############################################################################## # # # This CIF contains the data in a paper accepted for publication in # # Acta Crystallographica Section E. It conforms to the requirements of # # Notes for Authors for Acta Crystallographica Section E, and has been # # peer reviewed under the auspices of the IUCr Commission on Journals. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the journal # # article from which it was obtained. # # # ############################################################################## data_I _audit_creation_method 'SHELXL-2014/7' _journal_date_recd_electronic 2015-09-08 _journal_date_accepted 2015-09-17 _journal_name_full 'Acta Crystallographica, Section E' _journal_year 2015 _journal_volume 71 _journal_issue 10 _journal_page_first 1219 _journal_page_last 1221 _journal_paper_category GM _journal_paper_doi 10.1107/S2056989015017429 _journal_coeditor_code RZ5165 _publ_contact_author_name 'Alexander A. Golichenko' _publ_contact_author_address ; Department of Inorganic Chemistry, Ukrainian State University of Chemical Technology, Gagarin Ave. 8, Dnipropetrovsk 49005, Ukraine ; _publ_contact_author_email 'golichenko_alex@i.ua' _publ_contact_author_fax '+380562470672' _publ_contact_author_phone '+380562470672' _publ_section_title ; Crystal structure of di-\m-isobutyrato-\k^4^O:O'-bis[cis-dichlorido(dimethyl sulfoxide-\kS)rhenium(III)] ; loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Golichenko, Alexander A.' . ; Department of Inorganic Chemistry, Ukrainian State University of Chemical Technology, Gagarin Ave. 8, Dnipropetrovsk 49005, Ukraine ; 'Shtemenko, Alexander V.' . ; Department of Inorganic Chemistry, Ukrainian State University of Chemical Technology, Gagarin Ave. 8, Dnipropetrovsk 49005, Ukraine ; _publ_section_synopsis ; A binuclear bis(carboxylato)dirhenium(III) complex is reported. The compound is a representative of a small class of alkylcarboxylate complexes involving a quadruple metal--metal bonds ; _chemical_name_systematic ;\ Di-\m-isobutyrato-\k^4^O:O'-\ bis[cis-dichlorido(dimethyl sulfoxide-\kS)rhenium(III)] ; _chemical_name_common ? _chemical_formula_moiety 'C12 H26 Cl4 O6 Re2 S2' _chemical_formula_sum 'C12 H26 Cl4 O6 Re2 S2' _chemical_formula_iupac '[Re2 (C4 H7 O2)2 Cl4 (C2 H6 O S)2]' _chemical_formula_weight 844.65 _chemical_melting_point ? _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 10.5581(4) _cell_length_b 14.7406(5) _cell_length_c 15.6088(6) _cell_angle_alpha 90 _cell_angle_beta 100.794(2) _cell_angle_gamma 90 _cell_volume 2386.26(15) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9919 _cell_measurement_theta_min 2.40 _cell_measurement_theta_max 38.98 _cell_measurement_temperature 110(2) _exptl_crystal_description plate _exptl_crystal_colour blue _exptl_crystal_size_max 0.222 _exptl_crystal_size_mid 0.180 _exptl_crystal_size_min 0.086 _exptl_crystal_density_diffrn 2.351 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1584 _exptl_absorpt_coefficient_mu 10.783 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2008) ; _shelx_estimated_absorpt_T_min 0.198 _shelx_estimated_absorpt_T_max 0.457 _exptl_absorpt_correction_T_min 0.1325 _exptl_absorpt_correction_T_max 0.4780 _diffrn_ambient_temperature 110(2) _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Siemens SMART CCD area-detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 93039 _diffrn_reflns_av_R_equivalents 0.0403 _diffrn_reflns_theta_min 2.155 _diffrn_reflns_theta_max 40.224 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.967 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_limit_l_max 27 _refine_special_details ? _reflns_number_total 14497 _reflns_number_gt 11921 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0380 _refine_ls_R_factor_gt 0.0254 _refine_ls_wR_factor_gt 0.0459 _refine_ls_wR_factor_ref 0.0489 _refine_ls_goodness_of_fit_ref 1.004 _refine_ls_restrained_S_all 1.004 _refine_ls_number_reflns 14497 _refine_ls_number_parameters 243 _refine_ls_number_restraints 0 _refine_ls_hydrogen_treatment constr _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0183P)^2^+1.7981P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 1.708 _refine_diff_density_min -1.144 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Re' 'Re' -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX2 (Bruker, 2008) ; _computing_cell_refinement ; SAINT (Bruker, 2008) ; _computing_data_reduction ; SAINT (Bruker, 2008) ; _computing_structure_solution ; SHELXS97 (Sheldrick 2008) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 1999) ; _computing_publication_material ; WinGX (Farrugia, 2012) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Re Re1 -0.06723(2) 0.17363(2) 0.27880(2) 0.01130(2) Uani d 1 . . Re Re2 0.10986(2) 0.16371(2) 0.21905(2) 0.01147(2) Uani d 1 . . Cl Cl1 -0.01954(5) 0.08982(4) 0.40554(3) 0.02107(9) Uani d 1 . . Cl Cl2 -0.19965(5) 0.05974(3) 0.21084(3) 0.01810(8) Uani d 1 . . Cl Cl3 0.06421(5) 0.04494(3) 0.12210(3) 0.01726(8) Uani d 1 . . Cl Cl4 0.25202(5) 0.07759(3) 0.31739(3) 0.02151(9) Uani d 1 . . S S1 0.41251(5) 0.24240(4) 0.20176(3) 0.01935(9) Uani d 1 . . S S2 -0.23871(5) 0.25929(3) 0.42297(3) 0.01756(9) Uani d 1 . . O O1 -0.14493(13) 0.26371(9) 0.18365(9) 0.0142(2) Uani d 1 . . O O2 0.02927(14) 0.25241(9) 0.12399(9) 0.0145(2) Uani d 1 . . O O3 0.18421(14) 0.27603(9) 0.28722(9) 0.0159(3) Uani d 1 . . O O4 0.01121(14) 0.28533(9) 0.34802(9) 0.0158(3) Uani d 1 . . O O5 0.28531(14) 0.20575(10) 0.14988(10) 0.0189(3) Uani d 1 . . O O6 -0.24413(14) 0.23612(10) 0.32675(9) 0.0189(3) Uani d 1 . . C C1 -0.07803(18) 0.29012(12) 0.12848(12) 0.0133(3) Uani d 1 . . C C2 -0.1181(2) 0.37225(13) 0.07331(14) 0.0181(4) Uani d 1 . . H H2 -0.1090 0.3585 0.0120 0.022 Uiso calc 1 . . C C3 -0.2560(2) 0.40050(17) 0.07314(17) 0.0274(5) Uani d 1 . . H H3A -0.2788 0.4516 0.0330 0.041 Uiso calc 1 . . H H3B -0.2647 0.4188 0.1321 0.041 Uiso calc 1 . . H H3C -0.3138 0.3494 0.0542 0.041 Uiso calc 1 . . C C4 -0.0227(3) 0.44808(16) 0.1087(2) 0.0354(6) Uani d 1 . . H H4A 0.0658 0.4260 0.1125 0.053 Uiso calc 1 . . H H4B -0.0358 0.4662 0.1668 0.053 Uiso calc 1 . . H H4C -0.0371 0.5004 0.0694 0.053 Uiso calc 1 . . C C5 0.1204(2) 0.31512(13) 0.33854(12) 0.0152(3) Uani d 1 . . C C6 0.1796(2) 0.39547(14) 0.38935(14) 0.0197(4) Uani d 1 . . H H6 0.2283 0.4313 0.3518 0.024 Uiso calc 1 . . C C7 0.0785(3) 0.4565(2) 0.4167(2) 0.0469(8) Uani d 1 . . H H7A 0.0176 0.4764 0.3649 0.070 Uiso calc 1 . . H H7B 0.1206 0.5095 0.4476 0.070 Uiso calc 1 . . H H7C 0.0321 0.4229 0.4554 0.070 Uiso calc 1 . . C C8 0.2750(3) 0.36103(19) 0.46883(17) 0.0337(6) Uani d 1 . . H H8A 0.3380 0.3207 0.4495 0.051 Uiso calc 1 . . H H8B 0.2282 0.3276 0.5074 0.051 Uiso calc 1 . . H H8C 0.3200 0.4127 0.5004 0.051 Uiso calc 1 . . C C9 0.4146(3) 0.36054(17) 0.1775(2) 0.0360(6) Uani d 1 . . H H9A 0.4047 0.3689 0.1143 0.054 Uiso calc 1 . . H H9B 0.4968 0.3868 0.2065 0.054 Uiso calc 1 . . H H9C 0.3435 0.3908 0.1984 0.054 Uiso calc 1 . . C C10 0.5306(2) 0.20667(18) 0.14113(18) 0.0291(5) Uani d 1 . . H H10A 0.5367 0.1403 0.1425 0.044 Uiso calc 1 . . H H10B 0.6144 0.2329 0.1669 0.044 Uiso calc 1 . . H H10C 0.5057 0.2272 0.0806 0.044 Uiso calc 1 . . C C11 -0.3361(3) 0.17496(16) 0.46035(17) 0.0286(5) Uani d 1 . . H H11A -0.4191 0.1709 0.4200 0.043 Uiso calc 1 . . H H11B -0.3508 0.1913 0.5186 0.043 Uiso calc 1 . . H H11C -0.2922 0.1162 0.4631 0.043 Uiso calc 1 . . C C12 -0.3441(3) 0.35344(17) 0.42132(18) 0.0338(6) Uani d 1 . . H H12A -0.3087 0.4057 0.3950 0.051 Uiso calc 1 . . H H12B -0.3529 0.3685 0.4811 0.051 Uiso calc 1 . . H H12C -0.4289 0.3381 0.3870 0.051 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Re1 0.01040(3) 0.01222(3) 0.01171(3) -0.00114(2) 0.00320(2) 0.00002(2) Re2 0.00953(3) 0.01154(3) 0.01360(3) 0.00081(2) 0.00288(2) 0.00041(2) Cl1 0.0222(2) 0.0241(2) 0.0166(2) -0.00111(18) 0.00305(17) 0.00674(16) Cl2 0.0161(2) 0.01640(19) 0.0219(2) -0.00426(15) 0.00380(17) -0.00305(15) Cl3 0.0169(2) 0.01521(19) 0.0201(2) 0.00138(15) 0.00460(16) -0.00402(14) Cl4 0.0167(2) 0.0215(2) 0.0244(2) 0.00463(17) -0.00088(18) 0.00541(17) S1 0.0130(2) 0.0223(2) 0.0230(2) -0.00283(17) 0.00407(18) -0.00136(17) S2 0.0194(2) 0.0189(2) 0.0162(2) -0.00284(17) 0.00824(17) -0.00281(15) O1 0.0120(6) 0.0153(6) 0.0159(6) 0.0000(5) 0.0041(5) 0.0022(4) O2 0.0133(6) 0.0153(6) 0.0157(6) 0.0025(5) 0.0048(5) 0.0026(4) O3 0.0136(6) 0.0161(6) 0.0186(6) -0.0023(5) 0.0044(5) -0.0023(5) O4 0.0156(7) 0.0163(6) 0.0162(6) -0.0038(5) 0.0050(5) -0.0034(5) O5 0.0108(6) 0.0225(7) 0.0238(7) -0.0020(5) 0.0040(5) -0.0011(5) O6 0.0164(7) 0.0255(7) 0.0167(7) -0.0009(5) 0.0076(5) -0.0038(5) C1 0.0134(8) 0.0128(7) 0.0135(8) 0.0015(6) 0.0022(6) -0.0002(5) C2 0.0175(9) 0.0170(8) 0.0199(9) 0.0037(7) 0.0034(7) 0.0046(6) C3 0.0184(10) 0.0275(11) 0.0353(13) 0.0065(8) 0.0025(9) 0.0084(9) C4 0.0254(12) 0.0162(10) 0.0617(18) -0.0007(8) 0.0004(12) 0.0048(10) C5 0.0161(9) 0.0132(8) 0.0155(8) -0.0013(6) 0.0015(7) -0.0012(6) C6 0.0206(10) 0.0179(9) 0.0204(9) -0.0062(7) 0.0028(7) -0.0044(7) C7 0.0375(16) 0.0298(14) 0.072(2) -0.0008(11) 0.0079(15) -0.0319(14) C8 0.0341(14) 0.0370(14) 0.0254(12) -0.0122(11) -0.0065(10) -0.0026(9) C9 0.0340(14) 0.0203(11) 0.0549(17) -0.0051(10) 0.0113(13) -0.0022(10) C10 0.0134(9) 0.0340(13) 0.0412(14) 0.0010(8) 0.0083(9) -0.0067(10) C11 0.0379(14) 0.0239(11) 0.0294(12) -0.0072(9) 0.0206(11) -0.0015(8) C12 0.0494(17) 0.0237(11) 0.0322(13) 0.0104(11) 0.0172(12) -0.0002(9) _geom_special_details ; All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Re1 O1 . 2.0459(13) ? Re1 O4 . 2.0565(13) ? Re1 Re2 . 2.24502(13) ? Re1 Cl1 . 2.3065(5) ? Re1 Cl2 . 2.3115(5) ? Re1 O6 . 2.3282(15) ? Re2 O2 . 2.0401(13) ? Re2 O3 . 2.0437(14) ? Re2 Cl3 . 2.3052(5) ? Re2 Cl4 . 2.3147(5) ? Re2 O5 . 2.3938(15) ? S1 O5 . 1.5310(15) ? S1 C10 . 1.780(2) ? S1 C9 . 1.783(3) ? S2 O6 . 1.5308(15) ? S2 C12 . 1.776(3) ? S2 C11 . 1.780(2) ? O1 C1 . 1.273(2) ? O2 C1 . 1.276(2) ? O3 C5 . 1.276(2) ? O4 C5 . 1.268(3) ? C1 C2 . 1.500(3) ? C2 C3 . 1.514(3) ? C2 C4 . 1.536(3) ? C2 H2 . 1.0000 ? C3 H3A . 0.9800 ? C3 H3B . 0.9800 ? C3 H3C . 0.9800 ? C4 H4A . 0.9800 ? C4 H4B . 0.9800 ? C4 H4C . 0.9800 ? C5 C6 . 1.495(3) ? C6 C7 . 1.517(4) ? C6 C8 . 1.531(3) ? C6 H6 . 1.0000 ? C7 H7A . 0.9800 ? C7 H7B . 0.9800 ? C7 H7C . 0.9800 ? C8 H8A . 0.9800 ? C8 H8B . 0.9800 ? C8 H8C . 0.9800 ? C9 H9A . 0.9800 ? C9 H9B . 0.9800 ? C9 H9C . 0.9800 ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Re1 O4 . . 85.93(6) ? O1 Re1 Re2 . . 89.58(4) ? O4 Re1 Re2 . . 89.18(4) ? O1 Re1 Cl1 . . 164.51(4) ? O4 Re1 Cl1 . . 88.65(4) ? Re2 Re1 Cl1 . . 104.857(14) ? O1 Re1 Cl2 . . 90.71(4) ? O4 Re1 Cl2 . . 166.43(4) ? Re2 Re1 Cl2 . . 103.960(13) ? Cl1 Re1 Cl2 . . 91.189(19) ? O1 Re1 O6 . . 74.92(5) ? O4 Re1 O6 . . 77.45(6) ? Re2 Re1 O6 . . 160.04(4) ? Cl1 Re1 O6 . . 89.75(4) ? Cl2 Re1 O6 . . 88.98(4) ? O2 Re2 O3 . . 85.80(6) ? O2 Re2 Re1 . . 89.66(4) ? O3 Re2 Re1 . . 89.97(4) ? O2 Re2 Cl3 . . 90.11(4) ? O3 Re2 Cl3 . . 165.87(4) ? Re1 Re2 Cl3 . . 103.544(13) ? O2 Re2 Cl4 . . 164.60(4) ? O3 Re2 Cl4 . . 87.76(4) ? Re1 Re2 Cl4 . . 104.318(15) ? Cl3 Re2 Cl4 . . 92.789(18) ? O2 Re2 O5 . . 76.03(5) ? O3 Re2 O5 . . 76.76(5) ? Re1 Re2 O5 . . 161.00(4) ? Cl3 Re2 O5 . . 89.13(4) ? Cl4 Re2 O5 . . 88.89(4) ? O5 S1 C10 . . 104.28(10) ? O5 S1 C9 . . 106.08(12) ? C10 S1 C9 . . 97.94(14) ? O6 S2 C12 . . 104.59(11) ? O6 S2 C11 . . 104.36(10) ? C12 S2 C11 . . 98.71(14) ? C1 O1 Re1 . . 119.46(12) ? C1 O2 Re2 . . 119.54(12) ? C5 O3 Re2 . . 119.74(13) ? C5 O4 Re1 . . 120.10(13) ? S1 O5 Re2 . . 121.94(8) ? S2 O6 Re1 . . 121.25(8) ? O1 C1 O2 . . 121.00(17) ? O1 C1 C2 . . 120.20(17) ? O2 C1 C2 . . 118.55(17) ? C1 C2 C3 . . 112.98(18) ? C1 C2 C4 . . 106.60(17) ? C3 C2 C4 . . 111.48(19) ? C1 C2 H2 . . 108.6 ? C3 C2 H2 . . 108.6 ? C4 C2 H2 . . 108.6 ? C2 C3 H3A . . 109.5 ? C2 C3 H3B . . 109.5 ? H3A C3 H3B . . 109.5 ? C2 C3 H3C . . 109.5 ? H3A C3 H3C . . 109.5 ? H3B C3 H3C . . 109.5 ? C2 C4 H4A . . 109.5 ? C2 C4 H4B . . 109.5 ? H4A C4 H4B . . 109.5 ? C2 C4 H4C . . 109.5 ? H4A C4 H4C . . 109.5 ? H4B C4 H4C . . 109.5 ? O4 C5 O3 . . 121.00(17) ? O4 C5 C6 . . 120.74(18) ? O3 C5 C6 . . 118.24(18) ? C5 C6 C7 . . 111.87(19) ? C5 C6 C8 . . 108.26(18) ? C7 C6 C8 . . 111.1(2) ? C5 C6 H6 . . 108.5 ? C7 C6 H6 . . 108.5 ? C8 C6 H6 . . 108.5 ? C6 C7 H7A . . 109.5 ? C6 C7 H7B . . 109.5 ? H7A C7 H7B . . 109.5 ? C6 C7 H7C . . 109.5 ? H7A C7 H7C . . 109.5 ? H7B C7 H7C . . 109.5 ? C6 C8 H8A . . 109.5 ? C6 C8 H8B . . 109.5 ? H8A C8 H8B . . 109.5 ? C6 C8 H8C . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? S1 C9 H9A . . 109.5 ? S1 C9 H9B . . 109.5 ? H9A C9 H9B . . 109.5 ? S1 C9 H9C . . 109.5 ? H9A C9 H9C . . 109.5 ? H9B C9 H9C . . 109.5 ? S1 C10 H10A . . 109.5 ? S1 C10 H10B . . 109.5 ? H10A C10 H10B . . 109.5 ? S1 C10 H10C . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? S2 C11 H11A . . 109.5 ? S2 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? S2 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? S2 C12 H12A . . 109.5 ? S2 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? S2 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C11 H11B O2 4_566 0.98 2.40 3.324(3) 156 yes C6 H6 Cl3 2_555 1.00 2.73 3.519(2) 136 yes C12 H12A Cl2 2_455 0.98 2.82 3.751(3) 159 yes C12 H12B Cl3 4_566 0.98 2.82 3.760(3) 161 yes _shelx_hkl_file ; 1 0 0 -0.4493 0.27442 7 -1 0 0 -1.3898 0.21016 1 -1 0 0 -1.0422 0.44261 4 1 0 0 -0.0855 0.41520 3 -2 0 0 1008.29 32.3619 4 2 0 0 951.448 29.3049 3 2 0 0 943.748 28.6254 7 -3 0 0 2.92771 2.29785 4 3 0 0 -1.9742 1.28708 3 3 0 0 -1.7631 1.01082 7 -3 0 0 -2.7385 1.02030 1 -4 0 0 347.976 15.0487 4 -4 0 0 313.430 12.0780 1 4 0 0 329.036 12.7977 3 4 0 0 325.333 11.5081 7 -5 0 0 0.77800 1.31378 1 5 0 0 1.49945 1.84537 3 -5 0 0 2.89672 2.23174 4 5 0 0 -0.0907 1.07641 7 -6 0 0 3595.32 117.615 4 6 0 0 3731.20 106.344 7 6 0 0 3519.68 108.381 3 -6 0 0 3590.55 108.567 1 -7 0 0 -1.2818 2.36923 4 7 0 0 4.31007 2.03522 7 7 0 0 1.97477 2.25203 3 -7 0 0 1.16017 1.78255 1 8 0 0 12.9144 2.95533 7 -8 0 0 11.9156 3.43945 1 -8 0 0 9.20986 3.93988 4 -8 0 0 18.3071 4.94596 6 -8 0 0 11.5339 3.14932 8 -8 0 0 9.84292 4.39347 9 8 0 0 11.8045 3.82469 3 -9 0 0 0.92740 2.45531 1 -9 0 0 -0.2632 2.62234 8 9 0 0 3.27533 3.14085 3 -9 0 0 -0.1610 3.31413 4 -9 0 0 8.76348 4.76538 6 -9 0 0 2.89802 3.85900 9 -10 0 0 52.4087 7.88732 6 -10 0 0 53.4914 8.39139 4 10 0 0 54.3083 7.70908 3 -10 0 0 63.7245 6.79760 8 -10 0 0 50.4450 6.52996 1 -10 0 0 42.6573 7.06563 9 -11 0 0 4.02250 4.60623 9 11 0 0 0.84081 3.36694 3 -11 0 0 -0.1679 4.39086 4 -11 0 0 10.9975 4.74149 8 -11 0 0 -0.4267 4.59809 6 -11 0 0 -0.2682 3.07583 1 -12 0 0 41.7781 7.54164 1 -12 0 0 37.9074 8.43781 6 -12 0 0 17.5305 6.74021 4 -12 0 0 23.1901 7.30535 9 -12 0 0 21.5564 6.01538 8 12 0 0 29.8477 7.43298 3 -13 0 0 -0.4176 4.71058 1 -13 0 0 -6.4740 5.55037 9 -13 0 0 0.40351 5.37285 6 13 0 0 -2.9643 4.92305 3 -13 0 0 3.32828 4.60813 8 -13 0 0 5.50098 6.11121 4 -14 0 0 16.7019 6.72046 8 -14 0 0 8.63253 7.00289 9 -14 0 0 7.70451 6.90426 6 -15 0 0 -6.2768 6.30593 6 -15 0 0 -4.6305 6.17749 9 -16 0 0 179.929 16.6553 6 -17 0 0 -0.6957 8.63600 6 -18 0 0 77.9989 13.6434 6 0 -1 0 -7.9919 0.15837 4 0 1 0 -8.0362 0.06934 7 0 1 0 -8.0731 0.11225 2 1 -1 0 2462.42 67.1986 3 -1 -1 0 2187.05 71.8571 4 1 -1 0 2284.68 71.2922 4 1 1 0 2283.28 66.0727 7 1 1 0 2281.40 66.0541 3 1 1 0 2315.35 68.4977 2 -1 1 0 2226.83 66.9078 1 -2 -1 0 3.74334 0.95231 1 -2 -1 0 2.16130 1.40320 4 2 -1 0 4.29228 0.91176 7 2 -1 0 3.23876 1.25096 3 2 1 0 1.86437 0.74447 7 -2 1 0 2.68818 0.46699 2 -2 1 0 1.20048 0.72714 1 2 1 0 2.97238 0.56627 2 2 1 0 5.52296 1.05388 3 -2 1 0 2.98135 1.16089 4 -3 -1 0 9.89940 1.58336 1 -3 -1 0 15.6952 2.84216 4 3 -1 0 12.1864 1.51097 7 3 -1 0 11.0272 2.09138 3 -3 1 0 9.43194 1.56149 1 3 1 0 12.1099 1.14555 2 3 1 0 10.2910 1.42326 7 -3 1 0 15.1556 2.52516 4 3 1 0 10.0728 1.75178 3 -4 -1 0 574.084 19.9198 1 -4 -1 0 574.029 23.1240 4 4 -1 0 607.286 21.0745 3 4 -1 0 612.634 19.2916 7 -4 1 0 589.589 20.0503 1 4 1 0 592.666 18.5672 2 -4 1 0 656.582 23.4888 4 4 1 0 582.090 20.1980 3 4 1 0 589.919 19.2826 7 5 -1 0 421.543 17.3857 3 5 -1 0 418.981 15.4273 7 -5 -1 0 433.635 19.3678 4 -5 -1 0 440.366 16.3710 1 5 1 0 480.345 14.4322 2 -5 1 0 513.459 20.4767 4 -5 1 0 447.750 16.5237 1 5 1 0 432.035 16.8085 3 5 1 0 461.204 15.7630 7 -6 -1 0 1922.59 59.6769 1 6 -1 0 1935.18 58.0410 7 6 -1 0 1932.67 60.8172 3 -6 -1 0 1845.90 65.7057 4 -6 1 0 1957.69 66.0441 4 6 1 0 1847.41 59.7152 3 -6 1 0 1907.63 59.7821 1 6 1 0 1959.37 58.2206 7 -7 -1 0 342.864 15.0959 1 7 -1 0 383.032 14.3908 7 7 -1 0 387.023 16.9824 3 -7 -1 0 340.065 17.8881 4 -7 1 0 346.931 15.1747 1 -7 1 0 379.909 18.4488 4 7 1 0 366.342 16.0444 3 7 1 0 345.624 14.1146 7 8 -1 0 8.99824 3.77545 3 -8 -1 0 9.35820 3.93631 4 -8 -1 0 5.58522 3.40725 6 -8 -1 0 8.52948 3.98189 9 -8 -1 0 7.94274 2.98619 1 -8 -1 0 12.0647 3.26683 8 -8 1 0 14.8502 4.98652 6 8 1 0 15.2991 3.24344 7 -8 1 0 11.2483 3.12772 1 -8 1 0 11.7870 4.45991 4 -8 1 0 13.6229 4.55658 9 8 1 0 9.46788 3.36878 3 -9 -1 0 8.76641 3.36681 1 -9 -1 0 15.5875 3.89545 8 -9 -1 0 5.07967 4.30600 9 -9 -1 0 12.7650 4.75453 6 9 -1 0 12.3893 4.24905 3 -9 -1 0 4.13373 4.03655 4 -9 1 0 13.6352 5.06974 6 -9 1 0 6.32055 3.21413 1 -9 1 0 6.68335 4.54457 9 -9 1 0 10.8887 3.56284 8 9 1 0 10.0115 4.00238 3 -9 1 0 13.1957 4.67016 4 -10 -1 0 834.384 37.0165 4 -10 -1 0 880.661 30.8750 8 -10 -1 0 963.054 35.1366 6 -10 -1 0 889.260 33.5863 9 10 -1 0 849.248 34.9180 3 -10 -1 0 859.574 33.3332 1 10 1 0 885.057 34.5162 3 -10 1 0 918.514 34.6371 6 -10 1 0 899.924 33.7666 9 -10 1 0 885.462 33.6447 1 -10 1 0 869.508 30.7312 8 -10 1 0 775.350 36.2166 4 11 -1 0 5.12517 4.69340 3 -11 -1 0 10.5130 4.61487 8 -11 -1 0 5.70792 5.86951 6 -11 -1 0 8.82938 4.30405 1 -11 -1 0 0.42341 4.46499 9 -11 -1 0 7.21031 5.02694 4 -11 1 0 9.07415 5.51884 9 -11 1 0 9.36715 4.27281 1 11 1 0 13.8206 5.14988 3 -11 1 0 7.38796 4.19031 8 -11 1 0 5.28018 5.32519 4 -11 1 0 0.95843 5.30152 6 -12 -1 0 1265.48 47.5636 9 -12 -1 0 1329.16 49.3212 1 -12 -1 0 1281.11 53.0325 4 -12 -1 0 1385.98 48.5944 6 -12 -1 0 1358.57 45.3491 8 12 -1 0 1317.00 50.7310 3 -12 1 0 1358.87 48.3718 9 -12 1 0 1346.56 48.5446 6 12 1 0 1338.64 50.4953 3 -12 1 0 1313.77 49.5728 1 -12 1 0 1274.50 52.8106 4 -12 1 0 1369.66 45.2301 8 -13 -1 0 8.27509 5.00124 1 -13 -1 0 2.24640 4.98401 8 13 -1 0 14.8275 6.96715 3 -13 -1 0 13.2685 6.36007 6 -13 -1 0 8.25025 6.49656 9 -13 -1 0 10.0243 6.54089 4 -13 1 0 9.37660 5.60955 8 13 1 0 10.0702 5.26745 3 -13 1 0 0.94534 5.84218 6 -13 1 0 5.42315 6.49877 9 -13 1 0 12.6827 6.09658 1 -14 -1 0 16.9232 7.83890 6 -14 -1 0 6.46264 6.05110 8 -14 -1 0 7.77929 6.74968 9 -14 1 0 9.65198 7.34572 6 -14 1 0 21.8566 8.01372 9 -15 -1 0 13.5280 8.45031 6 -15 -1 0 51.6134 10.1658 9 -15 -1 0 16.5917 7.01632 8 -15 1 0 41.8134 9.79681 9 -15 1 0 26.4496 9.08809 6 -16 -1 0 395.277 23.3347 6 -16 1 0 346.678 22.7395 6 -17 -1 0 53.9346 11.7091 6 -17 1 0 64.0503 12.5144 6 -18 -1 0 86.1939 13.4528 6 -18 1 0 102.688 14.4581 6 0 -2 0 5600.02 154.005 3 0 -2 0 5287.22 164.660 4 0 2 0 5638.94 154.922 7 0 2 0 4725.02 155.798 1 0 2 0 5423.55 158.833 2 1 -2 0 131.304 4.64875 3 1 -2 0 124.473 4.07747 7 -1 -2 0 137.424 5.99415 4 1 -2 0 136.382 5.36392 4 -1 -2 0 122.091 4.75072 1 1 2 0 122.100 4.46786 3 -1 2 0 122.759 4.06708 7 -1 2 0 131.029 4.57230 1 -1 2 0 124.888 4.67344 2 1 2 0 134.076 4.78918 2 -2 -2 0 222.158 10.2049 4 2 -2 0 267.579 9.69039 3 2 -2 0 244.569 9.27619 4 2 -2 0 240.869 7.27332 7 -2 -2 0 225.773 8.31095 1 2 2 0 233.880 8.19886 3 2 2 0 227.647 8.15514 7 -2 2 0 229.611 7.87408 2 2 2 0 231.458 8.00553 2 -2 2 0 233.080 8.28278 1 3 -2 0 30.6321 3.35338 3 -3 -2 0 28.4312 3.75206 4 -3 -2 0 26.2336 2.31860 1 3 -2 0 27.5838 1.85699 7 3 2 0 28.9598 2.49467 3 -3 2 0 25.4786 2.30219 1 -3 2 0 26.2466 1.64066 2 3 2 0 29.2367 1.85424 2 3 2 0 28.8416 2.26069 7 4 -2 0 537.201 19.9052 3 -4 -2 0 546.620 18.3762 1 -4 -2 0 550.724 21.9471 4 4 -2 0 516.939 17.2651 7 4 2 0 532.417 17.8536 7 4 2 0 556.761 17.1940 2 -4 2 0 526.548 16.7952 2 4 2 0 538.863 18.4540 3 -4 2 0 544.062 18.5266 1 -4 2 0 546.078 20.8067 4 -5 -2 0 925.085 30.6627 1 5 -2 0 905.681 29.3063 7 5 -2 0 930.120 32.3584 3 -5 -2 0 976.049 35.5020 4 5 2 0 915.779 30.7304 3 5 2 0 1002.78 29.1790 2 -5 2 0 949.711 34.5890 4 -5 2 0 923.745 28.5784 2 5 2 0 943.334 29.8923 7 -5 2 0 926.617 30.8454 1 -6 -2 0 753.892 26.4312 1 6 -2 0 751.497 24.9879 7 6 -2 0 769.390 28.3334 3 -6 -2 0 696.001 30.1853 4 6 2 0 721.339 26.5493 3 6 2 0 837.643 24.2696 2 6 2 0 751.640 25.5186 7 -6 2 0 823.646 31.3905 4 -6 2 0 781.705 26.7166 1 -7 -2 0 1978.56 71.0304 4 7 -2 0 2007.71 65.9288 3 -7 -2 0 2082.60 64.3761 1 7 2 0 2046.18 64.4015 3 -7 2 0 2132.21 71.4323 4 -7 2 0 2013.93 64.4097 1 7 2 0 2035.64 62.6444 7 8 -2 0 0.08023 2.85916 3 -8 -2 0 1.74566 3.43131 4 -8 -2 0 1.10510 2.94583 6 -8 -2 0 0.24124 3.08058 9 -8 -2 0 8.86815 3.11638 8 -8 -2 0 2.36241 2.18093 1 8 2 0 3.42824 2.16040 7 -8 2 0 2.50411 3.37784 6 -8 2 0 4.36560 2.50261 1 8 2 0 2.07497 2.46394 3 -8 2 0 -0.3101 3.39554 9 -8 2 0 3.54103 3.29788 4 -9 -2 0 245.252 15.7341 4 9 -2 0 247.159 14.6359 3 -9 -2 0 257.527 14.1394 6 -9 -2 0 238.435 14.1698 9 -9 -2 0 253.224 13.1765 1 -9 -2 0 224.560 11.8203 8 9 2 0 230.367 13.5019 3 -9 2 0 246.886 14.0971 9 9 2 0 227.452 11.8045 7 -9 2 0 235.417 11.9803 8 -9 2 0 242.150 14.4412 6 -9 2 0 226.652 15.1119 4 -9 2 0 244.061 13.1179 1 10 -2 0 9.95829 4.77243 3 -10 -2 0 10.4932 4.99087 4 -10 -2 0 19.6810 4.80408 8 -10 -2 0 19.4666 4.90694 1 -10 -2 0 12.2357 5.55094 6 -10 -2 0 7.27770 4.42738 9 10 2 0 9.64073 4.15153 3 -10 2 0 15.7399 4.20278 8 -10 2 0 7.42339 5.11047 6 -10 2 0 9.65510 4.05328 1 -10 2 0 20.2366 6.04665 4 -10 2 0 9.53950 5.07185 9 -11 -2 0 809.139 32.5472 1 -11 -2 0 785.028 32.3473 9 11 -2 0 810.908 34.4776 3 -11 -2 0 811.693 36.3162 4 -11 -2 0 769.849 29.7769 8 -11 -2 0 828.126 33.3528 6 -11 2 0 758.205 32.0824 9 -11 2 0 815.875 33.2952 6 -11 2 0 877.855 30.4053 8 11 2 0 798.190 33.3578 3 -11 2 0 847.916 33.3286 1 12 -2 0 11.0569 5.75858 3 -12 -2 0 22.6614 7.48197 9 12 -2 0 19.7724 6.20077 4 -12 -2 0 16.0048 7.05205 6 -12 -2 0 14.5823 5.68406 1 -12 -2 0 9.53239 6.35865 4 -12 -2 0 6.57625 4.64431 8 -12 2 0 3.31566 6.14951 6 -12 2 0 11.2477 6.32261 9 12 2 0 15.0034 5.74974 3 -12 2 0 16.5174 5.84776 1 -12 2 0 20.2027 5.72004 8 -13 -2 0 290.104 18.4242 9 -13 -2 0 296.026 17.4541 8 -13 -2 0 344.055 19.9226 6 -13 -2 0 273.978 20.2335 4 13 -2 0 317.888 20.0414 3 13 -2 0 319.329 19.8036 4 -13 2 0 305.511 18.9831 9 -13 2 0 308.165 18.9745 6 13 2 0 295.631 19.3554 3 -13 2 0 331.332 19.7376 1 -14 -2 0 2.44299 6.10227 9 -14 -2 0 -3.3320 6.68917 6 -14 -2 0 -3.9034 4.67528 8 -14 2 0 -2.0291 6.04537 6 -14 2 0 2.19357 6.26497 9 -15 -2 0 210.642 16.8534 6 -15 -2 0 195.030 16.1414 8 -15 -2 0 225.178 16.9003 9 -15 2 0 220.243 17.3910 6 -16 -2 0 17.2984 8.43161 6 -16 -2 0 15.0391 7.98209 8 -16 2 0 3.95666 8.20938 6 -17 -2 0 256.695 19.3184 6 -17 2 0 265.736 20.3603 6 -18 -2 0 18.7555 9.50161 6 -18 2 0 19.8008 10.7484 6 0 -3 0 0.39688 0.57395 3 0 -3 0 0.55904 1.05309 4 0 3 0 3.19087 0.99556 2 0 3 0 3.27171 0.59865 1 0 3 0 1.35695 0.74063 7 1 -3 0 4251.29 120.613 3 1 -3 0 4242.26 120.457 7 1 -3 0 4070.57 130.352 4 -1 -3 0 4174.32 122.602 1 -1 -3 0 4154.03 120.522 3 -1 -3 0 4108.81 131.202 4 -1 3 0 4190.96 125.122 2 1 3 0 4237.18 125.166 2 1 3 0 4261.92 120.890 7 -1 3 0 4266.42 122.137 1 -1 3 0 4241.32 120.465 7 2 -3 0 199.298 8.67236 4 2 -3 0 213.200 8.03285 3 -2 -3 0 200.755 9.76745 4 -2 -3 0 211.901 8.06907 1 2 -3 0 202.881 6.55424 7 -2 3 0 205.299 6.56019 7 2 3 0 195.448 7.46908 3 -2 3 0 204.137 7.59430 2 -2 3 0 208.839 7.68046 1 2 3 0 200.336 7.63240 2 2 3 0 208.556 7.74540 7 3 -3 0 2.06342 1.40108 4 3 -3 0 11.1058 2.45398 3 -3 -3 0 1.29874 1.78576 4 -3 -3 0 5.33577 1.44136 1 3 -3 0 2.77750 0.62770 7 3 3 0 2.01434 1.02251 2 3 3 0 3.74497 1.31319 7 -3 3 0 0.46437 0.89984 2 -3 3 0 1.90925 1.19958 1 3 3 0 1.63872 1.14038 3 4 -3 0 142.318 8.11708 3 -4 -3 0 124.223 8.73212 4 -4 -3 0 144.850 6.72492 1 4 -3 0 149.356 5.21682 7 4 -3 0 126.251 7.58473 4 -4 3 0 140.194 6.77814 1 -4 3 0 152.110 5.72411 2 4 3 0 139.593 5.80015 2 4 3 0 144.746 6.80451 3 4 3 0 152.101 6.63312 7 5 -3 0 3350.02 94.9195 7 5 -3 0 3286.46 99.4129 3 -5 -3 0 2974.82 106.862 4 5 -3 0 3347.86 105.744 4 -5 -3 0 3285.91 97.8739 1 5 3 0 3244.99 97.0407 3 5 3 0 3280.81 96.3919 7 -5 3 0 3299.31 97.7676 2 -5 3 0 3318.19 98.2114 1 5 3 0 3300.43 98.0384 2 -6 -3 0 46.0492 4.25751 1 6 -3 0 48.0705 3.50763 7 -6 -3 0 43.6214 6.07144 4 6 -3 0 35.4308 5.08242 4 6 -3 0 50.1466 6.04687 3 6 3 0 46.1265 4.52007 3 -6 3 0 43.3952 4.38178 1 6 3 0 48.4469 4.17021 7 6 3 0 46.7234 3.11284 2 7 -3 0 547.622 24.0690 4 -7 -3 0 544.655 20.2470 1 -7 -3 0 520.746 18.7685 8 -7 -3 0 552.703 24.6495 4 7 -3 0 512.126 22.3571 3 -7 3 0 496.104 20.1471 1 -7 3 0 535.459 21.9881 6 7 3 0 515.636 20.4508 3 7 3 0 510.239 19.3027 7 8 -3 0 215.036 13.4853 4 -8 -3 0 191.861 11.1479 6 -8 -3 0 206.538 10.9264 1 -8 -3 0 189.976 10.0246 8 -8 -3 0 196.234 12.1244 9 8 -3 0 189.436 12.3683 3 -8 -3 0 194.803 13.3662 4 8 3 0 200.605 11.3976 3 -8 3 0 196.851 12.5358 6 -8 3 0 175.515 11.7078 9 8 3 0 198.514 10.1734 7 -8 3 0 205.492 11.1015 1 -9 -3 0 51.0161 7.94920 4 9 -3 0 52.2213 7.43804 3 -9 -3 0 56.5170 7.32934 9 9 -3 0 47.2692 7.05986 4 -9 -3 0 54.8834 6.94182 6 -9 -3 0 40.2316 5.45524 8 -9 -3 0 35.4114 5.35150 1 9 3 0 48.4807 6.46587 3 -9 3 0 48.1354 5.56074 8 -9 3 0 47.0076 7.23764 6 9 3 0 42.2709 5.20303 7 -9 3 0 36.9023 6.61844 9 -9 3 0 37.0181 5.47698 1 10 -3 0 127.406 10.9270 4 -10 -3 0 112.255 10.3184 9 -10 -3 0 108.149 8.90392 1 -10 -3 0 112.215 9.01272 8 -10 -3 0 129.757 11.0145 6 -10 -3 0 135.645 12.0121 4 10 -3 0 115.209 10.7164 3 -10 3 0 123.434 9.11153 8 10 3 0 132.058 10.2614 3 -10 3 0 128.457 10.0237 1 -10 3 0 133.126 11.2312 9 -10 3 0 104.719 10.7019 6 -11 -3 0 27.7146 7.20404 6 11 -3 0 18.7494 6.15893 3 -11 -3 0 21.3230 5.24030 8 11 -3 0 23.7558 6.57154 4 11 3 0 20.0265 5.77149 3 -11 3 0 26.2915 7.53426 9 -11 3 0 20.7782 5.58113 1 -11 3 0 25.3288 7.00756 6 -12 -3 0 168.694 12.4049 8 -12 -3 0 155.591 13.2522 9 -12 -3 0 180.089 15.4042 4 -12 -3 0 177.230 13.2436 1 12 -3 0 182.901 14.3169 4 12 -3 0 178.556 14.0664 3 -12 -3 0 177.588 14.3045 6 12 3 0 171.641 13.4932 3 -12 3 0 155.278 13.9628 6 -12 3 0 163.740 12.9849 1 -12 3 0 166.110 13.7633 9 -13 -3 0 6.04678 5.21725 8 13 -3 0 14.7108 5.83404 3 -13 -3 0 17.9353 7.44212 6 -13 -3 0 7.25995 6.53909 9 -13 -3 0 8.67951 6.73531 4 13 -3 0 4.27247 5.28718 4 -13 3 0 7.97886 7.16582 6 -13 3 0 20.9409 6.72749 1 -13 3 0 15.4988 7.56253 9 13 3 0 6.42374 5.86854 3 -14 -3 0 0.23083 5.57466 8 -14 -3 0 -0.0956 5.98590 9 -14 -3 0 1.08187 6.06404 6 -14 3 0 2.82474 6.54328 9 14 3 0 10.6897 5.54398 9 -14 3 0 12.8999 7.57400 6 -15 -3 0 3.17787 6.65166 9 -15 -3 0 12.0319 8.02424 6 -15 -3 0 7.29926 7.07156 8 -15 3 0 -3.3424 6.34189 6 -15 3 0 17.8339 8.18081 9 -16 -3 0 4.70089 7.18975 8 -16 -3 0 -7.8398 6.60291 6 -16 3 0 3.15576 8.16008 6 -17 -3 0 234.811 18.6946 6 -17 -3 0 206.124 18.2083 8 -17 3 0 253.250 19.6085 6 -18 -3 0 2.28826 9.06135 6 -18 3 0 1.34806 9.07091 6 0 -4 0 528.122 18.9788 4 0 -4 0 531.627 16.0669 3 0 4 0 509.801 16.4045 7 0 4 0 507.404 17.4409 2 0 4 0 547.807 16.0592 1 1 -4 0 14.7221 1.27944 3 -1 -4 0 13.9860 2.39475 4 -1 -4 0 13.9366 1.11555 1 1 -4 0 12.0649 1.94607 4 -1 -4 0 14.3342 1.35811 3 -1 4 0 12.9327 1.26196 1 -1 4 0 14.1730 1.25407 7 -1 4 0 13.3253 1.63884 2 1 4 0 11.9016 1.49267 7 1 4 0 13.4135 1.66156 2 -2 -4 0 103.962 6.63692 4 -2 -4 0 97.6110 5.11017 1 2 -4 0 111.979 4.84186 3 2 -4 0 113.586 3.98435 7 2 -4 0 107.156 5.77977 4 2 4 0 117.700 5.10519 2 -2 4 0 107.593 4.95017 2 -2 4 0 111.041 3.95580 7 2 4 0 105.521 4.94931 7 2 4 0 101.130 4.60884 3 -2 4 0 117.465 4.86010 1 3 -4 0 64.4180 4.32563 3 -3 -4 0 74.4393 6.02130 4 3 -4 0 62.8161 4.63521 4 3 -4 0 66.4311 2.65178 7 -3 -4 0 69.9520 4.05333 1 -3 4 0 68.0695 2.66602 7 3 4 0 65.0733 3.87547 3 -3 4 0 65.2504 3.89888 1 3 4 0 76.5661 4.21978 7 3 4 0 75.1379 3.91053 2 -3 4 0 63.6578 3.67508 2 -4 -4 0 637.385 25.9845 4 4 -4 0 623.280 18.9872 7 -4 -4 0 640.793 21.4202 1 4 -4 0 675.199 23.3887 3 4 -4 0 657.808 23.9450 4 -4 4 0 672.249 21.7631 1 4 4 0 645.605 21.3342 7 -4 4 0 609.476 20.8016 2 4 4 0 636.190 20.9733 2 4 4 0 613.189 21.1996 3 5 -4 0 2148.98 67.3960 3 5 -4 0 2223.26 71.6751 4 -5 -4 0 2127.46 73.8857 4 5 -4 0 2132.78 62.4840 7 -5 -4 0 2174.21 65.8343 1 -5 4 0 2147.04 65.5973 2 5 4 0 2148.88 65.0945 7 5 4 0 2184.47 65.7594 2 -5 4 0 2146.51 66.1939 1 5 4 0 2153.51 65.5159 3 -6 -4 0 120.931 9.99172 4 6 -4 0 133.277 9.03870 4 6 -4 0 126.779 8.80502 3 -6 -4 0 123.941 7.19302 1 6 4 0 139.871 6.15668 2 6 4 0 132.710 7.23180 7 6 4 0 132.018 7.63151 3 -6 4 0 125.670 7.47104 1 -7 -4 0 624.691 28.1243 4 7 -4 0 668.119 27.5683 4 -7 -4 0 644.202 21.9955 8 7 -4 0 659.278 25.7490 3 -7 -4 0 601.141 23.1884 1 -7 4 0 620.684 23.7935 1 7 4 0 657.099 23.1134 7 7 4 0 647.297 23.9360 3 -7 4 0 627.117 25.0848 6 -8 -4 0 10.9380 3.19327 1 -8 -4 0 25.6312 5.54505 9 -8 -4 0 11.5434 4.22040 6 -8 -4 0 29.5085 4.43391 8 8 -4 0 19.7045 4.99075 4 8 -4 0 39.6662 6.00643 3 -8 -4 0 17.1330 5.33109 4 8 4 0 19.9791 3.77857 7 -8 4 0 12.6647 4.69314 9 -8 4 0 20.6519 4.08026 1 -8 4 0 27.1433 5.65865 6 8 4 0 19.6816 4.19626 3 9 -4 0 35.7032 6.27576 3 -9 -4 0 30.5257 7.08024 4 -9 -4 0 43.1229 5.59300 8 9 -4 0 54.7538 5.06832 5 9 -4 0 50.2644 7.34237 4 -9 -4 0 38.1051 6.62720 9 -9 -4 0 47.6782 5.74965 1 -9 -4 0 38.2765 6.25372 6 -9 4 0 45.0396 7.33761 6 9 4 0 40.4736 5.22160 7 -9 4 0 31.0362 6.25675 9 -9 4 0 37.4283 5.48984 1 9 4 0 35.1077 5.57722 3 10 -4 0 60.2692 8.29778 3 -10 -4 0 58.6456 8.17940 9 -10 -4 0 68.0234 7.03744 8 10 -4 0 84.1705 9.49359 4 -10 -4 0 67.3951 7.42209 1 -10 -4 0 72.9776 8.65836 6 -10 -4 0 72.7365 9.87263 4 10 4 0 67.8091 6.96122 7 -10 4 0 79.3348 8.24259 1 -10 4 0 73.7012 9.17766 6 -10 4 0 69.3795 8.59059 9 10 4 0 60.6007 7.44206 3 11 -4 0 2180.86 72.8593 3 11 -4 0 2102.62 77.2668 4 -11 -4 0 2142.33 70.5090 9 -11 -4 0 2178.39 79.0686 4 -11 -4 0 2192.73 70.0508 6 -11 -4 0 2160.95 66.4062 8 -11 4 0 2063.87 70.2617 6 11 4 0 2075.59 71.7764 3 11 4 0 2175.17 70.2141 9 -11 4 0 2245.91 72.8576 1 -11 4 0 2085.10 70.5520 9 -12 -4 0 28.9989 7.71620 9 12 -4 0 34.6048 7.83284 4 -12 -4 0 34.0110 8.49313 4 12 -4 0 30.0708 7.35463 3 -12 -4 0 33.1830 6.67087 8 -12 -4 0 23.6477 7.61410 6 12 4 0 36.1481 7.10288 9 -12 4 0 25.9272 7.93058 9 -12 4 0 33.5638 7.33519 1 -12 4 0 21.9468 7.37240 6 12 4 0 27.6560 6.88221 3 -13 -4 0 257.838 16.3051 8 -13 -4 0 276.837 18.3157 6 -13 -4 0 286.544 18.2174 9 13 4 0 269.452 16.9824 9 -13 4 0 258.072 17.7120 6 -13 4 0 271.152 17.8048 1 -13 4 0 248.663 17.6715 9 -14 -4 0 27.7778 7.81686 8 -14 -4 0 32.6681 8.96354 6 -14 -4 0 43.0960 9.41443 9 -14 4 0 37.6668 9.17891 9 -14 4 0 27.0355 8.44936 6 14 4 0 48.3485 8.68479 9 -15 -4 0 40.1492 9.48194 8 -15 -4 0 52.1364 10.4068 6 -15 4 0 54.7082 10.6788 9 -15 4 0 41.0252 10.4952 6 -16 -4 0 23.9145 9.63387 6 -16 -4 0 20.2811 8.94439 8 -16 4 0 20.8612 9.41474 6 -17 -4 0 319.979 21.7743 8 -17 -4 0 261.603 20.1368 6 -17 4 0 223.653 19.5270 6 -18 -4 0 75.1657 13.6747 8 -18 -4 0 84.6427 13.4661 6 -18 4 0 75.4989 13.4042 6 0 -5 0 -1.9004 1.00013 4 0 -5 0 -0.3524 0.68986 3 0 5 0 0.40882 0.70753 1 0 5 0 1.04409 1.16689 2 0 5 0 0.51697 0.91436 7 1 -5 0 263.872 11.1861 4 -1 -5 0 272.109 8.64944 1 1 -5 0 257.762 8.86894 3 -1 -5 0 259.805 9.04937 3 -1 -5 0 260.208 11.8776 4 1 5 0 269.793 10.2644 2 -1 5 0 255.438 8.95700 1 1 5 0 287.944 9.80149 7 -1 5 0 268.321 9.02044 7 -1 5 0 269.164 10.2127 2 2 -5 0 393.351 16.5452 4 2 -5 0 450.592 13.7345 7 -2 -5 0 440.568 18.1338 4 -2 -5 0 437.517 14.8684 1 2 -5 0 453.509 14.4116 3 2 5 0 439.782 14.4894 3 2 5 0 442.099 15.0085 7 -2 5 0 440.831 13.7345 7 -2 5 0 435.108 14.5916 1 2 5 0 451.202 15.4502 2 -2 5 0 442.954 15.4409 2 3 -5 0 11.4578 2.49504 4 3 -5 0 21.5968 2.43344 3 -3 -5 0 23.4655 2.56627 1 -3 -5 0 9.32235 3.02940 4 3 -5 0 9.71432 1.06209 7 3 5 0 5.74818 1.52087 3 3 5 0 9.22024 1.87322 7 -3 5 0 10.1834 1.05503 7 3 5 0 5.50944 1.60493 2 -3 5 0 6.93777 1.57059 1 -3 5 0 6.73672 1.57341 2 4 -5 0 867.149 31.0399 4 -4 -5 0 835.286 33.1295 4 4 -5 0 851.651 25.3891 7 4 -5 0 896.124 28.9679 3 -4 -5 0 869.872 27.9462 1 4 5 0 863.992 28.0058 7 -4 5 0 860.730 28.0079 2 4 5 0 853.448 27.9719 2 4 5 0 833.531 27.6824 3 -4 5 0 842.575 28.0967 1 -4 5 0 898.097 25.4357 7 5 -5 0 1287.02 46.5959 4 -5 -5 0 1299.40 42.2802 1 5 -5 0 1356.58 44.4392 3 5 -5 0 1448.15 39.1964 7 -5 -5 0 1325.03 49.4304 4 -5 5 0 1328.21 42.2839 2 -5 5 0 1355.41 42.8735 1 5 5 0 1304.49 42.2685 3 -5 5 0 1399.56 39.1595 7 5 5 0 1363.25 42.3073 2 5 5 0 1282.12 42.0740 7 6 -5 0 1499.69 49.5837 3 -6 -5 0 1535.80 55.6427 4 -6 -5 0 1590.89 48.0141 1 6 -5 0 1501.62 52.8214 4 6 5 0 1549.46 47.1921 2 6 5 0 1430.21 47.6179 3 -6 5 0 1511.61 48.3769 1 6 5 0 1425.04 47.2254 7 -7 -5 0 393.109 16.1973 6 7 -5 0 369.288 18.5214 4 -7 -5 0 360.398 15.3603 1 -7 -5 0 369.231 14.6927 8 7 -5 0 361.291 17.0919 3 -7 -5 0 356.955 17.6397 9 -7 -5 0 358.565 19.7074 4 -7 5 0 393.272 16.9957 9 -7 5 0 373.336 15.9919 1 7 5 0 409.778 18.2144 9 -7 5 0 379.426 17.8681 6 7 5 0 366.449 15.3048 7 7 5 0 367.133 15.8811 3 -8 -5 0 323.461 16.6061 9 8 -5 0 318.446 17.6329 4 -8 -5 0 343.784 14.3458 8 -8 -5 0 335.952 14.7834 1 8 -5 0 327.544 13.0024 5 -8 -5 0 306.682 18.5866 4 8 -5 0 310.528 16.2089 3 -8 -5 0 339.957 15.5062 6 -8 5 0 318.189 15.2041 1 8 5 0 311.118 16.2498 9 8 5 0 321.151 15.1124 3 8 5 0 295.998 14.1664 7 -8 5 0 295.734 15.5393 9 -8 5 0 317.392 16.5101 6 -9 -5 0 54.0215 7.66902 9 -9 -5 0 62.2317 7.53557 6 -9 -5 0 50.0979 5.84653 8 9 -5 0 49.3988 7.16231 4 -9 -5 0 49.8435 5.77543 1 9 -5 0 45.3540 5.19405 5 -9 -5 0 43.6815 8.01573 4 9 -5 0 42.4279 6.72406 3 9 5 0 52.7916 6.34659 3 -9 5 0 46.7852 7.27495 9 9 5 0 34.5971 6.28234 9 9 5 0 58.2789 6.17985 7 -9 5 0 48.9274 6.30791 1 -9 5 0 56.0985 7.93463 6 -10 -5 0 915.304 32.6847 8 10 -5 0 999.072 39.4285 4 -10 -5 0 928.925 35.7585 9 -10 -5 0 916.469 34.6767 6 -10 -5 0 960.018 40.8350 4 10 -5 0 961.204 36.5611 3 -10 5 0 914.036 36.0073 6 -10 5 0 922.079 35.5014 1 10 5 0 926.803 33.8236 7 10 5 0 914.209 35.3847 3 -10 5 0 883.478 35.2768 9 10 5 0 901.893 35.1666 9 -11 -5 0 7.31647 4.66738 8 -11 -5 0 -1.0803 4.82467 9 -11 -5 0 0.92303 5.14645 4 11 -5 0 -0.2443 3.95202 4 11 -5 0 4.26294 4.12995 3 -11 -5 0 3.23170 4.94711 6 11 5 0 0.67629 3.55190 3 -11 5 0 -0.0190 4.82720 6 -11 5 0 2.55952 3.72500 1 -11 5 0 -1.1587 4.86962 9 11 5 0 -1.2291 4.15543 9 12 -5 0 1035.37 40.5006 3 -12 -5 0 1020.67 39.7248 9 12 -5 0 971.235 42.5416 4 -12 -5 0 1019.65 39.7537 6 -12 -5 0 1091.03 45.2804 4 -12 -5 0 964.596 36.7597 8 12 5 0 997.908 40.2757 3 -12 5 0 1022.48 40.6610 1 12 5 0 1028.33 39.1702 9 -12 5 0 973.744 39.4854 9 -12 5 0 994.587 39.9632 6 -13 -5 0 -3.6186 4.68987 8 -13 -5 0 -3.5547 5.46325 6 -13 -5 0 -2.4238 5.67286 4 13 -5 0 2.56374 5.17370 3 -13 -5 0 -1.1164 5.88821 9 -13 5 0 1.79184 6.59178 9 -13 5 0 0.59328 6.41139 6 13 5 0 -1.7344 4.46229 9 -14 -5 0 23.6559 8.32125 6 -14 -5 0 26.5310 7.81467 8 -14 -5 0 23.9171 8.10333 9 -14 5 0 28.2268 8.85717 6 -14 5 0 19.1161 8.37259 9 14 5 0 30.1919 7.67627 9 -15 -5 0 45.3422 9.58930 8 -15 -5 0 36.7141 9.71848 6 -15 5 0 28.4473 9.89653 6 -16 -5 0 223.138 17.8861 6 -16 -5 0 249.983 19.1181 8 -16 5 0 219.982 18.7923 6 -17 -5 0 117.031 14.3533 6 -17 -5 0 133.841 15.8972 8 -17 5 0 99.1621 14.2217 6 -18 -5 0 101.113 14.9463 8 -18 -5 0 87.6413 13.0920 6 -18 5 0 88.5763 14.3757 6 0 -6 0 1504.84 43.4954 3 0 -6 0 1504.67 49.5426 4 0 6 0 1482.84 46.4066 2 0 6 0 1444.96 43.5985 1 0 6 0 1409.93 43.9852 7 1 -6 0 39.4858 2.47877 3 -1 -6 0 40.2458 4.37164 4 -1 -6 0 46.3235 2.28784 1 -1 -6 0 49.5377 2.79847 3 1 -6 0 44.2318 4.20344 4 -1 6 0 34.8317 2.38680 1 -1 6 0 42.6763 3.42089 2 -1 6 0 41.0667 2.64893 7 1 6 0 40.9597 3.45788 2 1 6 0 40.1346 2.98421 7 -2 -6 0 1597.70 50.5898 1 -2 -6 0 1757.69 57.5287 4 2 -6 0 1680.98 55.8424 4 2 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-6 0 1147.57 39.0897 3 -6 6 0 1158.77 39.1997 6 -6 6 0 1166.71 37.7950 1 6 6 0 1166.87 36.6600 2 6 6 0 1049.14 36.8146 7 6 6 0 1134.62 37.3091 3 7 -6 0 5.88791 3.07078 3 -7 -6 0 6.15389 3.29299 6 -7 -6 0 6.34376 2.72072 8 -7 -6 0 0.75312 3.22486 4 -7 -6 0 -0.2776 1.75763 1 7 -6 0 0.80706 2.73788 4 7 -6 0 0.80649 2.42928 5 -7 -6 0 2.08639 3.67562 9 -7 6 0 1.72267 3.33419 6 -7 6 0 2.19047 3.32490 9 7 6 0 -0.4271 2.57793 9 -7 6 0 4.72716 2.55016 1 7 6 0 3.87371 2.39558 7 7 6 0 2.03321 2.16872 3 8 -6 0 154.513 10.5922 3 8 -6 0 166.990 8.72984 5 -8 -6 0 149.160 8.88838 8 -8 -6 0 140.927 9.94460 6 8 -6 0 139.215 11.2842 4 -8 -6 0 143.108 12.3029 4 -8 -6 0 135.296 10.6775 9 8 6 0 143.894 10.5827 9 8 6 0 150.418 9.17111 7 -8 6 0 130.362 9.03022 1 -8 6 0 137.575 10.4200 9 -8 6 0 160.107 11.6463 6 8 6 0 155.107 9.70230 3 9 -6 0 25.2528 5.48438 3 -9 -6 0 15.4623 4.02902 8 9 -6 0 19.0525 4.00079 5 -9 -6 0 12.4721 5.20591 9 9 -6 0 26.2993 6.19413 4 -9 -6 0 19.4767 6.01315 4 -9 -6 0 28.4664 5.79115 6 9 6 0 18.7273 4.34594 7 -9 6 0 16.4065 5.50385 9 -9 6 0 27.6556 6.70362 6 9 6 0 23.7906 5.61644 9 9 6 0 31.0814 5.40699 3 -9 6 0 22.8574 4.94511 1 -10 -6 0 120.063 12.5167 4 -10 -6 0 97.6158 8.60750 8 10 -6 0 77.6764 8.91745 3 10 -6 0 117.493 8.05543 5 -10 -6 0 83.6418 9.17497 6 -10 -6 0 96.8530 9.97921 9 10 -6 0 103.899 10.5063 4 10 6 0 104.903 9.27764 3 10 6 0 103.182 9.97914 9 -10 6 0 90.6605 10.1673 6 -10 6 0 94.1697 9.04571 1 -10 6 0 115.122 11.0312 9 10 6 0 103.404 8.82689 7 -11 -6 0 18.8065 5.34086 8 -11 -6 0 22.4638 6.82748 6 -11 -6 0 24.0816 6.95831 9 11 -6 0 8.82665 5.11167 4 -11 -6 0 35.7761 8.67466 4 11 -6 0 16.5138 5.72584 3 -11 6 0 15.9703 5.19629 1 11 6 0 8.28119 4.37367 3 11 6 0 21.2550 6.21355 9 -11 6 0 19.8936 6.60385 9 -11 6 0 29.4235 7.61982 6 11 6 0 15.3843 5.09021 7 12 -6 0 63.0289 9.70536 4 -12 -6 0 56.8854 8.62476 8 -12 -6 0 80.1041 11.6737 4 12 -6 0 75.0428 9.51902 3 -12 -6 0 67.3755 10.2026 6 -12 -6 0 91.3698 10.8483 9 12 6 0 66.2783 9.11052 3 -12 6 0 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0 76.6926 8.81799 4 3 11 0 68.8950 7.40862 9 3 11 0 76.8690 6.35193 2 -3 11 0 101.727 7.81578 9 3 11 0 74.3390 5.22974 3 3 11 0 71.4872 5.89070 7 -3 11 0 87.1642 5.36924 1 -3 11 0 90.4012 8.25173 6 -3 11 0 88.2032 7.06523 2 4 -11 0 5.46657 3.26043 4 -4 -11 0 11.3701 3.35885 6 -4 -11 0 6.53821 3.89089 9 4 -11 0 5.73758 2.82075 5 -4 -11 0 13.1591 2.89007 8 -4 -11 0 7.77021 4.34220 4 4 11 0 7.72707 2.50560 3 -4 11 0 6.03018 2.45621 1 -4 11 0 10.7905 4.41639 6 4 11 0 5.91842 2.75719 7 -4 11 0 8.38701 3.90617 9 -4 11 0 10.9548 3.37464 2 4 11 0 1.88851 2.89445 9 4 11 0 4.88269 2.85743 6 4 11 0 6.55930 3.19979 2 -5 -11 0 304.670 16.2415 9 5 -11 0 263.949 12.6166 5 -5 -11 0 300.402 18.5119 4 -5 -11 0 297.464 13.5105 6 5 -11 0 283.333 16.3446 4 -5 -11 0 273.183 12.0034 8 -5 11 0 288.875 12.8155 1 5 11 0 290.932 13.7681 2 -5 11 0 299.805 14.5492 2 5 11 0 291.089 13.5164 6 5 11 0 282.290 13.8351 7 5 11 0 239.880 15.0181 9 5 11 0 287.511 12.9706 3 -5 11 0 301.270 16.6008 6 -5 11 0 299.664 15.0062 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22.4940 5 -12 11 0 462.064 24.8668 9 12 11 0 418.340 23.5739 9 -12 11 0 426.439 25.3046 6 -13 -11 0 24.2170 8.16313 8 -13 -11 0 29.3861 8.86467 9 13 -11 0 32.4927 7.81012 5 -13 11 0 17.4523 8.81283 6 -13 11 0 24.5742 9.19771 9 13 11 0 29.2207 8.05043 9 -14 -11 0 8.39345 6.85955 9 -14 -11 0 0.63059 6.94009 8 14 11 0 0.10100 5.87869 9 -14 11 0 9.87108 7.60303 9 -14 11 0 5.45997 8.00435 6 -15 -11 0 34.1733 9.88242 8 -15 11 0 32.1099 10.2510 6 -16 -11 0 140.604 15.9042 8 -16 11 0 165.648 17.5488 6 -17 -11 0 26.3559 10.5457 8 0 -12 0 3078.12 91.8181 3 0 -12 0 3106.40 105.171 4 0 12 0 3048.15 98.5077 2 0 12 0 3041.22 94.4477 9 0 12 0 3246.55 91.6849 6 0 12 0 3196.16 93.8616 7 -1 -12 0 126.108 6.71337 3 1 -12 0 131.444 10.3687 4 1 -12 0 134.437 7.79026 5 -1 -12 0 135.424 8.40632 6 -1 -12 0 126.015 10.6011 4 1 12 0 128.335 8.42904 6 1 12 0 121.100 8.56283 2 1 12 0 110.924 8.83160 9 -1 12 0 129.371 8.89515 2 -1 12 0 132.680 7.53239 7 -1 12 0 138.782 9.21870 6 1 12 0 146.908 8.25994 7 -1 12 0 137.900 9.44824 9 2 -12 0 227.435 10.5716 5 -2 -12 0 198.551 10.6029 6 2 -12 0 205.592 13.3977 4 -2 -12 0 195.457 14.1139 4 -2 12 0 218.163 12.2326 9 -2 12 0 229.846 10.0455 7 -2 12 0 220.819 12.1821 6 2 12 0 204.755 10.6547 7 2 12 0 225.409 12.8987 9 -2 12 0 203.192 11.7732 2 2 12 0 208.197 11.0336 6 2 12 0 204.033 11.4798 2 3 -12 0 545.077 20.3763 5 3 -12 0 532.773 25.4932 4 -3 -12 0 576.505 21.4018 6 -3 -12 0 584.162 27.6736 4 -3 12 0 569.014 23.4134 2 3 12 0 573.662 24.2964 9 -3 12 0 563.939 20.0874 1 3 12 0 586.817 21.5863 6 -3 12 0 586.263 23.9667 6 3 12 0 553.116 21.9204 7 3 12 0 558.475 22.7658 2 -3 12 0 578.547 23.4149 9 3 12 0 586.738 20.4697 3 -4 -12 0 413.617 16.8457 6 -4 -12 0 384.764 22.0370 4 4 -12 0 387.179 20.4145 4 -4 -12 0 374.066 14.7150 8 4 -12 0 401.164 16.2769 5 -4 12 0 419.881 19.8310 6 4 12 0 398.692 17.3327 7 -4 12 0 390.575 18.2174 2 4 12 0 428.288 17.2453 6 4 12 0 390.199 15.8796 3 4 12 0 408.348 17.8310 2 4 12 0 383.024 19.3541 9 -4 12 0 417.333 15.8764 1 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0 585.125 22.4167 5 4 -13 0 627.800 28.6802 4 -4 13 0 637.979 25.7311 9 -4 13 0 596.476 25.3569 2 4 13 0 567.073 23.7439 7 4 13 0 640.155 23.8322 6 4 13 0 571.537 22.0954 3 -4 13 0 638.995 26.9640 6 4 13 0 603.176 24.7218 2 4 13 0 577.744 26.3981 9 -5 -13 0 145.619 10.2037 6 -5 -13 0 169.282 14.0829 4 5 -13 0 155.859 12.6210 4 5 -13 0 132.219 9.13154 5 -5 -13 0 154.632 8.86411 8 5 13 0 160.667 10.3304 2 5 13 0 148.494 9.02859 3 -5 13 0 135.510 10.9322 9 -5 13 0 185.801 13.5043 6 5 13 0 150.207 10.1197 6 -5 13 0 148.340 10.7747 2 -5 13 0 142.661 8.64377 1 5 13 0 153.374 12.2628 9 5 13 0 153.380 10.1789 7 6 -13 0 646.384 24.8749 5 6 -13 0 659.880 31.1309 4 -6 -13 0 678.354 25.9702 6 -6 -13 0 678.786 33.5878 4 -6 -13 0 633.805 29.0841 9 -6 -13 0 676.029 23.8767 8 -6 13 0 673.290 28.1453 9 6 13 0 667.750 26.2098 6 -6 13 0 671.361 25.3352 1 -6 13 0 648.814 30.1264 6 6 13 0 690.395 30.0529 9 6 13 0 685.431 27.1290 7 6 13 0 668.645 26.6697 2 6 13 0 713.305 25.8913 3 7 -13 0 52.6612 8.57766 4 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1074.48 35.2606 1 5 2 -1 1065.14 35.1923 3 -5 2 1 1112.30 38.5688 4 -5 2 1 1090.31 33.0787 2 5 2 -1 1139.33 33.9319 2 5 2 -1 1092.47 34.4990 7 4 -2 -1 2010.22 57.4367 7 4 -2 -1 1897.95 59.9085 3 -4 -2 1 1902.68 59.2244 1 -4 -2 1 1896.85 64.1181 4 -4 2 1 1906.82 58.6838 1 -4 2 1 1981.18 62.8884 4 4 2 -1 1939.52 58.3969 2 4 2 -1 1892.17 58.1255 3 -4 2 1 1868.12 57.8366 2 4 2 -1 1940.47 57.7818 7 -3 -2 1 13.9996 2.32985 1 -3 -2 1 21.3389 3.14861 4 3 -2 -1 11.6397 2.44057 3 3 -2 -1 12.1495 1.89203 4 3 -2 -1 12.7715 1.49226 7 3 2 -1 18.0244 2.07764 3 -3 2 1 15.8914 1.39318 2 3 2 -1 22.0421 2.20656 7 -3 2 1 12.9675 1.83000 1 3 2 -1 14.7507 1.56511 2 2 -2 -1 8.59297 1.59144 3 2 -2 -1 6.95269 1.22656 4 -2 -2 1 5.33876 1.67236 4 -2 -2 1 4.91098 1.67509 1 2 2 -1 6.08235 1.14626 3 2 2 -1 4.91562 1.23911 7 2 2 -1 3.04964 0.94682 2 -2 2 1 7.50192 1.01522 2 -2 2 1 12.0924 1.47145 1 -1 -2 1 11.4367 1.11864 1 -1 -2 1 8.20597 1.33460 4 1 -2 -1 10.6533 1.15870 4 1 -2 -1 13.4146 0.99192 7 1 -2 -1 9.48304 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465.103 15.7596 3 1 -3 -4 467.670 17.2309 4 1 -3 -4 485.953 15.7326 7 1 3 -4 469.094 17.6344 7 1 3 -4 471.023 17.6045 2 -1 3 4 472.187 16.7904 2 1 3 -4 459.170 15.1626 3 -1 3 4 473.116 17.0376 1 0 -3 4 3.30357 1.25012 4 0 -3 -4 3.41564 1.00006 3 0 -3 -4 4.68543 1.83889 4 0 -3 -4 5.28372 1.20529 7 0 3 -4 3.26007 1.07859 1 0 3 -4 1.82910 1.42233 2 0 3 4 2.94846 1.26748 2 0 3 -4 2.66920 1.52573 7 0 3 4 2.66618 1.03175 1 0 3 4 1.88467 0.91725 7 1 -3 4 8710.27 255.832 3 -1 -3 -4 9056.40 255.265 7 -1 -3 -4 8790.33 258.464 1 1 -3 4 8888.09 275.285 4 -1 -3 -4 9162.34 277.810 4 -1 -3 -4 8908.81 255.293 3 -1 3 -4 8681.64 265.723 2 -1 3 -4 8889.10 255.353 7 1 3 4 8833.50 255.208 7 1 3 4 8975.54 264.608 2 -1 3 -4 9162.38 258.709 1 -2 -3 -4 265.691 13.8196 4 -2 -3 -4 260.590 9.92519 3 -2 -3 -4 272.155 9.03262 1 2 -3 4 270.110 9.30535 3 2 -3 4 265.761 11.7297 4 -2 -3 -4 272.190 9.85420 7 -2 3 -4 277.986 8.81855 7 -2 3 -4 266.562 10.0578 1 2 3 4 264.690 10.1654 2 -2 3 -4 281.499 11.5124 2 2 3 4 270.034 9.82520 7 3 -3 4 1917.77 64.4514 4 3 -3 4 1930.75 58.1110 3 -3 -3 -4 1987.94 67.5391 4 -3 -3 -4 1897.15 57.8342 7 -3 -3 -4 2005.45 57.8850 1 3 -3 4 1900.70 56.2995 7 3 3 4 2047.47 59.7736 2 -3 3 -4 2047.85 56.3778 7 -3 3 -4 1912.69 58.9908 1 -3 3 -4 1971.73 61.4017 2 3 3 4 1868.61 57.9049 7 4 -3 4 222.194 11.8625 4 4 -3 4 227.815 9.76188 3 -4 -3 -4 229.646 8.61397 1 -4 -3 -4 228.317 13.7409 4 4 -3 4 237.680 7.18706 7 4 3 4 220.974 9.55329 3 -4 3 -4 246.028 10.6410 2 4 3 4 215.062 8.93029 7 4 3 4 235.787 8.79105 2 -4 3 -4 224.571 9.57386 1 5 -3 4 643.585 26.0654 4 -5 -3 -4 666.450 20.8016 1 -5 -3 -4 595.761 27.5372 4 5 -3 4 609.090 22.1957 3 5 3 4 626.416 21.7691 3 -5 3 -4 577.633 21.3326 2 5 3 4 630.086 20.2598 2 5 3 4 629.543 20.8026 7 -5 3 -4 615.656 21.7032 1 -6 -3 -4 285.925 16.1573 9 -6 -3 -4 259.493 12.3999 6 -6 -3 -4 282.166 16.7591 4 -6 -3 -4 278.471 11.0548 1 6 -3 4 267.509 12.7200 3 6 -3 4 294.481 15.7981 4 -6 3 -4 277.511 11.9913 1 6 3 4 255.227 10.7846 7 -6 3 -4 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13.5450 3 -8 -4 4 249.667 14.1792 1 -8 -4 4 247.882 14.4124 4 8 -4 -4 267.795 13.2139 4 -8 4 4 245.653 13.8173 1 8 4 -4 263.405 13.6896 7 8 4 -4 239.181 13.4410 3 -8 4 4 242.650 13.5703 6 -8 4 4 223.897 12.4670 8 -7 -4 4 10.1885 3.55037 4 7 -4 -4 14.5318 4.19118 3 7 -4 -4 12.1471 3.12044 4 -7 -4 4 9.69453 3.63094 8 7 -4 -4 9.19689 2.72351 7 -7 -4 4 15.4022 4.07497 1 -7 4 4 11.1328 3.93196 6 7 4 -4 27.9986 4.70548 3 7 4 -4 12.7229 2.73531 2 -7 4 4 12.7171 3.77756 1 7 4 -4 10.2649 3.42723 7 -6 -4 4 74.0097 6.99115 1 -6 -4 4 95.1356 7.69385 4 6 -4 -4 89.5532 7.34904 3 6 -4 -4 99.7994 5.76746 7 6 -4 -4 89.7339 6.35864 4 -6 4 4 96.5767 5.75693 2 6 4 -4 97.6268 7.15171 7 6 4 -4 86.8892 6.02104 2 6 4 -4 81.9542 6.67725 3 -6 4 4 86.1622 6.89732 1 5 -4 -4 1596.37 52.5245 4 -5 -4 4 1562.29 52.6448 1 -5 -4 4 1608.55 54.6082 4 5 -4 -4 1508.49 48.5042 7 5 -4 -4 1611.88 51.7676 3 -5 4 4 1626.20 50.5581 2 5 4 -4 1619.69 51.3062 2 5 4 -4 1661.88 50.9676 3 -5 4 4 1573.90 51.5073 1 5 4 -4 1577.68 51.2011 7 -4 -4 4 284.853 13.0649 1 -4 -4 4 296.410 12.9997 4 4 -4 -4 290.969 11.4218 4 4 -4 -4 276.657 12.1476 3 4 -4 -4 288.950 10.7328 7 -4 4 4 260.720 11.2324 2 4 4 -4 271.507 11.7979 3 -4 4 4 291.738 12.4911 1 4 4 -4 272.402 12.5310 7 4 4 -4 268.810 11.8295 2 3 -4 -4 278.509 11.1581 3 -3 -4 4 270.026 11.4596 1 -3 -4 4 284.135 12.0746 4 3 -4 -4 270.382 10.8185 4 3 -4 -4 263.893 10.1552 7 3 4 -4 283.070 11.1767 3 3 4 -4 281.399 12.1433 7 -3 4 4 280.226 11.2028 2 3 4 -4 270.969 11.6315 2 -3 4 4 286.213 11.7452 1 2 -4 -4 570.222 18.7074 3 -2 -4 4 556.560 20.2425 4 2 -4 -4 556.663 19.8793 4 2 -4 -4 548.477 18.1025 7 -2 -4 4 562.892 18.9296 1 -2 4 4 583.683 19.5423 1 2 4 -4 572.318 20.2067 2 2 4 -4 525.380 18.4056 3 2 4 -4 544.842 19.9758 7 -2 4 4 538.699 19.3424 2 -1 -4 4 17.0284 2.29970 4 -1 -4 4 14.1929 1.86714 1 1 -4 -4 16.8629 1.98191 7 1 -4 -4 17.2784 2.53766 4 1 -4 -4 14.0229 1.88116 3 -1 4 4 17.8364 2.48228 1 1 4 -4 15.1038 1.82007 3 -1 4 4 13.8963 1.79926 7 -1 4 4 14.5930 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60.4535 13.1675 9 -17 -5 -5 49.0345 12.8291 6 -17 5 -5 52.3694 13.0320 9 17 5 5 50.9390 11.1777 9 -17 5 -5 35.2258 12.2513 6 -18 -6 5 13.1175 8.61006 8 -18 6 5 13.0786 9.02193 6 -17 -6 5 106.703 13.5184 8 -17 6 5 112.102 13.8638 6 -16 -6 5 -5.8671 5.92036 8 -16 6 5 6.98992 8.17067 6 -15 -6 5 770.320 34.2171 8 -15 6 5 725.239 33.3757 6 -14 -6 5 13.3925 7.59132 8 -14 6 5 8.48493 7.01842 6 -13 -6 5 57.7304 9.96080 8 -13 6 5 82.9459 11.0011 6 -12 -6 5 45.8586 8.66465 8 12 -6 -5 30.0156 7.15860 3 12 6 -5 24.2817 6.96284 3 12 6 -5 34.9544 7.05099 7 -12 6 5 19.6916 6.99179 1 -12 6 5 30.5726 7.39931 6 -12 6 5 35.1144 7.24462 8 11 -6 -5 1125.52 43.9036 3 -11 -6 5 1180.06 42.3619 8 11 -6 -5 1199.60 39.7571 5 -11 -6 5 1119.75 44.2858 1 11 6 -5 1173.89 44.1990 7 11 6 -5 1219.60 45.3806 3 -11 6 5 1195.07 43.1066 6 -11 6 5 1237.11 46.9357 1 -11 6 5 1138.91 40.5641 8 10 -6 -5 0.68863 3.85894 3 -10 -6 5 -1.3808 3.94566 4 -10 -6 5 -1.6540 3.13983 1 10 -6 -5 6.45030 4.20103 5 -10 -6 5 2.34987 4.75787 8 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5.71720 8 -12 10 5 7.34700 7.02250 6 11 -10 -5 134.866 12.2598 3 11 -10 -5 117.576 10.7075 5 -11 -10 5 114.404 11.4519 8 -11 10 5 113.516 12.4771 6 11 10 -5 133.155 12.0552 3 -11 10 5 108.897 11.3084 1 10 -10 -5 114.659 11.2896 3 10 -10 -5 122.331 10.3064 5 -10 -10 5 114.762 12.1087 4 -10 -10 5 100.022 10.1155 8 10 10 -5 107.140 10.4052 3 10 10 -5 98.4473 10.6329 7 -10 10 5 90.6485 11.0301 6 -10 10 5 114.293 10.5783 1 -9 -10 5 273.342 17.9313 4 9 -10 -5 264.661 15.9858 3 9 -10 -5 296.719 15.4941 5 -9 -10 5 269.899 14.9941 8 -9 10 5 238.851 15.0241 1 9 10 -5 250.521 15.8554 7 -9 10 5 299.054 17.9929 6 9 10 -5 292.557 15.7842 3 8 -10 -5 88.7628 8.35241 5 8 -10 -5 79.4223 8.17570 3 -8 -10 5 91.3720 8.20065 8 -8 -10 5 70.5983 9.10480 4 -8 10 5 93.0060 8.28571 1 8 10 -5 79.3910 7.95408 3 -8 10 5 86.4656 9.88565 6 8 10 -5 98.2813 9.52161 7 7 -10 -5 96.7577 8.26760 5 -7 -10 5 68.4955 6.79661 8 7 -10 -5 86.5320 7.79941 3 -7 -10 5 84.8163 9.50315 4 7 10 -5 79.4651 7.36639 3 -7 10 5 90.8878 7.66544 9 7 10 -5 88.1936 8.95977 9 7 10 -5 92.9222 7.88243 2 7 10 -5 80.0965 8.27753 7 -7 10 5 86.7710 7.37971 1 -7 10 5 72.8363 8.65864 6 -6 -10 5 176.300 9.68331 8 6 -10 -5 149.865 9.83120 5 -6 -10 5 173.026 12.2797 4 6 -10 -5 184.477 10.6664 3 6 -10 -5 174.518 9.88319 8 -6 10 5 163.112 10.0037 9 -6 10 5 181.788 10.0229 1 6 10 -5 186.479 11.0779 2 -6 10 5 202.111 11.4551 2 -6 10 5 183.556 12.0383 6 6 10 -5 164.968 11.6833 9 6 10 -5 195.191 10.6041 3 6 10 -5 189.255 11.7788 7 -6 10 5 125.917 8.81403 8 -5 -10 5 269.605 15.9872 4 5 -10 -5 316.139 12.3697 7 5 -10 -5 300.972 16.2108 4 5 -10 -5 276.396 13.6521 5 5 -10 -5 301.828 13.8741 3 5 -10 -5 280.429 12.6237 8 5 10 -5 298.266 14.7704 2 -5 10 5 282.357 14.4247 2 -5 10 5 306.210 15.0605 6 -5 10 5 304.234 13.1333 1 -5 10 5 295.577 13.5405 9 5 10 -5 308.675 15.4021 7 -5 10 5 294.793 12.6251 8 5 10 -5 323.465 15.9377 9 -4 -10 5 2535.87 74.9841 1 -4 -10 5 2429.10 81.8428 4 4 -10 -5 2401.88 81.3670 4 4 -10 -5 2394.96 69.8927 5 4 -10 -5 2312.60 71.9436 7 4 -10 -5 2305.93 73.3706 3 4 10 -5 2338.60 75.5705 7 4 10 -5 2355.57 74.6062 9 -4 10 5 2401.67 72.1886 7 -4 10 5 2383.45 71.9021 9 -4 10 5 2359.97 72.3063 6 -4 10 5 2383.67 77.0678 2 -4 10 5 2448.92 73.0088 1 4 10 -5 2406.35 77.3190 2 -3 -10 5 143.554 10.5581 4 3 -10 -5 153.735 7.92277 7 3 -10 -5 159.800 11.0165 4 3 -10 -5 149.755 8.30913 3 -3 -10 5 151.971 8.29753 1 3 -10 -5 159.129 9.34153 5 -3 10 5 153.356 9.60413 2 -3 10 5 156.268 8.01230 7 -3 10 5 152.529 8.80328 9 3 10 -5 168.826 10.1507 2 -3 10 5 154.804 9.38238 6 3 10 -5 162.830 10.0157 7 3 10 -5 154.488 9.97177 9 2 -10 -5 572.607 20.8181 3 2 -10 -5 579.460 25.9309 4 -2 -10 5 586.536 24.7731 4 -2 -10 5 562.142 20.7200 1 2 -10 -5 570.473 20.5436 7 2 -10 -5 596.977 21.4143 5 -2 10 5 570.440 22.8149 2 -2 10 5 548.579 21.0923 6 2 10 -5 603.679 23.6279 2 -2 10 5 590.414 20.7438 7 2 10 -5 597.474 22.8972 7 1 -10 -5 37.0108 3.87850 3 1 -10 -5 33.1887 4.28986 6 -1 -10 5 41.7315 5.71914 4 1 -10 -5 40.9035 6.70588 4 1 -10 -5 40.7345 4.07232 7 -1 10 5 39.9692 4.88175 2 -1 10 5 36.0894 4.41258 6 -1 10 5 34.9913 4.66153 9 1 10 -5 45.5353 5.12813 7 -1 10 5 43.5742 4.21711 7 1 10 -5 34.9499 4.89833 2 1 10 -5 36.4524 5.48077 9 0 -10 5 1221.63 44.5216 4 0 -10 -5 1192.44 38.9280 3 0 -10 5 1256.07 36.6078 5 0 -10 -5 1220.62 39.1400 7 0 -10 -5 1134.49 46.7140 4 0 -10 -5 1190.40 38.3952 6 0 10 5 1185.98 38.5957 6 0 10 -5 1214.71 40.6037 7 0 10 5 1219.83 41.6231 2 0 10 5 1207.49 39.2505 7 0 10 -5 1199.89 38.9248 1 0 10 -5 1273.97 42.8520 2 0 10 -5 1310.36 41.9534 9 -1 -10 -5 24.4823 3.47101 7 -1 -10 -5 20.6900 3.04971 8 -1 -10 -5 36.0565 4.35545 6 -1 -10 -5 30.1475 3.61225 3 -1 -10 -5 25.7405 6.11679 4 1 -10 5 21.5396 3.28490 5 1 -10 5 27.1703 4.92033 4 -1 10 -5 27.6441 3.50049 5 1 10 5 22.7795 3.89893 2 1 10 5 22.3865 3.80944 6 1 10 5 20.8249 3.36529 7 1 10 5 19.8183 4.34552 9 -1 10 -5 27.4783 3.51665 1 -1 10 -5 23.5379 3.93287 7 -1 10 -5 29.2954 4.60270 2 -1 10 -5 33.0157 5.33058 9 2 -10 5 1951.92 67.2435 4 -2 -10 -5 1947.80 59.8140 3 2 -10 5 1929.38 55.9483 5 -2 -10 -5 1916.41 58.4462 6 -2 -10 -5 1969.08 55.5336 8 -2 -10 -5 1900.62 71.1546 4 -2 -10 -5 1890.55 61.2593 9 2 10 5 1953.79 60.3430 7 -2 10 -5 1950.34 60.2392 1 -2 10 -5 1943.09 64.3494 2 -2 10 -5 1937.43 61.8350 9 -2 10 -5 1943.28 55.8949 5 2 10 5 1971.97 62.9626 2 2 10 5 1979.32 58.7757 6 2 10 5 1907.58 61.5695 9 -3 -10 -5 433.312 16.4253 3 3 -10 5 422.421 15.5808 5 -3 -10 -5 368.005 14.4902 8 -3 -10 -5 403.903 16.5873 6 -3 -10 -5 389.361 18.3951 9 3 -10 5 415.813 19.7699 4 -3 -10 -5 434.681 23.5182 4 -3 10 -5 390.645 15.8569 1 -3 10 -5 405.638 15.3649 5 3 10 5 394.518 16.9312 2 -3 10 -5 374.183 18.1119 2 3 10 5 394.564 18.6628 9 3 10 5 385.150 16.2123 7 3 10 5 405.964 16.6341 6 -3 10 -5 425.674 18.8634 9 4 -10 5 348.561 14.1686 5 -4 -10 -5 324.592 17.2816 9 -4 -10 -5 344.166 13.6148 8 -4 -10 -5 356.187 21.7534 4 -4 -10 -5 341.489 15.4010 6 4 -10 5 346.602 18.3141 4 -4 10 -5 358.503 14.9021 1 -4 10 -5 401.339 20.0400 6 4 10 5 368.042 15.8735 6 -4 10 -5 323.968 13.9591 5 4 10 5 336.795 14.9963 7 4 10 5 343.672 17.7043 9 -4 10 -5 374.448 17.8464 9 -4 10 -5 344.649 16.9737 2 4 10 5 384.969 15.6288 2 -5 -10 -5 1.93036 3.67826 9 5 -10 5 12.8039 4.70125 4 5 -10 5 10.3446 3.20170 5 -5 -10 -5 13.2662 6.01560 4 -5 -10 -5 12.3613 3.36111 8 -5 -10 -5 7.21284 3.67316 6 5 10 5 3.55278 4.04419 9 -5 10 -5 13.5331 6.34130 6 -5 10 -5 7.86950 3.13397 1 -5 10 -5 15.5457 5.02930 9 5 10 5 10.8521 3.22581 7 5 10 5 5.61718 2.85716 2 5 10 5 9.15031 3.66463 6 5 10 5 8.86427 2.87420 3 6 -10 5 529.571 19.8711 5 -6 -10 -5 498.823 24.5836 9 -6 -10 -5 522.734 21.7617 6 -6 -10 -5 497.524 29.0374 4 -6 -10 -5 529.550 19.6442 8 6 -10 5 530.509 25.6083 4 -6 10 -5 550.290 21.6770 1 6 10 5 523.142 21.1077 7 -6 10 -5 603.507 27.5890 6 6 10 5 538.737 21.4900 3 -6 10 -5 538.083 24.4488 9 6 10 5 508.412 24.8708 9 7 -10 5 154.338 12.9099 4 -7 -10 -5 152.757 13.7164 9 -7 -10 -5 164.124 11.3051 6 7 -10 5 150.876 9.54205 5 -7 -10 -5 164.058 9.92878 8 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-5 34.5002 6.70380 1 10 10 5 40.7194 6.77777 7 -10 10 -5 54.8946 11.0999 6 10 10 5 31.5851 6.49398 3 10 10 5 24.2852 8.19977 9 -10 10 -5 35.3186 9.80176 9 -11 -10 -5 64.7044 11.7128 9 -11 -10 -5 69.7868 10.6520 6 -11 -10 -5 54.2522 8.15677 8 11 -10 5 48.8133 7.08651 5 -11 10 -5 15.6862 8.46322 9 11 10 5 55.0355 10.8545 9 -11 10 -5 43.5941 10.4676 6 -12 -10 -5 20.9647 8.75510 6 -12 -10 -5 25.7637 7.22284 8 -12 -10 -5 43.9475 11.5101 9 12 10 5 28.2140 9.19851 9 -12 10 -5 34.4129 10.3361 6 -12 10 -5 42.7091 10.4449 9 -13 -10 -5 169.730 17.8707 9 -13 -10 -5 164.593 13.9068 8 -13 -10 -5 154.042 16.0992 6 13 10 5 191.213 17.3157 9 -13 10 -5 127.109 16.5822 9 -13 10 -5 143.273 17.0219 6 -14 -10 -5 10.1838 7.18155 8 -14 -10 -5 13.2169 8.92215 6 -14 -10 -5 6.59584 8.92827 9 -14 10 -5 5.66054 8.85516 6 -14 10 -5 11.2901 9.13292 9 14 10 5 21.1381 8.97842 9 -15 -10 -5 0.58712 7.40088 8 -15 -10 -5 -4.4327 8.14837 9 -15 -10 -5 1.57818 8.92062 6 -15 10 -5 5.41309 9.75044 9 15 10 5 5.52921 7.10885 9 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32.6803 3.83145 1 2 7 -7 31.0539 4.62382 2 -2 7 7 26.9811 3.35002 7 -2 7 7 27.4836 4.12274 2 2 7 -7 21.4399 4.48256 7 1 -7 -7 117.694 8.96549 4 1 -7 -7 112.177 6.49483 3 -1 -7 7 110.246 7.39718 4 -1 -7 7 115.769 6.52288 1 1 -7 -7 109.268 6.37070 7 -1 7 7 114.646 6.42505 1 1 7 -7 112.741 8.42886 7 1 7 -7 112.559 8.13848 2 -1 7 7 103.315 6.26507 7 0 -7 -7 106.083 6.21481 7 0 -7 -7 101.472 6.06961 3 0 -7 -7 124.842 9.72310 4 0 -7 7 101.930 7.25020 4 0 7 -7 98.7659 6.08024 1 0 7 7 101.599 6.85991 2 0 7 7 95.0865 5.94611 7 0 7 -7 103.399 7.67420 7 0 7 -7 100.228 7.87381 2 -1 -7 -7 1007.79 33.4743 7 -1 -7 -7 1113.03 42.1039 4 -1 -7 -7 1058.39 33.7653 3 1 -7 7 982.607 37.1192 4 -1 7 -7 1058.07 34.8024 7 -1 7 -7 1004.64 37.3009 2 1 7 7 1035.42 35.3814 2 1 7 7 1010.36 33.5512 7 -1 7 -7 1061.11 33.9671 1 2 -7 7 55.8633 5.92549 4 -2 -7 -7 51.9738 4.43318 3 -2 -7 -7 55.1868 4.24968 8 -2 -7 -7 53.9671 4.56494 7 2 -7 7 50.0420 4.32924 5 -2 -7 -7 55.3702 4.87507 6 -2 -7 -7 68.9334 8.69061 4 2 7 7 52.1367 4.68965 6 -2 7 -7 54.6368 6.19302 2 -2 7 -7 44.8052 4.08655 5 -2 7 -7 47.5107 4.50162 1 2 7 7 54.1908 4.54075 7 2 7 7 46.0959 4.65534 2 -3 -7 -7 1903.12 59.4252 3 3 -7 7 1843.82 65.8101 4 -3 -7 -7 1940.63 57.6269 6 3 -7 7 1962.99 55.1354 5 -3 -7 -7 1983.32 59.3134 7 -3 -7 -7 1858.20 60.9844 9 -3 -7 -7 2026.64 72.1653 4 -3 -7 -7 1926.13 54.8799 8 3 7 7 1946.77 61.3108 9 3 7 7 1959.26 57.8877 6 -3 7 -7 1881.74 61.3702 9 -3 7 -7 1861.75 64.2141 2 -3 7 -7 1894.85 54.9605 5 3 7 7 1878.38 59.2016 7 3 7 7 1970.52 61.3863 2 -4 -7 -7 132.684 7.70210 3 -4 -7 -7 114.262 7.52630 6 4 -7 7 125.910 9.58049 4 4 -7 7 116.644 7.04976 5 -4 -7 -7 126.930 6.72379 8 -4 -7 -7 109.170 9.14184 9 -4 -7 -7 130.286 12.6573 4 -4 7 -7 113.479 9.46002 9 -4 7 -7 114.285 6.92814 5 -4 7 -7 130.129 7.64709 1 4 7 7 129.467 7.46628 2 4 7 7 116.175 7.21869 7 4 7 7 107.807 9.05931 9 -4 7 -7 119.259 9.18867 2 -5 -7 -7 4.04493 2.87461 6 5 -7 7 9.60025 2.94195 5 -5 -7 -7 10.9539 4.30322 9 -5 -7 -7 9.03625 2.74923 8 -5 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3 -2 -8 7 1916.81 64.3195 4 2 -8 -7 1905.68 58.7033 7 2 -8 -7 1892.82 56.9079 6 -2 -8 7 1899.01 59.7008 1 2 8 -7 1885.34 62.0024 7 2 8 -7 1929.03 63.5018 2 -2 8 7 1828.09 56.6436 6 -2 8 7 1976.38 58.6186 1 -2 8 7 1771.53 61.6858 2 -2 8 7 1978.18 58.9683 7 1 -8 -7 156.797 11.0277 4 1 -8 -7 129.496 7.60667 6 1 -8 -7 138.432 7.71421 3 -1 -8 7 158.636 7.94092 1 1 -8 -7 140.070 7.65182 7 -1 -8 7 144.589 9.07602 4 1 8 -7 162.945 10.0050 2 -1 8 7 133.026 7.59764 6 -1 8 7 136.738 8.57420 2 -1 8 7 148.996 7.77104 7 1 8 -7 148.763 9.73697 7 0 -8 7 287.168 14.1272 4 0 -8 -7 289.501 12.1540 7 0 -8 -7 278.178 11.0560 8 0 -8 -7 267.777 11.8281 6 0 -8 -7 295.469 16.8446 4 0 -8 -7 274.815 12.0074 3 0 8 -7 288.700 14.4175 7 0 8 -7 273.562 11.9327 1 0 8 7 289.970 12.1369 6 0 8 7 291.579 12.2023 7 0 8 -7 305.964 11.6632 5 0 8 7 263.750 12.9232 2 0 8 -7 320.395 15.0614 2 -1 -8 -7 22.2918 3.38219 6 1 -8 7 20.6589 3.12972 5 -1 -8 -7 21.3728 5.51092 4 -1 -8 -7 23.9752 3.31462 3 -1 -8 -7 19.5093 3.15488 7 1 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59.8852 8 -4 10 7 2083.15 59.9027 8 -4 10 7 2102.11 63.5484 6 4 10 -7 2016.60 67.6748 7 -4 10 7 2058.04 63.9062 7 4 10 -7 2064.46 68.9311 2 -4 10 7 2019.17 68.0569 2 -3 -10 7 62.5660 5.16613 5 3 -10 -7 51.7754 6.44187 5 -3 -10 7 57.9423 5.43690 1 -3 -10 7 64.3363 7.03358 4 3 -10 -7 53.5738 5.00212 7 3 -10 -7 62.9651 5.20284 8 3 -10 -7 49.4786 5.18435 3 -3 10 7 51.0405 4.83646 8 -3 10 7 54.2779 5.29664 9 -3 10 7 64.6878 5.33357 7 -3 10 7 52.3522 5.95171 2 3 10 -7 53.0082 6.60216 9 -3 10 7 43.1745 5.34518 6 3 10 -7 56.5882 6.82529 7 3 10 -7 35.4300 5.65782 2 -2 -10 7 752.167 24.7966 5 -2 -10 7 763.453 26.9125 1 2 -10 -7 715.757 26.3038 6 2 -10 -7 723.588 26.5734 3 -2 -10 7 756.713 30.2902 4 2 -10 -7 756.748 33.1366 4 2 -10 -7 777.477 26.5852 7 2 -10 -7 749.124 24.5099 8 2 -10 -7 773.343 27.8394 5 2 10 -7 782.508 29.5991 7 2 10 -7 817.882 29.5982 9 -2 10 7 793.410 26.7223 7 -2 10 7 744.261 26.5315 6 2 10 -7 750.869 29.8466 2 -2 10 7 764.521 24.5025 8 -2 10 7 728.402 28.6279 2 1 -10 -7 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479.190 19.1887 1 3 6 -9 495.047 21.7492 2 3 6 -9 484.925 21.0413 7 -3 6 9 466.877 18.4662 7 -3 6 9 478.610 17.0168 8 -3 6 9 486.556 20.2181 1 -3 6 9 456.092 20.2562 2 2 -6 -9 19.9191 2.96531 8 2 -6 -9 17.4034 3.31618 3 -2 -6 9 20.5188 3.52900 1 2 -6 -9 20.3618 3.34409 7 -2 -6 9 19.5157 3.31446 4 -2 6 9 19.3355 4.23919 2 -2 6 9 17.7754 4.04828 1 2 6 -9 20.0761 4.48802 7 -2 6 9 14.2181 3.00221 7 -2 6 9 17.0754 2.84721 8 2 6 -9 21.4236 5.00623 2 -1 -6 9 45.3633 4.61141 1 1 -6 -9 57.2620 4.83323 3 1 -6 -9 48.9420 4.54195 7 1 -6 -9 50.5635 4.17937 8 -1 -6 9 56.1433 5.13034 4 1 -6 -9 54.9231 5.34053 4 -1 6 9 46.7830 4.60105 7 1 6 -9 54.6134 6.37456 7 -1 6 9 44.4047 5.27323 2 -1 6 9 50.2731 5.22471 1 1 6 -9 54.3823 6.75711 2 1 6 -9 52.5254 4.70097 5 0 -6 -9 3.30982 1.99176 7 0 -6 -9 2.43419 1.62895 8 0 -6 -9 5.67968 2.82722 4 0 -6 9 0.68063 1.79266 4 0 -6 -9 1.71981 1.72924 3 0 -6 9 -0.2529 1.83366 5 0 6 9 3.71849 2.65668 2 0 6 -9 3.04616 2.23906 5 0 6 -9 0.54941 3.08891 2 0 6 -9 8.93596 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421.891 19.1637 9 -3 6 -9 445.035 17.4261 1 -3 6 -9 433.291 21.2494 2 -3 6 -9 443.290 20.4996 9 3 6 9 473.928 18.0865 2 -3 6 -9 413.134 15.8063 5 3 6 9 412.140 16.6352 7 -4 -6 -9 146.467 8.09470 7 4 -6 9 153.645 10.6205 4 -4 -6 -9 148.868 7.80425 8 -4 -6 -9 139.687 10.6866 9 -4 -6 -9 155.607 12.9547 4 -4 -6 -9 164.725 9.00530 3 -4 -6 -9 144.940 8.68476 6 4 -6 9 149.174 8.08323 5 4 6 9 144.012 8.56319 2 4 6 9 133.049 8.04304 7 -4 6 -9 150.333 12.0529 2 -4 6 -9 143.884 11.4140 9 -4 6 -9 138.498 7.82577 5 -4 6 -9 127.499 8.29132 1 4 6 9 132.632 10.8301 9 5 -6 9 209.494 13.6170 4 -5 -6 -9 198.760 13.8482 9 -5 -6 -9 203.158 16.3626 4 5 -6 9 211.236 10.1926 5 -5 -6 -9 213.249 11.3747 6 -5 -6 -9 200.604 9.56212 8 5 6 9 184.234 13.4445 9 -5 6 -9 211.821 10.9951 1 5 6 9 198.240 10.2217 7 -5 6 -9 213.711 14.9236 9 5 6 9 184.255 10.5885 3 -5 6 -9 207.778 11.4899 6 -5 6 -9 195.338 9.83093 5 -6 -6 -9 36.8901 8.80783 4 -6 -6 -9 30.9660 5.30132 6 -6 -6 -9 35.9693 7.62058 9 6 -6 9 24.8400 6.17817 4 6 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4 9 6 9 1369.93 55.6501 9 -9 6 -9 1311.79 54.3304 9 -9 6 -9 1422.14 49.4847 1 9 6 9 1408.66 49.5348 3 -9 6 -9 1372.93 50.2915 6 -10 -6 -9 82.5579 10.5104 6 -10 -6 -9 75.6518 7.88410 8 -10 -6 -9 80.7654 14.0874 9 -10 6 -9 87.2440 13.2788 9 10 6 9 77.4105 9.19040 3 -10 6 -9 88.9253 9.03813 1 -10 6 -9 74.7832 10.9272 6 10 6 9 87.5496 13.3070 9 -11 -6 -9 180.063 12.1502 8 -11 -6 -9 167.959 15.0518 6 -11 -6 -9 191.193 18.5957 9 -11 6 -9 183.373 17.9051 9 11 6 9 179.341 17.6264 9 -11 6 -9 185.406 16.6402 6 -12 -6 -9 73.9671 11.5926 6 -12 -6 -9 68.0254 8.58931 8 -12 -6 -9 66.8037 13.3232 9 12 6 9 56.1730 11.6905 9 -12 6 -9 77.1327 13.6789 9 -12 6 -9 65.8445 12.5396 6 -13 -6 -9 383.030 23.5948 6 -13 -6 -9 351.280 25.2264 9 -13 -6 -9 365.804 19.3622 8 -13 6 -9 360.345 25.5949 9 13 6 9 370.335 24.7294 9 -13 6 -9 373.815 25.7913 6 -14 -6 -9 -2.9308 7.98365 9 -14 -6 -9 9.55198 9.05495 6 -14 6 -9 0.39618 9.87268 6 14 6 9 -3.6480 7.32761 9 -14 6 -9 -1.6549 8.51487 9 -15 -6 -9 313.689 24.1959 6 -15 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6.00633 8 -11 7 9 9.54532 5.84858 6 10 -7 -9 240.972 15.5632 3 -10 -7 9 264.743 15.8931 8 10 -7 -9 227.457 14.5571 5 -10 -7 9 242.294 15.5461 1 -10 7 9 242.017 14.8558 8 10 7 -9 231.278 14.8162 3 -10 7 9 233.000 16.2330 1 -10 7 9 222.757 14.8783 6 10 7 -9 214.990 15.3331 7 -9 -7 9 218.131 14.1939 8 -9 -7 9 190.421 13.5278 1 9 -7 -9 187.658 13.6761 3 9 -7 -9 193.905 13.1402 5 9 7 -9 204.275 14.1938 7 -9 7 9 198.404 13.1802 8 9 7 -9 185.207 12.6866 3 -9 7 9 170.806 13.6029 1 -9 7 9 188.311 13.3010 6 8 -7 -9 459.706 21.0104 5 -8 -7 9 460.737 21.0643 8 8 -7 -9 491.657 23.0775 3 -8 -7 9 501.486 23.2409 1 8 -7 -9 476.264 19.9819 7 -8 7 9 483.240 23.1512 1 -8 7 9 476.192 21.0450 8 -8 7 9 460.271 20.8380 6 8 7 -9 438.595 21.4214 2 8 7 -9 474.937 23.1146 7 8 7 -9 469.838 21.1743 3 7 -7 -9 378.850 19.3192 3 7 -7 -9 391.850 18.7734 5 -7 -7 9 420.113 20.6235 1 7 -7 -9 421.288 17.7939 7 -7 -7 9 411.245 18.3858 8 7 -7 -9 356.256 17.3673 8 7 7 -9 408.317 19.6780 2 -7 7 9 423.793 20.6188 1 7 7 -9 427.728 20.8574 7 -7 7 9 442.852 18.8991 6 7 7 -9 424.880 18.7881 3 -7 7 9 421.915 19.8273 2 -7 7 9 402.208 18.0905 8 6 -7 -9 2.29348 2.41124 7 6 -7 -9 6.17401 3.91784 5 6 -7 -9 1.18190 3.02295 8 -6 -7 9 4.14040 3.69489 8 6 -7 -9 6.72370 3.15751 3 -6 -7 9 6.62354 3.64393 1 -6 7 9 1.81500 2.94561 2 6 7 -9 1.52921 2.98440 7 6 7 -9 0.82146 3.06105 2 -6 7 9 3.74224 3.35346 1 -6 7 9 1.98889 2.57920 8 -6 7 9 3.50199 3.31089 6 5 -7 -9 113.524 7.68140 7 -5 -7 9 136.561 8.83119 4 5 -7 -9 127.177 9.49848 5 5 -7 -9 133.019 8.13331 8 5 -7 -9 132.715 8.91537 3 -5 -7 9 122.649 8.90971 1 -5 7 9 123.101 8.29452 6 -5 7 9 119.584 9.02972 2 5 7 -9 108.263 9.36218 7 5 7 -9 145.385 10.3607 2 -5 7 9 110.861 7.73897 8 -5 7 9 123.894 9.40774 1 4 -7 -9 446.819 18.1660 3 -4 -7 9 411.988 18.2365 4 4 -7 -9 444.034 16.3054 8 -4 -7 9 440.472 18.4257 1 4 -7 -9 424.552 18.7567 5 4 -7 -9 443.891 17.3564 7 -4 7 9 393.489 17.0094 7 4 7 -9 426.199 20.1089 7 -4 7 9 394.139 18.8649 2 4 7 -9 442.114 20.2675 2 -4 7 9 461.722 19.4412 1 -4 7 9 410.388 16.0293 8 -4 7 9 425.157 16.9016 6 -3 -7 9 1954.14 65.5708 4 3 -7 -9 2044.50 62.2246 3 3 -7 -9 1970.93 56.8748 8 3 -7 -9 1959.06 60.3063 5 3 -7 -9 1989.63 61.3271 7 -3 -7 9 1859.79 62.4326 1 -3 7 9 1955.54 61.3306 7 -3 7 9 1932.58 63.4513 1 3 7 -9 2023.84 66.7410 2 -3 7 9 1976.75 65.1916 2 3 7 -9 1955.90 64.8090 7 -3 7 9 1994.94 58.7773 6 -3 7 9 1959.45 56.8800 8 3 7 -9 1984.59 57.0666 5 -2 -7 9 5.18125 2.59623 1 -2 -7 9 10.3728 2.96311 4 2 -7 -9 7.52441 2.48668 7 2 -7 -9 7.13315 3.52996 5 2 -7 -9 3.98626 2.36411 8 2 -7 -9 6.27610 2.47618 3 2 -7 -9 7.04816 2.55835 6 -2 7 9 8.63176 3.15979 1 2 7 -9 5.47040 2.62240 5 2 7 -9 2.86000 2.98189 2 -2 7 9 6.06921 2.63259 6 -2 7 9 4.18504 2.62742 2 -2 7 9 7.50699 2.33273 8 2 7 -9 9.95768 3.52960 7 -2 7 9 7.50317 2.51185 7 1 -7 -9 982.529 35.1070 4 -1 -7 9 914.328 33.5884 4 -1 -7 9 932.527 29.4244 5 1 -7 -9 892.994 31.1274 3 1 -7 -9 950.092 28.7437 8 1 -7 -9 935.557 29.9049 6 -1 -7 9 909.007 31.7680 1 1 -7 -9 907.916 31.1933 7 1 7 -9 959.223 35.9652 2 1 7 -9 922.144 29.2586 5 -1 7 9 898.930 33.4580 2 -1 7 9 896.489 31.1926 7 1 7 -9 936.557 34.2103 7 -1 7 9 941.583 29.9742 6 0 -7 -9 55.1430 4.86589 6 0 -7 -9 59.3722 5.07949 3 0 -7 -9 51.8101 4.36287 8 0 -7 9 63.2023 5.79323 4 0 -7 -9 58.6724 6.60101 4 0 -7 9 69.1957 5.41505 5 0 -7 -9 56.6492 5.04527 7 0 7 -9 61.8622 7.33002 2 0 7 -9 57.0991 4.91389 5 0 7 9 59.2730 5.03781 7 0 7 -9 68.5123 5.48287 1 0 7 9 59.9758 5.87887 2 0 7 9 51.5018 4.81269 6 0 7 -9 57.9736 6.05843 7 1 -7 9 470.553 20.8903 4 -1 -7 -9 499.086 17.2578 8 -1 -7 -9 542.136 24.0679 4 -1 -7 -9 487.899 18.8227 7 -1 -7 -9 511.120 18.4708 6 1 -7 9 489.319 17.8964 5 -1 -7 -9 480.986 18.8305 3 -1 7 -9 520.145 19.2719 7 -1 7 -9 512.024 19.2619 1 1 7 9 494.898 20.3535 2 -1 7 -9 508.923 22.9795 2 1 7 9 507.232 19.0470 7 -1 7 -9 486.380 17.8383 5 1 7 9 524.941 18.6601 6 -2 -7 -9 217.621 10.4271 6 -2 -7 -9 224.179 14.7095 4 2 -7 9 196.323 11.7680 4 -2 -7 -9 204.689 9.37967 8 -2 -7 -9 208.007 10.3545 3 -2 -7 -9 225.925 10.5393 7 -2 -7 -9 191.397 11.3643 9 2 -7 9 197.824 9.79311 5 -2 7 -9 214.507 13.6626 2 2 7 9 217.466 10.4065 6 -2 7 -9 197.200 9.72727 5 2 7 9 223.538 10.5280 7 -2 7 -9 217.934 10.5858 1 2 7 9 210.997 11.8105 9 -2 7 -9 213.887 12.8273 9 2 7 9 208.755 11.1981 2 -3 -7 -9 2062.10 63.4896 6 -3 -7 -9 2093.97 67.4710 9 -3 -7 -9 2134.15 65.9853 3 3 -7 9 2133.53 61.2668 5 3 -7 9 2008.53 72.5537 4 -3 -7 -9 2140.01 65.5332 7 -3 -7 -9 2065.11 60.6713 8 -3 -7 -9 2350.81 78.5322 4 3 7 9 2066.84 67.3114 9 3 7 9 2201.52 68.3902 2 -3 7 -9 2108.75 61.0984 5 -3 7 -9 2134.35 72.5404 2 3 7 9 2130.13 65.6907 7 3 7 9 2157.33 63.8517 6 -3 7 -9 2146.05 69.1169 9 -3 7 -9 2092.67 66.6173 1 -4 -7 -9 98.1544 9.28711 9 4 -7 9 81.8549 6.54212 5 4 -7 9 103.390 9.09483 4 -4 -7 -9 99.6713 7.22580 3 -4 -7 -9 95.3946 6.50847 8 -4 -7 -9 102.608 6.90352 7 -4 -7 -9 87.6032 11.0633 4 -4 -7 -9 100.536 7.63218 6 -4 7 -9 113.050 10.4615 2 -4 7 -9 73.7113 9.13707 9 4 7 9 98.2553 6.92991 7 -4 7 -9 94.5089 6.98910 1 4 7 9 100.841 7.08147 2 4 7 9 89.5574 8.97382 9 -4 7 -9 95.7077 6.56673 5 5 -7 9 431.218 21.7804 4 -5 -7 -9 426.281 18.2753 6 -5 -7 -9 507.727 27.4133 4 -5 -7 -9 432.455 21.5478 9 5 -7 9 441.239 16.6494 5 -5 -7 -9 420.687 16.2374 8 5 7 9 426.116 18.1451 3 -5 7 -9 417.017 18.1518 1 -5 7 -9 467.221 22.8725 9 5 7 9 409.600 17.3311 7 5 7 9 445.511 21.7027 9 -5 7 -9 418.731 16.4116 5 -6 -7 -9 2.49910 3.26938 6 6 -7 9 1.10067 2.75460 5 -6 -7 -9 4.65652 5.65897 4 -6 -7 -9 6.62536 4.75811 9 -6 -7 -9 0.58932 2.45843 8 6 -7 9 -2.2945 3.23219 4 6 7 9 2.26282 2.68172 3 -6 7 -9 4.50294 5.23659 9 -6 7 -9 2.06481 2.77865 1 -6 7 -9 0.47392 2.53482 5 6 7 9 3.04285 4.63139 9 6 7 9 4.27204 2.86817 7 -6 7 -9 2.52545 3.82786 6 -7 -7 -9 117.308 12.8023 9 -7 -7 -9 120.954 8.33602 8 -7 -7 -9 122.071 10.0579 6 7 -7 9 117.992 8.17732 5 7 -7 9 113.460 11.8188 4 -7 -7 -9 121.843 14.9316 4 -7 7 -9 141.407 14.1174 9 7 7 9 120.641 9.04625 3 7 7 9 138.813 13.7490 9 7 7 9 134.498 8.57962 7 -7 7 -9 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36.1841 2 2 8 -9 998.325 37.9388 2 2 8 -9 998.897 36.9809 7 2 8 -9 1009.27 31.5953 5 -2 8 9 978.220 33.7047 7 -2 8 9 1005.24 32.5513 6 -1 -8 9 135.208 8.71675 4 -1 -8 9 104.897 7.37175 1 1 -8 -9 117.687 7.24964 6 -1 -8 9 130.429 7.63304 5 1 -8 -9 126.028 7.66707 7 1 -8 -9 126.289 9.37934 4 1 -8 -9 147.630 10.7353 5 1 -8 -9 116.934 6.75869 8 1 -8 -9 105.457 7.15910 3 1 8 -9 115.662 9.42303 2 -1 8 9 123.873 7.53136 7 -1 8 9 103.286 7.22073 6 -1 8 9 143.564 8.99910 2 1 8 -9 119.668 9.04071 7 1 8 -9 122.387 7.37563 5 0 -8 9 7.05981 2.98830 4 0 -8 9 6.24366 2.66176 5 0 -8 -9 2.34818 3.14354 4 0 -8 -9 0.81855 2.03158 6 0 -8 -9 3.96733 2.23439 8 0 -8 -9 1.27333 1.88593 7 0 -8 -9 3.60105 2.19505 3 0 8 -9 2.79416 3.08087 2 0 8 9 4.57378 2.46111 6 0 8 -9 10.1577 3.68399 7 0 8 9 3.08062 2.16814 7 0 8 -9 10.1521 3.02304 5 0 8 -9 6.84146 2.60496 1 0 8 9 4.18931 2.65911 2 -1 -8 -9 5.80040 2.46812 8 -1 -8 -9 10.4778 3.48457 9 -1 -8 -9 10.2198 2.82681 7 -1 -8 -9 7.17441 2.84291 6 1 -8 9 6.39157 2.72715 5 1 -8 9 5.51645 3.11085 4 -1 -8 -9 5.68571 2.28889 3 -1 -8 -9 10.7808 4.36229 4 1 8 9 11.9251 3.32268 2 1 8 9 12.1781 3.03939 7 1 8 9 9.11247 3.38236 9 -1 8 -9 5.70990 2.54788 1 -1 8 -9 5.61683 3.92791 9 -1 8 -9 9.99793 3.01838 5 -1 8 -9 3.83739 3.51052 2 1 8 9 7.45530 2.74243 6 2 -8 9 1956.36 56.2098 5 -2 -8 -9 1891.15 57.9449 6 2 -8 9 1904.94 66.2091 4 -2 -8 -9 1887.19 60.8420 9 -2 -8 -9 2037.22 71.4498 4 -2 -8 -9 1861.73 59.9404 3 -2 -8 -9 1896.00 59.8905 7 -2 -8 -9 1961.21 55.5730 8 2 8 9 1887.65 60.9072 9 -2 8 -9 1918.57 60.7033 1 -2 8 -9 1862.79 55.7976 5 2 8 9 1981.99 62.8574 2 -2 8 -9 1884.31 66.2376 2 2 8 9 1971.72 60.2562 7 2 8 9 1875.35 58.0021 6 -2 8 -9 1939.09 62.8258 9 3 -8 9 476.298 21.5556 4 -3 -8 -9 456.439 25.2493 4 -3 -8 -9 449.486 18.1283 6 -3 -8 -9 443.986 17.9163 7 -3 -8 -9 437.754 16.5424 8 -3 -8 -9 433.331 19.9901 9 3 -8 9 447.199 17.2312 5 -3 -8 -9 452.140 18.3083 3 3 8 9 440.297 18.0818 7 3 8 9 458.901 20.5782 9 -3 8 -9 415.272 20.8644 9 -3 8 -9 480.203 18.6168 1 -3 8 -9 466.772 22.4721 2 3 8 9 462.054 18.3119 6 3 8 9 473.626 19.1052 2 -3 8 -9 483.371 17.3759 5 4 -8 9 1082.87 42.1660 4 -4 -8 -9 1001.29 39.3599 9 -4 -8 -9 1032.35 36.8741 3 -4 -8 -9 1042.99 33.7866 8 -4 -8 -9 1049.83 36.2050 6 -4 -8 -9 1067.27 36.4688 7 -4 -8 -9 1185.81 48.8468 4 4 -8 9 1124.26 34.6514 5 4 8 9 1107.77 36.6973 6 -4 8 -9 1062.60 37.2642 1 -4 8 -9 1139.55 42.8456 2 -4 8 -9 1134.64 41.6101 9 4 8 9 1088.06 36.8646 7 -4 8 -9 1132.11 34.5904 5 4 8 9 1142.33 38.0463 2 4 8 9 1070.85 39.9035 9 5 -8 9 6.69698 3.33977 5 5 -8 9 13.9138 4.86266 4 -5 -8 -9 15.2975 7.29483 4 -5 -8 -9 0.16052 4.08243 9 -5 -8 -9 5.83261 2.80961 8 -5 -8 -9 7.66610 3.85527 6 5 8 9 3.96138 2.89756 3 5 8 9 9.20576 4.85435 9 -5 8 -9 9.75117 3.37799 5 -5 8 -9 6.31573 5.24853 9 5 8 9 5.79016 3.01753 7 -5 8 -9 5.70979 3.06880 1 -6 -8 -9 66.5202 9.51015 9 6 -8 9 55.6205 8.60035 4 -6 -8 -9 49.7551 5.41508 8 -6 -8 -9 72.0972 11.8731 4 -6 -8 -9 66.6856 7.42654 6 6 -8 9 61.9195 6.09586 5 6 8 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7.54330 8 3 -8 -27 8.81515 7.12114 8 5 0 -28 -10.634 8.93381 5 4 0 -28 25.9042 11.4811 5 3 0 -28 -4.9709 8.89103 5 2 0 -28 173.994 18.3002 5 5 -1 -28 -6.8525 8.11389 5 5 1 -28 4.55859 9.89890 5 4 -1 -28 6.93704 9.82475 5 4 1 -28 10.8032 10.2105 5 3 -1 -28 19.3570 10.9013 5 3 1 -28 27.6717 10.9529 5 2 -1 -28 34.6550 11.4802 5 2 1 -28 39.0741 12.1288 5 5 -2 -28 10.0111 9.80780 5 4 -2 -28 24.7192 10.9682 5 4 2 -28 25.8336 11.7441 5 3 -2 -28 25.4000 11.7030 5 3 2 -28 20.6169 10.9459 5 2 -2 -28 35.7336 11.2612 5 4 -3 -28 -9.4099 8.05228 5 3 -3 -28 136.209 17.3933 5 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 58983 _shelx_res_file ; re1.res created by SHELXL-2014/7 TITL re1 in P2(1)/n REM REM color : pale green shape plate REM Tmin 0.1325 Tmax 0.4780 REM CELL 0.71073 10.5581 14.7406 15.6088 90.000 100.794 90.000 ZERR 4.00 0.0004 0.0005 0.0006 0.000 0.002 0.000 LATT 1 SYMM -x+1/2, y+1/2, -z+1/2 SFAC C H O S CL RE UNIT 48.00 104.00 24.00 8.00 16.00 8.00 TEMP -163 SIZE 0.086 0.180 0.222 OMIT 2 6 1 ! 132.20 25.42 5.85 OMIT 3 3 3 ! 618.99 402.08 5.48 OMIT -2 4 3 ! 1241.40 937.03 5.38 OMIT 0 1 1 ! -3.86 35.37 5.17 OMIT -4 3 4 ! 9347.68 8121.64 5.17 OMIT 3 3 7 ! 256.78 30.96 5.11 ACTA L.S. 8 FMAP 2 PLAN 5 BOND $H WGHT 0.018300 1.798100 FVAR 0.16854 RE1 6 -0.067228 0.173630 0.278802 11.00000 0.01040 0.01222 = 0.01171 0.00002 0.00320 -0.00114 RE2 6 0.109857 0.163710 0.219049 11.00000 0.00953 0.01154 = 0.01360 0.00041 0.00288 0.00081 CL1 5 -0.019535 0.089824 0.405540 11.00000 0.02223 0.02413 = 0.01662 0.00674 0.00305 -0.00111 CL2 5 -0.199649 0.059738 0.210838 11.00000 0.01607 0.01640 = 0.02193 -0.00305 0.00380 -0.00426 CL3 5 0.064215 0.044937 0.122102 11.00000 0.01687 0.01521 = 0.02014 -0.00402 0.00460 0.00138 CL4 5 0.252025 0.077591 0.317390 11.00000 0.01675 0.02153 = 0.02443 0.00541 -0.00088 0.00463 S1 4 0.412508 0.242396 0.201765 11.00000 0.01302 0.02230 = 0.02301 -0.00136 0.00407 -0.00283 S2 4 -0.238712 0.259293 0.422972 11.00000 0.01945 0.01890 = 0.01622 -0.00281 0.00824 -0.00284 O1 3 -0.144932 0.263711 0.183653 11.00000 0.01202 0.01528 = 0.01592 0.00224 0.00414 -0.00001 O2 3 0.029273 0.252409 0.123989 11.00000 0.01332 0.01534 = 0.01570 0.00257 0.00481 0.00245 O3 3 0.184208 0.276028 0.287223 11.00000 0.01356 0.01611 = 0.01857 -0.00225 0.00445 -0.00233 O4 3 0.011213 0.285333 0.348020 11.00000 0.01556 0.01630 = 0.01621 -0.00345 0.00500 -0.00376 O5 3 0.285310 0.205747 0.149879 11.00000 0.01080 0.02250 = 0.02384 -0.00105 0.00400 -0.00204 O6 3 -0.244129 0.236119 0.326752 11.00000 0.01639 0.02547 = 0.01666 -0.00380 0.00761 -0.00092 C1 1 -0.078033 0.290121 0.128478 11.00000 0.01344 0.01275 = 0.01348 -0.00018 0.00221 0.00147 C2 1 -0.118054 0.372251 0.073310 11.00000 0.01746 0.01705 = 0.01989 0.00457 0.00341 0.00367 AFIX 13 H2 2 -0.109020 0.358467 0.012012 11.00000 -1.20000 AFIX 0 C3 1 -0.256006 0.400496 0.073139 11.00000 0.01841 0.02746 = 0.03533 0.00844 0.00254 0.00649 AFIX 137 H3A 2 -0.278795 0.451575 0.033026 11.00000 -1.50000 H3B 2 -0.264694 0.418826 0.132114 11.00000 -1.50000 H3C 2 -0.313802 0.349367 0.054168 11.00000 -1.50000 AFIX 0 C4 1 -0.022656 0.448084 0.108699 11.00000 0.02537 0.01620 = 0.06165 0.00475 0.00038 -0.00070 AFIX 137 H4A 2 0.065781 0.426027 0.112481 11.00000 -1.50000 H4B 2 -0.035842 0.466157 0.166810 11.00000 -1.50000 H4C 2 -0.037060 0.500435 0.069376 11.00000 -1.50000 AFIX 0 C5 1 0.120416 0.315123 0.338537 11.00000 0.01614 0.01324 = 0.01550 -0.00117 0.00145 -0.00126 C6 1 0.179597 0.395470 0.389346 11.00000 0.02058 0.01786 = 0.02036 -0.00439 0.00277 -0.00617 AFIX 13 H6 2 0.228284 0.431342 0.351805 11.00000 -1.20000 AFIX 0 C7 1 0.078500 0.456466 0.416705 11.00000 0.03747 0.02984 = 0.07233 -0.03191 0.00789 -0.00076 AFIX 137 H7A 2 0.017561 0.476432 0.364862 11.00000 -1.50000 H7B 2 0.120558 0.509504 0.447572 11.00000 -1.50000 H7C 2 0.032065 0.422870 0.455358 11.00000 -1.50000 AFIX 0 C8 1 0.275040 0.361028 0.468827 11.00000 0.03413 0.03699 = 0.02539 -0.00256 -0.00652 -0.01215 AFIX 137 H8A 2 0.337990 0.320724 0.449531 11.00000 -1.50000 H8B 2 0.228240 0.327636 0.507402 11.00000 -1.50000 H8C 2 0.319982 0.412679 0.500424 11.00000 -1.50000 AFIX 0 C9 1 0.414636 0.360542 0.177506 11.00000 0.03397 0.02026 = 0.05485 -0.00222 0.01129 -0.00515 AFIX 137 H9A 2 0.404741 0.368904 0.114314 11.00000 -1.50000 H9B 2 0.496798 0.386828 0.206499 11.00000 -1.50000 H9C 2 0.343537 0.390822 0.198374 11.00000 -1.50000 AFIX 0 C10 1 0.530590 0.206674 0.141127 11.00000 0.01336 0.03403 = 0.04120 -0.00670 0.00834 0.00096 AFIX 137 H10A 2 0.536712 0.140333 0.142508 11.00000 -1.50000 H10B 2 0.614384 0.232866 0.166914 11.00000 -1.50000 H10C 2 0.505674 0.227157 0.080580 11.00000 -1.50000 AFIX 0 C11 1 -0.336143 0.174958 0.460348 11.00000 0.03794 0.02390 = 0.02939 -0.00150 0.02056 -0.00723 AFIX 137 H11A 2 -0.419083 0.170934 0.420000 11.00000 -1.50000 H11B 2 -0.350813 0.191322 0.518557 11.00000 -1.50000 H11C 2 -0.292172 0.116190 0.463062 11.00000 -1.50000 AFIX 0 C12 1 -0.344124 0.353444 0.421320 11.00000 0.04942 0.02369 = 0.03215 -0.00024 0.01724 0.01038 AFIX 137 H12A 2 -0.308732 0.405720 0.394954 11.00000 -1.50000 H12B 2 -0.352866 0.368476 0.481095 11.00000 -1.50000 H12C 2 -0.428936 0.338084 0.386999 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM re1 in P2(1)/n REM R1 = 0.0254 for 11921 Fo > 4sig(Fo) and 0.0380 for all 14497 data REM 243 parameters refined using 0 restraints END WGHT 0.0165 1.6515 REM Highest difference peak 1.708, deepest hole -1.144, 1-sigma level 0.198 Q1 1 -0.0439 0.1729 0.3245 11.00000 0.05 1.71 Q2 1 0.0825 0.1679 0.1740 11.00000 0.05 1.33 Q3 1 0.0192 0.1717 0.2735 11.00000 0.05 1.21 Q4 1 0.1366 0.1765 0.2627 11.00000 0.05 1.20 Q5 1 -0.0884 0.1685 0.2303 11.00000 0.05 1.00 ; _shelx_res_checksum 84271