# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 293.56 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7701 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 27.0933 _cell_length_b 4.5768 _cell_length_c 9.9009 _cell_angle_alpha 90.000 _cell_angle_beta 96.389 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 570.96 -0.61 0.41 o 4 0 0 375.55 383.94 6.42 o 6 0 0 2334.32 2470.87 89.91 o 8 0 0 2009.09 2065.34 26.38 o 10 0 0 5808.63 6030.72 73.18 o 12 0 0 2707.51 2659.52 34.71 o 14 0 0 5286.67 5546.29 139.33 o 16 0 0 374.81 431.84 22.04 o 18 0 0 393.64 367.52 10.21 o 20 0 0 773.89 760.94 32.54 o 22 0 0 6165.23 5733.65 120.12 o 24 0 0 7596.85 7243.27 146.69 o 26 0 0 340.98 307.12 25.18 o 28 0 0 1009.01 997.17 46.12 o 30 0 0 1832.28 1830.32 67.30 o 32 0 0 127.50 123.39 21.34 o 34 0 0 321.86 262.40 30.34 o 1 1 0 213.10 191.38 3.60 o 3 1 0 7200.13 7070.69 53.80 o 5 1 0 8290.59 8620.16 65.05 o 7 1 0 7816.49 7802.32 67.04 o 9 1 0 8925.01 9262.15 74.93 o 11 1 0 759.31 905.29 21.32 o 13 1 0 13.81 7.30 2.96 o 15 1 0 3579.93 3611.64 42.73 o 17 1 0 2029.21 1929.89 44.72 o 19 1 0 9235.32 8701.10 88.29 o 21 1 0 107.32 90.98 10.67 o 23 1 0 1123.35 1092.31 42.52 o 25 1 0 4.14 5.70 6.83 o 27 1 0 725.02 724.49 27.45 o 29 1 0 1394.61 1427.78 41.02 o 31 1 0 1574.17 1564.30 44.89 o 33 1 0 206.84 136.85 18.32 o 0 2 0 19664.68 20384.70 173.32 o 2 2 0 1523.07 1337.70 14.30 o 4 2 0 825.43 859.74 13.64 o 6 2 0 20.01 19.52 2.93 o 8 2 0 1.99 1.93 1.52 o 10 2 0 6335.42 6522.69 55.34 o 12 2 0 11596.79 12089.94 108.51 o 14 2 0 169.00 119.80 5.26 o 16 2 0 339.71 328.46 14.30 o 18 2 0 192.52 209.66 18.32 o 20 2 0 743.27 754.99 19.37 o 22 2 0 1020.48 1020.86 28.85 o 24 2 0 3336.48 3054.81 60.21 o 26 2 0 199.23 237.34 21.34 o 28 2 0 224.81 265.03 19.02 o 30 2 0 140.86 141.15 15.87 o 32 2 0 438.69 461.08 26.41 o 1 3 0 176.02 215.19 8.69 o 3 3 0 2037.07 2064.80 21.78 o 5 3 0 3663.39 3651.99 32.83 o 7 3 0 2605.92 2619.59 29.40 o 9 3 0 2487.96 2434.84 28.22 o 11 3 0 834.96 897.79 15.46 o 13 3 0 20.83 22.94 3.40 o 15 3 0 1162.36 1124.22 22.34 o 17 3 0 959.49 940.57 51.11 o 19 3 0 2373.34 2423.26 49.14 o 21 3 0 138.83 124.09 12.37 o 23 3 0 57.93 72.28 10.63 o 25 3 0 69.84 94.36 19.62 o 27 3 0 1184.86 1089.02 37.15 o 29 3 0 956.66 1096.90 38.71 o 0 4 0 407.12 451.77 27.31 o 2 4 0 1108.65 1101.30 22.49 o 4 4 0 441.98 437.23 12.29 o 6 4 0 134.62 130.28 11.66 o 8 4 0 205.33 187.92 8.97 o 10 4 0 712.36 751.23 17.20 o 12 4 0 7644.58 7913.49 76.03 o 14 4 0 3.55 6.05 4.32 o 16 4 0 110.89 105.84 12.43 o 18 4 0 516.43 546.46 33.44 o 20 4 0 103.30 137.85 14.66 o 22 4 0 347.45 357.98 21.73 o 24 4 0 357.53 381.06 22.75 o 1 5 0 10.05 21.20 7.35 o 3 5 0 772.06 802.66 38.76 o 5 5 0 276.91 321.10 19.70 o 7 5 0 2396.20 2391.79 43.50 o 9 5 0 20.80 23.13 6.57 o 11 5 0 81.81 79.11 9.57 o 13 5 0 360.18 336.31 21.35 o 15 5 0 879.65 935.47 34.09 o 17 5 0 635.63 713.65 30.24 o -33 1 1 168.34 187.10 17.95 o -31 1 1 199.64 217.88 18.11 o -29 1 1 19.09 15.10 7.08 o -27 1 1 89.16 95.44 11.91 o -25 1 1 16.85 20.64 6.63 o -23 1 1 178.10 204.25 21.42 o -21 1 1 502.03 504.07 14.36 o -19 1 1 620.82 638.92 15.54 o -17 1 1 208.81 219.56 19.25 o -15 1 1 1953.20 2241.88 36.16 o -13 1 1 1053.67 1126.81 22.27 o -11 1 1 528.25 657.26 15.51 o -9 1 1 0.50 -2.74 1.85 o -7 1 1 981.59 1005.07 14.11 o -5 1 1 5.74 6.01 1.53 o -3 1 1 9329.14 9877.51 73.85 o -1 1 1 10434.71 11015.63 81.40 o 1 1 1 3741.10 3971.59 32.88 o 3 1 1 961.95 1053.41 11.98 o 5 1 1 819.46 834.44 14.49 o 7 1 1 169.86 199.50 4.78 o 9 1 1 1610.12 1655.40 17.32 o 11 1 1 7494.87 8474.58 60.37 o 13 1 1 450.86 471.98 9.87 o 15 1 1 18.02 6.01 4.50 o 17 1 1 420.29 438.58 13.79 o 19 1 1 466.26 456.50 19.91 o 21 1 1 53.92 58.27 8.64 o 23 1 1 1544.64 1470.03 120.08 o 25 1 1 437.88 446.45 20.81 o 27 1 1 2.88 -0.89 5.17 o 29 1 1 74.01 89.74 33.32 o 31 1 1 27.66 36.69 9.29 o 33 1 1 136.60 135.70 16.36 o -32 2 1 3.32 18.32 11.08 o -30 2 1 13.95 7.05 6.66 o -28 2 1 23.12 28.89 8.23 o -26 2 1 569.32 512.96 27.68 o -24 2 1 188.33 141.37 10.07 o -22 2 1 1194.92 1140.64 29.75 o -20 2 1 177.37 137.97 12.76 o -18 2 1 227.96 262.06 13.02 o -16 2 1 0.32 1.22 3.64 o -14 2 1 303.61 322.03 13.35 o -12 2 1 217.40 221.39 9.11 o -10 2 1 385.64 391.38 10.34 o -8 2 1 249.01 249.89 6.06 o -6 2 1 63.47 72.84 3.43 o -4 2 1 1862.22 2032.45 18.63 o -2 2 1 519.95 582.28 7.62 o 0 2 1 544.46 646.73 8.31 o 2 2 1 33.48 44.28 3.30 o 4 2 1 145.81 168.73 6.26 o 6 2 1 214.58 253.03 6.79 o 8 2 1 48.27 47.02 3.52 o 10 2 1 367.44 412.57 9.03 o 12 2 1 57.66 88.84 4.67 o 14 2 1 0.34 3.71 1.90 o 16 2 1 90.98 98.96 6.80 o 18 2 1 70.46 65.50 5.52 o 20 2 1 20.34 11.30 4.01 o 22 2 1 22.06 21.77 11.53 o 24 2 1 52.39 36.71 8.35 o 26 2 1 206.84 185.89 15.89 o 28 2 1 10.53 5.31 6.33 o 30 2 1 22.31 35.79 9.81 o 32 2 1 52.05 60.48 11.91 o -29 3 1 37.60 14.95 8.24 o -27 3 1 117.27 92.04 13.38 o -25 3 1 93.74 93.36 12.08 o -23 3 1 1.42 5.00 7.85 o -21 3 1 121.38 121.13 12.14 o -19 3 1 34.64 31.14 7.08 o -17 3 1 74.14 68.34 9.05 o -15 3 1 644.68 612.21 16.25 o -13 3 1 1287.18 1284.21 25.09 o -11 3 1 468.05 496.07 14.22 o -9 3 1 0.90 5.51 2.48 o -7 3 1 9.00 8.98 2.42 o -5 3 1 22.68 36.39 3.63 o -3 3 1 1140.50 1342.43 17.05 o -1 3 1 1630.87 1938.04 19.30 o 1 3 1 104.54 110.29 4.80 o 3 3 1 0.02 -0.84 1.53 o 5 3 1 471.39 520.03 11.52 o 7 3 1 473.21 512.21 11.56 o 9 3 1 231.15 241.43 8.83 o 11 3 1 503.02 470.52 11.41 o 13 3 1 353.70 359.26 10.12 o 15 3 1 342.54 371.00 12.64 o 17 3 1 428.88 412.50 14.04 o 19 3 1 97.04 93.49 10.94 o 21 3 1 6.14 5.54 5.14 o 23 3 1 597.44 562.26 19.52 o 25 3 1 138.90 105.12 13.56 o 27 3 1 8.33 7.86 6.34 o 29 3 1 26.68 33.47 10.26 o -26 4 1 63.40 78.83 18.97 o -24 4 1 173.94 204.68 17.57 o -22 4 1 197.75 191.36 24.57 o -20 4 1 47.71 46.30 9.88 o -18 4 1 122.77 130.30 13.48 o -16 4 1 387.78 383.49 16.08 o -14 4 1 0.01 -0.41 3.33 o -12 4 1 1139.68 1227.71 22.85 o -10 4 1 184.50 178.79 10.24 o -8 4 1 3.56 4.17 3.18 o -6 4 1 205.85 186.90 8.88 o -4 4 1 110.15 106.51 6.99 o -2 4 1 29.25 17.52 4.28 o 0 4 1 16.01 10.19 6.33 o 2 4 1 571.89 561.13 13.94 o 4 4 1 587.36 594.00 18.05 o 6 4 1 546.87 541.59 28.51 o 8 4 1 46.53 59.27 5.94 o 10 4 1 568.21 598.89 20.63 o 12 4 1 135.91 154.76 17.84 o 14 4 1 6.98 2.20 5.81 o 16 4 1 339.06 323.42 19.16 o 18 4 1 278.74 245.60 40.48 o 20 4 1 103.54 107.71 13.47 o 22 4 1 43.37 72.10 12.43 o 24 4 1 10.55 4.81 7.62 o -19 5 1 21.23 8.37 9.81 o -17 5 1 58.15 65.18 22.28 o -15 5 1 76.19 34.18 15.21 o -13 5 1 0.00 3.81 6.03 o -11 5 1 557.45 541.55 29.63 o -9 5 1 40.65 53.13 8.30 o -7 5 1 230.82 234.91 17.51 o -5 5 1 21.57 16.45 10.88 o -3 5 1 106.55 96.79 12.63 o -1 5 1 293.65 285.99 18.96 o 1 5 1 8.58 2.69 5.25 o 3 5 1 31.87 49.41 9.76 o 5 5 1 55.37 45.42 7.61 o 7 5 1 718.40 746.44 23.43 o 9 5 1 8.35 11.41 5.42 o 11 5 1 662.35 672.59 22.34 o 13 5 1 139.59 133.90 15.66 o 15 5 1 304.29 316.38 75.43 o 17 5 1 4.78 6.96 8.44 o -34 0 2 1788.43 1908.49 73.27 o -32 0 2 711.54 735.02 42.27 o -30 0 2 428.25 452.43 31.64 o -28 0 2 2629.04 2592.00 77.68 o -26 0 2 420.89 363.55 25.68 o -24 0 2 1943.39 1886.82 59.28 o -22 0 2 41.28 30.42 9.49 o -20 0 2 414.76 431.74 14.25 o -18 0 2 3800.18 3977.55 54.90 o -16 0 2 769.29 613.56 17.42 o -14 0 2 2025.35 1846.38 29.95 o -12 0 2 8036.28 8389.10 140.23 o -10 0 2 5112.38 5515.16 95.67 o -4 0 2 86178.19 81754.95 1150.49 o 0 0 2 62.38 86.01 3.36 o 2 0 2 846.35 877.73 13.97 o 4 0 2 200.44 208.11 6.85 o 6 0 2 8613.15 8651.66 137.54 o 8 0 2 2360.51 2359.23 58.79 o 10 0 2 10577.00 10649.34 154.14 o 12 0 2 2477.17 2728.72 60.35 o 14 0 2 31.59 7.85 6.79 o 16 0 2 1417.19 1453.20 44.16 o 18 0 2 8101.47 7796.28 146.20 o 20 0 2 12648.04 11931.09 210.64 o 22 0 2 3561.40 3596.94 89.46 o 24 0 2 954.88 1007.89 43.91 o 26 0 2 6.36 9.40 7.44 o 28 0 2 174.22 176.46 22.08 o 30 0 2 1422.59 1479.86 60.75 o 32 0 2 1035.02 1030.13 52.17 o -33 1 2 198.91 197.42 18.33 o -31 1 2 1387.97 1402.36 41.66 o -29 1 2 67.14 68.86 17.83 o -27 1 2 849.40 769.41 28.03 o -25 1 2 61.21 56.52 9.39 o -23 1 2 7195.29 6878.03 95.95 o -21 1 2 1595.93 1658.84 28.37 o -19 1 2 1818.84 1861.41 37.64 o -17 1 2 21.99 25.49 4.76 o -15 1 2 526.45 588.28 16.21 o -13 1 2 4378.88 4583.62 83.53 o -11 1 2 3950.21 3981.48 63.13 o -9 1 2 4373.09 4395.31 65.13 o -7 1 2 2431.35 2342.00 32.28 o -5 1 2 3177.80 3381.69 25.84 o -3 1 2 9796.91 10041.49 67.53 o -1 1 2 34078.42 33605.52 214.49 o 1 1 2 25108.26 25326.79 162.34 o 3 1 2 507.69 423.53 6.52 o 5 1 2 6257.63 6376.52 45.70 o 7 1 2 189.76 202.96 4.65 o 9 1 2 33.62 48.43 2.57 o 11 1 2 12114.91 12644.84 87.03 o 13 1 2 1693.58 1578.04 23.80 o 15 1 2 4664.23 4591.49 51.42 o 17 1 2 851.40 848.34 16.98 o 19 1 2 101.96 104.41 7.90 o 21 1 2 157.15 136.74 11.55 o 23 1 2 3384.83 3251.78 60.48 o 25 1 2 1375.26 1336.22 42.11 o 27 1 2 1827.12 1759.19 45.13 o 29 1 2 319.90 354.27 21.51 o 31 1 2 61.60 58.83 24.69 o 33 1 2 158.78 132.92 17.13 o -32 2 2 340.32 389.14 24.26 o -30 2 2 272.29 350.05 22.00 o -28 2 2 1815.03 1818.21 46.65 o -26 2 2 261.54 271.69 21.59 o -24 2 2 623.97 646.13 33.53 o -22 2 2 1399.60 1445.31 33.83 o -20 2 2 968.22 1006.76 29.64 o -18 2 2 1506.48 1485.36 32.20 o -16 2 2 2491.36 2492.89 44.73 o -14 2 2 2564.91 2561.52 42.55 o -12 2 2 1373.83 1258.98 20.68 o -10 2 2 36.16 32.01 3.81 o -8 2 2 1425.79 1379.96 18.34 o -6 2 2 1635.89 1484.60 18.66 o -4 2 2 10718.48 11123.51 87.10 o -2 2 2 282.86 189.97 4.88 o 0 2 2 4933.24 5186.73 46.52 o 2 2 2 0.82 0.65 1.80 o 4 2 2 991.48 986.69 14.72 o 6 2 2 3814.46 3800.80 36.65 o 8 2 2 12765.65 13328.27 154.64 o 10 2 2 272.77 178.46 6.30 o 12 2 2 76.56 61.65 6.20 o 14 2 2 67.26 67.30 5.87 o 16 2 2 563.97 579.70 20.69 o 18 2 2 2742.66 2610.96 33.01 o 20 2 2 3508.40 3404.45 40.48 o 22 2 2 164.35 208.73 15.27 o 24 2 2 543.81 484.06 22.48 o 26 2 2 56.91 38.85 9.11 o 28 2 2 377.15 410.53 35.32 o 30 2 2 2773.39 2965.61 66.45 o -29 3 2 166.31 167.79 17.31 o -27 3 2 89.09 105.56 18.89 o -25 3 2 339.99 345.44 19.75 o -23 3 2 409.74 420.79 20.15 o -21 3 2 377.99 397.66 18.92 o -19 3 2 1394.14 1389.53 35.08 o -17 3 2 159.87 165.75 16.52 o -15 3 2 2351.22 2398.12 35.88 o -13 3 2 3224.20 3128.76 36.76 o -11 3 2 5962.67 5941.45 79.82 o -9 3 2 1055.65 1020.27 17.70 o -7 3 2 1124.53 1123.10 18.38 o -5 3 2 0.81 4.14 2.19 o -3 3 2 0.04 0.40 2.17 o -1 3 2 968.02 939.33 16.65 o 1 3 2 3474.48 3339.09 32.97 o 3 3 2 1424.44 1394.23 28.84 o 5 3 2 1657.10 1569.12 22.53 o 7 3 2 408.10 432.70 12.53 o 9 3 2 12.27 18.88 3.44 o 11 3 2 5811.31 5884.13 56.35 o 13 3 2 1041.18 1069.12 18.50 o 15 3 2 2002.14 1895.22 49.97 o 17 3 2 213.78 222.15 14.30 o 19 3 2 7.31 20.13 4.47 o 21 3 2 5.07 16.73 4.39 o 23 3 2 1876.10 1929.59 48.48 o 25 3 2 1070.20 1086.21 39.82 o 27 3 2 616.17 676.35 44.73 o 29 3 2 126.33 128.06 18.60 o -24 4 2 338.66 373.45 23.20 o -22 4 2 579.44 626.61 27.66 o -20 4 2 514.80 525.53 19.71 o -18 4 2 60.21 44.38 9.59 o -16 4 2 4380.49 4450.46 51.78 o -14 4 2 43.25 42.59 5.79 o -12 4 2 241.08 248.08 10.54 o -10 4 2 31.61 24.50 4.47 o -8 4 2 116.11 124.99 7.71 o -6 4 2 1201.73 1207.13 21.75 o -4 4 2 540.39 498.38 18.59 o -2 4 2 1101.06 1114.90 23.95 o 0 4 2 1187.35 1149.71 21.30 o 2 4 2 210.60 230.53 9.91 o 4 4 2 1009.14 986.34 29.28 o 6 4 2 1406.84 1457.30 24.13 o 8 4 2 5909.95 5948.15 72.33 o 10 4 2 363.74 416.68 15.51 o 12 4 2 348.72 359.64 14.74 o 14 4 2 72.36 79.70 11.25 o 16 4 2 40.70 50.34 9.86 o 18 4 2 739.60 746.68 28.84 o 20 4 2 536.38 559.32 25.58 o 22 4 2 1096.63 1174.31 34.42 o 24 4 2 168.49 163.24 17.60 o -17 5 2 37.10 20.94 9.14 o -15 5 2 16.53 14.48 16.48 o -13 5 2 49.48 66.89 8.77 o -11 5 2 1528.55 1489.57 32.64 o -9 5 2 265.21 285.99 35.16 o -7 5 2 466.89 447.45 22.85 o -5 5 2 46.55 38.75 9.39 o -3 5 2 2.49 5.43 5.76 o -1 5 2 1502.24 1510.99 41.75 o 1 5 2 35.47 40.38 9.31 o 3 5 2 1403.32 1396.52 43.30 o 5 5 2 120.62 148.42 20.03 o 7 5 2 47.96 53.87 8.34 o 9 5 2 421.85 434.31 18.37 o 11 5 2 835.52 858.74 32.93 o 13 5 2 1691.39 1740.91 48.31 o 15 5 2 45.02 46.62 11.05 o 17 5 2 365.69 407.89 25.02 o -33 1 3 0.36 3.04 7.00 o -31 1 3 0.30 -0.31 5.77 o -29 1 3 59.92 50.65 10.15 o -27 1 3 197.66 155.26 14.13 o -25 1 3 150.80 148.58 18.11 o -23 1 3 64.96 88.30 8.14 o -21 1 3 121.38 130.13 8.35 o -19 1 3 298.80 306.00 13.14 o -17 1 3 258.76 271.70 11.77 o -15 1 3 2.79 11.91 3.64 o -13 1 3 64.80 48.02 7.24 o -11 1 3 1427.06 1628.43 27.54 o -9 1 3 465.52 528.99 15.73 o -7 1 3 263.40 303.22 6.23 o -5 1 3 373.41 415.91 6.51 o -3 1 3 625.76 640.87 11.63 o -1 1 3 304.53 297.71 6.20 o 1 1 3 2784.31 2918.00 21.77 o 3 1 3 1658.70 1758.28 18.22 o 5 1 3 605.24 633.95 8.33 o 7 1 3 4761.80 5300.88 37.19 o 9 1 3 516.15 545.99 10.59 o 11 1 3 356.03 402.56 7.29 o 13 1 3 192.26 189.90 5.56 o 15 1 3 20.53 26.00 3.94 o 17 1 3 43.20 38.27 6.20 o 19 1 3 1662.79 1629.30 35.15 o 21 1 3 478.97 456.11 19.00 o 23 1 3 341.28 353.41 33.73 o 25 1 3 15.53 16.75 6.47 o 27 1 3 57.39 47.21 9.51 o 29 1 3 59.40 72.24 11.76 o 31 1 3 305.00 305.42 36.18 o -32 2 3 15.52 20.48 8.79 o -30 2 3 2.85 7.22 7.08 o -28 2 3 52.71 43.42 16.56 o -26 2 3 993.69 985.34 34.83 o -24 2 3 246.65 229.30 22.69 o -22 2 3 759.82 707.68 22.93 o -20 2 3 18.18 19.51 5.52 o -18 2 3 22.36 24.65 5.69 o -16 2 3 625.06 645.00 19.43 o -14 2 3 127.81 139.48 14.92 o -12 2 3 1597.46 1594.11 44.66 o -10 2 3 25.36 23.20 3.14 o -8 2 3 262.24 281.07 8.20 o -6 2 3 87.99 87.53 4.40 o -4 2 3 4185.91 4730.23 71.46 o -2 2 3 52.64 43.85 3.76 o 0 2 3 5488.64 5912.44 52.67 o 2 2 3 192.27 239.30 7.25 o 4 2 3 23.80 41.23 3.67 o 6 2 3 1.05 1.68 1.84 o 8 2 3 349.87 376.62 9.26 o 10 2 3 248.62 270.57 7.15 o 12 2 3 191.62 217.96 11.15 o 14 2 3 0.53 -0.34 2.12 o 16 2 3 30.36 40.65 4.63 o 18 2 3 618.70 581.86 18.53 o 20 2 3 14.85 10.22 3.39 o 22 2 3 116.96 94.09 8.99 o 24 2 3 0.01 1.39 3.93 o 26 2 3 70.61 70.90 11.46 o 28 2 3 62.21 68.75 17.95 o 30 2 3 0.09 12.55 7.34 o -29 3 3 108.15 105.07 22.98 o -25 3 3 13.43 15.36 7.57 o -23 3 3 14.94 3.46 5.99 o -21 3 3 409.64 459.60 20.22 o -19 3 3 1145.82 1218.36 26.78 o -17 3 3 954.40 935.13 22.33 o -15 3 3 2.39 6.26 3.64 o -13 3 3 264.87 237.12 9.17 o -11 3 3 87.68 95.63 6.16 o -9 3 3 213.85 224.30 8.38 o -7 3 3 240.07 270.54 8.66 o -5 3 3 311.13 363.29 9.89 o -3 3 3 197.86 223.95 9.62 o -1 3 3 54.33 71.52 6.55 o 1 3 3 97.85 86.63 8.78 o 3 3 3 173.60 174.98 7.66 o 5 3 3 20.87 19.35 3.45 o 7 3 3 1514.15 1432.84 22.23 o 9 3 3 1509.20 1506.49 23.09 o 11 3 3 151.16 176.28 8.07 o 13 3 3 89.48 78.20 7.05 o 15 3 3 55.82 57.54 6.76 o 17 3 3 19.54 21.35 4.31 o 19 3 3 408.71 362.50 19.46 o 21 3 3 225.41 207.83 11.38 o 23 3 3 27.49 27.54 6.48 o 25 3 3 14.04 19.88 8.29 o 27 3 3 238.23 221.05 19.30 o -24 4 3 49.37 73.69 13.36 o -22 4 3 8.53 5.31 7.65 o -20 4 3 10.07 13.46 7.87 o -18 4 3 18.14 26.07 8.37 o -16 4 3 472.94 470.24 17.29 o -14 4 3 12.24 12.44 4.90 o -12 4 3 70.44 58.87 7.52 o -10 4 3 298.27 281.13 16.50 o -8 4 3 317.24 337.82 13.97 o -6 4 3 83.53 75.16 7.87 o -4 4 3 83.49 56.74 7.92 o -2 4 3 764.66 710.69 19.33 o 0 4 3 354.96 328.73 12.55 o 2 4 3 95.56 92.55 10.37 o 4 4 3 133.36 135.81 8.25 o 6 4 3 657.19 644.80 16.11 o 8 4 3 248.27 257.72 10.62 o 10 4 3 514.41 528.45 22.77 o 12 4 3 52.33 31.51 8.14 o 14 4 3 0.01 4.45 5.95 o 16 4 3 86.93 109.74 13.24 o 18 4 3 96.21 109.93 17.74 o 20 4 3 23.38 8.43 5.88 o 22 4 3 84.96 107.07 11.61 o -17 5 3 37.47 56.35 11.56 o -15 5 3 1.57 7.18 5.78 o -13 5 3 99.69 128.57 21.10 o -11 5 3 8.72 8.77 5.43 o -9 5 3 5.57 8.91 5.23 o -7 5 3 93.99 52.18 8.01 o -5 5 3 472.45 389.52 22.14 o -3 5 3 0.08 -1.16 5.60 o -1 5 3 91.28 95.88 12.95 o 1 5 3 179.50 174.11 17.29 o 3 5 3 4.52 -6.14 4.89 o 5 5 3 0.00 -2.60 4.69 o 7 5 3 48.50 50.26 8.21 o 9 5 3 108.88 120.51 11.54 o 11 5 3 286.35 278.53 23.43 o 13 5 3 11.58 17.26 8.23 o 15 5 3 175.44 200.46 35.73 o -34 0 4 2.12 -2.13 10.30 o -32 0 4 1400.96 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