data_bos2_0m _diffrn_radiation_monochromator multilayer #Added by publCIF _cell_special_details ? #Added by publCIF _publ_section_related_literature ? _publ_contact_letter ; Please consider this CIF for publication. I certify that this contibution is the original work of those listed as authors; that it has not been published before (in any language or medium) and is not being considered for publication elsewhere; that all authors concur with and are aware of the submission; that all workers involved in the study are listed as authors or given proper credit in the acknowledgements; that I have obtained permission for and acknowledged the source of any excerpts from other copyright works; and that to the best of my knowledge the paper contains no statements which are libellous, unlawful or in any way actionable. All coauthors have made significant scientific contributions to the work reported, including the ideas and their execution, and share responsibility and accountability for the results. ; _publ_requested_category ? _publ_requested_journal ? _publ_contact_author_fax ? _publ_section_title ; Tandem dienone-photorearrangement-cycloaddition for the rapid generation of molecular complexity ; # Loop of author details loop_ _publ_author_name _publ_author_address _publ_author_footnote _publ_author_email 'Bos, Pieter H.' ; Department of Chemistry Center for Chemical Methodology and Library Development (CMLD-BU) Boston University 590 Commonwealth Avenue Boston, MA 02215 ; ; ? ; . 'Antalek, Mitchell T.' ; Department of Chemistry Center for Chemical Methodology and Library Development (CMLD-BU) Boston University 590 Commonwealth Avenue Boston, MA 02215 ; . . 'Porco, Jr., John A.' ; Department of Chemistry Center for Chemical Methodology and Library Development (CMLD-BU) Boston University 590 Commonwealth Avenue Boston, MA 02215 ; . ; porco@bu.edu ; 'Stephenson, Corey R.J.' ; Department of Chemistry Center for Chemical Methodology and Library Development (CMLD-BU) Boston University 590 Commonwealth Avenue Boston, MA 02215 ; . ; crjsteph@bu.edu ; _publ_section_abstract ; (type here to add abstract) ; _audit_update_record ; 2013-08-30 # Formatted by publCIF ; _audit_creation_date 2013-08-08 _audit_creation_method ; Olex2 1.2-beta (compiled Apr 23 2013 17:59:47, GUI svn.r4466) ; _publ_contact_author_address ; Department of Chemistry Center for Chemical Methodology and Library Development (CMLD-BU) Boston University 590 Commonwealth Avenue Boston, MA 02215 ; _publ_contact_author_email 'porco@bu.edu' _publ_contact_author_name 'John A. Porco, Jr.' _publ_contact_author_phone ? _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C18 H20 O4' _chemical_formula_sum 'C18 H20 O4' _chemical_formula_weight 300.34 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.1528(2) _cell_length_b 15.6908(5) _cell_length_c 11.0625(3) _cell_angle_alpha 90 _cell_angle_beta 90.1480(10) _cell_angle_gamma 90 _cell_volume 1415.15(7) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9637 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 66.594 _cell_measurement_theta_min 4.888 _exptl_absorpt_coefficient_mu 0.805 _exptl_absorpt_correction_T_max 0.7528 _exptl_absorpt_correction_T_min 0.7190 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_process_details 'SADABS (Sheldrick, 1997)' _exptl_crystal_colour 'colorless' _exptl_crystal_density_diffrn 1.410 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'block' _exptl_crystal_F_000 640 _exptl_crystal_size_max 0.135 _exptl_crystal_size_mid 0.106 _exptl_crystal_size_min 0.100 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0396 _diffrn_reflns_av_unetI/netI 0.0179 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 43332 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 66.741 _diffrn_reflns_theta_max 66.741 _diffrn_reflns_theta_min 4.891 _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker Proteum-R' _diffrn_measurement_method '\w & \f scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'rotating anode' _diffrn_standards_number 0 _diffrn_standards_interval_count 0 _diffrn_standards_decay_% 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2474 _reflns_number_total 2493 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement ? _computing_data_collection ? _computing_data_reduction ? _computing_molecular_graphics ; O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann, OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Cryst. (2009). 42, 339-341. ; _computing_publication_material ; O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann, OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Cryst. (2009). 42, 339-341. ; _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution ? _refine_diff_density_max 0.385 _refine_diff_density_min -0.462 _refine_diff_density_rms 0.141 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.157 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 202 _refine_ls_number_reflns 2493 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0382 _refine_ls_R_factor_gt 0.0351 _refine_ls_restrained_S_all 1.157 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0598P)^2^+0.6422P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0985 _refine_ls_wR_factor_ref 0.1102 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C5(H5) 2.b Secondary CH2 refined with riding coordinates: C8(H8A,H8B), C13(H13A,H13B), C14(H14A,H14B) 2.c Aromatic/amide H refined with riding coordinates: C6(H6), C7(H7), C16(H16), C17(H17) 2.d Idealised Me refined as rotating group: C1(H1A,H1B,H1C), C9(H9A,H9B,H9C), C18(H18A,H18B,H18C) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.51280(11) 0.85276(6) 0.76502(9) 0.0187(3) Uani 1 1 d . . . . . O2 O 0.97789(12) 1.02281(6) 0.76147(9) 0.0199(3) Uani 1 1 d . . . . . O3 O 1.07137(12) 0.68980(6) 0.63007(8) 0.0171(2) Uani 1 1 d . . . . . O4 O 0.96341(11) 0.71819(6) 0.89680(8) 0.0150(2) Uani 1 1 d . . . . . C1 C 0.50872(18) 1.00239(9) 0.72223(14) 0.0218(3) Uani 1 1 d . . . . . H1A H 0.4209 0.9971 0.6621 0.033 Uiso 1 1 calc R U . . . H1B H 0.5774 1.0517 0.7026 0.033 Uiso 1 1 calc R U . . . H1C H 0.4606 1.0101 0.8026 0.033 Uiso 1 1 calc R U . . . C2 C 0.61308(16) 0.92209(8) 0.72137(12) 0.0160(3) Uani 1 1 d . . . . . C3 C 0.76058(16) 0.92183(8) 0.81246(12) 0.0138(3) Uani 1 1 d . . . . . C4 C 0.79129(16) 0.82433(8) 0.82376(11) 0.0123(3) Uani 1 1 d . . . . . C5 C 0.87788(17) 0.79194(9) 0.94271(12) 0.0152(3) Uani 1 1 d . . . . . H5 H 0.8014 0.7797 1.0111 0.018 Uiso 1 1 calc R U . . . C6 C 1.02101(17) 0.84969(9) 0.97523(12) 0.0170(3) Uani 1 1 d . . . . . H6 H 1.0263 0.8892 1.0402 0.020 Uiso 1 1 calc R U . . . C7 C 1.13716(17) 0.83371(9) 0.89444(12) 0.0159(3) Uani 1 1 d . . . . . H7 H 1.2421 0.8597 0.8887 0.019 Uiso 1 1 calc R U . . . C8 C 0.61939(16) 0.78523(9) 0.80368(13) 0.0162(3) Uani 1 1 d . . . . . H8A H 0.6243 0.7401 0.7413 0.019 Uiso 1 1 calc R U . . . H8B H 0.5784 0.7597 0.8797 0.019 Uiso 1 1 calc R U . . . C9 C 0.71825(17) 0.96827(9) 0.92922(12) 0.0186(3) Uani 1 1 d . . . . . H9A H 0.8102 0.9635 0.9861 0.028 Uiso 1 1 calc R U . . . H9B H 0.6201 0.9426 0.9650 0.028 Uiso 1 1 calc R U . . . H9C H 0.6973 1.0285 0.9117 0.028 Uiso 1 1 calc R U . . . C10 C 0.91238(16) 0.95438(8) 0.74780(11) 0.0138(3) Uani 1 1 d . . . . . C11 C 0.96008(16) 0.88495(8) 0.65732(11) 0.0137(3) Uani 1 1 d . . . . . C12 C 0.92788(16) 0.80142(8) 0.72881(11) 0.0117(3) Uani 1 1 d . . . . . C13 C 0.90824(16) 0.72224(8) 0.64849(12) 0.0143(3) Uani 1 1 d . . . . . H13A H 0.8388 0.6791 0.6889 0.017 Uiso 1 1 calc R U . . . H13B H 0.8569 0.7376 0.5703 0.017 Uiso 1 1 calc R U . . . C14 C 1.16776(17) 0.70626(9) 0.73676(12) 0.0162(3) Uani 1 1 d . . . . . H14A H 1.2733 0.7333 0.7150 0.019 Uiso 1 1 calc R U . . . H14B H 1.1907 0.6525 0.7806 0.019 Uiso 1 1 calc R U . . . C15 C 1.06661(16) 0.76534(8) 0.81358(11) 0.0137(3) Uani 1 1 d . . . . . C16 C 0.82354(18) 0.89117(8) 0.56301(12) 0.0166(3) Uani 1 1 d . . . . . H16 H 0.8505 0.8853 0.4799 0.020 Uiso 1 1 calc R U . . . C17 C 0.66861(18) 0.90456(8) 0.59359(12) 0.0176(3) Uani 1 1 d . . . . . H17 H 0.5878 0.9030 0.5316 0.021 Uiso 1 1 calc R U . . . C18 C 1.12896(17) 0.89604(9) 0.60165(12) 0.0183(3) Uani 1 1 d . . . . . H18A H 1.1435 0.8544 0.5365 0.027 Uiso 1 1 calc R U . . . H18B H 1.2132 0.8870 0.6637 0.027 Uiso 1 1 calc R U . . . H18C H 1.1391 0.9538 0.5689 0.027 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0111(5) 0.0151(5) 0.0299(6) 0.0033(4) -0.0009(4) -0.0009(4) O2 0.0222(5) 0.0143(5) 0.0234(5) -0.0024(4) 0.0006(4) -0.0060(4) O3 0.0162(5) 0.0196(5) 0.0156(5) -0.0042(4) 0.0008(4) 0.0022(4) O4 0.0159(5) 0.0144(5) 0.0146(5) 0.0033(4) 0.0030(4) 0.0005(4) C1 0.0181(7) 0.0162(7) 0.0311(8) -0.0001(6) -0.0044(6) 0.0021(6) C2 0.0132(7) 0.0126(7) 0.0223(7) 0.0009(5) -0.0022(5) -0.0022(5) C3 0.0137(6) 0.0122(6) 0.0154(6) -0.0007(5) -0.0003(5) -0.0003(5) C4 0.0123(6) 0.0121(6) 0.0126(6) -0.0003(5) 0.0015(5) -0.0013(5) C5 0.0161(7) 0.0176(7) 0.0120(6) 0.0011(5) 0.0024(5) 0.0015(5) C6 0.0195(7) 0.0185(7) 0.0128(6) -0.0004(5) -0.0038(5) 0.0011(5) C7 0.0152(7) 0.0181(7) 0.0144(6) 0.0013(5) -0.0036(5) -0.0008(5) C8 0.0125(7) 0.0137(7) 0.0224(7) 0.0021(5) 0.0001(5) -0.0008(5) C9 0.0196(7) 0.0172(7) 0.0191(7) -0.0035(5) 0.0026(5) 0.0008(5) C10 0.0142(6) 0.0140(7) 0.0132(6) 0.0013(5) -0.0026(5) -0.0005(5) C11 0.0155(7) 0.0129(7) 0.0126(6) 0.0008(5) 0.0003(5) -0.0021(5) C12 0.0112(6) 0.0121(6) 0.0117(6) 0.0002(5) 0.0002(5) -0.0017(5) C13 0.0146(7) 0.0126(6) 0.0157(6) -0.0014(5) -0.0004(5) 0.0002(5) C14 0.0149(7) 0.0177(7) 0.0161(7) -0.0006(5) -0.0004(5) 0.0010(5) C15 0.0126(6) 0.0154(7) 0.0129(6) 0.0027(5) 0.0011(5) -0.0009(5) C16 0.0249(8) 0.0124(6) 0.0126(6) 0.0013(5) -0.0030(5) -0.0013(5) C17 0.0221(7) 0.0122(6) 0.0185(7) 0.0011(5) -0.0076(5) -0.0017(5) C18 0.0193(7) 0.0179(7) 0.0177(7) 0.0017(5) 0.0051(5) -0.0032(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C2 1.4446(16) . ? O1 C8 1.4349(16) . ? O2 C10 1.2086(17) . ? O3 C13 1.4391(16) . ? O3 C14 1.4397(16) . ? O4 C5 1.4440(16) . ? O4 C15 1.4515(15) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C1 C2 1.5203(19) . ? C2 C3 1.5670(18) . ? C2 C17 1.511(2) . ? C3 C4 1.5553(18) . ? C3 C9 1.5233(18) . ? C3 C10 1.5194(18) . ? C4 C5 1.5759(18) . ? C4 C8 1.5454(18) . ? C4 C12 1.5743(17) . ? C5 H5 1.0000 . ? C5 C6 1.5199(19) . ? C6 H6 0.9500 . ? C6 C7 1.328(2) . ? C7 H7 0.9500 . ? C7 C15 1.5097(19) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 C11 1.5303(18) . ? C11 C12 1.5534(17) . ? C11 C16 1.5268(18) . ? C11 C18 1.5197(18) . ? C12 C13 1.5355(18) . ? C12 C15 1.5728(18) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C15 1.5051(18) . ? C16 H16 0.9500 . ? C16 C17 1.325(2) . ? C17 H17 0.9500 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 O1 C2 108.23(10) . . ? C13 O3 C14 108.85(10) . . ? C5 O4 C15 95.50(9) . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? O1 C2 C1 107.75(11) . . ? O1 C2 C3 102.54(10) . . ? O1 C2 C17 110.30(11) . . ? C1 C2 C3 115.25(11) . . ? C17 C2 C1 109.02(11) . . ? C17 C2 C3 111.71(11) . . ? C4 C3 C2 100.21(10) . . ? C9 C3 C2 111.65(11) . . ? C9 C3 C4 116.05(11) . . ? C10 C3 C2 108.73(10) . . ? C10 C3 C4 103.73(10) . . ? C10 C3 C9 115.15(11) . . ? C3 C4 C5 117.13(11) . . ? C3 C4 C12 106.56(10) . . ? C8 C4 C3 103.49(10) . . ? C8 C4 C5 113.33(11) . . ? C8 C4 C12 117.14(11) . . ? C12 C4 C5 99.64(10) . . ? O4 C5 C4 100.39(10) . . ? O4 C5 H5 114.5 . . ? O4 C5 C6 100.94(10) . . ? C4 C5 H5 114.5 . . ? C6 C5 C4 110.33(11) . . ? C6 C5 H5 114.5 . . ? C5 C6 H6 127.0 . . ? C7 C6 C5 106.05(12) . . ? C7 C6 H6 127.0 . . ? C6 C7 H7 127.4 . . ? C6 C7 C15 105.18(12) . . ? C15 C7 H7 127.4 . . ? O1 C8 C4 107.34(10) . . ? O1 C8 H8A 110.2 . . ? O1 C8 H8B 110.2 . . ? C4 C8 H8A 110.2 . . ? C4 C8 H8B 110.2 . . ? H8A C8 H8B 108.5 . . ? C3 C9 H9A 109.5 . . ? C3 C9 H9B 109.5 . . ? C3 C9 H9C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? O2 C10 C3 126.86(12) . . ? O2 C10 C11 126.96(12) . . ? C3 C10 C11 106.10(10) . . ? C10 C11 C12 102.95(10) . . ? C16 C11 C10 102.43(10) . . ? C16 C11 C12 106.13(10) . . ? C18 C11 C10 114.56(11) . . ? C18 C11 C12 117.22(11) . . ? C18 C11 C16 112.05(11) . . ? C11 C12 C4 105.53(10) . . ? C11 C12 C15 119.01(11) . . ? C13 C12 C4 119.86(11) . . ? C13 C12 C11 113.93(10) . . ? C13 C12 C15 97.33(10) . . ? C15 C12 C4 101.14(10) . . ? O3 C13 C12 105.85(10) . . ? O3 C13 H13A 110.6 . . ? O3 C13 H13B 110.6 . . ? C12 C13 H13A 110.6 . . ? C12 C13 H13B 110.6 . . ? H13A C13 H13B 108.7 . . ? O3 C14 H14A 110.5 . . ? O3 C14 H14B 110.5 . . ? O3 C14 C15 105.95(10) . . ? H14A C14 H14B 108.7 . . ? C15 C14 H14A 110.5 . . ? C15 C14 H14B 110.5 . . ? O4 C15 C7 101.94(10) . . ? O4 C15 C12 98.31(9) . . ? O4 C15 C14 111.32(11) . . ? C7 C15 C12 111.71(11) . . ? C14 C15 C7 124.32(11) . . ? C14 C15 C12 106.22(10) . . ? C11 C16 H16 119.0 . . ? C17 C16 C11 121.97(12) . . ? C17 C16 H16 119.0 . . ? C2 C17 H17 118.1 . . ? C16 C17 C2 123.77(12) . . ? C16 C17 H17 118.1 . . ? C11 C18 H18A 109.5 . . ? C11 C18 H18B 109.5 . . ? C11 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C2 C3 C4 41.91(12) . . . . ? O1 C2 C3 C9 -81.57(13) . . . . ? O1 C2 C3 C10 150.31(10) . . . . ? O1 C2 C17 C16 -113.72(14) . . . . ? O2 C10 C11 C12 143.55(13) . . . . ? O2 C10 C11 C16 -106.41(15) . . . . ? O2 C10 C11 C18 15.16(19) . . . . ? O3 C14 C15 O4 90.81(12) . . . . ? O3 C14 C15 C7 -146.82(12) . . . . ? O3 C14 C15 C12 -15.15(13) . . . . ? O4 C5 C6 C7 33.53(13) . . . . ? C1 C2 C3 C4 158.66(11) . . . . ? C1 C2 C3 C9 35.18(16) . . . . ? C1 C2 C3 C10 -92.94(13) . . . . ? C1 C2 C17 C16 128.16(14) . . . . ? C2 O1 C8 C4 18.87(14) . . . . ? C2 C3 C4 C5 -155.71(11) . . . . ? C2 C3 C4 C8 -30.22(12) . . . . ? C2 C3 C4 C12 93.89(11) . . . . ? C2 C3 C10 O2 107.18(15) . . . . ? C2 C3 C10 C11 -69.95(12) . . . . ? C3 C2 C17 C16 -0.37(18) . . . . ? C3 C4 C5 O4 -149.67(11) . . . . ? C3 C4 C5 C6 -43.78(15) . . . . ? C3 C4 C8 O1 8.88(13) . . . . ? C3 C4 C12 C11 -5.15(13) . . . . ? C3 C4 C12 C13 -135.31(12) . . . . ? C3 C4 C12 C15 119.44(10) . . . . ? C3 C10 C11 C12 -39.33(13) . . . . ? C3 C10 C11 C16 70.72(12) . . . . ? C3 C10 C11 C18 -167.72(11) . . . . ? C4 C3 C10 O2 -146.83(13) . . . . ? C4 C3 C10 C11 36.04(13) . . . . ? C4 C5 C6 C7 -72.00(14) . . . . ? C4 C12 C13 O3 -146.39(11) . . . . ? C4 C12 C15 O4 39.71(11) . . . . ? C4 C12 C15 C7 -66.74(12) . . . . ? C4 C12 C15 C14 154.86(10) . . . . ? C5 O4 C15 C7 50.91(11) . . . . ? C5 O4 C15 C12 -63.48(10) . . . . ? C5 O4 C15 C14 -174.58(11) . . . . ? C5 C4 C8 O1 136.77(11) . . . . ? C5 C4 C12 C11 -127.36(10) . . . . ? C5 C4 C12 C13 102.48(12) . . . . ? C5 C4 C12 C15 -2.77(11) . . . . ? C5 C6 C7 C15 -0.83(14) . . . . ? C6 C7 C15 O4 -32.03(13) . . . . ? C6 C7 C15 C12 72.04(14) . . . . ? C6 C7 C15 C14 -158.49(12) . . . . ? C8 O1 C2 C1 -160.60(11) . . . . ? C8 O1 C2 C3 -38.59(13) . . . . ? C8 O1 C2 C17 80.51(13) . . . . ? C8 C4 C5 O4 89.90(12) . . . . ? C8 C4 C5 C6 -164.21(11) . . . . ? C8 C4 C12 C11 110.06(12) . . . . ? C8 C4 C12 C13 -20.11(17) . . . . ? C8 C4 C12 C15 -125.35(11) . . . . ? C9 C3 C4 C5 -35.36(16) . . . . ? C9 C3 C4 C8 90.13(13) . . . . ? C9 C3 C4 C12 -145.76(11) . . . . ? C9 C3 C10 O2 -18.94(19) . . . . ? C9 C3 C10 C11 163.93(11) . . . . ? C10 C3 C4 C5 91.97(12) . . . . ? C10 C3 C4 C8 -142.55(10) . . . . ? C10 C3 C4 C12 -18.44(13) . . . . ? C10 C11 C12 C4 26.50(12) . . . . ? C10 C11 C12 C13 160.03(11) . . . . ? C10 C11 C12 C15 -86.04(13) . . . . ? C10 C11 C16 C17 -39.66(16) . . . . ? C11 C12 C13 O3 87.27(13) . . . . ? C11 C12 C15 O4 154.62(10) . . . . ? C11 C12 C15 C7 48.17(15) . . . . ? C11 C12 C15 C14 -90.22(13) . . . . ? C11 C16 C17 C2 5.2(2) . . . . ? C12 C4 C5 O4 -35.35(11) . . . . ? C12 C4 C5 C6 70.54(12) . . . . ? C12 C4 C8 O1 -108.01(12) . . . . ? C12 C11 C16 C17 67.96(15) . . . . ? C13 O3 C14 C15 -10.56(13) . . . . ? C13 C12 C15 O4 -82.77(10) . . . . ? C13 C12 C15 C7 170.78(10) . . . . ? C13 C12 C15 C14 32.39(12) . . . . ? C14 O3 C13 C12 32.98(13) . . . . ? C15 O4 C5 C4 62.49(10) . . . . ? C15 O4 C5 C6 -50.78(11) . . . . ? C15 C12 C13 O3 -39.03(12) . . . . ? C16 C11 C12 C4 -80.75(12) . . . . ? C16 C11 C12 C13 52.78(14) . . . . ? C16 C11 C12 C15 166.71(11) . . . . ? C17 C2 C3 C4 -76.20(12) . . . . ? C17 C2 C3 C9 160.32(11) . . . . ? C17 C2 C3 C10 32.20(14) . . . . ? C18 C11 C12 C4 153.21(11) . . . . ? C18 C11 C12 C13 -73.26(15) . . . . ? C18 C11 C12 C15 40.67(16) . . . . ? C18 C11 C16 C17 -162.92(13) . . . . ? _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _shelx_hkl_checksum 1035 _shelx_hkl_file ; 1 0 0 0.45 0.07 3 0 0 0.00 0.07 -3 0 0 0.01 0.07 3 0 0 0.01 0.04 4 0 0 0.60 0.09 4 0 0 0.55 0.13 -4 0 0 0.47 0.13 5 0 0 0.11 0.07 5 0 0 0.04 0.08 5 0 0 0.09 0.05 5 0 0 0.02 0.08 6 0 0 1.51 0.21 6 0 0 1.17 0.13 6 0 0 1.24 0.14 6 0 0 1.37 0.15 6 0 0 1.53 0.13 6 0 0 1.14 0.14 7 0 0 -0.01 0.05 7 0 0 0.04 0.06 7 0 0 -0.07 0.12 7 0 0 0.05 0.06 7 0 0 0.05 0.08 7 0 0 -0.01 0.05 7 0 0 0.00 0.07 8 0 0 14.39 0.74 8 0 0 15.51 0.79 8 0 0 13.76 0.93 8 0 0 14.55 0.92 9 0 0 -0.03 0.06 9 0 0 0.02 0.09 9 0 0 0.08 0.06 0 -1 0 0.01 0.02 0 1 0 0.02 0.02 0 1 0 0.04 0.02 -1 -1 0 53.14 2.96 1 -1 0 52.02 2.75 1 -1 0 53.81 2.93 -1 1 0 53.83 2.93 1 1 0 53.13 2.96 2 -1 0 172.99 9.86 2 -1 0 186.72 9.24 -2 -1 0 188.55 9.90 -2 -1 0 184.52 10.88 2 -1 0 191.69 9.87 2 1 0 155.05 9.88 -2 1 0 176.21 10.35 -2 1 0 179.05 9.86 -3 -1 0 0.88 0.15 -3 -1 0 0.88 0.16 3 -1 0 1.01 0.13 3 -1 0 1.23 0.13 3 -1 0 0.99 0.08 3 1 0 0.86 0.11 3 1 0 0.58 0.13 -3 1 0 0.97 0.13 4 -1 0 0.30 0.10 4 -1 0 -0.10 0.14 4 -1 0 -0.10 0.10 4 1 0 0.14 0.07 4 1 0 0.26 0.12 5 -1 0 1.91 0.20 5 -1 0 2.09 0.15 5 -1 0 1.67 0.13 5 -1 0 2.02 0.14 5 1 0 1.78 0.19 5 1 0 1.69 0.17 5 1 0 1.76 0.25 -5 1 0 2.33 0.30 5 1 0 1.60 0.15 5 1 0 1.68 0.16 6 -1 0 53.26 2.64 6 -1 0 52.33 2.64 6 -1 0 53.90 2.46 6 -1 0 56.00 2.46 6 -1 0 56.13 2.96 6 1 0 53.50 2.66 6 1 0 53.67 2.49 6 1 0 49.18 2.64 6 1 0 55.53 2.67 6 1 0 54.16 2.95 6 1 0 49.13 3.21 6 1 0 53.71 2.95 6 1 0 51.63 3.11 6 1 0 54.99 2.71 7 -1 0 1.30 0.13 7 -1 0 1.02 0.10 7 -1 0 1.10 0.10 7 -1 0 0.95 0.13 7 1 0 0.82 0.14 7 1 0 1.63 0.24 7 1 0 1.04 0.17 7 1 0 1.05 0.14 7 1 0 0.98 0.14 7 1 0 1.21 0.14 8 -1 0 25.47 1.51 8 -1 0 25.27 1.34 8 -1 0 25.08 1.60 8 1 0 25.49 1.21 8 1 0 25.71 1.50 8 1 0 25.79 1.21 8 1 0 26.16 1.60 8 1 0 26.14 1.35 8 1 0 27.36 1.32 9 -1 0 3.61 0.28 9 -1 0 3.74 0.23 9 -1 0 3.69 0.32 9 1 0 3.84 0.24 9 1 0 3.66 0.29 -2 -2 0 131.68 6.79 2 -2 0 122.62 6.71 2 -2 0 127.36 6.71 2 -2 0 127.27 6.31 2 2 0 104.14 6.77 2 2 0 125.27 6.22 -2 2 0 119.01 6.71 3 -2 0 2.29 0.17 -3 -2 0 2.19 0.26 3 -2 0 1.98 0.17 3 -2 0 2.42 0.22 -3 2 0 2.15 0.21 3 2 0 2.32 0.19 3 2 0 1.78 0.23 4 -2 0 296.11 13.87 4 -2 0 313.25 13.90 4 -2 0 296.19 17.47 4 -2 0 305.08 17.77 -4 -2 0 282.70 17.86 4 -2 0 297.48 16.74 4 2 0 310.79 14.14 4 2 0 325.51 16.88 4 2 0 325.32 15.54 5 -2 0 22.24 1.07 -5 -2 0 20.70 1.42 5 -2 0 23.38 1.32 5 -2 0 23.36 1.44 5 -2 0 24.49 1.07 5 -2 0 23.43 1.16 5 2 0 23.11 1.31 -5 2 0 23.38 1.58 5 2 0 23.37 1.24 5 2 0 20.57 1.10 5 2 0 23.22 1.46 5 2 0 23.94 1.19 6 -2 0 37.54 1.79 6 -2 0 41.06 1.79 -6 -2 0 37.71 2.23 6 -2 0 40.55 2.19 6 -2 0 38.57 1.93 6 2 0 38.40 2.36 6 2 0 38.64 1.94 6 2 0 35.62 2.33 6 2 0 40.72 2.18 6 2 0 39.75 2.29 6 2 0 39.11 1.84 6 2 0 36.80 2.04 6 2 0 37.84 2.17 6 2 0 39.79 1.97 6 2 0 38.33 1.97 6 2 0 40.05 1.99 -7 -2 0 2.30 0.22 7 -2 0 1.99 0.26 7 -2 0 2.23 0.14 7 2 0 2.48 0.20 7 2 0 1.78 0.20 7 2 0 2.44 0.18 7 2 0 2.41 0.23 7 2 0 2.26 0.27 7 2 0 2.23 0.21 7 2 0 2.18 0.19 8 -2 0 36.37 2.07 -8 -2 0 36.07 2.10 8 -2 0 36.82 2.21 8 2 0 37.39 2.17 8 2 0 34.11 1.70 8 2 0 36.21 1.70 8 2 0 37.86 1.87 8 2 0 35.43 2.05 8 2 0 36.77 1.83 8 2 0 36.20 2.13 8 2 0 35.58 2.22 -9 -2 0 24.40 1.49 9 -2 0 26.27 1.48 9 -2 0 25.65 1.57 9 2 0 24.48 1.53 9 2 0 26.35 1.58 9 2 0 27.00 1.33 0 -3 0 0.01 0.06 0 3 0 0.12 0.06 -1 -3 0 13.47 0.88 1 -3 0 14.23 0.79 1 -3 0 14.58 0.83 1 -3 0 13.97 0.83 -1 3 0 14.01 0.83 1 3 0 14.62 0.88 -2 -3 0 122.09 6.64 2 -3 0 118.26 6.15 2 3 0 116.36 6.07 3 -3 0 225.18 11.26 -3 -3 0 210.67 11.11 -3 -3 0 239.34 12.12 3 3 0 187.76 12.08 3 3 0 214.07 11.10 -3 3 0 235.44 12.64 4 -3 0 0.50 0.05 -4 -3 0 0.44 0.11 4 -3 0 0.42 0.06 4 -3 0 0.48 0.12 4 3 0 0.46 0.16 4 3 0 0.44 0.11 5 -3 0 8.38 0.63 5 -3 0 8.79 0.41 5 -3 0 9.04 0.41 5 -3 0 8.41 0.45 5 -3 0 8.73 0.69 5 -3 0 8.17 0.56 -5 -3 0 8.76 0.60 5 3 0 8.74 0.42 5 3 0 8.63 0.53 5 3 0 7.80 0.54 5 3 0 8.76 0.42 5 3 0 8.05 0.52 5 3 0 8.59 0.51 5 3 0 8.57 0.69 5 3 0 8.78 0.53 6 -3 0 5.17 0.30 -6 -3 0 6.14 0.39 6 -3 0 5.74 0.44 6 3 0 6.45 0.40 6 3 0 5.77 0.35 6 3 0 6.19 0.42 6 3 0 5.64 0.37 6 3 0 4.90 0.35 6 3 0 5.70 0.38 6 3 0 5.13 0.32 6 3 0 4.99 0.37 6 3 0 5.07 0.40 -6 3 0 7.02 0.61 6 3 0 5.42 0.37 -7 -3 0 0.96 0.16 7 3 0 1.08 0.19 7 3 0 1.12 0.16 7 3 0 1.12 0.17 7 3 0 1.47 0.21 7 3 0 1.12 0.10 7 3 0 1.18 0.16 7 3 0 0.89 0.15 7 3 0 1.09 0.13 7 3 0 1.25 0.14 -8 -3 0 2.82 0.25 8 -3 0 3.16 0.33 8 3 0 2.88 0.23 8 3 0 2.32 0.24 8 3 0 2.82 0.22 8 3 0 2.66 0.23 8 3 0 3.41 0.29 8 3 0 3.00 0.23 8 3 0 2.89 0.21 9 -3 0 9.62 0.64 -9 -3 0 10.23 0.61 9 -3 0 10.31 0.65 9 3 0 8.90 0.64 9 3 0 9.80 0.65 9 3 0 10.55 0.55 0 -4 0 83.34 5.20 0 4 0 77.76 4.43 0 4 0 77.83 4.43 1 -4 0 26.74 1.67 1 -4 0 30.12 1.67 -1 -4 0 29.81 1.55 1 -4 0 29.86 1.57 1 4 0 31.20 1.73 -1 4 0 28.54 1.67 -2 -4 0 194.93 13.09 -2 -4 0 245.53 12.04 2 -4 0 246.38 12.20 2 4 0 262.16 12.05 -3 -4 0 30.52 1.59 -3 -4 0 30.65 1.81 -3 -4 0 27.46 1.80 3 -4 0 30.35 1.60 3 4 0 25.34 1.77 3 4 0 31.99 1.59 4 -4 0 0.63 0.04 4 -4 0 0.68 0.13 -4 -4 0 0.51 0.11 -4 -4 0 0.63 0.11 -4 -4 0 0.53 0.19 -4 -4 0 0.57 0.13 4 4 0 0.77 0.21 4 4 0 0.46 0.12 4 4 0 0.43 0.11 -4 4 0 0.64 0.14 4 4 0 0.49 0.09 4 4 0 0.75 0.20 5 -4 0 2.05 0.27 -5 -4 0 1.77 0.22 5 -4 0 2.19 0.23 5 -4 0 1.52 0.28 5 -4 0 1.76 0.11 5 4 0 1.77 0.16 5 4 0 2.14 0.19 5 4 0 1.98 0.16 5 4 0 1.50 0.20 5 4 0 1.75 0.17 5 4 0 1.92 0.15 5 4 0 2.32 0.33 5 4 0 1.63 0.18 5 4 0 1.88 0.18 5 4 0 1.58 0.18 -6 -4 0 86.12 5.00 6 -4 0 80.48 5.17 6 -4 0 74.12 4.77 -6 -4 0 88.69 5.25 6 4 0 93.16 4.39 6 4 0 91.43 4.58 6 4 0 89.09 4.44 6 4 0 91.74 4.38 6 4 0 90.45 4.88 -6 4 0 87.67 5.57 6 4 0 90.18 5.12 6 4 0 85.86 4.92 6 4 0 91.59 5.29 6 4 0 91.79 4.56 6 4 0 88.43 5.12 -7 -4 0 5.47 0.49 -7 -4 0 6.22 0.43 7 4 0 5.56 0.38 7 4 0 6.40 0.34 7 4 0 6.16 0.43 7 4 0 5.12 0.40 7 4 0 6.15 0.44 7 4 0 6.41 0.46 7 4 0 6.23 0.40 7 4 0 6.43 0.38 -8 -4 0 5.83 0.39 8 -4 0 5.84 0.46 8 4 0 5.96 0.39 8 4 0 4.73 0.34 8 4 0 6.02 0.39 8 4 0 4.72 0.36 8 4 0 5.12 0.33 8 4 0 5.62 0.42 -9 -4 0 6.58 0.46 9 4 0 7.70 0.50 9 4 0 7.61 0.49 9 4 0 7.42 0.40 9 4 0 7.16 0.41 0 -5 0 -0.02 0.08 0 5 0 0.19 0.13 1 -5 0 329.71 17.61 1 -5 0 316.76 16.23 1 -5 0 302.43 17.59 -1 -5 0 319.65 16.29 1 -5 0 341.58 16.48 -1 5 0 320.56 17.59 1 5 0 309.21 16.23 1 5 0 326.69 17.65 2 -5 0 9.36 0.55 2 -5 0 9.01 0.55 2 -5 0 9.27 0.56 -2 -5 0 9.62 0.69 -2 -5 0 9.64 0.56 2 5 0 8.72 0.67 2 5 0 9.50 0.56 3 -5 0 9.30 0.43 -3 -5 0 9.17 0.57 3 -5 0 9.08 0.61 3 -5 0 9.65 0.43 3 -5 0 9.29 0.61 -3 -5 0 8.79 0.62 -3 -5 0 9.04 0.70 3 5 0 8.92 0.61 3 5 0 8.97 0.70 3 5 0 9.46 0.52 3 5 0 9.93 0.58 -4 -5 0 63.51 3.38 4 -5 0 64.06 3.76 -4 -5 0 66.50 3.85 4 -5 0 66.83 3.83 -4 -5 0 65.36 3.78 4 -5 0 66.00 3.50 -4 -5 0 65.17 3.38 4 5 0 66.13 3.77 -4 5 0 63.93 3.85 4 5 0 66.07 3.77 4 5 0 61.78 3.82 4 5 0 57.27 3.35 -5 -5 0 12.25 0.79 5 -5 0 11.86 0.73 5 -5 0 11.37 0.82 -5 -5 0 10.10 0.76 -5 -5 0 11.30 0.68 -5 -5 0 11.11 0.71 5 -5 0 11.40 0.79 5 5 0 12.83 0.74 5 5 0 11.40 0.66 5 5 0 11.72 0.62 5 5 0 11.57 0.66 5 5 0 11.51 0.59 5 5 0 12.51 0.63 5 5 0 9.25 0.69 5 5 0 11.45 0.70 5 5 0 12.02 0.92 5 5 0 10.51 0.74 5 5 0 12.01 0.73 5 5 0 10.99 0.69 5 5 0 11.66 0.66 5 5 0 10.26 0.66 5 5 0 11.53 0.73 6 -5 0 1.59 0.23 -6 -5 0 2.01 0.23 6 -5 0 1.18 0.27 6 5 0 1.28 0.21 6 5 0 1.76 0.22 6 5 0 1.17 0.15 6 5 0 1.49 0.20 6 5 0 1.41 0.15 -6 5 0 2.22 0.34 6 5 0 1.41 0.18 6 5 0 1.18 0.18 6 5 0 1.38 0.17 -7 -5 0 0.53 0.17 7 -5 0 0.25 0.12 -7 -5 0 0.47 0.12 -7 -5 0 0.35 0.13 7 5 0 0.26 0.09 7 5 0 0.38 0.13 7 5 0 0.47 0.11 7 5 0 0.33 0.08 7 5 0 0.25 0.09 7 5 0 0.22 0.10 7 5 0 0.32 0.09 7 5 0 0.27 0.08 8 -5 0 7.06 0.52 -8 -5 0 5.76 0.52 -8 -5 0 7.26 0.47 -8 -5 0 6.73 0.47 8 5 0 6.54 0.48 8 5 0 7.70 0.50 8 5 0 7.04 0.47 8 5 0 7.50 0.45 8 5 0 7.53 0.42 8 5 0 6.90 0.46 8 5 0 5.70 0.40 -9 -5 0 1.89 0.17 9 5 0 1.76 0.15 9 5 0 1.80 0.15 9 5 0 1.63 0.19 9 5 0 1.71 0.18 0 -6 0 11.66 0.86 0 -6 0 11.00 0.77 0 -6 0 12.31 0.66 0 6 0 12.37 0.78 1 -6 0 326.62 16.71 1 -6 0 338.69 18.15 -1 -6 0 348.80 16.77 1 -6 0 336.85 16.95 1 6 0 335.18 18.18 -1 6 0 307.37 18.12 1 6 0 340.41 18.18 1 6 0 306.82 16.71 2 -6 0 264.70 14.19 -2 -6 0 290.49 14.03 -2 -6 0 275.17 15.29 -2 -6 0 273.02 16.15 2 -6 0 269.85 15.14 2 6 0 287.48 14.03 2 6 0 283.84 15.29 2 6 0 285.45 15.29 2 6 0 257.45 16.15 -3 -6 0 0.65 0.13 -3 -6 0 0.58 0.14 3 -6 0 0.63 0.05 -3 -6 0 0.59 0.10 -3 -6 0 0.64 0.20 3 -6 0 0.62 0.05 3 6 0 0.67 0.20 3 6 0 0.66 0.20 3 6 0 0.62 0.15 3 6 0 0.75 0.14 3 6 0 0.80 0.12 4 -6 0 278.42 16.02 -4 -6 0 293.50 16.39 4 -6 0 270.12 16.29 4 -6 0 277.03 14.88 -4 -6 0 279.95 14.44 -4 -6 0 264.72 15.56 -4 -6 0 277.02 14.25 4 6 0 272.68 14.39 4 6 0 275.67 15.59 4 6 0 287.80 16.38 4 6 0 293.50 15.59 -4 6 0 288.27 16.21 -5 -6 0 50.67 3.01 5 -6 0 44.20 2.94 5 -6 0 49.88 3.01 -5 -6 0 44.62 2.72 -5 -6 0 51.56 2.64 -5 -6 0 50.88 2.85 5 -6 0 50.15 2.74 -5 -6 0 46.29 3.00 5 6 0 50.49 3.00 5 6 0 51.15 2.62 5 6 0 53.94 2.79 5 6 0 51.06 2.82 5 6 0 45.42 3.02 5 6 0 52.14 2.53 5 6 0 48.61 2.98 5 6 0 51.11 2.92 5 6 0 49.22 2.52 5 6 0 49.37 2.50 5 6 0 50.11 2.92 5 6 0 46.21 2.71 5 6 0 52.59 2.35 5 6 0 50.24 2.98 -6 -6 0 87.67 4.96 -6 -6 0 81.68 5.22 -6 -6 0 89.07 5.22 6 -6 0 82.31 4.74 -6 -6 0 87.12 4.58 6 6 0 91.36 4.41 -6 6 0 78.88 5.57 6 6 0 87.11 4.89 6 6 0 92.29 4.35 6 6 0 90.16 4.03 6 6 0 87.07 5.23 6 6 0 88.85 5.08 6 6 0 85.58 4.35 6 6 0 93.77 4.85 6 6 0 90.59 4.55 6 6 0 83.42 4.72 6 6 0 82.65 5.08 6 6 0 88.29 4.55 -7 -6 0 153.21 8.86 -7 -6 0 170.18 8.18 7 -6 0 160.40 8.46 -7 -6 0 175.43 9.30 7 6 0 158.01 9.08 7 6 0 157.90 7.74 7 6 0 157.18 9.38 7 6 0 159.55 7.76 7 6 0 168.61 8.13 7 6 0 132.66 7.87 7 6 0 135.25 9.08 -8 -6 0 3.71 0.34 -8 -6 0 3.31 0.30 -8 -6 0 3.90 0.29 8 -6 0 3.70 0.34 8 6 0 3.14 0.24 8 6 0 4.05 0.29 8 6 0 3.48 0.29 8 6 0 3.21 0.31 8 6 0 3.46 0.25 8 6 0 3.41 0.28 -9 -6 0 17.77 1.08 9 6 0 19.56 0.96 9 6 0 19.26 1.12 9 6 0 17.06 1.14 0 -7 0 -0.01 0.06 0 -7 0 -0.02 0.09 0 -7 0 -0.01 0.06 0 7 0 -0.01 0.10 1 -7 0 150.92 8.88 1 -7 0 156.55 8.03 1 -7 0 165.72 8.58 -1 -7 0 160.66 7.90 -1 -7 0 131.42 8.61 1 -7 0 158.08 7.85 1 7 0 147.38 7.90 1 7 0 157.43 9.09 1 7 0 165.35 8.66 -2 -7 0 0.55 0.13 2 -7 0 0.55 0.07 -2 -7 0 0.60 0.12 -2 -7 0 0.50 0.17 2 -7 0 0.66 0.10 2 -7 0 0.79 0.08 -2 -7 0 0.64 0.10 2 7 0 0.48 0.10 2 7 0 0.62 0.20 2 7 0 0.46 0.11 2 7 0 0.76 0.21 2 7 0 0.54 0.13 3 -7 0 56.60 2.54 -3 -7 0 53.20 2.85 -3 -7 0 55.80 2.94 3 -7 0 57.16 2.54 3 -7 0 57.52 3.29 3 -7 0 52.97 3.32 -3 -7 0 57.00 3.36 -3 -7 0 55.14 3.33 3 -7 0 50.78 3.03 -3 -7 0 56.26 2.96 3 7 0 58.55 2.97 3 7 0 57.92 2.94 3 7 0 56.13 3.36 3 7 0 59.96 3.35 -4 -7 0 5.17 0.38 -4 -7 0 5.76 0.41 -4 -7 0 5.80 0.46 4 -7 0 6.17 0.46 -4 -7 0 6.34 0.47 -4 -7 0 6.11 0.40 4 -7 0 5.60 0.41 4 -7 0 5.97 0.45 -4 -7 0 6.12 0.62 4 7 0 5.39 0.45 4 7 0 6.52 0.42 4 7 0 6.02 0.37 -4 7 0 5.67 0.51 4 7 0 5.62 0.42 4 7 0 6.26 0.39 4 7 0 6.20 0.44 4 7 0 5.62 0.60 4 7 0 5.98 0.39 4 7 0 6.51 0.42 4 7 0 6.31 0.37 4 7 0 5.23 0.43 5 -7 0 14.85 0.84 -5 -7 0 13.35 0.80 -5 -7 0 15.03 0.84 -5 -7 0 12.28 0.89 -5 -7 0 12.52 0.91 -5 -7 0 14.22 0.80 5 -7 0 13.33 0.93 5 7 0 14.82 0.86 5 7 0 13.60 0.79 5 7 0 13.16 0.85 5 7 0 14.32 0.74 5 7 0 13.65 0.77 5 7 0 12.50 0.83 5 7 0 11.18 0.86 5 7 0 13.31 0.78 5 7 0 12.95 0.82 5 7 0 12.97 0.74 5 7 0 12.28 0.85 5 7 0 14.41 0.71 5 7 0 13.03 0.83 6 -7 0 51.36 2.82 -6 -7 0 50.76 2.90 -6 -7 0 49.40 3.08 6 -7 0 54.31 3.13 -6 -7 0 49.64 2.70 -6 -7 0 51.25 2.79 -6 -7 0 46.58 3.06 6 7 0 50.91 2.55 6 7 0 49.31 2.86 6 7 0 50.38 2.97 6 7 0 47.33 3.03 6 7 0 51.06 2.58 6 7 0 52.27 2.98 6 7 0 51.28 2.85 6 7 0 49.23 2.70 6 7 0 49.96 3.05 6 7 0 49.61 2.76 6 7 0 48.65 2.66 6 7 0 53.50 2.58 6 7 0 50.19 2.36 -7 -7 0 6.18 0.52 -7 -7 0 6.65 0.45 7 -7 0 5.90 0.48 7 7 0 5.84 0.44 7 7 0 7.19 0.41 7 7 0 6.02 0.37 7 7 0 7.53 0.46 7 7 0 5.64 0.42 7 7 0 6.46 0.46 7 7 0 5.08 0.38 -8 -7 0 38.87 2.14 -8 -7 0 40.26 2.30 8 -7 0 39.45 2.24 -8 -7 0 33.48 2.46 8 7 0 41.30 2.05 8 7 0 40.86 2.42 8 7 0 41.97 2.04 8 7 0 42.03 2.23 8 7 0 40.19 2.35 8 7 0 38.83 2.09 8 7 0 41.53 2.37 -9 -7 0 8.21 0.50 9 7 0 7.16 0.52 9 7 0 8.06 0.44 0 -8 0 14.13 0.88 0 -8 0 14.88 0.89 0 -8 0 13.67 0.94 0 -8 0 14.09 0.79 0 -8 0 14.02 0.68 0 8 0 12.61 0.89 1 -8 0 126.79 7.50 1 -8 0 135.74 7.15 1 -8 0 114.86 8.40 -1 -8 0 121.73 6.56 1 -8 0 133.22 6.52 1 -8 0 130.39 7.38 -1 -8 0 125.16 7.53 1 -8 0 130.46 6.69 1 -8 0 128.23 5.84 -1 -8 0 126.09 7.50 -1 -8 0 135.00 6.43 -1 -8 0 135.60 7.24 1 8 0 125.24 6.58 1 8 0 130.75 7.22 1 8 0 126.09 7.55 -2 -8 0 175.72 10.34 2 -8 0 174.13 10.12 -2 -8 0 174.81 9.09 2 -8 0 163.42 10.28 -2 -8 0 182.80 9.89 2 -8 0 179.38 7.99 -2 -8 0 183.13 8.81 2 -8 0 174.84 9.73 2 -8 0 168.96 7.99 -2 -8 0 165.65 9.00 2 8 0 188.03 9.91 2 8 0 185.64 10.36 2 8 0 174.07 9.11 2 8 0 178.08 9.02 3 -8 0 3.48 0.27 -3 -8 0 3.44 0.28 -3 -8 0 3.29 0.32 -3 -8 0 3.34 0.26 -3 -8 0 3.66 0.32 3 -8 0 3.11 0.20 -3 -8 0 3.65 0.45 3 -8 0 3.57 0.18 3 -8 0 3.67 0.31 3 8 0 4.03 0.33 3 8 0 3.37 0.26 3 8 0 3.63 0.45 3 8 0 3.32 0.30 4 -8 0 157.07 8.38 -4 -8 0 154.95 8.77 -4 -8 0 155.46 8.77 -4 -8 0 146.47 8.10 -4 -8 0 146.79 8.90 -4 -8 0 144.26 9.01 -4 -8 0 159.37 7.85 4 -8 0 156.50 9.03 -4 -8 0 167.93 8.08 -4 -8 0 156.49 8.11 -4 -8 0 164.82 8.46 4 -8 0 159.46 9.17 -4 -8 0 138.07 9.22 -4 -8 0 160.69 8.82 -4 -8 0 158.63 9.27 4 8 0 157.87 8.91 4 8 0 155.17 8.76 4 8 0 158.71 9.27 4 8 0 170.66 9.24 4 8 0 161.13 8.10 4 8 0 157.79 9.05 4 8 0 149.93 8.81 4 8 0 151.91 9.02 4 8 0 153.23 8.45 4 8 0 157.11 8.06 4 8 0 156.85 7.84 4 8 0 148.58 7.75 -4 8 0 167.91 9.21 4 8 0 165.17 8.09 5 -8 0 121.82 6.40 -5 -8 0 125.94 6.72 -5 -8 0 117.03 6.44 -5 -8 0 117.02 7.06 5 -8 0 116.30 7.00 -5 -8 0 98.41 6.17 5 8 0 118.19 6.87 5 8 0 122.04 6.17 5 8 0 118.27 5.54 5 8 0 124.21 5.91 5 8 0 121.95 6.43 5 8 0 123.08 6.67 5 8 0 113.64 5.96 5 8 0 111.59 7.08 5 8 0 122.39 6.58 5 8 0 121.06 6.89 5 8 0 123.87 6.17 5 8 0 116.15 7.02 5 8 0 120.69 7.05 -6 -8 0 134.88 7.72 6 -8 0 137.85 7.69 -6 -8 0 121.98 6.75 -6 -8 0 130.79 7.69 -6 -8 0 128.30 7.03 6 -8 0 145.88 7.01 -6 -8 0 117.25 7.32 6 -8 0 111.43 7.52 6 8 0 134.82 6.44 6 8 0 135.23 7.74 6 8 0 132.93 6.43 6 8 0 134.82 7.17 6 8 0 119.64 7.25 6 8 0 121.71 6.01 6 8 0 134.92 7.01 6 8 0 115.99 7.49 6 8 0 132.73 7.69 6 8 0 133.28 6.51 6 8 0 130.70 7.52 6 8 0 135.90 6.71 -7 -8 0 1.29 0.22 7 -8 0 2.01 0.26 -7 -8 0 1.89 0.23 -7 -8 0 1.43 0.18 7 8 0 1.02 0.14 7 8 0 1.09 0.17 7 8 0 1.32 0.17 7 8 0 1.42 0.18 7 8 0 0.95 0.18 7 8 0 1.37 0.16 7 8 0 1.67 0.24 -8 -8 0 5.76 0.45 8 -8 0 5.53 0.43 -8 -8 0 5.47 0.39 -8 -8 0 5.83 0.41 8 8 0 6.00 0.36 8 8 0 5.90 0.36 8 8 0 6.33 0.38 8 8 0 5.80 0.41 8 8 0 5.79 0.40 8 8 0 6.53 0.43 0 -9 0 0.05 0.07 0 -9 0 0.01 0.04 0 -9 0 0.04 0.08 0 -9 0 0.05 0.08 0 -9 0 -0.04 0.09 0 -9 0 -0.02 0.10 0 9 0 -0.05 0.07 -1 -9 0 28.06 1.84 -1 -9 0 31.18 1.60 1 -9 0 27.92 1.58 1 -9 0 30.56 1.83 1 -9 0 31.75 1.59 1 -9 0 30.31 1.43 -1 -9 0 28.26 1.52 -1 -9 0 31.84 1.84 1 -9 0 31.60 1.84 1 -9 0 31.86 2.14 -1 -9 0 29.13 1.45 1 -9 0 31.57 1.82 -1 -9 0 31.57 1.91 -1 -9 0 31.67 1.83 1 -9 0 29.60 1.53 1 9 0 28.78 1.63 1 9 0 31.22 1.87 2 -9 0 9.11 0.47 -2 -9 0 9.13 0.78 2 -9 0 9.28 0.80 -2 -9 0 9.53 0.53 -2 -9 0 9.12 0.64 -2 -9 0 9.75 0.57 2 -9 0 9.65 0.47 -2 -9 0 9.62 0.59 -2 -9 0 10.34 0.64 2 -9 0 9.26 0.51 -2 -9 0 8.56 0.52 2 -9 0 9.60 0.65 2 9 0 9.26 0.65 2 9 0 8.80 0.56 2 9 0 9.72 0.63 2 9 0 8.59 0.76 -3 -9 0 3.22 0.27 3 -9 0 2.78 0.29 -3 -9 0 3.57 0.27 -3 -9 0 2.93 0.30 -3 -9 0 3.44 0.27 3 -9 0 3.03 0.19 -3 -9 0 2.94 0.30 -3 -9 0 2.84 0.24 3 -9 0 3.84 0.43 -3 -9 0 3.55 0.30 3 -9 0 3.07 0.16 -3 -9 0 2.67 0.22 -3 -9 0 2.65 0.24 -3 -9 0 2.94 0.44 -3 -9 0 2.53 0.26 -3 -9 0 3.25 0.26 -3 -9 0 3.39 0.24 3 9 0 3.53 0.26 3 9 0 2.66 0.25 3 9 0 2.94 0.24 3 9 0 3.08 0.28 3 9 0 3.00 0.32 3 9 0 2.58 0.29 3 9 0 3.11 0.25 3 9 0 3.19 0.26 3 9 0 3.04 0.43 3 9 0 3.70 0.29 4 -9 0 10.34 0.67 -4 -9 0 11.05 0.69 4 -9 0 10.80 0.73 -4 -9 0 10.77 0.73 -4 -9 0 10.70 0.67 -4 -9 0 9.42 0.62 -4 -9 0 9.76 0.66 -4 -9 0 10.11 0.63 -4 -9 0 10.71 0.63 -4 -9 0 9.93 0.65 -4 -9 0 11.10 0.73 4 -9 0 9.96 0.91 4 9 0 9.99 0.74 4 9 0 9.91 0.69 4 9 0 11.63 0.68 4 9 0 10.55 0.65 4 9 0 11.17 0.62 4 9 0 11.35 0.68 4 9 0 9.96 0.66 4 9 0 9.40 0.58 -4 9 0 8.56 0.79 4 9 0 10.44 0.61 4 9 0 11.33 0.73 4 9 0 11.05 0.72 4 9 0 11.51 0.64 -5 -9 0 0.21 0.10 -5 -9 0 0.28 0.13 -5 -9 0 0.25 0.11 -5 -9 0 0.63 0.16 -5 -9 0 0.15 0.15 5 -9 0 0.11 0.11 -5 -9 0 0.44 0.12 5 -9 0 0.34 0.13 5 -9 0 0.37 0.20 -5 -9 0 0.25 0.12 -5 -9 0 0.15 0.12 5 9 0 0.18 0.10 5 9 0 0.36 0.13 5 9 0 0.42 0.12 5 9 0 0.36 0.13 5 9 0 0.17 0.14 5 9 0 0.24 0.12 5 9 0 0.30 0.12 5 9 0 0.16 0.10 5 9 0 0.22 0.13 5 9 0 0.39 0.10 5 9 0 0.29 0.12 -6 -9 0 103.74 6.82 -6 -9 0 127.25 7.19 6 -9 0 118.02 7.16 6 -9 0 114.26 7.04 -6 -9 0 110.88 6.29 -6 -9 0 126.35 6.56 6 -9 0 125.77 6.53 -6 -9 0 132.19 7.21 6 9 0 122.83 7.02 6 9 0 104.21 6.76 6 9 0 123.71 6.69 6 9 0 102.92 6.27 6 9 0 122.17 6.27 6 9 0 126.81 6.54 6 9 0 131.67 7.18 6 9 0 119.38 6.01 6 9 0 130.13 5.62 6 9 0 130.79 6.08 7 -9 0 0.81 0.16 -7 -9 0 0.97 0.16 -7 -9 0 0.93 0.19 -7 -9 0 0.79 0.13 -7 -9 0 0.54 0.15 -7 -9 0 1.00 0.16 7 9 0 0.63 0.15 7 9 0 0.57 0.10 7 9 0 0.50 0.13 7 9 0 0.67 0.12 7 9 0 0.60 0.13 7 9 0 0.90 0.14 7 9 0 0.66 0.12 7 9 0 0.56 0.12 -8 -9 0 0.52 0.13 -8 -9 0 0.55 0.11 -8 -9 0 0.62 0.11 8 9 0 0.66 0.09 8 9 0 0.60 0.10 8 9 0 0.66 0.10 8 9 0 0.78 0.13 8 9 0 0.65 0.13 8 9 0 0.72 0.12 0 -10 0 286.39 14.21 0 -10 0 285.11 15.34 0 -10 0 257.14 16.29 0 -10 0 283.69 16.04 0 -10 0 281.96 12.90 0 -10 0 288.23 13.96 0 -10 0 274.04 15.58 0 -10 0 285.26 15.54 0 -10 0 289.16 13.65 0 10 0 270.59 16.40 -1 -10 0 22.86 1.42 -1 -10 0 22.75 1.38 -1 -10 0 22.86 1.24 1 -10 0 23.49 1.42 1 -10 0 22.83 1.43 -1 -10 0 22.76 1.24 1 -10 0 24.11 1.41 -1 -10 0 22.96 1.21 1 -10 0 23.10 1.10 -1 -10 0 23.69 1.53 1 -10 0 22.66 1.29 -1 -10 0 23.03 1.11 1 -10 0 21.70 1.20 -1 -10 0 23.23 1.32 1 -10 0 22.59 1.18 1 -10 0 21.45 1.22 -1 -10 0 22.74 1.23 -1 -10 0 23.39 1.42 -1 -10 0 22.47 1.32 1 10 0 22.04 1.26 1 10 0 24.18 1.45 -2 -10 0 1.32 0.20 -2 -10 0 1.98 0.22 2 -10 0 1.88 0.22 2 -10 0 1.79 0.15 -2 -10 0 1.77 0.21 -2 -10 0 1.46 0.32 -2 -10 0 2.09 0.19 -2 -10 0 1.69 0.17 -2 -10 0 2.21 0.19 -2 -10 0 1.54 0.19 -2 -10 0 1.77 0.21 2 -10 0 1.66 0.12 -2 -10 0 1.61 0.21 -2 -10 0 1.86 0.22 -2 -10 0 1.66 0.21 2 -10 0 1.81 0.14 -2 -10 0 1.58 0.18 -2 -10 0 1.92 0.20 2 -10 0 2.10 0.31 -2 -10 0 1.52 0.19 -2 -10 0 1.31 0.18 2 10 0 1.61 0.20 2 10 0 1.87 0.19 2 10 0 1.97 0.23 2 10 0 1.52 0.21 2 10 0 1.77 0.19 2 10 0 1.76 0.24 -3 -10 0 37.76 1.96 -3 -10 0 41.85 2.35 -3 -10 0 39.56 2.26 -3 -10 0 39.90 2.02 -3 -10 0 39.85 2.28 -3 -10 0 40.01 2.11 -3 -10 0 37.74 2.04 -3 -10 0 36.56 2.20 3 -10 0 40.09 2.73 -3 -10 0 37.71 2.20 3 -10 0 39.50 1.88 -3 -10 0 37.25 2.33 3 -10 0 33.60 1.74 -3 -10 0 40.64 2.12 -3 -10 0 41.72 2.03 3 -10 0 37.82 2.31 3 -10 0 39.73 2.32 3 10 0 36.49 2.21 3 10 0 40.58 2.13 3 10 0 36.13 2.33 3 10 0 36.71 2.04 3 10 0 38.60 2.13 3 10 0 40.73 2.21 3 10 0 35.27 2.04 3 10 0 37.19 2.45 3 10 0 34.19 2.34 3 10 0 34.06 2.24 -4 -10 0 74.86 4.70 -4 -10 0 83.52 4.57 -4 -10 0 82.78 4.21 -4 -10 0 72.42 4.81 -4 -10 0 80.03 4.83 4 -10 0 77.78 4.79 -4 -10 0 74.39 4.67 4 -10 0 85.13 5.49 -4 -10 0 80.54 4.22 -4 -10 0 86.29 4.40 -4 -10 0 80.13 4.57 -4 -10 0 81.28 4.11 -4 -10 0 83.53 4.27 4 10 0 82.08 4.58 4 10 0 79.98 4.71 4 10 0 87.56 4.29 -4 10 0 79.94 4.88 4 10 0 81.22 4.83 4 10 0 80.07 4.57 4 10 0 78.88 4.04 4 10 0 75.52 4.67 4 10 0 80.81 4.83 4 10 0 79.09 4.40 4 10 0 82.76 4.23 4 10 0 83.50 4.21 -5 -10 0 126.96 7.07 -5 -10 0 118.48 8.06 -5 -10 0 140.44 7.08 -5 -10 0 138.01 7.39 5 -10 0 114.42 7.89 5 -10 0 134.48 7.32 -5 -10 0 139.47 7.08 -5 -10 0 135.66 7.09 -5 -10 0 144.30 8.12 -5 -10 0 139.71 7.70 -5 -10 0 145.36 7.67 5 10 0 136.35 6.78 5 10 0 143.62 7.55 5 10 0 138.68 7.87 5 10 0 136.26 7.38 5 10 0 122.63 7.64 5 10 0 143.58 8.07 5 10 0 136.78 7.08 5 10 0 135.63 7.91 5 10 0 144.92 8.11 5 10 0 144.80 7.09 -6 -10 0 2.98 0.28 -6 -10 0 3.01 0.32 6 -10 0 3.07 0.31 -6 -10 0 3.62 0.29 -6 -10 0 3.21 0.28 -6 -10 0 2.83 0.35 6 -10 0 3.57 0.47 -6 -10 0 4.01 0.34 6 10 0 3.58 0.24 6 10 0 3.28 0.25 6 10 0 2.82 0.30 6 10 0 3.08 0.27 6 10 0 3.25 0.35 6 10 0 3.80 0.32 6 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0 1.04 0.14 1 -11 0 0.81 0.12 1 -11 0 0.88 0.13 1 -11 0 0.88 0.09 1 -11 0 0.80 0.11 -1 -11 0 0.80 0.16 1 -11 0 0.90 0.13 1 -11 0 0.87 0.17 1 11 0 1.04 0.15 1 11 0 1.02 0.19 1 11 0 0.74 0.15 1 11 0 1.05 0.16 -2 -11 0 32.61 2.05 -2 -11 0 33.55 2.01 2 -11 0 30.84 1.97 -2 -11 0 33.30 1.62 2 -11 0 34.83 1.69 2 -11 0 34.31 1.58 -2 -11 0 34.65 1.80 -2 -11 0 33.27 1.87 -2 -11 0 33.99 2.06 -2 -11 0 33.92 1.80 2 -11 0 31.98 2.05 -2 -11 0 33.96 2.06 -2 -11 0 35.02 1.81 2 -11 0 34.95 1.57 -2 -11 0 34.27 2.07 -2 -11 0 35.03 1.94 -2 -11 0 34.26 2.05 -2 -11 0 33.69 1.72 -2 -11 0 32.70 1.75 -2 -11 0 35.07 2.01 -2 -11 0 33.74 1.74 -2 -11 0 33.51 1.92 2 11 0 33.11 2.07 2 11 0 31.49 2.08 2 11 0 32.42 1.88 2 11 0 32.97 1.96 2 11 0 33.74 1.83 -3 -11 0 7.09 0.51 -3 -11 0 7.73 0.55 3 -11 0 5.54 0.53 -3 -11 0 7.23 0.50 -3 -11 0 6.67 0.43 -3 -11 0 6.12 0.54 -3 -11 0 7.07 0.53 -3 -11 0 7.32 0.47 -3 -11 0 7.20 0.49 -3 -11 0 7.29 0.50 3 -11 0 8.19 0.39 -3 -11 0 6.91 0.46 -3 -11 0 7.15 0.51 -3 -11 0 7.28 0.55 -3 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3.76 1 -12 0 65.12 3.25 -1 -12 0 62.94 3.79 1 -12 0 64.27 3.74 -1 -12 0 66.00 3.38 1 -12 0 64.42 2.98 1 12 0 69.18 3.88 -1 12 0 59.73 3.65 1 12 0 64.09 3.40 1 12 0 68.24 3.67 1 12 0 59.34 3.86 2 -12 0 20.16 1.49 -2 -12 0 22.60 1.47 -2 -12 0 24.66 1.40 -2 -12 0 24.38 1.25 -2 -12 0 23.85 1.17 -2 -12 0 24.18 1.35 -2 -12 0 24.21 1.51 -2 -12 0 22.96 1.48 2 -12 0 23.77 1.24 2 -12 0 23.46 1.13 -2 -12 0 22.85 1.39 -2 -12 0 23.22 1.29 2 -12 0 25.07 1.14 2 -12 0 22.13 1.41 -2 -12 0 24.62 1.46 -2 -12 0 24.17 1.37 -2 -12 0 23.48 1.31 -2 -12 0 25.91 1.26 -2 -12 0 25.12 1.46 2 -12 0 25.08 1.23 2 12 0 24.71 1.34 2 12 0 24.18 1.42 2 12 0 22.37 1.50 -3 -12 0 28.37 1.74 -3 -12 0 28.65 1.74 -3 -12 0 27.66 1.52 -3 -12 0 28.35 1.68 -3 -12 0 28.06 1.62 3 -12 0 27.42 1.37 3 -12 0 23.64 1.72 -3 -12 0 27.03 1.37 -3 -12 0 27.68 1.45 -3 -12 0 27.86 1.45 -3 -12 0 29.75 1.57 -3 -12 0 25.78 1.74 -3 -12 0 28.13 1.69 -3 -12 0 29.16 1.60 -3 -12 0 27.00 1.62 -3 -12 0 27.83 1.73 3 12 0 26.16 1.61 3 12 0 28.76 1.58 3 12 0 28.52 1.64 3 12 0 27.75 1.65 3 12 0 27.77 1.75 -4 -12 0 27.40 1.41 -4 -12 0 27.79 1.70 -4 -12 0 27.08 1.63 -4 -12 0 26.56 1.68 -4 -12 0 25.97 1.69 -4 -12 0 27.55 1.57 -4 -12 0 27.91 1.47 -4 -12 0 26.84 1.47 4 -12 0 22.59 1.67 -4 -12 0 26.82 1.58 -4 -12 0 26.55 1.60 4 12 0 27.84 1.71 4 12 0 22.42 1.67 4 12 0 27.70 1.48 4 12 0 27.65 1.58 4 12 0 29.00 1.60 4 12 0 25.83 1.57 4 12 0 28.32 1.45 4 12 0 24.54 1.52 -5 -12 0 38.61 2.22 -5 -12 0 33.53 1.88 -5 -12 0 29.76 2.06 5 -12 0 37.58 2.21 -5 -12 0 33.33 2.19 -5 -12 0 36.75 1.84 -5 -12 0 36.59 2.06 -5 -12 0 37.89 1.93 5 12 0 33.23 2.06 5 12 0 37.62 1.93 5 12 0 37.39 1.84 5 12 0 37.52 2.14 5 12 0 37.08 2.21 5 12 0 30.14 2.18 -6 -12 0 12.59 0.76 6 -12 0 11.73 0.87 -6 -12 0 11.53 0.72 -6 -12 0 10.28 0.79 -6 -12 0 11.98 0.70 -6 -12 0 11.72 0.73 -6 -12 0 11.29 0.81 6 12 0 12.71 0.79 6 12 0 12.27 0.74 6 12 0 11.65 0.70 6 12 0 12.12 0.70 6 12 0 11.55 0.76 6 12 0 11.72 0.75 6 12 0 11.80 0.66 6 12 0 11.72 0.60 -7 -12 0 36.99 1.93 -7 -12 0 34.59 2.12 -7 -12 0 34.81 1.99 -7 -12 0 33.03 2.00 7 12 0 34.72 1.84 7 12 0 33.93 1.75 7 12 0 33.29 1.96 7 12 0 36.82 2.06 0 -13 0 -0.02 0.07 0 -13 0 0.02 0.07 0 -13 0 -0.01 0.11 0 -13 0 0.02 0.08 0 -13 0 -0.01 0.09 0 -13 0 0.08 0.08 0 -13 0 0.01 0.12 0 -13 0 0.00 0.09 0 -13 0 0.02 0.06 0 -13 0 0.10 0.11 0 13 0 0.06 0.09 0 13 0 0.13 0.11 -1 -13 0 167.48 9.53 1 -13 0 162.11 8.26 1 -13 0 161.07 9.51 -1 -13 0 167.47 8.27 1 -13 0 171.79 9.05 1 -13 0 168.56 9.84 1 -13 0 161.79 7.53 -1 -13 0 161.91 8.45 -1 -13 0 164.99 9.20 1 -13 0 165.72 8.28 -1 -13 0 167.54 9.08 -1 -13 0 168.37 8.16 1 -13 0 155.75 9.53 -1 -13 0 176.66 8.53 -1 -13 0 174.97 8.12 -1 -13 0 138.25 8.28 -1 -13 0 162.42 9.54 -1 -13 0 157.81 9.53 -1 -13 0 166.10 9.08 -1 -13 0 168.59 9.85 1 13 0 166.85 9.81 1 13 0 168.84 9.75 1 13 0 173.74 9.31 -1 13 0 153.23 9.29 1 13 0 171.18 8.58 -2 -13 0 69.59 4.26 -2 -13 0 72.89 4.18 -2 -13 0 72.53 3.76 -2 -13 0 70.72 4.02 -2 -13 0 70.94 3.59 2 -13 0 71.70 3.27 -2 -13 0 71.64 4.21 -2 -13 0 74.49 3.98 -2 -13 0 71.47 4.16 2 -13 0 71.81 3.60 -2 -13 0 74.96 3.57 -2 -13 0 69.73 3.73 2 -13 0 71.68 3.52 2 -13 0 73.06 3.27 2 -13 0 70.36 4.28 -2 -13 0 75.48 3.62 -2 -13 0 70.81 4.28 -2 -13 0 70.86 3.88 2 -13 0 61.07 4.19 2 13 0 65.92 4.29 2 13 0 72.47 4.07 -3 -13 0 10.26 0.68 -3 -13 0 8.13 0.63 -3 -13 0 9.93 0.65 -3 -13 0 10.77 0.70 -3 -13 0 10.44 0.74 -3 -13 0 10.50 0.62 -3 -13 0 10.72 0.67 -3 -13 0 9.84 0.69 -3 -13 0 10.44 0.59 3 -13 0 9.44 0.73 -3 -13 0 8.93 0.60 -3 -13 0 10.34 0.67 -3 -13 0 10.84 0.55 -3 -13 0 10.12 0.57 3 13 0 9.72 0.65 3 13 0 8.68 0.61 3 13 0 9.86 0.64 3 13 0 8.70 0.72 3 13 0 10.80 0.73 -4 -13 0 69.53 3.31 -4 -13 0 69.67 4.19 -4 -13 0 74.71 3.52 -4 -13 0 73.94 4.21 -4 -13 0 59.26 3.81 -4 -13 0 69.51 4.13 -4 -13 0 69.21 4.10 -4 -13 0 70.95 4.07 -4 -13 0 71.10 3.92 4 -13 0 69.42 4.14 -4 -13 0 71.35 3.60 -4 -13 0 63.32 3.71 4 13 0 71.39 3.69 4 13 0 71.27 3.66 4 13 0 72.73 3.99 4 13 0 72.00 4.22 4 13 0 71.26 3.98 4 13 0 65.30 3.74 -5 -13 0 0.89 0.17 -5 -13 0 1.12 0.18 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1.15 -1 -14 0 18.18 1.26 -1 -14 0 21.92 1.34 1 -14 0 22.90 1.38 -1 14 0 22.82 1.30 1 14 0 22.61 1.42 1 14 0 21.97 1.30 1 14 0 22.48 1.25 -2 -14 0 77.36 4.43 2 -14 0 82.09 3.64 -2 -14 0 81.37 4.69 -2 -14 0 66.79 3.97 2 -14 0 83.45 4.79 -2 -14 0 82.18 4.03 -2 -14 0 84.90 4.48 2 -14 0 82.19 3.92 2 -14 0 81.45 3.64 -2 -14 0 69.63 4.07 -2 -14 0 68.37 4.64 2 -14 0 82.48 4.02 -2 -14 0 79.74 4.32 2 -14 0 85.07 4.70 -2 -14 0 69.19 4.15 -2 -14 0 82.81 4.18 -2 -14 0 81.94 4.78 -2 -14 0 67.36 4.64 -2 -14 0 83.52 4.01 2 14 0 84.49 4.36 2 14 0 85.87 4.80 2 14 0 83.52 4.80 2 14 0 85.33 4.21 -3 -14 0 233.80 13.44 -3 -14 0 244.28 12.85 -3 -14 0 216.34 11.53 3 -14 0 242.51 13.45 -3 -14 0 239.65 12.84 -3 -14 0 232.22 11.95 -3 -14 0 237.59 11.68 -3 -14 0 244.29 12.57 -3 -14 0 242.05 13.79 3 -14 0 234.53 13.90 -3 -14 0 242.47 11.71 -3 -14 0 204.96 13.02 3 14 0 205.47 13.13 3 14 0 230.61 13.82 3 14 0 245.05 13.75 3 14 0 240.74 12.08 -4 -14 0 7.29 0.42 4 -14 0 7.16 0.59 -4 -14 0 7.24 0.58 -4 -14 0 6.74 0.48 -4 -14 0 7.41 0.53 -4 -14 0 6.55 0.49 -4 -14 0 7.49 0.53 -4 -14 0 8.45 0.56 -4 -14 0 7.81 0.49 -4 -14 0 7.69 0.52 -4 -14 0 7.98 0.51 -4 -14 0 7.69 0.46 -4 -14 0 7.94 0.53 4 14 0 6.71 0.55 4 14 0 7.13 0.58 4 14 0 7.95 0.50 4 14 0 7.25 0.45 4 14 0 6.78 0.49 4 14 0 8.13 0.55 4 14 0 7.70 0.50 -5 -14 0 29.43 1.55 -5 -14 0 29.36 1.80 5 -14 0 29.37 1.85 -5 -14 0 32.01 1.86 -5 -14 0 30.99 1.74 -5 -14 0 30.40 1.68 -5 -14 0 33.40 1.63 -5 -14 0 25.22 1.58 -5 -14 0 29.74 1.83 -5 -14 0 27.76 1.44 5 14 0 29.04 1.55 5 14 0 30.73 1.63 5 14 0 31.81 1.87 5 14 0 29.73 1.68 5 14 0 30.79 1.75 -6 -14 0 1.74 0.20 -6 -14 0 2.06 0.18 -6 -14 0 1.74 0.18 -6 -14 0 1.76 0.22 -6 -14 0 1.67 0.17 6 14 0 1.77 0.18 6 14 0 1.84 0.18 6 14 0 1.80 0.17 6 14 0 1.74 0.20 6 14 0 1.68 0.20 6 14 0 2.00 0.17 0 -15 0 0.04 0.08 0 -15 0 0.02 0.12 0 -15 0 -0.06 0.10 0 -15 0 0.00 0.08 0 -15 0 0.06 0.07 0 -15 0 0.32 0.13 0 -15 0 0.02 0.07 0 -15 0 0.04 0.08 0 -15 0 0.20 0.13 0 15 0 0.14 0.12 0 15 0 0.06 0.08 -1 -15 0 80.59 3.79 1 -15 0 61.53 3.63 1 -15 0 77.85 3.72 -1 -15 0 77.85 4.34 1 -15 0 71.90 4.29 1 -15 0 72.68 3.75 1 -15 0 75.45 4.26 -1 -15 0 74.87 3.68 -1 -15 0 72.95 3.83 -1 -15 0 74.36 3.65 1 -15 0 78.64 4.35 1 -15 0 73.38 3.39 -1 -15 0 69.58 4.29 1 -15 0 70.65 4.42 -1 15 0 73.14 4.17 1 15 0 76.47 4.42 1 15 0 65.43 4.18 1 15 0 74.05 3.88 -2 -15 0 27.73 1.76 2 -15 0 29.07 1.41 2 -15 0 29.30 1.78 -2 -15 0 29.20 1.51 -2 -15 0 28.38 1.73 2 -15 0 27.79 1.46 -2 -15 0 26.48 1.47 2 -15 0 29.53 1.76 -2 -15 0 27.91 1.55 -2 -15 0 24.80 1.52 2 15 0 29.26 1.61 2 15 0 28.86 1.57 2 15 0 29.21 1.80 2 15 0 27.34 1.77 -3 -15 0 1.12 0.14 -3 -15 0 0.75 0.16 -3 -15 0 0.94 0.18 -3 -15 0 0.84 0.18 -3 -15 0 0.89 0.15 -3 -15 0 0.78 0.14 3 -15 0 1.09 0.12 -3 -15 0 1.08 0.15 3 -15 0 0.91 0.19 -3 -15 0 0.88 0.15 -3 -15 0 0.93 0.16 -3 -15 0 0.60 0.11 3 -15 0 0.85 0.18 -3 -15 0 1.07 0.18 3 15 0 1.03 0.17 3 15 0 0.83 0.18 3 15 0 1.12 0.18 3 15 0 0.90 0.16 3 15 0 1.16 0.21 -4 -15 0 9.49 0.60 -4 -15 0 9.05 0.53 -4 -15 0 8.53 0.57 -4 -15 0 8.35 0.55 4 -15 0 8.74 0.64 -4 -15 0 8.28 0.59 -4 -15 0 8.36 0.54 -4 -15 0 10.25 0.61 -4 -15 0 8.75 0.51 4 -15 0 7.97 0.61 -4 -15 0 8.34 0.56 4 15 0 8.30 0.62 4 15 0 8.18 0.63 4 15 0 8.80 0.56 4 15 0 9.22 0.56 4 15 0 8.51 0.59 -5 -15 0 1.48 0.18 -5 -15 0 1.38 0.19 -5 -15 0 1.47 0.16 -5 -15 0 1.46 0.19 -5 -15 0 1.45 0.17 -5 -15 0 1.39 0.18 -5 -15 0 1.66 0.16 5 15 0 1.30 0.18 5 15 0 1.56 0.17 5 15 0 1.49 0.22 5 15 0 1.36 0.17 5 15 0 1.26 0.17 0 -16 0 135.16 6.90 0 -16 0 134.53 6.43 0 -16 0 142.26 7.70 0 -16 0 149.34 8.13 0 -16 0 138.45 8.14 0 -16 0 142.66 7.08 0 -16 0 146.03 8.12 0 16 0 144.13 7.93 0 16 0 132.32 7.32 1 -16 0 29.33 1.44 1 -16 0 28.51 1.33 1 -16 0 29.47 1.47 -1 -16 0 28.84 1.41 -1 -16 0 27.16 1.60 -1 -16 0 29.79 1.74 1 -16 0 24.64 1.75 1 -16 0 28.88 1.67 1 -16 0 25.56 1.33 -1 -16 0 29.87 1.49 -1 -16 0 28.01 1.76 -1 -16 0 25.03 1.69 -1 -16 0 26.94 1.70 1 -16 0 29.04 1.76 -1 -16 0 29.50 1.51 1 -16 0 29.20 1.71 -1 -16 0 30.73 1.55 1 16 0 27.63 1.78 1 16 0 29.37 1.57 1 16 0 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12.17 0.69 6 4 -3 13.21 0.78 6 4 -3 11.50 0.74 6 4 -3 11.53 0.57 6 4 -3 11.09 0.76 -5 -4 3 22.84 1.55 5 -4 -3 23.42 1.39 -5 -4 3 27.16 1.59 5 -4 -3 24.39 1.27 5 -4 -3 25.55 1.19 -5 -4 3 26.84 1.47 5 -4 -3 23.61 1.53 -5 -4 3 25.34 1.38 5 -4 -3 24.92 1.48 5 -4 -3 24.40 1.29 5 -4 -3 25.14 1.58 5 -4 -3 25.32 1.44 5 4 -3 24.92 1.21 5 4 -3 23.74 1.50 5 4 -3 25.79 1.35 5 4 -3 26.74 1.40 5 4 -3 25.55 1.54 5 4 -3 26.26 1.44 5 4 -3 25.94 1.51 5 4 -3 21.32 1.53 5 4 -3 26.17 1.70 5 4 -3 25.34 1.30 5 4 -3 24.52 1.29 5 4 -3 23.30 1.44 5 4 -3 25.33 1.55 5 4 -3 23.91 1.44 5 4 -3 24.00 1.32 -4 -4 3 310.15 15.08 4 -4 -3 297.60 16.13 -4 -4 3 304.89 17.12 -4 -4 3 297.19 16.26 4 -4 -3 297.90 15.54 4 -4 -3 295.96 13.25 4 -4 -3 298.55 15.17 4 -4 -3 296.61 14.22 4 -4 -3 291.09 16.72 -4 -4 3 282.77 14.87 4 -4 -3 289.64 14.77 4 4 -3 291.78 15.03 4 4 -3 250.75 14.84 4 4 -3 289.24 16.24 4 4 -3 290.25 17.10 3 -4 -3 343.61 16.59 -3 -4 3 326.10 17.76 3 -4 -3 323.16 16.26 3 -4 -3 297.70 18.30 3 -4 -3 328.17 17.67 -3 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1.76 6 2 -4 34.76 2.04 6 2 -4 34.83 1.94 6 2 -4 34.78 1.82 6 2 -4 35.47 1.74 6 2 -4 32.33 1.93 6 2 -4 32.33 1.95 6 2 -4 34.17 1.85 6 2 -4 32.85 2.04 -6 2 4 33.66 1.98 6 2 -4 35.09 1.78 6 2 -4 34.09 2.09 6 2 -4 35.59 1.77 -6 2 4 36.31 2.35 -5 -2 4 20.43 1.16 5 -2 -4 20.67 1.19 -5 -2 4 17.15 1.23 5 -2 -4 19.27 1.21 -5 -2 4 21.00 1.27 5 -2 -4 18.34 1.20 5 -2 -4 21.20 1.17 5 -2 -4 20.03 1.07 -5 -2 4 19.15 1.10 5 -2 -4 18.92 1.05 5 -2 -4 20.53 1.03 5 -2 -4 19.43 1.00 5 -2 -4 20.15 1.04 5 -2 -4 18.99 1.29 5 -2 -4 20.33 1.32 5 -2 -4 18.84 1.12 5 2 -4 20.88 1.17 5 2 -4 19.63 1.10 -5 2 4 20.26 1.25 5 2 -4 19.56 1.21 5 2 -4 19.38 1.06 5 2 -4 18.62 1.02 -5 2 4 19.82 1.16 5 2 -4 19.78 1.03 5 2 -4 18.98 1.14 5 2 -4 19.53 1.37 5 2 -4 20.35 1.20 -5 2 4 20.05 1.25 5 2 -4 19.58 1.20 5 2 -4 17.40 1.11 5 2 -4 16.65 1.20 5 2 -4 18.77 1.07 5 2 -4 17.83 1.11 5 2 -4 19.37 1.14 -5 2 4 18.60 1.15 5 2 -4 20.65 0.96 4 -2 -4 37.20 2.07 -4 -2 4 37.52 2.27 4 -2 -4 38.52 1.97 4 -2 -4 39.32 2.18 -4 -2 4 33.33 1.83 4 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26.07 0 2 -4 485.72 24.36 -1 -2 -4 270.97 13.88 -1 -2 -4 237.43 12.72 1 -2 4 239.92 13.82 -1 -2 -4 251.11 12.95 1 -2 4 257.84 12.74 -1 2 -4 254.82 12.88 1 2 4 272.09 12.73 1 2 4 225.71 13.85 -1 2 -4 249.12 13.83 3 -2 4 292.91 13.48 -3 -2 -4 311.05 15.39 3 -2 4 304.04 17.32 3 -2 4 300.60 15.82 3 -2 4 316.37 13.55 3 -2 4 294.30 16.35 -3 -2 -4 283.61 17.41 -3 2 -4 251.46 17.19 3 2 4 315.41 16.46 3 2 4 304.97 13.77 3 2 4 302.51 15.12 4 -2 4 169.11 7.60 4 -2 4 175.50 9.81 4 -2 4 176.71 7.60 4 -2 4 167.58 8.16 4 -2 4 165.06 8.95 -4 -2 -4 148.00 9.83 4 2 4 167.65 8.52 4 2 4 170.14 8.19 4 2 4 168.53 9.35 5 -2 4 55.79 2.70 5 -2 4 58.02 3.04 5 -2 4 52.56 2.51 5 -2 4 59.11 2.51 -5 -2 -4 52.86 3.13 5 -2 4 57.18 3.34 5 2 4 53.43 3.21 5 2 4 51.04 2.86 5 2 4 56.64 2.75 5 2 4 55.82 2.79 5 2 4 56.53 2.57 5 2 4 57.13 3.21 5 2 4 51.49 3.31 5 2 4 54.14 2.73 5 2 4 53.36 3.05 6 -2 4 7.30 0.52 6 2 4 7.24 0.41 6 2 4 6.69 0.47 6 2 4 7.23 0.49 6 2 4 6.57 0.43 6 2 4 7.36 0.43 6 2 4 7.02 0.42 7 -2 4 0.06 0.13 7 2 4 0.13 0.06 7 2 4 0.04 0.07 7 2 4 0.16 0.07 7 2 4 0.11 0.06 7 2 4 0.06 0.07 7 2 4 0.10 0.07 8 -2 4 3.56 0.31 8 2 4 3.00 0.27 8 2 4 3.35 0.23 9 -2 4 0.11 0.06 9 2 4 0.15 0.07 9 2 4 0.13 0.05 -9 -3 4 6.52 0.44 9 -3 -4 7.35 0.47 9 -3 -4 6.82 0.39 9 3 -4 6.89 0.40 9 3 -4 7.45 0.48 -8 -3 4 1.90 0.25 -8 -3 4 1.90 0.23 8 -3 -4 2.11 0.26 8 -3 -4 1.73 0.21 8 -3 -4 2.09 0.17 -8 -3 4 2.11 0.21 8 3 -4 2.18 0.20 8 3 -4 1.74 0.23 8 3 -4 2.10 0.22 8 3 -4 1.91 0.17 8 3 -4 1.86 0.16 8 3 -4 2.05 0.22 8 3 -4 2.03 0.25 8 3 -4 1.97 0.20 7 -3 -4 69.16 3.12 -7 -3 4 68.79 4.09 -7 -3 4 72.94 3.60 7 -3 -4 63.31 3.35 7 -3 -4 73.20 4.09 7 -3 -4 69.94 3.43 7 -3 -4 67.09 3.74 7 -3 -4 65.25 3.12 7 -3 -4 64.97 3.93 -7 -3 4 60.50 3.86 7 3 -4 71.40 3.38 -7 3 4 66.70 3.86 7 3 -4 71.37 3.74 7 3 -4 63.36 4.08 7 3 -4 72.10 3.98 7 3 -4 61.66 3.40 7 3 -4 69.24 3.54 6 -3 -4 -0.01 0.07 -6 -3 4 0.10 0.09 6 -3 -4 -0.02 0.06 -6 -3 4 0.01 0.13 6 -3 -4 0.18 0.09 6 -3 -4 0.20 0.10 6 -3 -4 0.05 0.11 6 -3 -4 0.11 0.06 6 -3 -4 0.01 0.07 -6 -3 4 -0.05 0.12 6 3 -4 0.05 0.08 6 3 -4 0.02 0.08 6 3 -4 0.08 0.08 6 3 -4 0.09 0.08 6 3 -4 0.14 0.11 6 3 -4 0.13 0.14 6 3 -4 0.20 0.13 6 3 -4 0.28 0.09 6 3 -4 0.09 0.08 6 3 -4 -0.01 0.08 6 3 -4 0.11 0.08 6 3 -4 -0.01 0.11 -6 3 4 0.06 0.08 5 -3 -4 43.19 2.28 -5 -3 4 43.71 2.50 5 -3 -4 39.73 2.58 5 -3 -4 43.23 2.63 -5 -3 4 43.71 2.65 5 -3 -4 40.74 2.52 5 -3 -4 43.70 2.22 5 -3 -4 43.87 2.05 5 -3 -4 43.05 2.42 -5 -3 4 44.78 2.66 5 -3 -4 44.39 2.20 5 -3 -4 43.52 2.43 5 -3 -4 43.79 2.56 5 -3 -4 43.06 2.17 -5 -3 4 45.22 2.34 5 3 -4 44.38 2.64 5 3 -4 44.95 2.39 5 3 -4 45.81 2.46 5 3 -4 42.71 2.20 -5 3 4 39.88 2.49 5 3 -4 44.59 2.23 5 3 -4 44.62 2.57 5 3 -4 43.72 2.57 5 3 -4 41.78 2.62 5 3 -4 37.97 2.33 5 3 -4 36.71 2.32 5 3 -4 44.40 2.48 5 3 -4 47.25 2.31 5 3 -4 47.11 2.07 5 3 -4 46.98 2.44 4 -3 -4 39.39 2.20 -4 -3 4 36.61 2.45 4 -3 -4 41.22 2.39 -4 -3 4 41.66 2.42 4 -3 -4 41.41 2.00 4 -3 -4 39.69 2.21 4 -3 -4 40.63 2.30 -4 -3 4 37.87 1.95 -4 -3 4 39.89 2.16 -4 -3 4 40.86 2.12 4 -3 -4 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6.23 -2 -2 9 105.89 6.22 -2 -2 9 109.03 6.04 2 -2 -9 108.65 6.21 2 -2 -9 105.25 5.44 -2 -2 9 102.12 5.24 2 -2 -9 105.02 5.67 -2 -2 9 107.76 6.20 2 -2 -9 105.84 6.07 -2 -2 9 106.55 5.21 -2 -2 9 105.06 5.80 -2 -2 9 100.83 6.06 2 2 -9 109.05 5.89 -2 2 9 107.03 5.89 -2 2 9 102.49 5.47 2 2 -9 105.92 6.23 -2 2 9 105.67 5.90 2 2 -9 103.54 5.47 2 2 -9 104.77 5.67 2 2 -9 90.68 5.43 -2 2 9 105.20 5.43 -2 2 9 105.34 5.44 -2 2 9 104.12 6.23 -2 2 9 103.98 5.67 -2 2 9 106.60 5.90 -2 2 9 91.99 6.19 -2 2 9 91.51 5.05 2 2 -9 109.57 5.91 2 2 -9 104.97 5.44 -1 -2 9 60.55 3.59 1 -2 -9 64.90 3.62 -1 -2 9 68.49 3.14 1 -2 -9 61.03 3.83 -1 -2 9 66.15 3.22 1 -2 -9 57.72 3.82 -1 -2 9 62.90 3.34 -1 -2 9 63.90 3.80 -1 -2 9 63.39 3.19 -1 -2 9 62.66 3.81 1 -2 -9 65.93 3.48 -1 -2 9 63.03 3.56 -1 -2 9 64.93 3.39 1 -2 -9 63.43 3.40 -1 -2 9 65.91 3.73 -1 -2 9 59.08 3.80 -1 -2 9 64.01 3.00 1 -2 -9 61.51 3.33 1 -2 -9 61.34 3.34 1 -2 -9 62.71 3.61 -1 -2 9 62.07 3.71 -1 2 9 65.35 3.48 1 2 -9 69.71 3.63 -1 2 9 63.83 3.61 -1 2 9 61.33 3.82 1 2 -9 62.01 3.83 -1 2 9 62.20 3.61 -1 2 9 62.68 3.61 -1 2 9 63.12 3.72 -1 2 9 61.40 3.70 -1 2 9 64.56 3.13 -1 2 9 66.12 3.41 -1 2 9 61.03 3.30 -1 2 9 59.84 3.19 -1 2 9 62.27 3.34 1 2 -9 65.30 3.49 -1 2 9 65.19 3.83 0 -2 9 38.06 2.14 0 -2 9 37.44 1.89 0 -2 -9 37.92 2.09 0 -2 9 37.55 2.05 0 -2 9 39.67 2.00 0 -2 9 36.20 2.27 0 -2 -9 36.83 2.17 0 -2 9 37.23 1.92 0 -2 9 39.31 2.23 0 -2 9 37.21 1.91 0 -2 9 31.31 1.97 0 -2 9 37.56 1.78 0 -2 9 37.27 2.23 0 -2 9 38.19 1.95 0 -2 -9 37.93 2.31 0 -2 -9 37.41 2.10 0 -2 9 37.30 2.27 0 -2 -9 37.72 2.17 0 -2 9 38.47 2.13 0 -2 -9 32.77 2.00 0 2 -9 37.72 2.03 0 2 9 37.50 2.29 0 2 9 36.43 1.92 0 2 9 38.89 2.08 0 2 9 37.82 2.23 0 2 -9 36.64 2.30 0 2 9 37.73 2.22 0 2 9 37.54 1.88 0 2 9 37.15 2.14 0 2 9 37.37 2.00 0 2 9 37.83 2.08 0 2 -9 35.76 2.31 0 2 -9 35.56 2.08 0 2 9 38.29 2.22 0 2 9 36.47 1.92 0 2 9 36.34 2.29 0 2 9 36.95 2.16 0 2 -9 38.69 2.17 1 -2 9 42.83 2.29 -1 -2 -9 36.57 2.31 1 -2 9 44.47 2.56 -1 -2 -9 43.54 2.40 1 -2 9 42.85 2.32 1 -2 9 42.50 2.44 1 -2 9 43.49 2.28 1 -2 9 41.45 2.44 1 -2 9 43.11 2.63 -1 -2 -9 46.35 2.50 1 -2 9 41.96 2.56 -1 -2 -9 43.00 2.65 1 -2 9 44.27 2.22 1 -2 9 44.14 2.18 1 -2 9 43.03 2.21 1 2 9 41.87 2.45 -1 2 -9 46.83 2.67 1 2 9 44.98 2.36 -1 2 -9 43.45 2.33 1 2 9 44.17 2.22 1 2 9 42.25 2.62 1 2 9 42.22 2.47 1 2 9 45.89 2.57 1 2 9 42.94 2.30 1 2 9 42.34 2.56 1 2 9 42.56 2.23 1 2 9 40.24 2.62 -1 2 -9 40.66 2.66 1 2 9 42.69 2.20 1 2 9 43.22 2.06 -1 2 -9 45.10 2.50 1 2 9 45.15 2.39 2 -2 9 69.54 4.15 -2 -2 -9 68.26 3.78 2 -2 9 68.63 3.54 2 -2 9 66.44 4.02 -2 -2 -9 68.47 4.15 2 -2 9 71.73 4.03 -2 -2 -9 69.40 3.94 2 -2 9 69.73 3.59 2 -2 9 67.36 3.49 2 -2 9 69.30 3.43 -2 -2 -9 68.89 4.16 -2 -2 -9 71.45 3.65 2 -2 9 65.06 3.82 2 -2 9 68.67 3.45 2 2 9 68.92 3.45 2 2 9 71.38 3.61 2 2 9 70.57 4.04 2 2 9 68.34 3.49 2 2 9 69.73 4.15 -2 2 -9 65.79 3.93 2 2 9 66.05 3.84 2 2 9 68.86 3.47 2 2 9 71.06 3.88 2 2 9 66.41 3.74 2 2 9 68.65 3.63 2 2 9 72.32 4.04 2 2 9 69.19 3.20 -2 2 -9 66.24 4.14 3 -2 9 36.72 1.98 3 -2 9 36.00 2.12 3 -2 9 35.82 1.70 -3 -2 -9 36.03 2.21 -3 -2 -9 37.26 2.07 -3 -2 -9 35.58 1.93 3 -2 9 35.83 2.17 3 -2 9 37.17 1.83 3 -2 9 35.21 2.09 3 2 9 34.12 1.90 3 2 9 37.63 1.85 3 2 9 29.67 2.10 3 2 9 36.88 1.89 3 2 9 31.06 1.82 3 2 9 37.38 2.13 3 2 9 34.05 1.79 -3 2 -9 35.62 2.06 3 2 9 34.70 2.16 3 2 9 34.48 2.16 4 -2 9 3.72 0.31 4 -2 9 3.80 0.27 -4 -2 -9 3.99 0.31 4 -2 9 3.90 0.26 -4 -2 -9 3.97 0.34 -4 -2 -9 3.99 0.38 4 -2 9 3.02 0.26 4 -2 9 4.03 0.25 4 -2 9 3.61 0.34 4 2 9 3.75 0.26 4 2 9 3.82 0.22 4 2 9 3.36 0.30 4 2 9 3.16 0.26 -4 2 -9 3.84 0.29 4 2 9 3.11 0.27 4 2 9 3.07 0.26 4 2 9 3.67 0.34 4 2 9 3.81 0.30 5 -2 9 9.97 0.49 5 -2 9 9.69 0.53 5 -2 9 10.21 0.64 -5 -2 -9 9.69 0.61 5 2 9 11.10 0.65 5 2 9 9.39 0.60 5 2 9 9.14 0.51 5 2 9 8.02 0.53 5 2 9 8.51 0.53 5 2 9 8.54 0.63 5 2 9 9.23 0.55 6 -2 9 0.08 0.06 6 -2 9 0.15 0.08 -6 -2 -9 0.07 0.07 6 2 9 0.16 0.10 6 2 9 0.15 0.09 6 2 9 0.06 0.07 6 2 9 0.08 0.06 7 -2 9 7.95 0.54 7 2 9 8.65 0.55 7 2 9 8.61 0.55 6 -3 -9 0.73 0.14 -6 -3 9 0.61 0.16 6 -3 -9 0.71 0.14 6 -3 -9 1.00 0.13 -6 -3 9 0.85 0.14 6 -3 -9 0.65 0.11 -6 -3 9 0.51 0.15 6 -3 -9 0.58 0.10 -6 3 9 1.03 0.15 6 3 -9 0.57 0.12 6 3 -9 0.73 0.12 6 3 -9 0.67 0.11 -6 3 9 0.66 0.16 -6 3 9 0.66 0.13 -6 3 9 0.58 0.13 6 3 -9 0.69 0.13 6 3 -9 0.99 0.16 6 3 -9 0.98 0.18 -5 -3 9 19.72 1.47 5 -3 -9 23.98 1.26 -5 -3 9 24.77 1.38 -5 -3 9 24.21 1.50 5 -3 -9 23.54 1.36 5 -3 -9 24.96 1.23 -5 -3 9 24.16 1.40 -5 -3 9 20.13 1.47 5 -3 -9 19.30 1.41 5 -3 -9 19.91 1.19 5 -3 -9 24.42 1.28 5 -3 -9 21.73 1.35 5 -3 -9 20.51 1.41 -5 -3 9 22.56 1.29 -5 -3 9 25.14 1.24 -5 3 9 20.47 1.37 5 3 -9 24.69 1.23 5 3 -9 21.77 1.37 5 3 -9 25.83 1.44 5 3 -9 22.52 1.40 -5 3 9 24.74 1.24 -5 3 9 24.32 1.30 5 3 -9 24.83 1.38 5 3 -9 24.38 1.47 -5 3 9 23.90 1.50 5 3 -9 26.01 1.33 -5 3 9 24.04 1.49 5 3 -9 23.68 1.13 5 3 -9 25.66 1.40 4 -3 -9 8.95 0.67 4 -3 -9 10.57 0.58 4 -3 -9 9.42 0.65 -4 -3 9 10.34 0.64 -4 -3 9 11.17 0.75 -4 -3 9 10.26 0.68 4 -3 -9 10.02 0.49 -4 -3 9 9.80 0.62 4 -3 -9 8.30 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7.00 0.50 -2 -3 9 5.71 0.39 -2 -3 9 5.46 0.39 -2 -3 9 4.80 0.45 -2 -3 9 6.98 0.53 -2 -3 9 4.67 0.42 2 -3 -9 4.98 0.42 -2 -3 9 4.94 0.41 2 -3 -9 5.93 0.50 -2 -3 9 6.70 0.45 2 -3 -9 5.34 0.40 -2 -3 9 6.11 0.42 -2 -3 9 5.24 0.43 2 -3 -9 5.76 0.38 2 -3 -9 5.19 0.46 -2 -3 9 5.28 0.44 -2 -3 9 6.08 0.45 2 -3 -9 5.32 0.43 2 -3 -9 5.28 0.42 2 3 -9 6.95 0.43 -2 3 9 6.60 0.42 -2 3 9 5.06 0.48 -2 3 9 5.80 0.49 2 3 -9 4.69 0.39 2 3 -9 5.91 0.50 2 3 -9 5.15 0.40 -2 3 9 5.25 0.41 -2 3 9 5.31 0.44 -2 3 9 5.47 0.41 2 3 -9 5.15 0.47 -2 3 9 4.93 0.38 -2 3 9 5.69 0.51 2 3 -9 5.21 0.45 1 -3 -9 4.33 0.37 -1 -3 9 4.17 0.37 1 -3 -9 4.32 0.39 -1 -3 9 4.41 0.33 1 -3 -9 3.78 0.41 -1 -3 9 4.05 0.33 1 -3 -9 4.21 0.30 -1 -3 9 4.42 0.36 -1 -3 9 4.54 0.38 -1 -3 9 4.24 0.34 1 -3 -9 3.91 0.39 -1 -3 9 3.16 0.34 1 -3 -9 3.72 0.35 1 -3 -9 3.82 0.32 1 -3 -9 3.76 0.32 -1 -3 9 4.36 0.41 -1 -3 9 4.21 0.35 -1 -3 9 4.53 0.30 -1 -3 9 4.60 0.32 1 -3 -9 3.95 0.33 -1 -3 9 4.38 0.35 -1 -3 9 4.55 0.36 -1 -3 9 4.18 0.29 1 -3 -9 4.04 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9 9.30 0.58 1 -3 9 9.15 0.62 1 -3 9 9.04 0.59 -1 -3 -9 9.04 0.59 1 -3 9 8.73 0.55 -1 3 -9 9.23 0.60 1 3 9 9.27 0.53 1 3 9 9.43 0.66 1 3 9 9.29 0.57 1 3 9 9.37 0.52 1 3 9 9.50 0.55 1 3 9 9.51 0.63 -1 3 -9 9.58 0.69 1 3 9 8.77 0.64 1 3 9 8.95 0.62 -1 3 -9 9.00 0.60 1 3 9 9.03 0.58 1 3 9 8.32 0.60 1 3 9 8.16 0.61 1 3 9 10.10 0.62 1 3 9 9.70 0.66 -2 -3 -9 2.61 0.31 2 -3 9 3.18 0.29 2 -3 9 2.09 0.23 2 -3 9 1.99 0.24 2 -3 9 2.72 0.18 2 -3 9 2.79 0.26 2 -3 9 2.66 0.21 2 -3 9 2.16 0.27 2 -3 9 2.68 0.21 2 -3 9 2.72 0.23 -2 -3 -9 2.31 0.24 -2 -3 -9 2.18 0.25 -2 -3 -9 2.08 0.30 2 3 9 2.58 0.22 2 3 9 2.67 0.24 2 3 9 2.40 0.30 2 3 9 3.00 0.28 -2 3 -9 2.37 0.29 2 3 9 2.38 0.24 2 3 9 2.64 0.23 2 3 9 2.48 0.29 2 3 9 2.19 0.23 2 3 9 2.03 0.18 2 3 9 2.49 0.24 -2 3 -9 2.08 0.23 2 3 9 2.23 0.25 2 3 9 2.80 0.27 -3 -3 -9 2.54 0.27 3 -3 9 3.24 0.24 -3 -3 -9 3.09 0.35 3 -3 9 3.11 0.30 -3 -3 -9 3.34 0.33 3 -3 9 2.36 0.24 3 -3 9 3.18 0.24 -3 -3 -9 3.48 0.30 3 -3 9 3.36 0.22 3 -3 9 3.08 0.25 3 -3 9 3.05 0.29 3 3 9 2.61 0.27 3 3 9 3.37 0.26 -3 3 -9 2.85 0.26 3 3 9 2.64 0.23 3 3 9 3.48 0.23 3 3 9 3.60 0.28 3 3 9 3.39 0.31 3 3 9 3.22 0.31 3 3 9 2.57 0.24 3 3 9 3.04 0.30 4 -3 9 0.84 0.13 4 -3 9 0.71 0.10 -4 -3 -9 0.78 0.16 4 -3 9 0.71 0.13 4 -3 9 0.75 0.11 4 -3 9 0.79 0.12 -4 -3 -9 0.59 0.12 4 -3 9 0.51 0.13 -4 -3 -9 1.13 0.21 4 3 9 0.62 0.15 4 3 9 0.64 0.12 4 3 9 0.61 0.11 4 3 9 0.74 0.11 4 3 9 0.53 0.11 4 3 9 0.49 0.11 4 3 9 0.59 0.12 4 3 9 0.79 0.16 4 3 9 0.74 0.12 5 -3 9 1.76 0.19 5 -3 9 1.70 0.15 5 -3 9 1.15 0.20 -5 -3 -9 1.57 0.19 -5 -3 -9 1.31 0.23 -5 -3 -9 1.56 0.22 5 3 9 1.34 0.16 5 3 9 1.60 0.17 5 3 9 1.61 0.20 5 3 9 1.36 0.17 5 3 9 1.70 0.14 5 3 9 1.74 0.23 5 3 9 1.57 0.20 6 -3 9 70.37 3.68 -6 -3 -9 72.51 4.16 6 -3 9 73.44 4.40 6 -3 9 73.63 4.40 6 3 9 75.54 4.40 6 3 9 76.69 4.27 6 3 9 70.69 4.24 6 3 9 73.42 3.61 6 3 9 74.15 3.70 6 -4 -9 22.22 1.21 -6 -4 9 25.24 1.31 -6 -4 9 23.25 1.35 -6 -4 9 23.26 1.45 6 -4 -9 22.83 1.40 -6 -4 9 23.02 1.37 6 -4 -9 22.35 1.29 6 -4 -9 23.90 1.20 6 -4 -9 23.59 1.38 6 4 -9 22.20 1.31 6 4 -9 22.97 1.34 -6 4 9 21.25 1.18 6 4 -9 22.70 1.34 6 4 -9 24.26 1.20 -6 4 9 23.38 1.36 -6 4 9 21.76 1.45 6 4 -9 23.58 1.26 6 4 -9 24.39 1.40 -5 -4 9 50.38 2.69 -5 -4 9 50.57 3.07 5 -4 -9 46.18 2.82 -5 -4 9 42.97 3.06 5 -4 -9 52.16 2.58 5 -4 -9 52.83 2.53 -5 -4 9 53.55 2.91 5 -4 -9 52.43 2.58 -5 -4 9 51.43 2.51 5 -4 -9 50.63 2.66 -5 -4 9 51.15 2.89 5 -4 -9 43.70 2.97 5 4 -9 52.77 2.99 -5 4 9 49.19 3.07 -5 4 9 51.19 2.69 -5 4 9 51.93 3.08 5 4 -9 50.69 2.89 5 4 -9 52.43 2.56 5 4 -9 54.42 2.78 5 4 -9 50.16 2.39 -5 4 9 51.74 2.52 5 4 -9 52.05 3.06 5 4 -9 50.33 2.68 -5 4 9 45.26 2.89 5 4 -9 50.42 2.86 5 4 -9 53.32 2.83 4 -4 -9 83.41 5.72 -4 -4 9 99.54 5.15 -4 -4 9 101.45 4.80 -4 -4 9 100.01 5.87 -4 -4 9 96.51 4.99 -4 -4 9 99.73 4.93 -4 -4 9 96.82 5.56 4 -4 -9 101.78 4.96 4 -4 -9 98.74 4.91 4 -4 -9 96.62 5.32 4 -4 -9 103.28 5.51 -4 -4 9 99.34 5.56 4 -4 -9 95.07 5.46 -4 4 9 104.63 5.16 -4 4 9 104.22 5.90 4 4 -9 104.49 5.15 4 4 -9 91.58 5.55 -4 4 9 89.03 4.78 4 4 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190.44 10.95 -2 -4 9 186.31 9.25 -2 -4 9 196.68 9.53 -2 -4 9 164.62 9.27 -2 -4 9 184.52 10.19 2 -4 -9 194.31 9.56 2 -4 -9 180.41 9.24 2 -4 -9 182.90 9.51 2 -4 -9 187.79 10.65 2 -4 -9 163.78 10.33 -2 4 9 171.21 8.86 -2 4 9 191.17 10.41 2 4 -9 185.36 10.41 -2 4 9 158.19 9.55 -2 4 9 186.01 9.98 2 4 -9 201.91 9.99 2 4 -9 200.57 10.97 -2 4 9 180.82 10.95 -2 4 9 190.37 10.36 -2 4 9 178.71 9.53 2 4 -9 186.58 10.36 -2 4 9 186.98 9.57 -1 -4 9 15.60 1.04 1 -4 -9 16.11 0.98 -1 -4 9 16.82 0.88 1 -4 -9 16.16 0.93 1 -4 -9 15.63 1.00 -1 -4 9 16.45 0.94 1 -4 -9 16.45 0.89 -1 -4 9 16.37 0.88 -1 -4 9 15.44 0.93 1 -4 -9 17.41 1.10 1 -4 -9 16.38 1.04 1 -4 -9 16.28 0.89 -1 -4 9 16.35 1.00 -1 -4 9 16.63 0.99 -1 -4 9 15.36 0.98 1 -4 -9 17.24 1.04 -1 -4 9 16.05 0.91 -1 -4 9 15.59 1.03 -1 -4 9 16.25 0.82 1 -4 -9 16.65 1.01 1 -4 -9 15.81 1.07 -1 -4 9 16.35 1.03 -1 -4 9 16.21 1.03 1 -4 -9 16.02 0.96 -1 4 9 16.31 1.01 -1 4 9 16.67 0.94 -1 4 9 16.03 1.04 1 4 -9 16.32 1.00 -1 4 9 15.02 1.08 -1 4 9 16.43 0.91 1 4 -9 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45.20 2.57 -3 -5 9 44.98 2.50 -3 -5 9 40.66 2.02 3 -5 -9 41.92 1.97 3 -5 -9 40.72 2.17 -3 -5 9 42.92 2.56 -3 -5 9 41.52 2.24 3 -5 -9 38.06 2.38 -3 -5 9 44.76 2.57 3 -5 -9 43.56 2.54 3 -5 -9 39.04 2.48 3 -5 -9 34.80 2.46 -3 -5 9 44.27 2.22 -3 -5 9 42.17 2.32 3 -5 -9 40.13 2.28 3 -5 -9 37.83 2.12 -3 -5 9 42.74 2.40 3 -5 -9 43.68 2.38 -3 -5 9 44.87 2.47 3 -5 -9 43.27 2.30 -3 -5 9 44.16 2.15 3 5 -9 44.20 2.42 -3 5 9 41.69 2.33 3 5 -9 40.87 2.24 -3 5 9 40.36 2.24 -3 5 9 40.52 2.58 3 5 -9 44.29 2.59 3 5 -9 46.60 2.44 3 5 -9 39.86 2.33 3 5 -9 44.79 2.23 -3 5 9 34.61 2.40 -3 5 9 43.72 2.58 3 5 -9 39.34 2.32 2 -5 -9 0.52 0.13 2 -5 -9 0.70 0.16 -2 -5 9 0.60 0.17 2 -5 -9 0.58 0.13 -2 -5 9 0.70 0.14 -2 -5 9 0.44 0.15 2 -5 -9 0.75 0.17 2 -5 -9 0.48 0.12 -2 -5 9 0.57 0.12 2 -5 -9 0.46 0.13 -2 -5 9 0.33 0.15 2 -5 -9 0.73 0.19 2 -5 -9 0.54 0.15 2 -5 -9 0.41 0.13 -2 -5 9 0.53 0.19 -2 -5 9 0.59 0.14 -2 -5 9 0.33 0.12 2 -5 -9 0.52 0.12 -2 -5 9 0.56 0.12 -2 -5 9 0.31 0.13 2 -5 -9 0.51 0.13 -2 -5 9 0.56 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1.43 0.24 1 2 10 1.41 0.23 -1 2 -10 1.54 0.23 1 2 10 1.49 0.24 -1 2 -10 1.90 0.27 1 2 10 1.57 0.18 -1 2 -10 1.54 0.19 1 2 10 1.20 0.19 1 2 10 1.15 0.20 1 2 10 1.46 0.16 1 2 10 1.63 0.24 1 2 10 1.43 0.23 1 2 10 1.41 0.19 2 -2 10 38.93 2.15 -2 -2 -10 37.34 2.02 -2 -2 -10 39.22 1.96 2 -2 10 38.18 2.15 2 -2 10 30.81 2.01 2 -2 10 37.71 1.91 -2 -2 -10 37.12 2.23 -2 -2 -10 29.18 2.07 2 -2 10 29.36 1.84 2 -2 10 32.32 2.12 2 -2 10 30.84 2.18 2 -2 10 36.86 1.90 2 -2 10 38.01 1.80 -2 -2 -10 40.18 2.25 2 2 10 31.66 2.04 2 2 10 37.42 1.85 2 2 10 38.07 2.19 -2 2 -10 38.83 2.24 -2 2 -10 36.39 1.96 2 2 10 37.11 2.03 2 2 10 40.31 1.89 -2 2 -10 38.36 2.09 2 2 10 34.38 1.95 2 2 10 30.87 1.91 -3 -2 -10 59.56 3.00 -3 -2 -10 56.83 3.41 3 -2 10 59.19 3.10 3 -2 10 49.92 2.81 3 -2 10 58.35 3.28 -3 -2 -10 59.65 3.42 3 -2 10 59.79 3.31 3 -2 10 55.45 2.62 -3 -2 -10 51.30 3.21 3 -2 10 48.85 2.85 -3 2 -10 57.71 3.22 3 2 10 61.09 2.86 3 2 10 48.71 2.85 3 2 10 60.36 2.95 3 2 10 50.69 3.30 3 2 10 57.48 2.80 3 2 10 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-2 -5 -12 14.66 0.99 -2 -5 -12 16.29 1.04 2 -5 12 16.48 0.99 2 -5 12 15.54 0.83 2 -5 12 16.69 0.85 2 -5 12 15.86 1.01 -2 -5 -12 16.59 0.96 -2 -5 -12 16.73 0.93 2 5 12 16.00 0.89 2 5 12 15.85 0.94 2 5 12 16.48 0.99 2 5 12 16.67 0.83 -2 5 -12 16.40 0.96 -3 -5 -12 10.55 0.74 3 -5 12 11.31 0.71 -3 -5 -12 11.21 0.68 3 -5 12 11.76 0.60 3 5 12 11.15 0.69 2 -6 -12 28.50 1.50 2 -6 -12 28.37 1.43 -2 -6 12 27.43 1.40 -2 -6 12 28.66 1.59 -2 -6 12 28.37 1.49 2 -6 -12 28.74 1.61 -2 -6 12 27.99 1.67 2 6 -12 26.58 1.61 2 6 -12 28.05 1.73 -2 6 12 29.92 1.73 2 6 -12 26.39 1.56 -2 6 12 28.43 1.63 1 -6 -12 30.20 1.72 -1 -6 12 30.71 1.77 1 -6 -12 30.45 1.60 -1 -6 12 29.18 1.57 -1 -6 12 31.07 1.68 1 -6 -12 30.78 1.65 -1 -6 12 28.53 1.53 1 -6 -12 29.90 1.82 -1 -6 12 29.49 1.77 1 -6 -12 30.06 1.53 1 6 -12 31.56 1.73 1 6 -12 28.51 1.66 -1 6 12 29.64 1.72 -1 6 12 27.96 1.53 1 6 -12 29.94 1.84 -1 6 12 30.86 1.83 -1 6 12 29.98 1.61 0 -6 -12 0.85 0.14 0 -6 -12 0.87 0.16 0 -6 12 0.84 0.13 0 -6 -12 0.85 0.14 0 -6 12 0.85 0.12 0 -6 -12 0.62 0.11 0 -6 -12 0.75 0.11 0 -6 12 0.77 0.13 0 -6 12 0.95 0.17 0 6 12 0.89 0.14 0 6 12 0.80 0.14 0 6 -12 0.84 0.15 0 6 12 0.78 0.13 0 6 12 0.84 0.15 0 6 12 0.83 0.13 0 6 -12 0.87 0.14 0 6 12 0.79 0.12 1 -6 12 37.47 2.12 1 -6 12 35.62 1.80 -1 -6 -12 37.14 1.99 1 -6 12 35.16 2.10 1 -6 12 37.01 1.83 -1 -6 -12 35.64 2.06 -1 -6 -12 33.19 1.91 1 -6 12 31.24 2.17 -1 -6 -12 37.14 2.19 1 6 12 36.23 2.12 -1 6 -12 36.52 2.06 1 6 12 36.60 2.03 1 6 12 37.94 1.91 1 6 12 36.63 1.82 2 -6 12 1.30 0.18 2 -6 12 1.19 0.17 -2 -6 -12 1.34 0.17 2 -6 12 1.50 0.14 2 6 12 1.35 0.14 2 6 12 1.66 0.19 2 6 12 1.29 0.16 -2 6 -12 1.36 0.14 2 6 12 1.24 0.16 1 -7 -12 11.73 0.64 -1 -7 12 11.77 0.74 -1 -7 12 12.50 0.74 1 -7 -12 12.14 0.68 1 -7 -12 11.51 0.69 -1 7 12 11.51 0.68 1 7 -12 10.62 0.78 1 7 -12 12.63 0.72 -1 7 12 12.24 0.78 -1 7 12 11.92 0.73 0 -7 -12 1.76 0.17 0 -7 12 1.41 0.15 0 -7 -12 1.58 0.16 0 -7 12 2.00 0.21 0 -7 -12 1.56 0.17 0 -7 12 1.46 0.15 0 -7 -12 1.89 0.22 0 -7 -12 1.88 0.20 0 7 12 1.60 0.18 0 7 12 1.89 0.19 0 7 -12 1.47 0.17 0 7 12 1.60 0.16 0 7 12 2.02 0.21 1 -7 12 3.49 0.23 1 -7 12 3.33 0.29 -1 -7 -12 3.64 0.26 -1 -7 -12 3.61 0.29 -1 -7 -12 3.32 0.31 1 7 12 3.23 0.24 -1 7 -12 3.60 0.26 1 0 -13 72.80 4.12 -1 0 13 66.89 4.00 -1 0 13 66.94 3.82 1 0 -13 68.82 3.74 -1 0 13 68.58 3.42 -1 0 13 69.51 3.59 0 0 13 0.04 0.10 0 0 13 0.02 0.05 0 0 13 0.05 0.08 0 0 -13 0.02 0.06 0 0 13 0.02 0.08 0 0 -13 0.01 0.06 0 0 -13 -0.04 0.10 1 0 13 22.61 1.21 -1 0 -13 19.97 1.24 1 0 13 22.20 1.28 -1 0 -13 22.43 1.34 1 0 13 19.79 1.27 -1 -1 13 21.48 1.11 1 -1 -13 22.82 1.37 -1 -1 13 21.53 1.26 1 -1 -13 21.95 1.23 -1 -1 13 22.55 1.18 -1 -1 13 21.07 1.31 -1 1 13 21.76 1.18 -1 1 13 21.57 1.28 1 1 -13 23.58 1.37 1 1 -13 20.95 1.23 -1 1 13 21.99 1.12 0 -1 -13 9.79 0.70 0 -1 13 11.36 0.67 0 -1 13 9.85 0.59 0 -1 13 10.30 0.63 0 -1 -13 10.68 0.62 0 1 13 11.57 0.64 0 1 13 10.74 0.66 0 1 13 10.31 0.60 0 1 -13 9.55 0.70 0 1 -13 10.30 0.62 0 1 -13 10.94 0.64 0 1 13 10.56 0.56 1 -1 13 0.45 0.09 -1 -1 -13 0.32 0.12 1 -1 13 0.30 0.10 -1 -1 -13 0.35 0.08 -1 -1 -13 0.35 0.09 -1 1 -13 0.44 0.09 1 1 13 0.45 0.10 1 1 13 0.28 0.09 -1 -2 13 68.70 3.61 -1 -2 13 69.36 3.84 -1 -2 13 71.35 4.04 -1 -2 13 68.32 3.44 1 -2 -13 70.54 3.77 1 -2 -13 72.01 4.15 1 2 -13 70.26 4.15 -1 2 13 68.50 3.62 1 2 -13 67.57 3.77 -1 2 13 68.52 3.45 0 -2 13 31.17 1.81 0 -2 13 31.05 1.71 0 -2 -13 31.92 1.88 0 -2 -13 30.31 1.69 0 2 13 28.76 1.81 0 2 13 30.46 1.73 0 2 13 31.51 1.62 0 2 13 30.56 1.54 0 2 -13 30.28 1.76 0 2 -13 30.20 1.87 -1 -2 -13 27.55 1.74 -1 -2 -13 33.00 1.93 1 -2 13 31.86 1.85 1 -2 13 33.51 1.85 1 2 13 31.83 1.77 1 2 13 31.62 1.86 -1 2 -13 31.26 1.81 0 -3 -13 19.32 1.13 0 -3 -13 16.90 1.01 0 -3 13 18.11 1.08 0 3 13 18.24 0.97 0 3 13 18.01 0.92 0 3 -13 16.55 1.05 0 0 0 0.00 0.00 ; _shelx_res_checksum 45348 _shelx_res_file ; TITL bos2_0m in P2(1)/n CELL 1.54178 8.1528 15.6908 11.0625 90 90.148 90 ZERR 4 0.0002 0.0005 0.0003 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H O UNIT 72 80 16 L.S. 10 PLAN -20 0 0 TEMP -173.14 HTAB BOND $H CONF fmap 2 acta REM //cicserver1/xray/structure%20workup/bos2/bos2_0m.hkl WGHT 0.059800 0.642200 FVAR 0.39632 O1 3 0.512804 0.852759 0.765023 11.00000 0.01109 0.01509 = 0.02992 0.00328 -0.00086 -0.00093 O2 3 0.977890 1.022814 0.761472 11.00000 0.02218 0.01429 = 0.02337 -0.00242 0.00056 -0.00599 O3 3 1.071369 0.689797 0.630066 11.00000 0.01617 0.01958 = 0.01564 -0.00422 0.00077 0.00216 O4 3 0.963413 0.718192 0.896804 11.00000 0.01588 0.01445 = 0.01457 0.00332 0.00303 0.00054 C1 1 0.508725 1.002385 0.722233 11.00000 0.01807 0.01622 = 0.03113 -0.00012 -0.00440 0.00210 AFIX 137 H1A 2 0.420896 0.997087 0.662053 11.00000 -1.50000 H1B 2 0.577382 1.051725 0.702617 11.00000 -1.50000 H1C 2 0.460630 1.010103 0.802588 11.00000 -1.50000 AFIX 0 C2 1 0.613076 0.922088 0.721368 11.00000 0.01318 0.01264 = 0.02230 0.00094 -0.00222 -0.00219 C3 1 0.760580 0.921835 0.812459 11.00000 0.01367 0.01224 = 0.01539 -0.00074 -0.00031 -0.00026 C4 1 0.791294 0.824329 0.823757 11.00000 0.01235 0.01211 = 0.01258 -0.00027 0.00151 -0.00126 C5 1 0.877879 0.791940 0.942712 11.00000 0.01610 0.01763 = 0.01203 0.00106 0.00244 0.00153 AFIX 13 H5 2 0.801434 0.779717 1.011100 11.00000 -1.20000 AFIX 0 C6 1 1.021014 0.849692 0.975235 11.00000 0.01953 0.01854 = 0.01278 -0.00040 -0.00385 0.00108 AFIX 43 H6 2 1.026298 0.889208 1.040191 11.00000 -1.20000 AFIX 0 C7 1 1.137165 0.833707 0.894441 11.00000 0.01520 0.01807 = 0.01444 0.00127 -0.00363 -0.00083 AFIX 43 H7 2 1.242099 0.859701 0.888741 11.00000 -1.20000 AFIX 0 C8 1 0.619394 0.785231 0.803682 11.00000 0.01255 0.01371 = 0.02236 0.00207 0.00014 -0.00078 AFIX 23 H8A 2 0.624292 0.740083 0.741282 11.00000 -1.20000 H8B 2 0.578430 0.759747 0.879702 11.00000 -1.20000 AFIX 0 C9 1 0.718250 0.968271 0.929215 11.00000 0.01957 0.01717 = 0.01905 -0.00351 0.00258 0.00079 AFIX 137 H9A 2 0.810167 0.963521 0.986078 11.00000 -1.50000 H9B 2 0.620096 0.942648 0.965004 11.00000 -1.50000 H9C 2 0.697255 1.028517 0.911675 11.00000 -1.50000 AFIX 0 C10 1 0.912376 0.954380 0.747801 11.00000 0.01416 0.01398 = 0.01317 0.00132 -0.00263 -0.00055 C11 1 0.960082 0.884949 0.657324 11.00000 0.01545 0.01289 = 0.01265 0.00081 0.00032 -0.00214 C12 1 0.927879 0.801419 0.728808 11.00000 0.01117 0.01209 = 0.01172 0.00015 0.00017 -0.00168 C13 1 0.908240 0.722241 0.648489 11.00000 0.01464 0.01264 = 0.01569 -0.00139 -0.00037 0.00019 AFIX 23 H13A 2 0.838846 0.679064 0.688891 11.00000 -1.20000 H13B 2 0.856918 0.737648 0.570285 11.00000 -1.20000 AFIX 0 C14 1 1.167757 0.706255 0.736764 11.00000 0.01489 0.01768 = 0.01613 -0.00062 -0.00041 0.00101 AFIX 23 H14A 2 1.273342 0.733312 0.715033 11.00000 -1.20000 H14B 2 1.190706 0.652539 0.780600 11.00000 -1.20000 AFIX 0 C15 1 1.066612 0.765339 0.813582 11.00000 0.01262 0.01541 = 0.01295 0.00273 0.00108 -0.00086 C16 1 0.823543 0.891169 0.563015 11.00000 0.02494 0.01237 = 0.01257 0.00134 -0.00298 -0.00134 AFIX 43 H16 2 0.850453 0.885264 0.479933 11.00000 -1.20000 AFIX 0 C17 1 0.668607 0.904559 0.593594 11.00000 0.02206 0.01222 = 0.01852 0.00114 -0.00756 -0.00166 AFIX 43 H17 2 0.587820 0.903046 0.531592 11.00000 -1.20000 AFIX 0 C18 1 1.128957 0.896038 0.601653 11.00000 0.01935 0.01791 = 0.01770 0.00170 0.00508 -0.00318 AFIX 137 H18A 2 1.143495 0.854440 0.536474 11.00000 -1.50000 H18B 2 1.213170 0.887009 0.663716 11.00000 -1.50000 H18C 2 1.139105 0.953815 0.568868 11.00000 -1.50000 AFIX 0 HKLF 4 REM bos2_0m in P2(1)/n REM R1 = 0.0351 for 2474 Fo > 4sig(Fo) and 0.0382 for all 2493 data REM 202 parameters refined using 0 restraints END WGHT 0.0598 0.6422 REM Instructions for potential hydrogen bonds EQIV $1 x-1/2, -y+3/2, z+1/2 HTAB C5 O3_$1 EQIV $2 -x+2, -y+2, -z+2 HTAB C6 O2_$2 EQIV $3 x+1, y, z HTAB C7 O1_$3 EQIV $4 x-1/2, -y+3/2, z-1/2 HTAB C17 O4_$4 REM Highest difference peak 0.385, deepest hole -0.462, 1-sigma level 0.141 Q1 1 0.6493 0.9103 0.6590 11.00000 0.05 0.39 Q2 1 0.6843 0.9262 0.7627 11.00000 0.05 0.38 Q3 1 0.6090 0.7424 0.6538 11.00000 0.05 0.33 Q4 1 0.7276 0.8588 0.5849 11.00000 0.05 0.33 Q5 1 0.5614 0.8789 0.7410 11.00000 0.05 0.32 Q6 1 0.5956 0.7619 0.7168 11.00000 0.05 0.32 Q7 1 0.6655 0.7997 0.6031 11.00000 0.05 0.31 Q8 1 0.4363 0.8564 0.7912 11.00000 0.05 0.31 Q9 1 0.5230 0.8213 0.7017 11.00000 0.05 0.31 Q10 1 0.5552 0.8224 0.7838 11.00000 0.05 0.30 Q11 1 0.3811 0.7523 0.8828 11.00000 0.05 0.30 Q12 1 0.3773 0.7834 0.8316 11.00000 0.05 0.30 Q13 1 0.6713 0.7356 0.5147 11.00000 0.05 0.30 Q14 1 0.3036 0.7554 0.9028 11.00000 0.05 0.30 Q15 1 0.5608 0.9592 0.7274 11.00000 0.05 0.29 Q16 1 0.7463 0.7694 0.5422 11.00000 0.05 0.29 Q17 1 0.4413 0.7682 0.7819 11.00000 0.05 0.28 Q18 1 0.6174 0.6789 0.4694 11.00000 0.05 0.28 Q19 1 0.7654 0.7759 0.5155 11.00000 0.05 0.28 Q20 1 0.4109 0.7068 0.8131 11.00000 0.05 0.28 ; _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2013-4