2704.43 198.657 4 -2 9 -2 2639.03 188.481 1 -2 9 -2 2778.26 181.175 2 2 -9 2 3047.04 200.807 8 2 -9 3 585.387 96.3442 8 -2 9 -3 390.009 82.5289 4 -2 9 -3 456.644 91.3296 1 -2 9 -3 403.006 80.6467 2 -2 9 -4 197.658 66.5950 4 -2 9 -4 88.7449 53.8556 2 2 -9 4 154.814 60.1237 8 -2 9 -5 173.746 59.6395 4 2 -9 5 196.666 67.6630 8 -2 9 -5 94.0523 58.4802 2 2 -9 6 113.075 57.9087 8 -2 9 -6-63.5402 53.2038 2 2 -9 7-3.85323 51.4814 8 -2 9 -7 35.6053 50.9700 2 2 -9 8 173.472 69.8048 8 -2 9 -8 39.4042 55.1102 2 -2 9 -9 81.5433 72.1904 2 2 -9 9 85.8996 64.7140 8 2 -9 10 197.799 73.6259 8 -2 9 -10 104.368 71.2767 2 -2 9 -11 1394.43 171.565 2 2 -9 11 1565.96 165.725 8 2 -9 12 2409.15 209.818 8 -2 9 -12 2675.06 236.486 2 2 -9 13 1049.94 147.072 8 -2 9 -13 1043.96 157.820 2 2 -9 14 1043.99 152.359 8 2 -8 -9 129.297 88.5715 8 -2 8 9 208.345 104.655 1 2 -8 -8 130.038 70.1561 8 -2 8 8 294.733 110.028 1 -2 8 7 2432.54 227.412 1 2 -8 -7 2435.83 209.131 8 2 -8 -6 4863.41 287.271 8 -2 8 6 5073.55 309.785 1 2 -8 -5 7612.84 349.491 8 -2 8 5 7057.01 355.498 1 2 -8 -4 4877.92 270.499 8 -2 8 4 5005.99 288.248 1 2 -8 -3 1051.56 129.126 8 -2 8 3 1255.40 146.844 1 -2 8 2-0.09965 35.8265 2 2 -8 -2 86.8469 49.5647 8 -2 8 2 50.8033 52.7770 1 2 -8 -1 777.192 106.284 8 -2 8 1 714.022 108.000 1 -2 8 1 715.282 77.7531 2 -2 8 0 1407.28 139.993 4 2 -8 0 1481.80 138.034 8 -2 8 0 1257.82 105.411 2 -2 8 0 1510.16 144.575 1 -2 8 -1 8748.04 345.178 4 2 -8 1 8742.58 329.740 8 -2 8 -1 8668.60 300.981 2 -2 8 -1 8764.05 334.328 1 2 -8 2 4035.61 111.651 7 -2 8 -2 4564.93 229.403 1 -2 8 -2 4777.42 224.143 2 2 -8 2 5127.85 240.392 8 -2 8 -2 4634.52 241.012 4 2 -8 3 2271.83 159.610 8 -2 8 -3 2352.08 172.511 4 2 -8 3 2124.06 92.0630 7 -2 8 -3 2392.67 161.610 2 -2 8 -3 1885.72 148.551 1 -2 8 -4 2486.13 176.076 4 2 -8 4 2704.09 176.909 8 -2 8 -4 2206.50 162.932 2 -2 8 -5 3020.98 197.289 4 2 -8 5 3556.95 205.181 8 -2 8 -5 3453.11 210.041 2 2 -8 6 707.384 98.1780 8 -2 8 -6 724.058 103.435 2 2 -8 7 173.012 61.5860 8 -2 8 -7 209.752 68.6730 2 2 -8 8 1130.06 127.161 8 -2 8 -8 1235.59 140.110 2 2 -8 9 710.387 108.226 8 -2 8 -9 684.789 116.338 2 2 -8 10 1.57970 47.2508 8 -2 8 -10 53.4500 66.4801 2 -2 8 -11 387.130 92.1791 2 2 -8 11 548.500 99.8721 8 -2 8 -12 12.4265 57.0015 2 2 -8 12 80.9991 63.6934 8 -2 8 -13 108.585 76.6282 2 2 -8 13 42.8775 63.0664 8 2 -8 14 459.655 112.336 8 -2 8 -14 329.206 99.7652 2 2 -8 15 368.067 100.232 8 2 -7 -10 208.740 90.2539 8 -2 7 10-17.2894 93.7796 1 -2 7 9 856.229 149.841 1 2 -7 -9 1045.26 146.833 8 -2 7 8 227.146 91.1330 1 2 -7 -8 59.1850 65.7284 8 -2 7 7 2505.51 218.225 1 2 -7 -7 2487.99 201.188 8 2 -7 -6 7264.84 335.569 8 -2 7 6 7246.04 356.070 1 -2 7 5 2270.04 189.378 1 2 -7 -5 2345.88 181.127 8 2 -7 -5 2112.29 110.578 7 -2 7 4 351.789 79.8824 1 2 -7 -4 396.697 44.1519 7 2 -7 -4 406.264 81.8982 8 2 -7 -3 255.828 70.3116 8 -2 7 3 220.530 34.2682 2 -2 7 3 228.558 75.0252 1 2 -7 -3 141.561 26.4251 7 -2 7 2 118.990 33.0536 2 2 -7 -2 131.102 21.0658 7 2 -7 -2 130.961 61.5119 8 2 -7 -2 165.921 35.3497 2 -2 7 2 97.5673 60.5288 1 2 -7 -1 724.389 92.4023 8 -2 7 1 771.359 98.2505 1 -2 7 1 626.627 64.8693 2 2 -7 -1 618.991 36.3064 7 2 -7 0 2875.34 84.2633 7 -2 7 0 3182.57 184.182 1 -2 7 0 3043.35 152.594 2 2 -7 0 3220.04 180.219 8 -2 7 -1 13300.9 406.086 4 2 -7 1 13247.3 295.888 3 2 -7 1 12480.5 246.002 7 -2 7 -1 13621.7 367.050 2 2 -7 1 11648.9 239.111 7 -2 7 -1 13592.6 393.022 1 2 -7 1 13588.5 389.802 8 2 -7 2 9290.03 310.548 8 -2 7 -2 9473.65 329.974 4 2 -7 2 9238.74 207.313 7 2 -7 2 8591.40 210.726 3 2 -7 2 8693.87 210.026 7 -2 7 -2 9407.48 307.884 2 -2 7 -2 8704.20 303.769 1 -2 7 -3 3347.19 191.048 4 2 -7 3 3188.67 116.579 7 2 -7 3 3228.69 173.723 8 -2 7 -3 3182.57 174.966 1 -2 7 -3 3267.57 177.670 2 -2 7 -4 748.264 96.5495 4 -2 7 -4 699.635 90.4228 2 2 -7 4 716.808 90.0573 8 2 -7 4 675.006 59.5633 7 2 -7 5 1453.92 121.832 8 -2 7 -5 1302.98 121.914 2 2 -7 6 2115.91 147.443 8 -2 7 -6 1768.45 148.488 2 -2 7 -7 8144.22 330.112 2 -2 7 -7 7205.93 160.819 3 2 -7 7 8111.60 302.301 8 -2 7 -8 10591.7 235.836 3 2 -7 8 11371.7 377.856 8 -2 7 -8 10797.5 400.256 2 -2 7 -9 6064.01 300.174 2 2 -7 9 5470.62 261.806 8 -2 7 -10 1692.92 167.745 2 2 -7 10 1838.62 155.941 8 2 -7 11 3614.15 227.050 8 -2 7 -11 3759.11 252.754 2 -2 7 -12-20.5157 74.9927 2 2 -7 12 68.9881 60.8940 8 -2 7 -13 0.87210 61.5452 5 2 -7 13-38.2212 61.8703 8 -2 7 -13 11.7207 62.2611 2 2 -7 14 123.614 71.2992 8 -2 7 -14 130.875 74.5782 5 -2 7 -15 450.546 109.739 2 2 -7 15 380.246 105.254 8 -2 7 -15 494.910 117.288 5 2 -7 16 530.194 117.223 8 2 -7 16 189.664 92.7175 1 -2 6 11 616.265 139.853 1 2 -6 -10 1445.96 166.254 8 -2 6 10 1640.30 195.911 1 -2 6 9 2781.64 237.518 1 2 -6 -9 2888.46 179.907 7 2 -6 -9 2898.15 223.984 8 2 -6 -8 7701.42 353.018 8 -2 6 8 7785.02 385.067 1 2 -6 -8 8423.88 296.748 7 -2 6 7 2573.41 212.991 1 2 -6 -7 2612.06 148.483 7 2 -6 -7 2860.78 203.429 8 2 -6 -6 785.302 77.4386 7 -2 6 6 835.681 125.494 1 2 -6 -6 860.183 112.756 8 2 -6 -5 895.834 74.6028 7 2 -6 -5 773.914 101.869 8 -2 6 5 875.557 119.739 1 -2 6 4 1280.94 131.853 1 2 -6 -4 1376.70 123.681 8 -2 6 4 1153.26 77.6306 7 2 -6 -4 1315.66 80.3349 7 2 -6 -3 27.6790 40.1617 8 -2 6 3 3.95533 15.4388 2 -2 6 3 15.9054 19.0047 7 -2 6 3 70.6445 53.0333 1 2 -6 -3 38.1581 22.2596 7 2 -6 -3 12.1499 16.4562 2 -2 6 2 706.985 56.7933 2 -2 6 2 766.867 96.2727 1 2 -6 -2 733.406 90.0006 8 2 -6 -2 641.500 57.0369 2 2 -6 -2 731.216 50.3248 7 -2 6 1 3968.60 153.633 2 2 -6 -1 4121.60 118.983 7 2 -6 -1 3964.16 158.009 2 -2 6 1 4149.10 202.069 1 2 -6 -1 4143.44 194.676 8 2 -6 0 8330.53 231.731 3 -2 6 0 8850.19 295.708 1 -2 6 0 8924.58 259.623 2 2 -6 0 8552.33 190.063 7 2 -6 0 8786.27 288.204 8 -2 6 -1 2562.88 136.215 2 2 -6 1 2419.90 92.8189 7 -2 6 -1 2676.14 148.814 1 -2 6 -1 2814.12 163.121 4 2 -6 1 2446.77 103.905 3 2 -6 1 2492.93 141.014 8 -2 6 -2 134.731 43.6422 2 2 -6 2 152.062 24.5545 3 2 -6 2 183.180 43.4624 8 -2 6 -2 173.637 46.3011 1 -2 6 -3 1186.65 98.5764 1 2 -6 3 1254.12 100.258 8 2 -6 3 1100.71 55.4384 3 2 -6 3 1202.05 74.3651 7 -2 6 -3 1223.98 105.125 2 -2 6 -4 2861.77 166.395 2 -2 6 -4 2998.85 172.215 4 -2 6 -4 2749.65 87.9549 3 2 -6 4 3006.56 129.739 7 2 -6 4 2995.81 156.245 8 2 -6 5 7815.61 263.467 8 -2 6 -5 7076.70 276.835 2 -2 6 -5 6960.36 161.309 3 -2 6 -6 19871.6 525.930 2 2 -6 6 20706.2 491.560 8 -2 6 -6 19348.4 361.839 3 -2 6 -7 26606.0 486.080 3 -2 6 -7 24704.4 632.483 2 2 -6 7 26398.8 600.747 8 -2 6 -8 16437.0 359.651 3 -2 6 -8 16026.3 485.545 2 2 -6 8 15226.2 435.322 8 -2 6 -9 2779.11 134.504 3 2 -6 9 3039.33 184.331 8 -2 6 -9 2801.41 197.058 2 -2 6 -10 1683.44 154.412 5 -2 6 -10 1781.07 115.508 3 -2 6 -10 1770.83 161.982 2 2 -6 10 1655.73 144.483 8 -2 6 -11 1739.23 168.676 2 2 -6 11 1709.39 155.931 8 -2 6 -11 1830.66 165.745 5 -2 6 -12 284.595 82.4176 2 -2 6 -12 75.9665 63.4844 5 2 -6 12 196.660 78.3628 8 -2 6 -13 1024.61 140.053 5 -2 6 -13 838.280 130.081 2 2 -6 13 963.680 132.573 8 2 -6 14 1791.85 184.282 8 -2 6 -14 1805.76 190.333 5 -2 6 -14 1769.89 186.046 2 -2 6 -15 623.197 122.303 2 -2 6 -15 747.255 138.888 5 2 -6 15 445.868 127.376 1 -2 6 -16 59.3516 64.4166 2 2 -6 16-87.3754 96.9996 1 2 -5 -13 109.711 66.1312 7 2 -5 -12 773.588 112.701 7 -2 5 12 510.497 128.495 1 -2 5 11 1013.35 162.042 1 -2 5 11 827.189 109.721 6 2 -5 -11 886.015 116.644 7 -2 5 10 623.898 93.2046 6 2 -5 -10 561.651 92.5913 7 -2 5 10 429.016 112.797 1 2 -5 -9 953.621 103.911 7 -2 5 9 1578.45 177.127 1 -2 5 9 988.774 110.593 6 -2 5 8 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128.890 79.7462 5 2 5 -13 171.119 74.9698 7 2 5 -13 138.846 73.2573 2 -2 -5 13 88.3109 65.2853 8 2 5 -12 247.269 82.9308 5 2 5 -12 137.010 61.0676 2 2 5 -12 173.951 69.8956 7 -2 -5 12 167.461 73.2038 8 2 5 -11 126.125 74.4435 2 2 5 -11 148.169 68.7844 7 -2 -5 11 49.1515 56.0503 8 2 5 -10 2920.59 188.971 7 -2 -5 10 3186.97 213.995 8 2 5 -10 3451.46 231.102 2 2 5 -9 6978.91 280.860 7 -2 -5 9 7079.26 311.420 8 2 5 -9 7109.56 326.463 2 -2 -5 8 4279.10 230.741 8 2 5 -8 4269.23 204.366 7 2 5 -8 4461.74 249.407 2 2 5 -7 6193.94 236.551 7 -2 -5 7 7121.19 202.745 4 2 5 -7 5670.13 163.254 3 2 5 -7 6889.53 304.758 2 -2 -5 7 6695.46 283.735 8 -2 -5 6 3094.31 182.440 8 2 5 -6 3026.76 148.920 7 2 5 -6 2554.31 91.8738 3 2 5 -6 3162.12 197.895 2 2 5 -5 6366.88 209.112 7 -2 -5 5 6554.83 269.298 8 2 5 -5 7194.85 296.625 2 -2 -5 4 4055.62 112.131 3 2 5 -4 4403.22 154.123 7 -2 -5 4 4710.03 162.076 7 -2 -5 4 4774.49 218.846 8 2 5 -4 4432.35 224.666 2 2 5 -3 67.1825 25.2849 4 -2 -5 3 98.5233 21.4233 3 2 5 -3 59.4055 47.7597 2 2 5 -3 95.9159 28.2072 7 -2 -5 3 120.119 51.1147 8 -2 -5 3 85.7834 24.7720 7 2 5 -2 232.519 36.7508 4 2 5 -2 295.989 69.1265 2 -2 -5 2 253.777 59.3304 8 2 5 -2 294.447 33.1603 7 -2 -5 2 300.067 35.9779 3 2 5 -2 232.624 57.4127 1 -2 -5 2 216.348 29.8482 7 -2 -5 1 1591.58 87.5160 3 2 5 -1 1391.57 57.4763 7 2 5 -1 1478.63 120.009 1 -2 -5 1 1616.51 124.013 8 2 5 -1 1330.79 115.429 2 2 5 0 2283.28 146.261 2 -2 -5 0 2421.70 152.194 8 -2 -5 0 2225.12 118.998 3 2 5 0 2066.66 66.9160 7 2 5 0 2395.83 159.271 1 2 5 1 2268.84 75.7009 7 2 5 1 2350.75 74.5769 7 2 5 1 2619.86 167.279 1 -2 -5 -1 2533.15 159.651 8 2 5 1 2722.08 155.615 2 2 5 2 6159.85 150.687 7 -2 -5 -2 6611.88 266.758 8 2 5 2 6098.80 157.144 7 2 5 2 6291.51 271.267 1 2 5 2 6189.07 240.408 2 2 5 3 11292.0 250.462 7 -2 -5 -3 11754.1 268.503 6 2 5 3 11588.7 341.070 2 -2 -5 -3 11455.3 374.541 8 2 5 3 11051.3 391.962 1 -2 -5 -4 10447.7 367.014 8 2 5 4 10468.6 389.769 1 2 5 4 10685.6 321.630 2 -2 -5 -5 1073.31 118.057 8 2 5 5 924.863 119.602 1 2 5 5 893.150 86.2990 2 -2 -5 -6 1761.41 153.166 8 2 5 6 1752.83 116.573 2 2 5 6 1746.69 170.188 1 2 5 7 1973.16 187.219 1 -2 -5 -7 1873.39 163.503 8 2 5 8 758.050 127.363 1 -2 -5 -8 687.670 111.769 8 2 5 9 1330.20 172.991 1 -2 -5 -9 1065.16 136.675 8 2 5 10 2571.58 245.155 1 -2 -5 -10 2250.79 205.542 8 -2 -5 -11 584.060 120.099 8 2 5 11 573.126 143.235 1 2 6 -16 1027.43 159.068 2 2 6 -15 1563.09 189.200 2 2 6 -15 1907.98 196.066 7 -2 -6 14 488.738 114.862 8 2 6 -14 402.664 105.828 2 2 6 -14 686.412 119.395 7 2 6 -13 361.456 101.614 2 -2 -6 13 409.858 104.281 8 2 6 -13 286.421 84.3620 7 -2 -6 12 1316.38 157.545 8 2 6 -12 1650.99 160.177 7 2 6 -12 1725.91 184.224 2 -2 -6 11 491.910 99.0425 8 2 6 -11 492.444 92.0525 7 2 6 -11 380.676 100.924 2 2 6 -10-61.4632 60.9576 2 2 6 -10-7.42416 44.3431 7 -2 -6 10 12.4010 47.0320 8 2 6 -9 112.722 64.2617 2 -2 -6 9 16.8205 46.2515 8 2 6 -9 43.7942 46.7015 7 2 6 -8 59.0602 55.0529 2 2 6 -8 67.9980 39.9801 7 -2 -6 8 155.078 65.0062 8 2 6 -7 2491.41 145.707 7 2 6 -7 2345.77 185.909 2 -2 -6 7 1894.51 158.935 8 -2 -6 6 3598.31 213.380 8 2 6 -6 3749.20 168.003 7 2 6 -6 3521.54 224.808 2 2 6 -5 333.465 78.5926 2 2 6 -5 272.970 45.1693 7 -2 -6 5 214.537 56.9619 8 2 6 -4 317.266 77.1525 2 2 6 -4 267.043 41.5926 4 -2 -6 4 381.627 74.4117 8 2 6 -4 396.341 44.7571 7 -2 -6 4 310.399 41.4208 7 2 6 -3 1918.59 105.711 4 2 6 -3 1938.46 84.6171 7 -2 -6 3 2058.60 151.593 8 -2 -6 3 1858.34 74.9642 3 2 6 -3 2024.48 159.992 2 -2 -6 3 1821.26 86.4292 7 2 6 -2 1319.94 92.8671 4 -2 -6 2 1498.46 77.1057 3 -2 -6 2 1298.02 124.730 8 2 6 -2 1132.33 52.5952 7 2 6 -2 1361.26 126.934 1 2 6 -2 1331.53 129.939 2 -2 -6 1 5264.36 178.597 3 2 6 -1 5197.06 245.092 1 2 6 -1 5272.15 247.943 2 -2 -6 1 5337.47 247.575 8 -2 -6 0 3869.65 213.130 8 -2 -6 0 3856.53 164.519 3 2 6 0 3624.03 211.596 1 2 6 0 3681.72 202.889 2 -2 -6 -1 2791.80 185.123 8 2 6 1 2997.27 194.983 1 2 6 1 3270.02 184.816 2 -2 -6 -2 5030.00 249.739 8 2 6 2 4340.93 247.238 1 2 6 2 4994.47 225.585 2 -2 -6 -3 242.888 67.8493 8 2 6 3 291.044 61.0534 2 2 6 3 165.409 72.1052 1 2 6 4 123.094 47.6296 2 -2 -6 -4 59.8095 54.0628 8 2 6 4 16.3952 56.8876 1 -2 -6 -5 0.67193 48.8501 8 2 6 5 80.4524 69.3681 1 -2 -6 -6 6955.11 330.144 8 2 6 6 6962.99 355.356 1 2 6 7 9087.31 422.178 1 -2 -6 -7 8690.96 382.577 8 -2 -6 -8 3178.86 234.499 8 2 6 8 3459.73 266.551 1 -2 -6 -9 1876.50 192.835 8 2 6 9 1876.59 212.531 1 2 6 10 1276.23 187.994 1 -2 -6 -10 1018.24 150.174 8 2 7 -15 408.895 103.623 7 2 7 -14 105.059 84.9763 2 -2 -7 14 137.172 85.5977 8 2 7 -14 150.622 73.6175 7 2 7 -13 1039.29 139.277 7 2 7 -13 1173.35 166.811 2 -2 -7 13 1346.10 168.562 8 -2 -7 12 2289.81 210.463 8 2 7 -12 2149.80 183.879 7 2 7 -12 2615.67 234.824 2 2 7 -11 1574.07 153.865 7 -2 -7 11 1829.61 183.530 8 2 7 -11 2019.28 201.314 2 2 7 -10 2007.34 161.592 7 2 7 -10 1860.80 189.234 2 -2 -7 10 1769.01 175.126 8 2 7 -9 1091.84 145.432 2 2 7 -9 1127.96 116.490 7 -2 -7 9 1286.85 150.685 8 -2 -7 8 348.473 90.3433 8 2 7 -8 363.304 98.0397 2 2 7 -8 419.206 72.5821 7 2 7 -7-4.86297 63.3260 2 2 7 -7 35.8656 36.8125 7 -2 -7 7 60.7219 58.4432 8 -2 -7 6 93.9435 57.7347 8 2 7 -6 30.5025 52.5034 2 2 7 -6 7.39159 28.4761 7 -2 -7 5-8.59396 50.3683 8 2 7 -5 17.4504 49.3525 2 2 7 -5 35.9716 26.5852 7 2 7 -4 561.309 62.7980 4 2 7 -4 541.352 99.1571 2 2 7 -4 520.826 47.7008 7 -2 -7 4 724.465 103.421 8 2 7 -3 7065.73 319.986 2 2 7 -3 5954.13 218.287 4 -2 -7 3 6932.09 306.214 8 2 7 -2 83.2498 59.8340 1 -2 -7 2 206.227 62.6037 8 -2 -7 2 198.298 33.5562 3 2 7 -2 146.457 66.8827 2 -2 -7 1 4637.45 170.841 3 -2 -7 1 4796.90 251.640 8 2 7 -1 4843.01 253.802 2 2 7 -1 4642.83 249.923 1 -2 -7 0 160.306 45.0393 3 -2 -7 0 55.3162 50.5783 8 2 7 0 146.159 56.3101 2 2 7 0 240.390 73.0375 1 -2 -7 -1 40.0596 61.2052 8 2 7 1 8.57502 48.7040 2 2 7 1 125.766 68.2875 1 2 7 2 381.781 92.5599 1 2 7 2 339.495 72.0148 2 -2 -7 -2 324.598 77.4111 8 2 7 3 581.251 108.830 1 2 7 3 663.821 89.4973 2 -2 -7 -3 723.296 111.317 8 -2 -7 -4 1642.88 163.087 8 2 7 4 1426.12 161.672 1 -2 -7 -5 1594.59 161.306 8 2 7 5 1714.48 181.627 1 -2 -7 -6 2616.11 212.718 8 2 7 6 2470.99 222.824 1 -2 -7 -7 131.472 77.7914 8 2 7 7 212.218 99.0617 1 -2 -7 -8 86.1706 74.1780 8 2 7 8 154.156 87.7495 1 2 7 9 913.999 161.497 1 -2 -7 -9 1358.61 172.579 8 2 8 -14 51.1749 63.1900 7 2 8 -13 96.2151 81.5917 2 2 8 -13 150.622 76.2295 7 -2 -8 13 3.79986 73.7460 8 2 8 -12 256.400 97.2122 2 2 8 -12 164.631 66.6238 7 -2 -8 12 258.739 99.8508 8 -2 -8 11 1520.31 178.735 8 2 8 -11 1608.95 152.995 7 2 8 -11 1318.49 176.882 2 2 8 -10 1800.08 193.724 2 -2 -8 10 1537.77 176.509 8 2 8 -9 482.125 112.795 2 -2 -8 9 532.138 113.462 8 2 8 -8 274.152 88.4857 2 -2 -8 8 295.426 86.8081 8 2 8 -7 495.082 106.265 2 -2 -8 7 426.453 92.1689 8 -2 -8 6 2353.49 196.888 8 2 8 -6 2145.88 195.864 2 2 8 -5 2779.08 221.369 2 -2 -8 5 3054.32 218.988 8 -2 -8 4 3785.44 241.914 8 2 8 -4 3619.17 246.295 2 2 8 -3 3424.78 236.984 2 -2 -8 3 3531.03 234.114 8 2 8 -2 735.100 85.3589 4 2 8 -2 672.331 110.489 2 -2 -8 2 614.929 103.129 8 2 8 -2 658.581 112.793 1 -2 -8 1 1522.50 155.216 8 2 8 -1 1419.81 154.806 1 2 8 -1 1417.95 147.350 2 2 8 0 312.801 83.0985 2 -2 -8 0 250.629 76.4112 8 2 8 0 230.822 83.2385 1 2 8 1 610.907 101.373 2 -2 -8 -1 611.877 111.382 8 2 8 1 662.032 124.271 1 2 8 2 716.760 120.100 1 -2 -8 -2 575.303 107.888 8 2 8 2 631.169 94.7352 2 2 8 3 472.383 103.391 1 -2 -8 -3 364.599 93.0856 8 2 8 4-57.2690 76.1887 1 -2 -8 -4 63.1457 66.6196 8 2 8 5 421.376 110.779 1 -2 -8 -5 393.274 95.2033 8 2 8 6 275.795 92.4220 1 -2 -8 -6 285.498 90.6050 8 2 8 7-23.1886 71.1214 1 -2 -8 -7 40.7504 58.0122 8 -2 -9 11 314.814 96.6865 8 2 9 -11 338.029 104.587 2 2 9 -10 45.1716 77.0733 2 -2 -9 10-18.3286 79.7377 8 -2 -9 9 14.7794 55.3207 8 2 9 -9 37.8815 69.4473 2 -2 -9 8 315.354 91.4871 8 2 9 -8 376.031 99.3712 2 -2 -9 7 737.646 124.315 8 2 9 -7 864.478 141.428 2 -2 -9 6 575.604 110.879 8 2 9 -6 529.801 115.953 2 -2 -9 5 1485.17 166.734 8 2 9 -5 1483.11 171.996 2 -2 -9 4 2895.20 228.328 8 2 9 -4 2670.68 225.311 2 -2 -9 3 2432.72 207.830 8 2 9 -3 2091.43 194.445 2 2 9 -2 1407.91 161.093 2 2 9 -2 1236.68 151.212 1 -2 -9 2 1390.41 160.669 8 2 9 -1 194.919 81.8194 1 -2 -9 1 292.278 84.7819 8 2 9 -1 231.154 78.5178 2 2 9 0 236.059 74.9437 2 -2 -9 0 365.875 95.0577 8 2 9 0 146.241 76.4794 1 -2 -9 -1 1734.26 180.351 8 2 9 1 1798.88 185.749 1 -2 -9 -2 3028.16 239.068 8 2 9 2 2827.41 238.390 1 -2 -9 -3 2442.21 221.891 8 2 9 3 1934.88 208.502 1 2 9 4 588.165 125.072 1 -2 -9 -4 568.586 122.504 8 2 9 5 381.707 122.099 1 -2 -10 9-77.1417 73.7024 8 2 10 -9 18.0468 70.4934 2 2 10 -8 466.926 114.730 2 -2 -10 8 317.962 97.5204 8 2 10 -7 642.966 140.177 2 -2 -10 7 591.976 118.366 8 2 10 -6 676.240 126.265 2 -2 -10 6 663.242 125.879 8 -2 -10 5 508.473 114.510 8 2 10 -5 703.528 125.227 2 2 10 -4 397.598 116.071 2 -2 -10 4 446.488 109.744 8 2 10 -3-29.8586 66.2254 2 -2 -10 3 63.5548 63.1854 8 2 10 -2 241.538 89.3251 2 2 10 -2-22.0315 67.2852 1 -2 -10 2 115.740 69.3023 8 -2 -10 1 64.7091 63.8020 8 2 10 -1 75.8850 70.5439 1 2 10 -1 157.726 68.7080 2 -2 -10 0 585.686 119.572 8 2 10 0 372.035 106.173 1 -2 -10 -1 1316.59 170.008 8 2 10 1 1410.50 177.374 1 2 11 -6 380.039 116.648 2 2 11 -5 299.743 97.7586 2 2 11 -4 183.929 89.8344 2 2 11 -3 191.417 82.1029 2 -3 13 -2-23.0072 68.9434 4 -3 13 -3-41.6895 65.1312 4 -3 13 -4 155.217 84.6984 4 -3 13 -5 171.122 65.2112 2 -3 13 -5 189.131 75.9318 4 -3 13 -6 60.6759 64.6485 2 3 -12 -1-135.622 78.3671 8 -3 12 1 38.9498 68.5000 4 -3 12 1 10.7974 72.0669 1 -3 12 0-15.1225 62.2462 4 3 -12 0 7.14836 58.7359 8 -3 12 0 15.2206 68.2824 1 -3 12 -1 154.105 91.6930 4 3 -12 1 79.6554 67.7742 8 -3 12 -1 227.208 83.2177 1 -3 12 -2 738.142 138.165 4 3 -12 2 605.822 122.880 8 -3 12 -2 781.389 132.902 1 -3 12 -3 1313.90 172.888 4 3 -12 3 1663.30 182.722 8 3 -12 4 565.355 123.061 8 -3 12 -4 649.412 125.889 4 -3 12 -4 679.072 114.571 2 3 -12 5 115.885 70.2959 8 -3 12 -5 157.393 74.3919 4 -3 12 -5 64.7810 67.6639 2 -3 12 -6-130.787 72.9728 2 3 -12 6 153.405 75.4931 8 -3 12 -7 220.257 84.9387 2 3 -12 7 11.7047 60.0000 8 -3 12 -8 51.8285 79.4730 2 3 -12 8 82.8876 67.3294 8 3 -12 9 605.167 119.044 8 3 -12 10 290.486 101.805 8 3 -12 11 625.150 128.490 8 -3 11 4 491.940 117.456 1 3 -11 -4 816.218 142.409 8 -3 11 3 586.680 128.733 1 3 -11 -3 392.174 110.926 8 3 -11 -2 408.709 100.874 8 -3 11 2 585.614 119.627 4 -3 11 2 208.018 82.0321 1 -3 11 1 40.0666 62.3653 4 3 -11 -1 156.117 81.2162 8 -3 11 1 111.916 78.3801 1 3 -11 0 495.925 107.061 8 -3 11 0 571.558 119.245 4 -3 11 0 725.744 126.272 1 -3 11 -1 540.419 118.384 4 3 -11 1 284.307 86.5712 8 -3 11 -1 527.953 112.319 1 -3 11 -2 649.419 123.803 4 3 -11 2 626.989 114.063 8 -3 11 -2 609.313 110.848 1 -3 11 -2 520.510 89.4090 2 -3 11 -3 169.337 74.9151 4 -3 11 -3 292.159 84.6516 1 3 -11 3 254.399 81.5990 8 -3 11 -3 199.438 71.8905 2 -3 11 -4 2.95985 48.5266 4 3 -11 4 125.070 68.4137 8 -3 11 -4 45.5856 53.8231 2 -3 11 -5 230.213 81.1950 4 3 -11 5 248.993 84.5330 8 -3 11 -5 109.490 57.3705 2 -3 11 -6 545.386 107.417 2 3 -11 6 559.509 111.846 8 -3 11 -7 992.156 145.947 2 3 -11 7 1196.70 147.629 8 3 -11 8 1766.66 182.578 8 -3 11 -8 1841.99 192.261 2 3 -11 9 1178.01 153.410 8 -3 11 -9 1329.41 173.093 2 3 -11 10 403.905 104.811 8 -3 11 -10 539.293 127.689 2 3 -11 11 559.884 120.317 8 3 -11 12 410.159 101.341 8 3 -11 13-126.521 72.8174 8 3 -10 -6 1129.53 161.610 8 -3 10 6 890.730 150.832 1 3 -10 -5 98.8457 67.6510 8 -3 10 5 55.7464 69.0434 1 3 -10 -4 571.744 112.496 8 -3 10 4 473.552 119.106 1 -3 10 3 79.7006 66.2307 1 3 -10 -3 198.371 76.7040 8 -3 10 2 733.152 123.193 4 3 -10 -2 596.784 108.237 8 -3 10 2 447.383 103.204 1 -3 10 1 3411.99 253.957 4 -3 10 1 3756.28 253.652 1 3 -10 -1 3530.53 239.337 8 -3 10 0 3653.98 256.679 4 -3 10 0 3618.56 244.311 1 3 -10 0 4328.96 260.405 8 -3 10 -1 2827.70 224.624 4 3 -10 1 2717.49 205.329 8 -3 10 -1 2509.03 170.899 2 -3 10 -1 2595.92 201.605 1 -3 10 -2 2298.83 197.688 4 3 -10 2 2335.41 185.045 8 -3 10 -2 2166.69 179.414 1 -3 10 -2 2001.28 160.205 2 -3 10 -3 616.554 108.508 4 3 -10 3 693.555 110.076 8 -3 10 -3 500.222 98.2261 1 -3 10 -3 507.309 90.1984 2 -3 10 -4 351.516 87.2154 4 3 -10 4 599.096 98.8418 8 -3 10 -4 446.293 85.6107 2 -3 10 -5 61.3021 59.1473 4 -3 10 -5-103.213 60.7925 2 3 -10 5 4.66168 51.2627 8 -3 10 -6 116.377 67.0192 2 3 -10 6 266.039 82.0921 8 -3 10 -7 654.633 112.487 2 3 -10 7 658.401 109.207 8 -3 10 -8 1391.77 156.337 2 3 -10 8 1461.52 156.249 8 3 -10 9 351.919 88.2271 8 -3 10 -9 277.292 84.4513 2 3 -10 10 21.3806 57.1528 8 -3 10 -10 125.703 70.5008 2 -3 10 -11 232.041 86.9463 2 3 -10 11 357.768 96.8097 8 3 -10 12 279.089 84.6491 8 -3 10 -12 361.704 98.1758 2 3 -10 13-13.0373 56.6180 8 3 -10 14 504.045 116.154 8 3 -9 -8 1922.93 203.902 8 -3 9 8 2021.70 221.946 1 3 -9 -7 3020.56 247.439 8 -3 9 7 3383.51 273.107 1 3 -9 -6 2194.74 203.404 8 -3 9 6 2169.73 215.604 1 3 -9 -5 1003.27 139.200 8 -3 9 5 944.530 145.552 1 3 -9 -4 644.958 106.865 8 -3 9 4 790.448 130.183 1 -3 9 3 353.433 95.2954 1 3 -9 -3 348.342 86.2099 8 -3 9 2 67.1879 70.1639 1 3 -9 -2 100.485 58.6554 8 -3 9 1 448.892 95.8930 1 -3 9 1 634.300 110.034 4 3 -9 -1 475.264 86.3221 8 -3 9 1 336.614 56.7627 2 -3 9 0 2988.48 218.112 4 -3 9 0 2897.01 166.472 2 3 -9 0 3113.92 207.778 8 -3 9 0 2918.53 202.617 1 -3 9 -1 8285.50 363.435 4 -3 9 -1 8151.96 301.641 2 -3 9 -1 7858.62 329.455 1 3 -9 1 8683.13 341.830 8 -3 9 -2 6339.03 276.308 2 -3 9 -2 7003.79 326.484 4 3 -9 2 6869.01 296.685 8 -3 9 -2 6496.12 291.796 1 -3 9 -3 1315.89 133.498 1 -3 9 -3 1439.12 153.602 4 3 -9 3 1466.75 139.447 8 -3 9 -3 1296.24 130.180 2 -3 9 -4 504.508 96.9284 4 3 -9 4 353.464 78.0494 8 -3 9 -4 508.134 93.2012 2 -3 9 -5 1849.40 168.843 4 3 -9 5 1888.62 157.569 8 -3 9 -5 1768.05 157.723 2 -3 9 -6 2156.59 180.976 2 3 -9 6 2530.09 184.143 8 3 -9 7 3680.13 222.190 8 -3 9 -7 3343.40 229.271 2 3 -9 8 558.425 99.4843 8 -3 9 -8 583.218 104.293 2 3 -9 9 74.6318 54.7333 8 -3 9 -9 78.9277 56.3446 2 3 -9 10 77.1052 48.5664 8 -3 9 -10-51.3909 74.0371 2 -3 9 -11-190.569 78.6601 2 3 -9 11 40.7852 64.1272 8 3 -9 12 77.7257 59.2270 8 -3 9 -12-233.670 87.9274 2 -3 9 -13-43.2987 75.3642 2 3 -9 13 101.954 62.6423 8 3 -9 14 1056.36 149.985 8 3 -9 15 849.070 144.306 8 -3 8 9 35.2817 73.8814 1 3 -8 -9 0.99283 55.9293 8 3 -8 -8 305.828 95.7177 8 -3 8 8 135.293 81.1404 1 3 -8 -7 19.0110 62.8131 8 -3 8 7 118.707 86.3045 1 -3 8 6 245.156 90.7495 1 3 -8 -6 209.217 83.4558 8 -3 8 5 279.094 92.5148 1 3 -8 -5 162.160 73.8131 8 3 -8 -4 3116.23 211.686 8 -3 8 4 2903.72 215.718 1 3 -8 -3 9850.31 376.146 8 -3 8 3 9857.25 392.275 1 -3 8 2 15644.0 370.065 2 3 -8 -2 15680.9 477.745 8 -3 8 2 15331.3 493.224 1 3 -8 -1 9569.33 352.893 8 3 -8 -1 9217.95 224.424 7 -3 8 1 9650.09 288.405 2 -3 8 1 10199.8 374.225 1 3 -8 0 1625.99 138.926 8 3 -8 0 1541.14 78.6342 7 -3 8 0 1603.97 118.558 2 -3 8 0 1443.79 137.700 1 -3 8 0 1489.22 147.734 4 3 -8 1 723.898 56.5764 7 -3 8 -1 796.956 108.834 4 -3 8 -1 574.474 77.3686 2 3 -8 1 686.540 91.2732 8 -3 8 -1 520.641 87.9045 1 -3 8 -2 19.0645 49.3000 4 3 -8 2 165.332 55.8145 8 -3 8 -2 90.1824 45.0408 2 3 -8 2 77.3646 25.9360 7 -3 8 -2-3.90189 49.4137 1 -3 8 -3 682.211 101.664 4 3 -8 3 763.651 94.1302 8 3 -8 3 769.625 69.4708 7 -3 8 -3 689.083 90.4846 1 -3 8 -3 1052.45 108.937 2 -3 8 -4 9874.91 378.025 4 3 -8 4 10204.8 347.654 8 -3 8 -4 9379.16 349.036 2 3 -8 5 8930.00 326.496 8 -3 8 -5 9322.53 354.527 2 -3 8 -6 4665.05 250.710 2 3 -8 6 4959.64 238.624 8 3 -8 7 3381.29 196.984 8 -3 8 -7 3255.69 215.157 2 -3 8 -8 720.658 110.911 2 3 -8 8 776.042 103.561 8 -3 8 -9 275.190 83.4105 2 3 -8 9 205.790 69.0343 8 -3 8 -10 543.145 106.716 2 3 -8 10 623.529 97.7369 8 3 -8 11 1482.92 149.211 8 -3 8 -11 1560.95 167.627 2 -3 8 -12 169.371 76.4450 2 3 -8 12 75.2874 60.6709 8 -3 8 -13 156.175 79.1850 2 3 -8 13 172.420 73.9270 8 3 -8 14 368.517 99.8758 8 -3 8 -14 325.694 101.955 2 3 -8 15-153.469 79.4997 8 3 -8 16 23.0434 71.3334 8 -3 7 11 969.252 172.921 1 3 -7 -11 1038.93 154.869 8 -3 7 10 54.3553 80.4854 1 3 -7 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4967.70 242.391 4 3 -7 2 4259.17 156.683 3 3 -7 2 4380.73 163.030 7 -3 7 -2 4924.55 213.933 2 -3 7 -2 4879.11 208.056 1 3 -7 2 4622.24 203.650 8 -3 7 -3 2450.90 172.012 4 -3 7 -3 2251.48 141.091 1 -3 7 -3 2364.01 152.765 2 3 -7 3 2250.94 101.667 3 3 -7 3 2568.61 148.856 8 -3 7 -4 3508.07 207.481 4 3 -7 4 3359.41 123.720 3 -3 7 -4 3328.48 122.220 3 3 -7 4 3896.27 185.457 8 -3 7 -4 3433.54 193.227 2 -3 7 -5 808.286 101.778 2 3 -7 5 943.460 95.6832 8 -3 7 -5 917.303 61.5911 3 -3 7 -6 4540.39 145.502 3 -3 7 -6 4597.04 239.428 2 3 -7 6 4721.09 214.819 8 3 -7 7 2172.60 149.667 8 -3 7 -7 2293.17 105.034 3 -3 7 -7 2148.30 168.356 2 -3 7 -8 870.695 115.119 2 -3 7 -8 990.840 76.4171 3 3 -7 8 931.826 102.889 8 3 -7 9 2103.74 155.861 8 -3 7 -9 2386.55 185.597 2 -3 7 -9 2491.86 128.563 3 -3 7 -10 7900.83 258.370 3 3 -7 10 7368.02 308.217 8 -3 7 -10 7460.73 349.740 2 -3 7 -11 5386.06 299.397 2 3 -7 11 4937.52 262.067 8 3 -7 12 1396.14 148.100 8 -3 7 -12 1541.21 168.689 2 -3 7 -12 1577.87 166.709 5 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1167.08 86.8877 7 3 -6 -3 1367.03 89.7149 7 3 -6 -3 1262.60 71.8430 2 -3 6 3 1187.60 64.1365 2 -3 6 2 35.5337 24.6775 2 3 -6 -2 64.3931 24.9896 2 -3 6 2 139.972 58.5007 1 3 -6 -2 56.8734 29.8854 7 3 -6 -2 44.3843 37.9424 8 -3 6 1 184.871 35.8054 2 3 -6 -1 191.812 38.8199 2 3 -6 -1 194.797 50.0035 8 3 -6 -1 230.675 37.0249 7 -3 6 1 258.289 58.0638 1 3 -6 0 3478.43 165.695 8 3 -6 0 3217.43 132.246 7 -3 6 0 3297.13 148.766 2 -3 6 0 3332.38 167.197 1 3 -6 1 2618.17 120.531 3 3 -6 1 2720.53 140.105 8 -3 6 -1 2757.30 143.878 2 -3 6 -1 2552.51 137.254 1 3 -6 1 2459.20 116.450 7 3 -6 2 459.278 49.2048 3 3 -6 2 433.834 57.8688 8 -3 6 -2 572.683 67.0484 1 -3 6 -2 502.139 68.6488 2 -3 6 -3 1523.69 130.767 4 -3 6 -3 1361.70 80.2883 3 -3 6 -3 1669.47 122.967 2 3 -6 3 1514.80 105.447 8 3 -6 3 1248.75 76.6851 3 3 -6 4 335.426 56.1692 8 -3 6 -4 341.756 65.6148 2 -3 6 -4 308.784 39.9977 3 -3 6 -4 329.195 69.0358 4 -3 6 -5 2092.48 146.906 2 -3 6 -5 1932.61 93.8603 3 3 -6 5 1919.02 119.067 8 3 -6 6 1062.06 94.1875 8 -3 6 -6 1259.71 122.396 2 -3 6 -6 1101.41 76.6690 3 3 -6 7 3131.87 165.044 8 -3 6 -7 3366.31 142.932 3 -3 6 -7 2962.67 189.845 2 3 -6 8 6467.78 253.311 8 -3 6 -8 6575.67 222.318 3 -3 6 -8 6336.50 290.117 2 -3 6 -9 10899.4 315.458 3 3 -6 9 10483.5 350.632 8 -3 6 -9 10414.6 392.867 2 -3 6 -9 10545.6 377.195 5 -3 6 -10 9833.05 313.989 3 -3 6 -10 10689.4 404.405 2 3 -6 10 9944.21 357.432 8 -3 6 -10 10012.3 380.013 5 -3 6 -11 1464.23 149.691 5 -3 6 -11 1517.26 123.831 3 -3 6 -11 1579.98 159.864 2 3 -6 11 1408.90 139.238 8 3 -6 12 670.499 110.818 8 -3 6 -12 886.379 127.140 2 -3 6 -12 791.569 121.676 5 -3 6 -12 720.780 95.2993 3 3 -6 13 1253.38 150.018 8 -3 6 -13 1346.40 135.386 3 -3 6 -13 1441.88 165.906 2 -3 6 -13 1528.94 168.783 5 3 -6 14 2027.52 214.408 1 -3 6 -14 2246.25 209.952 5 -3 6 -14 2122.72 201.833 2 -3 6 -15 1033.51 154.752 5 3 -6 15 656.883 142.795 1 -3 6 -15 827.885 142.333 2 -3 6 -16 1193.67 160.253 2 3 -6 16 947.077 174.392 1 3 -5 -14 643.826 119.205 7 3 -5 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1481.61 89.2528 3 -3 5 -5 1445.70 120.013 2 -3 5 -6 12009.9 305.119 3 -3 5 -6 12107.0 377.018 2 3 -5 6 11493.8 313.826 8 -3 5 -7 2731.92 136.853 3 3 -5 7 2581.26 142.449 8 -3 5 -7 3113.75 185.311 2 -3 5 -7 2711.03 160.616 5 -3 5 -8 1813.00 147.753 2 3 -5 8 2007.56 132.028 8 -3 5 -8 1832.13 118.644 3 -3 5 -8 1839.62 139.400 5 -3 5 -9 550.835 85.7174 5 -3 5 -9 426.953 80.7760 2 3 -5 9 448.638 71.8520 8 -3 5 -9 412.298 64.7543 3 3 -5 10 2162.32 159.001 8 -3 5 -10 2106.45 169.326 2 -3 5 -10 2124.99 164.034 5 -3 5 -11 13.8395 46.2392 5 -3 5 -11 115.457 63.5403 2 3 -5 11 69.9768 51.3118 8 -3 5 -12 720.319 113.769 5 3 -5 12 585.578 102.180 8 -3 5 -12 620.288 106.043 2 3 -5 12 754.785 125.255 1 3 -5 13 2965.53 244.433 1 -3 5 -13 3083.27 225.339 2 -3 5 -13 2989.28 228.790 5 -3 5 -14 2752.43 221.320 2 3 -5 14 3067.41 263.386 1 -3 5 -14 2861.87 231.366 5 3 -5 15 1446.29 190.119 1 -3 5 -15 1127.54 152.507 2 -3 5 -15 1687.96 188.236 5 -3 5 -16 929.444 141.730 2 3 -5 16 946.680 167.287 1 3 -4 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7 -3 4 2 32605.6 564.311 2 -3 4 2 34860.9 632.844 7 -3 4 1 31034.6 595.246 1 3 -4 -1 32259.6 610.425 1 3 -4 -1 31354.6 584.245 8 3 -4 -1 31291.9 584.825 7 -3 4 1 30876.2 556.883 2 -3 4 1 30591.8 584.339 7 3 -4 -1 31258.7 564.329 2 3 -4 0 27300.2 522.307 8 3 -4 0 29180.1 547.760 1 -3 4 0 28796.6 537.672 2 -3 4 0 28133.0 547.938 3 3 -4 0 29705.5 549.420 3 3 -4 0 28391.0 545.339 7 3 -4 0 28560.6 540.217 2 -3 4 0 28206.3 530.745 1 -3 4 -1 4316.24 159.960 2 3 -4 1 4031.58 133.878 8 3 -4 1 4418.69 151.008 3 -3 4 -1 4182.41 137.832 8 3 -4 1 4145.99 157.615 2 -3 4 -1 4112.80 136.364 1 3 -4 1 3838.28 150.417 7 3 -4 1 4457.10 148.594 1 -3 4 -1 4253.29 149.935 3 3 -4 2 6516.94 175.948 8 -3 4 -2 6620.85 178.365 8 3 -4 2 6799.10 194.736 3 -3 4 -2 6694.50 190.206 3 -3 4 -2 6666.23 179.573 1 -3 4 -2 6922.80 220.969 2 3 -4 2 6600.79 184.591 1 3 -4 2 6937.86 190.561 5 3 -4 3 17626.6 351.140 8 -3 4 -3 18319.8 424.005 2 3 -4 3 17400.5 372.845 3 -3 4 -3 17749.4 367.745 3 -3 4 -3 16644.1 345.021 8 3 -4 3 17393.1 357.829 1 3 -4 3 18275.7 376.158 5 3 -4 4 1634.46 86.3673 1 3 -4 4 1554.49 83.5887 8 -3 4 -4 1537.98 89.9767 3 -3 4 -4 1675.14 115.107 2 -3 4 -4 1514.95 80.5040 8 -3 4 -5 31614.8 585.946 8 -3 4 -5 31802.1 604.666 3 -3 4 -5 31381.6 664.759 2 3 -4 5 30773.8 582.090 8 -3 4 -5 31288.0 620.208 5 3 -4 6 18005.0 406.249 8 -3 4 -6 18197.8 419.225 3 -3 4 -6 18594.0 470.977 2 -3 4 -7 4672.65 191.000 3 3 -4 7 4352.86 182.941 8 -3 4 -7 4424.46 213.137 2 -3 4 -7 4301.69 196.448 5 -3 4 -8 574.048 77.7505 5 3 -4 8 513.369 71.9892 8 -3 4 -8 574.545 82.4664 2 -3 4 -9 140.526 57.2556 2 3 -4 9 135.197 45.7594 8 -3 4 -9 179.774 55.3718 5 3 -4 10 789.388 107.798 1 -3 4 -10 593.193 91.1129 2 -3 4 -10 542.204 86.1564 5 -3 4 -11 175.598 63.7124 2 3 -4 11 242.423 77.8444 1 -3 4 -11 34.1663 49.4418 5 3 -4 12 152.763 81.6427 1 -3 4 -12 254.384 68.2858 2 -3 4 -12 263.843 77.1822 5 3 -4 13 2986.58 243.229 1 -3 4 -13 3190.29 221.319 2 -3 4 -13 3012.08 225.918 5 -3 4 -14 1106.77 141.716 2 3 -4 14 926.598 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3 2 11 993.501 149.916 1 3 2 12 289.408 101.058 1 3 2 13 1053.13 163.974 1 3 2 14 47.9856 80.8207 1 3 3 -15 1087.88 154.994 5 -3 -3 15 1447.52 198.140 1 3 3 -15 1088.52 148.950 7 3 3 -15 1191.76 143.439 2 3 3 -14 721.554 123.300 5 -3 -3 14 1102.67 173.376 1 3 3 -14 798.990 125.243 7 3 3 -14 612.638 101.924 2 -3 -3 14 708.392 139.683 8 3 3 -13 559.376 109.141 5 3 3 -13 455.192 97.0571 2 -3 -3 13 501.204 112.036 8 3 3 -13 553.868 102.647 7 3 3 -12 56.6952 67.9131 5 -3 -3 12 94.0254 62.3089 8 3 3 -12 133.985 65.0153 7 3 3 -12 105.838 60.0979 2 3 3 -11 828.535 113.747 5 3 3 -11 955.452 122.462 2 -3 -3 11 783.206 120.762 8 3 3 -11 892.256 113.773 7 3 3 -10 6437.25 284.923 7 -3 -3 10 6310.48 304.013 8 3 3 -10 6994.31 311.956 2 3 3 -10 7288.65 308.964 5 3 3 -9 5831.97 259.307 7 -3 -3 9 5992.22 279.670 8 3 3 -9 6322.21 288.956 2 3 3 -9 6498.85 283.145 5 -3 -3 8 1044.47 112.109 8 3 3 -8 1172.39 108.562 7 3 3 -8 1249.04 127.050 2 3 3 -8 1095.25 113.824 5 -3 -3 7 1606.93 128.783 8 3 3 -7 1778.81 124.932 7 3 3 -7 1540.19 136.334 2 -3 -3 6 362.469 30.5955 4 -3 -3 6 433.434 69.5836 8 3 3 -6 453.398 77.7248 2 3 3 -6 427.400 51.9930 3 3 3 -6 407.664 60.1049 7 -3 -3 5 2002.57 132.158 8 3 3 -5 1944.71 99.7462 3 3 3 -5 1844.92 113.614 7 3 3 -5 2061.29 146.843 2 -3 -3 4 619.323 57.6383 3 3 3 -4 666.889 56.1609 3 -3 -3 4 551.600 70.3678 8 3 3 -4 669.443 84.2429 2 3 3 -4 602.916 62.4611 7 -3 -3 3 1118.87 75.0682 3 -3 -3 3 966.719 76.2009 7 3 3 -3 835.853 63.4893 3 3 3 -3 977.846 77.6449 7 -3 -3 3 951.113 88.9263 8 3 3 -3 1297.50 116.355 2 -3 -3 2 27571.1 583.050 8 -3 -3 2 27458.0 530.331 3 3 3 -2 28448.1 541.004 7 -3 -3 2 29159.9 552.248 7 3 3 -2 28248.1 541.853 3 3 3 -2 29592.8 649.171 2 3 3 -1 15031.5 419.023 2 -3 -3 1 14942.4 342.700 3 -3 -3 1 14512.9 368.343 8 3 3 -1 15591.6 334.523 7 3 3 -1 14160.9 366.616 1 3 3 0 47088.1 928.956 2 -3 -3 0 49126.7 875.721 8 -3 -3 0 48026.7 851.510 3 3 3 0 48149.2 812.721 7 3 3 0 45764.2 872.016 1 -3 -3 -1 1769.95 116.025 8 -3 -3 -1 1820.02 113.079 3 3 3 1 1638.86 90.1867 7 3 3 1 1770.53 121.197 1 -3 -3 -2 5404.68 210.704 8 3 3 2 5208.78 213.868 1 -3 -3 -3 10919.7 325.570 8 3 3 3 10262.7 330.837 1 -3 -3 -4 4027.17 190.309 8 3 3 4 3766.19 200.800 1 -3 -3 -5 539.313 75.8357 8 3 3 5 620.105 88.0891 1 -3 -3 -6 1681.43 134.327 8 3 3 6 1736.31 152.592 1 3 3 7 11590.9 424.590 1 -3 -3 -7 11307.4 380.166 8 -3 -3 -8 422.086 83.2456 8 3 3 8 493.740 99.9691 1 -3 -3 -9 667.598 104.046 8 3 3 9 580.014 114.560 1 -3 -3 -10 49.0692 51.2518 8 3 3 10 111.019 75.1068 1 -3 -3 -11 1372.22 154.302 8 3 3 11 1571.73 190.206 1 3 3 12 1576.48 197.164 1 -3 -3 -12 1114.75 148.547 8 -3 -3 -13 359.608 97.7901 8 3 3 13 551.934 141.059 1 3 4 -16 282.299 82.8578 2 3 4 -15-131.051 80.4319 5 -3 -4 15 32.5277 77.8777 8 3 4 -15 4.07990 68.0483 7 3 4 -15 112.375 62.2646 2 -3 -4 15 41.2267 87.1639 1 3 4 -14 124.688 74.8613 5 3 4 -14 171.441 78.3478 2 3 4 -14 148.549 76.2736 7 -3 -4 14 26.8093 65.8143 8 3 4 -13 83.1290 77.4596 5 -3 -4 13 67.7270 69.3770 8 3 4 -13-101.869 66.5270 2 3 4 -13 110.968 66.5550 7 3 4 -12 1032.85 139.235 5 -3 -4 12 1090.84 146.313 8 3 4 -12 1016.30 133.102 2 3 4 -12 1177.56 137.070 7 3 4 -11-33.4445 61.2407 5 -3 -4 11 31.0527 58.3459 8 3 4 -11 88.0765 64.2755 2 3 4 -11 28.6471 43.5807 7 3 4 -10 1.88531 46.2671 7 3 4 -10 49.0753 49.0544 2 -3 -4 10 75.3201 54.6565 8 3 4 -9 1923.77 144.759 7 -3 -4 9 2048.19 166.710 8 3 4 -9 2274.48 183.786 2 -3 -4 8 3522.48 207.680 8 3 4 -8 3351.42 182.269 7 3 4 -8 3365.80 216.599 2 -3 -4 7 9978.62 218.132 4 -3 -4 7 9409.34 340.693 8 3 4 -7 9604.78 310.624 7 3 4 -7 9925.08 374.215 2 -3 -4 6 4351.20 215.250 8 3 4 -6 3995.57 149.049 3 3 4 -6 4088.67 180.730 7 3 4 -6 4233.05 229.220 2 3 4 -5 2040.29 99.2923 3 3 4 -5 2270.09 124.491 7 -3 -4 5 2198.63 146.360 8 3 4 -5 2279.33 164.798 2 -3 -4 4 3802.64 193.461 8 -3 -4 4 4066.03 144.489 3 3 4 -4 4040.35 143.928 3 3 4 -4 4080.30 162.185 7 3 4 -4 4565.10 228.294 2 -3 -4 3 3817.18 186.680 8 -3 -4 3 3614.71 135.325 3 3 4 -3 3547.21 142.706 7 -3 -4 3 3872.57 153.327 7 3 4 -3 3698.93 203.496 2 -3 -4 2 19873.8 405.642 3 3 4 -2 18392.1 471.257 1 3 4 -2 18897.6 400.309 7 -3 -4 2 19989.0 414.296 7 -3 -4 2 19274.0 480.644 8 3 4 -2 19113.8 507.700 2 -3 -4 1 1278.84 105.781 8 -3 -4 1 1218.75 84.4529 3 3 4 -1 1239.99 74.6903 7 3 4 -1 1088.24 99.8122 1 3 4 -1 1360.43 119.998 2 -3 -4 0 603.173 76.7893 8 3 4 0 532.933 49.8239 7 3 4 0 510.309 76.2506 2 -3 -4 0 530.785 62.4760 3 3 4 0 649.084 80.8504 1 3 4 1 106.684 46.1034 1 3 4 1 29.6410 43.8703 2 -3 -4 -1 74.4620 31.3201 3 -3 -4 -1 118.808 44.9053 8 3 4 1 86.3943 26.9248 7 3 4 2 923.934 99.4498 2 3 4 2 750.907 91.1141 1 -3 -4 -2 804.431 87.7003 8 3 4 2 857.729 66.6352 7 3 4 3 506.285 82.9821 1 -3 -4 -3 490.804 73.7757 8 3 4 3 455.773 49.5784 7 -3 -4 -3 417.571 31.0949 6 -3 -4 -4 5132.61 235.465 8 3 4 4 5084.26 251.880 1 -3 -4 -5 2732.43 175.680 8 3 4 5 2589.29 186.683 1 3 4 6 13673.2 468.553 1 -3 -4 -6 13366.3 428.250 8 3 4 7 6820.43 333.993 1 -3 -4 -7 7267.10 310.302 8 3 4 8 81.6452 67.7483 1 -3 -4 -8 98.6836 56.9188 8 3 4 9 597.381 116.903 1 -3 -4 -9 400.997 89.3041 8 -3 -4 -10 594.522 110.749 8 3 4 10 677.984 139.383 1 -3 -4 -11 210.750 84.5183 8 3 4 11 183.224 90.8688 1 -3 -4 -12 261.957 93.3143 8 3 4 12 319.646 107.155 1 3 5 -16 319.096 100.815 2 3 5 -15 468.323 111.359 5 3 5 -15 128.918 70.0355 2 3 5 -15 510.908 112.766 7 3 5 -14-8.83601 68.2356 7 3 5 -14 200.032 78.6604 2 -3 -5 14 1.34208 72.0112 8 3 5 -13 199.210 81.3309 2 3 5 -13 107.878 68.7422 7 -3 -5 13 205.897 86.9458 8 3 5 -12 885.184 131.964 2 -3 -5 12 859.194 134.722 8 3 5 -12 840.045 120.719 7 3 5 -11 1582.13 168.930 2 3 5 -11 1356.94 139.210 7 -3 -5 11 1600.03 166.139 8 -3 -5 10 1291.24 148.558 8 3 5 -10 1052.98 117.741 7 3 5 -10 1366.24 153.727 2 -3 -5 9 47.7059 46.2821 8 3 5 -9 36.5566 58.6742 2 3 5 -9 27.1610 42.1323 7 -3 -5 8 5058.91 261.459 8 3 5 -8 4733.81 220.302 7 3 5 -8 5876.57 301.140 2 3 5 -7 542.001 99.5122 2 3 5 -7 437.918 67.6955 7 -3 -5 7 533.605 90.1759 8 -3 -5 6 8731.92 330.770 8 3 5 -6 8644.94 277.224 7 3 5 -6 8305.41 220.248 3 3 5 -6 8861.60 357.195 2 -3 -5 5 21063.2 553.089 8 3 5 -5 21066.6 418.750 3 3 5 -5 20527.2 462.061 7 3 5 -5 21327.2 587.071 2 -3 -5 4 14703.5 429.809 8 -3 -5 4 13878.7 305.423 3 3 5 -4 13036.3 325.537 7 3 5 -4 13724.2 444.052 2 3 5 -3 6198.91 164.905 4 -3 -5 3 6834.39 195.038 3 3 5 -3 6265.05 193.716 7 -3 -5 3 6218.50 265.604 8 3 5 -3 6870.56 293.576 2 -3 -5 3 7067.29 214.645 7 -3 -5 2 1470.51 125.926 8 -3 -5 2 1379.64 86.7221 3 3 5 -2 1204.78 117.247 1 3 5 -2 1431.71 132.878 2 3 5 -2 1376.81 77.8195 7 -3 -5 1 2531.96 160.081 8 3 5 -1 2391.18 100.188 7 3 5 -1 2412.49 162.325 1 3 5 -1 2533.23 172.093 2 -3 -5 1 2326.33 121.914 3 -3 -5 0 793.981 78.9572 3 3 5 0 802.625 96.7946 2 3 5 0 759.300 54.1194 7 -3 -5 0 804.365 97.2327 8 3 5 0 831.360 99.8031 1 3 5 1 250.526 63.9244 1 -3 -5 -1 262.431 61.9269 8 -3 -5 -1 236.384 51.3607 3 3 5 1 284.430 68.3439 2 3 5 1 190.931 31.1139 7 3 5 2 1686.96 88.8355 7 3 5 2 1635.62 147.482 1 -3 -5 -2 1767.78 141.535 8 3 5 2 1803.32 142.452 2 -3 -5 -3 4013.40 216.270 8 3 5 3 3280.19 136.559 7 3 5 3 3801.03 221.752 1 3 5 3 3916.64 208.614 2 -3 -5 -4 4986.83 250.207 8 3 5 4 4918.54 263.266 1 3 5 4 5301.17 242.872 2 -3 -5 -5 726.377 101.604 8 3 5 5 748.724 117.239 1 3 5 5 788.179 94.7178 2 3 5 6 1886.75 141.679 2 -3 -5 -6 2012.62 167.847 8 3 5 6 2008.09 186.558 1 3 5 7 449.679 104.511 1 -3 -5 -7 427.281 89.4030 8 3 5 8 113.833 80.8701 1 -3 -5 -8 144.574 75.9225 8 3 5 9 2109.02 215.444 1 -3 -5 -9 2045.40 190.417 8 3 5 10 3180.55 268.393 1 -3 -5 -10 2984.01 239.672 8 3 5 11 2508.90 252.928 1 -3 -5 -11 2865.12 242.108 8 3 6 -15 211.406 88.5120 2 3 6 -15 403.586 103.639 7 3 6 -14 87.7225 61.7676 2 -3 -6 14 98.0477 76.9031 8 3 6 -14 65.8300 63.1604 7 -3 -6 13 1573.46 182.500 8 3 6 -13 1481.90 162.910 7 3 6 -13 1650.74 189.860 2 -3 -6 12 1812.41 190.959 8 3 6 -12 1646.94 160.835 7 3 6 -12 1951.47 206.296 2 -3 -6 11 1839.85 181.217 8 3 6 -11 1830.72 161.749 7 3 6 -11 2091.93 202.911 2 -3 -6 10 1468.32 162.787 8 3 6 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229.273 65.9515 8 3 6 0 113.340 64.3974 1 -3 -6 -1 4130.18 232.455 8 -3 -6 -1 4105.38 198.145 3 3 6 1 3725.74 227.452 1 3 6 1 4235.75 228.170 2 -3 -6 -2 7586.92 321.863 8 -3 -6 -2 7706.61 295.856 3 3 6 2 7329.82 328.387 1 3 6 2 7144.27 300.788 2 -3 -6 -3 3890.79 229.140 8 3 6 3 3191.11 224.451 1 3 6 3 3589.87 205.446 2 3 6 4 191.385 77.3741 1 3 6 4 113.258 54.9069 2 -3 -6 -4 111.562 61.8292 8 3 6 5 272.511 85.0846 1 -3 -6 -5 361.972 84.5597 8 -3 -6 -6 818.514 119.054 8 3 6 6 725.955 124.243 1 3 6 7 21.9983 69.5347 1 -3 -6 -7 16.4273 66.6376 8 3 6 8 159.264 87.2616 1 -3 -6 -8 275.935 92.2027 8 -3 -6 -9 2742.62 232.515 8 3 6 9 2281.21 235.937 1 3 6 10 3027.01 275.874 1 3 7 -15 533.183 114.148 7 3 7 -14 169.656 79.8687 7 3 7 -13 533.747 126.563 2 3 7 -13 605.148 114.638 7 -3 -7 13 913.656 147.024 8 3 7 -12 113.296 64.1306 7 -3 -7 12 103.627 72.0872 8 3 7 -12 277.664 95.5677 2 3 7 -11 763.674 112.137 7 -3 -7 11 861.809 133.549 8 3 7 -11 760.756 135.737 2 -3 -7 10 1232.58 155.745 8 3 7 -10 1217.73 125.083 7 3 7 -10 1265.92 163.729 2 -3 -7 9 446.913 103.983 8 3 7 -9 597.782 115.605 2 3 7 -9 496.724 79.8387 7 3 7 -8 2686.77 165.820 7 -3 -7 8 2576.32 210.165 8 3 7 -8 2532.88 220.534 2 -3 -7 7 5055.00 286.366 8 3 7 -7 5040.07 216.952 7 3 7 -7 4934.48 299.672 2 -3 -7 6 5272.04 285.426 8 3 7 -6 4773.90 195.918 7 3 7 -6 4748.73 288.603 2 -3 -7 5 1090.14 132.088 8 3 7 -5 975.456 136.894 2 -3 -7 4 418.985 90.6197 8 3 7 -4 535.672 106.428 2 3 7 -3 38.1556 57.0743 2 -3 -7 3 128.478 63.6583 8 3 7 -2 291.175 47.0374 4 3 7 -2 123.935 59.5870 2 -3 -7 2 374.228 87.1091 8 3 7 -2 232.000 75.2862 1 -3 -7 1 1149.69 135.293 8 -3 -7 1 1287.53 94.6924 3 3 7 -1 1026.23 128.417 1 3 7 -1 1227.59 138.451 2 -3 -7 0 1399.91 110.474 3 3 7 0 1152.52 135.828 1 -3 -7 0 1131.29 131.780 8 3 7 0 1174.83 133.545 2 3 7 1 2565.44 202.436 1 -3 -7 -1 2496.55 157.096 3 -3 -7 -1 2361.96 189.413 8 3 7 1 2126.08 173.450 2 -3 -7 -2 1601.28 160.750 8 -3 -7 -2 1704.79 139.150 3 3 7 2 1586.29 165.095 1 3 7 2 1644.11 148.931 2 3 7 3 543.677 112.336 1 -3 -7 -3 482.909 95.6800 8 3 7 3 465.439 83.9769 2 -3 -7 -4-179.971 73.2640 8 3 7 4 12.4827 68.0380 1 3 7 5 663.196 126.577 1 -3 -7 -5 764.942 122.200 8 3 7 6 683.989 127.823 1 -3 -7 -6 790.128 124.646 8 -3 -7 -7 225.370 81.5625 8 3 7 7-54.3287 79.9407 1 3 7 8 608.873 134.417 1 -3 -7 -8 718.337 123.108 8 3 8 -12 679.143 143.320 2 -3 -8 12 821.787 145.935 8 3 8 -11 590.255 131.332 2 -3 -8 11 727.271 136.179 8 -3 -8 10 185.881 80.9149 8 3 8 -10 259.657 95.2444 2 3 8 -9 101.969 81.1207 2 -3 -8 9 61.2475 79.9553 8 3 8 -8 1329.79 175.314 2 -3 -8 8 1193.05 157.649 8 3 8 -7 893.039 141.704 2 -3 -8 7 1090.60 142.385 8 -3 -8 6 316.018 82.3302 8 3 8 -6 253.170 82.4136 2 3 8 -5 297.750 89.0084 2 -3 -8 5 282.344 85.3094 8 -3 -8 4 2030.91 183.879 8 3 8 -4 1975.33 194.257 2 -3 -8 3 3213.36 232.952 8 3 8 -3 3333.65 243.760 2 3 8 -2 2287.81 197.000 1 -3 -8 2 2690.75 208.522 8 3 8 -2 2253.23 199.035 2 3 8 -1 750.197 122.672 2 -3 -8 1 733.014 114.983 8 3 8 -1 423.904 101.977 1 -3 -8 0 766.495 120.582 8 3 8 0 750.022 117.451 2 3 8 0 643.378 117.625 1 -3 -8 -1 2343.47 202.881 8 3 8 1 1911.64 191.591 1 3 8 1 2108.07 184.455 2 -3 -8 -2 1316.27 157.297 8 3 8 2 1167.20 132.849 2 3 8 2 1161.86 153.903 1 -3 -8 -3 848.207 127.941 8 3 8 3 729.923 135.760 1 3 8 4 247.315 105.544 1 -3 -8 -4 130.034 73.2416 8 3 8 5 1147.71 166.899 1 -3 -8 -5 1170.02 152.763 8 3 8 6 138.782 89.1786 1 -3 -8 -6 181.939 79.3140 8 3 9 -10 538.915 124.937 2 -3 -9 10 564.176 125.991 8 -3 -9 9 379.168 107.705 8 3 9 -9 475.021 118.471 2 -3 -9 8 57.4151 68.3712 8 3 9 -8 451.578 117.561 2 -3 -9 7 15.3705 57.7180 8 3 9 -7-69.7881 72.7744 2 -3 -9 6-35.6798 56.8304 8 3 9 -6 74.8695 78.2538 2 -3 -9 5 337.628 97.8157 8 3 9 -5 330.815 100.905 2 -3 -9 4 2043.62 195.799 8 3 9 -4 2012.52 204.227 2 -3 -9 3 123.493 75.5984 8 3 9 -3 137.835 85.5098 2 3 9 -2 1440.09 172.827 1 -3 -9 2 1448.10 174.238 8 3 9 -2 1221.17 163.138 2 -3 -9 1 488.947 102.284 8 3 9 -1 398.147 99.1142 2 3 9 -1 266.600 96.4340 1 3 9 0 1203.77 160.388 1 3 9 0 1144.43 144.561 2 -3 -9 0 1280.65 161.453 8 -3 -9 -1 1128.60 151.151 8 3 9 1 921.905 142.213 1 -3 -9 -2 356.953 96.1984 8 3 9 2 431.158 116.266 1 -3 -9 -3 154.478 82.5558 8 3 9 3 341.807 103.170 1 3 10 -7 465.986 129.449 2 -3 -10 6 204.417 87.4919 8 3 10 -6 224.242 91.9110 2 3 10 -5 381.755 113.835 2 -3 -10 5 285.539 92.4342 8 -3 -10 4 610.925 126.663 8 3 10 -4 690.641 136.896 2 3 10 -3 212.371 82.7160 2 -3 -10 3 301.735 105.333 8 -3 -10 2 413.109 109.118 8 3 10 -2 193.817 91.2466 2 3 10 -1-70.9584 69.7533 2 3 10 -1-116.029 71.8038 1 3 11 -4 736.266 140.563 2 3 11 -3-31.3412 68.6528 2 4 -13 2 62.9392 71.9161 8 -4 13 -3 69.3538 81.0701 4 4 -13 3-209.276 81.8872 8 -4 13 -4-90.9839 75.9479 4 4 -13 4-31.4921 57.4542 8 -4 13 -5 269.423 81.5769 2 4 -13 5-204.812 84.8806 8 4 -13 6-26.6139 62.6774 8 -4 13 -6-51.1442 58.7681 2 4 -13 7 114.434 75.9317 8 4 -12 -2 1146.00 160.656 8 -4 12 2 1145.14 166.451 1 -4 12 1 404.227 117.506 4 4 -12 -1 416.685 103.565 8 -4 12 1 535.599 114.435 1 -4 12 0 344.030 107.174 4 -4 12 0 325.478 87.9069 1 4 -12 0 320.659 93.9442 8 -4 12 -1 98.5123 85.7795 4 4 -12 1 43.3840 63.0830 8 -4 12 -1 97.1314 69.0589 1 -4 12 -2 33.1979 64.8234 4 4 -12 2 127.559 69.0161 8 -4 12 -2 102.572 68.4461 1 -4 12 -3 92.3862 71.5649 4 4 -12 3 76.8661 63.9824 8 -4 12 -4 123.567 64.9195 2 4 -12 4 179.289 73.0377 8 -4 12 -4 241.836 89.9270 4 4 -12 5 322.694 90.9197 8 -4 12 -5 310.406 88.3205 4 -4 12 -5 252.794 79.1202 2 -4 12 -6 795.920 130.629 2 4 -12 6 1045.97 145.405 8 4 -12 7 657.207 119.605 8 -4 12 -7 524.000 108.426 2 4 -12 8 248.641 85.4810 8 -4 12 -8 207.966 82.9664 2 4 -12 9 179.776 81.1051 8 4 -12 10 157.768 81.1829 8 4 -11 -5 508.466 111.461 8 -4 11 4 309.949 104.295 1 4 -11 -4 356.910 102.311 8 -4 11 3 188.088 94.6058 4 4 -11 -3 39.6510 62.8818 8 -4 11 2-25.8798 62.1267 1 -4 11 2 149.412 73.7355 4 4 -11 -2 86.8217 68.3782 8 -4 11 1 733.706 139.477 4 4 -11 -1 508.310 105.115 8 -4 11 1 467.418 103.860 1 -4 11 0 1055.32 156.667 4 4 -11 0 1010.18 134.851 8 -4 11 0 1033.86 142.846 1 -4 11 -1 1121.99 161.080 4 4 -11 1 1167.76 142.288 8 -4 11 -1 985.325 136.482 1 -4 11 -2 569.869 121.545 4 4 -11 2 835.700 122.100 8 -4 11 -2 693.978 101.271 2 -4 11 -2 962.548 132.085 1 -4 11 -3 284.933 90.8139 4 -4 11 -3 421.545 88.1326 2 4 -11 3 557.338 104.065 8 -4 11 -3 399.986 88.0130 1 -4 11 -4 847.553 123.743 2 4 -11 4 1038.80 134.774 8 -4 11 -4 1172.23 163.546 4 -4 11 -5-19.5240 62.9661 4 -4 11 -5 92.4446 58.7320 2 4 -11 5-31.0339 68.7892 8 4 -11 6 59.8210 60.0909 8 -4 11 -6 47.4282 59.6287 2 4 -11 7 24.4544 52.2668 8 -4 11 -7 11.4431 70.9677 2 4 -11 8 588.582 105.794 8 -4 11 -8 439.102 99.6876 2 -4 11 -9 605.611 118.247 2 4 -11 9 741.275 117.320 8 -4 11 -10 693.146 125.266 2 4 -11 10 633.390 111.176 8 4 -11 11 951.092 136.490 8 4 -10 -7 633.265 131.430 8 -4 10 6 1363.14 183.068 1 4 -10 -6 1693.79 186.250 8 -4 10 5 1076.18 156.689 1 4 -10 -5 1116.25 152.635 8 4 -10 -4 1369.34 162.423 8 -4 10 4 1234.58 161.461 1 -4 10 3 590.378 114.222 1 4 -10 -3 515.478 102.729 8 -4 10 2 260.283 88.0496 1 -4 10 2 294.862 105.701 4 4 -10 -2 334.025 91.2775 8 -4 10 1 177.632 74.7256 1 -4 10 1 10.0713 66.0058 4 4 -10 -1 19.2408 50.6393 8 -4 10 0 279.652 91.3387 4 4 -10 0 281.002 79.8142 8 -4 10 0 241.542 82.9771 1 -4 10 -1 60.8588 59.1074 4 -4 10 -1 4.47660 40.5748 2 4 -10 1 24.5316 47.5597 8 -4 10 -1 34.1936 55.4554 1 -4 10 -2 2479.54 213.038 4 4 -10 2 2506.18 185.761 8 -4 10 -2 2382.19 172.132 2 -4 10 -2 2325.07 181.844 1 -4 10 -3 3728.36 260.555 4 -4 10 -3 3847.49 229.072 1 4 -10 3 3839.19 231.797 8 -4 10 -3 3942.57 231.480 2 -4 10 -4 4973.34 301.551 4 4 -10 4 5151.54 270.470 8 -4 10 -4 4566.90 258.064 2 4 -10 5 936.715 118.100 8 -4 10 -5 1243.44 139.658 2 -4 10 -5 980.946 142.142 4 4 -10 6 1554.44 150.325 8 -4 10 -6 1262.48 146.409 2 4 -10 7 1205.50 133.722 8 -4 10 -7 1283.66 150.870 2 -4 10 -8 461.964 103.754 2 4 -10 8 380.766 80.0418 8 -4 10 -9-62.1947 69.1012 2 4 -10 9 54.4629 57.3849 8 -4 10 -10 378.551 104.287 2 4 -10 10 574.135 106.693 8 -4 10 -11 373.941 110.581 2 4 -10 11 443.592 97.6065 8 4 -10 12-39.2020 55.3133 8 -4 9 8 463.908 125.319 1 4 -9 -8 595.586 122.857 8 -4 9 7 888.064 145.174 1 4 -9 -7 1267.91 160.811 8 4 -9 -6 1723.76 179.813 8 -4 9 6 1708.08 190.138 1 4 -9 -5 955.562 135.074 8 -4 9 5 878.861 132.171 1 4 -9 -4 322.360 82.0409 8 -4 9 4 62.0517 75.0094 1 -4 9 3 117.750 75.8839 1 4 -9 -3 280.975 77.4360 8 -4 9 2 1247.73 151.229 4 4 -9 -2 1056.38 126.683 8 -4 9 2 1358.77 152.182 1 -4 9 1 5448.49 305.994 4 4 -9 -1 5703.62 277.088 8 -4 9 1 5712.44 226.920 2 -4 9 1 5718.64 289.611 1 -4 9 0 4200.57 267.739 4 4 -9 0 4647.25 243.921 8 -4 9 0 4678.28 214.975 2 -4 9 0 4301.76 242.439 1 -4 9 -1 3163.22 229.507 4 4 -9 1 3737.77 213.857 8 -4 9 -1 3408.19 189.294 2 -4 9 -1 3459.44 209.636 1 -4 9 -2 1376.87 151.322 4 -4 9 -2 1170.98 118.618 2 -4 9 -2 1160.71 121.048 1 4 -9 2 1113.34 117.614 8 -4 9 -3 395.558 92.4685 4 -4 9 -3 422.961 80.5352 2 4 -9 3 455.769 80.7628 8 -4 9 -3 350.865 70.8624 1 4 -9 3 428.804 60.4479 7 4 -9 4 275.302 65.3182 8 -4 9 -4 256.312 77.2922 4 -4 9 -4 378.957 82.0793 2 4 -9 4 252.979 53.9259 7 -4 9 -5 609.801 100.500 2 4 -9 5 884.858 106.816 8 4 -9 6 2885.90 189.382 8 -4 9 -6 2786.66 203.350 2 -4 9 -7 4281.01 259.402 2 4 -9 7 4246.72 228.688 8 4 -9 8 3301.81 204.459 8 -4 9 -8 3369.03 233.423 2 -4 9 -9 1368.48 161.890 2 4 -9 9 1743.49 152.985 8 4 -9 10 1672.43 152.303 8 -4 9 -10 1547.53 174.593 2 4 -9 11 151.383 62.3736 8 -4 9 -11 76.2462 66.9193 2 -4 9 -12 171.707 79.4449 2 4 -9 12 20.6860 51.5667 8 4 -9 13-46.5289 55.9328 8 -4 9 -13 39.7988 65.5877 2 4 -8 -10 40.1032 77.1637 8 4 -8 -9 308.238 101.368 8 -4 8 9 506.447 123.498 1 4 -8 -8 960.773 140.195 8 -4 8 8 772.066 145.262 1 4 -8 -7 56.0482 61.6767 8 -4 8 7 195.168 98.7913 1 4 -8 -6-48.7983 54.7215 8 -4 8 6 173.631 78.1516 1 4 -8 -5 1160.43 134.649 8 -4 8 5 982.815 138.340 1 -4 8 4 808.920 120.590 1 4 -8 -4 593.420 100.992 8 4 -8 -3 672.645 69.7704 7 -4 8 3 859.921 118.506 1 4 -8 -3 731.776 101.000 8 4 -8 -2 5300.73 254.492 8 4 -8 -2 5549.18 196.382 7 -4 8 2 5730.02 201.590 2 -4 8 2 5407.70 270.452 1 -4 8 1 7964.23 352.776 4 4 -8 -1 8290.59 315.398 8 4 -8 -1 8552.39 250.343 7 -4 8 1 8666.66 274.573 2 -4 8 1 8036.91 324.331 1 -4 8 0 8432.16 360.267 4 4 -8 0 8969.53 321.883 8 4 -8 0 8927.93 259.554 7 -4 8 0 9181.73 298.938 2 -4 8 0 8964.63 331.547 1 -4 8 -1 11992.4 431.697 4 4 -8 1 11687.0 373.157 8 4 -8 1 11938.7 316.876 7 -4 8 -1 12481.4 372.737 2 -4 8 -1 11666.7 373.022 1 -4 8 -2 5529.06 285.148 4 4 -8 2 5537.07 235.711 8 4 -8 2 5358.18 202.816 7 -4 8 -2 5817.04 249.830 2 -4 8 -2 5263.31 232.390 1 -4 8 -3 1240.48 138.657 4 4 -8 3 1388.11 119.696 8 -4 8 -3 1316.07 115.693 1 4 -8 3 1335.31 104.191 7 -4 8 -3 1385.49 129.057 2 -4 8 -4 1806.30 164.978 4 4 -8 4 1806.05 134.543 8 -4 8 -4 1824.05 151.036 2 4 -8 5 49.4142 41.6177 8 -4 8 -5-44.7544 30.0595 3 -4 8 -5-33.3400 60.5271 2 -4 8 -6 3531.91 143.293 3 4 -8 6 3775.09 196.709 8 -4 8 -6 3521.36 219.477 2 -4 8 -7 8415.45 240.735 3 -4 8 -7 8535.49 357.099 2 4 -8 7 8844.12 316.557 8 4 -8 8 4805.26 230.887 8 -4 8 -8 4161.81 254.345 2 4 -8 9 1495.03 133.026 8 -4 8 -9 1544.57 159.938 2 -4 8 -10 1544.82 167.831 2 4 -8 10 1565.95 142.262 8 4 -8 11 415.936 86.9255 8 -4 8 -11 348.992 92.0537 2 4 -8 12-26.0768 54.7597 8 -4 8 -12 170.105 79.5797 2 4 -8 13 1574.00 163.611 8 -4 8 -13 1721.88 188.338 2 4 -8 14 1963.45 189.653 8 -4 8 -14 1717.10 195.686 2 4 -8 15 635.931 142.887 1 4 -7 -11 1317.61 179.250 8 -4 7 11 1078.97 178.172 1 -4 7 10 1954.30 220.842 1 4 -7 -10 2431.70 221.242 8 -4 7 9 3151.77 262.926 1 4 -7 -9 2731.83 226.671 8 4 -7 -8 1343.62 156.600 8 4 -7 -8 1155.09 116.287 7 -4 7 8 1194.43 161.391 1 4 -7 -7 62.1267 67.6916 8 -4 7 7 155.473 74.7797 1 4 -7 -7 114.256 47.6016 7 -4 7 6 62.8427 70.7534 1 4 -7 -6 23.7885 34.9467 7 4 -7 -6 16.0623 50.8873 8 4 -7 -5 1028.02 118.110 8 -4 7 5 710.338 115.864 1 4 -7 -5 815.577 84.6743 7 -4 7 4 3044.22 205.795 1 4 -7 -4 3047.68 156.003 7 4 -7 -4 3264.92 196.308 8 -4 7 3 7933.29 213.878 2 4 -7 -3 8233.27 310.893 8 4 -7 -3 7843.48 254.275 7 -4 7 3 8346.22 330.562 1 4 -7 -2 7116.97 280.918 8 4 -7 -2 7599.94 243.362 7 -4 7 2 7601.88 228.649 2 -4 7 2 7562.04 300.556 1 -4 7 1 344.099 54.7451 2 -4 7 1 507.899 84.9016 4 -4 7 1 429.659 72.0664 1 4 -7 -1 512.261 74.5477 8 4 -7 -1 396.397 55.4881 7 -4 7 0 502.296 75.5601 1 -4 7 0 362.763 78.7639 4 -4 7 0 301.701 54.1771 2 4 -7 0 372.317 62.8522 8 4 -7 0 283.935 49.6994 7 -4 7 -1 1322.70 129.625 4 -4 7 -1 1243.93 105.595 2 4 -7 1 1503.26 113.467 8 4 -7 1 1453.79 99.7457 7 -4 7 -1 1508.90 113.508 1 -4 7 -2 108.235 56.8216 4 -4 7 -2 169.309 52.5816 2 4 -7 2 150.868 40.0969 8 -4 7 -2 149.161 44.5053 1 4 -7 2 196.946 43.3951 7 -4 7 -3 2214.59 168.371 4 -4 7 -3 2022.08 112.881 3 4 -7 3 2122.81 131.055 8 -4 7 -3 2147.59 149.766 2 -4 7 -4 9063.08 358.149 4 4 -7 4 9124.56 289.148 8 -4 7 -4 8845.79 254.075 3 -4 7 -4 8880.69 327.505 2 4 -7 5 13233.5 368.266 8 -4 7 -5 13716.6 332.105 3 -4 7 -5 14098.7 436.568 2 -4 7 -6 5976.13 200.590 3 -4 7 -6 5321.78 264.231 2 4 -7 6 5663.50 224.211 8 -4 7 -7-62.0277 63.6803 2 4 -7 7 24.7648 36.9587 8 -4 7 -7 31.2524 29.1807 3 -4 7 -8 237.836 77.7885 2 4 -7 8 348.382 67.1015 8 -4 7 -8 295.245 53.2309 3 -4 7 -9 601.695 110.652 2 -4 7 -9 595.753 74.7291 3 4 -7 9 605.606 84.1213 8 4 -7 10 3700.80 208.593 8 -4 7 -10 3985.22 193.350 3 -4 7 -10 3343.37 234.297 2 -4 7 -11 1110.43 144.354 2 4 -7 11 1159.87 127.395 8 -4 7 -11 1297.63 115.438 3 4 -7 12 1831.39 166.008 8 -4 7 -12 2014.04 191.073 2 -4 7 -12 1914.73 183.983 5 4 -7 13 5748.93 306.375 8 -4 7 -13 5490.22 329.118 2 -4 7 -13 5932.33 330.298 5 -4 7 -14 2699.63 236.292 2 4 -7 14 2653.01 241.657 1 -4 7 -14 2375.40 224.401 5 -4 7 -15 1185.40 167.212 5 -4 7 -15 1183.72 172.164 2 4 -7 15 1089.89 172.649 1 4 -6 -12 1557.92 163.502 7 -4 6 12 1454.28 172.446 6 -4 6 12 1497.26 202.004 1 -4 6 11 967.388 172.259 1 4 -6 -11 1040.23 128.576 7 -4 6 11 1053.24 142.520 6 4 -6 -10 913.091 117.693 7 -4 6 10 1087.97 165.140 1 -4 6 10 927.678 135.527 6 4 -6 -9 652.973 99.4155 7 -4 6 9 660.104 132.474 1 -4 6 9 579.997 104.814 6 4 -6 -8 249.195 57.9107 7 -4 6 8 213.026 84.8468 1 -4 6 8 164.264 70.8780 6 -4 6 7 2013.23 185.011 1 4 -6 -7 1864.36 140.023 7 -4 6 7 1853.46 164.447 6 4 -6 -6 4120.80 200.390 7 -4 6 6 4219.98 250.650 1 -4 6 6 3792.92 225.642 6 -4 6 5 5652.94 279.285 1 4 -6 -5 5695.71 257.916 8 4 -6 -5 5996.03 233.212 7 -4 6 4 11648.6 394.495 1 4 -6 -4 12168.5 377.681 8 4 -6 -4 11588.0 333.299 7 4 -6 -4 11628.8 261.444 2 -4 6 3 14305.1 423.164 1 4 -6 -3 14000.5 368.558 7 4 -6 -3 14375.2 403.499 8 4 -6 -3 14275.9 325.632 2 4 -6 -2 6595.02 248.054 8 4 -6 -2 7074.55 233.426 7 -4 6 2 6917.72 208.022 2 4 -6 -2 7079.88 219.658 2 -4 6 2 7164.96 269.831 1 -4 6 1 663.734 91.7611 4 4 -6 -1 623.885 73.0401 8 4 -6 -1 688.565 71.1208 7 -4 6 1 574.093 64.3049 2 -4 6 1 781.988 85.9915 1 -4 6 0 244.612 53.0131 1 -4 6 0 286.856 51.7458 2 4 -6 0 259.602 49.3583 8 4 -6 0 228.905 44.3759 7 4 -6 1 2578.13 136.195 7 4 -6 1 2370.06 126.452 8 -4 6 -1 2642.53 137.562 3 -4 6 -1 2552.66 131.058 1 -4 6 -1 2832.74 150.649 2 4 -6 2 2105.70 113.150 8 -4 6 -2 1964.76 113.529 3 4 -6 2 2087.34 124.146 7 -4 6 -2 2191.29 138.342 2 -4 6 -2 1907.11 110.197 1 -4 6 -3 31.6691 24.2872 3 -4 6 -3 47.1208 41.0497 2 4 -6 3 14.9214 23.4265 8 4 -6 4 306.951 47.8933 8 -4 6 -4 326.977 48.2016 3 -4 6 -4 251.815 61.9269 2 -4 6 -5 1269.54 89.7828 3 -4 6 -5 1374.46 123.149 2 4 -6 5 1141.51 87.9075 8 4 -6 6 1375.95 98.4841 8 -4 6 -6 1378.87 98.9059 3 -4 6 -6 1383.20 131.592 2 4 -6 7 864.735 84.1503 8 -4 6 -7 859.914 83.9568 3 -4 6 -7 779.476 104.116 2 -4 6 -8 94.3285 41.8329 3 4 -6 8 23.0375 35.8585 8 -4 6 -8 16.6855 46.3918 2 -4 6 -9 841.334 109.642 5 -4 6 -9 617.163 100.984 2 4 -6 9 706.342 90.8515 8 -4 6 -9 845.597 91.4539 3 -4 6 -10 2222.09 184.175 2 -4 6 -10 2405.38 156.039 3 4 -6 10 2034.71 154.315 8 -4 6 -10 2509.87 184.078 5 -4 6 -11 159.217 66.1378 5 -4 6 -11 156.088 73.7691 2 4 -6 11 115.584 62.3481 8 -4 6 -11 376.738 74.3762 3 -4 6 -12 3796.37 220.265 3 -4 6 -12 3885.51 258.269 2 4 -6 12 3478.99 225.231 8 -4 6 -12 3445.62 238.968 5 -4 6 -13 4602.70 258.089 3 4 -6 13 4321.91 290.355 1 -4 6 -13 4705.14 291.220 2 -4 6 -13 4728.94 291.742 5 -4 6 -14 808.298 137.427 5 -4 6 -14 908.221 137.437 2 -4 6 -14 824.799 119.454 3 4 -6 14 900.831 153.123 1 -4 6 -15 329.934 103.048 5 -4 6 -15 315.262 99.7740 2 4 -6 15 302.303 105.950 1 -4 6 -16 473.373 107.167 2 4 -6 16 73.2350 85.8388 1 4 -5 -14 380.113 101.168 7 -4 5 13 1135.57 181.050 1 4 -5 -13 1129.06 153.429 7 -4 5 13 1360.40 167.132 6 -4 5 12 538.061 134.792 1 4 -5 -12 327.793 84.1053 7 -4 5 12 544.376 117.754 6 -4 5 11 196.740 93.1512 1 4 -5 -11 86.0527 60.8214 7 -4 5 11 153.225 71.2942 6 -4 5 10 378.062 103.918 1 4 -5 -10 230.083 68.2073 7 -4 5 10 439.447 94.3718 6 -4 5 9 3030.48 242.744 1 4 -5 -9 3300.84 203.480 7 -4 5 9 3661.25 234.449 6 -4 5 8 2835.64 219.675 1 4 -5 -8 2993.16 185.847 7 -4 5 8 3194.25 211.085 6 4 -5 -7 7737.58 291.503 7 -4 5 7 7928.60 349.987 1 -4 5 7 7922.06 328.218 6 -4 5 6 6849.99 306.980 1 4 -5 -6 7041.82 264.975 7 -4 5 6 6915.58 294.379 6 -4 5 5 2492.34 171.800 1 4 -5 -5 2302.24 84.6637 2 4 -5 -5 2511.22 147.527 7 -4 5 5 2800.52 179.809 6 -4 5 4 2182.73 153.942 1 4 -5 -4 2318.06 136.721 7 4 -5 -4 2276.21 95.6426 2 -4 5 4 2483.04 165.891 6 4 -5 -3 198.700 47.8730 8 4 -5 -3 145.057 41.3586 7 4 -5 -3 203.982 32.5457 2 -4 5 3 138.681 48.7418 1 -4 5 2 580.565 72.9227 1 4 -5 -2 552.117 65.3143 8 4 -5 -2 651.690 69.4059 7 -4 5 2 629.863 57.3871 2 4 -5 -2 668.026 59.6614 2 4 -5 -1 622.277 66.2112 8 4 -5 -1 689.075 69.7899 7 -4 5 1 608.849 60.9268 2 4 -5 -1 674.287 64.2072 2 -4 5 1 628.611 68.9956 1 4 -5 0 17173.6 379.431 8 -4 5 0 17250.8 413.807 3 4 -5 0 17942.8 406.109 1 4 -5 0 17287.4 415.653 7 -4 5 0 17343.3 400.460 2 -4 5 0 17649.1 389.073 1 4 -5 1 19471.3 420.118 1 -4 5 -1 19896.1 439.225 3 4 -5 1 19326.9 398.834 8 4 -5 1 18627.9 440.660 7 -4 5 -1 19534.4 446.977 2 -4 5 -1 19126.0 399.474 1 -4 5 -2 12803.4 318.966 3 -4 5 -2 11779.5 283.167 8 4 -5 2 12441.7 283.374 8 -4 5 -2 12538.5 347.607 2 -4 5 -2 12107.2 284.460 1 4 -5 2 12442.4 295.594 5 4 -5 2 12384.9 300.526 1 4 -5 3 1887.04 93.1012 8 -4 5 -3 1937.96 109.064 3 -4 5 -3 1854.60 92.2557 8 -4 5 -3 1976.58 131.291 2 4 -5 3 1968.32 100.487 1 4 -5 3 1744.86 97.7967 5 -4 5 -4 4112.30 145.333 8 -4 5 -4 4583.94 174.683 3 4 -5 4 4293.12 148.971 8 -4 5 -4 4707.29 211.676 2 4 -5 4 4527.34 160.222 1 -4 5 -5 4826.03 222.560 2 -4 5 -5 4530.99 160.424 8 -4 5 -5 5140.31 194.435 3 4 -5 5 4509.54 163.618 1 4 -5 5 4761.06 165.428 8 -4 5 -6 306.173 65.2847 2 4 -5 6 258.649 43.1317 8 -4 5 -6 256.120 49.9457 3 -4 5 -7 1201.09 119.207 2 4 -5 7 1344.31 98.7860 8 -4 5 -7 1289.39 103.813 3 -4 5 -7 1306.66 111.069 5 4 -5 8 4645.68 202.888 8 -4 5 -8 4762.74 210.072 3 -4 5 -8 4618.79 240.498 2 -4 5 -8 4397.31 214.912 5 4 -5 9 10805.8 343.796 8 -4 5 -9 10488.5 344.649 3 -4 5 -9 10775.2 390.449 2 -4 5 -9 10226.6 360.041 5 -4 5 -10 891.547 117.075 2 4 -5 10 801.103 97.7221 8 -4 5 -10 927.296 104.859 3 -4 5 -10 928.434 109.911 5 -4 5 -11 636.609 104.415 5 -4 5 -11 618.807 103.879 2 -4 5 -11 611.374 91.7085 3 4 -5 11 431.665 94.2405 1 -4 5 -12 208.968 69.2574 5 -4 5 -12 166.665 65.5675 2 4 -5 12 3.76604 68.1923 1 -4 5 -12 98.1684 61.2967 3 -4 5 -13 507.044 106.322 5 -4 5 -13 513.554 105.330 2 -4 5 -13 678.192 110.518 3 4 -5 13 385.831 99.2465 1 -4 5 -14 60.6335 71.1641 5 -4 5 -14 201.520 70.4433 2 -4 5 -14 222.863 84.0428 3 4 -5 14 107.306 68.1988 1 -4 5 -15 638.482 123.670 5 -4 5 -15 459.290 117.694 2 4 -5 15 590.054 132.571 1 -4 5 -15 542.183 109.077 3 -4 5 -16 709.206 131.983 2 -4 5 -16 928.304 145.604 3 4 -5 16 503.027 139.682 1 4 -4 -14 89.5532 70.0138 7 -4 4 14 74.2625 64.7326 6 4 -4 -13 84.7918 63.2147 7 -4 4 13 216.265 104.147 1 -4 4 13 71.6147 68.3379 6 -4 4 12 189.707 89.7549 1 4 -4 -12 145.883 69.9236 7 -4 4 12 69.6416 64.2534 6 -4 4 11 142.957 94.0465 1 4 -4 -11 146.879 64.1702 7 -4 4 11 141.257 71.7999 6 -4 4 10 2639.30 232.520 1 4 -4 -10 2922.22 199.189 7 -4 4 10 2931.50 215.841 6 -4 4 9 9286.34 413.800 1 4 -4 -9 8806.05 343.457 7 -4 4 9 9502.83 381.375 6 -4 4 8 5548.04 298.228 1 4 -4 -8 5662.97 254.297 7 -4 4 8 5517.90 277.362 6 -4 4 7 10541.7 396.582 1 -4 4 7 11822.2 393.156 6 4 -4 -7 9725.25 207.791 2 4 -4 -7 10651.4 345.429 7 -4 4 6 1100.70 118.669 1 4 -4 -6 1071.77 56.4290 2 4 -4 -6 1034.70 99.4765 7 -4 4 6 1234.35 122.283 6 4 -4 -6 1049.33 60.0349 2 -4 4 5 305.014 68.2804 1 4 -4 -5 415.616 39.1197 2 4 -4 -5 405.672 64.3270 7 -4 4 5 453.998 76.1143 6 -4 4 4 116.462 48.8891 1 4 -4 -4 78.5456 22.1271 2 4 -4 -4 81.0671 37.6638 7 -4 4 3 2353.55 134.223 1 4 -4 -3 2110.02 126.400 7 4 -4 -3 2196.85 99.4597 2 -4 4 2 1505.89 97.4731 1 4 -4 -2 1350.26 94.3855 1 4 -4 -2 1436.54 101.449 7 4 -4 -2 1412.54 84.1159 2 -4 4 1 1626.17 94.6747 1 4 -4 -1 1486.68 90.3580 1 4 -4 -1 1601.09 108.651 7 -4 4 1 1751.13 96.5694 2 4 -4 -1 1611.48 94.0214 2 4 -4 -1 1556.07 87.7913 8 -4 4 1 1629.49 111.793 3 -4 4 0 691.848 70.8293 3 4 -4 0 778.768 59.1691 1 4 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3 11 2014.72 206.432 1 4 -3 -11 2267.11 182.874 7 -4 3 11 2474.85 204.441 6 -4 3 10 4405.09 284.093 1 4 -3 -10 4794.87 255.081 7 -4 3 10 5056.75 278.244 6 -4 3 9 669.999 118.022 1 4 -3 -9 576.223 88.7277 7 -4 3 9 578.736 102.933 6 4 -3 -8 64.3948 28.6192 2 -4 3 8 5.61110 61.1155 1 4 -3 -8 116.274 55.4150 7 -4 3 8 75.2520 56.8244 6 4 -3 -7 15.8363 18.5167 2 -4 3 7 18.9397 51.0943 1 4 -3 -7 50.5689 48.9282 7 -4 3 7 91.6713 62.4512 6 -4 3 6 872.508 101.516 1 4 -3 -6 739.206 86.8494 7 4 -3 -6 865.201 59.5760 2 -4 3 6 822.717 97.6655 6 4 -3 -6 717.350 62.3698 2 4 -3 -5 35.4619 20.1037 2 -4 3 5 25.5428 37.0590 1 4 -3 -5 46.8546 35.8037 7 4 -3 -4 5958.43 221.456 7 -4 3 4 5154.35 210.260 1 4 -3 -4 5742.26 171.740 2 -4 3 3 23643.9 516.035 1 4 -3 -3 25828.9 544.384 7 4 -3 -3 25299.4 483.541 2 4 -3 -3 26233.2 529.366 1 -4 3 2 29323.7 601.893 3 -4 3 2 28262.3 543.560 1 4 -3 -2 29540.3 594.410 7 4 -3 -2 28623.5 547.187 1 4 -3 -2 28886.0 544.661 2 -4 3 1 40279.7 761.655 4 -4 3 1 39403.4 676.950 1 -4 3 1 40327.7 759.920 3 4 -3 -1 40264.7 753.402 7 4 -3 -1 40198.9 721.296 2 4 -3 -1 40945.8 683.416 1 -4 3 0 26134.4 539.016 4 -4 3 0 24258.7 508.095 3 4 -3 0 23732.5 408.532 8 4 -3 0 24189.4 418.027 1 -4 3 0 24630.4 489.028 2 4 -3 0 25480.8 526.063 7 -4 3 0 23759.3 409.545 1 -4 3 -1 5720.66 210.802 4 -4 3 -1 5416.28 189.684 3 4 -3 1 4578.38 110.792 1 -4 3 -1 5589.73 188.705 2 4 -3 1 5491.08 198.893 7 4 -3 1 4986.07 104.671 8 -4 3 -2 3521.08 152.808 2 -4 3 -2 3430.47 147.290 3 4 -3 2 2785.24 74.9094 1 -4 3 -3 97.1761 24.3653 5 -4 3 -3 135.615 43.6758 2 4 -3 3 98.7990 15.8690 8 -4 3 -3 69.9136 12.7210 8 -4 3 -3 91.2321 36.0715 3 4 -3 3 53.4543 13.5119 1 -4 3 -4 6153.19 222.058 3 -4 3 -4 5948.88 148.021 8 -4 3 -4 6395.33 232.324 2 -4 3 -4 6363.51 186.829 5 -4 3 -5 30738.8 551.810 8 -4 3 -5 32016.4 654.963 3 -4 3 -5 31715.7 664.861 2 4 -3 5 31674.9 591.596 1 -4 3 -5 32161.3 606.511 5 -4 3 -6 19814.0 410.424 8 -4 3 -6 20361.4 488.663 3 4 -3 6 20532.2 454.301 1 -4 3 -6 19929.4 496.682 2 -4 3 -7 4454.31 207.710 3 4 -3 7 4339.99 192.744 1 -4 3 -7 4332.91 208.860 2 -4 3 -8 291.613 64.3123 2 -4 3 -8 232.695 61.8268 3 4 -3 8 252.475 61.0885 1 -4 3 -9 553.863 87.0043 2 4 -3 9 529.618 87.2374 1 4 -3 10 1735.89 155.546 1 -4 3 -10 1561.91 141.195 2 4 -3 11 5575.65 293.661 1 -4 3 -11 5708.13 278.048 2 4 -3 12 4549.02 277.954 1 -4 3 -12 4454.32 253.240 2 4 -3 13 3014.49 241.248 1 -4 3 -13 2992.05 215.975 2 4 -3 14 2415.55 227.349 1 -4 3 -14 2709.76 214.376 2 -4 3 -15 171.209 75.2986 2 4 -3 15 354.690 115.527 1 4 -3 16-39.1468 71.8343 1 -4 2 16 46.8241 70.8610 6 4 -2 -15 7.38772 61.7736 7 -4 2 15 61.1129 75.0229 6 4 -2 -14 48.8861 64.0348 7 -4 2 14 84.7512 78.6881 1 4 -2 -13 654.222 113.595 7 -4 2 13 759.660 146.295 1 -4 2 12 2263.00 222.909 1 4 -2 -12 2250.86 191.487 7 -4 2 11 3225.38 252.342 1 4 -2 -11 3011.66 210.304 7 -4 2 10 2178.66 195.256 1 4 -2 -10 2004.56 165.227 7 4 -2 -10 2175.77 122.422 2 -4 2 9 362.465 93.3459 1 4 -2 -9 294.356 48.7512 2 4 -2 -9 86.3856 50.4541 7 4 -2 -8 345.898 52.8092 2 -4 2 8 439.015 87.5393 1 4 -2 -8 343.828 70.7548 7 -4 2 7 1376.14 133.105 1 4 -2 -7 1393.66 120.136 7 4 -2 -7 1274.40 91.8221 2 -4 2 6 645.324 87.8472 1 4 -2 -6 675.015 83.4184 7 4 -2 -6 511.365 61.8009 2 -4 2 5 1683.77 124.442 1 4 -2 -5 1808.38 123.264 7 -4 2 4 19810.1 455.995 1 4 -2 -4 19890.5 468.311 7 -4 2 3 30462.0 617.543 3 -4 2 3 29356.1 568.217 1 4 -2 -3 29597.2 603.860 7 4 -2 -3 28344.0 549.351 8 -4 2 2 1736.29 101.150 4 4 -2 -2 1912.13 85.8755 8 4 -2 -2 2071.64 119.929 7 -4 2 2 2114.30 122.128 3 -4 2 2 1828.66 89.1303 1 4 -2 -2 1950.25 102.652 2 -4 2 1 1003.41 78.3288 4 -4 2 1 967.106 81.9477 3 -4 2 1 878.332 49.5310 1 4 -2 -1 981.458 72.8350 2 4 -2 -1 842.264 77.6766 7 4 -2 -1 995.210 50.6786 8 -4 2 1 911.413 80.2497 6 4 -2 0 12921.3 310.132 4 -4 2 0 13170.4 321.180 4 -4 2 0 13698.1 329.771 3 4 -2 0 11436.1 208.170 8 4 -2 0 12691.6 307.305 6 -4 2 0 13108.0 316.693 6 4 -2 0 13587.1 337.852 7 4 -2 1 18401.4 419.097 4 -4 2 -1 19886.4 431.890 3 4 -2 1 19730.2 444.848 7 4 -2 1 19362.6 409.095 6 -4 2 -2 31652.3 619.883 3 -4 2 -2 30860.9 607.759 2 4 -2 2 30742.7 577.963 6 -4 2 -3 16693.5 286.032 8 4 -2 3 16631.9 306.113 1 -4 2 -3 18692.4 424.672 3 -4 2 -3 18628.1 416.083 2 4 -2 3 18720.9 379.957 6 -4 2 -4 16245.8 406.571 3 4 -2 4 16020.5 325.605 1 -4 2 -4 15638.2 298.728 8 -4 2 -4 16744.5 401.537 2 -4 2 -5 6038.13 231.514 3 4 -2 5 6364.42 196.745 1 -4 2 -5 6130.97 226.332 2 -4 2 -5 5885.45 167.957 8 -4 2 -6 1771.73 129.210 3 4 -2 6 1926.34 115.628 1 -4 2 -6 1955.11 99.6315 8 -4 2 -6 1741.38 121.248 2 -4 2 -7 136.321 49.0272 2 4 -2 7 132.483 45.0558 1 4 -2 8 2566.82 162.175 1 -4 2 -8 2509.77 158.590 2 4 -2 9 2174.23 160.087 1 -4 2 -9 2151.75 152.512 2 -4 2 -10 799.279 101.734 2 4 -2 10 913.376 119.576 1 4 -2 11 10240.9 410.458 1 -4 2 -11 10998.3 384.420 2 4 -2 12 3022.62 234.409 1 -4 2 -12 3409.15 213.008 2 -4 2 -13 764.478 110.555 2 4 -2 13 775.018 126.705 1 -4 2 -14-46.7653 53.4504 2 4 -2 14-72.7052 74.7309 1 4 -2 15 43.2854 68.7707 1 4 -2 16 185.815 87.2824 1 4 -1 -15 933.654 146.955 7 -4 1 15 1041.86 177.462 1 -4 1 14 1761.09 211.325 1 4 -1 -14 1841.82 188.645 7 -4 1 13 2880.16 258.565 1 4 -1 -13 2527.06 210.562 7 -4 1 12 1950.62 201.969 1 4 -1 -12 1951.98 175.876 7 -4 1 11 419.620 103.006 1 4 -1 -11 599.969 77.4319 2 4 -1 -11 517.004 97.3773 7 -4 1 10-14.5350 70.0469 1 4 -1 -10-64.0947 58.7192 7 4 -1 -10 13.7293 32.8098 2 4 -1 -9 77.1827 40.3598 2 4 -1 -9-0.93782 53.2267 7 -4 1 9-38.1185 67.8489 1 4 -1 -8 5303.74 246.561 7 -4 1 8 6033.80 282.627 1 4 -1 -8 5287.74 211.989 2 4 -1 -7 2202.55 149.807 7 -4 1 7 2422.29 166.857 1 4 -1 -7 2086.02 128.490 2 4 -1 -6 2910.05 164.355 7 -4 1 6 2983.64 172.765 1 4 -1 -6 2887.75 151.586 2 4 -1 -5 10950.9 323.038 2 4 -1 -5 11127.2 330.284 7 -4 1 5 10937.8 327.602 1 4 -1 -4 3560.14 168.094 7 -4 1 4 3453.44 156.800 1 -4 1 4 3323.24 149.037 8 4 -1 -3 781.364 60.1520 8 -4 1 3 814.083 78.7384 3 4 -1 -3 720.063 76.1855 7 -4 1 3 715.152 62.8832 8 4 -1 -3 802.101 52.0609 5 -4 1 2 51.6125 26.1530 8 -4 1 2 62.3394 27.0722 4 -4 1 2 73.5640 37.4838 3 4 -1 -2 45.8944 21.8712 8 4 -1 -2 81.9817 39.9617 7 -4 1 1 17200.2 363.100 4 -4 1 1 17164.7 314.901 8 -4 1 1 17687.3 401.618 3 4 -1 -1 17444.8 404.234 7 4 -1 -1 16324.2 309.768 8 -4 1 1 17185.9 382.031 6 4 -1 0 48884.4 814.066 4 -4 1 0 48823.1 730.531 8 4 -1 0 46898.2 728.095 8 -4 1 0 51049.4 862.848 3 4 -1 0 50371.9 873.567 7 -4 1 0 45435.3 725.138 1 -4 1 0 48765.7 825.525 6 4 -1 1 1495.82 90.5913 4 -4 1 -1 1439.10 45.3520 8 -4 1 -1 1246.10 45.8641 1 -4 1 -1 1612.27 103.562 3 4 -1 1 1551.62 102.991 7 -4 1 -1 1544.40 83.5432 6 -4 1 -2 5060.50 111.916 8 -4 1 -2 5471.45 201.970 3 -4 1 -2 4844.37 120.023 1 4 -1 2 5061.38 149.222 6 4 -1 2 5007.70 117.969 1 -4 1 -3 97.4027 22.5508 1 -4 1 -3 121.951 21.1138 8 4 -1 3 107.969 23.5251 1 -4 1 -3 148.748 44.2614 3 4 -1 3 85.3806 22.5455 6 4 -1 4 8205.85 221.286 1 -4 1 -4 8703.94 283.317 3 -4 1 -4 8712.35 262.410 2 -4 1 -4 8443.51 222.649 1 4 -1 4 8284.87 199.990 6 -4 1 -5 32.8913 31.5662 2 4 -1 5 19.4625 29.5357 1 -4 1 -5 44.2164 20.9746 8 -4 1 -5 2.20218 41.5611 3 -4 1 -6 1992.08 128.107 2 4 -1 6 1946.61 123.958 1 4 -1 7 855.114 92.7371 1 -4 1 -7 927.208 93.1091 2 4 -1 8 15913.9 463.402 1 -4 1 -8 16441.7 441.816 2 4 -1 9 6161.22 286.918 1 -4 1 -9 6069.85 254.683 2 4 -1 10 11939.4 438.232 1 -4 1 -10 12412.3 391.846 2 4 -1 11 4648.77 279.531 1 -4 1 -11 4920.52 241.042 2 4 -1 12 2890.02 233.854 1 -4 1 -12 3397.05 205.938 2 -4 1 -13 977.826 116.905 2 4 -1 13 838.160 142.716 1 4 -1 14 336.912 115.508 1 4 -1 15 1090.50 168.638 1 4 -1 16 350.089 121.565 1 -4 0 15 966.629 173.739 1 4 0 -15 858.168 142.233 7 4 0 -15 610.702 120.960 5 -4 0 14 688.886 151.896 1 4 0 -14 847.178 135.363 7 4 0 -14 882.766 133.050 5 -4 0 13 981.791 171.586 1 4 0 -13 793.465 122.168 7 4 0 -13 905.099 130.986 5 4 0 -12 239.764 63.4915 2 4 0 -12 168.883 56.8449 7 -4 0 12 180.850 87.3932 1 4 0 -12 252.556 77.5984 5 4 0 -11 2042.77 173.312 7 -4 0 11 2005.12 194.469 1 4 0 -11 1973.97 145.695 2 4 0 -10 3983.44 232.376 7 -4 0 10 4562.92 274.574 1 4 0 -10 4645.67 222.596 2 4 0 -9 11764.6 396.217 7 -4 0 9 11448.2 428.198 1 4 0 -9 11985.3 372.226 2 4 0 -9 11773.9 378.400 5 -4 0 8 7459.70 304.988 8 4 0 -8 8125.16 306.443 7 -4 0 8 8324.63 334.552 1 4 0 -8 7700.31 284.018 2 4 0 -8 8077.26 288.190 5 4 0 -7 2002.70 144.397 7 -4 0 7 1974.51 142.527 8 4 0 -7 2082.06 137.087 2 4 0 -7 2066.69 130.291 5 -4 0 6 8242.42 282.127 8 4 0 -6 8243.70 287.405 7 4 0 -6 8109.59 256.837 5 4 0 -6 7933.71 281.152 2 -4 0 5 18013.5 436.930 8 4 0 -5 18377.6 454.974 7 4 0 -5 18742.4 409.573 5 4 0 -5 17792.2 465.405 2 -4 0 4 11835.1 314.476 8 -4 0 4 11725.4 330.664 3 4 0 -4 12481.1 343.269 7 4 0 -4 12471.2 290.743 5 -4 0 3 1061.33 60.1539 4 -4 0 3 1006.20 74.7052 8 4 0 -3 1054.75 72.1816 8 4 0 -3 1213.74 93.8260 7 -4 0 3 1181.96 90.6573 3 -4 0 2 538.166 44.9643 4 4 0 -2 590.141 51.4788 8 4 0 -2 833.666 80.9849 7 -4 0 2 612.128 72.5579 3 -4 0 2 530.663 53.2698 8 -4 0 2 399.914 39.1035 5 4 0 -1 18200.6 350.201 4 4 0 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7519.75 275.159 7 4 3 -6 7689.11 320.750 2 -4 -3 5 6227.53 217.014 3 4 3 -5 6029.13 231.337 7 -4 -3 5 5875.93 243.886 8 4 3 -5 6179.90 280.839 2 -4 -3 4 720.456 82.2890 8 -4 -3 4 714.737 71.3533 3 4 3 -4 821.547 81.7682 7 4 3 -4 780.269 101.938 2 -4 -3 3 79.1822 37.2273 8 -4 -3 3 75.0749 31.6320 3 4 3 -3 122.725 52.7306 2 4 3 -3 149.590 40.9211 7 4 3 -2 1372.90 129.209 2 -4 -3 2 1510.69 109.830 8 -4 -3 2 1318.28 93.5912 3 4 3 -2 1512.55 100.488 7 -4 -3 1 127.510 41.4546 8 -4 -3 1 150.234 38.4167 3 4 3 -1 2.56986 50.5536 2 4 3 -1 253.093 51.0489 1 4 3 -1 111.483 32.8202 7 -4 -3 0 974.406 85.6760 8 -4 -3 0 1005.70 89.4821 3 4 3 0 864.686 85.0552 1 4 3 0 928.184 77.7828 7 4 3 1 8847.78 264.659 7 -4 -3 -1 9654.08 296.442 8 -4 -3 -1 9538.64 303.716 3 4 3 1 8983.91 296.807 1 -4 -3 -2 16135.6 418.505 8 -4 -3 -2 16213.3 435.424 3 4 3 2 15289.7 383.194 7 4 3 2 15979.7 431.141 1 -4 -3 -3 26092.6 589.040 8 -4 -3 -3 27633.8 632.209 3 4 3 3 25142.7 602.259 1 -4 -3 -4 3638.89 186.427 8 4 3 4 3513.21 194.720 1 4 3 5 359.377 75.3162 1 -4 -3 -5 427.492 70.3584 8 -4 -3 -6 1127.26 114.312 8 4 3 6 1125.58 125.038 1 4 3 7 2613.23 197.937 1 -4 -3 -7 2075.97 158.094 8 4 3 8 21.8975 65.5636 1 -4 -3 -8 26.6343 47.3412 8 4 3 9 6881.62 359.232 1 -4 -3 -9 7014.72 318.590 8 4 3 10 2177.10 209.949 1 -4 -3 -10 2129.52 182.244 8 -4 -3 -11 1226.62 149.638 8 4 3 11 1570.15 190.389 1 -4 -3 -12 85.9869 77.8210 8 4 3 12 316.016 112.251 1 4 3 13 16.7927 72.2775 1 -4 -3 -13 76.3081 69.3953 8 4 4 -16 250.078 90.1745 2 4 4 -15 512.409 117.876 5 4 4 -15 409.546 100.230 2 4 4 -15 544.553 115.646 7 4 4 -14 973.944 143.645 5 4 4 -14 556.408 108.640 2 4 4 -14 620.245 116.032 7 -4 -4 14 903.606 151.124 8 4 4 -13 541.608 109.815 5 -4 -4 13 552.768 117.464 8 4 4 -13 375.671 97.5774 2 4 4 -13 477.111 102.782 7 -4 -4 12 1.44220 60.6333 8 4 4 -12 110.999 75.2778 2 4 4 -12 127.549 63.1587 7 -4 -4 11 138.592 74.3316 8 4 4 -11 62.7417 62.2704 2 4 4 -11 42.5982 51.6042 7 4 4 -10 2396.45 174.567 7 -4 -4 10 2291.79 189.694 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2168.72 165.199 2 -4 -4 -1 1879.46 138.015 8 -4 -4 -1 2101.36 139.759 3 4 4 1 1985.19 112.932 7 4 4 1 1804.29 140.036 1 -4 -4 -2 2543.26 162.416 8 -4 -4 -2 2516.72 161.750 3 4 4 2 2454.19 129.684 7 4 4 2 2373.57 165.853 1 4 4 3-6.79503 46.6813 1 -4 -4 -3 6.19238 40.9528 8 -4 -4 -3-5.89358 47.2063 3 4 4 3-4.83808 32.5271 7 4 4 4-18.9437 55.7351 1 -4 -4 -4 66.4660 50.5692 8 4 4 5 695.206 105.626 1 -4 -4 -5 892.271 105.954 8 -4 -4 -6 1073.62 121.149 8 4 4 6 940.261 125.602 1 -4 -4 -7 2109.18 169.308 8 4 4 7 2313.74 196.772 1 4 4 8 624.802 122.348 1 -4 -4 -8 441.030 90.5491 8 4 4 9 4810.99 307.261 1 -4 -4 -9 4484.42 267.701 8 -4 -4 -10 1232.27 148.872 8 4 4 10 1542.31 188.650 1 -4 -4 -11 392.555 100.602 8 4 4 11 407.090 116.601 1 -4 -4 -12 122.161 91.5931 8 4 4 12 56.7233 87.2712 1 4 5 -15 513.418 124.822 2 -4 -5 14 119.434 77.1841 8 4 5 -14 41.0207 65.3917 2 4 5 -14 13.4259 57.7576 7 -4 -5 13 996.039 150.298 8 4 5 -13 913.527 145.539 2 4 5 -13 823.334 126.526 7 -4 -5 12 639.967 120.367 8 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152.854 1 -4 -5 -10 762.637 129.626 8 4 6 -14-3.07209 67.0719 2 4 6 -14 6.57170 52.5007 7 -4 -6 13 864.395 145.663 8 4 6 -13 737.803 141.737 2 4 6 -13 569.748 109.632 7 4 6 -12 353.937 109.159 2 4 6 -12 234.410 73.0392 7 -4 -6 12 346.133 95.1911 8 -4 -6 11 2221.05 204.336 8 4 6 -11 1752.81 162.481 7 4 6 -11 2306.72 220.855 2 -4 -6 10 2158.01 195.678 8 4 6 -10 2211.34 171.675 7 4 6 -10 2249.58 212.832 2 -4 -6 9 483.675 103.588 8 4 6 -9 614.045 124.880 2 4 6 -9 418.114 80.8457 7 -4 -6 8 586.612 107.053 8 4 6 -8 464.184 104.319 2 4 6 -8 402.560 75.9472 7 -4 -6 7 419.714 88.9650 8 4 6 -7 240.722 88.1245 2 4 6 -7 290.382 59.9220 7 -4 -6 6 2908.05 205.825 8 4 6 -6 2713.94 154.446 7 4 6 -6 2962.06 230.185 2 -4 -6 5 5555.57 283.148 8 4 6 -5 5135.69 205.051 7 4 6 -5 5151.84 296.146 2 -4 -6 4 4863.95 261.653 8 4 6 -4 4339.01 176.264 7 4 6 -4 4584.99 273.663 2 -4 -6 3 1241.36 134.390 8 -4 -6 3 1186.70 88.3582 3 4 6 -3 1374.40 90.7923 7 4 6 -3 1390.43 151.676 2 -4 -6 2 2699.32 192.199 8 4 6 -2 2403.29 115.541 7 -4 -6 2 2625.49 136.962 3 4 6 -2 2632.38 202.065 2 -4 -6 1 8.97359 56.8341 8 -4 -6 1 263.385 53.1426 3 4 6 -1 392.646 86.3910 2 4 6 -1 260.908 78.7280 1 -4 -6 0 61.4167 52.2427 8 -4 -6 0 23.8350 33.3988 3 4 6 0 127.972 66.1200 2 4 6 0 9.07487 50.2600 1 -4 -6 -1 2060.92 149.975 3 -4 -6 -1 2028.96 167.652 8 4 6 1 1835.97 165.571 1 4 6 1 1797.32 164.638 2 -4 -6 -2 2440.56 186.859 8 -4 -6 -2 2705.28 179.347 3 4 6 2 2338.02 191.123 1 4 6 2 2288.38 180.873 2 -4 -6 -3 1707.98 160.398 8 -4 -6 -3 1837.80 156.902 3 4 6 3 1721.49 168.679 1 4 6 3 1712.65 158.191 2 4 6 4 1130.65 147.674 1 -4 -6 -4 977.345 127.315 8 -4 -6 -4 996.607 127.716 3 4 6 4 868.043 116.564 2 -4 -6 -5 1735.33 166.510 8 -4 -6 -5 1769.36 171.335 3 4 6 5 1679.79 179.964 1 4 6 6 202.194 85.4923 1 -4 -6 -6 488.051 100.337 8 4 6 7 112.644 85.5095 1 -4 -6 -7 138.112 73.7383 8 -4 -6 -8 721.984 121.895 8 4 6 8 682.729 134.193 1 4 6 9 770.666 150.863 1 -4 -6 -9 674.480 129.911 8 4 7 -14 127.175 66.6113 7 4 7 -13 175.796 76.2946 7 4 7 -12 522.188 123.814 2 -4 -7 12 396.938 115.596 8 4 7 -12 284.980 76.6985 7 4 7 -11 1185.80 173.686 2 4 7 -11 1375.53 142.339 7 -4 -7 11 1368.44 168.923 8 -4 -7 10 315.843 99.2990 8 4 7 -10 332.335 104.171 2 4 7 -10 316.715 77.6704 7 4 7 -9 46.4288 63.7611 2 -4 -7 9-31.9445 58.7655 8 4 7 -9 130.517 56.8511 7 -4 -7 8 741.113 125.005 8 4 7 -8 1031.90 157.625 2 -4 -7 7 2306.16 200.678 8 4 7 -7 2157.51 208.467 2 -4 -7 6 2815.40 220.161 8 4 7 -6 2464.85 222.752 2 -4 -7 5 1645.74 166.059 8 4 7 -5 1336.92 162.854 2 -4 -7 4 3468.39 236.510 8 4 7 -4 3656.00 256.662 2 -4 -7 3 4164.40 258.897 8 4 7 -3 4106.87 268.905 2 -4 -7 2 2899.91 212.873 8 4 7 -2 2182.75 195.894 2 -4 -7 1-22.4259 62.1718 8 4 7 -1 19.2490 59.0334 2 4 7 -1-33.4612 65.5483 1 -4 -7 0 843.870 121.624 8 4 7 0 837.940 120.794 2 4 7 0 798.974 121.649 1 4 7 1 15.2145 55.7419 2 -4 -7 -1 62.6227 44.1901 3 -4 -7 -1-10.5351 56.8907 8 4 7 1 100.625 76.2028 1 -4 -7 -2 765.577 117.996 8 4 7 2 812.124 114.361 2 -4 -7 -2 814.939 107.543 3 4 7 2 645.799 118.705 1 -4 -7 -3 1272.48 153.284 8 -4 -7 -3 1484.68 144.987 3 4 7 3 1409.22 146.645 2 4 7 3 1326.27 162.494 1 4 7 4 249.100 91.6260 1 -4 -7 -4 384.660 91.7261 8 -4 -7 -4 308.961 82.4218 3 4 7 5 167.393 81.4686 1 -4 -7 -5 368.684 92.0280 8 -4 -7 -5 254.355 82.6441 3 4 7 6 66.6393 80.7425 1 -4 -7 -6 226.951 85.9369 8 -4 -7 -6 102.321 54.4830 3 4 7 7 147.417 84.7618 1 -4 -7 -7 154.420 80.2368 8 -4 -8 10-19.0750 65.2153 8 4 8 -10 120.965 75.6371 2 -4 -8 9 252.492 86.8537 8 4 8 -9 21.6720 62.0165 2 4 8 -8 1570.09 197.074 2 -4 -8 8 1564.51 180.784 8 -4 -8 7 1425.27 170.349 8 4 8 -7 1076.38 166.020 2 -4 -8 6 361.625 96.1293 8 4 8 -6 123.795 80.6201 2 -4 -8 5 468.252 106.397 8 4 8 -5 427.979 111.965 2 -4 -8 4 902.151 134.394 8 4 8 -4 889.147 148.024 2 -4 -8 3 24.9097 62.5223 8 4 8 -3 71.9415 73.7685 2 -4 -8 2 595.347 114.808 8 4 8 -2 450.172 107.422 2 -4 -8 1 382.992 96.7035 8 4 8 -1 444.479 108.836 2 4 8 -1 333.364 96.5603 1 4 8 0 3443.28 254.576 1 -4 -8 0 3707.40 256.907 8 4 8 0 3891.71 262.599 2 -4 -8 -1 4286.61 279.716 8 4 8 1 4673.31 296.434 1 4 8 1 4090.44 266.805 2 4 8 2 859.834 138.358 1 -4 -8 -2 727.760 128.036 8 -4 -8 -3 10.9751 66.8724 8 4 8 3 227.962 97.0334 1 -4 -8 -4 210.951 88.4411 8 4 8 4 140.721 75.5345 1 4 8 5 831.639 149.157 1 -4 -8 -5 559.924 122.573 8 -4 -9 8 389.804 106.671 8 4 9 -8 436.958 118.782 2 -4 -9 7 1012.44 156.114 8 4 9 -7 1044.41 165.658 2 -4 -9 6 626.865 122.067 8 4 9 -6 592.445 129.506 2 -4 -9 5 152.684 87.7541 8 4 9 -5 89.5418 75.0292 2 -4 -9 4 259.153 99.3878 8 4 9 -4 179.449 86.5148 2 -4 -9 3 112.214 74.6907 8 4 9 -3-5.21235 61.0177 2 4 9 -2 533.542 137.271 2 -4 -9 2 549.251 118.492 8 4 9 -1 300.972 95.5527 2 -4 -9 1 166.732 84.0566 8 4 9 -1-37.6388 67.1440 1 -4 -9 0 458.913 103.077 8 4 9 0 439.211 106.103 2 4 9 0 448.200 113.083 1 -4 -9 -1 979.818 145.084 8 4 9 1 887.225 150.232 1 4 9 2 573.803 120.495 1 4 10 -4 440.197 113.513 2 4 10 -3 371.142 117.051 2 4 10 -2 285.891 100.729 2 5 -13 1 856.282 138.765 8 -5 13 -1 988.756 155.073 1 5 -13 2 1072.47 151.810 8 -5 13 -2 981.631 146.979 1 5 -13 3 359.382 95.6475 8 -5 13 -5 208.709 67.6101 2 -5 13 -6 94.2681 66.0720 2 5 -12 -3 199.771 88.6287 8 5 -12 -2 835.635 139.059 8 -5 12 2 680.999 134.098 1 5 -12 -1 935.175 139.347 8 -5 12 1 1112.62 155.593 1 -5 12 0 1007.44 162.558 4 5 -12 0 809.325 131.951 8 -5 12 0 884.336 138.069 1 -5 12 -1 384.860 115.664 4 5 -12 1 470.118 102.749 8 -5 12 -1 529.250 108.726 1 -5 12 -2 467.486 119.778 4 5 -12 2 309.948 87.6909 8 -5 12 -2 269.625 85.6539 1 -5 12 -3-30.8177 68.2301 4 5 -12 3-62.8810 41.4552 8 -5 12 -4 2.42489 46.5725 2 -5 12 -4 119.720 84.1141 4 5 -12 4 182.299 73.2940 8 -5 12 -5 194.452 76.0004 2 5 -12 5 95.8322 58.3892 8 -5 12 -6 786.187 128.763 2 -5 12 -7 324.083 98.0695 2 -5 12 -8 284.362 89.3552 2 -5 11 5 214.042 89.9298 1 5 -11 -5 280.913 92.3827 8 -5 11 4 283.381 96.4123 1 5 -11 -4 357.043 93.1040 8 -5 11 3 1016.16 154.156 1 -5 11 3 797.943 147.283 4 5 -11 -3 756.600 133.678 8 -5 11 2 1040.75 148.555 1 -5 11 2 1127.08 170.398 4 5 -11 -2 992.538 138.142 8 -5 11 1 857.728 145.932 4 5 -11 -1 684.981 114.894 8 -5 11 1 767.420 124.492 1 -5 11 0 237.116 96.0340 4 5 -11 0 67.3630 57.4831 8 -5 11 0 149.580 74.7728 1 -5 11 -1 81.6064 75.9224 4 5 -11 1 176.565 70.7594 8 -5 11 -1 192.680 71.2721 1 -5 11 -2 407.681 81.5559 2 -5 11 -2 216.585 84.0159 4 5 -11 2 448.182 88.9669 8 -5 11 -2 402.994 87.6875 1 -5 11 -3 61.9828 52.6701 2 -5 11 -3 1.00894 62.4325 4 5 -11 3 56.3176 59.6087 8 -5 11 -4 343.502 92.9014 2 -5 11 -4 260.049 86.3804 4 5 -11 4 273.374 75.8063 8 -5 11 -5 519.093 101.384 2 5 -11 5 500.768 95.0558 8 5 -11 6 1542.34 154.468 8 -5 11 -6 1276.22 153.994 2 -5 11 -7 1276.55 154.452 2 5 -11 7 1412.05 149.400 8 -5 11 -8 308.160 92.0002 2 -5 11 -9-207.491 79.5991 2 -5 11 -10 158.021 76.0822 2 5 -10 -7 193.453 88.0115 8 -5 10 7 202.078 93.5075 1 -5 10 6 497.406 120.977 1 5 -10 -6 440.940 111.744 8 -5 10 5 792.161 136.615 1 5 -10 -5 827.412 135.806 8 -5 10 4 1632.06 191.026 4 5 -10 -4 1342.51 156.461 8 -5 10 4 1657.60 179.179 1 -5 10 3 2455.74 232.311 4 5 -10 -3 2403.66 197.900 8 -5 10 3 2188.09 199.858 1 -5 10 2 2234.24 212.875 4 5 -10 -2 2057.22 179.778 8 -5 10 2 2099.30 192.307 1 -5 10 1 1673.69 185.520 4 5 -10 -1 1839.08 164.011 8 -5 10 1 1726.49 166.066 1 -5 10 0 347.849 98.0173 4 5 -10 0 509.377 95.4138 8 -5 10 0 519.768 96.0358 1 -5 10 -1 135.892 47.1392 2 -5 10 -1 11.9756 75.0964 4 5 -10 1 116.975 56.0826 8 -5 10 -1 119.364 62.4961 1 -5 10 -2 26.2965 45.8160 2 -5 10 -2 100.526 68.7245 4 5 -10 2-88.7698 52.9617 8 -5 10 -2 58.2304 44.4735 1 -5 10 -3-47.3302 52.7955 2 -5 10 -3 59.2780 63.8645 4 5 -10 3 72.1444 56.8386 8 -5 10 -4 21.2346 57.5635 2 -5 10 -4 44.7161 67.7622 4 5 -10 4-45.8341 54.6953 8 5 -10 5 1895.91 157.820 8 -5 10 -5 1816.56 168.662 2 5 -10 6 2789.42 188.953 8 -5 10 -6 2418.39 200.341 2 5 -10 7 3091.22 200.648 8 -5 10 -7 2699.22 217.913 2 5 -10 8 1613.48 148.780 8 -5 10 -8 1466.09 166.961 2 -5 10 -9 1179.48 158.736 2 5 -10 9 1164.26 127.593 8 -5 10 -10 711.320 128.110 2 -5 10 -11 183.514 77.1340 2 -5 9 8 149.314 86.5953 1 5 -9 -8 80.7352 70.7336 8 -5 9 7-30.0471 64.3291 1 5 -9 -7-0.30405 61.3455 8 5 -9 -6 131.644 78.9269 8 -5 9 6 159.564 88.1412 1 -5 9 5 686.340 124.658 1 5 -9 -5 749.809 121.281 8 -5 9 4 493.234 103.320 1 5 -9 -4 447.114 96.9094 8 -5 9 3 972.943 142.693 4 -5 9 3 853.436 124.146 1 5 -9 -3 1012.24 121.437 8 -5 9 2 553.126 112.716 4 -5 9 2 565.568 99.5465 1 5 -9 -2 541.466 88.5275 8 -5 9 1 48.6572 52.9883 1 -5 9 1 25.4129 37.8940 2 -5 9 1 39.9783 58.8329 4 5 -9 -1-31.7941 47.3399 8 -5 9 0 36.7179 40.2479 2 -5 9 0 55.8392 55.0913 4 5 -9 0 84.4588 48.8581 8 -5 9 0 82.6130 54.4773 1 -5 9 -1 1774.30 175.747 4 5 -9 1 1789.12 122.434 7 -5 9 -1 1923.60 148.397 2 -5 9 -1 1719.96 140.798 1 5 -9 1 1689.19 139.951 8 -5 9 -2 6473.94 337.999 4 -5 9 -2 6619.60 288.876 2 5 -9 2 6574.20 245.555 7 -5 9 -2 6365.41 269.065 1 5 -9 2 6563.98 272.145 8 -5 9 -3 10111.0 430.762 4 5 -9 3 10698.7 338.896 7 -5 9 -3 10814.8 390.019 2 5 -9 3 10695.6 359.325 8 -5 9 -4 3723.54 259.036 4 5 -9 4 3978.79 208.742 8 5 -9 4 3835.39 201.734 7 -5 9 -4 4087.43 238.702 2 5 -9 5 1911.69 144.155 8 -5 9 -5 2016.43 171.347 2 -5 9 -6-12.8595 53.5018 2 5 -9 6 155.049 51.5378 8 -5 9 -7 23.2176 55.5681 2 5 -9 7 87.0460 46.2173 8 5 -9 8 272.509 65.1339 8 -5 9 -8 301.697 84.0827 2 -5 9 -9 1096.18 147.221 2 5 -9 9 1215.29 125.319 8 5 -9 10 2254.83 169.356 8 -5 9 -10 2687.83 224.705 2 -5 9 -11 1567.46 179.001 2 -5 9 -12 1449.23 178.291 2 5 -8 -10 364.279 106.221 8 -5 8 10 154.535 89.6051 1 5 -8 -9 921.590 143.253 8 -5 8 9 726.676 150.248 1 -5 8 8 967.354 156.134 1 5 -8 -8 1097.32 150.475 8 -5 8 7 2094.59 208.877 1 5 -8 -7 2320.64 202.173 8 5 -8 -6 992.010 135.093 8 -5 8 6 824.604 132.577 1 -5 8 5 85.6412 63.8517 1 5 -8 -5 15.5028 58.4292 8 5 -8 -5-8.69659 41.2008 7 -5 8 4 957.067 126.284 1 5 -8 -4 943.702 117.185 8 5 -8 -4 930.044 95.1241 7 5 -8 -3 745.905 101.369 8 5 -8 -3 754.691 84.3013 7 -5 8 3 639.098 101.070 1 -5 8 2 460.102 60.6108 2 -5 8 2 363.063 85.6020 4 -5 8 2 410.087 83.0710 1 5 -8 -2 320.238 71.5705 8 5 -8 -2 433.201 64.0193 7 -5 8 1 44.6503 36.9430 2 -5 8 1-39.7627 47.0687 1 -5 8 1-16.6512 47.8717 4 5 -8 -1 31.5286 42.1534 8 5 -8 -1-6.98583 37.4878 7 -5 8 0 2943.26 213.701 4 5 -8 0 3171.56 177.077 8 5 -8 0 3120.89 163.231 7 -5 8 0 3245.40 176.589 2 -5 8 0 3208.92 183.624 1 -5 8 -1 9568.22 395.299 4 5 -8 1 10085.6 326.792 8 5 -8 1 9847.40 312.215 7 -5 8 -1 10434.8 346.039 2 -5 8 -1 9934.68 326.284 1 -5 8 -2 4172.70 256.396 4 5 -8 2 4298.36 197.884 8 5 -8 2 4226.19 199.461 7 -5 8 -2 4624.18 228.496 2 -5 8 -2 4177.20 196.648 1 -5 8 -3 1917.44 173.271 4 -5 8 -3 1812.08 120.312 3 5 -8 3 1866.23 128.872 8 5 -8 3 1727.89 130.278 7 -5 8 -3 1966.75 155.424 2 -5 8 -4 1128.16 93.4634 3 5 -8 4 1050.38 99.7656 8 -5 8 -4 1255.47 128.547 2 -5 8 -4 1054.45 135.702 4 -5 8 -5 3073.15 153.826 3 5 -8 5 3093.41 164.759 8 -5 8 -5 3136.99 208.614 2 -5 8 -6 6009.91 220.706 3 5 -8 6 5795.23 234.294 8 -5 8 -6 6168.39 299.937 2 5 -8 7 2162.64 142.991 8 -5 8 -7 2576.46 142.853 3 -5 8 -7 2302.06 190.011 2 -5 8 -8 550.315 101.713 2 -5 8 -8 750.127 81.7670 3 5 -8 8 490.319 73.0790 8 -5 8 -9 854.344 124.931 2 5 -8 9 653.087 88.7076 8 -5 8 -10 252.404 84.0087 2 5 -8 10 208.504 64.8527 8 -5 8 -11 350.077 95.4016 2 5 -8 11 165.766 62.6319 8 -5 8 -12 573.829 117.731 2 -5 8 -13 1869.07 203.052 2 -5 7 11 53.8548 82.0958 1 -5 7 10 1487.62 194.265 1 -5 7 9 1809.75 203.650 1 5 -7 -9 2056.18 194.972 8 5 -7 -9 1981.49 166.156 7 -5 7 8 3112.82 249.494 1 5 -7 -8 2821.27 217.939 8 5 -7 -8 2915.69 194.315 7 -5 7 7 2992.83 231.366 1 5 -7 -7 2690.50 210.440 8 5 -7 -7 2859.95 183.741 7 5 -7 -6 1030.54 127.839 8 5 -7 -6 919.560 102.919 7 -5 7 6 947.150 131.348 1 5 -7 -5-36.7067 50.3788 8 -5 7 5 51.8489 57.7499 1 5 -7 -5-15.6582 42.7913 7 5 -7 -4 97.5402 54.4422 8 5 -7 -4 82.3276 43.6317 7 5 -7 -3 2828.35 172.077 8 5 -7 -3 2636.41 155.995 7 -5 7 3 2592.30 176.792 1 -5 7 2 7745.75 339.692 4 5 -7 -2 7681.88 286.119 8 5 -7 -2 8293.40 280.098 7 -5 7 2 8102.15 249.933 2 -5 7 2 7868.55 300.308 1 -5 7 1 7075.47 319.918 4 5 -7 -1 7714.27 270.000 8 5 -7 -1 7638.12 269.396 7 -5 7 1 7555.37 251.858 2 -5 7 1 7382.29 275.443 1 -5 7 0 5667.61 279.769 4 5 -7 0 5916.25 224.801 8 5 -7 0 5494.87 225.922 7 -5 7 0 5825.88 230.354 2 -5 7 0 5812.91 229.086 1 -5 7 -1 3449.63 219.569 4 5 -7 1 3635.77 166.634 8 5 -7 1 3286.03 173.221 7 -5 7 -1 3531.11 183.015 2 -5 7 -1 3463.71 164.281 1 -5 7 -2 25.5926 38.8163 2 -5 7 -2-5.83272 50.0638 4 5 -7 2 51.0126 31.0840 8 -5 7 -2-2.17977 32.3941 3 -5 7 -2 26.7698 32.5668 1 5 -7 2-15.6150 37.4251 7 -5 7 -3 719.159 92.6472 2 -5 7 -3 587.762 97.1946 4 -5 7 -3 596.373 73.7125 3 5 -7 3 716.536 71.8918 8 5 -7 3 626.161 80.6210 7 -5 7 -4 304.561 69.1550 2 5 -7 4 284.104 48.2277 8 -5 7 -4 248.682 52.3974 3 -5 7 -5 27.3499 51.0508 2 5 -7 5 58.7960 32.9846 8 -5 7 -5 29.0358 31.3108 3 -5 7 -6 5773.28 224.586 3 -5 7 -6 5802.96 284.912 2 5 -7 6 5847.02 215.444 8 5 -7 7 6479.50 237.054 8 -5 7 -7 6936.79 256.480 3 -5 7 -7 7150.58 322.634 2 5 -7 8 4407.99 200.290 8 -5 7 -8 4644.95 214.377 3 -5 7 -8 4506.21 260.662 2 5 -7 9 1438.22 122.811 8 -5 7 -9 1747.47 134.460 3 -5 7 -9 1474.28 161.969 2 -5 7 -10 536.797 107.323 2 5 -7 10 321.160 72.5592 8 -5 7 -10 417.170 75.9940 3 -5 7 -11 157.979 64.5550 5 -5 7 -11 169.527 82.2617 2 5 -7 11 183.779 61.0106 8 -5 7 -11 145.433 55.3167 3 -5 7 -12 549.462 109.704 5 -5 7 -12 675.668 121.685 2 -5 7 -12 614.716 93.6640 3 -5 7 -13 1915.62 198.784 2 -5 7 -13 2253.31 202.842 5 -5 7 -14 1654.21 190.823 2 -5 7 -14 1603.44 181.994 5 -5 7 -15 1285.54 170.476 5 -5 6 13 122.875 81.1908 6 5 -6 -12 681.355 123.266 7 -5 6 12 671.569 126.131 6 -5 6 12 773.793 160.263 1 -5 6 11 2391.92 243.423 1 5 -6 -11 2010.57 182.221 7 -5 6 11 2266.99 214.802 6 -5 6 10 2810.74 252.637 1 5 -6 -10 2595.00 198.159 7 -5 6 10 2687.64 225.271 6 5 -6 -9 1332.80 141.424 7 -5 6 9 1398.45 161.913 6 -5 6 9 1222.60 161.450 1 5 -6 -8 488.897 85.6274 7 -5 6 8 362.217 94.4439 1 -5 6 8 467.673 103.764 6 5 -6 -7 179.190 57.0997 7 -5 6 7 120.924 66.9594 1 -5 6 7 281.013 81.2902 6 5 -6 -6 31.4018 39.9593 7 -5 6 6 72.9352 67.2620 1 -5 6 6 2.98771 53.8590 6 5 -6 -5 323.805 74.1704 8 -5 6 5 276.170 75.9606 1 5 -6 -5 350.612 65.5560 7 -5 6 5 333.929 81.1296 6 -5 6 4 8609.10 327.058 1 5 -6 -4 8763.12 310.458 8 5 -6 -4 8848.87 306.571 7 -5 6 3 19342.1 506.738 1 5 -6 -3 18935.7 481.366 8 5 -6 -3 20067.7 490.423 7 -5 6 2 12787.3 422.677 4 5 -6 -2 12724.4 355.423 8 5 -6 -2 13118.7 371.342 7 -5 6 2 13103.7 375.471 1 -5 6 1 4792.35 246.057 4 5 -6 -1 5134.48 197.776 8 5 -6 -1 5074.54 216.152 7 -5 6 1 5325.48 202.127 2 -5 6 1 5146.44 206.045 1 -5 6 0 6137.09 275.002 4 -5 6 0 5944.62 236.917 3 5 -6 0 6001.47 205.801 8 5 -6 0 5953.94 235.230 7 -5 6 0 6214.51 227.761 2 -5 6 0 6164.48 212.341 1 -5 6 -1 4387.27 232.218 4 -5 6 -1 4365.02 193.844 3 5 -6 1 4272.02 161.976 8 5 -6 1 4314.35 200.789 7 -5 6 -1 4583.44 200.756 2 -5 6 -1 4154.69 161.002 1 -5 6 -2 1337.04 129.342 4 5 -6 2 1346.86 92.6950 1 -5 6 -2 1407.33 106.116 3 5 -6 2 1370.08 84.5149 8 5 -6 2 1251.12 109.467 7 -5 6 -2 1556.98 120.989 2 -5 6 -2 1419.78 87.7474 1 -5 6 -3 1418.36 137.054 4 5 -6 3 1346.34 82.6008 8 -5 6 -3 1189.77 97.0282 3 -5 6 -3 1277.91 81.9350 8 -5 6 -3 1267.05 116.641 2 5 -6 3 1331.43 90.8495 1 -5 6 -4 4113.63 183.044 3 -5 6 -4 3830.63 145.555 8 -5 6 -4 4300.47 217.375 2 5 -6 4 3746.19 143.869 8 5 -6 4 4020.78 159.956 1 5 -6 5 7055.56 212.542 8 -5 6 -5 7225.09 255.179 3 -5 6 -5 6881.03 207.235 8 -5 6 -5 7256.07 299.271 2 5 -6 6 1905.38 108.847 8 -5 6 -6 2092.08 136.028 3 -5 6 -6 1797.06 154.357 2 5 -6 7 1243.29 95.0959 8 -5 6 -7 1220.32 110.025 3 -5 6 -7 1344.65 138.955 2 5 -6 8 1196.81 101.341 8 -5 6 -8 1331.49 117.445 3 -5 6 -8 1396.49 143.340 2 -5 6 -8 1209.23 116.294 5 -5 6 -9-14.1495 42.8398 5 -5 6 -9 23.5987 49.0153 2 5 -6 9-35.9744 39.4366 8 -5 6 -9-10.2218 45.1397 3 -5 6 -10 893.732 112.902 5 -5 6 -10 512.564 100.975 2 5 -6 10 796.797 96.7718 8 -5 6 -10 754.286 99.6380 3 -5 6 -11 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4207.55 151.793 2 -5 5 6 4696.31 249.315 1 5 -5 -6 4955.82 231.584 7 -5 5 6 4667.72 254.459 6 -5 5 5 8412.28 322.792 1 5 -5 -5 8454.57 304.372 7 -5 5 5 8848.89 342.434 6 -5 5 4 17212.1 477.216 1 5 -5 -4 19342.7 487.190 7 5 -5 -4 18736.8 399.442 2 -5 5 4 18343.2 519.162 6 -5 5 3 11070.7 335.691 1 5 -5 -3 11189.7 341.701 7 -5 5 3 11092.7 378.031 6 -5 5 2 730.258 75.3139 1 -5 5 2 751.900 93.7154 4 5 -5 -2 552.126 64.7497 8 5 -5 -2 850.259 88.7098 7 -5 5 1 178.548 42.5244 2 -5 5 1 158.922 54.3112 4 -5 5 1 192.557 41.2653 1 -5 5 1 85.2770 41.3131 3 5 -5 -1 174.259 37.7075 8 5 -5 -1 200.321 52.9370 7 5 -5 -1 236.841 44.3986 1 -5 5 0 2006.06 145.753 4 5 -5 0 1739.83 91.6006 8 5 -5 0 1806.68 100.719 1 -5 5 0 1818.97 115.953 2 5 -5 0 1834.09 126.172 7 -5 5 0 1835.33 126.869 3 -5 5 0 1748.50 93.4645 1 5 -5 1 22.2400 16.3106 5 -5 5 -1 25.9713 33.4534 2 5 -5 1 1.06325 18.6343 1 -5 5 -1 12.2171 43.2951 4 -5 5 -1 20.3353 30.3340 3 5 -5 1 7.48738 17.3214 8 5 -5 1 20.1621 36.1474 7 -5 5 -1 14.6455 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72.9930 5 -5 5 -10 311.695 84.0786 2 5 -5 10 358.456 83.0610 1 -5 5 -10 356.724 83.9034 3 -5 5 -11 3783.70 230.637 3 5 -5 11 3676.40 233.024 1 -5 5 -11 3648.57 241.115 2 -5 5 -11 3225.50 219.467 5 -5 5 -12 4597.33 267.590 3 5 -5 12 4041.37 264.215 1 -5 5 -12 4318.19 271.291 2 -5 5 -12 4560.32 269.818 5 5 -5 13 1576.89 176.271 1 -5 5 -13 1466.11 172.434 2 -5 5 -13 1653.54 175.731 3 -5 5 -13 1450.59 165.744 5 -5 5 -14 121.405 75.8297 5 -5 5 -14 4.56952 67.9146 2 -5 5 -14 189.229 88.7651 3 -5 5 -15 238.105 87.2523 5 -5 5 -15 189.412 91.3566 2 -5 5 -15 354.769 99.6770 3 -5 5 -16 127.163 81.8698 2 -5 5 -16 211.314 89.8842 3 5 -4 -14 1766.16 194.217 7 -5 4 14 2061.32 220.222 6 -5 4 13 2121.16 244.453 1 5 -4 -13 1753.61 184.858 7 -5 4 13 1971.00 210.710 6 -5 4 12 816.425 153.203 1 5 -4 -12 623.753 110.842 7 -5 4 12 927.901 144.793 6 5 -4 -11-40.7908 50.9834 7 -5 4 11 63.6774 73.8179 6 -5 4 10 603.782 125.640 1 5 -4 -10 577.176 101.682 7 -5 4 10 767.488 125.764 6 -5 4 9 209.231 83.8999 1 5 -4 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419.827 7 -5 4 0 15565.0 304.449 1 -5 4 -1 2577.89 159.041 4 -5 4 -1 2750.83 146.705 3 5 -4 1 2627.58 79.4540 8 5 -4 1 2492.26 84.5849 1 -5 4 -1 2731.61 143.471 2 5 -4 1 2619.68 152.562 7 -5 4 -1 2627.45 79.6966 1 5 -4 1 2561.85 83.6231 5 5 -4 2 997.703 47.1456 1 -5 4 -2 1397.54 106.305 3 5 -4 2 1089.55 41.5244 8 -5 4 -2 1358.63 106.397 2 -5 4 -3 43.2015 36.3123 2 5 -4 3 9.68048 8.65065 8 -5 4 -3 18.0500 8.21631 8 -5 4 -3 31.7440 33.6734 3 5 -4 3 5.63531 10.1563 1 -5 4 -4 1060.59 49.1358 8 -5 4 -4 1128.79 101.529 3 5 -4 4 1227.67 55.5672 8 -5 4 -4 1282.47 110.362 2 5 -4 4 1159.79 57.7926 1 -5 4 -5 2141.39 83.6627 8 -5 4 -5 2463.38 149.719 3 -5 4 -5 2185.31 147.837 2 5 -4 5 2260.26 106.192 1 -5 4 -5 2451.62 120.816 5 -5 4 -6 463.154 59.1503 5 -5 4 -6 591.960 84.4714 2 -5 4 -6 556.629 49.5149 8 -5 4 -6 436.267 68.7664 3 5 -4 6 509.485 60.9116 1 -5 4 -7 4625.03 222.856 3 5 -4 7 5066.60 203.126 1 -5 4 -7 4761.40 235.884 2 -5 4 -7 5198.14 174.241 8 -5 4 -8 12932.5 408.377 3 5 -4 8 13207.0 383.283 1 -5 4 -8 12829.2 423.677 2 -5 4 -8 13511.5 392.174 5 -5 4 -9 8877.88 339.899 3 5 -4 9 8635.06 319.734 1 -5 4 -9 8433.94 341.743 2 -5 4 -9 8643.32 321.684 5 -5 4 -10 5151.78 268.246 3 5 -4 10 5322.78 261.575 1 -5 4 -10 5032.31 267.970 2 -5 4 -10 5301.19 260.959 5 5 -4 11 3314.63 217.683 1 -5 4 -11 3075.40 215.373 2 -5 4 -11 2984.06 216.636 3 -5 4 -11 3205.53 213.604 5 -5 4 -12 763.075 117.408 2 5 -4 12 603.936 108.814 1 -5 4 -12 907.767 131.247 3 -5 4 -12 754.957 116.607 5 -5 4 -13 52.5839 63.6332 2 -5 4 -13 19.3330 55.0408 3 5 -4 13-17.3165 64.5804 1 -5 4 -13 32.9387 56.8678 5 -5 4 -14 255.355 88.5143 2 -5 4 -14 358.004 107.583 3 5 -4 14 303.440 99.6325 1 -5 4 -14 234.660 89.0336 5 -5 4 -15 585.578 119.692 2 -5 4 -15 366.404 105.246 3 -5 4 -15 528.828 119.206 5 -5 3 14 369.495 124.838 1 5 -3 -14 671.856 125.658 7 -5 3 14 678.226 137.569 6 -5 3 13 80.2657 87.7431 1 5 -3 -13 122.799 70.6034 7 -5 3 13 178.520 84.4626 6 -5 3 12 427.806 107.374 1 5 -3 -12 437.272 98.4969 7 -5 3 12 489.609 109.795 6 5 -3 -11 1306.27 148.258 7 -5 3 11 1578.57 174.384 6 -5 3 11 1966.19 205.031 1 -5 3 10 4339.23 280.635 1 5 -3 -10 3612.83 228.407 7 -5 3 10 4336.14 270.958 6 -5 3 9 4398.90 272.102 1 5 -3 -9 4221.46 237.241 7 -5 3 9 4940.82 278.846 6 -5 3 8 3140.08 214.223 1 5 -3 -8 2802.10 185.959 7 -5 3 8 3233.10 215.754 6 5 -3 -8 2719.73 137.417 2 5 -3 -7 382.521 58.2079 2 -5 3 7 400.725 87.8856 1 5 -3 -7 436.433 81.0379 7 -5 3 7 532.464 93.1333 6 5 -3 -6 12.6053 29.6663 2 -5 3 6 30.7733 44.5372 1 5 -3 -6 124.966 52.3998 7 -5 3 6 24.0943 52.7770 6 -5 3 5 13.7860 42.4715 1 5 -3 -5 72.8021 43.7708 7 -5 3 5 90.3838 44.7756 6 -5 3 4 204.784 48.0758 1 5 -3 -4 272.245 54.7291 7 -5 3 3 225.634 49.4431 4 -5 3 3 274.106 46.5505 1 5 -3 -3 166.255 36.3803 8 -5 3 3 218.850 55.4598 3 5 -3 -3 276.558 58.1260 7 -5 3 2 1500.07 109.997 4 5 -3 -2 1687.81 87.7499 8 -5 3 2 1519.36 117.333 3 -5 3 2 1464.87 86.3828 1 5 -3 -2 1798.92 126.267 7 -5 3 1 37624.2 748.938 4 -5 3 1 37025.2 626.309 1 5 -3 -1 36766.9 621.721 8 -5 3 1 37974.3 753.963 3 5 -3 -1 39100.0 759.944 7 -5 3 1 38434.6 758.364 6 -5 3 0 8774.59 277.577 4 5 -3 0 7372.63 149.375 8 -5 3 0 8551.48 270.022 3 5 -3 0 7305.04 149.401 8 5 -3 0 8746.41 280.405 7 -5 3 0 8167.17 269.348 6 -5 3 0 6768.17 139.690 1 -5 3 -1 2328.87 136.239 3 5 -3 1 2362.62 145.059 7 -5 3 -2 3995.65 180.702 3 -5 3 -2 3873.48 174.747 2 -5 3 -3 6994.18 254.113 3 -5 3 -3 6761.86 245.687 2 -5 3 -3 6935.94 172.369 5 -5 3 -4 13795.5 374.297 3 5 -3 4 11596.4 238.311 1 -5 3 -4 11090.0 209.763 8 -5 3 -4 13483.7 366.918 2 -5 3 -4 13420.6 287.507 5 -5 3 -5 2454.42 88.1065 8 -5 3 -5 2457.88 151.509 3 5 -3 5 2350.27 104.495 1 -5 3 -5 2210.23 145.469 2 -5 3 -6 2538.42 106.019 8 -5 3 -6 2473.53 158.617 3 5 -3 6 2539.73 126.565 1 -5 3 -6 2668.64 163.864 2 -5 3 -7 13194.8 404.650 3 -5 3 -7 12214.2 303.095 8 5 -3 7 12280.6 344.199 1 -5 3 -7 13095.3 401.313 2 -5 3 -8 6328.42 280.530 3 5 -3 8 6241.65 249.248 1 -5 3 -8 6298.97 272.656 2 -5 3 -9 365.789 77.2737 2 -5 3 -9 335.746 79.2359 3 5 -3 9 309.142 64.7906 1 -5 3 -10 409.685 83.7973 2 -5 3 -10 484.541 95.7170 3 5 -3 10 437.331 84.0168 1 -5 3 -11 709.076 106.391 2 -5 3 -11 773.039 122.607 3 5 -3 11 639.312 109.987 1 -5 3 -12 2158.97 201.848 3 5 -3 12 1890.40 178.572 1 -5 3 -12 1762.48 165.976 2 -5 3 -13 250.900 77.5903 2 5 -3 13 323.649 89.8739 1 -5 3 -14 1154.59 146.841 2 5 -3 14 1302.29 170.367 1 -5 3 -15 816.251 136.998 2 -5 2 15 251.062 100.748 6 5 -2 -14-46.3127 76.8652 7 -5 2 14 141.587 97.8569 1 5 -2 -13 62.0867 51.1807 7 -5 2 13 101.292 92.2221 1 5 -2 -12 1208.76 145.070 7 -5 2 12 1321.23 178.921 1 -5 2 11 1720.40 192.226 1 5 -2 -11 1762.73 167.672 7 -5 2 10 4135.16 271.918 1 5 -2 -10 4262.60 247.271 7 5 -2 -10 4118.03 190.518 2 -5 2 9 1231.50 145.669 1 5 -2 -9 1144.60 126.961 7 5 -2 -9 1056.45 96.2753 2 -5 2 8 3890.97 235.510 1 5 -2 -8 3758.88 215.284 7 5 -2 -8 3843.86 182.400 2 -5 2 7 174.892 61.4899 1 5 -2 -7 167.220 46.5893 2 5 -2 -7 167.336 58.0761 7 -5 2 6-52.0110 47.7421 1 5 -2 -6 36.6777 30.8359 2 5 -2 -6 81.9533 45.9356 7 -5 2 5 11.6138 42.8353 1 5 -2 -5 41.1462 38.4235 7 -5 2 5 80.2827 46.8627 6 -5 2 4 3087.92 155.246 1 5 -2 -4 3194.99 173.994 7 -5 2 4 3465.69 180.617 3 -5 2 3 1932.11 115.836 4 5 -2 -3 2192.78 105.018 8 -5 2 3 2123.99 138.405 3 -5 2 3 2260.99 115.917 1 5 -2 -3 2101.61 137.292 7 -5 2 3 2108.40 138.855 6 5 -2 -3 2219.88 84.8208 5 -5 2 2 8305.91 252.549 4 5 -2 -2 7842.46 197.970 8 -5 2 2 8356.29 278.556 3 -5 2 2 7913.04 207.516 1 5 -2 -2 9011.16 286.929 7 -5 2 2 8517.91 276.856 6 5 -2 -2 6884.78 146.019 5 -5 2 1 4787.13 187.855 4 5 -2 -1 4848.44 126.788 8 -5 2 1 4874.23 202.481 3 -5 2 1 4808.04 128.574 1 5 -2 -1 5042.97 207.630 7 -5 2 1 4683.84 194.772 6 5 -2 0 2485.44 63.8098 8 -5 2 0 3146.26 157.462 3 5 -2 0 3041.84 160.598 7 -5 2 0 3082.29 147.245 6 -5 2 -1 126.286 42.6540 3 5 -2 1 96.2460 41.5140 7 -5 2 -1 74.0353 30.0097 6 -5 2 -2 761.189 84.3173 3 -5 2 -3 6966.22 252.620 3 5 -2 3 6348.78 196.833 6 5 -2 3 5302.19 115.183 1 5 -2 4 42166.2 685.420 1 -5 2 -4 39922.8 657.002 8 -5 2 -4 44660.1 848.415 3 -5 2 -4 46139.5 833.813 2 -5 2 -4 40161.8 656.209 8 5 -2 4 43011.9 746.777 6 -5 2 -5 29398.6 521.415 8 5 -2 5 30540.4 559.704 1 -5 2 -5 30479.2 670.770 3 -5 2 -5 31304.4 658.235 2 5 -2 5 27647.9 558.787 6 5 -2 6 25596.1 530.232 1 -5 2 -6 25773.9 611.876 3 -5 2 -6 25427.7 589.261 2 -5 2 -6 24091.7 481.178 8 5 -2 7 3334.52 167.992 1 -5 2 -7 3449.27 201.288 3 -5 2 -7 3430.22 188.795 2 -5 2 -8 3291.57 207.926 3 -5 2 -8 3221.24 188.816 2 5 -2 8 3252.98 182.757 1 5 -2 9 1981.40 151.027 1 -5 2 -9 1691.33 155.787 3 -5 2 -9 1821.78 147.153 2 5 -2 10 1325.99 139.155 1 -5 2 -10 1691.82 163.725 3 -5 2 -10 1360.29 135.446 2 5 -2 11 4703.23 271.164 1 -5 2 -11 4874.12 257.851 2 5 -2 12 5162.33 299.947 1 -5 2 -12 5101.74 272.162 2 5 -2 13 2448.48 224.259 1 -5 2 -13 2597.63 200.819 2 5 -2 14 1581.00 188.773 1 -5 2 -14 1637.05 164.165 2 5 -1 -15 478.925 109.227 5 -5 1 14 740.799 147.609 1 5 -1 -14 642.037 124.086 7 5 -1 -14 560.700 118.540 5 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610.468 98.5691 8 -5 -5 1 603.135 78.6962 3 5 5 -1 676.739 72.9821 7 5 5 -1 571.074 107.200 2 5 5 -1 404.138 83.9106 1 -5 -5 0 43.0509 54.1485 8 -5 -5 0 95.4819 45.8823 3 5 5 0-0.51688 57.5948 2 5 5 0 44.7691 30.9757 7 5 5 0-16.1194 62.0550 1 -5 -5 -1 3971.92 225.674 8 -5 -5 -1 3894.87 213.848 3 5 5 1 4231.68 180.917 7 5 5 1 3765.37 222.913 1 5 5 1 4014.36 255.606 2 5 5 2 6292.72 320.735 2 -5 -5 -2 5990.97 284.833 8 -5 -5 -2 6454.57 289.850 3 5 5 2 5732.85 287.084 1 5 5 3 2287.95 191.565 2 -5 -5 -3 2019.95 166.733 8 -5 -5 -3 2460.43 185.803 3 5 5 3 2193.60 178.687 1 5 5 4 175.897 69.0493 1 -5 -5 -4 236.705 73.8708 8 -5 -5 -4 254.830 75.6003 3 5 5 4 260.248 80.2501 2 5 5 5 1272.64 147.621 2 5 5 5 1137.92 142.960 1 -5 -5 -5 1300.86 139.163 8 -5 -5 -5 1291.00 151.609 3 -5 -5 -6 2429.01 191.683 8 -5 -5 -6 2413.27 209.656 3 5 5 6 2230.17 198.980 1 5 5 7 126.465 71.9408 1 -5 -5 -7 135.300 71.2438 8 -5 -5 -7 44.3896 66.5816 3 -5 -5 -8 1689.49 170.812 8 -5 -5 -8 1970.15 206.119 3 5 5 8 1796.13 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858.031 156.043 4 -6 12 -3 738.538 146.600 4 -6 12 -4 126.811 57.9351 2 -6 12 -4-92.0038 87.3542 4 -6 12 -5 110.231 67.5326 2 -6 12 -6 356.542 93.8268 2 -6 12 -7 694.055 128.150 2 -6 11 5 431.088 104.556 1 6 -11 -5 124.228 71.0454 8 -6 11 4 191.063 89.4298 1 6 -11 -4 162.951 81.0822 8 -6 11 3 331.875 86.8160 1 -6 11 3 327.332 108.429 4 6 -11 -3 262.918 84.1123 8 -6 11 2 536.015 125.696 4 6 -11 -2 427.036 89.9940 8 -6 11 2 637.666 113.153 1 -6 11 1 959.657 153.363 4 6 -11 -1 991.470 133.173 8 -6 11 1 930.315 132.240 1 -6 11 0 1087.33 166.194 4 6 -11 0 1283.83 140.826 8 -6 11 0 1206.90 142.167 1 -6 11 -1 1930.69 215.035 4 6 -11 1 2198.82 177.493 8 -6 11 -1 1813.91 165.789 1 -6 11 -2 732.539 108.438 2 -6 11 -2 782.380 138.915 4 6 -11 2 868.974 113.987 8 -6 11 -2 591.119 100.470 1 -6 11 -3 114.810 63.6248 2 -6 11 -3 268.347 91.9423 4 -6 11 -4-256.542 80.8828 2 -6 11 -4-227.016 92.7567 4 -6 11 -5 386.990 96.8367 2 -6 11 -6 756.119 125.042 2 -6 11 -7 345.505 89.7114 2 -6 11 -8 330.857 95.0530 2 -6 11 -9 100.590 72.9614 2 -6 10 7 269.232 101.299 1 6 -10 -7 414.141 119.653 8 6 -10 -6-102.099 75.0308 8 -6 10 6-2.33534 76.2797 1 -6 10 5 175.889 86.6993 4 -6 10 5 195.339 93.2695 1 6 -10 -5-67.2213 72.5136 8 -6 10 4 272.923 101.515 4 -6 10 4 183.549 83.5093 1 6 -10 -4 167.641 73.6888 8 -6 10 3 1329.79 175.887 4 -6 10 3 1101.29 143.573 1 6 -10 -3 1045.96 134.230 8 -6 10 2 2061.31 208.627 4 6 -10 -2 1994.29 172.380 8 -6 10 2 1753.59 169.459 1 -6 10 1 3299.16 259.987 4 6 -10 -1 3164.51 210.438 8 -6 10 1 3050.77 211.954 1 -6 10 0 2929.12 249.839 4 6 -10 0 3284.55 207.422 8 -6 10 0 2957.34 201.238 1 -6 10 -1 3022.24 248.012 4 6 -10 1 3155.94 195.626 8 -6 10 -1 2875.07 191.104 2 -6 10 -1 2878.84 190.256 1 -6 10 -2 143.075 66.6948 2 -6 10 -2 124.017 72.6668 4 6 -10 2 102.723 46.7467 8 -6 10 -2 139.294 56.6553 1 -6 10 -3-18.3309 50.3267 2 6 -10 3-8.38744 42.9486 8 -6 10 -3 19.1031 57.5651 4 -6 10 -4-8.19948 70.2744 2 -6 10 -4-13.5629 75.1663 4 6 -10 4 19.9907 42.8457 8 -6 10 -5 426.737 96.5669 2 6 -10 5 500.733 89.2733 7 -6 10 -6 624.128 114.011 2 -6 10 -7 836.996 129.780 2 -6 10 -8 663.823 119.953 2 -6 10 -9 332.287 91.7329 2 -6 10 -10 337.248 105.090 2 6 -9 -9 1004.46 161.319 8 -6 9 8 585.678 142.407 1 6 -9 -8 378.553 102.700 8 -6 9 7 41.9763 75.8134 1 6 -9 -7 222.761 84.3051 8 -6 9 6 39.9655 64.4949 1 6 -9 -6 0.27774 66.1283 8 -6 9 5-8.30695 61.2435 1 6 -9 -5 140.958 65.0617 8 -6 9 4 213.765 91.7419 4 -6 9 4 44.7088 57.3476 1 6 -9 -4 182.313 71.3872 8 -6 9 3 824.253 130.479 4 -6 9 3 719.090 112.767 1 6 -9 -3 761.524 106.230 8 -6 9 2 653.751 119.815 4 -6 9 2 792.529 113.675 1 6 -9 -2 812.957 105.572 8 -6 9 1 41.7032 52.9708 1 -6 9 1 161.682 50.3675 2 -6 9 1 140.676 73.8847 4 6 -9 -1 21.6638 43.1017 8 6 -9 -1 118.475 45.1320 7 -6 9 0 109.690 47.5313 2 -6 9 0 96.9360 67.1705 4 6 -9 0 58.7958 41.5016 8 6 -9 0 88.3811 45.6638 7 -6 9 0-42.2911 53.6121 1 -6 9 -1-9.90146 40.9844 2 -6 9 -1-6.63897 52.0517 4 6 -9 1-10.2906 37.2536 8 6 -9 1 32.6404 36.5803 7 -6 9 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4017.14 176.343 8 6 -8 4 4363.81 235.136 7 -6 8 -4 4621.83 251.830 2 6 -8 5 1829.32 116.490 8 -6 8 -5 1818.16 131.841 3 -6 8 -5 1865.06 172.229 2 -6 8 -6 471.615 94.5073 2 6 -8 6 569.563 67.7966 8 -6 8 -6 592.703 79.9587 3 -6 8 -7 510.763 100.457 2 -6 8 -7 607.395 83.3634 3 -6 8 -8 1595.97 132.006 3 -6 8 -8 1421.97 158.126 2 -6 8 -9 4102.57 217.430 3 -6 8 -9 4228.36 273.681 2 -6 8 -10 3229.93 247.965 2 -6 8 -11 1983.51 199.557 2 -6 8 -12 959.572 147.046 2 -6 8 -13-9.10598 66.4612 2 -6 7 11 118.103 88.2846 1 -6 7 11 11.4281 77.4855 6 6 -7 -10-95.7089 65.5020 7 -6 7 10 190.876 98.3862 1 -6 7 10 103.105 77.2595 6 6 -7 -9 126.016 57.9078 7 -6 7 9 154.149 88.0819 1 -6 7 9 262.061 91.3266 6 6 -7 -8 1626.02 168.671 8 6 -7 -8 1393.25 141.962 7 -6 7 8 1427.06 171.280 1 -6 7 8 1669.43 187.745 6 -6 7 7 3561.84 251.773 1 6 -7 -7 3998.64 249.409 8 6 -7 -7 3733.59 224.582 7 -6 7 6 3237.69 225.783 1 6 -7 -6 2790.10 198.854 8 6 -7 -6 3113.83 198.937 7 6 -7 -5 1139.50 122.333 8 -6 7 5 1114.59 131.358 1 6 -7 -5 1020.60 115.938 7 -6 7 4 1064.08 120.769 1 6 -7 -4 1026.09 111.188 8 6 -7 -4 1165.20 118.492 7 -6 7 3 247.243 82.2048 4 -6 7 3 393.238 74.8065 1 6 -7 -3 497.269 77.3407 8 6 -7 -3 318.744 67.3630 7 -6 7 2 444.018 92.1948 4 -6 7 2 722.908 91.3234 1 6 -7 -2 525.504 75.9651 8 6 -7 -2 680.662 87.9862 7 -6 7 1 4509.70 259.671 4 6 -7 -1 4857.72 200.491 8 -6 7 1 4702.13 204.335 2 6 -7 -1 4757.07 225.792 7 -6 7 1 4570.68 204.296 1 -6 7 0 8192.20 355.350 4 6 -7 0 8841.79 269.640 8 6 -7 0 7939.25 305.540 7 -6 7 0 8200.78 292.422 2 -6 7 0 8494.14 268.530 1 -6 7 -1 3944.01 244.310 4 -6 7 -1 3994.34 203.192 3 6 -7 1 4297.84 215.477 7 -6 7 -1 4059.92 205.494 2 6 -7 1 4260.28 171.321 8 -6 7 -1 4296.52 169.734 1 -6 7 -2 3678.69 234.805 4 -6 7 -2 3726.72 195.936 3 6 -7 2 4255.52 163.259 8 6 -7 2 4092.54 214.992 7 -6 7 -2 4306.93 218.292 2 -6 7 -3 280.740 71.0554 2 -6 7 -3 349.056 91.5391 4 6 -7 3 256.108 42.1607 8 -6 7 -3 242.791 56.7573 3 6 -7 3 183.384 58.6658 7 6 -7 4 1251.91 83.5764 8 -6 7 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3558.40 256.738 1 6 -6 -8 3732.26 230.998 7 -6 6 8 3702.33 262.742 6 -6 6 7 1971.16 183.553 1 6 -6 -7 2012.61 165.232 7 -6 6 7 1972.38 190.441 6 6 -6 -6 193.274 66.5363 7 -6 6 6 87.1484 62.5135 1 -6 6 6 146.064 68.8189 6 -6 6 5 76.9786 50.8260 1 6 -6 -5 99.6858 51.1751 7 -6 6 5 129.450 66.5447 6 6 -6 -4 329.280 66.6322 8 -6 6 4 347.682 70.3044 1 6 -6 -4 314.327 70.8911 7 -6 6 3 1722.18 131.578 1 -6 6 3 1764.72 159.328 4 6 -6 -3 1478.80 116.253 8 6 -6 -3 1424.57 126.569 7 -6 6 2 5263.70 267.280 4 6 -6 -2 5860.18 216.868 8 6 -6 -2 5854.40 254.589 7 -6 6 2 6034.22 230.967 1 -6 6 1 13578.4 449.342 4 -6 6 1 13744.6 415.727 3 6 -6 -1 13717.3 347.146 8 6 -6 -1 14705.1 423.857 7 -6 6 1 13915.6 354.547 1 -6 6 0 12182.3 421.287 4 -6 6 0 11724.7 372.468 3 6 -6 0 12156.4 300.095 8 6 -6 0 12968.6 323.920 1 -6 6 0 11714.3 352.425 2 6 -6 0 11661.5 373.392 7 -6 6 0 11982.2 301.443 1 -6 6 -1 2056.26 169.412 4 -6 6 -1 2325.91 153.034 3 6 -6 1 2238.06 103.746 8 6 -6 1 2015.00 108.931 1 -6 6 -1 2416.23 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32.6216 51.7195 3 -6 6 -12 384.291 94.6445 5 -6 6 -12 183.078 88.2752 2 -6 6 -12 349.236 83.7621 3 -6 6 -13 108.482 73.3116 5 -6 6 -13 329.138 96.9835 2 -6 6 -13 236.494 76.4063 3 -6 6 -14 2301.36 205.960 3 -6 6 -14 2077.98 212.837 2 -6 6 -14 2287.57 211.992 5 -6 6 -15 721.581 128.388 5 -6 6 -15 763.329 131.380 3 6 -5 -13 310.381 99.1413 7 -6 5 13 381.819 114.631 6 -6 5 12 1369.72 199.583 1 6 -5 -12 1380.70 162.625 7 -6 5 12 1399.03 183.867 6 -6 5 11 1988.93 217.929 1 6 -5 -11 1847.61 181.225 7 -6 5 11 2334.94 222.290 6 -6 5 10 553.781 116.784 1 6 -5 -10 522.043 102.925 7 -6 5 10 782.824 134.736 6 -6 5 9-21.9836 67.9036 1 6 -5 -9 40.4068 49.1887 7 -6 5 9 103.185 84.1892 6 -6 5 8 34.8131 64.8492 1 6 -5 -8 66.4718 49.1546 7 -6 5 8 192.570 87.5997 6 -6 5 7 262.469 84.5525 1 6 -5 -7 100.998 56.4361 7 -6 5 7 158.278 75.8535 6 -6 5 6 122.603 64.0662 1 6 -5 -6 114.293 53.4252 7 -6 5 6 252.916 83.5340 6 -6 5 5 1601.62 136.482 1 6 -5 -5 1459.60 136.609 7 -6 5 5 1802.29 160.805 6 -6 5 4 7410.80 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638.306 141.257 2 6 6 -11 477.199 98.1914 7 -6 -6 10 175.672 82.8721 8 6 6 -10 69.7557 75.9858 2 6 6 -10 125.663 55.3399 7 -6 -6 9 104.187 66.3873 8 6 6 -9-101.437 82.2002 2 6 6 -9-0.90564 54.7707 7 -6 -6 8 317.183 96.2093 8 6 6 -8 420.952 117.309 2 6 6 -8 413.507 82.2905 7 -6 -6 7 634.265 116.633 8 6 6 -7 845.655 155.140 2 -6 -6 6 582.312 107.497 8 6 6 -6 637.694 133.724 2 -6 -6 5 695.085 114.988 8 6 6 -5 504.998 123.058 2 -6 -6 4 514.243 98.4993 8 6 6 -4 378.703 103.617 2 -6 -6 3 722.826 118.243 8 6 6 -3 1019.33 150.458 2 -6 -6 2 2062.02 184.763 8 6 6 -2 2010.82 205.904 2 -6 -6 1 501.877 104.382 8 6 6 -1 389.317 108.526 2 -6 -6 0 773.204 118.891 8 6 6 0 786.700 131.448 2 6 6 0 688.678 117.605 1 -6 -6 -1 3719.88 244.378 8 -6 -6 -1 4020.81 235.888 3 6 6 1 3375.18 236.946 1 6 6 1 3383.85 261.918 2 -6 -6 -2 2146.41 188.670 8 -6 -6 -2 2346.74 187.399 3 6 6 2 1871.82 177.678 1 6 6 2 1840.61 195.482 2 -6 -6 -3 105.382 65.1824 8 -6 -6 -3 208.422 73.6901 3 6 6 3 204.525 88.3745 2 6 6 3 220.045 78.7843 1 -6 -6 -4 0.27469 51.2753 8 -6 -6 -4 1.97334 47.5607 3 6 6 4 136.914 77.4233 1 -6 -6 -5 123.572 78.9780 8 -6 -6 -5 11.0188 65.5238 3 6 6 5-97.3030 76.6326 1 6 6 6-5.58187 66.4424 1 -6 -6 -6 10.5881 60.1638 8 -6 -6 -6 17.6762 67.6181 3 6 6 7 143.645 81.3598 1 -6 -6 -7 217.499 75.5826 8 -6 -7 9 582.102 128.140 8 -6 -7 8 560.443 118.703 8 6 7 -8 612.359 141.649 2 -6 -7 7 355.218 101.414 8 6 7 -7 340.892 108.993 2 -6 -7 6 82.0527 67.3004 8 6 7 -6 85.1010 75.8204 2 -6 -7 5 214.530 77.5442 8 6 7 -5 0.73897 67.2229 2 -6 -7 4 18.3455 59.7577 8 6 7 -4 75.5444 63.6838 2 -6 -7 3 99.0855 67.2350 8 6 7 -3 123.652 89.4362 2 -6 -7 2 414.804 97.5957 8 6 7 -2 574.563 129.888 2 -6 -7 1 976.010 143.450 8 6 7 -1 869.773 147.585 2 -6 -7 0 1516.45 171.391 8 6 7 0 1385.66 176.678 2 6 7 0 1617.93 175.180 1 -6 -7 -1 1119.15 150.190 8 6 7 1 1110.32 156.416 2 6 7 1 921.800 137.819 1 -6 -7 -2 19.8029 59.1227 8 6 7 2 12.3299 61.8153 2 6 7 2 49.2944 62.8032 1 -6 -7 -3-135.689 71.2476 8 6 7 3-46.8949 64.4697 1 -6 -7 -4 1389.60 170.348 8 6 7 4 1317.81 170.969 1 6 7 5 2624.53 239.581 1 -6 -8 6-12.4026 63.6390 8 -6 -8 5 88.1931 65.1037 8 6 8 -5 90.7888 77.4933 2 -6 -8 4-15.1388 69.5584 8 6 8 -4 42.5986 74.3351 2 -6 -8 3 183.258 81.3331 8 6 8 -3 147.842 92.1208 2 -6 -8 2 348.957 95.0521 8 6 8 -2 324.486 114.276 2 -6 -8 1 20.7209 69.1431 8 6 8 -1 166.225 91.0701 2 -6 -8 0 462.414 119.893 8 6 8 0 295.809 101.540 2 6 8 1 45.0000 74.3339 2 6 8 1 299.943 102.227 1 -7 12 -4 616.582 115.508 2 -7 12 -5 784.618 134.254 2 -7 12 -6 491.815 114.236 2 -7 11 2 358.773 108.794 4 -7 11 1 227.111 91.9906 4 -7 11 0 288.013 103.840 4 -7 11 -1 232.829 86.1080 4 -7 11 -2 769.240 114.743 2 -7 11 -2 686.442 139.760 4 -7 11 -3 1581.75 200.381 4 -7 11 -3 1973.46 179.508 2 -7 11 -4 1293.23 155.106 2 -7 11 -5 941.136 144.754 2 -7 11 -6 298.515 99.1373 2 -7 11 -7 164.408 81.0899 2 -7 11 -8 3.73628 62.2469 2 -7 10 7 1039.13 153.385 1 7 -10 -7 1283.77 168.466 8 -7 10 6 608.327 127.105 1 7 -10 -6 453.963 109.664 8 -7 10 5 338.636 95.3603 1 7 -10 -5 201.232 75.8852 8 -7 10 4-1.10753 68.4198 4 -7 10 4 42.3228 60.0351 1 -7 10 3 70.1393 61.9535 4 -7 10 2 181.056 95.0431 4 -7 10 1 365.376 106.894 4 -7 10 0 1669.06 198.149 4 -7 10 -1 1590.54 190.633 4 -7 10 -1 1514.11 143.859 2 -7 10 -2 1263.14 172.724 4 -7 10 -2 1330.76 141.098 2 -7 10 -3 845.329 122.395 2 -7 10 -3 776.116 140.358 4 -7 10 -4 578.485 105.613 2 7 -10 4 681.440 104.993 7 -7 10 -5 776.923 128.356 2 7 -10 5 629.382 106.277 7 -7 10 -6 1274.63 158.560 2 7 -10 6 1098.59 140.720 7 -7 10 -7 423.102 104.986 2 -7 10 -8 244.456 86.2980 2 -7 10 -9-10.0625 67.7399 2 -7 9 8 2367.20 229.369 1 7 -9 -8 2137.92 219.456 8 -7 9 7 914.753 148.578 1 7 -9 -7 1103.20 152.542 8 -7 9 6 426.811 116.838 4 -7 9 6 205.800 83.1649 1 7 -9 -6 144.831 70.3223 8 -7 9 5 67.2951 78.5064 4 -7 9 5 7.45321 54.8545 1 7 -9 -5 91.6853 58.7845 8 -7 9 4 379.187 109.338 4 -7 9 4 330.298 87.4316 1 7 -9 -4 239.575 77.4417 8 -7 9 3 858.648 139.159 4 -7 9 3 945.653 119.600 1 7 -9 -3 933.177 112.842 8 7 -9 -3 1002.15 116.771 7 -7 9 2 1755.36 190.131 4 7 -9 -2 1938.43 152.476 8 7 -9 -2 1568.21 141.509 7 -7 9 2 1682.03 148.307 1 -7 9 1 894.643 137.514 4 7 -9 -1 1139.25 112.472 8 -7 9 1 1407.43 125.530 2 7 -9 -1 1133.96 119.789 7 -7 9 1 1023.81 113.077 1 -7 9 0 491.292 82.9795 2 -7 9 0 594.441 119.082 4 7 -9 0 459.359 84.1866 7 -7 9 -1-13.3484 42.8802 2 -7 9 -1 83.8426 73.7482 4 7 -9 1 78.3734 48.9030 7 -7 9 -2 387.014 81.7681 2 -7 9 -2 334.520 92.2334 4 7 -9 2 232.078 65.7948 7 -7 9 -3 181.754 71.4818 2 -7 9 -3 243.534 89.2340 4 -7 9 -3 274.559 63.4194 3 7 -9 3 285.831 72.2393 7 -7 9 -4 133.039 63.4735 2 -7 9 -4 76.9301 41.2719 3 7 -9 4 175.339 67.4630 7 -7 9 -5 970.727 130.854 2 -7 9 -5 749.758 95.4029 3 7 -9 5 927.860 125.562 7 -7 9 -6 3305.83 195.197 3 -7 9 -6 3806.50 259.190 2 -7 9 -7 2548.39 215.628 2 -7 9 -8 1234.69 155.908 2 -7 9 -9 1094.06 159.824 2 -7 9 -10 880.151 154.676 2 -7 9 -11 739.037 135.217 2 7 -8 -10 1686.46 196.166 8 -7 8 10 1413.42 205.554 1 7 -8 -9 1057.53 155.876 8 -7 8 9 1223.61 181.219 1 7 -8 -8 1348.96 165.182 8 -7 8 8 1411.97 175.761 1 7 -8 -7 101.805 72.1881 8 -7 8 7-27.4990 56.0000 1 7 -8 -7 177.190 64.3295 7 -7 8 6 152.419 78.0829 4 7 -8 -6 183.513 75.8669 8 -7 8 6 245.580 79.5666 1 7 -8 -6 91.4405 56.6567 7 -7 8 5 561.611 118.204 4 -7 8 5 435.909 97.2086 1 7 -8 -5 459.085 91.9365 8 7 -8 -5 347.107 79.6771 7 -7 8 4 2990.84 244.760 4 7 -8 -4 2894.69 191.586 8 7 -8 -4 3185.37 209.779 7 -7 8 4 2915.64 198.584 1 -7 8 3 4943.73 305.369 4 7 -8 -3 5478.50 252.966 8 7 -8 -3 5398.33 267.145 7 -7 8 3 5398.72 259.215 1 -7 8 2 4623.75 293.116 4 7 -8 -2 5226.26 231.205 8 7 -8 -2 5335.64 261.717 7 -7 8 2 5623.17 249.585 1 -7 8 1 2482.26 214.698 4 7 -8 -1 2948.49 163.985 8 7 -8 -1 2669.62 183.654 7 -7 8 1 2868.81 166.675 1 -7 8 0 219.213 60.6986 2 -7 8 0 142.805 66.0233 4 7 -8 0 158.652 41.3440 8 7 -8 0 102.673 50.6492 7 -7 8 0 173.493 47.8594 1 -7 8 -1 459.317 84.7044 2 -7 8 -1 263.320 83.6448 4 -7 8 -1 347.820 76.0906 3 7 -8 1 334.313 70.9814 7 -7 8 -2 180.277 67.4545 2 -7 8 -2 75.2076 63.7925 4 -7 8 -2 54.3449 44.2334 3 7 -8 2 174.335 60.2895 7 -7 8 -3 38.8865 49.7780 2 -7 8 -3 90.1121 52.8440 3 7 -8 3 11.2907 44.3866 7 -7 8 -4 2205.19 159.327 3 -7 8 -4 2133.65 181.646 2 7 -8 4 2173.67 179.250 7 -7 8 -5 1000.17 130.762 2 -7 8 -5 1064.15 113.934 3 -7 8 -6 475.690 100.406 2 -7 8 -6 466.119 81.9886 3 -7 8 -7 33.2953 57.9608 2 -7 8 -7 120.364 58.1892 3 -7 8 -8 317.596 95.2517 2 -7 8 -8 231.564 64.7136 3 -7 8 -9 286.836 92.3672 2 -7 8 -9 245.535 72.7430 3 -7 8 -10 2089.30 170.388 3 -7 8 -10 1899.64 197.962 2 -7 8 -11 3680.66 278.368 2 -7 8 -12 2539.32 235.773 2 7 -7 -11 229.139 84.5244 7 -7 7 11 268.773 114.285 1 7 -7 -10-36.3575 72.9033 7 -7 7 10 55.9099 76.5938 6 7 -7 -9-19.3391 52.9413 7 -7 7 9-33.8204 69.9022 1 -7 7 9 77.3514 84.6298 6 7 -7 -8 25.0107 55.9758 7 -7 7 8 40.3231 67.8027 1 -7 7 8 31.0652 71.6891 6 7 -7 -7 132.216 67.4106 8 -7 7 7-78.6438 66.4382 1 7 -7 -7 144.755 63.7901 7 -7 7 7 13.1530 75.8036 6 7 -7 -6 881.723 118.628 8 -7 7 6 850.770 123.003 1 7 -7 -6 1013.04 126.532 7 -7 7 5 3082.13 238.262 4 -7 7 5 4249.34 238.216 1 7 -7 -5 3891.11 222.599 8 7 -7 -5 3699.65 228.401 7 -7 7 4 5375.69 258.016 1 -7 7 4 5007.23 294.878 4 7 -7 -4 4976.10 239.759 8 7 -7 -4 5239.32 268.315 7 -7 7 3 2968.58 221.532 4 7 -7 -3 2933.21 169.874 8 7 -7 -3 3199.46 202.863 7 -7 7 3 3302.00 185.957 1 -7 7 2 386.972 92.5269 4 -7 7 2 309.216 61.8504 1 7 -7 -2 400.459 65.3767 8 7 -7 -2 318.057 74.1796 7 -7 7 1 131.205 44.5456 1 -7 7 1 176.799 76.1442 4 7 -7 -1 111.034 38.4700 8 7 -7 -1 163.116 60.3142 7 -7 7 0 662.597 109.775 4 7 -7 0 568.304 63.0916 8 -7 7 0 479.056 83.0693 3 -7 7 0 599.124 87.1616 2 7 -7 0 464.682 86.8644 7 -7 7 0 517.108 60.6195 1 -7 7 -1 1394.80 151.724 4 -7 7 -1 1554.15 139.184 3 7 -7 1 1507.92 90.1027 8 -7 7 -1 1964.41 149.965 2 7 -7 1 1411.26 136.586 7 -7 7 -1 1562.50 91.6449 1 -7 7 -2 7202.61 343.505 4 -7 7 -2 6593.74 285.649 3 -7 7 -2 7322.10 304.503 2 7 -7 2 7139.30 313.325 7 -7 7 -3 8088.97 315.130 3 -7 7 -3 8375.69 336.010 2 7 -7 3 8283.95 345.683 7 -7 7 -4 5440.69 256.403 3 -7 7 -4 5986.83 286.932 2 7 -7 4 5763.99 293.392 7 -7 7 -5 2064.95 158.819 3 -7 7 -5 2184.64 177.878 2 -7 7 -6 162.640 68.3826 2 -7 7 -6 106.758 51.2991 3 -7 7 -7 383.325 92.4547 2 -7 7 -7 237.385 66.2878 3 -7 7 -8 86.3272 70.6315 2 -7 7 -8 68.9989 52.1575 3 -7 7 -9 1245.00 162.370 2 -7 7 -9 1229.82 135.357 3 -7 7 -10 1993.41 171.926 3 -7 7 -10 2021.50 202.887 2 -7 7 -11 670.802 124.235 2 -7 7 -11 623.957 106.648 3 -7 7 -12 95.7269 80.2955 2 -7 7 -12-27.1560 50.0592 3 -7 7 -13-99.2306 64.4834 3 7 -6 -12 98.9583 71.8308 7 -7 6 11 5.54208 89.6482 1 7 -6 -11 32.4299 64.2275 7 -7 6 11 21.0317 71.5031 6 7 -6 -10-26.9637 63.3450 7 -7 6 10-48.7810 85.4542 6 -7 6 10 11.1150 75.7687 1 7 -6 -9 30.6926 61.2818 7 -7 6 9 93.5428 81.9278 6 -7 6 9-32.5698 73.1260 1 7 -6 -8 10.6771 52.0746 7 -7 6 8 134.831 69.9419 1 -7 6 8 147.536 89.2582 6 7 -6 -7 134.350 63.8665 7 -7 6 7 77.2512 56.4974 1 7 -6 -6 738.866 109.799 7 -7 6 6 573.444 102.006 1 -7 6 6 617.390 117.633 6 -7 6 5 981.543 130.206 4 -7 6 5 817.091 108.706 1 7 -6 -5 1011.43 122.330 7 -7 6 5 1081.43 144.377 6 -7 6 4 169.079 67.4826 4 7 -6 -4 157.201 53.8781 8 -7 6 4 162.839 51.7005 1 7 -6 -4 165.550 60.5303 7 -7 6 4 145.273 66.1783 6 -7 6 3 80.6441 55.8348 4 7 -6 -3 58.1576 37.6776 8 -7 6 3 55.7567 41.7316 1 7 -6 -3 116.502 58.0625 7 -7 6 2 470.223 89.4433 4 -7 6 2 582.235 71.3996 1 7 -6 -2 576.649 64.6180 8 7 -6 -2 525.524 87.2650 7 -7 6 1 2224.19 180.095 4 -7 6 1 1889.23 155.067 3 7 -6 -1 2218.02 112.229 8 7 -6 -1 2371.62 171.729 7 -7 6 1 2268.18 115.323 1 -7 6 0 3267.89 216.391 4 -7 6 0 3018.63 189.495 3 7 -6 0 3075.72 120.101 8 7 -6 0 2867.54 188.331 7 -7 6 0 2970.97 115.726 1 -7 6 -1 2834.63 204.910 4 -7 6 -1 2789.57 181.121 3 7 -6 1 2858.79 99.7393 8 -7 6 -1 3055.03 180.833 2 7 -6 1 3043.43 197.818 7 -7 6 -2 5770.90 261.493 3 -7 6 -2 5586.37 256.428 2 7 -6 2 5786.11 278.837 7 -7 6 -3 8205.90 315.086 3 -7 6 -3 7876.61 316.270 2 7 -6 3 7887.28 335.458 7 -7 6 -4 2290.35 165.204 3 -7 6 -4 2105.97 165.444 2 -7 6 -5 2893.07 188.602 3 -7 6 -5 2833.33 195.111 2 -7 6 -6 1015.01 118.590 3 -7 6 -6 1233.55 135.135 2 -7 6 -7 1008.51 126.423 2 -7 6 -7 709.983 103.233 3 -7 6 -8 5325.44 273.028 3 -7 6 -8 5098.13 286.874 2 -7 6 -9 3294.86 218.732 3 -7 6 -9 3645.41 248.945 2 -7 6 -9 3630.65 201.965 5 -7 6 -10 2949.44 211.390 3 -7 6 -10 3140.03 236.623 2 -7 6 -10 3087.25 196.311 5 -7 6 -11 781.946 108.687 5 -7 6 -11 748.102 125.584 2 -7 6 -11 812.513 119.767 3 -7 6 -12 62.5015 75.3944 2 -7 6 -12-89.4132 66.8238 3 -7 6 -13-27.0658 61.8951 2 -7 6 -13-54.0604 63.9226 3 -7 6 -14 143.805 73.6771 3 -7 5 12 7.09809 74.8925 1 7 -5 -12 37.6438 67.1445 7 -7 5 11 343.253 105.304 1 7 -5 -11 354.066 94.1631 7 -7 5 11 358.445 112.693 6 -7 5 10 953.881 154.216 1 7 -5 -10 1108.60 143.695 7 -7 5 10 1424.24 183.704 6 -7 5 9 5088.90 314.205 1 7 -5 -9 4521.95 276.272 7 -7 5 9 5150.31 326.712 6 -7 5 8 3611.10 250.648 1 7 -5 -8 3070.18 221.294 7 -7 5 8 3501.49 263.292 6 -7 5 7 552.692 102.358 1 7 -5 -7 324.500 85.8960 7 -7 5 7 605.141 117.666 6 -7 5 6 516.323 90.2425 1 7 -5 -6 548.651 94.5684 7 -7 5 6 614.432 114.960 6 -7 5 5 1238.73 136.168 4 -7 5 5 1392.05 127.466 1 7 -5 -5 1497.97 145.445 7 -7 5 5 1408.89 154.043 6 -7 5 4 346.805 77.6952 4 7 -5 -4 555.605 91.7039 7 -7 5 4 439.802 68.6218 1 -7 5 4 436.548 93.2433 6 -7 5 3 1032.72 90.9442 1 -7 5 3 811.892 108.186 4 7 -5 -3 1210.79 126.260 7 -7 5 3 1091.43 130.689 6 -7 5 2 7848.12 233.997 1 -7 5 2 7458.87 321.128 4 -7 5 2 7701.70 317.188 3 7 -5 -2 7650.92 227.073 8 7 -5 -2 7895.48 318.050 7 -7 5 2 7763.44 335.539 6 -7 5 1 7266.49 313.913 4 -7 5 1 8369.24 323.704 3 7 -5 -1 7694.57 202.312 8 7 -5 -1 7746.90 313.424 7 -7 5 1 7353.46 195.848 1 -7 5 0 3245.21 205.369 4 -7 5 0 3475.37 200.764 3 7 -5 0 3281.56 97.8378 8 7 -5 0 3518.46 206.583 7 -7 5 0 2736.77 83.4901 1 -7 5 -1 3970.92 234.726 4 -7 5 -1 4029.11 214.629 3 7 -5 1 4085.91 229.744 7 -7 5 -2 2523.60 168.379 3 -7 5 -2 2298.70 160.618 2 7 -5 2 2318.54 179.086 7 -7 5 -3 1536.06 135.571 3 -7 5 -3 1611.96 135.588 2 7 -5 3 1572.49 151.062 7 -7 5 -4 146.763 54.9151 2 -7 5 -4 245.046 64.6248 3 -7 5 -5 2714.70 182.204 3 -7 5 -5 2224.57 169.806 2 -7 5 -6 2011.31 160.865 3 -7 5 -6 1990.90 166.821 2 -7 5 -7 1948.24 161.572 3 -7 5 -7 1799.48 163.819 2 -7 5 -8 2956.15 203.431 3 -7 5 -8 3005.60 212.230 2 -7 5 -8 2966.98 167.413 5 -7 5 -9 1181.15 137.117 3 -7 5 -9 1377.43 152.331 2 -7 5 -9 1147.27 114.437 5 -7 5 -10 997.248 113.151 5 -7 5 -10 878.392 128.289 2 -7 5 -10 916.464 127.964 3 -7 5 -11 29.3534 51.0221 5 -7 5 -11 92.4113 68.2841 2 -7 5 -11 174.376 71.8840 3 -7 5 -12 168.877 65.3672 5 -7 5 -12 247.490 84.9340 2 -7 5 -12 208.646 80.1756 3 -7 5 -13 1977.37 204.890 3 -7 5 -13 1866.96 198.490 2 -7 5 -14 1768.04 203.569 3 -7 5 -14 1716.45 196.098 2 -7 4 13-236.430 109.483 1 -7 4 12 760.919 147.633 1 7 -4 -12 570.667 120.800 7 -7 4 12 517.704 125.685 6 -7 4 11 1583.28 195.583 1 7 -4 -11 1444.21 166.468 7 -7 4 11 1570.98 191.546 6 -7 4 10 1283.93 167.847 1 7 -4 -10 1590.35 170.020 7 -7 4 10 1965.17 206.906 6 -7 4 9 1140.61 153.907 1 7 -4 -9 796.757 121.348 7 -7 4 9 1088.55 152.039 6 -7 4 8 34.1478 53.9688 1 7 -4 -8 20.8525 58.6157 7 -7 4 8-23.4658 66.1679 6 -7 4 7 784.610 113.027 1 7 -4 -7 412.770 79.7131 2 7 -4 -7 497.269 92.7723 7 -7 4 7 431.659 101.540 6 -7 4 6 1931.77 157.805 1 7 -4 -6 1673.90 157.839 7 -7 4 6 1984.45 178.736 6 -7 4 5 6008.34 279.152 4 -7 4 5 6614.14 267.563 1 7 -4 -5 6114.73 291.389 7 -7 4 5 6809.70 318.908 6 -7 4 4 5964.26 272.414 4 -7 4 4 6171.18 236.528 1 7 -4 -4 6173.17 287.347 7 -7 4 4 6378.69 303.107 6 -7 4 3 5024.69 239.645 4 -7 4 3 4672.92 180.739 1 -7 4 3 5030.91 253.464 3 7 -4 -3 5030.82 253.377 7 -7 4 3 4969.74 258.722 6 7 -4 -3 4091.10 111.596 5 -7 4 2 1814.84 144.437 4 -7 4 2 1836.07 94.4841 1 7 -4 -2 1785.65 91.9275 8 -7 4 2 1741.18 145.663 3 7 -4 -2 1693.60 144.638 7 -7 4 2 1956.69 159.571 6 -7 4 1 83.9793 44.1617 4 -7 4 1 42.6645 15.7584 1 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2 -4 263.950 68.5198 3 -7 2 -5 3089.26 201.647 3 -7 2 -6 1248.95 133.192 3 -7 2 -7 2489.04 191.866 3 -7 2 -8 6917.02 333.185 3 -7 2 -9 7542.57 364.278 3 -7 2 -10 547.736 117.041 3 -7 2 -11 763.389 129.899 3 -7 2 -12 763.169 140.966 3 -7 1 14-17.5432 88.3907 1 -7 1 13 26.3240 88.1220 1 7 -1 -13 149.925 78.6366 7 -7 1 12-23.1861 79.8177 1 7 -1 -12-42.8376 70.4758 7 7 -1 -11 296.908 75.6868 5 -7 1 11 75.5978 71.4114 1 7 -1 -11 156.320 76.0841 7 7 -1 -10 1017.08 122.327 2 7 -1 -10 886.481 136.035 7 -7 1 10 1010.78 143.862 1 7 -1 -10 974.532 114.656 5 7 -1 -9 2922.60 219.500 7 -7 1 9 2467.92 206.889 1 7 -1 -9 2634.11 196.801 2 7 -1 -9 2944.50 178.723 5 -7 1 8 1176.91 139.931 1 7 -1 -8 1199.29 142.441 7 7 -1 -8 1278.81 110.906 5 7 -1 -8 1122.44 133.913 2 -7 1 7 3225.52 162.844 4 7 -1 -7 2930.66 206.303 7 -7 1 7 2809.26 192.328 1 7 -1 -7 2905.59 155.666 5 7 -1 -7 2688.88 203.599 2 -7 1 6 1370.76 103.703 4 7 -1 -6 1178.73 133.051 7 7 -1 -6 1019.33 133.521 2 -7 1 6 1216.84 121.263 1 -7 1 5 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628.805 96.3970 8 7 0 -7 706.477 117.670 2 7 0 -7 691.271 109.378 7 -7 0 6 259.556 72.5070 3 -7 0 6 295.985 68.4884 8 7 0 -6 129.045 64.0550 2 7 0 -6 299.836 77.0889 7 -7 0 5 1226.68 111.263 8 -7 0 5 1179.57 125.677 3 7 0 -5 1073.72 120.054 7 7 0 -5 1011.64 136.065 2 -7 0 4 3822.85 183.199 8 -7 0 4 3780.26 218.155 3 7 0 -4 3879.90 220.737 7 -7 0 3 13708.5 354.558 8 -7 0 3 12620.0 415.773 3 7 0 -3 12721.0 418.117 7 -7 0 2 4646.73 179.171 8 -7 0 2 5038.39 243.183 3 7 0 -2 4211.78 224.480 7 -7 0 2 4780.48 216.834 6 -7 0 2 4768.71 151.944 5 -7 0 1 3959.57 153.875 8 -7 0 1 3761.03 213.533 3 7 0 -1 3349.27 200.398 7 -7 0 1 3731.95 183.326 6 -7 0 1 4130.94 154.667 1 -7 0 1 3776.33 130.531 5 -7 0 0 2605.15 120.547 1 -7 0 0 2745.25 121.679 8 -7 0 0 2734.03 182.491 3 7 0 0 2788.04 180.894 7 -7 0 0 2392.11 141.019 6 -7 0 -1 257.370 40.1054 8 -7 0 -1 266.081 68.6345 3 7 0 1 274.107 64.1651 7 -7 0 -1 335.299 53.6257 6 -7 0 -2 2810.39 118.578 8 -7 0 -2 2741.51 189.666 3 7 0 2 2592.19 181.835 7 -7 0 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8 7 1 -7 702.987 119.629 2 7 1 -7 633.950 103.339 7 -7 -1 6 1641.71 142.394 8 -7 -1 6 1776.36 154.294 3 7 1 -6 1918.96 166.303 7 7 1 -6 1948.99 191.455 2 7 1 -5 1602.46 179.619 2 -7 -1 5 1650.38 131.125 8 -7 -1 5 1636.77 144.987 3 7 1 -5 1630.56 148.749 7 -7 -1 4 1236.20 108.402 8 -7 -1 4 1320.78 130.336 3 7 1 -4 1387.70 134.276 7 -7 -1 3 623.411 77.9325 8 -7 -1 3 529.348 91.3443 3 7 1 -3 638.846 95.7371 7 -7 -1 2 820.315 80.5349 8 -7 -1 2 776.297 100.363 3 7 1 -2 789.492 102.791 7 -7 -1 1 70.7313 34.5629 8 -7 -1 1 74.9221 48.7541 3 7 1 -1 0.18185 48.3499 7 -7 -1 1 37.9354 33.3782 6 -7 -1 0 407.367 53.6347 8 -7 -1 0 452.004 78.6963 3 7 1 0 495.073 80.8898 7 -7 -1 0 312.921 55.3618 6 -7 -1 -1 1174.53 88.9376 8 -7 -1 -1 1433.13 136.490 3 7 1 1 1347.89 128.883 7 -7 -1 -1 1240.38 90.7544 6 -7 -1 -2 7619.66 241.778 8 -7 -1 -2 7410.59 321.213 3 7 1 2 7676.85 317.797 7 7 1 2 7310.00 242.978 1 -7 -1 -2 7004.02 209.635 6 -7 -1 -3 6440.74 222.431 8 -7 -1 -3 6273.26 298.825 3 7 1 3 6115.09 285.955 7 7 1 3 6202.57 226.724 1 -7 -1 -4 2281.36 133.961 8 -7 -1 -4 2182.56 177.804 3 7 1 4 1941.89 165.498 7 7 1 4 2300.33 140.062 1 -7 -1 -5 1098.32 96.4149 8 -7 -1 -5 1035.49 129.316 3 7 1 5 1022.52 102.581 1 -7 -1 -6 1462.85 116.519 8 -7 -1 -6 1311.74 150.051 3 7 1 6 1275.17 118.208 1 -7 -1 -7 3143.59 238.279 3 -7 -1 -8 890.624 138.623 3 -7 -1 -9 1702.97 190.122 3 -7 -1 -10 846.609 145.586 3 -7 -2 13 49.1196 66.1541 8 -7 -2 13 277.469 116.143 1 7 2 -13 146.754 73.1161 2 -7 -2 12 175.721 79.3630 8 7 2 -12 142.590 71.1412 2 7 2 -12 95.0897 71.4350 7 -7 -2 11 196.251 83.6426 8 7 2 -11 38.5459 66.9024 2 7 2 -11 206.753 81.9987 7 -7 -2 10 498.312 110.521 8 7 2 -10 550.479 122.966 2 7 2 -10 514.392 104.897 7 -7 -2 9-16.9678 63.7174 8 7 2 -9 44.2092 73.0506 2 7 2 -9-67.5361 67.5635 7 -7 -2 8 1377.33 148.324 8 7 2 -8 1683.21 165.378 7 7 2 -8 1529.24 176.641 2 -7 -2 7 4230.54 242.504 8 7 2 -7 4679.32 263.861 7 7 2 -7 5138.38 312.535 2 -7 -2 6 6554.95 287.794 8 -7 -2 6 6368.13 291.413 3 7 2 -6 6277.61 301.233 7 7 2 -6 7311.95 374.773 2 -7 -2 5 3560.34 203.946 8 -7 -2 5 3468.31 210.030 3 7 2 -5 4107.70 236.769 7 7 2 -5 4122.37 276.406 2 -7 -2 4 283.606 66.2840 8 -7 -2 4 156.774 60.0585 3 7 2 -4 480.373 115.208 2 7 2 -4 376.646 81.7515 7 -7 -2 3 674.852 83.7479 8 -7 -2 3 494.052 84.3408 3 7 2 -3 588.009 124.578 2 7 2 -3 593.725 91.9252 7 -7 -2 2 52.5460 43.8984 8 -7 -2 2 159.744 64.7231 3 7 2 -2 137.457 53.6146 7 -7 -2 1 904.585 92.6198 8 -7 -2 1 1042.48 117.744 3 7 2 -1 957.818 107.864 7 -7 -2 0 1665.59 120.312 8 -7 -2 0 1765.44 152.593 3 7 2 0 1470.52 132.951 7 -7 -2 0 1621.79 107.451 6 -7 -2 -1 666.182 78.4739 8 -7 -2 -1 569.580 93.1427 3 7 2 1 545.157 87.8732 7 -7 -2 -2 4162.83 191.823 8 -7 -2 -2 4087.18 240.374 3 7 2 2 3993.65 223.235 7 7 2 2 4284.71 200.939 1 -7 -2 -3 14.0633 33.9246 8 -7 -2 -3 20.6426 50.7720 3 7 2 3 5.15662 47.5063 7 7 2 3 57.1503 41.3887 1 -7 -2 -4 47.5531 39.2315 8 -7 -2 -4 22.3892 53.5424 3 7 2 4-35.1506 53.3094 7 7 2 4-45.8468 47.8668 1 7 2 5 74.2225 40.2459 1 -7 -2 -5 130.329 44.8826 8 -7 -2 -5 15.1580 57.1853 3 7 2 5 60.6389 45.9919 7 -7 -2 -6 1221.25 120.820 8 -7 -2 -6 1265.24 157.464 3 7 2 6 1278.19 132.222 1 -7 -2 -7 1679.13 180.907 3 -7 -2 -8 1568.37 180.668 3 -7 -2 -9 1303.05 174.145 3 7 3 -14 202.354 90.5407 2 -7 -3 13 47.3692 62.0170 8 7 3 -13 325.297 107.070 2 -7 -3 12-46.6744 72.7078 8 7 3 -12-34.4787 71.7839 2 7 3 -12-7.38474 53.9684 7 -7 -3 11 43.2113 63.2716 8 7 3 -11 192.857 85.8611 2 7 3 -11 15.1763 65.1743 7 -7 -3 10 295.774 95.5111 8 7 3 -10 185.447 84.3110 2 7 3 -10 318.481 89.4038 7 -7 -3 9 307.286 84.6211 8 7 3 -9 369.163 112.474 2 7 3 -9 347.215 93.1681 7 -7 -3 8 1821.11 169.901 8 7 3 -8 1873.42 175.068 7 7 3 -8 1907.53 206.315 2 -7 -3 7 1907.55 167.132 8 7 3 -7 1730.83 163.135 7 7 3 -7 2149.11 211.754 2 -7 -3 6 1253.24 129.211 3 -7 -3 6 1423.59 140.487 8 7 3 -6 1130.29 132.513 7 7 3 -6 1561.96 182.288 2 -7 -3 5 1023.28 116.128 3 -7 -3 5 866.511 105.484 8 7 3 -5 934.189 147.103 2 7 3 -5 890.313 113.801 7 -7 -3 4 2061.25 155.676 8 -7 -3 4 1687.13 144.472 3 7 3 -4 1521.02 144.258 7 7 3 -4 1996.33 203.591 2 -7 -3 3 696.006 91.9477 8 -7 -3 3 772.007 100.438 3 7 3 -3 754.547 131.316 2 7 3 -3 844.335 104.974 7 -7 -3 2 1313.65 120.423 8 -7 -3 2 1184.46 124.833 3 7 3 -2 1228.79 123.005 7 7 3 -2 1371.38 170.345 2 -7 -3 1 1714.96 134.450 8 -7 -3 1 1723.72 150.265 3 7 3 -1 1872.71 149.332 7 -7 -3 0 35.7943 38.7434 8 -7 -3 0 4.38771 55.1122 3 7 3 0 8.45626 45.4853 7 -7 -3 -1 1102.22 110.619 8 -7 -3 -1 1144.51 131.463 3 7 3 1 1206.29 119.334 7 7 3 1 927.864 105.041 1 -7 -3 -2 897.530 101.084 8 -7 -3 -2 964.554 121.854 3 7 3 2 1055.36 115.953 7 7 3 2 939.136 108.177 1 -7 -3 -3-30.6257 42.4229 8 -7 -3 -3 36.0585 54.6701 3 7 3 3 6.10230 37.7889 7 7 3 3-34.1108 43.2060 1 -7 -3 -4 105.778 49.9957 8 -7 -3 -4-65.2559 66.6602 3 7 3 4 86.0716 49.7610 7 7 3 4 61.4951 46.7827 1 -7 -3 -5 336.467 80.3420 8 -7 -3 -5 253.727 85.9006 3 7 3 5 381.192 84.0051 7 7 3 5 310.116 79.3457 1 -7 -3 -6 3229.91 204.624 8 -7 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69.1306 7 -7 -5 9 471.427 108.412 8 7 5 -9 693.212 143.935 2 7 5 -9 527.808 101.580 7 -7 -5 8 75.5478 53.9358 8 7 5 -8 180.515 63.8894 7 -7 -5 7-45.7764 53.5767 8 7 5 -7 125.678 85.1884 2 7 5 -7 175.760 68.6260 7 -7 -5 6 37.0449 48.3116 8 7 5 -6 68.7143 73.9279 2 7 5 -6 66.7493 50.1768 7 -7 -5 5 291.524 84.9353 8 7 5 -5 345.737 107.096 2 7 5 -5 235.079 65.5467 7 -7 -5 4 189.667 72.9766 8 7 5 -4 193.430 84.6750 2 7 5 -4 142.335 55.7938 7 -7 -5 3 602.314 105.065 8 7 5 -3 528.518 124.000 2 -7 -5 2 1891.07 169.884 8 -7 -5 2 1792.48 150.071 3 7 5 -2 1692.76 198.930 2 -7 -5 1 596.980 100.326 8 -7 -5 1 684.358 100.674 3 7 5 -1 627.753 126.777 2 -7 -5 0 644.083 107.285 8 -7 -5 0 697.579 105.076 3 7 5 0 578.411 131.105 2 7 5 1 2058.45 216.114 2 -7 -5 -1 2629.95 199.125 8 -7 -5 -1 2380.69 192.585 3 7 5 1 2091.82 184.387 1 -7 -5 -2 523.750 91.9847 8 -7 -5 -2 631.578 109.173 3 7 5 2 560.610 124.653 2 7 5 2 776.957 119.488 1 -7 -5 -3 694.100 109.606 8 -7 -5 -3 564.248 106.735 3 7 5 3 434.042 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70.4746 2 -8 9 -4 3.01578 43.0848 3 8 -9 4 26.7234 51.4260 7 -8 9 -5 2.21091 58.6098 2 -8 9 -5 21.6621 45.1883 3 8 -9 5 83.4120 63.6519 7 -8 9 -6 45.9409 67.3083 2 -8 9 -6 53.5204 54.8464 3 8 -9 6-124.202 74.0247 7 -8 9 -7 223.947 85.3369 2 -8 9 -7 113.296 53.8281 3 -8 9 -8 443.811 109.756 2 -8 9 -9 1367.13 175.772 2 -8 8 8 1240.80 172.548 4 8 -8 -8 1083.90 144.651 7 -8 8 7 532.167 121.435 4 8 -8 -7 288.128 81.3645 7 -8 8 6 143.882 80.4414 4 8 -8 -6 68.9267 53.9213 7 -8 8 5 65.1139 62.5571 4 8 -8 -5-13.6214 55.2501 7 -8 8 4 480.968 109.525 4 8 -8 -4 651.132 107.797 7 -8 8 3 2494.99 225.087 4 8 -8 -3 2525.33 195.079 7 -8 8 2 3133.48 247.464 4 8 -8 -2 3459.38 223.381 7 -8 8 1 2637.38 225.713 4 8 -8 -1 2917.99 204.119 7 -8 8 0 847.177 137.844 4 -8 8 0 902.835 119.118 3 8 -8 0 890.978 118.842 7 -8 8 -1 749.480 127.152 4 -8 8 -1 618.917 101.797 3 -8 8 -1 689.923 101.897 2 8 -8 1 932.953 118.980 7 -8 8 -2 1316.50 164.611 4 -8 8 -2 1097.15 127.748 3 -8 8 -2 1319.60 138.600 2 8 -8 2 1603.85 158.342 7 -8 8 -3 386.561 87.3668 2 -8 8 -3 294.800 70.7543 3 8 -8 3 375.913 87.5182 7 -8 8 -4 903.929 125.716 2 -8 8 -4 900.479 117.585 3 8 -8 4 903.510 130.066 7 -8 8 -5 1224.53 135.527 3 -8 8 -5 1458.12 158.839 2 8 -8 5 1052.59 141.161 7 -8 8 -6 571.904 110.051 2 -8 8 -6 694.416 108.415 3 -8 8 -7 65.4415 69.0049 2 -8 8 -7 41.0769 53.4592 3 -8 8 -8 13.9340 64.0603 2 -8 8 -8-2.18475 52.3244 3 -8 8 -9 21.0021 66.2649 2 -8 8 -9 4.24753 48.5102 3 -8 8 -10 41.2896 70.4307 2 -8 8 -10-6.64580 51.1450 3 8 -7 -10 1097.56 150.675 7 8 -7 -9 428.608 106.358 7 -8 7 9 806.659 153.948 6 -8 7 8-199.794 82.2898 4 8 -7 -8-45.6945 54.2373 7 -8 7 8-168.464 93.1121 6 -8 7 7 28.2450 64.9791 4 8 -7 -7-86.7128 62.3300 7 -8 7 7-113.129 84.6622 6 -8 7 6 366.857 97.4975 4 8 -7 -6 271.294 80.1501 7 -8 7 5 114.823 70.5058 4 8 -7 -5 415.864 99.6995 7 -8 7 4 1386.22 163.572 4 8 -7 -4 1797.59 167.760 7 -8 7 3 4094.90 270.237 4 8 -7 -3 4328.47 251.959 7 -8 7 2 1776.23 178.988 4 8 -7 -2 1932.08 168.189 7 -8 7 1 471.422 106.530 4 -8 7 1 500.633 93.2133 3 8 -7 -1 608.380 99.0435 7 -8 7 0-67.4289 66.3093 4 -8 7 0 24.4618 44.6755 3 8 -7 0-89.7766 56.2869 7 -8 7 -1 309.480 86.1114 4 -8 7 -1 231.522 66.1774 3 8 -7 1 197.648 66.3975 7 -8 7 -2 1059.28 125.856 3 -8 7 -2 1317.03 137.456 2 8 -7 2 992.802 128.664 7 -8 7 -3 2232.89 175.344 3 -8 7 -3 2205.92 177.897 2 8 -7 3 2067.52 187.124 7 -8 7 -4 5667.21 283.542 3 -8 7 -4 5763.66 297.840 2 8 -7 4 6135.33 321.611 7 -8 7 -5 7218.12 328.256 3 -8 7 -5 7769.50 353.793 2 8 -7 5 8027.78 379.816 7 -8 7 -6 2209.82 181.576 3 -8 7 -6 1860.09 176.529 2 -8 7 -7 328.707 93.7444 2 -8 7 -7 279.944 81.4113 3 -8 7 -8 554.620 116.062 2 -8 7 -8 551.520 102.691 3 -8 7 -9 976.807 146.339 2 -8 7 -9 1003.75 132.281 3 -8 7 -10 547.083 116.766 2 -8 7 -10 789.979 122.264 3 -8 7 -11 332.324 103.309 2 -8 7 -11 194.922 73.0086 3 -8 7 -12 218.221 80.9611 3 -8 7 -13 431.544 99.9036 3 8 -6 -11 718.595 132.269 7 -8 6 11 721.161 148.205 1 8 -6 -10 110.015 75.9612 7 -8 6 10-102.132 82.6647 1 8 -6 -9-25.3164 59.6586 7 -8 6 9 83.0903 77.5669 6 -8 6 9 7.31529 55.8814 1 8 -6 -8 67.6391 65.1050 7 -8 6 8-114.048 72.9693 1 -8 6 8 55.8437 74.2725 6 -8 6 7 149.076 77.7524 4 8 -6 -7 66.0499 69.3399 7 -8 6 7 152.206 59.6176 1 -8 6 7 76.1216 72.7610 6 -8 6 6 885.262 133.346 4 8 -6 -6 645.576 109.241 7 -8 6 6 879.553 117.494 1 -8 6 6 865.262 140.805 6 -8 6 5 2328.79 198.877 4 8 -6 -5 2621.15 206.564 7 -8 6 5 2723.27 228.692 6 -8 6 4 1441.84 159.452 4 8 -6 -4 1291.17 146.048 7 -8 6 4 1591.74 174.081 6 -8 6 3 58.7694 56.0493 4 8 -6 -3 28.1164 47.4766 7 -8 6 2 597.184 107.251 4 -8 6 2 752.882 111.445 3 8 -6 -2 584.231 98.1064 7 -8 6 1 1552.12 157.851 4 -8 6 1 1306.28 137.369 3 8 -6 -1 1460.75 147.906 7 -8 6 0 20.7173 55.3887 4 -8 6 0-54.6229 49.0753 3 8 -6 0-23.2378 56.5525 7 -8 6 -1 3864.76 229.366 3 8 -6 1 3710.60 237.063 7 -8 6 -2 4930.53 260.275 3 8 -6 2 5272.39 287.350 7 -8 6 -3 7676.65 329.444 3 -8 6 -3 7158.34 314.740 2 8 -6 3 7394.41 350.013 7 -8 6 -4 4207.30 244.896 3 -8 6 -4 4075.51 242.466 2 8 -6 4 4618.03 280.775 7 -8 6 -5 1367.12 141.223 3 -8 6 -5 1367.45 145.329 2 -8 6 -6 81.6549 62.2458 2 -8 6 -6-27.5568 52.2852 3 -8 6 -7 136.733 75.2510 2 -8 6 -7 371.943 85.9387 3 -8 6 -8 2575.16 202.630 3 -8 6 -8 2407.51 203.865 2 -8 6 -9 4795.01 285.677 3 -8 6 -9 5207.97 308.528 2 -8 6 -10 1667.67 173.794 3 -8 6 -10 1923.87 194.370 2 -8 6 -11 1458.90 167.482 3 -8 6 -11 1537.08 181.901 2 -8 6 -12 1498.25 181.523 2 -8 6 -12 1319.99 164.037 3 -8 6 -13 429.736 108.769 3 -8 5 12-75.7723 83.5327 1 -8 5 11 154.802 91.1483 1 8 -5 -11 69.2531 61.2193 7 -8 5 10 128.121 85.8352 1 8 -5 -10 61.2522 62.2028 7 -8 5 10 132.314 94.2371 6 -8 5 9 696.305 122.574 1 8 -5 -9 421.028 97.2260 7 -8 5 9 534.983 132.072 6 -8 5 8 1233.77 147.028 4 -8 5 8 994.799 138.290 1 8 -5 -8 1094.66 145.125 7 -8 5 8 1030.78 157.051 6 -8 5 7 1340.61 148.290 4 -8 5 7 1521.26 151.578 1 8 -5 -7 1264.89 153.892 7 -8 5 7 1756.19 189.835 6 -8 5 6 2428.73 195.306 4 -8 5 6 2584.93 179.707 1 8 -5 -6 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252.098 3 -8 5 -9 4442.24 275.178 2 -8 5 -10 465.658 105.786 2 -8 5 -10 668.364 116.581 3 -8 5 -11 539.386 111.249 2 -8 5 -11 547.679 108.732 3 -8 5 -12 132.376 78.8363 2 -8 5 -12-26.7903 74.5831 3 -8 4 12 101.963 83.1988 1 -8 4 11 3.26752 67.0583 1 8 -4 -11 138.554 75.6485 7 -8 4 11 185.850 108.148 6 -8 4 10 282.721 98.7574 1 8 -4 -10 298.796 90.8014 7 -8 4 10 588.681 132.215 6 -8 4 9 913.170 136.826 1 8 -4 -9 732.273 126.750 7 -8 4 9 1004.63 155.992 6 -8 4 8 1168.13 133.545 4 -8 4 8 1158.55 141.663 1 8 -4 -8 1064.35 138.949 7 -8 4 8 1064.42 152.784 6 -8 4 7 707.279 105.675 4 -8 4 7 710.772 106.868 1 8 -4 -7 667.823 102.105 2 8 -4 -7 667.868 112.116 7 -8 4 7 541.209 107.826 6 -8 4 6 377.378 80.6614 4 -8 4 6 333.059 76.4178 1 8 -4 -6 428.141 97.8252 7 -8 4 6 260.263 82.5690 6 -8 4 5-28.2265 42.1976 4 -8 4 5-5.25642 34.4013 1 8 -4 -5-24.5647 45.3720 7 -8 4 5 76.0170 67.3703 6 -8 4 4 313.765 56.2482 1 -8 4 4 315.657 71.3227 4 -8 4 4 507.363 97.7652 3 8 -4 -4 344.125 79.4926 7 -8 4 4 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9 -4 581.932 106.110 3 9 -9 4 445.377 107.675 7 -9 9 -5 103.024 70.9931 2 -9 9 -5 22.8926 51.1736 3 9 -9 5-8.92971 65.3484 7 -9 9 -6 512.999 125.411 2 -9 9 -6 280.049 81.9558 3 9 -9 6 216.356 85.2131 7 -9 9 -7 170.559 85.1640 2 -9 9 -7 116.854 66.6584 3 9 -9 7-11.2389 67.9424 7 -9 9 -8 240.260 94.2205 2 9 -8 -8 127.155 67.6830 7 -9 8 7 486.098 120.708 4 9 -8 -7 692.920 128.963 7 -9 8 6 1241.39 172.702 4 9 -8 -6 1341.55 160.077 7 -9 8 5 788.251 145.307 4 9 -8 -5 851.506 132.427 7 -9 8 4 220.316 88.8218 4 9 -8 -4 293.349 85.8522 7 -9 8 3-64.2575 74.8612 4 9 -8 -3 109.074 70.0121 7 -9 8 2 19.4151 66.1127 4 9 -8 -2-31.3740 60.1568 7 -9 8 1 561.939 118.452 4 9 -8 -1 502.093 97.8259 7 -9 8 0 2418.78 225.221 4 -9 8 0 2172.52 190.226 3 9 -8 0 2495.55 206.594 7 -9 8 -1 4673.24 308.588 4 -9 8 -1 4357.11 266.282 3 9 -8 1 4662.64 282.217 7 -9 8 -2 2112.09 185.314 3 9 -8 2 2523.90 210.668 7 -9 8 -3 771.218 116.849 3 -9 8 -3 774.493 122.393 2 9 -8 3 702.959 122.265 7 -9 8 -4 113.814 64.3902 2 -9 8 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58.5620 3 -9 4 -7 782.376 124.855 3 -9 4 -8 304.421 86.3543 3 -9 4 -9 982.147 143.173 3 -9 4 -10 991.455 147.284 3 9 -3 -10 755.282 141.282 7 -9 3 10 988.618 158.377 6 9 -3 -9 999.040 152.439 7 -9 3 9 964.917 156.344 6 9 -3 -8 1801.34 189.443 7 -9 3 8 1939.97 205.479 6 9 -3 -8 1637.90 172.358 2 9 -3 -7 659.591 124.091 2 9 -3 -7 1081.89 148.417 7 -9 3 7 1104.33 152.035 6 9 -3 -6 596.202 115.944 7 -9 3 6 550.975 113.162 6 -9 3 5 16.8039 42.5209 4 -9 3 5-21.4225 48.3341 3 9 -3 -5 70.4938 69.6807 7 -9 3 5 1.34031 59.0350 6 -9 3 4 168.257 59.5044 4 -9 3 4 165.720 66.2987 3 9 -3 -4 184.918 68.9944 7 -9 3 4 338.699 87.5834 6 -9 3 3 243.502 80.8389 3 9 -3 -3 66.7652 62.0089 7 -9 3 3 164.437 64.9156 6 -9 3 2 3068.11 223.495 3 9 -3 -2 3009.13 220.292 7 -9 3 2 3195.26 218.845 6 -9 3 1 5940.96 309.548 3 9 -3 -1 5762.58 304.320 7 -9 3 1 6045.18 295.478 6 -9 3 0 4331.09 262.122 3 9 -3 0 4464.57 269.500 7 -9 3 -1 555.595 100.131 3 9 -3 1 225.018 76.2926 7 -9 3 -2 226.575 75.7570 3 9 -3 2 333.717 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7 -9 -1 -6 660.931 122.336 3 9 1 6 499.665 108.610 7 -9 -1 -7 1532.11 183.830 3 9 1 7 1240.29 162.114 7 9 1 8 736.505 132.573 7 -9 -2 11 173.490 82.9312 8 9 2 -11 256.770 95.8838 2 -9 -2 10 82.9584 66.5978 8 9 2 -10 48.1465 74.7242 2 9 2 -10 76.9177 68.3814 7 -9 -2 9 64.1347 55.6895 8 9 2 -9 69.3731 70.9876 2 9 2 -9 172.042 79.8194 7 -9 -2 8 371.208 88.8685 8 9 2 -8 449.868 111.015 2 9 2 -8 596.863 115.848 7 -9 -2 7 123.063 57.2822 3 -9 -2 7 223.884 70.2866 8 9 2 -7 290.842 99.6576 2 9 2 -7 72.7273 62.8737 7 -9 -2 6 65.7651 54.3026 3 9 2 -6 66.8158 75.7398 2 9 2 -6 40.1358 52.8394 7 -9 -2 5-4.36565 57.9470 3 9 2 -5 90.2714 84.9309 2 9 2 -5 43.3530 55.4187 7 -9 -2 4 224.049 77.3753 3 9 2 -4 234.875 93.9176 2 9 2 -4 291.089 80.2135 7 -9 -2 3 918.914 127.365 3 9 2 -3 1090.05 168.151 2 9 2 -3 984.752 130.562 7 -9 -2 2 1194.25 144.755 3 9 2 -2 1245.14 144.247 7 -9 -2 1 323.371 86.1570 3 9 2 -1 219.572 73.0324 7 -9 -2 0 428.196 99.5268 3 9 2 0 357.665 86.3878 7 -9 -2 -1 2239.26 198.054 3 9 2 1 1599.55 162.704 7 -9 -2 -2 1144.94 150.140 3 9 2 2 1056.75 136.841 7 -9 -2 -3 382.193 105.473 3 9 2 3 487.181 103.775 7 -9 -2 -4 847.769 136.435 3 9 2 4 668.423 114.476 7 -9 -2 -5 619.422 122.414 3 9 2 5 541.262 107.240 7 -9 -2 -6 140.951 87.6724 3 9 2 6 56.5791 56.3929 7 9 2 7-85.9787 65.4515 7 -9 -3 10 25.3508 61.1456 8 -9 -3 9 109.543 70.1095 8 9 3 -9 262.696 92.6000 7 -9 -3 8 36.8468 58.0069 8 9 3 -8 110.045 78.5689 2 9 3 -8 122.920 73.6325 7 -9 -3 7 91.8492 61.4329 3 -9 -3 7 197.384 74.2025 8 9 3 -7 326.774 110.625 2 9 3 -7 317.164 90.9117 7 -9 -3 6 420.564 87.4981 3 9 3 -6 455.996 124.345 2 9 3 -6 362.961 96.7989 7 -9 -3 5-108.424 58.1775 3 9 3 -5 35.9118 74.2490 2 9 3 -5 32.8414 64.9618 7 -9 -3 4 81.5134 53.4829 3 9 3 -4 164.447 93.5182 2 9 3 -4 196.742 70.9476 7 -9 -3 3 287.697 80.5333 3 9 3 -3 54.5636 82.0980 2 9 3 -3 198.834 75.5977 7 -9 -3 2 853.553 121.145 3 9 3 -2 860.691 168.994 2 9 3 -2 882.136 122.842 7 -9 -3 1 148.589 73.0717 3 9 3 -1 317.570 111.218 2 9 3 -1 76.6825 47.2336 7 -9 -3 0 325.313 92.8777 3 9 3 0 321.021 84.1812 7 -9 -3 -1 614.601 113.538 3 9 3 1 601.195 104.608 7 -9 -3 -2 319.936 89.7143 3 9 3 2 405.001 90.4116 7 -9 -3 -3 1615.33 181.183 3 -9 -3 -4 1639.24 189.828 3 -9 -3 -5 924.371 150.376 3 -9 -4 9 51.3041 63.7001 8 9 4 -9 474.274 107.278 7 -9 -4 8 159.301 70.3803 8 9 4 -8 255.089 80.7449 7 -9 -4 7 276.374 79.9298 8 9 4 -7 316.684 85.9626 7 9 4 -6 132.664 61.7208 7 9 4 -5 125.830 86.0625 2 9 4 -5 36.6526 59.8034 7 9 4 -4 233.300 97.5366 2 9 4 -4 67.4950 60.7075 7 9 4 -3 260.354 99.6859 2 -9 -4 2 39.3428 49.4723 3 9 4 -2 122.933 74.7835 2 -9 -4 1 97.1063 73.8102 3 9 4 -1 17.5633 87.6062 2 -9 -4 0 931.195 135.854 3 9 4 0 742.136 147.350 2 -9 -4 -1 1027.65 140.665 3 9 4 1 972.172 173.686 2 -9 -4 -2 407.206 101.423 3 9 4 2 276.150 105.197 2 -9 -4 -3 92.1071 81.3464 3 9 4 3 140.966 93.1448 2 -9 -4 -4 101.128 75.1967 3 10 -10 0 237.866 81.6527 7 10 -10 1 155.374 78.9506 7 -10 10 -2 11.0430 59.5132 3 10 -10 2-93.6000 68.2340 7 -10 10 -3 51.6561 52.8798 3 10 -10 3 15.5646 59.4853 7 -10 10 -4 334.367 92.7561 3 -10 10 -4 421.159 103.497 2 10 -10 4 273.083 92.4860 7 -10 10 -5 865.017 144.772 2 10 -10 5 876.269 155.538 7 10 -10 6 624.404 128.925 7 10 -10 7 713.161 136.647 7 10 -9 -5 386.786 104.245 7 10 -9 -4 451.625 112.240 7 -10 9 3 713.552 146.283 4 10 -9 -3 553.294 109.454 7 -10 9 2 468.424 116.530 4 10 -9 -2 466.095 106.409 7 -10 9 1 333.433 107.601 4 10 -9 -1 156.218 73.2807 7 -10 9 0-4.92941 68.1004 4 10 -9 0 168.385 74.0118 7 -10 9 -1 33.8203 62.5106 3 10 -9 1 266.995 87.8429 7 -10 9 -2 214.845 77.3855 3 10 -9 2 524.844 108.586 7 -10 9 -3 1210.00 156.589 3 10 -9 3 979.183 152.830 7 -10 9 -4 2023.17 196.148 3 10 -9 4 2628.66 241.825 7 -10 9 -5 1279.84 160.072 3 -10 9 -5 1860.76 194.920 2 10 -9 5 1567.49 191.791 7 -10 9 -6 619.982 126.242 2 -10 9 -6 682.752 122.597 3 10 -9 6 921.222 150.278 7 -10 9 -7 203.683 76.9609 3 10 -9 7 1.86937 73.2094 7 -10 9 -8 36.2960 63.4417 3 10 -8 -7 133.228 74.1166 7 -10 8 6 937.429 161.007 4 10 -8 -6 909.287 146.888 7 -10 8 5 1096.93 164.390 4 10 -8 -5 1623.50 189.470 7 -10 8 4 924.066 153.968 4 10 -8 -4 851.744 137.620 7 -10 8 3-12.1581 62.3237 4 10 -8 -3 12.8609 55.6385 7 -10 8 2-64.1714 74.3782 4 10 -8 -2-29.2869 56.8746 7 -10 8 1-17.4130 58.3617 4 -10 8 1 28.0937 60.3782 3 10 -8 -1-54.3651 59.2524 7 -10 8 0 279.353 83.9164 3 10 -8 0 298.140 95.7678 7 -10 8 -1 1168.96 151.839 3 10 -8 1 1153.35 155.883 7 -10 8 -2 1414.02 168.067 3 10 -8 2 2039.91 204.477 7 -10 8 -3 1664.63 178.072 3 10 -8 3 1836.07 198.807 7 -10 8 -4 1349.70 162.457 3 10 -8 4 1759.16 200.350 7 -10 8 -5 86.0500 67.9503 3 10 -8 5 154.764 84.4367 7 -10 8 -6 74.1048 65.0143 3 10 -8 6 210.522 84.4786 7 -10 8 -7 250.542 87.2882 3 -10 8 -7 350.915 105.604 2 10 -8 7 279.570 90.8820 7 -10 8 -8 767.220 133.302 3 -10 8 -9 795.129 135.890 3 -10 8 -10 1790.29 190.726 3 -10 7 8 154.226 83.3539 4 -10 7 7 921.221 147.718 4 10 -7 -7 912.769 145.536 7 -10 7 6 820.147 135.258 4 10 -7 -6 604.400 126.056 7 -10 7 5 356.455 96.5994 4 10 -7 -5 398.247 107.696 7 -10 7 4 62.1893 62.1214 4 10 -7 -4 5.49466 57.1494 7 -10 7 3 143.241 78.8391 4 10 -7 -3 98.4012 61.8542 7 -10 7 2-4.80370 64.3696 4 -10 7 2 27.3324 59.7101 3 10 -7 -2 51.9241 69.9312 7 -10 7 1 571.596 119.360 4 -10 7 1 513.144 108.741 3 10 -7 -1 542.914 121.193 7 -10 7 0 1970.92 193.412 3 10 -7 0 2630.15 225.662 7 -10 7 -1 1407.05 163.695 3 10 -7 1 1757.26 189.691 7 -10 7 -2 556.665 109.105 3 10 -7 2 534.069 116.014 7 -10 7 -3-7.88083 61.1559 3 10 -7 3 28.3328 65.7249 7 -10 7 -4 63.0647 69.9729 3 10 -7 4 37.4844 63.8696 7 -10 7 -5 240.611 86.0774 3 10 -7 5 187.077 96.4672 7 -10 7 -6 170.868 79.8827 3 10 -7 6 141.240 80.7608 7 -10 7 -7 1313.44 165.893 3 10 -7 7 1512.09 192.424 7 -10 7 -8 1339.67 169.372 3 -10 7 -9 1128.32 156.611 3 -10 6 7 424.266 106.298 4 10 -6 -7 481.254 115.560 7 -10 6 6 90.0245 57.4734 4 10 -6 -6 57.1458 72.0124 7 -10 6 6 263.500 103.029 6 -10 6 5 63.8300 58.8546 4 10 -6 -5 157.754 80.7293 7 -10 6 5-70.5183 77.0269 6 -10 6 4 33.4437 66.0520 4 10 -6 -4 86.6631 63.2099 7 -10 6 3 699.746 122.754 4 -10 6 3 583.874 112.515 3 10 -6 -3 566.108 111.581 7 -10 6 2 2483.72 215.943 4 -10 6 2 2355.24 210.872 3 10 -6 -2 2288.66 205.903 7 -10 6 1 2097.07 201.272 3 10 -6 -1 2673.04 225.552 7 -10 6 0 1490.03 170.207 3 10 -6 0 1358.09 163.700 7 -10 6 -1 67.8076 58.7885 3 10 -6 1-44.1077 55.7667 7 -10 6 -2 68.3841 62.4217 3 10 -6 2 190.888 85.1817 7 -10 6 -3 78.1985 65.6452 3 10 -6 3-31.7316 58.5438 7 -10 6 -4-50.4919 62.8980 3 10 -6 4-5.90329 65.2498 7 -10 6 -5 125.680 79.9246 3 10 -6 5 142.315 92.5508 7 -10 6 -6 665.997 122.890 3 10 -6 6 739.018 136.838 7 -10 6 -7 1041.45 150.122 3 10 -6 7 748.818 140.905 7 -10 6 -8 379.836 99.2996 3 -10 6 -9 517.505 112.400 3 10 -5 -8 54.9906 68.6731 7 10 -5 -7-14.7193 58.4746 7 -10 5 7 40.3441 72.3863 6 10 -5 -6 226.454 87.9358 7 -10 5 6 446.392 115.812 6 -10 5 5 574.603 104.361 4 10 -5 -5 538.769 113.889 7 -10 5 5 322.303 96.8582 6 -10 5 4 1118.39 142.410 4 -10 5 4 1041.86 146.468 3 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55.2842 7 10 0 7 82.9574 68.4677 7 10 1 -9-90.2006 79.0540 2 10 1 -8 570.199 139.688 2 10 1 -8 415.481 107.101 7 10 1 -7 265.728 114.780 2 10 1 -7 209.234 87.9179 7 -10 -1 6 383.996 99.0593 3 10 1 -6 466.427 132.501 2 10 1 -6 451.041 106.247 7 -10 -1 6 406.362 102.786 6 -10 -1 5-66.4219 62.8200 3 10 1 -5 134.425 94.2968 2 10 1 -5-77.9987 70.1128 7 -10 -1 5 0.53627 49.0884 6 -10 -1 4 7.38295 54.7505 3 10 1 -4-21.6187 73.9356 2 10 1 -4 35.5671 59.0468 7 -10 -1 4 51.7394 54.1959 6 -10 -1 3 345.975 91.6487 3 10 1 -3 172.847 74.2360 7 -10 -1 2 1245.23 159.194 3 10 1 -2 889.079 136.283 7 -10 -1 1 660.934 119.608 3 10 1 -1 438.698 101.896 7 -10 -1 0 729.426 130.706 3 10 1 0 721.550 121.574 7 -10 -1 -1 881.808 141.527 3 10 1 1 1233.76 151.619 7 -10 -1 -2 433.549 110.544 3 10 1 2 501.425 107.906 7 -10 -1 -3 261.611 91.0933 3 10 1 3 302.927 92.2538 7 -10 -1 -4-57.0223 77.4067 3 10 1 4 21.2077 54.1235 7 10 1 5 15.9692 61.1300 7 10 1 6 41.3162 67.0694 7 -10 -2 7 263.101 90.0248 3 10 2 -7 476.834 109.105 7 -10 -2 6 148.460 69.2239 3 10 2 -6 195.772 107.361 2 10 2 -6-37.9890 59.8478 7 -10 -2 5 64.2053 58.6669 3 10 2 -5-37.8570 73.3706 2 10 2 -5 62.5007 62.0742 7 -10 -2 4 179.525 79.2257 3 10 2 -4 391.418 123.538 2 10 2 -4 139.287 69.3118 7 -10 -2 3 327.164 95.9282 3 10 2 -3 284.813 108.153 2 10 2 -3 226.915 80.3182 7 -10 -2 2 580.034 118.634 3 10 2 -2 723.140 152.906 2 10 2 -2 804.598 124.596 7 -10 -2 1 69.1090 76.1557 3 10 2 -1 88.5587 62.7043 7 -10 -2 0 812.275 133.289 3 10 2 0 869.102 126.226 7 -10 -2 -1 551.762 118.567 3 10 2 1 216.382 73.8602 7 -10 -2 -2 229.785 90.3502 3 10 2 2 83.2641 64.8976 7 -10 -2 -3-103.908 75.8523 3 10 2 3 74.6938 61.9949 7 10 2 4 492.642 105.308 7 10 3 -7 45.5562 60.6458 7 10 3 -6 255.008 92.4804 7 10 3 -5 159.714 75.0885 7 -10 -3 4 92.7185 54.1078 3 10 3 -4 238.576 80.2053 7 -10 -3 3 519.534 110.718 3 10 3 -3 365.150 90.5185 7 -10 -3 2 380.509 89.1248 3 10 3 -2 376.427 92.6621 7 -10 -3 1 156.960 69.8624 3 10 3 -1 56.3966 54.7980 7 -10 -3 0 68.6478 59.1916 3 -10 -3 -1 122.680 81.1337 3 -10 -3 -2-46.2222 64.8496 3 11 -10 1 1134.32 165.700 7 11 -10 2 96.8888 76.4946 7 -11 10 -3-29.6889 66.0811 3 11 -9 -2 869.479 146.040 7 11 -9 -1 575.379 123.122 7 -11 9 0 252.203 93.2727 3 11 -9 0 573.059 121.054 7 -11 9 -1-108.932 74.9472 3 11 -9 1-68.1565 76.2274 7 -11 9 -2-69.1938 78.1712 3 11 -9 2 93.2408 71.3379 7 -11 9 -3-119.909 75.6220 3 11 -9 3 74.6834 66.2363 7 -11 9 -4 374.494 103.318 3 11 -9 4 335.128 105.943 7 -11 9 -5 899.001 148.867 3 -11 9 -6 1379.25 178.008 3 -11 8 4 407.354 118.964 4 -11 8 3 906.017 155.150 4 11 -8 -3 777.999 134.479 7 -11 8 2 579.227 133.048 4 11 -8 -2 458.364 116.883 7 -11 8 1 160.151 81.5600 3 11 -8 -1 199.262 86.8064 7 -11 8 0 111.968 76.0854 3 11 -8 0-10.6055 63.4540 7 -11 8 -1 13.0500 71.9193 3 11 -8 1-13.0385 62.3133 7 -11 8 -2-43.1062 67.5752 3 11 -8 2 51.7853 67.8465 7 -11 8 -3 572.996 119.517 3 11 -8 3 847.521 149.235 7 -11 8 -4 1301.49 171.025 3 11 -8 4 1262.44 189.807 7 -11 8 -5 1086.80 156.447 3 -11 8 -6 547.719 124.095 3 -11 7 5 828.936 150.299 4 -11 7 4 213.691 87.1435 4 11 -7 -4 183.171 87.6215 7 -11 7 3-119.723 74.6817 4 11 -7 -3 62.4968 70.0826 7 -11 7 2-104.316 69.8558 3 11 -7 -2 242.944 88.2737 7 -11 7 1 66.6174 61.2226 3 11 -7 -1-24.5812 68.6814 7 -11 7 0 387.884 101.314 3 11 -7 0 302.796 98.5109 7 -11 7 -1 663.877 127.923 3 11 -7 1 646.240 130.756 7 -11 7 -2 1431.17 179.754 3 11 -7 2 1272.01 185.458 7 -11 7 -3 951.796 148.637 3 11 -7 3 1029.96 163.162 7 -11 7 -4 207.493 90.5709 3 11 -7 4 126.476 80.5599 7 -11 7 -5 58.4465 71.7256 3 11 -7 5-41.9335 80.7282 7 -11 7 -6 175.622 81.1466 3 11 -6 -4 126.428 82.4729 7 -11 6 3 70.2647 64.5225 3 11 -6 -3-82.6491 68.9233 7 -11 6 2 265.585 93.7530 3 11 -6 -2 88.4882 76.0334 7 -11 6 1 566.535 123.305 3 11 -6 -1 716.909 137.345 7 -11 6 0 1007.92 152.964 3 11 -6 0 862.136 148.749 7 -11 6 -1 1402.11 177.034 3 11 -6 1 1548.84 194.346 7 -11 6 -2 964.341 148.147 3 11 -6 2 1012.31 161.141 7 -11 6 -3 285.570 97.2889 3 11 -6 3 147.675 83.2318 7 -11 6 -4 67.4711 66.0138 3 11 -6 4-16.4095 76.3333 7 -11 6 -5-21.4366 62.7826 3 11 -6 5-27.1137 70.6804 7 -11 6 -6 5.86604 60.9142 3 11 -5 -5 74.7643 71.2037 7 -11 5 5 141.147 86.3825 6 -11 5 4 167.968 82.3234 3 11 -5 -4 169.815 88.8712 7 -11 5 4 281.675 96.6165 6 -11 5 3 501.839 119.803 3 11 -5 -3 672.640 130.426 7 -11 5 2 1355.02 171.977 3 11 -5 -2 1581.54 186.997 7 -11 5 1 1364.93 171.900 3 11 -5 -1 1268.67 169.667 7 -11 5 0 197.747 81.1305 3 11 -5 0 430.336 113.723 7 -11 5 -1 223.106 84.3195 3 11 -5 1 317.154 93.7144 7 -11 5 -2 84.5464 75.0520 3 11 -5 2 115.464 82.5303 7 -11 5 -3 137.104 74.3038 3 11 -5 3 22.1313 64.6944 7 -11 5 -4 717.986 133.525 3 11 -5 4 884.133 159.385 7 -11 5 -5 1307.94 171.942 3 11 -5 5 1764.96 217.149 7 -11 4 6 262.120 90.2345 6 -11 4 5 313.207 95.0074 3 11 -4 -5 200.716 96.7735 7 -11 4 5 367.508 101.041 6 -11 4 4 693.252 133.820 3 11 -4 -4 756.596 139.271 7 -11 4 4 624.835 123.359 6 -11 4 3 859.476 142.901 3 11 -4 -3 937.284 151.572 7 -11 4 3 1038.41 150.025 6 -11 4 2 322.224 102.994 3 11 -4 -2 567.083 122.092 7 -11 4 1 5.23426 72.7567 3 11 -4 -1 290.116 94.5299 7 -11 4 0 243.919 93.1913 3 11 -4 0 52.1924 75.1082 7 -11 4 -1 127.239 82.3598 3 11 -4 1 104.840 59.6736 7 -11 4 -2 104.068 72.9957 3 11 -4 2 113.096 71.0254 7 -11 4 -3 373.280 110.211 3 11 -4 3 426.163 118.988 7 -11 4 -4 1271.34 169.071 3 11 -4 4 1162.50 176.322 7 -11 4 -5 694.214 130.366 3 11 -4 5 690.367 147.320 7 11 -3 -7 3.34532 71.1889 2 -11 3 6 277.588 93.6596 6 -11 3 5 703.765 134.522 3 11 -3 -5 682.351 131.749 7 -11 3 5 416.853 107.100 6 -11 3 4 276.310 96.8459 3 11 -3 -4 370.950 107.644 7 -11 3 4 561.728 113.942 6 -11 3 3 42.2274 65.0637 3 11 -3 -3 321.262 99.0619 7 -11 3 3 291.123 87.5298 6 -11 3 2-31.6782 58.5471 3 11 -3 -2 108.454 71.1303 7 -11 3 1 167.616 82.0948 3 11 -3 -1 113.154 71.8943 7 -11 3 0 488.321 115.174 3 11 -3 0 437.913 107.199 7 -11 3 -1 558.323 117.023 3 11 -3 1 671.554 125.977 7 -11 3 -2 1173.79 160.261 3 11 -3 2 1332.94 177.257 7 -11 3 -3 1021.44 156.799 3 11 -3 3 1242.89 173.306 7 -11 3 -4 365.769 101.116 3 11 -3 4 454.858 119.321 7 11 -3 5 115.032 82.2298 7 11 -2 -8 80.3831 78.3053 2 11 -2 -7 542.550 128.653 2 -11 2 7 385.377 110.129 6 -11 2 6 210.624 89.5830 3 11 -2 -6 293.421 103.294 2 -11 2 6 206.426 86.5133 6 -11 2 5 56.5875 72.8460 3 11 -2 -5-40.8894 70.4060 7 -11 2 5 54.1247 68.6739 6 -11 2 4 18.8070 75.4852 3 11 -2 -4-10.7124 59.7524 7 -11 2 4-135.117 71.3933 6 -11 2 3 7.33968 66.0421 3 -11 2 3 79.2600 58.9825 6 -11 2 2 313.257 96.8915 3 11 -2 -2 268.228 90.0381 7 -11 2 2 295.076 86.8975 6 -11 2 1 905.077 154.508 3 11 -2 -1 1029.88 152.339 7 -11 2 0 1137.29 161.936 3 11 -2 0 1285.97 169.782 7 -11 2 -1 1258.68 170.940 3 11 -2 1 969.657 152.816 7 -11 2 -2 724.560 135.083 3 11 -2 2 482.927 121.520 7 -11 2 -3 64.1762 62.1848 3 11 -2 3 126.476 83.4757 7 -11 2 -4-48.4474 69.8771 3 11 -2 4 35.6956 68.8435 7 11 -1 -8 145.689 104.758 2 11 -1 -7 276.698 108.160 2 -11 1 7-43.3845 64.9351 6 -11 1 6 59.2204 72.0304 3 11 -1 -6-24.4363 75.1332 2 -11 1 6 161.415 84.2010 6 -11 1 5-15.6088 71.4377 3 11 -1 -5 68.5939 67.0873 7 -11 1 5 130.231 71.1000 6 -11 1 4 318.335 95.8691 3 11 -1 -4 400.357 104.598 7 -11 1 4 282.668 90.0243 6 -11 1 3 495.419 115.968 3 11 -1 -3 737.320 129.697 7 -11 1 3 639.484 106.394 6 -11 1 2 809.375 138.635 3 11 -1 -2 943.336 145.999 7 -11 1 1 419.556 109.764 3 11 -1 -1 450.581 108.614 7 -11 1 0 46.6874 72.4936 3 11 -1 0 64.5776 58.8402 7 -11 1 -1 71.1293 67.4110 3 11 -1 1-48.4936 68.0605 7 -11 1 -2 59.9674 68.0696 3 11 -1 2-152.107 72.6130 7 -11 1 -3 115.763 74.6984 3 11 -1 3-31.3704 60.4216 7 11 -1 4 101.337 79.1082 7 -11 0 7-57.1790 66.8038 6 -11 0 6 117.676 84.1918 3 -11 0 6 251.178 86.7623 6 -11 0 5 114.079 72.6663 3 -11 0 5 292.699 91.7315 6 -11 0 4 174.968 85.1780 3 11 0 -4 324.435 95.0262 7 -11 0 3 343.264 99.5788 3 11 0 -3 198.418 78.7213 7 -11 0 2 250.954 99.1923 3 11 0 -2 212.836 84.7712 7 -11 0 1 186.619 91.2695 3 11 0 -1 305.101 94.1184 7 -11 0 0-97.1037 77.9644 3 11 0 0 97.9102 73.2104 7 -11 0 -1-10.2089 68.7209 3 11 0 1-48.6348 77.0714 7 -11 0 -2 212.338 84.0497 3 11 0 2 227.073 88.7761 7 11 0 3 392.980 106.307 7 -11 -1 7 415.689 106.581 6 -11 -1 6 405.525 106.291 3 -11 -1 5 139.639 73.1965 3 -11 -1 4 200.997 91.3803 3 11 1 -4 114.836 73.6123 7 -11 -1 3 97.7377 74.1712 3 11 1 -3 113.188 68.1348 7 -11 -1 2 147.465 77.1603 3 11 1 -2 106.134 65.5359 7 -11 -1 1-17.3415 75.1924 3 11 1 -1-74.9736 63.7392 7 -11 -1 0 200.396 82.3129 3 11 1 0 157.011 77.9768 7 11 1 1 534.223 110.414 7 11 1 2 607.371 125.395 7 11 1 3 458.077 100.082 7 -11 -2 5-41.4105 58.7671 3 -11 -2 4-10.1421 63.8253 3 -11 -2 3 192.610 87.4476 3 11 2 -3 177.345 84.1384 7 -11 -2 2 334.592 99.2928 3 11 2 -2 309.205 92.8859 7 -11 -2 1 97.7779 71.2077 3 11 2 -1 111.463 65.0539 7 11 2 0 219.009 87.8675 7 -12 4 4 258.975 105.973 6 -12 4 3 143.752 80.3767 6 -12 3 4 499.517 118.534 6 -12 3 3 175.359 72.7830 6 -12 2 5-10.6358 59.0352 6 -12 2 4 481.729 106.211 6 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 43074 data_4 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C3 H8 O)' _chemical_formula_sum 'C42 H48 Cl2 Cu N8 O10' _chemical_formula_weight 959.32 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1329(6) _cell_length_b 10.0787(7) _cell_length_c 13.0825(8) _cell_angle_alpha 103.496(6) _cell_angle_beta 94.562(5) _cell_angle_gamma 105.229(6) _cell_volume 1117.04(13) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4307 _cell_measurement_theta_min 6.5150 _cell_measurement_theta_max 29.3780 _exptl_crystal_description prism _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.426 _exptl_crystal_F_000 499 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.11 _exptl_absorpt_coefficient_mu 0.674 _shelx_estimated_absorpt_T_min 0.871 _shelx_estimated_absorpt_T_max 0.930 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.803 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 10056 _diffrn_reflns_av_unetI/netI 0.0351 _diffrn_reflns_av_R_equivalents 0.0253 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.023 _diffrn_reflns_theta_max 27.000 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 4829 _reflns_number_gt 4106 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0337P)^2^+1.0475P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4829 _refine_ls_number_parameters 296 _refine_ls_number_restraints 3 _refine_ls_R_factor_all 0.0470 _refine_ls_R_factor_gt 0.0362 _refine_ls_wR_factor_ref 0.0940 _refine_ls_wR_factor_gt 0.0861 _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_restrained_S_all 1.074 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.01401(10) Uani 1 2 d S . P . . N1A N -0.2226(2) -0.34109(18) 0.10577(14) 0.0196(4) Uani 1 1 d D . . . . H1A H -0.224(3) -0.4223(16) 0.116(2) 0.029 Uiso 1 1 d D U . . . N1B N -0.34454(19) -0.12484(19) -0.25864(14) 0.0198(4) Uani 1 1 d D . . . . H1B H -0.4329(16) -0.127(3) -0.2875(19) 0.030 Uiso 1 1 d D U . . . C2A C -0.1046(2) -0.2594(2) 0.07341(17) 0.0199(4) Uani 1 1 d . . . . . H2A H -0.0098 -0.2797 0.0648 0.024 Uiso 1 1 calc R U . . . C2B C -0.2825(2) -0.0552(2) -0.15812(16) 0.0190(4) Uani 1 1 d . . . . . H2B H -0.3325 -0.0055 -0.1082 0.023 Uiso 1 1 calc R U . . . N3A N -0.13802(18) -0.14695(17) 0.05517(13) 0.0168(3) Uani 1 1 d . . . . . N3B N -0.14208(18) -0.06484(17) -0.13743(13) 0.0164(3) Uani 1 1 d . . . . . C4A C -0.2854(2) -0.1585(2) 0.07592(16) 0.0179(4) Uani 1 1 d . . . . . H4A H -0.3404 -0.0921 0.0695 0.021 Uiso 1 1 calc R U . . . C4B C -0.1143(2) -0.1442(2) -0.23054(16) 0.0172(4) Uani 1 1 d . . . . . H4B H -0.0213 -0.1677 -0.2404 0.021 Uiso 1 1 calc R U . . . C5A C -0.3408(2) -0.2803(2) 0.10730(16) 0.0174(4) Uani 1 1 d . . . . . C5B C -0.2398(2) -0.1843(2) -0.30669(16) 0.0174(4) Uani 1 1 d . . . . . C6A C -0.4900(2) -0.3438(2) 0.13585(16) 0.0190(4) Uani 1 1 d . . . . . C6B C -0.2711(2) -0.2765(2) -0.41500(16) 0.0199(4) Uani 1 1 d . . . . . C7A C -0.5393(2) -0.4884(2) 0.13122(16) 0.0217(4) Uani 1 1 d . . . . . H7A H -0.4754 -0.5473 0.1095 0.026 Uiso 1 1 calc R U . . . C7B C -0.3981(3) -0.2875(2) -0.48579(17) 0.0236(4) Uani 1 1 d . . . . . H7B H -0.4662 -0.2330 -0.4645 0.028 Uiso 1 1 calc R U . . . C8A C -0.6815(3) -0.5468(3) 0.15819(18) 0.0291(5) Uani 1 1 d . . . . . H8A H -0.7138 -0.6452 0.1558 0.035 Uiso 1 1 calc R U . . . C8B C -0.4258(3) -0.3780(3) -0.58761(18) 0.0287(5) Uani 1 1 d . . . . . H8B H -0.5132 -0.3854 -0.6355 0.034 Uiso 1 1 calc R U . . . C9A C -0.7762(3) -0.4631(3) 0.18840(18) 0.0317(5) Uani 1 1 d . . . . . H9A H -0.8737 -0.5035 0.2064 0.038 Uiso 1 1 calc R U . . . C9B C -0.3275(3) -0.4569(3) -0.61955(19) 0.0322(5) Uani 1 1 d . . . . . H9B H -0.3463 -0.5181 -0.6895 0.039 Uiso 1 1 calc R U . . . C10A C -0.7281(3) -0.3195(3) 0.19229(19) 0.0302(5) Uani 1 1 d . . . . . H10A H -0.7931 -0.2614 0.2129 0.036 Uiso 1 1 calc R U . . . C10B C -0.2014(3) -0.4467(3) -0.5494(2) 0.0357(6) Uani 1 1 d . . . . . H10B H -0.1337 -0.5015 -0.5711 0.043 Uiso 1 1 calc R U . . . C11A C -0.5859(2) -0.2600(2) 0.16633(18) 0.0248(5) Uani 1 1 d . . . . . H11A H -0.5538 -0.1614 0.1694 0.030 Uiso 1 1 calc R U . . . C11B C -0.1729(3) -0.3574(3) -0.44760(19) 0.0290(5) Uani 1 1 d . . . . . H11B H -0.0859 -0.3513 -0.3998 0.035 Uiso 1 1 calc R U . . . Cl Cl 0.22978(5) -0.25601(5) -0.12266(4) 0.01921(12) Uani 1 1 d . . . . . O1 O 0.15430(19) -0.16512(17) -0.06170(12) 0.0276(4) Uani 1 1 d . . . . . O2 O 0.17607(19) -0.28164(19) -0.23395(13) 0.0314(4) Uani 1 1 d . . . . . O3 O 0.39081(19) -0.1914(2) -0.10117(16) 0.0480(5) Uani 1 1 d . . . . . O4 O 0.1909(3) -0.38821(19) -0.09421(17) 0.0471(5) Uani 1 1 d . . . . . C12 C 0.6765(3) 0.0001(3) 0.3723(2) 0.0360(6) Uani 1 1 d . . . . . H12A H 0.6907 -0.0649 0.3067 0.043 Uiso 1 1 calc R U . . . H12B H 0.5931 -0.0549 0.4030 0.043 Uiso 1 1 calc R U . . . C13 C 0.8222(3) 0.0494(3) 0.4503(2) 0.0365(6) Uani 1 1 d . . . . . H13A H 0.8496 -0.0350 0.4624 0.044 Uiso 1 1 calc R U . . . H13B H 0.9062 0.1031 0.4192 0.044 Uiso 1 1 calc R U . . . C14 C 0.8095(4) 0.1422(4) 0.5549(2) 0.0596(9) Uani 1 1 d . . . . . H14A H 0.9067 0.1696 0.6029 0.089 Uiso 1 1 calc R U . . . H14B H 0.7269 0.0896 0.5863 0.089 Uiso 1 1 calc R U . . . H14C H 0.7866 0.2279 0.5438 0.089 Uiso 1 1 calc R U . . . O5 O 0.63091(19) 0.1137(2) 0.34474(14) 0.0366(4) Uani 1 1 d D . . . . H5 H 0.695(3) 0.164(3) 0.316(2) 0.055 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.01325(17) 0.01377(17) 0.01510(18) 0.00377(13) 0.00192(12) 0.00413(13) N1A 0.0195(8) 0.0164(8) 0.0255(9) 0.0085(7) 0.0042(7) 0.0069(7) N1B 0.0161(8) 0.0248(9) 0.0196(9) 0.0048(7) -0.0003(7) 0.0094(7) C2A 0.0182(10) 0.0195(10) 0.0236(11) 0.0072(8) 0.0029(8) 0.0069(8) C2B 0.0190(10) 0.0195(10) 0.0196(10) 0.0036(8) 0.0036(8) 0.0084(8) N3A 0.0153(8) 0.0157(8) 0.0183(8) 0.0039(7) 0.0017(6) 0.0036(7) N3B 0.0154(8) 0.0176(8) 0.0167(8) 0.0054(7) 0.0021(6) 0.0050(7) C4A 0.0162(9) 0.0168(9) 0.0208(10) 0.0040(8) 0.0022(8) 0.0061(8) C4B 0.0152(9) 0.0191(10) 0.0184(10) 0.0044(8) 0.0049(8) 0.0068(8) C5A 0.0176(9) 0.0171(9) 0.0168(10) 0.0029(8) 0.0009(8) 0.0058(8) C5B 0.0165(9) 0.0177(10) 0.0189(10) 0.0060(8) 0.0046(8) 0.0050(8) C6A 0.0183(10) 0.0219(10) 0.0153(10) 0.0063(8) 0.0010(8) 0.0023(8) C6B 0.0192(10) 0.0211(10) 0.0190(10) 0.0053(8) 0.0039(8) 0.0046(8) C7A 0.0253(11) 0.0204(10) 0.0158(10) 0.0036(8) 0.0019(8) 0.0021(9) C7B 0.0254(11) 0.0257(11) 0.0201(11) 0.0042(9) 0.0026(9) 0.0098(9) C8A 0.0294(12) 0.0276(12) 0.0216(11) 0.0066(9) 0.0018(9) -0.0059(10) C8B 0.0291(12) 0.0349(13) 0.0199(11) 0.0038(10) -0.0026(9) 0.0104(10) C9A 0.0190(11) 0.0447(14) 0.0227(12) 0.0077(10) 0.0030(9) -0.0045(10) C9B 0.0410(14) 0.0339(13) 0.0187(11) -0.0014(10) 0.0017(10) 0.0141(11) C10A 0.0213(11) 0.0431(14) 0.0257(12) 0.0056(10) 0.0041(9) 0.0115(10) C10B 0.0365(13) 0.0431(15) 0.0274(13) -0.0021(11) 0.0037(10) 0.0217(12) C11A 0.0217(11) 0.0265(11) 0.0262(12) 0.0071(9) 0.0029(9) 0.0073(9) C11B 0.0257(11) 0.0358(13) 0.0253(12) 0.0020(10) 0.0003(9) 0.0152(10) Cl 0.0178(2) 0.0193(2) 0.0235(3) 0.00534(19) 0.00553(19) 0.00990(19) O1 0.0343(9) 0.0282(8) 0.0254(8) 0.0026(7) 0.0077(7) 0.0206(7) O2 0.0316(9) 0.0411(10) 0.0222(8) 0.0018(7) 0.0057(7) 0.0167(8) O3 0.0162(8) 0.0836(16) 0.0440(11) 0.0232(11) 0.0047(8) 0.0084(9) O4 0.0707(14) 0.0235(9) 0.0565(13) 0.0167(9) 0.0124(10) 0.0233(9) C12 0.0304(13) 0.0418(15) 0.0347(14) 0.0060(11) 0.0005(10) 0.0134(11) C13 0.0275(12) 0.0491(16) 0.0361(14) 0.0159(12) 0.0012(10) 0.0139(12) C14 0.0510(19) 0.083(2) 0.0316(16) 0.0016(16) -0.0013(13) 0.0109(18) O5 0.0246(9) 0.0572(12) 0.0399(10) 0.0247(9) 0.0082(7) 0.0205(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.9915(16) . ? Cu N3A 1.9916(16) 2 ? Cu N3B 1.9946(16) . ? Cu N3B 1.9946(16) 2 ? N1A C2A 1.337(3) . ? N1A C5A 1.374(3) . ? N1A H1A 0.855(10) . ? N1B C2B 1.336(3) . ? N1B C5B 1.375(3) . ? N1B H1B 0.857(10) . ? C2A N3A 1.315(3) . ? C2A H2A 0.9500 . ? C2B N3B 1.323(3) . ? C2B H2B 0.9500 . ? N3A C4A 1.375(3) . ? N3B C4B 1.374(3) . ? C4A C5A 1.369(3) . ? C4A H4A 0.9500 . ? C4B C5B 1.363(3) . ? C4B H4B 0.9500 . ? C5A C6A 1.463(3) . ? C5B C6B 1.461(3) . ? C6A C11A 1.388(3) . ? C6A C7A 1.393(3) . ? C6B C7B 1.389(3) . ? C6B C11B 1.391(3) . ? C7A C8A 1.388(3) . ? C7A H7A 0.9500 . ? C7B C8B 1.389(3) . ? C7B H7B 0.9500 . ? C8A C9A 1.377(4) . ? C8A H8A 0.9500 . ? C8B C9B 1.376(3) . ? C8B H8B 0.9500 . ? C9A C10A 1.385(4) . ? C9A H9A 0.9500 . ? C9B C10B 1.380(3) . ? C9B H9B 0.9500 . ? C10A C11A 1.384(3) . ? C10A H10A 0.9500 . ? C10B C11B 1.383(3) . ? C10B H10B 0.9500 . ? C11A H11A 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.4184(17) . ? Cl O1 1.4243(15) . ? Cl O4 1.4296(18) . ? Cl O2 1.4392(17) . ? C12 O5 1.427(3) . ? C12 C13 1.503(3) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.498(4) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? O5 H5 0.844(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 . 2 ? N3A Cu N3B 90.47(7) . . ? N3A Cu N3B 89.53(7) 2 . ? N3A Cu N3B 89.53(7) . 2 ? N3A Cu N3B 90.47(7) 2 2 ? N3B Cu N3B 180.0 . 2 ? C2A N1A C5A 108.71(17) . . ? C2A N1A H1A 122.8(17) . . ? C5A N1A H1A 128.0(17) . . ? C2B N1B C5B 108.31(17) . . ? C2B N1B H1B 124.4(18) . . ? C5B N1B H1B 127.2(18) . . ? N3A C2A N1A 110.58(18) . . ? N3A C2A H2A 124.7 . . ? N1A C2A H2A 124.7 . . ? N3B C2B N1B 110.96(18) . . ? N3B C2B H2B 124.5 . . ? N1B C2B H2B 124.5 . . ? C2A N3A C4A 106.34(16) . . ? C2A N3A Cu 124.63(14) . . ? C4A N3A Cu 128.94(13) . . ? C2B N3B C4B 105.65(16) . . ? C2B N3B Cu 129.79(14) . . ? C4B N3B Cu 124.28(13) . . ? C5A C4A N3A 109.54(17) . . ? C5A C4A H4A 125.2 . . ? N3A C4A H4A 125.2 . . ? C5B C4B N3B 110.00(17) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4A C5A N1A 104.83(17) . . ? C4A C5A C6A 131.69(18) . . ? N1A C5A C6A 123.46(18) . . ? C4B C5B N1B 105.06(17) . . ? C4B C5B C6B 130.88(18) . . ? N1B C5B C6B 123.96(18) . . ? C11A C6A C7A 119.03(19) . . ? C11A C6A C5A 119.88(19) . . ? C7A C6A C5A 121.07(19) . . ? C7B C6B C11B 119.0(2) . . ? C7B C6B C5B 121.69(19) . . ? C11B C6B C5B 119.25(19) . . ? C8A C7A C6A 120.2(2) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C8B C7B C6B 120.2(2) . . ? C8B C7B H7B 119.9 . . ? C6B C7B H7B 119.9 . . ? C9A C8A C7A 120.5(2) . . ? C9A C8A H8A 119.8 . . ? C7A C8A H8A 119.8 . . ? C9B C8B C7B 120.4(2) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C8A C9A C10A 119.5(2) . . ? C8A C9A H9A 120.2 . . ? C10A C9A H9A 120.2 . . ? C8B C9B C10B 119.6(2) . . ? C8B C9B H9B 120.2 . . ? C10B C9B H9B 120.2 . . ? C9A C10A C11A 120.4(2) . . ? C9A C10A H10A 119.8 . . ? C11A C10A H10A 119.8 . . ? C9B C10B C11B 120.5(2) . . ? C9B C10B H10B 119.7 . . ? C11B C10B H10B 119.7 . . ? C10A C11A C6A 120.3(2) . . ? C10A C11A H11A 119.8 . . ? C6A C11A H11A 119.8 . . ? C10B C11B C6B 120.2(2) . . ? C10B C11B H11B 119.9 . . ? C6B C11B H11B 119.9 . . ? O3 Cl O1 109.91(12) . . ? O3 Cl O4 110.66(13) . . ? O1 Cl O4 107.82(11) . . ? O3 Cl O2 109.92(11) . . ? O1 Cl O2 109.30(10) . . ? O4 Cl O2 109.19(12) . . ? O5 C12 C13 113.6(2) . . ? O5 C12 H12A 108.9 . . ? C13 C12 H12A 108.9 . . ? O5 C12 H12B 108.9 . . ? C13 C12 H12B 108.9 . . ? H12A C12 H12B 107.7 . . ? C14 C13 C12 113.0(2) . . ? C14 C13 H13A 109.0 . . ? C12 C13 H13A 109.0 . . ? C14 C13 H13B 109.0 . . ? C12 C13 H13B 109.0 . . ? H13A C13 H13B 107.8 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C12 O5 H5 115(2) . . ? _refine_diff_density_max 0.382 _refine_diff_density_min -0.456 _refine_diff_density_rms 0.064 _shelx_res_file ; 04.res created by SHELXL-2014/7 TITL EL50D in P-1 CELL 0.71073 9.1329 10.0787 13.0825 103.496 94.562 105.229 ZERR 1 0.0006 0.0007 0.0008 0.006 0.005 0.006 LATT 1 SFAC C H N O CL CU UNIT 42 48 8 10 2 1 MERG 2 FMAP 2 OMIT -2 54 SIZE 0.21 0.15 0.11 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND BOND $H HTAB L.S. 7 WGHT 0.033700 1.047500 FVAR 4.78925 CU 6 0.000000 0.000000 0.000000 10.50000 0.01325 0.01377 = 0.01510 0.00377 0.00192 0.00413 DFIX 0.86 0.01 N1A H1A N1B H1B N1A 3 -0.222603 -0.341095 0.105770 11.00000 0.01948 0.01644 = 0.02552 0.00851 0.00421 0.00686 H1A 2 -0.223539 -0.422272 0.115503 11.00000 -1.50000 N1B 3 -0.344540 -0.124838 -0.258640 11.00000 0.01615 0.02476 = 0.01958 0.00485 -0.00028 0.00937 H1B 2 -0.432907 -0.126812 -0.287486 11.00000 -1.50000 C2A 1 -0.104573 -0.259370 0.073407 11.00000 0.01818 0.01946 = 0.02358 0.00717 0.00289 0.00689 AFIX 43 H2A 2 -0.009751 -0.279684 0.064786 11.00000 -1.20000 AFIX 0 C2B 1 -0.282483 -0.055242 -0.158121 11.00000 0.01898 0.01951 = 0.01960 0.00365 0.00359 0.00839 AFIX 43 H2B 2 -0.332533 -0.005491 -0.108163 11.00000 -1.20000 AFIX 0 N3A 3 -0.138015 -0.146951 0.055169 11.00000 0.01532 0.01568 = 0.01829 0.00390 0.00175 0.00361 N3B 3 -0.142075 -0.064839 -0.137430 11.00000 0.01544 0.01761 = 0.01672 0.00538 0.00205 0.00502 C4A 1 -0.285444 -0.158492 0.075919 11.00000 0.01620 0.01683 = 0.02082 0.00396 0.00220 0.00606 AFIX 43 H4A 2 -0.340410 -0.092127 0.069471 11.00000 -1.20000 AFIX 0 C4B 1 -0.114327 -0.144216 -0.230544 11.00000 0.01521 0.01915 = 0.01844 0.00442 0.00489 0.00678 AFIX 43 H4B 2 -0.021329 -0.167676 -0.240369 11.00000 -1.20000 AFIX 0 C5A 1 -0.340836 -0.280323 0.107297 11.00000 0.01759 0.01710 = 0.01676 0.00287 0.00091 0.00582 C5B 1 -0.239828 -0.184312 -0.306693 11.00000 0.01648 0.01767 = 0.01895 0.00599 0.00462 0.00505 C6A 1 -0.490027 -0.343847 0.135854 11.00000 0.01828 0.02190 = 0.01534 0.00633 0.00105 0.00234 C6B 1 -0.271099 -0.276522 -0.415004 11.00000 0.01920 0.02109 = 0.01901 0.00529 0.00387 0.00464 C7A 1 -0.539349 -0.488410 0.131221 11.00000 0.02528 0.02041 = 0.01579 0.00359 0.00189 0.00213 AFIX 43 H7A 2 -0.475446 -0.547252 0.109525 11.00000 -1.20000 AFIX 0 C7B 1 -0.398078 -0.287529 -0.485789 11.00000 0.02539 0.02572 = 0.02014 0.00420 0.00264 0.00981 AFIX 43 H7B 2 -0.466201 -0.233004 -0.464484 11.00000 -1.20000 AFIX 0 C8A 1 -0.681528 -0.546789 0.158192 11.00000 0.02943 0.02763 = 0.02159 0.00655 0.00180 -0.00593 AFIX 43 H8A 2 -0.713835 -0.645221 0.155801 11.00000 -1.20000 AFIX 0 C8B 1 -0.425781 -0.377988 -0.587614 11.00000 0.02913 0.03494 = 0.01987 0.00383 -0.00262 0.01043 AFIX 43 H8B 2 -0.513157 -0.385422 -0.635534 11.00000 -1.20000 AFIX 0 C9A 1 -0.776152 -0.463080 0.188401 11.00000 0.01904 0.04468 = 0.02275 0.00774 0.00303 -0.00454 AFIX 43 H9A 2 -0.873655 -0.503534 0.206441 11.00000 -1.20000 AFIX 0 C9B 1 -0.327480 -0.456925 -0.619546 11.00000 0.04097 0.03390 = 0.01866 -0.00137 0.00172 0.01405 AFIX 43 H9B 2 -0.346276 -0.518069 -0.689476 11.00000 -1.20000 AFIX 0 C10A 1 -0.728108 -0.319454 0.192289 11.00000 0.02135 0.04311 = 0.02569 0.00559 0.00407 0.01155 AFIX 43 H10A 2 -0.793130 -0.261368 0.212898 11.00000 -1.20000 AFIX 0 C10B 1 -0.201378 -0.446739 -0.549357 11.00000 0.03646 0.04305 = 0.02741 -0.00213 0.00367 0.02171 AFIX 43 H10B 2 -0.133650 -0.501518 -0.571114 11.00000 -1.20000 AFIX 0 C11A 1 -0.585935 -0.260035 0.166331 11.00000 0.02168 0.02647 = 0.02624 0.00711 0.00286 0.00728 AFIX 43 H11A 2 -0.553842 -0.161386 0.169392 11.00000 -1.20000 AFIX 0 C11B 1 -0.172883 -0.357394 -0.447603 11.00000 0.02573 0.03576 = 0.02534 0.00203 0.00031 0.01516 AFIX 43 H11B 2 -0.085921 -0.351257 -0.399823 11.00000 -1.20000 AFIX 0 CL 5 0.229778 -0.256013 -0.122658 11.00000 0.01777 0.01928 = 0.02351 0.00534 0.00553 0.00990 O1 4 0.154301 -0.165117 -0.061703 11.00000 0.03428 0.02823 = 0.02540 0.00259 0.00769 0.02060 O2 4 0.176072 -0.281638 -0.233948 11.00000 0.03155 0.04108 = 0.02217 0.00183 0.00573 0.01668 O3 4 0.390809 -0.191367 -0.101169 11.00000 0.01620 0.08360 = 0.04401 0.02323 0.00465 0.00837 O4 4 0.190870 -0.388206 -0.094205 11.00000 0.07067 0.02349 = 0.05652 0.01670 0.01242 0.02330 DFIX 0.85 0.01 O5 H5 C12 1 0.676538 0.000080 0.372252 11.00000 0.03042 0.04177 = 0.03467 0.00605 0.00049 0.01337 AFIX 23 H12A 2 0.690688 -0.064870 0.306732 11.00000 -1.20000 H12B 2 0.593140 -0.054911 0.402996 11.00000 -1.20000 AFIX 0 C13 1 0.822222 0.049402 0.450256 11.00000 0.02754 0.04914 = 0.03609 0.01589 0.00122 0.01387 AFIX 23 H13A 2 0.849640 -0.034985 0.462417 11.00000 -1.20000 H13B 2 0.906182 0.103066 0.419182 11.00000 -1.20000 AFIX 0 C14 1 0.809502 0.142162 0.554860 11.00000 0.05104 0.08274 = 0.03165 0.00164 -0.00133 0.01091 AFIX 137 H14A 2 0.906706 0.169628 0.602880 11.00000 -1.50000 H14B 2 0.726867 0.089579 0.586286 11.00000 -1.50000 H14C 2 0.786613 0.227942 0.543825 11.00000 -1.50000 AFIX 0 O5 4 0.630907 0.113745 0.344738 11.00000 0.02465 0.05719 = 0.03990 0.02474 0.00820 0.02051 H5 2 0.694984 0.163874 0.315658 11.00000 -1.50000 HKLF 4 REM EL50D in P-1 REM R1 = 0.0362 for 4106 Fo > 4sig(Fo) and 0.0470 for all 4829 data REM 296 parameters refined using 3 restraints END WGHT 0.0326 1.1077 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y-1, -z HTAB N1A O4_$1 EQIV $2 -x, -y, -z HTAB N1B O5_$2 HTAB C2A O1 HTAB C2B O1_$2 HTAB C4B O2 EQIV $3 -x+1, -y, -z HTAB O5 Cl_$3 HTAB O5 O2_$3 REM Highest difference peak 0.382, deepest hole -0.456, 1-sigma level 0.064 Q1 1 0.2822 -0.3668 -0.0794 11.00000 0.05 0.38 Q2 1 -0.4302 -0.3111 0.1159 11.00000 0.05 0.38 Q3 1 -0.0741 -0.0846 0.0358 11.00000 0.05 0.38 Q4 1 -0.1224 -0.1019 -0.1815 11.00000 0.05 0.37 Q5 1 -0.5253 -0.4073 0.1257 11.00000 0.05 0.32 Q6 1 -0.2594 -0.2317 -0.3647 11.00000 0.05 0.31 Q7 1 -0.1580 -0.1415 -0.2881 11.00000 0.05 0.31 Q8 1 -0.1869 -0.0225 -0.1592 11.00000 0.05 0.30 Q9 1 0.7811 0.2058 0.5174 11.00000 0.05 0.29 Q10 1 -0.3167 -0.2504 -0.4595 11.00000 0.05 0.29 ; 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336.082 1 2 -10 -8 2321.55 297.938 1 2 -10 -7 3035.48 328.879 1 -2 10 6 1207.26 239.775 2 2 -10 -6 1077.40 195.844 1 2 -10 -5 124.898 110.909 1 -2 10 5-128.546 157.554 2 -2 10 4 7.21231 155.811 2 2 -10 -4 235.368 110.438 1 -2 10 3-257.698 147.947 2 2 -10 -3-113.533 87.6736 1 -2 10 2 9288.20 555.595 2 2 -10 -2 10187.2 460.479 1 -2 10 1 3280.72 316.521 2 2 -10 -1 3181.73 243.490 1 2 -10 0 27272.3 750.768 1 -2 10 0 23975.6 873.093 2 2 -10 1 14838.2 510.427 3 -2 10 -1 14953.5 629.263 5 -2 10 -1 14265.0 620.666 2 2 -10 2 8966.73 368.773 3 -2 10 -2 8966.73 458.576 2 -2 10 -2 8871.43 476.662 5 -2 10 -3 38.7875 80.7675 2 2 -10 3-82.5317 70.6606 3 -2 10 -3-206.956 143.532 5 2 -10 4 2553.79 256.246 4 2 -10 4 2472.55 187.947 3 -2 10 -4 3203.22 242.543 2 2 -10 5 239.779 110.374 4 -2 10 -5 178.352 63.7475 2 2 -10 6 51.9958 98.8974 4 -2 10 -6 17.7315 54.9439 2 -2 10 -7-13.2999 42.3570 2 2 -10 7 90.2689 100.486 4 2 -10 8 4332.85 353.306 4 2 -10 9 5809.30 339.510 3 2 -10 9 5770.92 424.975 4 2 -10 10 11472.5 615.864 4 2 -10 10 11464.3 514.694 3 2 -10 11 3100.76 323.074 4 2 -10 11 2777.99 265.584 3 2 -10 12-99.2021 136.611 4 2 -10 12 87.1614 95.7309 3 2 -10 13-146.867 148.132 4 -2 9 10 628.038 158.515 3 -2 9 8-99.3659 151.336 2 -2 9 7-202.231 166.622 2 -2 9 6-38.5935 133.567 2 2 -9 -6-213.977 142.308 1 -2 9 5-160.481 148.388 2 2 -9 -5-80.8957 123.013 1 2 -9 -4 2288.93 229.042 3 -2 9 4 2981.78 313.450 2 2 -9 -4 2763.44 256.014 1 2 -9 -3 14275.7 555.615 1 2 -9 -3 14168.1 565.516 3 -2 9 3 14088.4 674.998 2 2 -9 -2 17639.1 599.115 1 2 -9 -2 16540.2 594.067 3 -2 9 2 16649.1 715.398 2 -2 9 1 22643.8 827.216 2 2 -9 -1 25049.5 706.463 1 2 -9 0 10343.0 398.328 1 -2 9 0 9859.07 468.327 5 -2 9 0 9503.53 485.557 2 -2 9 -1 1812.62 198.187 2 2 -9 1 1983.48 158.336 1 2 -9 1 2104.32 176.591 3 -2 9 -1 1898.03 208.392 5 -2 9 -2 394.875 111.929 2 -2 9 -2 322.211 105.017 5 2 -9 2 402.889 79.3597 3 2 -9 3 628.134 96.2822 3 -2 9 -3 568.458 115.041 2 2 -9 4 4997.47 341.636 4 -2 9 -4 5345.23 290.422 2 -2 9 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34.5734 53.5455 1 2 -7 1 38861.8 805.759 1 -2 7 -1 40251.8 973.353 2 2 -7 1 38682.9 913.620 3 -2 7 -2 35174.4 864.786 2 -2 7 -3 25813.6 670.418 2 -2 7 -4 13047.8 401.777 2 2 -7 4 12193.8 491.299 4 -2 7 -4 11930.4 353.170 1 -2 7 -5 4766.13 200.538 2 -2 7 -5 4595.65 208.233 1 2 -7 5 4361.60 297.003 4 -2 7 -6 457.780 52.6751 2 -2 7 -6 468.720 78.2408 1 2 -7 6 587.699 129.070 4 -2 7 -6 548.990 59.1431 6 2 -7 7 2172.62 224.126 4 -2 7 -7 1869.24 154.007 1 -2 7 -7 1702.35 88.7748 6 2 -7 8 5900.26 376.011 4 2 -7 9 11056.3 539.143 4 2 -7 10 13964.9 586.848 3 2 -7 10 14321.0 639.927 4 2 -7 11 6444.27 437.856 4 2 -7 11 5849.78 390.748 3 2 -7 12 2608.42 282.491 3 2 -7 12 2686.40 300.542 4 2 -7 13 663.335 167.266 4 2 -7 13 446.073 137.643 3 2 -7 14 6735.56 516.407 4 2 -7 14 6594.68 485.112 3 2 -7 15-6.62814 117.536 4 2 -7 15 190.870 132.883 3 2 -7 16 333.018 135.136 3 -2 6 13-19.8451 150.624 3 -2 6 12-347.048 197.308 2 -2 6 12-191.034 161.255 3 -2 6 11 68.8700 136.725 2 -2 6 11-165.903 128.105 3 -2 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48.2485 34.2655 2 -2 6 -5 17.6772 40.5182 1 2 -6 6 10419.3 443.150 4 -2 6 -6 7936.36 196.367 6 2 -6 7 33996.4 945.444 4 2 -6 8 105038. 2156.26 4 2 -6 9 26263.4 814.452 3 2 -6 9 26744.6 864.566 4 2 -6 10 10491.6 506.988 3 2 -6 10 10899.8 541.099 4 2 -6 11 226.815 120.403 4 2 -6 11 166.567 92.2263 3 2 -6 12 129.768 109.899 4 2 -6 12 247.928 121.458 3 2 -6 13-130.668 136.463 4 2 -6 13-153.627 123.191 3 2 -6 14 2330.86 302.942 4 2 -6 14 2112.08 287.309 3 2 -6 15 3902.75 412.728 4 2 -6 15 3573.70 381.357 3 2 -6 16 2282.50 322.124 3 -2 5 13 158.074 129.347 3 -2 5 13 257.129 147.017 2 -2 5 12 4336.52 424.006 3 -2 5 12 4279.39 409.465 2 -2 5 11 3019.93 346.785 3 -2 5 11 2812.95 331.996 2 -2 5 10 6454.58 465.440 2 -2 5 10 6626.57 489.000 3 -2 5 9 3402.32 330.325 3 -2 5 9 3769.64 351.647 2 -2 5 8 1686.28 224.928 2 -2 5 8 2035.27 243.911 3 -2 5 7 76.0035 116.841 2 2 -5 -7 172.899 83.4008 3 -2 5 7 99.0695 86.1313 3 -2 5 6 578.805 135.477 2 -2 5 6 470.595 120.109 3 2 -5 -6 735.511 128.326 5 2 -5 -6 660.650 130.225 3 -2 5 5 9218.46 468.214 2 2 -5 -5 9659.32 399.398 5 -2 5 5 9840.43 458.682 3 2 -5 -5 9695.89 452.024 3 -2 5 4 768.530 131.562 3 2 -5 -4 807.223 109.732 5 -2 5 4 803.017 151.048 2 -2 5 3 12634.4 499.156 2 2 -5 -3 12573.2 419.919 5 2 -5 -2 47269.4 1074.97 3 -2 5 2 46910.2 1096.25 2 2 -5 -1 58156.6 1205.81 3 -2 5 1 58824.2 1232.20 2 -2 5 1 55758.9 1116.53 5 2 -5 0 2642.11 124.685 1 -2 5 0 2433.14 151.521 5 -2 5 0 3086.55 202.598 2 2 -5 0 2567.44 183.320 3 2 -5 1 257.621 44.7736 1 -2 5 -1 511.726 94.1294 2 -2 5 -2 4847.54 221.511 2 -2 5 -3 127.267 50.2107 2 -2 5 -3 80.7650 27.0524 1 2 -5 4 35657.6 867.822 4 -2 5 -4 34833.6 682.227 2 -2 5 -4 34760.1 681.295 1 2 -5 5 18526.0 579.240 4 -2 5 -5 17397.4 371.684 2 2 -5 6 11488.9 460.253 4 2 -5 7 50930.6 1215.58 4 2 -5 8 461.346 125.556 4 -2 5 -8 386.721 118.197 4 2 -5 9-37.2350 107.742 4 2 -5 9-61.4647 95.4349 3 2 -5 10 389.611 121.067 4 2 -5 10 579.746 142.204 3 2 -5 11 2987.09 287.323 3 2 -5 11 2710.69 287.284 4 2 -5 12 13487.9 642.296 3 2 -5 12 14340.4 681.583 4 2 -5 13 163.010 127.577 4 2 -5 13-62.7985 120.048 3 2 -5 14 4523.98 417.100 3 2 -5 14 5398.37 457.645 4 2 -5 15 7174.26 552.364 4 2 -5 15 7400.48 547.827 3 2 -5 16 3610.39 406.913 3 -2 4 14 3059.51 390.003 3 -2 4 14 2762.21 346.652 2 -2 4 13 3135.87 372.686 3 -2 4 13 3346.40 365.859 2 -2 4 12 9766.82 587.710 2 -2 4 12 9877.05 635.605 3 -2 4 11 10992.3 636.603 3 -2 4 11 10422.1 586.593 2 -2 4 10 292.371 123.345 3 -2 4 10 314.361 118.024 2 -2 4 9-162.091 141.547 2 -2 4 9-16.2644 123.696 3 -2 4 8 20.1027 107.823 3 -2 4 8 8.76323 98.1823 2 -2 4 7 85.9393 89.4876 2 -2 4 7 227.739 106.510 3 2 -4 -7 313.133 92.1708 3 2 -4 -6 16858.0 625.653 3 -2 4 6 15780.2 609.838 2 -2 4 6 16810.9 626.111 3 -2 4 5 12174.3 501.416 2 2 -4 -5 12234.2 502.319 3 -2 4 5 12464.5 499.772 3 -2 4 4 13508.2 506.817 2 -2 4 4 13003.9 487.504 3 2 -4 -3 45958.0 1064.85 3 2 -4 -3 45953.1 944.135 5 -2 4 3 48719.3 1082.58 3 -2 4 3 45700.3 1066.88 2 2 -4 -2 39564.3 920.639 3 -2 4 2 40114.6 927.585 2 2 -4 -2 39780.5 808.500 5 -2 4 1 27552.1 680.142 2 2 -4 -1 26434.5 670.748 3 -2 4 1 25943.6 568.196 5 -2 4 0 849.572 117.676 2 -2 4 0 646.669 71.5959 5 -2 4 -1 53029.0 1038.58 2 -2 4 -2 14343.8 355.617 2 -2 4 -2 10547.9 223.081 1 2 -4 3 18311.6 531.017 4 -2 4 -3 18860.1 423.236 2 2 -4 3 18504.4 436.846 2 -2 4 -4 5342.79 171.439 2 2 -4 4 5381.66 271.974 4 2 -4 4 5411.72 185.862 2 2 -4 5 104.134 36.5591 2 2 -4 5 71.5184 72.5257 4 2 -4 6 4660.33 152.958 2 2 -4 6 5615.33 302.552 4 2 -4 7 5273.46 166.622 2 2 -4 7 5859.03 329.308 4 2 -4 8 6022.80 190.557 2 2 -4 8 6048.33 199.300 6 2 -4 8 6201.62 351.720 4 2 -4 9 2332.47 226.996 4 -2 4 -9 2856.52 249.225 4 2 -4 9 2252.27 228.050 3 2 -4 9 2512.65 138.437 6 2 -4 9 2359.11 119.251 2 2 -4 10 4529.87 338.923 3 2 -4 10 4630.24 184.110 2 2 -4 10 5198.74 226.995 6 2 -4 10 5562.78 373.113 4 2 -4 11 17275.2 723.051 4 2 -4 11 18214.0 509.608 6 2 -4 11 16708.2 703.490 3 2 -4 12 7610.20 484.714 4 2 -4 12 6485.49 299.522 6 2 -4 12 7128.12 465.765 3 2 -4 13 14553.3 703.326 3 2 -4 13 14775.2 716.925 4 2 -4 14 6806.46 507.660 4 2 -4 14 6389.85 491.928 3 2 -4 15 7849.68 572.818 3 2 -4 15 8506.49 597.587 4 2 -4 16-13.7888 127.208 3 -2 3 16 6053.21 494.868 2 -2 3 15 4992.56 445.553 2 -2 3 14 2128.20 286.521 2 -2 3 14 2277.24 338.994 3 -2 3 13 1834.51 284.258 3 -2 3 13 859.941 190.905 2 -2 3 12-170.481 149.768 2 -2 3 12 32.4160 116.853 3 -2 3 11 6817.06 487.389 3 -2 3 11 5792.07 411.778 2 -2 3 10 1618.06 218.708 2 -2 3 10 1714.16 238.301 3 -2 3 9 9399.00 487.797 2 -2 3 9 9116.76 520.584 3 2 -3 -8 30879.1 945.785 3 -2 3 8 30197.0 954.006 3 -2 3 8 29062.2 900.382 2 -2 3 7 18470.9 679.962 3 -2 3 7 18181.9 651.163 2 2 -3 -7 19619.4 688.426 3 -2 3 6 30370.3 850.339 2 -2 3 6 31271.7 884.087 3 -2 3 5 6496.84 339.484 3 -2 3 5 6566.54 333.041 2 -2 3 4 43509.1 1007.09 2 -2 3 4 43274.9 1009.94 3 -2 3 3 41191.4 941.867 3 -2 3 3 39957.9 920.994 2 2 -3 -2 13017.5 324.268 5 -2 3 2 13554.4 426.911 2 -2 3 1 12905.8 394.008 2 -2 3 0 12374.3 361.582 2 -2 3 -1 21762.4 495.383 2 2 -3 1 21376.2 502.195 2 -2 3 -2 22146.8 468.104 2 2 -3 2 23212.8 485.512 2 2 -3 3 29998.3 593.466 2 2 -3 3 30387.1 704.547 4 -2 3 -3 29912.9 583.949 2 2 -3 4 27963.9 680.778 4 2 -3 4 26584.8 535.138 2 2 -3 5 38.7288 64.9847 4 2 -3 5 45.3007 28.8840 2 2 -3 6 19629.4 593.680 4 2 -3 6 17979.6 385.556 6 2 -3 6 18991.8 420.019 2 2 -3 7 620.363 119.040 4 2 -3 7 550.985 62.8412 6 2 -3 8 2040.67 128.850 6 2 -3 8 2114.47 206.510 4 2 -3 8 2036.70 204.005 3 2 -3 9 5068.29 339.294 4 2 -3 9 4516.97 320.638 3 2 -3 9 4565.32 216.048 6 -2 3 -9 4789.45 317.100 4 2 -3 10 9322.30 348.808 6 2 -3 10 9706.89 497.429 3 2 -3 10 9947.26 502.472 4 2 -3 11 3631.17 321.806 3 2 -3 11 3107.34 206.262 6 2 -3 11 3841.76 332.467 4 2 -3 12 1903.82 253.928 3 2 -3 12 1689.82 160.983 6 2 -3 12 1787.50 245.385 4 2 -3 13 3686.74 250.889 6 2 -3 13 4147.73 384.229 4 2 -3 13 3965.08 370.599 3 2 -3 14 6130.26 489.913 3 2 -3 14 5763.58 473.987 4 2 -3 15 1584.59 269.886 3 -2 2 16 41.5958 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73325.4 1344.63 4 -2 -5 4 2303.58 139.347 4 2 5 -4 2370.85 200.793 1 -2 -5 3 3381.58 155.860 4 -2 -5 3 3433.60 242.123 1 -2 -5 2 11770.6 308.305 4 -2 -5 2 12761.8 470.554 1 -2 -5 1-140.231 97.5407 1 2 5 -1-83.5833 83.3916 1 2 5 0 18068.6 387.554 3 -2 -5 0 24277.3 675.219 1 2 5 1 6761.61 234.712 3 -2 -5 -1 5905.05 339.289 1 -2 -5 -2 29259.4 851.503 1 -2 -5 -2 30240.4 861.519 5 2 5 2 30371.5 699.641 3 -2 -5 -3 10837.8 486.979 5 -2 -5 -3 10669.0 486.744 1 2 5 3 10816.3 395.944 3 2 5 4 10031.7 411.913 3 -2 -5 -4 9886.35 487.734 1 2 5 5 3703.98 265.419 3 -2 -5 -5 3218.25 286.805 1 2 5 6-28.5623 91.8131 3 -2 -5 -6 124.930 77.1473 4 -2 -5 -7 426.430 101.480 4 2 5 7 346.726 119.549 3 2 5 8 3946.84 337.186 3 2 5 9 8481.47 520.284 3 2 5 10 9470.50 579.075 3 2 5 11 906.279 217.028 3 2 5 12 1200.98 231.973 3 -2 -6 17 3917.98 409.516 3 -2 -6 16 43.9285 118.030 3 -2 -6 15 9924.57 609.248 3 -2 -6 14 8007.76 523.021 3 -2 -6 13 1661.39 229.140 3 2 6 -12-263.498 144.611 6 -2 -6 12-80.2805 115.860 4 -2 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359.566 4 -2 -7 -5 11035.4 583.757 1 2 7 5 11309.2 493.302 3 -2 -7 -5 10026.9 456.453 4 2 7 6 10651.8 519.189 3 -2 -7 -6 10081.9 590.705 1 -2 -7 -7 5654.09 452.951 1 2 7 7 5299.47 385.440 3 2 7 8 1444.41 216.899 3 -2 -7 -8 1471.85 257.841 1 2 7 9 31.8215 106.300 3 -2 -7 -9-300.648 203.108 1 2 7 10 140.746 105.434 3 -2 -8 14 4100.18 383.128 4 2 8 -13 1761.36 220.317 6 -2 -8 13 1733.76 246.442 4 -2 -8 12 2644.47 282.678 4 -2 -8 12 2855.15 250.976 3 2 8 -12 2416.50 240.305 6 2 8 -11 436.253 114.008 6 -2 -8 11 580.660 143.399 4 -2 -8 11 837.102 128.054 3 2 8 -10 2509.48 239.199 6 -2 -8 10 2150.31 175.892 3 -2 -8 10 2368.41 240.797 4 -2 -8 9 4474.55 221.054 3 2 8 -9 5194.16 329.949 6 -2 -8 9 5054.16 326.840 4 -2 -8 8-95.7545 98.3633 4 2 8 -8 70.6954 42.8141 2 2 8 -8 65.6719 86.6734 6 2 8 -7 13037.9 538.182 6 -2 -8 7 13745.4 491.719 4 2 8 -7 12021.5 397.735 2 -2 -8 6 9627.51 388.178 4 -2 -8 5 3686.76 222.456 4 2 8 -4 2215.43 253.467 5 -2 -8 4 2207.81 164.956 4 -2 -8 3 201.668 64.2290 4 2 8 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15834.0 703.975 1 2 10 -1 16380.1 779.346 5 -2 -10 0 5838.66 421.418 1 -2 -10 -1 423.012 140.586 1 -2 -10 -2 78.6819 118.660 1 -2 -10 -3 2502.07 304.912 1 -2 -10 -4-146.615 149.100 1 -2 -10 -5 277.804 148.384 1 2 11 -9 2014.54 247.555 6 2 11 -8 1953.85 238.453 6 2 11 -7 139.434 144.728 5 2 11 -6-197.060 157.167 5 2 11 -5-215.604 154.369 5 2 11 -4 4037.99 411.591 5 2 11 -3 2176.92 306.441 5 -2 -11 3 2099.91 268.175 1 -2 -11 2 3942.87 355.152 1 2 11 -2 3986.43 403.062 5 -2 -11 1 2938.97 311.066 1 -2 -11 0 1099.91 205.544 1 -2 -11 -1 319.456 128.836 1 -2 -11 -2 208.771 121.926 1 -2 -11 -3 134.719 118.958 1 -2 -12 2-245.822 142.230 1 -2 -12 1-138.785 119.740 1 -2 -12 0 1204.22 220.909 1 -2 -12 -1 2777.07 333.271 1 -3 14 -5-342.721 158.421 5 -3 13 1 1594.29 269.638 2 -3 13 0 1872.41 277.466 2 -3 13 -1 1371.10 230.963 2 -3 13 -2 2462.07 295.698 5 3 -13 3 71.0962 101.406 4 -3 13 -3 292.749 157.021 5 3 -13 4 1755.05 260.704 4 -3 13 -4 1845.79 268.269 5 -3 13 -5-56.2781 138.450 5 3 -13 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175.994 2 3 -10 5 1683.91 229.195 4 3 -10 6 741.643 170.152 4 -3 10 -6 1049.84 118.752 2 -3 10 -7 139.101 51.6763 2 3 -10 7 81.7774 99.4711 4 3 -10 8 1344.23 211.790 4 3 -10 9 7531.71 493.049 4 3 -10 10 4795.39 408.331 4 3 -10 11 2883.81 280.985 3 3 -10 11 2773.29 322.177 4 3 -10 12 554.964 164.300 4 3 -10 12 744.137 159.172 3 3 -10 13 361.189 137.357 4 3 -10 13 523.252 156.510 3 3 -10 14 615.221 172.276 3 -3 9 8 5655.64 508.527 2 -3 9 7 644.221 179.275 2 -3 9 6 57.4019 122.814 2 -3 9 5 1954.09 270.545 2 -3 9 4-62.2860 131.387 2 3 -9 -4 24.4557 92.1447 1 3 -9 -3 8512.91 394.053 1 3 -9 -3 8069.92 451.819 3 -3 9 3 8112.52 504.742 2 -3 9 2 1143.91 197.168 2 3 -9 -2 1314.76 181.949 3 3 -9 -2 1285.01 146.294 1 3 -9 -1 5631.38 352.935 3 -3 9 1 6159.31 403.861 2 3 -9 -1 6730.38 299.855 1 3 -9 0 39098.9 1042.25 3 -3 9 0 38097.5 1102.49 2 3 -9 0 40672.8 862.252 1 -3 9 0 39199.6 1012.44 5 -3 9 -1 22132.8 710.883 5 3 -9 1 22459.6 537.375 1 -3 9 -1 22870.0 765.445 2 -3 9 -2 10518.5 473.452 2 -3 9 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30731.5 902.528 3 -4 6 2 29526.1 868.208 2 -4 6 1 191.727 92.7585 2 4 -6 -1-14.2820 70.4951 3 -4 6 0 798.500 134.027 2 -4 6 0 728.378 102.467 6 -4 6 0 579.921 74.1993 5 -4 6 -1 19025.2 586.966 2 -4 6 -1 17574.8 491.486 6 -4 6 -2 2.23637 39.1392 6 -4 6 -2 102.535 67.0755 2 4 -6 3 215.684 70.0960 2 -4 6 -3 214.891 43.8294 6 -4 6 -3 166.023 60.8752 2 -4 6 -4 1790.35 145.478 2 4 -6 4 1451.34 177.704 4 4 -6 4 1627.25 149.857 2 4 -6 5 380.051 81.7105 2 4 -6 5 382.093 115.141 4 -4 6 -5 369.022 77.5940 2 4 -6 6 22259.1 748.359 4 4 -6 6 22607.3 592.042 2 4 -6 7 3200.30 279.881 4 4 -6 7 3454.37 190.231 2 4 -6 8 902.937 98.7095 2 4 -6 8 933.360 177.239 4 4 -6 9 6684.21 429.991 4 4 -6 9 5846.66 239.426 2 4 -6 10 5902.23 416.592 4 4 -6 10 4677.60 203.932 2 4 -6 11 8470.86 519.633 4 4 -6 12 5321.87 429.333 4 4 -6 12 5038.79 407.780 3 4 -6 13 6074.42 481.543 4 4 -6 13 6483.50 490.495 3 4 -6 14 5610.87 481.961 4 4 -6 14 5481.09 467.384 3 4 -6 15 1526.66 265.470 3 -4 5 13 2486.68 327.459 2 -4 5 13 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363.741 5 4 4 -1 8014.15 419.444 1 -4 -4 1 7540.74 396.612 1 4 4 -1 8068.57 406.789 5 -4 -4 0 42443.2 1099.48 1 4 4 0 42268.6 1087.80 5 -4 -4 -1 27732.4 854.900 1 -4 -4 -2 2508.40 249.804 1 -4 -4 -2 1926.68 97.7220 4 4 4 2 2506.97 175.706 3 -4 -4 -2 2376.06 221.614 5 -4 -4 -3 1336.07 100.852 4 -4 -4 -3 1180.83 186.844 1 4 4 3 1277.75 143.784 3 -4 -4 -4 1772.20 135.556 4 -4 -4 -4 1968.22 238.895 1 4 4 4 1760.70 176.184 3 -4 -4 -5 466.674 76.8286 4 -4 -4 -5 564.423 156.460 1 4 4 5 693.331 130.076 3 -4 -4 -6 5008.08 404.025 1 4 4 6 4687.94 324.734 3 -4 -4 -7 2838.99 228.797 4 4 4 7 2767.09 271.329 3 -4 -4 -7 3319.00 343.050 1 4 4 8 8271.53 502.296 3 -4 -4 -8 9308.62 603.049 1 -4 -4 -9 2922.11 351.284 1 4 4 9 3005.42 314.062 3 4 4 10 7.47500 113.058 3 4 4 11 1100.42 228.026 3 4 4 12 217.995 154.136 3 -4 -5 17 110.983 115.292 3 -4 -5 16 304.444 139.943 3 -4 -5 15 1441.14 224.887 3 -4 -5 14 887.133 192.145 3 -4 -5 13 6465.84 442.354 3 4 5 -13 6427.14 441.236 6 4 5 -12 9569.56 531.984 6 -4 -5 12 9902.01 520.970 3 -4 -5 11 5285.31 355.101 3 4 5 -11 5372.63 277.538 2 4 5 -11 4986.16 373.699 6 4 5 -10 3092.75 251.985 4 -4 -5 10 3052.09 260.050 3 4 5 -10 2910.38 205.190 2 4 5 -10 3056.81 284.604 6 4 5 -10 3543.39 257.286 3 4 5 -9 2004.25 191.952 4 -4 -5 9 1750.98 184.774 3 4 5 -9 1804.17 159.688 2 4 5 -9 1827.71 171.385 3 4 5 -9 1549.32 196.656 6 4 5 -8 35.2390 50.7834 4 4 5 -8-79.7473 116.283 6 4 5 -8 83.0117 55.8135 2 4 5 -8 35.7375 54.6467 3 4 5 -7 9365.74 354.149 4 4 5 -7 8842.40 367.548 2 4 5 -7 9316.20 463.218 6 4 5 -7 9331.32 340.445 3 4 5 -6 64.0662 42.9757 4 4 5 -6 218.755 106.434 6 4 5 -6 131.468 69.6134 2 4 5 -6 66.7620 43.8409 3 4 5 -5 243.295 77.2589 2 4 5 -5 179.457 43.8124 3 4 5 -4 51437.8 1112.48 2 4 5 -4 51748.2 1256.56 1 4 5 -3 104812. 1944.38 1 -4 -5 3 103492. 1899.97 1 4 5 -3 107547. 1945.01 5 4 5 -2 40344.5 1058.16 1 -4 -5 2 40389.8 1024.05 1 4 5 -2 41387.2 1059.34 5 4 5 -1 9196.42 465.468 5 -4 -5 1 9533.88 467.506 1 4 5 -1 8725.74 248.819 3 4 5 0 443.530 66.0808 3 4 5 0 407.758 118.154 5 4 5 1 4633.59 217.278 3 -4 -5 -1 4651.85 335.235 1 -4 -5 -2 2327.16 245.370 1 -4 -5 -2 1914.25 98.9198 4 4 5 2 2473.68 174.183 3 -4 -5 -3 938.882 89.4363 4 -4 -5 -3 962.378 183.543 1 4 5 3 987.141 128.533 3 -4 -5 -4 19849.2 535.724 4 -4 -5 -4 20947.5 815.339 1 4 5 4 21088.7 658.720 3 -4 -5 -5 1986.24 260.481 1 4 5 5 2211.27 219.442 3 -4 -5 -6 9531.26 406.725 4 -4 -5 -6 11487.8 628.251 1 4 5 6 10729.4 509.881 3 -4 -5 -7 3649.86 381.522 1 4 5 7 3373.95 301.738 3 -4 -5 -8 2556.58 329.062 1 4 5 8 2213.91 261.148 3 -4 -5 -9 900.153 225.740 1 4 5 9 619.685 165.609 3 4 5 10-13.7664 101.450 3 4 5 11 887.915 209.613 3 -4 -6 15 3145.75 336.879 3 -4 -6 14 2745.44 297.539 3 4 6 -14 2719.45 307.821 6 -4 -6 13 11652.5 584.354 3 4 6 -13 11363.5 604.158 6 -4 -6 12 4929.15 358.154 3 4 6 -12 4426.98 362.097 6 -4 -6 11 310.388 109.435 3 4 6 -11 127.988 110.536 6 4 6 -10-205.188 98.1713 4 4 6 -10-97.1334 111.901 6 4 6 -9-80.5674 79.0345 4 4 6 -9-85.5110 134.150 6 4 6 -8 1685.48 156.354 4 4 6 -8 1751.51 161.543 2 4 6 -8 1387.38 194.207 6 4 6 -7 19312.8 596.585 2 4 6 -7 19805.5 725.611 6 4 6 -6 19216.6 604.858 2 4 6 -6 19164.4 705.908 6 4 6 -5 10813.5 443.115 2 -4 -6 4 1914.46 228.422 1 4 6 -4 1593.16 225.088 5 4 6 -4 1542.49 166.377 2 -4 -6 3 2934.33 275.814 1 4 6 -3 2946.86 285.582 5 -4 -6 2 506.856 131.301 1 4 6 -2 225.451 121.920 5 -4 -6 1 4912.51 353.377 1 4 6 -1 5116.98 368.948 5 4 6 0 13040.3 331.569 3 -4 -6 0 15218.6 637.420 1 4 6 1 3653.06 183.818 3 -4 -6 -1 3467.37 313.655 1 -4 -6 -2 370.050 48.3246 4 4 6 2 657.176 98.7427 3 -4 -6 -2 490.533 145.670 1 -4 -6 -3 17013.6 723.391 1 4 6 3 16324.8 524.252 3 -4 -6 -4 875.637 191.650 1 4 6 4 617.173 122.471 3 -4 -6 -5 1457.41 240.955 1 4 6 5 1390.19 177.464 3 -4 -6 -6 61.6871 117.839 1 4 6 6 211.040 101.727 3 -4 -6 -7 256.656 127.642 1 4 6 7 220.126 105.967 3 -4 -6 -8 2092.72 327.309 1 4 6 8 1949.75 254.269 3 4 6 9 1383.17 225.139 3 4 7 -14 2185.98 281.782 6 4 7 -13 57.9633 100.153 6 4 7 -12-94.0372 132.314 6 4 7 -11-392.817 161.343 6 4 7 -10 8666.72 494.011 6 4 7 -9 15882.2 670.489 6 4 7 -8 8888.57 376.067 2 4 7 -8 8945.99 489.038 6 4 7 -7 18220.0 597.498 2 4 7 -7 19298.9 738.195 6 4 7 -6 4839.40 291.961 2 4 7 -5 4203.52 281.391 2 4 7 -5 5303.77 398.618 5 -4 -7 4 747.844 162.153 1 4 7 -4 744.817 168.039 5 4 7 -3 4610.72 379.386 5 -4 -7 3 5139.86 373.445 1 -4 -7 2 1881.98 229.747 1 4 7 -2 1791.29 242.675 5 -4 -7 1 307.635 124.567 1 4 7 -1 183.850 128.233 5 -4 -7 0 412.382 135.769 1 4 7 1 5301.36 199.739 3 -4 -7 -1 7352.26 464.714 1 4 7 2 18474.7 521.074 3 -4 -7 -2 21044.6 822.919 1 4 7 3 16150.1 534.015 3 -4 -7 -3 18797.8 792.019 1 -4 -7 -4 451.631 153.952 1 4 7 4 411.409 104.998 3 -4 -7 -5-180.943 136.362 1 -4 -7 -6-4.04698 135.421 1 -4 -7 -7 2157.72 316.801 1 4 8 -14 854.683 190.857 6 4 8 -13-93.4296 127.660 6 4 8 -12 144.812 130.476 6 4 8 -11 1456.92 215.495 6 4 8 -10 11101.3 579.438 6 4 8 -9 1367.09 207.076 6 4 8 -8 18057.2 742.326 6 4 8 -7 1087.89 185.124 6 4 8 -6 1875.38 189.910 2 4 8 -6 2709.12 305.695 5 4 8 -5-248.591 145.349 5 -4 -8 4 639.366 163.077 1 4 8 -4 650.310 197.447 5 -4 -8 3 4179.01 365.401 1 4 8 -3 5292.13 421.519 5 -4 -8 2 11280.9 591.403 1 4 8 -2 12190.0 644.819 5 -4 -8 1 9346.28 548.815 1 4 8 -1 9807.85 584.497 5 -4 -8 0-226.923 119.522 1 -4 -8 -1 228.300 135.230 1 -4 -8 -2 165.625 118.967 1 -4 -8 -3 211.598 141.565 1 -4 -8 -4 102.134 120.421 1 -4 -8 -5 3001.95 340.949 1 4 9 -13 338.801 144.803 6 4 9 -12 815.465 179.557 6 4 9 -11 2541.72 283.360 6 4 9 -10 1860.60 255.918 6 4 9 -9 3627.44 339.888 6 4 9 -8 758.583 174.409 6 4 9 -7-56.3383 117.803 6 4 9 -7 90.2785 147.057 5 4 9 -6 26.1622 134.458 5 4 9 -5 29.0425 140.561 5 4 9 -4 8078.11 561.605 5 -4 -9 3 8949.08 557.976 1 4 9 -3 9629.12 606.404 5 -4 -9 2 25520.3 970.688 1 4 9 -2 25906.2 1021.07 5 -4 -9 1 2792.84 318.561 1 -4 -9 0 266.290 130.317 1 -4 -9 -1 872.988 192.137 1 -4 -9 -2-225.607 154.121 1 -4 -9 -3-361.943 166.527 1 4 10 -11 5.31924 105.377 6 4 10 -10 356.978 137.301 6 4 10 -9 348.199 126.687 6 4 10 -8 430.530 155.494 6 4 10 -7 1090.21 209.296 6 4 10 -7 1051.19 235.196 5 4 10 -6 6203.38 517.156 5 4 10 -5 8699.48 605.532 5 4 10 -4 2736.12 350.708 5 -4 -10 3 913.008 210.951 1 4 10 -3 1063.54 221.337 5 -4 -10 2 111.153 112.009 1 4 10 -2-4.61933 129.584 5 -4 -10 1-0.33823 141.029 1 -4 -10 0 2906.16 343.409 1 -4 -10 -1 10113.9 632.497 1 4 11 -9 311.142 146.307 6 4 11 -8 876.076 195.716 6 4 11 -7 692.629 185.951 6 -4 -11 3 1471.92 246.712 1 -4 -11 2 809.087 179.876 1 -5 13 1 59.8533 133.022 2 -5 13 0-185.385 137.581 2 -5 13 -1 3160.59 339.237 2 -5 12 3 701.348 195.960 2 -5 12 2 964.179 207.877 2 -5 12 1 702.124 194.943 2 -5 12 0 1766.41 252.462 2 -5 12 -1 8560.87 521.273 2 -5 12 -2 1864.97 241.461 2 -5 12 -3 3977.14 326.631 2 -5 12 -3 3856.55 304.122 5 5 -12 4 106.092 110.435 4 -5 12 -4 116.307 95.7987 5 5 -12 5-29.0682 131.989 4 -5 12 -5-41.1996 92.8840 5 5 -12 6 85.2800 116.128 4 5 -12 7 1115.34 231.768 4 5 -12 8 645.454 180.877 4 -5 11 5 1409.59 253.589 2 -5 11 4 2703.06 338.470 2 -5 11 3-228.503 158.708 2 -5 11 2 31.0135 115.801 2 -5 11 1 4483.61 388.180 2 -5 11 0 10073.9 564.090 2 -5 11 -1 1715.43 235.861 2 -5 11 -2 1574.78 184.200 5 -5 11 -2 1405.61 208.059 2 -5 11 -3-89.9437 105.757 5 -5 11 -3-148.092 95.7707 2 5 -11 4-157.483 128.291 4 -5 11 -4-67.7007 95.6880 5 -5 11 -4-50.1340 79.6769 2 5 -11 5 427.565 145.183 4 -5 11 -5 456.855 116.406 2 5 -11 6 2834.82 324.482 4 5 -11 7 11109.6 639.637 4 5 -11 8 2476.84 307.689 4 5 -11 9 8943.66 584.365 4 5 -11 10 511.807 179.709 4 -5 10 6 285.945 151.298 2 -5 10 5 55.1241 124.161 2 -5 10 4 1193.13 228.595 2 -5 10 3 4930.36 416.506 2 -5 10 2 13940.0 680.200 2 -5 10 1 23108.4 873.256 2 -5 10 0 3080.99 302.629 2 -5 10 -1 720.433 128.816 6 -5 10 -1 490.061 104.364 5 -5 10 -1 510.336 143.307 2 -5 10 -2 400.397 93.9126 5 -5 10 -2 734.190 150.357 2 -5 10 -3 516.486 107.007 5 -5 10 -3 349.633 106.373 2 5 -10 4 857.038 175.778 4 -5 10 -4 838.343 138.720 2 5 -10 5 1035.40 212.966 4 -5 10 -5 778.852 126.020 2 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5 -9 12 5089.80 450.203 4 5 -9 13 131.819 108.659 3 -5 8 9 742.364 185.906 2 -5 8 8 4390.13 424.087 2 -5 8 7 11768.0 671.074 2 -5 8 6 11174.5 632.433 2 -5 8 5 1405.40 228.583 2 -5 8 4 179.235 113.933 2 -5 8 3 177.182 115.725 2 -5 8 2 348.917 122.219 2 -5 8 2 406.383 117.647 6 -5 8 1 112.418 94.1748 2 5 -8 -1 125.443 26.9249 1 -5 8 1 209.989 82.0598 6 -5 8 0 12867.0 490.238 6 -5 8 0 13435.4 571.869 2 5 -8 0 13779.3 618.287 3 -5 8 -1 18281.6 653.844 2 -5 8 -1 16988.3 546.108 6 -5 8 -1 17837.9 499.565 5 -5 8 -2 14044.6 542.871 2 -5 8 -2 12809.9 428.123 6 -5 8 -3 2623.57 216.967 2 -5 8 -3 2497.87 155.597 6 -5 8 -4 2423.19 203.045 2 5 -8 4 2044.01 239.445 4 -5 8 -4 1989.61 108.935 6 -5 8 -5 30431.5 788.475 2 5 -8 5 29119.2 965.423 4 5 -8 6 359.124 137.215 4 -5 8 -6 414.317 88.8116 2 5 -8 7 4332.14 352.294 4 -5 8 -7 2377.72 98.0381 1 5 -8 8 115.321 108.762 4 5 -8 9-180.328 145.936 4 5 -8 10 905.993 198.095 4 5 -8 11 5614.53 454.863 4 5 -8 12 5319.45 447.353 4 5 -8 13 3099.52 359.220 4 5 -8 13 3947.13 391.736 3 5 -8 14 1112.19 237.630 3 -5 7 10 1059.02 222.000 2 -5 7 9 5088.85 453.444 2 -5 7 8 4041.67 387.029 2 -5 7 7 7111.93 495.207 2 -5 7 6 5260.87 416.519 2 -5 7 5 1690.45 240.661 2 -5 7 4 6859.00 437.830 2 -5 7 3 7583.94 441.465 2 -5 7 3 7112.75 396.645 6 -5 7 2 14340.3 609.114 2 5 -7 -2 15526.3 653.861 3 -5 7 2 15033.2 567.518 6 -5 7 1 31962.6 903.799 2 -5 7 1 32055.2 819.434 6 -5 7 0 14967.3 579.002 2 -5 7 0 13963.9 491.203 6 -5 7 -1 5091.81 314.916 2 -5 7 -1 5220.20 258.830 6 -5 7 -1 5022.20 208.747 5 5 -7 2 95.7150 80.2393 2 -5 7 -2 14.6010 41.6592 6 -5 7 -2 0.15674 68.1333 2 -5 7 -3 11460.4 448.264 2 5 -7 3 10891.5 467.002 2 -5 7 -3 11359.3 326.548 6 5 -7 4 663.010 139.570 4 -5 7 -4 1134.51 137.863 2 5 -7 5 256.469 122.380 4 -5 7 -5 283.358 78.0584 2 5 -7 6 9873.95 502.367 4 -5 7 -6 6946.30 193.667 1 5 -7 7 24899.4 873.662 4 5 -7 7 25642.9 696.853 2 5 -7 8 20717.1 803.746 4 5 -7 8 21016.7 595.585 2 5 -7 9 3795.07 347.871 4 5 -7 9 3309.65 199.764 2 5 -7 10 66.0127 104.803 4 5 -7 11 65.2660 111.705 4 5 -7 12 117.230 114.091 4 5 -7 13 2053.63 286.662 4 5 -7 13 1954.28 285.353 3 5 -7 14 2013.40 308.062 3 -5 6 12-81.3547 125.994 2 -5 6 12 224.385 141.460 3 -5 6 11 12500.0 749.053 3 -5 6 11 13036.8 735.570 2 -5 6 10 8065.46 556.841 2 -5 6 9 2582.93 312.446 2 -5 6 8 2444.25 286.307 2 5 -6 -8 2394.01 202.032 5 -5 6 7 817.499 176.514 2 5 -6 -7 1279.46 138.053 5 -5 6 6 1980.91 241.643 2 5 -6 -6 1826.73 146.772 5 -5 6 5 684.138 156.660 2 -5 6 4 20040.1 748.109 2 -5 6 4 20100.6 710.231 6 -5 6 3 14167.7 596.126 2 5 -6 -3 14294.8 625.524 3 -5 6 3 14466.4 561.266 6 -5 6 2 25355.0 810.690 2 5 -6 -2 26275.7 873.041 3 -5 6 2 25635.2 754.764 6 -5 6 1 23024.8 722.495 2 5 -6 -1 23620.5 783.730 3 5 -6 -1 22597.0 743.469 2 -5 6 1 22941.5 654.424 6 -5 6 0 7560.95 380.329 2 5 -6 0 7594.41 396.861 2 -5 6 0 7265.69 317.574 6 -5 6 -1 2650.36 214.457 2 5 -6 1 2756.22 229.632 2 -5 6 -1 2488.18 164.559 6 5 -6 2 434.543 100.896 2 -5 6 -2 397.845 67.1266 6 -5 6 -2 420.576 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77.0781 4 8 1 -7-69.4275 131.126 6 8 1 -7 138.160 99.6749 5 8 1 -6 76.2472 125.997 6 8 1 -6 8.61088 91.6118 5 8 1 -5 2721.14 293.724 6 8 1 -5 2892.03 235.663 5 8 1 -4 1826.18 237.638 6 8 1 -4 1923.74 194.030 5 8 1 -3 6644.70 431.561 6 -8 -1 2 38.1138 118.234 1 8 1 -2-27.5000 61.0962 4 8 1 -1 14598.7 391.863 4 -8 -1 1 15485.5 655.429 1 8 1 -1 14842.7 646.893 6 8 1 0 10520.8 316.739 4 -8 -1 0 10512.6 535.067 1 8 1 0 10068.1 517.719 6 8 1 1 3622.86 176.020 4 -8 -1 -1 3933.52 339.107 1 8 1 2 37.2165 52.1262 4 -8 -1 -2-39.8238 107.365 1 -8 -1 -3 3709.03 338.161 1 8 1 3 3803.94 214.928 4 -8 -1 -4 8260.95 510.270 1 8 1 4 7881.86 344.441 4 -8 -1 -5 16965.4 767.349 1 8 1 5 16265.8 560.502 4 -8 -1 -6 3081.55 339.790 1 -8 -1 -7 812.906 199.633 1 -8 -1 -8-81.3746 153.556 1 -8 -1 -9 866.535 225.019 1 8 1 9 271.521 144.550 3 -8 -2 13 430.930 133.785 2 8 2 -12 1374.20 260.166 6 -8 -2 12 1094.76 194.418 2 8 2 -11 69.0565 126.073 6 8 2 -10 492.946 165.554 6 8 2 -9 2115.36 287.022 6 8 2 -8-184.751 160.062 6 8 2 -7 2848.06 314.165 6 8 2 -7 2686.43 253.206 5 8 2 -6 4919.18 409.067 6 8 2 -6 4904.14 337.223 5 8 2 -5 10385.6 572.432 6 8 2 -5 9820.16 480.225 5 8 2 -5 9243.13 329.302 4 8 2 -4 33198.1 988.753 3 8 2 -4 32574.5 1057.07 6 8 2 -4 34128.3 954.839 5 8 2 -3 455.628 43.6253 4 8 2 -3 273.768 84.0715 3 8 2 -3 586.264 52.2970 4 -8 -2 2 90.5189 107.796 1 8 2 -2 68.1750 105.240 6 8 2 -1 302.549 117.563 6 -8 -2 1 469.016 138.508 1 -8 -2 0 680.838 161.406 1 -8 -2 -1-233.882 136.554 1 -8 -2 -2 3777.32 345.958 1 -8 -2 -3 15091.5 714.332 1 -8 -2 -4 10726.6 610.976 1 -8 -2 -5 4256.35 400.040 1 -8 -2 -6-136.659 153.357 1 -8 -2 -7 198.015 118.878 1 8 2 7 163.656 128.509 3 8 2 8 866.484 197.410 3 8 2 9 298.649 160.427 3 8 3 -12 46.9825 140.969 6 8 3 -11-385.809 201.586 6 8 3 -10 1257.32 242.344 6 8 3 -9 2611.97 326.717 6 8 3 -8 9099.04 573.751 6 8 3 -8 8461.93 481.767 5 8 3 -7 9982.17 589.717 6 8 3 -7 9307.55 510.128 5 8 3 -6 6048.34 445.592 6 8 3 -6 5977.83 401.521 5 8 3 -5 2062.58 266.484 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440.554 6 9 -2 1 326.343 98.2986 4 9 -2 1 395.152 122.699 6 -9 2 -1 297.553 111.308 1 9 -2 2 26.7231 78.1705 4 9 -2 2 30.0652 82.1407 6 -9 2 -2-15.1107 92.7159 1 -9 2 -3 186.700 100.099 1 9 -2 3 150.477 92.9954 4 9 -2 3-40.5467 84.9030 6 -9 2 -3 86.6339 70.9607 5 9 -2 4 13476.6 553.727 4 9 -2 4 12851.5 556.297 6 -9 2 -4 13347.8 591.369 1 9 -2 5 32789.7 954.468 4 9 -2 5 30286.3 926.814 6 -9 2 -5 33456.5 1028.77 1 9 -2 6 4895.41 343.567 4 9 -2 6 4648.62 324.596 6 -9 2 -6 4788.14 375.678 1 9 -2 7 137.402 115.851 4 -9 2 -7 74.0923 107.469 1 -9 2 -8 18.0667 126.583 1 9 -2 8 120.229 98.3415 4 -9 2 -9 2827.14 330.593 1 9 -2 9 3259.82 321.146 4 -9 2 -10 492.525 168.339 1 -9 1 13 5997.53 485.945 2 -9 1 12 1162.98 212.556 2 -9 1 11-187.702 132.859 2 -9 1 10 145.495 123.752 2 9 -1 -10 264.467 143.481 6 -9 1 9 151.107 117.094 2 9 -1 -9 129.835 141.049 6 -9 1 8 1152.08 210.185 2 9 -1 -8 1591.89 255.440 6 -9 1 7 2696.23 297.318 2 9 -1 -7 2628.51 318.066 6 9 -1 -7 2306.43 178.501 5 -9 1 6 1334.70 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568.940 5 9 4 -5 206.003 135.969 6 9 4 -5-71.5277 130.995 5 9 4 -4-25.8643 115.978 6 9 4 -3 2249.30 300.644 6 -9 -4 2 2008.14 290.010 1 9 4 -2 1609.64 264.306 6 -9 -4 1 3222.25 354.399 1 9 4 -1 3677.66 378.401 6 -9 -4 0 5512.20 475.568 1 -9 -4 -1 7425.45 552.966 1 9 5 -11 1078.73 226.738 5 9 5 -10 1629.78 258.446 5 9 5 -9 739.630 193.085 5 9 5 -8 36.6724 142.181 5 9 5 -7 976.678 202.208 5 9 5 -6 231.762 141.528 5 9 5 -5 364.736 163.016 5 9 6 -7 79.1526 118.894 5 9 6 -6 548.234 185.228 5 9 6 -5 3054.08 373.356 5 -10 11 -2 3266.95 363.085 2 -10 11 -3 8089.08 535.673 2 -10 10 0 1816.89 280.973 2 -10 10 -1 548.171 164.989 2 -10 10 -2 821.281 189.547 2 -10 10 -3 340.351 146.619 2 -10 10 -4 71.2316 96.1498 2 -10 9 2 6852.00 521.490 2 -10 9 1 1703.54 264.312 2 -10 9 0 155.765 123.004 2 -10 9 -1 142.408 123.367 2 -10 9 -2 806.084 193.851 2 10 -9 3 1207.77 245.937 4 -10 9 -3 1514.45 240.253 2 10 -9 4 3201.16 368.218 4 -10 8 4 7766.01 557.290 2 -10 8 3-171.675 145.714 2 -10 8 2-74.4983 123.716 2 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8 4054.79 394.802 4 10 -6 9 3788.13 386.077 4 -10 5 7 249.213 129.027 2 -10 5 6 281.748 153.673 2 -10 5 5 1837.56 273.389 2 -10 5 4 3093.24 340.454 2 -10 5 3 12067.7 650.235 2 -10 5 2 13499.1 685.974 2 -10 5 1 548.715 157.068 2 10 -5 -1 172.438 100.892 6 -10 5 0 50.3603 108.368 2 10 -5 0-108.967 129.718 6 10 -5 1 59.3885 97.2646 6 10 -5 2-104.843 125.387 4 10 -5 2-198.916 129.860 6 10 -5 3 712.719 157.304 4 10 -5 3 525.779 110.944 6 10 -5 4 2568.55 286.819 4 10 -5 5 1897.73 244.608 4 10 -5 6 1242.49 215.870 4 10 -5 7 1544.53 240.530 4 10 -5 8 2174.45 283.890 4 10 -5 9 4434.83 406.757 4 -10 4 8 637.382 186.765 2 -10 4 7 553.416 168.583 2 -10 4 6 4816.20 423.448 2 -10 4 5 6073.42 467.940 2 -10 4 4 3969.52 375.810 2 10 -4 -4 3923.68 365.125 6 -10 4 3 564.121 153.824 2 10 -4 -3 316.295 136.163 6 -10 4 2 914.419 186.328 2 10 -4 -2 778.983 163.799 6 -10 4 1-33.0742 113.276 2 10 -4 -1-180.188 141.571 6 10 -4 0 1627.95 225.008 6 10 -4 1 5151.63 377.337 4 10 -4 1 5745.42 392.403 6 10 -4 2 1750.62 232.233 4 10 -4 2 1742.76 214.946 6 10 -4 3 7884.70 463.123 4 -10 4 -3 8356.12 427.808 1 10 -4 3 7894.34 438.347 6 10 -4 4 17003.1 711.460 4 -10 4 -4 17704.4 652.453 1 10 -4 4 17077.3 653.614 6 -10 4 -5 427.002 114.007 1 10 -4 5 700.204 164.053 4 -10 4 -6 338.474 126.703 1 10 -4 6 47.4776 104.089 4 10 -4 7 988.696 179.089 4 10 -4 8 514.091 151.470 4 10 -4 9 545.714 160.631 4 -10 3 9 5201.67 460.560 2 -10 3 8 7494.57 540.088 2 -10 3 7 6217.18 486.947 2 10 -3 -7 6827.25 524.787 6 -10 3 6 1235.51 224.648 2 10 -3 -6 1127.43 222.192 6 -10 3 5 186.721 124.510 2 10 -3 -5 227.479 136.259 6 -10 3 4 226.846 124.316 2 10 -3 -4 139.442 122.632 6 -10 3 3 230.676 117.943 2 10 -3 -3 93.2327 108.057 6 10 -3 -2 378.435 140.543 6 10 -3 -1 357.155 163.051 6 10 -3 0 20816.4 747.801 4 10 -3 0 19210.4 772.488 6 10 -3 1 12392.9 555.974 4 10 -3 1 11148.9 558.993 6 10 -3 2 6659.37 394.765 4 -10 3 -2 5969.36 379.943 1 10 -3 2 5842.47 385.326 6 10 -3 3 3932.31 307.178 4 -10 3 -3 4346.10 326.856 1 10 -3 3 3834.41 310.583 6 10 -3 4 273.495 111.772 4 10 -3 4 150.578 104.086 6 -10 3 -4-18.4318 101.362 1 -10 3 -5-121.038 113.251 1 10 -3 5-30.5074 101.202 4 10 -3 6 5132.70 370.932 4 -10 3 -6 4313.02 357.618 1 10 -3 7 4702.25 368.082 4 -10 3 -7 4369.23 368.355 1 -10 3 -8 4220.61 376.149 1 -10 2 10 741.243 207.393 2 -10 2 9 3221.78 362.747 2 -10 2 8 198.193 125.216 2 10 -2 -8 79.3340 134.441 6 -10 2 7 1916.77 271.805 2 10 -2 -7 2310.96 310.529 6 -10 2 6 71.6146 113.411 2 10 -2 -6 6.98416 138.431 6 -10 2 5 1036.21 208.545 2 10 -2 -5 779.511 182.538 6 10 -2 -4 4265.59 392.515 6 -10 2 4 4232.28 389.314 2 10 -2 -3 12376.7 644.985 6 10 -2 -2 6306.42 444.425 6 10 -2 -1 2577.83 291.257 6 10 -2 0 4629.46 308.010 4 10 -2 0 3908.08 340.037 6 10 -2 1 189.498 90.9899 4 -10 2 -1 164.832 96.0592 1 10 -2 1 92.8595 97.2486 6 10 -2 2 100.524 86.5850 4 10 -2 2 135.432 113.569 6 -10 2 -2-185.017 129.287 1 10 -2 3 683.708 140.040 4 10 -2 3 486.398 134.439 6 -10 2 -3 656.341 144.805 1 10 -2 4 3169.93 261.300 4 -10 2 -4 2834.24 293.544 1 10 -2 4 2401.47 251.589 6 -10 2 -5 1806.63 235.679 1 10 -2 5 1630.07 207.385 6 10 -2 6 7793.25 452.569 6 -10 2 -6 8497.94 520.495 1 -10 2 -7 3807.06 367.728 1 -10 2 -8 181.630 140.693 1 -10 2 -9 4942.77 445.408 1 -10 1 10 6406.72 501.148 2 -10 1 9 2095.39 297.043 2 10 -1 -9 2182.29 327.150 6 -10 1 8-37.8931 132.488 2 10 -1 -8-36.0963 134.801 6 -10 1 7 1086.73 210.233 2 10 -1 -7 927.488 211.965 6 10 -1 -6 318.939 153.958 6 -10 1 6 441.250 154.171 2 10 -1 -5 6564.56 493.737 6 10 -1 -4 10856.8 624.585 6 10 -1 -3 13181.3 674.174 6 10 -1 -2 105.646 137.641 6 10 -1 -1 5388.15 309.444 4 10 -1 -1 5615.58 416.363 6 -10 1 0 1004.62 183.316 1 10 -1 0 653.587 113.958 4 10 -1 0 1042.22 204.717 6 10 -1 1 60.2959 106.921 6 -10 1 -1-178.264 131.469 1 10 -1 2 1172.43 201.507 6 -10 1 -2 1469.82 218.054 1 -10 1 -3 1651.49 237.842 1 10 -1 3 1441.77 213.169 6 10 -1 4 2649.19 279.991 6 -10 1 -4 3110.13 323.193 1 -10 1 -5 1822.94 260.314 1 10 -1 5 1560.39 217.109 6 10 -1 6 2183.55 251.456 6 -10 1 -6 2894.83 324.376 1 -10 1 -7-12.9957 115.742 1 -10 1 -8-29.6941 126.228 1 -10 0 11-102.356 130.936 2 -10 0 10 41.2892 112.047 2 10 0 -9 398.190 163.767 6 -10 0 9 529.185 174.716 2 10 0 -8-176.911 170.605 6 10 0 -7 3966.66 402.998 6 10 0 -6 5867.89 483.302 6 10 0 -5 5277.32 450.365 6 10 0 -4 4324.52 396.639 6 10 0 -3 5284.47 434.433 6 10 0 -2 2007.73 264.774 6 10 0 -1 711.905 176.647 6 -10 0 0 1553.91 227.393 1 10 0 0 1428.86 220.603 6 10 0 1 1506.98 226.640 6 -10 0 -1 1376.35 222.036 1 -10 0 -2 5506.67 418.437 1 10 0 2 4571.60 387.269 6 -10 0 -3 7114.91 499.826 1 10 0 3 5570.74 417.985 6 -10 0 -4 1857.89 270.089 1 10 0 4 1454.75 219.840 6 -10 0 -5 611.133 180.357 1 -10 0 -6 328.823 168.778 1 10 1 -8-20.4217 130.535 6 10 1 -7 3299.12 377.424 6 10 1 -6 1913.38 291.770 6 10 1 -5 3865.54 393.481 6 10 1 -4-66.2623 142.162 6 10 1 -3 288.024 152.862 6 10 1 -2 1751.73 267.580 6 -10 -1 1 1035.19 213.058 1 10 1 -1 1464.55 231.502 6 10 1 0 146.640 118.690 6 -10 -1 0 241.786 146.436 1 -10 -1 -1 3134.61 341.336 1 10 1 1 3267.88 332.207 6 -10 -1 -2 5948.07 462.732 1 10 1 2 4959.99 416.881 6 -10 -1 -3-99.7781 134.575 1 10 1 3 84.1995 108.222 6 -10 -1 -4 219.819 145.335 1 -10 -1 -5-25.0236 145.768 1 10 2 -7 798.139 233.941 6 10 2 -7 1017.05 178.106 5 10 2 -6-214.616 157.397 6 10 2 -6-49.7994 92.8588 5 10 2 -5 1112.60 225.038 6 10 2 -4 230.057 138.798 6 10 2 -3 7721.23 538.303 6 10 2 -2 7400.31 525.332 6 -10 -2 1 3228.05 353.130 1 10 2 -1 3100.00 343.894 6 10 2 0 183.003 127.254 6 -10 -2 0 251.186 163.085 1 10 2 1 1231.51 224.370 6 -10 -2 -1 1467.61 257.199 1 -10 -2 -2 154.153 122.706 1 10 2 2 36.6198 120.656 6 -10 -2 -3-168.961 151.643 1 10 3 -7 330.392 126.757 5 10 3 -6 4446.18 369.211 5 10 3 -4 9628.34 625.494 6 10 3 -3 4168.95 410.488 6 10 3 -2 450.802 180.546 6 -10 -3 1-11.6959 130.541 1 10 3 -1 33.4200 114.795 6 10 3 0-91.8600 115.937 6 -10 -3 0 86.5109 133.774 1 10 4 -8 86.0208 108.205 5 10 4 -7 11773.2 643.201 5 10 4 -6 6242.56 475.261 5 10 5 -7 784.843 208.282 5 -11 9 -2-86.0751 141.326 2 -11 8 0 1435.10 252.787 2 -11 8 -1 63.5771 112.900 2 11 -8 2 978.458 222.680 4 -11 8 -2 611.366 168.076 2 11 -8 3 1286.56 247.242 4 -11 7 2-42.6575 140.809 2 -11 7 1 1808.65 279.203 2 -11 7 0 1666.27 260.651 2 -11 7 -1 358.677 154.735 2 11 -7 2 2049.62 300.196 4 11 -7 3 4482.98 419.435 4 11 -7 4 1287.26 247.042 4 11 -7 5 1211.98 215.386 4 11 -7 6 989.417 218.772 4 -11 6 3 1920.87 285.851 2 -11 6 2 761.321 193.369 2 -11 6 1 6306.91 495.053 2 -11 6 0 1955.51 288.801 2 11 -6 1 5547.77 444.566 4 11 -6 2 2092.33 279.390 4 11 -6 3 334.898 126.939 4 11 -6 4 566.204 154.407 4 11 -6 5 66.6928 126.208 4 11 -6 6-60.7285 118.354 4 11 -6 7 5444.10 456.254 4 -11 5 4 5715.14 480.451 2 -11 5 3 3125.08 362.766 2 -11 5 2 12096.1 680.015 2 11 -5 -2 11185.0 624.973 6 11 -5 -1 2029.98 263.618 6 -11 5 1 2082.45 279.626 2 11 -5 0 561.977 141.040 6 11 -5 1-246.991 134.212 4 11 -5 1-37.0589 98.5725 6 11 -5 2 470.315 147.221 4 11 -5 2 388.505 123.489 6 11 -5 3 1294.96 217.679 4 11 -5 4 254.343 105.058 4 11 -5 5 956.231 192.386 4 11 -5 6 5655.44 448.173 4 11 -5 7 9265.90 576.301 4 -11 4 5 849.301 211.301 2 11 -4 -5 384.742 179.029 6 -11 4 4 6331.27 497.100 2 11 -4 -4 5199.79 447.458 6 -11 4 3 2381.06 311.416 2 11 -4 -3 1693.96 260.510 6 11 -4 -2 2982.46 321.892 6 11 -4 -1 1022.90 196.148 6 11 -4 0-57.3501 103.641 4 11 -4 0-252.490 134.355 6 11 -4 1 502.673 145.752 4 11 -4 1 610.540 143.711 6 11 -4 2 261.068 129.289 4 11 -4 2 179.662 115.699 6 11 -4 3 4034.29 343.215 4 11 -4 3 4186.59 332.523 6 11 -4 4 2897.77 296.886 4 11 -4 5 4752.68 379.925 4 11 -3 -7 1293.21 260.472 6 11 -3 -6 2141.10 302.600 6 -11 3 5 6712.68 513.076 2 11 -3 -5 6806.40 523.222 6 11 -3 -4 3404.72 360.098 6 -11 3 4 3238.99 361.714 2 11 -3 -3-250.132 182.034 6 11 -3 -2-175.321 150.943 6 11 -3 -1 36.0043 87.7047 4 11 -3 -1 131.790 113.915 6 11 -3 0 924.552 160.817 4 11 -3 0 710.271 168.894 6 11 -3 1 4052.17 318.802 4 11 -3 1 3060.30 311.835 6 11 -3 2 4793.31 380.940 6 -11 3 -3 4556.91 361.865 1 11 -3 3 4572.40 354.553 6 -11 3 -4 4075.34 339.155 1 11 -2 -7 1041.94 219.914 6 11 -2 -6 342.249 142.102 6 -11 2 6 352.228 162.640 2 11 -2 -5-90.6379 132.021 6 11 -2 -4-219.238 165.376 6 11 -2 -3 774.666 184.638 6 11 -2 -2 6164.53 474.035 6 11 -2 -1 8153.71 528.712 6 11 -2 0 3628.96 351.585 6 11 -2 1 2341.06 275.571 6 -11 2 -2 2190.34 261.741 1 11 -2 2 2182.14 267.624 6 11 -2 3 519.027 140.930 6 -11 2 -3 455.117 140.394 1 11 -2 4 130.067 109.551 6 -11 2 -4-157.264 121.369 1 -11 2 -5 143.828 107.690 1 -11 2 -6 2716.85 310.874 1 11 -1 -6-95.9422 181.450 6 11 -1 -5 1344.43 254.216 6 11 -1 -4 1674.40 266.340 6 11 -1 -3 664.815 183.050 6 11 -1 -2 6056.89 472.196 6 11 -1 -1 2011.45 284.820 6 11 -1 0 2873.23 329.055 6 -11 1 -1 2189.30 279.411 1 11 -1 1 2288.90 283.235 6 11 -1 2 158.148 129.095 6 -11 1 -2-170.137 138.421 1 11 -1 3 99.8580 93.0285 6 -11 1 -3 68.5329 122.228 1 -11 1 -4 1780.57 261.623 1 11 -1 4 1396.90 218.603 6 -11 1 -5 2397.03 311.535 1 11 -1 5 2406.48 288.250 6 11 0 -5 5379.47 479.568 6 11 0 -4 4962.70 446.279 6 11 0 -3 4119.41 404.427 6 11 0 -2 975.938 206.072 6 11 0 -1 291.172 141.392 6 11 0 0 198.341 140.386 6 -11 0 -1 98.5318 141.579 1 11 0 1 144.061 120.977 6 11 0 2 1308.62 233.303 6 -11 0 -2 1928.64 276.405 1 -11 0 -3 3162.78 356.217 1 11 0 3 3497.98 355.763 6 -11 0 -4 11337.9 670.675 1 11 0 4 10082.8 603.634 6 11 0 5 4137.85 383.648 6 11 1 -3 290.870 165.521 6 11 1 -2 90.6925 112.748 6 11 1 -1 176.876 131.051 6 -11 -1 0 1254.18 240.408 1 11 1 0 1161.92 222.618 6 11 1 1 516.524 163.407 6 -11 -1 -1 283.519 156.210 1 11 1 2 3094.10 354.204 6 12 -7 1 512.701 167.304 4 12 -6 0 276.166 162.546 4 12 -6 1 419.435 159.830 4 12 -6 2 260.924 138.443 4 12 -6 3 2796.39 328.355 4 12 -5 -2 4517.64 420.241 6 12 -5 -1 4504.19 398.575 6 12 -5 0 8161.57 538.525 4 12 -5 1 3289.18 339.765 4 12 -4 -4 566.284 194.496 6 12 -4 -3 11346.7 678.190 6 12 -4 -2 2254.96 306.532 6 12 -4 -1 2775.72 322.090 6 12 -4 0 524.227 140.566 6 12 -3 -4 7343.92 556.133 6 12 -3 -3 731.492 194.769 6 12 -3 -2-208.660 160.473 6 12 -3 -1-262.944 169.026 6 12 -3 0 427.332 148.026 6 12 -3 1-62.0229 110.898 6 12 -2 -3-264.267 197.708 6 12 -2 -2 380.723 131.504 6 12 -2 -1-63.2337 156.886 6 12 -2 0 382.006 146.151 6 12 -2 1 5263.98 434.159 6 12 -2 2 4493.39 398.500 6 12 -1 -1 3778.42 388.660 6 12 -1 0 2515.89 316.495 6 12 -1 1 1459.37 240.544 6 -12 1 -2 0.35439 123.983 1 12 -1 2 305.043 135.866 6 0 0 0 0.00 0.00 0 TITL exp_4358-ms in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 9.132924 10.078694 13.082540 103.4960 94.5620 105.2285 ZERR 5.00 0.000575 0.000671 0.000786 0.0054 0.0050 0.0056 LATT 1 SFAC C H N O UNIT 55.00 50.00 5.00 5.00 TREF HKLF 4 END ; _shelx_hkl_checksum 24352 data_6 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C4 H10 O)' _chemical_formula_sum 'C44 H52 Cl2 Cu N8 O10' _chemical_formula_weight 987.37 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.4157(5) _cell_length_b 9.9855(6) _cell_length_c 13.6726(7) _cell_angle_alpha 106.181(5) _cell_angle_beta 96.455(4) _cell_angle_gamma 106.527(5) _cell_volume 1157.64(12) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 3159 _cell_measurement_theta_min 4.8640 _cell_measurement_theta_max 74.0670 _exptl_crystal_description block _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.416 _exptl_crystal_F_000 515 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.09 _exptl_absorpt_coefficient_mu 2.277 _shelx_estimated_absorpt_T_min 0.712 _shelx_estimated_absorpt_T_max 0.821 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.815 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'SuperNova (Cu) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 7216 _diffrn_reflns_av_unetI/netI 0.0489 _diffrn_reflns_av_R_equivalents 0.0346 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.441 _diffrn_reflns_theta_max 68.998 _diffrn_reflns_theta_full 67.684 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measured_fraction_theta_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_point_group_measured_fraction_full 0.986 _reflns_number_total 4229 _reflns_number_gt 3607 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0681P)^2^+2.4911P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4229 _refine_ls_number_parameters 306 _refine_ls_number_restraints 3 _refine_ls_R_factor_all 0.0680 _refine_ls_R_factor_gt 0.0587 _refine_ls_wR_factor_ref 0.1564 _refine_ls_wR_factor_gt 0.1498 _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_restrained_S_all 1.063 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.01616(19) Uani 1 2 d S . P . . N1B N -0.3501(3) -0.1331(3) -0.2577(2) 0.0228(6) Uani 1 1 d D . . . . H1B H -0.437(3) -0.138(5) -0.288(3) 0.034 Uiso 1 1 d D U . . . C2B C -0.2871(4) -0.0627(4) -0.1561(3) 0.0207(7) Uani 1 1 d . . . . . H2B H -0.3346 -0.0139 -0.1068 0.025 Uiso 1 1 calc R U . . . N3B N -0.1511(3) -0.0708(3) -0.1345(2) 0.0190(6) Uani 1 1 d . . . . . C4B C -0.1252(4) -0.1514(4) -0.2265(3) 0.0198(7) Uani 1 1 d . . . . . H4B H -0.0353 -0.1748 -0.2344 0.024 Uiso 1 1 calc R U . . . C5B C -0.2491(4) -0.1922(4) -0.3044(3) 0.0209(7) Uani 1 1 d . . . . . C6B C -0.2794(4) -0.2814(4) -0.4139(3) 0.0250(7) Uani 1 1 d . . . . . C7B C -0.4042(5) -0.2930(5) -0.4852(3) 0.0375(10) Uani 1 1 d . . . . . H7B H -0.4709 -0.2405 -0.4629 0.045 Uiso 1 1 calc R U . . . C8B C -0.4317(6) -0.3808(6) -0.5884(3) 0.0456(11) Uani 1 1 d . . . . . H8B H -0.5178 -0.3890 -0.6361 0.055 Uiso 1 1 calc R U . . . C9B C -0.3351(5) -0.4557(5) -0.6220(3) 0.0428(11) Uani 1 1 d . . . . . H9B H -0.3534 -0.5143 -0.6930 0.051 Uiso 1 1 calc R U . . . C10B C -0.2114(5) -0.4457(5) -0.5523(3) 0.0408(10) Uani 1 1 d . . . . . H10B H -0.1449 -0.4980 -0.5754 0.049 Uiso 1 1 calc R U . . . C11B C -0.1841(4) -0.3597(5) -0.4491(3) 0.0328(9) Uani 1 1 d . . . . . H11B H -0.0992 -0.3541 -0.4016 0.039 Uiso 1 1 calc R U . . . N1A N -0.2190(3) -0.3371(3) 0.1025(2) 0.0232(6) Uani 1 1 d D . . . . H1A H -0.219(5) -0.414(3) 0.119(4) 0.035 Uiso 1 1 d D U . . . C2A C -0.1037(4) -0.2568(4) 0.0722(3) 0.0228(7) Uani 1 1 d . . . . . H2A H -0.0117 -0.2769 0.0660 0.027 Uiso 1 1 calc R U . . . N3A N -0.1358(3) -0.1457(3) 0.0520(2) 0.0188(6) Uani 1 1 d . . . . . C4A C -0.2790(4) -0.1564(4) 0.0700(3) 0.0195(7) Uani 1 1 d . . . . . H4A H -0.3321 -0.0912 0.0613 0.023 Uiso 1 1 calc R U . . . C5A C -0.3327(4) -0.2753(4) 0.1022(2) 0.0194(7) Uani 1 1 d . . . . . C6A C -0.4780(4) -0.3365(4) 0.1297(3) 0.0212(7) Uani 1 1 d . . . . . C7A C -0.5286(4) -0.4809(4) 0.1310(3) 0.0241(7) Uani 1 1 d . . . . . H7A H -0.4679 -0.5421 0.1144 0.029 Uiso 1 1 calc R U . . . C8A C -0.6664(5) -0.5361(4) 0.1562(3) 0.0314(9) Uani 1 1 d . . . . . H8A H -0.6991 -0.6346 0.1577 0.038 Uiso 1 1 calc R U . . . C9A C -0.7573(4) -0.4494(5) 0.1792(3) 0.0330(9) Uani 1 1 d . . . . . H9A H -0.8528 -0.4883 0.1954 0.040 Uiso 1 1 calc R U . . . C10A C -0.7076(5) -0.3052(5) 0.1784(4) 0.0387(10) Uani 1 1 d . . . . . H10A H -0.7692 -0.2447 0.1943 0.046 Uiso 1 1 calc R U . . . C11A C -0.5681(4) -0.2490(5) 0.1545(3) 0.0330(9) Uani 1 1 d . . . . . H11A H -0.5341 -0.1496 0.1551 0.040 Uiso 1 1 calc R U . . . Cl Cl -0.21727(9) 0.26311(9) 0.13288(7) 0.0245(2) Uani 1 1 d . . . . . O1 O -0.1434(3) 0.1819(3) 0.0647(2) 0.0311(6) Uani 1 1 d . . . . . O2 O -0.1656(3) 0.2691(4) 0.2382(2) 0.0433(8) Uani 1 1 d . . . . . O3 O -0.3760(3) 0.1947(4) 0.1031(3) 0.0518(9) Uani 1 1 d . . . . . O4 O -0.1747(5) 0.4106(4) 0.1304(4) 0.0629(11) Uani 1 1 d . . . . . C12 C 0.1393(10) 0.8326(10) 0.3981(6) 0.095(3) Uani 1 1 d . . . . . H12A H 0.0964 0.7445 0.3362 0.142 Uiso 1 1 calc R U . . . H12B H 0.2153 0.9087 0.3818 0.142 Uiso 1 1 calc R U . . . H12C H 0.0584 0.8703 0.4198 0.142 Uiso 1 1 calc R U . . . C13 C 0.2106(8) 0.7945(9) 0.4825(5) 0.0720(19) Uani 1 1 d . . . . . H13A H 0.2796 0.7412 0.4559 0.086 Uiso 1 1 calc R U . . . H13B H 0.1309 0.7264 0.5039 0.086 Uiso 1 1 calc R U . . . C14 C 0.3055(6) 0.9361(7) 0.5838(4) 0.0518(13) Uani 1 1 d . . . . . H14 H 0.3884 1.0044 0.5637 0.062 Uiso 1 1 calc R U . . . C15 C 0.2024(7) 1.0162(7) 0.6278(4) 0.0603(15) Uani 1 1 d . . . . . H15A H 0.1658 1.0587 0.5778 0.091 Uiso 1 1 calc R U . . . H15B H 0.2580 1.0953 0.6930 0.091 Uiso 1 1 calc R U . . . H15C H 0.1161 0.9467 0.6414 0.091 Uiso 1 1 calc R U . . . O5 O 0.3701(3) 0.8788(4) 0.6566(2) 0.0396(7) Uani 1 1 d D . . . . H5 H 0.306(5) 0.829(6) 0.680(4) 0.059 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0162(3) 0.0152(3) 0.0177(3) 0.0068(3) 0.0034(2) 0.0046(3) N1B 0.0214(14) 0.0263(15) 0.0203(14) 0.0040(11) 0.0024(11) 0.0117(12) C2B 0.0216(16) 0.0210(16) 0.0208(16) 0.0054(13) 0.0049(13) 0.0100(13) N3B 0.0214(14) 0.0173(13) 0.0177(13) 0.0066(11) 0.0028(11) 0.0053(11) C4B 0.0182(15) 0.0234(17) 0.0204(16) 0.0084(13) 0.0050(13) 0.0091(13) C5B 0.0211(16) 0.0211(16) 0.0226(17) 0.0079(13) 0.0070(13) 0.0087(13) C6B 0.0240(17) 0.0285(18) 0.0230(17) 0.0074(14) 0.0040(14) 0.0108(15) C7B 0.038(2) 0.053(3) 0.0225(19) 0.0041(17) 0.0020(16) 0.025(2) C8B 0.045(3) 0.062(3) 0.024(2) 0.0010(19) -0.0040(18) 0.027(2) C9B 0.049(3) 0.054(3) 0.0196(18) -0.0010(18) 0.0053(17) 0.021(2) C10B 0.041(2) 0.050(3) 0.031(2) -0.0001(18) 0.0086(18) 0.025(2) C11B 0.0282(19) 0.042(2) 0.0256(18) 0.0034(16) 0.0035(15) 0.0159(17) N1A 0.0248(15) 0.0186(14) 0.0284(15) 0.0131(12) 0.0038(12) 0.0057(12) C2A 0.0192(16) 0.0202(17) 0.0299(18) 0.0116(14) 0.0038(14) 0.0049(13) N3A 0.0170(13) 0.0175(13) 0.0218(13) 0.0086(11) 0.0031(11) 0.0037(11) C4A 0.0171(15) 0.0188(16) 0.0224(16) 0.0074(13) 0.0024(12) 0.0055(13) C5A 0.0187(16) 0.0192(16) 0.0185(15) 0.0057(12) -0.0001(12) 0.0056(13) C6A 0.0208(16) 0.0215(17) 0.0191(15) 0.0085(13) 0.0017(13) 0.0030(13) C7A 0.0279(18) 0.0215(17) 0.0173(15) 0.0042(13) 0.0038(13) 0.0021(14) C8A 0.035(2) 0.0258(19) 0.0214(17) 0.0067(14) 0.0056(15) -0.0067(16) C9A 0.0203(17) 0.042(2) 0.031(2) 0.0136(17) 0.0054(15) -0.0003(16) C10A 0.0249(19) 0.044(2) 0.055(3) 0.024(2) 0.0122(18) 0.0133(18) C11A 0.0237(18) 0.032(2) 0.052(2) 0.0242(18) 0.0102(17) 0.0099(16) Cl 0.0239(4) 0.0237(4) 0.0324(4) 0.0111(3) 0.0105(3) 0.0136(3) O1 0.0402(15) 0.0319(14) 0.0283(13) 0.0084(11) 0.0127(11) 0.0217(12) O2 0.0380(16) 0.069(2) 0.0283(14) 0.0108(14) 0.0109(12) 0.0288(15) O3 0.0216(15) 0.083(3) 0.057(2) 0.0337(19) 0.0085(14) 0.0141(15) O4 0.066(2) 0.0317(18) 0.108(3) 0.0313(19) 0.023(2) 0.0301(17) C12 0.113(6) 0.125(7) 0.062(4) 0.022(4) 0.018(4) 0.070(6) C13 0.071(4) 0.116(6) 0.058(3) 0.031(4) 0.025(3) 0.067(4) C14 0.037(2) 0.085(4) 0.052(3) 0.040(3) 0.014(2) 0.028(3) C15 0.066(4) 0.064(3) 0.047(3) 0.002(2) -0.008(3) 0.040(3) O5 0.0283(15) 0.061(2) 0.0373(16) 0.0202(14) 0.0059(12) 0.0223(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.995(3) 2 ? Cu N3A 1.995(3) . ? Cu N3B 2.005(3) . ? Cu N3B 2.005(3) 2 ? N1B C2B 1.344(4) . ? N1B C5B 1.381(4) . ? N1B H1B 0.858(10) . ? C2B N3B 1.311(4) . ? C2B H2B 0.9500 . ? N3B C4B 1.380(4) . ? C4B C5B 1.368(5) . ? C4B H4B 0.9500 . ? C5B C6B 1.460(5) . ? C6B C11B 1.392(5) . ? C6B C7B 1.395(5) . ? C7B C8B 1.388(6) . ? C7B H7B 0.9500 . ? C8B C9B 1.374(7) . ? C8B H8B 0.9500 . ? C9B C10B 1.380(6) . ? C9B H9B 0.9500 . ? C10B C11B 1.384(6) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? N1A C2A 1.337(5) . ? N1A C5A 1.380(5) . ? N1A H1A 0.858(10) . ? C2A N3A 1.319(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.378(4) . ? C4A C5A 1.363(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.468(5) . ? C6A C11A 1.385(6) . ? C6A C7A 1.389(5) . ? C7A C8A 1.380(5) . ? C7A H7A 0.9500 . ? C8A C9A 1.382(6) . ? C8A H8A 0.9500 . ? C9A C10A 1.385(6) . ? C9A H9A 0.9500 . ? C10A C11A 1.389(6) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? Cl O3 1.412(3) . ? Cl O4 1.423(3) . ? Cl O1 1.433(3) . ? Cl O2 1.446(3) . ? C12 C13 1.465(9) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.622(9) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 O5 1.438(5) . ? C14 C15 1.499(7) . ? C14 H14 1.0000 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? O5 H5 0.827(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 2 . ? N3A Cu N3B 89.10(11) 2 . ? N3A Cu N3B 90.90(11) . . ? N3A Cu N3B 90.90(11) 2 2 ? N3A Cu N3B 89.10(11) . 2 ? N3B Cu N3B 180.0 . 2 ? C2B N1B C5B 108.2(3) . . ? C2B N1B H1B 125(3) . . ? C5B N1B H1B 127(3) . . ? N3B C2B N1B 110.8(3) . . ? N3B C2B H2B 124.6 . . ? N1B C2B H2B 124.6 . . ? C2B N3B C4B 106.5(3) . . ? C2B N3B Cu 131.9(2) . . ? C4B N3B Cu 121.5(2) . . ? C5B C4B N3B 109.4(3) . . ? C5B C4B H4B 125.3 . . ? N3B C4B H4B 125.3 . . ? C4B C5B N1B 105.1(3) . . ? C4B C5B C6B 130.5(3) . . ? N1B C5B C6B 124.4(3) . . ? C11B C6B C7B 118.3(3) . . ? C11B C6B C5B 119.9(3) . . ? C7B C6B C5B 121.8(3) . . ? C8B C7B C6B 120.5(4) . . ? C8B C7B H7B 119.8 . . ? C6B C7B H7B 119.8 . . ? C9B C8B C7B 120.4(4) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C8B C9B C10B 119.8(4) . . ? C8B C9B H9B 120.1 . . ? C10B C9B H9B 120.1 . . ? C9B C10B C11B 120.1(4) . . ? C9B C10B H10B 119.9 . . ? C11B C10B H10B 119.9 . . ? C10B C11B C6B 120.9(4) . . ? C10B C11B H11B 119.6 . . ? C6B C11B H11B 119.6 . . ? C2A N1A C5A 108.6(3) . . ? C2A N1A H1A 124(3) . . ? C5A N1A H1A 128(3) . . ? N3A C2A N1A 110.3(3) . . ? N3A C2A H2A 124.9 . . ? N1A C2A H2A 124.9 . . ? C2A N3A C4A 106.6(3) . . ? C2A N3A Cu 124.5(2) . . ? C4A N3A Cu 128.8(2) . . ? C5A C4A N3A 109.3(3) . . ? C5A C4A H4A 125.3 . . ? N3A C4A H4A 125.3 . . ? C4A C5A N1A 105.1(3) . . ? C4A C5A C6A 131.4(3) . . ? N1A C5A C6A 123.5(3) . . ? C11A C6A C7A 118.8(3) . . ? C11A C6A C5A 119.4(3) . . ? C7A C6A C5A 121.8(3) . . ? C8A C7A C6A 120.6(4) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C7A C8A C9A 120.6(4) . . ? C7A C8A H8A 119.7 . . ? C9A C8A H8A 119.7 . . ? C8A C9A C10A 119.3(4) . . ? C8A C9A H9A 120.4 . . ? C10A C9A H9A 120.4 . . ? C9A C10A C11A 120.1(4) . . ? C9A C10A H10A 119.9 . . ? C11A C10A H10A 119.9 . . ? C6A C11A C10A 120.7(4) . . ? C6A C11A H11A 119.7 . . ? C10A C11A H11A 119.7 . . ? O3 Cl O4 110.8(2) . . ? O3 Cl O1 110.5(2) . . ? O4 Cl O1 109.0(2) . . ? O3 Cl O2 109.75(19) . . ? O4 Cl O2 107.8(2) . . ? O1 Cl O2 108.92(17) . . ? C13 C12 H12A 109.5 . . ? C13 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C13 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C12 C13 C14 113.8(6) . . ? C12 C13 H13A 108.8 . . ? C14 C13 H13A 108.8 . . ? C12 C13 H13B 108.8 . . ? C14 C13 H13B 108.8 . . ? H13A C13 H13B 107.7 . . ? O5 C14 C15 111.9(4) . . ? O5 C14 C13 106.1(4) . . ? C15 C14 C13 109.9(4) . . ? O5 C14 H14 109.6 . . ? C15 C14 H14 109.6 . . ? C13 C14 H14 109.6 . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C14 O5 H5 113(4) . . ? _refine_diff_density_max 1.545 _refine_diff_density_min -0.507 _refine_diff_density_rms 0.087 # start Validation Reply Form _vrf_PLAT094_6 ; RESPONSE: See Response for Alert PLAT971 below. ; _vrf_PLAT971_6 ; RESPONSE: This density peak is near a mildly disordered 2-butanol solvent molecule. ; # end Validation Reply Form _shelx_res_file ; 6.res created by SHELXL-2014/7 TITL EL108B in P-1 CELL 1.54184 9.4157 9.9855 13.6726 106.181 96.455 106.527 ZERR 1 0.0005 0.0006 0.0007 0.005 0.004 0.005 LATT 1 SFAC C H N O CL CU UNIT 44 52 8 10 2 1 MERG 2 FMAP 2 OMIT -2 138 OMIT 1 0 0 SIZE 0.16 0.09 0.09 TEMP -173 ACTA MORE -3 LIST 4 PLAN 10 BOND $H HTAB L.S. 8 WGHT 0.068100 2.491100 FVAR 4.81059 CU 6 0.000000 0.000000 0.000000 10.50000 0.01615 0.01521 = 0.01766 0.00681 0.00336 0.00465 DFIX 0.86 0.01 N1A H1A N1B H1B N1B 3 -0.350120 -0.133050 -0.257682 11.00000 0.02136 0.02626 = 0.02033 0.00401 0.00237 0.01168 H1B 2 -0.437430 -0.137825 -0.287629 11.00000 -1.50000 C2B 1 -0.287117 -0.062735 -0.156133 11.00000 0.02158 0.02096 = 0.02083 0.00537 0.00489 0.01002 AFIX 43 H2B 2 -0.334638 -0.013883 -0.106755 11.00000 -1.20000 AFIX 0 N3B 3 -0.151128 -0.070757 -0.134512 11.00000 0.02136 0.01730 = 0.01769 0.00658 0.00279 0.00526 C4B 1 -0.125185 -0.151384 -0.226461 11.00000 0.01815 0.02339 = 0.02039 0.00840 0.00502 0.00908 AFIX 43 H4B 2 -0.035280 -0.174846 -0.234376 11.00000 -1.20000 AFIX 0 C5B 1 -0.249108 -0.192236 -0.304409 11.00000 0.02110 0.02108 = 0.02264 0.00793 0.00696 0.00866 C6B 1 -0.279440 -0.281352 -0.413875 11.00000 0.02399 0.02855 = 0.02297 0.00736 0.00402 0.01077 C7B 1 -0.404215 -0.293023 -0.485160 11.00000 0.03777 0.05250 = 0.02249 0.00406 0.00204 0.02490 AFIX 43 H7B 2 -0.470885 -0.240544 -0.462905 11.00000 -1.20000 AFIX 0 C8B 1 -0.431668 -0.380765 -0.588382 11.00000 0.04502 0.06244 = 0.02414 0.00095 -0.00401 0.02713 AFIX 43 H8B 2 -0.517758 -0.389037 -0.636099 11.00000 -1.20000 AFIX 0 C9B 1 -0.335080 -0.455750 -0.621985 11.00000 0.04878 0.05352 = 0.01964 -0.00103 0.00528 0.02085 AFIX 43 H9B 2 -0.353400 -0.514323 -0.692976 11.00000 -1.20000 AFIX 0 C10B 1 -0.211431 -0.445741 -0.552350 11.00000 0.04082 0.04952 = 0.03063 -0.00008 0.00863 0.02539 AFIX 43 H10B 2 -0.144905 -0.498010 -0.575353 11.00000 -1.20000 AFIX 0 C11B 1 -0.184131 -0.359728 -0.449083 11.00000 0.02818 0.04195 = 0.02556 0.00343 0.00350 0.01592 AFIX 43 H11B 2 -0.099163 -0.354101 -0.401567 11.00000 -1.20000 AFIX 0 N1A 3 -0.219046 -0.337092 0.102521 11.00000 0.02483 0.01865 = 0.02836 0.01310 0.00380 0.00572 H1A 2 -0.219026 -0.414266 0.118607 11.00000 -1.50000 C2A 1 -0.103684 -0.256796 0.072151 11.00000 0.01916 0.02022 = 0.02995 0.01163 0.00384 0.00493 AFIX 43 H2A 2 -0.011743 -0.276870 0.065959 11.00000 -1.20000 AFIX 0 N3A 3 -0.135764 -0.145669 0.052002 11.00000 0.01700 0.01751 = 0.02177 0.00856 0.00307 0.00369 C4A 1 -0.279028 -0.156399 0.069997 11.00000 0.01715 0.01880 = 0.02240 0.00739 0.00243 0.00551 AFIX 43 H4A 2 -0.332061 -0.091169 0.061316 11.00000 -1.20000 AFIX 0 C5A 1 -0.332749 -0.275252 0.102202 11.00000 0.01872 0.01918 = 0.01847 0.00573 -0.00005 0.00557 C6A 1 -0.478000 -0.336515 0.129687 11.00000 0.02082 0.02146 = 0.01914 0.00850 0.00168 0.00301 C7A 1 -0.528631 -0.480859 0.131009 11.00000 0.02787 0.02154 = 0.01727 0.00423 0.00378 0.00213 AFIX 43 H7A 2 -0.467898 -0.542052 0.114434 11.00000 -1.20000 AFIX 0 C8A 1 -0.666416 -0.536098 0.156198 11.00000 0.03505 0.02577 = 0.02139 0.00667 0.00555 -0.00667 AFIX 43 H8A 2 -0.699079 -0.634563 0.157714 11.00000 -1.20000 AFIX 0 C9A 1 -0.757269 -0.449441 0.179231 11.00000 0.02033 0.04156 = 0.03116 0.01356 0.00544 -0.00029 AFIX 43 H9A 2 -0.852755 -0.488343 0.195447 11.00000 -1.20000 AFIX 0 C10A 1 -0.707634 -0.305234 0.178424 11.00000 0.02491 0.04408 = 0.05452 0.02384 0.01219 0.01328 AFIX 43 H10A 2 -0.769167 -0.244702 0.194285 11.00000 -1.20000 AFIX 0 C11A 1 -0.568090 -0.249016 0.154472 11.00000 0.02371 0.03173 = 0.05173 0.02423 0.01016 0.00989 AFIX 43 H11A 2 -0.534070 -0.149571 0.155088 11.00000 -1.20000 AFIX 0 CL 5 -0.217267 0.263108 0.132885 11.00000 0.02391 0.02366 = 0.03238 0.01111 0.01049 0.01359 O1 4 -0.143408 0.181939 0.064741 11.00000 0.04018 0.03187 = 0.02834 0.00840 0.01271 0.02174 O2 4 -0.165604 0.269103 0.238158 11.00000 0.03796 0.06876 = 0.02835 0.01081 0.01093 0.02876 O3 4 -0.376038 0.194679 0.103062 11.00000 0.02157 0.08250 = 0.05670 0.03368 0.00851 0.01415 O4 4 -0.174691 0.410554 0.130446 11.00000 0.06584 0.03167 = 0.10753 0.03130 0.02276 0.03014 C12 1 0.139298 0.832636 0.398065 11.00000 0.11301 0.12471 = 0.06210 0.02247 0.01784 0.06989 AFIX 137 H12A 2 0.096440 0.744452 0.336151 11.00000 -1.50000 H12B 2 0.215327 0.908732 0.381757 11.00000 -1.50000 H12C 2 0.058445 0.870272 0.419787 11.00000 -1.50000 AFIX 0 C13 1 0.210553 0.794456 0.482499 11.00000 0.07070 0.11640 = 0.05788 0.03127 0.02483 0.06696 AFIX 23 H13A 2 0.279596 0.741160 0.455916 11.00000 -1.20000 H13B 2 0.130910 0.726402 0.503906 11.00000 -1.20000 AFIX 0 C14 1 0.305525 0.936126 0.583839 11.00000 0.03699 0.08502 = 0.05175 0.03985 0.01446 0.02846 AFIX 13 H14 2 0.388399 1.004387 0.563675 11.00000 -1.20000 AFIX 0 C15 1 0.202429 1.016159 0.627785 11.00000 0.06613 0.06427 = 0.04744 0.00223 -0.00790 0.03997 AFIX 137 H15A 2 0.165755 1.058733 0.577753 11.00000 -1.50000 H15B 2 0.258014 1.095325 0.692981 11.00000 -1.50000 H15C 2 0.116116 0.946744 0.641351 11.00000 -1.50000 AFIX 0 DFIX 0.83 0.01 O5 H5 O5 4 0.370076 0.878750 0.656590 11.00000 0.02835 0.06077 = 0.03729 0.02016 0.00592 0.02229 H5 2 0.305612 0.828583 0.680099 11.00000 -1.50000 HKLF 4 REM EL108B in P-1 REM R1 = 0.0587 for 3607 Fo > 4sig(Fo) and 0.0680 for all 4229 data REM 306 parameters refined using 3 restraints END WGHT 0.0674 2.5279 REM Instructions for potential hydrogen bonds EQIV $1 x-1, y-1, z-1 HTAB N1B O5_$1 HTAB C2B O1 EQIV $2 -x, -y, -z HTAB C4B O2_$2 EQIV $3 x, y-1, z HTAB N1A O4_$3 HTAB C2A O1_$2 EQIV $4 -x, -y+1, -z+1 HTAB O5 O2_$4 REM Highest difference peak 1.545, deepest hole -0.507, 1-sigma level 0.087 Q1 1 0.2864 0.8957 0.4832 11.00000 0.05 1.54 Q2 1 0.1276 1.1115 0.6264 11.00000 0.05 0.83 Q3 1 -0.0613 -0.0823 0.0339 11.00000 0.05 0.52 Q4 1 -0.0819 -0.0652 -0.0728 11.00000 0.05 0.43 Q5 1 -0.2623 0.3624 0.0914 11.00000 0.05 0.42 Q6 1 -0.3874 -0.0676 0.0038 11.00000 0.05 0.36 Q7 1 -0.2192 0.1709 -0.0158 11.00000 0.05 0.34 Q8 1 -0.1029 0.0200 -0.0538 11.00000 0.05 0.33 Q9 1 -0.4897 -0.3982 0.1388 11.00000 0.05 0.33 Q10 1 -0.0531 0.1489 0.1183 11.00000 0.05 0.31 ; _shelx_res_checksum 16849 _shelx_hkl_file ; 0 0 -1 170877. 1369.18 1 0 0 -2 53966.0 1119.93 1 0 0 -2 47535.1 939.547 3 0 0 -3 143495. 1968.01 3 0 0 -4 207021. 2735.12 3 0 0 -5 6951.89 609.308 3 0 0 -6 447.226 242.647 3 0 0 -7 31662.3 1540.38 3 0 0 -8 35442.9 1806.06 3 0 0 -9 3172.51 599.914 3 0 0 10 681.430 155.041 16 0 0 -10 1273.26 421.344 3 0 0 11 2881.93 312.959 16 0 0 -11 2711.99 645.027 3 0 0 12 1301.50 235.582 16 0 0 -12 1068.09 195.374 14 0 0 -13 4227.94 349.739 18 0 0 -13 3997.32 330.526 14 0 0 13 4450.92 377.167 16 0 0 14 5323.11 375.038 16 0 0 -14 5024.13 332.830 18 0 0 -15 2675.58 200.412 18 0 1 -15 3714.85 267.148 14 0 1 -14 2190.07 248.129 14 0 -1 14 2151.27 249.695 16 0 1 -14 2187.99 222.672 18 0 1 -13 231.930 128.160 14 0 1 -13 149.065 122.032 18 0 -1 13 281.801 137.304 16 0 1 -12 484.867 141.201 8 0 -1 12 453.386 144.788 16 0 -1 11 129.063 118.993 16 0 1 -11 56.0586 95.0480 8 0 1 -10 17926.0 637.961 8 0 -1 10 19477.8 718.158 16 0 1 -9 19782.5 1383.11 3 0 1 -8 3145.86 516.672 3 0 1 -7 14959.0 1005.32 3 0 1 -6 12476.1 807.176 3 0 1 -5 7351.46 584.024 3 0 1 -4 44397.8 1177.65 3 0 1 -3 53320.0 1038.21 3 0 1 -3 56890.6 1443.41 1 0 1 -2 2228.34 176.527 3 0 1 -2 2543.04 320.288 1 0 1 -1 111466. 1017.71 2 0 1 -1 116381. 1240.13 1 0 1 0 24855.1 558.635 2 0 1 1 10936.6 515.283 2 0 -1 -2 15427.1 644.621 3 0 -1 -3 273408. 3037.25 3 0 -1 -4 49577.8 1550.79 3 0 -1 -5 5838.34 626.123 3 0 -1 -6 33598.0 1531.42 3 0 -1 -7 1825.97 472.950 3 0 -1 -8 4474.52 762.456 3 0 -1 -9 6679.66 948.052 3 0 1 9 6126.11 436.028 16 0 -1 -10 4833.84 833.105 3 0 1 10 5026.43 411.542 16 0 1 11 1502.18 254.923 16 0 1 12 12359.9 634.244 16 0 1 13 6093.44 426.441 16 0 -1 -13 5795.78 402.780 18 0 -1 -14 4034.55 297.070 18 0 1 14 4224.22 264.514 9 0 -1 -15 349.164 87.8462 18 0 2 -16 98.0196 85.2979 14 0 2 -15 332.188 137.101 14 0 2 -14 771.026 157.621 8 0 2 -14 986.560 207.408 14 0 -2 14 876.404 163.370 16 0 -2 13 4238.06 345.569 16 0 2 -13 3972.87 327.496 8 0 2 -12 6293.38 418.223 8 0 -2 12 6405.30 424.777 16 0 2 -11 12309.1 567.013 8 0 -2 11 11650.4 567.018 16 0 2 -10 5074.72 348.734 8 0 2 -9 13.3005 186.661 3 0 2 -8 203.063 203.350 3 0 2 -7 4984.53 548.913 3 0 2 -6 33030.3 1228.18 3 0 2 -5 55302.0 1394.63 3 0 2 -4 4329.39 365.868 3 0 2 -3 37208.7 927.989 2 0 2 -2 9436.54 431.495 2 0 2 -1 41782.3 900.607 2 0 2 0 57675.1 1201.64 2 0 2 1 128886. 2017.63 2 0 -2 -2 370.522 214.230 3 0 -2 -3 50974.9 1492.91 3 0 -2 -4 1303.13 425.511 3 0 -2 -5 120454. 2866.59 3 0 -2 -6 45981.7 1980.55 3 0 -2 -7 36018.3 1897.29 3 0 -2 -8 4331.36 743.652 3 0 2 8 4547.31 367.096 17 0 2 8 4072.12 345.151 16 0 2 9 1261.50 230.258 16 0 -2 -9 874.892 389.892 3 0 2 10 26.5645 144.165 16 0 -2 -10 92.9627 281.871 3 0 2 11 12752.7 659.569 16 0 2 12 15.9952 153.973 16 0 2 13 750.794 140.892 9 0 -2 -13 782.736 187.218 18 0 -2 -14 416.054 117.940 18 0 3 -16 472.326 122.603 14 0 3 -15 3126.21 255.614 8 0 3 -15 3424.01 298.170 14 0 3 -14 3642.31 314.461 8 0 3 -14 3792.62 359.867 14 0 3 -13 1872.25 257.344 8 0 3 -12 5550.27 419.357 8 0 3 -11 86.1436 262.641 5 0 3 -11 6.86206 107.173 8 0 3 -10 4031.25 315.780 8 0 3 -10 4046.66 743.841 5 0 3 -10 3454.20 656.207 2 0 3 -9 16787.1 1253.22 2 0 3 -9 17590.2 1414.70 5 0 3 -8 27424.3 1616.12 5 0 3 -8 25128.3 1388.45 2 0 3 -7 72876.5 2134.80 2 0 3 -7 74585.7 2420.22 5 0 3 -6 6496.91 692.929 5 0 3 -6 7186.17 618.947 2 0 3 -5 2216.15 324.441 2 0 3 -5 1809.55 376.986 5 0 3 -4 415.346 288.382 5 0 3 -4 171.949 148.167 2 0 3 -3 9104.25 666.135 5 0 3 -3 10151.8 570.522 2 0 3 -3 8698.31 634.684 4 0 3 -2 79214.9 1547.08 2 0 3 -2 74744.9 1706.04 4 0 3 -1 254.830 198.985 4 0 3 -1 417.110 196.834 2 0 3 0 2188.29 345.757 2 0 3 1-48.3324 206.920 2 0 -3 -2 3147.64 431.724 3 0 -3 -3-62.4652 197.884 3 0 -3 -4 400.011 286.512 3 0 -3 -5 27066.5 1503.97 3 0 -3 -6 10403.8 1036.50 3 0 3 7 9372.71 524.922 17 0 3 7 9377.37 520.230 16 0 -3 -7 10044.1 1089.16 3 0 -3 -8 14757.6 1442.75 3 0 3 8 14040.3 687.936 17 0 3 8 14512.8 674.680 16 0 3 9 13442.4 669.167 16 0 -3 -9 13177.4 1413.39 3 0 3 10 13402.8 676.504 16 0 3 11 9844.21 565.717 16 0 3 11 9022.57 500.966 9 0 3 12 86.3321 101.288 9 0 -3 -12 95.9632 157.149 18 0 3 13 775.035 117.879 9 0 -3 -13 770.473 164.040 18 0 -3 -14 63.5790 65.4750 18 0 4 -16 5584.89 321.160 14 0 4 -16 5334.38 286.500 8 0 4 -15 2365.79 265.706 14 0 4 -15 2381.38 240.484 8 0 4 -14 393.046 154.157 8 0 4 -14 564.632 185.777 14 0 4 -13 3087.52 320.534 8 0 4 -12 490.265 178.987 8 0 4 -11 101.241 116.352 8 0 4 -11 88.7378 248.571 5 0 4 -10 6478.58 415.314 8 0 4 -10 7435.70 1034.39 5 0 4 -9 17442.6 1443.88 5 0 4 -8 56041.3 2049.17 2 0 4 -8 57729.1 2409.56 5 0 4 -7 46533.3 2027.37 5 0 4 -7 44974.6 1688.69 2 0 4 -7 41113.3 1683.48 4 0 4 -6 32218.3 1438.36 4 0 4 -6 33644.5 1368.57 2 0 4 -6 35940.9 1669.35 5 0 4 -5 6635.50 691.477 5 0 4 -5 5901.17 544.070 2 0 4 -5 5449.30 609.966 4 0 4 -4 51859.3 1694.50 4 0 4 -4 52214.2 1799.65 5 0 4 -4 49161.8 1477.34 2 0 4 -3 1975.77 374.083 4 0 4 -3 2066.59 329.966 2 0 4 -2 5648.12 583.491 4 0 4 -2 5754.37 539.272 2 0 4 -1 20605.7 1007.05 2 0 4 -1 18497.2 1019.79 4 0 4 0 23978.6 1156.24 2 0 4 1 22654.1 1267.07 2 0 -4 -2 33857.3 1484.20 3 0 -4 -3 10913.0 918.533 3 0 -4 -4 14777.8 1152.32 3 0 -4 -5 1623.67 446.812 3 0 4 6 13192.8 639.101 16 0 4 6 12525.6 623.000 17 0 -4 -6 12826.3 1234.18 3 0 4 7 7130.80 492.734 17 0 4 7 7310.70 502.267 16 0 -4 -7 7063.99 988.895 3 0 4 8 4507.24 414.400 16 0 4 8 4348.04 372.748 9 0 4 9 105.520 149.411 16 0 4 9-61.2881 136.418 9 0 4 10 1748.96 240.222 9 0 4 11 626.034 150.530 9 0 -4 -11 604.704 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584.011 17 0 5 4 12210.2 559.061 9 0 -5 -4 10901.4 1113.79 3 0 -5 -5 21697.7 1653.61 3 0 5 5 20630.8 756.171 9 0 5 5 21534.3 838.143 17 0 5 6 8160.11 488.898 9 0 -5 -6 7450.64 1028.27 3 0 5 7 2646.02 298.784 9 0 5 8 8168.97 485.438 9 0 5 9 496.032 165.791 9 0 5 10-39.4580 114.987 9 0 -5 -10 45.5732 139.063 18 0 -5 -11 2636.33 229.579 18 0 5 11 2623.53 211.120 9 0 -5 -12 4191.96 217.795 18 0 6 -16 1017.48 137.456 8 0 6 -16 842.681 132.465 14 0 6 -15 1814.64 216.632 8 0 6 -15 1703.51 212.087 14 0 6 -14 2113.69 258.053 14 0 6 -14 1994.21 254.951 8 0 6 -13 193.476 157.246 8 0 6 -12 4387.48 383.110 8 0 6 -12 3768.85 322.753 15 0 6 -11 13604.3 634.817 8 0 6 -11 12234.2 599.044 15 0 6 -10 2257.23 273.141 8 0 6 -10 2294.56 285.400 15 0 6 -10 2147.72 591.767 5 0 6 -9 1366.03 208.214 8 0 6 -9 1033.15 425.209 5 0 6 -9 945.044 191.841 15 0 6 -8 299.228 124.229 12 0 6 -8 156.501 120.581 15 0 6 -8 365.859 116.015 8 0 6 -7-95.7292 101.595 12 0 6 -7 10.3021 88.7620 15 0 6 -6 61.8527 200.297 4 0 6 -5 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558.270 155.405 6 5 4 -3 406.471 316.526 2 5 4 -2 4707.14 846.135 2 5 4 -2 5084.31 355.811 6 5 4 -1 22300.3 1804.94 2 5 4 -1 22379.8 732.057 6 5 4 0 8422.47 1135.68 2 5 4 0 9008.92 476.608 6 5 4 1 2573.72 706.460 2 5 4 1 3484.30 350.484 6 5 4 2 2352.73 285.510 6 5 4 3 3746.94 333.389 6 5 4 4 5900.57 403.881 6 -5 -4 -4 5629.15 387.644 18 5 4 5 2084.70 263.598 6 -5 -4 -5 2024.71 237.625 18 5 4 6 5289.14 357.978 6 -5 -4 -6 5192.66 343.928 18 -5 -4 -7 3538.35 272.663 18 5 4 7 4325.24 288.279 6 -5 -4 -8 4050.81 244.811 18 5 4 8 5034.77 261.109 6 5 5 -15 784.827 110.624 8 5 5 -14 994.798 150.605 8 5 5 -13 125.176 91.0867 15 5 5 -13 148.734 122.558 8 5 5 -12-16.2889 114.371 15 5 5 -11 8892.73 516.657 15 5 5 -10 14230.7 675.315 15 -5 -5 9 4308.50 353.458 16 -5 -5 8 1859.89 252.348 16 -5 -5 7 1785.41 246.512 16 -5 -5 6 715.243 167.300 7 5 5 -5 54.9030 137.473 6 5 5 -5 116.893 113.064 12 5 5 -5 33.6170 239.708 2 5 5 -4 1671.35 238.606 6 5 5 -4 940.606 466.585 2 5 5 -3 1271.98 503.033 2 5 5 -3 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264.918 11 -8 8 3 5217.17 389.077 17 -8 8 3 5016.18 346.884 11 -8 8 2 10053.4 519.321 11 -8 8 1 2023.48 266.150 11 -8 8 0 3908.05 381.281 11 -8 8 -1 2742.41 332.681 11 -8 8 -2 1207.45 248.850 11 -8 8 -3 316.222 161.551 11 -8 8 -4 1009.76 236.810 11 -8 8 -5 3392.38 264.614 10 -8 8 -5 3306.67 337.019 11 -8 8 -6 2574.07 238.853 10 -8 8 -6 1926.01 240.323 11 -8 8 -7 235.299 81.1080 11 -8 8 -7 834.845 148.971 10 -8 8 -8 855.002 144.818 10 -8 8 -9 827.807 126.805 10 -8 8 -10-7.50350 48.2753 10 -8 7 9 132.767 55.1068 17 -8 7 8 101.080 88.5706 17 -8 7 7 358.376 132.361 17 -8 7 6 167.470 127.843 17 -8 7 5 594.024 171.407 17 -8 7 5 635.725 131.961 11 -8 7 4 8950.10 488.278 13 -8 7 4 7380.57 424.316 11 -8 7 3 12396.0 578.304 13 -8 7 3 11280.1 571.013 11 -8 7 2 95.0127 147.978 11 -8 7 2 297.940 150.690 13 -8 7 1 96.8878 173.975 11 -8 7 1 273.672 135.362 13 -8 7 0 151.535 169.575 11 -8 7 0 226.133 125.765 13 -8 7 -1 186.185 155.819 11 -8 7 -2 10933.4 622.456 11 -8 7 -3 641.520 223.380 11 -8 7 -4 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198.019 69.0498 16 -8 4 10 1436.41 181.748 17 -8 4 10 1345.37 160.316 16 -8 4 9 655.820 153.681 17 -8 4 9 531.461 125.549 16 -8 4 9 698.546 156.343 13 -8 4 8 1267.97 217.624 17 -8 4 8 1450.20 201.271 16 -8 4 8 1266.12 212.052 13 -8 4 7 6703.39 416.948 16 -8 4 7 6851.64 444.916 13 -8 4 6 17.9885 141.692 13 -8 4 5 4881.94 396.106 13 -8 4 4 2522.16 299.820 13 -8 4 4 2476.16 283.443 11 -8 4 3 8065.10 519.342 13 -8 4 3 8260.63 502.026 11 -8 4 2 14796.9 1506.99 1 -8 4 2 14120.9 679.766 13 -8 4 1 7877.81 474.089 18 -8 4 1 7332.00 1080.48 1 -8 4 1 7045.02 488.540 13 -8 4 0 1361.61 257.199 18 -8 4 0 1136.29 503.137 1 -8 4 0 1083.86 206.498 13 -8 4 -1 4043.20 376.131 18 -8 4 -1 3707.19 340.993 13 -8 4 -2 5265.62 432.604 18 -8 4 -3 3585.13 351.056 18 -8 4 -4 62.4424 157.604 18 -8 4 -5 430.005 181.428 18 -8 4 -5 390.698 136.630 10 -8 4 -6 6538.90 443.701 18 -8 4 -6 6943.62 434.707 10 -8 4 -7 21632.1 743.000 18 -8 4 -7 22906.8 761.556 10 -8 4 -8 212.012 118.606 18 -8 4 -8 282.417 138.421 10 -8 4 -9 245.923 102.846 18 -8 4 -9 246.455 106.376 10 -8 4 -10 270.152 96.5263 10 -8 3 12 1462.81 145.372 16 -8 3 11 3686.90 260.015 16 -8 3 10 319.476 107.712 17 -8 3 10 324.971 121.778 16 -8 3 10 223.225 103.366 13 -8 3 9 282.443 119.912 17 -8 3 9 441.077 128.604 16 -8 3 9 571.138 153.763 13 -8 3 8 2432.77 289.445 16 -8 3 8 2845.51 308.460 13 -8 3 7 785.712 185.419 16 -8 3 7 911.200 208.307 13 -8 3 6 331.012 146.812 16 -8 3 6 248.110 154.513 13 -8 3 5 1472.72 222.979 16 -8 3 5 1458.87 245.914 13 -8 3 4 8246.81 507.920 16 -8 3 4 7945.88 521.318 13 -8 3 4 7475.02 456.635 11 -8 3 3 25507.5 1938.04 1 -8 3 2 35749.1 976.251 18 -8 3 2 33319.4 2204.27 1 -8 3 1 27475.3 885.624 18 -8 3 1 29300.5 2089.25 1 -8 3 0 11385.8 576.184 18 -8 3 0 11262.7 1276.43 1 -8 3 -1 1163.56 272.238 18 -8 3 -1 1388.97 508.107 1 -8 3 -2 11885.0 608.201 18 -8 3 -3 662.090 216.860 18 -8 3 -4 6384.39 453.769 18 -8 3 -5 5430.39 417.839 18 -8 3 -6 13567.6 622.411 18 -8 3 -7 73.0476 158.640 18 -8 3 -8 124.558 122.366 18 -8 3 -8 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944.125 215.098 18 -8 2 -8 450.601 162.646 18 -8 2 -9 4498.14 283.100 18 -8 2 -9 4477.47 285.938 10 -8 1 13 59.2083 61.5617 16 -8 1 12 1003.73 156.763 16 -8 1 11 3160.29 280.187 16 -8 1 10 648.261 185.311 16 -8 1 10 460.133 124.302 13 -8 1 9 8675.05 511.590 16 -8 1 9 8120.86 458.259 13 -8 1 8 16240.9 709.871 16 -8 1 8 15100.0 665.285 13 -8 1 7 11845.2 626.785 16 -8 1 6 8930.75 558.925 16 -8 1 5 702.228 193.117 16 -8 1 4 2583.90 315.169 16 -8 1 3 261.844 159.268 18 -8 1 3 314.850 164.452 16 -8 1 3 296.775 283.732 1 -8 1 2 11127.4 564.972 18 -8 1 2 11634.1 1297.88 1 -8 1 1 151.190 312.688 1 -8 1 1 197.806 139.024 18 -8 1 1-145.440 155.282 7 -8 1 0 12953.8 625.373 18 -8 1 0 13146.5 595.904 7 -8 1 -1 4865.29 396.567 18 -8 1 -1 4336.56 348.865 7 -8 1 -2 4313.84 392.130 18 -8 1 -2 3954.71 325.895 7 -8 1 -3 2331.35 314.749 18 -8 1 -4 3516.71 366.279 18 -8 1 -5 4444.05 386.323 18 -8 1 -6 4948.13 391.604 18 -8 1 -7 2118.96 255.082 18 -8 1 -8 2.92530 117.250 18 -8 1 -9-24.3912 73.4412 18 -8 0 13 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312.365 18 -9 -1 -5 2813.71 196.620 18 -9 -2 11 4967.02 260.616 16 -9 -2 10 1005.73 154.186 16 -9 -2 9-18.2137 112.045 16 -9 -2 9-44.9805 59.4044 13 -9 -2 8 237.045 116.332 16 -9 -2 7 702.799 179.816 16 -9 -2 6 2347.62 269.899 16 -9 -2 5 16586.1 673.034 16 -9 -2 4 737.443 206.582 16 -9 -2 3 13262.2 550.140 7 -9 -2 2 1748.13 239.692 7 -9 -2 1 127.929 136.846 7 -9 -2 0 379.038 125.606 7 -9 -2 -1 511.030 126.535 7 -9 -2 -2 492.472 99.5097 18 -9 -3 10 90.6135 71.5186 16 9 3 -10 46.0017 71.7875 15 -9 -3 9-13.6313 78.6118 16 -9 -3 8 4.49538 99.5101 16 -9 -3 7 677.570 158.615 16 -9 -3 6 14348.0 566.309 16 -9 -3 5 4498.77 335.572 16 -9 -3 4 1595.20 222.919 16 -9 -3 4 1624.39 208.527 7 -9 -3 3 2687.64 274.071 16 -9 -3 3 2479.34 241.691 7 -9 -3 2 187.616 119.225 7 -9 -3 1 101.292 107.524 7 -9 -3 0 1368.38 161.703 7 -9 -3 -1 8015.25 316.590 7 9 4 -9 1221.25 133.539 15 -9 -4 8 1145.38 135.593 16 9 4 -8 1233.63 149.771 15 -9 -4 7 3157.00 231.447 16 9 4 -7 3621.60 245.124 15 -9 -4 6 2030.28 204.785 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170.810 11 -10 7 -3 81.0515 110.668 11 -10 7 -4 329.024 122.014 11 -10 7 -5 104.840 81.4180 11 -10 6 7 671.856 107.509 17 -10 6 6-91.4224 83.5001 17 -10 6 5 67.9034 88.4168 13 -10 6 4 683.577 143.864 13 -10 6 3 5245.46 330.956 13 -10 6 3 4701.82 315.297 11 -10 6 2 3996.56 291.422 13 -10 6 2 2881.73 281.331 11 -10 6 1 3838.99 281.625 13 -10 6 1 4142.14 350.832 11 -10 6 0 629.055 178.046 11 -10 6 -1 18.8580 132.822 11 -10 6 -2 165.955 133.442 11 -10 6 -3 1029.00 193.350 11 -10 6 -4 5.76386 99.5558 11 -10 6 -5 5391.81 328.577 11 -10 6 -6 1847.71 174.990 11 -10 5 8 461.967 87.4754 17 -10 5 7 184.917 90.3312 17 -10 5 7 170.583 85.4749 13 -10 5 6 499.565 126.208 13 -10 5 5 2074.89 218.719 13 -10 5 4 6029.28 374.299 13 -10 5 3 13307.3 547.969 13 -10 5 3 9936.10 486.447 11 -10 5 2 5640.54 368.057 13 -10 5 2 6320.01 402.032 11 -10 5 1 125.535 124.583 11 -10 5 1-131.109 103.365 13 -10 5 0 915.015 201.348 11 -10 5 0 643.896 130.088 13 -10 5 -1 107.143 151.235 11 -10 5 -2 324.717 160.966 11 -10 5 -3 874.522 186.402 11 -10 5 -4 4362.54 330.916 11 -10 5 -5 229.539 114.228 11 -10 5 -6 0.10436 63.2357 11 -10 4 8 491.947 98.8413 17 -10 4 8 825.559 125.533 13 -10 4 7-34.7216 75.3163 17 -10 4 7 53.2537 91.3199 13 -10 4 6 7131.52 385.621 13 -10 4 5 1708.29 221.580 13 -10 4 4 1839.75 234.874 13 -10 4 3 205.426 106.923 11 -10 4 3 170.805 131.987 13 -10 4 2 1072.47 201.607 11 -10 4 2 691.482 168.051 13 -10 4 1 120.570 133.242 11 -10 4 1 220.973 127.348 13 -10 4 0 1723.76 206.599 13 -10 4 -2 3931.57 315.417 18 -10 4 -3 9592.75 466.215 18 -10 4 -4 5141.08 325.141 18 -10 4 -5 83.6147 97.5655 18 -10 4 -6 374.957 97.0178 11 -10 4 -6 500.186 101.523 18 -10 3 9 4161.84 229.823 13 -10 3 8 3338.46 222.049 17 -10 3 8 5229.86 292.868 13 -10 3 7 4412.85 304.615 13 -10 3 6 634.909 163.785 13 -10 3 5 5.12644 131.805 13 -10 3 4 912.205 191.699 13 -10 3 3-128.958 95.6726 11 -10 3 3 58.5257 130.061 13 -10 3 2 1678.08 230.934 13 -10 3 1 420.512 137.600 13 -10 3 0 25035.4 757.031 13 -10 3 -1 6286.65 402.333 18 -10 3 -1 5198.18 328.668 13 -10 3 -2 197.828 148.907 18 -10 3 -3 1356.41 211.222 18 -10 3 -4 542.811 146.962 18 -10 3 -5 2995.72 235.307 18 -10 3 -6 6770.08 296.308 18 -10 2 9 3892.76 233.465 16 -10 2 9 4421.65 242.903 13 -10 2 8 420.969 104.066 16 -10 2 8 664.858 132.791 13 -10 2 7 69.3407 80.3992 16 -10 2 7 164.711 112.605 13 -10 2 6 392.853 115.375 16 -10 2 6 682.600 167.503 13 -10 2 5 865.816 153.436 16 -10 2 5 905.018 192.819 13 -10 2 4 7230.68 410.793 16 -10 2 4 8218.60 467.327 13 -10 2 3 11428.3 516.245 16 -10 2 3 14742.4 614.822 13 -10 2 2 1428.83 196.436 16 -10 2 0 599.140 203.870 18 -10 2 -1 526.517 166.784 18 -10 2 -2-39.4263 137.503 18 -10 2 -3 4005.27 303.670 18 -10 2 -4 2358.36 228.845 18 -10 2 -5 3142.13 224.350 18 -10 2 -6 2134.15 161.149 18 -10 1 10 2712.31 184.166 16 -10 1 9 149.121 81.4816 16 -10 1 9 63.3139 63.7427 13 -10 1 8 1317.79 173.389 16 -10 1 8 1324.49 167.555 13 -10 1 7 2816.43 249.558 16 -10 1 7 2709.85 252.661 13 -10 1 6 570.332 137.475 16 -10 1 6 820.424 165.602 13 -10 1 5 10869.6 503.400 16 -10 1 5 11852.9 535.337 13 -10 1 4 9714.54 485.790 16 -10 1 3 3328.30 300.078 16 -10 1 2 158.339 112.160 16 -10 1 1 2744.59 256.873 16 -10 1 0 572.507 183.937 18 -10 1 0 546.246 132.654 16 -10 1 -1-70.0834 124.972 18 -10 1 -1-134.482 78.9175 16 -10 1 -2 1876.21 217.642 18 -10 1 -3 4373.67 292.783 18 -10 1 -4 116.079 95.8585 18 -10 1 -5 366.876 89.2372 18 -10 0 10 299.762 77.8006 16 -10 0 9 1091.10 144.132 16 -10 0 9 768.419 104.690 13 -10 0 8 238.818 109.351 16 -10 0 8 34.9064 75.2279 13 -10 0 7 2647.88 244.017 16 -10 0 7 2781.30 242.930 13 -10 0 6 5928.47 367.388 16 -10 0 6 6347.60 373.999 13 -10 0 5 1569.87 221.685 16 -10 0 4 1121.41 186.249 16 -10 0 3 4646.00 335.116 16 -10 0 2 3749.04 305.969 16 -10 0 1 117.437 104.431 16 -10 0 0 1422.81 187.275 18 -10 0 0 1215.38 168.308 16 -10 0 -1 898.640 149.827 18 -10 0 -1 709.354 129.766 16 -10 0 -2 5727.30 303.492 18 -10 0 -2 2916.95 215.017 16 -10 0 -3 2804.76 206.469 18 -10 0 -4-33.0848 51.9411 18 -10 -1 9 122.348 70.7668 16 -10 -1 8 401.441 108.058 16 -10 -1 8 352.877 95.0229 13 -10 -1 7 4014.95 281.362 16 -10 -1 7 3749.35 257.526 13 -10 -1 6 2519.82 237.220 16 -10 -1 5 1756.15 212.787 16 -10 -1 4 1293.25 194.270 16 -10 -1 3 760.086 162.681 16 -10 -1 2 1075.78 167.956 16 -10 -1 1 781.101 142.080 16 -10 -1 0 742.441 131.604 16 -10 -1 -1 491.165 106.457 16 -10 -1 -2 680.072 97.7337 16 -10 -2 8 483.003 94.9559 16 -10 -2 7 736.052 124.075 16 -10 -2 7 767.608 113.129 13 -10 -2 6 138.051 84.9386 16 -10 -2 5 698.167 135.486 16 -10 -2 4 1371.02 170.762 16 -10 -2 3 7254.31 363.071 16 -10 -2 2 2944.96 234.796 16 -10 -2 1 56.7295 67.2469 16 -10 -2 0-21.4927 51.6049 16 -10 -3 6 2343.05 173.068 16 -10 -3 5 2758.97 195.442 16 -10 -3 4 4035.45 232.768 16 -10 -3 3 292.054 77.0801 16 -11 7 1 200.064 69.5157 11 -11 7 0 475.696 91.9971 11 -11 7 -1 465.973 94.3250 11 -11 7 -2 1304.12 136.647 11 -11 6 2 54.8849 55.1701 11 -11 6 2 58.3800 47.8526 13 -11 6 1 4523.02 262.486 11 -11 6 0 1441.27 164.362 11 -11 6 -1 2115.68 200.461 11 -11 6 -2 77.2165 76.6600 11 -11 6 -3 169.867 76.1757 11 -11 5 6 227.017 66.6493 13 -11 5 5 294.548 84.1035 13 -11 5 4 3004.19 207.611 13 -11 5 3 3837.85 236.262 13 -11 5 2 2504.24 191.223 13 -11 5 2 1439.73 154.714 11 -11 5 1 451.719 132.349 11 -11 5 1 668.441 100.885 13 -11 5 0 602.881 137.761 11 -11 5 -1 196.528 102.544 11 -11 5 -2 106.839 86.8119 11 -11 5 -3 556.434 111.439 11 -11 5 -4 1313.22 137.234 11 -11 4 7 236.159 60.9309 13 -11 4 6 147.978 57.3348 17 -11 4 6 326.850 84.7210 13 -11 4 5 1983.36 173.925 13 -11 4 4 3542.83 241.113 13 -11 4 3 2941.89 224.395 13 -11 4 2 144.580 80.9130 11 -11 4 2 124.780 77.3829 13 -11 4 1 242.229 101.459 11 -11 4 1 196.731 69.0949 13 -11 4 0 185.058 99.4719 11 -11 4 -1 1041.20 156.823 11 -11 4 -2 2479.24 213.794 11 -11 4 -3 4796.16 266.780 11 -11 4 -4 949.018 116.466 11 -11 3 7 2117.91 158.572 13 -11 3 6 5050.55 263.475 13 -11 3 5 6338.90 313.393 13 -11 3 4 667.967 129.454 13 -11 3 3 704.527 134.894 13 -11 3 2-45.7407 69.9722 11 -11 3 2-30.3285 75.6397 13 -11 3 1 904.341 140.629 11 -11 3 1 742.690 119.517 13 -11 3 0 1481.18 180.346 11 -11 3 -1 2782.90 230.114 11 -11 3 -3 676.345 111.511 11 -11 2 7 88.8040 63.0923 13 -11 2 6 52.8579 75.4110 13 -11 2 5-20.6372 78.2775 13 -11 2 4 668.928 137.653 13 -11 2 3 2191.54 211.363 13 -11 2 2 5667.51 308.826 13 -11 2 2 4477.77 256.238 11 -11 2 1 4920.99 267.244 13 -11 2 1 5462.03 298.521 11 -11 2 0 247.237 68.6293 13 -11 1 7 348.106 78.0314 13 -11 1 6 18.7647 63.6324 13 -11 1 5 267.869 65.8475 16 -11 1 5 451.238 103.273 13 -11 1 4 378.940 80.6560 16 -11 1 4 708.650 124.294 13 -11 1 3 590.269 118.855 13 -11 1 2 5538.01 286.314 13 -11 1 1 504.430 95.7307 13 -11 0 6 3419.45 200.553 13 -11 0 5 4731.03 244.836 13 -11 0 4 534.036 91.1330 16 -11 0 4 855.373 122.392 13 -11 0 3 829.820 114.755 13 -11 0 2 117.492 59.6939 13 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 52018 data_7 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C3 H7 N O)' _chemical_formula_sum 'C42 H46 Cl2 Cu N10 O10' _chemical_formula_weight 985.33 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1544(4) _cell_length_b 9.8343(5) _cell_length_c 14.2557(8) _cell_angle_alpha 91.493(4) _cell_angle_beta 107.948(5) _cell_angle_gamma 109.075(5) _cell_volume 1142.38(11) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4143 _cell_measurement_theta_min 4.3940 _cell_measurement_theta_max 28.9180 _exptl_crystal_description block _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.432 _exptl_crystal_F_000 511 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.15 _exptl_absorpt_coefficient_mu 0.663 _shelx_estimated_absorpt_T_min 0.852 _shelx_estimated_absorpt_T_max 0.907 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.757 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 8820 _diffrn_reflns_av_unetI/netI 0.0321 _diffrn_reflns_av_R_equivalents 0.0223 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.034 _diffrn_reflns_theta_max 26.991 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 4905 _reflns_number_gt 4337 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0358P)^2^+1.1070P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4905 _refine_ls_number_parameters 303 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.0434 _refine_ls_R_factor_gt 0.0369 _refine_ls_wR_factor_ref 0.0947 _refine_ls_wR_factor_gt 0.0895 _refine_ls_goodness_of_fit_ref 1.056 _refine_ls_restrained_S_all 1.056 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.5000 0.5000 0.5000 0.01613(10) Uani 1 2 d S . P . . N1B N 0.6099(2) 0.41667(19) 0.24823(12) 0.0206(3) Uani 1 1 d D . . . . H1B H 0.670(3) 0.397(3) 0.2187(17) 0.031 Uiso 1 1 d D U . . . C2B C 0.6479(2) 0.4455(2) 0.34702(15) 0.0204(4) Uani 1 1 d . . . . . H2B H 0.7496 0.4519 0.3948 0.024 Uiso 1 1 calc R U . . . N3B N 0.52469(19) 0.46387(17) 0.36893(12) 0.0176(3) Uani 1 1 d . . . . . C4B C 0.4023(2) 0.4462(2) 0.27900(14) 0.0189(4) Uani 1 1 d . . . . . H4B H 0.2983 0.4532 0.2712 0.023 Uiso 1 1 calc R U . . . C5B C 0.4535(2) 0.4171(2) 0.20304(15) 0.0194(4) Uani 1 1 d . . . . . C6B C 0.3668(3) 0.3892(2) 0.09512(15) 0.0221(4) Uani 1 1 d . . . . . C7B C 0.4091(3) 0.3127(3) 0.03085(16) 0.0283(5) Uani 1 1 d . . . . . H7B H 0.4991 0.2805 0.0560 0.034 Uiso 1 1 calc R U . . . C8B C 0.3192(3) 0.2832(3) -0.07055(17) 0.0352(5) Uani 1 1 d . . . . . H8B H 0.3481 0.2301 -0.1141 0.042 Uiso 1 1 calc R U . . . C9B C 0.1890(3) 0.3300(3) -0.10851(17) 0.0351(5) Uani 1 1 d . . . . . H9B H 0.1276 0.3084 -0.1777 0.042 Uiso 1 1 calc R U . . . C10B C 0.1485(3) 0.4085(3) -0.04507(17) 0.0336(5) Uani 1 1 d . . . . . H10B H 0.0601 0.4425 -0.0709 0.040 Uiso 1 1 calc R U . . . C11B C 0.2362(3) 0.4380(3) 0.05616(16) 0.0285(5) Uani 1 1 d . . . . . H11B H 0.2072 0.4917 0.0993 0.034 Uiso 1 1 calc R U . . . N1A N 0.8173(2) 0.92475(18) 0.57926(12) 0.0191(3) Uani 1 1 d D . . . . H1A H 0.831(3) 1.0142(13) 0.5911(18) 0.029 Uiso 1 1 d D U . . . C2A C 0.6699(2) 0.8184(2) 0.54604(14) 0.0199(4) Uani 1 1 d . . . . . H2A H 0.5681 0.8329 0.5323 0.024 Uiso 1 1 calc R U . . . N3A N 0.6856(2) 0.69092(17) 0.53513(12) 0.0179(3) Uani 1 1 d . . . . . C4A C 0.8516(2) 0.7179(2) 0.56183(14) 0.0182(4) Uani 1 1 d . . . . . H4A H 0.8997 0.6460 0.5608 0.022 Uiso 1 1 calc R U . . . C5A C 0.9366(2) 0.8634(2) 0.59000(14) 0.0183(4) Uani 1 1 d . . . . . C6A C 1.1128(2) 0.9470(2) 0.62694(14) 0.0192(4) Uani 1 1 d . . . . . C7A C 1.1738(3) 1.0970(2) 0.65597(15) 0.0222(4) Uani 1 1 d . . . . . H7A H 1.1000 1.1477 0.6511 0.027 Uiso 1 1 calc R U . . . C8A C 1.3420(3) 1.1724(2) 0.69201(16) 0.0270(5) Uani 1 1 d . . . . . H8A H 1.3823 1.2746 0.7111 0.032 Uiso 1 1 calc R U . . . C9A C 1.4513(3) 1.1004(3) 0.70042(17) 0.0312(5) Uani 1 1 d . . . . . H9A H 1.5661 1.1526 0.7258 0.037 Uiso 1 1 calc R U . . . C10A C 1.3917(3) 0.9511(3) 0.67148(18) 0.0324(5) Uani 1 1 d . . . . . H10A H 1.4660 0.9008 0.6769 0.039 Uiso 1 1 calc R U . . . C11A C 1.2237(3) 0.8752(2) 0.63465(17) 0.0267(5) Uani 1 1 d . . . . . H11A H 1.1839 0.7732 0.6145 0.032 Uiso 1 1 calc R U . . . Cl Cl 0.84244(6) 0.34590(5) 0.62943(4) 0.02129(12) Uani 1 1 d . . . . . O1 O 0.69153(19) 0.35784(18) 0.56906(12) 0.0321(4) Uani 1 1 d . . . . . O2 O 0.8987(3) 0.4350(2) 0.72287(14) 0.0566(6) Uani 1 1 d . . . . . O3 O 0.9597(2) 0.3927(2) 0.5795(2) 0.0617(6) Uani 1 1 d . . . . . O4 O 0.8185(2) 0.19824(19) 0.64519(14) 0.0428(5) Uani 1 1 d . . . . . N2 N 0.8939(2) 0.1620(2) 0.09945(16) 0.0338(5) Uani 1 1 d . . . . . C12 C 0.8756(3) 0.2478(2) 0.16407(16) 0.0249(4) Uani 1 1 d . . . . . H12 H 0.9553 0.2742 0.2289 0.030 Uiso 1 1 calc R U . . . C13 C 0.7800(4) 0.1220(3) -0.0032(2) 0.0506(7) Uani 1 1 d . . . . . H13A H 0.6996 0.1705 -0.0121 0.076 Uiso 1 1 calc R U . . . H13B H 0.7230 0.0165 -0.0169 0.076 Uiso 1 1 calc R U . . . H13C H 0.8412 0.1524 -0.0492 0.076 Uiso 1 1 calc R U . . . C14 C 1.0252(3) 0.1026(3) 0.1280(2) 0.0435(7) Uani 1 1 d . . . . . H14A H 1.0973 0.1449 0.1963 0.065 Uiso 1 1 calc R U . . . H14B H 1.0888 0.1262 0.0827 0.065 Uiso 1 1 calc R U . . . H14C H 0.9780 -0.0032 0.1241 0.065 Uiso 1 1 calc R U . . . O5 O 0.7639(2) 0.29644(19) 0.14732(12) 0.0345(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.01511(17) 0.01507(17) 0.01618(17) -0.00271(12) 0.00430(12) 0.00399(13) N1B 0.0211(8) 0.0242(9) 0.0199(8) 0.0002(7) 0.0084(7) 0.0110(7) C2B 0.0188(9) 0.0204(10) 0.0208(9) -0.0006(7) 0.0048(8) 0.0076(8) N3B 0.0157(8) 0.0166(8) 0.0180(8) -0.0023(6) 0.0042(6) 0.0041(6) C4B 0.0172(9) 0.0178(9) 0.0202(9) -0.0008(7) 0.0051(7) 0.0055(7) C5B 0.0201(9) 0.0170(9) 0.0206(9) 0.0007(7) 0.0064(8) 0.0067(8) C6B 0.0226(10) 0.0224(10) 0.0195(10) 0.0020(8) 0.0073(8) 0.0055(8) C7B 0.0285(11) 0.0341(12) 0.0217(10) -0.0007(9) 0.0078(9) 0.0115(10) C8B 0.0378(13) 0.0439(15) 0.0222(11) -0.0026(10) 0.0096(10) 0.0132(11) C9B 0.0356(13) 0.0421(14) 0.0176(10) 0.0027(9) 0.0021(9) 0.0075(11) C10B 0.0307(12) 0.0396(14) 0.0276(12) 0.0088(10) 0.0036(9) 0.0142(10) C11B 0.0304(12) 0.0322(12) 0.0246(11) 0.0038(9) 0.0081(9) 0.0141(10) N1A 0.0199(8) 0.0145(8) 0.0228(8) -0.0013(7) 0.0058(7) 0.0073(7) C2A 0.0183(9) 0.0190(10) 0.0206(9) -0.0010(7) 0.0053(8) 0.0057(8) N3A 0.0188(8) 0.0170(8) 0.0173(8) -0.0013(6) 0.0056(6) 0.0063(7) C4A 0.0191(9) 0.0174(9) 0.0189(9) 0.0003(7) 0.0067(7) 0.0072(8) C5A 0.0199(10) 0.0183(10) 0.0183(9) 0.0026(7) 0.0071(7) 0.0083(8) C6A 0.0205(10) 0.0191(10) 0.0167(9) 0.0025(7) 0.0071(7) 0.0046(8) C7A 0.0249(10) 0.0201(10) 0.0202(10) 0.0011(8) 0.0086(8) 0.0052(8) C8A 0.0276(11) 0.0215(11) 0.0243(10) 0.0007(8) 0.0094(9) -0.0013(9) C9A 0.0193(10) 0.0374(13) 0.0305(12) 0.0048(10) 0.0096(9) 0.0008(9) C10A 0.0222(11) 0.0356(13) 0.0415(13) 0.0075(10) 0.0130(10) 0.0109(10) C11A 0.0233(11) 0.0219(11) 0.0357(12) 0.0024(9) 0.0109(9) 0.0081(9) Cl 0.0170(2) 0.0201(2) 0.0251(2) -0.00206(18) 0.00321(18) 0.00840(18) O1 0.0252(8) 0.0342(9) 0.0323(9) -0.0039(7) -0.0021(7) 0.0163(7) O2 0.0665(14) 0.0596(13) 0.0337(10) -0.0227(9) -0.0180(9) 0.0443(11) O3 0.0375(11) 0.0532(13) 0.1028(18) 0.0035(12) 0.0476(12) 0.0046(9) O4 0.0644(13) 0.0252(9) 0.0538(11) 0.0093(8) 0.0276(10) 0.0271(9) N2 0.0314(10) 0.0336(11) 0.0404(11) -0.0006(9) 0.0141(9) 0.0152(9) C12 0.0261(11) 0.0257(11) 0.0254(10) 0.0036(8) 0.0106(9) 0.0103(9) C13 0.0544(18) 0.0534(18) 0.0444(16) -0.0118(13) 0.0167(13) 0.0209(14) C14 0.0354(14) 0.0315(14) 0.0718(19) 0.0028(13) 0.0248(13) 0.0162(11) O5 0.0366(9) 0.0426(10) 0.0338(9) 0.0032(7) 0.0150(7) 0.0231(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3B 1.9866(16) 2_666 ? Cu N3B 1.9867(16) . ? Cu N3A 2.0009(16) . ? Cu N3A 2.0009(16) 2_666 ? N1B C2B 1.341(3) . ? N1B C5B 1.378(3) . ? N1B H1B 0.853(10) . ? C2B N3B 1.323(3) . ? C2B H2B 0.9500 . ? N3B C4B 1.380(2) . ? C4B C5B 1.363(3) . ? C4B H4B 0.9500 . ? C5B C6B 1.468(3) . ? C6B C7B 1.389(3) . ? C6B C11B 1.395(3) . ? C7B C8B 1.393(3) . ? C7B H7B 0.9500 . ? C8B C9B 1.378(4) . ? C8B H8B 0.9500 . ? C9B C10B 1.382(4) . ? C9B H9B 0.9500 . ? C10B C11B 1.387(3) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? N1A C2A 1.340(3) . ? N1A C5A 1.383(2) . ? N1A H1A 0.851(10) . ? C2A N3A 1.318(3) . ? C2A H2A 0.9500 . ? N3A C4A 1.378(2) . ? C4A C5A 1.365(3) . ? C4A H4A 0.9500 . ? C5A C6A 1.463(3) . ? C6A C11A 1.395(3) . ? C6A C7A 1.395(3) . ? C7A C8A 1.390(3) . ? C7A H7A 0.9500 . ? C8A C9A 1.382(3) . ? C8A H8A 0.9500 . ? C9A C10A 1.389(3) . ? C9A H9A 0.9500 . ? C10A C11A 1.389(3) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? Cl O2 1.4242(18) . ? Cl O3 1.427(2) . ? Cl O1 1.4288(15) . ? Cl O4 1.4307(17) . ? N2 C12 1.318(3) . ? N2 C14 1.456(3) . ? N2 C13 1.464(3) . ? C12 O5 1.227(3) . ? C12 H12 0.9500 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Cu N3B 180.0 2_666 . ? N3B Cu N3A 88.25(7) 2_666 . ? N3B Cu N3A 91.75(7) . . ? N3B Cu N3A 91.74(7) 2_666 2_666 ? N3B Cu N3A 88.26(7) . 2_666 ? N3A Cu N3A 180.0 . 2_666 ? C2B N1B C5B 108.22(16) . . ? C2B N1B H1B 125.7(17) . . ? C5B N1B H1B 126.0(17) . . ? N3B C2B N1B 110.77(17) . . ? N3B C2B H2B 124.6 . . ? N1B C2B H2B 124.6 . . ? C2B N3B C4B 106.01(16) . . ? C2B N3B Cu 130.49(14) . . ? C4B N3B Cu 123.44(13) . . ? C5B C4B N3B 109.64(17) . . ? C5B C4B H4B 125.2 . . ? N3B C4B H4B 125.2 . . ? C4B C5B N1B 105.37(17) . . ? C4B C5B C6B 129.71(18) . . ? N1B C5B C6B 124.91(18) . . ? C7B C6B C11B 119.02(19) . . ? C7B C6B C5B 121.69(19) . . ? C11B C6B C5B 119.27(19) . . ? C6B C7B C8B 119.9(2) . . ? C6B C7B H7B 120.1 . . ? C8B C7B H7B 120.1 . . ? C9B C8B C7B 120.9(2) . . ? C9B C8B H8B 119.6 . . ? C7B C8B H8B 119.6 . . ? C8B C9B C10B 119.4(2) . . ? C8B C9B H9B 120.3 . . ? C10B C9B H9B 120.3 . . ? C9B C10B C11B 120.4(2) . . ? C9B C10B H10B 119.8 . . ? C11B C10B H10B 119.8 . . ? C10B C11B C6B 120.4(2) . . ? C10B C11B H11B 119.8 . . ? C6B C11B H11B 119.8 . . ? C2A N1A C5A 108.48(16) . . ? C2A N1A H1A 123.9(17) . . ? C5A N1A H1A 127.6(17) . . ? N3A C2A N1A 110.71(17) . . ? N3A C2A H2A 124.6 . . ? N1A C2A H2A 124.6 . . ? C2A N3A C4A 106.15(16) . . ? C2A N3A Cu 124.59(14) . . ? C4A N3A Cu 128.99(13) . . ? C5A C4A N3A 109.92(17) . . ? C5A C4A H4A 125.0 . . ? N3A C4A H4A 125.0 . . ? C4A C5A N1A 104.74(17) . . ? C4A C5A C6A 131.54(18) . . ? N1A C5A C6A 123.70(18) . . ? C11A C6A C7A 118.71(19) . . ? C11A C6A C5A 119.43(18) . . ? C7A C6A C5A 121.86(18) . . ? C8A C7A C6A 120.2(2) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C9A C8A C7A 120.8(2) . . ? C9A C8A H8A 119.6 . . ? C7A C8A H8A 119.6 . . ? C8A C9A C10A 119.4(2) . . ? C8A C9A H9A 120.3 . . ? C10A C9A H9A 120.3 . . ? C11A C10A C9A 120.2(2) . . ? C11A C10A H10A 119.9 . . ? C9A C10A H10A 119.9 . . ? C10A C11A C6A 120.7(2) . . ? C10A C11A H11A 119.6 . . ? C6A C11A H11A 119.6 . . ? O2 Cl O3 110.28(15) . . ? O2 Cl O1 108.93(10) . . ? O3 Cl O1 108.75(13) . . ? O2 Cl O4 109.46(12) . . ? O3 Cl O4 109.25(12) . . ? O1 Cl O4 110.16(11) . . ? C12 N2 C14 121.4(2) . . ? C12 N2 C13 120.4(2) . . ? C14 N2 C13 118.3(2) . . ? O5 C12 N2 125.3(2) . . ? O5 C12 H12 117.3 . . ? N2 C12 H12 117.3 . . ? N2 C13 H13A 109.5 . . ? N2 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? N2 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N2 C14 H14A 109.5 . . ? N2 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? N2 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? _refine_diff_density_max 0.606 _refine_diff_density_min -0.457 _refine_diff_density_rms 0.061 # start Validation Reply Form _vrf_PLAT975_7 ; RESPONSE: This density peak is near a mildly disordered oxygen atom (O4) of the coordinated perchlorate ion. ; # end Validation Reply Form _shelx_res_file ; 7.res created by SHELXL-2014/7 TITL EL105B in P-1 CELL 0.71073 9.1544 9.8343 14.2557 91.493 107.948 109.075 ZERR 1 0.0004 0.0005 0.0008 0.004 0.005 0.005 LATT 1 SFAC C H N O CU CL UNIT 42 46 10 10 1 2 MERG 2 OMIT -2 54 MORE -3 FMAP 2 PLAN 10 SIZE 0.25 0.15 0.15 TEMP -173 ACTA BOND $H LIST 4 L.S. 6 WGHT 0.035800 1.107000 FVAR 4.32088 CU 5 0.500000 0.500000 0.500000 10.50000 0.01511 0.01507 = 0.01618 -0.00271 0.00430 0.00399 DFIX 0.86 0.01 N1A H1A N1B H1B N1B 3 0.609867 0.416666 0.248230 11.00000 0.02106 0.02419 = 0.01992 0.00021 0.00835 0.01097 H1B 2 0.670249 0.397107 0.218707 11.00000 -1.50000 C2B 1 0.647949 0.445522 0.347023 11.00000 0.01879 0.02043 = 0.02082 -0.00063 0.00476 0.00758 AFIX 43 H2B 2 0.749597 0.451927 0.394793 11.00000 -1.20000 AFIX 0 N3B 3 0.524687 0.463865 0.368929 11.00000 0.01565 0.01662 = 0.01803 -0.00232 0.00416 0.00408 C4B 1 0.402339 0.446204 0.278995 11.00000 0.01718 0.01780 = 0.02016 -0.00076 0.00507 0.00547 AFIX 43 H4B 2 0.298302 0.453236 0.271215 11.00000 -1.20000 AFIX 0 C5B 1 0.453511 0.417134 0.203039 11.00000 0.02011 0.01703 = 0.02065 0.00073 0.00640 0.00669 C6B 1 0.366813 0.389239 0.095118 11.00000 0.02263 0.02241 = 0.01951 0.00205 0.00730 0.00550 C7B 1 0.409064 0.312688 0.030851 11.00000 0.02853 0.03413 = 0.02174 -0.00074 0.00778 0.01151 AFIX 43 H7B 2 0.499110 0.280508 0.056010 11.00000 -1.20000 AFIX 0 C8B 1 0.319208 0.283174 -0.070547 11.00000 0.03778 0.04394 = 0.02216 -0.00260 0.00958 0.01323 AFIX 43 H8B 2 0.348057 0.230089 -0.114123 11.00000 -1.20000 AFIX 0 C9B 1 0.189010 0.329951 -0.108506 11.00000 0.03564 0.04207 = 0.01764 0.00272 0.00210 0.00753 AFIX 43 H9B 2 0.127641 0.308398 -0.177666 11.00000 -1.20000 AFIX 0 C10B 1 0.148537 0.408480 -0.045065 11.00000 0.03069 0.03959 = 0.02755 0.00885 0.00362 0.01422 AFIX 43 H10B 2 0.060115 0.442488 -0.070947 11.00000 -1.20000 AFIX 0 C11B 1 0.236204 0.437960 0.056162 11.00000 0.03040 0.03216 = 0.02456 0.00376 0.00807 0.01407 AFIX 43 H11B 2 0.207154 0.491660 0.099251 11.00000 -1.20000 AFIX 0 N1A 3 0.817299 0.924751 0.579261 11.00000 0.01987 0.01453 = 0.02283 -0.00130 0.00584 0.00732 H1A 2 0.831212 1.014222 0.591068 11.00000 -1.50000 C2A 1 0.669922 0.818380 0.546044 11.00000 0.01828 0.01900 = 0.02058 -0.00096 0.00528 0.00569 AFIX 43 H2A 2 0.568147 0.832885 0.532260 11.00000 -1.20000 AFIX 0 N3A 3 0.685557 0.690917 0.535126 11.00000 0.01881 0.01702 = 0.01731 -0.00130 0.00563 0.00627 C4A 1 0.851583 0.717926 0.561830 11.00000 0.01911 0.01744 = 0.01887 0.00032 0.00672 0.00715 AFIX 43 H4A 2 0.899727 0.645972 0.560789 11.00000 -1.20000 AFIX 0 C5A 1 0.936578 0.863415 0.589997 11.00000 0.01992 0.01829 = 0.01832 0.00256 0.00706 0.00826 C6A 1 1.112761 0.946962 0.626943 11.00000 0.02054 0.01906 = 0.01671 0.00249 0.00705 0.00456 C7A 1 1.173760 1.096971 0.655974 11.00000 0.02488 0.02012 = 0.02017 0.00107 0.00858 0.00519 AFIX 43 H7A 2 1.100044 1.147733 0.651091 11.00000 -1.20000 AFIX 0 C8A 1 1.341995 1.172402 0.692013 11.00000 0.02760 0.02152 = 0.02433 0.00065 0.00942 -0.00128 AFIX 43 H8A 2 1.382324 1.274644 0.711092 11.00000 -1.20000 AFIX 0 C9A 1 1.451292 1.100438 0.700420 11.00000 0.01930 0.03740 = 0.03052 0.00482 0.00956 0.00082 AFIX 43 H9A 2 1.566125 1.152584 0.725754 11.00000 -1.20000 AFIX 0 C10A 1 1.391682 0.951120 0.671479 11.00000 0.02224 0.03561 = 0.04155 0.00750 0.01297 0.01086 AFIX 43 H10A 2 1.465986 0.900848 0.676888 11.00000 -1.20000 AFIX 0 C11A 1 1.223696 0.875153 0.634653 11.00000 0.02329 0.02191 = 0.03565 0.00237 0.01087 0.00809 AFIX 43 H11A 2 1.183926 0.773189 0.614500 11.00000 -1.20000 AFIX 0 CL 6 0.842437 0.345898 0.629425 11.00000 0.01700 0.02011 = 0.02511 -0.00206 0.00321 0.00840 O1 4 0.691527 0.357839 0.569062 11.00000 0.02522 0.03424 = 0.03233 -0.00390 -0.00210 0.01627 O2 4 0.898712 0.434956 0.722868 11.00000 0.06648 0.05958 = 0.03367 -0.02266 -0.01802 0.04434 O3 4 0.959704 0.392714 0.579473 11.00000 0.03747 0.05323 = 0.10276 0.00347 0.04757 0.00465 O4 4 0.818543 0.198235 0.645190 11.00000 0.06436 0.02521 = 0.05378 0.00933 0.02755 0.02714 N2 3 0.893933 0.161951 0.099450 11.00000 0.03144 0.03358 = 0.04036 -0.00062 0.01407 0.01517 C12 1 0.875557 0.247821 0.164068 11.00000 0.02609 0.02569 = 0.02540 0.00364 0.01064 0.01027 AFIX 43 H12 2 0.955293 0.274215 0.228912 11.00000 -1.20000 AFIX 0 C13 1 0.779991 0.122018 -0.003174 11.00000 0.05436 0.05343 = 0.04437 -0.01184 0.01667 0.02090 AFIX 137 H13A 2 0.699551 0.170475 -0.012058 11.00000 -1.50000 H13B 2 0.723013 0.016472 -0.016948 11.00000 -1.50000 H13C 2 0.841154 0.152383 -0.049194 11.00000 -1.50000 AFIX 0 C14 1 1.025239 0.102608 0.127962 11.00000 0.03544 0.03148 = 0.07185 0.00282 0.02478 0.01616 AFIX 137 H14A 2 1.097290 0.144875 0.196292 11.00000 -1.50000 H14B 2 1.088802 0.126174 0.082669 11.00000 -1.50000 H14C 2 0.977995 -0.003163 0.124114 11.00000 -1.50000 AFIX 0 O5 4 0.763915 0.296438 0.147320 11.00000 0.03656 0.04259 = 0.03385 0.00316 0.01495 0.02312 HKLF 4 REM EL105B in P-1 REM R1 = 0.0369 for 4337 Fo > 4sig(Fo) and 0.0434 for all 4905 data REM 303 parameters refined using 2 restraints END WGHT 0.0352 1.1373 REM Highest difference peak 0.606, deepest hole -0.457, 1-sigma level 0.061 Q1 1 0.7303 0.1660 0.5924 11.00000 0.05 0.61 Q2 1 0.8417 0.3543 0.7370 11.00000 0.05 0.51 Q3 1 0.6497 0.0614 -0.0281 11.00000 0.05 0.44 Q4 1 0.5000 0.5562 0.4403 11.00000 0.05 0.38 Q5 1 0.4632 0.5122 0.4238 11.00000 0.05 0.36 Q6 1 0.8823 0.8925 0.5815 11.00000 0.05 0.34 Q7 1 0.9731 0.3672 0.6368 11.00000 0.05 0.34 Q8 1 0.6194 0.6206 0.5151 11.00000 0.05 0.34 Q9 1 0.3990 0.3848 0.1541 11.00000 0.05 0.33 Q10 1 0.4475 0.4432 0.3323 11.00000 0.05 0.32 ; _shelx_res_checksum 8691 _shelx_hkl_file ; 0 0 -2 40200.3 588.597 4 0 0 -3 53830.6 784.589 4 0 0 -3 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555.500 5 -2 4 0 27699.1 563.573 2 -2 4 0 28388.1 591.506 4 2 -4 1 26533.3 416.855 3 -2 4 -1 29273.4 576.960 2 -2 4 -1 27338.2 574.111 4 -2 4 -2 289.411 59.0336 4 -2 4 -2 297.493 50.2990 2 -2 4 -3 5754.00 231.908 4 -2 4 -4 7761.32 278.007 4 -2 4 -4 7390.52 155.649 3 -2 4 -5 21150.8 377.503 3 -2 4 -5 20718.9 447.326 5 -2 4 -5 21345.9 519.551 4 -2 4 -6 14977.9 368.980 5 -2 4 -6 14937.7 315.829 3 -2 4 -6 14298.1 417.580 4 -2 4 -7 1773.60 101.349 3 -2 4 -7 1971.73 123.088 5 -2 4 -7 2043.33 150.212 4 -2 4 -8 5264.02 216.110 5 -2 4 -8 5448.83 257.487 4 -2 4 -8 4912.68 188.853 3 -2 4 -9 3365.45 211.464 4 -2 4 -9 3136.23 172.017 5 -2 4 -10 1963.29 143.206 5 -2 4 -10 1600.05 150.949 4 -2 4 -11 39.7553 43.8176 5 -2 4 -11-40.1196 43.5707 4 -2 4 -12 2068.12 162.449 5 -2 4 -12 1841.00 173.327 4 -2 4 -13 7371.78 306.122 3 -2 4 -13 7893.36 370.450 4 -2 4 -13 7621.73 330.287 5 -2 4 -14 4476.96 244.477 3 -2 4 -14 5331.23 307.686 4 -2 4 -14 4871.73 268.864 5 -2 4 -15 4022.26 255.693 5 -2 4 -15 4338.55 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4872.88 335.756 4 -3 11 -3 610.625 123.261 4 -3 11 -4-47.9141 72.4642 4 -3 11 -5 845.436 140.702 4 -3 11 -6 101.073 59.5855 4 -3 11 -7-37.6202 73.2463 4 -3 11 -8 1020.64 160.854 4 -3 11 -9 5934.81 345.723 5 -3 11 -10 3261.39 256.180 5 3 -10 -9 8.35746 70.2489 5 -3 10 9 42.7519 60.5621 4 -3 10 8 25.6071 62.3627 4 3 -10 -8-45.4302 73.4833 5 -3 10 7 992.393 161.635 4 -3 10 6 548.267 121.196 4 -3 10 5 1845.47 211.501 4 -3 10 4 10481.7 498.675 4 -3 10 3 2384.34 233.060 4 -3 10 2 2595.15 237.609 4 -3 10 1 146.586 69.8190 4 -3 10 0 84.2092 56.7406 4 -3 10 -1 3424.69 269.032 4 -3 10 -2 5724.12 345.639 4 -3 10 -3 1242.05 166.611 4 -3 10 -4 6321.07 368.704 4 -3 10 -5 12450.5 528.581 4 -3 10 -6 3356.40 268.918 4 -3 10 -7 532.680 115.749 4 -3 10 -8 1742.89 171.437 5 -3 10 -8 2088.91 218.070 4 -3 10 -9 60.4568 63.1046 4 -3 10 -9-32.8689 51.0538 5 -3 10 -10 95.1523 71.1532 4 -3 10 -10 165.042 69.7750 5 -3 10 -11 4410.81 285.736 5 -3 10 -11 4082.95 311.631 4 -3 10 -12 2978.46 235.479 5 3 -9 -11 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668.840 4 -3 7 -2 155.683 65.7874 4 -3 7 -3 148.702 62.9855 4 -3 7 -4-124.600 80.2575 4 -3 7 -5-76.1046 68.3233 4 -3 7 -6 7505.54 346.795 4 -3 7 -7 3469.28 233.414 4 -3 7 -7 3489.73 195.503 5 -3 7 -8 1225.19 119.926 5 -3 7 -8 1356.67 149.833 4 -3 7 -9 1487.98 134.520 5 -3 7 -9 1462.39 157.966 4 -3 7 -10 519.420 109.227 4 -3 7 -10 511.802 85.0518 5 -3 7 -11 937.480 116.044 5 -3 7 -11 1250.89 160.055 4 -3 7 -12 2721.04 196.992 5 -3 7 -12 2750.96 240.478 4 -3 7 -13 183.723 64.3877 5 -3 7 -13 262.798 76.9314 4 -3 7 -14 1070.19 130.658 5 -3 7 -14 1409.03 178.035 4 -3 7 -15 2303.98 199.739 5 -3 7 -15 2687.92 251.108 4 3 -6 -15 3735.35 277.675 5 3 -6 -14 6294.80 351.750 5 3 -6 -13 4949.07 301.984 5 3 -6 -12 3655.36 248.231 5 3 -6 -11-130.522 74.4588 5 -3 6 11-72.6161 67.6785 4 -3 6 10 22.4946 51.8077 4 3 -6 -10 46.6408 53.7763 5 -3 6 10 79.9912 43.9583 1 3 -6 -9 8593.82 356.616 5 -3 6 9 8707.76 323.292 1 -3 6 9 9110.96 376.902 4 -3 6 8 22260.1 553.278 1 -3 6 8 21279.5 605.492 4 3 -6 -8 20322.7 575.471 5 -3 6 7 19087.1 502.248 1 3 -6 -7 17348.1 508.271 5 -3 6 7 18032.3 536.676 4 3 -6 -6 11980.3 334.308 2 -3 6 6 13285.9 432.311 4 3 -6 -6 12699.6 404.593 5 3 -6 -5 4291.90 183.607 2 -3 6 5 4255.21 228.355 4 3 -6 -5 4115.76 210.365 5 -3 6 4 666.942 98.8045 4 3 -6 -4 670.284 85.7994 5 3 -6 -4 531.505 65.9353 2 3 -6 -3 3612.26 188.745 5 3 -6 -3 2439.97 143.314 2 3 -6 -3 2529.27 154.411 1 -3 6 3 3459.41 205.085 4 3 -6 -2 1243.28 112.088 1 -3 6 2 1233.58 122.722 4 -3 6 1 1420.09 130.336 4 3 -6 -1 1345.22 123.043 1 -3 6 0 19715.2 530.179 4 -3 6 0 20322.3 517.783 2 3 -6 1 5742.65 142.450 3 -3 6 -1 5652.06 262.588 4 -3 6 -2 497.829 83.5871 4 -3 6 -3 2102.29 162.151 4 -3 6 -4 8052.80 325.740 4 -3 6 -5 20.1701 42.7482 4 -3 6 -6 4630.00 207.929 5 -3 6 -6 4015.82 240.193 4 -3 6 -7 3474.42 181.714 5 -3 6 -7 3188.41 101.335 3 -3 6 -7 3692.04 229.085 4 -3 6 -8 56588.4 1151.80 4 -3 6 -8 54067.5 869.968 3 -3 6 -8 57602.7 1037.59 5 -3 6 -9 3868.23 204.377 5 -3 6 -9 3809.98 249.352 4 -3 6 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50.9342 1 -7 -4 2 11.0808 54.8148 3 -7 -4 2 64.0972 53.6416 1 -7 -4 1 1184.53 158.731 3 7 4 -1 1084.36 142.359 2 -7 -4 0 5331.78 334.750 3 7 4 0 5249.70 299.024 2 -7 -4 -1 8665.72 437.323 3 -7 -4 -2 5481.99 352.742 3 -7 -4 -3 256.132 94.0053 3 -7 -4 -4-0.26552 61.8101 3 7 5 -14 1740.24 190.921 5 7 5 -13 2910.59 237.644 5 7 5 -12 3120.02 238.274 5 7 5 -11 1550.11 167.175 5 7 5 -10 397.968 100.273 4 7 5 -10 515.961 100.632 5 7 5 -9 1905.54 178.067 5 7 5 -9 2013.15 216.523 4 7 5 -8 1659.00 162.416 5 7 5 -7 2978.05 213.128 5 -7 -5 7 2964.50 250.897 3 7 5 -6 6158.05 303.867 5 -7 -5 6 5975.61 356.343 3 -7 -5 6 5638.90 361.748 1 -7 -5 5 3796.69 283.819 3 -7 -5 5 3763.36 295.288 1 -7 -5 4 1858.06 212.437 1 -7 -5 4 1944.61 202.194 3 -7 -5 3 1229.32 170.424 3 -7 -5 3 1303.63 172.119 1 -7 -5 2 2.10699 56.6475 3 -7 -5 1 1762.16 202.414 3 -7 -5 0 46.5942 59.7628 3 -7 -5 -1 1913.05 212.946 3 -7 -5 -2 5683.74 372.819 3 -7 -5 -3 3225.12 283.839 3 7 6 -12 944.224 138.232 5 7 6 -11 1826.26 188.620 5 7 6 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137.753 4 8 -7 -14-12.1337 50.6081 5 8 -7 -13 747.664 116.358 5 -8 7 13 765.840 159.719 1 8 -7 -12-15.7638 52.0788 5 -8 7 12-73.6559 63.0230 1 -8 7 11 46.7260 69.5472 1 8 -7 -11 48.9607 51.4013 5 8 -7 -10 933.301 124.538 5 -8 7 10 847.379 164.255 1 8 -7 -9 106.418 67.9524 2 8 -7 -9 97.5645 49.6651 5 -8 7 9 137.175 85.2631 1 8 -7 -8 2538.44 242.638 2 8 -7 -8 2774.47 191.067 5 -8 7 7 20504.5 571.021 4 8 -7 -7 19043.4 696.444 2 8 -7 -7 20303.3 549.786 5 -8 7 6 38982.7 893.378 4 8 -7 -6 36530.7 1028.22 2 8 -7 -6 39407.2 822.069 5 -8 7 5 5854.77 301.119 4 8 -7 -5 6268.99 371.431 2 8 -7 -5 6515.54 260.518 5 -8 7 4 3960.50 249.528 4 8 -7 -4 4673.65 323.870 2 8 -7 -3 1245.57 165.918 2 -8 7 3 1237.84 139.981 4 -8 7 2 626.032 110.378 4 8 -7 -2 702.885 128.792 2 -8 7 1 352.069 81.5180 4 8 -7 -1 452.371 105.661 2 -8 7 0 107.241 57.7922 4 -8 7 -1 6026.52 335.949 4 -8 7 -2 8066.80 399.731 4 -8 7 -3 1858.43 196.301 4 -8 7 -4 12.1397 56.7807 4 -8 7 -5-41.8008 63.9420 4 -8 7 -6 46.4737 50.9581 4 -8 7 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3 -8 6 -2 1043.72 140.050 4 -8 6 -3 6640.42 301.566 3 -8 6 -3 5871.95 347.925 4 -8 6 -4 629.097 97.2813 3 -8 6 -4 524.812 101.875 4 -8 6 -5 225.495 77.1152 4 -8 6 -6 1347.66 168.886 4 -8 6 -7 868.864 148.366 4 -8 5 17 1379.87 234.738 1 -8 5 16 1662.48 250.249 1 8 -5 -16 1536.04 179.117 5 8 -5 -15 356.885 89.7653 5 -8 5 15 358.016 110.174 1 -8 5 14 2327.25 276.622 1 8 -5 -14 2234.05 204.330 5 -8 5 13 5152.26 403.570 1 8 -5 -13 5147.81 297.801 5 -8 5 12 2281.32 264.655 1 8 -5 -12 2388.76 195.240 5 -8 5 11 11499.9 583.293 1 8 -5 -11 12234.9 441.883 5 8 -5 -10 396.875 76.0596 5 -8 5 10 304.428 96.7040 1 -8 5 9 4716.26 351.607 1 8 -5 -9 4533.06 234.143 5 -8 5 8 1502.40 115.293 4 -8 5 8 1328.57 196.778 1 8 -5 -8 1372.01 123.279 5 8 -5 -7 99.3335 40.8568 5 -8 5 7 121.978 82.0311 1 -8 5 7 123.253 45.7133 4 -8 5 6 13611.6 425.336 4 8 -5 -6 14049.1 374.707 5 -8 5 6 13787.2 613.188 1 -8 5 5 1965.39 159.588 4 8 -5 -5 1831.31 206.964 2 8 -5 -5 1953.45 115.906 5 -8 5 4 11085.8 406.444 4 8 -5 -4 11150.2 508.426 2 8 -5 -4 10474.4 272.666 5 -8 5 3 11787.7 429.878 4 8 -5 -3 11880.2 518.746 2 -8 5 2 4266.20 255.789 4 8 -5 -2 4484.42 314.021 2 -8 5 1 7334.82 350.268 4 8 -5 -1 7697.42 415.353 2 8 -5 0 3459.67 276.511 2 -8 5 0 3385.30 220.405 3 -8 5 0 3899.86 252.955 4 -8 5 -1 706.507 101.658 3 8 -5 1 734.101 134.995 2 -8 5 -1 654.761 109.837 4 -8 5 -2 2594.53 191.899 3 -8 5 -2 2433.84 211.528 4 -8 5 -3 16578.9 526.650 3 -8 5 -3 15680.8 576.118 4 -8 5 -4 4978.74 281.988 3 -8 5 -4 5182.80 324.937 4 -8 5 -5 1588.22 157.881 3 -8 5 -5 1568.97 189.044 4 -8 5 -6 951.038 126.471 3 -8 5 -6 741.967 138.816 4 -8 5 -7 985.709 131.146 3 -8 5 -7 850.670 146.574 4 -8 5 -8 399.091 104.954 4 8 -4 -16 710.228 120.800 5 -8 4 15 127.239 85.0717 1 8 -4 -15 101.874 52.9619 5 -8 4 14 18.3586 68.1005 1 8 -4 -14 36.6267 50.0875 5 -8 4 13 53.1640 65.9896 1 8 -4 -13 71.3512 55.6449 5 -8 4 12 6158.83 424.095 1 8 -4 -12 5476.27 284.395 5 -8 4 11 22158.0 818.270 1 8 -4 -11 21986.1 600.470 5 -8 4 10 1136.74 182.155 1 8 -4 -10 1516.61 136.815 5 8 -4 -9 145.171 45.8561 5 -8 4 9 187.319 83.0990 1 -8 4 8 1177.12 174.109 1 8 -4 -8 1364.70 117.741 5 -8 4 7 4069.00 318.554 1 8 -4 -7 4336.30 198.316 5 -8 4 6 2655.30 169.011 4 -8 4 6 2588.54 253.045 1 8 -4 -6 2381.24 130.711 5 -8 4 5 6796.79 289.468 4 -8 4 5 6390.06 399.351 1 8 -4 -5 6130.54 199.586 5 -8 4 4 4757.89 248.948 4 8 -4 -4 4516.68 315.385 2 8 -4 -4 4463.66 144.334 5 -8 4 3 24001.2 647.278 4 8 -4 -3 25959.4 806.384 2 -8 4 2 13484.7 472.529 4 8 -4 -2 14144.2 565.507 2 -8 4 1 11482.0 429.363 3 -8 4 1 12175.8 451.515 4 8 -4 -1 13002.5 554.160 2 8 -4 0 7144.00 402.197 2 -8 4 0 6709.42 321.788 3 -8 4 0 6089.96 321.756 4 -8 4 -1 407.993 84.5325 3 8 -4 1 512.596 109.982 2 -8 4 -1 515.306 98.2637 4 -8 4 -2 1548.99 157.244 3 -8 4 -2 1213.31 153.347 4 -8 4 -3 5735.56 307.327 3 -8 4 -3 5418.03 326.745 4 -8 4 -4 3908.31 281.221 4 -8 4 -4 3540.62 243.856 3 -8 4 -5 2792.61 248.787 4 -8 4 -5 2771.09 221.619 3 -8 4 -6 2456.24 239.356 4 -8 4 -6 2270.13 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2049.67 190.482 4 -8 3 -1 2228.71 192.338 3 8 -3 2 4439.13 312.472 2 -8 3 -2 4375.71 286.409 4 -8 3 -2 4158.86 267.907 3 -8 3 -3 1831.96 189.210 4 -8 3 -3 1802.99 177.166 3 -8 3 -4 114.159 65.5579 3 -8 3 -4 172.504 83.8970 4 -8 3 -5 1020.74 142.264 3 -8 3 -6 2456.08 217.212 3 -8 3 -7 1427.89 170.478 3 -8 3 -8 2094.39 213.242 3 -8 3 -9 80.5448 53.9903 3 -8 3 -10 566.260 117.777 3 8 -2 -17 230.196 78.8461 5 8 -2 -16 3696.28 263.070 5 8 -2 -15 241.240 69.3218 5 8 -2 -14 791.508 115.357 5 8 -2 -13 260.480 65.9605 5 8 -2 -12 543.039 88.4887 5 -8 2 11 13.5647 82.6648 1 8 -2 -11 140.476 48.0492 5 8 -2 -10 1643.64 136.112 5 -8 2 10 1562.63 199.107 1 8 -2 -9 3987.16 205.380 5 -8 2 9 4024.32 317.071 1 8 -2 -8 31868.0 667.330 5 -8 2 8 30650.7 931.741 1 8 -2 -7 48669.6 873.355 5 -8 2 7 45913.5 1190.95 1 -8 2 6 188.300 81.5082 1 8 -2 -6 241.322 42.2428 5 -8 2 5 862.536 153.382 1 8 -2 -5 767.781 64.3671 5 -8 2 4 6685.20 330.814 3 -8 2 4 7097.38 416.441 1 8 -2 -4 6400.02 165.709 5 -8 2 3 1651.74 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196.962 4 -9 7 -1 189.111 69.8474 4 -9 7 -2-66.1818 53.9917 4 -9 7 -3 63.7645 60.1862 4 -9 7 -4 289.507 88.6135 4 -9 7 -5 2287.21 237.861 4 -9 6 15 1767.37 271.175 1 9 -6 -15 1726.46 186.097 5 -9 6 14 3878.90 380.028 1 9 -6 -14 3491.14 259.767 5 -9 6 13 2196.77 282.577 1 9 -6 -13 1557.70 170.090 5 9 -6 -12 21.7382 45.9214 5 -9 6 12-33.8173 65.4587 1 9 -6 -11 203.924 60.4694 5 -9 6 11 166.611 80.5440 1 -9 6 10 4496.79 379.709 1 9 -6 -10 3722.83 225.064 5 -9 6 9 9146.93 544.742 1 9 -6 -9 9430.85 354.489 5 9 -6 -8 6170.16 402.434 2 -9 6 8 5943.16 434.291 1 -9 6 7 4801.24 252.756 4 9 -6 -7 5308.47 370.108 2 -9 6 6 3479.63 224.639 4 9 -6 -6 3852.08 317.125 2 -9 6 5 3887.85 246.024 4 9 -6 -5 3956.62 320.778 2 9 -6 -4 36.7039 65.2354 2 -9 6 4 111.384 46.5391 4 9 -6 -3 3.58019 60.7881 2 -9 6 3 43.2939 48.8987 4 9 -6 -2 132.033 75.6325 2 -9 6 2-55.6844 58.0510 4 9 -6 -1 1185.13 172.980 2 -9 6 1 765.914 122.058 4 9 -6 0 226.058 80.1041 2 -9 6 0 195.252 64.8084 4 -9 6 -1 1596.29 182.789 4 -9 6 -2 1494.75 152.636 3 -9 6 -2 1425.12 173.176 4 -9 6 -3 827.892 117.355 3 -9 6 -3 942.206 143.760 4 -9 6 -4 741.792 140.999 4 -9 6 -5 576.731 130.410 4 9 -5 -16 1090.44 155.603 5 9 -5 -15 176.198 65.2813 5 -9 5 15 245.326 113.304 1 -9 5 14 1667.83 252.346 1 9 -5 -14 1551.19 170.690 5 -9 5 13 2709.68 308.710 1 9 -5 -13 2511.00 211.437 5 9 -5 -12 414.461 85.1027 5 -9 5 12 326.295 120.719 1 -9 5 11 151.112 92.8605 1 9 -5 -11 249.160 65.5662 5 9 -5 -10 191.249 56.2911 5 -9 5 10 290.425 102.355 1 9 -5 -9 25.2705 38.6556 5 -9 5 9-62.3697 83.4911 1 -9 5 8 59.1716 65.1368 1 -9 5 7 13516.8 434.445 4 -9 5 7 12110.7 615.428 1 -9 5 6 2219.14 174.006 4 9 -5 -6 1695.77 211.443 2 9 -5 -5 524.526 122.681 2 -9 5 5 408.236 87.8332 4 -9 5 4 1679.23 163.699 4 9 -5 -4 1952.26 219.843 2 9 -5 -3 210.107 72.1271 2 -9 5 3 359.865 82.0721 4 9 -5 -2 194.789 79.7173 2 -9 5 2 286.619 83.4650 4 9 -5 -1 5.19017 59.2653 2 -9 5 1 154.500 65.1057 4 -9 5 0 1225.51 142.458 3 9 -5 0 1259.68 180.946 2 -9 5 0 974.312 140.681 4 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550.038 3 9 -2 -4 15219.0 644.734 2 -9 2 3 11904.7 492.032 3 9 -2 -3 12543.7 582.334 2 -9 2 2 3263.42 253.064 3 9 -2 -2 4280.78 332.867 2 9 -2 -1 1354.89 187.879 2 -9 2 1 1427.86 167.710 3 -9 2 0 642.789 121.528 3 9 -2 0 424.676 120.408 2 -9 2 -1 255.134 82.6991 3 9 -2 1 455.919 113.901 2 9 -2 2 3383.25 296.289 2 -9 2 -2 3085.77 255.049 3 -9 2 -3 5179.53 335.557 3 -9 2 -4 2755.12 250.863 3 -9 2 -5 3441.88 282.941 3 -9 2 -6-10.4381 61.7789 3 -9 2 -7 1173.89 172.435 3 9 -1 -16 6986.90 372.375 5 9 -1 -15 4708.81 293.961 5 9 -1 -14 36.1744 45.6035 5 9 -1 -13 47.3473 52.6634 5 -9 1 12 182.640 92.9628 1 9 -1 -12 39.0822 41.8735 5 -9 1 11 198.130 100.469 1 9 -1 -11 57.0125 39.9811 5 9 -1 -10 9986.81 356.716 5 -9 1 10 10220.6 545.664 1 9 -1 -9 3153.78 183.258 5 -9 1 9 2923.58 287.911 1 -9 1 8 11181.4 564.371 1 -9 1 7 147.433 90.2573 1 -9 1 6 1178.83 179.340 1 -9 1 5 673.332 130.668 3 -9 1 5 506.979 135.877 1 -9 1 4 8556.21 425.340 3 -9 1 4 8766.20 508.173 1 -9 1 3 7557.79 393.501 3 9 -1 -3 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2943.09 267.373 3 -9 -1 -3 718.677 136.569 3 9 2 -15 106.453 55.3983 5 9 2 -14 94.1811 54.5171 5 9 2 -13 1402.46 158.765 5 9 2 -12 772.034 116.164 5 9 2 -11 50.4865 42.5593 5 -9 -2 10 202.109 84.6225 1 9 2 -10 135.215 50.7226 5 -9 -2 9 3808.22 334.185 1 -9 -2 8 5280.16 391.420 1 -9 -2 7 995.131 172.217 1 -9 -2 6 8498.77 504.246 1 -9 -2 6 8928.49 459.836 3 -9 -2 5 9610.92 482.338 3 -9 -2 5 8846.06 521.240 1 -9 -2 4 1442.03 185.749 3 -9 -2 4 1110.77 191.241 1 -9 -2 3 108.558 76.1793 3 9 2 -3-15.8779 58.7067 2 -9 -2 3 147.875 83.9213 1 -9 -2 2 1322.29 187.211 3 9 2 -2 1517.43 202.896 2 -9 -2 1 34.5175 60.8111 3 9 2 -1 55.7568 64.7168 2 -9 -2 0 4097.83 320.367 3 9 2 0 4626.24 340.425 2 9 2 1 4282.44 321.466 2 -9 -2 -1 4248.40 321.907 3 9 3 -14 2689.73 230.252 5 9 3 -13 8929.89 412.326 5 9 3 -12 7478.86 365.120 5 9 3 -11 1030.94 133.139 5 -9 -3 10 54.3767 73.2398 1 -9 -3 9 773.781 159.336 1 -9 -3 8-89.2784 88.7408 1 -9 -3 7 1499.60 196.940 3 -9 -3 7 1518.35 215.486 1 -9 -3 6 6807.16 454.789 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116.445 2 10 -9 -7 6541.80 443.439 2 10 -9 -6 7457.76 474.704 2 10 -9 -5 5969.39 418.693 2 10 -9 -4-29.5493 71.6083 2 -10 9 4 96.9138 56.9005 4 -10 9 3 769.071 132.238 4 -10 9 2 71.3718 66.0742 4 -10 9 1 1634.10 203.449 4 -10 9 0 3637.05 300.650 4 -10 9 -1 1520.85 199.379 4 10 -8 -12 3890.78 352.800 2 10 -8 -11 1861.22 239.847 2 10 -8 -10-116.893 78.4898 2 10 -8 -9 19.5884 73.7373 2 10 -8 -8-16.5375 70.9467 2 10 -8 -7 2366.11 264.834 2 10 -8 -6 5905.09 422.623 2 -10 8 5 7138.83 387.275 4 10 -8 -5 8359.27 501.281 2 10 -8 -4 4009.42 343.662 2 -10 8 4 3294.29 259.949 4 10 -8 -3 3211.80 311.682 2 -10 8 3 3170.14 258.887 4 10 -8 -2 180.504 105.882 2 -10 8 2 106.121 66.8528 4 -10 8 1 54.2938 58.7804 4 -10 8 0 169.382 66.0101 4 -10 8 -1 564.851 122.603 4 -10 8 -2 4711.75 341.013 4 -10 7 13 3034.05 355.778 1 -10 7 12 2703.60 333.297 1 -10 7 11 7598.05 545.197 1 10 -7 -10 1623.74 223.948 2 -10 7 10 1397.49 230.735 1 10 -7 -9 652.962 148.109 2 10 -7 -8 485.771 125.085 2 10 -7 -7 259.669 105.285 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1216.08 171.323 4 -10 6 -2-24.1251 48.2772 3 -10 6 -2-59.4563 71.1011 4 -10 6 -3 1329.98 181.804 4 -10 5 13 133.425 96.9863 1 -10 5 12 127.851 105.628 1 -10 5 11 168.663 94.4391 1 -10 5 10 6193.96 470.266 1 -10 5 9 3614.24 355.437 1 -10 5 8 341.428 136.447 1 10 -5 -7 1601.52 218.350 2 -10 5 7 1447.62 217.943 1 10 -5 -6 341.799 110.710 2 10 -5 -5-55.1431 67.5063 2 -10 5 4 3340.70 247.870 4 10 -5 -4 3344.96 308.060 2 -10 5 3 5285.59 323.018 4 10 -5 -3 6049.24 421.475 2 -10 5 2 6881.52 382.999 4 10 -5 -2 7544.82 474.488 2 10 -5 -1 3361.21 320.278 2 -10 5 1 2809.33 248.381 4 10 -5 0 1615.19 217.901 2 -10 5 0 1569.39 176.855 3 -10 5 0 1408.39 177.687 4 -10 5 -1 148.136 65.7331 3 -10 5 -1 608.866 120.323 4 -10 5 -2 565.385 112.234 3 -10 5 -2 743.579 138.797 4 -10 5 -3 618.170 114.647 3 -10 5 -3 405.947 110.236 4 -10 5 -4 624.751 119.278 3 -10 4 13 154.588 102.542 1 -10 4 12-3.92378 69.0950 1 -10 4 11 265.940 109.062 1 -10 4 10 5752.96 442.326 1 -10 4 9 9219.82 560.399 1 -10 4 8 4004.99 366.074 1 -10 4 7 15172.1 723.048 1 10 -4 -6 415.452 119.587 2 -10 4 6 549.939 136.678 1 10 -4 -5 74.9711 59.8006 2 10 -4 -4 596.839 137.283 2 10 -4 -3 134.322 75.8531 2 -10 4 2 2113.15 207.216 3 10 -4 -2 3040.50 301.619 2 -10 4 1 3297.68 260.894 3 10 -4 -1 3899.77 340.795 2 10 -4 0 2533.74 275.886 2 -10 4 0 2268.34 219.664 3 -10 4 -1 408.577 101.164 3 10 -4 1 472.816 128.336 2 -10 4 -2 126.554 68.3155 3 -10 4 -3 70.7664 59.7808 3 -10 4 -4 155.985 81.9631 3 -10 4 -5 1526.45 192.108 3 -10 4 -6 2679.93 257.925 3 -10 3 13 7967.55 546.888 1 -10 3 12 868.518 184.017 1 -10 3 11 2.57174 74.1402 1 -10 3 10 462.069 134.181 1 -10 3 9 224.424 93.4129 1 -10 3 8 7607.41 500.931 1 -10 3 7 9034.71 542.924 1 -10 3 6 309.827 109.588 1 10 -3 -5 562.243 133.453 2 10 -3 -4 200.529 100.141 2 -10 3 3-62.5614 62.1666 3 10 -3 -3 16.0510 61.0040 2 -10 3 2 479.923 108.195 3 10 -3 -2 674.802 142.804 2 -10 3 1 752.112 126.764 3 10 -3 -1 1049.26 184.110 2 10 -3 0 4245.07 359.877 2 -10 3 0 3989.80 298.789 3 10 -3 1 10253.9 554.898 2 -10 3 -1 9242.21 463.642 3 -10 3 -2 4696.77 332.398 3 -10 3 -3 566.703 121.481 3 -10 3 -4 232.985 82.7374 3 -10 3 -5 8.90916 50.2491 3 -10 2 13 1347.88 226.137 1 -10 2 12 897.083 184.725 1 -10 2 11 4518.44 387.985 1 -10 2 10 120.019 91.1842 1 -10 2 9 2720.21 293.979 1 -10 2 8 2493.84 281.440 1 -10 2 7-60.5380 87.5846 1 -10 2 6 9471.05 561.165 1 -10 2 5 10903.9 610.866 1 10 -2 -5 11719.0 595.027 2 -10 2 4 2680.61 243.320 3 10 -2 -4 2790.18 284.905 2 -10 2 3 4473.02 314.163 3 10 -2 -3 4681.42 376.866 2 -10 2 2 240.201 85.7757 3 10 -2 -2 131.431 70.1078 2 -10 2 1 255.984 84.9401 3 10 -2 -1 485.603 125.724 2 -10 2 0 237.592 84.8222 3 10 -2 0 397.263 117.770 2 10 -2 1 3453.92 321.529 2 -10 2 -1 3223.77 280.349 3 -10 2 -2 941.402 159.892 3 -10 2 -3 4086.31 319.402 3 -10 2 -4 309.888 97.5798 3 -10 1 12 6717.08 483.886 1 -10 1 11 1075.44 194.111 1 -10 1 10 1335.23 216.462 1 -10 1 9 819.092 168.199 1 -10 1 8 1899.67 249.941 1 -10 1 7 278.978 117.570 1 -10 1 6 3415.53 335.498 1 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486.382 117.696 4 11 -8 -6 646.988 156.984 2 -11 8 4 64.5485 66.0235 4 -11 8 3 160.289 83.9961 4 -11 8 2 1035.29 159.957 4 -11 8 1 2425.39 248.042 4 11 -7 -9 38.6214 71.2582 2 11 -7 -8 1405.05 222.850 2 11 -7 -7 1320.83 210.095 2 11 -7 -6 4586.16 386.588 2 11 -7 -5 280.025 111.657 2 -11 7 4 2904.41 256.176 4 11 -7 -4 3399.60 333.506 2 11 -7 -3 140.933 94.0941 2 -11 7 3 57.4319 58.2155 4 -11 7 2 77.4594 68.0677 4 -11 7 1 86.3160 65.3752 4 -11 7 0 59.1500 57.1483 4 -11 6 10 95.8055 83.8888 1 11 -6 -9 536.733 131.602 2 11 -6 -8 231.420 82.1535 2 11 -6 -7 1726.48 244.896 2 11 -6 -6 4238.18 372.241 2 11 -6 -5 3079.58 321.194 2 -11 6 4 2457.26 230.892 4 11 -6 -4 2648.74 296.300 2 11 -6 -3 580.888 145.628 2 -11 6 3 382.799 102.841 4 11 -6 -2 252.288 100.127 2 -11 6 2 280.189 105.099 4 -11 6 1 65.0205 67.7514 4 -11 6 0 1894.76 221.882 4 -11 6 -1 8468.04 481.708 4 -11 5 10 2316.03 305.992 1 -11 5 9 339.855 129.903 1 11 -5 -8 741.235 161.934 2 11 -5 -7-3.86198 72.0337 2 11 -5 -6 864.410 182.494 2 11 -5 -5 2641.29 289.346 2 11 -5 -4 7151.90 481.776 2 11 -5 -3 5803.60 439.266 2 11 -5 -2 1444.77 223.313 2 11 -5 -1 9.78655 60.4106 2 -11 5 0 124.567 68.0980 3 -11 5 -1-28.3922 49.4085 3 -11 5 -2 2883.37 261.322 3 -11 5 -3 3543.09 294.478 3 -11 4 10 2839.94 328.108 1 -11 4 9 1712.45 253.353 1 -11 4 8 175.414 103.181 1 11 -4 -7 340.037 111.303 2 11 -4 -6 506.301 142.472 2 11 -4 -5 2171.37 275.608 2 11 -4 -4 2321.31 275.256 2 11 -4 -3 3665.36 350.455 2 11 -4 -2 589.687 145.718 2 -11 4 1 982.738 157.065 3 11 -4 -1 1387.97 220.269 2 -11 4 0-35.4305 45.9261 3 11 -4 0 67.7075 89.6906 2 -11 4 -1-86.7107 57.0520 3 -11 4 -2 39.6011 51.2764 3 -11 4 -3 617.216 131.308 3 -11 3 10 2213.80 289.600 1 -11 3 9 2493.50 299.773 1 -11 3 8 2343.35 304.310 1 -11 3 7 784.858 179.916 1 11 -3 -7 471.496 139.388 2 11 -3 -6 3.13556 76.7269 2 11 -3 -5 288.338 121.532 2 11 -3 -4 2761.93 306.940 2 11 -3 -3 7248.71 500.024 2 -11 3 2 3099.71 278.384 3 11 -3 -2 3434.24 337.395 2 11 -3 -1 2479.15 291.546 2 -11 3 1 1910.67 219.931 3 -11 3 0 112.012 62.8432 3 11 -3 0 16.9911 65.1801 2 -11 3 -1 47.7702 54.2915 3 -11 2 9 751.695 183.044 1 -11 2 8 8951.09 580.602 1 -11 2 7 5729.92 457.631 1 11 -2 -6 1372.63 219.176 2 -11 2 6 1291.67 228.109 1 11 -2 -5 791.129 175.732 2 -11 2 4-0.55412 60.4675 3 11 -2 -4-34.1458 87.8022 2 -11 2 3-51.5578 56.1952 3 11 -2 -3-10.0355 58.7471 2 -11 2 2 1582.70 204.463 3 11 -2 -2 1667.44 241.578 2 -11 2 1 5840.69 393.399 3 11 -2 -1 6331.95 466.363 2 11 -2 0 2169.19 272.555 2 -11 1 9 265.788 126.771 1 -11 1 8 2740.13 318.598 1 -11 1 7 198.811 105.147 1 11 -1 -6 568.405 148.908 2 -11 1 6 774.915 185.112 1 11 -1 -5 2325.32 278.541 2 -11 1 4 369.847 110.709 3 11 -1 -4 453.706 143.188 2 -11 1 3 392.350 124.393 3 11 -1 -3 142.969 80.4581 2 11 -1 -2 354.280 121.802 2 11 -1 -1 249.962 111.186 2 11 -1 0 1288.20 214.115 2 11 -1 1 2938.97 307.687 2 -11 0 8 130.018 104.009 1 -11 0 7 1613.90 254.831 1 -11 0 6 4557.39 419.693 1 11 0 -5 1282.02 212.476 2 11 0 -4 1189.05 200.347 2 11 0 -3 24.5910 61.8056 2 11 0 -2 108.809 85.1760 2 11 0 -1-41.5614 81.1216 2 11 0 0 2479.16 287.581 2 -11 -1 6 1116.41 212.070 1 11 1 -5 1604.32 239.721 2 11 1 -4 3713.22 359.804 2 11 1 -3 964.993 193.855 2 11 1 -2 1918.05 255.884 2 11 2 -5 3294.55 339.445 2 11 2 -4 4733.30 406.570 2 -12 7 3 2.56346 56.9116 4 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 85134 data_8 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C3 H6 O)' _chemical_formula_sum 'C42 H44 Cl2 Cu N8 O10' _chemical_formula_weight 955.29 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.4814(4) _cell_length_b 9.7136(5) _cell_length_c 13.3146(9) _cell_angle_alpha 69.117(6) _cell_angle_beta 80.660(5) _cell_angle_gamma 68.833(5) _cell_volume 1067.61(11) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 2736 _cell_measurement_theta_min 5.0260 _cell_measurement_theta_max 29.2670 _exptl_crystal_description prism _exptl_crystal_colour purple _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.486 _exptl_crystal_F_000 495 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.10 _exptl_absorpt_coefficient_mu 0.705 _shelx_estimated_absorpt_T_min 0.896 _shelx_estimated_absorpt_T_max 0.933 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.586 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 8762 _diffrn_reflns_av_unetI/netI 0.0695 _diffrn_reflns_av_R_equivalents 0.0449 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.880 _diffrn_reflns_theta_max 26.999 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 4579 _reflns_number_gt 3483 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0548P)^2^+0.4849P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4579 _refine_ls_number_parameters 294 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0727 _refine_ls_R_factor_gt 0.0517 _refine_ls_wR_factor_ref 0.1348 _refine_ls_wR_factor_gt 0.1189 _refine_ls_goodness_of_fit_ref 1.062 _refine_ls_restrained_S_all 1.062 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.5000 0.01941(16) Uani 1 2 d S . P . . N1A N -0.2753(3) 0.4572(3) 0.4290(2) 0.0218(5) Uani 1 1 d D . . . . H1A H -0.288(4) 0.545(2) 0.436(3) 0.033 Uiso 1 1 d D U . . . C2A C -0.1527(3) 0.3337(3) 0.4674(2) 0.0217(6) Uani 1 1 d . . . . . H2A H -0.0705 0.3364 0.4982 0.026 Uiso 1 1 calc R U . . . N3A N -0.1627(2) 0.2082(3) 0.4562(2) 0.0202(5) Uani 1 1 d . . . . . C4A C -0.2989(3) 0.2542(3) 0.4088(2) 0.0209(6) Uani 1 1 d . . . . . H4A H -0.3366 0.1879 0.3909 0.025 Uiso 1 1 calc R U . . . C5A C -0.3707(3) 0.4103(3) 0.3917(2) 0.0201(6) Uani 1 1 d . . . . . C6A C -0.5164(3) 0.5148(3) 0.3430(2) 0.0212(6) Uani 1 1 d . . . . . C7A C -0.5507(3) 0.6772(3) 0.3044(3) 0.0260(7) Uani 1 1 d . . . . . H7A H -0.4789 0.7221 0.3087 0.031 Uiso 1 1 calc R U . . . C8A C -0.6894(4) 0.7721(4) 0.2599(3) 0.0295(7) Uani 1 1 d . . . . . H8A H -0.7120 0.8821 0.2333 0.035 Uiso 1 1 calc R U . . . C9A C -0.7953(3) 0.7083(4) 0.2537(3) 0.0292(7) Uani 1 1 d . . . . . H9A H -0.8909 0.7743 0.2242 0.035 Uiso 1 1 calc R U . . . C10A C -0.7617(3) 0.5478(4) 0.2906(3) 0.0297(7) Uani 1 1 d . . . . . H10A H -0.8333 0.5034 0.2852 0.036 Uiso 1 1 calc R U . . . C11A C -0.6230(3) 0.4521(4) 0.3357(3) 0.0251(7) Uani 1 1 d . . . . . H11A H -0.6010 0.3421 0.3619 0.030 Uiso 1 1 calc R U . . . N1B N 0.3161(3) 0.1490(3) 0.2740(2) 0.0225(6) Uani 1 1 d . . . . . H1B H 0.410(4) 0.145(4) 0.259(3) 0.034 Uiso 1 1 d . U . . . C2B C 0.2715(3) 0.0715(3) 0.3720(3) 0.0227(6) Uani 1 1 d . . . . . H2B H 0.3354 0.0147 0.4316 0.027 Uiso 1 1 calc R U . . . N3B N 0.1281(3) 0.0841(3) 0.3752(2) 0.0212(5) Uani 1 1 d . . . . . C4B C 0.0791(3) 0.1737(3) 0.2724(3) 0.0217(6) Uani 1 1 d . . . . . H4B H -0.0206 0.2024 0.2498 0.026 Uiso 1 1 calc R U . . . C5B C 0.1949(3) 0.2149(3) 0.2080(3) 0.0212(6) Uani 1 1 d . . . . . C6B C 0.2045(3) 0.3041(3) 0.0933(3) 0.0239(7) Uani 1 1 d . . . . . C7B C 0.2942(4) 0.3995(4) 0.0550(3) 0.0341(8) Uani 1 1 d . . . . . H7B H 0.3489 0.4110 0.1037 0.041 Uiso 1 1 calc R U . . . C8B C 0.3038(4) 0.4782(4) -0.0549(3) 0.0442(10) Uani 1 1 d . . . . . H8B H 0.3666 0.5418 -0.0812 0.053 Uiso 1 1 calc R U . . . C9B C 0.2236(4) 0.4643(4) -0.1251(3) 0.0421(10) Uani 1 1 d . . . . . H9B H 0.2317 0.5176 -0.1999 0.050 Uiso 1 1 calc R U . . . C10B C 0.1311(4) 0.3740(4) -0.0884(3) 0.0395(9) Uani 1 1 d . . . . . H10B H 0.0735 0.3668 -0.1373 0.047 Uiso 1 1 calc R U . . . C11B C 0.1225(4) 0.2931(4) 0.0210(3) 0.0304(7) Uani 1 1 d . . . . . H11B H 0.0597 0.2295 0.0464 0.037 Uiso 1 1 calc R U . . . Cl Cl 0.22342(8) 0.16061(8) 0.62128(6) 0.02379(19) Uani 1 1 d . . . . . O1 O 0.1220(2) 0.0774(2) 0.62806(18) 0.0254(5) Uani 1 1 d . . . . . O2 O 0.3752(2) 0.0722(3) 0.5974(2) 0.0327(6) Uani 1 1 d . . . . . O3 O 0.2175(2) 0.1888(3) 0.7209(2) 0.0338(6) Uani 1 1 d . . . . . O4 O 0.1778(2) 0.3086(2) 0.5359(2) 0.0329(6) Uani 1 1 d . . . . . C12 C 0.6675(3) 0.1128(4) 0.1203(3) 0.0307(8) Uani 1 1 d . . . . . O5 O 0.6026(2) 0.1788(3) 0.18518(19) 0.0294(5) Uani 1 1 d . . . . . C13 C 0.5917(4) 0.0436(4) 0.0704(3) 0.0398(9) Uani 1 1 d . . . . . H13A H 0.4950 0.0409 0.1089 0.060 Uiso 1 1 calc R U . . . H13B H 0.6569 -0.0628 0.0748 0.060 Uiso 1 1 calc R U . . . H13C H 0.5737 0.1072 -0.0052 0.060 Uiso 1 1 calc R U . . . C14 C 0.8278(4) 0.1021(5) 0.0827(4) 0.0506(11) Uani 1 1 d . . . . . H14A H 0.8291 0.1760 0.0099 0.076 Uiso 1 1 calc R U . . . H14B H 0.8852 -0.0041 0.0820 0.076 Uiso 1 1 calc R U . . . H14C H 0.8740 0.1276 0.1315 0.076 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0183(3) 0.0178(3) 0.0185(3) -0.0032(2) -0.00156(19) -0.00400(19) N1A 0.0254(12) 0.0162(12) 0.0245(15) -0.0081(11) -0.0040(10) -0.0049(10) C2A 0.0210(14) 0.0207(15) 0.0201(17) -0.0026(12) -0.0041(12) -0.0058(11) N3A 0.0199(12) 0.0195(13) 0.0190(14) -0.0038(10) -0.0003(10) -0.0066(10) C4A 0.0220(14) 0.0220(15) 0.0180(17) -0.0046(12) -0.0016(12) -0.0080(12) C5A 0.0210(14) 0.0223(15) 0.0156(16) -0.0046(12) 0.0006(11) -0.0077(11) C6A 0.0239(14) 0.0209(15) 0.0171(16) -0.0079(12) -0.0003(12) -0.0040(11) C7A 0.0256(15) 0.0220(16) 0.0297(19) -0.0078(14) -0.0028(13) -0.0069(12) C8A 0.0343(17) 0.0186(16) 0.028(2) -0.0057(14) -0.0046(14) -0.0008(13) C9A 0.0236(15) 0.0325(18) 0.0257(19) -0.0126(15) -0.0058(13) 0.0026(13) C10A 0.0267(16) 0.0354(18) 0.030(2) -0.0117(15) -0.0044(14) -0.0106(13) C11A 0.0257(15) 0.0222(16) 0.0258(18) -0.0076(13) -0.0036(13) -0.0053(12) N1B 0.0194(12) 0.0265(14) 0.0224(15) -0.0079(11) 0.0014(10) -0.0094(10) C2B 0.0250(15) 0.0235(16) 0.0195(17) -0.0072(13) -0.0023(12) -0.0071(12) N3B 0.0210(12) 0.0192(13) 0.0212(15) -0.0054(11) -0.0015(10) -0.0051(10) C4B 0.0225(14) 0.0197(15) 0.0198(17) -0.0040(12) -0.0025(12) -0.0050(11) C5B 0.0208(14) 0.0178(14) 0.0222(17) -0.0055(12) -0.0017(12) -0.0037(11) C6B 0.0233(15) 0.0200(15) 0.0215(18) -0.0058(13) 0.0014(12) -0.0012(12) C7B 0.0292(17) 0.0292(18) 0.032(2) -0.0002(15) 0.0014(14) -0.0072(13) C8B 0.0361(19) 0.035(2) 0.042(3) 0.0042(17) 0.0075(17) -0.0090(16) C9B 0.040(2) 0.037(2) 0.021(2) 0.0008(16) 0.0082(16) 0.0046(16) C10B 0.044(2) 0.038(2) 0.023(2) -0.0105(16) -0.0042(16) 0.0028(16) C11B 0.0333(17) 0.0283(17) 0.0246(19) -0.0074(14) -0.0003(14) -0.0059(13) Cl 0.0234(4) 0.0229(4) 0.0267(4) -0.0086(3) -0.0042(3) -0.0075(3) O1 0.0257(11) 0.0217(11) 0.0293(13) -0.0078(9) -0.0018(9) -0.0086(9) O2 0.0222(11) 0.0412(14) 0.0337(15) -0.0130(11) -0.0023(10) -0.0079(10) O3 0.0404(13) 0.0366(13) 0.0306(14) -0.0170(11) -0.0063(10) -0.0116(10) O4 0.0387(13) 0.0238(12) 0.0368(15) -0.0027(10) -0.0109(11) -0.0140(10) C12 0.0266(16) 0.0357(19) 0.027(2) -0.0082(16) -0.0030(14) -0.0086(14) O5 0.0256(11) 0.0321(12) 0.0306(14) -0.0089(11) -0.0005(10) -0.0110(9) C13 0.0361(19) 0.045(2) 0.043(2) -0.0230(19) -0.0079(16) -0.0065(16) C14 0.034(2) 0.077(3) 0.049(3) -0.027(2) 0.0093(18) -0.0260(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3B 2.000(2) 2_556 ? Cu N3B 2.000(2) . ? Cu N3A 2.002(2) . ? Cu N3A 2.002(2) 2_556 ? N1A C2A 1.341(4) . ? N1A C5A 1.371(4) . ? N1A H1A 0.851(10) . ? C2A N3A 1.318(4) . ? C2A H2A 0.9500 . ? N3A C4A 1.384(4) . ? C4A C5A 1.368(4) . ? C4A H4A 0.9500 . ? C5A C6A 1.472(4) . ? C6A C11A 1.386(4) . ? C6A C7A 1.401(4) . ? C7A C8A 1.385(4) . ? C7A H7A 0.9500 . ? C8A C9A 1.383(5) . ? C8A H8A 0.9500 . ? C9A C10A 1.385(5) . ? C9A H9A 0.9500 . ? C10A C11A 1.389(4) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.341(4) . ? N1B C5B 1.378(4) . ? N1B H1B 0.87(3) . ? C2B N3B 1.316(4) . ? C2B H2B 0.9500 . ? N3B C4B 1.383(4) . ? C4B C5B 1.366(4) . ? C4B H4B 0.9500 . ? C5B C6B 1.470(4) . ? C6B C11B 1.385(5) . ? C6B C7B 1.391(4) . ? C7B C8B 1.395(5) . ? C7B H7B 0.9500 . ? C8B C9B 1.365(6) . ? C8B H8B 0.9500 . ? C9B C10B 1.374(5) . ? C9B H9B 0.9500 . ? C10B C11B 1.392(5) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.436(3) . ? Cl O2 1.436(2) . ? Cl O1 1.438(2) . ? Cl O4 1.447(2) . ? C12 O5 1.213(4) . ? C12 C13 1.494(5) . ? C12 C14 1.500(5) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Cu N3B 180.0 2_556 . ? N3B Cu N3A 91.61(9) 2_556 . ? N3B Cu N3A 88.39(9) . . ? N3B Cu N3A 88.39(9) 2_556 2_556 ? N3B Cu N3A 91.61(9) . 2_556 ? N3A Cu N3A 180.0 . 2_556 ? C2A N1A C5A 109.0(2) . . ? C2A N1A H1A 121(2) . . ? C5A N1A H1A 130(2) . . ? N3A C2A N1A 110.2(3) . . ? N3A C2A H2A 124.9 . . ? N1A C2A H2A 124.9 . . ? C2A N3A C4A 106.5(2) . . ? C2A N3A Cu 122.86(19) . . ? C4A N3A Cu 130.7(2) . . ? C5A C4A N3A 109.2(3) . . ? C5A C4A H4A 125.4 . . ? N3A C4A H4A 125.4 . . ? C4A C5A N1A 105.1(2) . . ? C4A C5A C6A 130.6(3) . . ? N1A C5A C6A 124.3(3) . . ? C11A C6A C7A 118.9(3) . . ? C11A C6A C5A 119.6(3) . . ? C7A C6A C5A 121.5(3) . . ? C8A C7A C6A 119.9(3) . . ? C8A C7A H7A 120.0 . . ? C6A C7A H7A 120.0 . . ? C9A C8A C7A 120.6(3) . . ? C9A C8A H8A 119.7 . . ? C7A C8A H8A 119.7 . . ? C8A C9A C10A 119.8(3) . . ? C8A C9A H9A 120.1 . . ? C10A C9A H9A 120.1 . . ? C9A C10A C11A 119.8(3) . . ? C9A C10A H10A 120.1 . . ? C11A C10A H10A 120.1 . . ? C6A C11A C10A 120.9(3) . . ? C6A C11A H11A 119.6 . . ? C10A C11A H11A 119.6 . . ? C2B N1B C5B 108.2(2) . . ? C2B N1B H1B 121(2) . . ? C5B N1B H1B 130(2) . . ? N3B C2B N1B 111.4(3) . . ? N3B C2B H2B 124.3 . . ? N1B C2B H2B 124.3 . . ? C2B N3B C4B 105.5(2) . . ? C2B N3B Cu 128.9(2) . . ? C4B N3B Cu 125.55(18) . . ? C5B C4B N3B 110.1(3) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 104.9(3) . . ? C4B C5B C6B 132.0(3) . . ? N1B C5B C6B 123.1(3) . . ? C11B C6B C7B 118.9(3) . . ? C11B C6B C5B 119.4(3) . . ? C7B C6B C5B 121.8(3) . . ? C6B C7B C8B 119.8(4) . . ? C6B C7B H7B 120.1 . . ? C8B C7B H7B 120.1 . . ? C9B C8B C7B 120.4(3) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C8B C9B C10B 120.6(3) . . ? C8B C9B H9B 119.7 . . ? C10B C9B H9B 119.7 . . ? C9B C10B C11B 119.5(4) . . ? C9B C10B H10B 120.3 . . ? C11B C10B H10B 120.3 . . ? C6B C11B C10B 120.8(3) . . ? C6B C11B H11B 119.6 . . ? C10B C11B H11B 119.6 . . ? O3 Cl O2 109.89(14) . . ? O3 Cl O1 110.05(13) . . ? O2 Cl O1 110.00(13) . . ? O3 Cl O4 109.00(14) . . ? O2 Cl O4 108.90(14) . . ? O1 Cl O4 108.98(13) . . ? O5 C12 C13 122.5(3) . . ? O5 C12 C14 121.2(3) . . ? C13 C12 C14 116.3(3) . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C12 C14 H14A 109.5 . . ? C12 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C12 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? _refine_diff_density_max 0.857 _refine_diff_density_min -0.856 _refine_diff_density_rms 0.090 _shelx_res_file ; 8.res created by SHELXL-2014/7 TITL EL26G in P-1 CELL 0.71073 9.4814 9.7136 13.3146 69.117 80.660 68.833 ZERR 1 0.0004 0.0005 0.0009 0.0056 0.0047 0.0045 LATT 1 SFAC C H N O CL CU UNIT 42 44 8 10 2 1 MERG 2 OMIT -2 54 OMIT -1 -1 2 OMIT 0 0 3 SIZE 0.16 0.11 0.10 TEMP -173 MORE -3 FMAP 2 PLAN 10 ACTA BOND BOND $H HTAB LIST 4 L.S. 7 WGHT 0.054800 0.484900 FVAR 2.88086 CU 6 0.000000 0.000000 0.500000 10.50000 0.01826 0.01778 = 0.01851 -0.00323 -0.00156 -0.00400 DFIX 0.86 0.01 N1A H1A N1A 3 -0.275252 0.457161 0.429048 11.00000 0.02537 0.01621 = 0.02452 -0.00814 -0.00404 -0.00486 H1A 2 -0.288010 0.544849 0.435813 11.00000 -1.50000 C2A 1 -0.152687 0.333726 0.467414 11.00000 0.02103 0.02073 = 0.02013 -0.00262 -0.00415 -0.00584 AFIX 43 H2A 2 -0.070488 0.336437 0.498212 11.00000 -1.20000 AFIX 0 N3A 3 -0.162681 0.208167 0.456248 11.00000 0.01986 0.01948 = 0.01905 -0.00378 -0.00031 -0.00660 C4A 1 -0.298922 0.254184 0.408777 11.00000 0.02197 0.02201 = 0.01805 -0.00464 -0.00156 -0.00798 AFIX 43 H4A 2 -0.336638 0.187909 0.390872 11.00000 -1.20000 AFIX 0 C5A 1 -0.370746 0.410256 0.391697 11.00000 0.02101 0.02233 = 0.01556 -0.00457 0.00058 -0.00766 C6A 1 -0.516406 0.514780 0.343015 11.00000 0.02391 0.02093 = 0.01714 -0.00789 -0.00033 -0.00405 C7A 1 -0.550729 0.677161 0.304376 11.00000 0.02562 0.02197 = 0.02969 -0.00781 -0.00280 -0.00685 AFIX 43 H7A 2 -0.478939 0.722098 0.308715 11.00000 -1.20000 AFIX 0 C8A 1 -0.689401 0.772079 0.259856 11.00000 0.03431 0.01865 = 0.02821 -0.00566 -0.00464 -0.00075 AFIX 43 H8A 2 -0.711954 0.882071 0.233298 11.00000 -1.20000 AFIX 0 C9A 1 -0.795349 0.708301 0.253685 11.00000 0.02363 0.03251 = 0.02569 -0.01258 -0.00583 0.00263 AFIX 43 H9A 2 -0.890888 0.774336 0.224189 11.00000 -1.20000 AFIX 0 C10A 1 -0.761744 0.547815 0.290649 11.00000 0.02672 0.03537 = 0.02973 -0.01174 -0.00441 -0.01058 AFIX 43 H10A 2 -0.833339 0.503370 0.285189 11.00000 -1.20000 AFIX 0 C11A 1 -0.623037 0.452081 0.335723 11.00000 0.02572 0.02216 = 0.02576 -0.00756 -0.00360 -0.00525 AFIX 43 H11A 2 -0.600961 0.342149 0.361904 11.00000 -1.20000 AFIX 0 N1B 3 0.316138 0.148966 0.274022 11.00000 0.01935 0.02654 = 0.02238 -0.00788 0.00140 -0.00939 H1B 2 0.409888 0.144885 0.259282 11.00000 -1.50000 C2B 1 0.271528 0.071461 0.372036 11.00000 0.02502 0.02354 = 0.01954 -0.00717 -0.00231 -0.00708 AFIX 43 H2B 2 0.335368 0.014661 0.431602 11.00000 -1.20000 AFIX 0 N3B 3 0.128075 0.084130 0.375164 11.00000 0.02103 0.01924 = 0.02119 -0.00536 -0.00153 -0.00514 C4B 1 0.079050 0.173704 0.272367 11.00000 0.02255 0.01970 = 0.01979 -0.00401 -0.00251 -0.00499 AFIX 43 H4B 2 -0.020576 0.202435 0.249788 11.00000 -1.20000 AFIX 0 C5B 1 0.194862 0.214857 0.208004 11.00000 0.02075 0.01776 = 0.02222 -0.00551 -0.00167 -0.00370 C6B 1 0.204475 0.304096 0.093306 11.00000 0.02329 0.02000 = 0.02155 -0.00584 0.00138 -0.00119 C7B 1 0.294228 0.399452 0.055026 11.00000 0.02916 0.02919 = 0.03227 -0.00015 0.00137 -0.00717 AFIX 43 H7B 2 0.348868 0.410962 0.103658 11.00000 -1.20000 AFIX 0 C8B 1 0.303841 0.478164 -0.054949 11.00000 0.03614 0.03483 = 0.04152 0.00420 0.00746 -0.00903 AFIX 43 H8B 2 0.366616 0.541790 -0.081193 11.00000 -1.20000 AFIX 0 C9B 1 0.223597 0.464311 -0.125069 11.00000 0.04021 0.03742 = 0.02094 0.00079 0.00825 0.00464 AFIX 43 H9B 2 0.231734 0.517577 -0.199890 11.00000 -1.20000 AFIX 0 C10B 1 0.131144 0.373977 -0.088363 11.00000 0.04416 0.03818 = 0.02330 -0.01054 -0.00415 0.00281 AFIX 43 H10B 2 0.073545 0.366790 -0.137269 11.00000 -1.20000 AFIX 0 C11B 1 0.122534 0.293080 0.021029 11.00000 0.03332 0.02829 = 0.02461 -0.00740 -0.00030 -0.00589 AFIX 43 H11B 2 0.059657 0.229518 0.046419 11.00000 -1.20000 AFIX 0 CL 5 0.223424 0.160609 0.621277 11.00000 0.02340 0.02289 = 0.02672 -0.00863 -0.00421 -0.00750 O1 4 0.121958 0.077360 0.628062 11.00000 0.02566 0.02169 = 0.02933 -0.00782 -0.00181 -0.00860 O2 4 0.375240 0.072208 0.597432 11.00000 0.02217 0.04120 = 0.03367 -0.01298 -0.00232 -0.00785 O3 4 0.217515 0.188822 0.720882 11.00000 0.04036 0.03661 = 0.03060 -0.01697 -0.00627 -0.01158 O4 4 0.177757 0.308629 0.535867 11.00000 0.03874 0.02384 = 0.03677 -0.00267 -0.01090 -0.01399 C12 1 0.667454 0.112823 0.120288 11.00000 0.02660 0.03572 = 0.02730 -0.00822 -0.00301 -0.00856 O5 4 0.602629 0.178780 0.185177 11.00000 0.02561 0.03208 = 0.03064 -0.00895 -0.00045 -0.01104 C13 1 0.591742 0.043583 0.070394 11.00000 0.03614 0.04487 = 0.04261 -0.02302 -0.00793 -0.00652 AFIX 137 H13A 2 0.494963 0.040901 0.108882 11.00000 -1.50000 H13B 2 0.656894 -0.062786 0.074766 11.00000 -1.50000 H13C 2 0.573692 0.107205 -0.005203 11.00000 -1.50000 AFIX 0 C14 1 0.827818 0.102132 0.082661 11.00000 0.03436 0.07736 = 0.04856 -0.02704 0.00932 -0.02598 AFIX 137 H14A 2 0.829061 0.175959 0.009882 11.00000 -1.50000 H14B 2 0.885196 -0.004109 0.082015 11.00000 -1.50000 H14C 2 0.873980 0.127560 0.131501 11.00000 -1.50000 AFIX 0 HKLF 4 REM EL26G in P-1 REM R1 = 0.0517 for 3483 Fo > 4sig(Fo) and 0.0727 for all 4579 data REM 294 parameters refined using 1 restraints END WGHT 0.0543 0.5068 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y+1, -z+1 HTAB N1A Cl_$1 HTAB N1A O4_$1 HTAB C2A O4 EQIV $2 -x, -y, -z+1 HTAB C4A O2_$2 HTAB N1B O5 HTAB C2B O2 EQIV $3 -x+1, -y, -z+1 HTAB C2B O2_$3 REM Highest difference peak 0.857, deepest hole -0.856, 1-sigma level 0.090 Q1 1 0.0848 0.0479 0.4669 11.00000 0.05 0.77 Q2 1 -0.1208 0.0775 0.5025 11.00000 0.05 0.53 Q3 1 0.0032 0.1025 0.4925 11.00000 0.05 0.51 Q4 1 -0.0173 0.1203 0.4575 11.00000 0.05 0.48 Q5 1 0.1427 0.1231 0.6438 11.00000 0.05 0.44 Q6 1 0.1711 0.1406 0.7041 11.00000 0.05 0.43 Q7 1 0.3183 0.1903 0.5926 11.00000 0.05 0.43 Q8 1 0.1413 0.1632 0.2184 11.00000 0.05 0.41 Q9 1 -0.4594 0.6915 0.2607 11.00000 0.05 0.40 Q10 1 -0.5234 0.5993 0.2982 11.00000 0.05 0.37 ; _shelx_res_checksum 66247 _shelx_hkl_file ; 0 0 2 6409.14 228.697 6 0 0 3 16072.2 459.021 6 0 0 4 3161.45 235.193 6 0 0 5 4117.25 295.762 6 0 0 6 8183.36 449.809 6 0 0 7 7376.08 463.081 6 0 0 8 11091.6 613.071 6 0 0 -8 10921.3 647.452 6 0 0 -9 15846.2 836.658 6 0 0 9 15816.3 773.852 6 0 0 10 2486.72 332.143 6 0 0 11 1512.71 270.744 6 0 0 12 759.000 220.487 6 0 0 13 8.36277 116.886 6 0 0 14 83.1235 88.6330 6 0 0 15-32.2574 115.718 6 0 0 16 333.258 192.630 6 0 -1 15 89.4655 104.294 6 0 -1 14-41.6387 114.072 6 0 -1 13-386.185 163.499 6 0 -1 12 622.767 190.412 6 0 -1 11 30.6252 101.738 6 0 -1 10 6386.04 525.737 6 0 -1 9 17996.1 828.701 6 0 -1 8 11577.3 625.113 6 0 1 -8 13630.2 743.767 6 0 -1 7 845.022 178.920 6 0 -1 6 1208.48 184.158 6 0 -1 5 6231.66 375.666 6 0 1 -4 3200.15 124.664 5 0 -1 4 3316.92 248.865 6 0 -1 3 1840.84 172.299 6 0 -1 2 23431.8 507.215 6 0 -1 1 16930.8 352.456 6 0 1 2 15941.8 375.641 6 0 1 3 24467.9 551.839 6 0 1 4 3704.11 259.754 6 0 1 5 136.776 81.5198 6 0 1 6 119.857 70.2233 6 0 1 7 24218.7 824.105 6 0 1 8 28301.4 960.372 6 0 -1 -9 7813.50 566.010 6 0 1 9 6914.37 517.691 6 0 1 10 918.634 204.028 6 0 1 11 200.545 105.713 6 0 1 12 562.896 181.298 6 0 1 13 220.244 136.381 6 0 1 14 2329.55 388.186 6 0 1 15 2170.80 392.481 6 0 1 16 1064.45 280.541 6 0 -2 14 1205.17 297.345 6 0 -2 13 1940.21 351.538 6 0 -2 12 3120.16 422.356 6 0 -2 11 6403.09 578.357 6 0 -2 10 324.892 140.506 6 0 -2 9 1940.62 299.023 6 0 -2 8-68.4806 68.4989 6 0 -2 7 2247.65 287.387 6 0 2 -7 2605.94 322.648 6 0 -2 6 901.945 173.891 6 0 2 -6 1035.56 97.5863 5 0 -2 5 495.455 122.822 6 0 -2 4 6629.20 381.977 6 0 -2 3 5727.35 332.701 6 0 -2 2 102405. 1202.07 6 0 -2 1 790.032 102.333 6 0 2 0 303.983 56.4087 4 0 2 1 13174.0 330.571 4 0 2 2 1120.94 116.205 4 0 2 3 18691.6 472.318 4 0 2 4 37318.3 815.165 6 0 2 5 12321.1 527.017 6 0 2 6 43113.8 1041.91 6 0 2 7 22135.8 805.436 6 0 2 8 5123.26 418.777 6 0 -2 -9 23.2483 68.1559 6 0 2 9 144.329 97.4220 6 0 2 10 323.392 104.263 6 0 2 11 4315.67 470.616 6 0 2 12 80.5131 91.6922 6 0 2 12 92.4737 21.3542 5 0 2 13 812.979 233.329 6 0 2 14 4595.13 545.602 6 0 2 15 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1525.52 232.012 6 -2 3 -5 1345.98 227.648 6 2 -3 6-47.4686 79.4852 6 2 -3 7-37.7391 100.380 6 2 -3 8 3949.87 414.908 6 2 -3 9 10890.9 722.745 6 2 -3 10 1876.35 315.919 6 2 -3 11 179.377 119.546 6 2 -3 12 2476.68 396.594 6 2 -3 13 199.571 143.586 6 -2 2 16 415.932 153.187 6 -2 2 15 66.5872 82.1792 6 -2 2 14-33.6028 78.6002 6 -2 2 13 1621.29 310.021 6 -2 2 12-107.632 136.395 6 -2 2 11 10.7586 98.2072 6 2 -2 -10-77.3415 97.6591 6 -2 2 10 70.4262 77.4080 6 2 -2 -9 2185.28 295.393 6 -2 2 9 2594.83 312.916 6 2 -2 -9 2526.08 306.524 4 -2 2 8 8766.22 534.653 6 2 -2 -8 8477.83 522.851 4 2 -2 -8 7891.76 523.301 6 2 -2 -7 14136.8 626.685 4 -2 2 7 14290.0 647.199 6 -2 2 6 98.1085 61.5433 6 2 -2 -6 81.8769 58.1093 1 -2 2 5 3636.60 278.912 4 2 -2 -5 3015.24 248.165 1 -2 2 5 3520.52 277.150 6 -2 2 4 536.501 110.208 6 2 -2 -4 571.731 99.2790 1 -2 2 4 576.075 105.071 4 2 -2 -3 353.659 65.6940 3 2 -2 -3 300.457 77.3404 1 -2 2 3 350.051 87.3537 4 -2 2 2 1110.63 111.892 1 -2 2 2 1151.70 131.632 4 2 -2 -2 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16392.6 817.867 6 2 -1 -9 14509.7 737.367 4 -2 1 9 13405.2 689.505 6 2 -1 -9 13858.8 747.935 6 2 -1 -8 1728.11 241.905 4 -2 1 8 1343.28 208.961 6 -2 1 7 1151.29 181.193 6 2 -1 -6 50.5205 51.1519 6 2 -1 -6 83.6805 50.5979 4 -2 1 6-26.2675 48.1620 6 2 -1 -6 93.7087 38.2010 1 -2 1 5 4687.02 304.361 6 2 -1 -5 4095.46 290.505 1 2 -1 -5 4078.35 285.810 4 2 -1 -5 4070.08 287.565 6 2 -1 -4 2609.80 213.424 1 -2 1 4 2368.64 195.725 6 2 -1 -4 2552.20 201.923 4 -2 1 3 146.547 62.9195 6 2 -1 -3 181.186 57.5666 1 -2 1 3 181.213 59.2581 4 2 -1 -2 34784.7 536.773 3 -2 1 2 35959.9 650.518 1 2 -1 -2 34664.3 638.901 1 -2 1 2 35206.2 604.888 4 -2 1 1 507.481 72.0687 1 2 -1 -1 539.547 76.6973 1 -2 1 1 510.145 60.4377 3 2 -1 -1 613.946 67.7975 3 -2 1 1 456.402 68.4688 4 -2 1 0 57689.3 666.719 6 -2 1 0 56897.4 611.122 3 -2 1 0 61866.8 751.395 4 -2 1 0 57908.8 698.378 2 2 -1 0 59154.9 626.538 6 -2 1 -1 2283.23 160.178 6 -2 1 -1 2350.08 149.109 2 2 -1 1 2442.83 162.363 6 -2 1 -2 75.6213 49.7513 6 2 -1 2 35.0801 49.7542 6 -2 1 -3 38804.6 850.182 6 2 -1 3 40331.7 857.112 6 2 -1 4 5751.59 356.699 6 2 -1 5 390.687 120.913 6 2 -1 6 2295.86 259.643 6 2 -1 7 6217.65 456.745 6 -2 1 -7 6521.55 499.757 6 2 -1 8 4545.45 420.409 6 2 -1 9 62.8139 71.1365 6 2 -1 10 73.2737 84.2852 6 2 -1 11 446.196 191.983 6 2 -1 12 1209.77 283.941 6 2 -1 13 2672.62 432.915 6 2 -1 14 2436.82 415.143 6 -2 0 16-238.608 147.024 6 -2 0 15 275.730 134.763 6 -2 0 14 24.5653 75.7916 6 -2 0 13 600.035 195.095 6 -2 0 12 5438.53 525.310 6 -2 0 11 2363.97 334.660 6 -2 0 11 2060.68 160.335 5 -2 0 10 4062.85 237.728 5 -2 0 10 4012.84 420.849 6 -2 0 9 2004.01 172.543 5 -2 0 9 2299.10 296.626 6 2 0 -9 2456.26 319.639 6 -2 0 8 4708.28 389.999 6 2 0 -8 5491.65 444.072 6 -2 0 7 9021.91 487.150 6 2 0 -6 70292.9 1321.11 1 -2 0 6 71765.6 1253.65 6 2 0 -6 70318.2 1310.98 6 2 0 -5 7187.38 391.103 1 2 0 -5 7050.86 377.748 6 -2 0 5 6693.94 347.738 6 2 0 -4 1064.77 142.368 1 -2 0 4 1146.16 133.120 6 2 0 -4 1290.79 147.482 4 2 0 -4 1116.38 130.186 6 2 0 -3 4964.84 235.058 6 2 0 -3 5073.60 279.923 1 -2 0 3 4769.10 218.093 6 2 0 -3 4785.90 240.087 4 -2 0 2 13940.4 293.064 6 -2 0 2 14649.7 352.404 4 2 0 -2 13303.6 293.605 6 2 0 -2 13351.0 330.643 4 2 0 -2 14337.0 422.759 1 2 0 -1 18.4027 35.9160 1 -2 0 1 47.6526 22.5709 4 -2 0 1 2.32202 15.5448 3 -2 0 0 96410.5 698.455 4 -2 0 0 96177.2 825.576 2 -2 0 0 92839.7 768.495 3 -2 0 -1 20.2699 29.0822 6 2 0 1 67.7135 37.2478 6 2 0 2 999.508 109.966 6 -2 0 -2 1067.55 109.512 6 -2 0 -3 9275.07 374.536 6 2 0 3 9268.34 374.847 6 2 0 4 26376.5 702.466 6 2 0 5 5110.33 347.196 6 -2 0 -6 4488.05 147.438 5 2 0 6 5927.95 401.401 6 2 0 7 418.149 123.790 6 2 0 8 6189.15 467.245 6 -2 0 -8 6884.48 518.629 6 2 0 9 3680.29 387.077 6 2 0 10 93.9652 96.9981 6 2 0 11 5691.63 534.870 6 2 0 12 6116.74 589.292 6 2 0 13 3114.88 444.385 6 2 0 14 1520.25 335.502 6 2 0 15 641.775 221.500 6 -2 -1 15 578.600 203.048 6 -2 -1 14 203.276 125.749 6 -2 -1 13 397.031 170.121 6 -2 -1 12 1932.35 316.189 6 -2 -1 11 3801.26 430.321 6 -2 -1 10 954.759 208.649 6 2 1 -9 426.982 141.675 6 -2 -1 9 479.065 138.804 6 2 1 -8 543.219 150.093 6 -2 -1 8 516.148 85.3525 5 -2 -1 8 522.951 138.071 6 2 1 -7 270.948 79.1004 1 -2 -1 7 253.847 61.9168 5 -2 -1 7 391.856 116.191 6 -2 -1 6 322.082 94.7136 6 -2 -1 6 215.797 54.5325 5 2 1 -6 367.840 103.670 1 2 1 -6 220.746 82.3134 6 2 1 -5 24661.8 736.628 1 -2 -1 5 23198.0 557.454 5 -2 -1 5 24542.8 682.873 6 2 1 -5 24450.4 730.332 6 -2 -1 4 24285.8 556.862 5 2 1 -4 27742.8 724.459 1 -2 -1 4 27066.3 640.279 6 2 1 -4 26264.6 677.377 6 2 1 -3 43005.9 832.087 1 -2 -1 3 42361.4 686.666 6 2 1 -3 40777.7 725.064 6 -2 -1 2 23922.9 429.617 6 2 1 -2 23853.1 451.456 6 2 1 -2 25685.2 588.436 1 2 1 -1 2535.77 171.180 1 -2 -1 1 2221.90 89.9613 6 2 1 -1 2480.41 107.941 6 -2 -1 0 6019.09 190.545 3 -2 -1 0 6118.54 194.684 2 2 1 1 16084.1 304.112 6 -2 -1 -1 15631.9 306.163 6 2 1 2 48015.9 678.576 6 -2 -1 -2 45059.4 658.099 6 2 1 3 20288.0 530.178 6 -2 -1 -3 20785.9 420.829 5 -2 -1 -4 33174.9 490.163 5 2 1 4 32686.3 761.907 6 2 1 5 16667.6 601.911 6 2 1 6 589.082 132.251 6 2 1 7 283.087 107.251 6 2 1 8 1129.98 206.317 6 2 1 9 2180.36 299.815 6 -2 -1 -9 1767.15 281.415 6 2 1 10 863.721 204.132 6 2 1 11 7019.16 588.097 6 2 1 12 3628.59 446.418 6 2 1 13 1870.16 341.652 6 2 1 14 1844.57 352.027 6 2 1 15 152.878 114.765 6 2 1 16 61.8761 107.271 6 -2 -2 15 719.537 256.821 6 -2 -2 14 620.536 209.413 6 -2 -2 13 105.060 101.268 6 -2 -2 12 1011.03 249.496 6 -2 -2 11 72.4932 81.7918 6 -2 -2 10 59.2013 61.9478 6 -2 -2 9 280.949 108.007 6 -2 -2 8 4708.34 404.545 6 2 2 -8 5401.09 485.475 6 2 2 -7 2107.68 257.149 1 -2 -2 7 2164.58 259.708 6 2 2 -7 2517.32 309.008 6 -2 -2 6 5.99239 43.3701 6 2 2 -6 73.3861 55.2365 1 -2 -2 5 453.142 110.359 6 2 2 -5 432.401 107.180 1 2 2 -5 390.433 115.535 6 2 2 -4 9415.22 436.150 1 -2 -2 4 9869.73 431.746 6 -2 -2 4 9520.44 347.761 5 2 2 -4 9438.37 455.066 6 2 2 -3 1.80185 34.2892 1 -2 -2 3-23.4391 42.6680 6 2 2 -3 17.7381 35.1357 6 -2 -2 3 40.3571 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577.513 4 2 3 0 44568.2 740.022 5 -2 -3 -1 944.335 86.2756 4 2 3 1 898.802 85.9782 4 -2 -3 -1 983.402 77.4486 3 2 3 1 951.707 77.7495 3 2 3 2 1439.41 113.515 4 -2 -3 -2 1319.16 92.2091 3 -2 -3 -2 1487.49 113.771 4 2 3 3 28.9198 31.2506 4 -2 -3 -3 48.2069 40.3435 4 -2 -3 -4 3567.97 231.735 4 2 3 4 4021.33 289.791 6 -2 -3 -5 720.005 121.757 4 2 3 5 608.943 131.135 6 2 3 6 4.68705 66.2924 6 -2 -3 -6-11.5433 45.3196 4 2 3 7 3999.07 351.048 6 2 3 8 41.7017 82.3100 6 -2 -3 -9 7773.64 563.171 6 2 3 9 7753.15 282.034 5 2 3 9 7597.03 544.658 6 2 3 10 4203.29 428.763 6 2 3 10 4061.47 202.138 5 2 3 11 3544.30 168.125 5 2 3 11 4015.95 449.009 6 2 3 12 276.188 127.030 6 2 3 13 2033.78 354.805 6 2 3 14 809.010 236.817 6 2 3 15 577.553 210.534 6 2 3 16-284.489 161.481 6 -2 -4 13 92.4218 99.7079 6 -2 -4 12 143.354 127.883 6 -2 -4 11 1910.01 338.033 6 -2 -4 10 3686.05 434.822 6 -2 -4 9 7283.04 567.732 6 -2 -4 8 1234.94 238.500 6 -2 -4 7 169.315 76.4741 6 2 4 -6 1924.16 296.008 6 -2 -4 6 1935.30 258.942 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21125.8 749.419 4 2 4 8 17274.8 791.690 6 -2 -4 -8 20464.7 792.817 4 -2 -4 -9 7565.15 521.163 4 -2 -4 -9 7374.59 558.185 6 2 4 9 7272.88 541.060 6 2 4 10 1092.85 235.010 6 2 4 11 978.701 222.293 6 2 4 12 1005.92 240.240 6 2 4 12 1134.25 124.078 5 2 4 13 2094.64 356.385 6 2 4 13 1863.69 143.950 5 2 4 14 452.993 180.511 6 2 4 15 1692.08 359.485 6 2 4 16 400.326 161.583 6 -2 -5 12 248.610 96.3955 6 -2 -5 11 28.6219 74.2782 6 -2 -5 10 917.315 232.171 6 -2 -5 9 933.781 215.484 6 -2 -5 8 92.4724 71.1573 6 2 5 -7 74.7752 53.5242 5 -2 -5 7 49.2758 63.1836 6 -2 -5 6 233.467 99.0654 6 2 5 -6 208.216 89.0707 1 2 5 -6 220.951 75.4677 5 2 5 -5 2206.98 265.333 1 -2 -5 5 2349.91 270.188 6 2 5 -5 2425.79 241.434 5 2 5 -4 1358.14 232.549 6 2 5 -4 1553.52 190.231 5 2 5 -4 1279.43 189.996 1 -2 -5 4 1409.56 198.478 6 2 5 -3 24023.8 741.406 1 -2 -5 3 25896.4 779.778 6 2 5 -3 27280.8 946.996 6 2 5 -2 16316.5 682.317 6 -2 -5 2 16951.1 594.473 6 2 5 -2 15097.9 536.383 1 2 5 -1 1409.22 149.785 1 2 5 -1 1772.45 187.503 4 2 5 -1 1542.41 121.954 3 2 5 0 4012.18 166.343 3 -2 -5 0 4083.38 235.338 1 2 5 0 3949.07 260.632 4 -2 -5 -1 65.4992 42.8988 1 2 5 1 28.1303 34.0482 4 2 5 2 235.002 60.8095 4 -2 -5 -2 175.520 59.7186 4 -2 -5 -3 28.6915 41.6413 4 2 5 3 36.8076 45.0260 4 -2 -5 -3 12.6959 12.7311 3 2 5 4 25.0320 36.9005 4 -2 -5 -4 51.4387 39.9251 4 -2 -5 -5 5587.07 347.193 4 2 5 5 5715.03 352.592 4 2 5 6 11343.6 530.626 4 2 5 6 10894.0 578.103 6 -2 -5 -6 12466.2 543.291 4 -2 -5 -7 14063.5 616.142 4 2 5 7 12441.3 653.286 6 -2 -5 -8 3963.08 352.011 4 2 5 8 3109.56 345.004 6 -2 -5 -9 120.924 74.3436 4 2 5 9-52.9532 107.762 6 2 5 10 2243.23 326.336 6 2 5 11 345.089 136.574 6 2 5 12 4934.67 533.366 6 2 5 13 1216.35 277.543 6 2 5 14 1218.44 290.094 6 2 5 15 2062.47 397.614 6 2 5 16 1160.85 297.388 6 -2 -6 11 4297.90 500.088 6 -2 -6 10 436.933 161.639 6 -2 -6 9 312.938 151.434 6 2 6 -8-45.5464 66.6065 5 -2 -6 8 9.48578 91.5182 6 2 6 -7-9.48563 67.3071 5 -2 -6 7 25.7597 66.8523 6 2 6 -6 867.151 161.509 5 2 6 -6 998.118 195.074 1 -2 -6 6 1232.59 222.182 6 -2 -6 5 941.059 202.105 6 2 6 -5 1188.31 180.635 5 2 6 -5 1456.44 225.002 1 2 6 -4 5984.26 415.659 1 2 6 -4 5414.02 373.982 5 -2 -6 4 6337.78 446.999 6 -2 -6 3 10369.9 534.821 6 2 6 -3 9215.15 477.018 1 2 6 -2 21113.2 745.972 4 2 6 -2 20520.4 844.631 6 2 6 -2 18348.6 611.936 1 2 6 -1 4054.48 200.039 3 2 6 -1 4560.22 330.752 4 2 6 -1 4436.24 377.175 6 2 6 0 792.056 75.7221 3 2 6 0 841.113 159.550 6 2 6 0 807.042 143.951 4 -2 -6 -1 1358.40 130.592 1 2 6 1 1274.43 164.658 4 2 6 2 589.371 115.908 4 -2 -6 -2 650.309 95.4300 1 2 6 3 663.517 115.058 4 -2 -6 -3 791.659 128.746 4 -2 -6 -4 43.3886 44.3600 4 -2 -6 -4 14.7697 12.8047 3 2 6 4-3.53137 35.3156 4 -2 -6 -5 1457.76 190.866 4 2 6 5 1627.06 204.812 4 2 6 6 6789.68 430.855 4 -2 -6 -6 8347.21 476.104 4 -2 -6 -7 212.388 85.0338 4 2 6 7 117.090 64.8536 4 2 6 7 74.3997 55.9194 6 2 6 8 145.856 102.852 6 -2 -6 -8 367.631 117.569 4 2 6 9 3473.19 402.865 6 2 6 10 167.434 89.5158 6 2 6 11-69.6149 116.123 6 2 6 12 449.570 188.081 6 2 6 13 3242.52 454.930 6 2 6 14 1248.49 304.521 6 2 6 15 2682.64 436.334 6 2 6 16 320.265 141.365 6 -2 -7 10-70.3339 111.651 6 -2 -7 9 170.190 93.1367 6 2 7 -8 1310.86 213.797 5 -2 -7 8 841.920 204.127 6 2 7 -7 1827.96 245.177 5 -2 -7 7 1741.58 294.996 6 2 7 -6 1024.69 185.934 5 -2 -7 6 769.599 187.819 6 -2 -7 5 305.430 118.640 6 2 7 -5 297.102 115.304 1 2 7 -5 319.015 113.374 5 2 7 -4 2559.86 279.592 1 -2 -7 4 2552.23 302.200 6 2 7 -4 3395.14 327.918 5 2 7 -3 282.303 81.4042 1 2 7 -3 421.556 127.581 4 2 7 -2 1949.47 163.255 3 2 7 -2 1913.32 259.448 4 2 7 -1 62.2358 71.2351 4 2 7 -1 57.6172 33.6176 3 2 7 0-9.69611 52.6847 4 2 7 0 1.96334 12.6101 3 2 7 1 6632.66 411.691 4 2 7 2 1810.10 216.548 4 -2 -7 -2 1846.86 141.472 1 -2 -7 -3 7042.89 286.305 1 2 7 3 7148.27 423.094 4 -2 -7 -3 7662.81 442.973 4 2 7 4 1031.58 169.546 4 -2 -7 -4 1438.26 196.470 4 -2 -7 -5 2035.01 104.303 3 2 7 5 2345.38 257.358 4 -2 -7 -5 2313.17 258.638 4 -2 -7 -6 2759.19 286.377 4 2 7 6 2531.82 278.348 4 2 7 7 21.5181 47.0622 4 2 7 8 282.045 115.088 6 2 7 8 711.611 169.537 4 2 7 9 1926.34 315.961 6 2 7 10 4445.90 483.440 6 2 7 11 7137.66 624.975 6 2 7 12 249.043 139.432 6 2 7 13 510.896 187.641 6 2 7 14-57.0039 120.154 6 2 7 15 9.56535 84.1643 6 2 7 16 57.7296 92.7501 6 -2 -8 8 101.653 75.0255 6 -2 -8 7 492.219 160.384 6 2 8 -7 568.317 154.603 5 2 8 -6 948.580 190.619 5 2 8 -5 3087.93 335.715 5 2 8 -5 3499.12 419.456 4 2 8 -4 146.001 82.9366 4 2 8 -3-93.0897 82.0959 4 2 8 -2 4130.12 231.413 3 2 8 -2 3996.89 395.273 4 2 8 -1 548.900 151.045 4 2 8 -1 611.932 71.5166 3 2 8 0 1337.02 214.888 4 2 8 1 4358.96 372.071 4 2 8 1 3875.12 150.504 2 2 8 2 7212.33 471.672 4 -2 -8 -3 3875.44 189.131 1 2 8 3 4162.38 357.624 4 2 8 4 3919.64 349.095 4 -2 -8 -4 4504.62 225.270 1 2 8 5 49.6168 45.4182 4 2 8 6 204.200 90.7001 4 -2 -8 -6 222.399 30.0563 3 2 8 7 1313.21 221.429 4 2 8 8 8739.05 587.626 4 2 8 8 8999.05 665.226 6 2 8 9 4190.67 466.222 6 2 8 9 3492.53 390.617 4 2 8 10 416.191 157.011 6 2 8 11 878.931 229.589 6 2 8 12 263.206 140.697 6 2 8 13 32.0475 84.2921 6 2 8 14 286.576 153.872 6 2 8 15-32.7853 82.0436 6 2 9 -7 4123.20 514.262 4 2 9 -6 3546.56 470.547 4 2 9 -6 3008.67 357.618 5 2 9 -5 1061.13 267.812 4 2 9 -5 781.766 186.380 5 2 9 -4 407.701 118.428 4 2 9 -4 819.943 185.065 5 2 9 -3 1040.57 226.399 4 2 9 -2 1576.03 262.316 4 2 9 -1 2555.95 330.430 4 2 9 0 3823.19 390.427 4 2 9 1 1529.51 243.165 4 2 9 2 0.90935 49.1544 4 2 9 3 153.875 93.2204 4 2 9 4 148.423 87.2502 4 -2 -9 -5 1109.84 105.684 1 2 9 5 1323.94 223.276 4 2 9 6-49.0183 94.4765 4 2 9 7 465.863 141.209 4 2 9 8 7878.69 580.488 4 2 9 9 6252.34 596.801 6 2 9 9 6267.28 540.615 4 2 9 10 2183.87 338.959 4 2 9 10 2257.39 382.805 6 2 9 11 1081.08 269.576 6 2 9 12 303.405 139.225 6 2 9 13 1465.01 326.748 6 2 9 14 1217.45 309.708 6 2 10 -5 329.249 139.580 4 2 10 -5 531.842 161.743 5 2 10 -4-189.564 135.476 4 2 10 -4 241.741 139.153 5 2 10 -3 62.9347 68.1194 4 2 10 -2 175.281 57.6368 4 2 10 -1 3980.78 446.697 4 2 10 0 3225.96 391.136 4 2 10 1 3632.99 415.942 4 2 10 2 661.133 175.836 4 2 10 3 47.2135 69.6464 4 2 10 4 138.471 89.6141 4 2 10 5 946.105 198.853 4 2 10 6 455.774 148.355 4 2 10 7 190.453 103.173 4 2 10 8 2993.25 382.723 4 2 10 9 4039.94 454.493 4 2 10 10 102.641 88.4089 4 2 10 10 51.3687 79.7809 6 2 10 11 202.000 93.8918 6 2 10 12 396.440 175.791 6 2 10 13 1061.19 293.318 6 2 11 -4 438.290 153.096 5 2 11 -3 1588.82 316.954 4 2 11 -2 678.530 216.238 4 2 11 -1 525.372 155.942 4 2 11 0 387.813 160.788 4 2 11 1 580.121 177.562 4 2 11 2 121.025 111.397 4 2 11 3-50.1282 82.4371 4 2 11 4 1153.69 242.572 4 2 11 5 1257.17 252.532 4 2 11 6 2791.62 373.238 4 2 11 7 3322.69 413.488 4 2 11 8 42.7507 74.7228 4 2 11 9 1746.14 310.649 4 2 11 10 207.776 159.581 6 2 11 10-8.18672 111.672 4 2 11 11-97.8208 99.0569 6 2 11 11-7.14806 77.2039 4 2 12 1 1072.60 255.406 4 2 12 2 236.274 122.030 4 2 12 3 325.214 134.722 4 2 12 4 1129.82 259.961 4 2 12 5 1286.57 269.757 4 2 12 6 1204.32 273.314 4 2 12 7 380.258 156.730 4 2 12 8-19.9092 56.5799 4 2 12 9 952.179 232.701 4 -3 10 10-6.78677 56.6121 6 -3 10 9 371.970 145.677 6 -3 9 13 712.358 221.689 6 -3 9 12 703.500 236.686 6 -3 9 11 1280.40 302.125 6 -3 9 10 860.561 239.506 6 -3 9 10 1016.60 253.839 4 -3 9 9 652.821 230.173 6 -3 9 9 497.462 171.066 4 -3 9 8 200.921 116.846 4 -3 9 7 115.283 93.1579 4 -3 9 6 48.8242 78.7990 4 -3 9 5 424.168 165.993 4 -3 9 4-3.19219 84.9971 4 -3 9 3 688.384 202.196 4 -3 9 2 769.301 222.499 4 -3 9 1 1417.06 296.559 4 -3 9 0 930.544 234.649 4 -3 9 -1 12.1623 63.1242 4 -3 8 14-240.767 144.814 6 -3 8 13 307.824 131.070 6 -3 8 12 48.8058 72.9762 6 -3 8 11 1254.92 284.299 6 -3 8 11 1481.47 308.771 4 -3 8 10 1972.35 348.765 4 -3 8 10 1926.24 340.489 6 -3 8 9 363.799 145.599 4 -3 8 9 253.590 148.416 6 -3 8 8 86.0082 91.4027 4 -3 8 7 206.477 115.916 4 -3 8 6 983.248 218.842 4 -3 8 5 9973.58 698.595 4 -3 8 4 6000.22 545.052 4 -3 8 3 1912.08 306.038 4 -3 8 2 2134.36 336.266 4 -3 8 1 1088.81 243.099 4 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393.160 6 4 -4 6 3845.92 312.365 2 4 -4 7 3491.54 407.802 6 4 -4 7 4182.24 331.997 2 4 -4 8 4047.17 335.160 2 4 -4 8 3542.77 438.368 6 4 -4 9 671.191 202.381 6 4 -4 9 880.301 162.535 2 4 -4 10 77.4471 84.9596 6 4 -4 10 80.1312 48.3950 2 4 -4 11 102.368 106.311 6 -4 3 16 211.440 136.580 6 -4 3 15-272.357 142.378 6 -4 3 14-78.8381 103.098 6 -4 3 13 1132.11 245.841 6 -4 3 12 193.294 125.408 6 -4 3 11 1444.17 251.768 6 -4 3 10 6004.36 499.805 6 4 -3 -9 2363.31 275.689 3 -4 3 9 2175.65 293.064 6 -4 3 8 3295.79 336.087 6 4 -3 -8 3380.03 313.517 3 -4 3 7 195.249 86.0303 6 -4 3 7 76.5810 64.6715 4 4 -3 -7 24.4038 54.8938 3 4 -3 -7 8.40877 47.2603 1 -4 3 6 923.113 172.403 4 4 -3 -6 1086.88 189.168 1 4 -3 -6 993.643 152.715 3 -4 3 6 972.021 170.737 6 4 -3 -6 1197.68 191.989 4 4 -3 -5 5751.16 329.945 3 -4 3 5 5749.56 402.103 4 4 -3 -5 5574.53 386.597 4 -4 3 5 5394.65 370.662 6 4 -3 -5 4898.71 370.318 1 4 -3 -4 5930.02 379.671 1 4 -3 -4 6492.31 408.199 4 4 -3 -4 6885.68 337.658 3 -4 3 4 6610.14 414.099 4 -4 3 3 1166.60 145.590 6 4 -3 -3 1245.99 139.634 3 -4 3 3 1051.07 168.318 4 4 -3 -3 1255.80 177.665 4 -4 3 3 1647.33 190.945 1 4 -3 -2 2605.30 249.660 4 -4 3 2 2842.60 230.046 1 -4 3 2 2418.74 184.256 3 -4 3 2 2703.43 246.520 2 -4 3 2 2409.22 216.944 6 -4 3 2 2889.90 265.842 4 -4 3 1 3425.91 266.873 6 -4 3 1 3463.06 269.033 2 -4 3 1 3366.11 214.545 3 -4 3 1 3626.37 249.644 1 -4 3 1 3273.28 277.449 4 -4 3 0 445.306 104.832 6 -4 3 0 587.882 128.457 4 -4 3 0 594.060 113.677 2 -4 3 0 500.286 84.8439 3 -4 3 0 537.742 100.423 1 -4 3 -1 3474.83 266.353 2 -4 3 -1 3224.55 220.974 3 -4 3 -1 3131.84 289.870 6 -4 3 -1 3283.17 292.845 4 4 -3 2 492.700 113.313 6 -4 3 -2 267.165 96.2611 6 -4 3 -2 311.780 99.2772 4 4 -3 3 7538.13 462.959 6 -4 3 -3 7874.52 513.529 6 -4 3 -4 7506.96 530.460 6 4 -3 4 7672.74 415.164 2 4 -3 4 7722.13 499.915 6 4 -3 5 1888.56 212.271 2 4 -3 5 1784.28 258.867 6 4 -3 6 800.270 186.394 6 4 -3 6 1033.20 165.711 2 4 -3 7 7447.47 448.522 2 4 -3 7 7522.37 578.310 6 4 -3 8 1108.60 177.993 2 4 -3 8 915.607 226.246 6 4 -3 9 486.506 175.221 6 4 -3 9 682.951 142.090 2 4 -3 10 148.168 118.236 6 4 -3 10-25.8197 40.4559 2 4 -3 11 584.221 145.557 2 4 -3 11 350.166 165.039 6 4 -3 12 4900.82 416.048 2 4 -3 12 4344.41 535.962 6 -4 2 16-79.6987 90.1814 6 -4 2 15 48.0410 75.2952 6 -4 2 14 2234.04 360.950 6 -4 2 13 2301.55 358.408 6 -4 2 12 1692.80 286.266 6 -4 2 11-48.3089 72.0274 6 -4 2 10-6.32071 70.1512 6 -4 2 9 1060.35 188.143 6 -4 2 8 974.953 176.584 6 4 -2 -8 839.700 176.196 4 4 -2 -7 1886.15 237.878 4 4 -2 -7 1663.05 245.404 1 4 -2 -7 1982.13 231.697 3 -4 2 7 1850.11 229.935 6 -4 2 6 10589.6 510.181 6 4 -2 -6 9835.40 478.391 3 -4 2 6 9336.49 519.587 4 4 -2 -6 8781.95 526.793 1 4 -2 -6 9402.83 510.699 4 -4 2 5 10843.9 486.044 6 4 -2 -5 10500.6 548.759 1 4 -2 -5 9718.25 448.623 3 -4 2 5 10170.5 505.039 4 -4 2 4 15678.6 540.574 6 -4 2 4 15864.3 618.922 1 4 -2 -4 15010.3 512.334 3 -4 2 4 14792.8 575.631 4 4 -2 -4 14409.3 614.168 1 -4 2 3 11528.6 495.717 1 4 -2 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294.191 6 4 -2 10 97.7908 78.8240 6 4 -2 11 126.937 81.0267 6 4 -2 12 1576.02 327.030 6 4 -2 13 1293.28 308.936 6 -4 1 16 710.200 221.311 6 -4 1 15 609.057 216.332 6 -4 1 14 401.641 166.988 6 -4 1 13 40.8599 84.0036 6 -4 1 12 1875.62 299.111 6 -4 1 11 92.8204 62.9163 6 4 -1 -10 1710.49 273.671 6 -4 1 10 1863.51 266.834 6 -4 1 9 637.016 154.071 6 4 -1 -9 568.085 148.893 6 4 -1 -8 3188.79 320.691 4 -4 1 8 3422.35 313.993 6 4 -1 -7 1506.13 227.468 1 4 -1 -7 1932.14 236.726 4 -4 1 7 2187.80 233.098 6 4 -1 -6 9488.36 546.093 1 4 -1 -6 10937.4 512.075 3 -4 1 6 10468.7 469.354 6 4 -1 -5 4537.88 362.640 1 4 -1 -5 5222.36 335.306 3 -4 1 5 5020.09 303.190 6 4 -1 -5 3837.13 286.864 4 -4 1 4 27215.1 631.371 6 -4 1 4 27743.4 822.898 1 4 -1 -4 28802.4 730.256 3 4 -1 -4 26722.5 834.273 1 -4 1 4 28017.4 741.814 4 4 -1 -4 25163.2 693.467 4 -4 1 3 1851.77 150.375 6 -4 1 3 1802.37 203.402 1 4 -1 -3 1901.90 174.453 3 -4 1 3 2006.58 189.967 4 4 -1 -3 1549.71 159.364 4 4 -1 -3 2115.03 224.410 1 -4 1 2 1412.68 173.397 1 -4 1 2 1161.63 131.252 3 4 -1 -2 1325.25 144.167 3 -4 1 2 1060.74 129.727 4 -4 1 2 1174.05 96.9258 6 4 -1 -2 1156.58 134.507 4 -4 1 1 14907.8 534.429 1 -4 1 1 14124.3 364.637 6 -4 1 1 14795.8 497.027 2 -4 1 1 15208.8 467.599 4 -4 1 1 15311.2 452.814 3 4 -1 -1 15842.3 468.991 3 -4 1 0 2015.13 183.420 2 -4 1 0 2244.74 170.172 3 -4 1 0 2009.41 191.551 1 -4 1 0 1881.69 167.079 4 -4 1 0 2001.83 157.486 6 -4 1 -1 28549.5 693.682 2 -4 1 -1 27584.7 650.378 6 4 -1 1 28810.9 596.932 6 -4 1 -1 28666.3 630.120 3 -4 1 -1 29731.0 691.268 4 4 -1 2 19323.8 574.762 6 -4 1 -2 17528.6 578.012 6 -4 1 -3 1187.70 172.456 6 4 -1 3 1311.77 181.188 6 4 -1 4 8253.38 458.992 6 -4 1 -4 8280.75 476.481 6 4 -1 5 10708.2 479.008 2 -4 1 -5 11242.4 605.142 6 4 -1 5 10722.6 564.280 6 -4 1 -6 4807.06 424.056 6 4 -1 6 4196.18 383.710 6 4 -1 7 1332.40 231.069 6 4 -1 8 101.795 82.6576 6 4 -1 9 2984.69 384.156 6 -4 1 -10 2415.14 122.938 5 4 -1 10 4305.43 471.201 6 4 -1 11 1468.50 292.626 6 4 -1 12 394.357 172.818 6 4 -1 13-23.6456 88.2925 6 4 -1 14 136.543 89.7203 6 -4 0 15 1621.07 307.040 6 -4 0 14 1915.72 331.364 6 -4 0 13 1883.66 324.203 6 -4 0 12 412.002 161.469 6 -4 0 11 786.651 186.576 6 -4 0 11 597.518 128.620 5 4 0 -10 2109.51 311.895 6 -4 0 10 2192.58 289.279 6 -4 0 9-63.0410 74.9634 6 4 0 -9 101.458 76.4295 6 -4 0 8 2668.10 281.128 6 4 0 -8 2847.22 302.002 4 4 0 -7 301.917 91.3038 4 -4 0 7 308.691 93.2575 6 4 0 -7 224.638 86.0059 6 -4 0 6 230.443 66.7848 6 4 0 -6 252.516 86.1463 6 4 0 -6 267.389 102.416 1 4 0 -5 1085.37 142.141 6 4 0 -5 1265.90 175.688 3 4 0 -5 1170.94 187.852 1 4 0 -5 1291.50 163.721 4 -4 0 5 1252.26 142.897 6 4 0 -4 4601.72 348.686 1 -4 0 4 4747.22 354.023 1 4 0 -4 4264.61 265.457 4 -4 0 4 4653.58 233.860 6 -4 0 3 332.161 75.7230 4 4 0 -3 304.367 72.4836 4 -4 0 3 301.138 51.4358 6 -4 0 3 290.584 100.556 1 4 0 -3 260.013 88.2064 1 -4 0 2 1344.56 170.231 1 4 0 -2 1400.41 174.759 1 -4 0 2 1099.88 70.7539 6 -4 0 2 1362.84 142.392 3 -4 0 2 1442.50 133.345 4 4 0 -2 1144.38 112.910 4 -4 0 1 341.362 94.1636 1 -4 0 1 225.495 55.1235 4 4 0 -1 192.307 49.5216 4 -4 0 1 204.861 58.7007 2 -4 0 1 222.312 59.3448 3 -4 0 0 103.460 36.8577 3 -4 0 0 49.5941 25.2535 6 -4 0 0 77.8042 33.3228 4 -4 0 0 112.512 69.0519 1 -4 0 0 75.2280 38.0147 2 -4 0 -1 14371.3 406.141 4 -4 0 -1 13733.8 426.828 3 4 0 1 14237.4 360.528 6 -4 0 -1 13871.0 379.318 6 4 0 2 206.555 70.6338 6 -4 0 -2 216.152 57.9423 6 -4 0 -3 1147.72 147.580 6 4 0 3 1229.52 154.545 6 4 0 4 4985.46 332.345 6 -4 0 -4 4884.64 335.373 6 4 0 5 17092.6 662.996 6 -4 0 -5 16396.9 677.087 6 4 0 6 3308.70 321.323 6 -4 0 -6 3516.52 338.937 6 4 0 7 827.132 175.639 6 -4 0 -7 1021.54 200.169 6 -4 0 -8 2335.69 178.583 5 4 0 8 2274.64 302.027 6 4 0 9 9818.59 656.735 6 -4 0 -9 8661.72 297.428 5 4 0 10 11931.6 757.122 6 4 0 11 3604.84 445.203 6 4 0 12 130.340 132.625 6 4 0 13 365.326 177.106 6 4 0 14 1752.55 346.613 6 -4 -1 15 170.474 114.813 6 -4 -1 14 13.6791 63.7213 6 -4 -1 13 18.5877 80.3412 6 -4 -1 12 396.008 154.766 6 -4 -1 11 4869.20 467.854 6 -4 -1 10 2605.58 256.872 5 -4 -1 10 2823.67 334.113 6 4 1 -9 4852.27 449.088 6 -4 -1 9 5019.90 416.792 6 -4 -1 9 3932.05 318.338 5 4 1 -8 7944.32 529.369 6 -4 -1 8 7176.47 426.079 5 4 1 -8 7006.92 479.177 4 -4 -1 8 8203.39 495.689 6 -4 -1 7 9165.86 485.106 6 4 1 -6 3008.67 272.788 6 -4 -1 6 3236.92 263.770 6 4 1 -6 2717.60 299.703 1 4 1 -6 2837.20 261.835 4 4 1 -5 72.7504 40.4006 4 -4 -1 5 28.2309 34.4127 6 4 1 -5 199.163 74.5182 6 4 1 -5 50.0898 54.8312 1 4 1 -4 2834.57 280.065 1 -4 -1 4 3091.70 196.959 6 4 1 -4 2976.69 214.206 4 4 1 -4 2948.07 205.038 6 -4 -1 3 2234.24 134.720 6 4 1 -3 2297.82 162.683 4 4 1 -3 2212.51 141.726 6 4 1 -3 2396.00 245.503 1 -4 -1 2 2782.18 195.790 2 4 1 -2 3066.00 265.419 1 4 1 -2 2498.13 144.196 4 4 1 -1 8720.39 225.573 4 -4 -1 1 10306.1 364.591 2 -4 -1 1 10043.5 362.631 3 -4 -1 1 10862.5 272.544 4 -4 -1 0 74.9215 25.8353 4 -4 -1 0 86.7112 45.2712 2 -4 -1 0 11.3835 22.5131 3 -4 -1 -1 8118.42 239.423 6 4 1 1 8461.85 235.406 6 -4 -1 -1 8432.32 239.538 4 -4 -1 -1 8244.44 319.837 3 -4 -1 -2 6920.16 280.591 6 -4 -1 -2 6833.40 303.290 3 4 1 2 7011.94 278.882 6 4 1 3 8313.17 358.526 6 -4 -1 -3 8192.10 358.504 6 -4 -1 -4 163.614 62.2625 6 4 1 4 136.191 66.0260 6 4 1 5 2873.47 264.028 6 -4 -1 -5 2466.74 250.198 6 -4 -1 -6 1663.48 167.145 5 -4 -1 -6 1453.06 206.052 6 4 1 6 1571.11 221.762 6 -4 -1 -7 3656.98 355.408 6 4 1 7 3996.84 368.144 6 -4 -1 -7 4020.96 244.494 5 -4 -1 -8 10917.1 367.699 5 4 1 8 10698.4 631.705 6 -4 -1 -8 10757.0 652.820 6 4 1 9 177.163 110.743 6 4 1 10 3787.06 428.600 6 4 1 11-11.7286 88.5630 6 4 1 12 345.996 164.377 6 4 1 13-25.2088 105.619 6 4 1 14 80.2597 102.899 6 4 1 15 1445.01 345.259 6 -4 -2 15 106.557 96.5936 6 -4 -2 14-138.319 107.679 6 -4 -2 13-11.7016 84.5162 6 -4 -2 12 519.943 171.549 6 -4 -2 11 1780.78 299.679 6 -4 -2 10 4865.26 462.334 6 -4 -2 10 3905.25 295.549 5 -4 -2 9 1355.23 233.865 6 4 2 -9 1216.87 237.944 6 -4 -2 9 1236.73 172.976 5 4 2 -8 732.817 180.866 6 -4 -2 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485.150 5 -4 -6 -8 9651.47 538.998 4 4 6 8 8563.36 591.581 6 4 6 9 16566.5 850.339 6 4 6 9 18863.6 695.337 5 -4 -6 -9 17737.9 778.526 4 4 6 10 6806.75 573.492 6 4 6 10 7336.15 441.871 5 4 6 11 7360.03 438.617 5 4 6 11 5900.25 552.953 6 4 6 12 99.5635 121.212 6 4 6 12 50.9085 48.9509 5 4 6 13 225.691 128.801 6 4 6 13 172.816 63.1202 5 4 6 14 1151.25 288.683 6 4 6 15 547.664 199.820 6 4 6 16-30.1310 76.2262 6 -4 -7 10 613.016 198.002 6 -4 -7 9 1290.84 255.699 6 -4 -7 8 1982.39 306.094 6 -4 -7 7 2781.42 353.506 6 4 7 -6 571.042 136.993 3 4 7 -6 387.337 134.902 5 -4 -7 6 268.438 119.409 6 4 7 -5 211.946 101.811 5 4 7 -5 202.738 72.3841 3 4 7 -4 707.221 161.865 5 4 7 -4 705.341 130.626 3 4 7 -3 1053.69 179.712 4 4 7 -3 1106.56 154.627 3 4 7 -3 907.023 179.333 5 4 7 -3 859.351 171.928 1 4 7 -2 5494.94 435.961 5 4 7 -2 5677.12 378.759 4 4 7 -1 13163.6 658.976 5 4 7 -1 13084.9 551.375 4 4 7 0 5712.82 433.987 5 4 7 0 5557.82 279.767 3 4 7 0 4593.82 387.499 6 4 7 0 4508.29 306.567 4 4 7 1 1655.69 105.285 2 4 7 1 1753.34 226.962 6 4 7 1 1881.90 248.556 5 4 7 1 1598.16 182.083 4 4 7 2 7026.63 443.588 6 4 7 2 6569.29 359.088 4 4 7 2 6464.70 441.611 5 4 7 3 1022.09 144.283 4 -4 -7 -3 1130.97 116.065 3 4 7 4 9.96749 35.7607 4 -4 -7 -4 13.6919 39.2256 4 -4 -7 -4 11.3187 19.9231 3 -4 -7 -5 69.4570 37.1509 3 -4 -7 -5 31.6045 64.5469 4 4 7 5 29.8503 49.6806 4 4 7 6 302.883 93.8908 4 -4 -7 -6 393.932 79.9854 3 -4 -7 -6 333.374 98.4624 4 4 7 7 3635.62 388.502 6 -4 -7 -7 4219.56 353.556 4 4 7 8 4925.30 473.299 6 -4 -7 -8 5320.50 415.142 4 4 7 9 3066.85 382.040 6 4 7 10-177.312 91.3792 6 4 7 10 502.112 149.131 5 4 7 11-97.3372 121.571 6 4 7 11 402.412 137.192 5 4 7 12-90.7246 154.708 6 4 7 12 11.8376 42.5499 5 4 7 13 906.569 239.233 6 4 7 13 1477.71 216.868 5 4 7 14 335.923 175.146 6 4 7 14 62.0112 48.5201 5 4 7 15 2935.86 460.457 6 4 7 16 1875.28 384.665 6 4 8 -9 953.951 204.265 3 -4 -8 9 567.869 187.848 6 -4 -8 8-24.7682 67.6432 6 4 8 -8-63.8433 53.9895 3 4 8 -7 691.831 163.208 3 4 8 -6 264.292 110.922 5 4 8 -6 231.587 82.5562 3 4 8 -5-25.7001 61.3234 4 4 8 -5-28.3609 79.7571 5 4 8 -5-13.9835 41.5083 3 4 8 -4 975.115 201.935 4 4 8 -4 850.955 185.449 5 4 8 -4 979.454 158.307 3 4 8 -3 2089.85 215.669 3 4 8 -3 1632.65 256.799 5 4 8 -3 2047.21 275.196 4 4 8 -2 13330.4 650.718 4 4 8 -2 12247.1 685.588 5 4 8 -1 10549.3 554.039 4 4 8 -1 10788.1 640.395 5 4 8 0 2696.63 318.925 5 4 8 0 2963.78 204.554 3 4 8 0 2865.20 273.807 4 4 8 1 2656.77 318.993 5 4 8 1 2447.15 254.141 4 4 8 2 1333.76 180.236 4 4 8 3 593.676 125.170 4 -4 -8 -4 3253.10 291.000 4 4 8 4 3518.91 301.842 4 4 8 5-61.2238 57.2007 4 -4 -8 -5 47.7446 36.4969 4 -4 -8 -5 11.7271 19.5582 3 -4 -8 -6 17233.2 476.676 3 4 8 6 16260.8 707.868 4 -4 -8 -6 16926.1 708.736 4 4 8 7 11415.7 626.297 4 -4 -8 -7 12540.9 449.433 3 -4 -8 -7 11991.4 617.074 4 4 8 8 4586.66 473.747 6 4 8 9 73.4876 92.7953 6 4 8 10 273.969 130.125 6 4 8 11-2.84705 98.7013 6 4 8 12 103.839 96.0273 6 4 8 13-1.61591 147.218 6 4 8 13 131.427 89.9079 5 4 8 14 94.5725 122.879 6 4 8 14 115.340 73.5290 5 4 8 15 497.644 206.708 6 4 9 -8 105.452 86.0096 4 4 9 -7 353.166 129.292 4 4 9 -6-52.6332 108.192 4 4 9 -6 111.591 63.4656 5 4 9 -5 256.827 116.430 4 4 9 -5 222.052 95.5960 5 4 9 -4 103.641 93.2035 4 4 9 -4 87.0953 76.9364 5 4 9 -4 156.998 71.7266 3 4 9 -3 1971.66 289.068 4 4 9 -3 1850.57 289.058 5 4 9 -3 2305.43 221.727 3 4 9 -2 987.832 199.084 4 4 9 -2 1339.37 242.772 5 4 9 -1 2182.37 313.522 5 4 9 -1 2293.34 286.136 4 4 9 0 488.540 126.020 4 4 9 0 673.230 186.095 5 4 9 1 408.174 115.883 4 4 9 1 899.582 214.540 5 4 9 2-0.96755 54.9368 4 4 9 3 616.277 131.881 4 -4 -9 -3 695.787 125.581 1 4 9 4 3789.77 338.387 4 4 9 5 1895.77 247.451 4 -4 -9 -6 2617.59 162.023 3 4 9 6 2286.60 276.273 4 4 9 7 42.1918 71.8833 4 -4 -9 -7 229.262 51.5953 3 4 9 8 79.3531 97.4704 6 4 9 8-49.3673 69.8760 4 4 9 9 842.117 236.795 6 4 9 10 884.709 236.789 6 4 9 11 387.432 169.229 6 4 9 12 1193.69 290.674 6 4 9 13 4500.16 551.710 6 4 9 14 943.807 280.195 6 4 9 14 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11 0 256.738 133.736 5 4 11 1 730.764 184.045 4 4 11 1 1113.33 251.568 5 4 11 2 267.730 122.311 4 4 11 3 1462.04 245.564 4 4 11 4 1726.37 271.532 4 4 11 5 584.745 164.918 4 4 11 6 96.1363 80.5619 4 4 11 7 504.781 152.719 4 4 11 8 163.576 99.4998 4 4 11 9-5.93722 69.2731 4 4 11 9 127.183 124.464 6 4 11 10 2771.42 451.016 6 4 11 11 1956.91 391.435 6 4 11 12 150.525 123.039 6 4 12 -1 92.7611 83.5266 4 4 12 0 316.501 138.159 4 4 12 1 333.896 140.028 4 4 12 2 687.313 185.374 4 4 12 3 5.19844 54.9953 4 4 12 4 72.4656 70.5095 4 4 12 5 239.001 99.8656 4 4 12 6 113.925 64.3886 4 4 12 7-15.8861 51.6791 4 4 12 8 194.343 91.3680 4 4 12 9 746.264 205.418 4 4 12 9 827.557 258.353 6 4 13 3-58.0202 66.2884 4 4 13 4 83.1392 73.2873 4 4 13 5 215.437 116.411 4 4 13 6 26.3836 91.3332 4 4 13 7 158.895 99.9786 4 4 13 8 727.933 213.340 4 4 13 9 1778.70 327.339 4 -5 9 9 70.0605 81.5573 6 -5 9 8-97.3563 102.388 6 -5 8 10 483.774 169.862 6 -5 8 9 242.502 129.364 6 -5 8 8 792.657 226.194 4 -5 8 8 862.771 230.892 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661.399 6 5 7 7 11275.9 603.518 5 -5 -7 -7 11543.2 562.898 4 5 7 8 3248.57 388.846 6 5 7 8 4175.94 371.402 5 -5 -7 -8 3780.35 339.552 4 5 7 9 421.870 153.454 6 5 7 9 531.808 141.365 5 5 7 10 786.498 213.735 6 5 7 10 635.991 143.069 5 5 7 11-10.2601 78.0313 6 5 7 11-99.0833 84.9480 5 5 7 12 2236.48 368.124 6 5 7 12 2486.95 289.248 5 5 7 13 598.454 200.120 6 5 7 13 1113.10 193.916 5 5 7 14 2197.90 399.509 6 5 7 15 1539.89 338.531 6 5 8 -9 133.260 64.9978 3 5 8 -8 393.265 138.480 3 5 8 -7 99.6068 62.4185 3 5 8 -6 706.486 153.728 3 5 8 -5 3673.79 413.015 5 5 8 -5 4862.12 395.980 3 5 8 -5 5087.29 459.842 4 5 8 -4 2634.06 344.566 5 5 8 -4 3433.06 316.847 3 5 8 -4 3143.25 340.702 4 5 8 -3 1923.88 289.065 5 5 8 -3 2200.23 232.589 3 5 8 -3 2403.77 273.433 4 5 8 -2 6890.21 531.842 5 5 8 -2 7307.59 396.153 3 5 8 -2 7184.54 445.315 4 -5 -8 1 1637.28 242.814 1 5 8 -1 1595.08 264.927 5 5 8 -1 1923.98 192.072 3 5 8 -1 1743.79 204.364 4 -5 -8 0 2096.05 262.571 1 5 8 0 2330.32 307.496 5 5 8 0 2267.93 232.648 4 -5 -8 -1 2031.50 247.492 1 5 8 1 2076.88 292.695 5 5 8 1 2107.95 214.788 4 5 8 2 5.39872 44.9567 4 5 8 2 43.5976 33.8015 2 -5 -8 -2-16.9482 71.5157 1 5 8 2 115.526 104.431 5 5 8 3 6818.22 509.791 5 5 8 3 6700.30 389.177 4 -5 -8 -3 6343.82 442.692 1 -5 -8 -4 7151.60 330.788 3 5 8 4 7949.46 543.870 5 5 8 4 6961.41 410.278 4 -5 -8 -4 6969.60 466.334 1 5 8 5 890.652 161.072 4 -5 -8 -5 880.474 145.331 4 -5 -8 -5 968.881 125.589 3 5 8 5 1195.61 227.581 5 5 8 6 4765.23 417.902 5 -5 -8 -6 4360.19 271.679 3 -5 -8 -6 4018.24 329.889 4 -5 -8 -7 246.474 70.7931 3 -5 -8 -7 293.712 106.397 4 5 8 7 267.306 134.905 6 5 8 7 207.207 97.0880 5 5 8 8 683.693 178.869 6 5 8 8 879.225 184.868 5 5 8 9 2671.30 375.411 6 5 8 9 2879.35 332.696 5 5 8 10 1525.31 299.892 6 5 8 10 2285.62 291.928 5 5 8 11 107.033 110.148 6 5 8 11-67.9030 93.7712 5 5 8 12 432.390 164.989 6 5 8 12 583.321 155.375 5 5 8 13 503.109 186.023 6 5 8 13 760.350 171.683 5 5 8 14 820.302 227.574 6 5 8 14 1548.30 242.005 5 5 8 15 1249.88 319.565 6 5 9 -6 113.671 70.1536 4 5 9 -5 1305.85 208.857 3 5 9 -5 1209.49 243.996 4 5 9 -5 843.590 209.901 5 5 9 -4 4816.00 452.539 4 5 9 -4 4236.51 456.130 5 5 9 -4 5222.63 386.903 3 5 9 -3 199.415 82.1747 4 5 9 -3 452.526 148.464 5 5 9 -3 431.611 111.094 3 5 9 -2 316.452 86.7980 3 5 9 -2 307.130 99.1373 4 5 9 -2 287.420 107.502 5 5 9 -1 34.2066 41.2415 3 5 9 -1 26.8269 44.6079 4 5 9 -1 7.43799 104.851 5 5 9 0 437.223 117.216 4 5 9 0 650.656 177.381 5 5 9 1 261.259 88.1711 4 5 9 1 406.534 142.914 5 -5 -9 -1 280.810 106.542 1 5 9 2 961.129 162.418 4 5 9 2 772.169 80.1668 2 5 9 2 1093.56 227.752 5 -5 -9 -2 705.126 151.266 1 5 9 3 717.362 141.026 4 -5 -9 -3 504.356 115.408 1 5 9 3 845.817 202.723 5 5 9 4 912.759 166.511 4 -5 -9 -4 877.808 154.279 1 -5 -9 -5 8585.89 490.358 4 -5 -9 -5 8869.46 356.374 3 5 9 5 10094.4 644.538 5 5 9 5 7617.64 482.994 4 -5 -9 -5 8905.37 538.573 1 -5 -9 -6 3438.58 231.258 3 5 9 6 3585.75 382.598 5 5 9 6 2584.47 292.766 4 -5 -9 -6 3044.44 304.079 4 5 9 7 2352.56 321.859 5 -5 -9 -7 2342.73 198.086 3 -5 -9 -8 23.1306 29.4499 3 5 9 8 243.635 105.005 6 5 9 9 816.305 238.576 6 5 9 9 1331.27 243.186 5 5 9 10 1487.91 303.175 6 5 9 10 1404.52 247.243 5 5 9 11 1473.95 307.777 6 5 9 11 1842.13 279.510 5 5 9 12 2349.99 394.648 6 5 9 12 2698.50 339.426 5 5 9 13 658.088 216.084 6 5 9 13 1184.64 227.319 5 5 9 14 585.212 173.143 6 5 9 14 942.738 204.011 5 5 10 -6-91.6410 87.6738 5 5 10 -5 135.592 90.6920 5 5 10 -4 880.671 214.765 4 5 10 -4 410.905 150.957 5 5 10 -3 261.073 116.372 4 5 10 -3 626.158 191.065 5 5 10 -2 897.219 185.677 4 5 10 -2 497.629 167.198 5 5 10 -1 91.9400 80.9896 4 5 10 -1 74.3696 73.0419 5 5 10 0 570.138 147.529 4 5 10 0 539.154 168.505 5 5 10 1 5173.02 506.106 5 5 10 1 4581.07 389.081 4 5 10 2 1947.23 311.801 5 5 10 2 1763.17 238.671 4 -5 -10 -2 1543.16 210.982 1 -5 -10 -3 5296.35 385.739 1 5 10 3 6150.76 539.888 5 5 10 3 5543.20 418.875 4 -5 -10 -4 4843.06 374.335 1 5 10 4 6050.15 527.109 5 5 10 4 4915.91 404.560 4 5 10 5 3092.53 379.552 5 5 10 5 2466.02 295.126 4 -5 -10 -5 2583.12 284.794 1 5 10 6 83.6101 76.9564 4 -5 -10 -6 26.5774 69.6605 1 5 10 7 3654.97 404.117 5 5 10 7 2714.84 333.297 4 5 10 8 8.37742 97.6911 6 5 10 8 302.740 151.151 5 5 10 9 1911.09 352.857 6 5 10 9 2158.27 321.004 5 5 10 10 3126.33 460.531 6 5 10 10 4188.18 436.803 5 5 10 11 332.313 171.300 6 5 10 11 788.464 198.226 5 5 10 12 609.341 224.972 6 5 10 12 1151.88 230.536 5 5 10 13 352.103 174.228 6 5 10 13 526.558 174.151 5 5 10 14 332.837 145.195 5 5 11 -4 391.213 156.255 5 5 11 -3-91.0143 91.3120 5 5 11 -2 154.934 142.474 5 5 11 -1-1.82406 33.9354 4 5 11 -1 63.3726 98.8646 5 5 11 0 990.471 211.070 4 5 11 0 656.572 194.077 5 5 11 1 1278.36 220.974 4 5 11 1 1301.14 274.155 5 5 11 2 93.5326 71.1645 4 5 11 2 277.377 135.964 5 5 11 3-49.3974 54.7715 4 5 11 3 216.439 137.113 5 5 11 4 596.509 161.465 4 5 11 4 664.401 190.839 5 5 11 5 228.297 89.7561 4 5 11 5 750.478 210.259 5 5 11 6 38.2800 50.5159 4 5 11 6 477.836 192.667 5 5 11 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397.834 6 8 3 5 364.225 88.1096 6 8 3 5 517.355 130.100 2 8 3 6-45.3378 75.2217 6 -8 -3 -6 143.569 75.6883 6 8 3 6 60.2787 49.2052 2 -8 -3 -7 4578.68 417.469 6 8 3 7 5148.39 413.392 2 8 3 7 4489.17 393.886 6 8 3 8 2100.43 288.254 6 8 3 9 42.4846 79.0799 6 8 3 10 223.388 88.5388 6 8 3 11-55.2007 129.892 6 8 3 12 287.138 155.939 6 8 3 13 318.564 172.876 6 8 3 14 2124.48 389.285 6 8 4 -9 212.832 108.305 3 8 4 -8 97.8170 93.0703 3 8 4 -7 42.4281 42.4595 3 8 4 -6-27.2088 64.6742 3 -8 -4 5 3447.31 439.375 1 8 4 -5 4016.14 376.992 3 -8 -4 4 4314.00 470.378 1 8 4 -4 4345.24 382.370 3 -8 -4 3 6373.08 562.605 1 8 4 -3 7387.72 491.134 3 -8 -4 2 4524.50 457.787 1 8 4 -2 5355.05 411.806 3 8 4 -1 38.8402 67.7896 3 -8 -4 1 95.5325 81.2065 1 -8 -4 0 1488.00 263.319 1 -8 -4 -1 1810.52 295.273 1 8 4 2 518.934 69.6678 6 -8 -4 -2 671.991 164.003 1 8 4 2 654.415 136.092 2 8 4 2 419.489 53.4220 6 8 4 3 837.220 113.470 6 8 4 3 859.442 152.965 2 8 4 4 2880.22 294.051 2 -8 -4 -4 2543.95 155.336 4 8 4 4 2659.90 231.116 6 8 4 5 17707.4 715.727 2 8 4 5 16634.9 654.992 6 8 4 6 10610.2 569.948 2 8 4 6 11508.8 591.925 6 8 4 7 4838.45 411.475 6 8 4 8 47.1126 65.5162 6 8 4 9 11.0199 63.2664 6 8 4 10 304.320 119.380 6 8 4 11 3497.40 438.758 6 8 4 12 2021.98 351.141 6 8 4 13 793.491 239.310 6 8 4 14 823.207 257.582 6 8 5 -8-14.6595 56.6828 3 8 5 -7 328.991 124.852 3 8 5 -6 223.042 93.1002 3 8 5 -5 2413.93 293.616 3 -8 -5 4 5726.62 547.544 1 8 5 -4 6082.13 452.591 3 -8 -5 3 3934.10 444.871 1 8 5 -3 4225.44 369.786 3 -8 -5 2 1556.94 279.178 1 8 5 -2 1599.61 228.924 3 8 5 -2 1371.99 136.678 6 8 5 -1 455.750 122.753 3 8 5 -1 359.335 66.4752 6 8 5 -1 283.601 59.2502 6 -8 -5 1 435.445 159.267 1 8 5 0 79.0496 29.8955 6 8 5 0 23.2226 22.2525 6 8 5 1 131.400 44.2670 6 8 5 1 157.255 49.8617 6 -8 -5 -1 84.0123 104.109 1 8 5 2 5549.68 375.155 2 8 5 2 4860.09 230.955 6 -8 -5 -2 5505.15 496.105 1 8 5 2 6192.03 322.845 6 8 5 3 7778.99 453.018 2 -8 -5 -3 7947.77 594.344 1 8 5 3 8609.43 416.861 6 8 5 4-19.0518 46.5095 6 8 5 4 99.1339 59.8655 2 8 5 5 10385.8 540.208 2 -8 -5 -5 10011.5 324.761 4 8 5 5 11310.6 562.042 6 -8 -5 -6-62.5555 39.5427 4 8 5 6-26.4382 82.7235 6 -8 -5 -7 529.004 113.963 4 8 5 7 464.052 144.332 6 8 5 8 588.489 163.630 6 -8 -5 -8 615.244 130.527 4 8 5 9 55.8017 92.5444 6 8 5 10 2954.61 382.922 6 8 5 11 1842.35 319.818 6 8 5 12 2584.06 402.901 6 8 5 13 731.209 217.277 6 8 5 14 23.4427 103.499 6 8 5 15 183.081 145.026 6 8 6 -8 271.839 114.469 3 8 6 -7 4889.90 450.977 3 8 6 -6 1831.24 263.725 3 8 6 -5 3305.35 346.848 3 -8 -6 4 2599.34 386.829 1 8 6 -4 3132.52 326.712 3 -8 -6 3 3016.27 404.348 1 8 6 -3 2648.68 296.698 3 8 6 -2-31.3230 79.0234 3 -8 -6 2 51.3847 84.9007 1 8 6 -1 104.544 55.8187 3 8 6 -1 207.657 67.9133 6 -8 -6 1 36.7705 84.6115 1 8 6 0 210.705 65.0598 6 -8 -6 0 59.6880 70.2296 1 -8 -6 -1-59.9734 98.0049 1 8 6 1 41.4814 33.3659 6 8 6 1 46.3105 44.4474 6 8 6 2 1616.02 203.622 6 8 6 2 1490.11 188.672 2 8 6 2 1259.63 142.731 6 -8 -6 -2 1516.59 262.500 1 8 6 3 4573.06 353.447 6 8 6 3 4061.84 313.960 2 -8 -6 -3 4138.75 445.415 1 8 6 4 3154.45 304.469 6 8 6 4 2949.90 281.254 2 -8 -6 -5 267.637 42.5603 4 8 6 5 355.120 115.348 6 8 6 5 416.967 106.331 2 8 6 6 995.816 188.952 6 -8 -6 -6 1034.19 119.502 4 8 6 7 1524.93 246.049 6 -8 -6 -7 1257.96 158.148 4 -8 -6 -8 1062.08 163.881 4 8 6 8 1118.20 225.559 6 -8 -6 -9-59.2387 68.3192 4 8 6 9 99.7778 89.1918 6 8 6 10 939.484 236.594 6 8 6 11 1450.18 284.531 6 8 6 12 1370.84 290.113 6 8 6 13 237.456 116.678 6 8 6 14-127.851 128.739 6 8 6 15-202.703 165.960 6 8 7 -7 39.1501 67.4000 3 8 7 -6 876.426 189.392 3 8 7 -5-41.2986 60.4515 3 8 7 -4 176.436 87.1768 3 8 7 -3 29.4577 75.8725 3 -8 -7 3-203.393 155.799 1 8 7 -2 1001.17 184.123 3 -8 -7 2 1194.81 251.298 1 8 7 -1 83.7814 75.2442 3 -8 -7 1 48.3032 87.5148 1 -8 -7 0 3330.74 403.754 1 -8 -7 -1 330.254 141.832 1 8 7 2 1070.31 156.552 2 8 7 2 958.227 190.632 6 -8 -7 -2 1066.23 225.561 1 8 7 3 7093.92 491.832 6 8 7 3 6958.74 403.628 2 8 7 3 5571.01 350.837 6 -8 -7 -3 7130.81 582.273 1 8 7 4 2448.61 289.891 6 8 7 4 1972.46 222.279 2 -8 -7 -4 1664.18 295.231 1 8 7 5 193.775 73.2916 2 8 7 5 205.711 59.9894 6 -8 -7 -6 151.725 46.2107 4 8 7 6 379.977 132.409 6 8 7 7 3428.93 381.349 6 8 7 8 2316.21 323.401 6 8 7 9 900.477 206.842 6 8 7 10 268.348 117.300 6 8 7 11 270.332 159.656 6 8 7 12 337.850 158.965 6 8 7 13 517.633 189.771 6 8 7 14 129.740 134.677 6 8 8 -7 148.030 96.4206 3 8 8 -6 187.636 94.4738 3 8 8 -5 322.937 124.714 3 8 8 -4 253.449 102.124 3 8 8 -3 80.2977 54.6894 3 8 8 -2 1379.61 222.171 3 -8 -8 2 1052.68 241.269 1 8 8 -1 585.669 138.921 3 -8 -8 1 796.649 206.630 1 -8 -8 0 381.501 142.092 1 -8 -8 -1 440.852 168.956 1 -8 -8 -2 333.502 122.843 1 8 8 3 128.281 52.3040 6 8 8 3 218.713 76.8344 2 -8 -8 -3 31.6136 78.8787 1 8 8 4 1939.33 285.484 6 8 8 4 1917.54 212.688 2 -8 -8 -4 1684.75 289.204 1 8 8 5 2957.79 364.382 6 8 8 5 3001.76 273.960 2 -8 -8 -5 3365.51 413.352 1 8 8 6 2520.65 345.632 6 8 8 7 5659.56 521.124 6 8 8 8 3962.88 453.565 6 8 8 9 465.322 168.219 6 8 8 10-95.3104 129.044 6 8 8 11 51.2325 84.1021 6 8 8 12-93.4803 101.738 6 8 8 13 245.711 150.773 6 8 8 14 357.335 170.317 6 8 9 -6-201.752 101.722 3 8 9 -5 298.393 121.854 3 8 9 -4 874.590 187.662 3 8 9 -3 1407.11 230.962 3 -8 -9 2 5236.41 546.932 1 8 9 -2 7224.49 512.845 3 -8 -9 1 2747.80 386.622 1 -8 -9 0 270.234 126.815 1 -8 -9 -1-70.0521 89.5024 1 -8 -9 -2 585.752 181.116 1 8 9 2 596.294 172.094 5 -8 -9 -3 244.354 126.101 1 8 9 3 278.618 90.2699 5 8 9 3 266.799 76.3892 2 8 9 4 190.246 69.8243 2 8 9 4 212.438 116.524 5 -8 -9 -4 41.6964 85.7999 1 8 9 5 725.351 132.203 2 8 9 5 838.774 210.226 6 8 9 5 673.758 180.324 5 -8 -9 -5 746.879 207.004 1 8 9 6 425.747 159.475 6 8 9 6 644.962 185.520 5 -8 -9 -6 516.045 176.838 1 8 9 7 389.020 154.275 6 8 9 7 381.553 158.018 5 8 9 8 907.735 239.655 6 8 9 8 845.941 233.404 5 8 9 9 349.483 146.387 6 8 9 9 155.794 110.032 5 8 9 10 1007.08 240.749 6 8 9 10 915.952 220.026 5 8 9 11 4.88725 89.7249 6 8 9 12 104.065 128.979 6 8 9 13 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94.6603 4 -9 4 2 344.493 125.069 4 -9 4 1 467.963 154.706 4 -9 4 0 875.650 215.830 4 -9 4 -1-4.27710 67.6411 4 -9 4 -2 47.3057 67.6886 4 -9 4 -3 120.803 54.7475 4 -9 4 -4 188.312 79.3451 4 -9 4 -5 131.133 84.6220 4 9 -3 -8 108.582 98.7706 3 9 -3 -7 1405.85 264.518 3 -9 3 6 1854.15 296.304 4 -9 3 5 607.040 167.662 4 -9 3 4 744.660 178.638 4 -9 3 4 1051.79 234.752 1 -9 3 3 1084.34 215.933 4 -9 3 3 1175.45 238.899 1 -9 3 2 203.037 113.125 4 -9 3 2 191.575 102.083 1 -9 3 1 11.8242 56.6685 4 -9 3 1 73.5112 87.8707 1 -9 3 0 52.0187 52.8861 4 -9 3 0 70.5048 69.9817 1 -9 3 -1 120.287 56.7027 1 -9 3 -1 207.544 87.3698 4 -9 3 -2 806.375 203.970 4 -9 3 -2 754.941 198.272 1 -9 3 -3 1124.73 235.256 4 -9 3 -3 875.023 220.225 1 -9 3 -4 249.220 120.289 4 -9 3 -4 440.309 152.294 1 -9 3 -5 1117.16 240.947 4 -9 3 -5 681.595 173.773 1 -9 3 -6 677.785 193.303 4 -9 3 -7 934.784 237.889 4 9 -2 -9-16.6100 56.2729 3 9 -2 -8 6.68177 47.9435 3 9 -2 -7 1373.41 256.148 3 9 -2 -6 3488.19 399.646 3 -9 2 5 379.126 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6 5 638.432 142.407 6 9 6 5 578.965 137.005 2 9 6 6 174.445 96.6624 6 9 6 6 324.156 102.047 2 9 6 7 967.538 180.198 2 9 6 7 825.736 177.525 6 9 6 8 1674.97 270.405 6 9 6 9 566.505 174.865 6 9 6 10 131.778 75.4591 6 9 6 11 29.6911 113.000 6 9 6 12 394.239 167.368 6 9 6 13-22.8360 74.3398 6 9 6 14 219.460 152.313 6 9 7 -6 157.971 99.0089 3 9 7 -5 172.001 88.3598 3 9 7 -4 174.536 86.7063 3 -9 -7 3 299.849 134.717 1 9 7 -3 235.549 87.7726 3 9 7 -2 2670.51 322.572 3 -9 -7 2 1940.36 339.456 1 -9 -7 1 6379.73 595.971 1 9 7 -1 7720.09 526.068 3 -9 -7 0 5871.80 571.456 1 -9 -7 -1 104.447 96.6095 1 9 7 1 169.261 73.8515 6 -9 -7 -2 64.3530 107.616 1 9 7 2 57.1016 52.5007 6 9 7 3 66.3838 59.7363 6 9 7 3 79.5290 49.0694 2 -9 -7 -3 63.1944 91.6633 1 9 7 4 1289.49 191.471 2 9 7 4 1388.07 215.243 6 -9 -7 -4 1081.71 242.816 1 9 7 5 2875.00 316.589 6 9 7 5 2680.63 281.559 2 9 7 6 37.0785 77.2260 6 9 7 6 142.668 71.6117 2 9 7 7 944.789 202.191 6 9 7 8 4942.91 475.890 6 9 7 9 592.122 180.479 6 9 7 10 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3 -5 272.939 118.374 4 -10 2 4 237.840 129.174 1 -10 2 3 215.331 148.666 1 -10 2 2 303.966 134.830 1 -10 2 1 1138.22 253.152 1 -10 2 0 291.640 114.289 4 -10 2 0 280.191 125.057 1 -10 2 -1 1795.26 315.836 1 -10 2 -1 1766.57 268.269 4 -10 2 -2 2228.88 349.968 1 -10 2 -2 2635.80 337.781 4 -10 2 -3 125.241 71.8336 4 -10 2 -3 312.689 146.448 1 -10 2 -4 78.1381 88.2061 4 -10 2 -4 38.6091 64.6873 1 -10 2 -5 234.959 116.369 4 -10 2 -5 388.482 177.769 1 -10 2 -6 1180.49 246.312 4 -10 2 -7 230.989 118.751 4 10 -1 -6-60.1732 99.7515 3 -10 1 5-70.8861 91.3353 1 -10 1 4 137.413 104.678 1 -10 1 3 87.2030 93.7602 1 -10 1 2 555.345 175.205 1 -10 1 1 3524.67 450.524 1 -10 1 0 2797.00 391.816 1 -10 1 -1 650.571 187.026 1 -10 1 -1 693.391 153.922 4 -10 1 -2 506.230 137.990 4 -10 1 -2 283.670 127.718 1 -10 1 -3-59.8058 57.1530 4 -10 1 -3 89.2248 127.146 1 -10 1 -4-65.8424 58.2457 4 -10 1 -4 97.1088 112.660 1 -10 1 -5 107.627 53.0786 4 -10 1 -5 144.431 106.666 1 -10 1 -6 979.567 202.316 4 -10 1 -7 812.808 191.740 4 -10 1 -8 2069.84 310.139 4 -10 1 -9 3753.52 431.015 4 10 0 -6 154.232 104.671 3 10 0 -5 1602.26 288.646 3 -10 0 5 1129.19 276.159 1 -10 0 4 145.366 146.221 1 -10 0 3 348.323 157.723 1 -10 0 2 272.606 145.107 1 -10 0 1 537.431 164.322 1 -10 0 0 2943.45 418.217 1 -10 0 -1 90.5505 87.9114 1 -10 0 -2-21.4986 39.1869 4 -10 0 -2-8.56915 87.6805 1 -10 0 -3 176.824 77.6857 4 -10 0 -3 203.984 147.789 1 -10 0 -4 2172.42 364.511 1 -10 0 -4 2231.36 268.776 4 -10 0 -5 2340.42 290.758 4 -10 0 -6 883.659 177.063 4 10 0 7 3051.49 387.551 2 -10 0 -7 2376.12 308.586 4 -10 0 -8-151.620 86.2261 4 10 1 -6 844.043 215.493 3 -10 -1 5 1891.10 348.918 1 10 1 -5 2325.07 341.204 3 -10 -1 4 4576.19 540.275 1 10 1 -4 5491.22 509.422 3 -10 -1 3 3476.51 463.363 1 -10 -1 2 735.957 217.855 1 -10 -1 1 12.7668 120.067 1 -10 -1 0-184.001 122.619 1 -10 -1 -1 506.894 195.268 1 -10 -1 -2 595.800 175.653 1 -10 -1 -3 1338.53 280.869 1 -10 -1 -3 1324.93 176.324 4 -10 -1 -4 1233.78 250.031 1 -10 -1 -4 1708.44 214.193 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226.190 6 10 4 9 1503.30 257.027 2 10 4 10 939.064 220.633 6 10 4 10 910.968 203.600 2 10 4 11 660.158 183.955 6 10 4 12 126.617 88.9278 6 10 4 13-209.158 132.637 6 10 5 -5 307.448 119.209 3 -10 -5 5 469.830 175.833 1 10 5 -4 31.8768 55.9195 3 -10 -5 4-11.8698 94.6909 1 10 5 -3 60.8597 85.4823 3 -10 -5 3 90.1361 137.167 1 10 5 -2 6.08803 44.1843 3 -10 -5 2 160.592 83.3283 1 -10 -5 1 2083.18 362.603 1 -10 -5 0 3430.22 453.638 1 -10 -5 -1 276.280 135.398 1 -10 -5 -2-151.744 160.285 1 -10 -5 -3 434.338 170.274 1 10 5 3 147.649 87.0526 2 -10 -5 -4 725.404 217.589 1 10 5 4 806.098 167.795 2 10 5 5-11.9054 43.5993 2 10 5 6 619.530 153.969 2 10 5 7 1907.08 281.116 2 10 5 7 1741.60 235.843 6 10 5 8 1424.38 235.592 6 10 5 8 1527.55 253.806 2 10 5 9 4485.92 441.438 2 10 5 9 3277.47 376.428 6 10 5 10 666.435 180.126 6 10 5 10 870.696 198.351 2 10 5 11 17.7872 82.0766 2 10 5 11-23.4546 92.3558 6 10 5 12-72.7327 133.513 6 10 5 13 86.8786 86.8804 6 10 6 -5-242.621 113.552 3 10 6 -4 115.371 76.3399 3 -10 -6 4-307.122 158.763 1 10 6 -3 767.555 190.912 3 -10 -6 3 842.976 232.972 1 -10 -6 2 2944.57 438.236 1 10 6 -2 3741.65 399.489 3 -10 -6 1 949.868 248.277 1 -10 -6 0 1195.99 281.623 1 -10 -6 -1 301.543 128.364 1 -10 -6 -2 1174.05 278.039 1 10 6 3 25.5384 50.4156 2 -10 -6 -3 62.7203 83.2039 1 -10 -6 -4 257.686 143.086 1 10 6 4 343.960 115.124 2 10 6 5 270.206 101.990 2 -10 -6 -5 200.777 150.495 1 10 6 6 278.064 102.315 2 10 6 7 4956.41 436.167 2 10 6 7 4341.32 390.329 6 10 6 8 4244.44 406.497 2 10 6 8 3764.53 390.330 6 10 6 9 1504.80 255.466 2 10 6 9 998.390 209.761 6 10 6 10-167.945 115.950 6 10 6 11 48.3494 89.3763 6 10 6 12 670.365 189.836 6 10 6 13 717.602 205.264 6 10 6 14 2129.07 388.501 6 -10 -7 4 1929.74 374.472 1 10 7 -4 2310.79 328.957 3 10 7 -3 2314.86 325.088 3 -10 -7 3 2027.09 371.740 1 10 7 -2 2470.32 324.325 3 -10 -7 2 2393.78 401.046 1 -10 -7 1 19.6047 87.0323 1 -10 -7 0 349.583 170.434 1 -10 -7 -1 1005.24 262.689 1 -10 -7 -2-19.6991 76.5288 1 10 7 3-70.4186 71.7762 2 -10 -7 -3-179.509 130.490 1 10 7 4 401.036 122.367 2 -10 -7 -4 302.713 129.950 1 10 7 5 2078.32 261.681 2 -10 -7 -5 2011.39 356.520 1 10 7 6 845.251 177.768 2 10 7 7 1155.93 226.631 6 10 7 7 1025.33 197.055 2 10 7 8 35.1113 75.3778 6 10 7 8-96.0924 71.3942 2 10 7 9-32.7496 73.9962 2 10 7 9-8.77669 71.2114 6 10 7 10 345.740 150.805 6 10 7 11 116.174 106.253 6 10 7 12 162.609 97.4772 6 10 7 13 27.5628 71.5855 6 10 7 14 34.0541 158.458 6 10 8 -4 3206.63 397.397 3 10 8 -3 538.311 161.013 3 -10 -8 3 235.610 132.492 1 -10 -8 2 739.971 238.874 1 -10 -8 1 182.211 109.898 1 -10 -8 0-37.9723 116.234 1 -10 -8 -1 1656.20 326.925 1 -10 -8 -2 1976.48 361.559 1 -10 -8 -3 706.813 215.414 1 10 8 4 432.103 113.167 2 -10 -8 -4 348.198 153.047 1 10 8 5 2396.24 272.911 2 -10 -8 -5 2254.58 387.433 1 10 8 6 118.396 63.5898 2 -10 -8 -6 117.401 117.420 1 10 8 7-348.952 131.785 6 10 8 7 38.2194 49.8030 2 10 8 8 460.592 158.040 6 10 8 8 108.333 84.0592 2 10 8 9 172.534 129.072 6 10 8 10 488.348 171.484 6 10 8 11 79.5135 115.055 6 10 8 12 255.793 130.743 6 10 8 13 515.690 204.589 6 10 9 -3 40.1028 52.4808 3 -10 -9 2 815.430 238.128 1 -10 -9 1 137.959 108.275 1 -10 -9 0 133.194 127.968 1 -10 -9 -1 772.138 226.375 1 -10 -9 -2 3129.27 453.730 1 -10 -9 -3 1571.33 320.298 1 10 9 4 494.247 123.491 2 -10 -9 -4 319.265 150.889 1 10 9 5 239.363 89.4143 2 -10 -9 -5-11.8045 108.161 1 10 9 6 172.433 80.7725 2 -10 -9 -6 411.175 183.936 1 10 9 7-21.1969 67.5172 2 -10 -9 -7-113.557 103.538 1 10 9 8 262.336 101.007 6 10 9 8 311.138 107.347 2 10 9 9 519.993 171.553 6 10 9 10 5718.37 593.589 6 10 9 11 1098.23 277.008 6 10 9 12 469.081 206.969 6 10 9 13 113.493 114.311 6 -10 -10 1-221.695 143.031 1 -10 -10 0 1547.08 334.400 1 -10 -10 -1 576.421 215.531 1 -10 -10 -2 1402.81 305.479 1 -10 -10 -3 953.998 249.800 1 -10 -10 -4 73.1367 96.9339 1 -10 -10 -5 38.0736 84.6683 1 -10 -10 -6 119.477 124.596 1 10 10 7 746.419 156.268 2 -10 -10 -7 405.672 179.274 1 10 10 8 1933.53 263.079 2 -10 -10 -8 1925.92 383.193 1 10 10 9 532.697 153.526 6 10 10 10 528.503 154.642 6 10 10 11 83.5391 104.723 6 10 10 12 269.752 135.839 6 -10 -11 -1 675.629 227.226 1 -10 -11 -2-165.567 127.111 1 -10 -11 -3 839.117 257.395 1 -10 -11 -4 40.1485 90.9049 1 -10 -11 -5-17.0548 77.9872 1 -10 -11 -6 65.3078 83.6030 1 -10 -11 -7 1077.59 283.698 1 -10 -11 -8 3187.41 476.739 1 -10 -11 -9 472.538 199.704 1 -11 2 4-206.115 128.591 1 -11 2 3 261.019 135.786 1 -11 2 2 605.323 195.732 1 -11 2 1 2309.25 380.620 1 -11 2 0 482.744 185.943 1 -11 2 -1 811.807 216.787 1 -11 2 -2 259.484 136.924 1 -11 1 4 24.3513 72.9951 1 -11 1 3 1379.96 312.202 1 -11 1 2 4182.22 518.196 1 -11 1 1 504.188 184.663 1 -11 1 0 379.197 150.871 1 -11 1 -1 167.292 120.656 1 -11 1 -2-381.474 169.818 1 -11 1 -3-184.519 124.021 1 -11 1 -4 687.116 229.271 1 -11 1 -5 2418.75 394.337 1 -11 1 -6 2817.94 432.779 1 -11 0 4 1589.15 337.693 1 -11 0 3 646.418 222.858 1 -11 0 2 2201.27 387.580 1 -11 0 1 760.264 234.169 1 -11 0 0-133.014 117.063 1 -11 0 -1 772.727 228.653 1 -11 0 -2-144.430 98.6944 1 -11 0 -3 1043.35 271.722 1 -11 0 -4 912.135 258.150 1 -11 0 -5 1102.14 280.804 1 -11 0 -6 1051.69 260.901 1 -11 -1 4 1305.67 313.931 1 -11 -1 3 476.197 193.368 1 -11 -1 2-74.8980 111.061 1 -11 -1 1-260.884 145.519 1 -11 -1 0 132.578 102.623 1 -11 -1 -1 109.191 110.573 1 -11 -1 -2-98.7509 110.591 1 -11 -1 -3 1599.84 340.099 1 -11 -1 -4 1769.49 342.797 1 -11 -1 -5 335.300 164.082 1 -11 -2 4 1371.43 311.555 1 -11 -2 3 273.290 135.579 1 -11 -2 2-44.1675 89.6172 1 -11 -2 1 109.449 106.711 1 -11 -2 0 210.767 141.286 1 -11 -2 -1 335.740 165.646 1 -11 -2 -2 3687.42 493.942 1 -11 -2 -3 341.538 155.524 1 -11 -2 -4 527.157 200.618 1 -11 -2 -5 415.535 183.015 1 11 2 6 142.613 108.114 2 -11 -3 4 600.561 219.772 1 -11 -3 3 58.5934 83.2173 1 -11 -3 2-87.6676 107.031 1 -11 -3 1 386.744 162.372 1 -11 -3 0 1045.99 264.302 1 -11 -3 -1 2722.19 421.871 1 -11 -3 -2 281.587 172.232 1 -11 -3 -3 814.210 235.161 1 -11 -3 -4 524.918 200.553 1 11 3 5 400.645 142.586 2 -11 -3 -5 575.458 195.460 1 11 3 6 882.351 199.101 2 11 3 7 227.739 106.188 2 -11 -4 3 2794.17 442.635 1 -11 -4 2 1099.34 292.197 1 -11 -4 1 3303.84 482.763 1 -11 -4 0 559.272 201.500 1 -11 -4 -1 225.537 150.051 1 -11 -4 -2-184.044 150.416 1 -11 -4 -3-8.25378 107.628 1 -11 -4 -4 1249.17 304.156 1 11 4 5-86.2197 91.6936 2 -11 -4 -5 25.7954 77.8939 1 11 4 6 159.916 79.2301 2 11 4 7 1065.95 223.001 2 11 4 8 1900.85 295.980 2 11 5 -3 1555.50 288.216 3 -11 -5 2 1161.93 301.443 1 -11 -5 1 357.583 175.172 1 -11 -5 0 145.567 112.016 1 -11 -5 -1 214.892 148.692 1 -11 -5 -2 666.581 219.049 1 -11 -5 -3 82.5841 107.542 1 -11 -5 -4 576.845 227.142 1 11 5 4 810.635 186.286 2 -11 -5 -5 1000.13 261.734 1 11 5 5 1415.04 239.703 2 11 5 6 1858.66 279.078 2 11 5 7 3525.41 389.368 2 11 5 8 1525.18 264.323 2 11 5 9-37.9433 60.7527 2 -11 -6 2-100.763 138.365 1 -11 -6 1-120.105 111.160 1 -11 -6 0 217.882 147.399 1 -11 -6 -1 175.245 108.293 1 -11 -6 -2 892.211 257.606 1 -11 -6 -3 205.927 135.490 1 11 6 4 2504.13 306.611 2 -11 -6 -4 2468.18 409.987 1 11 6 5 4200.31 403.905 2 -11 -6 -5 4482.24 550.177 1 11 6 6 1879.18 274.845 2 -11 -6 -6 2090.11 375.523 1 11 6 7-134.022 82.5507 2 11 6 8 54.2738 48.2628 2 11 6 9 208.268 114.377 2 -11 -7 1-114.009 117.967 1 -11 -7 0 117.464 119.631 1 -11 -7 -1 285.578 157.800 1 -11 -7 -2 1083.32 273.730 1 -11 -7 -3 2134.65 390.876 1 11 7 4 236.659 98.9010 2 -11 -7 -4 78.6949 95.9611 1 11 7 5 399.367 119.183 2 -11 -7 -5 199.837 108.267 1 -11 -7 -6 416.107 193.943 1 11 7 6 251.920 122.045 2 11 7 7 1.00374 42.5610 2 11 7 8 265.766 117.691 2 11 7 9 212.133 111.593 2 -11 -8 0 622.092 196.668 1 -11 -8 -1 542.166 211.138 1 -11 -8 -2 1099.36 272.128 1 -11 -8 -3 1029.50 278.336 1 -11 -8 -4 310.755 166.337 1 11 8 5 372.042 120.350 2 -11 -8 -5 435.972 187.540 1 -11 -8 -6 98.7975 124.171 1 11 8 6-18.0961 41.2568 2 11 8 7-57.6445 70.4567 2 -11 -8 -7-140.551 126.502 1 11 8 8 26.7292 36.6177 2 11 8 9 1532.49 254.938 2 -11 -9 -2 1580.24 340.562 1 -11 -9 -3 624.288 217.441 1 -11 -9 -4 243.606 138.984 1 11 9 5 68.7261 50.9741 2 -11 -9 -5-45.2529 152.584 1 11 9 6-125.049 75.2830 2 -11 -9 -6 91.6790 98.5408 1 11 9 7 1631.16 256.773 2 -11 -9 -7 1847.32 381.440 1 11 9 8 827.286 186.623 2 11 9 9 644.229 177.473 2 11 10 8 1554.31 245.029 2 11 10 9 1362.23 238.637 2 -12 -3 -2 337.228 170.074 1 12 6 6 276.091 119.321 2 12 7 5-23.6400 45.6934 2 12 7 6 631.179 168.624 2 12 8 6 236.203 103.802 2 12 8 7 714.978 177.407 2 12 9 6 237.021 106.159 2 12 9 7 1382.21 241.188 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 92120 data_9 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C4 H8 O)' _chemical_formula_sum 'C44 H48 Cl2 Cu N8 O10' _chemical_formula_weight 983.34 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.0943(5) _cell_length_b 25.0287(17) _cell_length_c 10.0253(5) _cell_angle_alpha 90 _cell_angle_beta 107.509(6) _cell_angle_gamma 90 _cell_volume 2176.2(2) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 3274 _cell_measurement_theta_min 3.2230 _cell_measurement_theta_max 28.7900 _exptl_crystal_description block _exptl_crystal_colour pink _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.501 _exptl_crystal_F_000 1022 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.13 _exptl_absorpt_coefficient_mu 0.694 _shelx_estimated_absorpt_T_min 0.857 _shelx_estimated_absorpt_T_max 0.915 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.503 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 8871 _diffrn_reflns_av_unetI/netI 0.1087 _diffrn_reflns_av_R_equivalents 0.0894 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_theta_min 2.857 _diffrn_reflns_theta_max 24.999 _diffrn_reflns_theta_full 24.999 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 0.995 _reflns_number_total 3808 _reflns_number_gt 2800 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+4.9457P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3808 _refine_ls_number_parameters 301 _refine_ls_number_restraints 3 _refine_ls_R_factor_all 0.0981 _refine_ls_R_factor_gt 0.0621 _refine_ls_wR_factor_ref 0.1568 _refine_ls_wR_factor_gt 0.1411 _refine_ls_goodness_of_fit_ref 1.175 _refine_ls_restrained_S_all 1.174 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 1.0000 0.5000 1.0000 0.0174(2) Uani 1 2 d S . P . . N1A N 0.7458(5) 0.53575(15) 0.5964(4) 0.0186(9) Uani 1 1 d D . . . . H1A H 0.740(6) 0.539(2) 0.5106(17) 0.028 Uiso 1 1 d D U . . . C2A C 0.8720(5) 0.52004(18) 0.6975(4) 0.0179(10) Uani 1 1 d . . . . . H2A H 0.9649 0.5081 0.6824 0.021 Uiso 1 1 calc R U . . . N3A N 0.8487(4) 0.52353(16) 0.8208(4) 0.0195(9) Uani 1 1 d . . . . . C4A C 0.7009(5) 0.5419(2) 0.7973(4) 0.0207(10) Uani 1 1 d . . . . . H4A H 0.6527 0.5483 0.8678 0.025 Uiso 1 1 calc R U . . . C5A C 0.6333(5) 0.54968(18) 0.6568(4) 0.0171(10) Uani 1 1 d . . . . . C6A C 0.4788(5) 0.56786(18) 0.5781(4) 0.0185(10) Uani 1 1 d . . . . . C7A C 0.4401(6) 0.58266(19) 0.4375(5) 0.0229(11) Uani 1 1 d . . . . . H7A H 0.5151 0.5802 0.3892 0.028 Uiso 1 1 calc R U . . . C8A C 0.2937(6) 0.6009(2) 0.3680(5) 0.0273(12) Uani 1 1 d . . . . . H8A H 0.2691 0.6105 0.2721 0.033 Uiso 1 1 calc R U . . . C9A C 0.1826(6) 0.6055(2) 0.4355(5) 0.0293(12) Uani 1 1 d . . . . . H9A H 0.0829 0.6188 0.3876 0.035 Uiso 1 1 calc R U . . . C10A C 0.2199(6) 0.5900(2) 0.5762(5) 0.0284(12) Uani 1 1 d . . . . . H10A H 0.1442 0.5923 0.6238 0.034 Uiso 1 1 calc R U . . . C11A C 0.3653(6) 0.5716(2) 0.6458(5) 0.0244(11) Uani 1 1 d . . . . . H11A H 0.3889 0.5612 0.7411 0.029 Uiso 1 1 calc R U . . . N1B N 1.3318(5) 0.61396(17) 1.0015(4) 0.0253(9) Uani 1 1 d D . . . . H1B H 1.412(3) 0.6263(19) 0.985(4) 0.038 Uiso 1 1 d D U . . . C2B C 1.2767(6) 0.5640(2) 0.9937(5) 0.0248(11) Uani 1 1 d . . . . . H2B H 1.3346 0.5327 0.9901 0.030 Uiso 1 1 calc R U . . . N3B N 1.1312(4) 0.56417(16) 0.9917(4) 0.0195(9) Uani 1 1 d . . . . . C4B C 1.0908(6) 0.6171(2) 0.9955(5) 0.0253(11) Uani 1 1 d . . . . . H4B H 0.9917 0.6297 0.9939 0.030 Uiso 1 1 calc R U . . . C5B C 1.2149(6) 0.6485(2) 1.0020(4) 0.0229(11) Uani 1 1 d . . . . . C6B C 1.2398(6) 0.7066(2) 1.0182(5) 0.0282(12) Uani 1 1 d . . . . . C7B C 1.3821(7) 0.7275(2) 1.0918(5) 0.0351(13) Uani 1 1 d . . . . . H7B H 1.4653 0.7041 1.1343 0.042 Uiso 1 1 calc R U . . . C8B C 1.4040(9) 0.7825(2) 1.1038(6) 0.0477(17) Uani 1 1 d . . . . . H8B H 1.5023 0.7965 1.1538 0.057 Uiso 1 1 calc R U . . . C9B C 1.2840(10) 0.8168(3) 1.0438(7) 0.0534(19) Uani 1 1 d . . . . . H9B H 1.2989 0.8544 1.0518 0.064 Uiso 1 1 calc R U . . . C10B C 1.1424(9) 0.7961(3) 0.9722(7) 0.0528(18) Uani 1 1 d . . . . . H10B H 1.0589 0.8195 0.9306 0.063 Uiso 1 1 calc R U . . . C11B C 1.1206(8) 0.7412(2) 0.9602(6) 0.0405(14) Uani 1 1 d . . . . . H11B H 1.0219 0.7274 0.9111 0.049 Uiso 1 1 calc R U . . . Cl Cl 0.75166(13) 0.56940(5) 1.20112(10) 0.0192(3) Uani 1 1 d . . . . . O1 O 0.8659(4) 0.56382(14) 1.1289(3) 0.0288(8) Uani 1 1 d . . . . . O2 O 0.6111(4) 0.54488(16) 1.1206(4) 0.0381(10) Uani 1 1 d . . . . . O3 O 0.7245(5) 0.62435(15) 1.2222(4) 0.0491(11) Uani 1 1 d . . . . . O4 O 0.8078(4) 0.54341(17) 1.3339(3) 0.0403(10) Uani 1 1 d . . . . . O5 O 0.5364(4) 0.66778(15) 0.8771(4) 0.0346(9) Uani 1 1 d . . . . . C12 C 0.6895(7) 0.6889(2) 0.9068(6) 0.0423(15) Uani 1 1 d . . . . . H12A H 0.7428 0.6734 0.8431 0.051 Uiso 1 1 calc R U . . . H12B H 0.7507 0.6811 1.0045 0.051 Uiso 1 1 calc R U . . . C13 C 0.6683(7) 0.7487(2) 0.8836(7) 0.0467(16) Uani 1 1 d . . . . . H13A H 0.6803 0.7674 0.9732 0.056 Uiso 1 1 calc R U . . . H13B H 0.7448 0.7631 0.8407 0.056 Uiso 1 1 calc R U . . . C14 C 0.5069(7) 0.7555(2) 0.7865(6) 0.0394(14) Uani 1 1 d . . . . . H14A H 0.5081 0.7726 0.6978 0.047 Uiso 1 1 calc R U . . . H14B H 0.4437 0.7774 0.8305 0.047 Uiso 1 1 calc R U . . . C15 C 0.4450(7) 0.6986(2) 0.7611(5) 0.0375(14) Uani 1 1 d . . . . . H15A H 0.3349 0.6976 0.7570 0.045 Uiso 1 1 calc R U . . . H15B H 0.4552 0.6846 0.6720 0.045 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0132(4) 0.0231(5) 0.0141(4) 0.0014(3) 0.0013(3) -0.0010(4) N1A 0.023(2) 0.020(2) 0.0130(18) -0.0003(16) 0.0055(17) -0.0007(18) C2A 0.018(3) 0.017(2) 0.018(2) 0.0013(19) 0.0029(19) 0.000(2) N3A 0.015(2) 0.026(2) 0.0177(19) -0.0007(17) 0.0050(16) -0.0026(18) C4A 0.019(3) 0.027(3) 0.017(2) 0.000(2) 0.0063(19) 0.001(2) C5A 0.017(2) 0.016(2) 0.016(2) -0.0020(19) 0.0020(19) -0.002(2) C6A 0.022(3) 0.012(2) 0.019(2) -0.0048(19) 0.003(2) -0.006(2) C7A 0.026(3) 0.021(3) 0.019(2) 0.003(2) 0.003(2) -0.002(2) C8A 0.032(3) 0.022(3) 0.021(2) 0.006(2) -0.002(2) -0.001(2) C9A 0.022(3) 0.019(3) 0.038(3) 0.004(2) -0.006(2) 0.003(2) C10A 0.020(3) 0.028(3) 0.036(3) -0.005(2) 0.006(2) -0.001(2) C11A 0.024(3) 0.027(3) 0.021(2) -0.001(2) 0.004(2) -0.001(2) N1B 0.022(2) 0.025(2) 0.032(2) 0.0012(19) 0.0117(19) -0.002(2) C2B 0.023(3) 0.024(3) 0.030(3) -0.004(2) 0.011(2) -0.004(2) N3B 0.018(2) 0.023(2) 0.0150(18) -0.0030(16) 0.0022(16) -0.0040(18) C4B 0.023(3) 0.026(3) 0.027(2) 0.006(2) 0.008(2) 0.006(2) C5B 0.026(3) 0.024(3) 0.017(2) 0.008(2) 0.005(2) 0.003(2) C6B 0.037(3) 0.023(3) 0.027(3) 0.007(2) 0.013(2) 0.004(3) C7B 0.043(4) 0.026(3) 0.040(3) 0.000(2) 0.017(3) -0.004(3) C8B 0.069(5) 0.032(3) 0.049(4) -0.004(3) 0.028(3) -0.010(3) C9B 0.088(6) 0.022(3) 0.060(4) 0.002(3) 0.038(4) 0.002(4) C10B 0.070(5) 0.035(4) 0.060(4) 0.013(3) 0.029(4) 0.018(4) C11B 0.048(4) 0.031(3) 0.046(3) 0.012(3) 0.020(3) 0.011(3) Cl 0.0194(6) 0.0216(6) 0.0170(5) -0.0004(5) 0.0061(4) 0.0012(5) O1 0.028(2) 0.040(2) 0.0213(17) -0.0002(15) 0.0128(15) 0.0006(17) O2 0.019(2) 0.049(3) 0.042(2) -0.0154(19) 0.0034(17) -0.0015(19) O3 0.064(3) 0.025(2) 0.068(3) -0.009(2) 0.036(2) 0.002(2) O4 0.031(2) 0.068(3) 0.0244(18) 0.0216(19) 0.0124(16) 0.014(2) O5 0.030(2) 0.033(2) 0.042(2) 0.0058(17) 0.0133(18) -0.0030(18) C12 0.031(3) 0.043(4) 0.052(3) 0.003(3) 0.012(3) -0.006(3) C13 0.040(4) 0.031(3) 0.071(4) 0.002(3) 0.020(3) -0.005(3) C14 0.049(4) 0.032(3) 0.043(3) 0.005(3) 0.022(3) 0.006(3) C15 0.041(4) 0.038(3) 0.035(3) 0.008(3) 0.014(3) 0.003(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.995(4) . ? Cu N3A 1.995(4) 3_767 ? Cu N3B 2.018(4) . ? Cu N3B 2.018(4) 3_767 ? N1A C2A 1.341(6) . ? N1A C5A 1.381(6) . ? N1A H1A 0.848(10) . ? C2A N3A 1.319(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.372(6) . ? C4A C5A 1.371(6) . ? C4A H4A 0.9500 . ? C5A C6A 1.461(7) . ? C6A C7A 1.396(6) . ? C6A C11A 1.398(7) . ? C7A C8A 1.382(7) . ? C7A H7A 0.9500 . ? C8A C9A 1.379(7) . ? C8A H8A 0.9500 . ? C9A C10A 1.402(7) . ? C9A H9A 0.9500 . ? C10A C11A 1.376(7) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.341(6) . ? N1B C5B 1.372(6) . ? N1B H1B 0.858(10) . ? C2B N3B 1.317(6) . ? C2B H2B 0.9500 . ? N3B C4B 1.379(6) . ? C4B C5B 1.361(7) . ? C4B H4B 0.9500 . ? C5B C6B 1.473(7) . ? C6B C11B 1.372(8) . ? C6B C7B 1.385(8) . ? C7B C8B 1.390(8) . ? C7B H7B 0.9500 . ? C8B C9B 1.377(9) . ? C8B H8B 0.9500 . ? C9B C10B 1.373(10) . ? C9B H9B 0.9500 . ? C10B C11B 1.389(8) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.424(4) . ? Cl O2 1.429(4) . ? Cl O4 1.430(3) . ? Cl O1 1.440(3) . ? O5 C12 1.435(7) . ? O5 C15 1.435(6) . ? C12 C13 1.517(8) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.507(8) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 C15 1.523(8) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0(2) . 3_767 ? N3A Cu N3B 89.11(15) . . ? N3A Cu N3B 90.89(15) 3_767 . ? N3A Cu N3B 90.90(15) . 3_767 ? N3A Cu N3B 89.10(15) 3_767 3_767 ? N3B Cu N3B 180.0 . 3_767 ? C2A N1A C5A 108.7(4) . . ? C2A N1A H1A 125(4) . . ? C5A N1A H1A 126(4) . . ? N3A C2A N1A 110.3(4) . . ? N3A C2A H2A 124.9 . . ? N1A C2A H2A 124.9 . . ? C2A N3A C4A 106.7(4) . . ? C2A N3A Cu 124.3(3) . . ? C4A N3A Cu 128.9(3) . . ? C5A C4A N3A 109.7(4) . . ? C5A C4A H4A 125.2 . . ? N3A C4A H4A 125.2 . . ? C4A C5A N1A 104.6(4) . . ? C4A C5A C6A 131.3(4) . . ? N1A C5A C6A 124.1(4) . . ? C7A C6A C11A 118.3(5) . . ? C7A C6A C5A 122.5(4) . . ? C11A C6A C5A 119.3(4) . . ? C8A C7A C6A 120.6(5) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C9A C8A C7A 121.1(5) . . ? C9A C8A H8A 119.4 . . ? C7A C8A H8A 119.4 . . ? C8A C9A C10A 118.7(5) . . ? C8A C9A H9A 120.7 . . ? C10A C9A H9A 120.7 . . ? C11A C10A C9A 120.4(5) . . ? C11A C10A H10A 119.8 . . ? C9A C10A H10A 119.8 . . ? C10A C11A C6A 120.9(4) . . ? C10A C11A H11A 119.5 . . ? C6A C11A H11A 119.5 . . ? C2B N1B C5B 108.2(4) . . ? C2B N1B H1B 131(4) . . ? C5B N1B H1B 119(3) . . ? N3B C2B N1B 110.7(4) . . ? N3B C2B H2B 124.7 . . ? N1B C2B H2B 124.7 . . ? C2B N3B C4B 106.2(4) . . ? C2B N3B Cu 126.9(3) . . ? C4B N3B Cu 126.7(3) . . ? C5B C4B N3B 109.4(4) . . ? C5B C4B H4B 125.3 . . ? N3B C4B H4B 125.3 . . ? C4B C5B N1B 105.6(4) . . ? C4B C5B C6B 132.3(5) . . ? N1B C5B C6B 122.0(4) . . ? C11B C6B C7B 118.7(5) . . ? C11B C6B C5B 120.0(5) . . ? C7B C6B C5B 121.3(5) . . ? C6B C7B C8B 120.5(6) . . ? C6B C7B H7B 119.8 . . ? C8B C7B H7B 119.8 . . ? C9B C8B C7B 120.3(7) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C10B C9B C8B 119.3(6) . . ? C10B C9B H9B 120.4 . . ? C8B C9B H9B 120.4 . . ? C9B C10B C11B 120.4(6) . . ? C9B C10B H10B 119.8 . . ? C11B C10B H10B 119.8 . . ? C6B C11B C10B 120.9(6) . . ? C6B C11B H11B 119.6 . . ? C10B C11B H11B 119.6 . . ? O3 Cl O2 109.5(3) . . ? O3 Cl O4 109.3(3) . . ? O2 Cl O4 109.8(2) . . ? O3 Cl O1 110.6(2) . . ? O2 Cl O1 109.4(2) . . ? O4 Cl O1 108.3(2) . . ? C12 O5 C15 105.0(4) . . ? O5 C12 C13 105.2(5) . . ? O5 C12 H12A 110.7 . . ? C13 C12 H12A 110.7 . . ? O5 C12 H12B 110.7 . . ? C13 C12 H12B 110.7 . . ? H12A C12 H12B 108.8 . . ? C14 C13 C12 105.4(5) . . ? C14 C13 H13A 110.7 . . ? C12 C13 H13A 110.7 . . ? C14 C13 H13B 110.7 . . ? C12 C13 H13B 110.7 . . ? H13A C13 H13B 108.8 . . ? C13 C14 C15 104.0(5) . . ? C13 C14 H14A 111.0 . . ? C15 C14 H14A 111.0 . . ? C13 C14 H14B 111.0 . . ? C15 C14 H14B 111.0 . . ? H14A C14 H14B 109.0 . . ? O5 C15 C14 105.8(5) . . ? O5 C15 H15A 110.6 . . ? C14 C15 H15A 110.6 . . ? O5 C15 H15B 110.6 . . ? C14 C15 H15B 110.6 . . ? H15A C15 H15B 108.7 . . ? _refine_diff_density_max 0.866 _refine_diff_density_min -0.585 _refine_diff_density_rms 0.111 # start Validation Reply Form _vrf_PLAT934_9 ; RESPONSE: This alert, and some of the following ones, are due to the medium diffraction quality of the crystals used (despite systematic trials to obtain better crystals for X-ray data collection). No twin law has been detected. Discordant reflections with error/esd > 12 have been removed from the refinement. ; # end Validation Reply Form _shelx_res_file ; 9.res created by SHELXL-2014/7 TITL EL101A in P21/n CELL 0.71073 9.0943 25.0287 10.0253 90.000 107.509 90.000 ZERR 2 0.0005 0.0017 0.0005 0.000 0.006 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O CL CU UNIT 88 96 16 20 4 2 MERG 2 FMAP 2 OMIT -2 50 OMIT 7 8 6 OMIT 7 5 4 OMIT 7 6 6 OMIT 7 7 6 OMIT 6 6 2 OMIT 6 11 5 OMIT 6 13 6 OMIT 7 8 5 OMIT 6 17 5 OMIT 7 5 6 OMIT 6 12 6 OMIT 6 15 5 SIZE 0.23 0.13 0.13 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND $H HTAB L.S. 7 DFIX 0.85 0.01 N1A H1A N1B H1B EQIV $1 1+X, Y, Z DFIX 2.05 0.01 H1B O5_$1 WGHT 0.045700 4.945700 FVAR 1.17493 CU 6 1.000000 0.500000 1.000000 10.50000 0.01317 0.02305 = 0.01415 0.00143 0.00129 -0.00103 N1A 3 0.745774 0.535749 0.596386 11.00000 0.02275 0.02016 = 0.01297 -0.00035 0.00554 -0.00070 H1A 2 0.739527 0.538616 0.510570 11.00000 -1.50000 C2A 1 0.871966 0.520045 0.697460 11.00000 0.01757 0.01687 = 0.01762 0.00129 0.00285 -0.00026 AFIX 43 H2A 2 0.964853 0.508118 0.682366 11.00000 -1.20000 AFIX 0 N3A 3 0.848663 0.523527 0.820818 11.00000 0.01523 0.02551 = 0.01768 -0.00068 0.00500 -0.00255 C4A 1 0.700867 0.541915 0.797338 11.00000 0.01873 0.02659 = 0.01745 0.00017 0.00627 0.00075 AFIX 43 H4A 2 0.652697 0.548295 0.867793 11.00000 -1.20000 AFIX 0 C5A 1 0.633276 0.549682 0.656813 11.00000 0.01707 0.01589 = 0.01642 -0.00197 0.00201 -0.00249 C6A 1 0.478813 0.567861 0.578115 11.00000 0.02190 0.01234 = 0.01918 -0.00483 0.00300 -0.00564 C7A 1 0.440125 0.582660 0.437499 11.00000 0.02551 0.02143 = 0.01936 0.00328 0.00299 -0.00215 AFIX 43 H7A 2 0.515133 0.580158 0.389196 11.00000 -1.20000 AFIX 0 C8A 1 0.293709 0.600911 0.368004 11.00000 0.03181 0.02177 = 0.02134 0.00614 -0.00237 -0.00082 AFIX 43 H8A 2 0.269127 0.610493 0.272104 11.00000 -1.20000 AFIX 0 C9A 1 0.182616 0.605458 0.435480 11.00000 0.02171 0.01851 = 0.03775 0.00365 -0.00602 0.00302 AFIX 43 H9A 2 0.082870 0.618782 0.387595 11.00000 -1.20000 AFIX 0 C10A 1 0.219877 0.590016 0.576203 11.00000 0.02025 0.02775 = 0.03562 -0.00469 0.00599 -0.00150 AFIX 43 H10A 2 0.144207 0.592303 0.623827 11.00000 -1.20000 AFIX 0 C11A 1 0.365331 0.571571 0.645773 11.00000 0.02377 0.02661 = 0.02098 -0.00129 0.00378 -0.00050 AFIX 43 H11A 2 0.388949 0.561218 0.741067 11.00000 -1.20000 AFIX 0 N1B 3 1.331752 0.613959 1.001519 11.00000 0.02193 0.02452 = 0.03188 0.00118 0.01167 -0.00218 H1B 2 1.412479 0.626300 0.984765 11.00000 -1.50000 C2B 1 1.276696 0.563955 0.993703 11.00000 0.02284 0.02384 = 0.03003 -0.00355 0.01131 -0.00354 AFIX 43 H2B 2 1.334644 0.532699 0.990099 11.00000 -1.20000 AFIX 0 N3B 3 1.131238 0.564168 0.991717 11.00000 0.01847 0.02321 = 0.01501 -0.00298 0.00216 -0.00397 C4B 1 1.090768 0.617125 0.995545 11.00000 0.02329 0.02599 = 0.02659 0.00642 0.00768 0.00641 AFIX 43 H4B 2 0.991702 0.629719 0.993927 11.00000 -1.20000 AFIX 0 C5B 1 1.214886 0.648522 1.002002 11.00000 0.02630 0.02443 = 0.01674 0.00761 0.00473 0.00327 C6B 1 1.239809 0.706632 1.018222 11.00000 0.03656 0.02343 = 0.02713 0.00728 0.01338 0.00372 C7B 1 1.382081 0.727527 1.091779 11.00000 0.04259 0.02559 = 0.03987 -0.00033 0.01670 -0.00392 AFIX 43 H7B 2 1.465262 0.704142 1.134292 11.00000 -1.20000 AFIX 0 C8B 1 1.404029 0.782492 1.103842 11.00000 0.06863 0.03199 = 0.04887 -0.00390 0.02752 -0.00988 AFIX 43 H8B 2 1.502327 0.796452 1.153763 11.00000 -1.20000 AFIX 0 C9B 1 1.283975 0.816808 1.043781 11.00000 0.08840 0.02218 = 0.05969 0.00236 0.03771 0.00186 AFIX 43 H9B 2 1.298946 0.854375 1.051808 11.00000 -1.20000 AFIX 0 C10B 1 1.142438 0.796115 0.972186 11.00000 0.07044 0.03454 = 0.05982 0.01301 0.02933 0.01777 AFIX 43 H10B 2 1.058923 0.819494 0.930606 11.00000 -1.20000 AFIX 0 C11B 1 1.120634 0.741182 0.960188 11.00000 0.04780 0.03125 = 0.04621 0.01243 0.01986 0.01126 AFIX 43 H11B 2 1.021868 0.727360 0.911137 11.00000 -1.20000 AFIX 0 CL 5 0.751665 0.569396 1.201123 11.00000 0.01940 0.02165 = 0.01699 -0.00039 0.00607 0.00117 O1 4 0.865869 0.563824 1.128905 11.00000 0.02822 0.04041 = 0.02132 -0.00019 0.01279 0.00055 O2 4 0.611071 0.544880 1.120588 11.00000 0.01907 0.04903 = 0.04237 -0.01543 0.00337 -0.00150 O3 4 0.724528 0.624347 1.222236 11.00000 0.06450 0.02498 = 0.06832 -0.00857 0.03582 0.00162 O4 4 0.807778 0.543410 1.333858 11.00000 0.03068 0.06847 = 0.02439 0.02160 0.01240 0.01350 O5 4 0.536447 0.667775 0.877095 11.00000 0.02979 0.03346 = 0.04215 0.00578 0.01325 -0.00296 C12 1 0.689528 0.688933 0.906764 11.00000 0.03147 0.04311 = 0.05219 0.00332 0.01232 -0.00603 AFIX 23 H12A 2 0.742809 0.673363 0.843101 11.00000 -1.20000 H12B 2 0.750696 0.681137 1.004529 11.00000 -1.20000 AFIX 0 C13 1 0.668307 0.748681 0.883582 11.00000 0.04026 0.03088 = 0.07117 0.00217 0.01994 -0.00502 AFIX 23 H13A 2 0.680307 0.767390 0.973242 11.00000 -1.20000 H13B 2 0.744810 0.763127 0.840659 11.00000 -1.20000 AFIX 0 C14 1 0.506919 0.755491 0.786457 11.00000 0.04935 0.03179 = 0.04265 0.00500 0.02213 0.00588 AFIX 23 H14A 2 0.508086 0.772606 0.697753 11.00000 -1.20000 H14B 2 0.443727 0.777449 0.830511 11.00000 -1.20000 AFIX 0 C15 1 0.444977 0.698643 0.761118 11.00000 0.04092 0.03772 = 0.03529 0.00812 0.01383 0.00327 AFIX 23 H15A 2 0.334881 0.697551 0.757006 11.00000 -1.20000 H15B 2 0.455194 0.684614 0.672000 11.00000 -1.20000 AFIX 0 HKLF 4 REM EL101A in P21/n REM R1 = 0.0621 for 2800 Fo > 4sig(Fo) and 0.0981 for all 3808 data REM 301 parameters refined using 3 restraints END WGHT 0.0454 4.5153 REM Instructions for potential hydrogen bonds EQIV $2 x, y, z-1 HTAB N1A O4_$2 EQIV $3 -x+2, -y+1, -z+2 HTAB C2A O4_$3 HTAB N1B O5_$1 HTAB C2B O2_$1 HTAB C2B O2_$3 HTAB C4B O1 REM Highest difference peak 0.866, deepest hole -0.585, 1-sigma level 0.111 Q1 1 1.0626 0.5002 0.9111 11.00000 0.05 0.87 Q2 1 0.6974 0.6183 1.1195 11.00000 0.05 0.53 Q3 1 0.9998 0.5327 1.0077 11.00000 0.05 0.50 Q4 1 0.5771 0.5714 0.6472 11.00000 0.05 0.49 Q5 1 1.0817 0.5231 0.8413 11.00000 0.05 0.45 Q6 1 0.8034 0.5463 0.8201 11.00000 0.05 0.42 Q7 1 1.3613 0.5249 1.0628 11.00000 0.05 0.42 Q8 1 0.6385 0.5485 0.7140 11.00000 0.05 0.42 Q9 1 0.9039 0.5283 1.1659 11.00000 0.05 0.41 Q10 1 0.7553 0.5255 0.9201 11.00000 0.05 0.41 ; _shelx_res_checksum 25276 _shelx_hkl_file ; 0 0 2 23508.6 239.144 1 0 0 -2 23217.4 273.225 3 0 0 -3-7.63728 40.4481 3 0 0 -3-7.75149 10.2516 2 0 0 3-15.7482 29.3150 1 0 0 3 4.69125 11.2793 2 0 0 -4 1568.69 106.231 3 0 0 4 1583.66 53.7820 2 0 0 4 1639.87 96.3175 1 0 0 5 80.7309 45.0482 1 0 0 -5 113.953 56.4995 3 0 0 5 65.8165 17.9842 2 0 0 6 8366.03 260.765 1 0 0 6 8203.23 138.231 2 0 0 -6 8816.97 295.177 3 0 0 7 331.707 70.0469 1 0 0 7 197.796 22.6178 2 0 0 -7 361.695 86.1668 3 0 0 -8 2166.54 176.592 3 0 0 8 2009.31 158.152 1 0 0 -9 137.873 74.7622 3 0 0 -10 5934.52 324.072 3 0 0 -11 17.3692 58.0258 3 0 0 -12 319.051 100.566 3 0 1 -2 194.425 20.5125 2 0 -1 -2 187.409 38.8423 3 0 -1 2 168.684 27.0990 1 0 -1 3 7946.40 128.387 2 0 -1 -3 8502.18 203.469 3 0 -1 3 7972.55 169.847 1 0 1 -3 8303.62 119.125 2 0 1 -3 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59.3721 2 0 25 -1 670.337 108.169 2 0 25 1 785.192 113.633 2 0 25 -2 481.481 98.4540 2 0 25 2 442.222 89.7069 2 0 25 3 382.999 79.6542 2 0 -25 -3 499.990 86.7502 3 0 25 -3 443.355 96.0333 2 0 -25 -4 471.994 109.209 3 0 25 -4 266.666 79.2135 2 0 -25 -5 454.087 167.637 3 0 25 -5 423.041 96.4510 2 0 25 -6 88.4463 61.0475 2 0 -25 -6-80.9876 154.820 3 0 25 -7 120.397 62.4941 2 0 -25 -8 122.057 88.9121 3 0 25 -8 192.528 71.3301 2 0 26 0 939.443 127.298 2 0 26 1 167.555 68.0424 2 0 26 -1 173.586 69.3531 2 0 26 2 400.015 89.5830 2 0 26 -2 582.237 106.932 2 0 26 -3 272.261 83.3151 2 0 26 3 194.849 66.6735 2 0 -26 -3 231.193 69.4508 3 0 26 -4 788.589 124.239 2 0 -26 -4 1119.83 142.809 3 0 26 -5 221.024 80.4743 2 0 -26 -5 297.602 114.684 3 0 26 -6 110.155 65.9268 2 0 -26 -6-115.879 138.363 3 0 26 -7 18.4357 42.5940 2 0 27 0 90.5182 61.0697 2 0 27 -1 349.158 88.8996 2 0 27 1 324.329 83.3200 2 0 27 -2 39.2641 53.1599 2 0 27 2 46.2851 53.5387 2 0 27 3 93.8923 60.1566 2 0 27 -3 127.626 65.8218 2 0 27 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4 3430.16 73.6188 2 1 -2 4 3374.93 113.199 1 1 2 4 3334.51 70.2006 2 -1 2 -4 3553.42 156.363 3 1 -2 5 73.0573 32.2402 1 1 2 5 73.7225 15.2987 2 -1 2 -5 94.8736 52.9629 3 -1 -2 -5 81.2042 48.1258 3 1 2 5 69.9707 15.5642 2 1 -2 5 68.5268 25.6930 2 1 -2 6 74.1287 26.0015 2 1 -2 6 40.7904 30.5417 1 -1 2 -6 36.7147 44.6458 3 -1 -2 -6 61.6494 49.2877 3 1 2 7 1053.88 112.893 1 1 -2 7 834.206 87.2705 1 -1 -2 -7 886.975 110.906 3 1 -2 7 904.172 66.0746 2 -1 2 -7 945.926 115.985 3 -1 -2 -8 835.032 116.012 3 1 -2 8 732.356 93.1429 1 1 2 8 811.262 108.832 1 -1 2 -8 827.836 117.176 3 1 2 9 1238.03 140.721 1 -1 -2 -9 1298.50 149.625 3 -1 2 -9 1272.71 148.019 3 1 2 10-27.2385 52.3160 1 -1 -2 -10 45.7920 60.2089 3 -1 2 -10 47.5977 58.3194 3 -1 2 -11 1132.53 159.793 3 -1 -2 -11 1316.60 168.920 3 1 3 -12 26.3850 69.5064 3 1 -3 -12 19.3887 73.3270 3 1 -3 -11 769.483 133.342 3 1 3 -11 703.662 132.619 3 1 -3 -10 327.056 89.9645 3 1 3 -10 133.557 68.8515 3 -1 3 10 172.294 82.1219 1 -1 3 9-31.8478 59.0719 1 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142.241 3 1 4 -11 985.622 152.111 3 1 4 -10 713.959 126.799 3 -1 4 10 630.356 125.704 1 1 -4 -10 763.477 126.654 3 -1 4 9 113.694 65.9253 1 1 4 -9 61.4168 64.5327 3 1 -4 -9 127.450 60.2474 3 -1 -4 8 960.553 84.2713 2 -1 4 8 1391.45 151.629 1 1 4 -8 1423.74 156.623 3 1 4 -8 1247.58 83.0472 2 1 -4 -8 1288.69 135.728 3 1 4 -7 1354.94 147.004 3 1 4 -7 1307.81 82.1661 2 1 -4 -7 1575.77 137.772 3 -1 4 7 1387.05 141.946 1 -1 -4 7 1335.68 94.8574 2 1 -4 -6 1516.62 124.798 3 -1 -4 6 1693.26 101.301 2 1 4 -6 1717.76 93.4223 2 -1 4 6 1640.39 139.670 1 1 4 -6 1472.16 104.537 1 1 -4 -5 2053.61 129.634 3 -1 4 5 1978.56 142.310 1 1 4 -5 1867.11 95.0349 2 1 4 -5 2100.08 118.532 1 -1 -4 5 1896.68 101.633 2 1 -4 -4 965.195 40.8572 2 1 4 -4 965.041 68.9681 2 1 4 -4 912.075 76.3716 1 -1 -4 4 924.155 70.7225 2 1 -4 -4 1038.38 86.1415 3 -1 4 4 997.983 96.6420 1 1 4 -3 3770.38 121.847 2 -1 -4 3 3514.81 123.939 2 1 -4 -3 3682.33 129.694 3 1 4 -2 58681.7 441.837 2 1 -4 -2 57790.4 409.198 3 1 -4 -1 13414.6 142.833 3 1 4 -1 14452.6 204.840 2 1 4 0 5915.13 126.444 2 -1 -4 0 5694.76 163.658 3 -1 -4 -1 2251.46 77.3193 2 1 4 1 2223.71 75.3435 2 1 4 2 7714.96 127.096 2 -1 -4 -2 7627.22 128.433 2 -1 -4 -2 7633.78 177.670 3 1 4 3 9609.98 129.686 2 -1 4 -3 9767.02 234.886 3 1 -4 3 9649.90 194.858 2 -1 -4 -3 9369.30 223.197 3 -1 -4 -4 355.646 61.9172 3 1 -4 4 373.300 46.3651 2 -1 4 -4 413.179 66.8552 3 -1 4 -5 1905.61 136.249 3 -1 -4 -5 1804.21 129.776 3 1 -4 5 1816.06 101.257 2 1 -4 6 113.814 31.7377 2 -1 4 -6 118.461 53.1842 3 -1 -4 -6 75.7914 51.6373 3 1 -4 7 1670.02 104.316 2 1 4 7 2044.67 164.566 1 -1 4 -7 1923.35 158.135 3 -1 -4 -7 1807.78 151.062 3 -1 -4 -8 405.459 90.2470 3 1 4 8 436.037 92.6738 1 -1 4 -8 415.034 89.6235 3 -1 4 -9 1317.56 154.410 3 -1 -4 -9 1200.60 146.982 3 1 4 9 1232.16 149.299 1 -1 -4 -10 777.285 128.281 3 -1 4 -10 883.979 136.266 3 1 4 10 796.053 130.587 1 -1 4 -11 17.1778 57.7678 3 -1 -4 -11-5.68295 53.0068 3 1 -5 -12 940.656 155.383 3 1 5 -12 828.611 155.271 3 1 -5 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57.0500 3 1 -6 -12-12.2229 55.0832 3 1 6 -11 2832.03 254.278 3 1 -6 -11 3057.16 248.199 3 -1 6 11 2599.00 256.685 1 1 6 -10 1063.71 153.447 3 1 -6 -10 1230.40 156.238 3 -1 6 10 1242.79 172.733 1 -1 6 9 146.497 80.2457 1 1 -6 -9 136.178 65.6526 3 1 6 -9 67.0369 61.4429 3 1 6 -9 132.609 38.4505 2 1 -6 -8 895.823 114.943 3 1 6 -8 879.697 78.2600 2 -1 6 8 816.796 127.957 1 1 6 -8 954.599 135.674 3 -1 -6 8 693.179 79.6651 2 -1 -6 7 2694.47 147.023 2 1 6 -7 2846.33 132.743 2 1 -6 -7 3155.50 189.273 3 -1 6 7 3226.23 218.771 1 1 6 -7 3103.38 158.547 1 -1 6 6 1944.05 161.163 1 1 6 -6 1892.05 108.787 2 1 -6 -6 1937.20 138.895 3 1 6 -6 1661.47 111.579 1 -1 -6 6 1780.37 115.208 2 -1 -6 5 4058.58 162.885 2 1 -6 -5 3909.64 72.9310 2 1 -6 -5 4149.44 178.576 3 1 -6 -5 4158.07 77.7127 2 -1 6 5 4226.77 212.050 1 1 6 -5 3894.48 161.866 1 1 6 -5 4079.72 152.826 2 1 6 -4 3296.09 135.151 2 -1 -6 4 3180.79 137.001 2 1 -6 -4 2868.78 76.8990 2 1 -6 -4 3212.95 141.439 3 1 -6 -3 2899.87 86.6666 2 1 -6 -3 2959.52 118.055 3 1 6 -3 3039.54 123.405 2 1 6 -2 1077.67 75.4609 2 1 -6 -2 955.479 58.8052 3 1 -6 -2 835.499 53.4276 2 -1 6 1 7115.00 131.857 3 1 6 -1 6736.42 168.542 2 -1 -6 0 48249.9 467.728 3 -1 6 0 44927.2 382.665 2 1 6 0 44854.6 397.609 2 -1 6 -1 9429.00 189.584 2 1 6 1 7981.72 159.615 2 -1 -6 -1 8358.95 172.813 2 -1 6 -2 419.852 48.7872 2 -1 -6 -2 484.557 61.6909 3 1 6 2 361.224 37.3456 2 -1 -6 -2 364.422 36.3061 2 -1 -6 -3 3960.29 154.723 3 1 6 3 4127.03 102.734 2 1 -6 3 4335.27 151.971 2 -1 -6 -3 3901.11 101.404 2 -1 6 -3 4361.99 142.517 2 1 6 4 4136.98 86.3865 2 1 -6 4 4257.44 159.808 2 -1 -6 -4 4063.56 169.554 3 -1 6 -5 3446.00 185.330 3 -1 -6 -5 3126.63 164.298 3 1 -6 5 3306.45 150.538 2 -1 6 -6 86.0354 51.4085 3 -1 -6 -6 44.9176 43.5885 3 1 -6 6 101.772 32.9483 2 -1 -6 -7 40.3285 55.4526 3 -1 6 -7 11.3890 48.9747 3 1 -6 7 31.3197 24.8584 2 -1 6 -8 73.8331 60.3835 3 -1 -6 -8 36.6475 49.7701 3 1 6 8 51.4822 66.1512 1 -1 -6 -9 2225.98 189.308 3 1 6 9 2261.86 209.504 1 -1 6 -9 2273.63 200.389 3 1 6 10 116.664 72.1085 1 -1 -6 -10 119.949 68.4770 3 -1 6 -10 124.114 68.6110 3 -1 -6 -11-20.6777 59.9762 3 -1 6 -11-7.57987 59.9772 3 -1 7 12 1167.58 191.721 1 1 7 -12 1472.76 196.028 3 1 7 -11 52.3150 74.4786 3 1 -7 -11 18.4061 65.3445 3 -1 7 11-15.4837 66.7651 1 1 7 -10 579.983 123.220 3 -1 7 10 486.146 120.201 1 1 -7 -10 651.205 118.366 3 1 7 -9 478.108 65.3806 2 1 -7 -9 481.378 95.4648 3 1 7 -9 431.967 102.085 3 -1 7 9 573.622 120.774 1 -1 7 8-14.1442 58.9268 1 1 -7 -8 3.63070 50.0497 3 1 7 -8-2.25171 26.9646 2 1 -7 -7 37.2363 46.3521 3 -1 7 7 1.19836 51.4911 1 1 7 -7 37.4520 28.0674 2 1 7 -7 17.4264 22.3368 1 -1 -7 7 22.4060 25.2469 2 -1 -7 6 1616.68 115.258 2 1 -7 -6 1763.83 135.757 3 1 7 -6 1618.04 112.574 1 1 7 -6 1874.96 113.270 2 -1 7 6 1851.16 159.150 1 1 -7 -5 213.259 54.0573 3 -1 -7 5 194.684 43.6461 2 -1 7 5 185.392 70.0706 1 1 7 -5 228.726 49.9430 2 1 -7 -5 180.499 21.8519 2 1 7 -4 121.262 40.6567 2 1 -7 -4 149.614 22.3616 2 -1 -7 4 157.301 37.4990 2 1 -7 -4 138.084 40.6473 3 1 -7 -3 1227.73 61.8609 2 -1 7 3 1316.61 89.1171 3 1 -7 -3 1342.89 83.4841 3 1 7 -3 1374.58 90.1405 2 1 7 -2 6741.13 183.534 2 -1 7 2 6672.38 164.823 3 1 -7 -2 6414.71 148.996 2 1 -7 -2 6356.33 148.562 3 1 7 -1 2175.73 104.104 2 -1 7 1 2094.86 78.2152 3 1 -7 -1 2091.80 93.1444 2 1 7 0 12901.9 231.235 2 -1 -7 0 14168.1 260.797 3 -1 7 0 13194.7 230.264 2 -1 7 -1 5295.31 157.999 2 -1 -7 -1 5120.27 145.930 2 1 7 1 5272.68 141.317 2 1 7 2 673.238 52.7365 2 -1 7 -2 642.465 64.3486 2 -1 -7 -2 418.694 87.4782 3 -1 -7 -2 623.764 50.8460 2 -1 7 -3 372.583 51.1702 2 -1 -7 -3 305.451 33.7293 2 1 7 3 330.401 36.2328 2 -1 -7 -3 351.546 56.8704 3 1 -7 3 376.461 50.2075 2 -1 -7 -4 6718.14 126.756 2 -1 7 -4 8082.60 209.396 2 1 7 4 7621.58 132.040 2 1 -7 4 8082.74 230.214 2 -1 -7 -4 7911.02 238.110 3 -1 -7 -5 158.668 54.2562 3 1 -7 5 139.703 39.8887 2 -1 -7 -6 103.513 52.1108 3 -1 7 -6 60.9316 49.6165 3 1 -7 6 60.0780 30.4730 2 -1 7 -7 193.018 67.9891 3 -1 -7 -7 133.526 55.5947 3 -1 -7 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747.636 119.764 3 -2 4 -9 701.533 112.914 3 -2 -4 -10 754.678 123.024 3 -2 4 -10 923.098 137.848 3 -2 -4 -11-10.0712 53.0394 3 -2 4 -11 7.83318 48.6848 3 2 5 -12 28.0560 62.6672 3 2 -5 -12 77.5805 75.4642 3 2 5 -11 952.939 155.422 3 2 -5 -11 944.629 141.828 3 2 5 -10 12.0982 65.3354 3 -2 5 10 49.1133 73.3929 1 2 -5 -10 29.5754 55.7215 3 2 5 -9 1823.11 111.628 2 -2 5 9 1894.27 198.330 1 2 5 -9 1850.78 190.504 3 2 -5 -9 1987.17 175.718 3 -2 5 8 372.008 96.9424 1 2 5 -8 376.724 55.2271 2 -2 -5 8 356.711 59.0369 2 2 -5 -8 394.461 87.7616 3 -2 5 7 569.345 103.423 1 2 -5 -7 621.515 36.6977 2 2 5 -7 622.828 69.1318 2 2 -5 -7 566.879 90.9052 3 -2 -5 7 536.927 68.8652 2 2 -5 -6 627.236 44.6694 2 -2 5 6 652.193 98.6417 1 2 5 -6 634.178 80.5396 1 -2 -5 6 684.135 74.7337 2 2 5 -6 739.956 73.6589 2 2 -5 -6 664.209 83.7772 3 2 -5 -5 5966.03 139.418 2 -2 -5 5 5862.33 202.069 2 2 5 -5 6037.61 187.250 2 2 -5 -5 5936.83 211.281 3 -2 -5 4 466.044 59.4248 2 2 5 -4 489.212 56.8463 2 2 -5 -4 489.423 60.6767 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5 -8 813.167 113.450 3 -2 -5 -8 725.894 108.767 3 2 5 9 806.798 128.762 1 -2 -5 -9 789.122 118.711 3 -2 5 -9 683.795 114.296 3 -2 5 -10 43.0996 56.0626 3 -2 -5 -10 42.9993 51.3337 3 -2 -5 -11 129.670 65.7610 3 -2 5 -11 138.126 74.8679 3 2 -6 -12 0.76525 62.7236 3 2 6 -12-2.62125 62.4178 3 2 6 -11-36.0472 69.5976 3 2 -6 -11-2.14607 50.1761 3 2 6 -10 1992.69 209.800 3 2 -6 -10 1925.60 184.402 3 -2 6 10 2114.98 227.153 1 2 -6 -9-16.3967 50.3294 3 -2 6 9-7.64738 63.6098 1 2 6 -9 10.1511 25.5660 2 -2 6 8 1641.37 175.614 1 2 6 -8 1574.46 110.017 2 2 -6 -8 1399.76 137.579 3 2 -6 -7 119.934 17.0156 2 2 -6 -7 116.801 52.2596 3 -2 6 7 158.480 75.9180 1 2 -6 -7 132.711 18.5548 2 -2 -6 7 124.987 38.4320 2 2 6 -7 103.683 36.2341 2 2 -6 -6 2239.16 83.2863 2 -2 -6 6 2313.31 138.926 2 2 6 -6 2241.70 148.555 1 2 6 -6 2540.03 133.565 2 -2 6 6 2599.70 191.136 1 2 -6 -6 2510.49 152.820 3 -2 -6 5 330.744 53.6357 2 2 6 -5 331.879 52.2898 2 2 -6 -5 367.318 59.4215 3 -2 -6 4 1149.29 92.9000 2 2 -6 -4 1114.07 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409.777 54.6406 3 -2 7 3 2242.82 109.631 3 2 -7 -3 2447.38 103.570 3 2 7 -3 2458.06 122.117 2 2 -7 -2 1347.20 62.8229 3 2 7 -2 1454.28 95.2525 2 -2 7 2 1415.89 70.3450 3 2 7 -1 19878.1 321.772 2 -2 7 1 19158.8 185.769 3 -2 -7 0 321.521 66.7121 3 -2 7 0 255.940 41.5970 1 2 7 0 237.903 46.3976 2 -2 -7 0 253.349 43.2948 2 -2 -7 -1 3986.88 144.967 2 -2 7 -1 4408.87 112.927 1 2 7 1 3927.39 138.529 2 -2 -7 -2 194.450 35.4735 2 2 7 2 199.114 37.6199 2 -2 -7 -2-52.9855 112.901 3 2 7 3 413.509 45.0949 2 -2 -7 -3 360.241 42.4477 2 2 -7 3 439.182 55.8090 2 -2 -7 -3 450.824 84.3325 3 -2 7 -3 416.666 57.6386 3 -2 7 -4 3329.32 158.150 3 2 -7 4 3298.01 150.788 2 2 7 4 3357.99 112.672 2 -2 -7 -4 3412.59 167.167 3 2 7 5 4402.21 114.806 2 -2 -7 -5 5077.76 215.638 3 -2 7 -5 5337.44 220.896 3 -2 -7 -6 523.606 83.1942 3 -2 7 -6 526.630 84.1118 3 -2 7 -7 75.0277 53.8667 3 -2 -7 -7 75.5661 56.5570 3 -2 7 -8 343.597 82.7266 3 -2 -7 -8 350.939 78.4822 3 -2 7 -9 1539.44 164.584 3 -2 -7 -9 1738.57 169.084 3 2 7 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2 -2 8 3 39.8376 26.2163 3 2 -8 -3 24.5174 23.9871 3 2 -8 -2 2328.52 84.4201 3 2 -8 -2 2203.54 101.948 2 2 8 -2 2246.95 118.075 2 -2 8 2 2094.90 88.2710 3 -2 8 1 89.7987 20.9614 3 2 8 -1 146.390 45.3860 2 2 -8 -1-36.6296 42.1907 3 -2 8 1 124.792 46.7881 1 -2 8 0 10268.7 214.178 1 -2 -8 0 10949.5 253.868 2 2 8 0 10535.2 236.215 2 -2 -8 0 11180.7 266.975 3 2 8 1 3749.60 138.922 2 -2 -8 -1 3706.72 147.582 2 -2 -8 -2 1240.16 83.0496 2 2 8 2 1257.20 79.8868 2 2 8 3 11.3691 23.2293 2 -2 -8 -3 13.7943 88.9933 3 -2 -8 -3 8.58383 18.5067 2 2 -8 3 6.05054 20.2050 2 -2 -8 -4 6287.76 238.357 3 -2 8 -4 4539.14 192.960 3 2 8 4 5819.57 153.040 2 -2 -8 -4 5457.50 149.732 2 -2 8 -5 185.413 61.3172 3 -2 -8 -5 190.127 59.8390 3 2 8 5 220.225 30.5873 2 -2 8 -6 5569.83 248.904 3 2 8 6 4981.28 85.6808 2 -2 -8 -6 4988.12 234.394 3 -2 8 -7 20.2980 46.4605 3 -2 -8 -7 36.9362 48.3086 3 -2 8 -8 6.03704 48.7609 3 -2 -8 -8 9.98068 50.0902 3 -2 8 -9-0.09956 50.8822 3 -2 -8 -9-18.1556 47.5648 3 -2 -8 -10 1306.43 158.215 3 2 8 10 1458.66 189.584 1 -2 8 -10 1380.96 167.549 3 -2 8 -11 248.749 86.5886 3 2 9 -12 140.776 85.0393 3 -2 9 12 269.417 120.671 1 2 -9 -12 279.615 91.1874 3 -2 9 11 910.930 170.861 1 2 9 -11 1220.80 180.915 3 2 -9 -11 1164.21 153.892 3 2 -9 -10 130.209 65.2150 3 -2 9 10 163.000 95.7520 1 -2 9 9 1237.43 170.252 1 2 9 -9 1117.72 104.521 2 2 -9 -9 1244.62 141.869 3 2 -9 -8 300.647 73.1050 3 2 9 -8 265.599 56.9928 2 -2 9 8 230.564 88.5390 1 2 -9 -7 290.176 66.0679 3 2 -9 -7 293.223 31.4226 2 2 -9 -7 318.467 30.2689 2 2 9 -7 344.389 63.4453 2 -2 9 7 280.053 87.9756 1 2 -9 -6 2459.36 93.5386 2 2 9 -6 2762.70 155.518 2 -2 9 6 2961.43 210.005 1 2 -9 -6 2707.54 159.003 3 2 9 -5 2924.93 152.964 2 2 -9 -5 2830.58 108.357 2 2 -9 -5 2791.81 145.325 3 2 9 -4 146.387 48.1319 2 2 -9 -4 108.241 29.3373 2 -2 9 4 90.2555 37.8343 3 2 -9 -4 129.935 39.6548 3 2 -9 -3 2127.63 98.9421 3 2 9 -3 2104.71 124.627 2 2 -9 -3 2236.81 105.687 2 -2 9 3 2244.24 111.628 3 2 -9 -2 412.322 50.5036 2 2 -9 -2 460.260 55.0119 3 -2 9 2 402.885 42.7480 3 2 9 -2 380.493 61.2916 2 2 -9 -1 11705.2 236.396 3 2 9 -1 13286.9 282.609 2 -2 9 1 13772.0 186.660 3 -2 9 1 12422.4 276.213 1 -2 -9 0 1273.43 95.1158 2 -2 9 0 1689.44 111.280 3 -2 -9 0 1367.79 102.422 3 2 9 0 1188.34 88.8824 2 -2 9 0 1221.65 82.0235 1 -2 -9 -1 831.251 76.3528 2 2 9 1 897.815 75.4234 2 -2 9 -1 928.208 60.5148 1 2 9 2 392.914 51.4642 2 -2 -9 -2 309.867 46.4885 2 -2 -9 -3 2907.60 124.068 2 2 9 3 2830.15 117.606 2 -2 -9 -4 1969.23 155.315 3 2 9 4 2013.91 97.9032 2 -2 -9 -4 1986.23 96.4360 2 -2 9 -5 5668.14 237.250 3 -2 -9 -5 5793.60 244.077 3 2 9 5 5691.78 144.972 2 -2 9 -6 496.045 84.7033 3 2 9 6 439.717 30.2931 2 -2 -9 -6 429.233 83.6952 3 -2 9 -7 21.4934 46.3231 3 -2 -9 -7 25.3859 45.9486 3 -2 9 -8 426.571 89.9745 3 -2 -9 -8 498.778 94.8500 3 -2 -9 -9 763.396 118.704 3 -2 9 -9 771.412 123.073 3 -2 9 -10 243.412 82.0375 3 -2 -9 -10 284.875 83.6548 3 2 9 10 294.295 106.635 1 -2 9 -11 513.278 111.414 3 -2 10 12 292.665 116.262 1 2 10 -11 926.670 165.112 3 2 -10 -11 1107.87 148.672 3 -2 10 11 897.787 172.585 1 2 -10 -10 2368.48 202.962 3 -2 10 10 2382.51 249.877 1 2 10 -10 2114.81 148.516 2 2 10 -9 1680.53 129.368 2 2 -10 -9 1590.41 158.863 3 -2 10 9 1664.28 205.761 1 2 -10 -8 285.688 70.8135 3 -2 10 8 238.123 86.4642 1 2 10 -8 262.834 58.0235 2 -2 10 7 35.7421 67.8010 1 2 -10 -7 54.3602 19.7769 2 2 -10 -7 27.3524 14.5457 2 2 -10 -7 9.60257 37.6749 3 2 10 -7 16.6957 38.2879 2 -2 10 6 3236.32 224.761 1 2 -10 -6 3153.47 112.896 2 2 10 -6 3191.53 171.664 2 2 -10 -6 3112.94 171.172 3 2 10 -5 900.376 92.5057 2 2 -10 -5 870.028 63.9003 2 2 -10 -5 875.124 84.7752 3 2 -10 -4 3295.97 128.975 2 2 10 -4 3317.06 165.395 2 2 -10 -4 3055.91 135.197 3 -2 10 4 3160.69 154.774 3 -2 10 3 34.3658 25.3917 3 2 -10 -3 32.6517 23.1888 2 2 -10 -3 49.7716 28.0008 3 2 10 -3 12.9596 38.0050 2 2 10 -2 78.9457 41.0030 2 2 -10 -2-14.4384 64.3496 3 2 -10 -2 81.9024 30.6954 2 -2 10 2 38.9484 23.0237 3 2 10 -1 4845.34 181.432 2 2 -10 -1 4863.61 176.172 2 2 -10 -1 4959.74 139.634 3 -2 10 1 4828.34 121.474 3 -2 -10 0 4697.27 183.740 3 2 10 0 4098.31 160.832 2 -2 -10 0 4361.61 175.805 2 2 10 1 66.7732 35.5706 2 -2 -10 -1 185.248 286.705 3 -2 10 -1 113.099 30.8705 1 -2 -10 -1 108.772 35.3390 2 -2 -10 -2 477.263 59.0247 2 2 10 2 508.188 59.0183 2 -2 10 -2 696.560 45.0079 1 -2 -10 -3 1222.54 86.5061 2 2 10 3 1195.32 83.6757 2 -2 -10 -4 1412.59 166.952 3 2 10 4 2310.88 109.297 2 -2 -10 -4 2165.07 107.349 2 -2 10 -5 181.703 59.8607 3 2 10 5 202.590 34.0750 2 -2 -10 -5 268.406 68.2805 3 -2 10 -6 2246.58 165.364 3 2 10 6 2225.22 72.3075 2 -2 -10 -6 2192.33 162.074 3 -2 -10 -7 48.0297 50.3764 3 -2 10 -7-38.3602 49.6357 3 -2 10 -8 801.830 119.263 3 -2 -10 -8 707.402 108.732 3 -2 -10 -9 348.697 92.6287 3 -2 10 -9 297.528 85.0031 3 2 10 10 669.261 144.142 1 -2 -10 -10 576.693 114.443 3 -2 10 -10 545.761 113.825 3 -2 10 -11 204.270 79.7726 3 -2 11 12 50.1038 78.9694 1 2 11 -11-0.15187 72.0141 3 -2 11 11 26.8750 80.5170 1 2 -11 -11 19.5644 49.8206 3 2 11 -10 184.907 53.9694 2 -2 11 10 217.569 108.990 1 2 -11 -10 280.858 80.2515 3 2 11 -9 1416.30 124.735 2 -2 11 9 1497.88 197.583 1 2 -11 -9 1416.58 148.748 3 2 11 -8 216.993 55.2589 2 -2 11 8 154.780 87.9531 1 2 -11 -8 189.184 62.1305 3 2 11 -7 2635.94 164.787 2 -2 11 7 2987.74 235.879 1 2 -11 -7 2451.65 96.1922 2 2 -11 -7 2562.90 168.855 3 2 -11 -6 1682.52 89.3454 2 2 -11 -6 1778.81 131.761 3 2 11 -6 2008.08 142.810 2 -2 11 6 1993.82 186.710 1 2 -11 -5 2238.55 106.061 2 2 11 -5 2310.50 148.313 2 2 -11 -5 2238.70 130.969 3 -2 11 4 1125.53 96.6802 3 2 -11 -4 1025.34 82.2673 3 2 -11 -4 1034.00 76.9962 2 2 11 -4 1000.86 97.8149 2 2 -11 -3 1390.44 91.1587 2 2 11 -3 1255.91 106.284 2 2 -11 -3 1614.70 97.3548 3 -2 11 3 1303.10 90.9315 3 2 -11 -2 1126.24 84.8093 2 2 11 -2 1145.03 99.1299 2 -2 11 2 1035.92 71.9163 3 2 -11 -1 5828.03 199.559 2 -2 11 1 7235.91 159.955 3 2 11 -1 5610.02 201.092 2 -2 -11 0 816.999 83.9870 2 2 11 0 864.002 83.0815 2 -2 -11 -1 2075.50 125.394 2 2 11 1 2035.18 117.912 2 -2 -11 -1 2087.56 230.311 3 -2 11 -2 2165.81 82.1398 1 -2 -11 -2 2464.44 131.677 2 2 11 2 2366.14 123.346 2 -2 -11 -3 3592.05 152.499 2 2 11 3 3724.04 150.181 2 2 11 4 4566.32 158.181 2 -2 -11 -4 4131.48 154.908 2 2 11 5 2725.14 113.738 2 -2 -11 -5 2474.98 201.367 3 -2 -11 -5 2362.13 105.915 2 -2 11 -6 40.9707 45.5160 3 2 11 6 61.7463 18.2273 2 -2 -11 -6 38.7276 58.3993 3 -2 11 -7 6.96042 47.1071 3 -2 -11 -7 36.0474 59.0594 3 -2 11 -8 54.9889 54.6923 3 -2 -11 -8 175.357 69.1785 3 -2 -11 -9 916.014 133.184 3 -2 11 -9 862.286 131.532 3 2 11 10 122.302 80.9621 1 -2 -11 -10 183.939 68.4155 3 -2 11 -10 127.496 66.4324 3 -2 11 -11 247.890 86.0157 3 -2 12 12 646.703 160.212 1 -2 12 11 487.894 138.259 1 2 12 -11 319.817 115.812 3 2 -12 -11 423.959 97.8617 3 -2 12 10 211.632 104.554 1 2 12 -10 136.452 49.3668 2 2 -12 -10 170.678 63.9992 3 2 -12 -9 1278.38 139.634 3 2 12 -9 1292.86 121.935 2 -2 12 9 1438.31 197.872 1 -2 12 8 345.310 107.938 1 2 -12 -8 241.239 67.6789 3 2 12 -8 227.638 58.7535 2 2 12 -7 420.836 76.1254 2 2 -12 -7 355.798 41.2549 2 -2 12 7 489.023 114.061 1 2 -12 -7 326.875 69.9291 3 2 -12 -6 2166.55 107.470 2 2 12 -6 2404.97 157.228 2 -2 12 6 2349.93 200.953 1 2 -12 -6 2069.45 139.495 3 2 -12 -5 702.505 64.6264 2 2 12 -5 847.946 96.9530 2 -2 12 5 629.159 105.271 1 2 -12 -5 700.771 76.5866 3 2 -12 -4 4553.44 171.176 3 2 -12 -4 4305.71 160.343 2 2 12 -4 4639.22 205.792 2 -2 12 4 4321.38 187.507 3 2 -12 -3 1850.30 108.070 2 2 12 -3 1741.57 126.480 2 -2 12 3 1879.83 111.031 3 -2 12 2 13.5529 22.0152 3 2 -12 -2 58.5250 28.8678 2 2 -12 -2-32.5542 46.3307 3 2 12 -2 86.4740 48.7904 2 2 12 -1 3804.27 174.033 2 -2 12 1 3833.47 124.327 3 2 -12 -1 4148.60 125.794 3 2 12 0 8950.36 255.965 2 -2 -12 0 10578.7 288.885 3 -2 -12 0 9097.77 272.789 2 -2 -12 -1 75.6136 34.3324 2 2 12 1 105.526 40.3592 2 2 12 2 7091.68 220.215 2 -2 12 -2 5290.64 139.130 1 -2 -12 -2 6689.40 223.754 2 -2 -12 -3 653.774 71.6317 2 2 12 3 698.054 72.8065 2 2 12 4 107.577 33.4115 2 -2 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13 -6 2637.94 169.944 2 2 13 -5 155.849 53.7460 2 2 -13 -5 150.149 35.1849 2 2 -13 -5 174.164 46.6535 3 -2 13 5 170.557 71.2576 1 2 13 -4 70.8413 47.9473 2 2 -13 -4 178.467 45.2728 3 2 -13 -4 61.1104 29.9501 2 2 -13 -3 858.443 80.5021 2 2 13 -3 934.725 98.8710 2 -2 13 3 954.129 83.6879 3 2 13 -2 78.8312 43.8060 2 -2 13 2 103.860 31.4116 3 2 13 -1 353.416 64.8356 2 -2 13 1 690.667 50.4414 3 -2 13 0 13328.3 423.890 3 2 13 0 52.9347 42.4966 2 -2 13 -1-21.4678 36.4185 3 2 13 1 59.9796 38.3165 2 2 13 2 47.0019 37.5901 2 -2 -13 -2 36.3171 29.2534 2 -2 -13 -3 4172.34 180.858 2 2 13 3 4531.15 176.918 2 -2 13 -3 4462.50 104.686 1 -2 -13 -4 3500.87 157.997 2 2 13 4 3830.14 158.155 2 -2 -13 -5 987.497 79.6530 2 2 13 5 1259.59 86.7172 2 -2 13 -6 159.569 60.0209 3 2 13 6 183.805 31.6182 2 -2 -13 -6 49.5338 78.6358 3 -2 13 -7 1200.09 136.206 3 -2 -13 -7 1126.21 159.703 3 -2 13 -8 82.4656 58.6818 3 -2 -13 -8 141.564 72.7633 3 -2 13 -9 234.338 79.0569 3 -2 -13 -9 275.870 89.5060 3 2 13 10 27.4041 71.9444 1 -2 -13 -10 7.66380 52.5730 3 -2 13 -10 17.6626 50.3801 3 -2 13 -11 62.7000 56.1136 3 2 13 11 8.99118 64.0424 1 -2 14 11 84.6463 89.5830 1 2 -14 -11 44.6023 49.6802 3 2 14 -10 20.2244 37.4581 2 -2 14 10 64.8098 82.9963 1 2 -14 -10 76.8999 53.4790 3 -2 14 9 36.7051 73.7411 1 2 14 -9 2.22444 32.8799 2 2 -14 -9-21.6580 46.9758 3 2 14 -8 237.417 62.7059 2 2 -14 -8 262.425 67.5452 3 -2 14 8 231.252 97.5437 1 2 -14 -7-20.6714 37.4533 3 2 14 -7 16.3998 38.6454 2 -2 14 7 18.2541 62.9710 1 -2 14 6 496.730 105.920 1 2 14 -6 547.546 86.3181 2 2 -14 -6 512.495 74.9230 3 2 -14 -6 451.069 56.3225 2 2 -14 -5 414.359 64.9697 3 2 14 -5 312.225 68.0911 2 2 -14 -5 306.744 49.2821 2 -2 14 5 408.726 95.0672 1 2 -14 -4 120.175 35.0001 2 2 -14 -4 63.5903 50.9716 3 2 14 -4 103.759 52.2181 2 -2 14 3 501.583 64.3109 3 2 14 -3 490.627 79.4587 2 2 14 -2 1341.56 116.957 2 -2 14 2 1295.43 90.7119 3 -2 14 1 713.725 62.9491 3 2 14 -1 670.212 85.0335 2 -2 14 0 2531.96 197.852 3 2 14 0 2313.83 144.903 2 2 14 1 725.724 82.4529 2 -2 -14 -1 787.735 114.357 3 2 14 2 8655.71 259.444 2 -2 -14 -2 3249.60 307.220 3 -2 -14 -3 374.607 59.7803 2 2 14 3 409.053 62.4635 2 -2 -14 -3 80.1508 98.3245 3 -2 14 -3 309.760 33.5642 1 -2 -14 -4 472.551 62.0908 2 2 14 4 638.800 71.3989 2 2 14 5 545.921 61.0378 2 -2 -14 -5 379.459 53.6415 2 2 14 6 723.043 60.7592 2 -2 -14 -6 137.211 101.277 3 -2 -14 -7 33.8490 104.723 3 -2 14 -7 125.103 59.2893 3 -2 -14 -8 787.085 151.226 3 -2 14 -8 991.439 134.800 3 -2 14 -9 129.968 67.4779 3 -2 -14 -9 226.619 91.7965 3 -2 14 -10-32.8809 51.5104 3 -2 14 -11 218.195 84.2274 3 2 14 11 374.020 131.543 1 2 -15 -11 11.5024 44.9232 3 -2 15 11 88.4984 91.1343 1 -2 15 10 236.162 110.726 1 2 15 -10 272.646 68.9552 2 2 -15 -10 257.694 71.1481 3 2 15 -9 98.6459 49.0148 2 -2 15 9 152.913 88.5321 1 2 -15 -9 128.234 59.1488 3 2 -15 -8 59.6971 45.9591 3 2 15 -8 85.2873 51.4905 2 -2 15 8 8.37833 66.6624 1 2 -15 -7 1875.10 148.461 3 2 15 -7 1941.62 156.852 2 -2 15 7 2010.67 214.946 1 2 15 -6 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72.3393 55.2320 2 2 30 0 14.1637 47.6225 2 2 30 1-25.0364 50.8744 2 2 30 2 1063.24 144.916 2 2 30 3 230.416 75.4093 2 2 31 -1 159.814 72.1982 2 2 31 0 31.2333 54.2567 2 2 31 1 293.119 86.8939 2 2 31 2 52.4019 48.6856 2 2 31 3 456.949 101.155 2 2 32 1 617.751 119.805 2 2 32 2 369.515 95.8452 2 3 0 -12 82.3218 67.6683 3 3 0 -11 2225.59 215.813 3 3 0 -10-29.7840 56.0692 3 3 0 -9 1926.45 183.575 3 3 0 -9 1483.96 90.7123 2 3 0 -8 5.15199 56.8658 3 3 0 -8 7.98126 21.5658 2 3 0 -7 96.6763 34.5109 2 3 0 -6-2.67442 22.3793 2 3 0 -5 159.709 42.4575 2 3 0 -4-0.45926 24.6164 2 3 0 -4 7.03588 26.8402 1 3 0 -3 155.516 40.9849 2 3 0 -2 8.49256 33.0481 2 3 0 -1 20747.8 320.472 2 3 0 -1 22452.3 275.092 3 -3 0 0-41.2184 47.1661 3 3 0 1 3061.50 112.119 3 -3 0 -1 231.663 74.9750 3 3 0 2 1.85167 22.4859 3 -3 0 -2 7.18088 28.7848 3 3 0 3 16225.3 339.677 3 -3 0 -3 15630.3 300.095 3 -3 0 -4-6.06872 35.6319 3 -3 0 -5 602.320 80.9236 3 -3 0 -6 5.09074 40.1475 3 3 0 6-7.46275 17.0190 2 3 0 7 1451.84 95.9763 2 -3 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929.851 111.614 2 4 -11 -8 822.060 105.016 3 4 -11 -8 924.284 84.0008 2 4 -11 -7 257.758 59.7476 3 -4 11 7 258.619 90.5659 1 4 11 -7 191.686 61.1038 2 -4 11 6 3917.16 261.053 1 4 11 -6 3852.13 208.347 2 4 -11 -6 3958.05 182.015 3 4 11 -5 384.295 72.6222 2 -4 11 5 259.689 82.3636 1 4 -11 -5 378.930 54.0119 3 4 11 -4 131.642 57.5419 2 -4 11 4 105.598 66.2590 1 4 -11 -4 136.742 33.6071 3 -4 11 3 239.852 67.6818 1 4 11 -3 338.186 68.7127 2 4 -11 -3 430.883 40.4897 3 4 11 -2 148.237 54.2660 2 4 -11 -2 104.951 22.4155 3 4 11 -1 1568.28 124.819 2 -4 -11 0-159.037 65.8253 3 4 11 0 13.4487 37.8217 2 -4 11 -1 4293.64 74.8197 3 4 11 1 4768.97 209.477 2 -4 11 -2 520.744 44.9353 3 4 11 2 559.061 75.6314 2 -4 -11 -3 565.723 174.941 3 4 11 3 1151.36 103.448 2 -4 11 -3 1117.33 77.4548 3 -4 -11 -4 131.069 141.094 3 4 11 4 449.086 66.3729 2 -4 11 -4 483.644 61.3036 3 -4 11 -5 177.803 49.4929 3 4 11 5 134.839 40.2189 2 -4 -11 -5-34.9422 127.038 3 -4 11 -6 284.649 62.8947 3 -4 -11 -7 53.8045 119.111 3 -4 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229.213 2 -4 12 -1 60.9988 13.3270 3 4 12 1 93.9114 45.4777 2 4 12 2 736.980 87.8540 2 -4 12 -2 712.889 53.4833 3 -4 -12 -3 1037.46 244.513 3 4 12 3 989.694 96.6598 2 -4 12 -3 837.937 69.0299 3 -4 -12 -4 313.419 200.268 3 4 12 4 789.188 87.7266 2 -4 12 -4 764.424 78.4269 3 4 12 5 73.7679 33.7703 2 -4 12 -5 52.5949 34.5358 3 -4 -12 -5-30.9542 142.251 3 -4 -12 -6-81.2785 155.215 3 -4 12 -6 1062.85 108.666 3 -4 12 -7 47.6796 41.0465 3 -4 12 -8 33.4235 43.9275 3 -4 -12 -8-66.1865 150.109 3 4 -13 -12-30.7056 41.4975 3 -4 13 11 962.495 197.886 1 4 -13 -11 823.250 123.261 3 -4 13 10 103.597 91.1865 1 4 13 -10 177.479 59.4859 2 4 -13 -10 146.275 60.6849 3 -4 13 9 1374.90 200.876 1 4 13 -9 1273.31 137.985 2 4 -13 -9 1355.64 137.785 3 -4 13 8 225.903 99.3106 1 4 -13 -8 202.785 44.7718 2 4 13 -8 154.015 62.4031 2 4 -13 -8 121.870 49.7220 3 -4 13 7 1139.90 162.116 1 4 13 -7 1176.48 126.599 2 4 -13 -7 1092.20 105.564 3 -4 13 6 2121.89 204.150 1 4 13 -6 2251.10 169.456 2 4 -13 -6 2264.36 135.892 3 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51.9276 74.3859 1 4 14 -9 119.100 56.0944 2 4 -14 -9 140.471 53.5801 3 4 14 -8 112.455 54.1088 2 -4 14 8 70.5002 81.0654 1 4 -14 -8 113.177 45.4552 3 -4 14 7 1067.88 163.929 1 4 14 -7 1008.71 122.811 2 4 -14 -7 1059.64 104.630 3 -4 14 6 2007.64 199.399 1 4 14 -6 2003.81 163.198 2 4 -14 -6 1977.41 127.364 3 4 14 -5 11.3592 45.0767 2 -4 14 5 59.1111 67.5469 1 4 -14 -5 71.4838 31.0896 3 4 -14 -4 1576.05 127.919 3 4 14 -4 2137.30 161.798 2 -4 14 3 838.779 114.052 1 4 14 -3 812.853 101.650 2 -4 14 2 437.004 80.1543 1 4 14 -2 494.596 82.8405 2 4 14 -1 92.2270 53.6437 2 -4 14 0 2892.64 165.151 1 4 14 0 2926.82 176.057 2 -4 14 -1 212.984 24.3605 3 4 14 1 241.217 59.8681 2 -4 -14 -1 393.391 93.6047 3 -4 14 -2 440.402 43.6669 3 4 14 2 435.230 72.4297 2 -4 14 -3 348.528 48.0254 3 4 14 3 371.435 67.5868 2 -4 -14 -3 566.833 285.002 3 4 14 4 5179.09 221.383 2 -4 14 -4 5259.88 195.492 3 -4 14 -5 121.044 44.3193 3 -4 -14 -5 281.860 168.723 3 4 14 5 128.534 45.9942 2 -4 -14 -6-31.9950 106.359 3 -4 14 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-4 15 0 310.204 21.5008 3 -4 15 -1 3811.94 166.777 3 -4 -15 -1 4359.81 228.861 3 4 15 1 3735.20 199.240 2 4 15 2 552.229 81.8059 2 -4 15 -2 506.025 49.4590 3 4 15 3 26.3261 37.8361 2 -4 15 -3 11.8561 24.1756 3 -4 15 -4 577.370 69.6083 3 4 15 4 693.994 87.2594 2 -4 -15 -4 803.285 241.233 3 4 15 5 1873.65 134.697 2 -4 15 -5 1771.59 128.813 3 -4 15 -6 49.0451 41.5397 3 -4 -15 -6 85.5320 119.974 3 -4 -15 -7-49.7025 128.321 3 -4 -15 -8-90.6793 151.324 3 4 -16 -11 528.762 100.865 3 -4 16 10 1332.04 216.156 1 4 16 -10 1186.53 143.014 2 4 -16 -10 1185.27 137.303 3 -4 16 9-13.6918 78.0200 1 4 16 -9 6.10360 46.8099 2 4 -16 -9 16.2391 35.3140 3 4 16 -8 261.715 76.3428 2 4 -16 -8 260.266 62.6330 3 -4 16 8 331.112 113.881 1 4 16 -7 360.509 84.5420 2 4 -16 -7 339.936 63.1956 3 -4 16 7 397.668 112.835 1 -4 16 6-14.4576 64.2797 1 4 16 -6 15.8241 51.6393 2 4 -16 -6 119.333 38.8422 3 -4 16 5 51.6895 63.5051 1 4 -16 -5 12.4188 48.4574 3 4 16 -5 39.6526 48.5578 2 -4 16 4 3183.22 233.760 1 -4 16 4 2689.21 146.088 3 4 16 -4 3111.66 202.469 2 4 16 -3 438.058 85.0906 2 -4 16 3 382.241 49.6710 3 -4 16 3 445.980 92.2753 1 4 -16 -3 341.927 71.3557 3 4 16 -2 140.086 58.0205 2 -4 16 2 116.994 26.4300 3 -4 16 2 84.3990 56.7154 1 4 16 -1 1861.49 151.185 2 -4 16 1 1764.88 66.0306 3 4 16 0 1710.54 146.974 2 -4 16 0 1515.74 54.9333 3 -4 -16 -1 618.731 113.054 3 4 16 1 513.651 83.3779 2 4 16 2 1062.90 112.942 2 -4 16 -2 1058.21 70.9066 3 -4 16 -3 444.692 56.6928 3 4 16 3 509.635 81.2740 2 -4 16 -4 1514.50 108.881 3 4 16 4 1593.31 131.827 2 -4 16 -5 76.7767 38.8478 3 4 16 5 45.5047 34.6214 2 -4 -16 -6 113.888 131.783 3 -4 -16 -7-43.3958 107.368 3 -4 -16 -8 65.6032 119.862 3 4 -17 -11 99.8514 52.8046 3 -4 17 10-40.8461 75.9369 1 4 17 -10 9.79793 42.6059 2 4 -17 -10 18.4251 32.2333 3 -4 17 9 87.1238 84.5172 1 4 17 -9 9.62086 42.9293 2 4 -17 -9 40.0824 36.4386 3 4 17 -8-0.09290 50.6793 2 -4 17 8 72.5261 83.4996 1 4 -17 -8 63.2556 40.0188 3 -4 17 7 129.542 95.1057 1 4 17 -7 149.206 63.0359 2 4 -17 -7 179.367 50.3811 3 -4 17 6 137.960 82.1723 1 4 17 -6 167.921 63.9382 2 4 -17 -6 187.289 52.8828 3 -4 17 5 173.860 79.9072 1 4 17 -5 226.321 73.9131 2 -4 17 4 860.065 133.245 1 -4 17 4 632.458 73.5977 3 4 17 -4 737.503 108.848 2 -4 17 3 90.3330 33.2492 3 -4 17 3 112.927 65.1955 1 4 -17 -3 121.284 40.2598 3 4 17 -3 100.959 60.5509 2 -4 17 2 1346.58 77.5647 3 -4 17 2 1455.33 146.132 1 4 17 -2 1431.78 139.717 2 4 17 -1-3.54615 44.8372 2 -4 17 1 11.9684 15.7252 3 -4 17 1 28.0155 43.0226 1 4 17 0 365.320 77.4397 2 -4 17 0 220.321 26.3373 3 -4 -17 -1 83.1222 80.1664 3 4 17 1 225.256 66.2991 2 -4 -17 -2 1777.49 195.345 3 4 17 2 892.669 107.344 2 -4 17 -3 106.609 34.6409 3 4 17 3 112.682 49.5861 2 -4 17 -4 40.5023 33.8829 3 4 17 4 27.7022 38.3250 2 -4 -17 -5 326.081 164.977 3 -4 -17 -6 316.588 192.497 3 -4 -17 -7 108.288 141.513 3 4 -18 -11 270.052 70.7222 3 -4 18 10-1.35981 76.7468 1 4 18 -10 3.94267 39.1335 2 4 -18 -10 87.6467 45.4420 3 -4 18 9 869.700 175.372 1 4 18 -9 692.701 117.905 2 4 -18 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19 -10 173.932 67.5191 2 4 -19 -10 296.727 70.8045 3 4 19 -9 41.4073 51.3677 2 4 -19 -9 141.353 54.8843 3 -4 19 9 131.359 102.635 1 4 19 -8 614.818 111.874 2 4 -19 -8 638.025 100.882 3 -4 19 8 760.701 159.590 1 -4 19 7 1130.20 180.164 1 4 19 -7 1116.36 141.855 2 4 -19 -7 541.210 112.474 3 -4 19 6 781.218 149.139 1 4 19 -6 825.466 123.533 2 -4 19 5 104.614 77.1320 1 4 -19 -5-66.6399 45.2059 3 4 19 -5 137.823 64.4875 2 4 19 -4 2686.80 202.103 2 -4 19 4 3011.53 242.110 1 4 -19 -3 1722.02 95.5428 3 4 19 -3 1609.62 155.973 2 -4 19 3 1794.28 179.353 1 -4 19 2 486.361 98.4347 1 4 19 -2 529.378 97.5576 2 -4 19 1 3145.08 206.667 1 4 19 -1 3060.19 205.934 2 4 19 0 1047.10 125.629 2 -4 19 -1 1166.25 109.055 1 4 19 1 1049.12 124.299 2 -4 -19 -2 839.018 138.438 3 4 19 2 101.579 52.1357 2 4 19 3 1688.84 148.316 2 -4 -19 -3 4736.85 347.362 3 -4 -19 -4 1758.11 341.760 3 4 19 4 232.681 65.5261 2 -4 -19 -5 478.668 280.141 3 -4 -19 -6 215.592 160.871 3 -4 -19 -7 912.951 228.971 3 4 20 -10 175.664 67.7855 2 4 -20 -10 308.141 78.9457 3 4 20 -9 721.319 121.154 2 4 -20 -9 527.984 106.986 3 -4 20 9 709.611 167.160 1 -4 20 8 291.893 123.777 1 4 20 -8 230.024 80.2034 2 4 -20 -8 55.6776 54.7114 3 -4 20 7 14.3237 80.6327 1 4 20 -7 20.6308 51.4792 2 -4 20 6 1071.27 167.406 1 4 20 -6 939.150 134.312 2 -4 20 5 52.3275 68.4432 1 4 -20 -5-0.63129 45.3693 3 4 20 -5 61.8689 56.7773 2 4 20 -4 645.133 107.861 2 4 -20 -4 528.197 96.4616 3 -4 20 4 738.779 128.050 1 -4 20 3 41.1895 57.6845 1 4 20 -3 18.3706 49.3784 2 4 20 -2 2363.66 187.626 2 -4 20 2 2615.94 204.776 1 -4 20 1 45.3529 47.1616 1 4 20 -1 42.3624 54.6661 2 -4 20 0 57.4478 43.4413 1 4 20 0 90.1281 54.8912 2 4 20 1 1560.15 149.479 2 4 20 2 579.837 94.6728 2 -4 -20 -2 759.969 127.444 3 -4 -20 -3 996.207 166.758 3 4 20 3 38.3507 42.2350 2 4 20 4 404.194 80.2876 2 -4 -20 -4 2059.96 316.384 3 -4 -20 -5 1822.96 367.139 3 -4 -20 -6 115.548 198.974 3 4 21 -10 13.9930 43.0732 2 4 -21 -10 145.837 65.4637 3 4 21 -9 114.449 60.7416 2 4 -21 -9 11.6961 41.0504 3 -4 21 8 48.3073 76.5637 1 4 21 -8 150.201 67.8147 2 -4 21 7 1840.06 229.712 1 4 21 -7 1996.90 193.712 2 4 21 -6 48.1678 57.1456 2 -4 21 6 120.143 94.9561 1 4 -21 -6-2.92768 32.6964 3 -4 21 5-13.0889 62.5741 1 4 21 -5-1.72813 48.3477 2 -4 21 4 160.282 79.7867 1 4 -21 -4 148.430 49.7887 3 4 21 -4 18.9745 54.1081 2 4 21 -3 2482.50 199.102 2 -4 21 3 2665.16 223.232 1 4 21 -2 43.1168 59.1879 2 -4 21 2-3.84880 48.0421 1 -4 21 1 1166.17 136.061 1 4 21 -1 1150.33 135.579 2 -4 21 0-9.71043 38.0338 1 4 21 0 28.6002 48.0098 2 4 21 1 172.635 63.4081 2 -4 -21 -2-43.1465 75.9333 3 4 21 2-5.46996 42.4631 2 4 21 3 2170.46 177.118 2 -4 -21 -3 2558.19 229.962 3 -4 -21 -4 1903.13 272.828 3 4 21 4 12.8128 37.2212 2 -4 -21 -5 1976.02 338.978 3 -4 -21 -6 651.459 297.552 3 4 22 -10-46.4283 46.7967 2 4 22 -9 163.325 69.1978 2 4 22 -8 799.972 129.687 2 -4 22 8 768.095 171.075 1 -4 22 7 132.321 101.742 1 4 22 -7 49.4669 64.4397 2 4 -22 -7-18.2250 48.3539 3 -4 22 6 1610.89 208.666 1 4 22 -6 1438.50 166.931 2 4 -22 -5 71.1540 63.1429 3 -4 22 5 133.335 76.9915 1 4 22 -5 74.4746 61.1207 2 -4 22 4 415.670 106.763 1 4 22 -4 515.927 105.248 2 -4 22 3 113.920 70.0475 1 4 22 -3 46.7146 56.0754 2 4 22 -2 1869.71 176.667 2 -4 22 2 2186.05 194.944 1 -4 22 1 221.752 74.0394 1 4 22 -1 270.664 84.7849 2 -4 22 0 233.104 68.0095 1 4 22 0 113.249 60.9166 2 4 22 1 129.667 57.9715 2 4 22 2 1734.56 164.057 2 -4 -22 -2 1511.85 163.333 3 -4 -22 -3 372.032 113.982 3 4 22 3 47.5114 42.6856 2 -4 -22 -4 2257.75 276.256 3 4 22 4 262.432 70.0365 2 -4 -22 -5 2227.07 344.107 3 -4 -22 -6 2375.08 426.276 3 4 23 -9 90.7991 57.0182 2 -4 23 8 146.130 113.723 1 4 23 -8 102.358 62.7727 2 -4 23 7 1916.75 246.185 1 4 23 -7 1926.66 195.666 2 -4 23 6-0.45687 70.5663 1 4 23 -6 17.5395 50.0433 2 -4 23 5 16.0834 61.8120 1 4 23 -5 69.6464 58.2139 2 -4 23 4 14.8041 61.6780 1 4 23 -4 51.0690 53.7598 2 4 23 -3 981.290 136.723 2 -4 23 3 937.552 144.493 1 -4 23 2 276.265 87.1165 1 4 23 -2 209.985 76.5085 2 4 23 -1 756.313 121.174 2 -4 23 1 880.673 127.605 1 -4 23 0 18.9021 45.2935 1 4 23 0 25.6650 49.0626 2 4 23 1 474.306 96.4998 2 4 23 2 564.406 101.025 2 4 23 3 698.854 110.429 2 -4 -23 -3 1018.46 151.258 3 -4 -23 -4 1086.34 186.019 3 4 23 4 17.9232 42.6712 2 -4 -23 -5 2674.36 343.208 3 4 24 -8 302.937 87.1314 2 -4 24 7 135.731 90.2934 1 4 24 -7 26.6489 57.0138 2 -4 24 6 245.729 104.333 1 4 24 -6 243.634 84.6517 2 -4 24 5 16.4043 70.8398 1 4 24 -5 20.6390 55.4704 2 -4 24 4 198.607 87.4407 1 4 24 -4 110.414 68.1173 2 4 24 -3 635.032 113.723 2 -4 24 3 682.787 130.497 1 -4 24 2 139.099 67.9285 1 4 24 -2 146.320 71.4217 2 4 24 -1 45.7307 55.9558 2 -4 24 1 43.3573 51.5153 1 -4 24 0 819.541 116.082 1 4 24 0 763.508 119.300 2 4 24 1 730.120 115.721 2 4 24 2 236.279 73.9888 2 -4 -24 -3-83.6176 74.5499 3 4 24 3-13.7922 40.5897 2 -4 -24 -4 989.633 161.329 3 -4 -24 -5 3162.58 329.049 3 -4 25 7 868.781 177.013 1 4 25 -7 912.219 141.730 2 -4 25 6 40.3958 70.6235 1 4 25 -6 10.4534 50.1730 2 -4 25 5 340.339 113.945 1 4 25 -5 361.398 95.5805 2 4 25 -4 945.102 139.482 2 -4 25 4 905.805 154.596 1 -4 25 3 81.3800 64.1579 1 4 25 -3 34.5904 54.9505 2 -4 25 2 258.906 83.1526 1 4 25 -2 245.368 81.3175 2 4 25 -1 463.249 100.345 2 -4 25 1 573.935 111.673 1 -4 25 0 44.4863 47.5717 1 4 25 0 3.32515 51.1553 2 4 25 1 88.3544 61.1148 2 4 25 2 122.179 60.5714 2 4 25 3 747.945 119.081 2 -4 -25 -3 718.665 125.246 3 -4 -25 -4 705.150 144.682 3 -4 26 7 222.861 105.567 1 -4 26 6 281.660 115.117 1 4 26 -6 329.752 91.2970 2 -4 26 5 309.137 117.865 1 4 26 -5 377.034 93.6597 2 -4 26 4 248.933 91.9707 1 4 26 -4 229.502 79.9355 2 -4 26 3 40.8995 61.4432 1 4 26 -3 67.4568 61.9991 2 -4 26 2 178.677 76.4954 1 4 26 -2 199.018 75.6042 2 -4 26 1 342.904 91.5646 1 4 26 -1 318.782 92.6926 2 4 26 0 766.681 125.118 2 4 26 1 39.8042 51.7831 2 4 26 2-0.30456 42.3387 2 4 26 3 366.279 85.7552 2 -4 -26 -4 534.119 127.160 3 -4 27 6 309.708 115.170 1 -4 27 5 433.948 125.068 1 4 27 -5 403.533 97.9207 2 -4 27 4 68.8037 66.2994 1 4 27 -4 15.8571 51.4108 2 -4 27 3-1.76137 55.7396 1 4 27 -3 14.7332 54.1404 2 -4 27 2 409.480 101.909 1 4 27 -2 578.651 115.109 2 -4 27 1 241.135 83.2618 1 4 27 -1 322.356 93.4679 2 4 27 0 65.3123 58.7025 2 4 27 1 6.75797 46.6906 2 4 27 2-8.98184 46.3921 2 4 27 3 13.9235 39.2945 2 -4 28 6 561.890 146.451 1 -4 28 5 40.3385 68.0370 1 -4 28 4 331.346 107.572 1 4 28 -4 270.754 89.3111 2 -4 28 3-17.0490 56.5329 1 4 28 -3 23.6432 55.5156 2 -4 28 2 161.903 77.5338 1 4 28 -2 144.987 69.8782 2 4 28 -1 68.6397 64.7206 2 4 28 0 1670.69 182.657 2 4 28 1 145.699 65.5112 2 4 28 2 29.9110 56.9505 2 4 28 3 153.769 65.0641 2 -4 29 5 967.946 176.829 1 -4 29 4 16.7614 74.7766 1 -4 29 3 82.1084 70.8346 1 4 29 -3 125.581 69.8786 2 -4 29 2 32.3098 61.1757 1 4 29 -2-43.4440 60.7043 2 4 29 -1 496.354 112.278 2 4 29 0 24.3475 49.7388 2 4 29 1 231.364 79.4628 2 4 29 2 37.5390 49.4949 2 -4 30 4 45.7982 70.1262 1 -4 30 3-2.70447 57.2058 1 -4 30 2 59.0676 57.5474 1 4 30 -1 37.6811 61.2008 2 4 30 0 1743.02 192.275 2 4 30 1 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5 14 3 303.501 67.7635 2 -5 14 -3 246.267 37.0863 3 -5 -14 -4 5887.82 528.593 3 5 14 4 540.650 82.1169 2 -5 -14 -5 2110.58 317.883 3 5 14 5 1533.20 127.859 2 -5 -14 -6 1059.05 281.314 3 -5 -14 -7 720.755 238.806 3 5 -15 -12 12.5941 35.0797 3 5 -15 -11 21.1919 36.6656 3 5 15 -10-7.25345 42.9074 2 -5 15 10-11.5132 85.2047 1 5 -15 -10 4.57059 31.3177 3 -5 15 9-1.03049 85.6528 1 5 15 -9 16.5994 43.8045 2 5 -15 -9 9.11504 31.3864 3 5 15 -8 1120.61 137.264 2 -5 15 8 1181.24 183.921 1 5 -15 -8 1161.91 114.510 3 -5 15 7 525.999 123.956 1 5 15 -7 644.151 108.644 2 5 -15 -7 519.865 72.3010 3 5 15 -6-27.4147 52.3812 2 -5 15 6-8.88533 68.5354 1 5 -15 -6-3.21918 21.6738 3 5 15 -5 256.639 72.8480 2 -5 15 5 231.313 90.6223 1 5 -15 -5 347.788 52.1544 3 -5 15 4 3545.06 253.581 1 5 15 -4 3761.70 222.781 2 -5 15 3 64.4068 62.4410 1 5 15 -3 92.5668 54.7172 2 5 -15 -3 150.655 24.5311 3 5 15 -2 3.14481 46.5886 2 5 15 -1 77.6012 55.3972 2 5 15 0 203.889 64.0406 2 5 15 1 122.938 53.1838 2 -5 -15 -1 292.491 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523.529 88.8369 2 5 16 1 359.166 77.2685 2 -5 -16 -1 179.447 78.9735 3 5 16 2 263.492 65.2834 2 -5 -16 -2 1692.42 187.396 3 5 16 3 188.882 58.1450 2 -5 -16 -3 5691.39 418.418 3 5 16 4 33.7199 39.1811 2 -5 -16 -4 5719.17 524.682 3 -5 -16 -5 2858.98 410.403 3 -5 -16 -6 2277.35 331.296 3 -5 -16 -7 2470.49 351.723 3 5 17 -11 89.4553 55.4050 2 5 -17 -11 45.2435 36.3067 3 -5 17 10 3.21651 93.8524 1 5 17 -10 60.6289 52.7743 2 5 -17 -10 13.1348 33.7190 3 -5 17 9 69.8488 80.6221 1 5 17 -9 55.7598 49.9465 2 5 -17 -9 40.4895 32.8107 3 -5 17 8 22.1236 67.5127 1 5 17 -8 78.2866 56.5636 2 5 -17 -8 152.697 46.1850 3 -5 17 7 1351.00 190.514 1 5 -17 -7 1652.23 126.137 3 5 17 -7 1463.83 161.416 2 -5 17 6 31.8933 67.5922 1 5 -17 -6 64.8617 40.0089 3 5 17 -6 62.7827 56.6116 2 -5 17 5 936.427 146.968 1 5 17 -5 993.373 129.209 2 5 17 -4 385.024 87.7630 2 5 -17 -4 18.7287 47.0206 3 -5 17 4 440.568 103.097 1 -5 17 3-33.7729 57.2334 1 5 17 -3-6.44918 51.2418 2 5 17 -2 131.798 62.4900 2 -5 17 2 150.934 65.0847 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448.551 3 5 19 4 747.940 106.350 2 -5 -19 -5 4975.21 517.593 3 -5 -19 -6 6682.33 626.376 3 5 20 -10 84.6434 53.7537 2 5 20 -9-38.3444 54.1122 2 -5 20 9 169.236 109.442 1 -5 20 8 51.0272 76.2359 1 5 20 -8 53.0508 53.9145 2 -5 20 7 4025.41 330.693 1 5 20 -7 3975.62 270.023 2 -5 20 6 29.1676 67.3483 1 5 20 -6 41.0340 57.9998 2 -5 20 5 1150.40 170.204 1 5 20 -5 1205.96 148.345 2 -5 20 4 108.265 67.4673 1 5 20 -4 50.7034 58.7184 2 -5 20 3 112.218 66.6103 1 5 20 -3 181.058 72.6399 2 -5 20 2 1143.65 143.810 1 5 20 -2 1095.87 137.392 2 -5 20 1 1723.81 163.044 1 5 20 -1 1528.85 157.510 2 5 20 0 207.447 74.0104 2 5 20 1 53.0097 50.7306 2 -5 -20 -2-121.880 80.2337 3 5 20 2-2.93822 42.9349 2 -5 -20 -3 2928.37 240.972 3 5 20 3 2508.61 194.140 2 -5 -20 -4 3416.45 319.985 3 5 20 4 364.216 79.6408 2 -5 -20 -5 5390.18 508.144 3 5 21 -10 128.568 65.3214 2 5 21 -9 24.3937 54.1741 2 -5 21 8 431.830 135.299 1 5 21 -8 501.725 107.493 2 -5 21 7 193.565 97.8814 1 5 21 -7 169.704 75.8468 2 -5 21 6 1974.90 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5 22 2 32.7602 46.2501 2 5 22 3 2376.83 196.283 2 -5 -22 -3 2155.91 200.709 3 -5 -22 -4 1046.82 185.718 3 -5 -22 -5 4517.68 406.844 3 -5 23 8 162.793 105.905 1 5 23 -8 314.519 93.2102 2 -5 23 7 12.3656 73.5771 1 5 23 -7 45.0674 53.0950 2 -5 23 6 823.488 161.263 1 5 23 -6 990.165 146.561 2 5 23 -5 179.824 74.7754 2 -5 23 5 184.229 88.0243 1 5 23 -4 94.5740 61.8079 2 -5 23 4 112.085 76.1993 1 -5 23 3 33.8022 66.3158 1 5 23 -3 37.4715 51.6146 2 -5 23 2 1962.42 192.893 1 5 23 -2 2311.73 205.695 2 5 23 -1 67.3586 57.9949 2 -5 23 1 106.257 61.6239 1 5 23 0 1245.31 149.927 2 5 23 1 16.2797 49.9907 2 5 23 2 586.986 106.925 2 -5 -23 -3-179.251 90.6694 3 5 23 3 7.78241 38.4121 2 -5 -23 -4 2280.01 241.538 3 -5 24 7 1582.91 225.986 1 5 24 -7 1390.00 174.857 2 5 24 -6 373.145 98.3569 2 -5 24 6 80.2523 83.5483 1 5 24 -5 226.674 83.3757 2 -5 24 5 238.579 100.453 1 5 24 -4-1.78372 49.6591 2 -5 24 4 30.3609 54.4088 1 -5 24 3 1364.96 176.758 1 5 24 -3 1773.57 187.534 2 -5 24 2 333.985 90.3084 1 5 24 -2 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894.295 143.333 2 10 -6 -6 810.216 135.430 2 10 -6 -5 37.8403 59.0355 2 10 6 -5 76.6740 64.0599 2 10 6 -4 957.923 147.416 2 10 -6 -4 1052.95 147.173 2 10 -6 -3 42.4657 55.9754 2 10 6 -3 23.1359 54.8255 2 10 -6 -2 148.179 71.7201 2 10 6 -2 190.794 77.6684 2 10 -6 -1 44.0968 58.8526 2 10 6 -1 49.4906 64.0417 2 10 -6 0 989.391 148.218 2 10 6 0 859.764 142.028 2 10 -6 1 38.2104 55.5719 2 10 6 1 49.8895 60.1439 2 10 -6 2 114.970 63.6707 2 10 6 2 207.810 83.9005 2 10 -6 3 46.8226 54.3606 2 10 6 3 15.4503 43.8950 2 10 7 -10 131.405 68.4000 2 10 7 -9 796.227 136.535 2 10 -7 -9 810.176 131.521 2 10 -7 -8 5.58322 40.1599 2 10 7 -8-31.4680 49.0150 2 10 -7 -7 3.78252 46.2769 2 10 7 -7 87.0162 68.2738 2 10 -7 -6 55.8583 55.6933 2 10 7 -6 54.3916 62.7359 2 10 7 -5 2019.61 208.321 2 10 -7 -5 2108.56 202.540 2 10 -7 -4 355.720 94.2910 2 10 7 -4 240.990 87.3250 2 10 -7 -3 54.5070 55.7092 2 10 7 -3 13.2520 52.5386 2 10 -7 -2 20.0162 51.0192 2 10 7 -2 37.8327 60.1438 2 10 -7 -1 1060.60 153.396 2 10 7 -1 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10 -11 -7 376.841 94.4854 2 10 11 -6 457.060 106.901 2 10 -11 -6 504.003 108.300 2 10 11 -5 331.283 98.4798 2 10 -11 -5 376.417 95.7146 2 10 11 -4 785.002 137.791 2 10 -11 -4 779.049 129.969 2 10 11 -3 657.794 125.478 2 10 11 -2 93.3006 72.7189 2 10 11 -1 13.8657 51.8072 2 10 11 0-2.76105 48.6334 2 10 11 1 54.4867 60.3729 2 10 11 2 23.8000 51.5902 2 10 -12 -9 237.314 81.1044 2 10 -12 -8 338.568 97.4774 2 10 12 -7 121.082 72.9438 2 10 -12 -7 21.6118 45.7628 2 10 12 -6 99.5617 58.6570 2 10 -12 -6 66.7743 57.6354 2 10 12 -5 26.6025 55.6033 2 10 -12 -5 53.3932 55.7218 2 10 12 -4 713.715 132.460 2 10 12 -3-28.0820 52.4194 2 10 12 -2 244.424 86.5257 2 10 12 -1 425.798 107.664 2 10 12 0 17.5560 50.6904 2 10 12 1 452.285 110.415 2 10 12 2 1012.38 152.790 2 10 -13 -8 2.34086 46.7312 2 10 -13 -7 1121.79 156.031 2 10 13 -6 403.047 105.691 2 10 -13 -6 295.071 94.1749 2 10 13 -5 66.7705 75.1586 2 10 13 -4 59.4574 56.0553 2 10 13 -3 1211.60 167.964 2 10 13 -2-3.78747 52.1478 2 10 13 -1 98.4726 71.3183 2 10 13 0 86.1061 64.5051 2 10 13 1 179.539 76.4191 2 10 13 2 212.461 79.0648 2 10 -14 -8 1031.66 149.944 2 10 -14 -7 30.7832 43.7178 2 10 -14 -6 213.378 78.3350 2 10 14 -5 39.1262 59.2156 2 10 14 -4-11.3513 50.7530 2 10 14 -3 56.6366 63.6077 2 10 14 -2 343.334 98.0233 2 10 14 -1 19.3896 53.1504 2 10 14 0 53.1729 61.9158 2 10 14 1 56.1784 61.5458 2 10 14 2 1910.54 211.846 2 10 -15 -8 31.1722 49.1038 2 10 -15 -7 1113.69 157.375 2 10 15 -3 1701.99 201.797 2 10 15 -2 0.13178 57.0561 2 10 15 -1 253.154 89.4148 2 10 15 0-14.1935 49.7694 2 10 15 1 49.1669 52.4626 2 10 -16 -8 146.673 63.0686 2 10 -16 -7 40.7260 46.9187 2 11 0 -8-34.5786 57.6286 2 11 0 -7 92.1879 64.2963 2 11 0 -6 10.7564 61.4677 2 11 0 -5 223.450 83.0918 2 11 0 -4-3.39135 59.7735 2 11 0 -3 17.9659 52.0109 2 11 0 -2-10.6758 50.2757 2 11 0 -1 138.635 73.8928 2 11 0 0 0.13465 55.2948 2 11 -1 -9 37.6317 49.0216 2 11 1 -8-5.01225 44.8302 2 11 -1 -8-9.26519 53.4456 2 11 -1 -7 139.860 74.0461 2 11 1 -7 56.5681 59.7893 2 11 1 -6 1493.36 188.554 2 11 -1 -6 1721.58 196.999 2 11 1 -5 27.3423 59.3828 2 11 -1 -5-36.6893 68.3408 2 11 1 -4 78.0352 65.8342 2 11 -1 -4 61.4590 59.1322 2 11 1 -3 64.0619 61.5156 2 11 -1 -3 7.73337 53.4817 2 11 1 -2 1115.08 164.308 2 11 -1 -2 1286.80 173.115 2 11 1 -1 48.8643 61.5238 2 11 -1 -1-15.8506 65.9099 2 11 1 0 360.312 99.5233 2 11 -1 0 331.317 102.445 2 11 1 1-6.21439 48.4184 2 11 -2 -9 245.645 82.1358 2 11 2 -8 176.122 76.9319 2 11 -2 -8 185.175 74.5376 2 11 -2 -7 535.435 118.206 2 11 2 -7 481.619 113.857 2 11 -2 -6 59.6694 61.8809 2 11 2 -6-21.2048 56.1567 2 11 2 -5 544.003 120.841 2 11 -2 -5 525.274 119.266 2 11 2 -4 210.368 84.2294 2 11 -2 -4 172.482 78.2800 2 11 2 -3 149.067 74.9016 2 11 -2 -3 183.653 79.8130 2 11 2 -2-20.8762 54.6443 2 11 -2 -2-18.7284 54.2101 2 11 2 -1 372.715 105.459 2 11 -2 -1 264.857 94.1535 2 11 2 0 150.569 75.1556 2 11 -2 0 115.742 68.5082 2 11 2 1 138.416 78.1219 2 11 -3 -9 38.8141 52.9925 2 11 -3 -8 305.668 91.1983 2 11 -3 -7 205.441 84.8482 2 11 3 -7 100.465 67.3604 2 11 3 -6 1154.88 166.289 2 11 -3 -6 1039.45 155.059 2 11 -3 -5 483.788 115.180 2 11 3 -5 456.486 111.774 2 11 3 -4 357.077 104.397 2 11 -3 -4 315.122 89.5072 2 11 3 -3-19.6189 58.0231 2 11 -3 -3 42.1786 58.4969 2 11 3 -2 697.877 130.276 2 11 -3 -2 659.654 129.781 2 11 3 -1 6.71413 55.9796 2 11 -3 -1 13.7746 46.8256 2 11 3 0 184.618 83.5866 2 11 -3 0 121.046 70.2522 2 11 3 1 149.551 73.9401 2 11 -4 -9 44.3415 46.6485 2 11 -4 -8 469.786 112.988 2 11 -4 -7 188.963 81.7769 2 11 4 -7 202.353 84.3302 2 11 -4 -6 53.5243 61.8037 2 11 4 -6 15.5476 57.3526 2 11 -4 -5 527.080 114.320 2 11 4 -5 606.406 126.013 2 11 -4 -4 232.049 90.0056 2 11 4 -4 157.250 79.1561 2 11 -4 -3 380.723 103.497 2 11 4 -3 371.694 104.082 2 11 4 -2-54.7266 66.4497 2 11 -4 -2 15.9586 50.9656 2 11 4 -1 17.2697 56.7508 2 11 -4 -1 25.1908 48.8148 2 11 4 0 514.645 115.797 2 11 4 1 332.854 99.0024 2 11 -5 -9 5.18267 40.1785 2 11 -5 -8 505.883 113.784 2 11 -5 -7 206.397 79.6986 2 11 -5 -6 31.2832 47.9083 2 11 5 -6 78.3153 61.7542 2 11 -5 -5 253.767 89.5080 2 11 5 -5 290.178 98.3126 2 11 -5 -4 507.571 112.965 2 11 5 -4 532.724 118.605 2 11 -5 -3 69.1208 59.4746 2 11 5 -3 65.4246 67.1998 2 11 -5 -2 56.9904 55.8104 2 11 5 -2 105.324 72.4383 2 11 -5 -1 58.9023 59.3136 2 11 5 -1 35.0642 59.3378 2 11 5 0 161.905 78.5353 2 11 -6 -8 78.4555 61.1858 2 11 -6 -7 115.171 70.1376 2 11 -6 -6 22.8515 53.6293 2 11 6 -6 99.0397 70.6475 2 11 6 -5 732.356 139.833 2 11 -6 -5 694.305 132.587 2 11 -6 -4-7.11406 53.8806 2 11 6 -4 7.34946 57.4280 2 11 6 -3 741.366 139.419 2 11 -6 -3 546.345 117.834 2 11 -6 -2 0.12867 47.7401 2 11 6 -2 15.8040 53.8086 2 11 6 -1 226.765 82.3519 2 11 6 0 33.0197 56.8368 2 11 -7 -8 1356.37 178.476 2 11 -7 -7 55.9458 57.8692 2 11 -7 -6 136.812 76.0606 2 11 -7 -5 573.953 120.641 2 11 7 -5 519.642 121.167 2 11 7 -4 949.599 156.679 2 11 -7 -4 1087.99 162.290 2 11 -7 -3 129.015 75.2807 2 11 7 -3-17.9682 62.9683 2 11 -7 -2-25.2029 57.1560 2 11 7 -2 2.95953 58.2852 2 11 7 -1-20.4565 58.3984 2 11 -8 -7 177.239 76.6418 2 11 -8 -6 54.4108 55.7727 2 11 -8 -5 343.563 105.384 2 11 -8 -4 14.5554 60.9879 2 11 8 -4-5.23146 54.4005 2 11 8 -3 555.095 129.527 2 11 -8 -3 698.669 133.614 2 11 8 -2 108.674 69.9941 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 77168 data_10 #============================================================================== # PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic 2024-03-26 _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code AW5090 _journal_coeditor_notes ; ? ; _journal_paper_category FA _journal_techeditor_code ? _iucr_compatibility_tag ACTA95 _journal_techeditor_notes ; ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C4 H8 O2)' _chemical_formula_sum 'C44 H48 Cl2 Cu N8 O12' _chemical_formula_weight 1015.34 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3679(9) _cell_length_b 10.2347(8) _cell_length_c 12.5311(15) _cell_angle_alpha 79.661(8) _cell_angle_beta 84.578(9) _cell_angle_gamma 73.249(8) _cell_volume 1130.6(2) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 2153 _cell_measurement_theta_min 3.9470 _cell_measurement_theta_max 27.7570 _exptl_crystal_description prism _exptl_crystal_colour pink _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.491 _exptl_crystal_F_000 527 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.10 _exptl_crystal_size_min 0.10 _exptl_absorpt_coefficient_mu 0.674 _shelx_estimated_absorpt_T_min 0.866 _shelx_estimated_absorpt_T_max 0.936 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.489 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 10186 _diffrn_reflns_av_unetI/netI 0.1230 _diffrn_reflns_av_R_equivalents 0.0825 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 2.869 _diffrn_reflns_theta_max 26.999 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 4867 _reflns_number_gt 3144 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0702P)^2^+0.2104P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4867 _refine_ls_number_parameters 310 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.1146 _refine_ls_R_factor_gt 0.0689 _refine_ls_wR_factor_ref 0.1842 _refine_ls_wR_factor_gt 0.1506 _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_restrained_S_all 1.061 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.0000 0.0228(2) Uani 1 2 d S . P . . N1A N -0.2415(4) 0.3720(3) 0.0907(3) 0.0226(8) Uani 1 1 d D . . . . H1A H -0.250(5) 0.4568(16) 0.093(4) 0.034 Uiso 1 1 d D U . . . C2A C -0.1179(5) 0.2842(4) 0.0555(3) 0.0231(9) Uani 1 1 d . . . . . H2A H -0.0243 0.3037 0.0390 0.028 Uiso 1 1 calc R U . . . N3A N -0.1446(4) 0.1658(3) 0.0469(3) 0.0239(8) Uani 1 1 d . . . . . C4A C -0.2928(5) 0.1820(4) 0.0779(3) 0.0233(9) Uani 1 1 d . . . . . H4A H -0.3443 0.1139 0.0804 0.028 Uiso 1 1 calc R U . . . C5A C -0.3546(5) 0.3102(4) 0.1045(3) 0.0226(9) Uani 1 1 d . . . . . C6A C -0.5088(5) 0.3775(4) 0.1388(3) 0.0231(9) Uani 1 1 d . . . . . C7A C -0.5577(5) 0.5199(4) 0.1414(3) 0.0282(10) Uani 1 1 d . . . . . H7A H -0.4897 0.5746 0.1239 0.034 Uiso 1 1 calc R U . . . C8A C -0.7057(5) 0.5806(4) 0.1697(4) 0.0340(11) Uani 1 1 d . . . . . H8A H -0.7382 0.6771 0.1715 0.041 Uiso 1 1 calc R U . . . C9A C -0.8062(5) 0.5038(4) 0.1953(3) 0.0331(11) Uani 1 1 d . . . . . H9A H -0.9071 0.5468 0.2149 0.040 Uiso 1 1 calc R U . . . C10A C -0.7596(5) 0.3645(5) 0.1922(4) 0.0349(11) Uani 1 1 d . . . . . H10A H -0.8287 0.3108 0.2087 0.042 Uiso 1 1 calc R U . . . C11A C -0.6110(5) 0.3017(4) 0.1650(4) 0.0348(11) Uani 1 1 d . . . . . H11A H -0.5795 0.2049 0.1644 0.042 Uiso 1 1 calc R U . . . N1B N 0.2299(5) -0.0630(4) 0.2816(3) 0.0327(9) Uani 1 1 d D . . . . H1B H 0.304(4) -0.061(5) 0.316(4) 0.049 Uiso 1 1 d D U . . . C2B C 0.2134(5) -0.0190(4) 0.1747(4) 0.0306(10) Uani 1 1 d . . . . . H2B H 0.2795 0.0224 0.1277 0.037 Uiso 1 1 calc R U . . . N3B N 0.0923(4) -0.0414(3) 0.1442(3) 0.0244(8) Uani 1 1 d . . . . . C4B C 0.0295(5) -0.1022(4) 0.2366(3) 0.0266(10) Uani 1 1 d . . . . . H4B H -0.0597 -0.1295 0.2394 0.032 Uiso 1 1 calc R U . . . C5B C 0.1135(5) -0.1177(4) 0.3233(3) 0.0261(10) Uani 1 1 d . . . . . C6B C 0.0977(5) -0.1841(4) 0.4363(3) 0.0288(10) Uani 1 1 d . . . . . C7B C 0.1703(6) -0.1587(5) 0.5189(4) 0.0389(12) Uani 1 1 d . . . . . H7B H 0.2261 -0.0928 0.5036 0.047 Uiso 1 1 calc R U . . . C8B C 0.1616(6) -0.2292(5) 0.6234(4) 0.0407(12) Uani 1 1 d . . . . . H8B H 0.2117 -0.2116 0.6795 0.049 Uiso 1 1 calc R U . . . C9B C 0.0801(6) -0.3252(5) 0.6467(4) 0.0400(12) Uani 1 1 d . . . . . H9B H 0.0760 -0.3750 0.7180 0.048 Uiso 1 1 calc R U . . . C10B C 0.0047(6) -0.3479(5) 0.5653(4) 0.0463(13) Uani 1 1 d . . . . . H10B H -0.0536 -0.4117 0.5812 0.056 Uiso 1 1 calc R U . . . C11B C 0.0139(6) -0.2777(5) 0.4602(4) 0.0392(12) Uani 1 1 d . . . . . H11B H -0.0376 -0.2942 0.4044 0.047 Uiso 1 1 calc R U . . . Cl Cl -0.26455(12) -0.23638(10) 0.12344(9) 0.0291(3) Uani 1 1 d . . . . . O1 O -0.1892(4) -0.1389(3) 0.0649(3) 0.0352(8) Uani 1 1 d . . . . . O2 O -0.2282(6) -0.2669(5) 0.2349(3) 0.0780(14) Uani 1 1 d . . . . . O3 O -0.4184(4) -0.1889(4) 0.1095(4) 0.0800(15) Uani 1 1 d . . . . . O4 O -0.2060(5) -0.3628(3) 0.0814(3) 0.0614(12) Uani 1 1 d . . . . . O5 O 0.4417(4) -0.0034(3) 0.4005(3) 0.0478(9) Uani 1 1 d . . . . . C12 C 0.4001(6) 0.1176(5) 0.4514(4) 0.0479(14) Uani 1 1 d . . . . . H12A H 0.2969 0.1714 0.4331 0.057 Uiso 1 1 calc R U . . . H12B H 0.4670 0.1763 0.4229 0.057 Uiso 1 1 calc R U . . . C13 C 0.5909(6) -0.0807(5) 0.4265(4) 0.0479(14) Uani 1 1 d . . . . . H13A H 0.6607 -0.0251 0.3971 0.057 Uiso 1 1 calc R U . . . H13B H 0.6197 -0.1660 0.3934 0.057 Uiso 1 1 calc R U . . . O6 O 0.4680(4) 0.3713(3) 0.5179(3) 0.0492(10) Uani 1 1 d . . . . . C14 C 0.4039(7) 0.4775(5) 0.4322(4) 0.0463(13) Uani 1 1 d . . . . . H14A H 0.3061 0.5337 0.4579 0.056 Uiso 1 1 calc R U . . . H14B H 0.3869 0.4356 0.3709 0.056 Uiso 1 1 calc R U . . . C15 C 0.4936(6) 0.4299(5) 0.6064(4) 0.0457(13) Uani 1 1 d . . . . . H15A H 0.5402 0.3555 0.6651 0.055 Uiso 1 1 calc R U . . . H15B H 0.3975 0.4848 0.6357 0.055 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0215(5) 0.0189(4) 0.0295(4) -0.0072(3) 0.0003(3) -0.0064(3) N1A 0.024(2) 0.0173(15) 0.0293(19) -0.0074(14) -0.0001(15) -0.0074(15) C2A 0.023(2) 0.0214(19) 0.028(2) -0.0074(16) 0.0004(17) -0.0089(17) N3A 0.024(2) 0.0198(16) 0.031(2) -0.0062(14) -0.0063(15) -0.0084(15) C4A 0.023(3) 0.0194(19) 0.030(2) -0.0044(16) -0.0022(18) -0.0097(17) C5A 0.023(2) 0.0226(19) 0.023(2) -0.0049(15) -0.0037(17) -0.0075(17) C6A 0.028(3) 0.0226(19) 0.021(2) -0.0034(16) -0.0024(17) -0.0092(18) C7A 0.025(3) 0.023(2) 0.035(2) -0.0068(17) -0.0007(19) -0.0039(18) C8A 0.035(3) 0.025(2) 0.037(3) -0.0082(18) -0.004(2) 0.002(2) C9A 0.025(3) 0.039(2) 0.028(2) -0.0039(19) 0.0025(19) 0.000(2) C10A 0.023(3) 0.046(3) 0.040(3) -0.011(2) 0.004(2) -0.016(2) C11A 0.033(3) 0.030(2) 0.045(3) -0.012(2) 0.002(2) -0.013(2) N1B 0.034(3) 0.041(2) 0.032(2) -0.0060(16) -0.0096(17) -0.0195(18) C2B 0.026(3) 0.032(2) 0.039(3) -0.0076(19) 0.002(2) -0.017(2) N3B 0.022(2) 0.0196(16) 0.032(2) -0.0069(14) 0.0007(15) -0.0054(15) C4B 0.022(3) 0.024(2) 0.036(2) -0.0115(17) -0.0007(19) -0.0043(18) C5B 0.020(2) 0.025(2) 0.036(2) -0.0127(18) -0.0001(19) -0.0060(18) C6B 0.022(3) 0.033(2) 0.030(2) -0.0116(18) -0.0020(19) -0.0016(19) C7B 0.036(3) 0.047(3) 0.038(3) -0.011(2) -0.010(2) -0.014(2) C8B 0.036(3) 0.057(3) 0.030(3) -0.010(2) -0.008(2) -0.011(2) C9B 0.033(3) 0.061(3) 0.027(2) -0.006(2) 0.004(2) -0.017(2) C10B 0.044(3) 0.070(3) 0.032(3) -0.007(2) 0.005(2) -0.031(3) C11B 0.035(3) 0.056(3) 0.034(3) -0.014(2) 0.001(2) -0.020(2) Cl 0.0283(7) 0.0276(5) 0.0376(6) -0.0122(4) 0.0053(5) -0.0157(5) O1 0.033(2) 0.0248(14) 0.052(2) -0.0033(13) 0.0039(15) -0.0167(13) O2 0.106(4) 0.123(3) 0.039(2) -0.014(2) 0.012(2) -0.089(3) O3 0.025(2) 0.055(2) 0.157(5) -0.004(3) 0.003(3) -0.0158(19) O4 0.068(3) 0.0314(17) 0.094(3) -0.0282(18) 0.023(2) -0.0252(18) O5 0.050(3) 0.059(2) 0.047(2) -0.0200(17) -0.0088(18) -0.0246(19) C12 0.039(3) 0.052(3) 0.057(4) -0.016(3) -0.004(3) -0.014(3) C13 0.048(4) 0.052(3) 0.053(3) -0.021(2) -0.004(3) -0.020(3) O6 0.069(3) 0.0434(19) 0.039(2) -0.0039(15) -0.0105(18) -0.0202(18) C14 0.052(4) 0.046(3) 0.043(3) -0.004(2) -0.015(3) -0.015(3) C15 0.055(4) 0.041(3) 0.044(3) -0.005(2) -0.011(3) -0.017(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.986(3) 2 ? Cu N3A 1.986(3) . ? Cu N3B 2.000(3) . ? Cu N3B 2.000(3) 2 ? N1A C2A 1.338(5) . ? N1A C5A 1.365(5) . ? N1A H1A 0.854(10) . ? C2A N3A 1.330(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.377(5) . ? C4A C5A 1.360(5) . ? C4A H4A 0.9500 . ? C5A C6A 1.470(6) . ? C6A C11A 1.379(6) . ? C6A C7A 1.402(5) . ? C7A C8A 1.387(6) . ? C7A H7A 0.9500 . ? C8A C9A 1.373(7) . ? C8A H8A 0.9500 . ? C9A C10A 1.372(6) . ? C9A H9A 0.9500 . ? C10A C11A 1.393(6) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.342(6) . ? N1B C5B 1.383(6) . ? N1B H1B 0.859(10) . ? C2B N3B 1.323(5) . ? C2B H2B 0.9500 . ? N3B C4B 1.377(5) . ? C4B C5B 1.362(6) . ? C4B H4B 0.9500 . ? C5B C6B 1.471(6) . ? C6B C11B 1.382(7) . ? C6B C7B 1.389(6) . ? C7B C8B 1.385(7) . ? C7B H7B 0.9500 . ? C8B C9B 1.386(7) . ? C8B H8B 0.9500 . ? C9B C10B 1.381(7) . ? C9B H9B 0.9500 . ? C10B C11B 1.390(7) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.399(4) . ? Cl O2 1.426(4) . ? Cl O4 1.426(3) . ? Cl O1 1.442(3) . ? O5 C13 1.429(6) . ? O5 C12 1.432(5) . ? C12 C13 1.514(7) 2_656 ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C12 1.514(7) 2_656 ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? O6 C14 1.421(6) . ? O6 C15 1.422(5) . ? C14 C15 1.526(8) 2_666 ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C14 1.526(8) 2_666 ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 2 . ? N3A Cu N3B 91.19(13) 2 . ? N3A Cu N3B 88.81(13) . . ? N3A Cu N3B 88.81(13) 2 2 ? N3A Cu N3B 91.19(13) . 2 ? N3B Cu N3B 180.0 . 2 ? C2A N1A C5A 108.8(3) . . ? C2A N1A H1A 124(3) . . ? C5A N1A H1A 126(3) . . ? N3A C2A N1A 110.3(4) . . ? N3A C2A H2A 124.8 . . ? N1A C2A H2A 124.8 . . ? C2A N3A C4A 105.7(3) . . ? C2A N3A Cu 127.0(3) . . ? C4A N3A Cu 127.3(2) . . ? C5A C4A N3A 109.8(4) . . ? C5A C4A H4A 125.1 . . ? N3A C4A H4A 125.1 . . ? C4A C5A N1A 105.4(4) . . ? C4A C5A C6A 130.4(4) . . ? N1A C5A C6A 124.2(3) . . ? C11A C6A C7A 118.3(4) . . ? C11A C6A C5A 120.2(3) . . ? C7A C6A C5A 121.4(4) . . ? C8A C7A C6A 119.7(4) . . ? C8A C7A H7A 120.2 . . ? C6A C7A H7A 120.2 . . ? C9A C8A C7A 121.3(4) . . ? C9A C8A H8A 119.4 . . ? C7A C8A H8A 119.4 . . ? C10A C9A C8A 119.4(4) . . ? C10A C9A H9A 120.3 . . ? C8A C9A H9A 120.3 . . ? C9A C10A C11A 120.0(5) . . ? C9A C10A H10A 120.0 . . ? C11A C10A H10A 120.0 . . ? C6A C11A C10A 121.3(4) . . ? C6A C11A H11A 119.4 . . ? C10A C11A H11A 119.4 . . ? C2B N1B C5B 108.6(4) . . ? C2B N1B H1B 124(4) . . ? C5B N1B H1B 127(4) . . ? N3B C2B N1B 110.5(4) . . ? N3B C2B H2B 124.8 . . ? N1B C2B H2B 124.8 . . ? C2B N3B C4B 106.0(4) . . ? C2B N3B Cu 131.8(3) . . ? C4B N3B Cu 122.2(3) . . ? C5B C4B N3B 110.3(4) . . ? C5B C4B H4B 124.9 . . ? N3B C4B H4B 124.9 . . ? C4B C5B N1B 104.6(4) . . ? C4B C5B C6B 130.5(4) . . ? N1B C5B C6B 124.8(4) . . ? C11B C6B C7B 119.3(4) . . ? C11B C6B C5B 119.3(4) . . ? C7B C6B C5B 121.3(4) . . ? C8B C7B C6B 120.2(5) . . ? C8B C7B H7B 119.9 . . ? C6B C7B H7B 119.9 . . ? C7B C8B C9B 120.3(4) . . ? C7B C8B H8B 119.9 . . ? C9B C8B H8B 119.9 . . ? C10B C9B C8B 119.5(5) . . ? C10B C9B H9B 120.2 . . ? C8B C9B H9B 120.2 . . ? C9B C10B C11B 120.2(5) . . ? C9B C10B H10B 119.9 . . ? C11B C10B H10B 119.9 . . ? C6B C11B C10B 120.3(4) . . ? C6B C11B H11B 119.8 . . ? C10B C11B H11B 119.8 . . ? O3 Cl O2 112.8(3) . . ? O3 Cl O4 109.2(3) . . ? O2 Cl O4 106.0(3) . . ? O3 Cl O1 111.1(2) . . ? O2 Cl O1 109.9(2) . . ? O4 Cl O1 107.5(2) . . ? C13 O5 C12 109.3(4) . . ? O5 C12 C13 111.5(4) . 2_656 ? O5 C12 H12A 109.3 . . ? C13 C12 H12A 109.3 2_656 . ? O5 C12 H12B 109.3 . . ? C13 C12 H12B 109.3 2_656 . ? H12A C12 H12B 108.0 . . ? O5 C13 C12 109.2(4) . 2_656 ? O5 C13 H13A 109.8 . . ? C12 C13 H13A 109.8 2_656 . ? O5 C13 H13B 109.8 . . ? C12 C13 H13B 109.8 2_656 . ? H13A C13 H13B 108.3 . . ? C14 O6 C15 110.2(4) . . ? O6 C14 C15 110.6(4) . 2_666 ? O6 C14 H14A 109.5 . . ? C15 C14 H14A 109.5 2_666 . ? O6 C14 H14B 109.5 . . ? C15 C14 H14B 109.5 2_666 . ? H14A C14 H14B 108.1 . . ? O6 C15 C14 109.4(4) . 2_666 ? O6 C15 H15A 109.8 . . ? C14 C15 H15A 109.8 2_666 . ? O6 C15 H15B 109.8 . . ? C14 C15 H15B 109.8 2_666 . ? H15A C15 H15B 108.3 . . ? _refine_diff_density_max 0.990 _refine_diff_density_min -0.586 _refine_diff_density_rms 0.103 # start Validation Reply Form _vrf_PLAT341_10 ; RESPONSE: The crystal used for data collection was of medium diffraction quality. However, the structure solution and refinement proceeded smoothly without any problems. ; # end Validation Reply Form _shelx_res_file ; 10.res created by SHELXL-2014/7 TITL EL100A in P-1 CELL 0.71073 9.3679 10.2347 12.5311 79.661 84.578 73.249 ZERR 1 0.0009 0.0008 0.0015 0.008 0.009 0.008 LATT 1 SFAC C H N O CU CL UNIT 44 48 8 12 1 2 MERG 2 OMIT -2 54 MORE -3 FMAP 2 PLAN 10 SIZE 0.10 0.10 0.22 TEMP -173 ACTA LIST 4 BOND $H HTAB L.S. 6 WGHT 0.070200 0.210400 FVAR 1.54152 CU 5 0.000000 0.000000 0.000000 10.50000 0.02146 0.01890 = 0.02949 -0.00716 0.00034 -0.00642 DFIX 0.86 0.01 N1A H1A N1B H1B N1A 3 -0.241548 0.371957 0.090707 11.00000 0.02358 0.01727 = 0.02926 -0.00742 -0.00008 -0.00741 H1A 2 -0.249881 0.456817 0.092767 11.00000 -1.50000 C2A 1 -0.117858 0.284246 0.055500 11.00000 0.02256 0.02137 = 0.02807 -0.00743 0.00036 -0.00891 AFIX 43 H2A 2 -0.024287 0.303720 0.039001 11.00000 -1.20000 AFIX 0 N3A 3 -0.144588 0.165843 0.046890 11.00000 0.02374 0.01977 = 0.03146 -0.00622 -0.00628 -0.00841 C4A 1 -0.292848 0.182022 0.077927 11.00000 0.02296 0.01937 = 0.03031 -0.00442 -0.00224 -0.00972 AFIX 43 H4A 2 -0.344257 0.113864 0.080421 11.00000 -1.20000 AFIX 0 C5A 1 -0.354630 0.310198 0.104470 11.00000 0.02347 0.02263 = 0.02339 -0.00487 -0.00365 -0.00753 C6A 1 -0.508841 0.377464 0.138810 11.00000 0.02786 0.02261 = 0.02062 -0.00342 -0.00241 -0.00925 C7A 1 -0.557675 0.519932 0.141432 11.00000 0.02537 0.02286 = 0.03529 -0.00680 -0.00074 -0.00394 AFIX 43 H7A 2 -0.489688 0.574649 0.123903 11.00000 -1.20000 AFIX 0 C8A 1 -0.705708 0.580609 0.169737 11.00000 0.03464 0.02491 = 0.03738 -0.00824 -0.00410 0.00234 AFIX 43 H8A 2 -0.738190 0.677145 0.171493 11.00000 -1.20000 AFIX 0 C9A 1 -0.806210 0.503806 0.195271 11.00000 0.02477 0.03932 = 0.02849 -0.00391 0.00250 -0.00032 AFIX 43 H9A 2 -0.907118 0.546766 0.214865 11.00000 -1.20000 AFIX 0 C10A 1 -0.759604 0.364450 0.192237 11.00000 0.02324 0.04603 = 0.04012 -0.01142 0.00364 -0.01595 AFIX 43 H10A 2 -0.828697 0.310765 0.208729 11.00000 -1.20000 AFIX 0 C11A 1 -0.611034 0.301733 0.164984 11.00000 0.03292 0.03013 = 0.04548 -0.01220 0.00230 -0.01273 AFIX 43 H11A 2 -0.579479 0.204921 0.164414 11.00000 -1.20000 AFIX 0 N1B 3 0.229856 -0.062963 0.281604 11.00000 0.03369 0.04056 = 0.03162 -0.00605 -0.00957 -0.01954 H1B 2 0.304482 -0.061341 0.315769 11.00000 -1.50000 C2B 1 0.213409 -0.018989 0.174747 11.00000 0.02591 0.03238 = 0.03890 -0.00759 0.00180 -0.01659 AFIX 43 H2B 2 0.279461 0.022391 0.127681 11.00000 -1.20000 AFIX 0 N3B 3 0.092252 -0.041387 0.144193 11.00000 0.02187 0.01963 = 0.03221 -0.00691 0.00071 -0.00542 C4B 1 0.029475 -0.102221 0.236578 11.00000 0.02165 0.02371 = 0.03557 -0.01151 -0.00068 -0.00432 AFIX 43 H4B 2 -0.059701 -0.129509 0.239390 11.00000 -1.20000 AFIX 0 C5B 1 0.113545 -0.117654 0.323317 11.00000 0.01998 0.02460 = 0.03624 -0.01272 -0.00008 -0.00597 C6B 1 0.097718 -0.184053 0.436335 11.00000 0.02245 0.03253 = 0.03024 -0.01157 -0.00195 -0.00156 C7B 1 0.170279 -0.158727 0.518908 11.00000 0.03648 0.04672 = 0.03837 -0.01105 -0.00984 -0.01390 AFIX 43 H7B 2 0.226054 -0.092826 0.503582 11.00000 -1.20000 AFIX 0 C8B 1 0.161600 -0.229179 0.623443 11.00000 0.03586 0.05745 = 0.02997 -0.00962 -0.00834 -0.01123 AFIX 43 H8B 2 0.211739 -0.211637 0.679499 11.00000 -1.20000 AFIX 0 C9B 1 0.080062 -0.325211 0.646673 11.00000 0.03345 0.06098 = 0.02678 -0.00598 0.00424 -0.01723 AFIX 43 H9B 2 0.076035 -0.375048 0.718047 11.00000 -1.20000 AFIX 0 C10B 1 0.004722 -0.347886 0.565263 11.00000 0.04448 0.07009 = 0.03220 -0.00698 0.00465 -0.03117 AFIX 43 H10B 2 -0.053598 -0.411660 0.581152 11.00000 -1.20000 AFIX 0 C11B 1 0.013946 -0.277710 0.460164 11.00000 0.03454 0.05610 = 0.03444 -0.01446 0.00066 -0.02038 AFIX 43 H11B 2 -0.037597 -0.294212 0.404431 11.00000 -1.20000 AFIX 0 CL 6 -0.264552 -0.236381 0.123443 11.00000 0.02833 0.02765 = 0.03765 -0.01223 0.00535 -0.01571 O1 4 -0.189201 -0.138876 0.064875 11.00000 0.03255 0.02481 = 0.05157 -0.00328 0.00386 -0.01672 O2 4 -0.228214 -0.266889 0.234853 11.00000 0.10648 0.12264 = 0.03872 -0.01427 0.01188 -0.08896 O3 4 -0.418375 -0.188945 0.109473 11.00000 0.02468 0.05504 = 0.15690 -0.00384 0.00280 -0.01577 O4 4 -0.205978 -0.362801 0.081375 11.00000 0.06821 0.03145 = 0.09361 -0.02821 0.02254 -0.02516 O5 4 0.441740 -0.003391 0.400459 11.00000 0.04999 0.05872 = 0.04667 -0.02000 -0.00877 -0.02459 C12 1 0.400069 0.117579 0.451355 11.00000 0.03894 0.05150 = 0.05747 -0.01635 -0.00427 -0.01401 AFIX 23 H12A 2 0.296870 0.171421 0.433095 11.00000 -1.20000 H12B 2 0.467026 0.176324 0.422930 11.00000 -1.20000 AFIX 0 C13 1 0.590931 -0.080667 0.426492 11.00000 0.04779 0.05204 = 0.05288 -0.02150 -0.00413 -0.01965 AFIX 23 H13A 2 0.660682 -0.025079 0.397060 11.00000 -1.20000 H13B 2 0.619717 -0.165976 0.393402 11.00000 -1.20000 AFIX 0 O6 4 0.467993 0.371272 0.517861 11.00000 0.06891 0.04335 = 0.03882 -0.00388 -0.01047 -0.02022 C14 1 0.403889 0.477468 0.432248 11.00000 0.05177 0.04601 = 0.04326 -0.00374 -0.01481 -0.01489 AFIX 23 H14A 2 0.306148 0.533695 0.457921 11.00000 -1.20000 H14B 2 0.386943 0.435554 0.370937 11.00000 -1.20000 AFIX 0 C15 1 0.493564 0.429889 0.606424 11.00000 0.05501 0.04136 = 0.04407 -0.00473 -0.01143 -0.01689 AFIX 23 H15A 2 0.540247 0.355452 0.665110 11.00000 -1.20000 H15B 2 0.397497 0.484785 0.635679 11.00000 -1.20000 AFIX 0 HKLF 4 REM EL100A in P-1 REM R1 = 0.0689 for 3144 Fo > 4sig(Fo) and 0.1146 for all 4867 data REM 310 parameters refined using 2 restraints END WGHT 0.0694 0.2480 REM Instructions for potential hydrogen bonds EQIV $1 x, y+1, z HTAB N1A O4_$1 EQIV $2 -x, -y, -z HTAB C2A O1_$2 HTAB C4A O1 HTAB N1B O5 HTAB C2B O1_$2 HTAB C4B O1 HTAB C4B O2 HTAB C12 O6 EQIV $3 x+1, y, z HTAB C13 O2_$3 EQIV $4 -x+1, -y, -z+1 HTAB C13 O6_$4 REM Highest difference peak 0.990, deepest hole -0.586, 1-sigma level 0.103 Q1 1 0.0455 -0.0397 0.0799 11.00000 0.05 0.87 Q2 1 -0.3034 -0.1588 0.2086 11.00000 0.05 0.79 Q3 1 -0.2204 -0.2827 0.2079 11.00000 0.05 0.57 Q4 1 -0.1990 -0.3571 0.1452 11.00000 0.05 0.52 Q5 1 -0.6735 0.5450 0.2405 11.00000 0.05 0.51 Q6 1 -0.5255 0.5203 0.2537 11.00000 0.05 0.47 Q7 1 0.1374 -0.0437 0.0232 11.00000 0.05 0.42 Q8 1 -0.2533 -0.3124 0.0646 11.00000 0.05 0.41 Q9 1 -0.0910 0.1031 0.0236 11.00000 0.05 0.41 Q10 1 -0.5414 0.4723 0.1233 11.00000 0.05 0.39 ; _shelx_res_checksum 13648 _shelx_hkl_file ; 0 0 2 11616.4 190.064 2 0 0 3 11598.0 233.608 2 0 0 4 6233.76 197.633 2 0 0 5 40.4263 20.2752 2 0 0 5 26.3818 9.95667 4 0 0 6 296.412 29.7092 4 0 0 6 450.073 67.8875 2 0 0 7 1083.27 55.6112 4 0 0 7 1406.37 130.617 2 0 0 8 399.552 77.0430 2 0 0 8 324.166 30.5833 4 0 0 -9 559.422 91.3845 1 0 0 -10 91.7590 45.4896 1 0 0 -11 99.4982 46.2609 1 0 0 -12 75.3373 43.6081 1 0 0 -13 84.2347 46.9425 1 0 0 -14 248.461 83.0021 1 0 0 -15 143.413 68.4694 1 0 1 -15 233.443 84.7725 1 0 1 -14 63.0990 39.2970 1 0 1 -13 265.581 79.0876 1 0 1 -12 614.928 119.000 1 0 1 -11-8.17914 21.4387 1 0 1 -10 238.047 62.2546 1 0 1 -9 28.6364 26.5812 1 0 -1 8 1188.57 131.144 2 0 -1 7 4362.55 229.301 2 0 -1 6 3721.98 192.537 2 0 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84.0412 1 0 7 14-124.234 116.109 5 0 -7 -14 29.6185 17.4270 1 0 -7 -15 170.824 70.7233 1 0 8 -11 4.53104 18.5747 1 0 -8 10 410.040 214.755 6 0 8 -10 250.728 95.3814 1 0 8 -9 549.126 128.916 1 0 -8 9 731.609 259.397 6 0 8 -8 280.150 85.6807 1 0 -8 8 354.831 163.665 6 0 -8 7 53.7430 88.6676 6 0 8 -7 21.9452 28.1193 1 0 -8 6 418.535 167.487 6 0 8 -6 160.912 60.0564 1 0 -8 5 63.3521 61.4813 6 0 8 -4 654.307 111.138 1 0 -8 4 735.964 80.0487 2 0 -8 4 689.919 199.372 6 0 -8 3-38.6990 34.2183 6 0 -8 3 41.9766 15.5358 2 0 8 -3 17.9745 21.7510 1 0 -8 3 55.7463 30.3983 2 0 -8 3 44.7532 17.2289 4 0 -8 2 1283.68 147.211 4 0 8 -2 1375.30 97.2032 1 0 -8 2 1597.21 288.014 6 0 -8 1 875.827 126.496 4 0 -8 1 917.446 206.425 6 0 -8 0 1829.11 179.506 4 0 -8 0 1939.09 280.013 6 0 8 1 502.832 128.704 5 0 -8 -1 766.641 167.171 6 0 -8 -1 524.812 98.8072 4 0 8 2 52.6382 46.6450 5 0 -8 -2-49.9025 53.1613 6 0 -8 -2-16.4943 32.2360 4 0 -8 -3-6.33910 20.7869 6 0 8 3-10.2520 48.5392 5 0 -8 -4 185.126 52.0536 3 0 8 4 127.632 77.4773 6 0 8 4 135.765 52.1745 2 0 -8 -4 89.5917 59.8467 6 0 8 4 260.031 111.702 5 0 8 5 25.4507 22.8831 6 0 8 5 35.7487 47.5432 5 0 -8 -5 2.99504 17.5582 3 0 -8 -5 30.0487 10.3620 1 0 8 5 7.54357 20.4782 2 0 -8 -5 8.33377 31.4260 6 0 8 6 998.848 220.056 5 0 8 6 703.553 160.733 6 0 -8 -6 843.152 74.3282 1 0 8 6 811.488 130.919 2 0 8 7 312.571 88.3179 2 0 -8 -7 366.031 56.2448 1 0 8 7 256.064 96.8142 6 0 8 7 445.493 152.542 5 0 8 8 775.437 165.736 6 0 -8 -8 856.057 95.7332 1 0 8 8 769.637 144.499 2 0 8 8 745.426 211.804 5 0 8 9 288.243 143.205 5 0 -8 -9 334.798 66.0238 1 0 8 9 168.625 77.9434 6 0 8 9 256.752 87.6412 2 0 -8 -10 39.7818 30.9956 1 0 8 10-30.2603 53.2246 5 0 -8 -11 44.3047 34.9578 1 0 8 11 7.18103 41.3721 5 0 8 12 48.1400 55.5405 5 0 -8 -12 187.682 58.1635 1 0 8 13 81.0728 78.5453 5 0 -8 -13 168.752 62.5717 1 0 8 14 525.140 240.926 5 0 -8 -14 283.819 85.6170 1 0 -8 -15 229.994 84.2571 1 0 -9 8 612.551 231.319 6 0 -9 7 179.007 109.910 6 0 9 -6 280.133 83.5759 1 0 -9 6 307.221 146.664 6 0 -9 5 734.734 238.662 6 0 9 -4 222.806 69.0064 1 0 -9 4 301.540 145.912 6 0 -9 3 157.096 84.8780 6 0 9 -3 75.6167 30.4966 1 0 -9 2 328.638 138.568 6 0 -9 1 61.1210 67.6465 6 0 -9 0 132.709 91.3988 6 0 -9 -1 232.421 98.8974 6 0 9 2 1438.71 238.808 5 0 -9 -2 1455.05 232.224 6 0 -9 -3 1600.29 236.263 6 0 9 3 1573.62 254.954 5 0 -9 -3 1727.44 172.076 3 0 -9 -4 384.543 81.2186 3 0 -9 -4 354.621 113.970 6 0 9 4 418.544 130.563 5 0 -9 -5 33.9528 17.9792 6 0 9 5 66.7527 77.7631 5 0 9 5 73.7156 39.8959 2 0 -9 -5 60.8553 23.7420 3 0 9 6 127.800 83.5089 6 0 -9 -6 73.9309 20.4951 1 0 9 6 108.876 59.8118 2 0 9 6 41.2869 69.1865 5 0 -9 -7 255.432 44.0885 1 0 9 7 400.507 128.628 5 0 9 7 367.979 128.878 6 0 9 8 919.366 232.411 5 0 -9 -8 876.740 95.9252 1 0 9 9 1719.28 339.176 5 0 -9 -9 1460.80 137.010 1 0 -9 -10 329.080 70.9438 1 0 9 10 287.853 147.963 5 0 9 11 366.865 176.384 5 0 9 12 50.8886 72.2546 5 0 -10 7-3.15940 38.9874 6 0 -10 6-14.8135 54.9137 6 0 -10 5 414.577 181.797 6 0 -10 4-75.8767 107.764 6 0 -10 3 91.3141 79.7823 6 0 -10 2 201.587 112.436 6 0 -10 1-169.940 99.5133 6 0 -10 0 55.1891 62.4578 6 0 -10 -1 185.837 100.900 6 0 10 2 1381.54 249.671 5 0 -10 -2 1168.80 226.482 6 0 10 3 829.018 189.371 5 0 -10 -3 738.371 119.657 3 0 -10 -3 943.642 197.411 6 0 -10 -4 911.819 184.441 6 0 -10 -4 1137.37 146.003 3 0 10 4 802.907 202.420 5 0 10 5 298.642 134.099 5 0 -10 -5 484.762 93.4589 3 0 -10 -5 547.568 138.201 6 0 -10 -6 498.659 126.167 6 0 10 6 131.127 85.5937 5 0 10 7-32.0456 78.1299 5 0 10 8 2.27112 43.5644 5 0 10 9 54.3350 70.3919 5 0 10 10 179.329 116.944 5 0 10 11 267.312 173.042 5 0 -11 5 11.6899 42.8244 6 0 -11 4 486.436 191.037 6 0 -11 3 357.651 165.726 6 0 -11 2 925.973 244.221 6 0 -11 1-34.5824 61.5754 6 0 -11 0 150.486 95.1751 6 0 -11 -1-72.9317 63.8527 6 0 -11 -2 216.502 100.910 6 0 -11 -3 0.32925 46.8716 6 0 -11 -3 93.1245 50.1023 3 0 11 3-21.5114 38.6157 5 0 11 4 807.972 213.590 5 0 -11 -4 648.908 162.525 6 0 -11 -5 476.672 138.973 6 0 11 5 442.810 166.331 5 0 11 6 54.1539 62.8812 5 0 -11 -6 44.3465 41.8924 6 0 11 7 138.976 108.504 5 0 11 8 5.83964 44.7964 5 0 11 9 132.970 101.673 5 0 -12 4 302.281 166.184 6 0 -12 3 197.610 117.376 6 0 -12 2 276.498 146.278 6 0 -12 1-72.3267 70.4316 6 0 -12 0 193.744 109.466 6 0 -12 -1 25.5298 72.4806 6 0 -12 -2 132.493 85.7180 6 0 -12 -3 87.2409 68.4561 6 0 12 4 36.1386 51.9167 5 0 -12 -4 134.330 80.1479 6 0 12 5 725.829 211.170 5 0 -13 1 187.061 122.057 6 0 -13 0 265.884 134.278 6 0 -13 -1 523.902 188.649 6 1 -13 -2 88.9377 77.4531 6 1 -13 -1 84.0634 70.6046 6 1 -13 0 105.401 89.0084 6 1 -12 -4 516.341 160.525 6 1 -12 -3-14.0064 33.0068 6 1 -12 -2 104.023 81.9312 6 1 -12 -1-56.3447 64.8694 6 1 -12 0 31.6522 50.4394 6 1 -12 1 162.135 98.2686 6 1 -12 2-143.579 106.029 6 -1 11 8-1.54338 53.0589 5 -1 11 7-122.723 94.1283 5 1 -11 -6 75.8106 51.9155 6 -1 11 6 98.3832 75.1628 5 -1 11 5 213.518 101.453 5 1 -11 -5 168.225 86.8451 6 1 -11 -4 216.762 101.940 6 -1 11 4 457.126 151.019 5 1 -11 -3 538.856 164.934 6 -1 11 3 599.250 181.707 5 1 -11 -2 102.529 76.1502 6 1 -11 -1 128.543 88.5082 6 1 -11 0-28.7756 41.1968 6 1 -11 1-235.035 125.312 6 1 -11 2 163.186 96.8874 6 1 -11 3 136.492 104.662 6 1 -11 4 1092.47 299.273 6 1 -11 5 196.479 147.164 6 -1 10 10 239.258 140.611 5 -1 10 9 687.723 235.915 5 -1 10 8 417.704 174.087 5 -1 10 7 306.911 139.610 5 -1 10 6-66.3789 67.2141 5 1 -10 -6 46.5840 52.4750 6 -1 10 5-36.9321 53.9583 5 1 -10 -5 97.7497 63.2385 6 1 -10 -4 775.400 179.021 6 -1 10 4 847.923 213.266 5 1 -10 -4 574.779 95.9676 3 -1 10 3 909.487 213.077 5 1 -10 -3 950.762 209.132 6 -1 10 2 1352.60 256.847 5 1 -10 -2 1555.73 277.820 6 1 -10 -1 1203.27 249.488 6 1 -10 0 144.858 92.0779 6 1 -10 1 189.574 104.473 6 1 -10 2 71.0464 48.5107 6 1 -10 3 235.178 162.783 6 1 -10 4 291.019 149.865 6 1 -10 5-135.415 107.792 6 1 -10 6 62.3260 81.6914 6 -1 9 11 194.992 148.401 5 -1 9 10-48.2064 66.6197 5 -1 9 9 261.965 143.358 5 -1 9 8 432.726 172.879 5 -1 9 7 912.779 233.705 5 -1 9 6 997.038 239.449 5 1 -9 -5 436.439 122.580 6 1 -9 -5 236.187 52.4202 3 -1 9 5 261.207 103.578 5 -1 9 4 580.127 167.102 5 1 -9 -4 393.746 125.486 6 1 -9 -4 521.156 83.2839 3 1 -9 -3 435.845 141.094 6 -1 9 3 290.685 118.132 5 1 -9 -2-5.37310 37.1211 6 -1 9 2 182.196 93.6390 5 1 -9 -1 571.600 162.445 6 -1 9 1 571.715 146.026 5 1 -9 0 1061.73 232.800 6 1 -9 1 772.159 205.003 6 1 -9 2 162.153 75.4038 6 1 -9 3-74.7661 70.2945 6 1 -9 4 112.954 107.205 6 1 -9 5-38.9347 63.6873 6 1 -9 6 64.1969 79.4906 6 1 -9 7-6.84337 43.5593 6 1 -9 8 196.538 145.684 6 -1 8 13 312.272 189.920 5 1 -8 -13 404.753 100.318 1 1 -8 -12 659.473 124.305 1 -1 8 12 477.498 249.764 5 1 -8 -11 327.509 80.5475 1 -1 8 11 265.881 153.812 5 1 -8 -10 422.615 86.7004 1 -1 8 10 818.784 247.423 5 -1 8 9 279.834 134.316 5 1 -8 -9 167.651 50.3708 1 -1 8 8 78.7526 103.028 5 1 -8 -8 99.8129 39.3312 1 -1 8 8 51.6715 35.4746 2 -1 8 8 50.1869 64.8071 6 -1 8 7 152.868 58.1514 2 -1 8 7-55.1821 87.8851 5 -1 8 7 26.7594 36.2456 6 1 -8 -7 208.057 48.5731 1 -1 8 6 215.909 96.2951 6 -1 8 6 165.294 100.215 5 1 -8 -6 157.921 35.4231 1 -1 8 6 267.139 69.7900 2 -1 8 5 285.855 114.759 6 -1 8 5 298.739 116.993 5 1 -8 -5 235.241 44.3291 3 -1 8 5 181.240 49.9019 2 1 -8 -5 239.364 87.7470 6 -1 8 4 88.1953 53.1594 5 1 -8 -4 192.261 91.0441 6 1 -8 -4 111.602 39.6391 3 -1 8 4 125.537 86.3153 6 -1 8 3 1307.07 242.071 6 -1 8 3 1711.87 258.511 5 1 -8 -3 1508.02 227.691 6 -1 8 2 184.999 88.9013 5 1 -8 -2 134.726 75.4786 6 1 -8 -1 37.6188 40.1298 6 -1 8 1 123.711 81.1023 5 1 -8 0-50.2925 57.9367 6 1 -8 1 310.961 122.725 6 1 -8 2 56.9122 30.2381 6 -1 8 -3 1720.17 141.662 1 1 -8 3 1612.97 299.805 6 1 -8 4 1071.86 261.873 6 -1 8 -4 1070.42 124.388 1 1 -8 5 605.604 207.965 6 -1 8 -6 21.4644 29.8979 1 1 -8 6 20.0085 55.8569 6 1 -8 7 159.346 103.340 6 -1 8 -7 93.9091 44.5771 1 1 -8 8 323.546 168.728 6 -1 8 -8 47.4007 30.6703 1 1 -8 9 129.920 113.610 6 -1 8 -9 181.689 67.0866 1 -1 8 -10 263.808 91.2247 1 1 -7 -15 89.1122 58.0277 1 -1 7 14 368.194 206.695 5 1 -7 -14 342.707 101.539 1 1 -7 -13 605.460 120.637 1 -1 7 13 699.133 260.898 5 1 -7 -12 852.507 137.331 1 -1 7 12 1046.53 321.748 5 1 -7 -11 66.5551 30.8504 1 -1 7 11 345.817 180.711 5 -1 7 10 69.3682 105.408 5 1 -7 -10 41.4804 10.8237 1 -1 7 9 135.170 70.9506 6 1 -7 -9 15.3629 15.8861 1 -1 7 9 99.8637 118.032 5 -1 7 8 91.6057 90.4509 5 -1 7 8 54.3144 47.8760 6 -1 7 8 26.5208 27.3849 2 1 -7 -8 46.6361 26.2729 1 -1 7 7 126.246 84.0737 5 -1 7 7 37.3523 22.3300 2 1 -7 -7 74.0191 31.2066 1 -1 7 7 40.6698 40.0832 6 -1 7 6 121.449 48.0502 2 -1 7 6 59.6110 48.3807 6 -1 7 6 193.056 101.587 5 1 -7 -6 82.2919 27.3192 1 1 -7 -5 45.7248 19.3419 1 -1 7 5 19.5643 58.7151 5 1 -7 -5 174.133 73.4247 6 -1 7 5 47.2944 29.8578 2 -1 7 5 52.7387 57.5874 6 -1 7 4 996.884 200.427 6 1 -7 -4 1046.66 95.5951 3 1 -7 -4 1017.14 166.598 6 -1 7 4 1027.87 204.231 5 -1 7 4 863.605 92.1400 2 -1 7 3 3912.03 380.338 5 -1 7 3 4110.64 399.960 6 1 -7 -3 3532.57 328.255 6 1 -7 -2 1385.64 208.745 6 -1 7 2 1491.26 242.234 6 -1 7 2 1213.10 195.905 5 -1 7 1 92.1071 55.8538 5 1 -7 -1 94.3846 64.5619 6 1 -7 0 40.1677 44.5187 6 -1 7 0 45.0798 52.1902 5 1 -7 1 134.591 79.6060 6 -1 7 -2 253.874 43.8171 1 1 -7 2 172.084 74.6372 6 1 -7 3 83.5063 79.0901 6 -1 7 -3 106.626 34.0020 1 1 -7 3 96.5852 28.6673 2 1 -7 4 2501.66 165.149 2 1 -7 4 2624.66 386.632 6 -1 7 -4 2429.19 169.442 1 1 -7 5 1085.21 119.740 2 1 -7 5 1102.88 259.901 6 1 -7 6 1118.25 134.522 2 1 -7 6 1756.10 352.408 6 -1 7 -7 139.279 50.7819 1 1 -7 7 254.484 149.836 6 -1 7 -8-30.4908 26.7413 1 1 -7 8 9.51019 48.2700 6 -1 7 -9 179.655 64.9177 1 1 -7 9 386.581 215.748 6 1 -7 10 61.0793 82.8478 6 -1 7 -10 93.5981 47.5823 1 1 -7 11-138.141 121.641 6 -1 7 -11 50.6799 43.4629 1 -1 7 -12 10.7737 21.6226 1 -1 7 -13 3.16816 11.3322 1 1 -6 -15 23.6624 25.5441 1 1 -6 -14-13.0452 25.0036 1 1 -6 -13 645.437 126.590 1 1 -6 -12-16.2985 15.4647 1 -1 6 12 96.3013 99.0132 5 -1 6 11 254.913 147.127 5 1 -6 -11 97.6056 41.3615 1 1 -6 -10 1676.88 167.245 1 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545.809 134.417 6 1 -6 1 471.553 138.400 6 1 -6 1 518.988 125.907 5 -1 6 -2 300.076 44.5350 1 1 -6 2 229.396 78.2668 5 1 -6 2 215.977 97.8008 6 1 -6 2 151.480 25.5931 2 1 -6 3 282.407 46.2596 2 1 -6 3 201.990 77.4478 5 1 -6 3 333.237 143.246 6 -1 6 -3 431.174 59.1321 1 1 -6 4 1934.50 319.342 6 -1 6 -4 1460.20 120.507 1 1 -6 4 1482.43 120.901 2 1 -6 4 1396.31 203.261 5 1 -6 5 3256.31 426.974 6 1 -6 5 2269.99 259.339 5 1 -6 5 2348.01 168.250 2 1 -6 6 989.495 120.644 2 1 -6 6 1202.09 269.222 6 -1 6 -6 907.194 112.489 1 1 -6 7 675.457 108.611 2 -1 6 -7 718.297 109.328 1 1 -6 7 847.238 243.560 6 -1 6 -8 15.2243 21.3111 1 1 -6 8-2.60871 7.72108 2 -1 6 -9 125.329 50.0242 1 -1 6 -10-22.6597 31.8788 1 -1 6 -11-45.2782 36.0341 1 -1 6 -12-42.1556 37.6187 1 -1 6 -13 28.5871 31.4211 1 1 -5 -15-47.0385 39.4587 1 1 -5 -14 74.3203 40.0174 1 1 -5 -13-21.3019 28.2825 1 1 -5 -12 117.496 52.1515 1 1 -5 -11-26.8929 34.3546 1 1 -5 -10 57.4793 28.3187 1 -1 5 10 84.0304 53.1956 6 1 -5 -9 3293.89 218.630 1 -1 5 9 3461.59 349.093 6 -1 5 8 1509.58 222.305 6 -1 5 8 1384.65 151.559 2 1 -5 -8 1396.53 132.042 1 -1 5 8 1546.41 145.671 4 -1 5 7 4794.40 259.307 2 1 -5 -7 4635.29 221.826 1 -1 5 7 5864.68 547.263 5 -1 5 7 5058.76 257.690 4 1 -5 -6 686.774 78.8478 1 -1 5 6 1025.16 213.815 5 -1 5 6 676.628 87.2737 2 -1 5 6 782.691 99.9709 4 1 -5 -5 290.551 44.8292 1 -1 5 5 453.613 73.2334 4 -1 5 5 331.801 55.0991 2 -1 5 5 408.745 130.174 5 -1 5 5 222.571 84.7443 6 -1 5 4 192.078 70.6759 6 1 -5 -4 211.892 66.6838 6 -1 5 4 189.051 38.0564 2 -1 5 4 220.038 105.479 5 -1 5 4 261.555 56.0847 4 1 -5 -4 151.402 30.0945 1 1 -5 -4 224.382 29.0803 3 -1 5 3 77.6253 52.7283 6 -1 5 3 48.7281 22.4263 4 1 -5 -3 65.2411 48.0899 6 -1 5 3 38.0290 15.5035 2 1 -5 -3 36.0600 11.8018 1 -1 5 3 65.5497 63.0999 5 -1 5 2 813.213 150.727 5 -1 5 2 749.587 142.701 6 -1 5 2 965.301 99.6437 4 1 -5 -2 810.278 135.288 6 -1 5 2 836.477 54.1586 2 -1 5 1 132.065 36.6097 4 -1 5 1 85.8718 50.9557 6 1 -5 -1 125.028 44.8951 6 1 -5 -1 45.6587 18.9369 5 -1 5 1 76.7168 52.3235 5 1 -5 0 53.1688 50.5771 6 1 -5 0 29.6265 34.2804 5 -1 5 0 28.2935 18.7501 4 -1 5 0 9.34696 23.7576 5 -1 5 -1 2600.45 229.327 5 -1 5 -1 2273.49 87.7552 1 1 -5 1 1711.08 209.256 5 1 -5 1 2533.99 287.777 6 -1 5 -2 3879.32 139.762 1 1 -5 2 4332.69 390.365 6 1 -5 2 3608.13 140.665 2 1 -5 2 3814.97 303.040 5 1 -5 3 964.074 202.648 6 1 -5 3 817.177 76.5110 2 -1 5 -3 807.656 75.0647 1 1 -5 3 753.153 133.526 5 -1 5 -4 765.899 80.4607 1 1 -5 4 676.536 78.9334 2 1 -5 4 705.672 128.035 5 1 -5 4 1102.31 226.797 6 1 -5 5 197.711 71.9950 5 1 -5 5 1.03059 12.4324 2 1 -5 6 9.68082 12.2620 2 1 -5 6 11.9971 27.9772 5 -1 5 -7 368.325 73.2271 1 1 -5 7 380.813 78.7227 2 -1 5 -8 434.152 84.4434 1 1 -5 8 440.350 90.8985 2 -1 5 -9 942.506 134.411 1 -1 5 -10 156.280 57.3235 1 -1 5 -11 286.088 84.9137 1 -1 5 -12 60.7009 46.5439 1 -1 5 -13-25.4819 30.8338 1 -1 5 -14-29.9475 34.5336 1 1 -4 -15 267.619 90.1428 1 1 -4 -14 294.124 87.3313 1 1 -4 -13 1354.24 182.239 1 1 -4 -12 5.62000 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275.639 73.7266 1 -1 -3 -13-0.30574 24.3037 1 -1 -3 -14 552.196 118.370 1 -1 -3 -15 106.862 51.2424 1 1 4 -14 138.163 73.1399 1 1 4 -13 119.834 62.9372 1 1 4 -12 94.3422 55.4729 1 1 4 -11-24.2564 33.9045 1 1 4 -10-18.5293 36.7272 1 -1 -4 9 150.626 23.6153 4 1 4 -9 182.792 60.2736 1 -1 -4 8 964.393 122.599 2 1 4 -8 950.341 131.652 1 -1 -4 7 3183.90 208.114 2 1 4 -7 2714.37 210.669 1 1 4 -6 3974.73 237.589 1 -1 -4 6 4428.33 225.060 1 -1 -4 5 1581.98 123.944 1 -1 -4 4 1143.95 98.0030 1 1 4 -4 1273.69 118.867 1 1 4 -3 1483.77 126.283 1 -1 -4 3 1513.24 104.326 1 1 4 -2 14.2180 22.2131 1 -1 -4 2 17.3985 11.4098 1 1 4 -1 25.6687 23.9691 1 -1 -4 1 26.4213 15.9885 1 -1 -4 0 973.585 125.069 2 -1 -4 0 770.613 68.6412 1 -1 -4 -1 5824.58 196.835 1 1 4 1 6622.26 329.528 2 -1 -4 -1 7064.08 306.374 6 1 4 1 6200.90 311.976 5 -1 -4 -1 6122.15 223.121 2 1 4 2 3349.12 208.620 2 -1 -4 -2 4132.57 166.259 2 -1 -4 -2 4417.04 189.285 3 1 4 2 3926.11 259.994 5 -1 -4 -2 3915.04 193.668 6 -1 -4 -3 520.503 66.3262 6 1 4 3 455.726 72.3790 2 1 4 3 493.292 68.9440 6 1 4 3 538.899 107.029 5 -1 -4 -3 545.712 60.8707 2 -1 -4 -3 512.628 68.6953 3 1 4 4 80.0227 50.6388 5 1 4 4 87.5130 24.3107 3 -1 -4 -4 84.8693 26.7987 2 1 4 4 80.2251 32.8096 2 1 4 4 86.1829 31.9726 6 1 4 5 4506.51 252.425 2 -1 -4 -5 4252.78 195.196 4 1 4 5 5371.14 203.506 3 1 4 5 4272.89 220.788 6 1 4 5 5136.98 393.358 5 -1 -4 -5 4829.30 199.210 2 1 4 6 456.172 82.9308 2 1 4 6 523.008 131.305 5 1 4 6 389.659 68.3562 6 -1 -4 -6 502.194 67.9396 2 -1 -4 -7 144.642 40.3911 2 1 4 7 145.582 49.7282 2 -1 -4 -8 2315.40 157.902 1 -1 -4 -8 2696.89 186.791 2 1 4 8 2554.42 225.152 2 -1 -4 -9 3730.83 215.477 1 -1 -4 -10 1706.11 155.949 1 -1 -4 -11 2402.23 202.680 1 -1 -4 -12 346.304 83.2717 1 -1 -4 -13 80.4865 46.4649 1 -1 -4 -14 46.7115 36.8521 1 -1 -4 -15-32.3244 31.6334 1 -1 -4 -16 9.70790 20.4296 1 1 5 -13 179.533 87.6561 1 1 5 -12 152.099 66.8317 1 1 5 -11 425.785 111.063 1 1 5 -10 154.744 67.2114 1 1 5 -9 130.779 59.3036 1 -1 -5 9 122.228 26.3226 4 -1 -5 8 16.0915 12.6254 4 1 5 -8-16.2789 19.2970 1 1 5 -7 469.574 93.1597 1 -1 -5 7 432.593 79.0504 2 -1 -5 7 357.451 48.3485 4 -1 -5 6 2637.46 134.478 4 -1 -5 6 2423.82 170.882 2 1 5 -6 2509.82 203.591 1 -1 -5 5 1298.39 115.486 1 -1 -5 4 877.731 87.8260 1 1 5 -4 904.566 109.824 1 1 5 -3 479.761 77.8559 1 -1 -5 3 385.364 53.4181 1 -1 -5 2 183.203 34.1300 1 1 5 -2 183.790 41.3206 1 -1 -5 1 495.207 51.6021 1 -1 -5 1 519.107 100.434 2 1 5 -1 455.017 66.5347 1 -1 -5 0 42.4613 47.7465 6 -1 -5 0 25.4138 14.3721 1 -1 -5 0 15.6345 18.2409 4 -1 -5 0 12.4348 26.6594 2 -1 -5 -1 2432.05 139.027 2 1 5 1 2667.77 228.428 5 -1 -5 -1 2664.15 137.807 1 -1 -5 -1 2887.29 231.211 6 1 5 2 1056.35 141.196 2 -1 -5 -2 1101.22 125.363 6 -1 -5 -2 1171.37 109.006 3 -1 -5 -2 1039.61 85.1153 2 1 5 2 1179.59 159.974 5 -1 -5 -3 904.134 95.9010 3 1 5 3 699.924 99.5182 2 -1 -5 -3 715.752 68.9341 2 1 5 3 670.501 118.535 5 1 5 3 711.020 104.550 6 -1 -5 -3 720.600 92.5677 6 1 5 4 2151.34 172.508 6 1 5 4 2186.99 240.624 5 1 5 4 2325.93 187.150 2 -1 -5 -4 2348.88 130.201 2 -1 -5 -4 2367.15 158.920 6 1 5 5 3014.01 221.786 2 -1 -5 -5 3199.84 161.506 2 1 5 5 3544.84 328.136 5 1 5 5 2863.08 199.458 6 1 5 6 189.500 39.1391 3 1 5 6 248.343 102.315 5 -1 -5 -6 157.864 39.3694 2 1 5 6 162.183 54.7846 2 1 5 6 150.974 47.5770 6 -1 -5 -7 2428.90 174.623 4 1 5 7 2486.69 205.339 6 1 5 7 2705.78 155.486 3 -1 -5 -7 2722.60 174.540 2 1 5 7 2881.16 238.848 2 1 5 7 3078.13 367.838 5 -1 -5 -8 1462.42 136.452 2 -1 -5 -8 1442.90 123.661 1 1 5 8 1987.30 297.840 5 1 5 8 1444.54 165.581 6 1 5 8 1418.21 128.090 3 1 5 8 1406.82 175.963 2 1 5 9-15.5757 31.8871 6 -1 -5 -9 26.0920 18.2483 1 1 5 9 58.0591 61.1521 5 -1 -5 -10 21.7020 14.3256 1 1 5 11 2965.98 302.930 6 -1 -5 -11 2724.06 212.298 1 -1 -5 -12 393.887 88.2856 1 -1 -5 -13 93.7523 41.4780 1 -1 -5 -14 392.230 96.7670 1 -1 -5 -15 47.5227 48.2111 1 -1 -5 -16 41.0000 35.3518 1 1 6 -13 233.564 99.4143 1 1 6 -12 480.481 133.583 1 1 6 -11 891.271 169.179 1 1 6 -10 299.196 94.3904 1 1 6 -9-48.8887 41.0650 1 -1 -6 9-12.9952 11.9300 4 -1 -6 8 206.962 40.5527 4 1 6 -8 170.350 61.7286 1 1 6 -7 48.0871 32.2716 1 -1 -6 7 82.6240 34.4194 2 -1 -6 7 74.1229 26.9954 4 1 6 -6-19.5946 22.7108 1 -1 -6 6 14.8392 9.34864 4 -1 -6 6 1.15516 9.64760 2 -1 -6 5 1002.39 97.9716 4 -1 -6 5 813.596 93.8526 2 -1 -6 4 69.6083 43.1619 5 -1 -6 4 44.0851 23.5885 1 -1 -6 4 70.5857 30.0595 4 -1 -6 3 932.067 153.495 5 -1 -6 3 1145.58 93.0792 1 1 6 -3 1227.80 135.078 1 -1 -6 3 1246.31 108.912 4 -1 -6 2 341.531 47.0292 1 -1 -6 2 377.626 61.0095 4 1 6 -2 407.952 73.3392 1 -1 -6 2 364.803 103.049 5 -1 -6 1 1051.82 145.967 2 -1 -6 1 927.636 69.8190 1 1 6 -1 786.918 86.1299 1 -1 -6 1 931.267 168.716 6 -1 -6 1 938.216 98.7676 4 -1 -6 0 790.701 92.6843 4 -1 -6 0 773.005 60.3609 1 -1 -6 0 819.564 95.2859 2 -1 -6 0 861.351 157.795 6 -1 -6 -1 95.3209 22.9831 1 -1 -6 -1 117.391 44.0531 6 -1 -6 -1 68.5810 25.6930 4 1 6 1 20.3847 21.7230 5 -1 -6 -1 51.9269 18.3080 2 -1 -6 -2 2908.03 134.829 2 -1 -6 -2 2838.37 151.292 1 -1 -6 -2 2841.25 232.352 6 1 6 2 2789.47 254.146 5 1 6 2 2860.58 236.486 2 -1 -6 -3 2012.91 157.147 3 -1 -6 -3 1799.73 173.830 6 1 6 3 1873.96 220.828 5 -1 -6 -3 1753.48 105.142 2 1 6 3 1545.00 175.827 2 -1 -6 -4 8394.92 329.158 3 -1 -6 -4 8377.01 350.255 6 1 6 4 8388.40 486.993 5 1 6 4 8712.22 404.961 6 1 6 4 7592.99 361.278 2 -1 -6 -4 8474.07 246.924 2 1 6 5 2511.59 289.361 5 1 6 5 1843.48 184.869 2 -1 -6 -5 2258.02 136.320 2 1 6 5 2025.57 195.244 6 1 6 6 1463.56 174.864 2 -1 -6 -6 1149.17 126.480 4 1 6 6 1528.95 248.336 5 1 6 6 1333.94 157.098 6 -1 -6 -6 1457.24 118.816 2 -1 -6 -7 923.152 117.551 4 1 6 7 1011.28 210.329 5 1 6 7 1095.39 143.050 6 1 6 7 1348.68 176.082 2 -1 -6 -7 1222.36 105.751 1 -1 -6 -7 1198.06 115.351 2 -1 -6 -8 146.971 42.5290 1 1 6 8 189.389 65.8801 2 1 6 8 111.382 47.3630 6 1 6 8 181.506 117.886 5 -1 -6 -9 8.00048 13.4927 1 1 6 9 32.6346 72.8815 5 1 6 9 59.0380 40.0895 6 1 6 9 10.6552 13.3084 3 1 6 10 330.842 58.1873 3 -1 -6 -10 279.372 63.4384 1 1 6 10 465.031 171.802 5 -1 -6 -11 278.148 69.3525 1 1 6 11 352.539 174.405 5 1 6 12-95.5297 90.1195 5 -1 -6 -12 84.9165 36.0960 1 1 6 13 28.9806 88.9463 5 -1 -6 -13 39.7633 22.4572 1 1 6 14 773.209 254.940 5 -1 -6 -14 483.604 107.516 1 -1 -6 -15 198.031 73.9441 1 1 6 15 196.314 168.293 5 1 6 16 154.527 152.624 5 -1 -6 -16 70.8934 53.9962 1 1 7 -13 91.9343 68.1046 1 1 7 -12 39.5650 56.9851 1 1 7 -11-14.7407 28.3314 1 1 7 -10 51.3234 48.4153 1 1 7 -9 740.567 149.106 1 -1 -7 8 187.556 43.6908 4 1 7 -8 181.152 65.4286 1 1 7 -7 26.7494 31.0071 1 -1 -7 7 50.6775 21.5477 4 -1 -7 7 39.9390 24.3807 2 -1 -7 6 123.692 40.5417 2 -1 -7 6 100.798 34.4920 4 1 7 -6 71.7157 46.9395 1 -1 -7 5 1016.62 108.171 4 -1 -7 5 925.069 100.032 2 -1 -7 4 477.740 65.2861 2 -1 -7 4 442.226 74.0680 4 -1 -7 3 99.7414 34.0835 4 1 7 -3 93.9489 40.2108 1 -1 -7 2 2381.21 171.442 4 -1 -7 2 3081.61 357.037 6 -1 -7 2 2354.61 233.989 2 -1 -7 2 2392.02 122.280 1 1 7 -2 2230.05 183.126 1 -1 -7 1 4482.38 412.107 6 -1 -7 1 3300.65 332.951 5 -1 -7 1 4015.35 262.917 2 -1 -7 1 3818.98 138.489 1 -1 -7 1 4032.91 223.310 4 -1 -7 0 5629.60 269.268 4 -1 -7 0 5336.98 215.971 2 -1 -7 0 5187.08 423.284 5 -1 -7 0 6038.05 444.882 6 -1 -7 0 5520.52 148.240 1 -1 -7 -1 1741.12 151.887 4 -1 -7 -1 1564.26 96.2426 2 -1 -7 -1 1206.54 208.419 5 -1 -7 -1 1538.51 207.322 6 -1 -7 -1 1535.25 75.1144 1 1 7 1 1625.16 210.633 5 1 7 2 1522.19 208.638 5 -1 -7 -2 1616.22 95.0789 1 -1 -7 -2 1663.35 254.805 5 -1 -7 -2 1507.53 141.119 4 -1 -7 -2 1386.53 182.113 6 -1 -7 -2 1538.71 90.3817 2 -1 -7 -3 688.227 101.368 3 -1 -7 -3 562.100 68.6487 1 -1 -7 -3 628.029 113.814 6 -1 -7 -3 578.914 154.909 5 1 7 3 719.651 128.814 2 -1 -7 -3 687.850 97.2113 4 1 7 3 672.700 138.072 5 -1 -7 -3 645.802 60.8456 2 -1 -7 -4 305.654 44.8245 2 -1 -7 -4 166.790 55.4744 6 -1 -7 -4 285.454 65.3145 3 1 7 4 206.208 76.0396 5 1 7 4 206.767 71.5534 2 -1 -7 -4 237.178 56.0265 4 1 7 5 43.2803 55.9807 5 -1 -7 -5 69.2809 24.3392 2 -1 -7 -5 92.7965 51.8316 6 1 7 5 25.0332 34.9164 2 1 7 5 84.4674 45.2184 6 -1 -7 -5 65.5505 33.8024 4 -1 -7 -6 1425.60 119.509 2 -1 -7 -6 1057.59 138.615 4 -1 -7 -6 1413.80 101.624 1 1 7 6 1396.07 178.697 6 1 7 6 1256.73 170.878 2 1 7 6 1638.17 253.842 5 1 7 7 1455.77 192.082 2 -1 -7 -7 1625.81 171.120 4 -1 -7 -7 1638.85 120.528 1 1 7 7 1879.35 296.192 5 1 7 7 1232.85 170.652 6 1 7 8 1158.66 167.567 6 1 7 8 1295.12 190.503 2 -1 -7 -8 1321.95 119.139 1 1 7 8 1312.55 254.134 5 -1 -7 -9 265.287 57.5586 1 1 7 9 269.932 87.0740 6 1 7 9 346.258 131.165 5 1 7 10 108.799 48.5881 5 -1 -7 -10 164.314 48.8857 1 -1 -7 -11 8.68439 12.7985 1 1 7 11-57.2540 106.708 5 1 7 12 203.826 131.711 5 -1 -7 -12 27.2644 28.3939 1 -1 -7 -13 37.4645 30.5415 1 1 7 13 205.552 134.793 5 -1 -7 -14 86.9521 52.1508 1 1 7 14 145.366 74.2678 5 1 7 15 516.013 251.363 5 -1 -7 -15 320.720 90.4240 1 1 8 -12 86.0657 62.7606 1 1 8 -11 93.8733 63.1689 1 1 8 -10 277.855 101.487 1 1 8 -9 10.0339 20.5372 1 1 8 -8 23.2535 18.2493 1 1 8 -7 510.399 120.429 1 -1 -8 7 473.472 81.3617 4 -1 -8 6 1051.71 122.560 4 1 8 -6 1065.59 168.781 1 -1 -8 5 606.761 92.4327 4 -1 -8 5 571.625 78.4667 2 1 8 -5 710.105 130.430 1 -1 -8 4 61.2212 58.9093 6 -1 -8 4 9.45345 9.91307 2 -1 -8 4 41.8015 22.7256 4 1 8 -3 58.8006 37.8953 1 -1 -8 3 25.2555 32.2528 2 -1 -8 3-0.20042 8.45154 2 -1 -8 3 10.9753 49.2175 6 -1 -8 3 25.2049 22.0607 4 -1 -8 2-10.6924 37.6184 6 -1 -8 2 42.9646 29.8919 4 -1 -8 2 35.5959 35.0924 2 1 8 -2-11.6074 8.19197 1 -1 -8 1 775.315 89.8940 2 -1 -8 1 923.784 197.870 6 -1 -8 1 817.622 112.634 4 -1 -8 0 2167.40 282.602 6 -1 -8 0 2024.50 176.661 4 -1 -8 0 1964.18 103.109 2 -1 -8 -1 3998.61 85.8431 1 -1 -8 -1 4198.80 120.948 2 -1 -8 -1 4242.82 259.805 4 -1 -8 -1 4501.78 384.968 6 -1 -8 -2 1881.83 175.210 4 -1 -8 -2 1931.96 85.4532 2 -1 -8 -2 1890.77 234.998 6 1 8 2 1881.01 247.636 5 -1 -8 -3 823.872 146.257 6 -1 -8 -3 956.195 128.246 3 1 8 3 891.383 173.031 5 -1 -8 -3 944.138 68.0428 2 -1 -8 -3 799.849 116.450 4 -1 -8 -3 927.950 68.0026 1 -1 -8 -4 34.0396 38.7875 6 -1 -8 -4-10.6470 15.1114 1 -1 -8 -4 33.4361 27.9755 3 1 8 4 46.9050 36.6190 5 -1 -8 -4 6.26299 8.69246 2 -1 -8 -4 14.8738 12.4548 4 1 8 4-0.58496 28.8797 2 -1 -8 -5 96.6959 22.2996 1 -1 -8 -5 107.073 30.7720 2 -1 -8 -5 63.3636 33.6173 4 1 8 5 35.4469 43.3516 2 1 8 5 260.260 109.608 5 -1 -8 -5 101.656 41.0429 6 -1 -8 -6 413.642 89.6000 4 1 8 6 467.672 115.781 6 1 8 6 399.803 106.617 2 -1 -8 -6 421.884 54.1561 1 1 8 6 327.975 119.259 5 1 8 7-24.5654 42.5591 6 1 8 7-47.7235 38.2705 2 -1 -8 -7 8.91558 13.2233 1 1 8 7-20.3520 50.2372 5 1 8 8 61.3746 65.8603 5 1 8 8 100.537 54.3610 2 1 8 8 187.677 66.3801 6 -1 -8 -8 175.630 43.5669 1 1 8 9 908.989 158.081 6 -1 -8 -9 1152.17 119.571 1 1 8 9 1289.39 275.455 5 1 8 10 483.232 190.109 5 -1 -8 -10 559.073 89.3643 1 -1 -8 -11 212.654 58.7090 1 1 8 11 217.917 144.861 5 1 8 12 135.866 69.1083 5 -1 -8 -12 274.050 71.3037 1 1 8 13-5.41438 37.2194 5 -1 -8 -13 28.2437 25.0265 1 -1 -8 -14-34.7849 30.4032 1 1 8 14-77.7835 91.8259 5 -1 -8 -15 60.1506 40.9906 1 1 9 -9-0.83429 17.1268 1 1 9 -8 90.2601 57.7066 1 -1 -9 8-67.9832 79.7356 6 -1 -9 7 358.526 162.173 6 1 9 -7 333.942 102.408 1 -1 -9 6 967.814 132.543 4 1 9 -6 1098.37 180.838 1 -1 -9 6 1243.73 308.922 6 -1 -9 5 1292.87 153.344 4 -1 -9 5 1699.00 339.143 6 1 9 -5 1190.69 178.928 1 -1 -9 4 525.148 97.4050 4 -1 -9 4 491.457 117.727 2 -1 -9 4 753.411 217.005 6 -1 -9 3 103.139 90.1780 6 -1 -9 3 155.957 53.1272 4 1 9 -3 161.948 49.6208 1 -1 -9 3 264.534 83.9812 2 -1 -9 2 58.1459 63.8745 6 -1 -9 2 63.9401 25.0168 2 -1 -9 2-1.67016 23.6749 4 -1 -9 1 36.3697 8.99216 2 -1 -9 1-8.48319 21.2794 4 -1 -9 1 63.9487 14.6906 2 -1 -9 1 53.2178 56.9503 6 -1 -9 0-40.4402 29.1687 4 -1 -9 0 47.8506 46.5905 6 -1 -9 -1 47.3511 25.0932 4 -1 -9 -1 1.60206 60.3877 6 -1 -9 -2-37.1859 38.8497 6 1 9 2-16.8212 48.5076 5 -1 -9 -2 0.42102 17.4961 4 -1 -9 -3 852.016 131.915 4 -1 -9 -3 673.138 115.806 3 1 9 3 937.635 188.932 5 -1 -9 -3 732.444 154.595 6 -1 -9 -4 625.842 137.893 6 1 9 4 449.071 100.387 2 -1 -9 -4 628.166 111.936 3 -1 -9 -4 402.012 92.5775 4 1 9 4 464.646 135.786 5 -1 -9 -5 27.3048 32.0864 4 -1 -9 -5 40.8962 23.0485 1 1 9 5 14.5140 21.8817 2 1 9 5 4.00984 40.8223 5 -1 -9 -5 38.2592 33.7641 6 -1 -9 -5 43.0995 17.7838 3 -1 -9 -5 35.2039 10.6990 1 -1 -9 -6 661.192 64.2934 1 1 9 6 684.464 179.526 5 1 9 6 605.869 138.763 2 -1 -9 -7 15.7745 12.2647 1 1 9 7 87.3678 75.0296 5 -1 -9 -8 1098.72 106.116 1 1 9 8 1046.16 238.766 5 1 9 8 687.574 152.062 2 -1 -9 -9 376.421 66.4629 1 1 9 9 458.349 165.794 5 1 9 10 289.604 151.447 5 -1 -9 -10 515.238 85.7042 1 -1 -9 -11 249.865 65.3484 1 1 9 11 181.737 116.723 5 1 9 12 1283.65 315.783 5 -1 -9 -12 972.907 136.116 1 1 9 13 142.718 112.753 5 -1 -10 7 145.923 123.444 6 -1 -10 6 508.561 198.329 6 -1 -10 5 334.710 85.3502 4 -1 -10 5 413.645 183.348 6 -1 -10 4 195.083 67.8640 4 -1 -10 4 226.790 121.221 6 -1 -10 3 632.906 200.938 6 -1 -10 3 690.021 125.215 4 -1 -10 2-32.7772 25.1161 4 -1 -10 2 15.9672 56.8218 6 -1 -10 1-29.3893 28.0163 4 -1 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-2 170.872 66.1042 3 -1 -11 -2 139.414 79.1612 6 -1 -11 -2 120.491 60.2536 4 -1 -11 -3 94.4118 48.3206 3 -1 -11 -3 64.8325 45.0140 6 -1 -11 -4 12.6994 22.6497 3 -1 -11 -4 35.7588 40.2586 6 1 11 5 430.837 165.597 5 -1 -11 -5 287.076 88.4592 3 -1 -11 -5 268.140 89.8334 6 1 11 6 88.0882 95.8969 5 1 11 7 696.322 209.222 5 1 11 8 173.361 107.288 5 1 11 9 235.463 133.271 5 1 11 10 277.144 174.584 5 -1 -12 4 26.8565 30.5718 6 -1 -12 3 98.6666 84.9908 6 -1 -12 2 132.167 94.2148 6 -1 -12 1 35.8115 49.0952 6 -1 -12 0 342.030 142.260 6 -1 -12 -1 453.362 111.793 3 -1 -12 -1 623.790 175.728 6 -1 -12 -2 207.615 76.3513 3 -1 -12 -2 86.8530 64.6476 6 -1 -12 -3 19.1081 31.4169 3 -1 -12 -3-147.777 83.3073 6 1 12 5-200.079 110.553 5 1 12 6-16.6173 72.8340 5 1 12 7 292.802 152.290 5 -1 -13 3 8.57634 32.6933 6 -1 -13 2 7.00856 30.6169 6 -1 -13 1 21.5580 41.4501 6 -1 -13 0 48.4731 56.4990 6 -1 -13 -1 435.585 117.907 3 2 -12 -5 399.658 145.153 6 2 -12 -4 85.5975 71.5848 6 2 -12 -3 540.324 185.690 6 2 -12 -2 135.887 106.908 6 2 -12 -1 146.055 101.683 6 2 -12 0 24.9026 46.8932 6 2 -12 1 71.3317 78.1083 6 -2 11 6 113.497 89.0408 5 -2 11 5 0.88133 49.4988 5 2 -11 -5 194.885 104.435 6 2 -11 -4-12.2994 22.5477 6 -2 11 4 99.6118 78.5455 5 2 -11 -3 33.3712 38.1657 6 -2 11 3 167.876 96.6336 5 2 -11 -2 339.437 149.758 6 -2 11 2 139.858 103.824 5 2 -11 -1 223.321 124.430 6 2 -11 0 308.720 133.659 6 2 -11 1 24.7875 33.2049 6 2 -11 2 237.835 136.183 6 2 -11 3-32.1295 62.0375 6 -2 10 9 64.6016 50.7769 5 -2 10 8-26.3934 37.3764 5 -2 10 7 235.239 127.647 5 -2 10 6 59.0611 76.2548 5 -2 10 5 163.400 97.5894 5 2 -10 -5 190.097 101.768 6 2 -10 -4 401.616 132.400 6 -2 10 4 512.741 177.203 5 2 -10 -3 22.9837 40.9635 6 -2 10 3-57.1655 58.3447 5 2 -10 -2-2.65663 28.0235 6 -2 10 2 11.6596 38.7068 5 -2 10 1 67.1533 63.0012 5 2 -10 -1 165.307 119.322 6 2 -10 0 774.985 208.758 6 2 -10 1 526.243 193.757 6 2 -10 2 1492.86 318.454 6 2 -10 3 446.251 187.500 6 2 -10 4 36.1746 62.0583 6 2 -10 5-52.5821 72.6805 6 -2 9 10-93.1406 90.9291 5 -2 9 9 34.0655 79.8328 5 -2 9 8-68.9763 76.5491 5 -2 9 7 271.501 127.949 5 -2 9 6-135.336 92.9683 5 -2 9 5 704.172 198.813 5 2 -9 -5 1016.92 202.780 6 2 -9 -4 1767.53 269.624 6 -2 9 4 1386.90 262.688 5 2 -9 -3 359.900 128.590 6 -2 9 3 465.727 147.500 5 -2 9 2 116.015 78.0108 5 2 -9 -2 207.826 98.5560 6 2 -9 -1 96.2745 60.0510 6 -2 9 1-10.8289 27.0344 5 2 -9 0 103.145 38.7400 6 2 -9 1 258.174 104.288 6 2 -9 2-78.2545 75.6920 6 2 -9 3 1926.02 359.752 6 2 -9 4 264.777 138.058 6 2 -9 5 432.865 195.759 6 2 -9 6 29.5503 39.2769 6 2 -9 7 221.460 131.641 6 -2 8 12 285.274 173.174 5 -2 8 11 846.082 281.936 5 -2 8 10 308.429 151.380 5 2 -8 -10 270.038 74.4017 1 2 -8 -9 683.743 117.812 1 -2 8 9 896.187 269.347 5 -2 8 8 253.019 150.274 5 2 -8 -8 89.3771 41.6264 1 2 -8 -7 656.572 93.2512 1 -2 8 7 1128.32 263.506 5 -2 8 6 107.762 74.7641 5 -2 8 6 93.1145 37.7239 2 2 -8 -6 75.1808 23.0574 1 -2 8 5 52.1868 60.9170 5 2 -8 -5 215.478 81.5234 6 -2 8 5 114.571 33.9352 2 2 -8 -5 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7-14.7254 47.6953 5 2 -7 -7 98.2420 42.4673 1 -2 7 7 70.4132 30.7557 2 -2 7 6 544.487 169.745 5 2 -7 -6 609.523 89.2723 1 -2 7 6 602.204 87.2045 2 2 -7 -5 516.501 65.1412 1 -2 7 5 524.506 159.952 6 -2 7 5 707.447 182.577 5 -2 7 5 579.040 76.5158 2 2 -7 -5 483.204 119.570 6 -2 7 4 248.159 42.1663 2 -2 7 4 287.985 108.537 5 2 -7 -4 288.577 94.6511 6 -2 7 4 220.628 99.7872 6 -2 7 3 2255.85 314.368 6 2 -7 -3 2029.74 263.566 6 -2 7 3 1642.20 250.546 5 -2 7 2 907.236 171.790 5 2 -7 -2 1356.78 223.970 6 2 -7 -1 593.804 151.047 6 -2 7 1 568.090 138.500 5 -2 7 0 560.908 129.254 5 2 -7 0 550.607 152.474 6 2 -7 1 517.222 160.774 6 -2 7 -2 33.7389 10.1849 1 2 -7 2 23.1972 56.2045 6 -2 7 -3 270.773 46.2227 1 2 -7 3 409.861 141.870 6 -2 7 -4-6.08399 13.1065 1 2 -7 4-1.29541 14.7809 2 2 -7 5 627.584 105.293 2 2 -7 5 720.002 212.630 6 2 -7 6 660.702 217.520 6 -2 7 -6 442.893 79.3736 1 -2 7 -7 488.261 90.2466 1 2 -7 7 765.282 234.250 6 -2 7 -8 247.774 64.8423 1 2 -7 8 393.202 193.543 6 2 -7 9 164.540 104.256 6 -2 7 -9 40.6821 30.9924 1 2 -7 10 446.225 217.245 6 -2 7 -10 174.794 67.1044 1 -2 7 -11 95.6633 52.1549 1 -2 7 -12-12.5382 21.3981 1 2 -6 -15 148.803 73.2925 1 2 -6 -14 334.046 98.1329 1 2 -6 -13 2.60109 32.2847 1 2 -6 -12 219.085 73.4886 1 2 -6 -11 20.3661 24.0796 1 -2 6 10 208.448 103.989 5 2 -6 -10 137.317 53.0731 1 -2 6 9 58.5017 74.9929 5 2 -6 -9 25.4307 25.4178 1 2 -6 -8 6.00359 14.8813 1 -2 6 8 26.3403 51.4781 5 -2 6 8 32.9987 15.0911 2 2 -6 -7 2290.86 183.453 1 -2 6 7 1982.59 167.380 2 -2 6 7 2138.71 295.685 6 -2 6 7 2843.61 412.158 5 -2 6 6 2232.75 160.646 2 2 -6 -6 2314.70 175.156 1 -2 6 6 2617.51 374.547 5 -2 6 6 2283.26 296.239 6 2 -6 -5 532.133 77.5573 1 2 -6 -5 515.611 126.752 6 -2 6 5 454.577 131.167 6 -2 6 5 462.819 65.4310 2 -2 6 5 473.408 158.269 5 -2 6 4 56.9810 43.4923 5 -2 6 4 111.664 72.3831 6 -2 6 4 145.916 33.0813 2 2 -6 -4 121.965 60.7315 6 2 -6 -4 71.1124 24.3318 1 -2 6 3 576.610 51.7210 2 2 -6 -3 418.946 110.688 6 -2 6 3 549.084 139.118 5 -2 6 3 478.066 137.299 6 -2 6 2 552.846 86.6541 4 -2 6 2 440.564 117.305 5 2 -6 -2 480.444 125.736 6 -2 6 2 475.099 142.228 6 -2 6 1-11.4376 17.9715 4 -2 6 1-2.78318 36.3070 5 2 -6 -1-85.9041 56.4585 6 -2 6 1 11.5559 25.2733 6 2 -6 -1 57.8505 56.0338 5 -2 6 0 643.946 130.449 5 -2 6 0 710.417 94.2842 4 2 -6 0 697.984 159.821 6 -2 6 0 701.889 174.164 6 2 -6 0 651.401 159.781 5 -2 6 -1 496.824 110.942 5 2 -6 1 460.803 125.848 5 2 -6 1 445.168 140.048 6 -2 6 -1 485.288 74.5955 4 -2 6 -2 144.031 41.6795 4 2 -6 2 62.7472 55.5669 5 2 -6 2 39.3235 57.9003 6 -2 6 -2 133.976 25.7465 1 -2 6 -3 913.295 78.9583 1 2 -6 3 877.993 172.924 5 2 -6 3 811.476 100.307 2 2 -6 3 908.431 205.990 6 2 -6 4 156.557 45.8163 2 2 -6 4 35.9069 31.0900 5 2 -6 4 272.868 122.635 6 -2 6 -4 104.058 31.1632 1 2 -6 5 48.3035 42.9775 5 2 -6 5 84.0474 38.2713 2 2 -6 5 64.3412 69.3030 6 2 -6 6 55.7998 33.7114 2 -2 6 -6 85.7810 36.7426 1 2 -6 6 58.8352 64.5803 6 2 -6 7 516.170 109.415 2 -2 6 -7 513.037 88.1055 1 2 -6 7 653.380 207.772 6 -2 6 -8 737.295 114.679 1 2 -6 8 890.350 266.230 6 2 -6 9 1267.83 320.983 6 -2 6 -9 1021.57 143.237 1 -2 6 -10 311.003 84.3937 1 2 -6 10 606.254 235.981 6 2 -6 11 224.995 147.916 6 -2 6 -11 30.3541 24.6525 1 -2 6 -12 53.3679 44.7356 1 -2 6 -13-53.2422 42.5331 1 2 -5 -15 325.622 100.791 1 2 -5 -14 380.593 107.742 1 2 -5 -13 105.733 51.4281 1 2 -5 -12-19.8299 24.7451 1 2 -5 -11 733.412 125.424 1 2 -5 -10 298.117 78.8655 1 2 -5 -9 248.433 65.0547 1 -2 5 8 1164.05 213.673 6 -2 5 8 1185.35 139.407 2 2 -5 -8 1104.86 131.159 1 -2 5 7 1486.17 235.828 6 2 -5 -7 1260.38 133.966 1 2 -5 -6 1911.67 157.020 1 -2 5 6 1770.52 138.325 2 -2 5 6 1827.92 167.820 4 -2 5 6 1956.96 315.788 5 -2 5 6 2019.20 264.062 6 -2 5 5 1952.87 169.635 4 -2 5 5 1658.12 235.718 6 2 -5 -5 1678.96 139.414 1 -2 5 5 1552.84 116.211 2 -2 5 5 2142.68 306.876 5 2 -5 -4 2183.32 151.216 1 -2 5 4 2341.02 181.521 4 -2 5 4 1751.45 107.982 2 2 -5 -4 2106.75 226.663 6 -2 5 4 1882.90 242.052 6 -2 5 4 2259.30 295.820 5 2 -5 -3 3252.02 138.453 1 2 -5 -3 3542.64 293.471 6 -2 5 3 4000.88 136.690 2 -2 5 3 4571.99 246.733 4 -2 5 3 4584.29 388.806 5 2 -5 -2 382.231 103.175 6 -2 5 2 606.247 130.285 5 -2 5 2 476.005 37.2939 2 -2 5 2 451.855 77.8712 4 -2 5 2 426.003 70.8263 2 -2 5 1 1226.17 121.490 4 -2 5 1 1145.38 196.187 6 2 -5 -1 982.880 168.206 6 -2 5 1 1015.81 163.051 5 -2 5 0-24.3925 31.9470 6 -2 5 0 33.8241 34.9251 5 -2 5 0-8.26086 13.4432 4 2 -5 0 30.3040 48.4936 6 2 -5 0 36.2113 38.6717 5 2 -5 1 82.2902 52.9228 5 -2 5 -1 40.0441 19.9779 4 -2 5 -1 61.2457 13.0105 1 -2 5 -1 115.982 45.2122 5 2 -5 1 118.750 73.5774 6 2 -5 2 1587.71 245.392 6 2 -5 2 1436.26 194.882 5 -2 5 -2 1497.17 119.451 4 2 -5 2 1606.36 134.809 2 -2 5 -2 1633.97 86.4079 1 2 -5 3 94.6120 29.4935 2 2 -5 3 60.3996 37.3372 5 -2 5 -3 142.407 36.6566 4 2 -5 3 84.4306 70.9227 6 -2 5 -3 131.933 29.8605 1 2 -5 4 2680.87 262.195 5 2 -5 4 2614.55 189.651 2 -2 5 -4 2782.50 151.134 1 2 -5 4 3442.99 396.535 6 2 -5 5 126.888 86.9814 6 2 -5 5 317.060 71.1234 2 2 -5 5 237.231 78.5762 5 2 -5 6 601.411 200.326 6 2 -5 6 540.256 98.0225 2 -2 5 -6 535.710 81.0066 1 2 -5 6 417.623 105.292 5 2 -5 7 102.851 97.2916 6 -2 5 -7 74.9998 35.0929 1 2 -5 7-40.7878 29.6533 2 2 -5 7 58.0997 47.1683 5 2 -5 8 46.6586 19.4914 2 -2 5 -8 89.0468 38.5301 1 2 -5 8-6.67043 41.3167 6 2 -5 9-22.8266 56.2582 6 -2 5 -9 5.68884 23.9797 1 -2 5 -10 375.648 88.8424 1 2 -5 10 677.342 232.686 6 2 -5 11 516.716 220.040 6 -2 5 -11 629.192 123.601 1 -2 5 -12 133.905 57.7900 1 2 -5 12 212.559 131.515 6 -2 5 -13 209.569 81.5005 1 2 -4 -15 0.95693 13.7153 1 2 -4 -14 16.3018 26.0367 1 2 -4 -13 294.135 88.1301 1 2 -4 -12 649.472 126.115 1 2 -4 -11 1258.18 164.103 1 2 -4 -10 1083.93 144.238 1 -2 4 9 374.850 122.070 6 2 -4 -9 287.972 71.3091 1 2 -4 -8 546.782 90.2385 1 -2 4 8 324.845 68.9996 4 -2 4 8 337.104 69.7920 2 -2 4 8 224.072 88.4653 6 2 -4 -7 35.2150 22.2901 1 -2 4 7 30.2711 15.7292 2 -2 4 7 18.7200 12.4752 4 -2 4 7 122.483 57.6284 6 -2 4 6 398.620 65.3108 2 -2 4 6 457.916 80.6217 4 -2 4 6 427.783 114.945 6 2 -4 -6 321.470 62.6113 1 2 -4 -5 218.930 49.8679 1 -2 4 5 245.010 57.2384 4 -2 4 5 269.561 48.4178 2 -2 4 4 331.831 65.3178 4 2 -4 -4 330.882 91.0188 6 2 -4 -4 336.431 57.7027 1 -2 4 4 343.265 49.0892 2 -2 4 4 307.381 40.7049 1 -2 4 4 412.675 122.130 5 -2 4 3 3722.80 217.001 4 2 -4 -3 3642.75 180.900 1 -2 4 3 3448.81 119.969 1 -2 4 3 4059.84 367.318 5 2 -4 -3 3228.33 266.203 6 -2 4 2 16031.8 218.847 1 2 -4 -2 16491.3 610.953 6 -2 4 2 17368.1 678.052 5 -2 4 2 14997.6 637.694 6 -2 4 2 16325.1 439.409 4 -2 4 1 677.219 75.8818 2 -2 4 1 568.186 39.3007 1 -2 4 1 604.846 82.1920 4 2 -4 -1 612.318 126.945 6 -2 4 1 579.822 117.860 5 -2 4 0 205.311 21.2399 2 2 -4 0 170.424 62.6272 5 -2 4 0 154.704 26.9573 1 -2 4 0 222.102 49.6808 4 -2 4 0 172.057 56.4736 5 2 -4 0 145.908 51.8700 6 2 -4 1 1806.50 202.037 5 -2 4 -1 1917.37 132.510 4 -2 4 -1 2203.48 72.3642 2 -2 4 -1 1942.79 178.625 5 2 -4 1 2057.99 237.389 6 2 -4 1 2226.97 148.357 2 2 -4 2 354.500 94.0195 5 2 -4 2 403.098 68.8927 2 2 -4 2 396.802 120.848 6 -2 4 -2 514.517 44.5337 2 -2 4 -2 429.703 59.8827 4 2 -4 3 2707.30 177.124 2 2 -4 3 2823.24 236.949 5 -2 4 -3 2797.03 143.351 4 2 -4 3 3233.81 350.087 6 2 -4 4 1625.30 262.347 6 -2 4 -4 1432.27 95.3476 4 2 -4 4 1410.52 134.814 2 -2 4 -4 1669.11 112.685 1 2 -4 4 1476.65 171.368 5 2 -4 5 532.437 161.157 6 2 -4 5 726.772 120.573 5 2 -4 5 628.190 95.8521 2 2 -4 6-27.1777 32.6547 5 2 -4 6-49.0023 91.4234 6 2 -4 6 2.83301 20.0580 2 2 -4 7 50.7739 73.7024 6 2 -4 7 81.8816 42.8955 2 -2 4 -7 68.5318 30.2265 1 -2 4 -8 40.5756 25.2312 1 2 -4 8-0.30614 7.09256 2 -2 4 -9 22.8910 22.4553 1 -2 4 -10 458.525 94.7927 1 -2 4 -11 326.872 83.8149 1 -2 4 -12 95.1450 51.2901 1 -2 4 -13 85.9469 51.1403 1 -2 4 -14 36.7604 26.3079 1 2 -3 -15 118.766 72.1179 1 2 -3 -14-2.94344 43.2907 1 2 -3 -13 102.932 64.0155 1 2 -3 -12 54.8330 26.0560 1 2 -3 -11 771.320 128.153 1 -2 3 11 760.283 104.116 4 -2 3 10 922.120 114.956 4 2 -3 -10 908.136 129.199 1 -2 3 9 855.451 110.081 4 2 -3 -9 840.532 117.760 1 -2 3 8 365.167 72.3529 4 2 -3 -8 275.893 65.1592 1 -2 3 8 313.738 35.2236 3 -2 3 8 393.735 76.6789 2 -2 3 7 183.761 71.9048 6 -2 3 7 199.053 49.2731 2 2 -3 -7 135.166 45.0059 1 -2 3 7 189.061 49.5204 4 -2 3 6 292.708 56.4740 2 -2 3 6 229.111 46.6675 1 2 -3 -6 299.081 59.8862 1 2 -3 -5 994.000 102.903 1 -2 3 5 927.612 84.8334 1 -2 3 4 2.02147 7.52559 1 -2 3 4-3.16836 20.3350 6 2 -3 -4 20.0617 18.5793 1 2 -3 -3 2765.45 223.770 6 -2 3 3 2655.86 117.348 1 2 -3 -3 2790.65 163.107 1 2 -3 -2 13348.3 323.974 1 -2 3 2 15772.7 631.347 5 -2 3 2 13982.4 248.926 1 2 -3 -2 14641.3 513.427 6 -2 3 1 2716.36 197.977 2 -2 3 1 2099.26 101.069 1 2 -3 -1 2231.74 217.231 6 -2 3 1 2190.67 214.301 5 -2 3 0 1605.62 86.0410 1 2 -3 0 2236.42 220.048 6 -2 3 0 2477.26 126.736 2 2 -3 0 2225.08 210.384 5 -2 3 0 2169.87 185.999 5 -2 3 -1 966.770 114.046 5 -2 3 -1 919.447 64.1276 2 2 -3 1 967.117 155.418 6 2 -3 1 958.901 115.209 2 2 -3 1 811.943 117.575 5 -2 3 -2 1172.35 93.9966 4 -2 3 -2 1338.14 79.5184 2 2 -3 2 1185.04 134.294 5 2 -3 2 1208.16 182.979 6 2 -3 3 463.760 71.9673 2 -2 3 -3 438.652 51.8022 4 -2 3 -3 523.620 54.3654 2 2 -3 3 483.277 84.2900 5 2 -3 3 550.872 140.919 6 2 -3 4 629.941 88.6257 2 2 -3 4 633.123 98.3757 5 -2 3 -4 693.668 70.5463 2 -2 3 -4 627.820 57.3857 4 2 -3 4 890.437 185.635 6 2 -3 5 443.893 77.8590 2 -2 3 -5 465.457 64.3961 2 2 -3 5 545.312 153.988 6 2 -3 6 1791.93 167.204 2 2 -3 7 626.895 105.389 2 -2 3 -7 560.348 82.8930 1 2 -3 8 745.530 124.998 2 -2 3 -8 810.505 107.823 1 -2 3 -9 488.222 88.9219 1 -2 3 -10 81.2979 37.4167 1 -2 3 -11 55.4222 37.4616 1 -2 3 -12 130.862 60.9027 1 -2 3 -13 44.3518 39.5352 1 -2 3 -14 454.223 118.805 1 2 -2 -15 345.472 111.625 1 2 -2 -14 777.765 153.981 1 2 -2 -13-23.1810 34.3662 1 -2 2 12 37.1594 23.6224 4 2 -2 -12-28.0649 36.5441 1 -2 2 11 1005.51 113.953 4 2 -2 -11 1005.42 146.764 1 2 -2 -10 299.045 75.5015 1 -2 2 10 291.751 61.6945 4 -2 2 9 1509.47 142.645 4 2 -2 -9 1333.87 149.039 1 -2 2 8 7098.84 326.286 2 2 -2 -8 5547.11 289.489 1 2 -2 -7 1100.32 119.787 1 -2 2 7 1235.34 117.224 1 2 -2 -6 1898.65 147.570 1 -2 2 6 1345.62 74.9893 3 -2 2 6 1688.05 127.989 1 -2 2 5 323.284 51.3053 1 -2 2 5 412.078 94.4842 6 -2 2 5 277.737 34.3157 3 2 -2 -5 258.196 50.0890 1 2 -2 -4 59.8178 31.4461 1 -2 2 4 45.6571 17.3482 1 2 -2 -3 842.762 90.0907 1 2 -2 -3 858.825 50.2138 3 -2 2 3 859.317 72.7544 1 -2 2 2 1651.60 97.1705 1 2 -2 -2 1595.69 157.288 6 2 -2 -2 1755.51 126.176 1 -2 2 1 11595.1 272.449 1 -2 2 1 12047.1 480.325 5 2 -2 -1 12218.8 436.096 6 -2 2 0 244.300 63.9700 5 -2 2 0 361.900 36.7917 1 -2 2 0 364.588 68.2936 2 2 -2 0 173.947 54.8894 6 2 -2 1 1861.27 190.404 6 -2 2 -1 1435.02 116.304 5 2 -2 1 1700.26 147.911 5 2 -2 1 1881.15 162.928 2 -2 2 -1 1700.24 110.149 2 -2 2 -2 474.073 54.1106 2 2 -2 2 456.437 68.1810 5 2 -2 2 426.116 67.5635 2 2 -2 2 498.554 107.141 6 2 -2 3 3512.86 186.029 5 2 -2 3 3362.35 189.900 2 2 -2 3 3719.95 312.478 6 -2 2 -3 3630.64 154.045 2 2 -2 4 29.1167 41.0155 6 2 -2 4 12.6002 9.89600 2 -2 2 -4-8.18196 9.94370 4 -2 2 -4 16.5083 14.1834 2 -2 2 -5 865.591 49.3619 4 2 -2 5 887.669 110.076 2 -2 2 -5 999.029 94.2605 2 2 -2 6 1090.81 127.856 2 -2 2 -7 72.0127 32.5754 1 2 -2 7 87.7169 38.7976 2 -2 2 -8 1962.84 160.882 1 2 -2 8 1892.71 194.463 2 -2 2 -9 24.0079 28.4529 1 -2 2 -10 382.456 80.0078 1 -2 2 -11 341.535 82.3933 1 -2 2 -12 231.365 70.5220 1 -2 2 -13 326.622 90.1450 1 -2 2 -14 90.0840 46.2798 1 2 -1 -15 315.617 111.764 1 2 -1 -14 553.624 127.236 1 2 -1 -13 757.579 142.660 1 2 -1 -12 715.041 130.859 1 2 -1 -11 131.054 54.1305 1 -2 1 11 115.068 36.3176 4 2 -1 -10 564.478 101.906 1 2 -1 -9 474.131 89.6074 1 -2 1 8 170.348 50.3943 2 -2 1 8 156.308 45.8352 1 2 -1 -8 84.3404 37.0241 1 2 -1 -7 271.133 59.7529 1 -2 1 7 292.719 57.4890 1 2 -1 -6 228.278 51.4055 1 -2 1 6 295.241 55.2314 1 -2 1 5 2347.75 144.461 1 2 -1 -5 2180.48 150.151 1 -2 1 4 607.501 71.5045 1 -2 1 4 527.099 50.6487 3 2 -1 -4 676.495 82.6208 1 -2 1 3 1836.48 102.807 3 -2 1 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5635.73 275.504 1 -2 -7 -2 5562.93 265.587 2 -2 -7 -2 5550.13 339.187 6 2 7 2 5678.36 398.030 5 -2 -7 -3 3465.53 199.381 1 -2 -7 -3 4690.22 227.478 2 -2 -7 -3 4897.59 296.038 3 2 7 3 4295.50 376.196 2 -2 -7 -3 4677.40 250.816 4 -2 -7 -3 4343.82 269.609 6 2 7 3 4531.04 351.144 5 -2 -7 -3 3830.06 387.804 5 -2 -7 -4-34.9145 55.7790 5 -2 -7 -4 4.41986 13.2135 2 -2 -7 -4 14.9938 18.6929 3 -2 -7 -4 37.6931 28.4221 4 -2 -7 -4 1.61693 22.5355 6 2 7 4-23.1270 43.3734 5 2 7 4 58.1400 37.4307 2 2 7 5 1076.14 188.037 5 -2 -7 -5 833.993 111.043 4 2 7 5 722.537 149.345 2 -2 -7 -5 1011.11 105.688 2 2 7 6 31.5401 50.5303 5 -2 -7 -6 27.0421 21.5950 4 -2 -7 -6 48.0644 25.3087 2 2 7 6 14.2207 30.4417 2 2 7 7 223.885 83.7152 2 -2 -7 -7 345.054 75.7826 4 2 7 7 450.728 145.246 5 -2 -7 -7 331.858 65.2192 2 2 7 7 204.586 53.8177 6 2 7 8 1110.85 228.162 5 -2 -7 -8 1001.89 118.213 2 2 7 8 863.749 170.319 2 2 7 8 979.998 122.138 6 -2 -7 -8 936.759 127.156 4 -2 -7 -9 364.303 76.7195 2 2 7 9 591.556 182.231 5 2 7 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5 -3 7 3 473.121 147.184 5 3 -7 -3 324.726 115.128 6 3 -7 -2 1665.34 258.941 6 -3 7 2 1648.22 255.940 5 -3 7 1 113.065 69.6072 5 3 -7 -1 220.437 103.327 6 3 -7 0 811.311 196.320 6 -3 7 0 847.971 166.101 5 3 -7 1 2220.01 325.847 6 -3 7 -1 2153.81 267.846 5 -3 7 -2 1010.75 80.1513 1 3 -7 2 1000.06 230.687 6 -3 7 -2 1186.04 67.9429 1 -3 7 -3 384.822 49.7852 1 3 -7 3 465.174 178.495 6 3 -7 4 29.8284 80.3152 6 -3 7 -4 86.6467 26.5812 1 3 -7 5-12.9848 48.5733 6 3 -7 6 209.319 155.860 6 -3 7 -6 105.608 38.8001 1 -3 7 -7-29.2937 22.5261 1 3 -7 7-329.279 164.466 6 3 -7 8 415.640 172.403 6 -3 7 -8 285.888 72.2151 1 -3 7 -9 281.890 77.2324 1 3 -7 9 616.279 240.602 6 -3 7 -10 498.579 110.517 1 3 -6 -15 16.9925 29.0227 1 3 -6 -14 184.737 87.6011 1 3 -6 -13 312.442 106.865 1 3 -6 -12 203.558 82.7162 1 3 -6 -11 30.8160 34.3695 1 -3 6 10 281.391 161.177 5 3 -6 -10 242.311 78.1576 1 -3 6 9-161.173 119.214 5 3 -6 -9-3.37488 20.7973 1 -3 6 8 1465.53 157.005 2 -3 6 8 2129.02 395.262 5 3 -6 -8 1369.61 172.630 1 -3 6 7-5.94111 101.702 5 -3 6 7 14.9695 18.1114 2 3 -6 -7-22.1161 15.7067 1 3 -6 -6 84.4343 27.0913 1 -3 6 6 116.637 63.0961 5 -3 6 6 115.954 36.9447 2 -3 6 5-16.1892 48.2808 5 -3 6 5 9.12113 7.72818 2 3 -6 -5 2.33858 16.6288 1 3 -6 -4 668.321 144.594 6 -3 6 4 549.602 62.7159 2 -3 6 4 783.145 190.607 5 3 -6 -3 6312.96 461.617 6 -3 6 3 5205.20 451.092 5 -3 6 2 30.1322 13.0274 2 -3 6 2 59.5022 12.3902 2 3 -6 -2-11.4601 38.7155 6 -3 6 2 52.5672 62.9158 5 -3 6 1 297.857 90.9676 5 3 -6 -1 288.066 111.943 6 -3 6 0 67.5014 50.1517 5 3 -6 0-7.73703 30.7249 6 3 -6 1 405.110 127.916 5 -3 6 -1 212.551 54.0773 4 -3 6 -1 279.405 45.3733 1 -3 6 -1 311.891 96.1156 5 -3 6 -1 278.803 29.0116 1 3 -6 1 197.875 95.9423 6 3 -6 2 601.678 155.484 5 -3 6 -2 847.191 105.881 4 -3 6 -2 850.135 64.8762 1 3 -6 2 759.968 190.462 6 -3 6 -3 1298.46 125.015 4 3 -6 3 1486.68 164.760 2 3 -6 3 1314.13 216.967 5 3 -6 3 1546.31 280.408 6 -3 6 -3 1517.37 101.731 1 -3 6 -4 262.708 47.6595 1 -3 6 -4 286.191 55.9340 4 3 -6 4 324.343 84.7965 2 3 -6 4 261.516 92.4700 5 3 -6 4 384.784 165.595 6 3 -6 5 64.6544 63.4659 6 3 -6 5 55.2822 36.3270 2 3 -6 5-1.00530 35.9747 5 3 -6 6 41.4435 33.9113 2 3 -6 6-42.2392 40.7992 5 -3 6 -6 15.0080 19.0835 1 3 -6 6 53.0545 46.0935 6 -3 6 -7 6.28344 14.0018 1 3 -6 7-269.638 141.635 6 -3 6 -8 24.9062 20.8127 1 3 -6 8 118.325 112.528 6 -3 6 -9 399.244 89.9411 1 3 -6 9 267.941 172.365 6 -3 6 -10 257.262 72.6866 1 3 -6 10 186.191 134.666 6 -3 6 -11 337.612 92.3140 1 3 -6 11 344.228 203.406 6 -3 6 -12 173.695 74.4552 1 -3 6 -13 213.662 82.5858 1 3 -5 -15 110.201 70.5551 1 3 -5 -14 96.9773 61.0396 1 3 -5 -13 44.8156 37.9704 1 3 -5 -12 925.257 166.175 1 3 -5 -11 748.032 142.927 1 3 -5 -10 442.175 106.012 1 3 -5 -9 57.1809 34.9643 1 3 -5 -8 1573.07 182.377 1 -3 5 8 1593.38 157.625 2 3 -5 -7 282.033 75.0923 1 -3 5 7 247.938 56.9601 2 -3 5 6 606.893 181.210 5 -3 5 6 543.962 154.938 6 3 -5 -6 532.991 97.8843 1 -3 5 6 476.043 73.4495 2 3 -5 -5 3409.92 240.211 1 -3 5 5 3019.18 346.445 6 -3 5 5 3030.90 150.482 1 -3 5 5 3202.89 173.711 2 -3 5 5 3487.58 418.079 5 3 -5 -4 4915.60 370.700 6 3 -5 -4 4506.56 247.126 1 -3 5 4 5437.31 503.323 5 -3 5 4 5330.20 452.724 6 -3 5 4 5129.31 177.054 1 -3 5 3 11449.4 438.497 4 3 -5 -3 11375.1 573.995 6 -3 5 3 11346.2 233.922 1 -3 5 3 11173.3 653.652 6 -3 5 3 11245.8 658.510 5 3 -5 -2 14.6777 26.4721 6 -3 5 2 34.8907 27.9437 4 -3 5 2 41.6784 61.3836 6 -3 5 2 28.5681 12.5146 1 -3 5 2-21.3255 42.9647 2 -3 5 2 35.3309 50.6829 5 -3 5 1 449.590 113.196 5 -3 5 1 438.939 81.3475 4 -3 5 1 409.964 53.2095 2 3 -5 -1 380.129 114.056 6 -3 5 1 465.058 140.915 6 -3 5 1 415.601 41.9807 1 -3 5 0 117.517 41.7442 4 -3 5 0 86.3800 16.7981 2 -3 5 0 30.4072 29.3655 5 -3 5 0 51.6099 17.5062 1 3 -5 0 109.616 76.6693 6 -3 5 0 123.222 70.1308 6 3 -5 1 157.743 75.5504 5 -3 5 -1 245.550 38.2240 1 -3 5 -1 142.730 42.0552 4 -3 5 -1 78.7351 14.5899 2 -3 5 -1 182.897 58.9225 5 3 -5 1 172.276 79.3390 6 -3 5 -1 123.995 79.3458 6 -3 5 -2 25.8311 19.5207 4 3 -5 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192.852 6 -4 6 -7 3.39706 7.69074 1 4 -6 7-276.425 145.061 6 -4 6 -8 18.2927 9.31874 1 4 -6 8-185.301 125.621 6 -4 6 -9-45.1250 30.4880 1 4 -6 9-18.9667 52.4358 6 -4 6 -10 66.1180 45.3605 1 4 -6 10 19.8100 50.2443 6 -4 6 -11 43.1071 33.2332 1 -4 6 -12 164.902 69.4131 1 4 -5 -14 20.7090 33.2285 1 4 -5 -13-48.7455 46.7859 1 4 -5 -12 521.795 140.542 1 4 -5 -11 453.793 125.883 1 4 -5 -10 554.681 129.920 1 4 -5 -9 333.585 99.1105 1 4 -5 -8 201.118 69.3800 1 -4 5 7 140.525 47.6969 2 -4 5 7 126.395 39.0768 1 4 -5 -7 115.746 54.3166 1 -4 5 6-22.7680 66.0816 5 -4 5 6 35.9237 18.1846 1 4 -5 -6 12.7218 30.4610 1 -4 5 5 415.543 153.087 5 4 -5 -5 384.465 88.7160 1 -4 5 5 475.267 66.3297 1 4 -5 -4 871.883 172.055 6 -4 5 4 631.003 163.001 5 -4 5 4 830.643 83.3153 1 -4 5 3 1260.61 228.575 5 4 -5 -3 1005.98 182.423 6 -4 5 3 1104.00 92.6945 1 -4 5 3 1162.19 202.205 2 -4 5 2 2518.34 259.035 2 4 -5 -2 2598.98 311.011 6 -4 5 2 2764.10 148.614 1 -4 5 2 2895.52 323.844 5 -4 5 1 6831.99 304.818 2 4 -5 -1 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41.2205 1 4 -5 8 119.284 61.7818 6 -4 5 -9 125.204 48.9888 1 4 -5 9 155.128 101.732 6 -4 5 -10 129.173 48.6896 1 4 -5 10 13.7247 70.3547 6 -4 5 -11 12.7661 22.8856 1 4 -5 11 103.406 101.199 6 -4 5 -12-24.6359 26.9163 1 -4 5 -13 147.818 66.3577 1 4 -4 -14 161.812 76.8797 1 4 -4 -13-66.1194 52.5925 1 4 -4 -12 140.319 63.2807 1 4 -4 -11-38.0318 38.6216 1 4 -4 -10 81.3184 51.2324 1 4 -4 -9 664.081 140.001 1 -4 4 8 4.80525 12.7404 1 4 -4 -8-29.3702 41.3085 1 4 -4 -7 1268.70 181.671 1 -4 4 7 1185.94 125.725 1 4 -4 -6 316.878 87.7994 1 -4 4 6 323.190 62.4874 1 -4 4 5 219.540 48.7327 1 4 -4 -5 271.072 77.8548 1 4 -4 -4 850.057 122.362 1 4 -4 -4 785.353 76.7165 3 -4 4 4 742.349 180.532 6 -4 4 4 812.817 89.6233 1 -4 4 3 82.2895 84.6132 5 4 -4 -3 29.9225 40.9442 6 -4 4 3-39.1063 49.9510 6 -4 4 3 34.7501 19.0813 1 -4 4 2 24.8432 18.6592 1 -4 4 2-5.16760 34.7318 5 4 -4 -2 23.3834 42.7432 6 -4 4 2 43.8487 37.7883 6 -4 4 2 5.40693 34.6480 2 -4 4 1 63.7358 55.6642 5 -4 4 1 63.4491 27.2808 1 4 -4 -1 98.5169 63.3257 6 -4 4 1 29.8631 29.4635 6 -4 4 1 134.622 64.4943 2 -4 4 0 328.672 91.9835 5 -4 4 0 264.908 65.5434 2 -4 4 0 168.165 49.1717 1 4 -4 0 274.892 106.549 6 -4 4 0 248.204 100.330 6 -4 4 -1 1620.22 183.144 5 -4 4 -1 2750.98 157.509 1 -4 4 -1 1751.10 142.832 2 4 -4 1 2054.24 275.710 6 -4 4 -1 1732.79 275.256 6 4 -4 2 970.174 198.124 6 4 -4 2 1137.43 180.205 2 -4 4 -2 1306.69 114.299 2 -4 4 -2 1240.45 151.359 5 4 -4 3 2552.52 326.571 6 4 -4 3 2597.69 293.228 2 -4 4 -3 2775.05 162.773 2 4 -4 3 2859.21 265.887 5 4 -4 4 17.7233 24.6737 5 -4 4 -4 27.1139 21.3285 4 -4 4 -4 38.5946 23.4127 2 4 -4 4 8.73305 48.6312 6 4 -4 4 81.0322 36.1418 2 4 -4 5 57.8176 34.6432 5 -4 4 -5 32.9708 19.6690 4 4 -4 5 98.0630 84.6654 6 4 -4 5 11.2824 28.4074 2 4 -4 6 212.574 84.1704 2 -4 4 -6 374.337 55.9208 4 4 -4 6 106.946 94.1698 6 -4 4 -6 360.805 65.9132 2 4 -4 6 353.507 88.8467 5 4 -4 7 704.560 128.183 5 4 -4 7 648.532 146.851 2 -4 4 -7 727.748 69.7904 4 -4 4 -7 1026.90 118.341 2 4 -4 7 609.617 188.241 6 4 -4 8 102.185 51.9728 5 -4 4 -8 295.116 70.6332 1 4 -4 8 132.000 96.6325 6 -4 4 -9 318.452 76.1805 1 4 -4 9 431.037 185.037 6 -4 4 -10 469.671 97.2677 1 4 -4 10 608.853 202.910 6 -4 4 -11 247.105 71.9668 1 4 -4 11 284.985 143.890 6 -4 4 -12 2.32058 12.0114 1 4 -4 12-61.0602 81.1337 6 -4 4 -13 55.0426 44.4378 1 4 -4 13-0.69422 180.368 6 4 -3 -14 216.446 94.3958 1 4 -3 -13 130.532 67.6816 1 4 -3 -12 92.8905 59.0203 1 4 -3 -11 226.730 84.5289 1 4 -3 -10-7.99815 16.8925 1 4 -3 -9-9.95676 29.8270 1 4 -3 -8 40.8774 33.1581 1 -4 3 7 596.055 91.2574 1 4 -3 -7 605.709 121.313 1 -4 3 6 541.825 82.6077 1 4 -3 -6 468.469 105.989 1 4 -3 -5 2079.05 213.549 1 -4 3 5 2089.28 288.667 6 -4 3 5 1976.30 152.136 1 4 -3 -4 1398.38 167.884 1 4 -3 -4 1349.52 96.7879 3 -4 3 4 1547.53 244.402 6 -4 3 4 1341.41 122.962 1 4 -3 -3 61.7331 25.3681 1 4 -3 -3 145.525 62.2252 6 -4 3 3 84.3106 31.2602 1 -4 3 2 495.537 128.247 5 -4 3 2 603.760 148.714 2 4 -3 -2 549.784 120.439 6 -4 3 2 436.879 74.4563 1 -4 3 1 778.361 104.098 1 -4 3 1 577.601 124.547 5 4 -3 -1 784.661 149.520 6 -4 3 1 796.121 167.211 2 -4 3 0 1014.13 123.589 1 -4 3 0 1156.24 158.662 5 -4 3 0 1032.56 152.572 2 4 -3 0 1129.85 181.583 6 -4 3 -1 1537.25 152.443 2 4 -3 1 1581.06 218.290 6 -4 3 -1 1411.21 153.629 5 -4 3 -2 2941.83 199.477 2 4 -3 2 2834.56 304.337 2 4 -3 2 2937.11 312.369 6 -4 3 -2 2533.75 188.590 5 -4 3 -3 4133.32 221.344 2 4 -3 3 3589.56 339.266 2 4 -3 3 3721.61 368.787 6 -4 3 -3 4117.98 401.925 6 4 -3 3 3652.75 264.050 5 4 -3 4 2751.96 291.663 2 4 -3 4 3238.76 355.384 6 -4 3 -4 3053.11 191.195 2 4 -3 4 2706.99 221.191 5 4 -3 5 10.2080 18.5572 2 4 -3 5-4.58398 22.4489 5 4 -3 5-39.4403 55.7872 6 4 -3 6 186.817 55.9351 5 4 -3 6 161.691 71.4318 2 -4 3 -6 114.910 31.6047 4 -4 3 -6 195.565 50.5167 2 4 -3 6-115.552 79.1788 6 4 -3 7 159.181 52.8863 5 4 -3 7 165.164 102.926 6 4 -3 7 103.274 60.9406 2 -4 3 -7 153.537 30.3074 4 -4 3 -7 132.103 41.7267 2 -4 3 -8-13.6327 26.7615 2 4 -3 8 18.2458 16.3473 5 -4 3 -9 526.585 98.8302 2 4 -3 9 398.269 136.191 6 4 -3 9 361.151 87.9371 5 -4 3 -10 567.493 104.221 1 4 -3 10 480.216 171.553 6 -4 3 -11 338.234 86.6789 1 4 -3 11 207.907 151.170 6 -4 3 -12 106.838 48.6909 1 4 -3 12 320.666 165.971 6 -4 3 -13 24.6110 27.5435 1 4 -3 13 18.2499 51.4635 6 -4 3 -14-21.0314 26.8345 1 4 -3 14-79.1706 92.9721 6 4 -2 -14-66.2248 54.3639 1 4 -2 -13-44.4258 44.7959 1 4 -2 -12 482.813 128.548 1 4 -2 -11 639.566 139.778 1 -4 2 11 698.248 101.977 3 4 -2 -10 758.571 148.051 1 -4 2 10 947.515 116.475 3 4 -2 -9 109.630 54.9755 1 4 -2 -8 13.6161 28.8004 1 -4 2 7 108.750 41.2005 1 4 -2 -7 86.4886 44.6185 1 4 -2 -6 1506.39 186.455 1 -4 2 6 1576.44 241.883 6 -4 2 6 1621.03 148.189 1 4 -2 -5 1442.80 186.778 1 -4 2 5 1505.30 232.775 6 -4 2 5 1494.86 137.846 1 4 -2 -4 3704.85 280.290 1 4 -2 -4 3512.64 162.167 3 -4 2 4 3136.63 195.542 1 4 -2 -3 426.400 94.5101 1 4 -2 -3 465.674 67.2105 3 -4 2 3 524.205 83.6920 1 4 -2 -2 3215.28 271.094 6 4 -2 -2 4462.42 203.711 1 -4 2 2 3664.71 385.851 2 -4 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463.000 6 5 1 5 1697.16 259.326 2 -5 -1 -5 1884.05 202.872 2 5 1 5 1867.40 209.149 6 5 1 6 1143.92 208.970 2 -5 -1 -6 1084.55 151.057 2 5 1 6 1143.83 171.357 6 -5 -1 -7 214.495 65.8119 2 5 1 7 232.819 84.5262 6 5 1 8 11.5633 10.7780 5 -5 -1 -8 40.3359 34.6097 2 5 1 8-36.9418 35.6732 6 5 1 9 2.33943 21.3019 5 -5 -1 -9 76.1952 37.2611 2 5 1 9 117.636 59.3653 6 -5 -1 -10 221.698 70.6870 2 5 1 10 131.746 68.1132 6 -5 -1 -11 217.926 73.3880 2 5 1 11 202.283 107.449 6 -5 -1 -12 514.852 109.535 2 5 1 12 630.315 177.157 6 -5 -1 -13 181.153 68.9339 2 5 1 13 82.6379 83.7219 6 -5 -1 -14 117.373 56.3694 1 5 1 14 37.5678 51.9086 6 5 1 15 58.1511 66.9009 6 -5 -2 13 148.160 56.7832 3 5 2 -13 219.327 105.984 1 -5 -2 12 13.4851 17.7722 3 5 2 -12-42.6157 46.7677 1 -5 -2 11 252.740 66.5072 3 5 2 -11 367.290 129.204 1 -5 -2 10 1563.53 162.439 3 5 2 -10 2279.79 298.035 1 5 2 -9 1477.27 232.360 1 -5 -2 9 1172.78 137.213 3 -5 -2 8 81.6465 35.9038 3 5 2 -8 57.4321 60.8719 1 -5 -2 7-18.4965 24.9512 3 5 2 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56.1913 45.8304 5 -5 -6 -8 19.8855 27.6782 2 5 6 9 110.826 48.6388 5 -5 -6 -9 120.148 54.5298 2 5 6 10 67.0715 45.0024 5 -5 -6 -10 53.9788 25.4568 4 -5 -6 -10 78.2517 43.4879 2 5 6 11-35.0275 38.8501 5 -5 -6 -11-11.8231 18.2805 4 -5 -6 -11 2.06212 16.1511 2 5 6 12 756.511 174.244 5 -5 -6 -12 915.640 115.759 4 -5 -6 -12 904.873 150.412 2 5 6 13 173.119 95.3526 5 -5 -6 -13 169.971 51.3451 4 -5 -6 -13 163.598 71.0770 2 -5 -6 -14 259.029 83.4052 2 5 7 -11-139.931 91.0070 1 5 7 -10-117.122 55.8742 1 5 7 -9 199.073 91.2596 1 5 7 -8 803.200 192.322 1 5 7 -7 282.295 114.537 1 5 7 -6 491.222 143.306 1 -5 -7 5 287.646 80.2711 3 5 7 -5 423.058 131.348 1 5 7 -4 17.2822 23.0342 1 -5 -7 4 18.7056 28.5318 3 -5 -7 4-22.2200 79.9129 2 5 7 -3 298.890 84.5040 1 -5 -7 3 505.061 104.993 3 -5 -7 3 641.930 202.228 2 -5 -7 2 540.238 112.836 1 5 7 -2 745.210 113.085 1 -5 -7 2 440.959 100.545 3 -5 -7 2 438.920 173.929 2 -5 -7 1 431.512 104.215 3 -5 -7 1 659.297 205.997 2 -5 -7 1 745.475 139.470 1 -5 -7 0 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491.536 119.544 2 5 8 4 317.031 144.327 2 -5 -8 -5 2565.68 265.082 2 -5 -8 -6 466.548 109.552 2 5 8 6 559.868 132.879 5 -5 -8 -7 74.4684 50.2698 2 5 8 7 13.4138 23.9384 5 -5 -8 -8 332.150 75.4019 4 -5 -8 -8 236.437 70.4269 2 5 8 8 263.128 97.9986 5 -5 -8 -9 285.855 72.6773 4 -5 -8 -9 261.047 78.8779 2 5 8 9 280.602 97.4859 5 5 8 10 523.205 138.490 5 -5 -8 -10 707.281 116.096 4 -5 -8 -10 695.056 129.494 2 -5 -8 -11 1615.99 177.416 4 -5 -8 -11 2052.73 224.495 2 5 8 11 1776.60 268.956 5 5 8 12 460.246 146.063 5 -5 -8 -12 435.773 92.7450 4 -5 -8 -12 475.715 111.516 2 5 8 13 6.35191 25.1282 5 -5 -8 -13 31.6719 35.8019 2 -5 -8 -14 8.88043 15.4894 2 5 9 -10 10.4978 31.2769 1 5 9 -9 8.63803 25.1865 1 5 9 -8 75.4833 60.2384 1 5 9 -7-26.1969 39.2458 1 5 9 -6 13.4015 28.4252 1 -5 -9 6 20.0521 44.5750 2 -5 -9 5 482.553 115.063 3 -5 -9 5 593.964 204.639 2 5 9 -5 371.896 115.174 1 -5 -9 4 92.3540 56.7327 3 -5 -9 4 124.435 94.1119 2 5 9 -4 106.489 54.1264 1 -5 -9 3 167.375 63.8538 3 -5 -9 3 221.077 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234.003 75.1032 1 -7 5 7 46.6835 73.8394 5 -7 5 7-7.96858 64.1232 2 -7 5 6 180.716 153.162 5 -7 5 6 13.1936 81.2382 2 -7 5 5 160.075 100.469 5 -7 5 5 339.633 147.517 2 -7 5 4 1134.07 264.657 5 -7 5 4 1259.42 293.441 2 -7 5 3 1288.00 264.338 5 -7 5 3 1484.80 283.392 2 -7 5 2 284.132 116.032 5 7 -5 -2 335.392 139.379 6 -7 5 2 356.891 121.827 2 -7 5 1 272.579 113.122 5 -7 5 1 399.707 107.948 2 7 -5 -1 174.997 97.8587 6 -7 5 0 2.91552 24.2531 5 7 -5 0 96.1922 87.7771 6 7 -5 1 158.843 99.3227 6 -7 5 -1 426.740 112.669 5 -7 5 -2 1.05515 22.4216 2 7 -5 2 30.9471 35.8242 6 -7 5 -2 32.2928 31.9709 5 -7 5 -3 27.2111 25.2667 2 7 -5 3 75.6517 99.7972 6 -7 5 -4 130.180 45.6972 2 7 -5 4 86.4821 84.8781 6 -7 5 -5 158.774 47.8182 2 7 -5 5 271.461 142.371 6 7 -5 6 385.832 177.036 6 7 -5 7-76.1477 80.9818 6 7 -5 8 8.52064 69.8033 6 7 -4 -12-14.2107 32.3473 1 7 -4 -11 114.880 79.1411 1 7 -4 -10 178.028 98.4729 1 7 -4 -9-15.5864 31.3556 1 7 -4 -8 245.242 96.0974 1 7 -4 -7 934.385 150.205 1 -7 4 6 336.931 168.376 2 -7 4 5-127.996 102.494 2 -7 4 4-10.8250 43.4859 5 -7 4 4 55.9795 72.5304 2 -7 4 3 1061.84 238.037 5 -7 4 3 1469.58 318.868 2 -7 4 3 946.345 145.669 1 -7 4 2 543.987 160.287 5 -7 4 2 377.169 97.5010 1 7 -4 -2 659.046 172.965 6 -7 4 2 340.584 135.586 2 -7 4 1 1280.23 237.661 2 7 -4 -1 1314.70 245.264 6 -7 4 1 1367.35 232.024 5 -7 4 1 1468.02 204.393 1 -7 4 0 1169.21 193.491 1 -7 4 0 1265.78 198.861 2 7 -4 0 1125.02 228.412 6 -7 4 0 1032.83 184.635 5 -7 4 -1 321.779 90.9972 5 -7 4 -1 318.345 94.3628 2 -7 4 -1 275.710 94.3774 1 7 -4 1 248.426 121.179 6 -7 4 -2 522.872 112.782 2 -7 4 -2 289.066 93.5174 1 7 -4 2 426.424 153.417 6 -7 4 -2 498.920 103.388 5 -7 4 -3 50.2647 32.8866 2 7 -4 3 51.8601 50.8452 6 -7 4 -4 84.5359 38.5796 2 7 -4 4 70.8989 59.9297 6 -7 4 -5 220.417 63.7002 2 7 -4 5 146.613 92.4436 6 -7 4 -6 44.3447 30.7678 2 7 -4 6-35.7984 44.1203 6 -7 4 -7 43.6672 35.8210 2 7 -4 7 55.5100 57.2259 6 -7 4 -8 1297.16 159.018 2 7 -4 8 1228.06 300.689 6 -7 4 -9 76.5335 44.0058 2 7 -4 9 91.1589 107.299 6 -7 4 -10 108.731 51.8328 2 7 -4 10 55.1458 101.908 6 -7 4 -11 32.2723 33.9120 1 7 -3 -12 34.9033 48.3584 1 7 -3 -11-69.8555 62.8476 1 7 -3 -10 137.844 86.1164 1 7 -3 -9 58.3026 56.2542 1 7 -3 -8 297.764 115.835 1 7 -3 -7 608.077 148.633 1 7 -3 -6 1610.14 188.049 1 -7 3 5 817.355 255.455 2 7 -3 -4 184.450 56.9647 3 -7 3 4 635.872 220.782 2 7 -3 -3 372.260 83.4353 3 -7 3 3 553.959 221.469 2 -7 3 2-4.73575 24.3032 5 -7 3 2 18.8775 24.8610 1 7 -3 -2-23.1225 35.8238 6 -7 3 2 14.3134 50.6110 2 -7 3 1 44.9947 27.8281 5 7 -3 -1 63.5681 58.7838 6 -7 3 1-26.7452 30.3293 1 -7 3 1-46.9204 56.4159 2 -7 3 0-43.1628 64.7716 2 -7 3 0 60.4340 39.3276 5 -7 3 0-15.3924 24.6003 1 -7 3 -1 142.556 56.1642 5 -7 3 -1 174.240 74.0143 2 7 -3 1 323.336 126.967 6 -7 3 -1 112.372 63.7500 1 -7 3 -2 849.691 156.269 1 -7 3 -2 1483.48 206.318 2 7 -3 2 1498.92 264.877 6 -7 3 -2 1528.10 166.696 5 -7 3 -3 283.403 92.8182 2 7 -3 3 129.674 80.5910 6 -7 3 -4 44.0896 28.8616 2 7 -3 4 32.3280 31.2161 6 7 -3 4 7.45651 49.5836 2 -7 3 -5 1.40416 26.8240 2 7 -3 5 95.9324 75.5720 6 -7 3 -6-2.11422 15.4009 2 7 -3 6 13.1766 50.2367 6 -7 3 -7 77.2529 43.8822 2 7 -3 7 107.426 81.1276 6 -7 3 -8 468.130 102.194 2 7 -3 8 330.342 160.697 6 -7 3 -9 260.405 74.1405 2 7 -3 9 386.981 163.068 6 -7 3 -10 348.927 90.2642 2 7 -3 10 437.287 194.644 6 -7 3 -11 344.105 93.8029 2 7 -3 11 396.658 200.518 6 -7 3 -12 60.3499 40.4130 1 7 -2 -12 244.038 129.137 1 7 -2 -11-33.2749 46.4480 1 7 -2 -10-45.6271 60.8386 1 7 -2 -9-17.6027 53.3318 1 7 -2 -8 45.7072 34.0520 1 7 -2 -7 188.675 92.3103 1 7 -2 -6 1137.88 198.650 1 7 -2 -5 2832.04 245.141 1 -7 2 5 2216.09 412.076 2 7 -2 -4 58.0742 30.1376 3 -7 2 4 34.3521 117.445 2 7 -2 -3 396.647 83.2936 3 -7 2 3 609.212 228.366 2 7 -2 -2 347.901 86.6246 3 -7 2 2 460.995 114.774 1 -7 2 2 471.617 178.910 2 7 -2 -1 32.0010 46.2455 6 -7 2 1 59.7262 40.1608 1 -7 2 1 88.6685 117.141 2 -7 2 0 58.2475 41.2507 5 -7 2 0 46.7923 42.0439 1 7 -2 0 25.6314 36.0325 6 -7 2 0 4.74919 55.5401 2 -7 2 -1 441.491 135.188 2 -7 2 -1 393.222 93.8160 5 -7 2 -1 405.650 113.925 1 7 -2 1 188.819 98.2379 6 -7 2 -2 695.226 154.867 2 -7 2 -2 434.589 98.4748 1 7 -2 2 908.797 187.270 6 -7 2 -2 735.473 104.069 5 7 -2 3 1637.25 305.845 2 -7 2 -3 2018.68 246.541 2 7 -2 3 1628.78 267.975 6 -7 2 -4 1035.67 169.880 2 7 -2 4 979.141 211.052 6 -7 2 -5 500.574 111.990 2 7 -2 5 572.913 165.774 6 -7 2 -6 57.1402 32.7369 2 7 -2 6 25.0138 36.2581 6 -7 2 -7 515.495 110.308 2 7 -2 7 365.178 140.551 6 -7 2 -8-83.9654 44.9868 2 7 -2 8 132.354 118.763 6 -7 2 -9 588.057 117.130 2 7 -2 9 416.191 157.958 6 -7 2 -10 72.4459 39.4135 2 7 -2 10 117.343 88.8489 6 -7 2 -11 64.0376 42.3707 2 7 -2 11-127.628 96.8965 6 -7 2 -12 335.738 97.2817 2 7 -2 12 84.1679 84.7703 6 -7 2 -13-87.0080 51.3879 2 7 -2 13-155.689 113.290 6 7 -1 -12 627.209 188.475 1 7 -1 -11 183.294 94.4864 1 7 -1 -10 853.980 213.738 1 7 -1 -9 446.020 146.878 1 7 -1 -8-40.1569 63.4605 1 7 -1 -7 495.151 153.595 1 7 -1 -6 10.3536 24.0738 1 7 -1 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31.1510 6 7 0 7 1958.22 283.368 6 -7 0 -7 2022.53 232.444 2 -7 0 -8 164.166 62.9496 2 7 0 8 159.410 88.2817 6 -7 0 -9 164.911 84.5063 2 7 0 9 164.224 75.3402 6 -7 0 -10 34.5679 43.9719 2 7 0 10 15.5161 56.0251 6 -7 0 -11 11.6971 21.2983 2 7 0 11 8.18425 32.3440 6 -7 0 -12-53.7095 39.7638 2 7 0 12 89.4572 80.7628 6 -7 0 -13 109.770 54.9470 2 7 0 13 232.145 127.495 6 7 1 -11-132.766 85.5609 1 7 1 -10 169.579 78.8301 1 7 1 -9 165.375 93.0344 1 7 1 -8 1556.34 266.367 1 7 1 -7 234.239 102.736 1 7 1 -6 1381.12 239.745 1 7 1 -5 2173.04 285.143 1 7 1 -4 20.8020 31.2356 1 -7 -1 4 79.7976 102.929 2 7 1 -3 35.0345 24.7679 3 -7 -1 3 55.2506 97.4964 2 7 1 -2 25.1560 13.9383 3 -7 -1 2 11.0226 116.304 2 7 1 -1 33.7385 28.7622 3 -7 -1 1-13.0036 42.3012 6 7 1 0 2393.73 242.697 3 -7 -1 0 3010.68 478.551 2 -7 -1 0 2594.84 324.127 6 -7 -1 -1 2137.36 363.525 2 -7 -1 -1 2212.82 294.259 6 -7 -1 -2 3102.32 395.634 2 7 1 2 3021.76 301.799 6 -7 -1 -2 2610.71 313.928 6 -7 -1 -3 102.032 75.6315 2 7 1 3 135.396 72.5503 6 -7 -1 -3 136.340 70.1054 6 -7 -1 -4 36.0097 26.5006 2 7 1 4 81.1225 65.9704 6 -7 -1 -4 70.6213 56.5162 6 -7 -1 -5 72.4342 49.0990 2 7 1 5 52.7457 49.3642 6 -7 -1 -5 112.866 70.2474 6 -7 -1 -6 475.599 119.323 2 7 1 6 295.244 100.154 6 -7 -1 -7 158.603 66.2668 2 7 1 7 203.384 96.0826 6 -7 -1 -8 600.768 129.137 2 7 1 8 591.858 150.168 6 -7 -1 -9 1193.83 181.373 2 7 1 9 1011.13 203.627 6 -7 -1 -10 653.713 130.665 2 7 1 10 614.265 164.556 6 -7 -1 -11 149.052 67.5839 2 7 1 11 147.230 85.1539 6 -7 -1 -12 61.8539 46.1789 2 7 1 12-48.5012 47.5851 6 -7 -1 -13 7.61648 15.6726 2 7 1 13 126.728 85.9869 6 7 2 -11 109.154 89.2428 1 -7 -2 11 45.2744 31.7692 3 7 2 -10 26.7441 50.7386 1 -7 -2 10 50.6167 31.3481 3 7 2 -9 180.022 95.9502 1 -7 -2 9 109.661 61.4865 3 7 2 -8 1031.68 222.613 1 -7 -2 8 806.450 151.399 3 -7 -2 7 382.079 105.368 3 7 2 -7 376.146 133.034 1 7 2 -6 564.855 158.042 1 7 2 -5 227.961 95.3167 1 7 2 -4 286.130 86.1600 1 -7 -2 4 439.901 208.321 2 -7 -2 3 513.878 221.632 2 7 2 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257.492 101.471 1 -7 -3 11 185.520 70.7618 3 7 3 -10 67.1312 33.4419 1 -7 -3 10 24.4794 26.8480 3 7 3 -9-11.5955 36.6130 1 -7 -3 9 90.1048 49.1078 3 -7 -3 8 237.578 78.1340 3 7 3 -8 470.249 147.874 1 -7 -3 7 65.4493 37.5855 3 7 3 -7 138.669 79.2654 1 7 3 -6 4.24750 26.0517 1 -7 -3 6 21.3933 30.0463 3 7 3 -5 4797.88 439.425 1 -7 -3 5 4498.10 359.678 3 7 3 -4 3883.65 334.004 1 -7 -3 4 7159.06 788.826 2 7 3 -3 7623.17 390.603 1 -7 -3 3 7004.10 800.910 2 -7 -3 2 114.269 65.9640 6 -7 -3 2 116.447 61.7605 2 -7 -3 1 582.699 132.234 6 -7 -3 1 1233.09 331.405 2 -7 -3 0 2599.23 468.596 2 -7 -3 0 2339.71 281.674 6 -7 -3 -1 1078.38 188.512 6 -7 -3 -1 1072.50 273.699 2 -7 -3 -2 1685.72 316.339 2 -7 -3 -2 1697.31 232.085 6 -7 -3 -3 1.44973 21.9476 6 -7 -3 -3 37.4631 24.1145 5 -7 -3 -4 2020.21 290.435 2 -7 -3 -4 1811.16 231.810 6 -7 -3 -4 1699.63 133.275 5 -7 -3 -5 2790.05 320.739 2 7 3 5 2519.57 230.991 6 -7 -3 -5 2493.16 269.076 6 -7 -3 -6 374.789 117.373 2 7 3 6 416.277 98.7012 6 -7 -3 -7 403.200 113.042 2 7 3 7 418.960 104.311 6 -7 -3 -8 13.5410 26.7631 2 7 3 8 7.78587 22.5124 6 -7 -3 -9 274.848 90.9307 2 7 3 9 200.482 71.9068 6 -7 -3 -10 188.784 74.1074 2 7 3 10 169.627 85.9371 6 -7 -3 -11 109.749 51.6461 2 7 3 11 70.4497 42.1074 6 -7 -3 -12 228.430 80.8957 2 -7 -3 -13 125.439 63.8609 2 -7 -4 12-1.43483 11.9249 3 7 4 -11 332.071 143.725 1 -7 -4 11 233.032 79.2323 3 7 4 -10 120.791 89.3839 1 -7 -4 10 268.651 84.6592 3 7 4 -9 527.337 170.390 1 -7 -4 9 374.526 97.3126 3 -7 -4 8 208.168 72.6495 3 7 4 -8 344.862 118.166 1 -7 -4 7 520.290 115.464 3 7 4 -7 677.780 179.485 1 7 4 -6 125.887 62.2301 1 -7 -4 6 153.596 59.6519 3 -7 -4 5 1.73599 28.8587 3 7 4 -5 31.0610 64.6986 1 7 4 -4-61.4082 44.8406 1 -7 -4 4 81.0299 50.8093 3 -7 -4 4-90.0703 139.165 2 7 4 -3 446.944 97.8287 1 -7 -4 3 358.449 214.596 2 -7 -4 2 5659.42 726.783 2 -7 -4 1 3090.79 538.232 2 -7 -4 1 2174.10 249.027 6 -7 -4 0 1017.64 168.826 6 -7 -4 0 1553.09 354.237 2 -7 -4 -1 64.2342 52.7768 6 -7 -4 -1 45.1267 61.2372 2 -7 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-11 1 -5 200.690 91.4391 2 11 -1 5 163.555 100.084 6 -11 1 -6 254.887 107.210 2 11 -1 6 109.700 104.849 6 -11 1 -7 3.95299 17.1216 2 -11 0 5-32.2843 79.7553 2 -11 0 4 177.710 159.039 2 -11 0 3 314.032 181.208 2 -11 0 2 464.051 259.627 2 -11 0 1 599.357 249.782 2 -11 0 0 353.491 179.082 2 -11 0 -1 55.9473 70.5146 2 -11 0 -2 86.7211 81.3731 2 -11 0 -3 71.7573 70.9222 2 -11 0 -4-45.5457 55.7354 2 -11 0 -5 215.904 111.168 2 11 0 5 286.394 145.028 6 -11 0 -6 429.368 156.189 2 11 0 6 293.462 136.096 6 -11 0 -7 76.4550 57.7547 2 11 0 7 5.38840 27.3611 6 11 0 8 278.518 143.985 6 -11 -1 5 76.9383 116.281 2 -11 -1 4-136.437 141.443 2 -11 -1 3-118.211 132.355 2 -11 -1 2-410.842 226.811 2 -11 -1 1 98.6519 111.394 2 -11 -1 0 313.694 172.121 2 -11 -1 -1 518.396 223.414 2 -11 -1 -2 786.456 246.783 2 -11 -1 -3 211.913 129.202 2 -11 -1 -4 198.966 120.645 2 -11 -1 -5 18.8363 28.8705 2 -11 -1 -6-9.97265 41.0438 2 11 1 6 74.9875 63.5227 6 -11 -1 -7 223.269 108.496 2 11 1 7 97.1981 73.1458 6 -11 -2 5 171.303 184.035 2 -11 -2 4 58.9242 102.462 2 -11 -2 3 102.771 63.7975 2 -11 -2 2-0.92515 136.156 2 -11 -2 1 656.670 274.284 2 -11 -2 0 82.6976 102.090 2 -11 -2 -1 460.149 206.218 2 -11 -2 -2-8.26698 90.2684 2 -11 -2 -3 1072.82 288.121 2 -11 -2 -4-17.5051 44.7809 2 -11 -2 -5-120.445 90.6159 2 -11 -2 -6-33.3840 47.0128 2 -11 -2 -7 125.499 96.1445 2 -11 -3 4 144.356 129.426 2 -11 -3 3 544.446 312.448 2 -11 -3 2 131.398 94.4013 2 -11 -3 1 316.373 217.194 2 -11 -3 0 9.14305 55.6884 2 -11 -3 -1 9.42106 47.8171 2 -11 -3 -2 113.674 95.4499 2 -11 -3 -3 318.142 176.348 2 -11 -3 -4-150.539 108.223 2 -11 -3 -5 1321.45 301.782 2 -11 -3 -6 474.787 171.401 2 -11 -3 -7 215.601 115.798 2 -11 -4 4-23.5729 96.2809 2 -11 -4 3 59.4995 97.9751 2 -11 -4 2 446.243 264.042 2 -11 -4 1 841.010 342.184 2 -11 -4 0 632.536 298.291 2 -11 -4 -1 124.185 121.240 2 -11 -4 -2 119.413 120.945 2 -11 -4 -3 55.6223 75.1526 2 -11 -4 -4 1.66279 60.6438 2 -11 -4 -5 298.807 156.594 2 -11 -4 -6 257.585 142.041 2 -11 -4 -7 419.694 161.133 2 -11 -5 3 343.247 280.243 2 -11 -5 2 462.351 249.597 2 -11 -5 1 254.298 165.059 2 -11 -5 0 465.542 233.809 2 -11 -5 -1 469.555 240.710 2 -11 -5 -2 478.534 208.717 2 -11 -5 -3 64.0180 88.0189 2 -11 -5 -4 61.2874 46.4040 2 -11 -5 -5 136.196 102.746 2 -11 -5 -6-7.46807 34.6188 2 -11 -5 -7-11.1954 45.5713 2 -11 -6 2 296.762 217.079 2 -11 -6 1 172.282 114.086 2 -11 -6 0 422.682 216.106 2 -11 -6 -1 189.293 151.008 2 -11 -6 -2 396.742 201.095 2 -11 -6 -3-0.63988 33.0570 2 -11 -6 -4 62.0142 71.7116 2 -11 -6 -5-8.74432 37.1008 2 -11 -6 -6 17.8540 37.9303 2 -11 -7 1 58.9719 96.2182 2 -11 -7 0-261.795 185.042 2 -11 -7 -1-157.972 135.938 2 -11 -7 -2-102.434 114.784 2 -11 -7 -3 464.683 205.028 2 -11 -7 -4 337.032 198.271 2 -11 -7 -5 525.179 205.684 2 -11 -8 -1 4.54097 55.2646 2 -11 -8 -2 220.889 148.434 2 -11 -8 -3 248.506 142.901 2 -11 -8 -4-50.3947 96.2173 2 -12 1 1 149.006 157.995 2 -12 1 0 171.521 119.904 2 -12 1 -1 357.226 165.946 2 -12 1 -2-6.99967 29.0861 2 -12 1 -3-0.46283 14.5144 2 -12 0 1 117.247 112.859 2 -12 0 0 495.952 227.028 2 -12 0 -1 27.6903 55.9846 2 -12 0 -2 691.429 246.541 2 -12 0 -3 150.782 104.400 2 -12 0 -4 4.74519 22.9043 2 -12 -1 1 35.2654 98.0270 2 -12 -1 0 174.174 143.411 2 -12 -1 -1 81.2794 102.795 2 -12 -1 -2 612.098 232.247 2 -12 -1 -3 50.9850 63.3615 2 -12 -2 0-65.2339 89.2823 2 -12 -2 -1 125.700 112.605 2 -12 -2 -2 39.5323 68.8502 2 -12 -2 -3 285.710 151.490 2 -12 -3 -1 258.516 169.291 2 -12 -3 -2 15.2722 49.8294 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 41979 data_11 #============================================================================== # PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic 2024-03-26 _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code AW5090 _journal_coeditor_notes ; ? ; _journal_paper_category FA _journal_techeditor_code ? _iucr_compatibility_tag ACTA95 _journal_techeditor_notes ; ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C4 H8 O2)' _chemical_formula_sum 'C44 H48 Cl2 Cu N8 O12' _chemical_formula_weight 1015.34 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0363(5) _cell_length_b 10.1867(6) _cell_length_c 11.9902(6) _cell_angle_alpha 83.078(5) _cell_angle_beta 82.032(4) _cell_angle_gamma 70.015(5) _cell_volume 1137.37(11) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 3986 _cell_measurement_theta_min 3.8780 _cell_measurement_theta_max 28.8990 _exptl_crystal_description prism _exptl_crystal_colour orange _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.482 _exptl_crystal_F_000 527 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.10 _exptl_absorpt_coefficient_mu 0.670 _shelx_estimated_absorpt_T_min 0.900 _shelx_estimated_absorpt_T_max 0.936 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.703 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 9285 _diffrn_reflns_av_unetI/netI 0.0448 _diffrn_reflns_av_R_equivalents 0.0326 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 2.845 _diffrn_reflns_theta_max 26.997 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.983 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.983 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 4877 _reflns_number_gt 4265 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0508P)^2^+0.8435P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4877 _refine_ls_number_parameters 312 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.0496 _refine_ls_R_factor_gt 0.0423 _refine_ls_wR_factor_ref 0.1132 _refine_ls_wR_factor_gt 0.1070 _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_restrained_S_all 1.067 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 1.0000 0.5000 1.0000 0.01548(12) Uani 1 2 d S . P . . N1A N 0.60749(19) 0.7687(2) 0.92316(15) 0.0180(4) Uani 1 1 d D . . . . H1A H 0.5210(13) 0.785(3) 0.913(2) 0.027 Uiso 1 1 d D U . . . C2A C 0.6982(2) 0.6449(2) 0.95736(18) 0.0183(4) Uani 1 1 d . . . . . H2A H 0.6755 0.5609 0.9733 0.022 Uiso 1 1 calc R U . . . N3A N 0.82432(19) 0.65544(19) 0.96611(15) 0.0170(4) Uani 1 1 d . . . . . C4A C 0.8111(2) 0.7942(2) 0.93622(18) 0.0169(4) Uani 1 1 d . . . . . H4A H 0.8847 0.8333 0.9350 0.020 Uiso 1 1 calc R U . . . C5A C 0.6764(2) 0.8670(2) 0.90860(17) 0.0166(4) Uani 1 1 d . . . . . C6A C 0.6084(2) 1.0129(2) 0.86708(17) 0.0169(4) Uani 1 1 d . . . . . C7A C 0.4766(2) 1.0548(3) 0.8247(2) 0.0231(5) Uani 1 1 d . . . . . H7A H 0.4300 0.9883 0.8229 0.028 Uiso 1 1 calc R U . . . C8A C 0.4128(3) 1.1928(3) 0.7853(2) 0.0269(5) Uani 1 1 d . . . . . H8A H 0.3225 1.2203 0.7571 0.032 Uiso 1 1 calc R U . . . C9A C 0.4799(3) 1.2909(3) 0.7865(2) 0.0261(5) Uani 1 1 d . . . . . H9A H 0.4359 1.3855 0.7595 0.031 Uiso 1 1 calc R U . . . C10A C 0.6115(3) 1.2498(3) 0.8277(2) 0.0251(5) Uani 1 1 d . . . . . H10A H 0.6583 1.3165 0.8282 0.030 Uiso 1 1 calc R U . . . C11A C 0.6758(2) 1.1119(2) 0.86818(19) 0.0208(5) Uani 1 1 d . . . . . H11A H 0.7658 1.0849 0.8967 0.025 Uiso 1 1 calc R U . . . N1B N 0.9876(2) 0.6772(2) 1.29786(16) 0.0198(4) Uani 1 1 d D . . . . H1B H 1.016(3) 0.726(3) 1.337(2) 0.030 Uiso 1 1 d D U . . . N3B N 0.98404(19) 0.56610(19) 1.15271(15) 0.0166(4) Uani 1 1 d . . . . . C2B C 1.0324(2) 0.6575(2) 1.18829(19) 0.0209(5) Uani 1 1 d . . . . . H2B H 1.0910 0.7032 1.1425 0.025 Uiso 1 1 calc R U . . . C4B C 0.9050(2) 0.5250(2) 1.24494(18) 0.0163(4) Uani 1 1 d . . . . . H4B H 0.8573 0.4588 1.2451 0.020 Uiso 1 1 calc R U . . . C5B C 0.9052(2) 0.5935(2) 1.33614(18) 0.0159(4) Uani 1 1 d . . . . . C6B C 0.8283(2) 0.5926(2) 1.44915(18) 0.0166(4) Uani 1 1 d . . . . . C7B C 0.8361(2) 0.6741(3) 1.53131(19) 0.0224(5) Uani 1 1 d . . . . . H7B H 0.8962 0.7301 1.5158 0.027 Uiso 1 1 calc R U . . . C8B C 0.7567(3) 0.6743(3) 1.6363(2) 0.0253(5) Uani 1 1 d . . . . . H8B H 0.7638 0.7296 1.6922 0.030 Uiso 1 1 calc R U . . . C9B C 0.6678(3) 0.5947(3) 1.6594(2) 0.0252(5) Uani 1 1 d . . . . . H9B H 0.6122 0.5965 1.7305 0.030 Uiso 1 1 calc R U . . . C10B C 0.6600(3) 0.5123(3) 1.5785(2) 0.0316(6) Uani 1 1 d . . . . . H10B H 0.6001 0.4561 1.5946 0.038 Uiso 1 1 calc R U . . . C11B C 0.7393(3) 0.5113(3) 1.4741(2) 0.0289(6) Uani 1 1 d . . . . . H11B H 0.7330 0.4546 1.4190 0.035 Uiso 1 1 calc R U . . . Cl Cl 0.72729(6) 0.29022(6) 1.13303(5) 0.02421(15) Uani 1 1 d . . . . . O1 O 0.84558(17) 0.32499(18) 1.06948(14) 0.0255(4) Uani 1 1 d . . . . . O2 O 0.71998(19) 0.31419(19) 1.24939(14) 0.0290(4) Uani 1 1 d . . . . . O3 O 0.7446(3) 0.1466(2) 1.12386(18) 0.0590(7) Uani 1 1 d . . . . . O4 O 0.5982(2) 0.3768(3) 1.08721(17) 0.0452(6) Uani 1 1 d . . . . . C12 C 0.9753(3) -0.0701(3) 0.6799(2) 0.0310(6) Uani 1 1 d . . . . . H12A H 1.0431 -0.1357 0.6286 0.046 Uiso 1 1 calc R U . . . H12B H 0.9179 -0.1184 0.7299 0.046 Uiso 1 1 calc R U . . . H12C H 1.0276 -0.0346 0.7254 0.046 Uiso 1 1 calc R U . . . C13 C 0.8799(3) 0.0494(3) 0.61274(19) 0.0237(5) Uani 1 1 d . . . . . C14 C 0.6787(3) 0.1169(3) 0.5061(2) 0.0280(5) Uani 1 1 d . . . . . H14A H 0.7165 0.1920 0.4715 0.034 Uiso 1 1 calc R U . . . H14B H 0.5908 0.1594 0.5561 0.034 Uiso 1 1 calc R U . . . C15 C 0.6465(3) 0.0450(3) 0.4156(2) 0.0314(6) Uani 1 1 d . . . . . H15A H 0.7310 0.0137 0.3611 0.047 Uiso 1 1 calc R U . . . H15B H 0.5672 0.1106 0.3768 0.047 Uiso 1 1 calc R U . . . H15C H 0.6203 -0.0362 0.4501 0.047 Uiso 1 1 calc R U . . . O5 O 0.8893(2) 0.1657(2) 0.59590(15) 0.0315(4) Uani 1 1 d . . . . . O6 O 0.78386(18) 0.01200(18) 0.57048(15) 0.0275(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0173(2) 0.0191(2) 0.00949(19) -0.00302(14) 0.00155(14) -0.00581(15) N1A 0.0153(9) 0.0252(10) 0.0151(9) -0.0041(8) 0.0016(7) -0.0092(8) C2A 0.0211(11) 0.0208(11) 0.0144(10) -0.0032(9) 0.0019(9) -0.0097(9) N3A 0.0194(9) 0.0218(9) 0.0108(9) -0.0020(7) 0.0017(7) -0.0090(8) C4A 0.0169(10) 0.0211(11) 0.0139(10) -0.0025(8) 0.0010(8) -0.0083(9) C5A 0.0172(10) 0.0227(11) 0.0110(10) -0.0051(8) 0.0035(8) -0.0087(9) C6A 0.0170(10) 0.0216(11) 0.0102(10) -0.0037(8) 0.0049(8) -0.0057(9) C7A 0.0234(11) 0.0256(12) 0.0196(11) -0.0029(9) -0.0019(9) -0.0071(10) C8A 0.0224(12) 0.0312(13) 0.0218(12) -0.0020(10) -0.0033(10) -0.0016(10) C9A 0.0284(12) 0.0215(11) 0.0197(12) -0.0004(9) 0.0058(10) -0.0007(10) C10A 0.0281(12) 0.0228(11) 0.0235(12) -0.0035(10) 0.0058(10) -0.0099(10) C11A 0.0174(10) 0.0257(11) 0.0185(11) -0.0033(9) 0.0034(9) -0.0077(9) N1B 0.0237(10) 0.0250(10) 0.0149(9) -0.0062(8) 0.0017(8) -0.0133(8) N3B 0.0159(8) 0.0204(9) 0.0127(9) -0.0025(7) 0.0009(7) -0.0053(7) C2B 0.0237(11) 0.0254(12) 0.0159(11) -0.0033(9) 0.0026(9) -0.0123(10) C4B 0.0175(10) 0.0187(10) 0.0132(10) -0.0014(8) 0.0004(8) -0.0073(8) C5B 0.0166(10) 0.0163(10) 0.0140(10) -0.0012(8) 0.0002(8) -0.0052(8) C6B 0.0170(10) 0.0187(10) 0.0126(10) -0.0009(8) -0.0008(8) -0.0045(8) C7B 0.0239(11) 0.0286(12) 0.0178(11) -0.0078(10) 0.0031(9) -0.0129(10) C8B 0.0289(12) 0.0314(13) 0.0167(11) -0.0105(10) 0.0042(10) -0.0112(11) C9B 0.0274(12) 0.0329(13) 0.0136(11) -0.0033(10) 0.0064(9) -0.0104(10) C10B 0.0421(15) 0.0391(15) 0.0217(12) -0.0046(11) 0.0066(11) -0.0270(13) C11B 0.0422(15) 0.0348(14) 0.0183(12) -0.0082(10) 0.0058(11) -0.0254(12) Cl 0.0354(3) 0.0313(3) 0.0150(3) -0.0008(2) -0.0007(2) -0.0237(3) O1 0.0230(8) 0.0319(9) 0.0218(9) -0.0027(7) 0.0060(7) -0.0123(7) O2 0.0403(10) 0.0394(10) 0.0152(8) -0.0046(7) 0.0017(7) -0.0244(9) O3 0.128(2) 0.0410(12) 0.0282(11) -0.0047(9) -0.0021(13) -0.0560(14) O4 0.0302(10) 0.0832(16) 0.0330(11) 0.0107(11) -0.0089(9) -0.0353(11) C12 0.0309(13) 0.0466(16) 0.0203(12) -0.0030(11) 0.0010(10) -0.0203(12) C13 0.0263(12) 0.0353(13) 0.0141(11) -0.0088(10) 0.0073(9) -0.0171(11) C14 0.0281(13) 0.0293(13) 0.0287(13) -0.0058(11) -0.0007(10) -0.0120(11) C15 0.0306(13) 0.0415(15) 0.0265(13) -0.0019(11) -0.0034(11) -0.0175(12) O5 0.0399(10) 0.0379(10) 0.0273(10) -0.0060(8) -0.0009(8) -0.0260(9) O6 0.0308(9) 0.0298(9) 0.0279(9) -0.0022(7) -0.0060(7) -0.0167(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.9790(18) 2_767 ? Cu N3A 1.9790(18) . ? Cu N3B 1.9934(17) . ? Cu N3B 1.9934(17) 2_767 ? N1A C2A 1.334(3) . ? N1A C5A 1.382(3) . ? N1A H1A 0.848(10) . ? C2A N3A 1.325(3) . ? C2A H2A 0.9500 . ? N3A C4A 1.381(3) . ? C4A C5A 1.366(3) . ? C4A H4A 0.9500 . ? C5A C6A 1.464(3) . ? C6A C7A 1.392(3) . ? C6A C11A 1.395(3) . ? C7A C8A 1.385(3) . ? C7A H7A 0.9500 . ? C8A C9A 1.385(4) . ? C8A H8A 0.9500 . ? C9A C10A 1.384(4) . ? C9A H9A 0.9500 . ? C10A C11A 1.389(3) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.344(3) . ? N1B C5B 1.380(3) . ? N1B H1B 0.857(10) . ? N3B C2B 1.321(3) . ? N3B C4B 1.378(3) . ? C2B H2B 0.9500 . ? C4B C5B 1.367(3) . ? C4B H4B 0.9500 . ? C5B C6B 1.464(3) . ? C6B C7B 1.389(3) . ? C6B C11B 1.395(3) . ? C7B C8B 1.393(3) . ? C7B H7B 0.9500 . ? C8B C9B 1.379(3) . ? C8B H8B 0.9500 . ? C9B C10B 1.384(3) . ? C9B H9B 0.9500 . ? C10B C11B 1.386(3) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.429(2) . ? Cl O2 1.4329(17) . ? Cl O4 1.434(2) . ? Cl O1 1.4446(16) . ? C12 C13 1.493(4) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 O5 1.211(3) . ? C13 O6 1.328(3) . ? C14 O6 1.452(3) . ? C14 C15 1.506(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 2_767 . ? N3A Cu N3B 89.86(7) 2_767 . ? N3A Cu N3B 90.14(7) . . ? N3A Cu N3B 90.14(7) 2_767 2_767 ? N3A Cu N3B 89.86(7) . 2_767 ? N3B Cu N3B 180.0 . 2_767 ? C2A N1A C5A 108.90(18) . . ? C2A N1A H1A 125.9(19) . . ? C5A N1A H1A 125.2(19) . . ? N3A C2A N1A 110.64(19) . . ? N3A C2A H2A 124.7 . . ? N1A C2A H2A 124.7 . . ? C2A N3A C4A 105.86(18) . . ? C2A N3A Cu 126.68(15) . . ? C4A N3A Cu 127.20(14) . . ? C5A C4A N3A 109.99(19) . . ? C5A C4A H4A 125.0 . . ? N3A C4A H4A 125.0 . . ? C4A C5A N1A 104.61(19) . . ? C4A C5A C6A 132.5(2) . . ? N1A C5A C6A 122.88(19) . . ? C7A C6A C11A 118.9(2) . . ? C7A C6A C5A 120.7(2) . . ? C11A C6A C5A 120.4(2) . . ? C8A C7A C6A 120.6(2) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C7A C8A C9A 120.4(2) . . ? C7A C8A H8A 119.8 . . ? C9A C8A H8A 119.8 . . ? C10A C9A C8A 119.4(2) . . ? C10A C9A H9A 120.3 . . ? C8A C9A H9A 120.3 . . ? C9A C10A C11A 120.6(2) . . ? C9A C10A H10A 119.7 . . ? C11A C10A H10A 119.7 . . ? C10A C11A C6A 120.2(2) . . ? C10A C11A H11A 119.9 . . ? C6A C11A H11A 119.9 . . ? C2B N1B C5B 108.05(18) . . ? C2B N1B H1B 124(2) . . ? C5B N1B H1B 128(2) . . ? C2B N3B C4B 105.76(18) . . ? C2B N3B Cu 131.48(15) . . ? C4B N3B Cu 122.63(14) . . ? N3B C2B N1B 111.1(2) . . ? N3B C2B H2B 124.5 . . ? N1B C2B H2B 124.5 . . ? C5B C4B N3B 109.98(19) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 105.11(18) . . ? C4B C5B C6B 130.0(2) . . ? N1B C5B C6B 124.73(19) . . ? C7B C6B C11B 118.5(2) . . ? C7B C6B C5B 122.5(2) . . ? C11B C6B C5B 118.96(19) . . ? C6B C7B C8B 120.6(2) . . ? C6B C7B H7B 119.7 . . ? C8B C7B H7B 119.7 . . ? C9B C8B C7B 120.3(2) . . ? C9B C8B H8B 119.9 . . ? C7B C8B H8B 119.9 . . ? C8B C9B C10B 119.6(2) . . ? C8B C9B H9B 120.2 . . ? C10B C9B H9B 120.2 . . ? C9B C10B C11B 120.3(2) . . ? C9B C10B H10B 119.9 . . ? C11B C10B H10B 119.9 . . ? C10B C11B C6B 120.7(2) . . ? C10B C11B H11B 119.6 . . ? C6B C11B H11B 119.6 . . ? O3 Cl O2 109.59(11) . . ? O3 Cl O4 108.88(15) . . ? O2 Cl O4 109.89(12) . . ? O3 Cl O1 110.03(13) . . ? O2 Cl O1 109.74(10) . . ? O4 Cl O1 108.70(11) . . ? C13 C12 H12A 109.5 . . ? C13 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C13 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O5 C13 O6 123.4(2) . . ? O5 C13 C12 125.0(2) . . ? O6 C13 C12 111.6(2) . . ? O6 C14 C15 107.7(2) . . ? O6 C14 H14A 110.2 . . ? C15 C14 H14A 110.2 . . ? O6 C14 H14B 110.2 . . ? C15 C14 H14B 110.2 . . ? H14A C14 H14B 108.5 . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 O6 C14 118.99(19) . . ? _refine_diff_density_max 0.664 _refine_diff_density_min -0.514 _refine_diff_density_rms 0.078 _shelx_res_file ; 11.res created by SHELXL-2014/7 TITL EL79E in P-1 CELL 0.71073 10.0363 10.1867 11.9902 83.078 82.032 70.015 ZERR 1 0.0005 0.0006 0.0006 0.005 0.004 0.005 LATT 1 SFAC C H N O CL CU UNIT 44 48 8 12 2 1 MERG 2 FMAP 2 OMIT -2 54 SIZE 0.16 0.13 0.10 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND $H HTAB L.S. 6 WGHT 0.050800 0.843500 FVAR 2.58332 CU 6 1.000000 0.500000 1.000000 10.50000 0.01726 0.01914 = 0.00949 -0.00302 0.00155 -0.00581 DFIX 0.86 0.01 N1A H1A N1B H1B N1A 3 0.607494 0.768652 0.923160 11.00000 0.01533 0.02516 = 0.01506 -0.00405 0.00164 -0.00921 H1A 2 0.521026 0.785288 0.913267 11.00000 -1.50000 C2A 1 0.698204 0.644946 0.957364 11.00000 0.02110 0.02081 = 0.01441 -0.00317 0.00190 -0.00967 AFIX 43 H2A 2 0.675528 0.560924 0.973260 11.00000 -1.20000 AFIX 0 N3A 3 0.824322 0.655441 0.966110 11.00000 0.01942 0.02181 = 0.01075 -0.00203 0.00175 -0.00896 C4A 1 0.811058 0.794221 0.936219 11.00000 0.01694 0.02106 = 0.01389 -0.00248 0.00099 -0.00833 AFIX 43 H4A 2 0.884734 0.833309 0.935043 11.00000 -1.20000 AFIX 0 C5A 1 0.676411 0.867005 0.908597 11.00000 0.01718 0.02267 = 0.01100 -0.00509 0.00353 -0.00871 C6A 1 0.608436 1.012870 0.867083 11.00000 0.01697 0.02163 = 0.01024 -0.00368 0.00488 -0.00565 C7A 1 0.476626 1.054848 0.824744 11.00000 0.02342 0.02564 = 0.01962 -0.00293 -0.00190 -0.00708 AFIX 43 H7A 2 0.430024 0.988265 0.822927 11.00000 -1.20000 AFIX 0 C8A 1 0.412842 1.192777 0.785258 11.00000 0.02236 0.03118 = 0.02177 -0.00202 -0.00331 -0.00158 AFIX 43 H8A 2 0.322527 1.220289 0.757104 11.00000 -1.20000 AFIX 0 C9A 1 0.479879 1.290889 0.786549 11.00000 0.02845 0.02148 = 0.01971 -0.00042 0.00583 -0.00074 AFIX 43 H9A 2 0.435946 1.385499 0.759464 11.00000 -1.20000 AFIX 0 C10A 1 0.611498 1.249808 0.827672 11.00000 0.02807 0.02284 = 0.02347 -0.00346 0.00583 -0.00993 AFIX 43 H10A 2 0.658268 1.316544 0.828192 11.00000 -1.20000 AFIX 0 C11A 1 0.675782 1.111873 0.868179 11.00000 0.01744 0.02569 = 0.01855 -0.00333 0.00344 -0.00771 AFIX 43 H11A 2 0.765831 1.084892 0.896700 11.00000 -1.20000 AFIX 0 N1B 3 0.987576 0.677174 1.297864 11.00000 0.02371 0.02501 = 0.01485 -0.00617 0.00171 -0.01326 H1B 2 1.016020 0.725898 1.336703 11.00000 -1.50000 N3B 3 0.984036 0.566097 1.152708 11.00000 0.01592 0.02038 = 0.01265 -0.00249 0.00094 -0.00533 C2B 1 1.032358 0.657470 1.188290 11.00000 0.02367 0.02544 = 0.01590 -0.00329 0.00261 -0.01225 AFIX 43 H2B 2 1.091045 0.703236 1.142455 11.00000 -1.20000 AFIX 0 C4B 1 0.904969 0.525001 1.244936 11.00000 0.01747 0.01867 = 0.01316 -0.00140 0.00045 -0.00734 AFIX 43 H4B 2 0.857323 0.458849 1.245082 11.00000 -1.20000 AFIX 0 C5B 1 0.905223 0.593453 1.336140 11.00000 0.01660 0.01631 = 0.01397 -0.00121 0.00016 -0.00521 C6B 1 0.828254 0.592616 1.449146 11.00000 0.01702 0.01869 = 0.01262 -0.00086 -0.00079 -0.00448 C7B 1 0.836090 0.674062 1.531307 11.00000 0.02395 0.02864 = 0.01776 -0.00777 0.00310 -0.01285 AFIX 43 H7B 2 0.896150 0.730111 1.515796 11.00000 -1.20000 AFIX 0 C8B 1 0.756658 0.674320 1.636296 11.00000 0.02891 0.03143 = 0.01667 -0.01051 0.00422 -0.01117 AFIX 43 H8B 2 0.763754 0.729572 1.692187 11.00000 -1.20000 AFIX 0 C9B 1 0.667801 0.594732 1.659419 11.00000 0.02740 0.03287 = 0.01357 -0.00335 0.00638 -0.01044 AFIX 43 H9B 2 0.612240 0.596495 1.730488 11.00000 -1.20000 AFIX 0 C10B 1 0.660007 0.512262 1.578512 11.00000 0.04208 0.03915 = 0.02173 -0.00463 0.00665 -0.02702 AFIX 43 H10B 2 0.600081 0.456110 1.594578 11.00000 -1.20000 AFIX 0 C11B 1 0.739289 0.511278 1.474145 11.00000 0.04222 0.03480 = 0.01830 -0.00816 0.00585 -0.02536 AFIX 43 H11B 2 0.732970 0.454596 1.419044 11.00000 -1.20000 AFIX 0 CL 5 0.727294 0.290220 1.133026 11.00000 0.03542 0.03130 = 0.01495 -0.00082 -0.00066 -0.02371 O1 4 0.845583 0.324988 1.069481 11.00000 0.02300 0.03186 = 0.02176 -0.00273 0.00603 -0.01234 O2 4 0.719984 0.314187 1.249392 11.00000 0.04033 0.03938 = 0.01524 -0.00460 0.00167 -0.02438 O3 4 0.744637 0.146619 1.123864 11.00000 0.12840 0.04099 = 0.02821 -0.00473 -0.00210 -0.05600 O4 4 0.598214 0.376763 1.087210 11.00000 0.03018 0.08320 = 0.03295 0.01067 -0.00893 -0.03526 C12 1 0.975312 -0.070112 0.679905 11.00000 0.03086 0.04661 = 0.02027 -0.00301 0.00098 -0.02027 AFIX 137 H12A 2 1.043068 -0.135746 0.628590 11.00000 -1.50000 H12B 2 0.917892 -0.118441 0.729860 11.00000 -1.50000 H12C 2 1.027639 -0.034596 0.725354 11.00000 -1.50000 AFIX 0 C13 1 0.879854 0.049390 0.612744 11.00000 0.02626 0.03529 = 0.01407 -0.00877 0.00727 -0.01711 C14 1 0.678702 0.116888 0.506086 11.00000 0.02811 0.02933 = 0.02869 -0.00577 -0.00070 -0.01196 AFIX 23 H14A 2 0.716510 0.192002 0.471451 11.00000 -1.20000 H14B 2 0.590845 0.159434 0.556126 11.00000 -1.20000 AFIX 0 C15 1 0.646478 0.044963 0.415619 11.00000 0.03059 0.04147 = 0.02648 -0.00194 -0.00340 -0.01753 AFIX 137 H15A 2 0.730996 0.013738 0.361070 11.00000 -1.50000 H15B 2 0.567216 0.110571 0.376798 11.00000 -1.50000 H15C 2 0.620256 -0.036215 0.450129 11.00000 -1.50000 AFIX 0 O5 4 0.889251 0.165669 0.595900 11.00000 0.03985 0.03786 = 0.02732 -0.00598 -0.00094 -0.02600 O6 4 0.783865 0.012002 0.570476 11.00000 0.03077 0.02985 = 0.02794 -0.00225 -0.00605 -0.01668 HKLF 4 REM EL79E in P-1 REM R1 = 0.0423 for 4265 Fo > 4sig(Fo) and 0.0496 for all 4877 data REM 312 parameters refined using 2 restraints END WGHT 0.0510 0.8564 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y+1, -z+2 HTAB N1A Cl_$1 HTAB N1A O3_$1 HTAB N1A O4_$1 HTAB C2A O4 EQIV $2 -x+2, -y+1, -z+2 HTAB C4A O1_$2 HTAB N1B O5_$2 HTAB C2B O1_$2 HTAB C4B O2 REM Highest difference peak 0.664, deepest hole -0.514, 1-sigma level 0.078 Q1 1 1.0029 1.0237 0.9544 11.00000 0.05 0.66 Q2 1 1.0197 0.5603 1.0628 11.00000 0.05 0.64 Q3 1 0.9069 0.5561 0.9575 11.00000 0.05 0.60 Q4 1 0.8244 0.1110 1.1163 11.00000 0.05 0.53 Q5 1 0.6494 0.3056 1.0871 11.00000 0.05 0.48 Q6 1 0.7894 0.2018 1.1389 11.00000 0.05 0.44 Q7 1 0.6461 0.9475 0.8928 11.00000 0.05 0.42 Q8 1 0.7089 0.1413 1.1309 11.00000 0.05 0.42 Q9 1 0.7108 0.2184 1.0802 11.00000 0.05 0.40 Q10 1 0.7787 0.3027 1.2068 11.00000 0.05 0.32 ; _shelx_res_checksum 66741 _shelx_hkl_file ; 0 0 -2 14406.4 327.708 5 0 0 -3 7351.29 201.523 5 0 0 -4 9178.06 256.797 5 0 0 5 80.4008 22.8973 4 0 0 -5 96.4853 25.5744 5 0 0 -6 162.936 37.4092 5 0 0 6 193.742 33.1207 4 0 0 7 4023.00 160.526 4 0 0 -7 4052.86 178.395 5 0 0 -8 1734.79 119.568 5 0 0 8 1911.32 112.854 4 0 0 9 2145.37 126.349 4 0 0 -9 2282.97 143.510 5 0 0 -10 70.3664 34.2709 5 0 0 10 37.9570 23.9526 4 0 0 11 713.349 75.7223 4 0 0 -11 470.576 73.7586 5 0 0 -12 778.115 97.9662 5 0 0 12 919.137 88.2515 4 0 0 -13 822.333 107.673 5 0 0 -14 1148.30 133.839 5 0 1 -14 1253.98 141.021 5 0 -1 13 2511.77 169.391 4 0 1 -13 2046.64 174.466 5 0 1 -12 1686.16 147.739 5 0 -1 12 1793.30 141.252 4 0 -1 11 5112.56 241.757 4 0 1 -11 4880.87 252.694 5 0 -1 10 584.104 74.8375 4 0 1 -10 473.648 72.3197 5 0 1 -9 157.845 38.0080 5 0 -1 9 141.246 38.4428 4 0 1 -8 3476.69 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195.677 1 8 0 3 4245.25 244.516 4 8 0 4 204.182 33.7785 1 8 0 4 129.760 44.5731 4 8 0 5 1170.07 75.5786 1 8 0 5 1117.35 127.352 4 8 0 6 70.2339 40.2815 4 8 0 7 72.6931 45.6774 4 8 0 8 1792.23 170.494 4 8 0 9 658.217 106.181 4 8 0 10 2055.48 194.410 4 8 0 11 194.818 66.6060 4 8 0 12 191.026 63.5723 4 8 0 13 26.8112 34.3023 4 8 1 -10 895.040 118.468 5 8 1 -9 32.2771 23.0762 5 8 1 -8 505.313 82.6347 5 8 1 -7 1629.19 142.096 5 8 1 -6 5690.18 265.268 4 8 1 -6 5550.53 266.301 5 8 1 -5 2207.85 157.178 4 8 1 -5 2379.93 158.338 5 8 1 -4 5247.78 256.777 4 8 1 -4 5191.93 239.463 5 8 1 -3 214.304 43.2425 5 8 1 -3 180.685 45.0707 4 8 1 -2 1032.51 109.903 4 8 1 -2 1019.18 91.2004 3 8 1 -2 1078.66 94.4901 5 8 1 -1 58.8883 21.8148 3 8 1 -1 39.1785 24.8046 5 8 1 -1-3.25891 22.2730 4 8 1 0 37.1396 19.1422 3 8 1 0 45.1561 24.7537 5 8 1 0 95.7813 40.6018 4 8 1 1 84.0255 26.5209 5 8 1 1 148.125 47.8428 4 8 1 1 137.501 24.9998 3 8 1 2 6109.67 229.805 5 8 1 2 5308.64 157.421 3 8 1 2 5431.62 270.147 4 8 1 3 2425.82 174.504 4 8 1 3 2347.56 133.752 1 8 1 4 3557.69 161.721 1 8 1 4 3564.91 222.154 4 8 1 5 302.193 39.3352 1 8 1 5 319.383 66.5665 4 8 1 6 68.7659 42.5420 4 8 1 7 141.491 49.1882 4 8 1 8 29.8403 26.7487 4 8 1 9 400.207 85.3925 4 8 1 10 1666.04 171.133 4 8 1 11 211.178 68.3267 4 8 1 12 81.1262 48.2890 4 8 1 13 276.948 81.8848 4 8 1 14 714.487 121.691 4 8 2 -10 2791.91 207.975 5 8 2 -9 1112.07 124.808 5 8 2 -8 1544.42 139.788 5 8 2 -7 1511.29 135.091 5 8 2 -6 302.412 56.7137 5 8 2 -5 307.723 56.9699 5 8 2 -5 261.388 50.2877 4 8 2 -4 9392.36 370.056 4 8 2 -4 9687.70 341.392 5 8 2 -3-3.07111 21.8606 5 8 2 -3-17.5785 27.3586 3 8 2 -3-6.30196 30.3322 4 8 2 -2 11747.8 425.061 4 8 2 -2 10650.3 366.539 3 8 2 -2 12047.0 366.411 5 8 2 -1 3697.60 215.072 4 8 2 -1 3638.19 174.547 3 8 2 -1 3726.31 168.262 5 8 2 0 672.267 66.3436 3 8 2 0 650.216 88.0603 4 8 2 0 553.532 59.5547 5 8 2 1 12.9339 16.4106 5 8 2 1 3.94265 28.1942 4 8 2 1 21.7924 12.9499 3 8 2 2 1057.97 78.5900 5 8 2 2 1104.76 70.7602 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987.183 72.8464 5 8 3 1 28.9654 13.4503 5 8 3 1-3.81112 31.3952 4 8 3 1 24.6387 15.8626 3 8 3 2 1746.38 92.7948 5 8 3 2 1792.92 105.154 3 8 3 2 1812.94 148.272 4 8 3 3 19.0617 12.4821 5 8 3 3 5.29816 12.4890 3 8 3 3 33.7995 31.2337 4 -8 -3 -4 23.9774 12.0563 3 8 3 4 18.8587 12.9399 5 8 3 4 46.7894 25.2688 1 8 3 4 51.9078 32.3036 4 8 3 5 4197.49 242.194 4 -8 -3 -5 4297.28 164.588 3 8 3 5 4002.39 157.170 5 8 3 6 3255.63 213.701 4 -8 -3 -6 3461.00 148.958 3 8 3 6 3424.34 144.852 5 8 3 7 13979.5 509.999 4 8 3 8 844.049 110.940 4 8 3 9 4.38922 27.0951 4 8 3 10 29.7964 35.2394 4 8 3 11 338.663 74.9738 4 8 3 12 23.9469 27.5227 4 8 3 13 597.025 104.590 4 8 4 -11 349.474 77.8026 5 8 4 -10 108.960 45.6931 5 8 4 -9 162.260 49.8065 5 8 4 -8 974.733 109.409 5 8 4 -7 27.9102 22.4965 5 8 4 -7 27.4792 26.0103 3 8 4 -6 740.969 107.760 3 8 4 -6 925.223 96.2423 5 8 4 -5 5.35795 18.0210 5 8 4 -5 51.1832 23.3414 3 8 4 -4 750.004 93.9212 3 8 4 -4 828.011 80.2659 5 8 4 -3 950.593 108.955 4 8 4 -3 718.000 89.9634 3 8 4 -3 751.652 72.9388 5 -8 -4 2 4119.18 181.666 5 8 4 -2 3999.74 232.064 4 8 4 -2 3843.87 206.606 3 8 4 -2 4027.37 170.072 5 8 4 -1 13777.1 482.262 4 8 4 -1 12604.6 432.768 3 8 4 -1 14108.5 374.388 5 8 4 0 14600.0 514.348 4 8 4 0 14900.1 463.872 3 8 4 0 15602.1 391.261 5 8 4 1 6944.06 314.482 4 8 4 1 6629.91 259.007 3 8 4 1 6686.11 198.564 5 8 4 2-4.92223 9.07951 5 8 4 2-13.8460 34.5685 4 8 4 2-0.07737 16.6691 3 8 4 3 4725.60 195.719 3 8 4 3 4682.69 250.585 4 -8 -4 -3 4504.44 193.610 3 8 4 3 4365.56 138.893 5 8 4 4 99.2912 17.0808 5 -8 -4 -4 89.3966 25.4480 3 8 4 4 113.884 30.9875 3 8 4 4 87.5717 16.7444 5 8 4 4 36.2068 28.6383 4 8 4 5 2373.51 175.585 4 -8 -4 -5 2232.19 127.205 3 8 4 5 2317.40 94.3503 5 8 4 6 1644.72 147.580 4 -8 -4 -6 1766.92 113.930 3 8 4 6 1562.31 80.5750 5 8 4 7 4753.20 258.034 4 -8 -4 -7 4340.92 195.459 3 8 4 8 6101.22 307.292 4 -8 -4 -9 537.698 60.6311 1 8 4 9 413.583 77.0566 4 8 4 10 563.446 94.3563 4 8 4 11 1739.40 164.571 4 8 4 12 117.630 45.0974 4 8 4 13 195.665 58.4899 4 8 5 -10 20.3213 27.8574 5 8 5 -9 229.954 58.9417 5 8 5 -9 269.936 71.7964 3 8 5 -8 718.866 114.480 3 8 5 -8 780.808 99.0540 5 8 5 -7 272.479 56.0375 5 8 5 -7 222.416 68.1447 3 8 5 -6 1599.48 154.447 3 8 5 -6 1695.25 132.190 5 8 5 -5 163.227 39.8229 5 8 5 -5 92.7703 39.4802 3 8 5 -4 382.627 71.4562 3 8 5 -4 500.249 62.1709 5 8 5 -3 324.440 45.5382 5 8 5 -3 218.307 56.6481 3 -8 -5 3 282.813 45.0863 5 8 5 -2-13.1880 24.3248 3 8 5 -2 9.31097 10.9103 5 -8 -5 2 21.7877 17.2444 5 8 5 -2-17.0102 27.3786 4 8 5 -1 536.229 78.3012 3 8 5 -1 573.902 85.7011 4 8 5 -1 491.036 45.3032 5 8 5 0 2839.62 194.475 4 8 5 0 2919.30 174.699 3 8 5 0 2883.75 108.339 5 8 5 1 2219.51 169.910 4 8 5 1 2292.77 147.512 3 8 5 1 2281.94 80.1419 5 8 5 2 3613.08 186.032 3 8 5 2 3704.30 223.947 4 8 5 3 5361.17 232.748 3 8 5 3 5754.22 284.809 4 8 5 4 5015.84 226.424 3 8 5 4 5085.78 271.441 4 -8 -5 -5 345.422 55.6788 1 8 5 5 380.137 74.1441 4 -8 -5 -6 571.883 71.7505 1 8 5 6 476.800 79.2843 4 -8 -5 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789.358 105.103 4 8 8 6 6217.90 314.297 4 -8 -8 -6 5642.55 297.189 1 -8 -8 -7 224.694 54.6345 1 8 8 7 150.385 52.3212 4 -8 -8 -8 41.8276 26.4681 1 8 8 8 46.7490 38.8456 4 -8 -8 -9-33.9286 32.0920 1 8 8 9-57.5202 47.7375 4 -8 -8 -10 328.846 66.7265 1 8 8 10 265.160 63.9117 4 -8 -8 -11 72.4759 36.2174 1 8 9 -6 1102.36 149.149 3 8 9 -5 560.018 103.233 3 8 9 -4 52.9228 38.0829 3 8 9 -3 3.40665 26.1838 3 8 9 -2 1515.97 156.156 3 8 9 -1 987.400 121.773 3 -8 -9 0 5095.95 288.745 1 8 9 0 4384.84 263.127 3 -8 -9 -1 866.165 117.357 1 8 9 1 671.849 98.3986 3 8 9 2 4416.24 265.547 3 -8 -9 -2 5219.70 293.601 1 8 9 3 1103.53 124.016 3 -8 -9 -3 1101.88 131.166 1 -8 -9 -4 43.0300 28.3022 1 8 9 4 69.2985 43.0502 3 -8 -9 -5 146.831 45.4158 1 -8 -9 -6 9.53037 25.3322 1 -8 -9 -7 194.344 59.1614 1 -8 -9 -8 2012.30 177.988 1 -8 -9 -9 219.844 61.4825 1 -8 -9 -10 205.078 60.5017 1 -8 -9 -11 60.9078 38.8453 1 8 10 -5 278.007 75.3308 3 8 10 -4 1957.03 196.891 3 8 10 -3 1059.60 140.134 3 8 10 -2 279.110 70.7922 3 8 10 -1 23.9693 26.3346 3 -8 -10 0 130.090 50.4788 1 8 10 0 110.633 38.4507 3 -8 -10 -1 5976.11 332.581 1 8 10 1 5314.27 307.225 3 8 10 2 2322.81 193.587 3 -8 -10 -2 2516.27 211.128 1 8 10 3 4119.55 264.661 3 -8 -10 -3 4724.47 289.895 1 8 10 4 1056.44 132.585 3 -8 -10 -4 1141.26 139.809 1 -8 -10 -5 290.644 72.5460 1 -8 -10 -6 35.5641 35.4962 1 -8 -10 -7 50.3438 32.1487 1 -8 -10 -8 1410.27 156.355 1 -8 -10 -9 909.807 122.555 1 -8 -10 -10 1714.82 172.389 1 -8 -10 -11 279.327 66.8201 1 8 11 -3 829.783 126.348 3 8 11 -2 273.641 68.1123 3 8 11 -1 24.3509 28.9232 3 -8 -11 0 15.7528 32.0398 1 8 11 0 9.72843 26.7124 3 -8 -11 -1 199.808 60.4251 1 8 11 1 214.409 66.8873 3 -8 -11 -2 889.819 129.899 1 8 11 2 639.552 106.463 3 -8 -11 -3 866.942 130.831 1 8 11 3 891.836 125.935 3 8 11 4 1704.49 177.411 3 -8 -11 -4 1940.11 193.238 1 -8 -11 -5 1665.18 178.914 1 -8 -11 -6 569.651 104.295 1 -8 -11 -7 50.9088 42.7254 1 -8 -11 -8 195.471 61.9712 1 -8 -11 -9 33.1830 23.3628 1 8 12 1 65.6525 32.5996 3 -8 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1767.90 186.797 4 9 -4 5 555.120 110.135 4 9 -4 6 288.415 81.1142 4 9 -3 -6 44.2224 30.6269 5 9 -3 -5 2273.73 183.711 5 9 -3 -4 949.318 107.072 4 9 -3 -4 901.261 113.801 5 9 -3 -3 473.812 84.5072 5 9 -3 -3 609.137 89.9397 4 9 -3 -2 1373.68 134.823 5 9 -3 -2 1229.16 130.415 4 9 -3 -1 1664.48 147.990 5 9 -3 -1 1620.29 153.854 4 9 -3 0 2037.41 161.441 5 9 -3 0 2240.69 184.386 4 9 -3 1 445.291 76.0509 5 9 -3 1 484.587 88.1316 4 9 -3 2 314.938 65.7319 5 9 -3 2 301.820 70.9074 4 9 -3 3 78.2635 39.2856 5 9 -3 3 200.585 64.6359 4 9 -3 4 456.437 91.0396 4 9 -3 5 71.6355 53.0237 4 9 -3 6 283.675 80.0820 4 9 -3 7 661.167 119.827 4 9 -2 -7 245.232 63.1853 5 9 -2 -6 1540.39 151.044 5 9 -2 -5 982.906 108.228 4 9 -2 -5 895.455 113.013 5 9 -2 -4 543.325 86.3285 5 9 -2 -4 715.967 94.1338 4 9 -2 -3 186.210 47.0976 5 9 -2 -3 230.948 56.8452 4 9 -2 -2 41.0823 28.0244 5 9 -2 -2 97.7379 38.0715 4 9 -2 -1 1099.30 114.213 5 9 -2 -1 1340.09 134.509 4 9 -2 0 6154.25 286.169 5 9 -2 0 6173.16 316.726 4 9 -2 1 2439.27 170.037 5 9 -2 1 2549.29 197.046 4 9 -2 2 2482.83 173.138 5 9 -2 2 2523.75 197.954 4 9 -2 3 78.3723 35.7816 5 9 -2 3 83.8776 42.5343 4 9 -2 4 69.0535 38.0315 4 9 -2 5 341.844 81.6378 4 9 -2 6 573.780 106.872 4 9 -2 7 876.096 131.783 4 9 -2 8 436.006 96.3482 4 9 -2 9 385.292 93.4012 4 9 -1 -8 183.651 55.4193 5 9 -1 -7 197.966 57.8278 5 9 -1 -6 1633.46 136.874 4 9 -1 -6 1885.40 160.661 5 9 -1 -5 301.209 63.4083 5 9 -1 -5 355.449 69.3526 4 9 -1 -4 96.8349 42.1227 5 9 -1 -4 53.0145 33.8104 4 9 -1 -3 241.744 55.0720 5 9 -1 -3 240.999 58.3229 4 9 -1 -2 216.910 51.1248 5 9 -1 -2 212.513 54.0765 4 9 -1 -1 1291.70 118.902 5 9 -1 -1 1356.45 136.326 4 9 -1 0 238.063 50.3497 5 9 -1 0 213.055 56.7083 4 9 -1 1 5086.95 245.662 5 9 -1 1 5695.61 295.704 4 9 -1 2 1171.02 111.857 5 9 -1 2 1185.83 130.375 4 9 -1 3 3492.02 197.472 5 9 -1 3 4072.94 255.906 4 9 -1 4 2833.86 216.656 4 9 -1 5 1052.56 134.484 4 9 -1 6 294.756 72.4885 4 9 -1 7 118.277 50.5601 4 9 -1 8 1151.42 151.675 4 9 -1 9 2387.48 220.189 4 9 -1 10 236.357 81.0684 4 9 0 -9 368.796 79.0051 5 9 0 -8 11.0161 21.3390 5 9 0 -7 155.508 48.4120 5 9 0 -6 1000.93 107.773 4 9 0 -6 996.691 114.534 5 9 0 -5 662.211 90.2742 4 9 0 -5 847.824 101.028 5 9 0 -4 145.632 41.6198 5 9 0 -4 241.220 60.7251 4 9 0 -3 1191.51 122.912 4 9 0 -3 1044.25 104.547 5 9 0 -2 422.429 66.0147 5 9 0 -2 559.261 66.8744 3 9 0 -2 499.507 83.1970 4 9 0 -1 999.160 114.738 4 9 0 -1 990.131 77.9269 3 9 0 -1 926.489 94.9315 5 9 0 0 209.809 31.9722 3 9 0 0 122.868 36.7858 5 9 0 0 335.774 74.2193 4 9 0 1 507.434 68.8107 5 9 0 1 575.031 90.2060 4 9 0 2 2324.13 150.543 5 9 0 2 2609.46 193.297 4 9 0 3 7942.45 307.356 5 9 0 3 8318.18 376.824 4 9 0 4 478.298 87.0105 4 9 0 5 3112.00 227.109 4 9 0 6 338.657 80.4752 4 9 0 7 1270.52 148.720 4 9 0 8 2364.18 208.313 4 9 0 9 577.195 107.652 4 9 0 10 1641.95 181.080 4 9 0 11 175.457 59.9395 4 9 1 -9 1926.33 175.226 5 9 1 -8 1863.14 164.592 5 9 1 -7 70.7641 35.2839 5 9 1 -6 1264.81 123.905 4 9 1 -6 1176.90 119.059 5 9 1 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188.632 3 9 2 -4 3108.43 180.673 5 9 2 -3 198.171 42.7566 5 9 2 -3 274.658 53.9570 3 9 2 -3 137.678 48.9333 4 9 2 -2 4433.19 253.783 4 9 2 -2 4630.38 217.296 3 9 2 -2 4612.31 209.638 5 9 2 -1 4734.82 263.330 4 9 2 -1 4919.31 215.539 3 9 2 -1 4914.53 210.910 5 9 2 0 7274.15 343.454 4 9 2 0 8350.43 283.022 3 9 2 0 7714.57 275.812 5 9 2 1 364.167 51.4630 5 9 2 1 445.724 50.8489 3 9 2 1 328.364 64.1531 4 9 2 2 240.385 41.1074 5 9 2 2 256.548 33.3858 3 9 2 2 280.538 62.5243 4 9 2 3 53.4468 20.1426 5 9 2 3 20.8989 25.7783 4 9 2 4 3446.81 163.068 5 9 2 4 3134.46 219.306 4 9 2 5 87.7757 40.6462 4 9 2 6-36.2950 44.3851 4 9 2 7 984.107 132.107 4 9 2 8 1424.60 153.642 4 9 2 9 260.969 67.5311 4 9 2 10-22.4662 38.3543 4 9 2 11 375.401 88.2742 4 9 2 12 2111.89 205.027 4 9 2 13 1453.23 173.815 4 9 3 -10 325.333 73.0416 5 9 3 -9 109.317 45.0265 5 9 3 -8 5058.32 272.226 5 9 3 -7 1780.69 150.530 5 9 3 -6 2489.94 194.450 3 9 3 -6 2798.72 180.745 5 9 3 -5 151.392 39.2815 5 9 3 -5 136.684 46.0139 3 9 3 -4 36.7022 23.0510 5 9 3 -4 63.6226 34.2766 3 9 3 -4-9.48604 38.9766 4 9 3 -3 2403.15 183.390 4 9 3 -3 2467.18 166.419 3 9 3 -3 2623.61 149.247 5 9 3 -2 1648.51 149.399 4 9 3 -2 1276.46 113.350 3 9 3 -2 1466.16 105.716 5 9 3 -1 7232.72 337.174 4 9 3 -1 7413.30 292.080 3 9 3 -1 7475.36 261.946 5 9 3 0 11069.6 440.192 4 9 3 0 11227.9 370.864 3 9 3 0 11298.8 339.840 5 9 3 1 7397.96 341.600 4 9 3 1 7607.13 269.228 3 9 3 1 7033.65 240.613 5 9 3 2 2045.63 116.370 3 9 3 2 1923.50 163.573 4 9 3 2 2096.33 110.219 5 9 3 3 151.222 29.7985 5 9 3 3 183.266 33.2619 3 9 3 3 157.912 55.7536 4 9 3 4 208.433 35.7023 5 9 3 4 241.848 69.4959 4 9 3 5 234.262 60.1958 4 9 3 6 45.7576 25.3166 4 9 3 7 1151.55 133.174 4 9 3 8 408.861 80.8859 4 9 3 9 346.251 78.4056 4 9 3 10 116.783 51.0586 4 9 3 11 81.3407 44.0490 4 9 3 12 494.729 95.8591 4 9 3 13 249.615 71.3506 4 9 4 -10 214.009 59.8305 5 9 4 -9 99.2547 42.4356 5 9 4 -9 80.7929 47.6107 3 9 4 -8 352.528 69.6130 5 9 4 -8 350.140 79.4423 3 9 4 -7 1002.60 129.829 3 9 4 -7 906.614 101.670 5 9 4 -6 440.518 66.9842 5 9 4 -6 425.118 81.9142 3 9 4 -5 3597.18 229.485 3 9 4 -5 4239.53 209.903 5 9 4 -4 2724.28 189.012 3 9 4 -4 2782.13 160.367 5 9 4 -3 282.796 47.5521 5 9 4 -3 259.005 53.4153 3 9 4 -3 294.335 68.0230 4 9 4 -2 3919.53 242.972 4 9 4 -2 3704.99 211.658 3 9 4 -2 4250.59 181.404 5 9 4 -1 134.980 39.8121 3 9 4 -1 181.701 32.3379 5 9 4 -1 63.9835 37.4459 4 9 4 0 89.1229 30.8832 3 9 4 0 89.2082 23.0861 5 9 4 0-19.5013 41.7477 4 9 4 1 2674.66 197.085 4 9 4 1 2829.70 160.744 3 9 4 1 2840.51 121.810 5 9 4 2 6418.36 252.458 3 9 4 2 6592.09 325.924 4 9 4 2 6652.16 203.666 5 9 4 3 3370.56 165.738 3 9 4 3 3528.42 228.873 4 9 4 3 3473.45 128.183 5 9 4 4 1571.63 79.6347 5 9 4 4 1546.53 150.690 4 9 4 5 4034.63 149.009 5 9 4 5 4280.42 255.403 4 9 4 6 1589.66 154.946 4 9 4 7 3305.74 226.126 4 9 4 8 48.1614 34.4629 4 9 4 9 773.624 111.464 4 9 4 10 451.169 87.0335 4 9 4 11 1590.50 166.330 4 9 4 12 171.875 52.3507 4 9 4 13 151.852 56.3707 4 9 5 -10 455.212 84.5764 5 9 5 -9 45.7095 26.9855 5 9 5 -8 65.9207 30.2458 5 9 5 -8 36.6848 44.2147 3 9 5 -7 130.502 41.6315 5 9 5 -7 52.7732 34.3764 3 9 5 -6 1108.42 132.893 3 9 5 -6 1572.88 128.320 5 9 5 -5 171.530 41.0918 5 9 5 -5 194.875 58.1179 3 9 5 -4 2076.01 170.795 3 9 5 -4 2195.74 135.923 5 9 5 -3 296.544 64.5417 3 9 5 -3 380.406 52.0659 5 9 5 -2 873.942 112.714 4 9 5 -2 720.632 94.9802 3 9 5 -2 985.461 76.8775 5 9 5 -1 1397.15 142.562 4 9 5 -1 1447.47 127.199 3 9 5 -1 1469.57 87.7125 5 9 5 0 428.136 80.0839 4 9 5 0 472.605 44.0640 5 9 5 0 434.879 67.3892 3 9 5 1 6336.82 319.022 4 9 5 1 6071.87 265.427 3 9 5 1 6224.48 180.922 5 9 5 2 2204.45 143.560 3 9 5 2 2154.43 175.894 4 9 5 2 2007.21 75.0038 5 9 5 3 817.452 82.7642 3 9 5 3 844.003 108.913 4 9 5 3 644.004 31.2447 5 9 5 4 1727.69 125.841 3 9 5 4 1494.58 151.252 4 9 5 5 1573.59 155.576 4 9 5 6 376.717 74.8863 4 9 5 7 924.431 119.931 4 9 5 8 451.493 83.8221 4 9 5 9 61.9246 38.9687 4 9 5 10 2075.95 184.593 4 9 5 11 4860.42 294.497 4 9 5 12 231.699 65.2386 4 9 6 -10 2264.20 192.697 5 9 6 -9 2175.68 177.510 5 9 6 -8 114.693 43.8073 5 9 6 -8 53.0644 36.6143 3 9 6 -7 12.4752 18.3339 5 9 6 -7-20.9621 29.3961 3 9 6 -6 994.181 133.868 3 9 6 -6 922.937 96.9119 5 9 6 -5 204.038 42.8737 5 9 6 -5 52.3401 35.2382 3 9 6 -4 461.882 82.6952 3 9 6 -4 491.796 62.3596 5 9 6 -3 4.71116 32.4059 3 9 6 -3 38.8658 20.5038 5 9 6 -2 5278.59 281.298 3 9 6 -2 5637.44 200.686 5 9 6 -1 483.720 77.7015 3 9 6 -1 647.054 99.5385 4 9 6 -1 572.769 48.2432 5 9 6 0 1560.62 152.004 4 9 6 0 1483.60 132.690 3 9 6 0 1422.62 65.9473 5 9 6 1 1221.87 136.865 4 9 6 1 1094.47 111.528 3 9 6 2 36.0695 35.1516 4 9 6 2-33.0761 27.1810 3 9 6 3 3748.91 205.500 3 9 6 3 4162.05 254.226 4 9 6 4 7381.02 306.731 3 9 6 4 7470.77 357.506 4 9 6 5 13250.2 507.625 4 -9 -6 -6 1080.28 109.275 1 9 6 6 912.386 118.714 4 -9 -6 -7 2763.25 178.671 1 9 6 7 2737.26 208.548 4 -9 -6 -8 936.764 99.8950 1 9 6 8 931.658 122.398 4 -9 -6 -9 1697.87 135.416 1 9 6 9 1719.37 167.203 4 9 6 10 321.032 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50.9092 3 9 8 3 223.258 65.4806 4 9 8 3 332.452 68.6660 3 -9 -8 -3 321.919 72.6955 1 9 8 4 182.204 58.9295 4 9 8 4 116.557 40.1617 3 -9 -8 -4 107.321 47.1932 1 9 8 5 1486.03 157.024 4 -9 -8 -5 1683.06 155.163 1 -9 -8 -6 78.3535 35.9182 1 9 8 6 101.061 45.1875 4 -9 -8 -7 554.578 87.3310 1 9 8 7 484.622 89.4376 4 9 8 8 2814.14 216.197 4 -9 -8 -8 2816.03 203.402 1 9 8 9 5644.73 315.798 4 -9 -8 -9 5175.37 282.462 1 9 8 10 1206.25 137.921 4 -9 -8 -10 1152.37 127.103 1 9 9 -5 4057.30 289.230 3 9 9 -4 3392.33 255.988 3 9 9 -3 2895.76 232.047 3 9 9 -2 247.639 70.9779 3 9 9 -1 124.724 47.9023 3 9 9 0 79.6875 36.8989 3 9 9 1 412.348 81.6492 3 -9 -9 -2 5079.65 295.059 1 9 9 2 4597.26 274.724 3 -9 -9 -3 1911.58 175.938 1 9 9 3 1497.35 150.888 3 9 9 4-7.42812 25.4942 3 -9 -9 -4 55.4942 36.4318 1 -9 -9 -5 29.3208 36.7892 1 -9 -9 -6 554.631 91.9568 1 -9 -9 -7 318.542 70.1432 1 9 9 8 56.5037 32.8274 4 -9 -9 -8 6.18928 30.4986 1 9 9 9 781.022 112.568 4 -9 -9 -9 843.931 114.867 1 9 9 10 341.277 76.9462 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10 -1 7 22.8459 45.5615 4 10 -1 8 271.308 76.1822 4 10 0 -7 67.1381 36.3223 5 10 0 -6-2.51169 32.4660 5 10 0 -5 15.6030 23.4499 5 10 0 -5 47.9534 29.8033 4 10 0 -4 6.55454 24.3530 5 10 0 -4 64.7297 37.1356 4 10 0 -3 1819.50 163.584 4 10 0 -3 1859.59 149.161 5 10 0 -2 41.6421 25.9179 5 10 0 -2 18.7242 29.1187 4 10 0 -1 7256.69 350.272 4 10 0 -1 7322.70 309.803 5 10 0 0 3412.51 197.218 5 10 0 0 3545.70 235.944 4 10 0 1 58.6563 29.8434 5 10 0 1 78.1994 35.3734 4 10 0 2 324.983 58.6485 5 10 0 2 290.499 73.6789 4 10 0 3 3.57044 28.3666 5 10 0 3 17.2195 32.5422 4 10 0 4 1688.74 134.378 5 10 0 4 1955.66 182.232 4 10 0 5 831.472 122.602 4 10 0 6 841.863 126.096 4 10 0 7 779.954 124.325 4 10 0 8 635.330 116.560 4 10 0 9 51.4860 48.8654 4 10 1 -8 268.146 66.2021 5 10 1 -7 1773.72 159.957 5 10 1 -6 360.200 69.6450 5 10 1 -6 463.201 76.0471 4 10 1 -5 64.6736 33.5527 5 10 1 -5 70.2059 41.3324 4 10 1 -4 69.8642 29.7815 5 10 1 -4 68.3418 33.5398 3 10 1 -4 29.1115 23.6145 4 10 1 -3 159.916 42.4776 5 10 1 -3 201.651 48.0344 3 10 1 -3 189.101 59.3772 4 10 1 -2 1000.79 122.162 4 10 1 -2 1246.13 103.442 3 10 1 -2 1028.68 102.344 5 10 1 -1 3512.87 232.155 4 10 1 -1 3222.35 183.567 5 10 1 0 699.756 102.619 4 10 1 0 760.030 83.9837 5 10 1 1 1436.80 115.640 5 10 1 1 1419.64 146.449 4 10 1 2 53.0719 25.5742 5 10 1 2 40.6508 37.0629 4 10 1 3 2256.34 146.963 5 10 1 3 2550.64 204.848 4 10 1 4 580.346 73.8238 5 10 1 4 497.666 97.7798 4 10 1 5 255.082 77.0456 4 10 1 6 790.698 120.466 4 10 1 7 1364.58 159.596 4 10 1 8 3240.75 254.100 4 10 1 9 257.587 75.3944 4 10 1 10-33.9104 55.5142 4 10 2 -8 1914.23 170.013 5 10 2 -7 4343.85 254.091 5 10 2 -6 1875.21 167.548 3 10 2 -6 1809.42 152.907 5 10 2 -5 664.531 86.8289 5 10 2 -5 430.919 78.9964 3 10 2 -5 728.539 100.863 4 10 2 -4 95.6276 37.5435 5 10 2 -4 91.1063 38.0798 3 10 2 -4 155.071 52.2107 4 10 2 -3 235.001 49.1635 5 10 2 -3 312.947 56.1275 3 10 2 -3 417.718 81.7505 4 10 2 -2 963.697 120.186 4 10 2 -2 986.201 95.7377 3 10 2 -2 903.880 90.7872 5 10 2 -1 1184.54 132.632 4 10 2 -1 1206.65 102.241 3 10 2 -1 1093.84 98.2409 5 10 2 0 1451.47 149.114 4 10 2 0 1395.15 100.812 3 10 2 0 1310.08 103.920 5 10 2 1 447.662 60.0356 5 10 2 1 516.371 53.6299 3 10 2 1 400.561 81.0762 4 10 2 2 2223.76 133.990 5 10 2 2 2247.60 187.529 4 10 2 3 110.788 29.7232 5 10 2 3 139.883 51.0744 4 10 2 4 496.368 61.8646 5 10 2 4 457.066 83.5421 4 10 2 5 27.0928 19.4824 5 10 2 5 47.7252 39.6187 4 10 2 6 1107.68 138.789 4 10 2 7 71.3915 42.5123 4 10 2 8 7032.49 378.993 4 10 2 9 548.378 106.082 4 10 2 10 220.882 69.2439 4 10 2 11 256.971 77.4763 4 10 3 -9 375.821 76.4791 5 10 3 -8-7.61127 23.3222 5 10 3 -8-43.4239 37.2364 3 10 3 -7 283.934 61.7669 5 10 3 -7 307.944 72.6040 3 10 3 -6 45.2200 26.2876 5 10 3 -6 27.7272 25.1424 3 10 3 -5 1268.89 132.159 3 10 3 -5 1510.16 128.280 5 10 3 -4 2717.53 205.140 4 10 3 -4 2240.81 170.290 3 10 3 -4 2469.85 159.608 5 10 3 -3 4312.06 263.028 4 10 3 -3 3935.84 223.456 3 10 3 -3 4266.92 208.033 5 10 3 -2 1.39311 20.6308 3 10 3 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59.5090 36.8372 4 10 4 -3 447.813 76.0759 3 10 4 -3 439.631 60.6588 5 10 4 -3 401.090 79.0229 4 10 4 -2-0.90809 21.2096 3 10 4 -2 22.5947 20.5548 5 10 4 -2 13.4532 24.0744 4 10 4 -1 560.959 78.4938 3 10 4 -1 582.548 98.0290 4 10 4 -1 580.075 62.9434 5 10 4 0 246.249 64.7838 4 10 4 0 370.625 48.0234 5 10 4 0 326.278 54.8257 3 10 4 1 1359.19 145.825 4 10 4 1 1579.44 117.730 3 10 4 1 1364.66 87.4809 5 10 4 2 1056.02 93.2204 3 10 4 2 941.934 123.433 4 10 4 2 930.419 67.7002 5 10 4 3 1152.21 92.3315 3 10 4 3 1038.74 127.102 4 10 4 3 1034.99 69.1414 5 10 4 4 4053.46 260.777 4 10 4 5 4241.25 269.316 4 10 4 6 879.484 122.174 4 10 4 7 0.18576 35.2883 4 10 4 8 64.3738 37.4317 4 10 4 9 103.077 56.9551 4 10 4 10 144.627 56.5379 4 10 4 11 1718.75 183.314 4 10 4 12 404.671 93.2538 4 10 5 -9 1574.03 152.834 5 10 5 -8 2086.25 201.661 3 10 5 -8 2083.74 169.681 5 10 5 -7 524.034 77.9128 5 10 5 -7 473.176 93.5800 3 10 5 -6 1738.29 172.309 3 10 5 -6 2037.36 149.885 5 10 5 -5 151.877 43.3938 5 10 5 -5 51.6865 29.4917 3 10 5 -4 496.202 83.3293 3 10 5 -4 636.447 73.7323 5 10 5 -3 434.938 76.7795 3 10 5 -3 416.780 58.0044 5 10 5 -2 5336.81 307.547 4 10 5 -2 5391.12 280.078 3 10 5 -2 5479.27 212.787 5 10 5 -1 5028.47 294.781 4 10 5 -1 4248.29 238.654 3 10 5 -1 4852.92 186.510 5 10 5 0 94.2441 43.9844 4 10 5 0 30.8102 20.8819 3 10 5 1 1198.80 141.063 4 10 5 1 980.734 100.471 3 10 5 2 4187.44 213.039 3 10 5 2 4203.53 269.629 4 10 5 3 164.763 62.5090 4 10 5 3 191.807 41.6767 3 10 5 4 3451.06 187.325 3 10 5 4 3652.11 249.202 4 10 5 5 3261.72 235.398 4 10 5 6 4772.19 294.550 4 10 5 7 5753.72 327.168 4 10 5 8 471.771 92.1760 4 10 5 9 76.7990 44.9151 4 10 5 10 29.1913 30.1387 4 10 5 11 5.31305 30.2993 4 10 5 12 805.236 123.145 4 10 6 -7 1341.20 157.938 3 10 6 -6 101.879 46.6916 3 10 6 -5 1419.76 156.579 3 10 6 -4 52.4800 40.5851 3 10 6 -3 1068.71 126.444 3 10 6 -2 2464.45 188.394 3 10 6 -1 4723.50 288.026 4 10 6 -1 3972.93 238.909 3 10 6 0 3677.05 252.296 4 10 6 0 3101.29 202.258 3 10 6 1 1243.12 142.676 4 10 6 1 1020.22 107.897 3 10 6 2 256.900 61.4836 4 10 6 2 336.987 61.8074 3 10 6 3-30.0298 38.8002 4 10 6 3-8.28906 23.2252 3 10 6 4 48.8110 32.9267 3 10 6 4-1.27840 33.6189 4 10 6 5 26.6870 39.2558 4 10 6 6 188.342 58.6318 4 10 6 7 8773.32 416.548 4 10 6 8 1011.55 131.267 4 10 6 9 665.622 110.452 4 10 6 10 1084.24 141.339 4 10 6 11 627.120 110.322 4 10 6 12 44.9832 49.4826 4 10 7 -6 171.674 65.5317 3 10 7 -5-16.3456 39.1067 3 10 7 -4 373.426 84.0530 3 10 7 -3 553.833 97.0339 3 10 7 -2 47.0405 29.0891 3 10 7 -1 3062.67 213.801 3 10 7 0 616.265 90.6578 3 10 7 1 3256.52 240.088 4 10 7 1 2833.67 196.107 3 10 7 2 2443.75 209.112 4 10 7 2 1917.49 159.074 3 10 7 3 981.330 110.515 3 10 7 3 1061.31 133.684 4 10 7 4 1342.70 130.008 3 10 7 4 1248.65 147.141 4 10 7 5 782.012 119.175 4 10 7 6 44.8608 29.0128 4 10 7 7 222.878 66.0238 4 -10 -7 -8 698.463 91.2860 1 10 7 8 707.853 110.400 4 10 7 9 2919.54 229.308 4 10 7 10 1205.78 146.715 4 10 7 11 50.7099 42.1618 4 10 8 -5 3028.24 247.287 3 10 8 -4 484.473 91.6008 3 10 8 -3 563.654 98.4824 3 10 8 -2 316.580 75.2594 3 10 8 -1 727.260 105.688 3 10 8 0 37.5263 33.8369 3 10 8 1 360.319 74.8327 3 10 8 2 1765.26 160.203 3 10 8 3 3159.20 216.858 3 10 8 3 3969.77 274.093 4 10 8 4 816.222 108.155 3 10 8 4 1174.41 147.766 4 10 8 5 77.0425 49.6059 4 -10 -8 -6 126.786 46.6674 1 10 8 6 153.353 55.3747 4 -10 -8 -7-11.0505 21.9582 1 10 8 7 36.3484 36.4548 4 -10 -8 -8 70.4796 29.6005 1 10 8 8 93.2028 44.2648 4 -10 -8 -9 467.637 81.2485 1 10 8 9 580.246 104.720 4 10 8 10 1471.89 163.073 4 10 8 11 1437.69 160.058 4 10 9 -4-9.27701 33.8624 3 10 9 -3 1869.68 188.496 3 10 9 -2 949.133 130.450 3 10 9 -1 1263.79 144.407 3 10 9 0 169.917 55.9050 3 10 9 1 189.333 58.7745 3 10 9 2 564.856 95.4507 3 10 9 3 231.862 62.1367 3 10 9 4 1787.25 171.203 3 -10 -9 -4 2345.15 197.718 1 -10 -9 -5 1640.58 165.429 1 -10 -9 -6 926.529 123.366 1 10 9 6 925.249 134.806 4 -10 -9 -7 2.76204 29.2752 1 10 9 7 17.5022 39.5564 4 10 9 8 758.238 112.548 4 -10 -9 -8 734.670 109.949 1 -10 -9 -9 20.5697 33.0704 1 10 9 9-53.8382 37.4173 4 10 9 10 180.209 67.0609 4 10 10 -2 1173.63 147.289 3 10 10 -1 746.908 118.292 3 10 10 0 804.374 120.365 3 10 10 1-54.3870 35.5534 3 10 10 2 47.0351 37.3653 3 10 10 3-37.2142 41.7081 3 -10 -10 -4 932.867 132.978 1 10 10 4 772.299 120.451 3 -10 -10 -5 24.0463 32.4406 1 -10 -10 -6 2146.48 200.619 1 -10 -10 -7 1113.69 141.710 1 -10 -10 -8 29.9235 39.1375 1 -10 -10 -9 111.508 44.8710 1 10 11 0 148.518 56.7436 3 10 11 1 649.237 113.968 3 10 11 2-57.5752 46.6889 3 -10 -11 -3 585.264 111.514 1 10 11 3 549.820 103.464 3 10 11 4 89.4439 45.3865 3 -10 -11 -4 142.507 61.3766 1 -10 -11 -5 109.516 51.9241 1 -10 -11 -6 102.219 44.7843 1 11 -3 -2 213.214 62.2304 4 11 -3 -1 26.0241 27.3541 4 11 -3 0 52.7117 39.0536 5 11 -3 0 10.8853 42.1704 4 11 -3 1 540.673 89.7855 5 11 -3 1 533.133 100.904 4 11 -3 2 1379.24 143.438 5 11 -3 2 1477.35 174.933 4 11 -3 3 1447.60 149.024 5 11 -3 4 234.927 62.2536 5 11 -2 -3 91.0665 44.6529 5 11 -2 -3 33.8012 27.4008 4 11 -2 -2 106.214 40.1449 5 11 -2 -2 85.4955 51.3035 4 11 -2 -1 181.262 51.0363 5 11 -2 -1 103.516 45.0837 4 11 -2 0 271.847 65.2718 5 11 -2 0 171.426 59.9985 4 11 -2 1 169.304 50.3636 5 11 -2 1 231.710 66.6866 4 11 -2 2 316.076 69.1745 5 11 -2 2 289.720 75.3214 4 11 -2 3 240.167 58.7694 5 11 -2 3 467.568 93.2836 4 11 -2 4 1153.69 127.843 5 11 -2 5 474.467 82.6125 5 11 -1 -5 724.445 106.741 5 11 -1 -4 42.1513 25.7364 5 11 -1 -4 45.6125 35.7119 4 11 -1 -3 33.4260 30.8394 5 11 -1 -3 18.3398 28.1163 4 11 -1 -2 2277.98 195.628 4 11 -1 -2 2256.42 175.758 5 11 -1 -1 29.5244 28.5244 5 11 -1 -1 141.117 51.3316 4 11 -1 0 1929.32 158.844 5 11 -1 0 1888.34 182.025 4 11 -1 1 52.4112 37.2037 5 11 -1 1-21.3761 27.4785 4 11 -1 2 249.128 56.9247 5 11 -1 2 207.676 64.1384 4 11 -1 3 24.8422 29.3683 5 11 -1 3 105.623 57.7657 4 11 -1 4 731.769 96.7881 5 11 -1 4 939.272 136.544 4 11 -1 5 203.943 50.0462 5 11 -1 5 287.432 85.8540 4 11 0 -6 903.498 117.320 5 11 0 -5 806.219 108.002 5 11 0 -4 653.926 95.9772 5 11 0 -4 685.751 105.044 4 11 0 -3 1835.21 174.808 4 11 0 -3 1925.17 159.355 5 11 0 -2 280.574 61.5478 5 11 0 -2 175.817 55.5270 4 11 0 -1 229.354 51.7037 5 11 0 -1 147.588 53.9136 4 11 0 0 1047.50 132.180 4 11 0 0 920.840 103.500 5 11 0 1 471.393 74.9088 5 11 0 1 493.700 92.2460 4 11 0 2 107.231 38.3285 5 11 0 2 199.539 66.5086 4 11 0 3 50.0353 31.2541 5 11 0 3-33.5360 42.8826 4 11 0 4 306.079 60.4998 5 11 0 4 518.046 100.226 4 11 0 5 7.96063 20.8487 5 11 0 5-54.0447 38.7384 4 11 0 6 366.366 92.3842 4 11 1 -7 1025.32 123.647 5 11 1 -6 353.123 71.1413 5 11 1 -5 159.419 48.4141 5 11 1 -5 133.242 47.8333 4 11 1 -4 1725.91 166.299 4 11 1 -4 1821.12 153.056 5 11 1 -3 46.3427 32.2009 5 11 1 -3-23.6784 35.9290 4 11 1 -2 216.110 55.2333 5 11 1 -2 181.340 57.9176 4 11 1 -1 54.8046 32.3389 5 11 1 -1 0.37326 31.4679 4 11 1 0 2500.95 207.026 4 11 1 0 2485.79 164.557 5 11 1 1 3965.58 266.492 4 11 1 1 3942.47 209.833 5 11 1 2 673.883 81.0853 5 11 1 2 643.250 109.369 4 11 1 3 711.736 83.8382 5 11 1 3 675.409 113.262 4 11 1 4 100.774 32.9269 5 11 1 4 80.2261 41.1985 4 11 1 5 180.318 44.6391 5 11 1 5 223.568 73.0480 4 11 1 6 136.397 60.3692 4 11 1 7 99.0430 45.8465 4 11 2 -7-19.1803 25.8565 5 11 2 -7 22.4884 21.5045 3 11 2 -6 122.597 46.6815 5 11 2 -6 59.5337 33.8023 3 11 2 -5 1039.03 127.340 4 11 2 -5 962.431 115.048 3 11 2 -5 729.000 95.7016 5 11 2 -4 1189.77 137.629 4 11 2 -4 1105.96 115.528 5 11 2 -3 923.272 122.822 4 11 2 -3 950.765 100.952 5 11 2 -2 454.025 68.8350 5 11 2 -2 370.092 82.5540 4 11 2 -1 995.388 133.076 4 11 2 -1 1064.14 101.820 5 11 2 0 3.69411 16.8622 5 11 2 0 32.9923 35.0566 4 11 2 1 100.579 28.3349 5 11 2 1 183.083 59.1843 4 11 2 2 3031.10 230.098 4 11 2 2 2711.33 157.833 5 11 2 3 796.040 80.7448 5 11 2 3 635.434 106.065 4 11 2 4 1352.19 107.611 5 11 2 4 1481.78 163.647 4 11 2 5 1110.79 143.216 4 11 2 6 417.021 92.7967 4 11 2 7 37.0986 46.8084 4 11 2 8 707.335 123.452 4 11 3 -8 206.492 56.5082 5 11 3 -7 704.134 108.260 3 11 3 -7 753.700 102.011 5 11 3 -6 649.421 92.3798 5 11 3 -6 558.707 93.3719 3 11 3 -5 919.282 116.085 3 11 3 -5 1002.16 108.888 5 11 3 -4 1028.39 128.744 4 11 3 -4 788.418 103.191 3 11 3 -4 893.838 96.8112 5 11 3 -3 164.593 47.1144 3 11 3 -3 166.146 42.5281 5 11 3 -3 102.999 49.6861 4 11 3 -2 143.042 38.9000 3 11 3 -2 218.262 46.5641 5 11 3 -2 261.938 65.2144 4 11 3 -1 1404.35 153.414 4 11 3 -1 1497.57 113.479 5 11 3 0 145.302 35.8911 5 11 3 0 11.3876 30.2892 4 11 3 1 108.400 28.9455 5 11 3 1 46.3376 39.1621 4 11 3 2 74.6726 46.5908 4 11 3 3 622.014 106.237 4 11 3 4 264.509 71.3811 4 11 3 5 1959.24 188.454 4 11 3 6 1599.53 171.993 4 11 3 7 175.661 66.1656 4 11 3 8 762.747 123.641 4 11 3 9 127.468 60.5770 4 11 4 -7-27.0431 37.1936 3 11 4 -6 90.2038 42.0995 3 11 4 -5 439.717 70.0980 5 11 4 -5 281.038 67.2259 3 11 4 -4-15.1777 26.1565 3 11 4 -4-23.3658 37.8440 4 11 4 -3 518.828 83.3688 3 11 4 -3 472.762 90.1841 4 11 4 -2 2276.56 200.491 4 11 4 -2 2216.75 170.069 3 11 4 -1 6889.55 362.342 4 11 4 -1 6519.91 294.098 3 11 4 0 1950.81 186.830 4 11 4 0 1801.43 137.227 3 11 4 1 47.0906 42.0424 4 11 4 2 14.7497 27.6212 4 11 4 3 1523.30 163.423 4 11 4 4 228.389 66.2969 4 11 4 5 540.386 99.5239 4 11 4 6 2619.55 223.157 4 11 4 7 329.056 82.1403 4 11 4 8 3735.01 271.590 4 11 4 9 440.283 94.0727 4 11 4 10-18.8870 46.5521 4 11 5 -7 2043.07 195.577 3 11 5 -6 369.015 79.5773 3 11 5 -5 86.6680 42.8110 3 11 5 -4 356.831 75.4527 3 11 5 -3 1156.75 148.820 4 11 5 -3 1085.33 125.189 3 11 5 -2-4.54965 20.1987 3 11 5 -2-37.5880 46.8939 4 11 5 -1 309.962 73.3191 4 11 5 -1 232.976 56.4278 3 11 5 0 3794.19 265.539 4 11 5 0 4018.92 223.972 3 11 5 1 2999.65 235.043 4 11 5 1 2835.25 177.825 3 11 5 2-21.5251 44.3027 4 11 5 2-11.0007 23.0413 3 11 5 3 924.793 129.448 4 11 5 4 5.21087 29.6286 4 11 5 5 1126.73 143.152 4 11 5 6 21.7811 29.9722 4 11 5 7 69.4977 44.4111 4 11 5 8 1661.97 180.070 4 11 5 9 174.473 60.3697 4 11 5 10 456.784 98.4267 4 11 6 -6 2201.50 204.179 3 11 6 -5 812.983 118.725 3 11 6 -4 446.661 87.5948 3 11 6 -3 154.200 51.6179 3 11 6 -2-10.6504 27.3603 3 11 6 -1 307.444 82.0205 4 11 6 -1 208.781 53.6730 3 11 6 0 539.996 103.980 4 11 6 0 641.321 91.6143 3 11 6 1 1131.11 142.453 4 11 6 1 903.950 103.437 3 11 6 2 434.218 95.0763 4 11 6 2 449.398 75.0792 3 11 6 3 503.366 99.0687 4 11 6 3 429.213 70.5822 3 11 6 4 1766.85 141.804 3 11 6 4 1842.59 183.888 4 11 6 5 40.5139 48.9800 4 11 6 6 214.193 66.9135 4 11 6 7 324.198 76.9189 4 11 6 8 1424.43 167.161 4 11 6 9 1474.88 170.173 4 11 6 10 998.318 142.657 4 11 7 -5 43.2726 30.9619 3 11 7 -4 3509.58 255.966 3 11 7 -3 201.539 54.6653 3 11 7 -2 866.837 118.478 3 11 7 -1 264.846 63.0591 3 11 7 0 18.6523 43.2979 4 11 7 0 36.7937 30.3951 3 11 7 1 488.146 99.4654 4 11 7 1 434.185 75.7550 3 11 7 2 376.152 89.1919 4 11 7 2 304.933 62.4550 3 11 7 3 3400.45 215.859 3 11 7 3 3949.04 276.163 4 11 7 4 946.075 111.579 3 11 7 4 1071.64 144.614 4 11 7 5 590.752 106.281 4 11 7 6-9.55831 28.5660 4 11 7 7 82.9969 52.2785 4 11 7 8 224.298 68.8666 4 11 7 9-26.0564 41.6799 4 11 7 10 1491.08 172.330 4 11 8 -4-167.218 60.0847 3 11 8 -3 1360.92 157.540 3 11 8 -2 2131.48 194.735 3 11 8 -1 844.548 116.980 3 11 8 0 9.66251 27.3226 3 11 8 1 163.708 53.0585 3 11 8 2 136.230 65.5583 4 11 8 2 114.197 45.3627 3 11 8 3 2581.96 197.181 3 11 8 3 3114.59 250.812 4 11 8 4 2297.91 187.690 3 11 8 4 2512.41 220.044 4 11 8 5 2399.68 219.641 4 11 8 6 2130.62 204.648 4 11 8 7 116.489 48.8310 4 11 8 8 237.159 71.9100 4 11 8 9 201.457 67.7525 4 11 8 10 180.823 55.1107 4 11 9 -3-56.0391 31.6220 3 11 9 -2 1006.86 136.547 3 11 9 -1 546.218 98.2992 3 11 9 0 878.262 120.447 3 11 9 1 5.12349 34.2917 3 11 9 2 597.525 100.633 3 11 9 3 93.9454 45.0112 3 11 9 4 103.352 48.8947 3 11 9 5 31.7004 32.0296 4 11 9 6 1120.09 152.069 4 11 9 7 3056.67 250.436 4 -11 -9 -8 1735.77 168.024 1 11 9 8 1545.23 174.292 4 11 9 9 15.9430 28.2146 4 11 10 -1-46.7721 50.0242 3 11 10 0 1010.78 137.840 3 11 10 1 1256.62 153.411 3 11 10 2 30.1924 25.1369 3 11 10 3 342.820 80.7798 3 11 10 4 562.021 102.652 3 -11 -10 -6 1247.82 150.978 1 -11 -10 -7 25.5717 28.2088 1 -11 -10 -8 892.358 129.786 1 11 11 4 763.881 127.846 3 12 -1 -2 290.551 65.2697 5 12 -1 -2 257.367 70.3172 4 12 -1 -1 13.8409 24.1100 5 12 -1 -1 6.38148 33.4976 4 12 -1 0 1361.12 162.896 4 12 -1 0 1669.82 152.888 5 12 -1 1 280.204 62.8406 5 12 -1 2 14.5873 28.2318 5 12 -1 3 51.8270 26.4386 5 12 -1 4-76.1529 35.8179 5 12 -1 5 436.016 85.7257 5 12 0 -4 781.199 107.814 5 12 0 -3 102.043 40.4699 5 12 0 -3 82.7299 43.2238 4 12 0 -2 230.706 59.5256 5 12 0 -2 182.531 61.0525 4 12 0 -1 104.361 41.8225 5 12 0 -1 46.2750 35.1546 4 12 0 0 1594.18 174.367 4 12 0 0 1277.61 127.742 5 12 0 1 816.481 125.993 4 12 0 1 867.050 103.556 5 12 0 2 1078.23 116.945 5 12 0 2 969.117 137.227 4 12 0 3 841.676 101.819 5 12 0 4 279.902 56.4683 5 12 1 -5 209.524 54.8781 5 12 1 -4 404.959 77.3993 5 12 1 -4 397.655 84.5646 4 12 1 -3 1580.98 168.406 4 12 1 -3 1589.64 145.661 5 12 1 -2 1644.58 173.213 4 12 1 -2 1431.23 133.546 5 12 1 -1 23.5710 17.1464 5 12 1 -1 77.7994 36.8577 4 12 1 0 1137.42 146.813 4 12 1 0 1131.05 112.858 5 12 1 1 9.20114 21.2322 5 12 1 1-11.2467 27.4804 4 12 1 2 251.539 65.8059 4 12 1 3 1188.29 151.324 4 12 1 4 602.145 109.966 4 12 2 -5-6.40340 26.9568 5 12 2 -5-28.1767 43.0167 4 12 2 -4 382.531 69.0584 5 12 2 -4 299.991 76.7497 4 12 2 -3 301.682 60.8343 5 12 2 -3 333.083 77.3350 4 12 2 -2 329.690 80.0751 4 12 2 -1 689.877 114.180 4 12 2 0 759.328 120.215 4 12 2 1 411.761 89.8079 4 12 2 2 342.443 84.1376 4 12 2 3 566.251 103.754 4 12 2 4-11.6255 32.5043 4 12 2 5 807.591 127.571 4 12 3 -4-19.5130 30.8207 4 12 3 -3 19.7125 26.9185 4 12 3 -2-11.1293 28.8330 4 12 3 -1 1106.90 145.256 4 12 3 0 3245.62 251.998 4 12 3 1 560.151 107.642 4 12 3 2 308.767 79.1646 4 12 3 3 246.023 73.8019 4 12 3 4 311.615 84.6131 4 12 3 5 71.6059 35.4505 4 12 3 6 1443.56 171.628 4 12 4 -4 241.942 75.0520 4 12 4 -3 6.04190 26.4309 4 12 4 -2 189.163 66.0494 4 12 4 -1 376.012 88.3738 4 12 4 0 477.857 96.5998 4 12 4 1 878.912 128.739 4 12 4 2 290.786 74.9308 4 12 4 3 22.8145 32.7815 4 12 4 4 737.631 121.233 4 12 4 5 1012.56 141.891 4 12 4 6-22.1566 40.3935 4 12 5 -5 716.832 109.895 3 12 5 -4 341.070 74.1135 3 12 5 -3 177.857 64.2291 4 12 5 -2 195.595 66.5835 4 12 5 -1-6.58819 34.2547 4 12 5 0 992.573 142.002 4 12 5 1 185.615 67.0595 4 12 5 2 1286.81 158.016 4 12 5 3 164.916 62.3243 4 12 5 4 487.130 102.084 4 12 5 5 89.8914 43.1359 4 12 5 6-14.8713 33.3349 4 12 6 -5 226.930 67.7413 3 12 6 -4 1040.94 133.606 3 12 6 -3 1123.34 133.116 3 12 6 -2 1051.54 129.569 3 12 6 -1 204.467 70.0387 4 12 6 -1 131.810 46.8049 3 12 6 0 36.6484 39.2097 4 12 6 1 86.5176 47.7576 4 12 6 2 170.387 63.0265 4 12 6 3 143.564 55.9787 4 12 6 4 3433.32 267.194 4 12 6 5 1897.98 195.817 4 12 6 6 168.536 62.4192 4 12 7 -4 1171.89 147.322 3 12 7 -3 437.666 88.3233 3 12 7 -2 3501.89 245.620 3 12 7 -1 2735.65 209.450 3 12 7 0 57.9980 46.6541 4 12 7 0-22.5638 34.2628 3 12 7 1-0.23244 31.7696 4 12 7 1-14.2319 25.7225 3 12 7 2 224.253 71.5275 4 12 7 3 1067.91 147.316 4 12 7 4 685.132 121.256 4 12 7 5 1439.15 171.588 4 12 8 -3 117.006 55.9315 3 12 8 -2 51.5161 28.9749 3 12 8 -1 741.217 115.186 3 12 8 0 1935.54 177.097 3 12 8 1 706.560 109.120 3 12 8 2 563.971 93.0392 3 12 8 3 184.303 56.3517 3 12 9 -1-0.20646 28.5351 3 12 9 0 355.592 88.0020 3 12 9 1 308.026 76.3839 3 12 9 2 179.002 57.3593 3 12 9 3 39.8946 31.3909 3 12 9 4 185.961 56.7741 3 12 10 1 41.1235 35.9930 3 12 10 2 161.930 50.5241 3 12 10 3 702.102 115.224 3 12 10 4 337.197 86.6976 3 0 0 0 0.00 0.00 0 TITL exp_5096-ms in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 10.036315 10.186695 11.990204 83.0777 82.0323 70.0152 ZERR 5.00 0.000488 0.000567 0.000621 0.0045 0.0042 0.0047 LATT 1 SFAC C H N O UNIT 55.00 50.00 5.00 5.00 TREF HKLF 4 END ; _shelx_hkl_checksum 79776 data_12 #============================================================================== # PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic 2024-03-26 _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code AW5090 _journal_coeditor_notes ; ? ; _journal_paper_category FA _journal_techeditor_code ? _iucr_compatibility_tag ACTA95 _journal_techeditor_notes ; ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, C4 H10 O' _chemical_formula_sum 'C40 H42 Cl2 Cu N8 O9' _chemical_formula_weight 913.25 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.6577(4) _cell_length_b 9.8396(4) _cell_length_c 12.8200(6) _cell_angle_alpha 97.084(4) _cell_angle_beta 93.897(4) _cell_angle_gamma 108.096(4) _cell_volume 1023.61(8) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4469 _cell_measurement_theta_min 4.2850 _cell_measurement_theta_max 28.7910 _exptl_crystal_description prism _exptl_crystal_colour blue _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.482 _exptl_crystal_F_000 473 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.09 _exptl_absorpt_coefficient_mu 0.730 _shelx_estimated_absorpt_T_min 0.880 _shelx_estimated_absorpt_T_max 0.937 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.812 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'SuperNova (Mo) X-ray Source' _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean 10.4223 _diffrn_reflns_number 7915 _diffrn_reflns_av_unetI/netI 0.0300 _diffrn_reflns_av_R_equivalents 0.0228 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.921 _diffrn_reflns_theta_max 26.999 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 4386 _reflns_number_gt 4098 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0370P)^2^+0.6760P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4386 _refine_ls_number_parameters 330 _refine_ls_number_restraints 10 _refine_ls_R_factor_all 0.0337 _refine_ls_R_factor_gt 0.0311 _refine_ls_wR_factor_ref 0.0830 _refine_ls_wR_factor_gt 0.0803 _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_restrained_S_all 1.050 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.5000 0.5000 0.0000 0.01443(9) Uani 1 2 d S . P . . N1A N 0.23606(17) 0.10513(15) 0.07610(11) 0.0159(3) Uani 1 1 d D . . . . H1A H 0.232(3) 0.0184(12) 0.0797(17) 0.024 Uiso 1 1 d D U . . . C2A C 0.3595(2) 0.19666(18) 0.03637(13) 0.0170(3) Uani 1 1 d . . . . . H2A H 0.4490 0.1729 0.0095 0.020 Uiso 1 1 calc R U . . . N3A N 0.33873(16) 0.32474(14) 0.03994(10) 0.0151(3) Uani 1 1 d . . . . . C4A C 0.19500(19) 0.31291(17) 0.08347(12) 0.0149(3) Uani 1 1 d . . . . . H4A H 0.1490 0.3886 0.0958 0.018 Uiso 1 1 calc R U . . . C5A C 0.12830(19) 0.17613(17) 0.10639(12) 0.0137(3) Uani 1 1 d . . . . . C6A C -0.02134(19) 0.10991(17) 0.15313(12) 0.0138(3) Uani 1 1 d . . . . . C7A C -0.0473(2) -0.01865(18) 0.19543(14) 0.0195(3) Uani 1 1 d . . . . . H7A H 0.0332 -0.0658 0.1938 0.023 Uiso 1 1 calc R U . . . C8A C -0.1905(2) -0.07763(19) 0.23985(15) 0.0238(4) Uani 1 1 d . . . . . H8A H -0.2077 -0.1656 0.2678 0.029 Uiso 1 1 calc R U . . . C9A C -0.3084(2) -0.00990(19) 0.24389(14) 0.0220(4) Uani 1 1 d . . . . . H9A H -0.4058 -0.0505 0.2749 0.026 Uiso 1 1 calc R U . . . C10A C -0.2833(2) 0.11789(19) 0.20227(14) 0.0207(3) Uani 1 1 d . . . . . H10A H -0.3638 0.1651 0.2050 0.025 Uiso 1 1 calc R U . . . C11A C -0.1419(2) 0.17721(18) 0.15683(13) 0.0173(3) Uani 1 1 d . . . . . H11A H -0.1266 0.2642 0.1279 0.021 Uiso 1 1 calc R U . . . N1B N 0.13121(17) 0.42449(15) -0.24305(11) 0.0171(3) Uani 1 1 d D . . . . H1B H 0.0292(13) 0.391(2) -0.2641(16) 0.026 Uiso 1 1 d D U . . . C2B C 0.1915(2) 0.43359(17) -0.14255(13) 0.0169(3) Uani 1 1 d . . . . . H2B H 0.1269 0.4040 -0.0873 0.020 Uiso 1 1 calc R U . . . N3B N 0.35165(16) 0.48879(15) -0.13034(10) 0.0156(3) Uani 1 1 d . . . . . C4B C 0.3952(2) 0.5160(2) -0.22964(14) 0.0255(4) Uani 1 1 d . . . . . H4B H 0.5040 0.5567 -0.2457 0.031 Uiso 1 1 calc R U . . . C5B C 0.2589(2) 0.4756(2) -0.30072(13) 0.0214(4) Uani 1 1 d . . . . . C6B C 0.2275(5) 0.4518(4) -0.4167(2) 0.0176(12) Uani 0.5 1 d G . P A 1 C7B C 0.0841(5) 0.3549(4) -0.4720(3) 0.0222(12) Uani 0.5 1 d G . P A 1 H7B H 0.0042 0.2957 -0.4352 0.027 Uiso 0.5 1 calc R U P A 1 C8B C 0.0575(4) 0.3445(4) -0.5813(3) 0.0289(13) Uani 0.5 1 d G . P A 1 H8B H -0.0405 0.2783 -0.6191 0.035 Uiso 0.5 1 calc R U P A 1 C9B C 0.1744(4) 0.4311(4) -0.6352(2) 0.0242(11) Uani 0.5 1 d G . P A 1 H9B H 0.1562 0.4241 -0.7099 0.029 Uiso 0.5 1 calc R U P A 1 C10B C 0.3178(3) 0.5280(4) -0.5799(2) 0.0259(8) Uani 0.5 1 d G . P A 1 H10B H 0.3976 0.5872 -0.6167 0.031 Uiso 0.5 1 calc R U P A 1 C11B C 0.3443(3) 0.5383(3) -0.4706(2) 0.0218(8) Uani 0.5 1 d G . P A 1 H11B H 0.4424 0.6046 -0.4328 0.026 Uiso 0.5 1 calc R U P A 1 C6C C 0.2419(5) 0.4922(4) -0.4147(2) 0.0164(11) Uani 0.5 1 d G . P A 2 C7C C 0.1351(6) 0.3726(4) -0.4809(3) 0.0265(12) Uani 0.5 1 d G . P A 2 H7C H 0.0735 0.2909 -0.4519 0.032 Uiso 0.5 1 calc R U P A 2 C8C C 0.1184(5) 0.3724(3) -0.5896(3) 0.0319(14) Uani 0.5 1 d G . P A 2 H8C H 0.0454 0.2906 -0.6348 0.038 Uiso 0.5 1 calc R U P A 2 C9C C 0.2084(5) 0.4919(4) -0.6320(2) 0.0258(12) Uani 0.5 1 d G . P A 2 H9C H 0.1970 0.4917 -0.7062 0.031 Uiso 0.5 1 calc R U P A 2 C10C C 0.3152(4) 0.6115(3) -0.56579(19) 0.0264(8) Uani 0.5 1 d G . P A 2 H10C H 0.3768 0.6932 -0.5948 0.032 Uiso 0.5 1 calc R U P A 2 C11C C 0.3319(4) 0.6117(3) -0.45717(18) 0.0217(7) Uani 0.5 1 d G . P A 2 H11C H 0.4049 0.6935 -0.4119 0.026 Uiso 0.5 1 calc R U P A 2 Cl Cl 0.26988(5) 0.72337(4) 0.12601(3) 0.01654(10) Uani 1 1 d . . . . . O1 O 0.39920(15) 0.66131(13) 0.13604(10) 0.0214(3) Uani 1 1 d . . . . . O2 O 0.21253(17) 0.74779(16) 0.22694(11) 0.0319(3) Uani 1 1 d . . . . . O3 O 0.13731(15) 0.62726(13) 0.05218(10) 0.0228(3) Uani 1 1 d . . . . . O4 O 0.33199(16) 0.85956(13) 0.08722(12) 0.0271(3) Uani 1 1 d . . . . . O5 O 0.5000 0.0000 0.5000 0.0568(7) Uani 1 2 d DS . P . . C12A C 0.6054(6) -0.0650(5) 0.5269(4) 0.0401(10) Uani 0.5 1 d D . P B 1 H12A H 0.5910 -0.1481 0.4708 0.048 Uiso 0.5 1 calc R U P B 1 H12B H 0.5746 -0.1051 0.5924 0.048 Uiso 0.5 1 calc R U P B 1 C13A C 0.7838(6) 0.0207(7) 0.5451(5) 0.0426(13) Uani 0.5 1 d D U P B 1 H13A H 0.8470 -0.0425 0.5617 0.064 Uiso 0.5 1 calc R U P B 1 H13B H 0.8031 0.0993 0.6043 0.064 Uiso 0.5 1 calc R U P B 1 H13C H 0.8180 0.0615 0.4812 0.064 Uiso 0.5 1 calc R U P B 1 C12B C 0.6568(5) 0.0530(5) 0.5237(4) 0.0401(11) Uani 0.5 1 d D . P B 2 H12C H 0.6807 0.1339 0.5829 0.048 Uiso 0.5 1 calc R U P B 2 H12D H 0.7055 0.0937 0.4621 0.048 Uiso 0.5 1 calc R U P B 2 C13B C 0.7390(9) -0.0509(8) 0.5543(7) 0.069(2) Uani 0.5 1 d D U P B 2 H13D H 0.8576 -0.0027 0.5660 0.104 Uiso 0.5 1 calc R U P B 2 H13E H 0.7134 -0.1335 0.4975 0.104 Uiso 0.5 1 calc R U P B 2 H13F H 0.7001 -0.0849 0.6194 0.104 Uiso 0.5 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.01181(14) 0.01697(15) 0.01191(14) 0.00545(10) 0.00048(10) -0.00014(11) N1A 0.0163(7) 0.0130(6) 0.0196(7) 0.0043(5) 0.0047(5) 0.0051(5) C2A 0.0147(8) 0.0191(8) 0.0163(7) 0.0028(6) 0.0022(6) 0.0040(6) N3A 0.0135(6) 0.0164(7) 0.0133(6) 0.0042(5) 0.0002(5) 0.0014(5) C4A 0.0158(7) 0.0147(7) 0.0141(7) 0.0038(6) 0.0016(6) 0.0042(6) C5A 0.0151(7) 0.0137(7) 0.0121(7) 0.0025(6) 0.0001(6) 0.0045(6) C6A 0.0145(7) 0.0133(7) 0.0122(7) 0.0021(6) 0.0016(6) 0.0025(6) C7A 0.0218(8) 0.0156(8) 0.0239(8) 0.0063(6) 0.0067(7) 0.0078(7) C8A 0.0285(9) 0.0161(8) 0.0279(9) 0.0095(7) 0.0103(8) 0.0048(7) C9A 0.0181(8) 0.0225(9) 0.0215(8) 0.0023(7) 0.0074(7) 0.0005(7) C10A 0.0158(8) 0.0229(9) 0.0232(8) 0.0024(7) 0.0019(7) 0.0064(7) C11A 0.0180(8) 0.0160(8) 0.0180(8) 0.0044(6) 0.0004(6) 0.0053(6) N1B 0.0118(6) 0.0198(7) 0.0191(7) 0.0022(5) -0.0005(5) 0.0051(5) C2B 0.0166(8) 0.0175(8) 0.0178(8) 0.0047(6) 0.0035(6) 0.0063(6) N3B 0.0143(6) 0.0183(7) 0.0133(6) 0.0039(5) 0.0024(5) 0.0036(5) C4B 0.0150(8) 0.0441(11) 0.0161(8) 0.0119(8) 0.0033(7) 0.0045(8) C5B 0.0180(8) 0.0317(10) 0.0163(8) 0.0045(7) 0.0018(6) 0.0103(7) C6B 0.020(2) 0.019(2) 0.018(2) 0.0056(16) 0.0028(19) 0.0108(19) C7B 0.022(3) 0.025(2) 0.016(2) -0.0009(17) -0.0021(17) 0.0053(17) C8B 0.030(3) 0.033(3) 0.021(2) -0.0018(18) -0.005(2) 0.011(2) C9B 0.039(3) 0.025(3) 0.013(2) 0.0026(18) 0.0000(18) 0.017(2) C10B 0.031(2) 0.031(2) 0.0186(18) 0.0052(16) 0.0045(17) 0.0124(18) C11B 0.0220(19) 0.024(2) 0.0201(18) 0.0034(16) 0.0010(14) 0.0081(16) C6C 0.018(2) 0.020(3) 0.013(2) -0.0001(13) -0.0037(16) 0.0096(16) C7C 0.029(3) 0.026(2) 0.023(2) 0.0058(19) 0.001(2) 0.006(2) C8C 0.040(4) 0.033(3) 0.017(2) -0.005(2) -0.009(2) 0.010(3) C9C 0.038(3) 0.029(3) 0.018(2) 0.0063(19) 0.0049(19) 0.019(2) C10C 0.030(2) 0.034(2) 0.0197(18) 0.0092(17) 0.0051(15) 0.0137(18) C11C 0.0245(19) 0.024(2) 0.0175(17) 0.0047(15) 0.0019(14) 0.0084(16) Cl 0.01331(18) 0.01325(18) 0.0218(2) -0.00059(14) 0.00448(15) 0.00314(14) O1 0.0178(6) 0.0201(6) 0.0281(6) 0.0037(5) 0.0030(5) 0.0087(5) O2 0.0281(7) 0.0382(8) 0.0252(7) -0.0053(6) 0.0114(6) 0.0066(6) O3 0.0163(6) 0.0192(6) 0.0289(7) -0.0034(5) -0.0008(5) 0.0034(5) O4 0.0217(6) 0.0154(6) 0.0463(8) 0.0084(5) 0.0090(6) 0.0066(5) O5 0.0474(15) 0.088(2) 0.0395(13) -0.0021(13) 0.0006(11) 0.0344(15) C12A 0.055(3) 0.031(2) 0.035(2) 0.0031(18) 0.008(2) 0.015(2) C13A 0.040(3) 0.050(4) 0.033(2) -0.010(3) -0.003(2) 0.015(3) C12B 0.034(2) 0.043(3) 0.031(2) -0.0044(19) 0.0016(18) 0.000(2) C13B 0.033(4) 0.065(5) 0.096(6) -0.009(4) -0.012(3) 0.006(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 2.0012(13) . ? Cu N3A 2.0012(13) 2_665 ? Cu N3B 2.0072(13) 2_665 ? Cu N3B 2.0072(13) . ? N1A C2A 1.342(2) . ? N1A C5A 1.377(2) . ? N1A H1A 0.851(9) . ? C2A N3A 1.323(2) . ? C2A H2A 0.9500 . ? N3A C4A 1.376(2) . ? C4A C5A 1.367(2) . ? C4A H4A 0.9500 . ? C5A C6A 1.463(2) . ? C6A C7A 1.398(2) . ? C6A C11A 1.400(2) . ? C7A C8A 1.389(2) . ? C7A H7A 0.9500 . ? C8A C9A 1.382(3) . ? C8A H8A 0.9500 . ? C9A C10A 1.387(2) . ? C9A H9A 0.9500 . ? C10A C11A 1.384(2) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.339(2) . ? N1B C5B 1.371(2) . ? N1B H1B 0.852(9) . ? C2B N3B 1.313(2) . ? C2B H2B 0.9500 . ? N3B C4B 1.386(2) . ? C4B C5B 1.361(2) . ? C4B H4B 0.9500 . ? C5B C6B 1.469(3) . ? C5B C6C 1.493(3) . ? C6B C7B 1.3900 . ? C6B C11B 1.3900 . ? C7B C8B 1.3900 . ? C7B H7B 0.9500 . ? C8B C9B 1.3900 . ? C8B H8B 0.9500 . ? C9B C10B 1.3900 . ? C9B H9B 0.9500 . ? C10B C11B 1.3900 . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? C6C C7C 1.3900 . ? C6C C11C 1.3900 . ? C7C C8C 1.3900 . ? C7C H7C 0.9500 . ? C8C C9C 1.3900 . ? C8C H8C 0.9500 . ? C9C C10C 1.3900 . ? C9C H9C 0.9500 . ? C10C C11C 1.3900 . ? C10C H10C 0.9500 . ? C11C H11C 0.9500 . ? Cl O2 1.4364(13) . ? Cl O3 1.4370(12) . ? Cl O1 1.4379(12) . ? Cl O4 1.4441(13) . ? O5 C12B 1.293(4) 2_656 ? O5 C12B 1.293(4) . ? O5 C12A 1.317(4) 2_656 ? O5 C12A 1.317(4) . ? C12A C13A 1.499(6) . ? C12A H12A 0.9900 . ? C12A H12B 0.9900 . ? C13A H13A 0.9800 . ? C13A H13B 0.9800 . ? C13A H13C 0.9800 . ? C12B C13B 1.489(7) . ? C12B H12C 0.9900 . ? C12B H12D 0.9900 . ? C13B H13D 0.9800 . ? C13B H13E 0.9800 . ? C13B H13F 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 . 2_665 ? N3A Cu N3B 89.00(5) . 2_665 ? N3A Cu N3B 91.00(5) 2_665 2_665 ? N3A Cu N3B 91.00(5) . . ? N3A Cu N3B 89.00(5) 2_665 . ? N3B Cu N3B 180.0 2_665 . ? C2A N1A C5A 108.81(13) . . ? C2A N1A H1A 121.5(15) . . ? C5A N1A H1A 129.7(15) . . ? N3A C2A N1A 110.30(14) . . ? N3A C2A H2A 124.8 . . ? N1A C2A H2A 124.8 . . ? C2A N3A C4A 106.19(13) . . ? C2A N3A Cu 124.72(11) . . ? C4A N3A Cu 128.89(11) . . ? C5A C4A N3A 109.94(14) . . ? C5A C4A H4A 125.0 . . ? N3A C4A H4A 125.0 . . ? C4A C5A N1A 104.74(14) . . ? C4A C5A C6A 131.12(15) . . ? N1A C5A C6A 124.13(14) . . ? C7A C6A C11A 118.68(15) . . ? C7A C6A C5A 121.88(15) . . ? C11A C6A C5A 119.44(14) . . ? C8A C7A C6A 120.18(16) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C9A C8A C7A 120.77(16) . . ? C9A C8A H8A 119.6 . . ? C7A C8A H8A 119.6 . . ? C8A C9A C10A 119.35(16) . . ? C8A C9A H9A 120.3 . . ? C10A C9A H9A 120.3 . . ? C11A C10A C9A 120.54(16) . . ? C11A C10A H10A 119.7 . . ? C9A C10A H10A 119.7 . . ? C10A C11A C6A 120.48(15) . . ? C10A C11A H11A 119.8 . . ? C6A C11A H11A 119.8 . . ? C2B N1B C5B 108.59(14) . . ? C2B N1B H1B 122.8(15) . . ? C5B N1B H1B 128.6(15) . . ? N3B C2B N1B 111.10(14) . . ? N3B C2B H2B 124.5 . . ? N1B C2B H2B 124.5 . . ? C2B N3B C4B 105.49(14) . . ? C2B N3B Cu 126.11(11) . . ? C4B N3B Cu 127.74(11) . . ? C5B C4B N3B 109.91(15) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 104.91(15) . . ? C4B C5B C6B 135.0(2) . . ? N1B C5B C6B 118.9(2) . . ? C4B C5B C6C 129.9(2) . . ? N1B C5B C6C 125.0(2) . . ? C7B C6B C11B 120.0 . . ? C7B C6B C5B 123.0(2) . . ? C11B C6B C5B 116.9(2) . . ? C8B C7B C6B 120.0 . . ? C8B C7B H7B 120.0 . . ? C6B C7B H7B 120.0 . . ? C7B C8B C9B 120.0 . . ? C7B C8B H8B 120.0 . . ? C9B C8B H8B 120.0 . . ? C8B C9B C10B 120.0 . . ? C8B C9B H9B 120.0 . . ? C10B C9B H9B 120.0 . . ? C11B C10B C9B 120.0 . . ? C11B C10B H10B 120.0 . . ? C9B C10B H10B 120.0 . . ? C10B C11B C6B 120.0 . . ? C10B C11B H11B 120.0 . . ? C6B C11B H11B 120.0 . . ? C7C C6C C11C 120.0 . . ? C7C C6C C5B 115.1(2) . . ? C11C C6C C5B 124.7(2) . . ? C6C C7C C8C 120.0 . . ? C6C C7C H7C 120.0 . . ? C8C C7C H7C 120.0 . . ? C9C C8C C7C 120.0 . . ? C9C C8C H8C 120.0 . . ? C7C C8C H8C 120.0 . . ? C10C C9C C8C 120.0 . . ? C10C C9C H9C 120.0 . . ? C8C C9C H9C 120.0 . . ? C9C C10C C11C 120.0 . . ? C9C C10C H10C 120.0 . . ? C11C C10C H10C 120.0 . . ? C10C C11C C6C 120.0 . . ? C10C C11C H11C 120.0 . . ? C6C C11C H11C 120.0 . . ? O2 Cl O3 109.66(8) . . ? O2 Cl O1 110.24(8) . . ? O3 Cl O1 109.57(7) . . ? O2 Cl O4 109.28(8) . . ? O3 Cl O4 109.24(8) . . ? O1 Cl O4 108.82(7) . . ? C12B O5 C12B 180.0 2_656 . ? C12A O5 C12A 180.0 2_656 . ? O5 C12A C13A 118.8(4) . . ? O5 C12A H12A 107.6 . . ? C13A C12A H12A 107.6 . . ? O5 C12A H12B 107.6 . . ? C13A C12A H12B 107.6 . . ? H12A C12A H12B 107.1 . . ? C12A C13A H13A 109.5 . . ? C12A C13A H13B 109.5 . . ? H13A C13A H13B 109.5 . . ? C12A C13A H13C 109.5 . . ? H13A C13A H13C 109.5 . . ? H13B C13A H13C 109.5 . . ? O5 C12B C13B 115.5(4) . . ? O5 C12B H12C 108.4 . . ? C13B C12B H12C 108.4 . . ? O5 C12B H12D 108.4 . . ? C13B C12B H12D 108.4 . . ? H12C C12B H12D 107.5 . . ? C12B C13B H13D 109.5 . . ? C12B C13B H13E 109.5 . . ? H13D C13B H13E 109.5 . . ? C12B C13B H13F 109.5 . . ? H13D C13B H13F 109.5 . . ? H13E C13B H13F 109.5 . . ? _refine_diff_density_max 0.373 _refine_diff_density_min -0.460 _refine_diff_density_rms 0.058 # start Validation Reply Form _vrf_PLAT301_12 ; RESPONSE: The structure exhibits disorder affecting i) the phenyl ring C6B to C11B which has been modelled over two orientations (B and C) with a 50:50 domain ratio, and ii) the diethyl ether solvent molecule orientationally disordered about a center of symmetry (50:50), as calculated in both cases after detailed refinement. ; _vrf_PLAT154_12 ; RESPONSE: The provided s.u.'s values are correct. Unrounded s.u.'s show slight differences. ; # end Validation Reply Form _shelx_res_file ; 12.res created by SHELXL-2014/7 TITL EL23G in P-1 CELL 0.71073 8.6577 9.8396 12.8200 97.084 93.897 108.096 ZERR 1 0.0004 0.0004 0.0006 0.004 0.004 0.004 LATT 1 SFAC C H N O CL CU UNIT 40 42 8 9 2 1 MERG 2 FMAP 2 OMIT -2 54 SIZE 0.18 0.11 0.09 TEMP -173 ACTA LIST 4 MORE -3 BOND BOND $H HTAB PLAN 10 L.S. 6 WGHT 0.037000 0.676000 FVAR 4.94084 CU 6 0.500000 0.500000 0.000000 10.50000 0.01181 0.01697 = 0.01191 0.00545 0.00048 -0.00014 DFIX 0.86 0.01 N1A H1A N1A 3 0.236060 0.105126 0.076097 11.00000 0.01633 0.01298 = 0.01960 0.00425 0.00466 0.00506 H1A 2 0.232416 0.018392 0.079655 11.00000 -1.50000 C2A 1 0.359485 0.196660 0.036365 11.00000 0.01470 0.01910 = 0.01631 0.00276 0.00223 0.00398 AFIX 43 H2A 2 0.448963 0.172866 0.009511 11.00000 -1.20000 AFIX 0 N3A 3 0.338732 0.324736 0.039944 11.00000 0.01346 0.01643 = 0.01329 0.00418 0.00023 0.00145 C4A 1 0.195005 0.312908 0.083475 11.00000 0.01576 0.01473 = 0.01414 0.00383 0.00161 0.00417 AFIX 43 H4A 2 0.148952 0.388594 0.095778 11.00000 -1.20000 AFIX 0 C5A 1 0.128305 0.176134 0.106392 11.00000 0.01515 0.01372 = 0.01210 0.00251 0.00011 0.00448 C6A 1 -0.021345 0.109909 0.153133 11.00000 0.01452 0.01332 = 0.01218 0.00206 0.00162 0.00247 C7A 1 -0.047306 -0.018646 0.195431 11.00000 0.02183 0.01561 = 0.02392 0.00632 0.00673 0.00780 AFIX 43 H7A 2 0.033232 -0.065802 0.193797 11.00000 -1.20000 AFIX 0 C8A 1 -0.190541 -0.077632 0.239848 11.00000 0.02849 0.01608 = 0.02785 0.00951 0.01029 0.00485 AFIX 43 H8A 2 -0.207660 -0.165553 0.267773 11.00000 -1.20000 AFIX 0 C9A 1 -0.308449 -0.009904 0.243889 11.00000 0.01809 0.02249 = 0.02155 0.00234 0.00745 0.00045 AFIX 43 H9A 2 -0.405766 -0.050466 0.274863 11.00000 -1.20000 AFIX 0 C10A 1 -0.283290 0.117895 0.202269 11.00000 0.01582 0.02285 = 0.02318 0.00235 0.00193 0.00645 AFIX 43 H10A 2 -0.363774 0.165073 0.204983 11.00000 -1.20000 AFIX 0 C11A 1 -0.141933 0.177214 0.156834 11.00000 0.01803 0.01595 = 0.01804 0.00436 0.00035 0.00529 AFIX 43 H11A 2 -0.126616 0.264248 0.127944 11.00000 -1.20000 AFIX 0 DFIX 0.86 0.01 N1B H1B N1B 3 0.131213 0.424492 -0.243055 11.00000 0.01185 0.01982 = 0.01908 0.00218 -0.00055 0.00509 H1B 2 0.029174 0.391404 -0.264073 11.00000 -1.50000 C2B 1 0.191525 0.433589 -0.142548 11.00000 0.01664 0.01752 = 0.01784 0.00466 0.00355 0.00632 AFIX 43 H2B 2 0.126931 0.403986 -0.087314 11.00000 -1.20000 AFIX 0 N3B 3 0.351646 0.488787 -0.130340 11.00000 0.01432 0.01832 = 0.01335 0.00387 0.00238 0.00357 C4B 1 0.395191 0.515983 -0.229640 11.00000 0.01499 0.04407 = 0.01608 0.01192 0.00334 0.00445 AFIX 43 H4B 2 0.503977 0.556729 -0.245722 11.00000 -1.20000 AFIX 0 C5B 1 0.258914 0.475635 -0.300716 11.00000 0.01802 0.03172 = 0.01633 0.00451 0.00184 0.01025 PART 1 AFIX 66 C6B 1 0.227491 0.451756 -0.416686 10.50000 0.02029 0.01901 = 0.01759 0.00556 0.00278 0.01083 C7B 1 0.084075 0.354859 -0.472028 10.50000 0.02200 0.02524 = 0.01600 -0.00094 -0.00208 0.00529 AFIX 43 H7B 2 0.004213 0.295685 -0.435172 10.50000 -1.20000 AFIX 65 C8B 1 0.057508 0.344543 -0.581295 10.50000 0.02985 0.03323 = 0.02136 -0.00175 -0.00472 0.01083 AFIX 43 H8B 2 -0.040511 0.278317 -0.619117 10.50000 -1.20000 AFIX 65 C9B 1 0.174358 0.431123 -0.635221 10.50000 0.03888 0.02456 = 0.01326 0.00261 0.00003 0.01695 AFIX 43 H9B 2 0.156200 0.424072 -0.709900 10.50000 -1.20000 AFIX 65 C10B 1 0.317775 0.528021 -0.579881 10.50000 0.03090 0.03070 = 0.01864 0.00521 0.00451 0.01243 AFIX 43 H10B 2 0.397636 0.587195 -0.616738 10.50000 -1.20000 AFIX 65 C11B 1 0.344343 0.538339 -0.470614 10.50000 0.02202 0.02372 = 0.02009 0.00342 0.00098 0.00811 AFIX 43 H11B 2 0.442362 0.604565 -0.432791 10.50000 -1.20000 AFIX 66 PART 2 C6C 1 0.241866 0.492247 -0.414732 10.50000 0.01775 0.01976 = 0.01262 -0.00013 -0.00365 0.00963 C7C 1 0.135091 0.372567 -0.480928 10.50000 0.02931 0.02587 = 0.02281 0.00585 0.00107 0.00621 AFIX 43 H7C 2 0.073539 0.290903 -0.451927 10.50000 -1.20000 AFIX 65 C8C 1 0.118374 0.372375 -0.589555 10.50000 0.03992 0.03285 = 0.01743 -0.00500 -0.00905 0.00997 AFIX 43 H8C 2 0.045398 0.290579 -0.634797 10.50000 -1.20000 AFIX 65 C9C 1 0.208433 0.491863 -0.631988 10.50000 0.03766 0.02901 = 0.01753 0.00635 0.00493 0.01907 AFIX 43 H9C 2 0.197008 0.491731 -0.706231 10.50000 -1.20000 AFIX 65 C10C 1 0.315209 0.611543 -0.565794 10.50000 0.02960 0.03411 = 0.01969 0.00916 0.00510 0.01374 AFIX 43 H10C 2 0.376760 0.693207 -0.594796 10.50000 -1.20000 AFIX 65 C11C 1 0.331927 0.611737 -0.457166 10.50000 0.02452 0.02390 = 0.01750 0.00469 0.00189 0.00838 AFIX 43 H11C 2 0.404904 0.693533 -0.411926 10.50000 -1.20000 AFIX 0 PART 0 CL 5 0.269879 0.723369 0.126012 11.00000 0.01331 0.01325 = 0.02176 -0.00059 0.00448 0.00314 O1 4 0.399195 0.661306 0.136039 11.00000 0.01778 0.02012 = 0.02808 0.00375 0.00298 0.00866 O2 4 0.212526 0.747793 0.226939 11.00000 0.02809 0.03818 = 0.02516 -0.00533 0.01136 0.00663 O3 4 0.137311 0.627256 0.052180 11.00000 0.01632 0.01920 = 0.02889 -0.00344 -0.00082 0.00342 O4 4 0.331988 0.859564 0.087221 11.00000 0.02174 0.01544 = 0.04633 0.00843 0.00904 0.00657 O5 4 0.500000 0.000000 0.500000 10.50000 0.04744 0.08839 = 0.03946 -0.00208 0.00058 0.03442 SADI 0.01 O5 C12A O5 C12B SADI 0.01 C12A C13A C12B C13B SIMU 0.01 1.0 C13A C13B PART 1 C12A 1 0.605360 -0.065020 0.526860 10.50000 0.05516 0.03107 = 0.03464 0.00312 0.00848 0.01475 AFIX 23 H12A 2 0.591001 -0.148114 0.470809 10.50000 -1.20000 H12B 2 0.574575 -0.105107 0.592427 10.50000 -1.20000 AFIX 0 C13A 1 0.783808 0.020733 0.545088 10.50000 0.03978 0.04952 = 0.03305 -0.00998 -0.00322 0.01450 AFIX 137 H13A 2 0.846976 -0.042533 0.561711 10.50000 -1.50000 H13B 2 0.803104 0.099347 0.604316 10.50000 -1.50000 H13C 2 0.818035 0.061462 0.481157 10.50000 -1.50000 AFIX 0 PART 2 C12B 1 0.656839 0.052993 0.523703 10.50000 0.03393 0.04343 = 0.03134 -0.00439 0.00155 0.00033 AFIX 23 H12C 2 0.680702 0.133920 0.582899 10.50000 -1.20000 H12D 2 0.705539 0.093678 0.462101 10.50000 -1.20000 AFIX 0 C13B 1 0.739004 -0.050917 0.554257 10.50000 0.03285 0.06468 = 0.09575 -0.00891 -0.01247 0.00612 AFIX 137 H13D 2 0.857571 -0.002672 0.566010 10.50000 -1.50000 H13E 2 0.713446 -0.133536 0.497458 10.50000 -1.50000 H13F 2 0.700069 -0.084924 0.619410 10.50000 -1.50000 AFIX 0 HKLF 4 REM EL23G in P-1 REM R1 = 0.0311 for 4098 Fo > 4sig(Fo) and 0.0337 for all 4386 data REM 330 parameters refined using 10 restraints END WGHT 0.0371 0.6659 REM Instructions for potential hydrogen bonds EQIV $1 x, y-1, z HTAB N1A O4_$1 EQIV $2 -x+1, -y+1, -z HTAB C2A O4_$2 HTAB C4A O3 EQIV $3 -x, -y+1, -z HTAB N1B O2_$3 HTAB C2B O3 HTAB C2B O3_$3 EQIV $4 -x+1, -y+1, -z+1 HTAB C13A O2_$4 HTAB C12B O2_$4 REM Highest difference peak 0.373, deepest hole -0.460, 1-sigma level 0.058 Q1 1 0.2303 0.6728 0.2404 11.00000 0.05 0.37 Q2 1 0.3960 0.4926 -0.0627 11.00000 0.05 0.36 Q3 1 0.0541 0.1421 0.1304 11.00000 0.05 0.32 Q4 1 0.1916 0.4401 -0.2790 11.00000 0.05 0.29 Q5 1 0.3307 0.5297 -0.2674 11.00000 0.05 0.29 Q6 1 0.3276 0.4693 -0.2716 11.00000 0.05 0.29 Q7 1 -0.1281 -0.0575 0.2005 11.00000 0.05 0.28 Q8 1 -0.2815 0.0565 0.2221 11.00000 0.05 0.28 Q9 1 0.3811 0.4847 -0.1750 11.00000 0.05 0.27 Q10 1 0.1930 0.6727 0.0763 11.00000 0.05 0.27 ; _shelx_res_checksum 13638 _shelx_hkl_file ; 0 0 2 51032.5 914.219 2 0 0 -3 132774. 2326.71 3 0 0 3 133495. 2324.44 3 0 0 3 137313. 2348.44 2 0 0 4 2234.44 102.405 2 0 0 -4 1804.52 79.0198 3 0 0 4 1960.95 82.9829 3 0 0 -5 120.591 23.7471 3 0 0 5 98.8484 24.2731 3 0 0 5 227.002 37.2811 2 0 0 5 127.517 28.0017 4 0 0 6 9062.35 257.905 4 0 0 6 9862.64 290.742 2 0 0 -6 9376.17 254.613 3 0 0 6 9126.16 253.736 3 0 0 7 12039.8 322.117 3 0 0 7 12268.5 360.528 2 0 0 -7 11916.9 317.773 3 0 0 7 12432.5 336.206 4 0 0 8 40718.8 838.680 3 0 0 -8 39142.9 823.025 3 0 0 8 39652.3 888.020 2 0 0 8 40989.9 848.859 4 0 0 9 21258.2 571.679 2 0 0 -9 19479.6 495.217 3 0 0 9 21177.1 519.712 4 0 0 9 20445.6 513.598 3 0 0 9 21454.5 475.030 1 0 0 10 373.479 59.4783 3 0 0 10 581.818 74.3265 4 0 0 10 422.323 45.4030 1 0 0 10 822.790 102.760 2 0 0 11 7021.24 207.346 1 0 0 11 6747.77 273.269 4 0 0 11 6525.73 311.818 2 0 0 11 6570.29 264.156 3 0 0 12 163.914 50.3197 2 0 0 12 123.519 38.4957 4 0 0 13 4021.07 260.444 2 0 0 13 4224.45 226.144 4 0 0 14 4785.64 299.359 2 0 0 14 4277.24 236.318 4 0 0 15 1671.89 180.516 2 0 0 16 2208.16 221.297 2 0 -1 16 2441.55 242.693 2 0 -1 15 35.8376 35.5080 2 0 -1 15-15.5632 22.2725 4 0 -1 14 416.288 85.7092 2 0 -1 14 524.729 82.4118 4 0 -1 13 76.6824 30.3945 4 0 -1 13 152.766 53.5134 2 0 -1 12 1678.64 135.604 4 0 -1 12 1771.64 163.685 2 0 -1 11 72.7839 32.4644 4 0 -1 11 38.3285 32.3728 2 0 -1 10 14415.4 426.729 4 0 -1 10 14068.1 463.046 2 0 1 -10 13839.7 386.836 3 0 1 -9 33042.4 726.431 3 0 -1 9 34781.0 773.625 4 0 -1 9 34445.1 820.976 2 0 -1 8 8856.20 288.938 4 0 1 -8 8627.63 260.975 3 0 -1 8 8602.37 319.473 2 0 -1 7 12497.5 348.631 4 0 1 -7 11602.0 317.162 3 0 -1 6 11040.4 323.843 2 0 1 -6 9728.00 261.438 3 0 -1 6 10322.1 291.426 4 0 -1 5 7489.94 236.849 2 0 -1 5 6845.35 214.337 4 0 1 -5 6933.98 193.157 3 0 1 -4 9354.34 226.140 3 0 -1 4 9010.19 243.838 4 0 1 -4 8582.44 240.605 4 0 1 -3 28403.6 522.674 1 0 -1 3 28232.0 563.118 4 0 -1 3 29589.9 578.445 2 0 -1 2 72359.1 1284.23 4 0 -1 2 72174.9 1288.87 2 0 1 1 4723.90 107.209 2 0 1 2 4049.95 119.335 3 0 1 2 4171.08 110.951 2 0 1 3 113552. 2018.20 3 0 1 3 117170. 2014.48 2 0 -1 -3 113413. 2020.95 3 0 1 4 794.947 56.5768 3 0 -1 -4 764.507 55.1849 2 0 1 4 945.886 62.9719 2 0 -1 -4 769.624 54.9362 3 0 -1 -5 20168.3 447.759 3 0 1 5 20477.4 450.716 3 0 -1 -5 19480.2 449.520 2 0 1 5 19839.1 456.409 2 0 -1 -6 36287.8 727.541 3 0 -1 -6 32600.3 727.574 2 0 1 6 35954.6 746.167 2 0 1 6 34982.0 723.414 3 0 1 7 124849. 2279.84 2 0 -1 -7 123945. 2245.64 3 0 1 7 121908. 2245.64 3 0 1 8 32115.0 709.220 3 0 1 8 32654.3 747.304 2 0 -1 -8 31948.5 706.831 3 0 1 9 8.35669 19.7825 2 0 1 9 14.1394 20.7221 3 0 1 9 34.3555 21.6937 4 0 1 10 4392.48 203.309 3 0 1 10 3660.52 208.992 2 0 1 10 4021.19 188.923 4 0 1 11 2609.57 157.984 4 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3439.28 2 1 -3 0 197595. 3489.00 6 -1 3 -1 4509.94 150.629 6 -1 3 -1 4114.07 136.735 3 1 -3 1 4240.59 142.238 6 -1 3 -2 32320.4 653.327 2 1 -3 2 33860.1 666.839 2 1 -3 2 35056.0 700.395 4 -1 3 -3 248.657 33.0368 2 1 -3 3 191.957 30.3983 2 1 -3 3 250.777 39.7453 4 1 -3 4 36714.0 765.435 4 1 -3 4 36252.6 762.497 2 -1 3 -4 37616.4 761.249 2 -1 3 -4 36991.0 759.379 4 1 -3 5 9345.46 282.812 4 1 -3 5 9070.70 287.648 2 -1 3 -5 8839.63 267.238 4 -1 3 -6 3660.82 160.001 4 1 -3 6 3468.63 173.672 2 1 -3 6 3371.80 161.431 4 1 -3 7 1865.28 120.217 4 -1 3 -7 1787.64 114.216 4 1 -3 7 1719.50 128.904 2 -1 3 -7 1691.97 85.3300 3 -1 3 -7 1569.77 62.8933 1 1 -3 8 15832.9 478.548 2 1 -3 8 15384.9 439.294 4 -1 3 -8 16508.8 440.828 4 -1 3 -8 16051.1 373.846 3 1 -3 9 8297.16 335.214 2 1 -3 9 8348.89 302.213 4 -1 3 -9 8132.85 239.010 3 -1 3 -10 155.417 30.0212 3 1 -3 10 107.658 39.7446 2 1 -3 10 136.429 39.9477 4 1 -3 11 391.209 65.2885 4 1 -3 11 336.160 72.0361 2 -1 3 -11 437.374 52.0927 3 1 -3 12 11686.9 474.083 2 1 -3 12 11369.7 404.746 4 1 -3 13 13204.7 456.335 4 1 -3 13 13321.4 532.241 2 1 -3 14 14137.3 493.605 4 1 -3 14 14301.9 580.983 2 1 -3 15 7801.41 430.231 2 -1 2 16 1437.36 176.861 2 -1 2 15 78.9073 48.0812 2 -1 2 15-29.7387 37.9393 3 -1 2 14 2358.58 178.265 4 -1 2 14 2292.26 182.913 3 -1 2 14 2507.37 204.470 2 -1 2 13 5809.12 292.426 3 -1 2 13 6047.56 289.909 4 -1 2 13 5782.54 305.221 2 -1 2 12 1387.46 135.810 2 -1 2 12 1185.42 121.128 3 -1 2 12 1076.80 108.647 4 -1 2 11 7995.21 323.604 3 -1 2 11 8068.05 330.146 2 -1 2 10 51463.9 1130.15 3 -1 2 10 52302.5 1140.04 2 -1 2 9 27858.9 692.923 3 -1 2 9 29539.1 705.691 2 -1 2 8 6973.10 265.158 3 -1 2 8 7250.39 261.282 2 1 -2 -7 2176.62 131.856 3 -1 2 7 2048.18 126.324 3 -1 2 7 2134.36 121.127 2 1 -2 -7 2046.22 115.675 2 1 -2 -6 1395.80 98.4190 3 -1 2 6 1340.38 97.4829 3 -1 2 6 1256.81 83.3198 2 1 -2 -6 1230.09 80.4063 2 1 -2 -5 29507.2 627.835 2 -1 2 5 31754.1 640.837 2 -1 2 5 32382.9 686.216 3 1 -2 -5 33522.9 690.494 3 -1 2 4 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2 -4 8 81.4858 32.3865 4 -2 4 -8 86.0870 16.7880 3 2 -4 8 103.573 38.8204 2 -2 4 -9 397.751 37.6967 3 2 -4 9 369.744 60.3481 4 2 -4 9 363.437 72.4134 2 2 -4 10 14902.2 456.326 4 2 -4 10 15124.7 512.118 2 -2 4 -10 14245.8 337.255 3 2 -4 11 23552.6 633.320 4 2 -4 11 22411.1 694.953 2 2 -4 12 17734.4 622.069 2 2 -4 12 18599.5 552.799 4 2 -4 13 1829.20 152.463 4 2 -4 13 1678.83 180.257 2 2 -4 14 136.582 46.0960 4 2 -4 14 243.662 72.7989 2 2 -4 15 557.834 113.782 2 -2 3 16 945.464 133.290 3 -2 3 15 4098.30 273.767 3 -2 3 15 4230.06 268.989 4 -2 3 14 480.251 92.6556 3 -2 3 14 489.519 83.9012 4 -2 3 13 2294.00 186.831 3 -2 3 12 26.8361 33.5075 3 -2 3 12 5.92913 26.3087 2 -2 3 11 7091.23 303.160 2 -2 3 11 6179.64 301.199 3 -2 3 10 343.712 66.6039 3 -2 3 10 464.596 70.5265 2 -2 3 9 17325.8 518.626 3 -2 3 9 18104.7 488.132 2 -2 3 8 16013.7 422.189 2 -2 3 8 15954.3 468.240 3 2 -3 -8 14404.4 392.022 2 -2 3 7 27435.9 590.600 2 -2 3 7 25149.5 639.037 3 2 -3 -7 25303.1 565.682 2 -2 3 6 1323.99 81.4711 2 -2 3 6 1407.90 109.853 3 2 -3 -6 1201.98 73.5256 2 -2 3 5 2516.53 142.312 3 -2 3 5 2417.89 102.664 2 2 -3 -5 2288.88 92.3063 2 -2 3 4 539.801 61.4833 3 2 -3 -4 550.819 35.9209 2 -2 3 3 14555.7 366.124 3 2 -3 -3 13208.1 256.672 2 2 -3 -2 24359.1 585.364 5 -2 3 2 30776.9 606.294 3 2 -3 -1 63120.1 1222.72 5 -2 3 1 65590.0 1207.43 3 2 -3 0 42641.1 761.084 2 -2 3 0 42235.7 759.900 2 -2 3 0 43540.3 822.503 3 2 -3 1 80645.9 1420.37 2 2 -3 1 80870.5 1488.47 6 2 -3 1 76517.1 1439.63 3 -2 3 -1 84130.8 1443.25 3 -2 3 -1 78582.5 1419.98 2 -2 3 -2 48761.7 954.989 4 2 -3 2 51681.9 977.470 6 -2 3 -2 47853.3 915.509 2 2 -3 2 47871.6 920.484 2 -2 3 -2 49552.2 901.298 3 2 -3 3 45623.4 911.296 2 -2 3 -3 46275.6 917.621 4 -2 3 -3 46969.4 853.959 3 2 -3 3 48814.6 933.485 4 -2 3 -3 47315.7 909.990 2 2 -3 4 14406.5 370.472 2 -2 3 -4 14287.4 352.586 4 -2 3 -4 14154.3 291.440 3 -2 3 -4 14083.0 360.611 2 2 -3 4 13965.9 359.060 4 2 -3 5 6265.97 214.963 4 -2 3 -5 6401.98 208.495 4 2 -3 5 6497.49 234.987 2 -2 3 -5 6012.29 221.346 2 2 -3 6 42700.8 921.509 2 2 -3 6 44033.3 880.298 4 -2 3 -6 45296.3 866.668 4 -2 3 -6 41313.6 770.844 3 2 -3 7 10727.0 315.474 4 -2 3 -7 11107.2 307.030 4 2 -3 7 10551.9 354.596 2 -2 3 -7 10033.2 227.203 3 2 -3 8 7680.68 264.623 4 -2 3 -8 7242.67 244.454 4 -2 3 -8 7047.51 181.248 3 2 -3 8 7516.77 301.079 2 -2 3 -9 922.583 81.3361 4 2 -3 9 917.175 104.549 2 2 -3 9 947.987 89.6599 4 -2 3 -9 922.990 54.6256 3 -2 3 -10 21.3642 9.83606 3 2 -3 10 88.7733 33.5867 4 2 -3 10 42.8661 23.8304 2 2 -3 11 1680.03 129.869 4 2 -3 11 1592.82 156.885 2 2 -3 12 2184.49 152.966 4 2 -3 12 2200.89 200.881 2 2 -3 13 1420.63 128.274 4 2 -3 13 1554.85 170.583 2 2 -3 14 399.086 85.0924 2 2 -3 15 2551.21 238.286 2 -2 2 15 948.029 123.372 4 -2 2 14 333.653 71.3786 3 -2 2 14 339.578 72.3904 4 -2 2 13 8133.24 347.338 1 -2 2 13 7061.56 323.967 4 -2 2 13 7229.83 338.837 3 -2 2 12 251.525 61.0359 3 -2 2 12 205.379 50.4612 4 -2 2 11 5197.13 266.098 3 -2 2 11 6073.58 286.184 2 -2 2 10 36417.1 906.488 3 -2 2 10 42425.2 945.702 2 -2 2 9 22926.7 588.002 2 -2 2 9 19905.8 569.027 3 -2 2 8 20296.6 517.431 2 -2 2 8 18739.4 526.129 3 -2 2 7 3776.07 171.787 2 -2 2 7 3263.08 171.969 3 2 -2 -7 3416.27 150.889 2 2 -2 -6 2344.51 112.448 2 -2 2 6 2275.27 134.451 3 2 -2 -6 2535.91 140.619 3 -2 2 5 305.922 50.1771 3 2 -2 -5 300.165 34.8397 2 2 -2 -4 18883.9 397.155 2 -2 2 4 19777.8 462.288 3 2 -2 -3 38858.3 761.755 2 -2 2 3 50240.8 856.766 3 2 -2 -2 39059.3 752.997 5 -2 2 2 37770.5 759.838 3 2 -2 -1 442413. 7594.56 5 2 -2 -1 441367. 7526.25 2 -2 2 1 455154. 7595.76 3 2 -2 0 449.452 29.5768 2 -2 2 0 402.605 27.4266 2 -2 2 0 456.579 36.5128 3 2 -2 1 182772. 3130.98 6 -2 2 -1 177254. 3081.33 2 -2 2 -1 179268. 3068.25 3 2 -2 1 177106. 3083.38 2 2 -2 1 171464. 3067.02 3 -2 2 -2 84.8736 17.9010 4 2 -2 2 69.2551 18.9658 2 2 -2 2 127.163 13.9603 3 -2 2 -2 122.774 13.7980 3 -2 2 -2 91.5214 18.1285 2 2 -2 2 101.249 20.0414 6 -2 2 -3 589.144 44.4104 4 2 -2 3 576.523 52.9692 2 -2 2 -4 17510.6 378.894 4 2 -2 4 17962.9 429.267 2 2 -2 4 17107.3 386.090 4 -2 2 -5 6166.10 181.687 4 2 -2 5 6528.25 232.746 2 2 -2 5 6637.26 193.452 4 -2 2 -6 11313.2 270.085 4 2 -2 6 10516.7 268.788 4 2 -2 6 10511.2 327.397 2 -2 2 -6 8951.37 195.637 3 2 -2 7 9077.85 261.678 4 -2 2 -7 9120.77 256.841 4 2 -2 7 9493.68 321.862 2 -2 2 -7 8469.63 194.532 3 2 -2 8 402.103 48.5184 4 -2 2 -8 346.573 30.3770 3 2 -2 8 490.753 72.6127 2 2 -2 9 4850.48 246.065 2 2 -2 9 4853.67 194.823 4 -2 2 -9 4690.34 145.227 3 -2 2 -10 3252.85 123.304 3 2 -2 10 3460.88 168.414 4 2 -2 10 3384.92 214.743 2 2 -2 11 251.837 46.8844 4 2 -2 11 228.511 58.9443 2 2 -2 12 70.6394 29.4788 4 2 -2 12 111.478 48.8789 2 2 -2 13 2395.72 210.012 2 2 -2 14 4212.84 300.242 2 2 -2 15 4904.62 330.340 2 -2 1 16 104.850 49.2814 4 -2 1 15 143.724 52.9393 4 -2 1 14 269.260 65.5913 4 -2 1 13 607.560 76.9389 1 -2 1 13 487.026 86.0599 4 -2 1 12 259.006 51.8809 1 -2 1 12 188.868 52.7341 3 -2 1 12 148.966 46.7740 4 -2 1 11 8572.04 336.333 4 -2 1 11 9158.85 341.609 1 -2 1 11 8499.36 343.488 3 -2 1 10 3684.34 206.555 1 -2 1 10 3489.39 191.726 4 -2 1 10 3445.60 197.074 3 -2 1 9 10233.4 355.394 3 -2 1 8 14.0626 21.6006 3 -2 1 7 7299.09 264.671 3 2 -1 -7 6939.46 238.207 2 -2 1 6 225.234 41.5304 3 2 -1 -6 211.729 39.7988 3 2 -1 -6 192.755 32.9723 2 2 -1 -5 26272.1 563.635 2 -2 1 5 27087.5 600.284 3 -2 1 4 100909. 1795.36 3 2 -1 -4 95487.4 1752.53 2 -2 1 3 138631. 2461.47 3 2 -1 -2 49905.1 926.227 5 -2 1 2 53284.4 966.849 3 -2 1 1 231869. 3995.04 3 2 -1 0 22658.7 443.557 2 -2 1 0 22683.0 442.654 3 -2 1 0 22412.1 446.173 2 2 -1 1 4219.34 137.382 6 -2 1 -1 4371.79 141.570 1 2 -1 1 3991.85 126.481 2 2 -1 1 4161.22 106.284 3 2 -1 2 497.072 43.7300 6 2 -1 2 477.543 43.9837 2 -2 1 -2 502.768 36.3395 1 -2 1 -3 45182.5 809.346 4 2 -1 3 45300.1 883.142 2 -2 1 -4 151188. 2621.83 4 2 -1 4 152952. 2717.84 2 2 -1 4 153104. 2625.43 4 2 -1 5 85665.7 1469.20 4 2 -1 5 81931.7 1433.70 3 -2 1 -5 81954.9 1459.79 4 2 -1 5 83045.8 1572.42 2 -2 1 -6 18172.9 378.771 3 2 -1 6 19682.0 408.911 4 2 -1 6 20346.4 383.739 3 2 -1 6 20236.7 505.684 2 -2 1 -7 1773.90 75.3206 3 2 -1 7 1727.53 85.8056 4 2 -1 7 2027.96 79.3262 3 2 -1 7 1756.36 127.366 2 -2 1 -8 469.239 39.9978 3 2 -1 8 369.967 35.9124 3 2 -1 8 300.751 38.5661 4 2 -1 8 416.999 70.4867 2 -2 1 -9 589.565 49.8128 3 2 -1 9 628.588 85.1099 2 2 -1 9 536.043 55.2428 4 2 -1 10 5966.08 213.703 4 -2 1 -10 6005.79 195.472 3 2 -1 10 5990.78 289.586 2 2 -1 11 964.812 81.7178 4 2 -1 11 1021.18 119.947 2 2 -1 12 11988.3 354.658 4 2 -1 12 11221.8 458.713 2 2 -1 13 13088.3 517.415 2 2 -1 14 665.312 114.725 2 2 -1 15 1030.83 152.735 2 -2 0 16 2.18461 33.1068 4 -2 0 15 486.671 92.0038 4 -2 0 14 2075.94 180.029 4 -2 0 13 481.899 81.7454 4 -2 0 12 17238.1 464.036 1 -2 0 12 15667.4 521.880 4 -2 0 11 15217.6 501.169 4 -2 0 11 16724.1 452.176 1 -2 0 10 6180.98 242.482 1 -2 0 10 6387.13 283.064 4 -2 0 9 9657.46 314.011 1 -2 0 9 9314.47 342.261 4 -2 0 8 1778.06 125.626 4 -2 0 8 1751.78 118.018 1 -2 0 7 544.349 65.9107 4 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201.272 3 2 0 10 9423.64 267.146 4 -2 0 -10 8668.69 271.759 3 2 0 10 9593.16 377.397 2 2 0 10 9401.25 277.062 3 2 0 11 8663.59 375.393 2 2 0 11 9725.04 293.512 3 2 0 11 8964.02 274.989 4 2 0 12 8417.02 278.769 3 2 0 12 7563.15 365.538 2 2 0 13 4451.51 282.735 2 2 0 14 359.102 88.8186 2 2 0 15 1941.19 202.108 2 -2 -1 17 494.563 95.5783 4 -2 -1 16 5293.85 315.284 4 -2 -1 15 10361.7 449.238 4 -2 -1 14 4641.46 280.246 4 -2 -1 13 10995.2 443.193 4 -2 -1 12 14524.5 503.526 4 -2 -1 11 18799.2 577.308 4 -2 -1 10 651.430 95.1540 4 -2 -1 9 17041.2 504.385 4 -2 -1 8 11365.7 373.689 4 -2 -1 8 11489.3 330.105 1 -2 -1 7 26779.2 638.076 4 -2 -1 7 25359.8 583.683 1 2 1 -7 25753.0 609.825 3 -2 -1 6 374.890 57.5015 4 2 1 -6 445.360 55.6527 3 -2 -1 6 416.852 49.7272 1 2 1 -5 4018.90 180.766 1 2 1 -5 4076.81 170.724 3 -2 -1 5 4068.13 177.618 4 -2 -1 4 35098.1 751.706 4 2 1 -4 35762.7 750.496 1 -2 -1 3 3098.59 133.671 4 -2 -1 2 979.695 66.9008 4 -2 -1 1 48.1296 17.1743 4 -2 -1 0 33452.0 572.163 4 2 1 0 25559.6 556.613 4 -2 -1 -1 30709.8 561.596 4 2 1 1 28760.6 559.019 4 2 1 1 30459.2 615.624 2 2 1 1 30001.0 545.829 6 -2 -1 -2 12484.7 245.638 4 2 1 2 11824.0 309.110 2 -2 -1 -2 12357.0 255.196 6 2 1 2 12191.0 244.580 4 2 1 3 7031.11 200.100 3 2 1 3 7149.42 224.501 2 -2 -1 -3 7162.93 180.412 6 2 1 4 131.925 32.9560 2 2 1 4 69.1777 19.0126 3 2 1 5 4127.11 144.158 3 2 1 5 3344.83 88.2166 4 2 1 5 4255.18 179.059 2 2 1 6 35847.8 669.205 4 2 1 6 37676.8 742.177 3 2 1 6 37856.7 808.651 2 2 1 7 9665.18 223.342 4 2 1 7 9309.37 322.707 2 2 1 7 9818.84 277.054 3 2 1 8 30095.4 580.056 4 2 1 8 27485.6 713.227 2 2 1 8 28522.9 634.342 3 2 1 9 58774.8 1316.69 2 2 1 9 63804.6 1154.82 4 2 1 9 60943.3 1216.31 3 2 1 10 46395.2 904.901 4 2 1 10 46313.1 1086.61 2 2 1 10 47411.7 971.862 3 2 1 11 13486.2 347.314 4 2 1 11 14013.9 498.843 2 2 1 11 14792.2 408.133 3 2 1 12 7434.13 357.711 2 2 1 12 7914.21 284.416 3 2 1 13 3863.24 262.395 2 2 1 14-43.9928 47.2791 2 2 1 15 2686.13 236.692 2 -2 -2 17 64.7029 49.5461 4 -2 -2 16 1078.08 147.006 4 -2 -2 15 3710.82 261.284 4 -2 -2 14 9563.86 423.390 4 -2 -2 13 2446.11 195.339 4 -2 -2 12 91.7956 40.3414 4 -2 -2 11 148.726 51.3491 4 -2 -2 10 1812.98 155.480 4 -2 -2 9 72862.4 1521.31 4 -2 -2 8 66953.1 1394.91 4 2 2 -7 32600.3 753.293 1 -2 -2 7 31882.9 767.906 4 2 2 -6 24930.9 589.839 1 -2 -2 6 24308.5 611.430 4 2 2 -5 3215.71 150.718 1 -2 -2 5 2992.19 162.391 4 2 2 -4 19934.6 480.947 1 -2 -2 4 20678.4 502.760 4 -2 -2 3 11754.5 324.018 4 2 2 -3 11327.1 247.112 5 -2 -2 2 15774.0 333.847 5 -2 -2 2 17524.6 403.211 4 2 2 -1 25689.8 551.273 4 -2 -2 1 26268.5 556.084 4 -2 -2 0 65695.8 1235.41 4 2 2 0 68313.3 1237.19 4 -2 -2 -1 12452.2 287.512 4 2 2 1 11819.3 282.750 4 2 2 1 12500.3 323.737 2 -2 -2 -2 109.289 19.7115 4 2 2 2 86.6339 25.9514 2 2 2 2 158.044 22.8978 4 2 2 3 26416.6 548.226 3 -2 -2 -3 24764.3 450.540 6 2 2 3 26520.5 556.934 2 2 2 4 332.739 29.5083 4 2 2 4 348.720 44.8171 3 2 2 4 352.910 48.8940 2 -2 -2 -4 308.935 46.6758 2 2 2 5 12479.9 334.804 3 2 2 5 12073.0 354.408 2 2 2 5 11606.9 264.067 4 2 2 6 33131.5 657.259 4 2 2 6 35657.0 783.695 2 2 2 6 36035.0 742.353 3 2 2 7 11272.4 364.629 2 2 2 7 11686.3 337.467 3 2 2 8 23316.8 625.606 2 2 2 8 24912.2 586.567 3 2 2 9 151.332 48.0064 2 2 2 9 163.451 34.4099 3 2 2 9 189.799 28.5055 4 2 2 10 2236.50 104.092 4 2 2 10 2143.99 167.589 2 2 2 10 2214.42 143.169 3 2 2 11 30.8113 25.9650 3 2 2 11 51.0504 36.8637 2 2 2 12 2654.65 206.840 2 2 2 12 2798.57 168.756 3 2 2 13 2551.22 212.381 2 2 2 14 757.077 118.898 2 2 2 15 5812.57 354.876 2 -2 -3 17 3955.94 300.808 4 -2 -3 16 1468.92 177.380 4 -2 -3 15 707.496 117.899 4 -2 -3 14 4079.49 272.700 4 -2 -3 13 91.3217 42.6328 4 -2 -3 12 6852.63 339.484 4 -2 -3 11 37047.8 948.643 4 -2 -3 10 2153.17 170.170 4 -2 -3 9 46702.4 1089.33 4 2 3 -9 48069.5 1061.72 1 2 3 -8 1019.55 95.6855 1 -2 -3 8 1034.09 109.473 4 2 3 -7 400.350 55.8872 1 -2 -3 7 345.243 62.9735 4 -2 -3 6 2176.21 147.922 4 2 3 -6 2538.58 140.757 1 2 3 -5 306.596 35.6534 5 -2 -3 5 332.833 54.2534 4 2 3 -4 19638.8 427.296 5 -2 -3 4 19583.6 511.660 4 -2 -3 3 2866.99 150.348 4 -2 -3 2 46252.6 924.738 4 -2 -3 2 43766.5 855.252 5 -2 -3 1 58226.1 1099.17 5 2 3 -1 57706.2 1125.13 4 -2 -3 1 58476.1 1138.98 4 -2 -3 0 42084.1 843.226 4 2 3 0 41464.8 836.193 4 2 3 1 1456.03 85.9615 4 -2 -3 -1 1372.74 85.3316 4 2 3 1 1320.25 93.8808 2 2 3 2 3725.51 141.930 4 2 3 2 3921.55 168.363 2 -2 -3 -2 4285.60 155.170 4 2 3 3 2682.59 113.041 4 2 3 3 2589.04 137.255 2 2 3 3 2808.52 145.631 3 2 3 4 45555.3 973.918 3 2 3 4 44606.9 896.702 4 2 3 5 36363.8 731.553 4 2 3 5 38680.5 832.198 2 2 3 5 37560.3 814.598 3 2 3 6 6809.80 203.675 4 2 3 6 6986.49 268.080 2 2 3 6 7381.26 267.364 3 2 3 7 9665.83 260.624 4 2 3 7 9507.91 338.617 2 2 3 7 10033.5 335.269 3 2 3 8 53095.5 1024.67 3 2 3 8 49174.4 1043.76 2 2 3 9 2063.92 155.569 2 2 3 9 1530.68 123.628 3 2 3 10 4588.47 254.095 2 2 3 10 4696.72 228.539 3 2 3 11 7241.89 340.687 2 2 3 11 7226.23 303.015 3 2 3 12 1563.61 159.838 2 2 3 12 1696.13 140.252 3 2 3 13 16843.1 597.589 2 2 3 14 5182.33 323.238 2 2 3 15 3402.31 268.641 2 -2 -4 16 129.739 57.2474 4 -2 -4 15 6.60117 26.6493 4 -2 -4 14 2567.81 224.013 4 -2 -4 13 2729.91 227.348 4 -2 -4 12 2121.44 194.580 4 -2 -4 11 22305.0 697.987 4 -2 -4 10 20384.7 641.518 4 -2 -4 9 40453.3 1005.96 4 -2 -4 8 3880.88 231.036 4 -2 -4 7 31123.7 795.824 4 2 4 -6 3874.86 163.331 5 -2 -4 6 3966.41 217.100 4 -2 -4 5 3080.78 182.521 4 2 4 -5 3354.42 144.568 5 2 4 -4 24116.6 540.407 5 -2 -4 4 25402.5 630.415 4 -2 -4 3 8045.86 295.220 4 -2 -4 2 37837.7 794.534 5 -2 -4 2 40617.8 863.933 4 2 4 -1 19756.2 505.277 4 -2 -4 1 21908.4 531.457 4 -2 -4 1 21489.7 502.833 5 2 4 0 575.630 31.8284 6 2 4 0 675.242 66.7997 4 -2 -4 0 667.978 68.3344 4 -2 -4 -1 14.2077 16.2576 4 2 4 1 52.2467 22.0737 4 2 4 1 1.70053 17.5839 2 2 4 2 8429.14 258.328 4 2 4 2 8295.49 278.950 2 2 4 3 48505.0 974.731 4 2 4 3 48567.1 1011.10 2 2 4 3 50518.9 1054.09 3 2 4 4 55294.5 1128.08 2 2 4 4 53495.4 1073.30 4 2 4 4 56853.5 1167.17 3 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464.484 4 4 6 -1 13266.2 482.743 2 -4 -6 0 17100.3 522.091 4 4 6 0 15099.7 515.513 2 4 6 1 3583.64 220.696 2 -4 -6 -1 3872.34 216.818 4 4 6 2 4959.71 264.924 2 4 6 3 14447.4 517.878 3 4 6 3 13042.7 465.601 2 4 6 4 20510.3 647.002 3 4 6 4 19420.1 606.256 2 4 6 5 4821.46 280.708 3 4 6 5 4132.53 245.717 2 4 6 6 2028.18 174.288 2 4 6 6 2090.41 179.944 3 4 6 7 77.9839 37.7926 2 4 6 7 52.9636 31.9694 3 4 6 8 16.9553 27.7883 2 4 6 8 55.7868 33.1085 3 4 6 9 205.531 55.9573 2 4 6 9 246.875 62.4209 3 4 6 10 822.671 121.188 2 -4 -7 11 2666.51 254.329 4 -4 -7 10-8.35967 48.2837 4 -4 -7 9 165.328 69.4411 4 -4 -7 8 62.8487 45.8998 4 -4 -7 7 8622.38 432.361 4 -4 -7 6 23414.5 768.402 4 -4 -7 5 34888.6 965.741 4 -4 -7 4 7845.05 381.428 4 -4 -7 3 1280.22 141.780 4 -4 -7 2 164.748 51.2005 4 -4 -7 1 3789.20 239.180 4 4 7 -1 3382.03 230.603 2 -4 -7 0 534.328 92.2579 4 4 7 0 475.752 82.8781 2 4 7 1 79.1717 42.9678 2 4 7 2 1997.09 187.598 3 4 7 2 1662.53 156.891 2 4 7 3 13212.0 520.343 3 4 7 3 13109.1 476.508 2 4 7 4 5548.52 319.959 3 4 7 4 4873.98 277.169 2 4 7 5 5.97374 26.8525 3 4 7 5 41.3012 35.7662 2 4 7 6 2284.14 192.343 2 4 7 6 2375.91 205.553 3 4 7 7 144.378 55.5468 2 4 7 7 163.334 56.7723 3 4 7 8-42.6861 38.0517 2 4 7 8-10.9036 39.1401 3 4 7 9 3085.52 240.687 2 4 7 9 3667.13 268.983 3 -4 -8 9 298.408 91.6840 4 -4 -8 8 3129.53 267.648 4 -4 -8 7 8439.46 446.120 4 -4 -8 6 10186.1 484.805 4 -4 -8 5 5061.64 324.330 4 -4 -8 4 2759.37 230.044 4 -4 -8 3-22.8684 41.1750 4 -4 -8 2 2506.64 208.960 4 4 8 -2 2381.86 205.849 2 -4 -8 1 82.5773 41.4878 4 4 8 -1 91.4653 39.1113 2 4 8 0 13850.7 511.227 2 4 8 1 33097.6 960.709 3 4 8 1 30089.7 855.335 2 4 8 2 21599.1 726.062 3 4 8 2 19419.6 642.460 2 4 8 3 1828.21 192.920 3 4 8 3 1653.15 161.117 2 4 8 4 1436.04 170.050 3 4 8 4 1181.72 138.708 2 4 8 5 1394.22 166.128 3 4 8 5 1302.65 147.631 2 4 8 6 184.124 59.0569 2 4 8 6 183.484 62.6472 3 4 8 7 3083.80 256.445 3 -4 -9 7 373.273 99.8582 4 -4 -9 6 244.479 74.5691 4 -4 -9 5 1018.60 151.485 4 -4 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362.407 2 8 -9 8 12482.4 516.707 2 8 -9 9 3359.62 268.598 2 8 -9 10 516.865 113.366 2 -8 8 8 432.121 98.3934 3 -8 8 7-5.07944 31.2330 3 -8 8 6-31.3992 38.4046 3 -8 8 5 1842.17 181.852 3 -8 8 4 4884.85 290.997 3 -8 8 3 5576.70 302.798 3 -8 8 2 8793.33 379.116 3 -8 8 1 1632.36 147.863 3 -8 8 0 7127.98 364.841 5 -8 8 0 6994.59 310.518 3 -8 8 -1 6515.74 353.404 5 -8 8 -1 6026.53 276.784 3 -8 8 -2 911.694 129.353 5 -8 8 -2 898.373 98.8041 3 -8 8 -3 164.789 55.4865 5 -8 8 -4 194.947 68.1296 5 8 -8 4 118.087 41.3560 2 -8 8 -5 1122.50 153.720 5 -8 8 -5 1054.04 138.724 1 8 -8 5 1351.85 135.167 2 8 -8 6 2305.07 187.424 2 8 -8 7 213.553 64.9653 2 8 -8 8 146.387 62.7959 2 8 -8 9 3496.22 266.898 2 8 -8 10 48.4090 38.2851 2 -8 7 9 43.8060 40.6631 3 -8 7 8 33.1971 30.6789 3 -8 7 7 2010.59 197.597 3 -8 7 6 2044.18 192.834 3 -8 7 5 8198.12 391.185 3 -8 7 4 681.346 105.994 3 -8 7 3 4053.96 249.737 3 -8 7 2 7469.38 337.867 3 -8 7 1 5282.27 287.159 5 -8 7 1 4972.99 262.484 3 -8 7 0 4684.93 276.924 5 -8 7 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328.358 2 -8 6 -2 982.241 122.568 5 -8 6 -2 1103.59 149.326 1 8 -6 2 987.443 100.962 2 8 -6 3 10.4773 27.1031 2 -8 6 -3-37.1523 31.5959 1 8 -6 4 60.8717 32.0975 2 -8 6 -4 103.115 45.3886 1 -8 6 -5 1949.47 157.316 1 8 -6 5 1667.94 153.229 2 -8 6 -6 5028.01 246.747 1 8 -6 6 5287.23 293.551 2 8 -6 7 6559.69 344.019 2 8 -6 8 5646.89 327.706 2 8 -6 9 5601.53 343.255 2 8 -6 10 5177.81 336.259 2 -8 5 11 817.443 148.141 1 -8 5 10 9459.34 512.843 1 -8 5 9 18071.8 738.145 1 -8 5 8 10711.7 543.328 1 -8 5 7 13958.4 622.979 1 -8 5 6 117.563 57.4365 1 8 -5 -5 87.8263 24.3283 2 -8 5 5 106.975 48.2059 1 8 -5 -4 9823.24 320.544 2 -8 5 4 9433.35 479.680 1 8 -5 -3 549.446 68.4007 2 -8 5 3 403.692 83.8827 1 8 -5 -2 2661.96 154.728 2 -8 5 2 2620.55 172.080 5 -8 5 2 2423.95 222.077 1 8 -5 -1 4136.94 203.781 2 -8 5 1 3668.99 263.211 1 -8 5 1 4040.93 224.001 5 8 -5 0 1529.79 123.716 2 -8 5 0 1635.70 139.703 5 -8 5 0 1175.04 142.131 1 -8 5 -1 4179.43 236.145 5 -8 5 -1 3751.85 249.778 1 8 -5 1 4246.19 219.112 2 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476.549 2 8 -3 6 1469.23 156.566 2 8 -3 7 971.714 128.260 2 8 -3 8 73.7030 39.0929 2 8 -3 9 2203.01 213.642 2 8 -3 10 2066.25 212.224 2 -8 2 13 2427.91 229.962 1 -8 2 12 1902.17 202.056 1 -8 2 11 119.246 55.8482 4 -8 2 11 37.3976 45.8900 1 -8 2 10 3279.82 261.134 1 -8 2 10 3481.09 257.185 4 -8 2 9 368.619 84.6908 4 -8 2 9 355.902 86.3577 1 -8 2 8 4079.63 283.576 1 -8 2 7 6392.53 354.425 1 -8 2 6 4081.98 274.715 1 8 -2 -6 4625.60 257.834 2 8 -2 -5 386.998 72.5138 2 -8 2 5 489.232 89.0787 1 -8 2 4 1373.65 152.784 1 8 -2 -4 1422.93 131.710 2 8 -2 -3 1740.42 145.941 2 -8 2 3 1871.39 172.134 1 -8 2 2 95.3422 23.9229 5 8 -2 -2 137.276 49.6741 2 -8 2 2 70.0633 39.2942 1 -8 2 1 3975.48 177.119 5 8 -2 -1 4074.86 230.153 2 -8 2 1 4061.42 244.826 1 8 -2 0 3968.18 230.589 2 8 -2 1 21956.0 639.728 2 8 -2 2 38571.1 959.060 2 8 -2 3 16747.0 559.619 2 -8 2 -3 17295.5 423.828 4 8 -2 4 9751.61 413.342 2 8 -2 5 214.954 61.7360 2 8 -2 6 494.464 93.7648 2 8 -2 7-26.4054 43.4131 2 8 -2 8 21.0598 35.8007 2 8 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334.390 2 -8 0 4 118.572 48.0942 4 8 0 -4 83.3799 28.1468 2 -8 0 3 9583.82 384.141 4 8 0 -3 11879.2 443.583 2 -8 0 2 8298.14 328.693 4 8 0 -2 7552.58 348.868 2 -8 0 1 6780.94 282.656 4 8 0 -1 5761.86 303.591 2 8 0 0 15636.6 546.782 2 -8 0 0 16465.0 471.999 4 8 0 1 14275.9 521.454 2 -8 0 -1 16217.4 440.342 4 8 0 2 3463.01 234.861 2 8 0 3 726.051 107.768 2 8 0 4 1196.40 143.601 2 8 0 5 5571.27 326.314 2 8 0 6 26288.9 812.814 2 8 0 7 12942.2 536.976 2 8 0 8 2716.19 235.806 2 -8 -1 11 6691.21 400.389 4 -8 -1 10 6195.15 375.263 4 -8 -1 9 9058.48 449.090 4 -8 -1 8 1754.20 181.692 4 -8 -1 7 256.510 69.4423 4 -8 -1 6 3879.54 257.839 4 -8 -1 5 3157.53 221.268 4 -8 -1 4 23308.9 691.347 4 8 1 -4 23944.8 730.947 2 -8 -1 3 29235.9 774.132 4 8 1 -3 28195.8 814.593 2 -8 -1 2 1535.99 136.055 4 8 1 -2 1713.37 163.806 2 -8 -1 1 782.889 91.6080 4 8 1 -1 737.817 108.374 2 8 1 0 6.16489 31.5643 2 -8 -1 0 4.45917 18.1135 4 8 1 1 3803.24 249.552 2 8 1 2 6477.57 341.256 2 8 1 3 910.619 125.601 2 8 1 4 25583.7 790.406 2 8 1 5 11338.5 487.573 2 8 1 6 1580.41 178.321 2 8 1 7 70.2173 40.9042 2 -8 -2 10 1672.88 191.162 4 -8 -2 9 491.421 100.664 4 -8 -2 8 171.018 64.4927 4 -8 -2 7 563.111 98.6705 4 -8 -2 6 8935.64 410.331 4 -8 -2 5 23191.8 707.441 4 -8 -2 4 24332.9 712.558 4 8 2 -4 25488.5 782.847 2 -8 -2 3 12517.6 459.271 4 8 2 -3 14558.8 539.596 2 -8 -2 2 2846.50 189.039 4 8 2 -2 2476.89 206.726 2 -8 -2 1 634.083 84.3824 4 8 2 -1 654.767 107.157 2 8 2 0 83.7635 42.6205 2 -8 -2 0 18.8666 17.1566 4 8 2 1 1084.10 137.721 2 8 2 2-13.6694 35.3475 2 8 2 3 1439.14 161.536 2 8 2 4 3838.38 269.754 2 8 2 5 171.998 60.4734 2 8 2 6 75.8811 51.5078 2 -8 -3 9 2194.26 220.321 4 -8 -3 8 4468.08 304.911 4 -8 -3 7 11233.1 490.616 4 -8 -3 6 8100.35 397.179 4 -8 -3 5 3162.58 232.284 4 -8 -3 4 2784.42 210.873 4 8 3 -4 2709.11 230.131 2 -8 -3 3 78.0424 46.8971 4 8 3 -3 106.760 47.0539 2 -8 -3 2 748.387 99.7889 4 8 3 -2 741.099 117.455 2 -8 -3 1-12.6936 20.3177 4 8 3 -1-6.59544 35.5574 2 8 3 0 13671.5 545.773 2 8 3 1 14707.8 571.094 2 8 3 2 17253.7 631.083 2 8 3 3 5337.33 330.112 2 8 3 4 410.852 92.3458 2 8 3 5 1521.74 174.675 2 -8 -4 9 6587.56 401.545 4 -8 -4 8 4858.26 333.300 4 -8 -4 7 4467.27 312.017 4 -8 -4 6 380.601 86.5370 4 -8 -4 5 499.529 98.3103 4 8 4 -5 769.997 133.776 2 -8 -4 4 253.250 68.3720 4 8 4 -4 398.751 94.1568 2 -8 -4 3 128.432 45.2578 4 8 4 -3 298.860 83.7055 2 -8 -4 2 3106.44 215.810 4 8 4 -2 3558.24 263.990 2 8 4 -1 7863.05 409.416 2 8 4 0 9031.54 443.161 2 8 4 1 4042.14 287.226 2 8 4 2 2341.10 216.584 2 8 4 3 1323.58 166.088 2 -8 -5 7 110.772 47.1502 4 -8 -5 6-25.8288 38.7698 4 -8 -5 5 40.3623 37.2960 4 -8 -5 4 2807.30 227.474 4 -8 -5 3 2066.41 188.997 4 8 5 -3 1945.02 202.570 2 8 5 -2 2778.55 241.766 2 8 5 -1 1869.02 199.767 2 -8 -6 6 637.207 121.341 4 -8 -6 5 1042.99 150.124 4 -9 11 2 3935.34 282.758 3 -9 10 4 88.4943 46.0598 3 -9 10 3 752.374 124.781 3 -9 10 2 58.2178 40.3573 3 -9 10 1 388.547 81.8373 3 -9 10 -1 983.680 151.840 5 -9 10 -2 2051.59 220.928 5 -9 10 -3 1707.79 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