data_x14001 _audit_creation_method SHELXL-2012 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C35 H33 Br N3 P Pd' _chemical_formula_weight 712.92 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.1917(7) _cell_length_b 11.9481(8) _cell_length_c 14.9831(10) _cell_angle_alpha 97.5770(10) _cell_angle_beta 109.4170(10) _cell_angle_gamma 113.6010(10) _cell_volume 1500.88(18) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9566 _cell_measurement_theta_min 2.41 _cell_measurement_theta_max 31.62 _exptl_crystal_description block _exptl_crystal_colour yellow _exptl_crystal_density_meas . _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.578 _exptl_crystal_F_000 720 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.330 _exptl_crystal_size_mid 0.240 _exptl_crystal_size_min 0.210 _exptl_absorpt_coefficient_mu 2.032 _shelx_estimated_absorpt_T_min 0.554 _shelx_estimated_absorpt_T_max 0.675 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6337 _exptl_absorpt_correction_T_max 0.7463 _exptl_absorpt_process_details 'SADABS (Sheldrick, 2009)' _exptl_special_details ; Bruker X8 Kappa DUO four-circle diffractometer, Bruker APEX2 CCD. The instrument was purchased with the help of funding from the National Science Foundation (NSF) under Grant Number CHE-0946721. Please acknowledge this grant in all publications of this structure. ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'I\mS micro-focus sealed tube, multilayer optics' _diffrn_measurement_device_type 'Bruker Smart APEX2 CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 8.3 _diffrn_reflns_number 66034 _diffrn_reflns_av_unetI/netI 0.0128 _diffrn_reflns_av_R_equivalents 0.0224 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 1.514 _diffrn_reflns_theta_max 30.999 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 9570 _reflns_number_gt 9148 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX2 v2011.4.0 (Bruker-AXS, 2011)' _computing_cell_refinement 'SAINT 7.46A (Bruker-AXS, 2011)' _computing_data_reduction 'SAINT 7.46A (Bruker-AXS, 2011)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-2012 (Sheldrick, 2012)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0222P)^2^+0.8526P] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 9570 _refine_ls_number_parameters 374 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0192 _refine_ls_R_factor_gt 0.0180 _refine_ls_wR_factor_ref 0.0474 _refine_ls_wR_factor_gt 0.0468 _refine_ls_goodness_of_fit_ref 1.044 _refine_ls_restrained_S_all 1.044 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.74832(2) 0.61353(2) 0.89935(2) 0.01773(3) Uani 1 1 d . . . . . Pd1 Pd 0.59823(2) 0.37877(2) 0.82144(2) 0.01180(2) Uani 1 1 d . . . . . P1 P 0.43733(3) 0.16560(3) 0.76578(2) 0.01160(5) Uani 1 1 d . . . . . C1 C 0.51572(13) 0.05494(10) 0.79028(8) 0.01393(18) Uani 1 1 d . . . . . C2 C 0.55875(14) 0.03731(12) 0.88435(9) 0.0179(2) Uani 1 1 d . . . . . H2 H 0.5474 0.0836 0.9354 0.022 Uiso 1 1 calc R U . . . C3 C 0.61803(15) -0.04787(13) 0.90294(10) 0.0217(2) Uani 1 1 d . . . . . H3 H 0.6459 -0.0603 0.9665 0.026 Uiso 1 1 calc R U . . . C4 C 0.63685(14) -0.11489(12) 0.82912(10) 0.0218(2) Uani 1 1 d . . . . . H4 H 0.6764 -0.1736 0.8420 0.026 Uiso 1 1 calc R U . . . C5 C 0.59756(14) -0.09561(12) 0.73657(10) 0.0198(2) Uani 1 1 d . . . . . H5 H 0.6124 -0.1399 0.6864 0.024 Uiso 1 1 calc R U . . . C6 C 0.53646(14) -0.01159(11) 0.71678(9) 0.0164(2) Uani 1 1 d . . . . . H6 H 0.5088 0.0005 0.6530 0.020 Uiso 1 1 calc R U . . . C7 C 0.27835(13) 0.11802(11) 0.80652(8) 0.01555(19) Uani 1 1 d . . . . . C8 C 0.19968(14) -0.00527(13) 0.81213(9) 0.0203(2) Uani 1 1 d . . . . . H8 H 0.2284 -0.0685 0.7945 0.024 Uiso 1 1 calc R U . . . C9 C 0.07861(15) -0.03543(15) 0.84372(10) 0.0279(3) Uani 1 1 d . . . . . H9 H 0.0251 -0.1192 0.8477 0.033 Uiso 1 1 calc R U . . . C10 C 0.03664(15) 0.05702(17) 0.86932(10) 0.0313(3) Uani 1 1 d . . . . . H10 H -0.0442 0.0368 0.8921 0.038 Uiso 1 1 calc R U . . . C11 C 0.11135(15) 0.17798(16) 0.86193(9) 0.0273(3) Uani 1 1 d . . . . . H11 H 0.0803 0.2401 0.8782 0.033 Uiso 1 1 calc R U . . . C12 C 0.23241(14) 0.20938(13) 0.83071(9) 0.0199(2) Uani 1 1 d . . . . . H12 H 0.2839 0.2929 0.8258 0.024 Uiso 1 1 calc R U . . . C21 C 0.33114(12) 0.11913(10) 0.63164(8) 0.01229(18) Uani 1 1 d . . . . . C22 C 0.21303(13) -0.00711(11) 0.57602(8) 0.01490(19) Uani 1 1 d . . . . . H22 H 0.1923 -0.0719 0.6078 0.018 Uiso 1 1 calc R U . . . C23 C 0.12632(13) -0.03756(11) 0.47457(9) 0.0170(2) Uani 1 1 d . . . . . H23 H 0.0480 -0.1235 0.4367 0.020 Uiso 1 1 calc R U . . . C24 C 0.15398(13) 0.05770(12) 0.42828(8) 0.0171(2) Uani 1 1 d . . . . . H24 H 0.0930 0.0372 0.3591 0.021 Uiso 1 1 calc R U . . . C25 C 0.27075(13) 0.18271(11) 0.48324(8) 0.01546(19) Uani 1 1 d . . . . . H25 H 0.2883 0.2474 0.4513 0.019 Uiso 1 1 calc R U . . . C26 C 0.36334(12) 0.21504(10) 0.58525(8) 0.01248(18) Uani 1 1 d . . . . . C27 C 0.49954(13) 0.34811(10) 0.63682(8) 0.01282(18) Uani 1 1 d . . . . . C28 C 0.65560(13) 0.36365(10) 0.66287(8) 0.01339(18) Uani 1 1 d . . . . . C29 C 0.78174(14) 0.48287(11) 0.68145(9) 0.0169(2) Uani 1 1 d . . . . . H29 H 0.8852 0.4925 0.7000 0.020 Uiso 1 1 calc R U . . . C30 C 0.75581(14) 0.58682(11) 0.67286(9) 0.0183(2) Uani 1 1 d . . . . . H30 H 0.8417 0.6674 0.6845 0.022 Uiso 1 1 calc R U . . . C31 C 0.60600(14) 0.57489(11) 0.64751(9) 0.0174(2) Uani 1 1 d . . . . . H31 H 0.5913 0.6479 0.6426 0.021 Uiso 1 1 calc R U . . . C32 C 0.47588(13) 0.45779(11) 0.62891(8) 0.01444(19) Uani 1 1 d . . . . . N1 N 0.67595(11) 0.25129(9) 0.65886(7) 0.01447(17) Uani 1 1 d . . . . . C33 C 0.82963(14) 0.27348(13) 0.72993(10) 0.0206(2) Uani 1 1 d . . . . . H33A H 0.9116 0.3213 0.7091 0.031 Uiso 1 1 calc R U . . . H33B H 0.8265 0.1909 0.7323 0.031 Uiso 1 1 calc R U . . . H33C H 0.8537 0.3231 0.7961 0.031 Uiso 1 1 calc R U . . . C34 C 0.64413(15) 0.18620(12) 0.55815(9) 0.0197(2) Uani 1 1 d . . . . . H34A H 0.5389 0.1681 0.5116 0.030 Uiso 1 1 calc R U . . . H34B H 0.6483 0.1055 0.5569 0.030 Uiso 1 1 calc R U . . . H34C H 0.7239 0.2415 0.5387 0.030 Uiso 1 1 calc R U . . . N2 N 0.32469(12) 0.44557(10) 0.59646(8) 0.01799(18) Uani 1 1 d . . . . . C35 C 0.22085(15) 0.37982(12) 0.64038(11) 0.0241(2) Uani 1 1 d . . . . . H35A H 0.2307 0.3035 0.6501 0.036 Uiso 1 1 calc R U . . . H35B H 0.1113 0.3540 0.5960 0.036 Uiso 1 1 calc R U . . . H35C H 0.2504 0.4375 0.7047 0.036 Uiso 1 1 calc R U . . . C36 C 0.30484(17) 0.55331(13) 0.57142(10) 0.0237(2) Uani 1 1 d . . . . . H36A H 0.3521 0.6241 0.6325 0.036 Uiso 1 1 calc R U . . . H36B H 0.1919 0.5265 0.5367 0.036 Uiso 1 1 calc R U . . . H36C H 0.3571 0.5818 0.5282 0.036 Uiso 1 1 calc R U . . . C41 C 0.66318(13) 0.36595(11) 0.95907(8) 0.01426(19) Uani 1 1 d . . . . . C42 C 0.80040(14) 0.35422(12) 0.99877(8) 0.0180(2) Uani 1 1 d . . . . . H42 H 0.8586 0.3548 0.9606 0.022 Uiso 1 1 calc R U . . . C43 C 0.85276(14) 0.34164(12) 1.09337(9) 0.0186(2) Uani 1 1 d . . . . . H43 H 0.9461 0.3337 1.1197 0.022 Uiso 1 1 calc R U . . . C44 C 0.76678(13) 0.34077(11) 1.14947(8) 0.0164(2) Uani 1 1 d . . . . . C45 C 0.63285(13) 0.35760(11) 1.11189(8) 0.0165(2) Uani 1 1 d . . . . . H45 H 0.5766 0.3600 1.1509 0.020 Uiso 1 1 calc R U . . . C46 C 0.58223(13) 0.37078(11) 1.01740(8) 0.01591(19) Uani 1 1 d . . . . . H46 H 0.4920 0.3831 0.9923 0.019 Uiso 1 1 calc R U . . . N3 N 0.85708(14) 0.30254(13) 1.32061(9) 0.0263(2) Uani 1 1 d . . . . . C47 C 0.81611(14) 0.32051(12) 1.24514(9) 0.0194(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.02129(6) 0.01255(5) 0.01611(5) 0.00111(4) 0.00710(4) 0.00678(4) Pd1 0.01275(4) 0.01108(4) 0.01063(4) 0.00197(3) 0.00442(3) 0.00564(3) P1 0.01231(11) 0.01143(11) 0.01087(11) 0.00295(9) 0.00463(9) 0.00583(10) C1 0.0128(4) 0.0128(4) 0.0155(5) 0.0050(4) 0.0051(4) 0.0060(4) C2 0.0167(5) 0.0196(5) 0.0159(5) 0.0066(4) 0.0052(4) 0.0081(4) C3 0.0183(5) 0.0233(6) 0.0234(6) 0.0131(5) 0.0064(4) 0.0099(5) C4 0.0164(5) 0.0185(5) 0.0334(7) 0.0134(5) 0.0098(5) 0.0098(4) C5 0.0191(5) 0.0158(5) 0.0284(6) 0.0076(4) 0.0119(5) 0.0101(4) C6 0.0175(5) 0.0146(5) 0.0196(5) 0.0066(4) 0.0091(4) 0.0085(4) C7 0.0133(4) 0.0200(5) 0.0117(4) 0.0035(4) 0.0050(4) 0.0071(4) C8 0.0165(5) 0.0241(6) 0.0171(5) 0.0075(4) 0.0066(4) 0.0067(4) C9 0.0164(5) 0.0384(8) 0.0193(6) 0.0110(5) 0.0075(5) 0.0039(5) C10 0.0141(5) 0.0556(10) 0.0162(5) 0.0055(6) 0.0069(4) 0.0107(6) C11 0.0171(5) 0.0453(8) 0.0156(5) -0.0012(5) 0.0043(4) 0.0167(6) C12 0.0166(5) 0.0262(6) 0.0145(5) 0.0010(4) 0.0044(4) 0.0113(5) C21 0.0124(4) 0.0130(4) 0.0119(4) 0.0025(3) 0.0049(4) 0.0070(4) C22 0.0145(5) 0.0130(5) 0.0163(5) 0.0033(4) 0.0063(4) 0.0064(4) C23 0.0140(5) 0.0153(5) 0.0164(5) -0.0002(4) 0.0044(4) 0.0054(4) C24 0.0151(5) 0.0207(5) 0.0124(4) 0.0016(4) 0.0035(4) 0.0087(4) C25 0.0167(5) 0.0176(5) 0.0128(4) 0.0051(4) 0.0060(4) 0.0089(4) C26 0.0126(4) 0.0129(4) 0.0125(4) 0.0027(3) 0.0053(4) 0.0069(4) C27 0.0142(4) 0.0122(4) 0.0123(4) 0.0034(3) 0.0056(4) 0.0066(4) C28 0.0148(4) 0.0137(4) 0.0120(4) 0.0034(4) 0.0056(4) 0.0072(4) C29 0.0158(5) 0.0163(5) 0.0167(5) 0.0044(4) 0.0074(4) 0.0058(4) C30 0.0196(5) 0.0137(5) 0.0186(5) 0.0051(4) 0.0087(4) 0.0047(4) C31 0.0230(5) 0.0130(5) 0.0170(5) 0.0053(4) 0.0092(4) 0.0085(4) C32 0.0177(5) 0.0145(5) 0.0127(4) 0.0044(4) 0.0068(4) 0.0087(4) N1 0.0153(4) 0.0154(4) 0.0148(4) 0.0043(3) 0.0061(3) 0.0095(3) C33 0.0162(5) 0.0239(6) 0.0230(5) 0.0081(5) 0.0063(4) 0.0119(5) C34 0.0235(5) 0.0209(5) 0.0184(5) 0.0037(4) 0.0102(4) 0.0136(5) N2 0.0198(5) 0.0184(4) 0.0204(5) 0.0076(4) 0.0084(4) 0.0129(4) C35 0.0205(6) 0.0187(5) 0.0377(7) 0.0088(5) 0.0158(5) 0.0106(5) C36 0.0300(6) 0.0222(6) 0.0264(6) 0.0102(5) 0.0112(5) 0.0189(5) C41 0.0144(4) 0.0140(5) 0.0114(4) 0.0019(4) 0.0042(4) 0.0057(4) C42 0.0157(5) 0.0247(6) 0.0141(5) 0.0049(4) 0.0067(4) 0.0101(4) C43 0.0157(5) 0.0246(6) 0.0153(5) 0.0050(4) 0.0056(4) 0.0106(4) C44 0.0154(5) 0.0173(5) 0.0142(5) 0.0041(4) 0.0056(4) 0.0064(4) C45 0.0146(5) 0.0177(5) 0.0156(5) 0.0040(4) 0.0072(4) 0.0061(4) C46 0.0146(5) 0.0174(5) 0.0149(5) 0.0033(4) 0.0059(4) 0.0076(4) N3 0.0277(6) 0.0350(6) 0.0227(5) 0.0133(5) 0.0129(5) 0.0176(5) C47 0.0179(5) 0.0219(5) 0.0189(5) 0.0063(4) 0.0087(4) 0.0092(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 Pd1 2.4666(2) . ? Pd1 C41 1.9926(11) . ? Pd1 P1 2.2490(3) . ? Pd1 C27 2.5269(11) . ? Pd1 C28 2.6296(11) . ? P1 C21 1.8158(11) . ? P1 C1 1.8166(11) . ? P1 C7 1.8256(11) . ? C1 C6 1.3957(16) . ? C1 C2 1.4015(15) . ? C2 C3 1.3907(17) . ? C2 H2 0.9500 . ? C3 C4 1.3899(19) . ? C3 H3 0.9500 . ? C4 C5 1.3876(18) . ? C4 H4 0.9500 . ? C5 C6 1.3927(16) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.3970(17) . ? C7 C12 1.3999(16) . ? C8 C9 1.3977(17) . ? C8 H8 0.9500 . ? C9 C10 1.388(2) . ? C9 H9 0.9500 . ? C10 C11 1.378(2) . ? C10 H10 0.9500 . ? C11 C12 1.3932(17) . ? C11 H11 0.9500 . ? C12 H12 0.9500 . ? C21 C26 1.4017(15) . ? C21 C22 1.4023(15) . ? C22 C23 1.3884(16) . ? C22 H22 0.9500 . ? C23 C24 1.3919(17) . ? C23 H23 0.9500 . ? C24 C25 1.3878(16) . ? C24 H24 0.9500 . ? C25 C26 1.4033(15) . ? C25 H25 0.9500 . ? C26 C27 1.4991(15) . ? C27 C28 1.4312(15) . ? C27 C32 1.4369(15) . ? C28 C29 1.3966(16) . ? C28 N1 1.4348(14) . ? C29 C30 1.3825(17) . ? C29 H29 0.9500 . ? C30 C31 1.3862(17) . ? C30 H30 0.9500 . ? C31 C32 1.3998(16) . ? C31 H31 0.9500 . ? C32 N2 1.3910(15) . ? N1 C33 1.4634(15) . ? N1 C34 1.4663(15) . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? N2 C35 1.4505(17) . ? N2 C36 1.4575(15) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C41 C46 1.3972(15) . ? C41 C42 1.3983(16) . ? C42 C43 1.3906(16) . ? C42 H42 0.9500 . ? C43 C44 1.3997(16) . ? C43 H43 0.9500 . ? C44 C45 1.3998(16) . ? C44 C47 1.4408(16) . ? C45 C46 1.3905(16) . ? C45 H45 0.9500 . ? C46 H46 0.9500 . ? N3 C47 1.1492(17) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C41 Pd1 P1 88.18(3) . . ? C41 Pd1 Br1 86.55(3) . . ? P1 Pd1 Br1 170.048(8) . . ? C41 Pd1 C27 168.62(4) . . ? P1 Pd1 C27 81.22(3) . . ? Br1 Pd1 C27 104.54(2) . . ? C41 Pd1 C28 144.72(4) . . ? P1 Pd1 C28 89.91(3) . . ? Br1 Pd1 C28 99.26(2) . . ? C27 Pd1 C28 32.15(3) . . ? C21 P1 C1 106.22(5) . . ? C21 P1 C7 102.78(5) . . ? C1 P1 C7 104.41(5) . . ? C21 P1 Pd1 108.05(4) . . ? C1 P1 Pd1 120.89(4) . . ? C7 P1 Pd1 112.88(4) . . ? C6 C1 C2 119.26(10) . . ? C6 C1 P1 120.71(8) . . ? C2 C1 P1 120.02(9) . . ? C3 C2 C1 120.01(11) . . ? C3 C2 H2 120.0 . . ? C1 C2 H2 120.0 . . ? C4 C3 C2 120.46(11) . . ? C4 C3 H3 119.8 . . ? C2 C3 H3 119.8 . . ? C5 C4 C3 119.68(11) . . ? C5 C4 H4 120.2 . . ? C3 C4 H4 120.2 . . ? C4 C5 C6 120.34(12) . . ? C4 C5 H5 119.8 . . ? C6 C5 H5 119.8 . . ? C5 C6 C1 120.23(11) . . ? C5 C6 H6 119.9 . . ? C1 C6 H6 119.9 . . ? C8 C7 C12 119.40(11) . . ? C8 C7 P1 122.82(9) . . ? C12 C7 P1 117.76(9) . . ? C7 C8 C9 119.89(13) . . ? C7 C8 H8 120.1 . . ? C9 C8 H8 120.1 . . ? C10 C9 C8 119.98(14) . . ? C10 C9 H9 120.0 . . ? C8 C9 H9 120.0 . . ? C11 C10 C9 120.46(12) . . ? C11 C10 H10 119.8 . . ? C9 C10 H10 119.8 . . ? C10 C11 C12 120.14(13) . . ? C10 C11 H11 119.9 . . ? C12 C11 H11 119.9 . . ? C11 C12 C7 120.11(13) . . ? C11 C12 H12 119.9 . . ? C7 C12 H12 119.9 . . ? C26 C21 C22 120.36(10) . . ? C26 C21 P1 118.06(8) . . ? C22 C21 P1 121.46(8) . . ? C23 C22 C21 120.05(10) . . ? C23 C22 H22 120.0 . . ? C21 C22 H22 120.0 . . ? C22 C23 C24 120.07(11) . . ? C22 C23 H23 120.0 . . ? C24 C23 H23 120.0 . . ? C25 C24 C23 119.93(10) . . ? C25 C24 H24 120.0 . . ? C23 C24 H24 120.0 . . ? C24 C25 C26 121.04(10) . . ? C24 C25 H25 119.5 . . ? C26 C25 H25 119.5 . . ? C21 C26 C25 118.48(10) . . ? C21 C26 C27 123.51(9) . . ? C25 C26 C27 117.84(10) . . ? C28 C27 C32 118.26(10) . . ? C28 C27 C26 117.77(9) . . ? C32 C27 C26 120.41(9) . . ? C28 C27 Pd1 77.88(6) . . ? C32 C27 Pd1 102.62(7) . . ? C26 C27 Pd1 107.20(7) . . ? C29 C28 C27 120.72(10) . . ? C29 C28 N1 120.69(10) . . ? C27 C28 N1 118.25(10) . . ? C29 C28 Pd1 105.91(7) . . ? C27 C28 Pd1 69.97(6) . . ? N1 C28 Pd1 98.99(6) . . ? C30 C29 C28 119.92(11) . . ? C30 C29 H29 120.0 . . ? C28 C29 H29 120.0 . . ? C29 C30 C31 120.77(11) . . ? C29 C30 H30 119.6 . . ? C31 C30 H30 119.6 . . ? C30 C31 C32 121.54(11) . . ? C30 C31 H31 119.2 . . ? C32 C31 H31 119.2 . . ? N2 C32 C31 120.58(10) . . ? N2 C32 C27 120.49(10) . . ? C31 C32 C27 118.77(10) . . ? C28 N1 C33 114.57(9) . . ? C28 N1 C34 111.82(9) . . ? C33 N1 C34 110.07(9) . . ? N1 C33 H33A 109.5 . . ? N1 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? N1 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? N1 C34 H34A 109.5 . . ? N1 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? N1 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C32 N2 C35 119.95(10) . . ? C32 N2 C36 117.59(10) . . ? C35 N2 C36 112.25(10) . . ? N2 C35 H35A 109.5 . . ? N2 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? N2 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? N2 C36 H36A 109.5 . . ? N2 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? N2 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C46 C41 C42 119.17(10) . . ? C46 C41 Pd1 123.99(8) . . ? C42 C41 Pd1 116.83(8) . . ? C43 C42 C41 120.89(10) . . ? C43 C42 H42 119.6 . . ? C41 C42 H42 119.6 . . ? C42 C43 C44 119.46(11) . . ? C42 C43 H43 120.3 . . ? C44 C43 H43 120.3 . . ? C43 C44 C45 120.00(11) . . ? C43 C44 C47 119.40(11) . . ? C45 C44 C47 120.59(10) . . ? C46 C45 C44 119.93(10) . . ? C46 C45 H45 120.0 . . ? C44 C45 H45 120.0 . . ? C45 C46 C41 120.44(10) . . ? C45 C46 H46 119.8 . . ? C41 C46 H46 119.8 . . ? N3 C47 C44 178.23(14) . . ? _refine_diff_density_max 0.534 _refine_diff_density_min -0.401 _refine_diff_density_rms 0.059 _shelxl_version_number 2012-9 _shelx_res_file ; TITL X14001 in P-1 CELL 0.71073 10.1917 11.9481 14.9831 97.577 109.417 113.601 ZERR 2.00 0.0007 0.0008 0.0010 0.001 0.001 0.001 LATT 1 SFAC C H N P BR PD UNIT 70 66 6 2 2 2 TEMP -173 SIZE 0.21 0.24 0.33 WPDB -2 ACTA OMIT 1 -5 4 ! outlier OMIT -5 0 6 ! outlier REM All hydrogen atoms visible in difference Fourier map. L.S. 10 BOND $H FMAP 2 PLAN 20 WGHT 0.022200 0.852600 FVAR 0.16832 BR1 5 0.748319 0.613532 0.899353 11.00000 0.02129 0.01255 = 0.01611 0.00111 0.00710 0.00678 PD1 6 0.598231 0.378771 0.821444 11.00000 0.01275 0.01108 = 0.01063 0.00197 0.00442 0.00564 P1 4 0.437328 0.165597 0.765778 11.00000 0.01231 0.01143 = 0.01087 0.00295 0.00463 0.00583 C1 1 0.515725 0.054939 0.790282 11.00000 0.01276 0.01284 = 0.01553 0.00500 0.00513 0.00600 C2 1 0.558748 0.037314 0.884347 11.00000 0.01669 0.01960 = 0.01590 0.00661 0.00522 0.00814 AFIX 43 H2 2 0.547412 0.083567 0.935410 11.00000 -1.20000 AFIX 0 C3 1 0.618028 -0.047875 0.902942 11.00000 0.01830 0.02328 = 0.02336 0.01306 0.00637 0.00993 AFIX 43 H3 2 0.645858 -0.060349 0.966549 11.00000 -1.20000 AFIX 0 C4 1 0.636846 -0.114894 0.829120 11.00000 0.01636 0.01852 = 0.03337 0.01339 0.00976 0.00983 AFIX 43 H4 2 0.676411 -0.173618 0.841965 11.00000 -1.20000 AFIX 0 C5 1 0.597560 -0.095608 0.736569 11.00000 0.01912 0.01576 = 0.02838 0.00757 0.01187 0.01010 AFIX 43 H5 2 0.612417 -0.139944 0.686444 11.00000 -1.20000 AFIX 0 C6 1 0.536463 -0.011594 0.716776 11.00000 0.01754 0.01457 = 0.01965 0.00658 0.00912 0.00853 AFIX 43 H6 2 0.508806 0.000471 0.653023 11.00000 -1.20000 AFIX 0 C7 1 0.278351 0.118022 0.806524 11.00000 0.01327 0.02003 = 0.01171 0.00354 0.00502 0.00706 C8 1 0.199678 -0.005273 0.812125 11.00000 0.01651 0.02408 = 0.01706 0.00751 0.00658 0.00673 AFIX 43 H8 2 0.228416 -0.068511 0.794491 11.00000 -1.20000 AFIX 0 C9 1 0.078610 -0.035433 0.843718 11.00000 0.01642 0.03840 = 0.01934 0.01104 0.00746 0.00389 AFIX 43 H9 2 0.025075 -0.119189 0.847666 11.00000 -1.20000 AFIX 0 C10 1 0.036636 0.057019 0.869318 11.00000 0.01409 0.05561 = 0.01625 0.00555 0.00694 0.01067 AFIX 43 H10 2 -0.044180 0.036751 0.892096 11.00000 -1.20000 AFIX 0 C11 1 0.111354 0.177979 0.861929 11.00000 0.01714 0.04532 = 0.01559 -0.00123 0.00434 0.01667 AFIX 43 H11 2 0.080267 0.240110 0.878152 11.00000 -1.20000 AFIX 0 C12 1 0.232414 0.209382 0.830712 11.00000 0.01656 0.02621 = 0.01453 0.00098 0.00439 0.01132 AFIX 43 H12 2 0.283875 0.292934 0.825832 11.00000 -1.20000 AFIX 0 REM --------------------------------------------------- C21 1 0.331137 0.119133 0.631640 11.00000 0.01236 0.01299 = 0.01188 0.00248 0.00486 0.00698 C22 1 0.213030 -0.007114 0.576021 11.00000 0.01453 0.01301 = 0.01631 0.00328 0.00628 0.00637 AFIX 43 H22 2 0.192334 -0.071855 0.607784 11.00000 -1.20000 AFIX 0 C23 1 0.126316 -0.037563 0.474569 11.00000 0.01400 0.01535 = 0.01642 -0.00023 0.00439 0.00537 AFIX 43 H23 2 0.048011 -0.123516 0.436700 11.00000 -1.20000 AFIX 0 C24 1 0.153981 0.057705 0.428278 11.00000 0.01511 0.02074 = 0.01237 0.00156 0.00353 0.00868 AFIX 43 H24 2 0.092995 0.037175 0.359136 11.00000 -1.20000 AFIX 0 C25 1 0.270749 0.182711 0.483236 11.00000 0.01670 0.01760 = 0.01281 0.00510 0.00601 0.00888 AFIX 43 H25 2 0.288274 0.247418 0.451295 11.00000 -1.20000 AFIX 0 C26 1 0.363342 0.215040 0.585246 11.00000 0.01257 0.01289 = 0.01248 0.00271 0.00527 0.00689 C27 1 0.499542 0.348107 0.636824 11.00000 0.01423 0.01216 = 0.01234 0.00341 0.00560 0.00662 C28 1 0.655604 0.363651 0.662869 11.00000 0.01476 0.01370 = 0.01198 0.00340 0.00562 0.00721 C29 1 0.781738 0.482873 0.681451 11.00000 0.01583 0.01627 = 0.01667 0.00437 0.00737 0.00577 AFIX 43 H29 2 0.885240 0.492532 0.699970 11.00000 -1.20000 AFIX 0 C30 1 0.755807 0.586819 0.672864 11.00000 0.01957 0.01369 = 0.01864 0.00512 0.00868 0.00473 AFIX 43 H30 2 0.841664 0.667371 0.684478 11.00000 -1.20000 AFIX 0 C31 1 0.606003 0.574886 0.647506 11.00000 0.02300 0.01297 = 0.01696 0.00527 0.00918 0.00852 AFIX 43 H31 2 0.591298 0.647876 0.642632 11.00000 -1.20000 AFIX 0 C32 1 0.475882 0.457795 0.628913 11.00000 0.01770 0.01446 = 0.01273 0.00443 0.00684 0.00866 N1 3 0.675952 0.251292 0.658858 11.00000 0.01525 0.01541 = 0.01479 0.00433 0.00606 0.00948 C33 1 0.829631 0.273480 0.729932 11.00000 0.01615 0.02395 = 0.02302 0.00809 0.00631 0.01195 AFIX 137 H33A 2 0.911602 0.321265 0.709069 11.00000 -1.50000 H33B 2 0.826480 0.190895 0.732270 11.00000 -1.50000 H33C 2 0.853724 0.323140 0.796053 11.00000 -1.50000 AFIX 0 C34 1 0.644135 0.186197 0.558152 11.00000 0.02352 0.02092 = 0.01842 0.00374 0.01017 0.01357 AFIX 137 H34A 2 0.538930 0.168106 0.511588 11.00000 -1.50000 H34B 2 0.648302 0.105492 0.556852 11.00000 -1.50000 H34C 2 0.723907 0.241488 0.538711 11.00000 -1.50000 AFIX 0 N2 3 0.324693 0.445570 0.596464 11.00000 0.01978 0.01843 = 0.02045 0.00756 0.00844 0.01289 C35 1 0.220851 0.379822 0.640385 11.00000 0.02045 0.01867 = 0.03768 0.00878 0.01580 0.01065 AFIX 137 H35A 2 0.230707 0.303538 0.650072 11.00000 -1.50000 H35B 2 0.111272 0.353978 0.596047 11.00000 -1.50000 H35C 2 0.250416 0.437528 0.704711 11.00000 -1.50000 AFIX 0 C36 1 0.304841 0.553314 0.571423 11.00000 0.02997 0.02223 = 0.02641 0.01025 0.01121 0.01894 AFIX 137 H36A 2 0.352141 0.624085 0.632466 11.00000 -1.50000 H36B 2 0.191914 0.526469 0.536719 11.00000 -1.50000 H36C 2 0.357121 0.581831 0.528248 11.00000 -1.50000 AFIX 0 REM --------------------------------------------------- C41 1 0.663182 0.365954 0.959069 11.00000 0.01440 0.01401 = 0.01141 0.00190 0.00422 0.00569 C42 1 0.800398 0.354219 0.998774 11.00000 0.01574 0.02475 = 0.01409 0.00493 0.00670 0.01013 AFIX 43 H42 2 0.858636 0.354846 0.960612 11.00000 -1.20000 AFIX 0 C43 1 0.852761 0.341643 1.093373 11.00000 0.01566 0.02465 = 0.01529 0.00501 0.00556 0.01060 AFIX 43 H43 2 0.946125 0.333713 1.119706 11.00000 -1.20000 AFIX 0 C44 1 0.766783 0.340765 1.149475 11.00000 0.01537 0.01731 = 0.01416 0.00414 0.00555 0.00635 C45 1 0.632853 0.357601 1.111888 11.00000 0.01463 0.01774 = 0.01558 0.00404 0.00716 0.00613 AFIX 43 H45 2 0.576610 0.360024 1.150892 11.00000 -1.20000 AFIX 0 C46 1 0.582226 0.370776 1.017398 11.00000 0.01458 0.01740 = 0.01492 0.00331 0.00590 0.00762 AFIX 43 H46 2 0.491984 0.383139 0.992334 11.00000 -1.20000 AFIX 0 N3 3 0.857078 0.302541 1.320605 11.00000 0.02768 0.03498 = 0.02267 0.01329 0.01286 0.01757 C47 1 0.816106 0.320509 1.245143 11.00000 0.01790 0.02190 = 0.01888 0.00633 0.00867 0.00919 HKLF 4 REM X14001 in P-1 REM R1 = 0.0180 for 9148 Fo > 4sig(Fo) and 0.0192 for all 9570 data REM 374 parameters refined using 0 restraints END WGHT 0.0222 0.8526 REM Highest difference peak 0.534, deepest hole -0.401, 1-sigma level 0.059 Q1 1 0.2099 0.1829 0.4087 11.00000 0.05 0.53 Q2 1 0.6234 0.3688 0.9884 11.00000 0.05 0.53 Q3 1 0.5776 -0.0462 0.7292 11.00000 0.05 0.47 Q4 1 0.6958 0.3455 1.1314 11.00000 0.05 0.46 Q5 1 0.7661 0.5311 0.6749 11.00000 0.05 0.45 Q6 1 0.5934 0.0037 0.8976 11.00000 0.05 0.45 Q7 1 0.2110 0.1203 0.4600 11.00000 0.05 0.45 Q8 1 0.6048 0.3545 1.0601 11.00000 0.05 0.44 Q9 1 0.5378 0.0483 0.8376 11.00000 0.05 0.44 Q10 1 0.4830 0.4003 0.6257 11.00000 0.05 0.44 Q11 1 0.2715 0.0612 0.6019 11.00000 0.05 0.44 Q12 1 0.3049 0.1910 0.5309 11.00000 0.05 0.42 Q13 1 0.8192 0.3403 1.0439 11.00000 0.05 0.42 Q14 1 0.4246 0.2802 0.6125 11.00000 0.05 0.42 Q15 1 0.6233 -0.0941 0.7863 11.00000 0.05 0.42 Q16 1 0.7992 0.3304 1.1184 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64.23 1.70 2 3 0 65.95 1.61 2 3 0 60.55 1.61 2 3 0 58.77 1.61 2 3 0 63.67 1.66 -3 -3 0 69.28 1.99 -3 -3 0 72.30 1.87 -3 -3 0 71.06 1.98 -3 -3 0 72.09 1.95 -3 -3 0 73.92 1.87 -3 -3 0 75.36 1.87 3 3 0 74.52 1.87 3 3 0 72.17 1.93 3 3 0 70.13 1.88 3 3 0 73.93 1.89 3 3 0 74.22 1.86 3 3 0 74.54 1.98 3 3 0 72.42 1.99 -4 -3 0 39.15 1.22 -4 -3 0 42.22 1.13 -4 -3 0 41.67 1.19 -4 -3 0 38.00 1.13 -4 -3 0 41.88 1.14 -4 -3 0 39.93 1.22 -4 -3 0 41.48 1.18 4 3 0 39.54 1.14 4 3 0 39.84 1.22 4 3 0 41.54 1.12 4 3 0 42.40 1.22 4 3 0 39.72 1.18 4 3 0 38.24 1.14 -5 -3 0 13.08 0.53 -5 -3 0 12.63 0.57 -5 -3 0 12.75 0.57 -5 -3 0 12.04 0.53 -5 -3 0 13.81 0.53 -5 -3 0 12.42 0.50 5 3 0 12.84 0.52 5 3 0 13.88 0.58 5 3 0 12.46 0.56 5 3 0 12.26 0.53 5 3 0 12.82 0.53 -6 -3 0 1.54 0.25 -6 -3 0 1.40 0.24 -6 -3 0 1.66 0.26 -6 -3 0 2.10 0.27 6 3 0 2.32 0.30 6 3 0 0.93 0.21 6 3 0 1.09 0.23 6 3 0 1.21 0.25 -7 -3 0 5.16 0.40 -7 -3 0 5.45 0.45 -7 -3 0 4.56 0.45 7 3 0 4.90 0.46 7 3 0 4.87 0.44 7 3 0 5.66 0.42 -8 -3 0 31.61 1.08 -8 -3 0 30.70 1.15 -8 -3 0 29.50 1.18 8 3 0 28.61 1.17 8 3 0 31.21 1.09 8 3 0 30.05 1.13 -9 -3 0 76.64 2.48 -9 -3 0 80.37 2.42 -9 -3 0 79.69 2.31 9 3 0 83.20 2.31 9 3 0 81.97 2.50 9 3 0 76.03 2.39 -10 -3 0 9.18 0.67 -10 -3 0 8.61 0.72 -10 -3 0 7.59 0.72 10 3 0 9.89 0.76 10 3 0 8.68 0.70 13 -4 0 3.25 0.54 13 -4 0 1.73 0.33 13 -4 0 1.89 0.40 13 -4 0 2.02 0.40 13 -4 0 2.26 0.41 12 -4 0 47.17 1.56 12 -4 0 49.13 1.65 12 -4 0 46.32 1.50 12 -4 0 48.77 1.63 12 -4 0 48.63 1.57 12 -4 0 46.38 1.47 -12 4 0 47.80 1.50 11 -4 0 43.16 1.39 11 -4 0 43.41 1.45 11 -4 0 44.38 1.47 11 -4 0 43.22 1.33 11 -4 0 42.72 1.39 11 -4 0 42.64 1.36 -11 4 0 43.79 1.35 10 -4 0 4.53 0.42 10 -4 0 4.51 0.41 10 -4 0 4.49 0.37 10 -4 0 4.55 0.41 10 -4 0 4.41 0.43 10 -4 0 5.14 0.37 -10 4 0 3.68 0.35 9 -4 0 9.16 0.50 9 -4 0 9.82 0.45 9 -4 0 9.91 0.49 9 -4 0 9.36 0.47 9 -4 0 10.26 0.48 9 -4 0 9.57 0.50 -9 4 0 9.83 0.44 -9 4 0 9.67 0.44 8 -4 0 19.13 0.69 8 -4 0 19.26 0.70 8 -4 0 19.47 0.69 8 -4 0 18.48 0.66 8 -4 0 19.76 0.67 8 -4 0 19.36 0.64 -8 4 0 19.44 0.63 -8 4 0 19.37 0.64 7 -4 0 12.74 0.45 7 -4 0 12.77 0.49 7 -4 0 11.98 0.49 7 -4 0 12.39 0.47 7 -4 0 12.09 0.47 7 -4 0 12.42 0.40 7 -4 0 13.63 0.45 7 -4 0 13.56 0.52 -7 4 0 13.05 0.49 -7 4 0 12.82 0.44 -7 4 0 12.45 0.45 -7 4 0 13.77 0.48 -7 4 0 13.12 0.45 6 -4 0 376.64 9.68 6 -4 0 376.83 8.71 6 -4 0 364.40 9.47 6 -4 0 400.03 9.40 6 -4 0 378.64 8.95 6 -4 0 390.20 9.06 6 -4 0 371.67 9.09 6 -4 0 361.10 8.74 6 -4 0 375.90 9.44 -6 4 0 372.68 9.10 -6 4 0 364.25 9.23 -6 4 0 383.28 9.19 -6 4 0 357.32 9.12 -6 4 0 380.89 9.30 -6 4 0 368.52 9.44 5 -4 0 295.52 7.44 5 -4 0 284.83 6.96 5 -4 0 286.14 6.81 5 -4 0 284.23 6.66 5 -4 0 277.99 6.68 5 -4 0 290.10 7.17 5 -4 0 297.61 6.89 5 -4 0 277.86 7.39 5 -4 0 284.54 7.05 -5 4 0 283.84 7.00 -5 4 0 277.28 6.99 -5 4 0 291.63 7.01 -5 4 0 285.30 7.25 -5 4 0 286.00 7.01 4 -4 0 93.78 2.35 4 -4 0 92.16 2.36 4 -4 0 88.38 2.34 4 -4 0 87.93 2.22 4 -4 0 92.10 2.21 4 -4 0 91.56 2.21 4 -4 0 91.63 2.35 4 -4 0 91.58 2.29 -4 4 0 95.13 2.24 -4 4 0 91.94 2.24 -4 4 0 95.08 2.35 -4 4 0 92.85 2.24 3 -4 0 68.37 1.67 3 -4 0 68.26 1.64 3 -4 0 68.90 1.75 3 -4 0 69.81 1.65 3 -4 0 68.09 1.76 3 -4 0 70.32 1.70 3 -4 0 67.99 1.77 3 -4 0 67.96 1.74 -3 4 0 68.99 1.74 -3 4 0 66.07 1.67 -3 4 0 69.67 1.67 -3 4 0 68.17 1.67 2 -4 0 2.10 0.11 2 -4 0 2.07 0.09 2 -4 0 1.90 0.10 2 -4 0 1.93 0.12 2 -4 0 2.26 0.09 2 -4 0 2.18 0.10 2 -4 0 2.07 0.11 2 -4 0 2.20 0.13 -2 4 0 2.25 0.09 -2 4 0 1.99 0.09 -2 4 0 1.94 0.09 -2 4 0 1.88 0.09 1 -4 0 11.63 0.33 1 -4 0 11.95 0.36 1 -4 0 11.43 0.33 1 -4 0 11.79 0.33 1 -4 0 11.75 0.35 1 -4 0 11.90 0.31 1 -4 0 11.52 0.36 1 -4 0 11.14 0.36 -1 4 0 11.18 0.33 -1 4 0 11.71 0.33 -1 4 0 12.02 0.35 -1 4 0 11.60 0.34 0 -4 0 650.00 16.97 0 -4 0 669.52 16.80 0 -4 0 665.78 16.46 0 -4 0 673.31 15.87 0 -4 0 661.22 15.94 0 -4 0 646.43 16.08 0 -4 0 639.37 16.87 0 -4 0 651.19 16.07 0 -4 0 688.18 16.89 0 4 0 657.87 16.14 0 4 0 648.08 16.83 0 4 0 648.10 16.14 0 4 0 651.65 16.11 0 4 0 714.45 16.91 0 4 0 652.50 16.42 -1 -4 0 627.58 15.53 -1 -4 0 641.33 16.53 -1 -4 0 625.80 16.32 -1 -4 0 644.41 16.08 -1 -4 0 650.68 16.60 -1 -4 0 628.93 15.84 -1 -4 0 637.28 16.59 1 4 0 629.18 15.89 1 4 0 677.09 16.20 1 4 0 655.98 15.82 1 4 0 628.04 16.62 1 4 0 658.42 16.58 1 4 0 657.74 15.84 -2 -4 0 40.57 1.15 -2 -4 0 39.07 1.16 -2 -4 0 37.59 1.11 -2 -4 0 42.42 1.17 -2 -4 0 38.56 1.07 -2 -4 0 38.07 1.07 -2 -4 0 38.30 1.14 2 4 0 39.34 1.15 2 4 0 40.93 1.12 2 4 0 42.50 1.10 2 4 0 39.56 1.07 2 4 0 37.88 1.08 2 4 0 43.28 1.16 -3 -4 0 48.07 1.34 -3 -4 0 48.51 1.34 -3 -4 0 48.10 1.44 -3 -4 0 49.01 1.39 -3 -4 0 48.14 1.44 -3 -4 0 49.65 1.41 3 4 0 50.65 1.36 3 4 0 50.27 1.44 3 4 0 51.79 1.36 3 4 0 52.77 1.34 3 4 0 49.15 1.43 3 4 0 48.88 1.39 -4 -4 0 2.04 0.23 -4 -4 0 1.91 0.23 -4 -4 0 2.24 0.24 -4 -4 0 2.19 0.23 -4 -4 0 1.55 0.25 -4 -4 0 1.94 0.27 4 4 0 1.75 0.25 4 4 0 1.83 0.25 4 4 0 1.93 0.27 4 4 0 1.88 0.23 4 4 0 1.69 0.23 -5 -4 0 18.87 0.76 -5 -4 0 18.31 0.68 -5 -4 0 17.36 0.74 -5 -4 0 18.50 0.67 -5 -4 0 18.61 0.72 -5 -4 0 18.03 0.69 5 4 0 17.39 0.73 5 4 0 18.71 0.72 5 4 0 18.07 0.73 5 4 0 18.26 0.68 -6 -4 0 61.70 1.90 -6 -4 0 63.10 1.76 -6 -4 0 60.95 1.82 6 4 0 60.71 1.76 6 4 0 61.43 1.82 6 4 0 62.09 1.89 -7 -4 0 12.50 0.71 -7 -4 0 12.10 0.61 -7 -4 0 12.12 0.64 7 4 0 10.99 0.68 7 4 0 12.19 0.67 7 4 0 12.30 0.63 -8 -4 0 45.62 1.55 -8 -4 0 46.09 1.46 -8 -4 0 43.44 1.59 8 4 0 46.98 1.55 8 4 0 44.50 1.47 8 4 0 44.26 1.59 -9 -4 0 19.70 0.98 -9 -4 0 21.20 0.93 -9 -4 0 21.14 1.07 9 4 0 22.54 1.06 9 4 0 20.85 1.00 9 4 0 20.47 0.92 -10 -4 0 0.28 0.37 -10 -4 0 0.48 0.33 -10 -4 0 0.00 0.33 10 4 0 0.59 0.34 10 4 0 0.13 0.36 13 -5 0 6.90 0.62 13 -5 0 7.74 0.64 13 -5 0 7.85 0.66 13 -5 0 6.49 0.58 13 -5 0 7.66 0.62 13 -5 0 5.70 0.50 -13 5 0 6.16 0.55 12 -5 0 1.88 0.30 12 -5 0 2.07 0.35 12 -5 0 1.89 0.33 12 -5 0 1.55 0.34 12 -5 0 1.87 0.36 12 -5 0 1.43 0.33 -12 5 0 1.97 0.31 11 -5 0 0.38 0.25 11 -5 0 0.52 0.30 11 -5 0 1.06 0.28 11 -5 0 0.76 0.25 11 -5 0 1.00 0.26 11 -5 0 0.72 0.21 -11 5 0 0.80 0.22 10 -5 0 -0.07 0.16 10 -5 0 0.08 0.21 10 -5 0 0.09 0.17 10 -5 0 0.24 0.20 10 -5 0 0.33 0.20 10 -5 0 0.27 0.16 -10 5 0 0.03 0.15 9 -5 0 4.30 0.33 9 -5 0 4.88 0.33 9 -5 0 4.53 0.35 9 -5 0 4.51 0.34 9 -5 0 4.48 0.30 9 -5 0 4.52 0.39 -9 5 0 4.44 0.30 -9 5 0 4.10 0.30 8 -5 0 108.83 2.82 8 -5 0 109.25 2.73 8 -5 0 109.56 2.74 8 -5 0 114.00 2.93 8 -5 0 109.41 2.77 8 -5 0 110.65 2.91 -8 5 0 109.67 2.76 -8 5 0 109.86 2.77 -8 5 0 103.79 2.76 7 -5 0 3.61 0.29 7 -5 0 3.66 0.25 7 -5 0 3.22 0.21 7 -5 0 3.30 0.23 7 -5 0 3.67 0.21 7 -5 0 3.40 0.22 7 -5 0 3.01 0.24 -7 5 0 3.97 0.24 -7 5 0 3.52 0.21 -7 5 0 3.41 0.22 -7 5 0 3.58 0.25 -7 5 0 3.81 0.22 6 -5 0 36.48 0.94 6 -5 0 34.79 0.94 6 -5 0 35.55 0.98 6 -5 0 35.36 1.01 6 -5 0 36.78 1.02 6 -5 0 36.56 1.02 6 -5 0 36.54 1.00 6 -5 0 34.77 1.01 -6 5 0 34.95 0.96 -6 5 0 35.18 0.95 -6 5 0 36.98 0.99 -6 5 0 36.75 0.99 -6 5 0 36.44 1.01 -6 5 0 36.64 0.96 5 -5 0 0.97 0.12 5 -5 0 0.68 0.10 5 -5 0 0.74 0.13 5 -5 0 0.74 0.12 5 -5 0 0.74 0.09 5 -5 0 0.94 0.09 5 -5 0 0.79 0.12 5 -5 0 0.61 0.09 5 -5 0 0.62 0.09 -5 5 0 0.71 0.10 -5 5 0 0.64 0.10 -5 5 0 0.86 0.10 -5 5 0 0.60 0.10 4 -5 0 2.50 0.14 4 -5 0 2.43 0.16 4 -5 0 2.44 0.13 4 -5 0 2.47 0.16 4 -5 0 2.43 0.13 4 -5 0 2.35 0.11 4 -5 0 2.18 0.11 4 -5 0 2.44 0.11 4 -5 0 2.47 0.18 -4 5 0 2.46 0.12 -4 5 0 2.55 0.12 -4 5 0 2.51 0.12 -4 5 0 2.38 0.12 3 -5 0 200.78 4.86 3 -5 0 206.07 4.76 3 -5 0 194.42 6.00 3 -5 0 200.00 5.18 3 -5 0 199.82 5.12 3 -5 0 204.22 5.19 3 -5 0 200.43 5.04 3 -5 0 206.94 5.19 -3 5 0 208.22 4.93 -3 5 0 207.93 4.92 -3 5 0 202.85 5.00 -3 5 0 205.50 5.15 2 -5 0 179.01 4.11 2 -5 0 175.80 4.22 2 -5 0 172.84 4.22 2 -5 0 164.72 4.44 2 -5 0 178.76 4.31 2 -5 0 180.91 4.42 2 -5 0 175.32 4.46 2 -5 0 175.76 4.44 -2 5 0 178.13 4.26 -2 5 0 170.55 4.27 -2 5 0 180.29 4.42 -2 5 0 176.82 4.30 1 -5 0 84.15 2.15 1 -5 0 84.90 2.07 1 -5 0 85.83 2.20 1 -5 0 83.68 2.07 1 -5 0 86.27 2.22 1 -5 0 84.42 2.20 1 -5 0 87.60 2.07 -1 5 0 82.29 2.10 -1 5 0 85.97 2.16 -1 5 0 84.92 2.11 -1 5 0 89.03 2.21 -1 5 0 84.53 2.10 0 -5 0 436.87 11.04 0 -5 0 449.97 11.29 0 -5 0 462.96 11.16 0 -5 0 448.45 11.56 0 -5 0 443.39 11.66 0 -5 0 479.85 11.69 0 -5 0 463.54 11.01 0 -5 0 455.46 11.55 0 5 0 469.91 11.43 0 5 0 460.42 11.25 0 5 0 455.15 11.65 0 5 0 434.75 11.07 0 5 0 439.65 11.10 -1 -5 0 149.23 3.53 -1 -5 0 140.78 3.75 -1 -5 0 142.15 3.54 -1 -5 0 139.52 3.66 -1 -5 0 146.85 3.75 -1 -5 0 147.37 3.57 -1 -5 0 141.93 3.77 1 5 0 143.55 3.76 1 5 0 148.60 3.59 1 5 0 145.90 3.57 1 5 0 147.30 3.67 1 5 0 152.72 3.76 1 5 0 142.04 3.58 -2 -5 0 5.41 0.31 -2 -5 0 5.29 0.27 -2 -5 0 6.35 0.32 -2 -5 0 5.59 0.30 -2 -5 0 5.40 0.28 -2 -5 0 6.32 0.33 -2 -5 0 5.23 0.32 2 5 0 5.76 0.28 2 5 0 6.09 0.32 2 5 0 5.30 0.30 2 5 0 5.30 0.31 2 5 0 5.31 0.29 2 5 0 5.71 0.30 -3 -5 0 25.86 0.88 -3 -5 0 26.35 0.81 -3 -5 0 25.02 0.85 -3 -5 0 26.46 0.88 -3 -5 0 26.40 0.80 -3 -5 0 24.98 0.83 3 5 0 26.72 0.79 3 5 0 26.57 0.85 3 5 0 23.80 0.85 3 5 0 24.85 0.86 3 5 0 24.71 0.81 -4 -5 0 13.52 0.55 -4 -5 0 13.21 0.53 -4 -5 0 13.25 0.59 -4 -5 0 13.14 0.60 -4 -5 0 13.61 0.61 -4 -5 0 12.42 0.56 -4 -5 0 12.64 0.57 4 5 0 12.91 0.59 4 5 0 13.09 0.54 4 5 0 12.94 0.57 -5 -5 0 111.57 3.04 -5 -5 0 106.98 2.95 -5 -5 0 107.24 3.05 -5 -5 0 113.92 2.86 -5 -5 0 110.68 2.86 -5 -5 0 103.91 3.05 5 5 0 107.53 2.88 5 5 0 108.91 2.96 5 5 0 109.71 3.04 -6 -5 0 236.38 5.96 -6 -5 0 228.83 5.78 -6 -5 0 220.81 6.12 6 5 0 232.21 5.95 6 5 0 232.25 5.82 6 5 0 231.03 6.12 -7 -5 0 8.49 0.59 -7 -5 0 8.35 0.55 -7 -5 0 8.62 0.63 7 5 0 7.78 0.61 7 5 0 7.94 0.56 7 5 0 7.92 0.55 -8 -5 0 0.51 0.28 -8 -5 0 0.74 0.34 -8 -5 0 0.41 0.32 8 5 0 0.19 0.30 8 5 0 0.45 0.28 8 5 0 0.56 0.33 -9 -5 0 0.17 0.35 -9 -5 0 0.06 0.34 -9 -5 0 -0.01 0.28 9 5 0 0.03 0.34 9 5 0 0.06 0.34 9 5 0 0.31 0.30 13 -6 0 16.02 0.77 13 -6 0 15.90 0.84 13 -6 0 16.83 0.88 13 -6 0 15.84 0.87 13 -6 0 17.53 0.84 13 -6 0 15.69 0.71 -13 6 0 16.76 0.77 12 -6 0 0.22 0.24 12 -6 0 0.77 0.33 12 -6 0 0.26 0.23 12 -6 0 0.44 0.21 12 -6 0 0.37 0.28 12 -6 0 0.01 0.27 -12 6 0 0.17 0.21 11 -6 0 4.84 0.46 11 -6 0 5.08 0.40 11 -6 0 5.45 0.45 11 -6 0 4.51 0.36 11 -6 0 5.42 0.50 11 -6 0 4.62 0.42 -11 6 0 5.68 0.40 10 -6 0 3.76 0.36 10 -6 0 2.89 0.30 10 -6 0 2.90 0.28 10 -6 0 3.23 0.38 10 -6 0 3.12 0.36 10 -6 0 2.77 0.32 -10 6 0 3.09 0.30 -10 6 0 2.50 0.28 9 -6 0 164.94 4.04 9 -6 0 162.59 4.30 9 -6 0 166.24 4.20 9 -6 0 162.35 4.06 9 -6 0 166.66 4.10 9 -6 0 169.66 4.34 -9 6 0 165.16 4.11 -9 6 0 164.16 4.11 8 -6 0 61.74 1.54 8 -6 0 61.80 1.67 8 -6 0 58.48 1.61 8 -6 0 59.20 1.63 8 -6 0 57.02 1.64 8 -6 0 57.92 1.53 8 -6 0 58.32 1.60 -8 6 0 59.37 1.58 -8 6 0 61.07 1.57 -8 6 0 59.82 1.56 7 -6 0 0.10 0.10 7 -6 0 0.05 0.09 7 -6 0 0.56 0.12 7 -6 0 0.24 0.08 7 -6 0 0.36 0.16 7 -6 0 -0.01 0.11 7 -6 0 0.19 0.08 -7 6 0 0.18 0.09 -7 6 0 0.23 0.09 -7 6 0 0.18 0.09 6 -6 0 2.50 0.23 6 -6 0 2.53 0.14 6 -6 0 2.39 0.17 6 -6 0 2.17 0.16 6 -6 0 2.61 0.23 6 -6 0 2.20 0.15 6 -6 0 2.24 0.14 6 -6 0 2.09 0.17 6 -6 0 2.26 0.18 -6 6 0 2.41 0.16 -6 6 0 2.46 0.16 -6 6 0 2.28 0.15 -6 6 0 2.31 0.15 5 -6 0 60.64 1.55 5 -6 0 59.92 1.58 5 -6 0 59.55 1.47 5 -6 0 60.03 1.59 5 -6 0 59.46 1.47 5 -6 0 60.42 1.62 5 -6 0 61.75 1.56 5 -6 0 60.95 1.59 5 -6 0 60.31 1.53 -5 6 0 59.09 1.52 -5 6 0 62.36 1.57 -5 6 0 61.64 1.51 -5 6 0 59.76 1.51 4 -6 0 13.37 0.45 4 -6 0 13.07 0.41 4 -6 0 12.94 0.40 4 -6 0 13.36 0.41 4 -6 0 13.28 0.36 4 -6 0 13.50 0.45 4 -6 0 13.07 0.35 4 -6 0 13.49 0.38 4 -6 0 13.12 0.45 -4 6 0 13.78 0.38 -4 6 0 13.48 0.39 -4 6 0 13.18 0.39 -4 6 0 12.94 0.38 3 -6 0 903.26 22.85 3 -6 0 926.79 22.96 3 -6 0 895.42 21.50 3 -6 0 898.94 22.83 3 -6 0 911.70 21.15 3 -6 0 891.93 23.04 3 -6 0 898.23 22.25 3 -6 0 924.66 21.40 3 -6 0 876.90 21.48 -3 6 0 926.92 21.90 -3 6 0 891.95 21.90 -3 6 0 917.32 22.79 -3 6 0 913.28 21.85 2 -6 0 441.95 11.29 2 -6 0 447.62 11.01 2 -6 0 429.69 11.37 2 -6 0 452.48 11.32 2 -6 0 448.05 10.72 2 -6 0 445.78 10.67 2 -6 0 442.29 11.40 2 -6 0 439.65 10.56 2 -6 0 437.27 11.41 -2 6 0 443.77 10.83 -2 6 0 445.84 10.90 -2 6 0 453.96 11.34 -2 6 0 439.53 10.74 1 -6 0 0.33 0.10 1 -6 0 0.26 0.08 1 -6 0 0.25 0.07 1 -6 0 0.21 0.07 1 -6 0 0.58 0.08 1 -6 0 0.51 0.09 1 -6 0 0.38 0.09 -1 6 0 0.49 0.09 -1 6 0 0.42 0.08 -1 6 0 0.25 0.08 -1 6 0 0.51 0.09 -1 6 0 0.42 0.10 0 -6 0 5.07 0.21 0 -6 0 4.44 0.24 0 -6 0 4.46 0.24 0 -6 0 4.30 0.22 0 -6 0 4.31 0.21 0 -6 0 4.54 0.25 0 -6 0 4.58 0.26 0 6 0 4.07 0.24 0 6 0 4.38 0.23 0 6 0 4.06 0.23 0 6 0 4.57 0.23 0 6 0 4.78 0.25 -1 -6 0 2.73 0.21 -1 -6 0 2.34 0.19 -1 -6 0 2.02 0.21 -1 -6 0 1.69 0.21 -1 -6 0 2.11 0.18 -1 -6 0 1.90 0.19 1 6 0 1.94 0.19 1 6 0 1.92 0.20 1 6 0 1.86 0.18 1 6 0 1.75 0.21 1 6 0 1.75 0.17 1 6 0 2.00 0.21 -2 -6 0 86.47 2.45 -2 -6 0 93.08 2.44 -2 -6 0 91.83 2.29 -2 -6 0 85.23 2.36 -2 -6 0 88.36 2.29 2 6 0 91.80 2.39 2 6 0 90.43 2.29 2 6 0 88.60 2.32 2 6 0 86.81 2.44 -3 -6 0 98.29 2.53 -3 -6 0 99.78 2.53 -3 -6 0 97.12 2.70 -3 -6 0 95.57 2.62 -3 -6 0 99.65 2.72 -3 -6 0 96.62 2.68 3 6 0 96.43 2.69 3 6 0 100.36 2.63 3 6 0 94.77 2.55 -4 -6 0 15.24 0.61 -4 -6 0 15.22 0.70 -4 -6 0 15.08 0.66 -4 -6 0 15.15 0.63 -4 -6 0 15.75 0.69 -4 -6 0 15.95 0.71 4 6 0 14.96 0.63 4 6 0 15.46 0.67 4 6 0 14.36 0.68 -5 -6 0 13.99 0.68 -5 -6 0 14.21 0.62 -5 -6 0 15.23 0.73 -5 -6 0 13.61 0.69 -5 -6 0 14.17 0.72 -5 -6 0 13.36 0.63 5 6 0 13.68 0.67 5 6 0 14.03 0.69 5 6 0 13.48 0.64 -6 -6 0 12.39 0.63 -6 -6 0 12.88 0.68 -6 -6 0 12.31 0.73 6 6 0 12.13 0.68 6 6 0 12.86 0.71 6 6 0 11.76 0.64 -7 -6 0 1.36 0.30 -7 -6 0 1.24 0.36 -7 -6 0 1.48 0.37 7 6 0 1.16 0.30 7 6 0 1.46 0.36 7 6 0 1.28 0.36 -8 -6 0 0.04 0.32 -8 -6 0 -0.02 0.32 -8 -6 0 0.46 0.30 8 6 0 -0.10 0.30 8 6 0 -0.25 0.27 8 6 0 0.03 0.31 -9 -6 0 6.20 0.70 9 6 0 5.06 0.62 9 6 0 5.69 0.73 9 6 0 6.24 0.71 13 -7 0 6.36 0.51 13 -7 0 6.86 0.61 13 -7 0 5.44 0.60 13 -7 0 5.92 0.53 13 -7 0 6.90 0.45 13 -7 0 7.24 0.61 -13 7 0 6.52 0.51 12 -7 0 22.25 0.94 12 -7 0 22.31 0.89 12 -7 0 21.07 0.77 12 -7 0 22.14 0.84 12 -7 0 22.24 0.93 12 -7 0 22.68 0.93 -12 7 0 21.29 0.82 11 -7 0 56.82 1.60 11 -7 0 54.72 1.65 11 -7 0 56.72 1.67 11 -7 0 57.71 1.70 11 -7 0 52.59 1.50 11 -7 0 53.17 1.67 -11 7 0 54.44 1.56 10 -7 0 -0.06 0.15 10 -7 0 0.29 0.18 10 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3.10 5 -7 0 119.96 2.94 5 -7 0 116.22 3.06 -5 7 0 123.15 3.05 -5 7 0 122.45 2.95 -5 7 0 117.99 2.95 -5 7 0 117.66 2.94 4 -7 0 0.83 0.11 4 -7 0 0.96 0.08 4 -7 0 1.26 0.14 4 -7 0 1.11 0.15 4 -7 0 0.72 0.11 4 -7 0 0.99 0.16 4 -7 0 1.03 0.10 4 -7 0 1.28 0.09 4 -7 0 0.93 0.15 -4 7 0 0.96 0.09 -4 7 0 0.97 0.11 -4 7 0 0.87 0.11 -4 7 0 1.07 0.11 -4 7 0 0.75 0.11 3 -7 0 230.37 5.36 3 -7 0 227.16 5.69 3 -7 0 231.16 5.54 3 -7 0 227.42 5.30 3 -7 0 229.46 5.73 3 -7 0 216.91 5.74 3 -7 0 226.49 5.74 3 -7 0 220.25 5.42 -3 7 0 226.08 5.46 -3 7 0 229.46 5.68 -3 7 0 224.35 5.45 -3 7 0 224.19 5.45 2 -7 0 116.96 3.00 2 -7 0 114.74 2.78 2 -7 0 113.27 3.01 2 -7 0 114.02 2.78 2 -7 0 113.22 2.96 2 -7 0 114.84 2.99 2 -7 0 117.99 2.97 2 -7 0 114.24 2.89 -2 7 0 117.44 2.96 -2 7 0 117.48 2.91 -2 7 0 112.94 2.84 -2 7 0 116.14 2.84 -2 7 0 113.25 2.84 1 -7 0 0.54 0.09 1 -7 0 0.47 0.11 1 -7 0 0.57 0.12 1 -7 0 0.45 0.09 1 -7 0 0.70 0.09 1 -7 0 0.59 0.11 1 -7 0 0.62 0.12 -1 7 0 0.55 0.10 -1 7 0 0.46 0.10 -1 7 0 0.57 0.11 -1 7 0 0.68 0.11 -1 7 0 0.61 0.12 0 -7 0 81.67 2.08 0 -7 0 79.76 2.23 0 -7 0 83.82 2.22 0 -7 0 84.03 2.07 0 -7 0 78.64 2.21 0 -7 0 80.60 2.16 0 -7 0 84.19 2.07 0 7 0 84.01 2.12 0 7 0 81.85 2.12 0 7 0 81.53 2.22 0 7 0 83.14 2.10 0 7 0 84.46 2.17 -1 -7 0 66.72 1.84 -1 -7 0 63.79 1.86 -1 -7 0 68.11 1.72 -1 -7 0 65.29 1.79 -1 -7 0 63.55 1.72 -1 -7 0 65.64 1.71 1 7 0 65.16 1.84 1 7 0 62.49 1.75 1 7 0 66.97 1.81 1 7 0 69.36 1.74 1 7 0 65.00 1.76 -2 -7 0 76.89 2.21 -2 -7 0 76.12 2.12 -2 -7 0 78.94 2.04 -2 -7 0 78.43 2.05 -2 -7 0 74.98 2.18 2 7 0 78.73 2.08 2 7 0 77.04 2.18 2 7 0 78.17 2.14 2 7 0 80.41 2.05 -3 -7 0 191.33 4.97 -3 -7 0 193.79 5.09 -3 -7 0 195.16 4.83 -3 -7 0 192.01 5.13 -3 -7 0 192.40 4.80 3 7 0 196.88 4.98 3 7 0 188.64 4.86 3 7 0 196.16 5.11 -4 -7 0 34.26 1.17 -4 -7 0 33.77 1.06 -4 -7 0 31.97 1.12 -4 -7 0 32.93 1.08 -4 -7 0 30.28 1.16 4 7 0 32.77 1.09 4 7 0 32.85 1.12 4 7 0 33.27 1.16 -5 -7 0 1.30 0.25 -5 -7 0 0.91 0.30 -5 -7 0 1.05 0.28 -5 -7 0 1.25 0.31 5 7 0 1.19 0.28 5 7 0 1.39 0.30 5 7 0 1.03 0.28 -6 -7 0 3.49 0.49 -6 -7 0 3.12 0.40 -6 -7 0 3.02 0.52 6 7 0 2.91 0.46 6 7 0 3.59 0.44 6 7 0 3.63 0.51 -7 -7 0 0.28 0.32 -7 -7 0 0.40 0.34 7 7 0 -0.14 0.29 7 7 0 0.18 0.30 7 7 0 0.08 0.28 -8 -7 0 43.34 1.66 -8 -7 0 45.26 1.75 8 7 0 45.10 1.71 8 7 0 43.93 1.66 8 7 0 46.60 1.60 13 -8 0 1.12 0.32 13 -8 0 1.10 0.22 13 -8 0 0.77 0.27 13 -8 0 0.94 0.35 13 -8 0 0.90 0.27 13 -8 0 0.68 0.36 -13 8 0 0.76 0.25 12 -8 0 36.61 1.30 12 -8 0 40.13 1.32 12 -8 0 37.51 1.11 12 -8 0 37.94 1.27 12 -8 0 40.12 1.37 12 -8 0 38.37 1.20 -12 8 0 37.66 1.19 11 -8 0 48.38 1.54 11 -8 0 49.38 1.36 11 -8 0 47.81 1.51 11 -8 0 54.56 1.58 11 -8 0 50.30 1.58 11 -8 0 53.71 1.47 -11 8 0 51.55 1.44 -11 8 0 48.48 1.45 10 -8 0 21.71 0.84 10 -8 0 23.81 0.75 10 -8 0 21.96 0.78 10 -8 0 21.96 0.68 10 -8 0 24.14 0.83 10 -8 0 21.07 0.85 -10 8 0 23.77 0.75 -10 8 0 22.76 0.76 9 -8 0 0.32 0.13 9 -8 0 0.02 0.20 9 -8 0 0.51 0.16 9 -8 0 0.17 0.20 9 -8 0 0.15 0.13 9 -8 0 0.25 0.10 9 -8 0 0.31 0.10 -9 8 0 0.30 0.13 -9 8 0 0.26 0.13 -9 8 0 0.24 0.12 8 -8 0 11.37 0.46 8 -8 0 11.89 0.41 8 -8 0 12.05 0.37 8 -8 0 12.24 0.46 8 -8 0 11.20 0.52 8 -8 0 12.15 0.53 8 -8 0 11.34 0.36 8 -8 0 11.92 0.44 -8 8 0 11.84 0.42 -8 8 0 11.81 0.42 -8 8 0 11.56 0.43 7 -8 0 5.27 0.20 7 -8 0 5.16 0.25 7 -8 0 5.55 0.30 7 -8 0 5.33 0.28 7 -8 0 5.04 0.34 7 -8 0 5.35 0.34 7 -8 0 5.39 0.23 7 -8 0 5.90 0.29 7 -8 0 5.30 0.19 -7 8 0 5.57 0.24 -7 8 0 4.94 0.25 -7 8 0 5.04 0.25 6 -8 0 126.55 3.10 6 -8 0 127.76 3.23 6 -8 0 122.47 3.26 6 -8 0 123.84 3.19 6 -8 0 126.34 3.08 6 -8 0 120.13 3.08 6 -8 0 126.80 3.22 -6 8 0 126.31 3.07 -6 8 0 122.64 3.08 -6 8 0 128.99 3.07 5 -8 0 218.90 5.61 5 -8 0 230.89 5.50 5 -8 0 221.20 5.28 5 -8 0 218.63 5.29 5 -8 0 217.21 5.30 5 -8 0 228.41 5.64 5 -8 0 230.87 5.67 5 -8 0 222.20 5.69 -5 8 0 232.09 5.41 -5 8 0 221.39 5.39 -5 8 0 218.03 5.40 4 -8 0 2.80 0.18 4 -8 0 2.59 0.23 4 -8 0 2.67 0.19 4 -8 0 2.61 0.23 4 -8 0 2.27 0.21 4 -8 0 2.45 0.17 4 -8 0 2.87 0.15 4 -8 0 2.73 0.12 4 -8 0 2.43 0.12 -4 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110.41 2.80 -2 -8 0 16.03 0.59 -2 -8 0 16.18 0.59 -2 -8 0 15.76 0.66 -2 -8 0 14.90 0.69 -2 -8 0 16.57 0.69 -2 -8 0 16.57 0.63 2 8 0 15.14 0.67 2 8 0 16.53 0.67 2 8 0 16.06 0.63 -3 -8 0 46.98 1.45 -3 -8 0 48.16 1.41 -3 -8 0 48.85 1.40 -3 -8 0 44.78 1.50 -3 -8 0 46.16 1.49 3 8 0 47.73 1.49 3 8 0 44.56 1.45 3 8 0 44.70 1.40 -4 -8 0 0.14 0.23 -4 -8 0 0.10 0.21 -4 -8 0 0.05 0.23 -4 -8 0 0.34 0.23 4 8 0 0.23 0.21 4 8 0 0.25 0.21 4 8 0 0.18 0.22 -5 -8 0 4.67 0.50 -5 -8 0 4.46 0.51 -5 -8 0 4.15 0.52 5 8 0 4.84 0.47 5 8 0 5.14 0.52 5 8 0 5.55 0.54 -6 -8 0 25.19 1.11 -6 -8 0 26.82 1.18 6 8 0 26.85 1.13 6 8 0 27.48 1.08 6 8 0 24.35 1.23 -7 -8 0 0.18 0.35 -7 -8 0 0.45 0.37 7 8 0 0.25 0.32 7 8 0 0.50 0.36 13 -9 0 1.40 0.38 13 -9 0 2.18 0.27 13 -9 0 1.81 0.35 13 -9 0 0.87 0.37 13 -9 0 1.85 0.30 -13 9 0 1.96 0.31 12 -9 0 6.07 0.56 12 -9 0 6.08 0.49 12 -9 0 5.47 0.31 12 -9 0 5.84 0.45 12 -9 0 5.60 0.53 12 -9 0 5.13 0.38 -12 9 0 5.68 0.42 11 -9 0 2.10 0.30 11 -9 0 2.48 0.35 11 -9 0 2.04 0.32 11 -9 0 2.18 0.21 11 -9 0 2.19 0.28 11 -9 0 1.83 0.33 -11 9 0 2.21 0.30 -11 9 0 2.25 0.29 10 -9 0 3.39 0.32 10 -9 0 2.18 0.27 10 -9 0 2.34 0.19 10 -9 0 3.01 0.20 10 -9 0 2.37 0.24 10 -9 0 2.57 0.40 10 -9 0 2.64 0.38 -10 9 0 2.17 0.26 -10 9 0 2.19 0.27 9 -9 0 42.29 1.33 9 -9 0 43.70 1.26 9 -9 0 43.32 1.10 9 -9 0 44.62 1.10 9 -9 0 46.19 1.30 9 -9 0 43.90 1.19 9 -9 0 43.92 1.33 -9 9 0 43.72 1.20 -9 9 0 44.34 1.23 -9 9 0 43.58 1.21 8 -9 0 52.95 1.51 8 -9 0 53.33 1.51 8 -9 0 56.10 1.49 8 -9 0 51.21 1.45 8 -9 0 50.77 1.49 8 -9 0 54.23 1.39 -8 9 0 52.98 1.42 -8 9 0 54.23 1.40 -8 9 0 52.50 1.40 7 -9 0 4.14 0.19 7 -9 0 4.22 0.31 7 -9 0 4.34 0.29 7 -9 0 3.96 0.31 7 -9 0 4.06 0.25 7 -9 0 3.91 0.22 -7 9 0 4.19 0.24 -7 9 0 3.94 0.22 -7 9 0 4.03 0.22 6 -9 0 97.84 2.50 6 -9 0 99.13 2.65 6 -9 0 100.36 2.58 6 -9 0 102.52 2.60 6 -9 0 98.52 2.56 6 -9 0 95.99 2.51 6 -9 0 100.84 2.47 -6 9 0 99.47 2.47 -6 9 0 97.11 2.48 -6 9 0 102.12 2.48 5 -9 0 44.95 1.32 5 -9 0 45.17 1.25 5 -9 0 45.42 1.24 5 -9 0 45.07 1.22 5 -9 0 45.29 1.25 5 -9 0 45.45 1.24 5 -9 0 45.16 1.16 -5 9 0 44.59 1.19 -5 9 0 45.48 1.19 -5 9 0 45.31 1.19 4 -9 0 6.93 0.22 4 -9 0 7.05 0.30 4 -9 0 7.56 0.38 4 -9 0 6.84 0.29 4 -9 0 6.92 0.32 4 -9 0 6.99 0.26 4 -9 0 6.73 0.33 4 -9 0 6.98 0.23 -4 9 0 7.10 0.29 -4 9 0 7.02 0.29 -4 9 0 6.87 0.29 3 -9 0 19.55 0.57 3 -9 0 22.16 0.69 3 -9 0 21.19 0.62 3 -9 0 19.61 0.72 3 -9 0 21.29 0.58 3 -9 0 20.96 0.66 3 -9 0 20.35 0.65 -3 9 0 21.26 0.64 -3 9 0 20.48 0.64 -3 9 0 21.01 0.63 2 -9 0 31.38 0.97 2 -9 0 31.37 0.90 2 -9 0 28.83 0.93 2 -9 0 31.45 0.85 2 -9 0 30.88 0.99 2 -9 0 30.96 0.85 2 -9 0 31.32 0.96 -2 9 0 31.02 0.89 -2 9 0 30.97 0.90 -2 9 0 30.90 0.90 1 -9 0 0.95 0.15 1 -9 0 1.05 0.18 1 -9 0 1.05 0.19 1 -9 0 0.77 0.14 1 -9 0 0.85 0.17 -1 9 0 0.93 0.16 -1 9 0 1.36 0.21 -1 9 0 0.73 0.15 0 -9 0 123.59 3.23 0 -9 0 121.99 3.32 0 -9 0 123.53 3.36 0 -9 0 126.77 3.12 0 9 0 123.94 3.18 0 9 0 126.07 3.16 -1 -9 0 99.09 2.68 -1 -9 0 95.63 2.59 -1 -9 0 95.80 2.49 -1 -9 0 94.08 2.69 1 9 0 97.47 2.52 1 9 0 94.64 2.55 -2 -9 0 14.71 0.61 -2 -9 0 14.22 0.67 -2 -9 0 12.88 0.66 -2 -9 0 13.97 0.63 2 9 0 13.43 0.62 -3 -9 0 12.45 0.66 -3 -9 0 12.42 0.70 -3 -9 0 12.96 0.62 -3 -9 0 13.31 0.69 3 9 0 13.20 0.64 3 9 0 14.92 0.69 -4 -9 0 2.20 0.37 -4 -9 0 2.24 0.36 -4 -9 0 2.67 0.41 -4 -9 0 2.10 0.35 4 9 0 2.84 0.43 4 9 0 2.94 0.41 -5 -9 0 18.69 0.97 -5 -9 0 18.72 0.98 -5 -9 0 19.69 0.93 5 9 0 19.81 0.90 5 9 0 20.36 0.95 -6 -9 0 86.15 2.73 -6 -9 0 80.91 2.58 6 9 0 86.89 2.53 6 9 0 84.92 2.60 13 -10 0 14.91 0.69 13 -10 0 16.30 0.78 13 -10 0 15.28 0.87 13 -10 0 13.51 0.81 -13 10 0 14.72 0.67 12 -10 0 14.80 0.81 12 -10 0 14.35 0.75 12 -10 0 14.53 0.65 12 -10 0 15.82 0.71 -12 10 0 16.17 0.67 -12 10 0 14.47 0.62 11 -10 0 24.16 0.83 11 -10 0 22.42 0.95 11 -10 0 25.81 0.88 11 -10 0 22.80 0.95 -11 10 0 23.75 0.83 -11 10 0 24.65 0.80 10 -10 0 2.17 0.30 10 -10 0 1.28 0.27 10 -10 0 2.12 0.26 10 -10 0 1.60 0.30 -10 10 0 2.37 0.28 -10 10 0 1.88 0.25 9 -10 0 43.41 1.37 9 -10 0 46.83 1.37 9 -10 0 47.57 1.42 9 -10 0 44.13 1.30 9 -10 0 48.97 1.35 -9 10 0 46.48 1.29 -9 10 0 46.05 1.26 -9 10 0 47.26 1.26 8 -10 0 86.13 2.31 8 -10 0 89.99 2.34 8 -10 0 85.36 2.30 8 -10 0 89.62 2.40 8 -10 0 90.83 2.35 -8 10 0 86.88 2.22 -8 10 0 87.04 2.25 -8 10 0 87.72 2.23 7 -10 0 8.99 0.46 7 -10 0 9.04 0.47 7 -10 0 9.67 0.39 7 -10 0 9.20 0.44 7 -10 0 9.08 0.35 7 -10 0 9.07 0.30 -7 10 0 8.56 0.36 -7 10 0 9.88 0.36 -7 10 0 10.03 0.36 6 -10 0 0.18 0.09 6 -10 0 0.18 0.16 6 -10 0 0.19 0.16 6 -10 0 0.11 0.10 6 -10 0 0.06 0.11 6 -10 0 0.04 0.15 6 -10 0 0.08 0.07 -6 10 0 0.47 0.11 -6 10 0 0.17 0.10 -6 10 0 0.21 0.10 5 -10 0 11.34 0.35 5 -10 0 10.92 0.42 5 -10 0 10.83 0.41 5 -10 0 10.80 0.50 5 -10 0 10.89 0.45 5 -10 0 10.49 0.39 -5 10 0 10.62 0.40 -5 10 0 10.13 0.39 -5 10 0 10.46 0.39 4 -10 0 1.93 0.20 4 -10 0 2.24 0.14 4 -10 0 2.15 0.23 4 -10 0 1.92 0.28 4 -10 0 2.07 0.13 4 -10 0 2.18 0.17 4 -10 0 1.77 0.23 -4 10 0 2.16 0.20 -4 10 0 2.00 0.20 -4 10 0 1.95 0.19 3 -10 0 102.62 2.79 3 -10 0 107.35 2.71 3 -10 0 109.51 2.84 3 -10 0 106.26 2.59 3 -10 0 103.19 2.59 3 -10 0 107.80 2.88 -3 10 0 107.47 2.68 -3 10 0 106.03 2.69 -3 10 0 106.05 2.69 2 -10 0 235.98 5.95 2 -10 0 230.57 6.15 2 -10 0 240.07 6.16 2 -10 0 237.91 6.11 2 -10 0 241.85 5.72 2 -10 0 242.94 6.17 2 -10 0 234.08 5.73 -2 10 0 249.19 5.85 -2 10 0 237.04 5.87 -2 10 0 239.06 5.86 1 -10 0 3.65 0.32 1 -10 0 4.09 0.34 1 -10 0 3.76 0.28 1 -10 0 4.01 0.31 1 -10 0 4.03 0.34 -1 10 0 4.74 0.32 -1 10 0 4.33 0.30 0 -10 0 2.73 0.28 0 -10 0 2.96 0.35 0 -10 0 2.65 0.31 0 -10 0 2.53 0.32 0 10 0 2.75 0.28 0 10 0 2.90 0.31 -1 -10 0 0.25 0.19 -1 -10 0 0.06 0.18 -1 -10 0 0.27 0.21 -1 -10 0 0.57 0.18 1 10 0 0.05 0.16 -2 -10 0 8.80 0.53 -2 -10 0 9.83 0.60 -2 -10 0 9.47 0.52 -2 -10 0 8.88 0.57 2 10 0 8.85 0.53 -3 -10 0 35.06 1.29 -3 -10 0 38.43 1.37 -3 -10 0 38.18 1.25 -3 -10 0 37.75 1.39 3 10 0 39.51 1.29 -4 -10 0 7.94 0.67 -4 -10 0 9.09 0.62 -4 -10 0 8.70 0.64 -4 -10 0 9.29 0.67 4 10 0 8.51 0.61 -5 -10 0 40.26 1.58 -5 -10 0 39.59 1.49 5 10 0 41.60 1.47 -6 -10 0 53.57 1.89 13 -11 0 1.71 0.42 13 -11 0 1.79 0.43 13 -11 0 2.43 0.35 -13 11 0 2.01 0.29 12 -11 0 13.41 0.77 12 -11 0 12.49 0.57 12 -11 0 13.64 0.76 12 -11 0 13.06 0.64 -12 11 0 12.46 0.57 -12 11 0 11.89 0.59 11 -11 0 26.02 1.04 11 -11 0 29.33 0.95 11 -11 0 24.83 1.04 11 -11 0 27.60 0.89 -11 11 0 26.54 0.86 -11 11 0 27.39 0.91 10 -11 0 0.26 0.26 10 -11 0 0.69 0.16 10 -11 0 0.42 0.27 10 -11 0 0.84 0.20 -10 11 0 0.64 0.17 -10 11 0 0.69 0.18 9 -11 0 67.66 1.87 9 -11 0 63.88 1.85 9 -11 0 69.52 1.83 9 -11 0 64.42 1.76 9 -11 0 64.13 1.85 -9 11 0 65.47 1.72 -9 11 0 64.97 1.75 -9 11 0 63.63 1.72 8 -11 0 64.63 1.84 8 -11 0 62.81 1.79 8 -11 0 62.70 1.79 8 -11 0 67.82 1.77 8 -11 0 62.59 1.71 -8 11 0 64.20 1.67 -8 11 0 65.02 1.68 -8 11 0 62.72 1.69 7 -11 0 2.01 0.19 7 -11 0 2.49 0.24 7 -11 0 2.26 0.32 7 -11 0 2.50 0.30 7 -11 0 2.53 0.32 -7 11 0 2.11 0.22 -7 11 0 2.37 0.22 -7 11 0 2.50 0.22 6 -11 0 14.58 0.58 6 -11 0 14.29 0.48 6 -11 0 14.86 0.61 6 -11 0 14.78 0.52 -6 11 0 14.08 0.49 -6 11 0 13.77 0.50 -6 11 0 13.61 0.49 5 -11 0 47.88 1.43 5 -11 0 46.72 1.31 5 -11 0 48.43 1.35 5 -11 0 47.45 1.22 5 -11 0 44.70 1.29 -5 11 0 46.56 1.27 -5 11 0 46.58 1.28 -5 11 0 46.97 1.27 4 -11 0 14.82 0.48 4 -11 0 14.58 0.42 4 -11 0 14.43 0.64 4 -11 0 15.23 0.58 4 -11 0 14.72 0.53 4 -11 0 14.59 0.42 -4 11 0 14.19 0.52 -4 11 0 14.78 0.53 -4 11 0 15.11 0.53 3 -11 0 141.07 3.75 3 -11 0 145.04 3.47 3 -11 0 147.26 3.64 3 -11 0 143.69 3.84 3 -11 0 140.62 3.48 3 -11 0 144.54 3.80 -3 11 0 146.31 3.60 -3 11 0 141.37 3.61 -3 11 0 143.35 3.61 2 -11 0 28.54 0.99 2 -11 0 28.92 0.83 2 -11 0 27.78 0.97 2 -11 0 27.47 0.88 2 -11 0 29.11 0.94 2 -11 0 28.22 0.96 -2 11 0 29.17 0.89 -2 11 0 27.87 0.90 1 -11 0 7.53 0.38 1 -11 0 7.51 0.49 1 -11 0 7.37 0.47 1 -11 0 7.70 0.45 -1 11 0 8.33 0.42 -1 11 0 7.45 0.43 0 -11 0 30.61 1.10 0 -11 0 31.37 1.10 0 -11 0 30.42 1.03 0 -11 0 29.45 0.96 0 -11 0 30.24 1.07 0 11 0 31.93 1.03 -1 -11 0 42.03 1.42 -1 -11 0 40.62 1.38 -1 -11 0 42.16 1.26 -1 -11 0 41.82 1.33 1 11 0 39.31 1.31 -2 -11 0 8.62 0.61 -2 -11 0 8.35 0.52 -2 -11 0 8.42 0.58 -2 -11 0 9.00 0.63 2 11 0 8.56 0.57 -3 -11 0 105.01 3.09 -3 -11 0 106.34 2.83 -3 -11 0 106.37 3.05 -3 -11 0 95.86 2.91 3 11 0 101.59 2.88 -4 -11 0 30.92 1.25 -4 -11 0 31.99 1.21 -4 -11 0 32.41 1.36 -4 -11 0 32.82 1.34 4 11 0 32.14 1.24 -5 -11 0 0.39 0.35 13 -12 0 0.56 0.38 13 -12 0 0.25 0.20 13 -12 0 0.06 0.30 -13 12 0 0.23 0.22 12 -12 0 24.05 1.07 12 -12 0 24.45 1.05 12 -12 0 27.10 0.86 -12 12 0 24.33 0.89 11 -12 0 56.92 1.59 11 -12 0 56.30 1.77 11 -12 0 56.68 1.76 -11 12 0 57.12 1.61 10 -12 0 5.68 0.52 10 -12 0 5.42 0.51 10 -12 0 5.65 0.31 -10 12 0 5.41 0.36 9 -12 0 0.64 0.19 9 -12 0 0.77 0.15 9 -12 0 1.15 0.24 9 -12 0 1.04 0.26 9 -12 0 0.79 0.27 -9 12 0 0.83 0.16 -9 12 0 0.85 0.17 8 -12 0 15.36 0.66 8 -12 0 15.82 0.58 8 -12 0 16.04 0.69 8 -12 0 15.21 0.51 8 -12 0 14.93 0.66 -8 12 0 15.47 0.56 -8 12 0 15.10 0.53 7 -12 0 0.24 0.15 7 -12 0 0.41 0.12 7 -12 0 0.41 0.20 7 -12 0 0.40 0.20 7 -12 0 0.51 0.21 -7 12 0 0.32 0.13 -7 12 0 0.19 0.13 -7 12 0 0.29 0.14 6 -12 0 21.20 0.83 6 -12 0 20.53 0.76 6 -12 0 23.39 0.74 6 -12 0 21.00 0.67 -6 12 0 22.07 0.70 -6 12 0 21.26 0.70 -6 12 0 21.75 0.69 5 -12 0 29.05 1.04 5 -12 0 30.62 0.92 5 -12 0 32.50 0.98 5 -12 0 30.26 0.95 -5 12 0 29.71 0.91 -5 12 0 29.98 0.92 -5 12 0 32.18 0.93 4 -12 0 5.42 0.28 4 -12 0 4.67 0.39 4 -12 0 5.21 0.21 4 -12 0 4.71 0.21 4 -12 0 5.02 0.32 4 -12 0 5.20 0.37 -4 12 0 5.29 0.33 -4 12 0 4.90 0.32 -4 12 0 4.95 0.33 3 -12 0 1.00 0.14 3 -12 0 1.35 0.27 3 -12 0 1.06 0.14 3 -12 0 1.09 0.23 3 -12 0 1.16 0.18 3 -12 0 0.94 0.19 -3 12 0 0.80 0.19 -3 12 0 1.10 0.18 2 -12 0 0.13 0.19 2 -12 0 0.21 0.19 2 -12 0 0.10 0.16 2 -12 0 0.08 0.19 2 -12 0 0.08 0.16 2 -12 0 -0.04 0.12 -2 12 0 0.17 0.14 -2 12 0 0.16 0.17 1 -12 0 0.75 0.18 1 -12 0 0.55 0.21 1 -12 0 0.46 0.23 1 -12 0 0.48 0.25 1 -12 0 0.52 0.20 1 -12 0 0.74 0.25 -1 12 0 0.59 0.21 0 -12 0 58.96 1.67 0 -12 0 61.27 1.88 0 -12 0 60.68 1.76 0 -12 0 58.05 1.85 0 -12 0 59.40 1.83 0 12 0 60.03 1.76 -1 -12 0 43.12 1.46 -1 -12 0 42.24 1.38 -1 -12 0 42.04 1.30 -1 -12 0 43.92 1.49 -1 -12 0 38.81 1.41 1 12 0 41.27 1.37 -2 -12 0 5.59 0.56 -2 -12 0 6.20 0.62 -2 -12 0 5.79 0.59 -2 -12 0 6.05 0.56 -2 -12 0 5.89 0.51 2 12 0 5.10 0.51 -3 -12 0 33.73 1.24 -3 -12 0 34.88 1.32 -3 -12 0 35.52 1.43 -3 -12 0 34.24 1.31 -3 -12 0 35.40 1.39 3 12 0 36.10 1.31 -4 -12 0 9.30 0.78 -4 -12 0 8.48 0.66 -4 -12 0 9.18 0.71 -4 -12 0 7.34 0.70 13 -13 0 7.26 0.65 13 -13 0 6.11 0.66 12 -13 0 9.98 0.46 12 -13 0 10.53 0.74 12 -13 0 9.87 0.71 -12 13 0 10.93 0.55 11 -13 0 11.91 0.72 11 -13 0 12.77 0.75 11 -13 0 12.13 0.48 -11 13 0 12.96 0.57 10 -13 0 2.18 0.37 10 -13 0 2.96 0.40 10 -13 0 2.55 0.23 -10 13 0 2.28 0.29 -10 13 0 2.67 0.30 9 -13 0 10.15 0.40 9 -13 0 11.32 0.63 9 -13 0 10.09 0.61 9 -13 0 10.41 0.58 -9 13 0 10.96 0.45 -9 13 0 10.43 0.47 8 -13 0 25.28 0.92 8 -13 0 23.84 0.90 8 -13 0 24.88 0.73 8 -13 0 25.30 0.93 -8 13 0 25.28 0.80 -8 13 0 23.24 0.76 7 -13 0 0.09 0.23 7 -13 0 0.25 0.16 7 -13 0 0.10 0.12 7 -13 0 0.23 0.22 -7 13 0 0.16 0.13 -7 13 0 -0.04 0.13 6 -13 0 105.26 2.71 6 -13 0 97.34 2.80 6 -13 0 97.71 2.62 6 -13 0 100.66 2.59 -6 13 0 96.40 2.57 -6 13 0 98.28 2.57 -6 13 0 104.83 2.59 5 -13 0 65.92 1.87 5 -13 0 69.43 1.95 5 -13 0 68.51 2.04 -5 13 0 70.50 1.85 -5 13 0 68.74 1.85 4 -13 0 1.08 0.14 4 -13 0 1.41 0.21 4 -13 0 1.48 0.26 4 -13 0 1.31 0.14 4 -13 0 1.24 0.27 4 -13 0 1.14 0.20 -4 13 0 1.52 0.23 -4 13 0 1.41 0.20 3 -13 0 16.84 0.72 3 -13 0 16.42 0.61 3 -13 0 16.53 0.77 3 -13 0 15.92 0.66 3 -13 0 16.08 0.53 -3 13 0 17.64 0.67 -3 13 0 17.36 0.65 2 -13 0 30.99 1.04 2 -13 0 29.60 0.96 2 -13 0 28.75 1.09 2 -13 0 28.32 1.07 2 -13 0 28.37 0.88 -2 13 0 28.45 0.99 -2 13 0 31.65 0.99 1 -13 0 4.71 0.42 1 -13 0 5.57 0.46 1 -13 0 3.70 0.47 1 -13 0 5.29 0.48 1 -13 0 4.18 0.45 1 -13 0 5.01 0.36 -1 13 0 4.95 0.44 0 -13 0 36.13 1.31 0 -13 0 33.99 1.24 0 -13 0 32.51 1.16 0 -13 0 32.96 1.22 0 -13 0 33.02 1.08 0 -13 0 34.65 1.27 0 13 0 31.46 1.16 -1 -13 0 23.12 1.04 -1 -13 0 22.33 0.99 -1 -13 0 22.77 0.87 -1 -13 0 21.90 0.99 -1 -13 0 21.16 0.92 1 13 0 22.59 0.95 -2 -13 0 6.26 0.61 -2 -13 0 6.68 0.67 -2 -13 0 6.75 0.54 -2 -13 0 7.88 0.66 -2 -13 0 5.57 0.59 2 13 0 6.60 0.60 12 -14 0 1.42 0.23 12 -14 0 0.91 0.37 12 -14 0 1.23 0.37 -12 14 0 1.06 0.24 11 -14 0 10.39 0.71 11 -14 0 10.63 0.40 11 -14 0 9.80 0.68 -11 14 0 11.39 0.53 -11 14 0 9.87 0.52 10 -14 0 1.60 0.20 10 -14 0 2.24 0.39 10 -14 0 1.72 0.36 -10 14 0 2.13 0.31 9 -14 0 24.75 0.97 9 -14 0 24.25 0.96 9 -14 0 24.85 0.97 9 -14 0 24.67 0.72 -9 14 0 24.41 0.82 8 -14 0 63.25 1.89 8 -14 0 61.40 1.64 8 -14 0 62.64 1.80 -8 14 0 59.80 1.69 7 -14 0 0.56 0.24 7 -14 0 0.83 0.27 7 -14 0 0.53 0.14 -7 14 0 0.67 0.18 6 -14 0 2.83 0.26 6 -14 0 2.64 0.34 6 -14 0 3.27 0.44 -6 14 0 2.97 0.30 5 -14 0 14.45 0.58 5 -14 0 15.47 0.74 5 -14 0 15.69 0.66 -5 14 0 16.25 0.63 -5 14 0 14.82 0.60 4 -14 0 1.79 0.33 4 -14 0 2.39 0.31 4 -14 0 3.16 0.39 -4 14 0 2.22 0.34 -4 14 0 2.38 0.32 3 -14 0 31.14 1.07 3 -14 0 30.48 1.18 3 -14 0 31.80 0.89 3 -14 0 32.89 1.15 3 -14 0 32.83 1.00 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