data_baran477 _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common RR12-264-minor _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C19 H25 I O5' _chemical_formula_weight 460.29 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 9.8414(10) _cell_length_b 24.468(3) _cell_length_c 7.9373(9) _cell_angle_alpha 90 _cell_angle_beta 108.333(4) _cell_angle_gamma 90 _cell_volume 1814.3(3) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 4711 _cell_measurement_theta_min 2.74 _cell_measurement_theta_max 26.40 _exptl_crystal_description plate _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.685 _exptl_crystal_F_000 928 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.180 _exptl_crystal_size_min 0.060 _exptl_absorpt_coefficient_mu 1.792 _shelx_estimated_absorpt_T_min 0.673 _shelx_estimated_absorpt_T_max 0.900 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.701 _exptl_absorpt_correction_T_max 0.940 _exptl_absorpt_process_details SADABS _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 12506 _diffrn_reflns_av_unetI/netI 0.0441 _diffrn_reflns_av_R_equivalents 0.0421 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_theta_min 2.180 _diffrn_reflns_theta_max 26.470 _diffrn_reflns_theta_full 25.000 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 3713 _reflns_number_gt 3097 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0284P)^2^+2.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 3713 _refine_ls_number_parameters 232 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0444 _refine_ls_R_factor_gt 0.0328 _refine_ls_wR_factor_ref 0.0719 _refine_ls_wR_factor_gt 0.0678 _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_restrained_S_all 1.038 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.47380(2) 0.29413(2) 1.09687(3) 0.01896(8) Uani 1 1 d . . . . . O1 O 0.1553(2) 0.27792(8) 0.4085(3) 0.0139(5) Uani 1 1 d . . . . . O2 O 0.1606(2) 0.33241(9) 0.8114(3) 0.0121(5) Uani 1 1 d . . . . . H3 H 0.155(4) 0.3038(16) 0.829(5) 0.018 Uiso 1 1 d . U . . . O3 O 0.3203(2) 0.41848(8) 0.3667(3) 0.0104(5) Uani 1 1 d . . . . . O4 O 0.1743(2) 0.48310(8) 0.5632(3) 0.0117(5) Uani 1 1 d . . . . . O5 O 0.0961(2) 0.51671(9) 0.2926(3) 0.0138(5) Uani 1 1 d . . . . . C1 C 0.6267(4) 0.38983(14) 0.5551(4) 0.0172(7) Uani 1 1 d . . . . . H9 H 0.6199 0.3518 0.5142 0.026 Uiso 1 1 calc R U . . . H1 H 0.7229 0.3967 0.6372 0.026 Uiso 1 1 calc R U . . . H10 H 0.6083 0.4144 0.4530 0.026 Uiso 1 1 calc R U . . . C2 C 0.5153(3) 0.40012(13) 0.6510(4) 0.0116(6) Uani 1 1 d . . . . . C3 C 0.3684(3) 0.38497(13) 0.5249(4) 0.0100(6) Uani 1 1 d . . . . . H20 H 0.3784 0.3471 0.4826 0.012 Uiso 1 1 calc R U . . . C4 C 0.2413(3) 0.38285(12) 0.5985(4) 0.0088(6) Uani 1 1 d . . . . . C5 C 0.1185(3) 0.37542(12) 0.4226(4) 0.0084(6) Uani 1 1 d . . . . . C6 C 0.1062(3) 0.31984(13) 0.3296(4) 0.0092(6) Uani 1 1 d . . . . . C7 C 0.0139(4) 0.32005(13) 0.1376(4) 0.0127(7) Uani 1 1 d . . . . . H23 H 0.0772 0.3106 0.0649 0.015 Uiso 1 1 calc R U . . . C8 C -0.1037(4) 0.27653(14) 0.0997(5) 0.0190(8) Uani 1 1 d . . . . . H25 H -0.0601 0.2405 0.1327 0.029 Uiso 1 1 calc R U . . . H2 H -0.1583 0.2768 -0.0270 0.029 Uiso 1 1 calc R U . . . H24 H -0.1679 0.2845 0.1692 0.029 Uiso 1 1 calc R U . . . C9 C 0.2770(3) 0.33780(12) 0.7425(4) 0.0090(6) Uani 1 1 d . . . . . H22 H 0.2910 0.3023 0.6875 0.011 Uiso 1 1 calc R U . . . C10 C 0.4182(3) 0.35406(12) 0.8835(4) 0.0114(7) Uani 1 1 d . . . . . H21 H 0.4050 0.3904 0.9340 0.014 Uiso 1 1 calc R U . . . C11 C 0.5419(3) 0.35845(13) 0.8052(4) 0.0120(7) Uani 1 1 d . . . . . H4 H 0.5589 0.3220 0.7615 0.014 Uiso 1 1 calc R U . . . H5 H 0.6299 0.3691 0.9008 0.014 Uiso 1 1 calc R U . . . C12 C 0.5328(4) 0.45908(13) 0.7227(4) 0.0162(7) Uani 1 1 d . . . . . H7 H 0.4783 0.4840 0.6294 0.024 Uiso 1 1 calc R U . . . H6 H 0.6343 0.4692 0.7597 0.024 Uiso 1 1 calc R U . . . H8 H 0.4971 0.4615 0.8246 0.024 Uiso 1 1 calc R U . . . C13 C 0.1657(3) 0.42087(12) 0.3157(4) 0.0099(6) Uani 1 1 d . . . . . C14 C 0.1383(3) 0.47725(12) 0.3859(4) 0.0108(6) Uani 1 1 d . . . . . C15 C 0.2073(3) 0.43600(12) 0.6812(4) 0.0099(6) Uani 1 1 d . . . . . H11 H 0.1248 0.4291 0.7244 0.012 Uiso 1 1 calc R U . . . H12 H 0.2904 0.4452 0.7856 0.012 Uiso 1 1 calc R U . . . C16 C 0.0929(4) 0.41542(13) 0.1175(4) 0.0132(7) Uani 1 1 d . . . . . H18 H 0.1595 0.3988 0.0609 0.016 Uiso 1 1 calc R U . . . H19 H 0.0643 0.4519 0.0641 0.016 Uiso 1 1 calc R U . . . C17 C -0.0404(3) 0.37877(13) 0.0873(4) 0.0125(7) Uani 1 1 d . . . . . H13 H -0.1018 0.3804 -0.0398 0.015 Uiso 1 1 calc R U . . . C18 C -0.1262(4) 0.39751(13) 0.2103(4) 0.0144(7) Uani 1 1 d . . . . . H15 H -0.2186 0.3778 0.1785 0.017 Uiso 1 1 calc R U . . . H14 H -0.1468 0.4371 0.1934 0.017 Uiso 1 1 calc R U . . . C19 C -0.0407(3) 0.38626(13) 0.4080(4) 0.0103(6) Uani 1 1 d . . . . . H17 H -0.0809 0.3541 0.4512 0.012 Uiso 1 1 calc R U . . . H16 H -0.0473 0.4182 0.4817 0.012 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.01855(13) 0.01879(13) 0.01451(12) 0.00880(9) -0.00202(9) -0.00472(10) O1 0.0172(12) 0.0081(11) 0.0140(12) -0.0013(9) 0.0016(10) 0.0015(9) O2 0.0168(12) 0.0077(11) 0.0136(12) 0.0020(9) 0.0070(10) -0.0002(10) O3 0.0118(11) 0.0118(11) 0.0077(11) 0.0039(8) 0.0033(9) 0.0014(9) O4 0.0192(12) 0.0061(11) 0.0100(11) 0.0009(8) 0.0049(10) 0.0012(9) O5 0.0162(12) 0.0113(12) 0.0137(12) 0.0044(9) 0.0044(10) 0.0021(9) C1 0.0131(17) 0.0204(18) 0.0193(18) 0.0010(14) 0.0067(15) -0.0026(14) C2 0.0119(16) 0.0105(16) 0.0122(16) -0.0020(12) 0.0036(13) -0.0007(13) C3 0.0135(16) 0.0077(15) 0.0093(15) 0.0029(12) 0.0042(13) 0.0008(13) C4 0.0110(15) 0.0068(14) 0.0083(15) 0.0004(11) 0.0026(13) -0.0007(12) C5 0.0107(16) 0.0076(15) 0.0081(15) 0.0012(11) 0.0046(13) 0.0002(12) C6 0.0063(15) 0.0112(16) 0.0119(16) -0.0007(12) 0.0058(13) -0.0017(12) C7 0.0167(17) 0.0110(16) 0.0095(16) -0.0009(12) 0.0028(14) 0.0012(13) C8 0.0187(19) 0.0149(17) 0.0180(18) -0.0027(13) -0.0020(15) -0.0010(14) C9 0.0122(16) 0.0081(15) 0.0069(15) 0.0016(11) 0.0033(13) 0.0021(13) C10 0.0168(17) 0.0067(15) 0.0097(16) 0.0052(11) 0.0028(14) 0.0012(13) C11 0.0108(16) 0.0119(16) 0.0107(16) 0.0012(12) -0.0002(13) -0.0003(13) C12 0.0180(18) 0.0136(17) 0.0168(18) -0.0003(13) 0.0051(15) -0.0062(14) C13 0.0096(16) 0.0088(15) 0.0114(16) 0.0030(12) 0.0033(13) 0.0012(12) C14 0.0104(15) 0.0101(16) 0.0127(16) -0.0005(12) 0.0047(14) -0.0013(13) C15 0.0140(16) 0.0074(15) 0.0067(15) 0.0015(11) 0.0013(13) 0.0017(13) C16 0.0188(18) 0.0130(16) 0.0092(16) 0.0026(12) 0.0064(14) 0.0023(14) C17 0.0162(17) 0.0126(15) 0.0061(15) -0.0006(12) -0.0003(13) 0.0028(14) C18 0.0131(16) 0.0130(17) 0.0170(17) -0.0002(13) 0.0044(15) 0.0023(13) C19 0.0126(16) 0.0078(15) 0.0106(15) -0.0003(12) 0.0036(13) 0.0002(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 C10 2.176(3) . ? O1 C6 1.220(4) . ? O2 C9 1.423(4) . ? O3 C13 1.447(4) . ? O3 C3 1.449(3) . ? O4 C14 1.346(4) . ? O4 C15 1.456(3) . ? O5 C14 1.208(4) . ? C1 C2 1.539(4) . ? C2 C3 1.523(5) . ? C2 C12 1.540(4) . ? C2 C11 1.550(4) . ? C3 C4 1.539(4) . ? C4 C15 1.540(4) . ? C4 C5 1.543(4) . ? C4 C9 1.547(4) . ? C5 C6 1.534(4) . ? C5 C13 1.556(4) . ? C5 C19 1.557(4) . ? C6 C7 1.509(4) . ? C7 C8 1.531(5) . ? C7 C17 1.541(4) . ? C9 C10 1.537(4) . ? C10 C11 1.535(4) . ? C13 C16 1.516(4) . ? C13 C14 1.543(4) . ? C16 C17 1.545(5) . ? C17 C18 1.548(4) . ? C18 C19 1.554(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 O3 C3 107.1(2) . . ? C14 O4 C15 121.4(2) . . ? C3 C2 C1 108.1(3) . . ? C3 C2 C12 116.3(3) . . ? C1 C2 C12 108.8(3) . . ? C3 C2 C11 104.4(2) . . ? C1 C2 C11 108.2(3) . . ? C12 C2 C11 110.7(3) . . ? O3 C3 C2 114.6(2) . . ? O3 C3 C4 105.4(2) . . ? C2 C3 C4 118.4(3) . . ? C3 C4 C15 116.4(3) . . ? C3 C4 C5 99.2(2) . . ? C15 C4 C5 105.8(2) . . ? C3 C4 C9 106.4(2) . . ? C15 C4 C9 108.4(2) . . ? C5 C4 C9 121.1(3) . . ? C6 C5 C4 117.4(3) . . ? C6 C5 C13 111.3(2) . . ? C4 C5 C13 97.2(2) . . ? C6 C5 C19 100.9(2) . . ? C4 C5 C19 122.1(2) . . ? C13 C5 C19 107.7(2) . . ? O1 C6 C7 122.5(3) . . ? O1 C6 C5 122.7(3) . . ? C7 C6 C5 114.5(3) . . ? C6 C7 C8 111.9(3) . . ? C6 C7 C17 108.3(3) . . ? C8 C7 C17 114.7(3) . . ? O2 C9 C10 113.4(2) . . ? O2 C9 C4 109.1(2) . . ? C10 C9 C4 107.3(2) . . ? C11 C10 C9 111.9(2) . . ? C11 C10 I1 109.0(2) . . ? C9 C10 I1 109.91(19) . . ? C10 C11 C2 114.0(3) . . ? O3 C13 C16 113.5(3) . . ? O3 C13 C14 102.9(2) . . ? C16 C13 C14 112.0(3) . . ? O3 C13 C5 106.7(2) . . ? C16 C13 C5 112.2(3) . . ? C14 C13 C5 109.0(2) . . ? O5 C14 O4 118.9(3) . . ? O5 C14 C13 123.9(3) . . ? O4 C14 C13 117.0(3) . . ? O4 C15 C4 115.3(2) . . ? C13 C16 C17 108.3(3) . . ? C7 C17 C16 107.0(3) . . ? C7 C17 C18 109.0(3) . . ? C16 C17 C18 109.6(3) . . ? C17 C18 C19 110.8(3) . . ? C18 C19 C5 108.6(2) . . ? _refine_diff_density_max 1.010 _refine_diff_density_min -0.665 _refine_diff_density_rms 0.106 _shelxl_version_number 2013-3 _shelx_res_file ; TITL baran477 in P2(1)/c CELL 0.71073 9.8414 24.4681 7.9373 90.000 108.333 90.000 ZERR 4.00 0.0010 0.0025 0.0009 0.000 0.004 0.000 LATT 1 SYMM -x, y+1/2, -z+1/2 SFAC C H O I UNIT 76 100 20 4 TEMP -173.000 SIZE 0.060 0.180 0.240 ACTA 50 L.S. 4 FMAP 2 PLAN -5 0 0.00 BOND WGHT 0.028400 2.000000 FVAR 0.12247 I1 4 0.473798 0.294132 1.096873 11.00000 0.01855 0.01879 = 0.01451 0.00880 -0.00202 -0.00472 O1 3 0.155283 0.277918 0.408488 11.00000 0.01719 0.00807 = 0.01402 -0.00129 0.00161 0.00145 O2 3 0.160606 0.332411 0.811446 11.00000 0.01677 0.00767 = 0.01357 0.00196 0.00703 -0.00023 H3 2 0.155444 0.303826 0.829291 11.00000 -1.50000 O3 3 0.320311 0.418478 0.366667 11.00000 0.01183 0.01180 = 0.00771 0.00387 0.00327 0.00145 O4 3 0.174326 0.483095 0.563165 11.00000 0.01924 0.00613 = 0.01000 0.00093 0.00492 0.00116 O5 3 0.096101 0.516705 0.292579 11.00000 0.01617 0.01128 = 0.01371 0.00437 0.00436 0.00210 C1 1 0.626733 0.389828 0.555145 11.00000 0.01310 0.02042 = 0.01929 0.00102 0.00667 -0.00259 AFIX 137 H9 2 0.619862 0.351834 0.514243 11.00000 -1.50000 H1 2 0.722942 0.396655 0.637155 11.00000 -1.50000 H10 2 0.608324 0.414440 0.453001 11.00000 -1.50000 AFIX 0 C2 1 0.515317 0.400123 0.651021 11.00000 0.01186 0.01050 = 0.01222 -0.00197 0.00364 -0.00070 C3 1 0.368426 0.384972 0.524854 11.00000 0.01352 0.00772 = 0.00933 0.00294 0.00423 0.00078 AFIX 13 H20 2 0.378372 0.347131 0.482603 11.00000 -1.20000 AFIX 0 C4 1 0.241304 0.382851 0.598498 11.00000 0.01102 0.00682 = 0.00828 0.00035 0.00262 -0.00074 C5 1 0.118498 0.375422 0.422640 11.00000 0.01072 0.00759 = 0.00812 0.00115 0.00461 0.00022 C6 1 0.106194 0.319838 0.329605 11.00000 0.00632 0.01123 = 0.01192 -0.00066 0.00577 -0.00171 C7 1 0.013899 0.320047 0.137554 11.00000 0.01672 0.01104 = 0.00945 -0.00088 0.00279 0.00121 AFIX 13 H23 2 0.077205 0.310568 0.064942 11.00000 -1.20000 AFIX 0 C8 1 -0.103689 0.276535 0.099733 11.00000 0.01873 0.01493 = 0.01801 -0.00267 -0.00200 -0.00095 AFIX 137 H25 2 -0.060101 0.240476 0.132735 11.00000 -1.50000 H2 2 -0.158335 0.276813 -0.026969 11.00000 -1.50000 H24 2 -0.167895 0.284465 0.169224 11.00000 -1.50000 AFIX 0 C9 1 0.277045 0.337798 0.742524 11.00000 0.01220 0.00807 = 0.00688 0.00164 0.00328 0.00213 AFIX 13 H22 2 0.291005 0.302349 0.687461 11.00000 -1.20000 AFIX 0 C10 1 0.418248 0.354060 0.883544 11.00000 0.01680 0.00666 = 0.00973 0.00525 0.00277 0.00116 AFIX 13 H21 2 0.405013 0.390382 0.933997 11.00000 -1.20000 AFIX 0 C11 1 0.541945 0.358453 0.805165 11.00000 0.01077 0.01192 = 0.01071 0.00118 -0.00020 -0.00032 AFIX 23 H4 2 0.558908 0.322000 0.761479 11.00000 -1.20000 H5 2 0.629896 0.369130 0.900771 11.00000 -1.20000 AFIX 0 C12 1 0.532845 0.459085 0.722712 11.00000 0.01805 0.01355 = 0.01680 -0.00033 0.00512 -0.00625 AFIX 137 H7 2 0.478250 0.484048 0.629354 11.00000 -1.50000 H6 2 0.634299 0.469238 0.759745 11.00000 -1.50000 H8 2 0.497135 0.461477 0.824645 11.00000 -1.50000 AFIX 0 C13 1 0.165741 0.420871 0.315704 11.00000 0.00959 0.00875 = 0.01135 0.00298 0.00329 0.00117 C14 1 0.138289 0.477253 0.385943 11.00000 0.01039 0.01008 = 0.01265 -0.00049 0.00469 -0.00129 C15 1 0.207295 0.435995 0.681225 11.00000 0.01403 0.00739 = 0.00675 0.00151 0.00127 0.00168 AFIX 23 H11 2 0.124806 0.429129 0.724441 11.00000 -1.20000 H12 2 0.290400 0.445225 0.785612 11.00000 -1.20000 AFIX 0 C16 1 0.092938 0.415419 0.117457 11.00000 0.01884 0.01304 = 0.00925 0.00259 0.00642 0.00231 AFIX 23 H18 2 0.159483 0.398842 0.060879 11.00000 -1.20000 H19 2 0.064251 0.451889 0.064105 11.00000 -1.20000 AFIX 0 C17 1 -0.040429 0.378771 0.087267 11.00000 0.01623 0.01260 = 0.00606 -0.00057 -0.00034 0.00281 AFIX 13 H13 2 -0.101839 0.380376 -0.039757 11.00000 -1.20000 AFIX 0 C18 1 -0.126170 0.397513 0.210333 11.00000 0.01306 0.01300 = 0.01699 -0.00016 0.00438 0.00225 AFIX 23 H15 2 -0.218576 0.377751 0.178482 11.00000 -1.20000 H14 2 -0.146846 0.437091 0.193364 11.00000 -1.20000 AFIX 0 C19 1 -0.040664 0.386261 0.407995 11.00000 0.01262 0.00784 = 0.01056 -0.00026 0.00365 0.00018 AFIX 23 H17 2 -0.080944 0.354077 0.451162 11.00000 -1.20000 H16 2 -0.047254 0.418170 0.481722 11.00000 -1.20000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM baran477 in P2(1)/c REM R1 = 0.0328 for 3097 Fo > 4sig(Fo) and 0.0444 for all 3713 data REM 232 parameters refined using 0 restraints END WGHT 0.0268 2.1681 REM Highest difference peak 1.010, deepest hole -0.665, 1-sigma level 0.106 Q1 1 0.3683 0.2954 1.0835 11.00000 0.05 1.01 Q2 1 0.5808 0.2953 1.1257 11.00000 0.05 0.96 Q3 1 0.6516 0.2899 1.0635 11.00000 0.05 0.51 Q4 1 0.5780 0.3960 0.6335 11.00000 0.05 0.46 Q5 1 0.2460 0.4229 0.3428 11.00000 0.05 0.43 ; _shelx_res_checksum 112 _shelx_hkl_file ; 0 0 1 0.49 0.26 0 0 -1 0.00 0.32 0 0 2 8.25 0.83 0 0 -2 6.00 0.83 0 0 3 -0.44 0.51 0 0 -3 0.16 0.72 0 0 -4 464.81 17.04 0 0 4 512.90 17.05 0 0 5 -0.12 0.59 0 0 6 195.18 7.64 0 0 7 -0.41 0.77 0 0 8 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2.65 0 -22 2 25.05 2.31 0 -22 -2 26.23 2.69 0 22 -3 46.80 3.46 0 22 3 44.92 3.19 0 22 3 49.73 2.38 0 -22 3 48.05 3.20 0 22 4 28.85 2.61 0 22 -4 30.29 2.89 0 22 4 27.30 1.89 0 -22 4 27.30 2.62 0 22 5 -0.02 0.75 0 22 -5 -0.37 1.28 0 22 5 0.14 1.05 0 -22 5 1.18 1.06 0 22 -6 62.49 3.93 0 22 6 51.58 3.22 0 22 6 64.55 3.64 0 23 0 0.05 1.27 0 -23 0 3.43 1.18 0 23 -1 9.19 1.82 0 23 1 4.72 1.59 0 -23 -1 4.26 1.41 0 -23 1 4.95 1.34 0 23 -2 58.53 3.89 0 23 2 57.85 3.72 0 -23 -2 58.86 3.78 0 -23 2 60.01 3.52 0 23 -3 0.65 1.48 0 23 3 3.45 1.41 0 -23 3 0.81 1.00 0 23 4 50.22 2.68 0 23 -4 52.42 3.73 0 23 4 47.51 3.39 0 -23 4 58.68 3.61 0 23 -5 0.83 1.35 0 23 5 -0.17 0.72 0 23 5 -0.13 0.96 0 -23 5 1.51 1.25 0 23 -6 10.76 2.07 0 23 6 14.92 1.95 0 23 6 14.84 2.03 0 24 0 53.52 3.78 0 -24 0 63.85 3.68 0 24 -1 4.99 1.57 0 24 1 4.92 1.56 0 -24 1 4.59 1.32 0 -24 -1 5.51 1.38 0 24 -2 11.05 2.02 0 24 2 5.44 1.59 0 -24 -2 7.39 1.71 0 -24 2 10.35 1.76 0 24 3 1.61 1.35 0 24 -3 4.78 1.68 0 -24 3 5.91 1.48 0 24 -4 22.60 2.81 0 24 4 22.12 2.50 0 -24 4 23.23 2.63 0 24 5 2.07 1.25 0 24 -5 0.65 1.43 0 -24 5 2.31 1.58 0 25 0 1.75 1.42 0 -25 0 -0.13 1.03 0 25 -1 17.80 2.55 0 25 1 14.17 2.23 0 -25 -1 18.82 2.34 0 -25 1 21.29 2.40 0 25 -2 39.46 3.51 0 25 2 39.04 3.29 0 -25 2 40.09 3.08 0 -25 -2 53.07 3.57 0 25 3 5.35 1.64 0 25 -3 3.82 1.72 0 -25 3 6.96 1.63 0 25 4 28.62 2.84 0 25 -4 35.67 3.31 0 -25 4 36.65 3.10 0 25 5 25.75 2.66 0 25 -5 20.80 2.67 0 26 0 19.21 2.69 0 -26 0 20.93 2.42 0 26 1 11.31 2.07 0 26 -1 9.01 2.06 0 -26 -1 8.94 1.90 0 -26 1 7.23 1.66 0 26 2 1.77 1.31 0 26 -2 2.30 1.57 0 -26 -2 0.75 1.40 0 -26 2 -0.53 1.06 0 26 3 49.53 3.71 0 26 -3 50.83 3.96 0 -26 3 53.83 3.60 0 26 4 4.82 1.57 0 26 -4 4.30 1.85 0 -26 4 6.05 1.82 0 27 0 1.50 1.59 0 -27 0 0.69 1.24 0 27 1 36.12 3.36 0 27 -1 44.53 3.72 0 -27 -1 42.88 3.36 0 -27 1 39.14 3.16 0 27 -2 7.11 1.99 0 27 2 6.48 1.82 0 -27 -2 3.69 1.72 0 -27 2 7.12 1.69 0 27 3 2.42 1.52 0 27 -3 4.11 1.78 0 -27 3 0.98 1.26 0 27 4 3.15 1.41 0 27 -4 3.72 1.83 0 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263.16 8.88 -2 -2 1 249.73 8.82 2 -2 -1 266.32 8.81 2 2 0 349.49 12.10 -2 2 0 349.29 11.83 2 2 0 349.21 12.09 2 -2 0 379.23 11.83 -2 -2 0 345.44 12.10 -2 -2 0 341.03 12.07 2 2 1 2.79 0.72 2 2 1 2.77 0.58 -2 -2 -1 2.54 0.63 -2 -2 -1 1.43 0.64 2 -2 1 1.42 0.34 2 -2 1 1.66 0.68 2 2 2 321.98 12.05 2 2 2 344.88 11.96 -2 -2 -2 366.56 12.21 2 -2 2 333.16 12.12 2 2 3 172.94 6.55 2 2 3 167.17 6.66 2 -2 3 173.42 6.77 -2 -2 -3 179.52 6.94 2 2 4 45.97 2.64 2 -2 4 42.28 2.59 2 2 5 45.66 2.83 2 -2 5 42.18 2.77 2 2 6 103.98 5.01 2 -2 6 99.17 4.95 2 2 7 16.29 2.12 2 -2 7 15.67 2.25 2 2 8 6.81 1.75 2 -2 8 7.74 1.93 -2 3 9 74.77 4.68 -2 -3 9 81.00 4.69 -2 3 8 60.88 3.92 -2 3 8 64.97 3.15 -2 -3 8 66.89 3.25 -2 -3 8 56.48 3.78 -2 3 7 2.15 1.20 -2 3 7 4.45 0.82 -2 -3 7 1.50 1.20 -2 -3 7 2.83 0.80 -2 3 6 35.40 2.46 -2 3 6 35.38 1.92 -2 -3 6 36.70 2.04 -2 -3 6 32.11 2.42 2 -3 -6 32.95 2.59 -2 3 5 87.35 3.54 -2 3 5 93.76 4.10 -2 -3 5 82.64 4.00 2 -3 -5 90.08 3.85 -2 -3 5 91.81 3.68 -2 3 4 41.08 1.83 2 3 -4 40.36 1.80 -2 3 4 41.92 2.29 2 -3 -4 41.88 2.07 -2 -3 4 39.83 2.25 -2 -3 4 38.41 1.91 -2 3 3 41.28 1.68 2 3 -3 37.30 2.13 -2 3 3 37.37 2.03 -2 -3 3 37.64 2.02 2 -3 -3 39.24 1.73 -2 3 2 253.10 8.76 2 3 -2 238.29 8.73 -2 -3 2 255.04 8.86 2 -3 -2 249.98 8.51 -2 -3 2 241.12 8.73 2 -3 -2 255.88 8.76 2 3 -1 65.13 2.68 -2 3 1 73.27 2.76 2 3 -1 71.90 2.79 2 3 -1 74.78 2.86 -2 -3 1 75.36 2.90 2 -3 -1 69.94 2.72 -2 -3 1 68.05 2.66 2 3 0 38.32 1.84 2 3 0 37.94 1.81 -2 -3 0 40.57 1.89 -2 -3 0 39.02 1.78 2 3 1 368.74 13.10 2 3 1 401.81 13.20 -2 -3 -1 367.66 13.10 2 3 2 115.07 4.43 2 3 2 100.72 4.23 -2 -3 -2 110.74 4.48 2 -3 2 108.46 4.41 2 3 3 26.58 1.90 2 3 3 27.71 1.36 2 3 3 24.66 1.68 2 -3 3 28.94 2.02 -2 -3 -3 24.27 2.23 2 3 4 142.01 5.28 2 3 4 151.60 6.09 2 -3 4 153.86 6.19 2 3 5 119.41 5.39 2 -3 5 124.91 5.50 2 3 6 3.11 1.15 2 -3 6 1.41 1.10 2 3 7 32.16 2.77 2 -3 7 31.36 2.88 2 3 8 43.25 3.50 2 -3 8 40.07 3.48 -2 4 9 1.91 1.46 -2 -4 9 -0.80 1.29 -2 4 8 12.72 1.43 -2 4 8 15.21 2.18 -2 -4 8 14.61 2.04 -2 -4 8 12.76 1.51 -2 4 7 60.06 3.62 -2 4 7 59.51 2.94 -2 -4 7 59.69 3.59 -2 -4 7 66.99 3.10 -2 4 6 1.13 0.64 -2 4 6 1.89 1.02 2 -4 -6 0.92 1.41 -2 -4 6 0.55 0.95 -2 -4 6 0.07 0.67 -2 4 5 93.69 3.68 -2 4 5 92.56 4.16 2 4 -5 93.74 3.50 -2 -4 5 84.46 3.77 -2 -4 5 90.14 4.09 2 -4 -5 93.25 3.99 -2 4 4 27.79 1.87 -2 4 4 29.92 1.51 -2 -4 4 26.14 1.82 -2 -4 4 28.88 1.57 2 -4 -4 27.54 1.73 -2 4 3 152.41 5.30 -2 4 3 157.97 5.62 2 4 -3 140.55 5.35 2 4 -3 145.70 5.61 2 -4 -3 146.38 5.31 -2 -4 3 142.87 5.54 -2 4 2 84.48 3.34 2 4 -2 81.95 3.35 2 -4 -2 90.86 3.35 2 -4 -2 87.68 3.18 -2 -4 2 80.78 3.30 -2 -4 2 81.21 3.46 -2 4 1 590.75 19.08 2 4 -1 541.62 19.10 2 4 -1 523.57 19.05 2 4 -1 555.94 19.24 -2 -4 1 566.93 19.08 2 -4 -1 583.82 19.07 -2 -4 1 585.56 19.29 2 4 0 31.73 1.69 2 4 0 34.88 1.76 -2 -4 0 32.93 1.66 -2 -4 0 34.95 1.79 2 4 1 78.18 3.25 2 4 1 82.81 3.25 -2 -4 -1 75.38 3.24 -2 -4 -1 79.20 3.26 2 4 2 30.75 1.82 2 4 2 37.11 1.68 2 4 2 35.28 1.98 2 -4 2 34.23 2.04 -2 -4 -2 34.59 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5.58 1.27 -2 6 5 40.35 2.38 -2 6 5 38.78 2.04 2 6 -5 38.60 1.89 -2 -6 5 37.27 2.08 2 -6 -5 38.52 2.47 -2 -6 5 31.85 2.23 2 6 -4 1.36 0.65 -2 6 4 1.59 0.63 -2 6 4 1.36 0.78 -2 -6 4 0.92 0.68 -2 -6 4 1.80 0.84 2 -6 -4 2.23 0.88 2 6 -3 160.92 6.13 -2 6 3 166.90 6.22 -2 6 3 167.61 6.07 2 6 -3 162.08 6.23 -2 -6 3 164.01 6.19 -2 -6 3 174.96 6.44 2 -6 -3 172.35 6.12 -2 6 2 46.79 2.07 2 6 -2 45.90 2.19 2 6 -2 43.45 2.11 2 6 -2 42.79 2.17 2 -6 -2 45.76 2.10 -2 -6 2 42.52 2.26 2 -6 -2 49.01 2.09 -2 -6 2 44.01 2.00 2 6 -1 328.63 11.66 -2 6 1 342.77 11.50 2 6 -1 339.15 11.51 2 6 -1 323.56 11.58 -2 6 1 354.00 11.46 2 6 -1 314.30 11.72 2 -6 -1 358.11 11.46 -2 -6 1 314.81 11.57 2 6 0 17.99 1.29 -2 6 0 17.70 0.88 2 6 0 16.54 1.27 2 6 0 17.64 1.34 -2 -6 0 15.07 1.25 -2 -6 0 18.40 1.47 2 6 1 3.30 0.75 2 6 1 3.81 0.73 2 6 1 3.39 0.80 -2 -6 -1 2.84 0.80 2 -6 1 2.31 0.39 -2 -6 -1 1.74 0.70 2 6 2 10.28 0.98 2 6 2 8.54 1.13 2 6 2 8.20 1.05 -2 -6 -2 6.73 1.06 -2 -6 -2 7.79 1.33 2 6 3 218.92 7.96 2 6 3 227.84 8.44 2 -6 3 224.83 8.48 2 6 4 53.95 2.91 2 6 4 51.17 2.27 2 -6 4 49.73 2.93 2 6 5 19.88 2.11 2 6 5 14.87 1.11 2 -6 5 18.57 2.09 2 6 6 0.07 1.08 2 -6 6 0.35 1.08 2 6 7 31.75 2.96 2 -6 7 30.49 2.91 2 6 8 3.42 1.72 2 -6 8 3.08 1.69 -2 7 9 18.50 2.55 -2 -7 9 15.27 2.55 -2 7 8 13.26 2.03 -2 7 8 14.99 1.67 -2 -7 8 10.39 1.96 -2 -7 8 12.46 1.74 -2 7 7 2.00 0.83 -2 7 7 -1.37 0.99 -2 -7 7 -0.68 0.73 -2 -7 7 0.57 0.92 2 7 -6 26.99 1.63 -2 7 6 30.87 1.97 -2 7 6 31.59 2.33 -2 -7 6 31.87 2.14 -2 -7 6 32.93 2.29 -2 7 5 119.52 5.26 2 7 -5 125.08 4.84 -2 7 5 126.61 5.00 2 -7 -5 142.17 5.31 -2 -7 5 117.43 5.41 -2 -7 5 125.93 5.25 -2 7 4 0.72 0.73 -2 7 4 1.69 0.66 2 7 -4 1.98 0.74 -2 -7 4 1.30 0.80 -2 -7 4 1.11 0.70 2 -7 -4 2.27 0.91 2 7 -3 86.62 3.74 -2 7 3 95.43 3.74 2 7 -3 88.68 3.70 -2 7 3 97.93 3.66 -2 -7 3 85.56 3.65 -2 -7 3 85.03 3.87 2 -7 -3 94.46 3.70 2 7 -2 82.74 3.46 2 7 -2 90.27 3.63 -2 7 2 89.43 3.45 2 7 -2 88.82 3.66 -2 -7 2 86.93 3.47 -2 -7 2 83.00 3.37 -2 -7 2 93.92 3.80 2 -7 -2 89.90 3.53 -2 7 1 94.12 3.57 2 7 -1 85.47 3.67 2 7 -1 93.41 3.83 -2 7 1 94.06 3.48 2 7 -1 94.01 3.58 -2 -7 1 92.68 3.69 2 -7 -1 94.80 3.46 -2 -7 1 103.60 3.97 2 7 0 27.79 1.56 2 7 0 19.28 1.56 -2 7 0 25.47 1.19 2 7 0 28.90 1.72 -2 -7 0 27.46 1.61 -2 -7 0 27.38 1.70 2 -7 0 24.15 1.16 2 7 1 385.78 13.05 2 7 1 379.80 13.16 2 7 1 377.94 13.21 -2 -7 -1 360.73 13.17 2 -7 1 368.75 12.67 -2 -7 -1 369.62 13.14 2 7 2 23.90 1.50 2 7 2 23.17 1.67 2 7 2 25.28 1.76 2 -7 2 25.29 1.34 -2 -7 -2 23.73 1.76 -2 -7 -2 26.83 2.01 2 7 3 4.75 0.76 2 7 3 3.60 0.98 2 7 4 11.88 1.11 2 7 4 16.48 1.76 2 -7 4 13.85 1.71 2 7 5 131.08 5.02 2 7 5 133.95 5.90 2 -7 5 141.94 6.09 2 7 6 2.73 1.24 2 -7 6 1.70 1.14 2 7 7 55.21 3.74 2 -7 7 52.03 3.74 2 7 8 20.58 2.75 2 -7 8 22.54 2.96 -2 8 9 27.55 3.02 -2 -8 9 26.90 3.34 -2 -8 9 34.34 3.31 -2 8 8 11.93 1.58 -2 8 8 14.76 2.11 -2 -8 8 10.03 1.61 -2 -8 8 8.67 1.85 -2 8 7 151.59 6.61 -2 8 7 152.38 6.07 -2 -8 7 143.08 6.71 -2 -8 7 147.47 6.29 -2 -8 7 152.52 6.56 -2 8 6 31.29 2.04 -2 8 6 26.55 2.28 2 8 -6 34.43 1.79 -2 -8 6 27.33 2.47 -2 -8 6 29.81 2.08 -2 -8 6 26.68 2.24 -2 8 5 11.58 1.22 -2 8 5 6.23 1.16 2 8 -5 8.02 1.05 2 -8 -5 8.34 1.55 -2 -8 5 7.06 1.17 -2 -8 5 8.54 1.38 -2 8 4 73.10 3.30 -2 8 4 69.53 3.13 2 8 -4 72.99 3.16 -2 -8 4 71.08 3.46 2 -8 -4 74.20 3.34 -2 -8 4 71.33 3.23 -2 8 3 84.33 3.37 2 8 -3 75.29 3.39 2 8 -3 76.46 3.37 -2 -8 3 84.45 3.62 -2 -8 3 74.69 3.25 2 -8 -3 80.05 3.39 -2 8 2 23.80 1.35 2 8 -2 20.84 1.48 2 8 -2 22.38 1.48 -2 8 2 22.06 1.43 2 8 -2 21.18 1.60 2 -8 -2 22.05 1.56 -2 -8 2 20.24 1.24 -2 -8 2 20.21 1.33 -2 -8 2 23.98 1.72 -2 8 1 144.55 5.36 -2 8 1 140.20 5.11 -2 8 1 141.59 4.96 2 8 -1 134.73 5.32 2 8 -1 133.79 5.04 2 -8 -1 148.27 4.97 -2 -8 1 128.63 5.21 -2 -8 1 138.85 5.47 2 8 0 54.85 2.51 2 8 0 45.86 2.38 -2 8 0 52.47 2.53 2 8 0 53.28 2.55 -2 8 0 49.79 2.09 -2 -8 0 51.24 2.59 -2 -8 0 53.53 2.48 2 -8 0 55.05 2.03 2 -8 0 51.87 2.07 2 8 1 5.88 0.91 2 8 1 6.06 0.92 2 8 1 4.75 0.91 -2 -8 -1 4.26 0.92 2 -8 1 5.38 0.55 -2 -8 -1 5.11 0.94 2 8 2 51.28 2.65 2 8 2 49.24 2.56 2 8 2 53.92 2.43 -2 -8 -2 52.84 2.71 2 -8 2 49.05 2.18 -2 -8 -2 52.53 2.91 2 8 3 217.32 8.36 2 8 3 216.95 7.97 2 -8 3 225.69 7.99 2 8 4 24.36 2.05 2 8 4 22.77 1.50 2 -8 4 24.75 2.07 2 8 5 3.09 1.21 2 8 5 4.49 0.79 2 -8 5 3.99 1.32 2 8 6 46.96 3.23 2 -8 6 46.78 3.33 2 8 7 14.61 2.17 2 -8 7 8.05 1.92 2 8 8 7.87 2.09 2 -8 8 4.89 1.90 -2 9 9 12.44 2.11 -2 -9 9 13.23 2.55 -2 -9 9 10.99 2.18 -2 9 8 24.63 2.67 -2 9 8 21.57 2.10 -2 -9 8 24.27 2.85 -2 -9 8 22.96 2.40 -2 -9 8 32.07 3.03 -2 9 7 6.97 1.22 -2 9 7 6.63 1.45 -2 -9 7 6.08 1.39 -2 -9 7 3.32 1.20 -2 -9 7 6.01 1.60 -2 9 6 123.77 5.13 2 9 -6 124.39 4.86 -2 9 6 116.80 5.41 -2 -9 6 123.08 5.39 -2 -9 6 117.66 5.62 -2 -9 6 134.08 5.32 2 9 -5 80.80 3.70 -2 9 5 86.74 4.04 -2 9 5 90.19 3.85 -2 -9 5 89.21 4.29 -2 -9 5 88.81 3.97 2 -9 -5 91.44 4.20 -2 9 4 13.13 1.38 2 9 -4 13.61 1.36 -2 9 4 14.45 1.37 -2 -9 4 13.31 1.55 -2 -9 4 13.12 1.37 2 -9 -4 13.20 1.54 2 9 -3 13.92 1.35 -2 9 3 15.61 1.29 -2 9 3 16.44 1.40 2 9 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1.71 2 9 7 53.01 3.71 2 -9 7 46.28 3.73 2 9 8 39.12 3.60 2 -9 8 38.44 3.63 -2 10 9 1.55 1.23 -2 -10 9 3.25 1.62 -2 -10 9 6.04 2.03 -2 10 8 27.54 2.78 -2 10 8 29.07 2.33 -2 -10 8 26.85 3.05 -2 -10 8 21.90 2.77 -2 -10 8 34.33 2.81 -2 10 7 36.91 2.38 -2 10 7 32.09 2.65 -2 -10 7 26.25 2.86 -2 -10 7 33.98 2.60 -2 -10 7 36.73 2.57 2 10 -6 54.03 2.69 -2 10 6 51.67 2.88 -2 10 6 52.61 3.11 -2 -10 6 53.01 3.37 -2 -10 6 56.53 3.07 2 10 -5 33.39 2.12 -2 10 5 36.63 2.31 -2 10 5 34.69 2.15 -2 -10 5 36.71 2.58 -2 -10 5 33.82 2.17 -2 10 4 120.99 4.82 2 10 -4 114.33 4.80 -2 10 4 117.17 4.84 -2 -10 4 123.93 5.14 -2 -10 4 118.40 4.78 2 -10 -4 115.58 4.96 2 10 -3 103.47 4.51 -2 10 3 113.06 4.40 -2 10 3 115.97 4.99 -2 -10 3 106.78 4.29 2 -10 -3 115.27 4.63 -2 -10 3 110.48 4.73 -2 10 2 1.82 0.56 -2 10 2 0.65 0.55 2 10 -2 1.08 0.72 2 10 -2 0.62 0.58 -2 10 2 1.41 0.75 2 10 -2 0.34 0.72 2 -10 -2 1.73 0.97 -2 -10 2 1.27 0.65 -2 -10 2 1.46 0.84 -2 -10 2 0.17 0.46 -2 10 1 106.50 4.12 -2 10 1 107.84 3.87 2 10 -1 96.76 4.34 -2 10 1 108.24 4.39 2 10 -1 100.55 4.32 2 10 -1 105.02 3.99 -2 -10 1 106.26 4.52 -2 -10 1 104.22 4.28 2 -10 -1 113.24 3.88 2 10 0 252.22 9.57 2 10 0 281.61 9.79 2 10 0 267.59 9.62 -2 10 0 280.23 9.69 -2 10 0 265.39 9.28 2 -10 0 263.13 9.23 -2 -10 0 254.38 9.70 -2 -10 0 253.74 9.60 -2 10 -1 88.91 3.37 2 10 1 90.83 3.82 -2 10 -1 91.30 3.90 2 10 1 91.23 3.93 2 10 1 88.33 3.92 -2 -10 -1 89.23 3.86 2 -10 1 88.71 3.40 -2 -10 -1 92.09 4.04 2 10 2 70.64 3.21 2 10 2 74.49 3.44 -2 -10 -2 67.61 3.49 2 -10 2 75.67 2.96 2 10 3 110.96 4.72 2 10 3 107.42 4.33 2 -10 3 100.52 4.21 2 10 4 78.06 3.42 2 10 4 78.98 3.93 2 -10 4 78.55 3.56 2 10 5 101.74 4.82 2 10 5 96.62 4.05 2 -10 5 93.29 4.35 2 -10 5 98.81 4.87 2 10 6 68.77 4.12 2 -10 6 75.21 4.34 2 -10 6 73.43 3.85 2 10 7 1.80 1.54 2 -10 7 4.86 1.83 2 -10 7 4.41 1.33 2 10 8 1.62 1.76 2 -10 8 2.18 1.77 -2 11 9 0.88 1.09 -2 -11 9 -0.07 1.32 -2 -11 9 1.91 1.61 -2 11 8 78.17 4.39 -2 11 8 76.11 4.08 -2 -11 8 86.05 5.81 -2 -11 8 77.23 4.36 -2 -11 8 73.03 4.70 -2 11 7 10.48 1.50 -2 11 7 8.70 1.66 -2 -11 7 8.43 1.84 -2 -11 7 11.98 1.73 -2 -11 7 10.97 1.70 -2 11 6 15.82 1.94 2 11 -6 18.38 1.69 -2 11 6 20.53 1.80 -2 -11 6 19.87 2.30 -2 -11 6 19.41 2.00 -2 11 5 1.30 0.82 -2 11 5 0.77 0.78 2 11 -5 1.16 0.86 -2 -11 5 0.96 0.89 -2 -11 5 0.36 0.71 2 11 -4 34.52 2.20 -2 11 4 38.34 2.28 -2 11 4 35.10 2.11 -2 -11 4 37.49 2.06 2 -11 -4 38.12 3.05 -2 -11 4 33.87 2.37 -2 11 3 8.50 1.01 -2 11 3 5.56 0.95 2 11 -3 6.93 1.14 -2 -11 3 8.70 1.30 2 -11 -3 8.11 1.38 -2 -11 3 8.75 0.94 2 11 -2 87.74 3.69 2 11 -2 93.53 4.06 -2 11 2 97.44 3.97 2 11 -2 92.68 4.07 -2 11 2 97.58 3.65 -2 11 2 96.62 4.07 -2 -11 2 91.90 4.20 -2 -11 2 91.37 3.97 2 -11 -2 101.72 4.15 2 11 -1 2.90 0.74 -2 11 1 2.44 0.67 -2 11 1 2.28 0.86 2 11 -1 3.23 0.90 2 11 -1 3.49 0.83 -2 -11 1 2.93 0.85 -2 -11 1 3.25 1.03 -2 11 0 51.58 2.66 2 11 0 45.80 2.52 -2 11 0 52.98 2.23 2 11 0 43.86 2.51 2 11 0 48.27 2.63 2 -11 0 49.16 2.15 -2 -11 0 47.76 2.67 -2 -11 0 48.80 2.52 -2 11 -1 8.54 0.80 -2 11 -1 8.96 1.23 2 11 1 8.70 1.19 2 11 1 7.78 1.14 -2 -11 -1 7.80 1.22 2 -11 1 8.47 0.81 -2 11 -2 257.32 9.42 2 11 2 253.75 9.33 2 11 2 249.07 9.51 -2 -11 -2 256.63 9.64 2 -11 2 258.15 9.06 2 11 3 5.25 0.96 2 11 3 4.42 1.10 2 -11 3 4.02 0.80 2 11 4 46.42 2.88 2 11 4 47.56 2.46 2 -11 4 44.82 2.50 2 11 5 1.38 1.18 2 11 5 1.80 0.78 2 -11 5 1.71 1.22 2 -11 5 1.72 0.91 2 11 6 14.72 2.13 2 -11 6 18.13 2.48 2 -11 6 16.71 1.95 2 11 7 1.20 1.46 2 -11 7 2.80 1.75 2 -11 7 1.88 1.23 2 11 8 35.81 3.70 2 -11 8 41.13 4.13 -2 12 9 3.40 1.38 -2 -12 9 2.18 1.76 -2 -12 9 7.25 1.87 -2 12 8 11.34 1.84 -2 12 8 13.11 2.04 -2 -12 8 10.67 1.94 -2 -12 8 5.96 1.82 -2 12 7 10.54 1.73 -2 12 7 9.30 1.50 -2 -12 7 13.96 2.06 -2 -12 7 11.38 1.77 -2 -12 7 9.84 1.60 2 12 -6 28.96 2.05 -2 12 6 28.99 2.17 -2 12 6 25.89 2.19 -2 -12 6 25.86 2.44 -2 -12 6 29.08 2.16 2 12 -5 1.36 0.90 -2 12 5 2.84 0.99 -2 12 5 2.81 0.91 -2 -12 5 1.96 1.04 -2 -12 5 3.42 0.94 2 12 -4 259.57 9.61 -2 12 4 257.09 9.48 -2 -12 4 250.06 9.35 -2 -12 4 265.09 9.95 2 12 -3 46.16 2.62 -2 12 3 52.67 2.37 -2 12 3 44.09 2.50 2 -12 -3 44.93 3.32 -2 -12 3 46.45 2.18 -2 -12 3 51.24 2.81 -2 12 2 25.18 1.83 2 12 -2 23.89 1.60 -2 12 2 26.22 1.70 -2 12 2 27.32 1.40 2 12 -2 21.65 1.81 2 -12 -2 25.56 2.12 -2 -12 2 20.75 1.51 2 12 -1 13.83 1.48 -2 12 1 10.63 1.31 -2 12 1 12.79 1.15 2 12 -1 12.65 1.06 2 -12 -1 12.59 1.20 -2 -12 1 11.90 1.26 -2 -12 1 16.47 1.71 2 12 0 372.22 13.58 -2 12 0 390.75 13.29 -2 12 0 379.14 13.62 2 12 0 387.17 13.60 2 -12 0 378.32 13.19 -2 -12 0 373.96 13.69 -2 12 -1 9.41 1.33 -2 12 -1 7.45 0.79 2 12 1 5.86 1.10 2 12 1 9.19 1.22 -2 -12 -1 7.60 1.31 2 -12 1 7.00 0.78 -2 12 -2 103.64 4.54 2 12 2 103.59 4.61 2 12 2 107.75 4.46 -2 -12 -2 104.65 4.72 2 -12 2 108.07 4.16 2 12 3 29.52 2.21 2 12 3 28.35 1.93 2 -12 3 27.14 1.74 2 12 4 2.59 0.84 2 12 4 0.64 0.97 2 -12 4 0.95 0.74 2 12 5 -0.28 1.03 2 12 5 -0.24 0.67 2 -12 5 -1.62 1.01 2 -12 5 0.73 0.83 2 12 6 186.49 7.87 2 -12 6 181.56 8.03 2 -12 6 174.48 7.43 2 12 7 8.18 1.96 2 -12 7 6.54 2.00 2 -12 7 9.44 1.81 2 12 8 7.51 2.13 2 -12 8 8.18 2.25 -2 13 8 59.73 4.68 -2 13 8 51.20 3.44 -2 -13 8 50.55 3.44 -2 -13 8 45.77 3.81 -2 13 7 13.47 1.73 -2 13 7 9.23 1.58 -2 -13 7 9.75 1.90 -2 -13 7 12.02 1.83 -2 -13 7 10.02 1.74 -2 13 6 34.13 2.31 -2 13 6 27.15 2.22 2 13 -6 26.37 2.13 -2 -13 6 23.14 2.60 -2 -13 6 28.21 2.14 -2 13 5 39.11 2.53 2 13 -5 45.42 2.68 -2 13 5 46.72 2.71 -2 -13 5 45.18 2.53 -2 -13 5 48.08 3.07 2 13 -4 42.32 2.67 -2 13 4 44.15 2.44 -2 -13 4 52.39 3.03 -2 -13 4 45.02 2.33 -2 13 3 2.32 0.86 2 13 -3 2.17 0.97 -2 13 3 1.71 0.65 -2 -13 3 3.74 1.06 -2 -13 3 2.24 0.62 -2 13 2 166.04 6.56 -2 13 2 170.37 6.01 2 13 -2 157.74 6.57 -2 13 2 180.56 6.52 2 13 -2 156.06 6.04 -2 -13 2 168.96 6.80 2 13 -1 2.47 0.93 2 13 -1 1.82 0.70 -2 13 1 2.86 0.90 -2 13 1 2.39 0.73 -2 -13 1 2.49 0.98 2 -13 -1 2.45 0.76 -2 13 0 48.52 2.59 2 13 0 41.79 2.49 -2 13 0 42.69 2.16 2 13 0 40.99 2.51 2 -13 0 47.32 2.16 -2 -13 0 41.90 2.61 -2 13 -1 44.90 2.05 2 13 1 44.48 2.54 -2 13 -1 42.36 2.57 2 13 1 48.42 2.58 2 -13 1 44.82 2.07 -2 -13 -1 43.41 2.71 2 13 2 22.60 1.80 -2 13 -2 23.58 1.98 2 13 2 25.39 1.94 2 -13 2 23.02 1.47 -2 -13 -2 25.93 2.17 2 13 3 4.09 1.12 2 13 3 3.55 0.93 2 -13 3 4.07 0.84 2 13 4 247.36 9.71 2 13 4 247.50 9.23 2 -13 4 248.80 9.27 2 13 5 23.08 1.88 2 13 5 28.52 2.53 2 -13 5 27.31 2.10 2 13 6 1.66 1.38 2 -13 6 -1.40 0.90 2 -13 6 -0.12 1.34 2 13 7 9.31 2.01 2 -13 7 9.95 2.17 -2 14 8 4.34 1.40 -2 -14 8 3.78 1.68 -2 -14 8 6.52 1.62 -2 14 7 50.64 3.12 -2 14 7 48.28 3.17 -2 -14 7 49.95 3.62 -2 -14 7 49.25 3.15 -2 14 6 51.77 3.06 2 14 -6 48.42 2.96 -2 14 6 46.48 3.00 -2 -14 6 52.75 2.93 -2 -14 6 50.42 3.43 2 14 -5 11.64 1.61 -2 14 5 11.62 1.48 -2 -14 5 11.28 1.39 -2 -14 5 11.80 1.85 2 14 -4 87.46 4.15 -2 14 4 85.55 3.99 -2 14 4 90.91 3.88 -2 -14 4 93.86 4.49 -2 -14 4 84.72 3.70 -2 14 3 55.18 2.54 -2 14 3 54.78 2.92 2 14 -3 58.16 3.09 -2 -14 3 54.89 3.20 -2 -14 3 51.82 2.41 2 14 -2 8.77 1.32 2 14 -2 8.44 1.01 -2 14 2 7.51 0.78 -2 14 2 6.57 1.17 -2 -14 2 6.91 1.32 2 14 -1 89.50 4.21 2 14 -1 87.60 3.61 -2 14 1 92.91 3.95 -2 14 1 101.75 4.30 2 -14 -1 98.65 3.97 -2 -14 1 94.14 4.38 2 14 0 56.13 2.87 -2 14 0 51.76 2.47 -2 14 0 45.22 2.75 -2 -14 0 53.26 2.95 2 -14 0 47.62 2.37 2 14 1 32.38 2.17 -2 14 -1 29.16 2.21 2 14 1 31.57 2.18 -2 14 -1 28.31 1.61 -2 -14 -1 31.38 2.33 2 -14 1 29.39 1.64 -2 14 -2 44.36 2.78 2 14 2 47.07 2.83 2 14 2 49.72 2.74 -2 -14 -2 52.34 2.99 2 -14 2 48.16 2.31 2 14 3 195.29 8.10 2 14 3 207.39 7.86 2 -14 3 210.13 7.66 -2 -14 -3 198.93 8.25 2 14 4 0.42 0.80 2 14 4 -0.30 0.96 2 -14 4 -0.31 0.69 2 14 5 1.92 0.95 2 14 5 0.17 1.05 2 -14 5 -0.26 0.78 2 14 6 59.28 3.87 2 -14 6 53.82 3.34 2 -14 6 55.97 3.89 2 14 7 19.85 2.68 2 -14 7 18.42 2.68 -2 15 8 20.34 2.41 -2 -15 8 19.14 2.71 -2 -15 8 20.30 2.50 -2 15 7 -0.16 0.97 -2 15 7 1.64 1.02 -2 -15 7 -0.18 1.35 -2 -15 7 1.65 0.97 -2 15 6 11.44 1.67 -2 15 6 10.60 1.58 2 15 -6 11.46 1.68 -2 -15 6 10.83 1.98 -2 -15 6 10.79 1.55 -2 15 5 47.28 2.69 2 15 -5 48.61 2.95 -2 -15 5 47.82 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40.42 3.78 4 -9 7 41.97 3.95 -4 10 9 0.71 1.26 -4 -10 9 -1.02 1.35 -4 -10 9 0.26 1.57 -4 10 8 62.56 3.82 -4 -10 8 49.82 3.90 -4 -10 8 54.81 3.76 -4 10 7 -1.35 0.91 4 10 -7 1.76 0.92 -4 -10 7 0.22 1.29 -4 -10 7 0.16 1.03 4 10 -6 9.31 1.38 -4 10 6 6.29 1.36 4 -10 -6 7.04 1.71 -4 -10 6 7.29 1.64 -4 -10 6 4.49 1.26 -4 10 5 1.11 0.86 4 10 -5 -0.70 0.88 4 -10 -5 0.89 1.19 -4 -10 5 -0.03 0.97 -4 -10 5 0.84 0.78 -4 -10 5 -0.14 0.59 -4 10 4 286.09 10.14 -4 -10 4 265.29 10.07 -4 -10 4 265.26 9.89 4 -10 -4 284.91 10.02 -4 -10 4 276.08 10.56 -4 10 3 8.39 1.10 4 10 -3 9.75 1.36 4 10 -3 11.39 1.54 -4 -10 3 9.23 1.09 4 -10 -3 11.67 1.17 -4 -10 3 7.34 1.31 4 -10 -3 10.28 1.37 4 10 -2 13.50 1.51 -4 10 2 11.22 1.12 -4 10 2 11.71 1.14 4 10 -2 13.60 1.42 -4 -10 2 9.52 1.42 -4 -10 2 12.78 1.32 4 -10 -2 12.22 1.10 -4 10 1 5.41 0.68 4 10 -1 4.20 0.94 4 10 -1 5.36 1.13 4 -10 -1 5.74 0.76 -4 -10 1 5.31 1.22 -4 -10 1 6.28 0.93 4 10 0 62.47 3.10 4 10 0 62.71 3.13 -4 -10 0 63.80 3.32 4 10 1 5.87 1.17 4 10 1 5.89 1.16 -4 -10 -1 6.22 1.22 4 10 2 175.68 7.10 4 10 2 181.52 6.91 -4 -10 -2 165.07 7.11 4 10 3 2.13 1.12 4 10 3 1.48 0.88 4 -10 3 2.10 1.20 4 -10 3 1.19 0.53 4 10 4 22.46 1.85 4 10 4 21.30 2.48 4 -10 4 22.47 2.56 4 -10 4 18.95 1.59 4 10 5 12.60 2.19 4 10 5 18.76 1.76 4 -10 5 13.38 2.38 4 -10 5 13.62 2.36 4 10 6 65.92 4.38 4 -10 6 65.28 4.53 4 10 7 3.87 1.77 4 -10 7 1.89 1.76 -4 11 9 3.20 1.21 -4 -11 9 1.90 1.43 -4 -11 9 2.04 1.70 -4 11 8 27.57 2.79 -4 -11 8 27.19 3.23 -4 -11 8 34.11 2.88 4 11 -7 1.18 1.05 -4 11 7 4.06 1.34 -4 -11 7 4.58 1.40 -4 -11 7 2.74 1.50 4 11 -6 323.10 11.53 -4 11 6 308.27 11.73 -4 -11 6 326.23 12.26 4 -11 -6 292.08 11.77 -4 -11 6 304.02 11.69 -4 11 5 4.44 1.08 4 11 -5 4.05 1.20 -4 -11 5 3.48 0.99 4 -11 -5 4.14 1.47 -4 -11 5 2.57 0.91 -4 -11 5 2.03 1.26 -4 11 4 1.21 0.73 4 11 -4 2.20 1.10 -4 -11 4 3.37 0.85 4 -11 -4 2.37 1.29 -4 -11 4 -0.54 0.84 -4 -11 4 1.63 0.73 -4 11 3 3.12 0.78 4 11 -3 2.29 1.33 -4 11 3 1.90 0.74 4 11 -3 1.58 0.92 4 -11 -3 2.01 1.16 -4 -11 3 1.15 0.94 4 -11 -3 2.79 0.65 -4 -11 3 1.28 0.75 4 11 -2 238.15 9.33 -4 11 2 254.87 8.95 4 11 -2 246.60 9.08 -4 -11 2 259.05 9.59 4 -11 -2 242.22 8.84 -4 -11 2 244.38 9.12 4 11 -1 7.68 1.18 4 11 -1 10.98 1.43 -4 11 1 8.42 0.86 4 -11 -1 9.45 0.90 -4 -11 1 10.43 1.53 4 11 0 172.60 6.76 4 11 0 167.83 6.69 -4 -11 0 163.62 6.85 4 -11 0 170.70 6.19 4 11 1 35.88 2.34 4 11 1 34.10 2.30 -4 -11 -1 33.73 2.49 4 11 2 30.43 2.16 4 11 2 29.57 2.33 -4 -11 -2 30.95 2.48 4 11 3 8.55 1.57 4 11 3 10.55 1.41 4 -11 3 7.61 0.81 -4 -11 -3 9.01 1.69 4 11 4 209.06 8.48 4 11 4 196.84 7.68 4 -11 4 187.51 8.37 4 -11 4 201.01 7.35 4 11 5 0.18 1.30 4 11 5 1.00 0.91 4 -11 5 -0.23 1.34 4 11 6 6.00 1.84 4 -11 6 2.01 1.66 4 11 7 4.03 1.78 4 -11 7 9.94 2.33 -4 12 9 0.36 1.01 -4 -12 9 0.51 1.60 -4 -12 9 1.53 1.52 -4 12 8 24.82 2.59 -4 -12 8 22.30 2.96 -4 -12 8 22.99 2.71 4 12 -7 -0.54 0.99 -4 12 7 -0.41 0.87 -4 -12 7 0.20 1.26 -4 -12 7 -1.11 0.92 -4 12 6 17.65 1.94 4 12 -6 13.71 1.71 -4 -12 6 11.26 1.98 -4 -12 6 15.12 1.78 -4 12 5 11.05 1.46 4 12 -5 10.45 1.48 -4 -12 5 8.32 0.99 -4 -12 5 8.21 1.67 -4 -12 5 11.44 1.45 4 12 -4 143.09 5.97 -4 12 4 145.81 5.71 -4 -12 4 136.18 6.22 -4 -12 4 135.81 5.63 4 -12 -4 149.51 5.92 -4 -12 4 143.07 5.59 4 12 -3 -0.24 1.32 -4 12 3 1.19 0.68 4 12 -3 0.62 0.99 -4 12 3 0.47 0.76 4 -12 -3 -0.24 0.44 -4 -12 3 0.59 0.94 4 -12 -3 1.23 1.21 -4 -12 3 -0.42 0.34 -4 12 2 45.90 2.32 4 12 -2 47.09 2.68 4 12 -2 41.62 2.68 -4 -12 2 46.83 2.96 4 -12 -2 50.80 2.25 4 12 -1 6.81 1.32 4 12 -1 8.61 1.24 4 12 -1 5.62 1.17 -4 12 1 7.88 0.83 -4 -12 1 7.63 1.43 4 -12 -1 8.48 0.85 4 12 0 154.89 6.41 4 12 0 165.45 6.51 4 -12 0 157.17 5.87 -4 -12 0 163.47 6.65 4 12 1 4.88 1.16 4 12 1 4.04 1.04 -4 -12 -1 3.68 1.20 4 12 2 73.78 3.59 4 12 2 68.66 3.73 -4 -12 -2 74.57 3.92 4 12 3 17.26 2.10 4 12 3 19.73 1.87 -4 -12 -3 17.19 2.19 4 -12 3 14.77 1.09 4 12 4 14.89 1.69 4 12 4 17.75 2.35 4 -12 4 13.64 1.43 4 -12 4 11.81 2.11 4 12 5 1.29 1.41 4 12 5 0.50 0.89 4 -12 5 1.74 1.58 4 12 6 62.04 4.32 4 -12 6 58.96 4.44 4 12 7 3.34 1.85 4 -12 7 1.15 1.85 -4 13 8 24.65 2.60 -4 -13 8 20.44 2.84 -4 -13 8 24.19 2.71 4 13 -7 24.07 2.26 -4 13 7 22.37 2.38 -4 -13 7 29.50 2.49 -4 -13 7 23.82 2.92 -4 13 6 30.62 2.49 4 13 -6 32.24 2.50 -4 -13 6 33.69 3.07 -4 -13 6 33.52 2.42 4 13 -5 7.03 1.42 -4 13 5 6.63 1.23 -4 -13 5 7.44 1.64 -4 -13 5 8.26 1.35 4 13 -4 3.12 1.19 -4 13 4 1.65 0.79 -4 -13 4 1.58 0.79 -4 -13 4 3.15 1.22 4 13 -3 39.80 2.59 -4 13 3 43.18 2.17 4 13 -3 34.82 2.91 -4 -13 3 38.70 2.82 4 13 -2 143.26 6.08 -4 13 2 148.95 5.66 4 13 -2 139.73 5.77 4 -13 -2 146.72 5.48 -4 -13 2 147.80 6.31 4 13 -1 0.12 1.06 4 13 -1 0.68 0.94 4 13 -1 -0.19 0.76 -4 13 1 1.70 0.57 -4 -13 1 0.37 1.01 4 -13 -1 1.06 0.46 4 13 0 47.68 2.81 4 13 0 45.88 2.81 -4 13 0 48.79 1.98 4 -13 0 48.38 2.16 -4 -13 0 50.46 3.02 4 13 1 92.56 4.19 4 13 1 90.87 4.28 -4 -13 -1 80.84 4.31 4 13 2 27.02 2.25 4 13 2 29.42 2.21 -4 -13 -2 25.75 2.45 4 13 3 16.27 1.77 4 13 3 16.11 2.06 4 -13 3 15.27 1.06 -4 -13 -3 16.29 2.09 4 13 4 191.91 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22.03 2.81 4 20 3 27.17 3.04 4 20 3 30.72 2.79 -4 -20 -3 29.78 3.30 4 20 4 16.18 2.48 4 20 4 15.17 2.12 4 20 5 18.60 2.67 4 20 5 18.00 2.24 4 21 -7 2.03 1.41 -4 21 7 0.79 1.16 -4 -21 7 1.76 1.86 4 21 -6 76.45 4.48 -4 21 6 76.29 3.92 -4 -21 6 73.28 5.11 4 21 -5 25.25 2.81 -4 21 5 20.74 1.79 -4 -21 5 22.82 3.14 4 21 -4 2.03 1.47 -4 21 4 4.46 0.82 -4 -21 4 2.36 1.62 4 21 -3 13.86 2.17 -4 -21 3 16.86 2.52 4 21 -2 33.30 2.85 -4 -21 2 26.70 2.97 4 21 -1 22.83 2.57 -4 -21 1 25.77 2.88 4 21 0 74.31 4.26 -4 -21 0 70.18 4.50 4 21 1 29.42 2.74 4 21 1 30.71 2.79 -4 -21 -1 34.25 3.24 4 21 2 7.91 1.84 4 21 2 11.05 1.88 -4 -21 -2 10.48 2.16 4 21 3 17.23 2.22 4 21 3 13.19 2.30 -4 -21 -3 18.55 2.69 4 21 4 69.60 4.02 4 21 4 62.26 4.38 4 21 5 2.41 1.29 4 21 5 3.08 1.58 4 22 -6 24.50 2.82 -4 -22 6 12.64 2.70 4 22 -5 1.83 1.50 -4 -22 5 -0.84 1.53 4 22 -4 106.94 5.56 -4 -22 4 104.44 5.96 4 22 -3 0.26 1.28 -4 -22 3 0.16 1.39 4 22 -2 14.82 2.12 -4 -22 2 15.95 2.42 4 22 -1 3.63 1.43 -4 -22 1 3.13 1.54 4 22 0 51.66 3.51 -4 -22 0 43.28 3.65 4 22 1 2.73 1.40 -4 -22 -1 3.19 1.74 4 22 2 58.14 3.84 4 22 2 65.67 4.12 -4 -22 -2 55.31 4.30 4 22 3 -0.15 1.29 4 22 3 -0.39 1.12 -4 -22 -3 -2.16 1.53 4 22 4 5.41 1.62 4 22 4 5.30 1.83 4 23 -6 8.14 1.92 -4 -23 6 11.74 2.63 4 23 -5 6.22 1.89 -4 -23 5 7.95 2.29 4 23 -4 -1.90 1.28 -4 -23 4 3.31 1.81 4 23 -3 0.72 1.33 -4 -23 3 0.32 1.63 4 23 -2 66.52 4.17 -4 -23 2 61.05 4.35 4 23 -1 -0.26 1.19 -4 -23 1 -0.68 1.34 4 23 0 28.53 3.07 -4 -23 0 25.47 3.01 4 23 1 0.37 1.22 -4 -23 -1 -0.36 1.50 4 23 2 32.77 3.09 4 23 2 35.91 3.26 -4 -23 -2 35.93 3.65 4 23 3 0.84 1.43 4 23 3 3.94 1.51 -4 -23 -3 0.11 1.65 4 23 4 51.38 3.70 4 23 4 55.04 4.09 4 24 -6 1.65 1.53 -4 -24 6 2.90 1.97 4 24 -5 7.05 1.99 -4 -24 5 11.79 2.68 4 24 -4 70.99 4.52 -4 -24 4 67.42 4.92 4 24 -3 8.26 1.99 -4 -24 3 6.84 2.11 4 24 -2 3.00 1.58 -4 -24 2 3.46 1.72 4 24 -1 17.67 2.49 -4 -24 1 16.09 2.48 4 24 0 60.74 4.01 -4 -24 0 60.28 4.39 4 24 1 0.84 1.39 -4 -24 -1 0.16 1.60 4 24 2 31.72 3.03 -4 -24 -2 29.00 3.38 4 24 3 12.04 2.29 4 24 3 13.09 2.22 -4 -24 -3 9.49 2.40 4 24 4 5.90 1.89 4 25 -5 14.74 2.47 -4 -25 5 9.17 2.51 4 25 -4 9.89 2.18 -4 -25 4 13.68 2.81 4 25 -3 3.39 1.64 -4 -25 3 4.89 1.90 4 25 -2 40.24 3.50 -4 -25 2 42.33 3.73 4 25 -1 -0.99 1.30 -4 -25 1 1.42 1.55 4 25 0 5.56 1.76 -4 -25 0 8.20 2.09 4 25 1 28.89 3.05 -4 -25 -1 24.11 3.12 4 25 2 14.80 2.36 -4 -25 -2 15.69 2.71 4 25 3 1.22 1.55 4 25 3 3.08 1.58 -4 -25 -3 3.75 2.02 4 26 -4 14.62 2.44 -4 -26 4 8.95 2.49 4 26 -3 -1.90 1.34 -4 -26 3 0.89 1.72 4 26 -2 -2.66 1.13 -4 -26 2 0.38 1.46 4 26 -1 53.22 3.85 -4 -26 1 43.18 4.01 4 26 0 10.43 2.02 -4 -26 0 8.96 2.21 4 26 1 1.06 1.39 -4 -26 -1 0.83 1.69 4 26 2 26.65 3.19 -4 -26 -2 29.23 3.58 4 27 -4 1.41 1.52 -4 -27 4 1.49 1.77 4 27 -3 22.86 2.95 -4 -27 3 21.94 3.27 4 27 -2 7.90 1.98 -4 -27 2 5.11 2.04 4 27 -1 8.91 2.05 -4 -27 1 7.03 2.18 4 27 0 1.13 1.47 -4 -27 0 1.38 1.66 4 27 1 26.83 3.13 -4 -27 -1 20.78 3.04 4 27 2 4.94 1.81 -4 -27 -2 3.57 1.93 4 28 -3 16.72 2.72 -4 -28 3 20.99 3.14 4 28 -2 3.03 1.73 -4 -28 2 5.69 2.25 4 28 -1 41.57 3.72 -4 -28 1 38.16 3.77 4 28 0 1.51 1.63 -4 -28 0 1.11 1.68 4 28 1 0.16 1.40 -4 -28 -1 4.48 2.06 4 29 -1 -1.80 1.46 -5 0 9 0.62 1.43 -5 0 8 115.26 5.79 -5 0 7 0.05 1.17 -5 0 6 5.75 1.39 -5 0 5 -1.27 0.82 -5 0 3 -0.46 0.65 -5 0 3 0.04 0.73 5 0 -2 497.41 17.43 5 0 -2 513.59 18.16 -5 0 2 519.83 17.66 -5 0 1 -0.14 0.59 5 0 -1 -0.08 0.50 -5 0 1 -1.25 0.51 5 0 -1 -0.99 0.52 5 0 0 253.15 8.55 5 0 0 239.17 8.83 -5 0 0 230.61 8.55 -5 0 0 233.99 8.82 -5 0 -1 -0.78 0.53 5 0 1 0.12 0.76 5 0 1 0.31 0.48 5 0 2 254.65 9.66 5 0 2 250.09 9.13 5 0 3 0.46 0.58 5 0 3 0.33 0.98 5 0 4 7.39 1.63 5 0 5 2.11 1.47 5 0 6 107.88 5.85 5 0 7 -0.74 1.53 -5 1 9 1.85 1.58 -5 -1 9 1.41 1.54 -5 1 8 20.37 2.49 -5 -1 8 16.52 2.37 -5 1 7 9.52 1.75 -5 -1 7 6.32 1.56 -5 1 6 123.96 5.60 -5 -1 6 127.57 5.65 -5 1 5 14.39 1.70 -5 -1 5 13.62 1.66 -5 1 4 -0.43 0.75 -5 -1 4 -0.05 0.79 -5 -1 4 1.59 0.88 -5 1 3 38.98 2.17 -5 1 3 34.67 2.18 -5 -1 3 37.19 2.20 -5 -1 3 36.75 2.23 -5 1 2 198.50 7.01 5 1 -2 185.28 6.81 -5 -1 2 197.87 6.82 5 -1 -2 186.21 7.35 5 -1 -2 188.23 6.83 -5 -1 2 182.72 7.07 5 1 -1 3.18 0.69 5 1 -1 1.29 0.66 -5 1 1 2.34 0.69 5 -1 -1 3.17 0.76 -5 -1 1 3.03 0.79 -5 -1 1 1.78 0.66 5 1 0 32.58 1.72 5 1 0 27.52 1.93 -5 1 0 29.04 1.65 -5 -1 0 29.37 1.95 5 -1 0 31.01 2.03 5 -1 0 34.04 1.60 -5 -1 0 31.21 1.83 5 1 1 11.75 1.14 5 1 1 12.09 1.51 -5 1 -1 11.97 1.13 5 -1 1 15.47 1.65 -5 -1 -1 11.12 1.18 5 -1 1 12.92 1.03 5 1 2 27.04 2.21 5 1 2 26.70 1.73 5 -1 2 28.66 1.64 5 -1 2 30.16 2.29 5 1 3 1.23 1.08 5 1 3 0.64 0.62 5 -1 3 0.66 0.60 5 -1 3 0.30 0.93 5 1 4 112.07 5.50 5 -1 4 120.16 5.60 5 1 5 1.62 1.42 5 -1 5 2.57 1.46 5 1 6 12.38 2.29 5 -1 6 9.00 2.12 5 1 7 1.19 1.69 5 -1 7 1.64 1.67 -5 2 9 -0.15 1.40 -5 -2 9 3.98 1.68 -5 2 8 22.44 2.67 -5 -2 8 22.24 2.71 -5 2 7 6.97 1.66 -5 -2 7 8.65 1.69 -5 2 6 29.35 2.42 -5 -2 6 28.79 2.48 -5 2 5 37.53 2.51 -5 -2 5 37.19 2.54 -5 2 4 128.79 5.34 -5 -2 4 129.51 5.43 -5 2 3 59.36 2.90 -5 -2 3 57.18 2.89 -5 -2 3 58.72 2.92 5 2 -2 22.50 1.42 -5 2 2 22.50 1.49 5 -2 -2 20.22 1.46 5 -2 -2 24.54 1.51 -5 -2 2 20.94 1.64 -5 -2 2 21.46 1.30 5 2 -1 191.40 7.24 5 2 -1 198.42 7.29 -5 2 1 189.66 7.06 5 -2 -1 201.98 7.29 -5 -2 1 212.69 7.42 -5 -2 1 191.34 7.26 5 2 0 64.03 2.75 5 2 0 57.92 2.93 -5 2 0 60.23 2.51 -5 -2 0 61.01 2.83 -5 -2 0 57.57 2.93 5 -2 0 60.29 2.46 5 -2 0 59.46 2.99 5 2 1 7.36 1.22 5 2 1 5.29 0.85 -5 2 -1 5.86 0.76 -5 -2 -1 6.08 0.94 5 -2 1 7.31 1.28 5 -2 1 6.86 0.75 5 2 2 217.66 8.44 5 2 2 212.96 8.05 5 -2 2 214.09 7.77 5 -2 2 218.90 8.48 5 2 3 99.13 4.68 5 -2 3 94.91 4.62 5 -2 3 92.08 3.94 5 2 4 1.17 1.25 5 -2 4 1.46 1.25 5 2 5 30.87 2.99 5 -2 5 29.61 3.16 5 2 6 47.91 3.77 5 -2 6 47.04 3.76 5 2 7 9.16 2.23 5 -2 7 8.32 2.22 -5 3 9 37.36 3.37 -5 -3 9 39.63 3.45 -5 3 8 11.90 2.01 -5 -3 8 8.89 1.92 -5 3 7 0.39 1.16 -5 -3 7 1.80 1.29 -5 3 6 29.49 2.50 -5 -3 6 32.16 2.56 -5 3 5 0.58 0.89 -5 -3 5 1.39 0.97 -5 -3 5 1.46 1.02 -5 3 4 4.83 1.04 -5 -3 4 5.40 1.12 -5 -3 4 5.75 1.16 5 3 -3 8.97 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1.14 -5 -4 6 2.54 1.24 -5 4 5 121.44 5.22 -5 -4 5 116.44 5.34 -5 -4 5 119.54 5.23 -5 4 4 57.68 2.92 -5 -4 4 57.38 2.96 -5 -4 4 51.01 2.97 -5 4 3 65.40 3.13 5 4 -3 61.29 2.65 -5 -4 3 72.57 3.28 -5 -4 3 69.40 3.19 -5 -4 3 65.58 2.58 5 4 -2 0.57 0.54 5 4 -2 -0.32 0.54 -5 4 2 -0.09 0.53 5 -4 -2 -0.60 0.35 5 -4 -2 -0.20 0.59 -5 -4 2 -0.08 0.65 -5 -4 2 -0.42 0.48 -5 4 1 141.47 5.01 5 4 -1 139.24 5.40 5 4 -1 131.20 5.29 5 -4 -1 138.99 5.37 -5 -4 1 136.65 5.51 -5 -4 1 135.57 5.27 5 -4 -1 138.04 5.30 -5 4 0 40.36 1.68 5 4 0 40.25 2.28 5 4 0 42.46 2.20 -5 -4 0 41.38 2.31 5 -4 0 37.21 2.28 -5 -4 0 38.99 2.17 5 4 1 4.20 1.12 5 4 1 4.14 0.89 5 -4 1 5.28 0.53 5 -4 1 4.21 1.08 -5 -4 -1 4.08 0.95 5 4 2 18.58 1.98 5 -4 2 17.62 1.10 -5 -4 -2 16.95 1.67 5 -4 2 19.97 2.08 5 4 3 35.41 2.61 5 -4 3 33.05 1.80 5 -4 3 36.86 2.75 5 4 4 3.11 1.41 5 -4 4 2.60 1.40 5 4 5 109.25 5.53 5 -4 5 99.40 5.41 5 4 6 45.80 3.69 5 -4 6 46.05 3.70 5 4 7 7.04 1.98 5 -4 7 3.87 1.82 -5 5 9 58.81 4.03 -5 -5 9 62.15 4.36 -5 -5 9 50.60 3.97 -5 5 8 19.63 2.41 -5 -5 8 18.92 2.71 -5 -5 8 14.94 2.31 -5 5 7 18.21 2.21 5 5 -7 19.76 1.79 -5 -5 7 15.52 2.32 -5 -5 7 18.06 2.33 -5 5 6 1.81 1.14 -5 -5 6 1.12 1.09 -5 -5 6 1.67 1.15 -5 5 5 184.26 7.36 -5 -5 5 193.50 7.42 -5 -5 5 175.38 7.52 -5 5 4 4.43 1.03 -5 -5 4 5.34 1.09 -5 -5 4 3.03 1.04 -5 5 3 178.79 6.62 -5 -5 3 169.84 6.11 -5 -5 3 165.03 6.75 5 5 -2 12.90 1.40 5 5 -2 11.20 1.02 -5 -5 2 12.09 1.03 -5 -5 2 10.71 1.33 5 -5 -2 11.69 1.15 5 5 -1 0.20 0.59 5 5 -1 0.50 0.68 -5 5 1 1.31 0.46 -5 -5 1 1.18 0.86 5 -5 -1 2.61 0.81 5 -5 -1 1.47 0.66 -5 -5 1 1.01 0.63 5 5 0 -0.52 0.66 5 5 0 -0.18 0.53 -5 -5 0 -0.51 0.74 5 -5 0 -0.13 0.72 -5 -5 0 -0.71 0.37 5 5 1 254.03 9.58 5 5 1 250.76 9.43 -5 -5 -1 256.50 9.47 5 -5 1 256.51 9.62 5 5 2 5.61 1.25 -5 -5 -2 4.51 1.10 5 -5 2 4.59 0.59 5 -5 2 2.63 1.18 5 5 3 121.91 5.64 5 -5 3 120.70 5.66 5 -5 3 126.72 4.74 5 5 4 5.18 1.65 5 5 4 2.14 0.96 5 -5 4 4.10 1.53 5 5 5 75.24 4.57 5 -5 5 81.40 4.72 5 5 6 2.24 1.54 5 -5 6 -0.13 1.44 5 5 7 63.81 4.57 5 -5 7 58.26 4.48 -5 6 9 0.66 1.24 -5 -6 9 -1.42 1.44 -5 -6 9 2.44 1.57 -5 6 8 4.61 1.57 -5 -6 8 5.40 1.90 -5 -6 8 7.38 1.78 5 6 -7 88.75 4.39 -5 6 7 103.85 5.08 -5 -6 7 107.24 5.42 -5 -6 7 111.09 5.18 5 6 -6 -2.22 0.77 -5 6 6 0.32 0.95 -5 -6 6 -0.63 1.05 -5 -6 6 1.76 1.13 -5 6 5 132.03 5.50 -5 -6 5 125.17 5.64 -5 -6 5 124.10 5.45 -5 6 4 44.60 2.45 -5 -6 4 37.43 1.72 5 -6 -4 38.63 1.92 -5 -6 4 38.29 2.53 -5 -6 4 37.89 2.39 -5 6 3 33.71 2.05 -5 -6 3 34.45 2.25 -5 -6 3 30.95 1.62 5 6 -2 4.08 0.72 -5 -6 2 3.68 1.01 5 -6 -2 3.03 0.56 -5 -6 2 4.91 0.78 5 6 -1 305.26 11.21 5 6 -1 313.38 11.40 -5 6 1 313.24 10.74 -5 -6 1 321.85 11.49 5 -6 -1 318.78 11.22 -5 -6 1 307.14 11.17 5 6 0 1.82 0.89 5 6 0 0.86 0.61 -5 -6 0 1.74 0.90 5 -6 0 0.19 0.76 5 6 1 47.79 2.72 5 -6 1 46.88 2.72 -5 -6 -1 42.87 2.62 5 6 2 5.91 1.33 5 -6 2 3.01 1.22 -5 -6 -2 5.29 1.18 5 6 3 154.16 6.77 5 -6 3 156.12 5.77 5 -6 3 162.88 6.90 5 6 4 0.66 1.28 5 6 4 1.54 0.98 5 -6 4 3.26 1.62 5 6 5 67.57 4.33 5 -6 5 68.31 4.41 5 6 6 0.23 1.53 5 -6 6 1.77 1.55 5 6 7 3.90 1.84 5 -6 7 -2.11 1.40 -5 7 9 38.96 3.36 -5 -7 9 39.47 3.79 -5 -7 9 49.01 3.74 -5 7 8 -0.06 1.17 -5 -7 8 1.34 1.51 -5 -7 8 3.45 1.49 5 7 -7 14.38 1.67 -5 7 7 17.71 2.17 -5 -7 7 15.24 2.18 -5 -7 7 16.42 2.38 5 7 -6 2.58 1.05 -5 7 6 4.55 1.26 -5 -7 6 3.45 1.35 5 -7 -6 2.80 1.04 -5 -7 6 3.45 1.26 -5 7 5 88.55 4.17 -5 -7 5 82.26 3.35 -5 -7 5 93.21 4.20 5 -7 -5 88.12 3.53 -5 -7 5 90.49 4.40 -5 7 4 2.75 0.93 5 -7 -4 2.24 0.91 -5 -7 4 1.54 0.56 -5 -7 4 2.60 0.94 -5 -7 4 3.40 1.08 -5 7 3 230.31 8.35 -5 -7 3 221.24 8.64 -5 -7 3 220.43 8.01 5 7 -2 20.27 1.36 5 -7 -2 20.11 1.33 -5 -7 2 20.49 1.39 -5 -7 2 19.81 1.91 5 7 -1 30.93 1.98 -5 7 1 33.81 1.45 -5 -7 1 32.28 2.00 5 -7 -1 31.84 1.92 -5 -7 1 31.79 2.27 5 7 0 16.31 1.65 -5 -7 0 15.48 1.71 5 7 1 182.23 7.47 5 -7 1 192.53 7.53 -5 -7 -1 196.40 7.55 5 7 2 1.65 1.02 -5 -7 -2 1.64 1.02 5 -7 2 1.98 1.17 5 7 3 23.96 2.47 5 7 3 24.08 1.99 5 -7 3 22.29 1.27 5 -7 3 23.19 2.48 5 7 4 29.58 2.90 5 7 4 35.80 2.34 5 -7 4 32.00 3.23 5 7 5 32.81 3.29 5 -7 5 27.88 3.19 5 7 6 4.07 1.84 5 -7 6 3.03 1.70 5 7 7 114.07 6.39 5 -7 7 117.61 6.50 -5 8 9 -1.00 1.13 -5 -8 9 -2.53 1.37 -5 -8 9 -1.85 1.46 -5 8 8 13.12 2.09 -5 -8 8 9.69 2.07 -5 -8 8 12.30 2.31 5 8 -7 68.22 3.59 -5 8 7 69.87 4.03 -5 -8 7 74.95 4.46 -5 -8 7 74.79 4.18 5 8 -6 4.90 1.19 -5 8 6 2.87 1.13 -5 -8 6 3.48 1.32 -5 -8 6 2.88 1.34 5 -8 -6 4.74 1.22 -5 8 5 3.71 1.16 5 8 -5 6.56 1.19 5 -8 -5 4.70 1.11 -5 -8 5 6.02 1.43 -5 -8 5 5.25 0.77 -5 -8 5 6.17 1.22 -5 8 4 41.88 2.43 5 -8 -4 41.59 2.28 -5 -8 4 43.41 2.51 -5 -8 4 39.89 2.75 -5 -8 4 39.90 2.00 -5 8 3 1.07 0.73 -5 -8 3 0.45 0.89 -5 -8 3 0.56 0.54 5 8 -2 7.89 1.08 5 -8 -2 10.35 0.95 -5 -8 2 8.27 1.04 -5 -8 2 10.02 1.41 -5 8 1 265.14 8.76 5 8 -1 252.25 9.36 -5 -8 1 258.45 9.66 -5 -8 1 243.65 9.29 5 -8 -1 252.20 9.23 5 8 0 39.92 2.37 -5 -8 0 38.37 2.48 5 8 1 2.67 1.00 -5 -8 -1 2.02 0.97 5 8 2 119.17 4.96 5 8 2 113.24 5.19 5 -8 2 111.25 5.20 -5 -8 -2 110.52 5.12 5 8 3 94.35 4.32 5 8 3 95.74 4.81 5 -8 3 96.63 4.89 5 8 4 3.19 1.08 5 8 4 3.40 1.50 5 -8 4 3.01 1.61 5 8 5 33.99 3.25 5 -8 5 32.09 3.41 5 8 6 36.53 3.76 5 -8 6 43.62 3.84 5 8 7 3.87 1.96 5 -8 7 4.52 2.02 -5 9 9 2.74 1.33 -5 -9 9 4.89 1.89 -5 -9 9 2.26 1.62 -5 9 8 15.03 2.21 -5 -9 8 20.10 2.66 -5 -9 8 13.69 2.48 5 9 -7 1.10 1.09 -5 9 7 0.04 1.09 -5 -9 7 3.56 1.40 -5 -9 7 0.98 1.40 -5 9 6 75.24 4.09 -5 -9 6 84.38 4.54 -5 -9 6 84.60 4.20 -5 9 5 43.70 2.70 5 9 -5 46.61 2.70 -5 -9 5 39.52 2.90 -5 -9 5 42.20 2.07 -5 -9 5 45.01 2.71 5 -9 -5 42.97 2.49 5 9 -4 3.90 1.16 -5 9 4 1.91 0.91 5 -9 -4 2.52 1.05 -5 -9 4 2.18 0.69 -5 -9 4 3.40 1.16 -5 -9 4 5.07 1.06 -5 9 3 4.36 0.93 5 9 -3 3.28 1.05 -5 -9 3 5.84 0.90 -5 -9 3 4.24 1.18 5 9 -2 102.63 4.32 -5 -9 2 104.44 4.82 -5 -9 2 111.72 4.40 5 -9 -2 105.00 4.24 5 9 -1 49.35 2.63 -5 9 1 48.92 2.05 5 -9 -1 52.38 2.52 -5 -9 1 54.74 3.00 5 9 0 116.93 5.09 -5 -9 0 124.18 5.29 5 9 1 71.85 3.65 5 9 1 71.22 3.55 -5 -9 -1 69.25 3.70 5 9 2 8.63 1.48 5 9 2 12.57 1.55 -5 -9 -2 8.49 1.53 5 -9 2 7.78 1.49 5 9 3 0.07 1.13 5 9 3 -0.13 0.90 5 -9 3 1.25 1.32 5 9 4 101.52 5.46 5 9 4 114.96 4.92 5 -9 4 111.34 5.69 5 9 5 19.54 2.70 5 -9 5 16.44 2.67 5 9 6 13.36 2.65 5 -9 6 16.18 2.78 -5 10 9 -0.99 1.07 -5 -10 9 0.18 1.68 -5 -10 9 0.40 1.56 -5 10 8 65.97 4.12 -5 -10 8 72.63 4.37 -5 -10 8 69.36 4.65 -5 10 7 38.11 2.96 5 10 -7 39.63 2.72 -5 -10 7 39.92 3.44 -5 -10 7 42.90 3.09 5 10 -6 3.58 1.26 -5 10 6 1.56 1.07 -5 -10 6 4.48 1.25 -5 -10 6 2.24 1.37 -5 10 5 1.60 0.91 5 10 -5 1.69 1.05 -5 -10 5 2.19 0.99 5 -10 -5 1.08 1.24 -5 -10 5 1.40 1.19 -5 -10 5 -0.34 0.49 5 10 -4 203.69 8.24 -5 10 4 217.37 8.14 -5 -10 4 211.33 7.86 5 -10 -4 220.16 7.99 -5 -10 4 220.96 8.67 -5 -10 4 208.22 8.15 -5 10 3 52.70 2.62 5 10 -3 49.92 2.86 -5 -10 3 49.34 3.09 -5 -10 3 49.76 2.53 5 10 -2 91.94 4.29 5 10 -2 90.94 4.02 -5 -10 2 93.09 3.99 5 -10 -2 96.70 3.86 -5 -10 2 97.05 4.55 5 10 -1 27.21 2.11 5 10 -1 28.74 1.98 -5 10 1 26.08 1.34 -5 -10 1 28.60 2.33 5 -10 -1 27.87 1.74 5 10 0 115.31 5.05 5 10 0 115.52 5.08 -5 -10 0 121.79 5.28 5 10 1 20.25 1.94 5 10 1 20.25 1.95 -5 -10 -1 17.66 1.95 5 10 2 114.71 5.01 5 10 2 110.91 5.27 -5 -10 -2 114.38 5.32 5 -10 2 115.93 5.36 5 10 3 29.99 2.69 5 10 3 26.21 2.27 5 -10 3 25.49 2.70 -5 -10 -3 29.83 2.64 5 10 4 3.61 1.58 5 10 4 2.83 1.12 5 -10 4 1.01 1.45 5 10 5 31.53 3.39 5 -10 5 26.02 3.25 5 10 6 54.02 4.19 5 -10 6 48.69 4.19 -5 11 9 2.62 1.45 -5 -11 9 0.57 1.57 -5 -11 9 4.31 1.90 -5 11 8 25.02 2.68 -5 -11 8 27.34 3.24 -5 -11 8 25.75 2.89 5 11 -7 0.79 1.09 -5 11 7 1.09 1.13 -5 -11 7 1.27 1.42 -5 -11 7 0.07 1.17 -5 11 6 50.51 3.05 5 11 -6 46.15 2.93 -5 -11 6 46.85 2.95 -5 -11 6 39.88 3.37 -5 11 5 -1.20 0.67 5 11 -5 0.50 0.98 -5 -11 5 0.61 0.82 5 -11 -5 -0.39 1.34 -5 -11 5 -1.24 0.54 -5 -11 5 0.28 1.18 5 11 -4 22.92 2.16 -5 11 4 29.17 1.96 -5 -11 4 25.19 2.38 -5 -11 4 25.24 1.92 -5 -11 4 23.26 1.75 5 -11 -4 28.39 2.38 5 11 -3 -0.55 0.85 -5 11 3 0.88 0.75 -5 -11 3 0.38 0.97 -5 -11 3 1.21 0.80 5 11 -2 77.03 3.53 5 11 -2 76.10 3.78 -5 11 2 74.70 3.23 -5 -11 2 83.08 4.12 5 -11 -2 78.91 3.31 5 11 -1 10.45 1.40 -5 11 1 9.67 0.87 5 11 -1 10.10 1.51 -5 -11 1 10.52 1.61 5 -11 -1 9.64 1.11 5 11 0 55.87 3.12 5 11 0 58.80 3.12 -5 -11 0 56.33 3.25 5 11 1 2.60 1.05 5 11 1 3.16 1.11 -5 -11 -1 0.78 1.10 5 11 2 44.65 2.91 5 11 2 46.92 3.12 -5 -11 -2 49.94 3.22 5 11 3 19.44 2.37 5 11 3 15.39 1.78 5 -11 3 16.01 2.25 -5 -11 -3 17.28 2.24 5 11 4 51.32 3.73 5 11 4 50.33 3.01 5 -11 4 48.30 3.77 5 11 5 0.25 1.41 5 -11 5 -1.20 1.48 5 11 6 2.23 1.61 5 -11 6 0.18 1.76 -5 12 9 2.96 1.43 -5 -12 9 2.38 1.67 -5 -12 9 3.40 1.82 -5 12 8 27.15 2.84 -5 -12 8 19.78 2.91 -5 -12 8 29.01 3.02 5 12 -7 -0.95 0.94 -5 12 7 1.41 1.21 -5 -12 7 0.71 1.17 -5 -12 7 0.78 1.39 5 12 -6 2.50 1.19 -5 12 6 3.46 1.21 -5 -12 6 1.58 1.12 -5 -12 6 2.36 1.53 5 12 -5 3.99 1.27 -5 12 5 3.28 1.09 5 -12 -5 4.30 1.51 -5 -12 5 3.85 1.49 -5 -12 5 5.35 1.18 -5 12 4 204.06 7.63 -5 -12 4 196.84 8.23 5 -12 -4 202.33 7.70 -5 -12 4 189.31 7.43 5 12 -3 0.06 0.88 -5 12 3 1.74 0.79 -5 12 3 3.15 0.80 -5 -12 3 1.75 1.10 5 12 -2 18.27 1.99 5 12 -2 19.58 1.67 -5 12 2 21.27 1.41 5 -12 -2 19.87 1.39 -5 -12 2 20.62 2.22 -5 12 1 2.93 0.59 5 12 -1 2.92 1.10 5 12 -1 3.62 0.99 5 -12 -1 2.41 0.72 -5 -12 1 2.06 1.19 5 12 0 50.51 2.99 5 12 0 53.89 2.99 -5 -12 0 53.33 3.22 5 -12 0 48.35 2.51 5 12 1 8.60 1.49 5 12 1 10.35 1.61 -5 -12 -1 9.44 1.67 5 12 2 119.40 5.52 5 12 2 118.32 5.23 -5 -12 -2 111.31 5.44 5 12 3 4.26 1.60 5 12 3 5.92 1.35 5 -12 3 7.46 1.77 -5 -12 -3 5.71 1.62 5 12 4 8.89 2.00 5 12 4 8.42 1.50 5 -12 4 11.66 2.19 5 12 5 0.91 1.58 5 -12 5 1.40 1.77 5 12 6 79.85 5.14 5 -12 6 80.09 5.30 -5 13 8 13.82 2.13 -5 -13 8 8.87 2.25 -5 -13 8 15.29 2.32 -5 13 7 8.67 1.70 5 13 -7 7.55 1.53 -5 -13 7 4.09 1.72 -5 -13 7 8.68 1.69 5 13 -6 78.02 4.01 -5 13 6 75.24 3.99 -5 -13 6 74.68 4.62 -5 -13 6 75.13 3.95 5 13 -5 6.03 1.42 -5 13 5 3.55 1.03 -5 -13 5 3.56 1.56 -5 -13 5 4.72 1.20 -5 13 4 2.08 0.86 5 13 -4 1.28 1.14 -5 -13 4 2.64 1.31 -5 13 3 3.64 1.07 5 13 -3 2.15 1.07 -5 13 3 3.37 0.87 -5 -13 3 0.05 1.00 -5 13 2 105.95 4.38 -5 -13 2 111.24 5.26 5 -13 -2 112.92 4.42 5 13 -1 0.91 0.89 -5 13 1 1.83 0.55 5 13 -1 1.70 1.12 5 -13 -1 1.64 0.66 -5 -13 1 -0.11 1.12 5 13 0 87.24 4.24 5 -13 0 87.60 3.67 -5 -13 0 87.17 4.41 5 13 1 27.27 2.36 5 13 1 32.50 2.45 -5 -13 -1 31.31 2.55 5 13 2 19.38 2.05 5 13 2 15.72 2.09 -5 -13 -2 17.77 2.26 5 13 3 2.38 1.12 5 13 3 3.52 1.53 5 -13 3 3.22 1.62 -5 -13 -3 4.27 1.59 5 13 4 159.89 6.63 5 13 4 162.04 7.35 5 -13 4 145.84 7.30 5 13 5 7.87 2.10 5 -13 5 8.90 2.31 5 13 6 1.76 1.54 5 -13 6 4.41 1.93 -5 14 8 19.56 2.45 -5 -14 8 14.34 2.66 -5 -14 8 18.47 2.47 5 14 -7 8.02 1.62 -5 14 7 10.17 1.68 -5 -14 7 9.90 2.27 -5 -14 7 10.01 1.81 -5 14 6 25.04 2.39 5 14 -6 26.07 2.50 -5 -14 6 25.31 2.29 -5 -14 6 24.06 2.97 5 14 -5 1.00 1.09 -5 14 5 3.45 1.05 -5 -14 5 2.12 0.93 -5 -14 5 3.04 1.48 5 14 -4 58.77 3.47 -5 14 4 64.44 3.12 -5 -14 4 57.64 3.87 -5 14 3 0.93 0.75 5 14 -3 2.58 1.20 -5 -14 3 2.05 1.28 -5 14 2 1.11 0.69 5 14 -2 0.93 1.06 5 -14 -2 1.19 0.64 -5 -14 2 1.52 1.16 5 14 -1 29.61 2.49 5 14 -1 35.45 2.41 -5 14 1 37.13 1.72 -5 -14 1 32.05 2.63 5 -14 -1 30.91 1.82 5 14 0 34.87 2.51 5 14 0 35.71 2.61 5 -14 0 32.38 1.90 -5 -14 0 36.87 2.82 5 14 1 0.43 1.04 5 14 1 0.25 1.02 -5 -14 -1 1.39 1.24 5 14 2 100.78 4.81 5 14 2 100.80 5.05 -5 -14 -2 100.59 5.20 5 14 3 8.70 1.60 5 14 3 7.12 1.81 -5 -14 -3 9.56 1.95 5 14 4 0.49 1.46 5 14 4 1.88 1.15 5 -14 4 2.09 1.68 5 14 5 11.09 2.32 5 14 5 12.70 2.43 5 -14 5 7.12 2.13 5 14 6 28.79 3.48 5 -14 6 29.12 3.73 -5 15 8 5.23 1.55 -5 -15 8 11.32 2.41 -5 -15 8 5.86 1.78 5 15 -7 30.76 2.61 -5 15 7 29.15 2.65 -5 -15 7 32.07 2.76 -5 -15 7 30.96 3.48 5 15 -6 19.32 2.25 -5 15 6 16.74 2.00 -5 -15 6 14.05 2.38 -5 -15 6 16.68 2.01 5 15 -5 18.22 2.19 -5 15 5 23.83 1.99 -5 -15 5 19.82 1.84 -5 -15 5 21.60 2.71 5 15 -4 0.52 1.17 -5 15 4 3.66 0.95 -5 -15 4 -0.30 1.23 5 15 -3 138.36 6.12 -5 -15 3 137.81 6.43 5 15 -2 93.35 4.46 -5 15 2 89.31 3.81 5 -15 -2 82.42 3.69 -5 -15 2 90.30 4.68 -5 15 1 4.29 0.70 5 15 -1 5.61 1.45 5 15 -1 4.03 1.20 5 -15 -1 4.55 0.76 -5 -15 1 7.49 1.57 5 15 0 3.61 1.15 5 15 0 4.64 1.32 -5 -15 0 4.21 1.43 5 -15 0 2.04 0.69 5 15 1 62.98 3.70 5 15 1 59.67 3.60 -5 -15 -1 65.68 3.93 5 15 2 27.59 2.68 5 15 2 28.97 2.56 -5 -15 -2 31.16 2.98 5 15 3 9.83 1.90 5 15 3 12.74 1.78 -5 -15 -3 9.63 2.06 5 15 4 8.52 1.65 5 15 4 5.74 1.85 5 -15 4 11.16 2.37 5 15 5 4.46 1.89 5 15 5 1.66 1.71 5 -15 5 5.35 2.10 5 15 6 5.59 1.94 5 -15 6 0.31 1.70 -5 16 8 7.10 1.72 -5 -16 8 6.60 1.76 -5 -16 8 5.26 2.12 -5 16 7 90.72 4.67 5 16 -7 84.58 4.64 -5 -16 7 95.59 4.69 -5 -16 7 88.48 5.53 -5 16 6 5.43 1.36 5 16 -6 8.37 1.77 -5 -16 6 5.91 1.94 -5 -16 6 6.30 1.39 -5 16 5 83.96 3.93 5 16 -5 77.41 4.27 -5 -16 5 77.07 4.73 5 16 -4 14.61 2.02 -5 16 4 18.08 1.62 -5 -16 4 16.42 2.40 5 16 -3 46.96 3.06 -5 -16 3 44.02 3.37 -5 16 2 5.17 1.01 5 16 -2 7.94 1.54 -5 -16 2 5.71 1.64 5 -16 -2 5.69 0.93 5 16 -1 157.25 6.69 -5 16 1 158.83 5.90 5 16 -1 162.30 6.81 5 -16 -1 152.18 5.89 -5 -16 1 163.97 7.08 5 16 0 33.34 2.53 5 16 0 32.51 2.60 -5 -16 0 30.93 2.81 5 -16 0 29.26 1.77 5 16 1 14.91 2.03 5 16 1 13.64 1.87 -5 -16 -1 10.19 1.90 5 16 2 3.29 1.27 5 16 2 4.34 1.53 -5 -16 -2 3.76 1.61 5 16 3 125.73 5.83 5 16 3 129.11 6.28 -5 -16 -3 125.61 6.43 5 16 4 0.20 1.48 5 16 4 0.62 1.15 5 -16 4 1.11 1.72 5 16 5 46.47 3.91 5 16 5 42.29 3.40 5 -16 5 44.56 4.55 -5 17 8 6.36 1.72 -5 -17 8 5.89 1.71 -5 -17 8 5.97 2.22 -5 17 7 12.99 1.80 5 17 -7 15.50 2.27 -5 -17 7 11.64 1.97 -5 -17 7 13.53 2.62 -5 17 6 2.41 1.09 5 17 -6 0.35 1.28 -5 -17 6 -0.99 0.83 -5 -17 6 0.06 1.41 -5 17 5 70.48 3.58 5 17 -5 74.49 4.19 -5 -17 5 72.96 4.70 -5 17 4 8.38 1.19 5 17 -4 9.02 1.72 -5 -17 4 8.37 2.00 5 17 -3 111.23 5.48 -5 -17 3 122.87 6.00 -5 17 2 13.85 1.42 5 17 -2 10.85 1.81 -5 -17 2 11.68 2.05 5 17 -1 0.72 1.02 5 17 -1 -0.31 1.01 -5 17 1 0.37 0.51 -5 -17 1 0.07 1.24 5 17 0 0.92 1.02 5 17 0 2.11 1.22 -5 -17 0 1.36 1.28 5 17 1 106.03 5.25 5 17 1 108.61 5.38 -5 -17 -1 111.30 5.60 5 17 2 7.35 1.60 5 17 2 9.56 1.88 -5 -17 -2 8.31 1.96 5 17 3 41.23 3.48 5 17 3 38.96 3.04 -5 -17 -3 39.57 3.51 5 17 4 -1.12 1.49 5 17 4 1.14 1.22 5 -17 4 -1.33 1.62 5 17 5 10.77 2.09 5 17 5 13.87 2.50 5 -17 5 10.77 2.45 5 18 -7 58.32 3.83 -5 18 7 60.78 3.66 -5 -18 7 56.50 4.62 -5 -18 7 59.51 3.65 -5 18 6 10.28 1.65 5 18 -6 7.38 1.84 -5 -18 6 10.25 2.21 5 18 -5 30.49 2.94 -5 18 5 30.05 2.14 -5 -18 5 21.90 2.95 -5 18 4 5.62 1.07 5 18 -4 5.86 1.61 -5 -18 4 7.28 1.96 5 18 -3 12.19 1.88 -5 -18 3 7.64 1.94 5 18 -2 0.34 1.06 -5 18 2 0.27 0.61 -5 -18 2 -0.50 1.37 5 18 -1 72.53 4.14 -5 -18 1 77.24 4.44 5 18 0 12.02 1.85 5 18 0 10.00 1.77 -5 -18 0 17.33 2.44 5 18 1 3.98 1.43 5 18 1 5.72 1.56 -5 -18 -1 6.46 1.74 5 18 2 4.69 1.40 5 18 2 0.93 1.38 -5 -18 -2 1.87 1.69 5 18 3 55.58 4.01 5 18 3 53.44 3.61 -5 -18 -3 58.40 4.20 5 18 4 7.71 1.72 5 18 4 10.58 2.34 5 18 5 36.29 3.31 5 18 5 39.28 3.69 5 -18 5 37.19 4.02 5 19 -7 -0.87 1.27 -5 19 7 0.47 1.11 -5 -19 7 0.70 1.73 5 19 -6 34.73 3.06 -5 19 6 34.29 2.57 -5 -19 6 32.31 3.64 5 19 -5 23.53 2.70 -5 19 5 20.18 1.82 -5 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6.21 -6 -11 2 160.43 6.75 6 11 -1 1.15 1.12 6 11 -1 2.49 0.92 -6 -11 1 1.94 1.20 6 11 0 118.94 5.30 6 11 0 118.82 5.38 -6 -11 0 116.28 5.49 6 11 1 4.89 1.36 6 11 1 3.12 1.22 -6 -11 -1 5.01 1.43 6 11 2 1.05 1.25 6 11 2 2.15 1.15 -6 -11 -2 4.65 1.53 6 -11 2 1.99 1.45 6 11 3 -0.19 1.10 6 11 3 0.18 1.35 -6 -11 -3 0.37 1.31 6 -11 3 -0.94 1.36 6 11 4 132.79 6.75 6 11 4 141.11 6.15 6 -11 4 136.41 6.96 6 11 5 0.85 1.75 6 -11 5 2.20 1.92 6 11 6 30.47 3.66 6 -11 6 38.31 4.05 -6 12 8 32.29 2.98 -6 -12 8 27.99 3.42 -6 -12 8 32.54 3.27 6 12 -7 1.66 1.35 -6 12 7 0.13 1.15 -6 -12 7 2.53 1.47 -6 -12 7 2.25 1.74 6 12 -6 4.59 1.43 -6 12 6 3.96 1.37 -6 -12 6 8.57 1.64 -6 -12 6 1.50 1.55 -6 12 5 5.75 1.34 6 12 -5 4.10 1.42 -6 -12 5 4.48 1.60 6 12 -4 45.17 2.89 -6 12 4 42.87 2.62 -6 -12 4 45.47 3.19 -6 -12 4 45.26 2.41 6 12 -3 3.48 1.22 -6 -12 3 1.74 1.15 6 12 -2 40.19 2.78 -6 12 2 42.48 2.10 6 12 -2 43.02 2.53 -6 -12 2 42.25 3.05 6 12 -1 -0.16 1.03 6 12 -1 3.42 1.07 -6 -12 1 3.19 1.31 6 12 0 22.71 2.19 6 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