data_test _audit_creation_date 2015-06-15 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3151 for OlexSys, GUI svn.r4998) ; _shelxl_version_number 2014-3 _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ; ? ; _chemical_formula_moiety '2(C26 H59 B2 Ir O4 P2)' _chemical_formula_sum 'C52 H118 B4 Ir2 O8 P4' _chemical_formula_weight 1422.98 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'B' 'B' 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ir' 'Ir' -1.4442 7.9887 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.6009(5) _cell_length_b 14.7110(7) _cell_length_c 20.1115(11) _cell_angle_alpha 100.827(3) _cell_angle_beta 92.604(3) _cell_angle_gamma 96.944(3) _cell_volume 3338.2(3) _cell_formula_units_Z 2 _cell_measurement_reflns_used 9691 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 27.117 _cell_measurement_theta_min 2.413 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 4.122 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.5592 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2007/4 (Bruker,2007) was used for absorption correction. wR2(int) was 0.0810 before and 0.0341 after correction. The Ratio of minimum to maximum transmission is 0.7501. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.416 _exptl_crystal_density_meas . _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 1456 _exptl_crystal_size_max 0.604 _exptl_crystal_size_mid 0.252 _exptl_crystal_size_min 0.17 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0238 _diffrn_reflns_av_unetI/netI 0.0236 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 53994 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 27.134 _diffrn_reflns_theta_min 1.586 _diffrn_ambient_temperature 172.99 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'graphite' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 12862 _reflns_number_total 14567 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v7.46A (Bruker, 2008)' _computing_data_collection ? _computing_data_reduction 'SAINT v7.46A (Bruker, 2008)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _refine_diff_density_max 0.931 _refine_diff_density_min -0.468 _refine_diff_density_rms 0.069 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.014 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 687 _refine_ls_number_reflns 14567 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0245 _refine_ls_R_factor_gt 0.0191 _refine_ls_restrained_S_all 1.014 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0198P)^2^+1.5152P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0421 _refine_ls_wR_factor_ref 0.0440 _refine_special_details ; ? ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C4(H0AA), C7(H7), C10(H10), C13(H13), C31(H31), C34(H34), C37(H37), C40(H40) 2.b Secondary CH2 refined with riding coordinates: C1(H1A,H1B), C2(H2A,H2B), C28(H28A,H28B), C29(H29A,H29B) 2.c Idealised Me refined as rotating group: C3(H3A,H3B,H3C), C5(H5A,H5B,H5C), C6(H6A,H6B,H6C), C8(H8A,H8B,H8C), C9(H9A, H9B,H9C), C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C14(H14A,H14B,H14C), C15(H15A,H15B,H15C), C17(H17A,H17B,H17C), C18(H18A,H18B,H18C), C20(H20A,H20B, H20C), C21(H21A,H21B,H21C), C23(H23A,H23B,H23C), C24(H24A,H24B,H24C), C26(H26A, H26B,H26C), C30(H30A,H30B,H30C), C32(H32A,H32B,H32C), C33(H33A,H33B,H33C), C35(H35A,H35B,H35C), C36(H36A,H36B,H36C), C38(H38A,H38B,H38C), C39(H39A,H39B, H39C), C41(H41A,H41B,H41C), C42(H42A,H42B,H42C), C44(H44A,H44B,H44C), C45(H45A, H45B,H45C), C47(H47A,H47B,H47C), C48(H48A,H48B,H48C), C50(H50A,H50B,H50C), C51(H51A,H51B,H51C), C53(H53A,H53B,H53C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.95754(2) 0.62462(2) 0.25247(2) 0.02113(3) Uani 1 1 d . . . . . H1 H 1.006(2) 0.5369(19) 0.2676(14) 0.051(8) Uiso 1 1 d . . . . . H2 H 0.995(3) 0.594(2) 0.1754(15) 0.062(9) Uiso 1 1 d . . . . . H3 H 0.932(3) 0.649(2) 0.3315(16) 0.074(10) Uiso 1 1 d . . . . . P1 P 0.91139(5) 0.76939(4) 0.23140(4) 0.02798(14) Uani 1 1 d . . . . . P2 P 1.14587(5) 0.70327(4) 0.28060(3) 0.02294(12) Uani 1 1 d . . . . . O1 O 0.76510(14) 0.58279(11) 0.13650(9) 0.0330(4) Uani 1 1 d . . . . . O2 O 0.82190(14) 0.44768(11) 0.15617(8) 0.0312(4) Uani 1 1 d . . . . . O3 O 0.70492(12) 0.58712(11) 0.30137(8) 0.0268(4) Uani 1 1 d . . . . . O4 O 0.82497(12) 0.48829(11) 0.33219(8) 0.0260(3) Uani 1 1 d . . . . . C1 C 1.03801(19) 0.85819(16) 0.26427(14) 0.0313(5) Uani 1 1 d . . . . . H1A H 1.0390 0.9094 0.2385 0.038 Uiso 1 1 calc R . . . . H1B H 1.0284 0.8849 0.3124 0.038 Uiso 1 1 calc R . . . . C2 C 1.15507(19) 0.82011(15) 0.25946(13) 0.0289(5) Uani 1 1 d . . . . . H2A H 1.2143 0.8633 0.2909 0.035 Uiso 1 1 calc R . . . . H2B H 1.1803 0.8170 0.2128 0.035 Uiso 1 1 calc R . . . . C3 C 0.7998(2) 0.82717(19) 0.35017(16) 0.0487(8) Uani 1 1 d . . . . . H3A H 0.7374 0.8594 0.3710 0.073 Uiso 1 1 calc GR . . . . H3B H 0.8754 0.8599 0.3706 0.073 Uiso 1 1 calc GR . . . . H3C H 0.7910 0.7629 0.3578 0.073 Uiso 1 1 calc GR . . . . C4 C 0.7928(2) 0.82608(17) 0.27399(16) 0.0404(7) Uani 1 1 d . . . . . H0AA H 0.8024 0.8924 0.2679 0.049 Uiso 1 1 calc R . . . . C5 C 0.6733(2) 0.78024(19) 0.24132(19) 0.0551(9) Uani 1 1 d . . . . . H5A H 0.6631 0.7139 0.2440 0.083 Uiso 1 1 calc GR . . . . H5B H 0.6675 0.7864 0.1936 0.083 Uiso 1 1 calc GR . . . . H5C H 0.6126 0.8110 0.2654 0.083 Uiso 1 1 calc GR . . . . C6 C 0.8621(3) 0.8824(2) 0.13456(18) 0.0613(9) Uani 1 1 d . . . . . H6A H 0.7942 0.8984 0.1593 0.092 Uiso 1 1 calc GR . . . . H6B H 0.8468 0.8836 0.0864 0.092 Uiso 1 1 calc GR . . . . H6C H 0.9301 0.9279 0.1532 0.092 Uiso 1 1 calc GR . . . . C7 C 0.8862(2) 0.78384(18) 0.14215(15) 0.0406(7) Uani 1 1 d . . . . . H7 H 0.8149 0.7400 0.1226 0.049 Uiso 1 1 calc R . . . . C8 C 0.9843(3) 0.7556(2) 0.09898(15) 0.0565(8) Uani 1 1 d . . . . . H8A H 0.9634 0.7576 0.0516 0.085 Uiso 1 1 calc GR . . . . H8B H 0.9975 0.6920 0.1025 0.085 Uiso 1 1 calc GR . . . . H8C H 1.0554 0.7988 0.1150 0.085 Uiso 1 1 calc GR . . . . C9 C 1.1284(3) 0.78807(19) 0.41623(14) 0.0439(7) Uani 1 1 d . . . . . H9A H 1.0481 0.7572 0.4134 0.066 Uiso 1 1 calc GR . . . . H9B H 1.1291 0.8479 0.4014 0.066 Uiso 1 1 calc GR . . . . H9C H 1.1614 0.7990 0.4632 0.066 Uiso 1 1 calc GR . . . . C10 C 1.2006(2) 0.72627(18) 0.37067(13) 0.0344(6) Uani 1 1 d . . . . . H10 H 1.2816 0.7598 0.3741 0.041 Uiso 1 1 calc R . . . . C11 C 1.2066(3) 0.6350(2) 0.39552(16) 0.0499(8) Uani 1 1 d . . . . . H11A H 1.2402 0.6487 0.4425 0.075 Uiso 1 1 calc GR . . . . H11B H 1.2555 0.5967 0.3667 0.075 Uiso 1 1 calc GR . . . . H11C H 1.1281 0.6011 0.3934 0.075 Uiso 1 1 calc GR . . . . C12 C 1.2456(2) 0.6317(2) 0.15999(14) 0.0435(7) Uani 1 1 d . . . . . H12A H 1.2448 0.6909 0.1444 0.065 Uiso 1 1 calc GR . . . . H12B H 1.1706 0.5926 0.1466 0.065 Uiso 1 1 calc GR . . . . H12C H 1.3080 0.5992 0.1395 0.065 Uiso 1 1 calc GR . . . . C13 C 1.26632(19) 0.65112(17) 0.23711(14) 0.0316(6) Uani 1 1 d . . . . . H13 H 1.2701 0.5896 0.2509 0.038 Uiso 1 1 calc R . . . . C14 C 1.3858(2) 0.7095(2) 0.25719(16) 0.0453(7) Uani 1 1 d . . . . . H14A H 1.4454 0.6782 0.2324 0.068 Uiso 1 1 calc GR . . . . H14B H 1.4038 0.7163 0.3061 0.068 Uiso 1 1 calc GR . . . . H14C H 1.3846 0.7713 0.2459 0.068 Uiso 1 1 calc GR . . . . C15 C 0.6710(2) 0.5382(2) 0.02402(15) 0.0486(7) Uani 1 1 d . . . . . H15A H 0.6288 0.5927 0.0300 0.073 Uiso 1 1 calc GR . . . . H15B H 0.6256 0.4866 -0.0082 0.073 Uiso 1 1 calc GR . . . . H15C H 0.7467 0.5542 0.0065 0.073 Uiso 1 1 calc GR . . . . C16 C 0.6893(2) 0.50913(17) 0.09172(13) 0.0310(5) Uani 1 1 d . . . . . C17 C 0.5741(2) 0.4985(2) 0.12445(14) 0.0438(7) Uani 1 1 d . . . . . H17A H 0.5864 0.4792 0.1680 0.066 Uiso 1 1 calc GR . . . . H17B H 0.5187 0.4511 0.0945 0.066 Uiso 1 1 calc GR . . . . H17C H 0.5429 0.5583 0.1320 0.066 Uiso 1 1 calc GR . . . . C18 C 0.8481(3) 0.4195(3) 0.03720(16) 0.0665(10) Uani 1 1 d . . . . . H18A H 0.8968 0.4800 0.0425 0.100 Uiso 1 1 calc GR . . . . H18B H 0.8084 0.4034 -0.0083 0.100 Uiso 1 1 calc GR . . . . H18C H 0.8970 0.3715 0.0433 0.100 Uiso 1 1 calc GR . . . . C19 C 0.7580(2) 0.42512(18) 0.09008(13) 0.0374(6) Uani 1 1 d . . . . . C20 C 0.6831(3) 0.3310(2) 0.08299(18) 0.0624(10) Uani 1 1 d . . . . . H20A H 0.7331 0.2828 0.0867 0.094 Uiso 1 1 calc GR . . . . H20B H 0.6392 0.3157 0.0387 0.094 Uiso 1 1 calc GR . . . . H20C H 0.6288 0.3340 0.1190 0.094 Uiso 1 1 calc GR . . . . C21 C 0.5150(2) 0.5171(2) 0.32546(16) 0.0427(7) Uani 1 1 d . . . . . H21A H 0.4808 0.5754 0.3288 0.064 Uiso 1 1 calc GR . . . . H21B H 0.4749 0.4782 0.3541 0.064 Uiso 1 1 calc GR . . . . H21C H 0.5067 0.4836 0.2782 0.064 Uiso 1 1 calc GR . . . . C22 C 0.64364(19) 0.53926(16) 0.34917(13) 0.0288(5) Uani 1 1 d . . . . . C23 C 0.6598(3) 0.60523(19) 0.41755(14) 0.0440(7) Uani 1 1 d . . . . . H23A H 0.7425 0.6165 0.4332 0.066 Uiso 1 1 calc GR . . . . H23B H 0.6148 0.5773 0.4504 0.066 Uiso 1 1 calc GR . . . . H23C H 0.6327 0.6645 0.4132 0.066 Uiso 1 1 calc GR . . . . C24 C 0.6622(2) 0.37338(17) 0.28771(13) 0.0330(6) Uani 1 1 d . . . . . H24A H 0.6615 0.3971 0.2453 0.050 Uiso 1 1 calc GR . . . . H24B H 0.5829 0.3480 0.2953 0.050 Uiso 1 1 calc GR . . . . H24C H 0.7125 0.3241 0.2847 0.050 Uiso 1 1 calc GR . . . . C25 C 0.70800(18) 0.45235(15) 0.34636(12) 0.0249(5) Uani 1 1 d . . . . . C26 C 0.7144(2) 0.41644(18) 0.41243(13) 0.0340(6) Uani 1 1 d . . . . . H26A H 0.7512 0.3592 0.4055 0.051 Uiso 1 1 calc GR . . . . H26B H 0.6356 0.4031 0.4269 0.051 Uiso 1 1 calc GR . . . . H26C H 0.7604 0.4639 0.4475 0.051 Uiso 1 1 calc GR . . . . B1 B 0.8370(2) 0.54390(18) 0.17685(14) 0.0255(5) Uani 1 1 d . . . . . B2 B 0.8172(2) 0.56287(18) 0.29910(14) 0.0241(5) Uani 1 1 d . . . . . Ir2 Ir 0.15723(2) 0.14349(2) 0.26497(2) 0.01980(3) Uani 1 1 d . . . . . H4 H 0.282(2) 0.2102(19) 0.2903(15) 0.057(9) Uiso 1 1 d . . . . . H5 H 0.046(2) 0.077(2) 0.2301(15) 0.060(9) Uiso 1 1 d . . . . . H6 H 0.176(3) 0.063(2) 0.3041(15) 0.062(9) Uiso 1 1 d . . . . . P3 P 0.05016(5) 0.22423(4) 0.34881(3) 0.02354(12) Uani 1 1 d . . . . . P4 P 0.09324(5) 0.24023(4) 0.19678(3) 0.02476(12) Uani 1 1 d . . . . . O5 O 0.30999(14) 0.15937(11) 0.40057(8) 0.0302(4) Uani 1 1 d . . . . . O6 O 0.38834(13) 0.07549(12) 0.31004(8) 0.0308(4) Uani 1 1 d . . . . . O7 O 0.33160(15) 0.12804(12) 0.15524(10) 0.0400(5) Uani 1 1 d . . . . . O8 O 0.24816(15) -0.01643(11) 0.16176(9) 0.0375(4) Uani 1 1 d . . . . . C28 C -0.0436(2) 0.29089(17) 0.30564(13) 0.0305(5) Uani 1 1 d . . . . . H28A H -0.1169 0.2503 0.2874 0.037 Uiso 1 1 calc R . . . . H28B H -0.0637 0.3442 0.3390 0.037 Uiso 1 1 calc R . . . . C29 C 0.0153(2) 0.32775(17) 0.24735(13) 0.0318(5) Uani 1 1 d . . . . . H29A H 0.0709 0.3842 0.2663 0.038 Uiso 1 1 calc R . . . . H29B H -0.0444 0.3459 0.2175 0.038 Uiso 1 1 calc R . . . . C30 C 0.2180(2) 0.37949(18) 0.39581(14) 0.0434(7) Uani 1 1 d . . . . . H30A H 0.1797 0.4168 0.3681 0.065 Uiso 1 1 calc GR . . . . H30B H 0.2714 0.3439 0.3685 0.065 Uiso 1 1 calc GR . . . . H30C H 0.2618 0.4209 0.4350 0.065 Uiso 1 1 calc GR . . . . C31 C 0.1263(2) 0.31228(17) 0.42033(12) 0.0305(5) Uani 1 1 d . . . . . H31 H 0.1687 0.2775 0.4497 0.037 Uiso 1 1 calc R . . . . C32 C 0.0449(2) 0.3672(2) 0.46544(15) 0.0476(7) Uani 1 1 d . . . . . H32A H 0.0903 0.4074 0.5046 0.071 Uiso 1 1 calc GR . . . . H32B H -0.0132 0.3234 0.4813 0.071 Uiso 1 1 calc GR . . . . H32C H 0.0054 0.4057 0.4393 0.071 Uiso 1 1 calc GR . . . . C33 C 0.0100(3) 0.1043(2) 0.43955(15) 0.0469(7) Uani 1 1 d . . . . . H33A H -0.0466 0.0665 0.4613 0.070 Uiso 1 1 calc GR . . . . H33B H 0.0580 0.1507 0.4744 0.070 Uiso 1 1 calc GR . . . . H33C H 0.0600 0.0637 0.4135 0.070 Uiso 1 1 calc GR . . . . C34 C -0.0542(2) 0.15391(17) 0.39207(13) 0.0318(6) Uani 1 1 d . . . . . H34 H -0.1016 0.1971 0.4200 0.038 Uiso 1 1 calc R . . . . C35 C -0.1366(2) 0.08257(19) 0.34166(16) 0.0455(7) Uani 1 1 d . . . . . H35A H -0.0914 0.0421 0.3118 0.068 Uiso 1 1 calc GR . . . . H35B H -0.1837 0.1150 0.3144 0.068 Uiso 1 1 calc GR . . . . H35C H -0.1878 0.0446 0.3663 0.068 Uiso 1 1 calc GR . . . . C36 C 0.3016(2) 0.3611(2) 0.20618(15) 0.0468(7) Uani 1 1 d . . . . . H36A H 0.3599 0.3935 0.1820 0.070 Uiso 1 1 calc GR . . . . H36B H 0.3374 0.3161 0.2279 0.070 Uiso 1 1 calc GR . . . . H36C H 0.2715 0.4067 0.2408 0.070 Uiso 1 1 calc GR . . . . C37 C 0.2018(2) 0.30971(17) 0.15603(13) 0.0333(6) Uani 1 1 d . . . . . H37 H 0.2362 0.2647 0.1213 0.040 Uiso 1 1 calc R . . . . C38 C 0.1495(3) 0.3783(2) 0.11840(16) 0.0519(8) Uani 1 1 d . . . . . H38A H 0.1059 0.4186 0.1496 0.078 Uiso 1 1 calc GR . . . . H38B H 0.0969 0.3434 0.0802 0.078 Uiso 1 1 calc GR . . . . H38C H 0.2121 0.4168 0.1014 0.078 Uiso 1 1 calc GR . . . . C39 C -0.1305(2) 0.14675(19) 0.14825(14) 0.0399(6) Uani 1 1 d . . . . . H39A H -0.1823 0.1160 0.1085 0.060 Uiso 1 1 calc GR . . . . H39B H -0.1665 0.1978 0.1743 0.060 Uiso 1 1 calc GR . . . . H39C H -0.1174 0.1014 0.1768 0.060 Uiso 1 1 calc GR . . . . C40 C -0.0144(2) 0.18583(17) 0.12515(13) 0.0318(5) Uani 1 1 d . . . . . H40 H -0.0304 0.2361 0.1001 0.038 Uiso 1 1 calc R . . . . C41 C 0.0351(2) 0.11116(19) 0.07503(13) 0.0410(6) Uani 1 1 d . . . . . H41A H 0.0476 0.0587 0.0970 0.062 Uiso 1 1 calc GR . . . . H41B H 0.1093 0.1379 0.0608 0.062 Uiso 1 1 calc GR . . . . H41C H -0.0200 0.0891 0.0352 0.062 Uiso 1 1 calc GR . . . . C42 C 0.4587(3) 0.1727(2) 0.49101(15) 0.0487(8) Uani 1 1 d . . . . . H42A H 0.4918 0.2319 0.4797 0.073 Uiso 1 1 calc GR . . . . H42B H 0.5214 0.1420 0.5078 0.073 Uiso 1 1 calc GR . . . . H42C H 0.4037 0.1847 0.5262 0.073 Uiso 1 1 calc GR . . . . C43 C 0.3959(2) 0.11015(17) 0.42838(13) 0.0322(5) Uani 1 1 d . . . . . C44 C 0.3296(2) 0.02337(19) 0.44696(15) 0.0437(7) Uani 1 1 d . . . . . H44A H 0.2701 0.0419 0.4780 0.065 Uiso 1 1 calc GR . . . . H44B H 0.3839 -0.0096 0.4691 0.065 Uiso 1 1 calc GR . . . . H44C H 0.2922 -0.0180 0.4057 0.065 Uiso 1 1 calc GR . . . . C45 C 0.5649(2) 0.1665(2) 0.36218(17) 0.0472(7) Uani 1 1 d . . . . . H45A H 0.5984 0.1540 0.3180 0.071 Uiso 1 1 calc GR . . . . H45B H 0.6263 0.1727 0.3985 0.071 Uiso 1 1 calc GR . . . . H45C H 0.5299 0.2246 0.3668 0.071 Uiso 1 1 calc GR . . . . C46 C 0.4715(2) 0.08594(17) 0.36712(13) 0.0304(5) Uani 1 1 d . . . . . C47 C 0.5253(2) -0.00371(18) 0.36251(15) 0.0408(6) Uani 1 1 d . . . . . H47A H 0.4636 -0.0564 0.3595 0.061 Uiso 1 1 calc GR . . . . H47B H 0.5774 0.0004 0.4030 0.061 Uiso 1 1 calc GR . . . . H47C H 0.5697 -0.0132 0.3220 0.061 Uiso 1 1 calc GR . . . . C48 C 0.5208(3) 0.0844(3) 0.1460(2) 0.0785(12) Uani 1 1 d . . . . . H48A H 0.5510 0.1507 0.1518 0.118 Uiso 1 1 calc GR . . . . H48B H 0.5711 0.0471 0.1174 0.118 Uiso 1 1 calc GR . . . . H48C H 0.5193 0.0662 0.1904 0.118 Uiso 1 1 calc GR . . . . C49 C 0.3982(2) 0.06728(18) 0.11222(14) 0.0364(6) Uani 1 1 d . . . . . C50 C 0.3991(4) 0.0985(3) 0.04507(18) 0.0798(13) Uani 1 1 d . . . . . H50A H 0.3196 0.0887 0.0240 0.120 Uiso 1 1 calc GR . . . . H50B H 0.4484 0.0620 0.0152 0.120 Uiso 1 1 calc GR . . . . H50C H 0.4298 0.1649 0.0523 0.120 Uiso 1 1 calc GR . . . . C51 C 0.4099(3) -0.0987(2) 0.1335(2) 0.0803(13) Uani 1 1 d . . . . . H51A H 0.4378 -0.0764 0.1812 0.121 Uiso 1 1 calc GR . . . . H51B H 0.4766 -0.1023 0.1053 0.121 Uiso 1 1 calc GR . . . . H51C H 0.3650 -0.1608 0.1282 0.121 Uiso 1 1 calc GR . . . . C52 C 0.3336(2) -0.03217(17) 0.11169(13) 0.0342(6) Uani 1 1 d . . . . . C53 C 0.2660(3) -0.0763(3) 0.04530(17) 0.0794(13) Uani 1 1 d . . . . . H53A H 0.2222 -0.1359 0.0496 0.119 Uiso 1 1 calc GR . . . . H53B H 0.3201 -0.0870 0.0095 0.119 Uiso 1 1 calc GR . . . . H53C H 0.2118 -0.0345 0.0337 0.119 Uiso 1 1 calc GR . . . . B3 B 0.2984(2) 0.12715(19) 0.33021(14) 0.0269(6) Uani 1 1 d . . . . . B4 B 0.2506(2) 0.07771(19) 0.18730(13) 0.0256(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.01796(4) 0.01697(5) 0.02798(5) 0.00476(4) 0.00173(4) -0.00026(3) P1 0.0232(3) 0.0193(3) 0.0419(4) 0.0089(3) 0.0012(3) 0.0007(2) P2 0.0194(2) 0.0206(3) 0.0283(3) 0.0051(2) 0.0031(2) -0.0008(2) O1 0.0317(8) 0.0267(9) 0.0398(11) 0.0103(8) -0.0088(8) -0.0008(7) O2 0.0376(9) 0.0236(9) 0.0286(9) 0.0000(7) -0.0101(8) 0.0018(7) O3 0.0223(7) 0.0261(9) 0.0344(10) 0.0113(7) 0.0054(7) 0.0031(6) O4 0.0205(7) 0.0254(8) 0.0339(9) 0.0111(7) 0.0028(7) 0.0018(6) C1 0.0278(11) 0.0189(11) 0.0465(16) 0.0074(11) 0.0034(11) -0.0013(9) C2 0.0264(11) 0.0219(12) 0.0381(15) 0.0085(11) 0.0036(10) -0.0032(9) C3 0.0441(15) 0.0319(15) 0.072(2) 0.0066(14) 0.0265(15) 0.0096(12) C4 0.0283(12) 0.0198(12) 0.075(2) 0.0116(13) 0.0092(13) 0.0048(10) C5 0.0242(12) 0.0347(16) 0.109(3) 0.0188(17) 0.0045(15) 0.0059(11) C6 0.078(2) 0.0364(17) 0.073(2) 0.0288(17) -0.0169(19) 0.0006(16) C7 0.0448(15) 0.0288(14) 0.0494(18) 0.0193(13) -0.0124(13) -0.0026(11) C8 0.072(2) 0.065(2) 0.0384(18) 0.0245(16) 0.0038(16) 0.0098(17) C9 0.0566(17) 0.0430(17) 0.0288(15) 0.0031(12) 0.0055(13) -0.0022(13) C10 0.0329(12) 0.0371(15) 0.0308(14) 0.0075(12) -0.0002(11) -0.0046(11) C11 0.0552(17) 0.0570(19) 0.0430(18) 0.0243(15) -0.0027(15) 0.0092(15) C12 0.0378(14) 0.0431(16) 0.0466(18) -0.0005(13) 0.0179(13) 0.0027(12) C13 0.0227(11) 0.0271(13) 0.0465(16) 0.0084(11) 0.0103(11) 0.0045(9) C14 0.0215(11) 0.0487(17) 0.065(2) 0.0089(15) 0.0094(13) 0.0032(11) C15 0.0450(16) 0.066(2) 0.0377(17) 0.0245(15) -0.0047(13) 0.0004(14) C16 0.0296(12) 0.0342(14) 0.0288(14) 0.0091(11) -0.0021(10) -0.0008(10) C17 0.0292(13) 0.064(2) 0.0373(16) 0.0127(14) -0.0014(12) 0.0008(12) C18 0.060(2) 0.103(3) 0.0331(17) -0.0106(18) -0.0011(15) 0.036(2) C19 0.0419(14) 0.0368(15) 0.0293(14) -0.0015(12) -0.0103(12) 0.0066(11) C20 0.081(2) 0.0340(17) 0.060(2) -0.0040(15) -0.0378(19) -0.0044(15) C21 0.0252(12) 0.0492(17) 0.0596(19) 0.0228(15) 0.0099(12) 0.0063(11) C22 0.0247(11) 0.0289(13) 0.0350(14) 0.0108(11) 0.0087(10) 0.0025(9) C23 0.0545(17) 0.0379(16) 0.0410(17) 0.0057(13) 0.0173(14) 0.0099(13) C24 0.0346(12) 0.0283(13) 0.0345(15) 0.0067(11) 0.0016(11) -0.0034(10) C25 0.0224(10) 0.0249(12) 0.0279(13) 0.0089(10) 0.0029(9) -0.0014(9) C26 0.0344(12) 0.0352(14) 0.0333(14) 0.0132(12) 0.0011(11) -0.0016(11) B1 0.0223(11) 0.0262(14) 0.0264(14) 0.0035(11) 0.0032(11) -0.0016(10) B2 0.0225(11) 0.0224(13) 0.0268(14) 0.0040(11) 0.0012(11) 0.0015(10) Ir2 0.02017(4) 0.01859(5) 0.02141(5) 0.00454(3) 0.00286(3) 0.00409(3) P3 0.0241(3) 0.0211(3) 0.0261(3) 0.0035(2) 0.0048(2) 0.0060(2) P4 0.0278(3) 0.0212(3) 0.0259(3) 0.0065(2) -0.0004(2) 0.0037(2) O5 0.0348(9) 0.0341(9) 0.0245(9) 0.0050(7) -0.0003(7) 0.0178(7) O6 0.0294(8) 0.0396(10) 0.0261(9) 0.0059(8) 0.0026(7) 0.0158(7) O7 0.0452(10) 0.0272(9) 0.0491(12) 0.0058(8) 0.0270(9) 0.0045(8) O8 0.0458(10) 0.0262(9) 0.0400(11) 0.0019(8) 0.0243(9) 0.0026(8) C28 0.0305(12) 0.0278(13) 0.0343(14) 0.0029(11) 0.0014(11) 0.0127(10) C29 0.0376(13) 0.0241(13) 0.0351(14) 0.0058(11) -0.0021(11) 0.0110(10) C30 0.0503(16) 0.0329(15) 0.0388(16) -0.0043(12) 0.0044(13) -0.0098(12) C31 0.0327(12) 0.0283(13) 0.0286(13) -0.0002(10) 0.0041(11) 0.0051(10) C32 0.0448(15) 0.0457(17) 0.0431(17) -0.0164(14) 0.0067(14) 0.0073(13) C33 0.0534(17) 0.0456(17) 0.0508(19) 0.0254(14) 0.0206(15) 0.0118(14) C34 0.0303(12) 0.0271(13) 0.0401(15) 0.0065(11) 0.0156(11) 0.0074(10) C35 0.0333(13) 0.0356(15) 0.066(2) 0.0072(14) 0.0155(14) -0.0014(11) C36 0.0465(16) 0.0436(17) 0.0489(18) 0.0187(14) -0.0010(14) -0.0134(13) C37 0.0395(13) 0.0300(13) 0.0312(14) 0.0112(11) 0.0042(11) -0.0009(11) C38 0.0619(19) 0.0480(18) 0.053(2) 0.0321(16) 0.0020(16) 0.0023(15) C39 0.0324(13) 0.0418(16) 0.0431(17) 0.0057(13) -0.0076(12) 0.0031(11) C40 0.0355(12) 0.0313(14) 0.0288(14) 0.0076(11) -0.0071(11) 0.0053(10) C41 0.0445(15) 0.0446(16) 0.0292(15) -0.0020(12) -0.0056(12) 0.0044(12) C42 0.0593(18) 0.0452(17) 0.0390(17) -0.0031(14) -0.0150(15) 0.0218(14) C43 0.0370(13) 0.0326(14) 0.0292(14) 0.0070(11) -0.0033(11) 0.0138(11) C44 0.0486(16) 0.0455(17) 0.0429(17) 0.0196(14) 0.0072(13) 0.0121(13) C45 0.0366(14) 0.0441(17) 0.062(2) 0.0161(15) 0.0011(14) 0.0027(12) C46 0.0297(11) 0.0282(13) 0.0334(14) 0.0054(11) -0.0028(11) 0.0074(10) C47 0.0407(14) 0.0380(15) 0.0463(17) 0.0074(13) -0.0011(13) 0.0190(12) C48 0.0392(17) 0.058(2) 0.131(4) 0.001(2) 0.013(2) 0.0002(15) C49 0.0413(14) 0.0331(14) 0.0382(15) 0.0082(12) 0.0202(12) 0.0098(11) C50 0.137(4) 0.062(2) 0.052(2) 0.0223(18) 0.048(2) 0.029(2) C51 0.067(2) 0.056(2) 0.141(4) 0.054(2) 0.044(2) 0.0294(18) C52 0.0344(13) 0.0323(14) 0.0354(15) 0.0005(11) 0.0166(11) 0.0065(10) C53 0.076(2) 0.093(3) 0.046(2) -0.021(2) 0.0194(19) -0.031(2) B3 0.0275(12) 0.0267(14) 0.0284(15) 0.0067(12) 0.0040(11) 0.0078(11) B4 0.0266(12) 0.0300(14) 0.0222(14) 0.0071(11) 0.0042(11) 0.0074(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 H1 1.54(3) . ? Ir1 H2 1.62(3) . ? Ir1 H3 1.61(3) . ? Ir1 P1 2.3656(6) . ? Ir1 P2 2.3371(6) . ? Ir1 B1 2.099(3) . ? Ir1 B2 2.111(2) . ? P1 C1 1.851(2) . ? P1 C4 1.854(3) . ? P1 C7 1.861(3) . ? P2 C2 1.839(2) . ? P2 C10 1.847(3) . ? P2 C13 1.851(2) . ? O1 C16 1.446(3) . ? O1 B1 1.382(3) . ? O2 C19 1.453(3) . ? O2 B1 1.386(3) . ? O3 C22 1.456(3) . ? O3 B2 1.392(3) . ? O4 C25 1.456(2) . ? O4 B2 1.395(3) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C1 C2 1.531(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C3 C4 1.527(4) . ? C4 H0AA 1.0000 . ? C4 C5 1.527(4) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C6 C7 1.543(4) . ? C7 H7 1.0000 . ? C7 C8 1.513(4) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C9 C10 1.519(4) . ? C10 H10 1.0000 . ? C10 C11 1.525(4) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C12 C13 1.526(4) . ? C13 H13 1.0000 . ? C13 C14 1.534(3) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C15 C16 1.516(3) . ? C16 C17 1.520(3) . ? C16 C19 1.546(4) . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C18 C19 1.522(4) . ? C19 C20 1.521(4) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C21 C22 1.523(3) . ? C22 C23 1.516(4) . ? C22 C25 1.550(3) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C24 C25 1.518(3) . ? C25 C26 1.521(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? Ir2 H4 1.65(3) . ? Ir2 H5 1.57(3) . ? Ir2 H6 1.57(3) . ? Ir2 P3 2.3647(6) . ? Ir2 P4 2.3136(6) . ? Ir2 B3 2.116(3) . ? Ir2 B4 2.095(3) . ? P3 C28 1.841(2) . ? P3 C31 1.853(2) . ? P3 C34 1.850(2) . ? P4 C29 1.839(2) . ? P4 C37 1.844(2) . ? P4 C40 1.854(2) . ? O5 C43 1.452(3) . ? O5 B3 1.400(3) . ? O6 C46 1.439(3) . ? O6 B3 1.395(3) . ? O7 C49 1.443(3) . ? O7 B4 1.383(3) . ? O8 C52 1.452(3) . ? O8 B4 1.380(3) . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C28 C29 1.536(3) . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C30 C31 1.526(3) . ? C31 H31 1.0000 . ? C31 C32 1.535(3) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C33 C34 1.526(4) . ? C34 H34 1.0000 . ? C34 C35 1.521(4) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C36 C37 1.525(4) . ? C37 H37 1.0000 . ? C37 C38 1.534(4) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C39 C40 1.527(3) . ? C40 H40 1.0000 . ? C40 C41 1.530(3) . ? C41 H41A 0.9800 . ? C41 H41B 0.9800 . ? C41 H41C 0.9800 . ? C42 H42A 0.9800 . ? C42 H42B 0.9800 . ? C42 H42C 0.9800 . ? C42 C43 1.511(4) . ? C43 C44 1.526(4) . ? C43 C46 1.557(3) . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C45 C46 1.527(3) . ? C46 C47 1.515(3) . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C48 H48A 0.9800 . ? C48 H48B 0.9800 . ? C48 H48C 0.9800 . ? C48 C49 1.519(4) . ? C49 C50 1.506(4) . ? C49 C52 1.559(3) . ? C50 H50A 0.9800 . ? C50 H50B 0.9800 . ? C50 H50C 0.9800 . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C51 C52 1.507(4) . ? C52 C53 1.508(4) . ? C53 H53A 0.9800 . ? C53 H53B 0.9800 . ? C53 H53C 0.9800 . ? B3 H4 1.61(3) . ? B3 H6 1.61(3) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1 Ir1 H2 87.1(14) . . ? H1 Ir1 H3 87.5(15) . . ? H2 Ir1 H3 173.7(14) . . ? P1 Ir1 H1 171.8(10) . . ? P1 Ir1 H2 91.6(10) . . ? P1 Ir1 H3 93.3(11) . . ? P2 Ir1 H1 86.9(10) . . ? P2 Ir1 H2 87.7(10) . . ? P2 Ir1 H3 88.8(11) . . ? P2 Ir1 P1 84.93(2) . . ? B1 Ir1 H1 91.7(10) . . ? B1 Ir1 H2 59.8(10) . . ? B1 Ir1 H3 123.6(11) . . ? B1 Ir1 P1 94.65(8) . . ? B1 Ir1 P2 147.48(7) . . ? B1 Ir1 B2 71.06(10) . . ? B2 Ir1 H1 78.8(10) . . ? B2 Ir1 H2 128.2(10) . . ? B2 Ir1 H3 53.5(11) . . ? B2 Ir1 P1 108.16(7) . . ? B2 Ir1 P2 139.79(7) . . ? C1 P1 Ir1 107.36(8) . . ? C1 P1 C4 100.51(11) . . ? C1 P1 C7 103.20(12) . . ? C4 P1 Ir1 121.25(9) . . ? C4 P1 C7 102.52(13) . . ? C7 P1 Ir1 119.15(9) . . ? C2 P2 Ir1 109.88(8) . . ? C2 P2 C10 103.83(12) . . ? C2 P2 C13 104.04(11) . . ? C10 P2 Ir1 117.58(8) . . ? C10 P2 C13 102.30(12) . . ? C13 P2 Ir1 117.55(8) . . ? B1 O1 C16 109.33(18) . . ? B1 O2 C19 107.78(19) . . ? B2 O3 C22 108.36(17) . . ? B2 O4 C25 108.32(16) . . ? P1 C1 H1A 108.8 . . ? P1 C1 H1B 108.8 . . ? H1A C1 H1B 107.7 . . ? C2 C1 P1 113.79(16) . . ? C2 C1 H1A 108.8 . . ? C2 C1 H1B 108.8 . . ? P2 C2 H2A 109.3 . . ? P2 C2 H2B 109.3 . . ? C1 C2 P2 111.65(15) . . ? C1 C2 H2A 109.3 . . ? C1 C2 H2B 109.3 . . ? H2A C2 H2B 108.0 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? P1 C4 H0AA 107.5 . . ? C3 C4 P1 111.95(18) . . ? C3 C4 H0AA 107.5 . . ? C5 C4 P1 111.4(2) . . ? C5 C4 C3 110.7(2) . . ? C5 C4 H0AA 107.5 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C7 C6 H6A 109.5 . . ? C7 C6 H6B 109.5 . . ? C7 C6 H6C 109.5 . . ? P1 C7 H7 106.6 . . ? C6 C7 P1 114.5(2) . . ? C6 C7 H7 106.6 . . ? C8 C7 P1 112.33(19) . . ? C8 C7 C6 109.5(2) . . ? C8 C7 H7 106.6 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? H9A C9 H9B 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C10 C9 H9A 109.5 . . ? C10 C9 H9B 109.5 . . ? C10 C9 H9C 109.5 . . ? P2 C10 H10 107.7 . . ? C9 C10 P2 112.53(18) . . ? C9 C10 H10 107.7 . . ? C9 C10 C11 110.3(2) . . ? C11 C10 P2 110.80(19) . . ? C11 C10 H10 107.7 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C13 C12 H12A 109.5 . . ? C13 C12 H12B 109.5 . . ? C13 C12 H12C 109.5 . . ? P2 C13 H13 107.1 . . ? C12 C13 P2 112.57(17) . . ? C12 C13 H13 107.1 . . ? C12 C13 C14 108.9(2) . . ? C14 C13 P2 113.62(18) . . ? C14 C13 H13 107.1 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C16 C15 H15A 109.5 . . ? C16 C15 H15B 109.5 . . ? C16 C15 H15C 109.5 . . ? O1 C16 C15 108.6(2) . . ? O1 C16 C17 106.9(2) . . ? O1 C16 C19 101.77(18) . . ? C15 C16 C17 109.9(2) . . ? C15 C16 C19 115.0(2) . . ? C17 C16 C19 113.9(2) . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C19 C18 H18A 109.5 . . ? C19 C18 H18B 109.5 . . ? C19 C18 H18C 109.5 . . ? O2 C19 C16 102.32(19) . . ? O2 C19 C18 106.9(2) . . ? O2 C19 C20 109.1(2) . . ? C18 C19 C16 113.2(2) . . ? C20 C19 C16 114.8(2) . . ? C20 C19 C18 109.9(3) . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C22 C21 H21A 109.5 . . ? C22 C21 H21B 109.5 . . ? C22 C21 H21C 109.5 . . ? O3 C22 C21 109.0(2) . . ? O3 C22 C23 107.05(19) . . ? O3 C22 C25 101.69(16) . . ? C21 C22 C25 114.5(2) . . ? C23 C22 C21 110.3(2) . . ? C23 C22 C25 113.6(2) . . ? C22 C23 H23A 109.5 . . ? C22 C23 H23B 109.5 . . ? C22 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C25 C24 H24A 109.5 . . ? C25 C24 H24B 109.5 . . ? C25 C24 H24C 109.5 . . ? O4 C25 C22 101.91(16) . . ? O4 C25 C24 107.21(18) . . ? O4 C25 C26 108.89(18) . . ? C24 C25 C22 113.0(2) . . ? C24 C25 C26 110.47(19) . . ? C26 C25 C22 114.6(2) . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? O1 B1 Ir1 122.81(18) . . ? O1 B1 O2 109.8(2) . . ? O2 B1 Ir1 127.20(18) . . ? O3 B2 Ir1 127.04(17) . . ? O3 B2 O4 109.56(19) . . ? O4 B2 Ir1 123.39(16) . . ? H4 Ir2 H5 171.3(14) . . ? H4 Ir2 H6 97.8(15) . . ? H5 Ir2 H6 85.1(15) . . ? P3 Ir2 H4 95.1(10) . . ? P3 Ir2 H5 92.9(10) . . ? P3 Ir2 H6 95.1(11) . . ? P4 Ir2 H4 94.8(10) . . ? P4 Ir2 H5 82.3(10) . . ? P4 Ir2 H6 167.4(11) . . ? P4 Ir2 P3 85.23(2) . . ? B3 Ir2 H4 48.5(10) . . ? B3 Ir2 H5 133.7(10) . . ? B3 Ir2 H6 49.2(11) . . ? B3 Ir2 P3 97.42(7) . . ? B3 Ir2 P4 143.32(7) . . ? B4 Ir2 H4 84.6(10) . . ? B4 Ir2 H5 87.3(10) . . ? B4 Ir2 H6 88.2(11) . . ? B4 Ir2 P3 176.71(7) . . ? B4 Ir2 P4 91.54(7) . . ? B4 Ir2 B3 84.82(10) . . ? C28 P3 Ir2 107.00(8) . . ? C28 P3 C31 103.93(11) . . ? C28 P3 C34 103.23(11) . . ? C31 P3 Ir2 120.38(7) . . ? C34 P3 Ir2 117.73(8) . . ? C34 P3 C31 102.56(11) . . ? C29 P4 Ir2 109.46(8) . . ? C29 P4 C37 104.16(12) . . ? C29 P4 C40 102.89(11) . . ? C37 P4 Ir2 118.74(8) . . ? C37 P4 C40 102.57(12) . . ? C40 P4 Ir2 117.18(8) . . ? B3 O5 C43 107.54(18) . . ? B3 O6 C46 108.38(19) . . ? B4 O7 C49 111.33(19) . . ? B4 O8 C52 110.83(18) . . ? P3 C28 H28A 109.2 . . ? P3 C28 H28B 109.2 . . ? H28A C28 H28B 107.9 . . ? C29 C28 P3 112.22(15) . . ? C29 C28 H28A 109.2 . . ? C29 C28 H28B 109.2 . . ? P4 C29 H29A 109.2 . . ? P4 C29 H29B 109.2 . . ? C28 C29 P4 112.03(16) . . ? C28 C29 H29A 109.2 . . ? C28 C29 H29B 109.2 . . ? H29A C29 H29B 107.9 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C31 C30 H30A 109.5 . . ? C31 C30 H30B 109.5 . . ? C31 C30 H30C 109.5 . . ? P3 C31 H31 106.9 . . ? C30 C31 P3 111.62(17) . . ? C30 C31 H31 106.9 . . ? C30 C31 C32 110.1(2) . . ? C32 C31 P3 114.15(17) . . ? C32 C31 H31 106.9 . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? H33A C33 H33B 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C34 C33 H33A 109.5 . . ? C34 C33 H33B 109.5 . . ? C34 C33 H33C 109.5 . . ? P3 C34 H34 108.2 . . ? C33 C34 P3 110.72(17) . . ? C33 C34 H34 108.2 . . ? C35 C34 P3 111.78(18) . . ? C35 C34 C33 109.6(2) . . ? C35 C34 H34 108.2 . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C37 C36 H36A 109.5 . . ? C37 C36 H36B 109.5 . . ? C37 C36 H36C 109.5 . . ? P4 C37 H37 106.9 . . ? C36 C37 P4 112.01(18) . . ? C36 C37 H37 106.9 . . ? C36 C37 C38 110.1(2) . . ? C38 C37 P4 113.54(19) . . ? C38 C37 H37 106.9 . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? H39A C39 H39B 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C40 C39 H39A 109.5 . . ? C40 C39 H39B 109.5 . . ? C40 C39 H39C 109.5 . . ? P4 C40 H40 107.0 . . ? C39 C40 P4 113.05(18) . . ? C39 C40 H40 107.0 . . ? C39 C40 C41 111.0(2) . . ? C41 C40 P4 111.42(17) . . ? C41 C40 H40 107.0 . . ? C40 C41 H41A 109.5 . . ? C40 C41 H41B 109.5 . . ? C40 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? C43 C42 H42A 109.5 . . ? C43 C42 H42B 109.5 . . ? C43 C42 H42C 109.5 . . ? O5 C43 C42 109.1(2) . . ? O5 C43 C44 106.8(2) . . ? O5 C43 C46 101.90(18) . . ? C42 C43 C44 110.2(2) . . ? C42 C43 C46 115.7(2) . . ? C44 C43 C46 112.4(2) . . ? C43 C44 H44A 109.5 . . ? C43 C44 H44B 109.5 . . ? C43 C44 H44C 109.5 . . ? H44A C44 H44B 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C46 C45 H45A 109.5 . . ? C46 C45 H45B 109.5 . . ? C46 C45 H45C 109.5 . . ? O6 C46 C43 102.30(17) . . ? O6 C46 C45 107.2(2) . . ? O6 C46 C47 108.6(2) . . ? C45 C46 C43 112.3(2) . . ? C47 C46 C43 115.8(2) . . ? C47 C46 C45 110.0(2) . . ? C46 C47 H47A 109.5 . . ? C46 C47 H47B 109.5 . . ? C46 C47 H47C 109.5 . . ? H47A C47 H47B 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? H48A C48 H48B 109.5 . . ? H48A C48 H48C 109.5 . . ? H48B C48 H48C 109.5 . . ? C49 C48 H48A 109.5 . . ? C49 C48 H48B 109.5 . . ? C49 C48 H48C 109.5 . . ? O7 C49 C48 106.0(2) . . ? O7 C49 C50 106.6(2) . . ? O7 C49 C52 103.48(18) . . ? C48 C49 C52 113.8(2) . . ? C50 C49 C48 109.8(3) . . ? C50 C49 C52 116.2(3) . . ? C49 C50 H50A 109.5 . . ? C49 C50 H50B 109.5 . . ? C49 C50 H50C 109.5 . . ? H50A C50 H50B 109.5 . . ? H50A C50 H50C 109.5 . . ? H50B C50 H50C 109.5 . . ? H51A C51 H51B 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C52 C51 H51A 109.5 . . ? C52 C51 H51B 109.5 . . ? C52 C51 H51C 109.5 . . ? O8 C52 C49 104.06(18) . . ? O8 C52 C51 107.6(2) . . ? O8 C52 C53 106.4(2) . . ? C51 C52 C49 114.3(2) . . ? C51 C52 C53 110.4(3) . . ? C53 C52 C49 113.5(3) . . ? C52 C53 H53A 109.5 . . ? C52 C53 H53B 109.5 . . ? C52 C53 H53C 109.5 . . ? H53A C53 H53B 109.5 . . ? H53A C53 H53C 109.5 . . ? H53B C53 H53C 109.5 . . ? Ir2 B3 H4 50.5(10) . . ? Ir2 B3 H6 47.4(10) . . ? H4 B3 H6 97.9(15) . . ? O5 B3 Ir2 125.18(17) . . ? O5 B3 H4 111.6(10) . . ? O5 B3 H6 113.2(11) . . ? O6 B3 Ir2 124.61(19) . . ? O6 B3 H4 115.2(10) . . ? O6 B3 H6 108.5(10) . . ? O6 B3 O5 110.0(2) . . ? O7 B4 Ir2 121.63(18) . . ? O8 B4 Ir2 128.84(17) . . ? O8 B4 O7 109.5(2) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ir1 P1 C1 C2 32.0(2) . . . . ? Ir1 P1 C4 C3 47.1(2) . . . . ? Ir1 P1 C4 C5 -77.5(2) . . . . ? Ir1 P1 C7 C6 -177.44(18) . . . . ? Ir1 P1 C7 C8 -51.6(2) . . . . ? Ir1 P2 C2 C1 29.3(2) . . . . ? Ir1 P2 C10 C9 -61.71(19) . . . . ? Ir1 P2 C10 C11 62.2(2) . . . . ? Ir1 P2 C13 C12 53.7(2) . . . . ? Ir1 P2 C13 C14 178.05(16) . . . . ? P1 C1 C2 P2 -39.8(2) . . . . ? O1 C16 C19 O2 29.0(2) . . . . ? O1 C16 C19 C18 -85.6(3) . . . . ? O1 C16 C19 C20 147.0(2) . . . . ? O3 C22 C25 O4 31.1(2) . . . . ? O3 C22 C25 C24 -83.7(2) . . . . ? O3 C22 C25 C26 148.51(18) . . . . ? C1 P1 C4 C3 -70.8(2) . . . . ? C1 P1 C4 C5 164.6(2) . . . . ? C1 P1 C7 C6 -58.6(2) . . . . ? C1 P1 C7 C8 67.2(2) . . . . ? C2 P2 C10 C9 59.87(19) . . . . ? C2 P2 C10 C11 -176.17(18) . . . . ? C2 P2 C13 C12 -68.1(2) . . . . ? C2 P2 C13 C14 56.3(2) . . . . ? C4 P1 C1 C2 159.61(19) . . . . ? C4 P1 C7 C6 45.5(2) . . . . ? C4 P1 C7 C8 171.3(2) . . . . ? C7 P1 C1 C2 -94.7(2) . . . . ? C7 P1 C4 C3 -177.02(18) . . . . ? C7 P1 C4 C5 58.4(2) . . . . ? C10 P2 C2 C1 -97.27(19) . . . . ? C10 P2 C13 C12 -175.92(18) . . . . ? C10 P2 C13 C14 -51.5(2) . . . . ? C13 P2 C2 C1 156.01(18) . . . . ? C13 P2 C10 C9 167.90(18) . . . . ? C13 P2 C10 C11 -68.1(2) . . . . ? C15 C16 C19 O2 146.2(2) . . . . ? C15 C16 C19 C18 31.5(3) . . . . ? C15 C16 C19 C20 -95.8(3) . . . . ? C16 O1 B1 Ir1 -177.56(16) . . . . ? C16 O1 B1 O2 6.5(3) . . . . ? C17 C16 C19 O2 -85.7(2) . . . . ? C17 C16 C19 C18 159.7(2) . . . . ? C17 C16 C19 C20 32.3(3) . . . . ? C19 O2 B1 Ir1 -161.95(18) . . . . ? C19 O2 B1 O1 13.7(3) . . . . ? C21 C22 C25 O4 148.4(2) . . . . ? C21 C22 C25 C24 33.7(3) . . . . ? C21 C22 C25 C26 -94.1(3) . . . . ? C22 O3 B2 Ir1 -169.27(18) . . . . ? C22 O3 B2 O4 11.7(3) . . . . ? C23 C22 C25 O4 -83.6(2) . . . . ? C23 C22 C25 C24 161.7(2) . . . . ? C23 C22 C25 C26 33.8(3) . . . . ? C25 O4 B2 Ir1 -169.10(16) . . . . ? C25 O4 B2 O3 10.0(3) . . . . ? B1 O1 C16 C15 -144.0(2) . . . . ? B1 O1 C16 C17 97.5(2) . . . . ? B1 O1 C16 C19 -22.3(2) . . . . ? B1 O2 C19 C16 -26.5(2) . . . . ? B1 O2 C19 C18 92.6(3) . . . . ? B1 O2 C19 C20 -148.6(2) . . . . ? B2 O3 C22 C21 -147.9(2) . . . . ? B2 O3 C22 C23 92.8(2) . . . . ? B2 O3 C22 C25 -26.6(2) . . . . ? B2 O4 C25 C22 -25.7(2) . . . . ? B2 O4 C25 C24 93.3(2) . . . . ? B2 O4 C25 C26 -147.2(2) . . . . ? Ir2 P3 C28 C29 -35.12(19) . . . . ? Ir2 P3 C31 C30 47.2(2) . . . . ? Ir2 P3 C31 C32 172.79(16) . . . . ? Ir2 P3 C34 C33 70.9(2) . . . . ? Ir2 P3 C34 C35 -51.62(19) . . . . ? Ir2 P4 C29 C28 -29.49(19) . . . . ? Ir2 P4 C37 C36 -48.4(2) . . . . ? Ir2 P4 C37 C38 -173.96(17) . . . . ? Ir2 P4 C40 C39 64.46(19) . . . . ? Ir2 P4 C40 C41 -61.31(19) . . . . ? P3 C28 C29 P4 42.1(2) . . . . ? O5 C43 C46 O6 -30.9(2) . . . . ? O5 C43 C46 C45 83.8(2) . . . . ? O5 C43 C46 C47 -148.7(2) . . . . ? O7 C49 C52 O8 -7.6(3) . . . . ? O7 C49 C52 C51 -124.5(3) . . . . ? O7 C49 C52 C53 107.7(3) . . . . ? C28 P3 C31 C30 -72.5(2) . . . . ? C28 P3 C31 C32 53.2(2) . . . . ? C28 P3 C34 C33 -171.55(19) . . . . ? C28 P3 C34 C35 65.95(19) . . . . ? C29 P4 C37 C36 73.6(2) . . . . ? C29 P4 C37 C38 -51.9(2) . . . . ? C29 P4 C40 C39 -55.7(2) . . . . ? C29 P4 C40 C41 178.57(18) . . . . ? C31 P3 C28 C29 93.24(18) . . . . ? C31 P3 C34 C33 -63.7(2) . . . . ? C31 P3 C34 C35 173.75(18) . . . . ? C34 P3 C28 C29 -160.00(18) . . . . ? C34 P3 C31 C30 -179.73(18) . . . . ? C34 P3 C31 C32 -54.1(2) . . . . ? C37 P4 C29 C28 -157.46(17) . . . . ? C37 P4 C40 C39 -163.60(18) . . . . ? C37 P4 C40 C41 70.6(2) . . . . ? C40 P4 C29 C28 95.80(19) . . . . ? C40 P4 C37 C36 -179.44(19) . . . . ? C40 P4 C37 C38 55.0(2) . . . . ? C42 C43 C46 O6 -149.0(2) . . . . ? C42 C43 C46 C45 -34.4(3) . . . . ? C42 C43 C46 C47 93.2(3) . . . . ? C43 O5 B3 Ir2 162.39(18) . . . . ? C43 O5 B3 O6 -12.4(3) . . . . ? C44 C43 C46 O6 83.1(2) . . . . ? C44 C43 C46 C45 -162.2(2) . . . . ? C44 C43 C46 C47 -34.7(3) . . . . ? C46 O6 B3 Ir2 176.15(17) . . . . ? C46 O6 B3 O5 -9.0(3) . . . . ? C48 C49 C52 O8 107.0(3) . . . . ? C48 C49 C52 C51 -10.0(4) . . . . ? C48 C49 C52 C53 -137.8(3) . . . . ? C49 O7 B4 Ir2 170.17(18) . . . . ? C49 O7 B4 O8 -7.5(3) . . . . ? C50 C49 C52 O8 -124.0(3) . . . . ? C50 C49 C52 C51 119.0(3) . . . . ? C50 C49 C52 C53 -8.8(3) . . . . ? C52 O8 B4 Ir2 -175.42(19) . . . . ? C52 O8 B4 O7 2.0(3) . . . . ? B3 O5 C43 C42 149.4(2) . . . . ? B3 O5 C43 C44 -91.5(2) . . . . ? B3 O5 C43 C46 26.6(2) . . . . ? B3 O6 C46 C43 24.7(2) . . . . ? B3 O6 C46 C45 -93.6(2) . . . . ? B3 O6 C46 C47 147.6(2) . . . . ? B4 O7 C49 C48 -110.7(3) . . . . ? B4 O7 C49 C50 132.3(3) . . . . ? B4 O7 C49 C52 9.3(3) . . . . ? B4 O8 C52 C49 3.6(3) . . . . ? B4 O8 C52 C51 125.2(3) . . . . ? B4 O8 C52 C53 -116.6(3) . . . . ? _iucr_refine_instructions_details ; TITL test in P-1 CELL 0.71073 11.6009 14.711 20.1115 100.827 92.604 96.944 ZERR 2 0.0005 0.0007 0.0011 0.003 0.003 0.003 LATT 1 SFAC C H B Ir O P UNIT 104 236 8 4 16 8 L.S. 12 PLAN 5 TEMP -100.16 BOND $H fmap 2 MORE -1 ACTA 52 CONF REM REM REM WGHT 0.019800 1.515200 FVAR 0.06681 IR1 4 0.957544 0.624622 0.252471 11.00000 0.01796 0.01697 = 0.02798 0.00476 0.00173 -0.00026 H1 2 1.005840 0.536923 0.267593 11.00000 0.05070 H2 2 0.995309 0.594480 0.175436 11.00000 0.06157 H3 2 0.931837 0.649165 0.331532 11.00000 0.07445 P1 6 0.911395 0.769392 0.231402 11.00000 0.02323 0.01930 = 0.04194 0.00892 0.00122 0.00071 P2 6 1.145865 0.703271 0.280601 11.00000 0.01936 0.02059 = 0.02830 0.00513 0.00313 -0.00083 O1 5 0.765098 0.582787 0.136499 11.00000 0.03170 0.02670 = 0.03979 0.01033 -0.00878 -0.00082 O2 5 0.821896 0.447677 0.156167 11.00000 0.03756 0.02356 = 0.02860 -0.00004 -0.01012 0.00177 O3 5 0.704924 0.587120 0.301366 11.00000 0.02226 0.02614 = 0.03439 0.01128 0.00541 0.00311 O4 5 0.824965 0.488289 0.332185 11.00000 0.02054 0.02541 = 0.03393 0.01113 0.00276 0.00180 C1 1 1.038013 0.858194 0.264273 11.00000 0.02778 0.01886 = 0.04652 0.00740 0.00338 -0.00129 AFIX 23 H1A 2 1.038976 0.909394 0.238544 11.00000 -1.20000 H1B 2 1.028434 0.884936 0.312368 11.00000 -1.20000 AFIX 0 C2 1 1.155067 0.820112 0.259456 11.00000 0.02636 0.02187 = 0.03810 0.00853 0.00364 -0.00324 AFIX 23 H2A 2 1.214308 0.863281 0.290924 11.00000 -1.20000 H2B 2 1.180288 0.817021 0.212804 11.00000 -1.20000 AFIX 0 C3 1 0.799762 0.827167 0.350166 11.00000 0.04415 0.03191 = 0.07176 0.00661 0.02647 0.00956 AFIX 137 H3A 2 0.737364 0.859399 0.371006 11.00000 -1.50000 H3B 2 0.875353 0.859906 0.370581 11.00000 -1.50000 H3C 2 0.791049 0.762895 0.357785 11.00000 -1.50000 AFIX 0 C4 1 0.792779 0.826076 0.273993 11.00000 0.02832 0.01983 = 0.07500 0.01161 0.00918 0.00477 AFIX 13 H0AA 2 0.802381 0.892442 0.267940 11.00000 -1.20000 AFIX 0 C5 1 0.673312 0.780236 0.241322 11.00000 0.02424 0.03469 = 0.10870 0.01880 0.00448 0.00594 AFIX 137 H5A 2 0.663149 0.713946 0.244010 11.00000 -1.50000 H5B 2 0.667548 0.786372 0.193640 11.00000 -1.50000 H5C 2 0.612573 0.810973 0.265352 11.00000 -1.50000 AFIX 0 C6 1 0.862137 0.882422 0.134556 11.00000 0.07794 0.03643 = 0.07284 0.02884 -0.01695 0.00058 AFIX 137 H6A 2 0.794193 0.898422 0.159279 11.00000 -1.50000 H6B 2 0.846814 0.883555 0.086415 11.00000 -1.50000 H6C 2 0.930093 0.927885 0.153152 11.00000 -1.50000 AFIX 0 C7 1 0.886250 0.783841 0.142151 11.00000 0.04482 0.02885 = 0.04943 0.01931 -0.01235 -0.00255 AFIX 13 H7 2 0.814942 0.740047 0.122641 11.00000 -1.20000 AFIX 0 C8 1 0.984293 0.755562 0.098985 11.00000 0.07204 0.06507 = 0.03835 0.02447 0.00382 0.00979 AFIX 137 H8A 2 0.963436 0.757578 0.051563 11.00000 -1.50000 H8B 2 0.997525 0.692029 0.102476 11.00000 -1.50000 H8C 2 1.055426 0.798760 0.114954 11.00000 -1.50000 AFIX 0 C9 1 1.128382 0.788065 0.416234 11.00000 0.05657 0.04300 = 0.02877 0.00310 0.00552 -0.00220 AFIX 137 H9A 2 1.048093 0.757186 0.413432 11.00000 -1.50000 H9B 2 1.129118 0.847907 0.401440 11.00000 -1.50000 H9C 2 1.161369 0.798962 0.463218 11.00000 -1.50000 AFIX 0 C10 1 1.200580 0.726266 0.370670 11.00000 0.03294 0.03712 = 0.03081 0.00752 -0.00024 -0.00464 AFIX 13 H10 2 1.281568 0.759794 0.374119 11.00000 -1.20000 AFIX 0 C11 1 1.206636 0.635049 0.395524 11.00000 0.05516 0.05699 = 0.04305 0.02433 -0.00272 0.00921 AFIX 137 H11A 2 1.240226 0.648722 0.442481 11.00000 -1.50000 H11B 2 1.255501 0.596732 0.366654 11.00000 -1.50000 H11C 2 1.128072 0.601093 0.393402 11.00000 -1.50000 AFIX 0 C12 1 1.245575 0.631716 0.159989 11.00000 0.03783 0.04307 = 0.04660 -0.00054 0.01786 0.00265 AFIX 137 H12A 2 1.244834 0.690876 0.144372 11.00000 -1.50000 H12B 2 1.170559 0.592602 0.146593 11.00000 -1.50000 H12C 2 1.308009 0.599205 0.139469 11.00000 -1.50000 AFIX 0 C13 1 1.266321 0.651124 0.237111 11.00000 0.02270 0.02715 = 0.04646 0.00844 0.01029 0.00446 AFIX 13 H13 2 1.270080 0.589617 0.250888 11.00000 -1.20000 AFIX 0 C14 1 1.385805 0.709492 0.257193 11.00000 0.02145 0.04870 = 0.06508 0.00887 0.00938 0.00320 AFIX 137 H14A 2 1.445407 0.678173 0.232436 11.00000 -1.50000 H14B 2 1.403752 0.716258 0.306102 11.00000 -1.50000 H14C 2 1.384595 0.771337 0.245871 11.00000 -1.50000 AFIX 0 C15 1 0.670989 0.538235 0.024020 11.00000 0.04496 0.06649 = 0.03766 0.02451 -0.00467 0.00044 AFIX 137 H15A 2 0.628825 0.592732 0.030011 11.00000 -1.50000 H15B 2 0.625638 0.486621 -0.008180 11.00000 -1.50000 H15C 2 0.746681 0.554172 0.006451 11.00000 -1.50000 AFIX 0 C16 1 0.689273 0.509129 0.091724 11.00000 0.02962 0.03423 = 0.02878 0.00909 -0.00210 -0.00084 C17 1 0.574100 0.498500 0.124447 11.00000 0.02916 0.06424 = 0.03728 0.01275 -0.00143 0.00080 AFIX 137 H17A 2 0.586416 0.479184 0.168002 11.00000 -1.50000 H17B 2 0.518734 0.451138 0.094462 11.00000 -1.50000 H17C 2 0.542901 0.558324 0.131974 11.00000 -1.50000 AFIX 0 C18 1 0.848069 0.419518 0.037201 11.00000 0.06031 0.10286 = 0.03306 -0.01059 -0.00113 0.03620 AFIX 137 H18A 2 0.896755 0.480048 0.042537 11.00000 -1.50000 H18B 2 0.808366 0.403397 -0.008325 11.00000 -1.50000 H18C 2 0.897041 0.371504 0.043347 11.00000 -1.50000 AFIX 0 C19 1 0.758041 0.425120 0.090085 11.00000 0.04192 0.03683 = 0.02932 -0.00152 -0.01025 0.00655 C20 1 0.683142 0.331041 0.082988 11.00000 0.08120 0.03398 = 0.05984 -0.00403 -0.03783 -0.00436 AFIX 137 H20A 2 0.733121 0.282815 0.086687 11.00000 -1.50000 H20B 2 0.639208 0.315711 0.038672 11.00000 -1.50000 H20C 2 0.628850 0.333997 0.119035 11.00000 -1.50000 AFIX 0 C21 1 0.515042 0.517139 0.325457 11.00000 0.02520 0.04916 = 0.05957 0.02284 0.00990 0.00627 AFIX 137 H21A 2 0.480791 0.575413 0.328815 11.00000 -1.50000 H21B 2 0.474914 0.478200 0.354095 11.00000 -1.50000 H21C 2 0.506657 0.483564 0.278198 11.00000 -1.50000 AFIX 0 C22 1 0.643636 0.539263 0.349173 11.00000 0.02475 0.02885 = 0.03498 0.01080 0.00874 0.00252 C23 1 0.659826 0.605228 0.417546 11.00000 0.05452 0.03788 = 0.04097 0.00568 0.01734 0.00990 AFIX 137 H23A 2 0.742459 0.616470 0.433232 11.00000 -1.50000 H23B 2 0.614750 0.577307 0.450407 11.00000 -1.50000 H23C 2 0.632734 0.664544 0.413190 11.00000 -1.50000 AFIX 0 C24 1 0.662182 0.373376 0.287706 11.00000 0.03456 0.02825 = 0.03452 0.00671 0.00155 -0.00336 AFIX 137 H24A 2 0.661545 0.397103 0.245320 11.00000 -1.50000 H24B 2 0.582866 0.347958 0.295259 11.00000 -1.50000 H24C 2 0.712545 0.324063 0.284659 11.00000 -1.50000 AFIX 0 C25 1 0.708004 0.452353 0.346362 11.00000 0.02241 0.02487 = 0.02794 0.00887 0.00294 -0.00140 C26 1 0.714361 0.416444 0.412429 11.00000 0.03444 0.03524 = 0.03326 0.01319 0.00109 -0.00164 AFIX 137 H26A 2 0.751237 0.359185 0.405490 11.00000 -1.50000 H26B 2 0.635562 0.403124 0.426858 11.00000 -1.50000 H26C 2 0.760378 0.463889 0.447502 11.00000 -1.50000 AFIX 0 B1 3 0.837003 0.543904 0.176849 11.00000 0.02226 0.02621 = 0.02641 0.00349 0.00315 -0.00162 B2 3 0.817245 0.562872 0.299101 11.00000 0.02245 0.02235 = 0.02683 0.00401 0.00119 0.00153 IR2 4 0.157233 0.143494 0.264965 11.00000 0.02017 0.01859 = 0.02141 0.00454 0.00286 0.00409 H4 2 0.282415 0.210155 0.290336 11.00000 0.05735 H5 2 0.046397 0.076902 0.230128 11.00000 0.05953 H6 2 0.175899 0.063160 0.304122 11.00000 0.06196 P3 6 0.050155 0.224228 0.348810 11.00000 0.02408 0.02109 = 0.02608 0.00354 0.00481 0.00604 P4 6 0.093238 0.240231 0.196784 11.00000 0.02784 0.02120 = 0.02590 0.00651 -0.00039 0.00369 O5 5 0.309987 0.159369 0.400571 11.00000 0.03484 0.03407 = 0.02449 0.00499 -0.00032 0.01775 O6 5 0.388339 0.075488 0.310036 11.00000 0.02940 0.03961 = 0.02608 0.00590 0.00255 0.01580 O7 5 0.331598 0.128037 0.155241 11.00000 0.04521 0.02719 = 0.04905 0.00583 0.02696 0.00454 O8 5 0.248165 -0.016426 0.161755 11.00000 0.04581 0.02625 = 0.04001 0.00192 0.02426 0.00256 C28 1 -0.043616 0.290893 0.305640 11.00000 0.03047 0.02780 = 0.03429 0.00294 0.00144 0.01269 AFIX 23 H28A 2 -0.116916 0.250330 0.287444 11.00000 -1.20000 H28B 2 -0.063655 0.344207 0.339011 11.00000 -1.20000 AFIX 0 C29 1 0.015321 0.327752 0.247350 11.00000 0.03763 0.02411 = 0.03510 0.00584 -0.00212 0.01101 AFIX 23 H29A 2 0.070930 0.384193 0.266302 11.00000 -1.20000 H29B 2 -0.044441 0.345927 0.217490 11.00000 -1.20000 AFIX 0 C30 1 0.217982 0.379493 0.395806 11.00000 0.05028 0.03295 = 0.03878 -0.00428 0.00437 -0.00979 AFIX 137 H30A 2 0.179662 0.416817 0.368125 11.00000 -1.50000 H30B 2 0.271361 0.343888 0.368513 11.00000 -1.50000 H30C 2 0.261796 0.420941 0.435032 11.00000 -1.50000 AFIX 0 C31 1 0.126314 0.312279 0.420327 11.00000 0.03267 0.02833 = 0.02864 -0.00018 0.00410 0.00513 AFIX 13 H31 2 0.168658 0.277501 0.449700 11.00000 -1.20000 AFIX 0 C32 1 0.044852 0.367151 0.465439 11.00000 0.04484 0.04572 = 0.04312 -0.01637 0.00673 0.00733 AFIX 137 H32A 2 0.090342 0.407379 0.504591 11.00000 -1.50000 H32B 2 -0.013225 0.323433 0.481260 11.00000 -1.50000 H32C 2 0.005418 0.405683 0.439272 11.00000 -1.50000 AFIX 0 C33 1 0.010049 0.104261 0.439551 11.00000 0.05343 0.04559 = 0.05081 0.02544 0.02061 0.01183 AFIX 137 H33A 2 -0.046603 0.066468 0.461253 11.00000 -1.50000 H33B 2 0.057972 0.150690 0.474430 11.00000 -1.50000 H33C 2 0.060016 0.063743 0.413456 11.00000 -1.50000 AFIX 0 C34 1 -0.054176 0.153915 0.392074 11.00000 0.03029 0.02714 = 0.04006 0.00650 0.01561 0.00736 AFIX 13 H34 2 -0.101613 0.197125 0.419953 11.00000 -1.20000 AFIX 0 C35 1 -0.136580 0.082571 0.341661 11.00000 0.03334 0.03556 = 0.06608 0.00716 0.01554 -0.00142 AFIX 137 H35A 2 -0.091374 0.042114 0.311767 11.00000 -1.50000 H35B 2 -0.183698 0.115002 0.314428 11.00000 -1.50000 H35C 2 -0.187769 0.044623 0.366303 11.00000 -1.50000 AFIX 0 C36 1 0.301573 0.361104 0.206182 11.00000 0.04647 0.04356 = 0.04892 0.01870 -0.00103 -0.01337 AFIX 137 H36A 2 0.359917 0.393492 0.182010 11.00000 -1.50000 H36B 2 0.337408 0.316143 0.227938 11.00000 -1.50000 H36C 2 0.271524 0.406713 0.240836 11.00000 -1.50000 AFIX 0 C37 1 0.201808 0.309707 0.156029 11.00000 0.03951 0.02999 = 0.03124 0.01124 0.00416 -0.00092 AFIX 13 H37 2 0.236195 0.264719 0.121319 11.00000 -1.20000 AFIX 0 C38 1 0.149460 0.378316 0.118399 11.00000 0.06190 0.04801 = 0.05301 0.03211 0.00202 0.00225 AFIX 137 H38A 2 0.105942 0.418609 0.149555 11.00000 -1.50000 H38B 2 0.096877 0.343398 0.080167 11.00000 -1.50000 H38C 2 0.212122 0.416769 0.101436 11.00000 -1.50000 AFIX 0 C39 1 -0.130545 0.146753 0.148254 11.00000 0.03239 0.04185 = 0.04305 0.00566 -0.00762 0.00307 AFIX 137 H39A 2 -0.182302 0.115973 0.108464 11.00000 -1.50000 H39B 2 -0.166522 0.197821 0.174275 11.00000 -1.50000 H39C 2 -0.117353 0.101389 0.176849 11.00000 -1.50000 AFIX 0 C40 1 -0.014377 0.185834 0.125148 11.00000 0.03553 0.03126 = 0.02877 0.00765 -0.00708 0.00528 AFIX 13 H40 2 -0.030402 0.236138 0.100130 11.00000 -1.20000 AFIX 0 C41 1 0.035099 0.111157 0.075033 11.00000 0.04454 0.04457 = 0.02916 -0.00203 -0.00557 0.00441 AFIX 137 H41A 2 0.047642 0.058696 0.096959 11.00000 -1.50000 H41B 2 0.109320 0.137882 0.060818 11.00000 -1.50000 H41C 2 -0.019977 0.089064 0.035224 11.00000 -1.50000 AFIX 0 C42 1 0.458706 0.172660 0.491010 11.00000 0.05928 0.04521 = 0.03904 -0.00314 -0.01496 0.02180 AFIX 137 H42A 2 0.491758 0.231916 0.479691 11.00000 -1.50000 H42B 2 0.521376 0.141965 0.507771 11.00000 -1.50000 H42C 2 0.403703 0.184654 0.526196 11.00000 -1.50000 AFIX 0 C43 1 0.395939 0.110146 0.428385 11.00000 0.03701 0.03258 = 0.02920 0.00698 -0.00326 0.01385 C44 1 0.329626 0.023367 0.446959 11.00000 0.04865 0.04553 = 0.04295 0.01961 0.00718 0.01208 AFIX 137 H44A 2 0.270136 0.041906 0.477972 11.00000 -1.50000 H44B 2 0.383949 -0.009579 0.469131 11.00000 -1.50000 H44C 2 0.292208 -0.017955 0.405702 11.00000 -1.50000 AFIX 0 C45 1 0.564896 0.166536 0.362183 11.00000 0.03660 0.04413 = 0.06220 0.01605 0.00106 0.00272 AFIX 137 H45A 2 0.598427 0.154001 0.318048 11.00000 -1.50000 H45B 2 0.626262 0.172724 0.398490 11.00000 -1.50000 H45C 2 0.529912 0.224603 0.366842 11.00000 -1.50000 AFIX 0 C46 1 0.471537 0.085944 0.367119 11.00000 0.02971 0.02820 = 0.03340 0.00542 -0.00275 0.00736 C47 1 0.525303 -0.003714 0.362510 11.00000 0.04074 0.03799 = 0.04626 0.00737 -0.00106 0.01898 AFIX 137 H47A 2 0.463584 -0.056360 0.359482 11.00000 -1.50000 H47B 2 0.577377 0.000434 0.403029 11.00000 -1.50000 H47C 2 0.569723 -0.013208 0.322038 11.00000 -1.50000 AFIX 0 C48 1 0.520779 0.084357 0.145962 11.00000 0.03923 0.05765 = 0.13092 0.00083 0.01262 0.00020 AFIX 137 H48A 2 0.550979 0.150730 0.151796 11.00000 -1.50000 H48B 2 0.571136 0.047108 0.117437 11.00000 -1.50000 H48C 2 0.519302 0.066250 0.190418 11.00000 -1.50000 AFIX 0 C49 1 0.398203 0.067280 0.112223 11.00000 0.04128 0.03312 = 0.03819 0.00817 0.02025 0.00982 C50 1 0.399072 0.098457 0.045074 11.00000 0.13730 0.06212 = 0.05199 0.02232 0.04755 0.02853 AFIX 137 H50A 2 0.319556 0.088746 0.024031 11.00000 -1.50000 H50B 2 0.448434 0.062048 0.015195 11.00000 -1.50000 H50C 2 0.429793 0.164868 0.052291 11.00000 -1.50000 AFIX 0 C51 1 0.409927 -0.098726 0.133489 11.00000 0.06657 0.05586 = 0.14107 0.05398 0.04372 0.02941 AFIX 137 H51A 2 0.437824 -0.076358 0.181179 11.00000 -1.50000 H51B 2 0.476586 -0.102272 0.105309 11.00000 -1.50000 H51C 2 0.365028 -0.160824 0.128153 11.00000 -1.50000 AFIX 0 C52 1 0.333563 -0.032173 0.111692 11.00000 0.03443 0.03228 = 0.03535 0.00053 0.01664 0.00654 C53 1 0.266015 -0.076257 0.045298 11.00000 0.07612 0.09349 = 0.04582 -0.02068 0.01940 -0.03122 AFIX 137 H53A 2 0.222215 -0.135928 0.049554 11.00000 -1.50000 H53B 2 0.320090 -0.087009 0.009456 11.00000 -1.50000 H53C 2 0.211846 -0.034481 0.033740 11.00000 -1.50000 AFIX 0 B3 3 0.298378 0.127152 0.330214 11.00000 0.02746 0.02668 = 0.02838 0.00666 0.00397 0.00783 B4 3 0.250634 0.077708 0.187304 11.00000 0.02662 0.03003 = 0.02215 0.00710 0.00420 0.00738 HKLF 4 REM test in P-1 REM R1 = 0.0191 for 12862 Fo > 4sig(Fo) and 0.0245 for all 14567 data REM 687 parameters refined using 0 restraints END WGHT 0.0198 1.5152 REM Highest difference peak 0.931, deepest hole -0.468, 1-sigma level 0.069 Q1 1 0.0947 0.1334 0.2920 11.00000 0.05 0.93 Q2 1 0.8979 0.6135 0.2825 11.00000 0.05 0.85 Q3 1 1.0195 0.6322 0.2222 11.00000 0.05 0.82 Q4 1 0.2196 0.1480 0.2338 11.00000 0.05 0.78 Q5 1 0.1563 0.0837 0.2689 11.00000 0.05 0.65 REM The information below was added by Olex2. REM REM R1 = 0.0191 for 12862 Fo > 4sig(Fo) and 0.0245 for all 53994 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.93, deepest hole -0.47 REM Mean Shift 0, Max Shift -0.004. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0245 REM R1_gt = 0.0191 REM wR_ref = 0.0440 REM GOOF = 1.014 REM Shift_max = -0.004 REM Shift_mean = 0 REM Reflections_all = 53994 REM Reflections_gt = 12862 REM Parameters = n/a REM Hole = -0.47 REM Peak = 0.93 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 0 0 0.81 0.08 -2 0 0 0.82 0.09 -2 0 0 0.99 0.14 2 0 0 0.97 0.07 -3 0 0 1.26 0.21 -3 0 0 1.48 0.11 -3 0 0 1.58 0.12 -3 0 0 1.32 0.14 3 0 0 1.41 0.14 3 0 0 1.47 0.09 -4 0 0 7.31 0.27 -4 0 0 6.96 0.31 -4 0 0 7.21 0.26 -4 0 0 6.65 0.4 4 0 0 7.43 0.22 4 0 0 6.98 0.23 4 0 0 7.14 0.31 -5 0 0 5.54 0.26 -5 0 0 6.3 0.28 -5 0 0 5.59 0.31 -5 0 0 6.35 0.43 -5 0 0 5.98 0.31 5 0 0 5.77 0.2 5 0 0 5.91 0.21 5 0 0 5.6 0.31 -6 0 0 75.29 1.77 -6 0 0 71.68 1.71 -6 0 0 73.89 1.68 -6 0 0 73.48 2.11 -6 0 0 71.41 2.11 -6 0 0 70.46 1.86 6 0 0 72.14 1.59 6 0 0 73.67 1.6 6 0 0 72.59 1.86 -7 0 0 14.04 0.53 -7 0 0 15.35 0.61 -7 0 0 14.08 0.77 -7 0 0 14.32 0.53 -7 0 0 14.04 0.76 7 0 0 15.24 0.61 -8 0 0 19.52 0.69 -8 0 0 19.21 0.67 -8 0 0 19.8 0.98 -8 0 0 19.04 0.57 -8 0 0 19.6 0.96 8 0 0 19.96 0.76 -9 0 0 81.65 2.64 -9 0 0 87.26 2.14 -9 0 0 85.92 2.1 -9 0 0 87.06 2.67 -9 0 0 85.1 1.92 -10 0 0 77.41 1.99 -10 0 0 78.9 2.57 -10 0 0 75.59 1.99 -10 0 0 74.09 2.52 -10 0 0 75.74 1.78 -11 0 0 37.09 1.2 -11 0 0 35.6 1.6 -11 0 0 35.78 1.61 -11 0 0 34.82 1.02 -11 0 0 34.29 1.17 -12 0 0 0.88 0.3 -12 0 0 0.83 0.32 -12 0 0 1.38 0.53 -12 0 0 0.81 0.43 -12 0 0 0.83 0.23 -13 0 0 0.13 0.27 -13 0 0 0.24 0.5 -13 0 0 0.25 0.24 -13 0 0 -0.14 0.29 -13 0 0 0.26 0.45 -14 0 0 3.81 0.46 -14 0 0 4.7 0.6 -14 0 0 4.73 0.56 -14 0 0 3.59 0.73 -14 1 0 10.62 0.72 -14 1 0 13.19 1.22 -14 1 0 7.43 0.95 -14 1 0 10.44 0.62 -14 1 0 10.5 0.76 -13 1 0 29.14 1.14 -13 1 0 26.34 1.5 -13 1 0 27.36 1.1 -13 1 0 28.88 1.58 -13 1 0 28.44 0.96 -12 1 0 6.63 0.45 -12 1 0 6.7 0.52 -12 1 0 6.5 0.85 -12 1 0 5.29 0.71 -12 1 0 7.76 0.58 -11 1 0 -0.05 0.32 -11 1 0 0.09 0.24 -11 1 0 0.02 0.4 -11 1 0 0.16 0.18 -11 1 0 -0.01 0.2 -10 1 0 -0.1 0.28 -10 1 0 -0.25 0.3 -10 1 0 -0.03 0.17 -10 1 0 0.21 0.22 -10 1 0 -0.34 0.14 -9 1 0 7.07 0.62 -9 1 0 7.2 0.42 -9 1 0 7.17 0.7 -9 1 0 6.97 0.45 -8 1 0 67.54 1.71 -8 1 0 71.45 2.18 -8 1 0 68.4 1.71 -8 1 0 67.39 2.17 7 -1 0 137.08 2.98 7 -1 0 136.95 2.98 -7 1 0 142.16 3.12 -7 1 0 139.42 3.09 -7 1 0 139.89 3.69 -7 1 0 135.4 3.7 6 -1 0 43.16 1 6 -1 0 42.57 0.99 -6 1 0 44.72 1.14 -6 1 0 42.95 1.09 -6 1 0 40.49 1.4 -6 1 0 42.81 1.4 -6 1 0 42.38 1.09 5 -1 0 1.89 0.15 5 -1 0 1.68 0.13 -5 1 0 1.46 0.18 -5 1 0 1.88 0.17 -5 1 0 1.74 0.26 -5 1 0 1.44 0.19 -5 1 0 1.36 0.25 4 -1 0 3.5 0.16 -4 1 0 3.56 0.2 -4 1 0 3.26 0.19 -4 1 0 3.68 0.31 -4 1 0 3.81 0.19 -4 1 0 3.52 0.28 3 -1 0 0.16 0.06 -3 1 0 0.41 0.09 -3 1 0 0.64 0.1 -3 1 0 0.34 0.14 -3 1 0 0.72 0.13 -3 1 0 0.47 0.09 2 -1 0 139.76 2.92 2 -1 0 134.35 3.07 -2 1 0 135.73 3.22 -2 1 0 137.02 2.89 -2 1 0 134.51 2.85 -2 1 0 132.62 3.24 -1 1 0 37.43 0.95 -1 1 0 38.24 0.85 -1 1 0 38.78 0.96 -1 -1 0 283.41 6.26 -1 -1 0 277.27 6.85 1 1 0 282.34 6.26 -2 -1 0 108.03 2.48 -2 -1 0 105.68 2.25 -2 -1 0 105.03 2.59 -2 -1 0 106.84 2.33 2 1 0 111.63 2.33 2 1 0 104.1 2.47 -3 -1 0 297.21 6.27 -3 -1 0 294.19 6.12 -3 -1 0 297.27 6.65 3 1 0 294.26 6.64 3 1 0 298.76 6.31 -4 -1 0 185.22 3.87 -4 -1 0 172.04 4.37 -4 -1 0 176.8 4.13 -4 -1 0 174.49 3.75 -4 -1 0 182.7 3.87 4 1 0 183.43 3.83 4 1 0 178.58 4.13 4 1 0 179.11 3.83 -5 -1 0 1.28 0.18 -5 -1 0 1.07 0.13 -5 -1 0 1.11 0.12 -5 -1 0 1.67 0.27 -5 -1 0 1.36 0.18 -5 -1 0 1.38 0.2 5 1 0 1.14 0.1 5 1 0 1.37 0.21 5 1 0 1.22 0.1 -6 -1 0 4.22 0.3 -6 -1 0 4 0.27 -6 -1 0 4.08 0.2 -6 -1 0 4.45 0.45 -6 -1 0 4.14 0.31 -6 -1 0 4.3 0.26 6 1 0 4.49 0.33 6 1 0 4.6 0.15 -7 -1 0 9.69 0.64 -7 -1 0 9.36 0.51 -7 -1 0 10.02 0.35 -7 -1 0 10.25 0.43 -7 -1 0 10.22 0.45 7 1 0 10.11 0.51 -8 -1 0 4.6 0.34 -8 -1 0 4.38 0.52 -8 -1 0 4.15 0.26 -8 -1 0 4.09 0.39 -8 -1 0 4.67 0.36 8 1 0 4.51 0.39 -9 -1 0 2.02 0.42 -9 -1 0 2.39 0.31 -9 -1 0 1.84 0.45 -9 -1 0 2.67 0.32 -9 -1 0 2.15 0.25 -10 -1 0 0.6 0.23 -10 -1 0 0.57 0.23 -10 -1 0 0.55 0.18 -10 -1 0 0.82 0.4 -10 -1 0 0.66 0.35 -11 -1 0 14.3 1.04 -11 -1 0 14.54 0.59 -11 -1 0 11.25 0.91 -11 -1 0 14.09 0.71 -11 -1 0 14.92 0.72 -12 -1 0 30.87 1.59 -12 -1 0 31.93 1.02 -12 -1 0 33.08 1.18 -12 -1 0 33.72 1.2 -12 -1 0 32.06 1.61 -13 -1 0 13.7 1.11 -13 -1 0 12.05 1.04 -13 -1 0 12.77 0.66 -13 -1 0 11.57 0.76 -13 -1 0 12.19 0.76 -14 -1 0 0.31 0.36 -14 -1 0 -0.13 0.3 -14 -1 0 -0.17 0.46 -14 -1 0 0.08 0.28 -14 2 0 16.44 0.92 -14 2 0 15.14 0.73 -14 2 0 17.33 1.34 -14 2 0 16.26 0.88 -14 2 0 14.81 1.17 -13 2 0 2.66 0.68 -13 2 0 2.34 0.38 -13 2 0 2.25 0.32 -13 2 0 2.42 0.42 -13 2 0 2.79 0.6 -12 2 0 6.41 0.51 -12 2 0 5.99 0.84 -12 2 0 6.87 0.45 -12 2 0 4.59 0.68 -12 2 0 6.48 0.56 -11 2 0 23.44 1.26 -11 2 0 20.84 0.84 -11 2 0 20.68 1.17 -11 2 0 21.68 0.73 -11 2 0 20.49 0.87 -10 2 0 17.67 0.75 -10 2 0 16.55 1.02 -10 2 0 18.53 1.03 -10 2 0 17.92 0.72 -9 2 0 1.92 0.43 -9 2 0 1.7 0.24 -9 2 0 2.03 0.4 -9 2 0 2.32 0.32 8 -2 0 1.57 0.13 8 -2 0 2.15 0.26 -8 2 0 2.32 0.27 -8 2 0 1.75 0.24 -8 2 0 1.89 0.36 -8 2 0 1.65 0.4 7 -2 0 10.66 0.34 7 -2 0 10.62 0.36 7 -2 0 10.93 0.45 -7 2 0 9.85 0.45 -7 2 0 10.75 0.45 -7 2 0 11.69 0.65 -7 2 0 12.1 0.7 6 -2 0 76.83 1.75 6 -2 0 77.34 1.86 6 -2 0 76.77 1.71 -6 2 0 73.08 2.18 -6 2 0 74.32 2.14 -6 2 0 77.6 1.79 -6 2 0 74.83 1.78 5 -2 0 209.45 4.46 5 -2 0 201.01 4.64 5 -2 0 210.85 4.43 -5 2 0 202.97 5.06 -5 2 0 204.86 5.01 -5 2 0 204.08 4.43 -5 2 0 204.06 4.37 4 -2 0 68.43 1.65 4 -2 0 72.39 1.6 -4 2 0 71.05 1.88 -4 2 0 69.29 1.91 -4 2 0 69.69 1.61 -4 2 0 72.88 1.6 3 -2 0 17.01 0.45 3 -2 0 16.44 0.43 -3 2 0 17.26 0.47 -3 2 0 16.72 0.46 -3 2 0 16.53 0.58 -3 2 0 16.12 0.61 2 -2 0 21.74 0.55 -2 2 0 21.12 0.66 -2 2 0 22.37 0.65 -2 2 0 22.51 0.56 -2 2 0 21.83 0.54 1 -2 0 19.97 0.5 -1 2 0 21.53 0.58 -1 2 0 20.38 0.51 -1 2 0 20.51 0.5 0 -2 0 13.03 0.38 0 2 0 12.9 0.39 0 2 0 12.49 0.37 0 2 0 13.4 0.42 -1 -2 0 553.99 11.5 -1 -2 0 552.29 12.33 -1 -2 0 554.86 13.64 1 2 0 556.26 12.33 1 2 0 580.73 13.57 1 2 0 554.35 11.97 -2 -2 0 22.15 0.53 -2 -2 0 22 0.67 -2 -2 0 21.46 0.64 2 2 0 21.81 0.64 2 2 0 21.82 0.58 -3 -2 0 52.3 1.17 -3 -2 0 50.81 1.36 -3 -2 0 53.46 1.13 -3 -2 0 51 1.44 3 2 0 55.17 1.22 3 2 0 52.76 1.36 -4 -2 0 287.8 6.56 -4 -2 0 282.89 6.17 -4 -2 0 287.59 5.83 -4 -2 0 284.38 5.99 -4 -2 0 279.21 6.86 4 2 0 290.63 6.56 4 2 0 298.9 6.14 4 2 0 297.14 6.16 -5 -2 0 243.74 6.11 -5 -2 0 260 5.43 -5 -2 0 245.11 5.27 -5 -2 0 246.7 5.45 -5 -2 0 251.12 5.8 -5 -2 0 251.84 5.11 5 2 0 256.81 5.37 5 2 0 256.47 5.36 5 2 0 252.94 5.81 -6 -2 0 86.51 2.5 -6 -2 0 89.46 2.13 -6 -2 0 88.86 1.91 -6 -2 0 95.77 2.13 -6 -2 0 87.74 2 -6 -2 0 86.71 2.3 6 2 0 88.03 1.94 6 2 0 91.14 2.31 -7 -2 0 7.04 0.41 -7 -2 0 6.8 0.3 -7 -2 0 7.98 0.62 -7 -2 0 6.27 0.43 -7 -2 0 6.34 0.34 7 2 0 7.42 0.47 -8 -2 0 -0.03 0.11 -8 -2 0 -0.09 0.19 -8 -2 0 0.13 0.16 -8 -2 0 0.13 0.29 -8 -2 0 0.22 0.17 -9 -2 0 4.15 0.39 -9 -2 0 3.27 0.51 -9 -2 0 3.51 0.44 -9 -2 0 4.04 0.37 -9 -2 0 3.85 0.31 -10 -2 0 29.46 1.04 -10 -2 0 29.28 0.87 -10 -2 0 27.83 0.97 -10 -2 0 29.68 1.41 -10 -2 0 29.59 1.38 -11 -2 0 24.25 1.34 -11 -2 0 25.35 0.83 -11 -2 0 25.07 0.94 -11 -2 0 24.01 0.97 -11 -2 0 22.44 1.29 -12 -2 0 5.7 0.78 -12 -2 0 5.86 0.55 -12 -2 0 5.21 0.72 -12 -2 0 5.67 0.53 -12 -2 0 5.89 0.46 -13 -2 0 11.95 0.66 -13 -2 0 11.67 1.03 -13 -2 0 12.36 0.76 -13 -2 0 9.92 0.72 -13 -2 0 11.55 1.06 -14 -2 0 25.1 1.12 -14 -2 0 26.76 1.6 -14 -2 0 23.84 0.99 14 2 0 25.64 1.44 -14 3 0 6.81 0.89 -14 3 0 5.37 0.49 -14 3 0 4.79 0.55 -14 3 0 5.51 0.88 -14 3 0 4.9 0.62 -13 3 0 34.25 1.71 -13 3 0 35.42 1.12 -13 3 0 36.88 1.79 -13 3 0 36.73 1.32 -13 3 0 36.12 1.28 -12 3 0 62.04 1.81 -12 3 0 63.41 2.33 -12 3 0 62.21 1.78 -12 3 0 59.6 2.32 -12 3 0 60.35 1.59 -11 3 0 11.24 0.66 -11 3 0 12.25 0.63 -11 3 0 11.66 0.54 -11 3 0 12.17 0.89 -11 3 0 11.94 0.93 -10 3 0 1.17 0.25 -10 3 0 0.81 0.26 -10 3 0 1.09 0.38 -10 3 0 1.82 0.49 9 -3 0 45.76 1.04 -9 3 0 47.91 1.69 -9 3 0 47.63 1.33 -9 3 0 44.33 1.29 -9 3 0 44.87 1.7 8 -3 0 73.93 1.68 8 -3 0 70.92 1.64 -8 3 0 72.57 1.81 -8 3 0 74.03 2.29 -8 3 0 70.93 1.8 -8 3 0 72.4 2.22 7 -3 0 0.42 0.13 7 -3 0 0.2 0.1 7 -3 0 0.27 0.12 -7 3 0 0.25 0.14 -7 3 0 0.3 0.26 -7 3 0 0.08 0.14 -7 3 0 0.3 0.21 6 -3 0 5.11 0.25 6 -3 0 5.36 0.29 6 -3 0 5.6 0.26 -6 3 0 6.2 0.48 -6 3 0 5.68 0.31 -6 3 0 5.32 0.3 -6 3 0 5.05 0.41 5 -3 0 0.25 0.09 5 -3 0 0.24 0.08 -5 3 0 0.36 0.11 -5 3 0 0.31 0.11 -5 3 0 0.58 0.2 -5 3 0 0.24 0.16 -5 3 0 0.52 0.12 4 -3 0 99.03 2.18 4 -3 0 95.87 2.22 -4 3 0 96.75 2.19 -4 3 0 98.76 2.16 -4 3 0 96.17 2.5 -4 3 0 97.8 2.53 3 -3 0 322.8 6.87 -3 3 0 321.96 6.69 -3 3 0 321.06 7.52 -3 3 0 319.09 7.54 -3 3 0 323.71 6.81 2 -3 0 35.63 0.86 2 -3 0 36.98 0.89 -2 3 0 36.68 1.01 -2 3 0 36.03 0.86 -2 3 0 36.53 1.01 -2 3 0 35.24 0.88 1 -3 0 48.8 1.16 1 -3 0 50.34 1.16 -1 3 0 49.6 1.28 -1 3 0 49 1.25 -1 3 0 49.48 1.16 -1 3 0 49.09 1.12 0 -3 0 49.96 1.22 0 -3 0 50.67 1.13 0 3 0 50.63 1.31 0 3 0 49.46 1.17 0 3 0 51.1 1.22 0 3 0 49.58 1.27 -1 -3 0 27.53 0.81 -1 -3 0 28.27 0.77 -1 -3 0 28.51 0.68 1 3 0 27.6 0.77 1 3 0 28.28 0.87 1 3 0 28.27 0.81 1 3 0 27.4 0.71 -2 -3 0 14.47 0.53 -2 -3 0 14.62 0.42 -2 -3 0 15.13 0.53 -2 -3 0 14.31 0.43 2 3 0 14.29 0.51 2 3 0 15.51 0.54 2 3 0 16.2 0.63 2 3 0 15.77 0.48 2 3 0 15.22 0.51 -3 -3 0 83.86 2.18 -3 -3 0 79.69 2.03 -3 -3 0 80.53 1.77 -3 -3 0 82.47 1.79 3 3 0 79.93 1.88 3 3 0 83.78 2.04 -4 -3 0 81.87 2.22 -4 -3 0 83.25 1.79 -4 -3 0 79.81 2.1 -4 -3 0 81.2 2.24 -4 -3 0 82.72 1.84 4 3 0 83.42 2.11 4 3 0 85.64 1.85 4 3 0 85.16 1.89 -5 -3 0 0.4 0.13 -5 -3 0 0.51 0.21 -5 -3 0 0.44 0.1 -5 -3 0 0.66 0.12 -5 -3 0 0.68 0.19 5 3 0 0.59 0.09 5 3 0 0.22 0.15 5 3 0 0.44 0.08 -6 -3 0 142.6 3.12 -6 -3 0 137.14 3.39 -6 -3 0 134.49 2.89 -6 -3 0 132.53 3.6 -6 -3 0 134.26 2.99 6 3 0 139.66 2.96 6 3 0 135.97 2.95 6 3 0 137.78 3.4 -7 -3 0 148.01 3.66 -7 -3 0 144.44 3.91 -7 -3 0 146.29 3.12 -7 -3 0 146.32 3.23 -7 -3 0 147.93 3.4 -8 -3 0 53.24 1.38 -8 -3 0 53.99 1.31 -8 -3 0 55.04 1.65 -8 -3 0 51.68 1.83 -8 -3 0 54.09 1.51 -9 -3 0 13.09 0.87 -9 -3 0 13.54 0.53 -9 -3 0 12.87 0.59 -9 -3 0 13.54 0.67 -10 -3 0 1.44 0.28 -10 -3 0 2.45 0.31 -10 -3 0 1.77 0.47 -11 -3 0 4.44 0.46 -11 -3 0 4.64 0.69 -11 -3 0 4.53 0.4 -12 -3 0 7.85 0.85 -12 -3 0 8.24 0.88 -12 -3 0 8.69 0.56 -12 -3 0 7.88 0.59 -13 -3 0 14.43 1.2 -13 -3 0 15.02 0.83 -13 -3 0 12.38 1.11 -13 -3 0 14.34 0.74 13 3 0 13.22 1.08 -14 -3 0 6.61 0.68 -14 -3 0 5.31 0.59 14 3 0 5.81 0.83 -14 4 0 0.14 0.31 -14 4 0 0.61 0.37 -14 4 0 -0.24 0.51 -14 4 0 0.11 0.45 -14 4 0 0.1 0.25 -14 4 0 0.25 0.36 -13 4 0 0.23 0.48 -13 4 0 0.21 0.39 -13 4 0 0.13 0.27 -13 4 0 -0.11 0.23 -13 4 0 -0.27 0.3 -13 4 0 0.12 0.3 -12 4 0 16.47 0.69 -12 4 0 17.39 1.2 -12 4 0 16.54 0.79 -12 4 0 16.58 0.83 -12 4 0 16.96 0.82 -12 4 0 17.69 1.11 -11 4 0 69.24 1.89 -11 4 0 68.38 1.89 -11 4 0 68.17 2.44 -11 4 0 69.21 2.39 -11 4 0 68.18 1.9 -10 4 0 84.2 2.15 -10 4 0 82.18 2.64 -10 4 0 80.5 2.67 -10 4 0 83.44 2.15 -10 4 0 86.71 2.17 9 -4 0 47.47 1.14 -9 4 0 48.48 1.73 -9 4 0 49.32 1.36 -9 4 0 47.97 1.36 -9 4 0 46.18 1.34 -9 4 0 47.21 1.76 8 -4 0 2 0.2 -8 4 0 1.77 0.35 -8 4 0 2.39 0.29 -8 4 0 1.69 0.23 -8 4 0 2.25 0.41 -8 4 0 2.09 0.26 7 -4 0 51.48 1.3 7 -4 0 52.17 1.28 -7 4 0 51.3 1.35 -7 4 0 53.32 1.74 -7 4 0 54.3 1.37 -7 4 0 50.62 1.66 -7 4 0 53.02 1.37 6 -4 0 22.6 0.65 6 -4 0 23.15 0.61 -6 4 0 21.84 0.7 -6 4 0 22.41 0.92 -6 4 0 22.69 0.9 -6 4 0 22.63 0.7 5 -4 0 6.28 0.3 5 -4 0 6.52 0.21 -5 4 0 6.09 0.32 -5 4 0 6.52 0.33 -5 4 0 5.45 0.4 -5 4 0 5.62 0.43 4 -4 0 2 0.18 -4 4 0 1.51 0.19 -4 4 0 1.52 0.18 -4 4 0 1.55 0.23 -4 4 0 1.63 0.23 3 -4 0 0.87 0.11 -3 4 0 0.81 0.15 -3 4 0 0.66 0.11 -3 4 0 0.78 0.12 -3 4 0 0.58 0.15 2 -4 0 16.16 0.44 2 -4 0 17.14 0.51 2 -4 0 16.75 0.5 -2 4 0 16.67 0.44 -2 4 0 18.98 0.61 -2 4 0 16.96 0.51 -2 4 0 15.93 0.48 -2 4 0 16.69 0.57 1 -4 0 340.83 7.33 1 -4 0 345.39 7.62 1 -4 0 342.18 7.12 -1 4 0 341.81 7.97 -1 4 0 333.58 7.93 -1 4 0 346.72 7.12 -1 4 0 348.11 7.33 -1 4 0 343.9 7.61 0 -4 0 446.64 9.93 0 -4 0 454.74 9.24 0 4 0 461.02 10.8 0 4 0 446.47 9.92 0 4 0 441.65 9.51 0 4 0 438.38 10.3 0 4 0 442.26 10.35 -1 -4 0 13.98 0.43 -1 -4 0 13.65 0.52 -1 -4 0 15.32 0.51 1 4 0 14.62 0.46 1 4 0 15.95 0.5 1 4 0 15.55 0.53 1 4 0 14.44 0.5 1 4 0 14.47 0.59 -2 -4 0 6.22 0.33 -2 -4 0 5.88 0.26 -2 -4 0 6.52 0.32 2 4 0 5.97 0.32 2 4 0 5.57 0.31 2 4 0 6.41 0.29 2 4 0 5.78 0.4 -3 -4 0 1.68 0.19 -3 -4 0 1.92 0.18 -3 -4 0 2.01 0.22 -3 -4 0 1.9 0.22 3 4 0 2.51 0.22 3 4 0 2.41 0.24 3 4 0 2.15 0.28 -4 -4 0 2.33 0.26 -4 -4 0 2.48 0.27 -4 -4 0 2.58 0.23 -4 -4 0 2.79 0.22 -4 -4 0 2.32 0.31 4 4 0 2.58 0.3 4 4 0 2.35 0.26 4 4 0 2.01 0.21 4 4 0 2.68 0.18 -5 -4 0 60.02 1.44 -5 -4 0 60.76 1.43 -5 -4 0 60.07 1.71 -5 -4 0 61.32 1.81 -5 -4 0 57.9 1.77 5 4 0 61.68 1.4 5 4 0 60.69 1.71 5 4 0 62.62 1.45 -6 -4 0 52.75 1.66 -6 -4 0 55.92 1.62 -6 -4 0 52.81 1.33 -6 -4 0 53.29 1.31 -6 -4 0 56.13 1.75 6 4 0 55.3 1.26 6 4 0 53.93 1.24 -7 -4 0 3.67 0.3 -7 -4 0 3.08 0.45 -7 -4 0 3.93 0.38 -7 -4 0 4.33 0.42 -7 -4 0 3.4 0.3 -8 -4 0 12.28 0.68 -8 -4 0 13.69 0.85 -8 -4 0 12.06 0.5 -8 -4 0 11.44 0.52 -9 -4 0 68.83 1.76 -9 -4 0 67.22 2.16 -9 -4 0 69.65 2.32 -9 -4 0 67.38 1.68 -10 -4 0 51.21 1.46 -10 -4 0 51.1 1.39 -10 -4 0 51.48 1.97 -11 -4 0 12.02 0.62 -11 -4 0 10.51 0.63 -11 -4 0 11.53 0.95 11 4 0 12.04 0.93 -12 -4 0 0.69 0.29 -12 -4 0 0.37 0.51 -12 -4 0 0.32 0.3 12 4 0 0.65 0.47 -13 -4 0 0.7 0.33 -13 -4 0 0.65 0.47 -13 -4 0 1.08 0.39 -13 -4 0 1.2 0.58 13 4 0 1.19 0.56 -14 5 0 11.66 0.68 -14 5 0 14.61 1.21 -14 5 0 10.77 1.02 -14 5 0 13.53 0.8 -14 5 0 13.75 0.86 -13 5 0 6.49 0.62 -13 5 0 6.88 0.57 -13 5 0 6.21 0.78 -13 5 0 5.24 0.46 -13 5 0 6.7 0.92 -12 5 0 0.09 0.45 -12 5 0 0.76 0.4 -12 5 0 0.26 0.29 -12 5 0 -0.1 0.22 -11 5 0 0.36 0.23 -11 5 0 0.26 0.34 -11 5 0 0.16 0.39 -11 5 0 0.49 0.27 10 -5 0 6.45 0.29 -10 5 0 6.64 0.68 -10 5 0 6.67 0.69 -10 5 0 6.32 0.44 -10 5 0 6.35 0.49 9 -5 0 30.2 0.83 -9 5 0 31.38 1 -9 5 0 30.26 1.01 -9 5 0 31.22 1.3 -9 5 0 30 1.31 8 -5 0 177.24 3.95 -8 5 0 178.46 4.05 -8 5 0 180.26 4.68 -8 5 0 179.47 4.71 -8 5 0 177.97 4 7 -5 0 186.42 4.07 -7 5 0 183.36 4.12 -7 5 0 180.72 4.69 -7 5 0 181.66 4.05 -7 5 0 185.59 4.73 6 -5 0 21.45 0.64 -6 5 0 19.24 0.67 -6 5 0 20.32 0.86 -6 5 0 20.22 0.89 -6 5 0 20.12 0.67 5 -5 0 3.69 0.25 -5 5 0 3.32 0.26 -5 5 0 3.56 0.39 -5 5 0 3.4 0.27 -5 5 0 3.27 0.33 4 -5 0 91.33 2.11 -4 5 0 89.85 2.11 -4 5 0 92.7 2.39 -4 5 0 92.65 2.08 -4 5 0 86.87 2.39 3 -5 0 37.61 0.99 3 -5 0 37.87 0.9 -3 5 0 36.71 0.99 -3 5 0 37.62 0.97 -3 5 0 37.04 1.14 -3 5 0 36.93 1.12 2 -5 0 54.04 1.3 2 -5 0 54.81 1.33 2 -5 0 55.46 1.33 -2 5 0 53.67 1.29 -2 5 0 56 1.3 -2 5 0 52.06 1.49 -2 5 0 53.31 1.46 -2 5 0 54.8 1.34 -2 5 0 53.65 1.32 1 -5 0 0.44 0.1 1 -5 0 0.39 0.1 1 -5 0 0.56 0.11 -1 5 0 0.23 0.12 -1 5 0 0.27 0.12 -1 5 0 0.33 0.1 -1 5 0 0.28 0.09 -1 5 0 0.2 0.09 -1 5 0 0.32 0.1 0 -5 0 21.52 0.67 0 -5 0 22.64 0.65 0 -5 0 23.35 0.64 0 5 0 22.46 0.71 0 5 0 21.97 0.65 0 5 0 21.93 0.74 0 5 0 22.72 0.79 0 5 0 21.96 0.67 0 5 0 23.06 0.65 0 5 0 22.6 0.65 -1 -5 0 223.76 4.64 -1 -5 0 214.55 5.02 1 5 0 210.16 5.02 1 5 0 220.47 5.32 1 5 0 222.36 4.92 1 5 0 223.84 4.79 -2 -5 0 133.81 3.26 -2 -5 0 135.65 2.96 -2 -5 0 135.49 3.5 2 5 0 138.38 3.19 2 5 0 137.76 3.07 2 5 0 136.88 3.27 -3 -5 0 51.89 1.49 -3 -5 0 54.9 1.29 -3 -5 0 54.77 1.3 -3 -5 0 52.69 1.56 3 5 0 55.89 1.38 3 5 0 52.65 1.44 3 5 0 52.83 1.36 3 5 0 52.58 1.49 -4 -5 0 5.53 0.39 -4 -5 0 6.22 0.34 -4 -5 0 5.95 0.31 -4 -5 0 5.56 0.39 4 5 0 6.49 0.44 4 5 0 6.76 0.36 4 5 0 5.85 0.4 -5 -5 0 23.4 0.72 -5 -5 0 21.88 0.86 -5 -5 0 22.03 0.68 -5 -5 0 22 0.93 -5 -5 0 22.1 0.86 5 5 0 22.27 0.69 5 5 0 23.49 0.64 5 5 0 23.15 0.86 -6 -5 0 4.18 0.39 -6 -5 0 4.13 0.33 -6 -5 0 3.76 0.41 -6 -5 0 4.4 0.31 -6 -5 0 3.63 0.45 6 5 0 3.63 0.42 6 5 0 3.95 0.22 6 5 0 3.74 0.25 -7 -5 0 19.12 0.86 -7 -5 0 20.03 0.96 -7 -5 0 17.6 0.65 -7 -5 0 18 0.66 7 5 0 19.59 0.5 7 5 0 18.34 0.86 7 5 0 18.09 0.48 -8 -5 0 37.13 1.09 -8 -5 0 38.6 1.51 -8 -5 0 39.25 1.11 -8 -5 0 36.32 1.37 8 5 0 37.65 1.37 -9 -5 0 15.49 0.68 -9 -5 0 15.7 0.85 -9 -5 0 16.57 0.99 -9 -5 0 16.25 0.68 9 5 0 18.1 0.97 -10 -5 0 3.63 0.43 -10 -5 0 3.01 0.4 -10 -5 0 3.54 0.59 10 5 0 3.55 0.55 -11 -5 0 18.03 0.79 -11 -5 0 18.04 0.81 -11 -5 0 16.02 1.12 11 5 0 16.91 1.08 -12 -5 0 30.1 1.15 -12 -5 0 31.25 1.61 -12 -5 0 30.52 1.11 12 5 0 30.4 1.45 -13 -5 0 13.72 0.82 -13 -5 0 14.39 0.83 13 5 0 16.33 1.18 -14 6 0 7.96 0.91 -14 6 0 7.33 0.57 -14 6 0 7.19 0.63 -14 6 0 8.15 0.99 -14 6 0 6.75 0.66 -13 6 0 0.13 0.49 -13 6 0 0.32 0.44 -13 6 0 -0.24 0.22 -13 6 0 0.4 0.32 -13 6 0 0.33 0.3 -12 6 0 5.73 0.81 -12 6 0 5 0.55 -12 6 0 6.79 0.74 -12 6 0 5.57 0.51 11 -6 0 9.42 0.33 -11 6 0 10.11 0.62 -11 6 0 8.96 0.78 -11 6 0 8.39 0.55 -11 6 0 10.82 0.91 10 -6 0 0.21 0.14 -10 6 0 0.4 0.31 -10 6 0 0.11 0.37 -10 6 0 0.38 0.23 -10 6 0 0.47 0.22 9 -6 0 1.04 0.18 -9 6 0 1 0.23 -9 6 0 1.38 0.26 -9 6 0 0.62 0.34 -9 6 0 1.42 0.36 8 -6 0 0.22 0.14 -8 6 0 0.04 0.23 -8 6 0 0.25 0.18 -8 6 0 -0.17 0.25 -8 6 0 0.2 0.2 7 -6 0 52.42 1.38 -7 6 0 55.19 1.47 -7 6 0 53.01 1.44 -7 6 0 58.28 1.8 -7 6 0 54.37 1.75 6 -6 0 246.71 5.37 -6 6 0 242.41 5.28 -6 6 0 247.29 6.03 -6 6 0 241.16 6.02 -6 6 0 243.33 5.37 5 -6 0 219.09 4.85 -5 6 0 214.78 5.39 -5 6 0 216.47 4.74 -5 6 0 227.43 5.4 -5 6 0 219.62 4.84 4 -6 0 85.47 2.03 -4 6 0 85.08 2 -4 6 0 87.08 2.06 -4 6 0 86.66 2.29 -4 6 0 83.89 2.03 -4 6 0 83.62 2.31 3 -6 0 6.88 0.35 3 -6 0 7.01 0.26 3 -6 0 6.65 0.35 -3 6 0 6.57 0.36 -3 6 0 7.19 0.43 -3 6 0 6.47 0.33 -3 6 0 7.01 0.36 -3 6 0 7.22 0.43 2 -6 0 0.65 0.13 2 -6 0 0.83 0.15 2 -6 0 0.92 0.15 2 -6 0 0.76 0.12 -2 6 0 0.84 0.14 -2 6 0 0.92 0.14 -2 6 0 0.74 0.18 -2 6 0 0.9 0.15 -2 6 0 1.1 0.18 1 -6 0 1.49 0.2 1 -6 0 1.93 0.19 1 -6 0 1.45 0.21 -1 6 0 1.79 0.21 -1 6 0 1.8 0.21 -1 6 0 1.67 0.22 -1 6 0 1.5 0.24 -1 6 0 1.78 0.25 -1 6 0 2.38 0.23 -1 6 0 1.58 0.19 0 -6 0 6.04 0.33 0 -6 0 5.84 0.31 0 -6 0 6.33 0.32 0 6 0 5.9 0.32 0 6 0 5.67 0.32 0 6 0 5.47 0.38 0 6 0 5.73 0.31 0 6 0 5.99 0.33 0 6 0 5.93 0.36 -1 -6 0 5.48 0.34 -1 -6 0 5.86 0.31 1 6 0 5.64 0.42 1 6 0 5.35 0.33 1 6 0 5.35 0.34 1 6 0 5.72 0.3 -2 -6 0 24.53 0.84 -2 -6 0 24.07 0.87 -2 -6 0 24.48 0.72 2 6 0 25.18 0.82 2 6 0 28.07 1.04 2 6 0 25.02 0.76 2 6 0 25.53 0.85 -3 -6 0 149.63 3.87 -3 -6 0 148.05 3.26 -3 -6 0 146.12 3.63 3 6 0 147.36 3.63 3 6 0 148.03 3.53 3 6 0 151.68 3.4 3 6 0 150.43 3.94 -4 -6 0 158.53 3.44 -4 -6 0 157.41 4.13 -4 -6 0 161.4 3.48 -4 -6 0 156.12 3.88 4 6 0 160.63 3.8 4 6 0 154.82 3.61 -5 -6 0 103.17 2.83 -5 -6 0 99.14 2.35 -5 -6 0 101.14 2.36 -5 -6 0 106.54 2.73 -5 -6 0 102.72 2.84 5 6 0 100.88 2.43 5 6 0 102.07 2.64 -6 -6 0 3.95 0.32 -6 -6 0 4.73 0.52 -6 -6 0 4.78 0.36 -6 -6 0 4.34 0.41 6 6 0 4.73 0.3 6 6 0 4.42 0.46 -7 -6 0 0.72 0.2 -7 -6 0 0.68 0.21 -7 -6 0 0.67 0.26 -7 -6 0 0.74 0.33 7 6 0 1 0.32 7 6 0 1.12 0.14 -8 -6 0 6.09 0.53 -8 -6 0 6.2 0.44 -8 -6 0 5.27 0.43 -8 -6 0 6.14 0.63 8 6 0 5.97 0.58 -9 -6 0 7.68 0.51 -9 -6 0 8.48 0.76 -9 -6 0 7.53 0.51 9 6 0 7.58 0.72 -10 -6 0 31.63 1.1 -10 -6 0 34.02 1.12 -10 -6 0 32.71 1.53 10 6 0 32.33 1.42 -11 -6 0 19.66 1.25 -11 -6 0 21.05 0.91 -11 -6 0 20.64 0.89 11 6 0 20.48 1.15 -12 -6 0 0 0.3 -12 -6 0 0.98 0.34 -12 -6 0 0.04 0.52 12 6 0 0.93 0.55 -13 -6 0 12.06 0.78 -13 -6 0 12.55 0.81 13 6 0 10.91 1.06 -14 7 0 13.02 0.87 -14 7 0 12.94 1.14 -14 7 0 13.56 0.74 -14 7 0 13.54 0.83 -14 7 0 14.46 1.2 -13 7 0 35.65 1.32 -13 7 0 34.25 1.7 -13 7 0 36.82 1.35 -13 7 0 34.3 1.74 -12 7 0 21.15 1.29 -12 7 0 21.11 0.92 -12 7 0 20.42 1.2 -12 7 0 18.81 0.9 11 -7 0 2.09 0.25 -11 7 0 1.84 0.53 -11 7 0 2.69 0.5 -11 7 0 2.06 0.36 -11 7 0 1.78 0.32 10 -7 0 9.76 0.45 -10 7 0 10.01 0.59 -10 7 0 9.92 0.59 -10 7 0 10.36 0.86 -10 7 0 10.04 0.78 9 -7 0 13.62 0.56 -9 7 0 14.37 0.67 -9 7 0 13.37 0.86 -9 7 0 14.58 0.67 -9 7 0 14.67 0.87 8 -7 0 4.39 0.32 -8 7 0 3.93 0.37 -8 7 0 4.4 0.57 -8 7 0 4.51 0.51 -8 7 0 4.27 0.39 7 -7 0 19.8 0.68 -7 7 0 19.21 0.72 -7 7 0 20 0.95 -7 7 0 20.97 0.76 -7 7 0 19.28 0.92 6 -7 0 16.18 0.59 -6 7 0 14.59 0.61 -6 7 0 15.07 0.77 -6 7 0 15.42 0.61 -6 7 0 15.11 0.75 5 -7 0 19.44 0.68 -5 7 0 18.68 0.68 -5 7 0 19.97 0.85 -5 7 0 19.85 0.83 -5 7 0 19.78 0.71 -5 7 0 20.79 0.73 4 -7 0 184.44 4.03 4 -7 0 178.69 4.05 4 -7 0 181.16 4.04 -4 7 0 178.7 4.03 -4 7 0 177.22 4.49 -4 7 0 179.39 4.07 -4 7 0 177.76 3.95 -4 7 0 180.01 4.45 3 -7 0 323.25 7.07 3 -7 0 323.38 7.23 3 -7 0 319.38 6.85 3 -7 0 333.8 7.02 -3 7 0 326 7.23 -3 7 0 325.71 7.68 -3 7 0 322.27 6.88 -3 7 0 322.75 7.08 -3 7 0 324.39 7.75 2 -7 0 261.52 5.7 2 -7 0 261.27 5.53 2 -7 0 260.28 5.66 2 -7 0 262.46 5.85 -2 7 0 257.09 6.17 -2 7 0 256.66 5.54 -2 7 0 257.89 5.71 -2 7 0 260.24 6.27 -2 7 0 256.38 5.84 1 -7 0 38.53 1.05 1 -7 0 36.94 1.01 1 -7 0 37.59 1.05 -1 7 0 37.09 1.04 -1 7 0 37.62 1.04 -1 7 0 37.29 1.13 -1 7 0 37.67 1.22 -1 7 0 35.92 1.03 -1 7 0 37.69 1.02 0 -7 0 1.19 0.19 0 -7 0 1.27 0.18 0 -7 0 1.51 0.21 0 7 0 1.33 0.2 0 7 0 1.66 0.25 0 7 0 1.3 0.25 0 7 0 1.37 0.21 0 7 0 1.13 0.17 0 7 0 1.41 0.19 0 7 0 1.31 0.19 -1 -7 0 9.62 0.43 -1 -7 0 10.01 0.44 -1 -7 0 9.65 0.48 1 7 0 9.57 0.47 1 7 0 9.58 0.43 1 7 0 9.17 0.42 1 7 0 9.37 0.46 1 7 0 9.41 0.58 -2 -7 0 31.79 1.09 -2 -7 0 30.62 1.03 -2 -7 0 32.71 0.91 2 7 0 32.44 1.04 2 7 0 32.07 1.21 2 7 0 31.49 0.99 2 7 0 31.63 0.93 -3 -7 0 23.68 0.89 -3 -7 0 24.42 0.91 -3 -7 0 23.87 0.75 3 7 0 24.72 0.88 3 7 0 24.56 1.07 3 7 0 24.55 0.8 -4 -7 0 0.3 0.16 -4 -7 0 0.29 0.18 -4 -7 0 0.05 0.18 4 7 0 -0.01 0.21 4 7 0 0.38 0.17 4 7 0 0.27 0.16 -5 -7 0 45.12 1.49 -5 -7 0 44.41 1.21 -5 -7 0 43.7 1.22 5 7 0 45.34 1.43 5 7 0 43.78 1.26 -6 -7 0 116.76 3.25 -6 -7 0 114.49 3.23 -6 -7 0 117.25 2.69 -6 -7 0 118.14 2.71 6 7 0 112.18 2.71 6 7 0 115.44 3.03 -7 -7 0 86.77 2.16 -7 -7 0 88.07 2.67 -7 -7 0 86.03 2.16 -7 -7 0 85.97 2.62 7 7 0 90.55 2.06 7 7 0 87.33 2.49 -8 -7 0 26.85 0.93 -8 -7 0 27.11 1.16 -8 -7 0 26.07 0.94 -8 -7 0 25.78 1.24 8 7 0 25.07 1.16 -9 -7 0 0.74 0.27 -9 -7 0 0.14 0.37 -9 -7 0 0.3 0.25 9 7 0 0.5 0.4 -10 -7 0 0.01 0.26 -10 -7 0 0.36 0.27 -10 -7 0 0.27 0.43 10 7 0 0.33 0.4 -11 -7 0 3.04 0.42 -11 -7 0 3.07 0.41 -11 -7 0 4.52 0.7 11 7 0 2.99 0.6 -12 -7 0 13.12 0.8 -12 -7 0 13.46 0.8 12 7 0 13.22 1.09 -14 8 0 0.31 0.3 -14 8 0 0.33 0.35 -14 8 0 0.14 0.38 -13 8 0 0.51 0.31 -13 8 0 0.89 0.59 -13 8 0 0.39 0.49 -13 8 0 0.91 0.4 12 -8 0 6.38 0.31 -12 8 0 6.24 0.8 -12 8 0 6.24 0.6 -12 8 0 5.67 0.55 -12 8 0 4.76 0.68 11 -8 0 39.98 1.11 -11 8 0 39.16 1.34 -11 8 0 39.2 1.35 -11 8 0 42.08 1.73 -11 8 0 42.67 1.76 10 -8 0 43.42 1.22 -10 8 0 46.33 1.76 -10 8 0 43.31 1.39 -10 8 0 42.84 1.72 -10 8 0 43.62 1.38 9 -8 0 15.63 0.62 -9 8 0 15.04 0.71 -9 8 0 16.17 0.97 -9 8 0 15.75 0.92 -9 8 0 16.63 0.73 8 -8 0 0.15 0.17 -8 8 0 0.15 0.31 -8 8 0 0.07 0.25 -8 8 0 -0.01 0.19 -8 8 0 0.16 0.2 7 -8 0 5.6 0.38 -7 8 0 5.47 0.41 -7 8 0 4.63 0.4 -7 8 0 5.6 0.53 -7 8 0 4.49 0.49 6 -8 0 1.31 0.21 -6 8 0 1.59 0.25 -6 8 0 1.56 0.32 -6 8 0 1.17 0.3 -6 8 0 1.41 0.24 5 -8 0 31.77 0.99 -5 8 0 32.22 1 -5 8 0 33.88 1.16 -5 8 0 32.81 1.02 -5 8 0 33.84 1.21 4 -8 0 28.34 0.88 4 -8 0 27.17 0.74 -4 8 0 27 1.04 -4 8 0 27.81 0.9 -4 8 0 27.13 0.87 -4 8 0 28.95 1 3 -8 0 1.55 0.18 3 -8 0 1.29 0.2 3 -8 0 1.49 0.21 3 -8 0 1.95 0.26 -3 8 0 2.05 0.27 -3 8 0 1.33 0.21 -3 8 0 2.51 0.31 -3 8 0 1.87 0.23 -3 8 0 1.53 0.27 -3 8 0 1.57 0.18 2 -8 0 77.29 1.86 2 -8 0 74.04 1.9 2 -8 0 77.14 1.9 -2 8 0 76.15 1.86 -2 8 0 76.36 1.92 -2 8 0 76.5 2.17 -2 8 0 77.56 1.9 -2 8 0 76.22 2.07 1 -8 0 174.65 4.06 1 -8 0 172.06 3.82 1 -8 0 171.49 3.94 -1 8 0 169.9 3.97 -1 8 0 170.26 4.25 -1 8 0 172.53 3.94 -1 8 0 167.7 4.37 -1 8 0 175.42 3.83 -1 8 0 177.76 4.06 -1 8 0 177.67 3.91 0 -8 0 145.15 3.33 0 -8 0 139.75 3.45 0 -8 0 145.07 3.23 0 8 0 139.74 3.45 0 8 0 143.76 3.75 0 8 0 143.24 3.32 0 8 0 141.28 3.6 0 8 0 152.18 3.31 0 8 0 144.34 3.22 0 8 0 141.57 3.36 -1 -8 0 44.89 1.34 -1 -8 0 43.75 1.21 -1 -8 0 45.92 1.26 1 8 0 45.9 1.34 1 8 0 47.94 1.26 1 8 0 45.42 1.53 1 8 0 42.64 1.24 1 8 0 46.78 1.3 -2 -8 0 7.7 0.49 -2 -8 0 8.53 0.44 -2 -8 0 7.57 0.42 2 8 0 8.19 0.42 2 8 0 7.45 0.58 2 8 0 8.32 0.49 -3 -8 0 37.21 1.08 -3 -8 0 38.71 1.3 -3 -8 0 37.74 1.26 3 8 0 37.73 1.2 3 8 0 40.11 1.49 3 8 0 36.39 1.11 -4 -8 0 30.88 1.18 -4 -8 0 33.97 1 -4 -8 0 32.44 1.18 4 8 0 32.51 1.04 4 8 0 34.78 1.07 4 8 0 33.37 1.15 -5 -8 0 27.16 0.87 -5 -8 0 25.26 1.04 5 8 0 25.7 0.9 5 8 0 24.95 1.02 -6 -8 0 12.83 0.59 -6 -8 0 14.14 0.76 -6 -8 0 13.32 0.8 6 8 0 12.22 0.73 6 8 0 12.38 0.58 -7 -8 0 11.06 0.7 -7 -8 0 10.32 0.56 -7 -8 0 9.39 0.55 -7 -8 0 8.7 0.72 7 8 0 11.23 0.76 7 8 0 9.64 0.46 -8 -8 0 41.75 1.7 -8 -8 0 44.95 1.35 -8 -8 0 45.38 1.35 8 8 0 42.03 1.6 8 8 0 44.94 1.03 -9 -8 0 28.21 1.39 -9 -8 0 27.61 1.02 -9 -8 0 29.36 1.05 9 8 0 29.78 1.31 -10 -8 0 12.97 0.73 -10 -8 0 14.13 1.04 -10 -8 0 12.17 0.73 10 8 0 13.59 0.99 -11 -8 0 1.35 0.57 -11 -8 0 2.21 0.41 -11 -8 0 2.66 0.42 11 8 0 2.26 0.57 -12 -8 0 0.33 0.34 -12 -8 0 0.52 0.38 12 8 0 -0.1 0.53 -13 9 0 1.48 0.62 -13 9 0 1.12 0.39 -13 9 0 1.68 0.57 -13 9 0 1.63 0.4 12 -9 0 0.33 0.18 -12 9 0 0.33 0.41 -12 9 0 0.03 0.31 -12 9 0 -0.12 0.47 -12 9 0 0.04 0.29 11 -9 0 -0.28 0.17 -11 9 0 0.11 0.26 -11 9 0 0.09 0.43 -11 9 0 0.07 0.35 -11 9 0 0.12 0.27 10 -9 0 10.84 0.54 -10 9 0 11.78 0.85 -10 9 0 10.66 0.88 -10 9 0 11.19 0.66 -10 9 0 11.93 0.67 9 -9 0 54.71 1.49 -9 9 0 52.67 1.92 -9 9 0 56.28 1.93 -9 9 0 50.67 1.58 -9 9 0 54.66 1.59 8 -9 0 87.08 2.21 -8 9 0 86.74 2.67 -8 9 0 87.15 2.26 -8 9 0 92.54 2.66 -8 9 0 86.31 2.29 7 -9 0 37.09 1.13 -7 9 0 37.71 1.44 -7 9 0 36.19 1.18 -7 9 0 38.28 1.18 -7 9 0 37.86 1.39 6 -9 0 5.76 0.4 -6 9 0 5.1 0.52 -6 9 0 6.1 0.43 -6 9 0 4.3 0.4 -6 9 0 5.2 0.5 5 -9 0 39.29 1.18 -5 9 0 39.21 1.4 -5 9 0 39.41 1.18 -5 9 0 40.31 1.21 -5 9 0 39.87 1.35 4 -9 0 0.05 0.16 -4 9 0 0.75 0.2 -4 9 0 0.11 0.19 -4 9 0 0.52 0.23 -4 9 0 0.05 0.18 -4 9 0 0.31 0.19 3 -9 0 41.72 1.18 3 -9 0 41.12 1.13 3 -9 0 43.75 1.24 3 -9 0 41.79 1.21 -3 9 0 41.67 1.33 -3 9 0 39.37 1.41 -3 9 0 42.06 1.13 -3 9 0 39.5 1.21 2 -9 0 63.8 1.69 2 -9 0 65.26 1.67 -2 9 0 62.63 1.63 -2 9 0 64.01 1.69 -2 9 0 64.13 1.66 -2 9 0 62.68 1.82 -2 9 0 63.43 1.94 -2 9 0 64.66 1.69 1 -9 0 12.44 0.56 1 -9 0 13.23 0.56 -1 9 0 13.04 0.7 -1 9 0 12.88 0.55 -1 9 0 13.69 0.56 -1 9 0 13.75 0.58 -1 9 0 12.43 0.55 -1 9 0 12.69 0.56 -1 9 0 12.06 0.6 0 -9 0 19.73 0.72 0 -9 0 19.52 0.69 0 -9 0 18.58 0.73 0 9 0 19.29 0.9 0 9 0 18.75 0.77 0 9 0 18.21 0.72 0 9 0 19.28 0.71 0 9 0 19.42 0.71 0 9 0 18.75 0.72 -1 -9 0 95.05 2.43 -1 -9 0 90.89 2.2 -1 -9 0 93.96 2.29 1 9 0 89.3 2.31 1 9 0 91.36 2.27 1 9 0 87.47 2.65 1 9 0 92.29 2.41 -2 -9 0 123.72 3.15 -2 -9 0 120.05 2.85 2 9 0 124.68 3.47 2 9 0 123.55 2.94 2 9 0 122.24 3.03 -3 -9 0 44.48 1.42 -3 -9 0 41.29 1.2 3 9 0 42.64 1.34 3 9 0 40.83 1.61 3 9 0 42.48 1.26 -4 -9 0 5.83 0.5 -4 -9 0 6.51 0.43 4 9 0 5.28 0.63 4 9 0 5.52 0.52 4 9 0 6.22 0.44 -5 -9 0 -0.01 0.2 -5 -9 0 0.16 0.23 5 9 0 0.32 0.29 5 9 0 0.1 0.22 -6 -9 0 5.93 0.46 -6 -9 0 5.98 0.55 -6 -9 0 5.34 0.59 6 9 0 4.85 0.59 6 9 0 5.92 0.45 -7 -9 0 42.61 1.59 -7 -9 0 42.3 1.65 -7 -9 0 41.69 1.29 7 9 0 39.64 1.18 7 9 0 40.46 1.5 -8 -9 0 24.26 0.96 -8 -9 0 25.22 1.27 -8 -9 0 24.21 0.94 8 9 0 24.94 0.69 8 9 0 24.57 1.19 -9 -9 0 1.12 0.31 -9 -9 0 0.52 0.44 -9 -9 0 0.47 0.3 9 9 0 0.53 0.45 -10 -9 0 14.67 0.81 -10 -9 0 16.61 1.17 -10 -9 0 14.22 0.79 10 9 0 15.38 1.06 -11 -9 0 32.8 1.74 -11 -9 0 36.1 1.3 -11 -9 0 34.8 1.29 11 9 0 31.54 1.54 -13 10 0 0.57 0.46 -13 10 0 0.55 0.6 -13 10 0 0.72 0.35 -13 10 0 0.7 0.39 12 -10 0 8.92 0.49 -12 10 0 9.15 0.68 -12 10 0 9.9 0.72 -12 10 0 9.92 0.93 -12 10 0 9.56 0.92 11 -10 0 10.44 0.55 -11 10 0 10.61 0.71 -11 10 0 12.21 0.72 -11 10 0 10.46 0.89 -11 10 0 12.51 1 10 -10 0 0.07 0.21 -10 10 0 0.32 0.41 -10 10 0 0.3 0.28 -10 10 0 0.15 0.33 -10 10 0 -0.22 0.26 9 -10 0 0.27 0.2 -9 10 0 0.33 0.27 -9 10 0 0.49 0.39 -9 10 0 0.24 0.32 -9 10 0 0.11 0.25 8 -10 0 0.47 0.22 -8 10 0 0.32 0.24 -8 10 0 0.15 0.35 -8 10 0 0.64 0.28 -8 10 0 0.29 0.29 7 -10 0 29.95 0.99 -7 10 0 28.33 1.2 -7 10 0 27.63 1 -7 10 0 27.45 1.22 -7 10 0 28.17 1.02 6 -10 0 84.06 2.14 -6 10 0 80.23 2.39 -6 10 0 81.4 2.12 -6 10 0 84.41 2.18 -6 10 0 81.26 2.48 5 -10 0 48.33 1.41 -5 10 0 49.87 1.6 -5 10 0 49.54 1.69 -5 10 0 49.21 1.42 4 -10 0 1.14 0.23 -4 10 0 1.26 0.32 -4 10 0 1.4 0.26 -4 10 0 1.34 0.26 -4 10 0 1.11 0.24 -4 10 0 1.64 0.31 3 -10 0 8.58 0.49 -3 10 0 8.25 0.49 -3 10 0 7.87 0.58 -3 10 0 8.58 0.51 -3 10 0 7.05 0.53 2 -10 0 19.87 0.74 2 -10 0 18.66 0.75 2 -10 0 20.27 0.72 -2 10 0 20.66 0.78 -2 10 0 17.24 0.79 -2 10 0 18.98 0.74 -2 10 0 19.1 0.7 -2 10 0 17.74 0.89 -2 10 0 19.44 0.75 1 -10 0 3.87 0.37 1 -10 0 4.34 0.37 1 -10 0 4.35 0.39 -1 10 0 5.41 0.54 -1 10 0 4.33 0.37 -1 10 0 4.79 0.43 -1 10 0 4.36 0.37 -1 10 0 4.15 0.38 0 -10 0 20.55 0.78 0 -10 0 20.51 0.81 0 -10 0 20.6 0.76 0 10 0 20.22 0.98 0 10 0 20.07 0.77 0 10 0 20.05 0.8 0 10 0 20.59 0.87 0 10 0 20.11 0.77 -1 -10 0 30.58 1.07 -1 -10 0 29.61 0.97 1 10 0 31.16 1.04 1 10 0 27.33 0.97 1 10 0 32.12 1.3 -2 -10 0 0.34 0.22 -2 -10 0 0.16 0.2 2 10 0 0.3 0.2 2 10 0 0.7 0.27 2 10 0 0.63 0.32 -3 -10 0 27.12 0.95 3 10 0 29.26 1.07 3 10 0 27.34 0.97 3 10 0 30.17 1.36 -4 -10 0 57.81 1.93 -4 -10 0 58.32 1.62 4 10 0 59.17 1.78 4 10 0 59.08 1.68 4 10 0 61 2.18 -5 -10 0 44.81 1.61 -5 -10 0 42 1.3 5 10 0 44.3 1.36 5 10 0 43.71 1.5 -6 -10 0 7.8 0.64 -6 -10 0 6.96 0.66 -6 -10 0 6.22 0.5 6 10 0 6.61 0.51 6 10 0 6.74 0.66 -7 -10 0 1.97 0.5 -7 -10 0 2.27 0.36 7 10 0 1.66 0.44 7 10 0 1.62 0.28 -8 -10 0 10.87 0.66 -8 -10 0 11.91 0.91 8 10 0 10.77 0.45 8 10 0 10.49 0.81 -9 -10 0 22.91 1.31 -9 -10 0 22.65 0.99 9 10 0 24.31 1.25 -10 -10 0 16.92 1.22 -10 -10 0 14.6 0.85 10 10 0 17.64 1.09 -11 -10 0 1.6 0.44 11 10 0 1.13 0.62 13 -11 0 32.75 0.95 -13 11 0 32.65 1.37 -13 11 0 32.15 1.35 -13 11 0 32 1.7 12 -11 0 10.87 0.58 -12 11 0 12.07 1.05 -12 11 0 12.06 0.8 -12 11 0 11.6 0.79 -12 11 0 11.41 0.99 11 -11 0 0.2 0.23 -11 11 0 0.33 0.46 -11 11 0 1.3 0.5 -11 11 0 0.72 0.35 -11 11 0 -0.39 0.26 10 -11 0 8.63 0.54 -10 11 0 8.95 0.66 -10 11 0 7.69 0.77 -10 11 0 9.92 0.88 -10 11 0 9.01 0.66 9 -11 0 3.53 0.42 -9 11 0 4.53 0.49 -9 11 0 4.72 0.68 -9 11 0 4.02 0.5 -9 11 0 4.05 0.58 8 -11 0 0.06 0.22 -8 11 0 0.13 0.27 -8 11 0 -0.02 0.24 -8 11 0 0.65 0.35 -8 11 0 -0.17 0.31 7 -11 0 1.14 0.27 -7 11 0 0.84 0.29 -7 11 0 0.79 0.36 -7 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