This PDF file includes:

• Fig. S1. Turbidity assay to monitor Fmoc-DOPA optical transition over time.
• Fig. S2. Sealed capillary assay to monitor Fmoc-DOPA assembly.
• Fig. S3. Cryo-TEM of Fmoc-DOPA assemblies at additional time points.
• Fig. S4. Additional NMR analysis of Fmoc-DOPA assembly.
• Fig. S5. The influence of lyophilization on the assemblies.
• Fig. S6. Exploring Fmoc-DOPA phase transition.
• Table S1. Hydrogen bonding parameters from Fmoc-DOPA crystal structure.
• Table S2. Crystal data and structure refinement for the Fmoc-DOPA crystal.

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