data_a14105 _audit_creation_date 2014-03-26 # start Validation Reply Form _vrf_CELLZ01_ALERT_1_G ; PROBLEM: WARNING: H atoms missing from atom site list. Is this intentional? From the CIF: _cell_formula_units_Z 4 From the CIF: _chemical_formula_sum C17 H23 Br O5 TEST: Compare cell contents of formula and atom_site data atom Z*formula cif sites diff C 68.00 68.00 0.00 H 92.00 90.00 2.00 Br 4.00 4.00 0.00 O 20.00 20.00 0.00 RESPONSE: Yes, could not locate 1/2 hydrogen atom on water; it was ignored as no suitable hydrogen bond could be found. ; # end Validation Reply Form _audit_creation_method ; Olex2 1.2 (compiled 2014.03.12 svn.r2899 for OlexSys, GUI svn.r4796), SHELXL-2014, and manual edit ; _database_code_depnum_ccdc_archive ? _publ_contact_author_name 'Xray Staff' _publ_contact_author_address ; Beckman Institute Caltech 139-74 Pasadena CA 91125 USA ; _publ_contact_author_email xray@caltech.edu _publ_section_acknowledgements ; The Bruker KAPPA APEXII X-ray diffractometer was purchased via an NSF CRIF:MU award to the California Institute of Technology (CHE-0639094). ; _shelxl_version_number 2014-2 _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122 Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122 ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety 'C17 H21 Br O4, H2 O' _chemical_formula_sum 'C17 H23 Br O5' _chemical_formula_weight 387.26 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 5 _space_group_name_H-M_alt 'C 1 2 1' _space_group_name_Hall 'C 2y' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 18.8295(9) _cell_length_b 7.8451(4) _cell_length_c 11.4443(5) _cell_angle_alpha 90 _cell_angle_beta 95.208(2) _cell_angle_gamma 90 _cell_volume 1683.56(14) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9869 _cell_measurement_temperature 100 _cell_measurement_theta_max 45.67 _cell_measurement_theta_min 2.82 _shelx_estimated_absorpt_T_max 0.535 _shelx_estimated_absorpt_T_min 0.417 _exptl_absorpt_coefficient_mu 2.464 _exptl_absorpt_correction_T_max 0.5777 _exptl_absorpt_correction_T_min 0.4462 _exptl_absorpt_correction_type 'multi-scan' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1.00 0.00 0.00 0.1910 -1.00 -1.00 -1.00 0.1780 -1.00 -1.00 1.00 0.1530 5.00 -1.00 -5.00 0.1560 0.00 5.00 -1.00 0.2200 -2.00 4.00 1.00 0.1880 -4.00 2.00 3.00 0.1750 3.00 -4.00 -2.00 0.1980 1.00 0.00 0.00 0.1050 -4.00 -4.00 -5.00 0.1690 -5.00 1.00 1.00 0.1600 0.00 4.00 5.00 0.2010 -3.00 4.00 0.00 0.1850 3.00 0.00 -5.00 0.1730 -1.00 -1.00 -5.00 0.1540 -4.00 1.00 -5.00 0.2110 -2.00 1.00 0.00 0.1760 -3.00 3.00 5.00 0.1940 -5.00 0.00 1.00 0.1460 -5.00 1.00 2.00 0.1510 8.00 -1.00 -2.00 0.1310 1.00 6.00 5.00 0.1950 2.00 -1.00 1.00 0.1720 1.00 0.00 4.00 0.2020 8.00 0.00 -3.00 0.1300 2.00 1.00 0.00 0.2150 _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. A face-indexed correction (linear absorption coefficient refined to 2.58 mm-1) was followed by default multi-scan. wR2(int) was 0.0809 before and 0.0746 after correction. The Ratio of minimum to maximum transmission is 0.7724. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.528 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'chunk' _exptl_crystal_F_000 800 _exptl_crystal_size_max 0.43 _exptl_crystal_size_mid 0.42 _exptl_crystal_size_min 0.29 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0370 _diffrn_reflns_av_unetI/netI 0.0452 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 39 _diffrn_reflns_limit_h_min -39 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 78240 _diffrn_reflns_point_group_measured_fraction_full 0.977 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 48.826 _diffrn_reflns_theta_min 1.787 _diffrn_ambient_temperature 100 _diffrn_detector_area_resol_mean 8.33 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_source_target Mo _diffrn_radiation_wavelength 0.71073 _diffrn_source_voltage 50 _diffrn_source_current 30 _diffrn_source_power 1.5 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.899 _reflns_Friedel_fraction_full 0.952 _reflns_Friedel_fraction_max 0.980 _reflns_number_gt 14231 _reflns_number_total 16574 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_data_collection 'APEX2 2014.1-1 (Bruker-AXS, 2007)' _computing_cell_refinement 'SAINT V8.34A (Bruker-AXS, 2007)' _computing_data_reduction 'SAINT V8.34A (Bruker-AXS, 2007)' _computing_structure_solution 'XT-2014/1 (Sheldrick, 2012)' _computing_structure_refinement 'SHELXL-2014/2 (Sheldrick, 2014)' _computing_molecular_graphics 'DIAMOND 3 (Crystal Impact, 1999)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _refine_diff_density_max 0.653 _refine_diff_density_min -0.707 _refine_diff_density_rms 0.100 _refine_ls_abs_structure_details ; Flack x determined using 5880 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.0289(17) _refine_ls_abs_structure_Hooft 0.045(2) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.966 _refine_ls_hydrogen_treatment refxyz _refine_ls_matrix_type full _refine_ls_number_parameters 299 _refine_ls_number_reflns 16574 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0344 _refine_ls_R_factor_gt 0.0256 _refine_ls_restrained_S_all 0.966 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0157P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0521 _refine_ls_wR_factor_ref 0.0538 _refine_special_details ; There is one water molecule in the asymmetric unit. One of the hydrogen atoms (H5B) is too close to itself via a symmetry operation, so its population was set to 1/2. No other reasonable electron density or hydrogen bonding was found, so the other half hydrogen was ignored. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.5 times of: All H(H) groups 2. Others Fixed Sof: H5B(0.5) ; _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.26113(2) 1.01060(2) 0.96894(2) 0.01509(2) Uani 1 1 d . . . . . O1 O 0.36229(3) 0.74011(9) 0.88671(6) 0.01444(11) Uani 1 1 d . . . . . O2 O 0.38980(5) 0.53191(13) 0.64869(9) 0.0315(2) Uani 1 1 d . . . . . O3 O 0.20806(4) 0.47510(8) 0.59062(6) 0.01458(11) Uani 1 1 d . . . . . O4 O 0.07461(4) 0.66953(10) 0.52562(6) 0.01466(11) Uani 1 1 d . . . . . H4A H 0.073(2) 0.581(5) 0.527(4) 0.110(14) Uiso 1 1 d . . . . . C1 C 0.17916(4) 0.85478(10) 0.77219(7) 0.00967(10) Uani 1 1 d . . . . . C2 C 0.24440(4) 0.86109(10) 0.83981(7) 0.01018(11) Uani 1 1 d . . . . . C3 C 0.29846(4) 0.74475(10) 0.81879(7) 0.01026(11) Uani 1 1 d . . . . . C4 C 0.28583(4) 0.62060(10) 0.73284(7) 0.01035(11) Uani 1 1 d . . . . . C5 C 0.21904(4) 0.60656(10) 0.66968(7) 0.01004(11) Uani 1 1 d . . . . . C6 C 0.16629(4) 0.72348(10) 0.68956(7) 0.00946(10) Uani 1 1 d . . . . . C7 C 0.08832(4) 0.72890(11) 0.64232(7) 0.01113(11) Uani 1 1 d . . . . . C8 C 0.04334(5) 0.63123(13) 0.72610(9) 0.01515(14) Uani 1 1 d . . . . . H8A H 0.0504(8) 0.509(3) 0.7183(13) 0.018(3) Uiso 1 1 d . . . . . H8B H -0.0034(10) 0.658(3) 0.6933(16) 0.024(4) Uiso 1 1 d . . . . . C9 C 0.05842(5) 0.68894(14) 0.85425(9) 0.01745(15) Uani 1 1 d . . . . . H9A H 0.0199(10) 0.648(3) 0.9068(15) 0.023(4) Uiso 1 1 d . . . . . H9B H 0.1018(11) 0.625(3) 0.8880(17) 0.027(5) Uiso 1 1 d . . . . . C10 C 0.06546(5) 0.88309(14) 0.86799(9) 0.01679(14) Uani 1 1 d . . . . . H10A H 0.0863(11) 0.908(3) 0.9475(18) 0.033(5) Uiso 1 1 d . . . . . H10B H 0.0216(9) 0.932(2) 0.8589(16) 0.024(4) Uiso 1 1 d . . . . . C11 C 0.11103(4) 0.96100(11) 0.77572(8) 0.01238(12) Uani 1 1 d . . . . . C12 C 0.07345(4) 0.91871(12) 0.65385(8) 0.01326(13) Uani 1 1 d . . . . . H12A H 0.0213(9) 0.940(2) 0.6506(16) 0.021(4) Uiso 1 1 d . . . . . H12B H 0.0947(8) 0.977(2) 0.5920(13) 0.012(3) Uiso 1 1 d . . . . . C13 C 0.41399(5) 0.86083(15) 0.85430(11) 0.02129(18) Uani 1 1 d . . . . . H13A H 0.4561(12) 0.843(3) 0.9001(19) 0.037(5) Uiso 1 1 d . . . . . H13B H 0.4005(10) 0.979(3) 0.8697(17) 0.034(5) Uiso 1 1 d . . . . . H13C H 0.4233(10) 0.841(2) 0.7769(16) 0.023(4) Uiso 1 1 d . . . . . C14 C 0.34396(4) 0.49578(13) 0.71216(8) 0.01405(13) Uani 1 1 d . . . . . C15 C 0.34219(6) 0.32797(13) 0.77278(11) 0.02122(18) Uani 1 1 d . . . . . H15A H 0.3716(14) 0.252(4) 0.731(2) 0.053(7) Uiso 1 1 d . . . . . H15B H 0.2962(11) 0.280(3) 0.7559(18) 0.034(5) Uiso 1 1 d . . . . . H15C H 0.3523(11) 0.343(3) 0.8598(19) 0.035(5) Uiso 1 1 d . . . . . C16 C 0.22468(6) 0.5220(2) 0.47442(9) 0.02309(19) Uani 1 1 d . . . . . H16A H 0.2770(12) 0.556(3) 0.4724(17) 0.036(6) Uiso 1 1 d . . . . . H16B H 0.1930(11) 0.612(3) 0.4436(18) 0.031(5) Uiso 1 1 d . . . . . H16C H 0.2168(13) 0.432(3) 0.436(2) 0.043(6) Uiso 1 1 d . . . . . C17 C 0.12001(6) 1.15315(13) 0.79181(11) 0.02065(18) Uani 1 1 d . . . . . H17A H 0.1378(10) 1.186(3) 0.8703(18) 0.029(5) Uiso 1 1 d . . . . . H17B H 0.0737(13) 1.197(3) 0.784(2) 0.042(6) Uiso 1 1 d . . . . . H17C H 0.1619(10) 1.215(3) 0.7333(18) 0.032(5) Uiso 1 1 d . . . . . O5 O 0.43530(7) 0.82974(16) 0.53985(14) 0.0433(3) Uani 1 1 d . . . . . H5A H 0.4075(17) 0.747(5) 0.534(3) 0.076(10) Uiso 1 1 d . . . . . H5B H 0.476(4) 0.800(11) 0.503(9) 0.114 Uiso 0.5 1 d R . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.01585(3) 0.01588(3) 0.01337(3) -0.00553(3) 0.00035(2) -0.00195(3) O1 0.0087(2) 0.0190(3) 0.0149(3) 0.0022(2) -0.00307(18) -0.00120(19) O2 0.0240(3) 0.0297(5) 0.0443(5) 0.0124(4) 0.0223(3) 0.0116(3) O3 0.0151(2) 0.0140(2) 0.0145(2) -0.00527(19) 0.0005(2) 0.00071(18) O4 0.0122(2) 0.0201(3) 0.0110(2) -0.0027(2) -0.00233(18) 0.0014(2) C1 0.0086(2) 0.0105(2) 0.0100(3) -0.0003(2) 0.0011(2) 0.00104(19) C2 0.0098(2) 0.0113(3) 0.0094(3) -0.0007(2) 0.0005(2) -0.0005(2) C3 0.0077(2) 0.0124(3) 0.0104(3) 0.0009(2) -0.0004(2) -0.0003(2) C4 0.0081(2) 0.0115(3) 0.0115(3) 0.0007(2) 0.0011(2) 0.0013(2) C5 0.0086(2) 0.0111(3) 0.0103(3) -0.0012(2) 0.0005(2) 0.0007(2) C6 0.0075(2) 0.0116(2) 0.0091(3) -0.0002(2) -0.00006(19) 0.00080(19) C7 0.0076(2) 0.0155(3) 0.0101(3) 0.0001(2) -0.0004(2) 0.0007(2) C8 0.0100(3) 0.0196(3) 0.0158(3) 0.0019(3) 0.0011(2) -0.0024(2) C9 0.0139(3) 0.0251(4) 0.0136(3) 0.0040(3) 0.0028(3) -0.0028(3) C10 0.0124(3) 0.0247(4) 0.0138(3) -0.0019(3) 0.0040(3) 0.0023(3) C11 0.0105(3) 0.0134(3) 0.0134(3) -0.0004(2) 0.0016(2) 0.0036(2) C12 0.0102(3) 0.0160(3) 0.0133(3) 0.0018(3) 0.0000(2) 0.0039(2) C13 0.0112(3) 0.0257(4) 0.0265(5) 0.0010(4) -0.0006(3) -0.0055(3) C14 0.0104(2) 0.0158(4) 0.0160(3) -0.0001(3) 0.0017(2) 0.0034(2) C15 0.0207(4) 0.0147(3) 0.0286(5) 0.0037(3) 0.0043(4) 0.0065(3) C16 0.0224(4) 0.0326(5) 0.0147(3) -0.0081(4) 0.0043(3) 0.0010(5) C17 0.0217(4) 0.0136(3) 0.0261(5) -0.0029(3) -0.0003(4) 0.0057(3) O5 0.0340(5) 0.0314(5) 0.0658(9) 0.0169(6) 0.0115(6) 0.0017(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 C2 1.8906(8) . ? O1 C3 1.3713(9) . ? O1 C13 1.4310(12) . ? O2 C14 1.2111(12) . ? O3 C5 1.3751(10) . ? O3 C16 1.4412(14) . ? O4 H4A 0.70(4) . ? O4 C7 1.4158(11) . ? C1 C2 1.3921(11) . ? C1 C6 1.4044(11) . ? C1 C11 1.5333(11) . ? C2 C3 1.4041(11) . ? C3 C4 1.3893(12) . ? C4 C5 1.3969(11) . ? C4 C14 1.5033(12) . ? C5 C6 1.3859(11) . ? C6 C7 1.5183(10) . ? C7 C8 1.5397(13) . ? C7 C12 1.5231(12) . ? C8 H8A 0.98(2) . ? C8 H8B 0.949(19) . ? C8 C9 1.5366(14) . ? C9 H9A 1.035(18) . ? C9 H9B 1.01(2) . ? C9 C10 1.5357(16) . ? C10 H10A 0.98(2) . ? C10 H10B 0.906(18) . ? C10 C11 1.5458(13) . ? C11 C12 1.5417(13) . ? C11 C17 1.5262(13) . ? C12 H12A 0.993(18) . ? C12 H12B 0.961(15) . ? C13 H13A 0.92(2) . ? C13 H13B 0.98(2) . ? C13 H13C 0.932(18) . ? C14 C15 1.4899(15) . ? C15 H15A 0.97(3) . ? C15 H15B 0.95(2) . ? C15 H15C 1.00(2) . ? C16 H16A 1.02(2) . ? C16 H16B 0.97(2) . ? C16 H16C 0.84(3) . ? C17 H17A 0.96(2) . ? C17 H17B 0.93(2) . ? C17 H17C 1.19(2) . ? O5 H5A 0.83(4) . ? O5 H5B 0.93(8) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 O1 C13 114.67(7) . . ? C5 O3 C16 112.54(9) . . ? C7 O4 H4A 108(4) . . ? C2 C1 C6 119.34(7) . . ? C2 C1 C11 131.62(7) . . ? C6 C1 C11 108.83(6) . . ? C1 C2 Br1 122.18(6) . . ? C1 C2 C3 119.90(7) . . ? C3 C2 Br1 117.73(6) . . ? O1 C3 C2 122.13(7) . . ? O1 C3 C4 117.87(7) . . ? C4 C3 C2 119.80(7) . . ? C3 C4 C5 120.65(7) . . ? C3 C4 C14 119.20(7) . . ? C5 C4 C14 120.09(7) . . ? O3 C5 C4 118.31(7) . . ? O3 C5 C6 122.49(7) . . ? C6 C5 C4 119.20(7) . . ? C1 C6 C7 108.75(7) . . ? C5 C6 C1 120.90(7) . . ? C5 C6 C7 130.12(7) . . ? O4 C7 C6 114.47(7) . . ? O4 C7 C8 111.11(7) . . ? O4 C7 C12 112.59(7) . . ? C6 C7 C8 109.45(7) . . ? C6 C7 C12 100.13(6) . . ? C12 C7 C8 108.47(7) . . ? C7 C8 H8A 110.3(9) . . ? C7 C8 H8B 100.8(11) . . ? H8A C8 H8B 108.1(15) . . ? C9 C8 C7 112.54(7) . . ? C9 C8 H8A 111.3(9) . . ? C9 C8 H8B 113.4(11) . . ? C8 C9 H9A 112.7(10) . . ? C8 C9 H9B 107.0(11) . . ? H9A C9 H9B 102.1(15) . . ? C10 C9 C8 113.37(8) . . ? C10 C9 H9A 107.8(11) . . ? C10 C9 H9B 113.4(12) . . ? C9 C10 H10A 108.4(13) . . ? C9 C10 H10B 109.6(12) . . ? C9 C10 C11 111.74(8) . . ? H10A C10 H10B 108.0(17) . . ? C11 C10 H10A 110.9(12) . . ? C11 C10 H10B 108.2(12) . . ? C1 C11 C10 108.71(7) . . ? C1 C11 C12 100.11(7) . . ? C12 C11 C10 107.17(7) . . ? C17 C11 C1 117.14(8) . . ? C17 C11 C10 111.74(8) . . ? C17 C11 C12 111.01(8) . . ? C7 C12 C11 102.47(6) . . ? C7 C12 H12A 110.7(10) . . ? C7 C12 H12B 108.1(9) . . ? C11 C12 H12A 111.6(10) . . ? C11 C12 H12B 112.1(9) . . ? H12A C12 H12B 111.5(14) . . ? O1 C13 H13A 108.7(14) . . ? O1 C13 H13B 112.7(11) . . ? O1 C13 H13C 109.0(12) . . ? H13A C13 H13B 105.4(18) . . ? H13A C13 H13C 106.8(17) . . ? H13B C13 H13C 113.8(16) . . ? O2 C14 C4 120.71(9) . . ? O2 C14 C15 122.24(9) . . ? C15 C14 C4 117.05(8) . . ? C14 C15 H15A 106.0(16) . . ? C14 C15 H15B 108.4(13) . . ? C14 C15 H15C 110.2(13) . . ? H15A C15 H15B 102(2) . . ? H15A C15 H15C 120(2) . . ? H15B C15 H15C 109.7(18) . . ? O3 C16 H16A 112.2(11) . . ? O3 C16 H16B 110.1(12) . . ? O3 C16 H16C 102.7(17) . . ? H16A C16 H16B 111.1(18) . . ? H16A C16 H16C 110(2) . . ? H16B C16 H16C 110.8(19) . . ? C11 C17 H17A 113.8(12) . . ? C11 C17 H17B 105.1(16) . . ? C11 C17 H17C 114.3(10) . . ? H17A C17 H17B 103.5(19) . . ? H17A C17 H17C 102.8(16) . . ? H17B C17 H17C 117.1(19) . . ? H5A O5 H5B 108(5) . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O4 H4A O5 0.70(4) 2.11(4) 2.7707(15) 158(5) 4_546 C12 H12A O2 0.993(18) 2.577(18) 3.5655(12) 173.5(14) 3_455 C13 H13B Br1 0.98(2) 2.963(19) 3.4746(12) 113.5(13) . C16 H16B O4 0.97(2) 2.54(2) 3.1572(13) 121.7(15) . O5 H5A O2 0.83(4) 2.18(4) 2.8176(15) 133(3) . O5 H5B O5 0.93(8) 1.80(7) 2.678(3) 155(8) 2_656 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br1 C2 C3 O1 -1.53(11) . . . . ? Br1 C2 C3 C4 173.23(6) . . . . ? O1 C3 C4 C5 172.81(7) . . . . ? O1 C3 C4 C14 -4.40(12) . . . . ? O3 C5 C6 C1 179.12(8) . . . . ? O3 C5 C6 C7 5.42(14) . . . . ? O4 C7 C8 C9 178.38(7) . . . . ? O4 C7 C12 C11 -164.95(7) . . . . ? C1 C2 C3 O1 -176.65(8) . . . . ? C1 C2 C3 C4 -1.89(12) . . . . ? C1 C6 C7 O4 150.32(7) . . . . ? C1 C6 C7 C8 -84.20(8) . . . . ? C1 C6 C7 C12 29.65(9) . . . . ? C1 C11 C12 C7 40.37(8) . . . . ? C2 C1 C6 C5 -3.86(12) . . . . ? C2 C1 C6 C7 171.06(7) . . . . ? C2 C1 C11 C10 -84.97(11) . . . . ? C2 C1 C11 C12 162.89(9) . . . . ? C2 C1 C11 C17 42.84(14) . . . . ? C2 C3 C4 C5 -2.18(12) . . . . ? C2 C3 C4 C14 -179.38(8) . . . . ? C3 C4 C5 O3 -176.12(8) . . . . ? C3 C4 C5 C6 3.18(12) . . . . ? C3 C4 C14 O2 -84.34(12) . . . . ? C3 C4 C14 C15 95.72(11) . . . . ? C4 C5 C6 C1 -0.15(12) . . . . ? C4 C5 C6 C7 -173.85(8) . . . . ? C5 C4 C14 O2 98.44(12) . . . . ? C5 C4 C14 C15 -81.50(11) . . . . ? C5 C6 C7 O4 -35.38(12) . . . . ? C5 C6 C7 C8 90.10(11) . . . . ? C5 C6 C7 C12 -156.05(9) . . . . ? C6 C1 C2 Br1 -170.04(6) . . . . ? C6 C1 C2 C3 4.85(12) . . . . ? C6 C1 C11 C10 89.61(8) . . . . ? C6 C1 C11 C12 -22.54(9) . . . . ? C6 C1 C11 C17 -142.58(9) . . . . ? C6 C7 C8 C9 50.99(10) . . . . ? C6 C7 C12 C11 -42.94(8) . . . . ? C7 C8 C9 C10 42.10(11) . . . . ? C8 C7 C12 C11 71.66(8) . . . . ? C8 C9 C10 C11 -43.70(11) . . . . ? C9 C10 C11 C1 -47.37(10) . . . . ? C9 C10 C11 C12 60.01(9) . . . . ? C9 C10 C11 C17 -178.18(8) . . . . ? C10 C11 C12 C7 -72.96(8) . . . . ? C11 C1 C2 Br1 4.07(13) . . . . ? C11 C1 C2 C3 178.96(8) . . . . ? C11 C1 C6 C5 -179.21(8) . . . . ? C11 C1 C6 C7 -4.29(9) . . . . ? C12 C7 C8 C9 -57.35(9) . . . . ? C13 O1 C3 C2 -83.51(11) . . . . ? C13 O1 C3 C4 101.63(10) . . . . ? C14 C4 C5 O3 1.06(12) . . . . ? C14 C4 C5 C6 -179.64(8) . . . . ? C16 O3 C5 C4 -91.05(10) . . . . ? C16 O3 C5 C6 89.68(10) . . . . ? C17 C11 C12 C7 164.77(8) . . . . ? _shelx_res_file ; TITL a14105 in C2 CELL 0.71073 18.8295 7.8451 11.4443 90 95.208 90 ZERR 4 0.0009 0.0004 0.0005 0 0.0021 0 LATT -7 SYMM -X,+Y,-Z SFAC C H Br O UNIT 68 92 4 20 EQIV $1 0.5-X,-0.5+Y,1-Z EQIV $2 -0.5+X,0.5+Y,+Z EQIV $3 1-X,+Y,1-Z L.S. 25 PLAN 40 SIZE 0.29 0.42 0.43 TEMP -173 HTAB O4 O5_$1 HTAB C12 O2_$2 HTAB C13 Br1 HTAB C16 O4 HTAB O5 O2 HTAB O5 O5_$3 REM Solution 2 R1 0.055 Rweak 0.031, Alpha = 0.0265 in C2 BOND $h htab MORE -1 CONF fmap -2 acta 50 REM Z:/frames/bstoltz/a14105/work/a14105.hkl WGHT 0.015700 FVAR 0.17520 BR1 3 0.261127 1.010600 0.968945 11.00000 0.01585 0.01588 = 0.01337 -0.00553 0.00035 -0.00195 O1 4 0.362292 0.740106 0.886709 11.00000 0.00870 0.01901 = 0.01485 0.00218 -0.00307 -0.00120 O2 4 0.389803 0.531907 0.648687 11.00000 0.02403 0.02967 = 0.04429 0.01240 0.02228 0.01159 O3 4 0.208055 0.475100 0.590624 11.00000 0.01513 0.01397 = 0.01449 -0.00527 0.00054 0.00071 O4 4 0.074614 0.669528 0.525625 11.00000 0.01222 0.02012 = 0.01103 -0.00267 -0.00233 0.00142 H4A 2 0.073367 0.580730 0.526807 11.00000 0.11015 C1 1 0.179159 0.854777 0.772193 11.00000 0.00864 0.01046 = 0.00996 -0.00027 0.00111 0.00104 C2 1 0.244402 0.861091 0.839815 11.00000 0.00979 0.01131 = 0.00937 -0.00066 0.00052 -0.00045 C3 1 0.298457 0.744749 0.818794 11.00000 0.00773 0.01244 = 0.01040 0.00090 -0.00038 -0.00028 C4 1 0.285835 0.620598 0.732840 11.00000 0.00806 0.01155 = 0.01149 0.00068 0.00114 0.00127 C5 1 0.219041 0.606558 0.669676 11.00000 0.00862 0.01109 = 0.01035 -0.00118 0.00046 0.00072 C6 1 0.166287 0.723475 0.689561 11.00000 0.00750 0.01159 = 0.00914 -0.00021 -0.00006 0.00080 C7 1 0.088318 0.728897 0.642322 11.00000 0.00759 0.01548 = 0.01009 0.00009 -0.00044 0.00071 C8 1 0.043343 0.631234 0.726097 11.00000 0.00999 0.01963 = 0.01581 0.00189 0.00108 -0.00238 H8A 2 0.050404 0.508532 0.718300 11.00000 0.01836 H8B 2 -0.003437 0.658027 0.693293 11.00000 0.02371 C9 1 0.058419 0.688943 0.854255 11.00000 0.01391 0.02510 = 0.01361 0.00405 0.00280 -0.00278 H9A 2 0.019882 0.648133 0.906847 11.00000 0.02312 H9B 2 0.101772 0.624754 0.888000 11.00000 0.02714 C10 1 0.065457 0.883090 0.867987 11.00000 0.01241 0.02469 = 0.01379 -0.00188 0.00400 0.00227 H10A 2 0.086286 0.907798 0.947498 11.00000 0.03257 H10B 2 0.021641 0.931524 0.858858 11.00000 0.02438 C11 1 0.111033 0.961002 0.775720 11.00000 0.01047 0.01341 = 0.01335 -0.00044 0.00158 0.00362 C12 1 0.073452 0.918705 0.653852 11.00000 0.01023 0.01604 = 0.01332 0.00185 0.00002 0.00392 H12A 2 0.021336 0.940421 0.650570 11.00000 0.02083 H12B 2 0.094740 0.977122 0.591956 11.00000 0.01210 C13 1 0.413994 0.860832 0.854297 11.00000 0.01118 0.02573 = 0.02654 0.00096 -0.00063 -0.00554 H13A 2 0.456060 0.842770 0.900069 11.00000 0.03747 H13B 2 0.400504 0.979436 0.869707 11.00000 0.03357 H13C 2 0.423323 0.840687 0.776856 11.00000 0.02267 C14 1 0.343965 0.495781 0.712156 11.00000 0.01039 0.01581 = 0.01605 -0.00010 0.00165 0.00339 C15 1 0.342190 0.327973 0.772784 11.00000 0.02068 0.01471 = 0.02862 0.00366 0.00427 0.00650 H15A 2 0.371585 0.252082 0.730972 11.00000 0.05301 H15B 2 0.296192 0.279807 0.755906 11.00000 0.03384 H15C 2 0.352264 0.343313 0.859768 11.00000 0.03456 C16 1 0.224675 0.521977 0.474424 11.00000 0.02243 0.03262 = 0.01469 -0.00807 0.00430 0.00103 H16A 2 0.276962 0.556130 0.472409 11.00000 0.03633 H16B 2 0.193004 0.612436 0.443571 11.00000 0.03055 H16C 2 0.216820 0.431662 0.436493 11.00000 0.04290 C17 1 0.120011 1.153149 0.791812 11.00000 0.02171 0.01363 = 0.02614 -0.00289 -0.00028 0.00567 H17A 2 0.137840 1.186176 0.870264 11.00000 0.02851 H17B 2 0.073687 1.197085 0.783870 11.00000 0.04194 H17C 2 0.161875 1.215386 0.733278 11.00000 0.03195 O5 4 0.435304 0.829744 0.539848 11.00000 0.03402 0.03141 = 0.06575 0.01691 0.01154 0.00169 H5A 2 0.407530 0.747251 0.534193 11.00000 0.07614 H5B 2 0.475747 0.800450 0.503085 10.50000 -1.50000 HKLF 4 REM a14105 in C2 REM R1 = 0.0256 for 14231 Fo > 4sig(Fo) and 0.0344 for all 16574 data REM 299 parameters refined using 1 restraints END WGHT 0.0157 0.0000 REM Instructions for potential hydrogen bonds HTAB O4 O5_$1 HTAB C12 O2_$2 HTAB C13 Br1 HTAB C16 O4 HTAB O5 O2 HTAB O5 O5_$3 REM Highest difference peak 0.653, deepest hole -0.707, 1-sigma level 0.100 Q1 1 0.2431 1.0107 0.9633 11.00000 0.05 -0.71 Q2 1 0.2659 1.0592 0.9743 11.00000 0.05 -0.65 Q3 1 0.2325 1.0213 1.0172 11.00000 0.05 -0.64 Q4 1 0.4388 0.8579 0.5820 11.00000 0.05 -0.62 Q5 1 0.2699 0.9775 0.9857 11.00000 0.05 -0.59 Q6 1 0.2340 0.9762 0.9092 11.00000 0.05 -0.58 Q7 1 0.0552 0.7153 0.4727 11.00000 0.05 -0.57 Q8 1 0.2587 1.0035 1.0120 11.00000 0.05 -0.57 Q9 1 0.2682 1.0266 1.0421 11.00000 0.05 -0.57 Q10 1 0.2190 1.0148 0.9349 11.00000 0.05 -0.54 Q11 1 0.2375 1.0500 0.9114 11.00000 0.05 -0.52 Q12 1 0.2829 1.0559 1.0304 11.00000 0.05 -0.51 Q13 1 0.2630 1.0094 0.9372 11.00000 0.05 -0.51 Q14 1 0.2470 0.9065 0.9617 11.00000 0.05 -0.50 Q15 1 0.4155 0.8314 0.5300 11.00000 0.05 -0.50 Q16 1 0.2443 0.9630 1.0401 11.00000 0.05 -0.50 Q17 1 0.2768 0.9630 1.0422 11.00000 0.05 -0.50 Q18 1 0.2911 1.0027 0.9175 11.00000 0.05 -0.49 Q19 1 0.0535 0.6607 0.4208 11.00000 0.05 -0.47 Q20 1 0.2725 1.1178 0.9806 11.00000 0.05 -0.47 Q21 1 0.2135 1.0398 1.0691 11.00000 0.05 -0.47 Q22 1 0.3807 0.5111 0.6012 11.00000 0.05 -0.47 Q23 1 0.2700 0.9069 0.9759 11.00000 0.05 -0.45 Q24 1 0.2454 1.1133 0.9638 11.00000 0.05 -0.45 Q25 1 0.2236 1.0030 1.1091 11.00000 0.05 -0.44 Q26 1 0.4258 0.7848 0.4930 11.00000 0.05 0.43 Q27 1 0.2463 1.1068 0.9353 11.00000 0.05 -0.41 Q28 1 0.0844 0.6965 0.4685 11.00000 0.05 -0.41 Q29 1 0.2938 0.9446 0.9419 11.00000 0.05 -0.41 Q30 1 0.2343 1.0170 1.0698 11.00000 0.05 -0.40 Q31 1 0.2362 0.9287 1.0001 11.00000 0.05 -0.38 Q32 1 0.2573 0.9212 0.9227 11.00000 0.05 -0.37 Q33 1 0.2708 1.0599 0.9004 11.00000 0.05 -0.37 Q34 1 0.2964 0.6863 0.7763 11.00000 0.05 0.37 Q35 1 0.2587 0.7610 0.7671 11.00000 0.05 -0.36 Q36 1 0.2135 0.8557 0.8133 11.00000 0.05 0.36 Q37 1 0.0895 1.0161 0.8687 11.00000 0.05 -0.36 Q38 1 0.3042 1.0448 1.0023 11.00000 0.05 -0.36 Q39 1 0.3139 0.5279 0.7212 11.00000 0.05 0.36 Q40 1 0.0657 1.0358 0.8520 11.00000 0.05 -0.35 REM The information below was added by Olex2. REM REM R1 = 0.0256 for 14231 Fo > 4sig(Fo) and 0.0344 for all 78240 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.65, deepest hole -0.71 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0344 REM R1_gt = 0.0256 REM wR_ref = 0.0538 REM GOOF = 0.966 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 78240 REM Reflections_gt = 14231 REM Parameters = n/a REM Hole = -0.71 REM Peak = 0.65 REM Flack = 0.029(2) ; loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 4 0 0 44.14 3.4 4 0 0 45.23 3.41 4 0 0 45.13 3.45 -4 0 0 45.39 3.45 -4 0 0 47.87 3.41 -4 0 0 45.67 3.41 6 0 0 1000 75.06 8 0 0 19.5 1.54 -8 0 0 19.32 1.56 8 0 0 22.19 1.57 8 0 0 19.52 1.55 -8 0 0 19.87 1.55 -8 0 0 19.05 1.54 10 0 0 140.59 10.01 10 0 0 135.49 9.88 -10 0 0 131.62 10.01 10 0 0 126.04 9.9 -10 0 0 131.24 9.9 -10 0 0 130.26 9.88 12 0 0 83.82 6.52 -12 0 0 87.37 6.09 12 0 0 79.49 6.45 -12 0 0 83.3 6.45 12 0 0 84.89 5.22 12 0 0 88.78 6.33 -12 0 0 88.34 6.44 12 0 0 90.28 6.44 12 0 0 88.54 6.18 -12 0 0 83.18 6.52 -12 0 0 83.5 6.08 -12 0 0 88.51 6.05 14 0 0 1.36 0.34 -14 0 0 1.4 0.34 -14 0 0 1.46 0.34 14 0 0 1.73 0.33 14 0 0 0.68 0.33 -14 0 0 1.57 0.36 14 0 0 1.25 0.32 -14 0 0 1.24 0.34 -14 0 0 1.12 0.25 14 0 0 1.26 0.35 -14 0 0 1.47 0.36 -16 0 0 12.94 1.01 16 0 0 12.67 1.13 16 0 0 13.21 1.14 16 0 0 13.75 1.17 16 0 0 12.33 1.2 -16 0 0 12.45 1.11 -16 0 0 11.84 1.07 -16 0 0 13.69 1.22 16 0 0 13.07 1.2 16 0 0 13.14 1.13 16 0 0 14.11 1.15 -16 0 0 13.24 1.21 -16 0 0 13.58 1.2 18 0 0 1.04 0.4 -18 0 0 0.61 0.31 -18 0 0 0.4 0.38 -18 0 0 0.21 0.38 18 0 0 -0.15 0.36 18 0 0 0.45 0.42 18 0 0 0.62 0.44 -18 0 0 0.34 0.34 18 0 0 0.28 0.4 -18 0 0 0.99 0.42 18 0 0 0.43 0.36 -20 0 0 -0.39 0.5 20 0 0 0.12 0.43 -20 0 0 0.03 0.36 20 0 0 0.06 0.47 -20 0 0 0.14 0.34 20 0 0 0.27 0.52 -20 0 0 0.04 0.44 20 0 0 1.16 0.48 -22 0 0 14.72 1.33 22 0 0 15.68 1.42 22 0 0 13.82 1.38 -22 0 0 13.94 1.4 -22 0 0 15.27 1.28 24 0 0 4.1 0.84 -24 0 0 2.81 0.76 -24 0 0 3.38 0.78 24 0 0 3.52 0.8 -24 0 0 3.3 0.59 -26 0 0 0.98 0.78 26 0 0 0.13 0.78 -26 0 0 1.82 0.79 26 0 0 0.75 0.81 -26 0 0 0.94 0.57 28 0 0 0.6 0.8 -28 0 0 0.13 0.75 -28 0 0 -0.08 0.76 -28 0 0 0.42 0.62 28 0 0 -0.3 0.77 -30 0 0 -0.05 0.83 -30 0 0 1.26 0.97 30 0 0 1.13 0.97 -30 0 0 0.88 0.97 30 0 0 0.81 1.01 -32 0 0 4.67 1.19 -32 0 0 5.09 1.17 -32 0 0 5.22 1.12 -32 0 0 3.47 1.02 32 0 0 4.53 1.13 34 0 0 1.99 1.16 -34 0 0 2.11 1.11 -34 0 0 2.54 1.13 -34 0 0 1.07 1.08 -36 0 0 0.91 1.14 -36 0 0 0.8 1.16 36 0 0 1.85 1.18 -36 0 0 1.42 1.16 -38 0 0 0.66 1.08 -38 0 0 2.45 1.22 -38 0 0 2.79 1.18 38 0 0 1.78 1.18 -1 -1 0 94.28 5.94 1 -1 0 100.3 7.25 -1 -1 0 96.63 7.25 -1 -1 0 89.11 7.26 1 -1 0 101.84 7.26 1 -1 0 98.8 7.34 -1 -1 0 95.71 7.34 1 -1 0 91.18 5.94 1 -1 0 92.37 6.2 1 1 0 96.14 7.26 1 1 0 109.94 7.34 -1 1 0 96.03 7.25 -1 1 0 99.03 6.2 -1 1 0 89.86 7.26 -1 1 0 90.97 7.34 1 1 0 106.02 5.94 1 1 0 98.4 7.25 -1 1 0 95.79 5.94 -3 -1 0 39.11 2.96 -3 -1 0 40.15 2.96 -3 -1 0 40.82 2.41 3 -1 0 42.25 2.42 3 -1 0 41.92 2.98 3 -1 0 40.59 2.95 3 -1 0 41.84 2.94 -3 -1 0 37.73 2.99 -3 1 0 37.02 2.95 -3 1 0 38.02 2.98 3 1 0 35.17 2.99 3 1 0 39.06 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5.52 15 -3 0 79.53 5.58 -15 -3 0 85.05 5.69 -15 -3 0 79.42 5.3 15 -3 0 80.77 5.58 15 -3 0 82.36 5.7 -15 -3 0 85.15 5.39 -15 -3 0 84.01 5.38 15 -3 0 81.83 5.4 15 3 0 64.36 5.4 15 3 0 67.19 5.37 15 3 0 63.17 5.65 15 3 0 71.4 5.68 15 3 0 69.05 5.65 -15 3 0 68.55 5.68 -15 3 0 66.18 5.29 -15 3 0 64.75 5.62 15 3 0 70.93 5.65 15 3 0 62.57 5.73 -15 3 0 66.77 5.32 -15 3 0 63.9 5.61 15 3 0 67.29 5.51 -15 3 0 64.95 5.1 -17 -3 0 82.06 5.7 17 -3 0 75.94 5.87 -17 -3 0 70.44 5.98 -17 -3 0 78.11 5.4 -17 -3 0 77.65 5.61 -17 -3 0 76.87 5.65 17 -3 0 80.02 4.84 17 -3 0 76.34 5.71 -17 -3 0 77.29 5.69 -17 3 0 83.37 5.41 -17 3 0 76.88 5.64 -17 3 0 73.95 5.61 17 3 0 82.28 5.99 17 3 0 76.92 5.73 -17 3 0 83.15 5.97 17 3 0 82.79 5.85 17 3 0 81.89 5.69 17 3 0 81.82 6.04 19 -3 0 80.96 6.4 -19 -3 0 83.38 6.29 19 -3 0 80.49 6.56 -19 -3 0 82.33 6.33 -19 -3 0 87.56 6.38 -19 -3 0 86.53 6.04 -19 -3 0 88.56 6.71 19 3 0 90.68 6.7 19 3 0 92.58 6.44 -19 3 0 90.85 6.29 19 3 0 97.2 6.56 -19 3 0 93.86 6.06 -19 3 0 91.48 6.34 -21 -3 0 50.21 4.28 21 -3 0 51.14 4.21 -21 -3 0 52.79 3.99 -21 -3 0 52.82 4.04 -21 -3 0 55.31 4.04 21 -3 0 52.71 4.06 -21 3 0 54.52 3.98 21 3 0 57.03 4.28 -21 3 0 59.84 3.84 21 3 0 54.88 4.09 -21 3 0 55.44 4.05 21 3 0 60.01 4.18 -23 -3 0 31.97 3 -23 -3 0 32.44 2.78 23 -3 0 30.17 2.9 -23 -3 0 32.05 2.82 23 -3 0 32.09 2.82 -23 -3 0 33.24 2.84 23 3 0 39.29 2.91 -23 3 0 39.91 2.76 -23 3 0 42.43 2.66 23 3 0 39.71 2.98 -23 3 0 39.56 2.82 -23 3 0 38.53 2.8 23 3 0 42.07 2.91 -25 -3 0 16.47 1.65 25 -3 0 14.49 1.51 25 -3 0 14.4 1.48 -25 -3 0 16.15 1.44 -25 -3 0 14.44 1.55 25 3 0 13.05 1.52 -25 3 0 14.76 1.37 -25 3 0 11.94 1.38 -25 3 0 12.28 1.4 25 3 0 11.63 1.41 25 3 0 15.47 1.5 -27 -3 0 33.73 2.62 27 -3 0 36.43 2.6 -27 -3 0 33.51 2.78 -27 -3 0 35.6 2.62 27 -3 0 33.56 2.73 27 3 0 26.61 2.67 27 3 0 30.12 2.62 -27 3 0 26.68 2.6 27 3 0 25.99 2.56 -27 3 0 27.73 2.6 -27 3 0 31.25 2.48 29 -3 0 27.44 2.51 29 -3 0 24.91 2.61 -29 -3 0 28.02 2.42 -29 -3 0 26.13 2.51 -29 -3 0 29.16 2.68 29 3 0 30.58 2.58 -29 3 0 30.53 2.53 -29 3 0 28.79 2.51 -29 3 0 29.81 2.38 -31 -3 0 8.77 1.38 -31 -3 0 10.19 1.27 31 -3 0 10.01 1.32 -31 -3 0 9.61 1.4 31 -3 0 8.67 1.36 31 3 0 8.99 1.37 -31 3 0 9.53 1.34 -31 3 0 8.46 1.33 -31 3 0 10.18 1.14 33 -3 0 18 1.65 -33 -3 0 15.68 1.74 -33 -3 0 15.51 1.63 -33 -3 0 15.72 1.63 -33 3 0 9.6 1.54 33 3 0 12.02 1.61 -33 3 0 11.62 1.56 -33 3 0 12.06 1.38 -35 -3 0 5.93 1.24 35 -3 0 5.28 1.22 -35 -3 0 4.67 1.27 -35 -3 0 3.69 1.27 -35 3 0 6.32 1.25 -35 3 0 5.81 1.01 35 3 0 4.55 1.33 -35 3 0 6.15 1.21 -37 -3 0 0.88 1.18 37 -3 0 0.51 1.08 -37 -3 0 0.02 1.09 -37 -3 0 1 1.17 -37 3 0 0.93 1.18 -37 3 0 -1.59 1.1 -37 3 0 0.16 1.08 37 3 0 0.61 1.28 0 -4 0 241.83 16.25 0 -4 0 240.35 16.25 0 -4 0 238.41 16.43 0 -4 0 222.07 13.3 0 -4 0 223.45 13.87 0 -4 0 218.82 16.42 0 4 0 199.07 13.3 0 4 0 190.91 16.22 0 4 0 188.67 16.22 -2 -4 0 472.18 31.1 2 -4 0 477.88 31.09 2 -4 0 475.12 29.79 2 -4 0 502.21 36.42 -2 -4 0 477.15 29.78 -2 -4 0 473.77 36.43 -2 -4 0 471.97 36.82 2 -4 0 506.73 36.81 -2 -4 0 487.04 36.82 -2 -4 0 512.42 36.43 2 4 0 526.12 36.37 2 4 0 505.88 29.79 -2 4 0 516.81 29.79 -2 4 0 487.46 36.42 2 4 0 465.73 36.37 -2 4 0 483.34 36.36 -4 -4 0 95.02 6.58 -4 -4 0 94.09 8.13 -4 -4 0 93 6.87 4 -4 0 97.87 8.03 -4 -4 0 93.49 8.02 -4 -4 0 98.24 8.05 -4 4 0 124.78 6.86 4 4 0 122.88 6.59 4 4 0 116.72 8.14 4 4 0 120.66 8.05 4 4 0 127.7 8.06 -6 -4 0 40.93 3.34 -6 -4 0 46.97 3.37 -6 -4 0 44.54 2.74 6 -4 0 46.37 3.27 6 -4 0 45.32 3.33 -6 -4 0 46.24 3.15 6 -4 0 44.12 3.36 -6 -4 0 46.66 3.17 6 -4 0 43.85 2.84 6 -4 0 45.83 2.76 -6 -4 0 46.88 3.41 6 -4 0 48.58 3.22 6 -4 0 46.35 3.21 6 4 0 46.88 3.36 -6 4 0 44.53 2.75 -6 4 0 43.13 3.32 6 4 0 43.16 3.36 -6 4 0 41.71 3.36 6 4 0 43.14 2.74 6 4 0 44.68 3.22 6 4 0 41.2 3.36 -6 4 0 41.32 3.32 6 4 0 42.05 3.35 6 4 0 39.73 3.39 -6 4 0 42.24 2.83 -8 -4 0 278.82 19.54 8 -4 0 274.95 17.02 -8 -4 0 285.66 20.79 -8 -4 0 270.2 20.83 8 -4 0 267.65 20.79 8 -4 0 272.47 21.02 -8 -4 0 275.79 17.01 -8 -4 0 266.81 21.05 -8 -4 0 281.66 19.66 -8 -4 0 281.95 20.32 8 -4 0 275.88 20.32 8 -4 0 281.09 19.96 8 4 0 287.47 21.05 8 4 0 305.12 20.87 8 4 0 262.27 20.82 8 4 0 278.73 19.69 8 4 0 292.82 19.97 -8 4 0 282.38 19.67 -8 4 0 277.3 17.74 8 4 0 277.5 20.8 8 4 0 285.55 17.01 8 4 0 284.99 20.79 -8 4 0 273.06 21.01 -8 4 0 279.31 20.79 -8 4 0 289.41 20.76 -10 -4 0 49.11 4.17 10 -4 0 50.76 3.41 -10 -4 0 52.42 3.4 -10 -4 0 52.03 3.94 -10 -4 0 50.59 3.91 -10 -4 0 48.39 4.2 -10 -4 0 52.18 3.78 10 -4 0 52.57 4.2 10 -4 0 51.58 4 -10 -4 0 48.96 4.18 10 -4 0 52.91 4.1 10 -4 0 50.91 4.1 -10 -4 0 50.88 4.08 10 -4 0 50.11 4.15 -10 -4 0 48.03 4.24 10 -4 0 51.17 4.08 10 4 0 58.08 4.19 10 4 0 60.61 4.01 10 4 0 52.56 4.24 10 4 0 60.17 4.01 10 4 0 58.69 4.21 -10 4 0 61.69 3.8 -10 4 0 61.15 4.2 10 4 0 59.62 4.19 -10 4 0 59.69 4.15 10 4 0 63.15 3.94 -10 4 0 60.54 3.53 -10 4 0 61 3.91 -10 4 0 61.59 4.16 10 4 0 59.78 3.4 10 4 0 55.76 4.2 12 -4 0 30.06 2.42 -12 -4 0 28.82 2.33 -12 -4 0 30.49 2.22 12 -4 0 28.88 2.36 12 -4 0 29.21 2.41 -12 -4 0 31.45 2.34 12 -4 0 29.39 2.01 12 -4 0 29.73 2.37 12 -4 0 31.9 2.47 12 -4 0 30.28 2.37 -12 -4 0 29.41 2.47 -12 -4 0 30.23 2.33 -12 -4 0 27.86 2.5 -12 -4 0 28.79 2.53 -12 -4 0 29.06 2.3 12 -4 0 29.22 2.44 -12 -4 0 28.37 2.48 12 4 0 35.35 2.55 12 4 0 34 2.5 -12 4 0 33.29 2.44 12 4 0 33.43 2.36 -12 4 0 34.26 2.23 12 4 0 36.36 2.32 -12 4 0 33.14 2.27 -12 4 0 32.96 2.46 12 4 0 32.97 1.98 -12 4 0 34.62 2.06 12 4 0 34.74 2.48 12 4 0 33.78 2.37 12 4 0 33.39 2.5 -12 4 0 33.59 2.45 12 4 0 33.18 2.52 14 -4 0 40.62 3.51 -14 -4 0 40.35 3.53 14 -4 0 41.14 3.43 14 -4 0 39.62 3.43 -14 -4 0 44.35 3.16 -14 -4 0 41.13 3.27 -14 -4 0 41.36 3.51 14 -4 0 42.96 2.84 -14 -4 0 44.28 3.32 -14 -4 0 42.03 3.31 14 -4 0 43.08 3.4 -14 -4 0 43.64 3.32 14 -4 0 44.44 3.33 14 -4 0 45.2 3.48 -14 -4 0 40.53 3.57 -14 4 0 49.66 3.18 14 4 0 46.23 3.52 -14 4 0 50.11 3.48 -14 4 0 51.78 3.49 14 4 0 52.61 3.41 -14 4 0 49.01 3.26 14 4 0 48.65 3.37 14 4 0 48.55 3.34 14 4 0 52.53 3.29 14 4 0 48 3.56 14 4 0 49.64 2.82 -16 -4 0 2.47 0.5 -16 -4 0 2.36 0.51 -16 -4 0 2.54 0.42 -16 -4 0 2.37 0.43 -16 -4 0 2.3 0.47 16 -4 0 2.38 0.53 16 -4 0 2.05 0.43 16 -4 0 2.48 0.33 16 -4 0 1.82 0.54 -16 -4 0 2.29 0.52 -16 -4 0 2.51 0.41 16 4 0 1.17 0.45 16 4 0 0.61 0.39 -16 4 0 1.64 0.43 -16 4 0 1.04 0.4 16 4 0 1.6 0.41 16 4 0 1.13 0.5 16 4 0 2.23 0.53 -16 4 0 1.29 0.46 -16 4 0 1.11 0.3 -18 -4 0 9.44 0.99 18 -4 0 10.19 0.9 -18 -4 0 8.25 0.96 -18 -4 0 9.31 0.85 -18 -4 0 8.46 0.9 18 -4 0 9.04 0.94 -18 -4 0 9.31 0.83 18 4 0 7.43 0.86 -18 4 0 7.17 0.77 18 4 0 7.38 0.88 18 4 0 6.86 0.84 -18 4 0 7.44 0.85 -18 4 0 7.32 0.88 18 4 0 7.47 0.92 -20 -4 0 16.39 1.62 20 -4 0 18.93 1.48 -20 -4 0 16.39 1.53 -20 -4 0 16.36 1.47 20 -4 0 15.67 1.53 -20 -4 0 18.73 1.43 -20 4 0 16.53 1.49 -20 4 0 18.4 1.4 20 4 0 16.69 1.56 -20 4 0 15.97 1.38 20 4 0 15.13 1.54 20 4 0 17.24 1.51 -22 -4 0 1.87 0.66 -22 -4 0 2.07 0.77 22 -4 0 2.84 0.65 22 -4 0 2.38 0.71 -22 -4 0 3.07 0.68 -22 4 0 2.16 0.73 22 4 0 2.72 0.65 -22 4 0 2.4 0.61 -22 4 0 1.67 0.49 22 4 0 2.21 0.69 22 4 0 2.3 0.66 -24 -4 0 2.48 0.81 24 -4 0 0.87 0.84 24 -4 0 2.52 0.75 -24 -4 0 1.53 0.76 -24 -4 0 2 0.73 24 4 0 2 0.86 -24 4 0 2.88 0.65 -24 4 0 2.58 0.83 24 4 0 4.3 0.77 -24 4 0 2.87 0.58 -24 4 0 2.93 0.74 24 4 0 2.56 0.8 26 -4 0 2.26 0.85 -26 -4 0 1.08 0.81 -26 -4 0 1.68 0.9 26 -4 0 2.5 0.8 -26 -4 0 1.5 0.79 26 4 0 2.15 0.84 26 4 0 3.07 0.82 26 4 0 1.97 0.82 -26 4 0 1.19 0.79 -26 4 0 2.87 0.88 -26 4 0 1.76 0.61 -28 -4 0 17.28 1.85 28 -4 0 19.15 1.72 28 -4 0 14.4 1.77 -28 -4 0 17.45 1.71 -28 -4 0 16.82 1.93 -28 4 0 17.83 1.63 28 4 0 15.82 1.72 -28 4 0 13.35 1.62 28 4 0 17.81 1.84 -28 4 0 14.27 1.63 -30 -4 0 14.33 1.68 -30 -4 0 14.33 1.61 30 -4 0 13.67 1.64 -30 -4 0 15.13 1.63 30 -4 0 17.37 1.8 -30 4 0 13.34 1.59 30 4 0 14.65 1.67 -30 4 0 13.47 1.61 -30 4 0 15.61 1.6 -32 -4 0 13.68 1.71 -32 -4 0 15.83 1.69 32 -4 0 15.62 1.6 -32 -4 0 13.22 1.6 32 4 0 12.6 1.65 -32 4 0 13.09 1.62 -32 4 0 12.45 1.58 -32 4 0 15.33 1.45 -34 -4 0 6.88 1.46 -34 -4 0 7.26 1.3 -34 -4 0 7.27 1.33 -34 -4 0 8.95 1.41 -34 4 0 6.82 1.05 -34 4 0 4.89 1.17 34 4 0 7.06 1.35 -34 4 0 5.79 1.23 -36 -4 0 0.62 1.18 -36 -4 0 0.82 1.23 -36 -4 0 -0.5 1.12 -36 -4 0 -0.5 1.11 -36 4 0 0 1.11 -36 4 0 0.88 0.84 -36 4 0 -0.63 1.02 36 4 0 0.02 1.26 -38 -4 0 3.83 1.32 -38 -4 0 2.03 1.12 -38 -4 0 2.43 1.22 -38 -4 0 2.81 1.19 -38 4 0 2.93 1.1 -38 4 0 0.86 1.12 -38 4 0 3.31 1.25 38 4 0 2.15 1.29 -1 -5 0 23.7 1.65 1 -5 0 22.61 1.45 1 -5 0 22.54 1.7 1 -5 0 22.91 1.61 -1 -5 0 21.44 1.67 -1 -5 0 22.43 1.44 1 -5 0 21.82 1.45 1 -5 0 23.21 1.65 -1 -5 0 19.94 1.72 1 -5 0 20.79 1.71 -1 -5 0 21.19 1.46 1 -5 0 22.17 1.7 -1 -5 0 21.11 1.71 -1 -5 0 22.73 1.61 1 -5 0 22.86 1.72 -1 -5 0 22.97 1.73 -1 -5 0 21.78 1.71 1 5 0 21.28 1.66 1 5 0 20.95 1.71 1 5 0 20.1 1.58 1 5 0 21.27 1.7 -1 5 0 20.96 1.7 1 5 0 21.58 1.43 -1 5 0 22.74 1.7 -1 5 0 22.45 1.45 -1 5 0 22.25 1.58 -3 -5 0 7.71 0.73 -3 -5 0 8.41 0.72 3 -5 0 9.33 0.69 -3 -5 0 8.25 0.72 3 -5 0 9.64 0.73 -3 -5 0 7.2 0.72 -3 -5 0 8.08 0.68 3 -5 0 9.17 0.7 3 -5 0 8.77 0.68 3 -5 0 9.29 0.66 3 -5 0 9.78 0.7 -3 -5 0 7.54 0.63 -3 -5 0 7.65 0.66 3 -5 0 8.88 0.59 -3 -5 0 8.91 0.64 -3 -5 0 8.47 0.67 -3 -5 0 7.62 0.73 3 5 0 5.86 0.68 -3 5 0 6.2 0.67 3 5 0 5.84 0.71 3 5 0 5.37 0.7 3 5 0 5.18 0.62 -3 5 0 6.24 0.58 -5 -5 0 37.86 2.92 -5 -5 0 41.16 2.7 -5 -5 0 39.57 2.88 5 -5 0 41.23 2.85 5 -5 0 44.22 2.76 -5 -5 0 40.33 2.47 -5 -5 0 40.88 2.8 -5 -5 0 41.71 2.72 -5 -5 0 43.8 2.75 5 -5 0 42.53 2.81 -5 -5 0 37.91 2.85 -5 -5 0 43.83 2.9 -5 -5 0 42.56 2.93 -5 -5 0 41.42 2.37 5 -5 0 42.78 2.38 5 -5 0 42.77 2.43 5 -5 0 42.86 2.77 5 5 0 31.97 2.87 -5 5 0 33.4 2.42 -5 5 0 33.07 2.87 5 5 0 30.95 2.9 5 5 0 32.68 2.86 5 5 0 30.67 2.76 5 5 0 32.75 2.86 5 5 0 31.28 2.36 5 5 0 31.48 2.69 -5 5 0 32.71 2.83 -5 5 0 31.4 2.83 -5 5 0 33.69 2.66 7 -5 0 218.94 15.62 -7 -5 0 211.38 16.28 -7 -5 0 223.56 13.33 7 -5 0 229.53 16.46 7 -5 0 223.05 15.93 -7 -5 0 221.44 16.5 -7 -5 0 228.57 13.94 -7 -5 0 224.5 15.92 7 -5 0 220.04 15.65 -7 -5 0 219.59 15.4 -7 -5 0 211.79 16.32 7 -5 0 214.8 16.28 -7 -5 0 223.3 15.31 -7 -5 0 235.08 15.63 7 -5 0 221.4 13.34 -7 5 0 223.42 16.28 7 5 0 209.89 16.31 -7 5 0 211.75 16.26 7 5 0 200.48 16.49 7 5 0 211.24 15.42 7 5 0 209.32 16.34 7 5 0 219.98 15.65 7 5 0 223.89 13.34 7 5 0 227.13 16.3 -7 5 0 223.26 14.65 -7 5 0 219.99 15.39 7 5 0 204.1 16.29 -7 5 0 217.53 16.45 -7 5 0 214.65 13.89 -9 -5 0 33.3 2.59 -9 -5 0 32.75 2.66 -9 -5 0 32.63 2.6 -9 -5 0 30.74 2.23 -9 -5 0 32.44 2.56 9 -5 0 31.29 2.67 -9 -5 0 31.73 2.72 -9 -5 0 32.23 2.58 9 -5 0 30.22 2.63 9 -5 0 29.67 2.66 9 -5 0 31.01 2.7 -9 -5 0 29.93 2.76 -9 -5 0 30.95 2.79 9 -5 0 31.39 2.25 -9 -5 0 33.08 2.73 -9 5 0 39.41 2.7 9 5 0 39.86 2.24 9 5 0 37.35 2.76 -9 5 0 38.54 2.29 9 5 0 40.33 2.58 9 5 0 41.43 2.62 9 5 0 39.69 2.81 -9 5 0 39.01 2.53 -9 5 0 40.86 2.73 -9 5 0 38.95 2.71 9 5 0 38.93 2.76 -9 5 0 39.58 2.46 9 5 0 40.1 2.64 9 5 0 39.23 2.77 11 -5 0 42.38 2.96 -11 -5 0 41.09 2.82 -11 -5 0 39.38 2.79 11 -5 0 39.44 2.46 -11 -5 0 45.09 2.99 -11 -5 0 41.67 3 -11 -5 0 41.17 2.93 -11 -5 0 41.44 2.43 11 -5 0 39.32 2.92 -11 -5 0 44.89 3.05 -11 -5 0 43.45 3.07 11 -5 0 42.52 2.93 11 -5 0 41.05 2.87 -11 -5 0 42.3 2.83 11 -5 0 43.9 2.99 -11 -5 0 42.45 2.84 -11 5 0 36.09 2.65 11 5 0 34.98 2.42 11 5 0 35.7 3.05 -11 5 0 33.43 2.94 11 5 0 36.04 2.85 -11 5 0 36.79 2.97 -11 5 0 35.07 2.75 11 5 0 37.76 2.8 -11 5 0 34.6 2.71 -11 5 0 35.18 2.49 11 5 0 33.8 3.01 -11 5 0 37.36 2.94 11 5 0 33.99 2.86 11 5 0 36.45 3 11 5 0 34.62 3 11 5 0 34.35 2.99 13 -5 0 129.48 7.79 -13 -5 0 123.06 9.54 -13 -5 0 131.58 9.57 13 -5 0 124.36 9.14 13 -5 0 123.76 9.3 -13 -5 0 132.51 9.1 -13 -5 0 132.32 9.11 -13 -5 0 122.78 8.94 -13 -5 0 124.14 8.99 -13 -5 0 120.72 9.29 13 -5 0 125.42 9.35 -13 5 0 126.22 9.5 13 5 0 122.25 9 -13 5 0 128.25 8.65 -13 5 0 121.84 8.96 13 5 0 136.62 9.57 -13 5 0 122.98 9.49 13 5 0 132.26 7.76 -13 5 0 131.5 8.54 13 5 0 125.07 9.55 13 5 0 128.85 9.14 13 5 0 126.71 9.13 -15 -5 0 36.56 2.89 15 -5 0 36.46 3.04 15 -5 0 36.55 2.51 15 -5 0 34.62 3.01 -15 -5 0 37.62 3.1 -15 -5 0 37.93 2.78 -15 -5 0 35.9 3.14 -15 -5 0 36.66 3.01 -15 -5 0 37.16 2.91 -15 -5 0 38.15 2.92 -15 -5 0 39.12 2.93 -15 5 0 46.84 2.86 15 5 0 48.95 2.97 -15 5 0 49.37 2.81 -17 -5 0 76.7 5.75 -17 -5 0 75.75 5.56 -17 -5 0 76.94 5.89 17 -5 0 82.54 5.62 -17 -5 0 76.75 5.31 -17 -5 0 76.54 5.51 17 -5 0 75.23 5.74 17 -5 0 75.15 5.77 -17 -5 0 79.75 5.58 -17 5 0 76.43 5.56 17 5 0 76.72 5.61 17 5 0 77.84 5.89 -17 5 0 77.3 5.33 17 5 0 78.23 5.64 -17 5 0 74.08 5.49 -19 -5 0 61.62 5.05 -19 -5 0 64.68 4.93 19 -5 0 70.16 4.8 19 -5 0 66.48 4.94 19 -5 0 64.98 4.93 -19 -5 0 67.74 4.74 -19 -5 0 65.12 4.75 -19 -5 0 67.79 4.55 -19 5 0 63.05 4.69 19 5 0 65.4 4.84 -19 5 0 64.17 4.78 -19 5 0 63.6 4.55 19 5 0 63.72 4.79 19 5 0 65.4 5.06 -21 -5 0 17.48 1.4 21 -5 0 17.32 1.51 -21 -5 0 17.51 1.54 -21 -5 0 18.01 1.46 -21 5 0 11.5 1.36 21 5 0 12.8 1.5 21 5 0 10.95 1.36 -21 5 0 11.98 1.28 -21 5 0 12.06 1.24 -23 -5 0 28.43 2.22 -23 -5 0 31.69 2.43 -23 -5 0 31.06 2.39 23 -5 0 29.71 2.38 -23 -5 0 30.33 2.24 -23 5 0 24.16 2.29 -23 5 0 25.89 2.09 -23 5 0 23.83 2.11 23 5 0 23.25 2.32 23 5 0 22.86 2.3 -25 -5 0 14.3 1.64 -25 -5 0 13.07 1.64 -25 -5 0 13.27 1.57 25 -5 0 14.02 1.63 -25 -5 0 16.8 1.74 -25 5 0 20.49 1.58 25 5 0 18.31 1.78 -25 5 0 15.98 1.5 25 5 0 16.8 1.64 -25 5 0 18.57 1.75 -27 -5 0 22.35 2.2 27 -5 0 20.01 2.16 -27 -5 0 22.66 2.19 -27 -5 0 21.56 2.08 -27 -5 0 22.06 1.98 27 5 0 17.18 2.09 -27 5 0 20.89 2.07 27 5 0 21.29 2.14 -27 5 0 21.18 1.88 -27 5 0 20.15 2.07 -29 -5 0 31.24 2.54 -29 -5 0 28.2 2.39 -29 -5 0 29.16 2.43 -29 -5 0 28.5 2.52 29 -5 0 28.16 2.49 -29 5 0 22.92 2.19 29 5 0 23.8 2.42 -29 5 0 20.04 2.34 -29 5 0 19.52 2.36 29 5 0 21.33 2.42 -31 -5 0 5.7 1.33 -31 -5 0 4.38 1.18 -31 -5 0 5.17 1.21 -31 -5 0 5.06 1.2 -31 5 0 4.6 1.17 31 5 0 4.86 1.21 -31 5 0 4.03 1.14 -31 5 0 4.49 0.92 -33 -5 0 5.9 1.28 -33 -5 0 5.96 1.35 -33 -5 0 4.13 1.2 -33 -5 0 4.07 1.25 -33 5 0 4.8 1.23 -33 5 0 6.27 1 -33 5 0 5.79 1.24 33 5 0 5.01 1.18 -35 -5 0 2.39 1.28 -35 -5 0 1.9 1.13 -35 -5 0 1.99 1.15 -35 -5 0 1.55 1.21 -35 5 0 1.5 0.87 -35 5 0 -0.28 1.05 35 5 0 0.83 1.2 -35 5 0 1.41 1.1 -37 -5 0 1.45 1.1 -37 -5 0 0.67 1.28 -37 -5 0 0.06 1.09 -37 -5 0 1.27 1.17 37 5 0 1.16 1.27 -37 5 0 1.54 1.04 -37 5 0 2.4 0.87 -37 5 0 2.98 1.13 0 -6 0 343.95 23.93 0 -6 0 335.36 23.46 0 -6 0 323.54 20.45 0 -6 0 349.16 24.99 0 -6 0 331.69 23.97 0 -6 0 331.76 24.4 0 -6 0 331.12 24.98 0 -6 0 347.88 25.26 0 -6 0 325.41 21.33 0 -6 0 364.51 25.26 0 6 0 336.36 23.64 0 6 0 337.01 23.99 0 6 0 330.39 24.95 0 6 0 326.31 24.95 0 6 0 322.11 25.03 -2 -6 0 115.66 8.63 2 -6 0 117.53 7.36 2 -6 0 113.02 8.29 -2 -6 0 110.66 7.36 -2 -6 0 119.6 8.26 2 -6 0 113.9 7.08 -2 -6 0 118.85 8.73 2 -6 0 120.11 8.71 -2 -6 0 112.45 8.72 -2 -6 0 116.04 8.28 2 -6 0 120.64 8.71 2 -6 0 114.77 8.43 2 -6 0 120.06 8.61 2 -6 0 115.2 8.26 2 -6 0 116.07 8.1 -2 -6 0 112.5 8.63 2 -6 0 118.22 8.61 -2 -6 0 113.24 7.08 -2 -6 0 114.8 8.43 -2 -6 0 115.9 8.1 -2 6 0 114.25 8.62 2 6 0 114.95 8.14 -2 6 0 112.85 8.28 -2 6 0 109.33 8.6 -2 6 0 107.79 8.6 -2 6 0 113.79 8.13 2 6 0 112.95 8.63 2 6 0 119.11 8.62 2 6 0 113.81 8.29 2 6 0 116.72 8.61 -4 -6 0 106.63 7.55 -4 -6 0 107.8 7.83 4 -6 0 105.97 6.36 4 -6 0 107.87 7.41 4 -6 0 108.24 7.56 4 -6 0 110.16 7.71 -4 -6 0 109.62 7.39 4 -6 0 113.19 7.72 -4 -6 0 105.05 6.35 -4 -6 0 105.86 7.74 -4 -6 0 107.27 7.31 -4 -6 0 104.33 6.61 -4 -6 0 105.09 7.82 4 -6 0 104.92 7.79 4 -6 0 106.19 7.43 4 -6 0 109.27 6.59 -4 -6 0 110.99 7.42 -4 -6 0 108.17 7.26 -4 -6 0 109.96 7.74 -4 6 0 96.27 7.41 4 6 0 97.24 7.3 4 6 0 87.7 7.71 -4 6 0 90.16 7.69 4 6 0 94.45 7.43 -4 6 0 91.52 7.27 4 6 0 89.03 7.73 -4 6 0 97.98 7.72 4 6 0 96.79 7.72 6 -6 0 138.44 10.49 -6 -6 0 147.52 10.95 6 -6 0 138.85 10.68 -6 -6 0 142.44 10.33 -6 -6 0 141.85 10.27 6 -6 0 145.7 9.31 6 -6 0 142.17 10.48 -6 -6 0 144.43 10.49 6 -6 0 137.3 11.03 -6 -6 0 152.09 10.96 -6 -6 0 146.31 10.46 6 -6 0 149.51 10.91 -6 -6 0 142.8 9.35 6 -6 0 142.68 8.97 -6 -6 0 145.61 10.68 -6 -6 0 150.72 11.07 -6 -6 0 130.65 11.06 -6 -6 0 142.36 8.96 -6 6 0 154.24 11.03 -6 6 0 158.15 10.49 6 6 0 157.51 10.94 6 6 0 148.28 10.51 6 6 0 140.87 10.94 -6 6 0 145.67 10.31 6 6 0 158.42 10.97 -6 6 0 143.11 10.9 6 6 0 153.05 10.34 -6 6 0 152.96 10.91 -8 -6 0 65.74 4.02 -8 -6 0 61.72 4.88 -8 -6 0 64.08 4.79 8 -6 0 61.62 4.79 -8 -6 0 63.43 4.21 -8 -6 0 67.64 4.67 -8 -6 0 63.65 4.63 -8 -6 0 68.66 4.99 8 -6 0 66.62 4.92 8 -6 0 66.33 4.79 8 -6 0 65.11 4.87 -8 -6 0 72.86 4.9 8 -6 0 66.59 4.04 -8 -6 0 63.99 4.6 8 -6 0 63.1 4.71 -8 -6 0 66.26 4.93 -8 -6 0 68.48 4.7 -8 6 0 64.52 4.41 -8 6 0 63.1 4.86 8 6 0 64.45 4.98 8 6 0 62.99 4.71 8 6 0 67.56 4.68 8 6 0 63.23 4.62 -8 6 0 64.67 4.58 8 6 0 62.91 4.92 -8 6 0 60.85 4.86 8 6 0 61.31 4.91 -8 6 0 61.76 4.91 8 6 0 62.37 4.91 8 6 0 63.37 4.92 -10 -6 0 119.52 8.66 10 -6 0 121.12 9.04 10 -6 0 115.43 9.19 -10 -6 0 118.86 9.21 -10 -6 0 122.11 9.24 -10 -6 0 118.84 9.01 10 -6 0 117.92 8.86 10 -6 0 121.18 7.56 -10 -6 0 133.17 9.27 -10 -6 0 125.68 8.81 -10 -6 0 119.88 7.54 -10 -6 0 116.92 8.72 -10 -6 0 128.9 8.84 10 -6 0 116.87 9.01 -10 -6 0 119.72 7.9 10 6 0 120.38 9.26 -10 6 0 132.74 9.19 -10 6 0 118.52 9.18 10 6 0 126.31 9.26 -10 6 0 121.6 8.68 10 6 0 126.83 8.87 10 6 0 133.41 8.73 -10 6 0 123.97 8.29 10 6 0 131.38 8.85 12 -6 0 108.86 7.38 -12 -6 0 111.92 8.52 -12 -6 0 126.47 9.07 -12 -6 0 113.97 9.03 12 -6 0 109.76 8.8 -12 -6 0 114.37 7.36 -12 -6 0 116.26 8.63 12 -6 0 115.37 8.84 -12 -6 0 116.62 8.6 -12 -6 0 112.4 8.46 -12 -6 0 110.95 7.72 12 -6 0 112.72 8.66 -12 -6 0 112.38 8.81 12 6 0 130.84 8.52 12 6 0 133.61 8.66 12 6 0 119.42 9.05 -12 6 0 127.25 8.48 12 6 0 139.75 9.07 12 6 0 124.01 8.66 -12 6 0 126.34 8.98 -12 6 0 126.74 8.2 -12 6 0 129.63 8.09 -14 -6 0 42.57 3.06 14 -6 0 42.03 3.15 -14 -6 0 42.55 3.04 -14 -6 0 41.45 3.03 -14 -6 0 40.5 3.16 14 -6 0 38.93 3.17 -14 -6 0 38.81 3 -14 -6 0 43.1 3.23 14 -6 0 39.94 2.64 14 -6 0 36.86 3.08 -14 -6 0 40.89 3.28 -14 -6 0 40.96 2.8 14 6 0 41.47 3.09 -14 6 0 42.89 3.18 -14 6 0 40.48 2.91 14 6 0 36.64 3.21 14 6 0 39.68 3.01 14 6 0 43.08 3.09 -14 6 0 45.53 2.86 -14 6 0 41.29 2.96 16 -6 0 34.04 2.2 -16 -6 0 32.35 2.66 -16 -6 0 32.76 2.51 16 -6 0 31.81 2.64 -16 -6 0 30.95 2.57 16 -6 0 30.03 2.67 -16 -6 0 32.43 2.72 16 6 0 32.98 2.74 -16 6 0 35.33 2.46 16 6 0 34.67 2.56 16 6 0 37.5 2.53 -16 6 0 33.02 2.45 16 6 0 35.93 2.58 18 -6 0 7.68 1.02 -18 -6 0 7.23 0.98 -18 -6 0 7.87 0.94 18 -6 0 7.23 0.95 -18 -6 0 8 0.97 -18 -6 0 8.2 1.06 -18 6 0 12.19 1.11 18 6 0 11.61 1.13 18 6 0 11.87 1.25 -18 6 0 12.44 1.05 18 6 0 11.22 1.06 -20 -6 0 0.39 0.72 -20 -6 0 0.51 0.73 -20 -6 0 0.81 0.74 -20 -6 0 1.12 0.63 20 -6 0 1.2 0.78 20 -6 0 -0.03 0.6 -20 6 0 0.36 0.41 -20 6 0 0.29 0.6 -20 6 0 0.44 0.66 20 6 0 -0.52 0.67 20 6 0 0.86 0.72 20 6 0 0.24 0.56 -22 -6 0 4.43 0.89 -22 -6 0 4.34 0.95 22 -6 0 4.93 0.93 -22 -6 0 5.29 0.96 -22 -6 0 5.33 0.98 -22 6 0 3.8 0.63 22 6 0 4.58 0.78 22 6 0 3.48 0.88 -22 6 0 5.35 0.79 22 6 0 3.58 0.93 -22 6 0 4.39 0.84 -24 -6 0 1.39 0.94 -24 -6 0 0.52 0.9 24 -6 0 2.04 0.91 -24 -6 0 0.75 0.86 -24 -6 0 1.07 0.78 -24 6 0 1.94 0.73 -24 6 0 1.74 0.89 24 6 0 2.22 0.88 -24 6 0 1.73 0.57 24 6 0 1.51 0.86 -26 -6 0 8.78 1.22 -26 -6 0 8.19 1.27 26 -6 0 9.47 1.29 -26 -6 0 7.51 1.22 -26 -6 0 7.5 1.13 -26 6 0 7.26 0.92 26 6 0 5.76 1.16 -26 6 0 7.55 1.19 -26 6 0 8.33 1.04 26 6 0 8.59 1.23 -28 -6 0 3.15 1.09 -28 -6 0 1.72 0.97 -28 -6 0 3.76 1.16 -28 -6 0 3.51 1.16 28 6 0 5.02 1.13 -28 6 0 4.11 1.09 -28 6 0 4.51 0.81 28 6 0 5.02 1.16 -28 6 0 4.18 1.12 -30 -6 0 1.43 1.09 -30 -6 0 0.69 1.15 -30 -6 0 2.26 1.22 -30 -6 0 1.02 1.11 30 6 0 3.18 1.15 -30 6 0 3.25 0.82 30 6 0 2.64 1.12 -30 6 0 2.97 1.07 -30 6 0 1.83 1.12 -32 -6 0 0.46 1.26 -32 -6 0 0.23 1.09 -32 -6 0 0.22 1.15 -32 -6 0 0.37 1.09 32 6 0 0.87 1.17 -32 6 0 0.27 1.07 -32 6 0 0.26 0.81 -32 6 0 0.04 0.99 -34 -6 0 5.26 1.49 -34 -6 0 7.33 1.32 -34 -6 0 4.78 1.29 -34 -6 0 5.42 1.37 -34 6 0 6.03 1.25 -34 6 0 7.41 1.29 -34 6 0 6.15 1.03 34 6 0 6.87 1.4 -36 -6 0 8.54 1.51 -36 -6 0 7.98 1.31 -36 -6 0 6.64 1.35 -36 -6 0 5.89 1.3 36 6 0 6.97 1.46 -36 6 0 4.41 1.2 -36 6 0 5.22 1.03 -36 6 0 6.38 1.28 1 -7 0 1.52 0.34 -1 -7 0 1.77 0.4 -1 -7 0 1.01 0.31 -1 -7 0 1.72 0.4 -1 -7 0 1.56 0.38 1 -7 0 1.75 0.35 -1 -7 0 1.76 0.44 -1 -7 0 1.79 0.36 1 -7 0 1.04 0.38 1 -7 0 1.51 0.32 1 -7 0 1.77 0.34 1 -7 0 1.55 0.45 -1 -7 0 2.25 0.39 1 -7 0 1.92 0.4 1 -7 0 1.54 0.33 1 -7 0 1.38 0.34 -1 -7 0 1.31 0.34 -1 -7 0 1.26 0.34 -1 -7 0 1.57 0.37 1 -7 0 1.52 0.41 1 7 0 1.08 0.35 -1 7 0 1.25 0.33 1 7 0 1.37 0.41 -1 7 0 1.08 0.33 1 7 0 1.74 0.36 1 7 0 2.22 0.37 -1 7 0 1.31 0.25 -1 7 0 1.32 0.43 1 7 0 1.38 0.26 -1 7 0 2.33 0.35 3 -7 0 7.67 0.84 -3 -7 0 8.97 0.86 -3 -7 0 9.09 0.79 -3 -7 0 7.61 0.81 -3 -7 0 8.58 0.92 3 -7 0 8.26 0.84 -3 -7 0 7.82 0.93 -3 -7 0 8.78 0.91 -3 -7 0 9.29 0.85 3 -7 0 7.66 0.88 -3 -7 0 9.31 0.82 3 -7 0 7.32 0.87 -3 -7 0 8.51 0.93 3 -7 0 7.56 0.84 3 -7 0 8.63 0.75 3 -7 0 7.76 0.85 3 -7 0 8.91 0.87 3 7 0 11.73 0.91 -3 7 0 11.99 0.88 -3 7 0 11.17 0.89 -3 7 0 12.2 0.91 -3 7 0 10.49 0.75 -3 7 0 11.36 0.85 5 -7 0 7.22 0.78 5 -7 0 6.86 0.82 -5 -7 0 7.87 0.88 -5 -7 0 7.5 0.76 -5 -7 0 7.74 0.79 -5 -7 0 7.89 0.8 5 -7 0 6.7 0.79 -5 -7 0 6.9 0.88 5 -7 0 7.72 0.71 -5 -7 0 6.64 0.77 -5 -7 0 7.77 0.77 -5 -7 0 8.1 0.91 5 -7 0 7.51 0.68 5 -7 0 8.11 0.79 -5 -7 0 7.11 0.78 5 -7 0 7.57 0.82 -5 7 0 9.27 0.81 -5 7 0 9.49 0.8 5 7 0 9.26 0.74 5 7 0 9 0.9 5 7 0 9.56 0.88 5 7 0 8.79 0.83 -5 7 0 8.17 0.66 5 7 0 9.4 0.87 -7 -7 0 57.43 3.94 7 -7 0 54.75 3.99 -7 -7 0 52.97 4.23 -7 -7 0 55.54 3.92 7 -7 0 58.62 3.52 7 -7 0 55.81 4.07 7 -7 0 54.42 4 -7 -7 0 59.16 3.96 7 -7 0 59.2 3.45 -7 -7 0 59.06 4 -7 -7 0 56.55 3.58 -7 -7 0 57.76 3.44 -7 -7 0 55.51 4.06 -7 7 0 50.42 3.97 -7 7 0 49.08 3.73 7 7 0 53.41 4.17 -7 7 0 49.12 3.87 7 7 0 52.45 4.17 -7 7 0 53 4.12 7 7 0 49.22 3.91 7 7 0 50.44 4.02 9 -7 0 35.43 2.76 -9 -7 0 35.73 2.81 -9 -7 0 36.34 2.94 -9 -7 0 38.79 2.85 -9 -7 0 38.02 2.74 -9 -7 0 39.11 2.36 9 -7 0 37.62 2.39 -9 -7 0 36.46 2.48 -9 -7 0 37.34 2.73 -9 -7 0 37.67 2.7 -9 -7 0 38.11 2.69 9 -7 0 36.56 2.8 9 7 0 35.11 2.68 9 7 0 37.22 2.88 -9 7 0 35.42 2.58 9 7 0 34.38 2.76 9 7 0 36.58 2.72 -9 7 0 35.33 2.82 -9 7 0 32.97 2.62 11 -7 0 43.73 2.82 -11 -7 0 43.1 3.33 11 -7 0 44.41 3.31 -11 -7 0 46.01 3.5 -11 -7 0 44.39 2.95 -11 -7 0 45.08 3.25 -11 -7 0 43.4 3.24 -11 -7 0 42.51 3.21 11 -7 0 41.62 3.28 -11 -7 0 45.79 2.79 11 -7 0 40.96 3.32 -11 -7 0 44.91 3.39 -11 -7 0 46.02 3.21 11 7 0 41.32 3.19 11 7 0 47.13 3.24 -11 7 0 43.05 3.04 11 7 0 41.9 3.42 11 7 0 41.59 3.26 -11 7 0 41.94 3.13 13 -7 0 39.9 3.18 -13 -7 0 42.54 3.03 -13 -7 0 39.3 3.03 -13 -7 0 37.28 3.12 13 -7 0 40.67 2.66 13 -7 0 36.79 3.12 -13 -7 0 41.9 3.07 -13 -7 0 41.4 3.21 -13 -7 0 38.35 3.01 13 -7 0 42.49 3.13 13 7 0 41.13 3.09 13 7 0 41.43 3.25 -13 7 0 43.72 2.88 -13 7 0 40.89 2.92 13 7 0 42.66 3.07 13 7 0 41.32 3.02 -13 7 0 40.92 2.95 -15 -7 0 14.49 1.4 15 -7 0 13.25 1.53 15 -7 0 14.85 1.24 15 -7 0 14.72 1.43 -15 -7 0 14.28 1.5 -15 -7 0 16.11 1.49 15 -7 0 13.38 1.51 -15 -7 0 15.24 1.39 -15 7 0 17.66 1.39 15 7 0 17.26 1.41 15 7 0 17.79 1.56 15 7 0 15.61 1.45 15 7 0 16.45 1.38 -15 7 0 15.22 1.24 -15 7 0 16.28 1.29 17 -7 0 12.08 1.31 -17 -7 0 11.84 1.23 -17 -7 0 12.49 1.37 -17 -7 0 11.91 1.24 -17 -7 0 12.7 1.38 17 -7 0 12.74 1.27 -17 7 0 11.2 1.22 17 7 0 12.02 1.25 -17 7 0 11.36 1.06 17 7 0 12.66 1.41 17 7 0 11.47 1.28 19 -7 0 37.8 3.26 -19 -7 0 41.39 3.36 -19 -7 0 41.43 3.25 -19 -7 0 43.87 3.18 19 -7 0 42.14 3.27 -19 -7 0 44.36 3.21 19 7 0 38.97 3.38 -19 7 0 39.96 3.04 19 7 0 41.05 3.15 19 7 0 42.91 3.21 -19 7 0 40.86 3.16 -19 7 0 39.64 3.02 -21 -7 0 36.54 2.98 -21 -7 0 36.08 2.93 21 -7 0 34.69 2.83 -21 -7 0 33.08 2.77 21 -7 0 33.56 2.95 -21 -7 0 34.12 2.73 21 7 0 36.2 2.83 -21 7 0 35.15 2.78 21 7 0 36.03 2.78 -21 7 0 36.48 2.66 21 7 0 32.04 2.99 -21 7 0 33.8 2.64 -23 -7 0 17.35 1.94 -23 -7 0 16.36 1.75 23 -7 0 16.87 1.89 -23 -7 0 16.83 1.98 -23 -7 0 17.58 1.91 23 7 0 19.85 1.8 -23 7 0 19.16 1.89 23 7 0 20.25 1.86 -23 7 0 19.69 1.69 23 7 0 16.96 1.97 -23 7 0 19.41 1.63 -25 -7 0 14.25 1.64 -25 -7 0 11.95 1.53 -25 -7 0 14.59 1.59 -25 -7 0 13.63 1.6 25 7 0 13.98 1.53 -25 7 0 13.66 1.43 -25 7 0 14.41 1.59 25 7 0 15.07 1.66 -25 7 0 12.95 1.35 -27 -7 0 3.26 1.18 -27 -7 0 3.48 1.12 -27 -7 0 2.36 1.14 -27 -7 0 3.7 1.21 27 7 0 4.67 1.21 -27 7 0 5.17 1.12 -27 7 0 6.12 0.83 27 7 0 5.19 1.05 -29 -7 0 12.85 1.6 -29 -7 0 9.15 1.45 -29 -7 0 10.67 1.48 -29 -7 0 12.63 1.6 29 7 0 10.56 1.5 -29 7 0 7.94 1.39 29 7 0 11.43 1.48 -29 7 0 10.04 1.47 -29 7 0 12.13 1.21 -31 -7 0 3.22 1.16 -31 -7 0 3.36 1.26 -31 -7 0 2.58 1.18 -31 -7 0 2.9 1.33 -31 7 0 3.59 0.89 31 7 0 4.06 1.22 -31 7 0 4.46 1.15 31 7 0 3.39 1.16 -31 7 0 3.66 1.2 -33 -7 0 0.49 1.11 -33 -7 0 1.06 1.16 -33 -7 0 0.77 1.13 -33 -7 0 0.43 1.26 -33 7 0 1.84 0.83 -33 7 0 1.05 1.08 33 7 0 0.5 1.15 -33 7 0 0.28 1.15 -35 -7 0 0.64 1.15 -35 -7 0 2.52 1.16 -35 -7 0 0.87 1.29 -35 -7 0 0.08 1.06 -35 7 0 0.61 1.07 -35 7 0 -0.12 0.81 -35 7 0 1.17 1.11 35 7 0 0.77 1.21 0 -8 0 175.64 11.96 0 -8 0 183.97 10.06 0 -8 0 173.48 11.75 0 -8 0 174.73 11.49 0 -8 0 180.39 10.45 0 -8 0 175.17 11.71 0 8 0 149.91 11.54 0 8 0 141.69 12.22 0 8 0 150.76 11.74 0 8 0 146.57 12.2 0 8 0 147.9 12.2 -2 -8 0 153.33 8.8 -2 -8 0 149.71 10.47 2 -8 0 158.9 9.14 -2 -8 0 154.93 10.29 -2 -8 0 150.35 10.06 -2 -8 0 156.44 10.25 2 -8 0 153.67 10.26 2 -8 0 155.41 10.47 2 -8 0 157.75 8.81 2 -8 0 150.25 10.3 -2 -8 0 151.88 9.15 -2 8 0 133.68 10.69 -2 8 0 130.2 10.09 2 8 0 124.36 10.1 2 8 0 124.59 10.68 -2 8 0 128.93 10.67 2 8 0 134.29 10.71 2 8 0 127.42 10.28 -2 8 0 133.9 10.68 -2 8 0 130.46 10.28 4 -8 0 91.5 6.49 4 -8 0 93.02 5.76 4 -8 0 87.91 6.51 4 -8 0 90.84 5.58 -4 -8 0 87.3 6.35 4 -8 0 92.64 6.62 -4 -8 0 90.65 5.79 -4 -8 0 91.54 6.62 -4 -8 0 94.98 5.58 -4 -8 0 93.3 6.47 -4 -8 0 90.27 6.5 4 8 0 84.74 6.51 -4 8 0 84.9 6.35 4 8 0 82.77 6.37 -4 8 0 88.04 6.73 4 8 0 84.58 6.76 -4 8 0 93.98 6.74 -4 8 0 88.9 6.5 6 -8 0 66.46 4.28 6 -8 0 63.48 5.05 -6 -8 0 65.31 4.85 -6 -8 0 65.02 4.95 -6 -8 0 66.96 5.05 6 -8 0 61.72 4.98 6 -8 0 64.08 4.94 -6 -8 0 67.32 4.27 -6 -8 0 62.15 4.42 -6 -8 0 64.6 4.9 -6 -8 0 66 4.93 6 8 0 68.65 5.18 -6 8 0 74.28 4.83 6 8 0 74 4.88 6 8 0 72.47 5.01 -6 8 0 77.17 4.97 -6 8 0 71.98 4.68 8 -8 0 63.96 4.06 -8 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1.13 3 9 0 10.05 1.11 -3 9 0 9.35 0.95 -5 -9 0 8.12 0.94 5 -9 0 7.7 0.94 -5 -9 0 7.67 0.81 5 -9 0 9 1.03 -5 -9 0 8.93 0.96 5 -9 0 9.25 1.05 -5 -9 0 7.66 0.93 -5 -9 0 8.88 0.95 -5 9 0 10.07 0.95 5 9 0 8.73 0.92 5 9 0 10.04 1.06 -5 9 0 9.74 1.01 -5 9 0 8.22 0.81 5 9 0 9.23 1.02 -7 -9 0 3.67 0.57 7 -9 0 2.73 0.73 -7 -9 0 2.67 0.6 7 -9 0 2.09 0.62 -7 -9 0 3.12 0.64 -7 -9 0 3.81 0.72 7 9 0 1.67 0.6 -7 9 0 1.93 0.64 7 9 0 1.04 0.69 -7 9 0 1.47 0.36 7 9 0 1.4 0.46 -7 9 0 1.69 0.54 9 -9 0 27.04 2.14 -9 -9 0 26.48 2.12 -9 -9 0 26.59 2.04 -9 -9 0 30.23 2.05 -9 -9 0 27.98 2.12 9 -9 0 28.25 2.13 -9 -9 0 29.35 2.09 -9 9 0 22.78 1.91 9 9 0 23.39 2.17 9 9 0 22.13 2 -9 9 0 22.07 1.95 9 9 0 21.14 2.15 -11 -9 0 10.72 1.14 11 -9 0 9.37 1.15 -11 -9 0 9.92 1.15 -11 -9 0 10.12 1.1 11 -9 0 9.33 1.15 -11 -9 0 9.62 1.07 -11 9 0 10.14 1.02 11 9 0 10.54 1.12 -11 9 0 11.02 0.93 11 9 0 10.01 1.13 11 9 0 8.94 1.09 13 -9 0 9.86 1.25 -13 -9 0 12.27 1.31 -13 -9 0 13.04 1.38 13 -9 0 11.33 1.31 -13 -9 0 11.75 1.27 -13 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3.59 -4 -10 0 51.48 3.73 4 -10 0 51.09 3.59 4 -10 0 48.51 3.68 -4 -10 0 52.74 3.66 -4 -10 0 48.76 3.58 4 -10 0 49.31 3.72 -4 10 0 43.64 3.59 -4 10 0 44.47 3.4 -4 10 0 44.78 3.47 4 10 0 45.48 3.74 4 10 0 43.68 3.5 4 10 0 45.28 3.64 6 -10 0 20.97 1.82 -6 -10 0 23.71 1.73 6 -10 0 19.47 1.8 -6 -10 0 20.47 1.74 -6 -10 0 22.92 1.83 -6 -10 0 21.3 1.89 -6 10 0 19.91 1.75 -6 10 0 20.27 1.75 6 10 0 19.17 1.82 -6 10 0 19.22 1.6 6 10 0 17.78 1.68 6 10 0 18.02 1.89 -8 -10 0 14.37 1.47 -8 -10 0 12.92 1.41 -8 -10 0 15.21 1.58 8 -10 0 14.41 1.49 -8 -10 0 16.7 1.37 8 -10 0 12.81 1.45 -8 10 0 14.53 1.23 8 10 0 14.41 1.38 8 10 0 15.5 1.53 8 10 0 13.14 1.49 -8 10 0 14.65 1.4 10 -10 0 30.37 2.47 -10 -10 0 32.84 2.47 -10 -10 0 31.9 2.43 -10 -10 0 29.84 2.53 10 -10 0 29.06 2.53 -10 10 0 28.47 2.28 10 10 0 27.94 2.46 10 10 0 28.17 2.54 10 10 0 29.52 2.35 -10 10 0 28.19 2.23 12 -10 0 10.12 1.33 12 -10 0 10.5 1.35 -12 -10 0 11.57 1.27 -12 -10 0 11.73 1.33 -12 -10 0 13.52 1.26 -12 -10 0 11.93 1.3 12 10 0 12.45 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3.73 0.8 -5 -11 0 2.73 0.86 -5 -11 0 1.81 0.74 5 -11 0 2.61 0.89 5 11 0 2.73 0.72 5 11 0 3.16 0.86 -5 11 0 2.25 0.74 5 11 0 2.56 0.62 -5 11 0 2.83 0.85 -5 11 0 2.03 0.53 -7 -11 0 11.04 1.13 -7 -11 0 11.95 1.19 7 -11 0 11.58 1.25 7 -11 0 9.75 1.26 -7 -11 0 9.4 1.2 7 11 0 9.05 1.14 -7 11 0 9.77 1.19 -7 11 0 8.04 0.88 7 11 0 8.23 1.19 7 11 0 7.83 0.98 -7 11 0 8.2 1.09 9 -11 0 23.64 2.09 -9 -11 0 23.86 2.07 -9 -11 0 26.73 2.07 9 -11 0 22.62 2.17 -9 -11 0 23.12 2.15 9 11 0 21.28 1.96 -9 11 0 20.67 1.8 -9 11 0 22.46 1.94 9 11 0 21.56 2.11 9 11 0 19.98 2.16 11 -11 0 20.49 2.17 -11 -11 0 22.67 2.15 11 -11 0 21.1 2.07 -11 -11 0 21.06 1.96 -11 -11 0 20.31 2.07 -11 11 0 22.69 1.78 -11 11 0 21.34 1.89 11 11 0 20.65 2.13 11 11 0 23.56 2.18 11 11 0 23.31 1.95 -13 -11 0 2.25 0.88 -13 -11 0 1.59 1 13 -11 0 2.35 1.06 13 -11 0 2.69 1.09 -13 11 0 4.11 0.61 13 11 0 3.28 0.77 -13 11 0 5.03 0.89 13 11 0 3.17 0.89 13 11 0 3.24 0.99 13 11 0 2.9 0.96 -13 11 0 5 1 -15 -11 0 3.07 0.98 15 -11 0 3.12 1.15 -15 -11 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39.99 2.97 -10 -8 -4 43.46 3.12 10 8 4 35.46 3 -10 8 -4 37.02 2.86 10 8 4 34.52 3.13 -10 8 -4 37.96 2.91 10 8 4 40.2 2.97 10 8 4 36.3 2.9 -10 8 -4 37.83 2.83 12 -8 4 37.58 2.99 -12 -8 -4 35.76 2.87 -12 -8 -4 41.13 2.95 -12 -8 -4 36.64 2.79 -12 -8 -4 37.92 3.01 -12 8 -4 36.21 2.8 12 8 4 37.02 3.04 -12 8 -4 36 2.77 -12 8 -4 38.54 2.73 12 8 4 35.74 2.9 12 8 4 36.17 2.81 12 8 4 41.43 2.89 14 -8 4 47.17 3.64 -14 -8 -4 53.14 3.58 14 -8 4 52.84 3.65 -14 -8 -4 49.27 3.67 -14 -8 -4 47.51 3.5 -14 -8 -4 49.09 3.44 14 8 4 44.15 3.52 -14 8 -4 43.93 3.43 14 8 4 43.83 3.58 14 8 4 41.88 3.44 -14 8 -4 46 3.31 -14 8 -4 44.48 3.41 14 8 4 40.43 3.7 16 -8 4 19.06 1.68 -16 -8 -4 15.34 1.8 -16 -8 -4 17.85 1.63 -16 -8 -4 19.02 1.69 16 -8 4 18.68 1.66 -16 -8 -4 19.02 1.59 16 8 4 16.44 1.62 -16 8 -4 15.96 1.49 16 8 4 17.05 1.75 -16 8 -4 16.52 1.49 16 8 4 14.87 1.54 -16 8 -4 15.43 1.56 16 8 4 14.88 1.68 -18 -8 -4 23.54 2.3 18 -8 4 23.34 2.37 18 -8 4 23.36 2.28 -18 -8 -4 24.59 2.17 -18 -8 -4 22.01 2.27 -18 -8 -4 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10.49 -1 3 -9 137.22 10.93 -1 3 -9 131.45 11.07 1 3 9 137.18 10.9 -1 3 -9 134.69 10.92 -1 3 -9 131.38 10.95 3 -3 9 119.05 8.3 -3 -3 -9 110.85 8.21 3 -3 9 114.71 7.82 -3 -3 -9 109.74 8.36 -3 -3 -9 117.95 8.28 -3 -3 -9 109.67 7.94 3 -3 9 115.02 8.12 3 -3 9 115.4 7.04 -3 -3 -9 113.81 8.06 -3 -3 -9 111.25 7.52 -3 -3 -9 110.71 7.09 3 -3 9 115.85 7.92 3 -3 9 116.88 8.32 -3 -3 -9 114.64 7.79 -3 -3 -9 113.75 8.2 3 3 9 102.91 7.79 -3 3 -9 104.58 7.94 3 3 9 96.63 8.35 3 3 9 101.54 8.26 -3 3 -9 100.12 8.3 3 3 9 106.74 8.12 3 3 9 107.9 8.27 -3 3 -9 104.05 7.51 -3 3 -9 110.52 8.4 -5 -3 -9 143.53 9.36 5 -3 9 135.76 10.97 5 -3 9 146.57 10.74 -5 -3 -9 141.81 9.94 -5 -3 -9 139.78 10.5 5 -3 9 136.02 10.96 -5 -3 -9 145.54 10.66 -5 -3 -9 145.21 10.89 5 -3 9 152.6 10.47 5 -3 9 148.71 10.47 -5 -3 -9 152.02 10.31 5 3 9 146.83 10.51 -5 3 -9 156.07 11.12 -5 3 -9 150.26 10.31 -5 3 -9 147.48 10.5 -5 3 -9 144.46 10.98 5 3 9 149.19 10.74 5 3 9 147.43 10.33 5 3 9 151.18 10.94 -5 3 -9 145.49 9.95 5 3 9 142.37 10.95 7 -3 9 151.59 10.45 7 -3 9 142.31 10.72 -7 -3 -9 139.1 10.48 -7 -3 -9 145.51 10.29 -7 -3 -9 149.58 10.88 7 -3 9 148.02 10.44 -7 -3 -9 149 10.65 -7 -3 -9 147.92 9.34 7 -3 9 136.76 10.93 -7 -3 -9 139.23 9.92 7 -3 9 146.94 10.96 7 3 9 142.4 10.71 -7 3 -9 152.72 10.47 -7 3 -9 151.04 10.29 7 3 9 143.63 10.48 7 3 9 136.53 10.93 -7 3 -9 144.93 9.93 7 3 9 143.78 10.3 7 3 9 155.94 10.94 -7 3 -9 146.91 10.96 9 -3 9 149.58 10.28 -9 -3 -9 146.27 10.73 -9 -3 -9 144.59 10.49 -9 -3 -9 142.64 9.78 -9 -3 -9 147.11 10.14 -9 -3 -9 150.65 9.2 9 -3 9 146.11 10.56 9 -3 9 138.48 10.77 -9 -3 -9 138.28 10.32 9 -3 9 152.9 10.29 -9 3 -9 137.99 9.78 9 3 9 142.87 10.77 -9 3 -9 140.5 10.29 9 3 9 137.58 10.15 9 3 9 135.59 10.32 -9 3 -9 142.19 10.14 9 3 9 143.33 10.55 -11 -3 -9 51.3 3.19 -11 -3 -9 49.19 3.59 11 -3 9 46.86 3.62 -11 -3 -9 47.87 3.55 11 -3 9 50.18 3.51 -11 -3 -9 47.71 3.37 11 -3 9 51.93 3.51 -11 -3 -9 49.72 3.47 11 -3 9 52.99 3.7 11 3 9 43.02 3.69 11 3 9 43.99 3.61 -11 3 -9 42.65 3.35 11 3 9 41.55 3.53 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35.07 2.76 22 4 -9 36.16 2.81 22 4 -9 35.94 2.78 -22 4 9 34.42 2.59 -20 -4 9 6.75 1.02 -20 -4 9 7.32 1.03 -20 -4 9 7.46 0.98 -20 -4 9 8.79 0.85 20 4 -9 7.29 1.02 -20 4 9 6.31 0.9 -20 4 9 6.38 0.74 20 4 -9 6.2 0.91 -18 -4 9 55.73 4.77 18 -4 -9 61.7 4.6 -18 -4 9 56.77 4.45 -18 -4 9 60.25 4.44 -18 -4 9 57.52 4.56 18 4 -9 64.84 4.53 -18 4 9 64.22 4.35 -18 4 9 65.51 4.45 -16 -4 9 59.81 5.04 16 -4 -9 67.62 4.87 -16 -4 9 64.43 4.72 -16 -4 9 65.71 4.7 -16 -4 9 65.27 4.83 16 4 -9 64.09 4.82 -16 4 9 65.89 4.7 -16 4 9 65.12 4.62 16 4 -9 67.84 5.03 -14 -4 9 25.7 2.07 -14 -4 9 23.67 2.13 -14 -4 9 24.24 2.05 -14 -4 9 23.52 2.2 14 -4 -9 25.03 2.11 -14 4 9 30.56 1.9 14 4 -9 30.6 2.14 -12 -4 9 96.48 6.71 -12 -4 9 92.54 6.87 -12 -4 9 86.62 7.18 -12 -4 9 93.49 6.76 12 -4 -9 96.72 6.84 12 -4 -9 97.15 6.97 12 4 -9 99.42 6.89 10 -4 -9 30.28 2.32 -10 -4 9 29.97 2.25 10 -4 -9 31.05 2.27 -10 -4 9 29.1 2.31 -10 -4 9 29.01 2.44 -10 -4 9 29.95 2.24 -10 -4 9 31.15 2.49 8 -4 -9 33.64 2.56 -8 -4 9 32.94 2.55 -8 -4 9 31.31 2.68 8 -4 -9 34.27 2.53 -8 -4 9 37.23 2.73 -8 -4 9 33.15 2.48 -8 -4 9 33.69 2.74 -8 -4 9 34.13 2.47 6 -4 -9 43.86 3.28 -6 -4 9 44 3.31 -6 -4 9 44.52 3.2 -6 -4 9 44.78 3.46 -6 -4 9 42.63 3.52 -6 -4 9 42.45 3.22 -6 -4 9 43.71 3.49 6 -4 -9 43.63 3.33 -6 -4 9 45.92 3.35 6 4 -9 50.14 3.33 4 -4 -9 42.61 3.04 -4 -4 9 38.16 3.15 -4 -4 9 39.72 3.06 -4 -4 9 39.31 2.91 4 -4 -9 41.17 3.01 -4 -4 9 42.73 3.21 -4 -4 9 41.61 3.22 4 -4 -9 42.53 3.1 -4 -4 9 40.25 2.95 -4 -4 9 37.78 3 2 -4 -9 37.48 2.91 -2 -4 9 37.43 2.9 2 -4 -9 36.99 2.93 -2 -4 9 40.37 2.81 -2 -4 9 36.78 3.05 2 -4 -9 37.2 2.99 -2 -4 9 39.33 2.84 -2 -4 9 40.88 3.09 -2 -4 9 39.08 2.96 -2 4 9 39.93 2.97 2 4 -9 41.24 3.09 -2 4 9 40.5 2.97 -2 4 9 40.13 2.77 -2 4 9 39.95 2.98 2 4 -9 39.99 2.73 2 4 -9 37.65 2.92 0 -4 -9 5.58 0.57 0 -4 -9 5.46 0.52 0 -4 9 6.12 0.7 0 -4 -9 5.79 0.57 0 -4 -9 5.12 0.56 0 -4 -9 5.28 0.57 0 -4 9 5.38 0.62 0 -4 9 3.95 0.61 0 -4 9 5.74 0.65 0 -4 9 5.28 0.57 0 -4 -9 4.97 0.6 0 4 9 4.67 0.57 0 4 9 5.05 0.57 0 4 -9 4.44 0.51 0 4 -9 5.41 0.68 0 4 -9 4.39 0.59 0 4 9 4.8 0.53 0 4 9 4.59 0.45 0 4 9 4.69 0.55 -2 -4 -9 6.07 0.62 2 -4 9 6.7 0.78 -2 -4 -9 7.02 0.66 -2 -4 -9 7.84 0.72 -2 -4 -9 7.03 0.73 2 -4 9 6.4 0.74 -2 -4 -9 7.44 0.71 2 -4 9 7.09 0.74 -2 -4 -9 6.46 0.68 2 -4 9 6.11 0.69 2 4 9 6.51 0.69 2 4 9 7.29 0.75 2 4 9 6.64 0.74 -2 4 -9 5.29 0.75 -2 4 -9 5.81 0.67 -2 4 -9 5.69 0.63 2 4 9 6.21 0.57 2 4 9 6.01 0.69 -4 -4 -9 19.83 1.43 -4 -4 -9 18.61 1.44 -4 -4 -9 18.59 1.5 -4 -4 -9 18.97 1.5 4 -4 9 21.38 1.5 -4 -4 -9 18.36 1.38 4 -4 9 20.82 1.53 4 -4 9 21.89 1.66 4 -4 9 19.65 1.58 -4 4 -9 17.89 1.4 -4 4 -9 19.03 1.51 4 4 9 16.13 1.38 4 4 9 15.72 1.5 4 4 9 16.98 1.55 4 4 9 16.17 1.48 4 4 9 17.61 1.51 -6 -4 -9 30.91 2.36 6 -4 9 29.1 2.44 6 -4 9 29.87 2.32 6 -4 9 31.74 2.38 -6 -4 -9 31.44 2.13 -6 -4 -9 30.1 2.21 -6 -4 -9 30.36 2.26 -6 -4 -9 29.28 2.34 6 4 9 30.73 2.45 -6 4 -9 29.82 2.2 6 4 9 29.76 2.41 6 4 9 29.94 2.35 -6 4 -9 32.11 2.32 6 4 9 30.27 2.37 -6 4 -9 33.06 2.26 6 4 9 29.68 2.23 -8 -4 -9 33.96 2.41 -8 -4 -9 33.57 2.24 -8 -4 -9 31.09 2.48 -8 -4 -9 33.16 2.48 8 -4 9 30.97 2.5 -8 -4 -9 32.34 2.35 8 -4 9 31.27 2.56 8 -4 9 31.77 2.42 -8 4 -9 32.13 2.34 8 4 9 30.35 2.49 8 4 9 31.99 2.38 -8 4 -9 34.62 2.44 8 4 9 30.66 2.56 -8 4 -9 32.31 2.4 8 4 9 33.5 2.49 -10 -4 -9 29.62 2.18 10 -4 9 29.47 2.36 -10 -4 -9 33.61 2.08 10 -4 9 30.07 2.35 -10 -4 -9 30.23 2.33 -10 -4 -9 30.19 2.34 10 -4 9 32.92 2.27 -10 -4 -9 30.88 2.24 -10 4 -9 29.5 2.24 -10 4 -9 28.06 2.17 10 4 9 25.38 2.38 10 4 9 24.9 2.27 10 4 9 27.45 2.31 12 -4 9 35.65 2.79 -12 -4 -9 36.24 2.77 -12 -4 -9 34.35 2.87 -12 -4 -9 36.84 2.55 12 -4 9 33.98 2.87 12 -4 9 35.12 2.95 -12 -4 -9 35.31 2.87 -12 -4 -9 34.25 2.69 12 4 9 39.65 2.84 12 4 9 40.22 2.87 -12 4 -9 39.94 2.77 12 4 9 39.21 2.74 12 4 9 36.09 2.96 -12 4 -9 38.86 2.74 -14 -4 -9 36.58 2.7 -14 -4 -9 34.12 2.76 14 -4 9 39.52 2.87 14 -4 9 36.24 2.84 -14 -4 -9 35.11 2.8 -14 -4 -9 33.76 2.65 14 4 9 35.93 2.78 -14 4 -9 33.82 2.65 14 4 9 32.77 2.87 -14 4 -9 34.68 2.69 14 4 9 34.43 2.75 14 4 9 35.2 2.66 -16 -4 -9 46.38 3.17 16 -4 9 44.7 3.38 -16 -4 -9 45.45 3.35 16 -4 9 47.93 3.41 -16 -4 -9 44.98 3.34 -16 -4 -9 47.15 3.24 16 4 9 39.34 3.16 16 4 9 37.65 3.43 -16 4 -9 38.6 3.1 16 4 9 38.04 3.26 -16 4 -9 39.04 3.21 16 4 9 41.59 3.32 -18 -4 -9 65.06 4.84 18 -4 9 74.87 5.33 -18 -4 -9 69.86 5.21 -18 -4 -9 69.22 5 18 -4 9 69.15 5.24 -18 -4 -9 70.68 5.15 18 4 9 72.84 5.2 -18 4 -9 66.76 5.02 18 4 9 65.91 5.36 -18 4 -9 64.66 4.83 18 4 9 62.48 5.09 -20 -4 -9 21.87 2.08 20 -4 9 21.51 2.11 -20 -4 -9 20.48 1.99 -20 -4 -9 21.04 2.08 -20 -4 -9 20.87 1.87 20 4 9 22.51 2.06 -20 4 -9 22.26 1.89 20 4 9 22.29 1.98 20 4 9 19.21 2.1 -20 4 -9 21.21 1.88 -22 -4 -9 7.65 1.19 -22 -4 -9 8.35 1.18 22 -4 9 7.61 1.18 -22 -4 -9 6.43 1.22 -22 -4 -9 7.37 1.07 22 4 9 7.76 1.15 -22 4 -9 7.87 1.17 -22 4 -9 8 1.15 22 4 9 8.35 1.16 22 4 9 8.16 1.19 -24 -4 -9 29.94 2.57 -24 -4 -9 25.96 2.51 -24 -4 -9 29.01 2.64 -24 -4 -9 29.09 2.43 24 -4 9 25.95 2.64 24 4 9 26.02 2.46 24 4 9 30.93 2.53 -24 4 -9 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