data_p16323_2_a _audit_creation_date 2016-09-25 _audit_creation_method ; Olex2 1.2 (compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155) ; _publ_contact_author_address ; Beckman Institute Caltech 139-74 Pasadena CA 91125 USA ; _publ_contact_author_email xray@caltech.edu _publ_contact_author_name 'Sarah E. Reisman' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common CX-10-076 _chemical_name_systematic CX-10-076 _chemical_formula_moiety 'C25 H35 N O9, 2(C4 H10 O), H2 O' _chemical_formula_sum 'C33 H57 N O12' _chemical_formula_weight 659.79 _chemical_absolute_configuration ad _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 10.9374(3) _cell_length_b 11.9604(3) _cell_length_c 27.4814(7) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3595.00(16) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9851 _cell_measurement_temperature 200 _cell_measurement_theta_max 78.52 _cell_measurement_theta_min 3.22 _shelx_estimated_absorpt_T_max 0.869 _shelx_estimated_absorpt_T_min 0.827 _exptl_absorpt_coefficient_mu 0.759 _exptl_absorpt_correction_T_max 0.7543 _exptl_absorpt_correction_T_min 0.6648 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2014/5 (Sheldrick, 2014)' _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.219 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1432 _exptl_crystal_size_max 0.26 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.19 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0438 _diffrn_reflns_av_unetI/netI 0.0166 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 35 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 91317 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 79.361 _diffrn_reflns_theta_min 3.216 _diffrn_ambient_temperature 200 _diffrn_detector 'CMOS Area Detector' _diffrn_detector_area_resol_mean 10.24 _diffrn_detector_type 'Bruker PHOTON 100 CMOS' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON 100 CMOS' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'I\mS HB micro-focus sealed tube' _diffrn_source_current 1 _diffrn_source_power 0.05 _diffrn_source_type 'Incoatech I\mS HB' _diffrn_source_voltage 50 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.781 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.992 _reflns_number_gt 7391 _reflns_number_total 7764 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker-AXS, 2007)' _computing_data_collection 'APEX2 v2014.11-0 (Bruker-AXS, 2014)' _computing_data_reduction 'SAINT v8.34A (Bruker-AXS, 2007)' _computing_molecular_graphics ? _computing_publication_material ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-2013/1 (She ldrick, 2013)' _refine_diff_density_max 0.588 _refine_diff_density_min -0.333 _refine_diff_density_rms 0.041 _refine_ls_abs_structure_details ; Flack x determined using 3121 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.05(3) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 439 _refine_ls_number_reflns 7764 _refine_ls_number_restraints 9 _refine_ls_R_factor_all 0.0411 _refine_ls_R_factor_gt 0.0389 _refine_ls_restrained_S_all 1.045 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0638P)^2^+0.9060P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1064 _refine_ls_wR_factor_ref 0.1083 _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All C(H,H,H,H,H,H,H,H,H,H,H) groups 2. Restrained distances H7-O7 = H8-O8 = H5-O5 = H6-O6 = H9-O9 = H2-O2 0.84 with sigma of 0.02 H12A-O12 = H12B-O12 0.87 with sigma of 0.02 N1-H1 0.88 with sigma of 0.02 3. Others Fixed U11: O7(0.02047) O12(0.02307) Fixed U12: O7(-0.00208) O12(-0.00339) Fixed U13: O7(0.00283) O12(0.00043) Fixed U22: O7(0.04486) O12(0.05241) Fixed U23: O7(0.00317) O12(-0.00732) Fixed U33: O7(0.02783) O12(0.04513) 4.a Ternary CH refined with riding coordinates: C13(H13), C10(H10), C3(H3), C9(H9A) 4.b Secondary CH2 refined with riding coordinates: C14(H14A,H14B), C7(H7A,H7B), C8(H8A,H8B), C27(H27A,H27B), C28(H28A,H28B), C31(H31A,H31B), C32(H32A,H32B) 4.c Aromatic/amide H refined with riding coordinates: C23(H23), C25(H25), C24(H24) 4.d Idealised Me refined as rotating group: C16(H16A,H16B,H16C), C19(H19A,H19B,H19C), C17(H17A,H17B,H17C), C29(H29A,H29B, H29C), C20(H20A,H20B,H20C), C18(H18A,H18B,H18C), C26(H26A,H26B,H26C), C30(H30A, H30B,H30C), C33(H33A,H33B,H33C) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.55051(13) 0.37238(12) 0.38678(5) 0.0232(3) Uani 1 1 d . . . . . O3 O 0.44104(16) 0.76511(12) 0.37232(5) 0.0286(3) Uani 1 1 d . . . . . O5 O 0.42457(14) 0.46004(14) 0.27562(5) 0.0288(3) Uani 1 1 d D . . . . O2 O 0.41717(15) 0.42617(14) 0.44682(5) 0.0286(3) Uani 1 1 d D . . . . O8 O 0.57264(15) 0.65404(14) 0.28164(6) 0.0299(3) Uani 1 1 d D . . . . O9 O 0.22391(15) 0.58156(15) 0.32160(6) 0.0320(3) Uani 1 1 d D . . . . O7 O 0.74372(14) 0.51262(15) 0.29818(6) 0.031 Uani 1 1 d D . . . . O6 O 0.52606(16) 0.22495(14) 0.30737(6) 0.0314(3) Uani 1 1 d D . . . . O4 O 0.44457(18) 0.89289(14) 0.31125(6) 0.0377(4) Uani 1 1 d . . . . . O10 O 0.97042(17) 0.48192(14) 0.20334(7) 0.0376(4) Uani 1 1 d . . . . . O12 O 0.97524(16) 0.59030(17) 0.29269(7) 0.040 Uani 1 1 d D . . . . N1 N 0.4860(2) 1.06158(17) 0.38393(8) 0.0361(5) Uani 1 1 d D . . . . C12 C 0.47963(19) 0.48383(17) 0.32081(7) 0.0220(4) Uani 1 1 d . . . . . C15 C 0.47493(19) 0.46212(17) 0.40503(7) 0.0224(4) Uani 1 1 d . . . . . C6 C 0.69501(18) 0.48816(19) 0.34588(7) 0.0252(4) Uani 1 1 d . . . . . C11 C 0.58709(19) 0.40698(18) 0.33876(7) 0.0231(4) Uani 1 1 d . . . . . C21 C 0.4517(2) 0.86997(19) 0.35406(8) 0.0286(4) Uani 1 1 d . . . . . C5 C 0.62780(19) 0.59324(18) 0.36555(8) 0.0248(4) Uani 1 1 d . . . . . C4 C 0.5268(2) 0.60732(17) 0.32566(7) 0.0243(4) Uani 1 1 d . . . . . C2 C 0.31526(19) 0.59159(18) 0.35949(7) 0.0250(4) Uani 1 1 d . . . . . C13 C 0.2477(2) 0.6321(2) 0.40547(8) 0.0307(5) Uani 1 1 d . . . . . H13 H 0.3107 0.6491 0.4308 0.037 Uiso 1 1 calc R . . . . C22 C 0.4696(2) 0.94978(19) 0.39314(9) 0.0321(5) Uani 1 1 d . . . . . C1 C 0.38404(18) 0.47749(17) 0.36229(7) 0.0223(4) Uani 1 1 d . . . . . C14 C 0.5608(2) 0.56154(18) 0.41337(7) 0.0245(4) Uani 1 1 d . . . . . H14A H 0.6217 0.5420 0.4386 0.029 Uiso 1 1 calc R . . . . H14B H 0.5131 0.6265 0.4251 0.029 Uiso 1 1 calc R . . . . C10 C 0.6248(2) 0.30328(18) 0.31058(8) 0.0264(4) Uani 1 1 d . . . . . H10 H 0.6507 0.3255 0.2770 0.032 Uiso 1 1 calc R . . . . C3 C 0.4131(2) 0.67522(18) 0.33920(7) 0.0246(4) Uani 1 1 d . . . . . H3 H 0.3797 0.7089 0.3087 0.030 Uiso 1 1 calc R . . . . C9 C 0.7323(2) 0.2458(2) 0.33659(9) 0.0331(5) Uani 1 1 d . . . . . H9A H 0.7011 0.2148 0.3680 0.040 Uiso 1 1 calc R . . . . C16 C 0.3031(2) 0.37314(19) 0.35822(8) 0.0285(4) Uani 1 1 d . . . . . H16A H 0.2334 0.3892 0.3369 0.043 Uiso 1 1 calc GR . . . . H16B H 0.2733 0.3522 0.3906 0.043 Uiso 1 1 calc GR . . . . H16C H 0.3509 0.3114 0.3445 0.043 Uiso 1 1 calc GR . . . . C7 C 0.7960(2) 0.4327(2) 0.37543(8) 0.0312(5) Uani 1 1 d . . . . . H7A H 0.7654 0.4130 0.4082 0.037 Uiso 1 1 calc R . . . . H7B H 0.8659 0.4846 0.3792 0.037 Uiso 1 1 calc R . . . . C8 C 0.8369(2) 0.3269(2) 0.34844(9) 0.0361(5) Uani 1 1 d . . . . . H8A H 0.8982 0.2873 0.3686 0.043 Uiso 1 1 calc R . . . . H8B H 0.8774 0.3491 0.3177 0.043 Uiso 1 1 calc R . . . . C19 C 0.7120(2) 0.6935(2) 0.37317(10) 0.0352(5) Uani 1 1 d . . . . . H19A H 0.7767 0.6736 0.3962 0.053 Uiso 1 1 calc GR . . . . H19B H 0.6646 0.7563 0.3862 0.053 Uiso 1 1 calc GR . . . . H19C H 0.7486 0.7150 0.3420 0.053 Uiso 1 1 calc GR . . . . C23 C 0.4682(3) 0.9361(2) 0.44296(10) 0.0435(6) Uani 1 1 d . . . . . H23 H 0.4582 0.8676 0.4600 0.052 Uiso 1 1 calc R . . . . C25 C 0.4949(3) 1.1171(2) 0.42649(11) 0.0465(7) Uani 1 1 d . . . . . H25 H 0.5066 1.1954 0.4300 0.056 Uiso 1 1 calc R . . . . C27 C 1.0156(3) 0.3704(2) 0.20301(11) 0.0436(6) Uani 1 1 d . . . . . H27A H 1.0367 0.3482 0.1693 0.052 Uiso 1 1 calc R . . . . H27B H 0.9518 0.3187 0.2152 0.052 Uiso 1 1 calc R . . . . C24 C 0.4841(4) 1.0417(2) 0.46381(11) 0.0516(8) Uani 1 1 d . . . . . H24 H 0.4870 1.0582 0.4976 0.062 Uiso 1 1 calc R . . . . C17 C 0.1588(3) 0.5461(2) 0.42696(10) 0.0415(6) Uani 1 1 d . . . . . H17A H 0.1003 0.5229 0.4019 0.062 Uiso 1 1 calc GR . . . . H17B H 0.1146 0.5797 0.4543 0.062 Uiso 1 1 calc GR . . . . H17C H 0.2047 0.4808 0.4384 0.062 Uiso 1 1 calc GR . . . . C29 C 0.8178(3) 0.6132(3) 0.18012(13) 0.0525(7) Uani 1 1 d . . . . . H29A H 0.7405 0.6216 0.1625 0.079 Uiso 1 1 calc GR . . . . H29B H 0.8800 0.6615 0.1653 0.079 Uiso 1 1 calc GR . . . . H29C H 0.8061 0.6348 0.2142 0.079 Uiso 1 1 calc GR . . . . C20 C 0.7792(3) 0.1486(3) 0.30611(12) 0.0499(7) Uani 1 1 d . . . . . H20A H 0.7124 0.0957 0.3002 0.075 Uiso 1 1 calc GR . . . . H20B H 0.8454 0.1106 0.3236 0.075 Uiso 1 1 calc GR . . . . H20C H 0.8100 0.1768 0.2749 0.075 Uiso 1 1 calc GR . . . . C28 C 0.8588(3) 0.4942(3) 0.17763(13) 0.0519(7) Uani 1 1 d . . . . . H28A H 0.7958 0.4450 0.1921 0.062 Uiso 1 1 calc R . . . . H28B H 0.8704 0.4720 0.1432 0.062 Uiso 1 1 calc R . . . . C18 C 0.1757(3) 0.7396(2) 0.39577(11) 0.0450(6) Uani 1 1 d . . . . . H18A H 0.2274 0.7927 0.3780 0.068 Uiso 1 1 calc GR . . . . H18B H 0.1504 0.7727 0.4268 0.068 Uiso 1 1 calc GR . . . . H18C H 0.1031 0.7222 0.3763 0.068 Uiso 1 1 calc GR . . . . C26 C 1.1260(3) 0.3626(3) 0.23444(13) 0.0538(8) Uani 1 1 d . . . . . H26A H 1.1896 0.4126 0.2219 0.081 Uiso 1 1 calc GR . . . . H26B H 1.1564 0.2855 0.2344 0.081 Uiso 1 1 calc GR . . . . H26C H 1.1048 0.3845 0.2678 0.081 Uiso 1 1 calc GR . . . . O11 O 0.5175(2) 0.4249(2) 0.53746(7) 0.0575(6) Uani 1 1 d . . . . . C30 C 0.6815(4) 0.3047(4) 0.51439(17) 0.0791(12) Uani 1 1 d . . . . . H30A H 0.6566 0.3005 0.4802 0.119 Uiso 1 1 calc GR . . . . H30B H 0.7231 0.2353 0.5236 0.119 Uiso 1 1 calc GR . . . . H30C H 0.7371 0.3680 0.5189 0.119 Uiso 1 1 calc GR . . . . C31 C 0.5747(6) 0.3197(5) 0.54463(16) 0.1001(18) Uani 1 1 d . . . . . H31A H 0.5151 0.2596 0.5374 0.120 Uiso 1 1 calc R . . . . H31B H 0.5988 0.3126 0.5792 0.120 Uiso 1 1 calc R . . . . C32 C 0.4135(6) 0.4425(5) 0.56630(15) 0.1002(18) Uani 1 1 d . . . . . H32A H 0.4374 0.4372 0.6010 0.120 Uiso 1 1 calc R . . . . H32B H 0.3540 0.3820 0.5597 0.120 Uiso 1 1 calc R . . . . C33 C 0.3552(6) 0.5471(5) 0.55854(19) 0.104(2) Uani 1 1 d . . . . . H33A H 0.3336 0.5545 0.5241 0.156 Uiso 1 1 calc GR . . . . H33B H 0.4108 0.6077 0.5678 0.156 Uiso 1 1 calc GR . . . . H33C H 0.2808 0.5512 0.5784 0.156 Uiso 1 1 calc GR . . . . H8 H 0.636(5) 0.619(6) 0.274(3) 0.156 Uiso 1 1 d DR . . . . H2 H 0.463(6) 0.434(6) 0.4710(18) 0.156 Uiso 1 1 d DR . . . . H5 H 0.474(6) 0.463(6) 0.253(2) 0.156 Uiso 1 1 d DR . . . . H7 H 0.819(3) 0.534(6) 0.299(3) 0.156 Uiso 1 1 d DR . . . . H6 H 0.503(7) 0.219(6) 0.2780(13) 0.156 Uiso 1 1 d DR . . . . H9 H 0.250(7) 0.552(6) 0.2962(17) 0.156 Uiso 1 1 d DR . . . . H1 H 0.493(6) 1.091(5) 0.3548(13) 0.125 Uiso 1 1 d DR . . . . H12A H 1.043(4) 0.577(6) 0.308(2) 0.156 Uiso 1 1 d DR . . . . H12B H 0.988(8) 0.563(6) 0.2628(14) 0.156 Uiso 1 1 d DR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0253(7) 0.0240(7) 0.0203(6) 0.0011(5) -0.0005(5) 0.0024(6) O3 0.0374(9) 0.0217(7) 0.0266(7) 0.0031(6) -0.0021(6) 0.0006(6) O5 0.0246(7) 0.0413(9) 0.0206(7) -0.0021(6) -0.0046(6) -0.0002(7) O2 0.0310(8) 0.0338(8) 0.0209(7) 0.0049(6) 0.0031(6) -0.0006(6) O8 0.0264(8) 0.0386(9) 0.0247(7) 0.0108(6) 0.0032(6) -0.0008(6) O9 0.0221(7) 0.0432(9) 0.0306(8) 0.0041(7) -0.0051(6) 0.0016(7) O7 0.020 0.045 0.028 0.003 0.003 0.000 O6 0.0352(8) 0.0306(8) 0.0285(7) -0.0049(6) -0.0048(6) -0.0028(7) O4 0.0481(10) 0.0332(8) 0.0317(8) 0.0097(6) 0.0004(7) -0.0041(8) O10 0.0364(9) 0.0298(8) 0.0468(10) -0.0037(7) -0.0071(8) -0.0031(7) O12 0.023 0.052 0.045 0.000 0.000 0.000 N1 0.0401(11) 0.0272(9) 0.0409(11) 0.0055(8) -0.0057(9) -0.0013(8) C12 0.0199(9) 0.0276(10) 0.0185(8) -0.0003(7) -0.0026(7) -0.0010(8) C15 0.0235(9) 0.0234(9) 0.0203(9) 0.0013(7) 0.0001(7) 0.0012(8) C6 0.0194(9) 0.0321(10) 0.0239(9) 0.0015(8) -0.0015(7) -0.0016(8) C11 0.0220(9) 0.0272(10) 0.0202(9) 0.0011(7) -0.0016(7) -0.0005(8) C21 0.0245(10) 0.0278(10) 0.0336(11) 0.0070(8) 0.0007(8) 0.0000(8) C5 0.0223(9) 0.0280(10) 0.0243(10) 0.0023(8) -0.0029(8) -0.0038(8) C4 0.0235(9) 0.0284(10) 0.0209(9) 0.0054(7) -0.0003(8) -0.0024(8) C2 0.0211(9) 0.0302(10) 0.0235(9) 0.0036(8) -0.0013(8) 0.0010(8) C13 0.0292(11) 0.0335(11) 0.0293(10) 0.0030(9) 0.0046(8) 0.0075(9) C22 0.0361(12) 0.0242(10) 0.0360(11) 0.0040(9) -0.0025(10) 0.0015(9) C1 0.0200(9) 0.0262(10) 0.0207(9) 0.0019(7) -0.0002(7) -0.0018(8) C14 0.0257(10) 0.0263(10) 0.0215(9) 0.0000(8) -0.0036(8) 0.0002(8) C10 0.0248(10) 0.0293(10) 0.0252(10) -0.0035(8) -0.0004(8) 0.0021(8) C3 0.0265(10) 0.0262(10) 0.0212(9) 0.0030(7) -0.0013(8) 0.0000(8) C9 0.0296(11) 0.0364(12) 0.0333(11) -0.0059(9) -0.0030(9) 0.0091(10) C16 0.0244(10) 0.0292(10) 0.0317(11) 0.0009(8) -0.0006(8) -0.0058(9) C7 0.0220(10) 0.0397(12) 0.0320(11) 0.0004(9) -0.0058(8) 0.0016(9) C8 0.0244(11) 0.0439(14) 0.0401(12) -0.0009(10) -0.0033(9) 0.0081(10) C19 0.0314(12) 0.0333(12) 0.0408(12) 0.0000(9) -0.0029(10) -0.0103(10) C23 0.0654(18) 0.0298(12) 0.0354(12) 0.0029(10) -0.0059(12) 0.0016(12) C25 0.0575(18) 0.0276(12) 0.0543(16) -0.0017(11) -0.0124(13) 0.0014(11) C27 0.0515(16) 0.0301(12) 0.0493(15) -0.0030(11) -0.0070(12) -0.0013(12) C24 0.079(2) 0.0363(14) 0.0395(14) -0.0025(11) -0.0108(14) 0.0017(14) C17 0.0334(13) 0.0475(15) 0.0436(13) 0.0081(11) 0.0156(11) 0.0040(11) C29 0.0494(17) 0.0481(16) 0.0600(18) -0.0009(14) -0.0117(14) 0.0076(13) C20 0.0464(16) 0.0503(16) 0.0531(16) -0.0186(13) -0.0059(13) 0.0217(13) C28 0.0449(16) 0.0435(15) 0.0673(19) -0.0061(14) -0.0207(14) -0.0015(13) C18 0.0410(14) 0.0400(14) 0.0542(15) 0.0078(12) 0.0100(12) 0.0170(12) C26 0.0593(19) 0.0375(14) 0.0648(19) -0.0022(13) -0.0184(15) 0.0109(14) O11 0.0620(13) 0.0780(16) 0.0326(10) -0.0011(9) -0.0078(9) 0.0023(12) C30 0.067(3) 0.090(3) 0.080(3) 0.011(2) -0.015(2) 0.011(2) C31 0.145(5) 0.098(4) 0.056(2) 0.021(2) 0.005(3) 0.034(4) C32 0.139(5) 0.116(4) 0.0446(19) -0.001(2) 0.027(2) 0.026(4) C33 0.113(4) 0.130(5) 0.070(3) -0.027(3) 0.003(3) 0.043(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C15 1.445(2) . ? O1 C11 1.440(2) . ? O3 C21 1.356(3) . ? O3 C3 1.442(3) . ? O5 C12 1.409(2) . ? O5 H5 0.82(3) . ? O2 C15 1.380(2) . ? O2 H2 0.84(3) . ? O8 C4 1.424(2) . ? O8 H8 0.83(3) . ? O9 C2 1.448(3) . ? O9 H9 0.83(3) . ? O7 C6 1.445(2) . ? O7 H7 0.87(3) . ? O6 C10 1.433(3) . ? O6 H6 0.85(3) . ? O4 C21 1.210(3) . ? O10 C27 1.423(3) . ? O10 C28 1.418(3) . ? O12 H12A 0.87(3) . ? O12 H12B 0.89(3) . ? N1 C22 1.373(3) . ? N1 C25 1.349(4) . ? N1 H1 0.88(3) . ? C12 C11 1.572(3) . ? C12 C4 1.570(3) . ? C12 C1 1.549(3) . ? C15 C1 1.550(3) . ? C15 C14 1.533(3) . ? C6 C11 1.541(3) . ? C6 C5 1.553(3) . ? C6 C7 1.523(3) . ? C11 C10 1.519(3) . ? C21 C22 1.450(3) . ? C5 C4 1.565(3) . ? C5 C14 1.552(3) . ? C5 C19 1.526(3) . ? C4 C3 1.531(3) . ? C2 C13 1.542(3) . ? C2 C1 1.560(3) . ? C2 C3 1.567(3) . ? C13 H13 1.0000 . ? C13 C17 1.533(3) . ? C13 C18 1.532(3) . ? C22 C23 1.379(4) . ? C1 C16 1.534(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C10 H10 1.0000 . ? C10 C9 1.538(3) . ? C3 H3 1.0000 . ? C9 H9A 1.0000 . ? C9 C8 1.535(4) . ? C9 C20 1.522(3) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C7 C8 1.533(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C23 H23 0.9500 . ? C23 C24 1.397(4) . ? C25 H25 0.9500 . ? C25 C24 1.371(4) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C26 1.488(4) . ? C24 H24 0.9500 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C29 C28 1.494(4) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? O11 C31 1.419(6) . ? O11 C32 1.402(6) . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C30 C31 1.445(7) . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C32 C33 1.420(8) . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C11 O1 C15 105.29(14) . . ? C21 O3 C3 118.31(17) . . ? C12 O5 H5 112(6) . . ? C15 O2 H2 111(5) . . ? C4 O8 H8 108(5) . . ? C2 O9 H9 114(5) . . ? C6 O7 H7 113(5) . . ? C10 O6 H6 110(5) . . ? C28 O10 C27 113.1(2) . . ? H12A O12 H12B 105(6) . . ? C22 N1 H1 125(4) . . ? C25 N1 C22 109.2(2) . . ? C25 N1 H1 126(4) . . ? O5 C12 C11 118.56(17) . . ? O5 C12 C4 113.91(16) . . ? O5 C12 C1 110.51(16) . . ? C4 C12 C11 106.12(16) . . ? C1 C12 C11 104.19(15) . . ? C1 C12 C4 101.85(16) . . ? O1 C15 C1 101.07(15) . . ? O1 C15 C14 106.12(16) . . ? O2 C15 O1 108.64(16) . . ? O2 C15 C1 111.98(17) . . ? O2 C15 C14 113.45(16) . . ? C14 C15 C1 114.49(16) . . ? O7 C6 C11 107.15(16) . . ? O7 C6 C5 109.06(17) . . ? O7 C6 C7 107.71(17) . . ? C11 C6 C5 101.04(16) . . ? C7 C6 C11 110.42(18) . . ? C7 C6 C5 120.68(18) . . ? O1 C11 C12 104.36(15) . . ? O1 C11 C6 106.12(15) . . ? O1 C11 C10 107.95(16) . . ? C6 C11 C12 104.13(16) . . ? C10 C11 C12 121.38(17) . . ? C10 C11 C6 111.77(17) . . ? O3 C21 C22 110.26(19) . . ? O4 C21 O3 124.3(2) . . ? O4 C21 C22 125.4(2) . . ? C6 C5 C4 100.21(16) . . ? C14 C5 C6 108.70(17) . . ? C14 C5 C4 106.63(16) . . ? C19 C5 C6 113.47(18) . . ? C19 C5 C4 115.92(18) . . ? C19 C5 C14 111.13(18) . . ? O8 C4 C12 114.37(17) . . ? O8 C4 C5 112.88(17) . . ? O8 C4 C3 106.51(16) . . ? C5 C4 C12 100.97(16) . . ? C3 C4 C12 104.63(17) . . ? C3 C4 C5 117.40(17) . . ? O9 C2 C13 106.56(17) . . ? O9 C2 C1 107.19(17) . . ? O9 C2 C3 105.54(16) . . ? C13 C2 C1 117.73(17) . . ? C13 C2 C3 114.72(18) . . ? C1 C2 C3 104.28(16) . . ? C2 C13 H13 107.7 . . ? C17 C13 C2 114.1(2) . . ? C17 C13 H13 107.7 . . ? C18 C13 C2 111.56(19) . . ? C18 C13 H13 107.7 . . ? C18 C13 C17 107.7(2) . . ? N1 C22 C21 121.5(2) . . ? N1 C22 C23 107.4(2) . . ? C23 C22 C21 131.0(2) . . ? C12 C1 C15 97.51(15) . . ? C12 C1 C2 104.26(16) . . ? C15 C1 C2 116.77(17) . . ? C16 C1 C12 112.07(17) . . ? C16 C1 C15 109.20(17) . . ? C16 C1 C2 115.45(17) . . ? C15 C14 C5 110.62(16) . . ? C15 C14 H14A 109.5 . . ? C15 C14 H14B 109.5 . . ? C5 C14 H14A 109.5 . . ? C5 C14 H14B 109.5 . . ? H14A C14 H14B 108.1 . . ? O6 C10 C11 111.11(17) . . ? O6 C10 H10 109.3 . . ? O6 C10 C9 108.24(18) . . ? C11 C10 H10 109.3 . . ? C11 C10 C9 109.61(17) . . ? C9 C10 H10 109.3 . . ? O3 C3 C4 112.12(18) . . ? O3 C3 C2 113.33(17) . . ? O3 C3 H3 107.9 . . ? C4 C3 C2 107.61(17) . . ? C4 C3 H3 107.9 . . ? C2 C3 H3 107.9 . . ? C10 C9 H9A 107.8 . . ? C8 C9 C10 112.7(2) . . ? C8 C9 H9A 107.8 . . ? C20 C9 C10 110.1(2) . . ? C20 C9 H9A 107.8 . . ? C20 C9 C8 110.4(2) . . ? C1 C16 H16A 109.5 . . ? C1 C16 H16B 109.5 . . ? C1 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C6 C7 H7A 110.0 . . ? C6 C7 H7B 110.0 . . ? C6 C7 C8 108.25(19) . . ? H7A C7 H7B 108.4 . . ? C8 C7 H7A 110.0 . . ? C8 C7 H7B 110.0 . . ? C9 C8 H8A 108.8 . . ? C9 C8 H8B 108.8 . . ? C7 C8 C9 113.99(19) . . ? C7 C8 H8A 108.8 . . ? C7 C8 H8B 108.8 . . ? H8A C8 H8B 107.7 . . ? C5 C19 H19A 109.5 . . ? C5 C19 H19B 109.5 . . ? C5 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C22 C23 H23 126.3 . . ? C22 C23 C24 107.4(2) . . ? C24 C23 H23 126.3 . . ? N1 C25 H25 125.7 . . ? N1 C25 C24 108.6(2) . . ? C24 C25 H25 125.7 . . ? O10 C27 H27A 109.7 . . ? O10 C27 H27B 109.7 . . ? O10 C27 C26 109.7(2) . . ? H27A C27 H27B 108.2 . . ? C26 C27 H27A 109.7 . . ? C26 C27 H27B 109.7 . . ? C23 C24 H24 126.3 . . ? C25 C24 C23 107.4(3) . . ? C25 C24 H24 126.3 . . ? C13 C17 H17A 109.5 . . ? C13 C17 H17B 109.5 . . ? C13 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? C9 C20 H20A 109.5 . . ? C9 C20 H20B 109.5 . . ? C9 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? O10 C28 C29 109.5(2) . . ? O10 C28 H28A 109.8 . . ? O10 C28 H28B 109.8 . . ? C29 C28 H28A 109.8 . . ? C29 C28 H28B 109.8 . . ? H28A C28 H28B 108.2 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C27 C26 H26A 109.5 . . ? C27 C26 H26B 109.5 . . ? C27 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C32 O11 C31 114.4(4) . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C31 C30 H30A 109.5 . . ? C31 C30 H30B 109.5 . . ? C31 C30 H30C 109.5 . . ? O11 C31 C30 112.8(4) . . ? O11 C31 H31A 109.0 . . ? O11 C31 H31B 109.0 . . ? C30 C31 H31A 109.0 . . ? C30 C31 H31B 109.0 . . ? H31A C31 H31B 107.8 . . ? O11 C32 H32A 108.7 . . ? O11 C32 H32B 108.7 . . ? O11 C32 C33 114.3(5) . . ? H32A C32 H32B 107.6 . . ? C33 C32 H32A 108.7 . . ? C33 C32 H32B 108.7 . . ? C32 C33 H33A 109.5 . . ? C32 C33 H33B 109.5 . . ? C32 C33 H33C 109.5 . . ? H33A C33 H33B 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O8 H8 O7 0.83(3) 1.86(5) 2.563(2) 141(7) . O2 H2 O11 0.84(3) 1.93(4) 2.722(3) 159(7) . O5 H5 O4 0.82(3) 2.15(4) 2.897(2) 151(7) 3_645 O7 H7 O12 0.87(3) 1.84(3) 2.701(2) 172(7) . O6 H6 O8 0.85(3) 1.99(4) 2.805(2) 160(7) 3_645 O9 H9 O5 0.83(3) 2.27(6) 2.920(2) 135(7) . N1 H1 O6 0.88(3) 2.10(4) 2.905(3) 152(5) 1_565 O12 H12A O9 0.87(3) 2.01(4) 2.835(2) 157(7) 1_655 O12 H12B O10 0.89(3) 1.91(3) 2.777(3) 163(8) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C15 C1 C12 -49.60(18) . . . . ? O1 C15 C1 C2 -159.77(16) . . . . ? O1 C15 C1 C16 66.96(19) . . . . ? O1 C15 C14 C5 57.7(2) . . . . ? O1 C11 C10 O6 59.4(2) . . . . ? O1 C11 C10 C9 -60.2(2) . . . . ? O3 C21 C22 N1 178.3(2) . . . . ? O3 C21 C22 C23 -5.3(4) . . . . ? O5 C12 C11 O1 -127.03(18) . . . . ? O5 C12 C11 C6 121.86(18) . . . . ? O5 C12 C11 C10 -5.1(3) . . . . ? O5 C12 C4 O8 -34.5(2) . . . . ? O5 C12 C4 C5 -155.99(17) . . . . ? O5 C12 C4 C3 81.7(2) . . . . ? O5 C12 C1 C15 159.95(16) . . . . ? O5 C12 C1 C2 -79.9(2) . . . . ? O5 C12 C1 C16 45.7(2) . . . . ? O2 C15 C1 C12 -165.08(16) . . . . ? O2 C15 C1 C2 84.8(2) . . . . ? O2 C15 C1 C16 -48.5(2) . . . . ? O2 C15 C14 C5 176.90(17) . . . . ? O8 C4 C3 O3 -94.02(19) . . . . ? O8 C4 C3 C2 140.71(17) . . . . ? O9 C2 C13 C17 67.6(2) . . . . ? O9 C2 C13 C18 -54.7(3) . . . . ? O9 C2 C1 C12 81.78(19) . . . . ? O9 C2 C1 C15 -172.00(16) . . . . ? O9 C2 C1 C16 -41.6(2) . . . . ? O9 C2 C3 O3 128.96(18) . . . . ? O9 C2 C3 C4 -106.50(18) . . . . ? O7 C6 C11 O1 172.61(16) . . . . ? O7 C6 C11 C12 -77.57(19) . . . . ? O7 C6 C11 C10 55.2(2) . . . . ? O7 C6 C5 C4 60.73(19) . . . . ? O7 C6 C5 C14 172.32(16) . . . . ? O7 C6 C5 C19 -63.5(2) . . . . ? O7 C6 C7 C8 -58.4(2) . . . . ? O6 C10 C9 C8 -171.99(18) . . . . ? O6 C10 C9 C20 64.3(3) . . . . ? O4 C21 C22 N1 -3.0(4) . . . . ? O4 C21 C22 C23 173.3(3) . . . . ? N1 C22 C23 C24 -0.1(4) . . . . ? N1 C25 C24 C23 0.0(4) . . . . ? C12 C11 C10 O6 -60.8(2) . . . . ? C12 C11 C10 C9 179.61(18) . . . . ? C12 C4 C3 O3 144.51(16) . . . . ? C12 C4 C3 C2 19.2(2) . . . . ? C15 O1 C11 C12 -28.79(19) . . . . ? C15 O1 C11 C6 80.86(18) . . . . ? C15 O1 C11 C10 -159.18(16) . . . . ? C6 C11 C10 O6 175.72(16) . . . . ? C6 C11 C10 C9 56.1(2) . . . . ? C6 C5 C4 O8 -76.4(2) . . . . ? C6 C5 C4 C12 46.18(18) . . . . ? C6 C5 C4 C3 159.15(17) . . . . ? C6 C5 C14 C15 -55.5(2) . . . . ? C6 C7 C8 C9 -54.3(3) . . . . ? C11 O1 C15 O2 168.51(16) . . . . ? C11 O1 C15 C1 50.58(18) . . . . ? C11 O1 C15 C14 -69.17(18) . . . . ? C11 C12 C4 O8 97.78(19) . . . . ? C11 C12 C4 C5 -23.73(19) . . . . ? C11 C12 C4 C3 -146.08(16) . . . . ? C11 C12 C1 C15 31.55(18) . . . . ? C11 C12 C1 C2 151.70(16) . . . . ? C11 C12 C1 C16 -82.7(2) . . . . ? C11 C6 C5 C4 -51.93(18) . . . . ? C11 C6 C5 C14 59.66(19) . . . . ? C11 C6 C5 C19 -176.15(17) . . . . ? C11 C6 C7 C8 58.3(2) . . . . ? C11 C10 C9 C8 -50.7(3) . . . . ? C11 C10 C9 C20 -174.4(2) . . . . ? C21 O3 C3 C4 100.8(2) . . . . ? C21 O3 C3 C2 -137.17(19) . . . . ? C21 C22 C23 C24 -176.8(3) . . . . ? C5 C6 C11 O1 -73.28(18) . . . . ? C5 C6 C11 C12 36.54(18) . . . . ? C5 C6 C11 C10 169.28(16) . . . . ? C5 C6 C7 C8 175.63(19) . . . . ? C5 C4 C3 O3 33.6(2) . . . . ? C5 C4 C3 C2 -91.7(2) . . . . ? C4 C12 C11 O1 103.35(17) . . . . ? C4 C12 C11 C6 -7.75(19) . . . . ? C4 C12 C11 C10 -134.73(19) . . . . ? C4 C12 C1 C15 -78.68(17) . . . . ? C4 C12 C1 C2 41.47(18) . . . . ? C4 C12 C1 C16 167.03(17) . . . . ? C4 C5 C14 C15 51.8(2) . . . . ? C13 C2 C1 C12 -158.24(18) . . . . ? C13 C2 C1 C15 -52.0(3) . . . . ? C13 C2 C1 C16 78.4(2) . . . . ? C13 C2 C3 O3 12.0(2) . . . . ? C13 C2 C3 C4 136.52(18) . . . . ? C22 N1 C25 C24 -0.1(4) . . . . ? C22 C23 C24 C25 0.0(4) . . . . ? C1 C12 C11 O1 -3.72(19) . . . . ? C1 C12 C11 C6 -114.83(17) . . . . ? C1 C12 C11 C10 118.19(19) . . . . ? C1 C12 C4 O8 -153.47(17) . . . . ? C1 C12 C4 C5 85.02(18) . . . . ? C1 C12 C4 C3 -37.33(18) . . . . ? C1 C15 C14 C5 -52.9(2) . . . . ? C1 C2 C13 C17 -52.7(3) . . . . ? C1 C2 C13 C18 -175.0(2) . . . . ? C1 C2 C3 O3 -118.25(18) . . . . ? C1 C2 C3 C4 6.3(2) . . . . ? C14 C15 C1 C12 64.0(2) . . . . ? C14 C15 C1 C2 -46.2(2) . . . . ? C14 C15 C1 C16 -179.46(17) . . . . ? C14 C5 C4 O8 170.45(17) . . . . ? C14 C5 C4 C12 -67.01(19) . . . . ? C14 C5 C4 C3 46.0(2) . . . . ? C10 C9 C8 C7 51.6(3) . . . . ? C3 O3 C21 O4 -3.4(3) . . . . ? C3 O3 C21 C22 175.22(19) . . . . ? C3 C2 C13 C17 -176.0(2) . . . . ? C3 C2 C13 C18 61.7(3) . . . . ? C3 C2 C1 C12 -29.82(19) . . . . ? C3 C2 C1 C15 76.4(2) . . . . ? C3 C2 C1 C16 -153.22(17) . . . . ? C7 C6 C11 O1 55.6(2) . . . . ? C7 C6 C11 C12 165.39(16) . . . . ? C7 C6 C11 C10 -61.9(2) . . . . ? C7 C6 C5 C4 -173.87(18) . . . . ? C7 C6 C5 C14 -62.3(2) . . . . ? C7 C6 C5 C19 61.9(3) . . . . ? C19 C5 C4 O8 46.1(3) . . . . ? C19 C5 C4 C12 168.70(19) . . . . ? C19 C5 C4 C3 -78.3(2) . . . . ? C19 C5 C14 C15 178.98(18) . . . . ? C25 N1 C22 C21 177.2(2) . . . . ? C25 N1 C22 C23 0.1(3) . . . . ? C27 O10 C28 C29 179.6(3) . . . . ? C20 C9 C8 C7 175.1(2) . . . . ? C28 O10 C27 C26 -174.8(3) . . . . ? C31 O11 C32 C33 -179.0(5) . . . . ? C32 O11 C31 C30 -179.9(5) . . . . ? _shelx_res_file ; p16323_2_a.res created by SHELXL-2014/7 TITL P16323_2_a.res in P2(1)2(1)2(1) REM Old TITL P16323_2 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.112, Rweak 0.029, Alpha 0.001, Orientation as input REM Flack x = 0.063 ( 0.030 ) from Parsons' quotients REM Formula found by SHELXT: C33 N2 O11 CELL 1.54178 10.9374 11.9604 27.4814 90 90 90 ZERR 4 0.0003 0.0003 0.0007 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 132 228 4 48 EQIV $1 1+X,+Y,+Z EQIV $2 1-X,-0.5+Y,0.5-Z EQIV $3 +X,1+Y,+Z DFIX 0.84 H7 O7 H8 O8 H5 O5 H6 O6 H9 O9 H2 O2 DFIX 0.87 H12a O12 H12b O12 DFIX 0.88 N1 H1 L.S. 20 PLAN 20 SIZE 0.19 0.22 0.26 TEMP -73 HTAB O5 O4_$2 HTAB O2 O11 HTAB O8 O7 HTAB O9 O5 HTAB O7 O12 HTAB O6 O8_$2 HTAB O12 O9_$1 HTAB O12 O10 HTAB N1 O6_$3 BOND $H MORE -1 CONF fmap -2 acta REM REM REM WGHT 0.063800 0.906000 FVAR 0.43307 O1 4 0.550506 0.372383 0.386777 11.00000 0.02527 0.02400 = 0.02029 0.00106 -0.00047 0.00239 O3 4 0.441041 0.765112 0.372324 11.00000 0.03742 0.02172 = 0.02658 0.00314 -0.00208 0.00063 O5 4 0.424574 0.460036 0.275615 11.00000 0.02462 0.04132 = 0.02061 -0.00214 -0.00461 -0.00023 O2 4 0.417172 0.426170 0.446824 11.00000 0.03100 0.03379 = 0.02092 0.00487 0.00311 -0.00062 O8 4 0.572636 0.654040 0.281643 11.00000 0.02636 0.03861 = 0.02466 0.01083 0.00322 -0.00082 O9 4 0.223913 0.581558 0.321596 11.00000 0.02211 0.04318 = 0.03063 0.00412 -0.00509 0.00156 O7 4 0.743723 0.512617 0.298175 11.00000 10.02047 10.04486 = 10.02783 10.00317 10.00283 -10.00208 O6 4 0.526055 0.224949 0.307365 11.00000 0.03517 0.03058 = 0.02851 -0.00487 -0.00479 -0.00283 O4 4 0.444569 0.892894 0.311249 11.00000 0.04810 0.03325 = 0.03165 0.00967 0.00040 -0.00413 O10 4 0.970419 0.481921 0.203341 11.00000 0.03637 0.02978 = 0.04678 -0.00370 -0.00714 -0.00307 O12 4 0.975236 0.590304 0.292691 11.00000 10.02307 10.05241 = 10.04513 -10.00732 10.00043 -10.00339 N1 3 0.486019 1.061577 0.383930 11.00000 0.04009 0.02724 = 0.04089 0.00551 -0.00573 -0.00133 C12 1 0.479627 0.483832 0.320809 11.00000 0.01993 0.02763 = 0.01852 -0.00029 -0.00257 -0.00098 C15 1 0.474932 0.462119 0.405028 11.00000 0.02350 0.02341 = 0.02027 0.00126 0.00007 0.00119 C6 1 0.695009 0.488160 0.345878 11.00000 0.01942 0.03215 = 0.02395 0.00148 -0.00148 -0.00164 C11 1 0.587087 0.406978 0.338763 11.00000 0.02195 0.02718 = 0.02023 0.00109 -0.00162 -0.00049 C21 1 0.451681 0.869972 0.354059 11.00000 0.02450 0.02777 = 0.03356 0.00703 0.00068 0.00000 C5 1 0.627802 0.593239 0.365554 11.00000 0.02225 0.02798 = 0.02430 0.00233 -0.00288 -0.00381 C4 1 0.526803 0.607320 0.325665 11.00000 0.02351 0.02838 = 0.02089 0.00541 -0.00032 -0.00244 C2 1 0.315259 0.591595 0.359489 11.00000 0.02114 0.03019 = 0.02354 0.00356 -0.00134 0.00102 C13 1 0.247739 0.632087 0.405474 11.00000 0.02921 0.03351 = 0.02929 0.00302 0.00464 0.00750 AFIX 13 H13 2 0.310678 0.649092 0.430809 11.00000 -1.20000 AFIX 0 C22 1 0.469641 0.949776 0.393135 11.00000 0.03614 0.02424 = 0.03602 0.00399 -0.00251 0.00149 C1 1 0.384039 0.477489 0.362288 11.00000 0.02001 0.02617 = 0.02070 0.00188 -0.00019 -0.00175 C14 1 0.560827 0.561543 0.413372 11.00000 0.02566 0.02632 = 0.02149 0.00000 -0.00363 0.00022 AFIX 23 H14A 2 0.621705 0.542017 0.438640 11.00000 -1.20000 H14B 2 0.513097 0.626461 0.425147 11.00000 -1.20000 AFIX 0 C10 1 0.624842 0.303283 0.310580 11.00000 0.02480 0.02927 = 0.02517 -0.00352 -0.00041 0.00211 AFIX 13 H10 2 0.650745 0.325461 0.277044 11.00000 -1.20000 AFIX 0 C3 1 0.413073 0.675216 0.339195 11.00000 0.02649 0.02615 = 0.02123 0.00300 -0.00126 -0.00001 AFIX 13 H3 2 0.379689 0.708927 0.308662 11.00000 -1.20000 AFIX 0 C9 1 0.732336 0.245824 0.336589 11.00000 0.02955 0.03640 = 0.03335 -0.00585 -0.00297 0.00915 AFIX 13 H9A 2 0.701111 0.214766 0.368005 11.00000 -1.20000 AFIX 0 C16 1 0.303104 0.373143 0.358224 11.00000 0.02444 0.02925 = 0.03174 0.00090 -0.00057 -0.00581 AFIX 137 H16A 2 0.233388 0.389167 0.336936 11.00000 -1.50000 H16B 2 0.273326 0.352226 0.390602 11.00000 -1.50000 H16C 2 0.350899 0.311382 0.344537 11.00000 -1.50000 AFIX 0 C7 1 0.796050 0.432676 0.375425 11.00000 0.02196 0.03975 = 0.03202 0.00039 -0.00575 0.00156 AFIX 23 H7A 2 0.765359 0.412978 0.408213 11.00000 -1.20000 H7B 2 0.865930 0.484566 0.379200 11.00000 -1.20000 AFIX 0 C8 1 0.836940 0.326891 0.348437 11.00000 0.02435 0.04391 = 0.04015 -0.00094 -0.00330 0.00808 AFIX 23 H8A 2 0.898244 0.287320 0.368582 11.00000 -1.20000 H8B 2 0.877364 0.349118 0.317690 11.00000 -1.20000 AFIX 0 C19 1 0.711960 0.693533 0.373174 11.00000 0.03144 0.03335 = 0.04078 0.00004 -0.00287 -0.01032 AFIX 137 H19A 2 0.776710 0.673599 0.396245 11.00000 -1.50000 H19B 2 0.664557 0.756344 0.386154 11.00000 -1.50000 H19C 2 0.748641 0.715047 0.342015 11.00000 -1.50000 AFIX 0 C23 1 0.468185 0.936140 0.442963 11.00000 0.06537 0.02977 = 0.03539 0.00289 -0.00589 0.00162 AFIX 43 H23 2 0.458198 0.867608 0.459981 11.00000 -1.20000 AFIX 0 C25 1 0.494856 1.117146 0.426488 11.00000 0.05746 0.02759 = 0.05434 -0.00173 -0.01237 0.00137 AFIX 43 H25 2 0.506566 1.195432 0.430015 11.00000 -1.20000 AFIX 0 C27 1 1.015627 0.370353 0.203012 11.00000 0.05147 0.03007 = 0.04933 -0.00296 -0.00701 -0.00129 AFIX 23 H27A 2 1.036662 0.348209 0.169325 11.00000 -1.20000 H27B 2 0.951793 0.318735 0.215161 11.00000 -1.20000 AFIX 0 C24 1 0.484107 1.041714 0.463806 11.00000 0.07898 0.03628 = 0.03951 -0.00248 -0.01075 0.00166 AFIX 43 H24 2 0.486956 1.058180 0.497605 11.00000 -1.20000 AFIX 0 C17 1 0.158827 0.546117 0.426959 11.00000 0.03337 0.04747 = 0.04365 0.00811 0.01562 0.00404 AFIX 137 H17A 2 0.100350 0.522898 0.401902 11.00000 -1.50000 H17B 2 0.114629 0.579707 0.454319 11.00000 -1.50000 H17C 2 0.204682 0.480805 0.438389 11.00000 -1.50000 AFIX 0 C29 1 0.817825 0.613241 0.180120 11.00000 0.04941 0.04815 = 0.05998 -0.00092 -0.01165 0.00764 AFIX 137 H29A 2 0.740499 0.621569 0.162473 11.00000 -1.50000 H29B 2 0.879982 0.661457 0.165310 11.00000 -1.50000 H29C 2 0.806089 0.634762 0.214210 11.00000 -1.50000 AFIX 0 C20 1 0.779191 0.148552 0.306106 11.00000 0.04641 0.05026 = 0.05305 -0.01856 -0.00587 0.02166 AFIX 137 H20A 2 0.712374 0.095679 0.300192 11.00000 -1.50000 H20B 2 0.845398 0.110604 0.323559 11.00000 -1.50000 H20C 2 0.809962 0.176759 0.274945 11.00000 -1.50000 AFIX 0 C28 1 0.858849 0.494209 0.177631 11.00000 0.04486 0.04347 = 0.06732 -0.00610 -0.02072 -0.00148 AFIX 23 H28A 2 0.795758 0.445049 0.192105 11.00000 -1.20000 H28B 2 0.870392 0.471955 0.143239 11.00000 -1.20000 AFIX 0 C18 1 0.175654 0.739599 0.395768 11.00000 0.04096 0.04002 = 0.05417 0.00783 0.00999 0.01702 AFIX 137 H18A 2 0.227372 0.792681 0.378040 11.00000 -1.50000 H18B 2 0.150365 0.772741 0.426789 11.00000 -1.50000 H18C 2 0.103106 0.722160 0.376264 11.00000 -1.50000 AFIX 0 C26 1 1.126039 0.362562 0.234444 11.00000 0.05925 0.03746 = 0.06481 -0.00224 -0.01843 0.01090 AFIX 137 H26A 2 1.189609 0.412590 0.221895 11.00000 -1.50000 H26B 2 1.156420 0.285478 0.234393 11.00000 -1.50000 H26C 2 1.104820 0.384483 0.267751 11.00000 -1.50000 AFIX 0 O11 4 0.517488 0.424899 0.537461 11.00000 0.06199 0.07800 = 0.03259 -0.00114 -0.00780 0.00234 C30 1 0.681461 0.304661 0.514393 11.00000 0.06724 0.08971 = 0.08033 0.01081 -0.01535 0.01131 AFIX 137 H30A 2 0.656557 0.300531 0.480185 11.00000 -1.50000 H30B 2 0.723124 0.235251 0.523568 11.00000 -1.50000 H30C 2 0.737143 0.368009 0.518915 11.00000 -1.50000 AFIX 0 C31 1 0.574679 0.319686 0.544629 11.00000 0.14543 0.09836 = 0.05649 0.02074 0.00531 0.03442 AFIX 23 H31A 2 0.515145 0.259581 0.537412 11.00000 -1.20000 H31B 2 0.598799 0.312642 0.579215 11.00000 -1.20000 AFIX 0 C32 1 0.413507 0.442525 0.566304 11.00000 0.13939 0.11648 = 0.04462 -0.00078 0.02749 0.02594 AFIX 23 H32A 2 0.437398 0.437171 0.600973 11.00000 -1.20000 H32B 2 0.353967 0.382049 0.559712 11.00000 -1.20000 AFIX 0 C33 1 0.355165 0.547054 0.558540 11.00000 0.11270 0.12956 = 0.07035 -0.02731 0.00344 0.04265 AFIX 137 H33A 2 0.333610 0.554495 0.524079 11.00000 -1.50000 H33B 2 0.410780 0.607663 0.567809 11.00000 -1.50000 H33C 2 0.280835 0.551154 0.578373 11.00000 -1.50000 AFIX 0 H8 2 0.635564 0.618903 0.273876 11.00000 -1.50000 H2 2 0.462777 0.433849 0.470965 11.00000 -1.50000 H5 2 0.474325 0.462548 0.253117 11.00000 -1.50000 H7 2 0.819466 0.533711 0.299023 11.00000 -1.50000 H6 2 0.502625 0.219134 0.277972 11.00000 -1.50000 H9 2 0.250037 0.551656 0.296207 11.00000 -1.50000 H1 2 0.493422 1.090679 0.354788 11.00000 -1.20000 H12A 2 1.042896 0.576600 0.308414 11.00000 -1.50000 H12B 2 0.987511 0.563073 0.262817 11.00000 -1.50000 HKLF 4 REM P16323_2_a.res in P2(1)2(1)2(1) REM R1 = 0.0389 for 7391 Fo > 4sig(Fo) and 0.0411 for all 7764 data REM 439 parameters refined using 9 restraints END WGHT 0.0638 0.9036 REM Highest difference peak 0.588, deepest hole -0.333, 1-sigma level 0.041 Q1 1 0.6425 0.4028 0.5440 11.00000 0.05 0.59 Q2 1 0.5973 0.3383 0.5454 11.00000 0.05 -0.33 Q3 1 0.5418 0.4951 0.5327 11.00000 0.05 0.33 Q4 1 0.4788 0.4996 0.5675 11.00000 0.05 0.31 Q5 1 0.9853 0.6276 0.3060 11.00000 0.05 -0.23 Q6 1 0.9537 0.5626 0.2834 11.00000 0.05 -0.21 Q7 1 0.6018 0.3615 0.3218 11.00000 0.05 0.18 Q8 1 0.3455 0.2998 0.3695 11.00000 0.05 0.18 Q9 1 0.6626 0.5416 0.3590 11.00000 0.05 0.17 Q10 1 0.7123 0.3985 0.5674 11.00000 0.05 0.16 Q11 1 0.5281 0.4420 0.3280 11.00000 0.05 0.16 Q12 1 0.2961 0.3562 0.3210 11.00000 0.05 0.16 Q13 1 0.4354 0.4748 0.3428 11.00000 0.05 0.16 Q14 1 0.6463 0.4417 0.3420 11.00000 0.05 0.16 Q15 1 0.6736 0.6370 0.3690 11.00000 0.05 0.15 Q16 1 1.0043 0.5559 0.3051 11.00000 0.05 0.15 Q17 1 0.5206 0.4426 0.4245 11.00000 0.05 -0.15 Q18 1 0.4255 0.4745 0.3850 11.00000 0.05 0.15 Q19 1 0.6768 0.2015 0.3266 11.00000 0.05 -0.15 Q20 1 0.7613 0.2801 0.3082 11.00000 0.05 -0.15 ; _shelx_res_checksum 74556 _shelx_hkl_file ; 1 0 0 -1.10 1.00 1 0 0 0.20 0.40 1 0 0 0.40 0.50 1 0 0 0.20 0.20 1 0 0 0.30 0.20 1 0 0 1.60 1.10 1 0 0 0.40 0.30 -1 0 0 0.20 0.20 -1 0 0 0.40 0.60 -1 0 0 0.00 0.40 -1 0 0 0.80 0.50 2 0 0 6326.27 242.58 2 0 0 6949.70 244.28 2 0 0 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491.75 23.50 -3 -4 0 504.35 19.00 -3 -4 0 530.95 19.10 -3 4 0 479.35 19.10 -3 -4 0 513.15 22.10 -3 -4 0 529.55 18.90 3 -4 0 483.75 20.60 3 -4 0 547.35 38.00 -3 -4 0 464.35 18.60 3 -4 0 488.95 23.50 4 -4 0 2.50 3.50 4 -4 0 8.00 1.40 4 -4 0 5.90 1.60 4 -4 0 4.30 3.00 4 -4 0 1.50 4.30 4 -4 0 5.50 18.40 4 -4 0 17.20 6.80 4 -4 0 -1.90 6.10 4 -4 0 10.70 7.00 -4 -4 0 11.50 2.70 -4 -4 0 11.10 5.00 4 -4 0 11.00 4.30 4 -4 0 30.70 19.50 4 -4 0 13.10 8.10 -4 4 0 4.90 1.60 -4 4 0 6.70 4.30 5 -4 0 42.70 6.40 -5 -4 0 62.09 7.10 5 -4 0 66.59 10.50 -5 4 0 50.79 7.60 -5 4 0 58.89 3.70 5 -4 0 84.59 31.30 5 -4 0 56.99 7.90 5 -4 0 53.19 2.30 -5 4 0 50.49 3.90 5 -4 0 51.19 2.80 -5 -4 0 46.10 7.50 5 -4 0 67.09 29.40 5 -4 0 52.39 10.20 5 -4 0 45.10 7.10 -6 -4 0 21.40 9.50 6 4 0 50.59 4.00 6 -4 0 50.39 2.30 6 -4 0 52.29 3.40 -6 4 0 56.69 3.90 6 -4 0 46.40 3.50 6 4 0 46.80 3.20 -6 4 0 45.20 3.80 -6 4 0 47.80 4.80 -6 4 0 49.50 3.50 6 4 0 55.69 4.00 6 -4 0 44.70 3.30 7 -4 0 127.89 5.80 7 -4 0 124.39 6.10 -7 4 0 123.29 5.60 -7 4 0 119.29 6.00 7 4 0 121.09 6.30 7 4 0 123.29 5.80 7 -4 0 129.19 5.70 7 -4 0 127.19 5.90 -7 4 0 122.89 6.60 7 4 0 123.69 6.10 7 4 0 122.89 5.50 8 4 0 73.49 4.70 8 4 0 70.09 4.00 -8 4 0 69.79 4.00 8 -4 0 73.89 4.30 8 -4 0 69.49 4.10 8 4 0 64.69 4.30 8 4 0 65.29 4.60 -8 4 0 71.99 6.20 -8 4 0 71.99 4.40 8 -4 0 73.39 4.40 8 -4 0 70.99 4.80 -9 4 0 4.40 1.90 9 -4 0 3.30 1.60 9 4 0 6.40 1.90 -9 4 0 3.20 1.60 9 4 0 5.30 1.80 9 -4 0 3.00 1.90 9 4 0 3.10 1.90 9 -4 0 5.00 2.10 -10 4 0 2.60 1.90 10 4 0 -0.70 1.80 10 -4 0 3.60 1.90 10 -4 0 1.60 2.00 10 -4 0 1.30 1.70 -10 4 0 1.30 1.50 10 -4 0 0.70 2.00 10 -4 0 2.80 1.50 -10 4 0 -1.20 1.80 11 -4 0 17.90 2.40 -11 4 0 15.40 2.10 11 -4 0 14.70 2.00 11 4 0 19.00 3.10 11 4 0 16.80 2.50 -11 4 0 16.00 2.10 11 -4 0 21.40 3.20 12 -4 0 1.40 1.30 12 4 0 -0.90 2.10 12 -4 0 0.20 1.30 -12 4 0 2.80 1.00 12 4 0 1.50 1.20 12 -4 0 1.00 1.50 13 -4 0 47.50 2.40 13 -4 0 43.10 2.60 -13 4 0 40.10 2.20 0 -5 0 -2.30 4.30 0 -5 0 2.70 3.40 0 -5 0 1.70 3.90 0 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34.90 -4 5 0 259.37 10.20 4 -5 0 160.48 32.80 -4 5 0 238.68 14.50 4 -5 0 222.48 15.10 4 -5 0 221.78 13.00 -4 -5 0 226.38 16.60 4 -5 0 205.68 22.10 -4 5 0 282.07 10.10 4 -5 0 256.77 19.30 4 -5 0 229.18 19.60 4 -5 0 271.57 9.60 4 -5 0 221.28 11.10 -5 5 0 184.18 7.60 5 -5 0 176.28 17.60 5 -5 0 182.38 7.00 5 -5 0 166.08 22.90 5 -5 0 174.58 7.90 5 -5 0 167.98 7.50 -5 5 0 182.18 8.10 -5 5 0 171.88 26.50 5 5 0 179.98 7.80 -5 5 0 183.08 7.90 5 -5 0 188.58 7.30 5 -5 0 122.19 47.60 -5 5 0 185.48 7.30 -5 -5 0 159.98 19.00 5 -5 0 170.08 7.60 5 -5 0 171.18 7.50 -6 5 0 4.40 1.30 6 -5 0 4.50 1.70 6 5 0 5.70 1.70 -6 5 0 2.70 2.10 6 -5 0 3.60 1.00 6 5 0 7.20 2.00 -6 5 0 5.30 2.00 6 -5 0 8.70 1.80 6 5 0 3.90 1.80 6 -5 0 8.60 1.80 -6 5 0 5.70 1.80 7 -5 0 191.48 10.10 7 5 0 200.08 8.50 7 5 0 208.88 8.70 7 5 0 189.48 8.30 7 -5 0 203.98 8.50 7 -5 0 217.78 8.90 7 5 0 180.88 8.90 -7 5 0 204.38 9.20 7 -5 0 209.78 8.60 -8 5 0 0.30 1.40 -8 5 0 -3.00 3.00 8 5 0 0.10 2.00 8 5 0 -1.20 1.90 8 -5 0 1.80 1.90 8 -5 0 0.30 1.60 -8 5 0 2.30 1.80 -8 5 0 1.80 1.80 8 -5 0 2.50 2.10 8 -5 0 0.90 2.00 8 5 0 1.50 1.50 8 5 0 4.70 2.20 9 -5 0 46.80 4.30 -9 5 0 45.60 3.90 -9 5 0 43.50 3.90 9 -5 0 47.60 3.90 9 -5 0 50.09 3.80 9 5 0 47.60 4.10 9 -5 0 50.79 3.50 -9 5 0 49.80 3.40 9 5 0 48.40 3.40 9 5 0 47.60 4.30 10 -5 0 0.70 1.40 10 -5 0 1.60 2.10 10 -5 0 2.00 1.70 -10 5 0 1.30 2.00 10 -5 0 4.90 2.10 10 -5 0 2.40 1.90 -11 5 0 35.80 3.00 11 5 0 37.00 2.90 11 -5 0 40.30 2.80 11 -5 0 42.30 3.10 11 -5 0 38.60 3.00 -11 5 0 41.20 2.70 11 -5 0 48.90 3.70 -11 5 0 33.80 4.20 12 5 0 0.10 1.30 12 -5 0 1.40 1.20 12 -5 0 -0.80 1.30 -12 5 0 0.30 1.60 -12 5 0 1.20 0.90 13 -5 0 4.50 1.20 0 -6 0 728.33 32.60 0 -6 0 738.53 33.10 0 -6 0 750.72 30.50 0 -6 0 720.83 29.30 0 6 0 757.52 27.20 0 -6 0 720.53 29.20 0 -6 0 760.22 50.79 0 -6 0 725.03 31.50 0 -6 0 716.33 32.30 0 -6 0 733.53 49.00 0 6 0 763.92 27.00 0 -6 0 761.22 27.50 0 -6 0 679.53 28.30 0 -6 0 748.13 30.50 0 -6 0 746.33 32.60 1 -6 0 106.79 5.40 1 -6 0 112.19 13.20 1 -6 0 129.59 29.70 -1 -6 0 127.29 11.50 -1 -6 0 104.29 11.60 1 -6 0 116.79 10.30 -1 -6 0 119.49 21.90 1 -6 0 108.29 5.30 1 -6 0 117.99 15.20 -1 6 0 116.79 6.20 1 -6 0 102.19 8.70 1 -6 0 84.79 24.00 1 -6 0 116.39 13.00 1 -6 0 111.29 14.00 1 6 0 102.29 4.30 1 -6 0 126.69 10.70 -1 6 0 107.99 5.10 -1 -6 0 147.99 22.70 -1 -6 0 108.99 11.50 -1 -6 0 105.79 7.20 -1 -6 0 104.99 8.60 -1 -6 0 98.99 5.70 1 -6 0 140.99 10.90 1 -6 0 116.49 8.00 -1 -6 0 117.19 7.60 -1 -6 0 120.19 12.40 -1 -6 0 126.19 11.60 -1 -6 0 102.89 5.20 -1 -6 0 114.39 8.40 -2 -6 0 448.46 21.60 -2 -6 0 436.36 18.20 2 -6 0 428.96 16.80 2 -6 0 436.36 19.60 -2 -6 0 445.16 20.50 2 -6 0 418.46 20.40 -2 -6 0 430.66 16.80 2 -6 0 462.35 22.00 -2 6 0 439.16 16.80 -2 -6 0 429.86 35.00 -2 -6 0 440.86 18.10 2 -6 0 486.05 51.29 2 -6 0 468.45 26.50 2 -6 0 466.45 21.60 -2 -6 0 419.96 20.90 2 -6 0 503.15 56.19 -2 -6 0 420.96 18.70 -2 -6 0 455.85 21.30 -2 6 0 458.15 16.70 -2 -6 0 448.96 22.80 2 -6 0 410.56 19.90 -2 -6 0 445.26 18.80 2 -6 0 450.05 24.80 -2 -6 0 419.46 35.50 -2 6 0 420.16 18.50 2 -6 0 440.56 17.00 2 -6 0 396.46 26.20 2 -6 0 453.05 24.50 3 -6 0 13.30 11.70 3 -6 0 5.10 9.00 -3 -6 0 -7.40 14.60 -3 -6 0 0.70 3.00 -3 6 0 1.40 1.40 -3 -6 0 21.30 14.80 3 -6 0 11.70 9.50 -3 -6 0 -6.50 5.30 3 -6 0 0.10 1.30 3 -6 0 -7.10 5.50 3 -6 0 -4.80 5.00 -3 -6 0 2.10 2.40 3 -6 0 5.40 1.90 3 -6 0 1.50 1.40 3 6 0 2.20 1.90 3 -6 0 7.90 7.60 3 -6 0 2.90 13.50 3 -6 0 1.70 1.90 3 -6 0 5.40 4.30 -3 -6 0 1.00 4.70 3 -6 0 2.80 1.90 -3 -6 0 5.50 3.00 -3 6 0 1.40 1.60 -3 6 0 12.60 5.50 -3 6 0 2.10 1.20 -3 6 0 -0.90 1.80 -3 -6 0 2.60 7.70 3 -6 0 30.40 39.20 -3 -6 0 3.20 5.10 -3 6 0 3.10 1.60 -3 -6 0 3.60 5.20 -3 -6 0 -1.60 2.40 4 -6 0 211.08 20.70 -4 6 0 234.78 9.30 4 -6 0 240.78 25.90 4 6 0 240.08 9.70 4 -6 0 231.88 25.80 -4 6 0 242.58 10.10 -4 6 0 231.28 9.80 4 -6 0 213.48 53.99 4 -6 0 238.98 9.80 4 -6 0 243.88 9.70 4 -6 0 248.58 9.80 4 -6 0 244.38 9.50 4 -6 0 234.68 9.90 -4 6 0 233.78 17.40 -4 6 0 232.58 9.60 4 -6 0 235.18 9.60 4 -6 0 262.57 15.60 -4 -6 0 238.18 12.00 4 6 0 233.98 9.80 -4 -6 0 233.18 9.80 -4 6 0 247.68 9.90 -5 6 0 211.68 8.80 5 -6 0 204.48 8.50 5 -6 0 167.38 23.90 5 6 0 202.08 8.30 5 -6 0 210.58 8.40 5 6 0 185.88 8.30 5 -6 0 200.28 8.30 5 -6 0 206.38 8.60 -5 6 0 209.88 8.10 -5 6 0 196.48 8.40 5 6 0 201.48 8.70 5 -6 0 204.18 8.40 -5 6 0 192.98 9.80 -5 6 0 196.48 8.50 5 6 0 186.28 8.40 -5 6 0 211.28 9.10 5 -6 0 214.48 8.10 6 -6 0 15.30 2.10 6 6 0 11.00 2.20 6 6 0 11.80 2.10 -6 6 0 11.30 2.20 6 -6 0 10.50 2.10 -6 6 0 12.30 2.60 -6 6 0 11.20 2.40 6 -6 0 18.10 2.30 -6 6 0 12.40 2.40 -6 6 0 13.00 2.50 6 6 0 15.40 2.00 -7 6 0 154.98 6.50 7 -6 0 155.58 7.20 7 -6 0 156.78 7.00 7 6 0 150.88 6.90 -7 6 0 149.19 6.80 7 6 0 140.29 6.60 -7 6 0 150.88 7.00 -7 6 0 152.38 8.40 7 -6 0 158.28 6.90 7 6 0 148.99 7.10 -7 6 0 143.19 7.80 7 -6 0 156.98 7.00 8 6 0 22.40 3.60 8 -6 0 30.60 3.30 -8 6 0 25.00 2.70 -8 6 0 27.30 3.30 8 6 0 26.60 2.80 -8 6 0 26.60 3.30 8 -6 0 22.60 3.20 8 -6 0 28.80 3.50 8 -6 0 23.50 3.90 -8 6 0 17.10 4.50 9 -6 0 8.00 2.20 9 6 0 8.10 2.20 -9 6 0 7.10 1.90 -9 6 0 -3.20 4.70 -9 6 0 9.50 1.50 9 6 0 7.00 1.70 9 -6 0 11.00 2.20 9 -6 0 9.30 2.20 -9 6 0 8.80 1.90 9 -6 0 5.80 1.70 -10 6 0 9.10 1.50 10 -6 0 5.40 1.70 10 -6 0 6.90 1.90 10 -6 0 6.80 1.70 10 -6 0 9.60 2.10 -10 6 0 9.00 1.70 -10 6 0 7.00 1.90 10 6 0 8.30 1.70 11 6 0 21.20 2.40 -11 6 0 22.40 2.00 11 -6 0 26.60 2.60 11 -6 0 26.60 2.40 11 -6 0 22.60 2.70 -11 6 0 20.00 3.10 11 -6 0 25.00 2.20 12 -6 0 1.20 1.20 -12 6 0 0.90 1.30 12 -6 0 2.30 1.40 -12 6 0 0.70 0.80 0 -7 0 -3.80 10.70 0 7 0 0.50 1.90 0 -7 0 -3.70 8.60 0 -7 0 15.60 10.00 0 -7 0 1.80 1.60 0 -7 0 9.70 9.20 0 -7 0 -4.80 11.10 0 7 0 0.70 1.60 0 -7 0 -1.90 5.80 0 -7 0 5.90 6.50 0 -7 0 49.60 33.30 0 -7 0 0.00 1.70 0 -7 0 3.00 5.30 0 -7 0 4.10 4.30 0 7 0 3.60 1.80 0 7 0 1.70 1.00 -1 -7 0 20.70 8.60 -1 7 0 10.30 2.30 1 -7 0 17.40 7.30 -1 -7 0 8.00 8.70 1 -7 0 8.30 35.40 1 -7 0 11.00 2.10 -1 -7 0 33.00 49.60 1 -7 0 9.40 10.20 1 7 0 12.10 2.10 -1 7 0 12.60 2.20 1 -7 0 15.60 2.30 1 -7 0 3.90 10.80 1 -7 0 14.00 2.00 -1 -7 0 8.10 8.80 -1 -7 0 7.60 4.10 1 -7 0 3.90 13.20 -1 -7 0 1.20 10.50 -1 -7 0 8.90 2.40 -1 7 0 15.50 2.70 1 -7 0 7.90 14.10 1 -7 0 13.00 4.80 1 7 0 11.90 2.00 1 7 0 12.10 2.10 1 7 0 16.00 2.30 -1 7 0 12.20 2.00 -1 7 0 14.30 1.90 -1 -7 0 2.40 8.10 1 -7 0 10.20 1.60 1 -7 0 -20.50 36.60 -1 -7 0 12.10 2.00 1 -7 0 16.40 2.20 1 -7 0 24.80 7.80 1 -7 0 7.30 6.60 1 -7 0 3.40 7.80 -1 7 0 10.70 1.60 -2 -7 0 467.05 20.80 -2 7 0 483.35 19.00 2 -7 0 485.05 18.60 2 7 0 520.45 18.90 2 -7 0 502.95 23.10 2 7 0 509.05 18.70 2 -7 0 455.25 18.60 -2 7 0 524.15 18.80 2 7 0 482.75 18.70 2 -7 0 511.85 18.80 -2 -7 0 489.95 26.10 2 -7 0 486.15 18.30 -2 -7 0 510.45 19.00 -2 7 0 502.25 18.90 2 -7 0 482.95 26.10 -2 -7 0 474.45 25.20 2 -7 0 449.06 25.20 2 -7 0 445.46 36.60 -2 7 0 493.15 18.80 2 7 0 470.75 18.60 2 -7 0 486.15 30.90 -2 7 0 478.15 18.60 2 -7 0 397.46 53.49 2 -7 0 530.85 19.10 -2 7 0 479.05 18.30 -2 7 0 501.85 18.80 2 7 0 501.95 18.80 -2 7 0 510.15 18.60 2 -7 0 478.15 26.90 2 -7 0 478.75 24.90 2 -7 0 502.65 31.60 3 -7 0 0.90 1.10 -3 -7 0 -7.40 7.60 3 -7 0 1.30 1.60 -3 7 0 2.50 1.40 -3 7 0 5.40 2.40 3 7 0 2.60 1.80 3 -7 0 -0.60 2.50 3 -7 0 1.80 1.60 3 -7 0 4.80 7.10 3 -7 0 1.80 1.50 -3 7 0 2.10 1.40 -3 7 0 5.60 1.20 3 7 0 2.00 1.60 3 -7 0 3.60 1.60 3 7 0 5.10 1.70 3 7 0 3.80 1.80 -3 7 0 2.20 1.70 3 -7 0 2.70 12.80 3 7 0 2.80 1.80 -3 7 0 2.80 1.60 3 -7 0 -15.60 15.30 -3 7 0 3.10 1.90 -3 7 0 2.00 2.20 -4 7 0 392.16 16.90 4 -7 0 427.86 16.80 -4 7 0 431.56 17.20 4 7 0 446.26 16.80 -4 7 0 419.96 16.60 -4 7 0 438.36 16.80 -4 7 0 466.15 17.10 4 -7 0 435.16 16.60 -4 7 0 453.05 17.30 4 7 0 417.96 16.50 4 7 0 431.26 16.80 4 -7 0 437.56 16.70 4 7 0 411.36 16.60 4 -7 0 452.45 16.90 -4 7 0 435.36 16.30 4 -7 0 429.36 16.70 4 -7 0 443.46 16.70 5 7 0 -0.90 1.70 5 7 0 1.10 1.70 6 -7 0 338.07 14.00 6 7 0 329.07 13.80 6 -7 0 349.07 13.80 6 7 0 329.47 13.50 -6 7 0 351.56 13.40 6 7 0 345.07 14.00 -6 7 0 360.46 14.60 6 -7 0 360.26 13.80 -6 7 0 349.27 13.80 -6 7 0 337.77 14.20 6 -7 0 346.17 13.50 6 -7 0 360.96 13.90 -6 7 0 360.26 13.70 6 -7 0 358.36 13.50 -7 7 0 0.90 1.40 -7 7 0 -1.30 1.70 7 7 0 2.30 2.10 7 -7 0 -1.00 2.00 7 -7 0 2.20 1.90 -7 7 0 -4.70 2.70 -7 7 0 6.10 2.00 7 -7 0 0.30 1.80 7 -7 0 1.90 2.10 -7 7 0 3.90 2.40 7 7 0 0.50 1.60 8 -7 0 34.10 3.60 -8 7 0 39.70 3.00 -8 7 0 36.70 5.70 -8 7 0 34.10 6.30 -8 7 0 42.10 3.50 -8 7 0 41.60 3.60 8 -7 0 38.30 4.00 8 -7 0 41.30 3.50 8 -7 0 39.00 3.50 8 7 0 46.80 3.70 8 7 0 33.70 3.10 9 -7 0 18.20 2.30 9 7 0 17.50 2.60 9 7 0 14.30 2.40 -9 7 0 19.30 2.40 9 -7 0 12.90 2.30 -9 7 0 17.50 2.80 10 7 0 1.90 1.50 10 -7 0 1.20 1.40 10 -7 0 -1.40 1.60 -10 7 0 0.30 1.30 -10 7 0 -0.30 1.10 10 -7 0 0.40 1.50 -10 7 0 1.20 1.60 10 -7 0 1.70 1.80 -11 7 0 87.99 3.90 11 -7 0 87.99 4.50 11 -7 0 78.69 4.00 11 -7 0 88.59 3.90 -11 7 0 87.59 3.70 -12 7 0 4.80 0.80 0 8 0 76.59 3.60 0 -8 0 79.49 4.90 0 8 0 78.49 4.40 0 8 0 81.99 4.30 0 8 0 70.09 4.40 0 -8 0 85.49 5.70 0 -8 0 87.09 4.60 0 8 0 79.49 4.30 0 -8 0 78.69 4.20 0 8 0 68.09 4.30 -1 -8 0 40.60 3.90 1 -8 0 52.79 3.80 1 -8 0 49.70 4.40 -1 8 0 53.89 3.70 1 -8 0 48.80 3.50 -1 8 0 51.19 3.20 -1 -8 0 47.40 3.80 -1 8 0 44.30 3.40 -1 -8 0 50.39 4.10 -1 -8 0 42.10 5.00 1 8 0 49.60 3.60 -1 8 0 44.90 3.50 1 8 0 47.50 3.40 -1 8 0 50.49 2.60 1 8 0 48.30 3.40 -1 8 0 46.10 3.40 1 8 0 47.20 3.30 -1 8 0 49.30 3.60 1 -8 0 43.50 3.60 1 -8 0 47.30 3.00 1 8 0 48.30 3.60 -2 -8 0 17.70 2.60 2 -8 0 18.70 3.10 -2 8 0 24.00 3.10 2 8 0 22.10 2.90 -2 -8 0 18.60 2.80 2 -8 0 18.20 2.80 -2 8 0 21.30 2.70 2 8 0 19.50 2.80 2 -8 0 19.50 2.00 -2 8 0 20.80 2.60 -2 8 0 17.60 2.40 -2 8 0 18.70 3.20 2 -8 0 20.50 3.10 -2 8 0 19.20 2.40 2 8 0 21.50 2.60 2 8 0 21.10 2.60 -2 8 0 18.50 2.50 2 8 0 15.70 2.60 3 -8 0 8.50 3.10 3 -8 0 14.00 2.10 -3 8 0 12.20 2.30 -3 8 0 12.10 1.80 3 -8 0 8.60 1.80 3 8 0 11.10 2.00 -3 8 0 14.10 1.90 3 -8 0 9.00 2.00 3 8 0 14.80 2.50 -3 8 0 9.00 2.00 3 8 0 10.80 1.80 3 8 0 13.50 1.80 3 8 0 13.40 2.20 3 -8 0 10.20 2.20 -3 8 0 12.70 2.10 -3 8 0 8.70 2.30 -3 8 0 11.30 1.90 4 -8 0 123.19 5.90 -4 8 0 110.99 6.20 4 8 0 115.79 5.80 4 8 0 120.69 5.90 -4 8 0 120.39 6.00 -4 8 0 119.79 6.30 4 -8 0 131.79 6.00 4 8 0 117.89 5.60 4 -8 0 122.99 6.10 4 8 0 119.29 6.00 4 -8 0 123.89 6.20 4 -8 0 129.79 5.80 -4 8 0 121.89 5.30 -4 8 0 122.49 5.70 -4 8 0 123.69 6.10 5 8 0 93.09 4.50 5 -8 0 77.79 4.90 5 -8 0 90.29 4.70 -5 8 0 86.29 5.30 -5 8 0 90.09 4.70 5 -8 0 90.49 5.00 5 8 0 91.29 5.10 5 -8 0 84.29 5.00 -5 8 0 95.99 5.80 5 8 0 75.89 4.80 5 -8 0 94.79 5.00 5 -8 0 85.79 4.60 -5 8 0 92.29 5.00 -5 8 0 78.39 5.50 -5 8 0 90.49 4.30 -6 8 0 5.40 2.60 6 -8 0 8.90 2.70 -6 8 0 2.40 2.10 6 8 0 2.00 1.90 -6 8 0 0.60 2.00 6 8 0 5.70 2.20 6 8 0 -0.60 1.90 -7 8 0 25.90 3.20 -7 8 0 27.90 2.60 7 8 0 24.20 3.00 -7 8 0 26.60 3.30 7 -8 0 27.10 3.30 -7 8 0 32.50 5.80 -7 8 0 25.10 4.50 7 8 0 27.70 3.40 -7 8 0 18.00 3.20 7 -8 0 28.70 3.40 7 -8 0 26.60 3.90 -8 8 0 0.60 1.80 -8 8 0 4.00 3.40 8 -8 0 4.10 1.90 -8 8 0 4.40 1.40 8 8 0 -0.50 2.70 -8 8 0 6.00 1.80 8 -8 0 6.40 2.00 8 -8 0 1.70 2.50 8 8 0 2.80 1.90 9 -8 0 17.00 2.60 -9 8 0 16.90 2.10 -9 8 0 16.10 2.00 -9 8 0 16.50 2.60 9 -8 0 17.50 2.40 9 -8 0 18.30 2.60 9 8 0 17.00 2.80 10 -8 0 53.09 3.60 -10 8 0 47.60 2.60 10 -8 0 48.70 2.90 -10 8 0 47.10 2.90 -10 8 0 49.30 3.10 -11 8 0 1.00 0.70 -11 8 0 0.90 1.00 11 -8 0 0.70 1.00 11 -8 0 0.90 1.40 0 -9 0 4.30 2.30 0 -9 0 0.00 1.80 0 9 0 -1.90 2.50 0 9 0 1.50 1.60 0 -9 0 -0.70 2.10 0 -9 0 0.40 2.10 1 9 0 44.90 3.60 1 -9 0 49.30 3.90 -1 -9 0 45.90 4.90 1 9 0 39.20 3.40 -1 9 0 49.30 3.10 -1 -9 0 41.90 3.70 -1 -9 0 46.30 4.10 -1 -9 0 52.29 3.40 1 -9 0 52.79 4.70 -1 9 0 48.10 3.60 1 9 0 49.50 3.80 1 9 0 41.30 3.60 1 9 0 49.50 4.50 -1 9 0 49.50 3.80 1 -9 0 45.30 3.10 -1 9 0 48.70 3.40 1 -9 0 47.30 4.30 2 -9 0 39.60 4.10 2 -9 0 35.20 3.40 2 9 0 37.00 3.50 -2 9 0 33.70 3.40 -2 -9 0 22.60 3.50 -2 9 0 35.10 3.40 -2 9 0 33.60 3.30 -2 -9 0 33.70 3.70 2 -9 0 30.50 4.40 -2 9 0 37.70 3.30 -2 9 0 35.00 3.40 -2 9 0 36.90 3.80 -2 9 0 34.50 3.60 2 -9 0 36.30 2.80 2 -9 0 31.20 3.40 2 9 0 36.70 3.00 2 9 0 36.00 3.30 -2 9 0 33.00 2.70 2 9 0 31.90 3.10 3 -9 0 85.19 4.70 3 -9 0 82.79 5.20 -3 9 0 78.79 4.80 -3 9 0 76.69 4.50 3 -9 0 86.39 5.40 3 -9 0 80.89 4.80 3 9 0 86.59 4.40 -3 9 0 78.69 4.80 3 9 0 83.39 4.60 -3 9 0 84.09 4.80 3 9 0 80.49 4.80 3 9 0 78.49 4.20 -3 9 0 78.79 4.60 3 9 0 84.89 4.70 -3 9 0 85.89 5.20 -3 9 0 80.89 4.40 4 -9 0 10.30 2.50 4 -9 0 11.00 1.90 4 -9 0 10.90 2.30 -4 9 0 15.40 2.00 -4 9 0 12.60 2.40 -4 9 0 9.20 2.30 -4 9 0 7.70 1.70 4 -9 0 9.20 2.00 -4 9 0 7.70 2.10 4 9 0 7.70 1.60 4 9 0 11.80 2.40 4 9 0 8.10 1.90 -4 9 0 11.60 2.30 5 -9 0 14.30 2.30 -5 9 0 10.30 2.40 5 9 0 11.60 1.80 5 -9 0 18.50 3.20 -5 9 0 13.60 2.40 -5 9 0 11.10 2.40 5 -9 0 11.00 2.30 -5 9 0 13.60 2.50 -5 9 0 15.00 2.10 5 -9 0 14.80 2.10 5 9 0 13.90 2.20 5 -9 0 13.10 2.20 5 9 0 21.20 3.40 5 -9 0 21.00 3.30 6 9 0 7.20 2.00 6 -9 0 9.00 1.70 6 -9 0 9.10 1.80 -6 9 0 5.60 1.90 6 -9 0 4.10 1.80 -6 9 0 4.00 2.50 6 9 0 6.20 2.10 -6 9 0 7.60 1.30 -6 9 0 4.20 2.30 6 -9 0 8.70 2.10 -6 9 0 5.80 2.60 -6 9 0 6.40 1.80 -7 9 0 23.00 3.00 -7 9 0 18.70 2.80 -7 9 0 16.50 2.10 7 -9 0 15.10 2.30 7 -9 0 17.70 2.90 7 9 0 15.80 2.50 8 -9 0 20.10 2.80 -8 9 0 20.30 2.10 8 -9 0 16.90 2.70 8 9 0 15.30 2.20 -8 9 0 18.40 2.50 -8 9 0 18.30 3.80 -8 9 0 21.70 2.80 -9 9 0 6.40 1.50 -9 9 0 6.30 1.10 9 -9 0 5.40 1.40 9 9 0 7.30 1.60 -9 9 0 4.50 1.30 10 -9 0 3.30 1.20 -10 9 0 4.00 1.40 10 -9 0 1.20 1.00 -10 9 0 1.40 0.90 -10 9 0 1.80 0.80 -10 9 0 0.60 1.10 -11 9 0 6.00 1.00 -11 9 0 7.20 0.90 0 -10 0 6.80 2.20 0 -10 0 7.60 2.00 0 10 0 7.80 2.10 0 10 0 9.40 2.20 0 10 0 7.00 2.00 0 10 0 6.40 2.00 1 10 0 5.10 2.00 -1 10 0 4.40 2.00 1 -10 0 4.70 1.50 1 10 0 5.30 1.90 1 -10 0 5.10 1.90 -1 10 0 5.80 2.10 1 10 0 6.50 1.80 -1 -10 0 9.10 2.50 1 -10 0 8.40 3.10 -1 -10 0 6.20 1.70 -1 -10 0 5.20 1.80 -1 -10 0 5.20 3.20 1 -10 0 7.70 3.70 1 -10 0 4.90 2.00 -1 10 0 5.60 2.10 -1 10 0 6.80 1.40 1 10 0 4.70 2.00 -1 10 0 5.70 2.00 2 10 0 55.39 3.70 -2 10 0 60.29 4.10 2 10 0 59.79 4.10 -2 10 0 60.39 3.60 2 10 0 59.09 3.90 -2 -10 0 54.19 4.10 -2 10 0 63.39 4.50 -2 10 0 60.99 4.20 2 -10 0 49.99 4.20 -2 -10 0 58.99 3.80 -2 10 0 56.79 3.60 2 -10 0 67.79 4.30 2 -10 0 63.59 5.20 2 10 0 59.29 3.80 2 -10 0 56.19 5.00 -2 -10 0 49.80 4.80 -2 10 0 61.29 3.90 2 10 0 63.29 4.40 -3 -10 0 98.69 5.20 -3 10 0 103.39 5.40 3 10 0 102.19 5.00 -3 10 0 93.79 5.10 3 -10 0 107.89 6.00 3 -10 0 98.69 6.20 -3 10 0 102.59 5.30 3 10 0 108.89 5.50 -3 -10 0 92.29 5.50 3 -10 0 95.89 5.50 3 -10 0 102.29 5.40 3 10 0 99.19 4.70 -3 10 0 102.29 5.00 3 10 0 104.39 5.60 -3 10 0 106.49 5.80 -3 10 0 107.79 5.50 -3 10 0 109.09 5.40 3 10 0 97.99 5.30 4 -10 0 11.00 1.90 4 10 0 17.10 2.60 -4 -10 0 14.50 2.40 -4 10 0 15.40 2.70 -4 10 0 10.50 2.20 4 10 0 11.00 2.00 -4 10 0 16.50 2.80 -4 10 0 23.10 3.40 4 -10 0 15.60 2.50 4 -10 0 21.80 4.00 -4 10 0 14.00 1.90 4 10 0 16.70 2.60 4 -10 0 18.70 2.50 -4 10 0 11.00 2.30 -4 10 0 13.40 2.30 -5 10 0 12.20 2.40 -5 10 0 11.70 2.00 5 10 0 7.90 1.60 -5 10 0 8.10 2.70 5 -10 0 8.60 2.60 5 10 0 11.80 2.00 5 10 0 11.10 2.30 -5 10 0 10.90 1.90 5 -10 0 13.60 2.40 -5 10 0 10.50 2.80 5 -10 0 5.40 2.00 5 -10 0 8.70 1.80 -5 10 0 8.00 2.10 -5 10 0 6.50 1.40 5 -10 0 12.70 2.00 5 -10 0 11.60 2.60 -6 10 0 10.00 2.50 -6 10 0 9.20 2.10 6 -10 0 6.40 2.00 -6 10 0 7.60 1.60 6 -10 0 4.70 1.90 6 -10 0 10.30 3.60 -6 10 0 10.60 3.00 -6 10 0 8.90 1.90 6 10 0 9.60 2.20 7 -10 0 70.79 4.20 -7 10 0 72.79 5.60 -7 10 0 79.79 3.90 7 10 0 73.29 4.20 -7 10 0 69.89 3.30 -7 10 0 73.19 4.00 7 -10 0 76.59 4.10 -7 10 0 74.59 5.00 -7 10 0 70.29 4.20 -8 10 0 9.00 1.20 8 -10 0 8.50 1.50 8 10 0 13.70 2.40 -8 10 0 8.80 1.40 -8 10 0 9.50 1.60 -8 10 0 12.20 1.70 -9 10 0 70.69 3.20 9 10 0 58.49 3.30 -9 10 0 64.69 3.30 -9 10 0 64.89 3.30 9 -10 0 71.49 3.20 10 -10 0 11.90 1.20 -10 10 0 10.70 1.40 10 -10 0 11.80 1.50 -10 10 0 12.40 1.30 0 -11 0 -1.30 3.90 0 11 0 2.50 1.80 0 -11 0 8.10 3.80 0 11 0 -1.60 2.00 0 11 0 0.80 1.70 0 -11 0 0.20 1.70 0 11 0 1.70 1.70 0 -11 0 2.40 1.90 1 -11 0 131.59 8.40 -1 11 0 140.29 6.50 -1 -11 0 148.09 6.20 1 11 0 134.69 6.30 1 11 0 137.49 6.30 -1 -11 0 138.79 6.50 -1 11 0 137.49 6.40 -1 11 0 142.59 6.60 1 -11 0 132.69 6.70 -1 -11 0 126.09 6.60 1 -11 0 138.49 8.30 1 11 0 140.39 6.60 1 -11 0 145.09 6.60 -1 -11 0 137.49 10.20 1 11 0 138.39 6.50 -1 11 0 140.39 6.70 -2 11 0 29.80 3.30 -2 11 0 25.80 2.60 2 11 0 35.20 2.80 -2 -11 0 30.10 4.20 2 -11 0 32.00 3.50 -2 -11 0 33.40 3.20 -2 -11 0 33.50 3.20 2 -11 0 38.40 3.50 2 -11 0 28.80 3.70 2 -11 0 44.10 5.20 2 11 0 28.50 3.00 2 11 0 28.50 3.30 2 11 0 32.70 3.40 -2 11 0 31.90 3.10 -2 11 0 32.60 3.60 -2 11 0 31.90 3.30 -3 11 0 8.70 1.60 -3 11 0 11.30 2.20 3 11 0 6.60 2.00 -3 11 0 11.40 2.10 3 11 0 7.80 1.60 3 -11 0 5.70 1.70 -3 -11 0 6.30 1.90 -3 -11 0 6.90 1.70 -3 11 0 9.20 2.20 3 11 0 5.40 1.20 -3 11 0 6.10 2.30 3 -11 0 6.00 1.90 -4 11 0 9.30 3.80 -4 11 0 6.10 2.00 -4 11 0 12.10 2.20 -4 11 0 5.80 1.50 -4 11 0 9.70 2.00 -4 -11 0 8.80 1.80 4 11 0 9.20 1.60 4 -11 0 8.80 2.30 4 -11 0 4.70 1.60 4 -11 0 7.80 1.90 4 -11 0 5.90 2.10 4 11 0 8.90 2.20 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2.70 3 12 0 1.10 1.70 3 -12 0 -0.40 1.70 -3 12 0 1.60 1.70 -3 12 0 1.80 1.50 4 -12 0 33.10 4.60 -4 12 0 22.60 2.20 4 12 0 29.10 2.90 -4 12 0 27.00 2.70 4 12 0 26.60 2.40 -4 12 0 30.20 3.00 4 -12 0 28.00 2.90 4 -12 0 27.00 2.80 5 -12 0 4.30 1.50 5 -12 0 2.70 1.30 -5 12 0 4.30 1.10 -5 12 0 4.50 1.40 5 12 0 4.50 1.60 -5 12 0 5.20 1.40 6 12 0 25.70 2.30 6 -12 0 24.60 2.20 -6 12 0 21.60 2.60 -6 12 0 25.60 1.90 -6 12 0 29.40 2.30 -7 12 0 0.90 1.00 -7 12 0 -0.10 1.50 7 12 0 0.60 1.20 7 -12 0 0.60 1.00 -7 12 0 -1.40 1.00 -8 12 0 1.80 0.90 8 -12 0 0.60 0.80 -8 12 0 0.10 0.80 0 13 0 -0.10 1.10 0 -13 0 -0.70 1.30 0 -13 0 -0.60 1.70 0 13 0 -0.10 1.20 1 -13 0 1.70 1.40 1 -13 0 3.40 1.60 -1 13 0 2.80 1.40 1 13 0 1.50 1.40 -1 13 0 2.20 1.20 1 13 0 3.20 1.30 1 13 0 3.00 1.10 2 13 0 0.30 1.20 2 -13 0 3.10 1.60 2 13 0 3.10 1.00 2 13 0 5.60 1.50 -2 13 0 1.40 1.30 -2 13 0 3.90 1.30 2 -13 0 2.70 1.50 3 -13 0 4.10 1.40 3 13 0 2.80 1.20 -3 13 0 4.70 1.30 3 -13 0 4.00 1.50 3 13 0 4.60 1.40 -3 13 0 4.20 1.40 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3 75.69 4.40 6 -2 -3 63.69 21.90 6 -2 -3 70.29 7.90 6 -2 -3 106.29 15.10 6 2 3 78.19 5.10 6 -2 -3 97.89 10.60 -6 2 -3 78.49 4.70 6 -2 -3 74.69 4.10 -6 -2 3 89.39 14.90 -6 -2 3 83.69 9.50 6 -2 -3 80.19 4.40 6 -2 -3 87.09 32.50 -6 2 -3 103.59 15.60 7 -2 3 253.67 10.30 7 -2 3 249.58 10.50 7 -2 3 254.47 10.30 -7 2 3 278.97 11.30 7 -2 3 263.57 10.20 7 2 -3 249.88 10.20 7 2 -3 243.08 10.50 7 -2 -3 258.07 10.20 7 2 3 247.88 10.50 7 2 3 258.57 10.20 7 2 3 259.37 10.20 7 2 3 252.27 10.60 7 -2 -3 257.37 10.30 8 -2 3 175.88 7.50 8 -2 3 180.18 7.70 8 -2 3 179.08 8.00 8 -2 3 178.28 7.70 8 2 -3 177.08 7.50 8 2 -3 173.88 8.00 8 2 3 191.68 9.20 8 -2 -3 179.88 8.10 8 2 3 174.58 7.70 8 2 3 166.78 8.00 8 -2 -3 185.68 7.70 8 -2 -3 166.08 8.90 9 -2 3 108.19 5.30 9 -2 3 114.99 6.10 -9 2 3 102.89 5.90 9 2 -3 109.49 5.90 9 2 -3 100.19 5.40 9 -2 3 115.39 5.60 9 -2 3 110.69 5.50 9 -2 3 110.09 5.30 9 2 3 104.99 7.40 9 -2 -3 105.39 5.20 9 -2 -3 113.69 6.20 9 -2 -3 109.59 5.50 9 2 3 112.59 5.40 9 -2 -3 113.39 5.60 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1146.49 46.80 0 -3 -3 1090.79 40.40 0 -3 3 1156.08 41.00 0 3 3 1020.90 40.30 0 3 -3 1024.10 40.30 0 -3 -3 1140.29 46.70 0 3 -3 1032.40 40.20 0 -3 3 1156.58 42.00 0 -3 3 1022.10 40.30 0 3 3 1067.39 41.30 0 3 3 1164.08 40.50 0 3 3 1032.20 42.10 0 3 3 1091.79 42.10 0 3 -3 1181.48 41.50 0 3 3 1067.39 46.90 0 -3 -3 1129.59 42.10 0 3 3 1034.70 40.20 0 -3 -3 1155.68 41.70 0 3 -3 1114.79 41.00 0 3 -3 1116.39 47.50 0 -3 3 1158.98 42.10 0 -3 -3 1163.28 40.60 0 -3 -3 1145.39 41.30 0 3 -3 1149.29 42.20 0 -3 -3 1114.49 40.90 0 3 3 1014.10 40.20 0 -3 3 1132.79 41.30 0 3 3 1055.19 41.00 0 3 -3 1147.59 42.20 -1 -3 -3 253.77 11.00 -1 3 3 245.48 10.70 1 3 -3 236.18 8.90 -1 -3 -3 235.48 9.10 1 -3 3 239.68 9.30 1 3 -3 243.68 9.70 -1 -3 -3 249.38 10.60 -1 3 3 223.88 9.20 -1 -3 -3 250.37 14.90 1 -3 3 246.28 10.10 1 -3 3 237.48 11.40 1 -3 3 253.97 17.90 1 -3 3 240.68 9.20 -1 3 3 243.88 11.70 1 3 -3 251.27 10.90 1 3 -3 253.27 10.20 1 -3 3 246.98 11.50 -1 3 3 240.88 10.20 1 3 -3 252.47 11.00 -1 3 3 262.47 9.90 -1 -3 -3 254.27 9.70 1 3 -3 224.48 8.90 1 3 -3 240.18 9.10 -1 -3 -3 243.88 9.90 1 -3 3 249.28 10.50 -1 -3 -3 249.78 10.50 -1 3 3 240.78 9.20 1 3 -3 240.88 9.70 -1 3 3 245.38 11.90 1 3 -3 234.98 16.20 -1 3 -3 248.88 10.60 1 -3 -3 251.87 11.60 1 -3 -3 246.58 10.10 1 3 3 220.88 9.00 -1 -3 3 257.37 15.10 -1 3 -3 236.48 9.30 -1 -3 3 267.77 10.10 -1 -3 3 254.27 10.70 1 3 3 223.88 9.70 1 -3 -3 241.88 9.30 1 -3 -3 244.98 10.60 -1 -3 3 213.38 9.20 -1 3 -3 242.88 9.30 -1 3 -3 236.08 10.10 1 -3 -3 240.28 9.20 1 -3 -3 267.27 17.80 1 3 3 237.48 9.00 1 3 3 225.28 10.80 -1 3 -3 230.78 17.90 -1 3 -3 253.17 11.60 -1 -3 3 261.77 9.70 1 -3 -3 248.08 11.40 1 3 3 234.48 10.80 -1 -3 3 264.97 10.90 -1 3 -3 226.08 11.40 1 -3 -3 250.47 10.50 2 3 -3 1911.31 75.39 2 -3 3 1964.80 72.79 -2 -3 -3 1979.70 70.89 2 -3 3 1929.11 71.69 -2 -3 -3 1960.20 70.99 -2 -3 -3 1918.71 73.29 -2 -3 -3 2009.70 70.79 -2 -3 -3 1735.53 70.09 2 -3 3 1877.81 79.19 -2 3 3 2022.00 71.49 -2 -3 -3 2021.60 74.59 2 3 -3 2018.40 71.49 2 -3 3 1978.70 72.69 2 -3 3 1764.82 70.29 -2 3 3 1860.41 72.79 2 -3 3 1958.70 71.19 2 3 -3 1961.30 71.49 2 -3 3 1846.32 70.29 -2 3 3 1929.81 72.99 -2 -3 -3 1893.01 70.49 -2 -3 -3 1921.41 70.39 -2 -3 -3 2054.99 70.49 -2 3 3 1938.71 71.29 -2 -3 -3 1980.70 71.99 2 3 -3 1947.31 70.89 -2 3 3 1764.82 70.29 -2 3 3 1832.92 70.29 2 3 -3 1911.41 70.59 2 3 -3 1934.31 70.89 -2 -3 3 1991.90 70.69 2 -3 -3 1987.60 72.79 -2 -3 3 1980.30 71.19 -2 -3 3 1932.21 70.59 2 -3 -3 1953.20 72.59 -2 -3 3 1758.62 70.09 -2 3 -3 1994.10 72.89 -2 -3 3 2013.80 71.59 -2 3 -3 1945.51 79.69 2 -3 -3 2036.60 71.79 -2 3 -3 1739.63 70.39 2 -3 -3 1797.02 70.29 -2 3 -3 2009.40 72.79 2 -3 -3 1879.81 70.19 -2 3 -3 1997.00 71.29 2 -3 -3 1985.10 71.19 -2 -3 3 1973.10 74.29 2 -3 -3 2050.49 79.89 2 -3 -3 1892.81 71.09 -2 3 -3 1804.72 70.29 -2 -3 3 1968.80 70.79 -2 3 -3 1848.81 71.69 3 3 -3 102.49 5.70 -3 3 3 102.99 4.40 -3 -3 -3 104.79 4.10 -3 -3 -3 98.29 3.90 3 -3 3 96.89 8.10 -3 -3 -3 99.09 5.20 3 3 -3 95.59 4.80 -3 -3 -3 104.39 7.00 3 -3 3 92.99 4.30 3 -3 3 98.79 5.80 -3 3 3 87.99 5.00 3 -3 3 98.39 4.10 3 3 -3 97.19 5.50 -3 3 3 99.19 6.10 -3 3 3 95.19 9.40 3 -3 3 91.59 6.50 -3 3 3 102.29 6.60 -3 -3 -3 100.89 4.90 -3 -3 -3 105.59 4.50 3 3 -3 100.89 4.40 3 -3 3 101.39 8.40 3 -3 3 82.89 13.20 3 3 -3 101.49 5.70 -3 -3 -3 107.59 4.20 -3 3 3 100.19 8.80 3 -3 3 87.49 6.00 -3 -3 -3 93.39 4.40 3 -3 3 92.29 9.10 3 3 -3 92.29 11.20 3 -3 3 105.89 8.70 -3 3 -3 102.79 17.10 3 -3 -3 90.79 14.10 -3 -3 3 92.99 4.00 -3 -3 3 100.29 4.30 -3 -3 3 105.29 4.50 3 -3 -3 103.79 4.80 3 -3 -3 98.69 6.80 -3 -3 3 94.29 9.30 -3 3 -3 97.09 6.40 3 -3 -3 116.89 20.30 3 -3 -3 105.49 8.30 3 -3 -3 97.09 8.10 3 -3 -3 100.69 4.10 3 -3 -3 93.49 9.20 3 -3 -3 96.79 4.20 -3 -3 3 104.39 5.20 3 -3 -3 92.09 6.50 -3 -3 3 110.99 5.10 3 -3 -3 99.39 5.70 -3 3 -3 93.99 4.40 -3 3 -3 93.09 4.60 -3 -3 3 93.99 5.50 4 -3 3 709.03 28.80 -4 3 3 727.53 26.30 4 -3 3 622.64 25.80 4 -3 3 701.63 30.40 4 -3 3 699.03 27.80 4 -3 3 720.43 28.40 -4 -3 -3 723.33 27.50 4 -3 3 691.03 25.80 4 -3 3 717.03 27.50 4 -3 3 710.23 44.10 -4 -3 -3 715.33 28.40 -4 3 3 725.73 28.90 4 -3 3 691.73 26.00 4 -3 3 680.43 30.00 -4 3 3 676.23 26.40 4 -3 3 726.43 30.80 4 -3 3 677.73 41.70 4 -3 -3 716.53 28.80 -4 -3 3 704.33 27.70 -4 3 -3 684.23 26.30 4 -3 -3 726.83 27.90 4 -3 -3 752.82 27.60 4 -3 -3 707.13 45.20 -4 3 -3 663.43 26.40 4 -3 -3 616.44 26.30 -4 -3 3 714.93 26.00 4 -3 -3 685.83 29.70 4 -3 -3 741.23 28.50 -4 -3 3 727.43 26.40 4 -3 -3 752.02 42.00 4 -3 -3 702.03 26.00 -4 -3 3 713.93 26.60 4 -3 -3 712.33 25.90 4 -3 -3 749.33 30.20 4 -3 -3 710.03 30.90 5 -3 3 78.59 12.20 -5 3 3 78.29 4.60 5 -3 3 74.49 3.20 5 -3 3 62.39 19.50 5 -3 3 63.79 6.80 5 -3 3 70.09 9.00 -5 -3 -3 72.69 8.30 5 -3 3 58.69 22.30 5 -3 3 76.49 12.40 5 -3 3 94.49 12.30 -5 3 3 79.29 4.20 5 -3 3 100.29 11.40 -5 -3 -3 74.59 7.80 -5 3 3 100.89 10.50 5 -3 3 62.19 7.80 5 -3 3 77.09 6.60 5 -3 -3 84.49 9.30 -5 -3 3 83.19 10.00 -5 -3 3 93.19 8.30 5 -3 -3 89.69 14.10 5 -3 -3 68.69 7.30 -5 3 -3 76.09 4.20 5 -3 -3 71.99 9.10 5 -3 -3 64.99 24.50 5 -3 -3 77.59 10.50 5 -3 -3 54.19 8.90 5 -3 -3 73.19 6.10 -5 3 -3 88.09 10.80 5 -3 -3 76.99 3.30 -6 -3 -3 18.10 7.10 6 -3 3 23.50 2.70 6 -3 3 19.50 2.60 -6 3 3 12.90 2.00 6 3 -3 17.30 2.50 6 -3 3 15.50 2.50 6 -3 3 15.50 2.30 -6 3 3 16.90 2.80 6 -3 -3 18.40 2.10 6 3 3 11.70 2.20 6 3 3 15.90 2.40 -6 -3 3 15.50 7.60 6 -3 -3 15.60 2.20 -6 -3 3 3.90 12.60 -6 3 -3 15.60 2.40 6 -3 -3 16.40 7.90 6 3 3 15.10 2.40 7 3 -3 69.19 4.70 -7 3 3 67.39 4.20 -7 3 3 58.89 4.80 7 -3 3 71.69 3.80 -7 3 3 69.29 4.60 7 3 -3 66.99 3.60 7 -3 3 69.49 3.80 7 -3 3 66.29 4.30 7 -3 3 68.79 3.90 7 -3 -3 69.49 3.80 -7 3 -3 59.99 7.60 7 3 3 67.59 4.40 -7 3 -3 53.89 4.50 7 3 3 61.49 4.10 7 -3 -3 73.59 4.10 7 -3 -3 70.69 4.20 7 3 3 67.09 3.70 7 3 3 70.59 3.80 -7 3 -3 62.79 4.50 8 3 -3 166.88 7.20 8 -3 3 166.38 7.20 8 -3 3 167.38 7.40 8 -3 3 178.78 7.50 -8 3 3 156.78 7.50 8 -3 3 168.78 7.70 -8 3 3 159.98 7.20 8 -3 -3 172.18 7.90 -8 3 -3 152.78 7.60 8 3 3 169.88 7.20 -8 3 -3 160.18 7.30 8 3 3 172.18 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7.70 2.30 -6 9 3 8.00 2.50 6 -9 3 7.60 1.90 6 -9 3 7.70 2.10 6 -9 -3 10.10 2.80 -6 9 -3 8.40 2.70 6 9 3 7.70 2.30 -6 9 -3 6.50 1.60 6 9 3 7.00 1.80 -6 9 -3 7.10 2.00 -6 9 -3 9.00 2.60 -6 9 -3 8.60 1.40 -6 9 -3 13.30 2.60 6 -9 -3 8.70 1.80 6 -9 -3 10.20 1.90 6 -9 -3 11.00 2.20 6 -9 -3 12.30 2.30 -7 9 3 51.49 3.50 -7 9 3 43.40 2.70 7 9 -3 42.10 3.60 -7 9 3 44.90 3.70 7 -9 3 40.90 3.40 7 -9 3 41.60 3.50 -7 9 3 40.80 4.70 7 -9 -3 45.30 3.50 7 9 3 41.90 3.80 -7 9 -3 49.10 5.50 7 -9 -3 43.00 7.30 7 -9 -3 48.50 3.50 -7 9 -3 49.30 3.50 -7 9 -3 43.50 5.10 7 9 3 42.70 4.60 -7 9 -3 43.70 3.30 -7 9 -3 44.10 2.80 -8 9 3 3.10 1.10 8 -9 3 2.60 1.60 -8 9 3 5.60 1.60 -8 9 3 3.80 1.70 8 9 -3 2.20 1.80 8 9 -3 3.20 1.50 -8 9 3 4.60 3.20 -8 9 -3 5.10 1.70 8 -9 -3 4.80 1.50 -8 9 -3 2.50 1.40 8 -9 -3 3.70 1.70 8 -9 -3 2.30 2.20 -8 9 -3 1.80 1.10 8 9 3 3.70 1.80 8 9 3 0.50 1.70 -8 9 -3 -0.80 3.60 -9 9 3 12.10 1.60 -9 9 3 10.30 1.50 -9 9 3 10.90 1.70 9 -9 3 12.00 1.50 -9 9 -3 11.70 1.60 9 -9 -3 11.00 1.60 9 9 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3.90 -2 10 -3 54.39 3.40 2 10 3 49.20 4.10 -2 10 -3 50.69 4.10 3 -10 3 149.59 7.60 3 10 -3 147.99 7.00 3 10 -3 156.88 6.70 3 10 -3 157.48 6.40 -3 10 3 154.58 7.10 -3 10 3 152.88 7.10 -3 -10 -3 143.79 6.90 -3 -10 -3 142.39 7.20 3 -10 3 145.59 7.70 3 10 -3 156.28 7.10 3 -10 3 161.08 6.90 -3 10 3 166.18 7.50 -3 10 3 144.99 6.80 3 -10 3 152.98 7.00 -3 10 3 144.19 6.60 -3 10 3 159.08 6.70 3 -10 -3 146.49 7.10 3 10 3 160.88 7.10 3 -10 -3 155.98 7.10 3 -10 -3 140.49 7.70 -3 10 -3 150.88 7.00 -3 10 -3 146.49 6.80 3 10 3 150.88 6.70 -3 10 -3 149.59 6.90 3 10 3 145.89 6.40 3 -10 -3 149.39 7.70 -3 10 -3 135.19 6.70 -3 10 -3 151.48 6.50 -3 10 -3 152.98 7.20 -3 -10 3 154.88 6.60 3 10 3 154.78 6.90 -3 -10 3 147.99 6.90 3 10 3 150.98 7.10 -3 10 -3 149.99 7.10 -4 -10 -3 5.00 2.20 -4 10 3 4.60 2.10 4 -10 3 6.10 1.90 4 10 -3 4.10 1.50 -4 10 3 3.00 2.10 -4 10 3 3.20 2.00 -4 10 3 1.60 2.00 -4 10 3 -1.00 1.90 4 -10 3 5.70 1.90 -4 10 3 2.10 1.80 4 10 -3 5.40 2.10 4 -10 3 4.50 1.70 4 10 -3 8.80 2.60 4 -10 3 5.20 2.40 4 -10 3 2.80 2.10 -4 10 3 5.30 2.00 4 -10 -3 5.90 2.00 4 10 3 3.10 1.60 4 -10 -3 4.00 2.10 -4 10 -3 5.30 2.00 -4 10 -3 5.30 1.50 4 10 3 3.00 1.70 -4 10 -3 5.40 2.20 4 -10 -3 5.40 1.90 -4 10 -3 3.40 1.60 -4 10 -3 2.90 2.00 4 -10 -3 2.60 2.20 4 -10 -3 5.80 2.40 -4 10 -3 5.20 1.90 4 10 3 2.50 1.90 4 10 3 2.30 2.20 5 10 -3 96.59 5.20 5 -10 3 102.69 5.20 -5 10 3 93.29 5.90 5 10 -3 92.39 4.70 5 -10 3 110.79 5.80 5 -10 3 93.29 5.00 -5 10 3 96.79 4.90 -5 10 3 101.39 5.70 -5 10 3 96.49 5.00 -5 10 3 95.39 5.20 -5 10 3 97.49 5.40 -5 10 -3 101.09 5.60 5 -10 -3 93.69 5.30 -5 10 -3 96.09 4.10 5 10 3 101.49 5.00 -5 10 -3 99.79 4.80 -5 10 -3 85.39 5.90 5 -10 -3 89.29 4.90 5 -10 -3 93.19 5.20 5 -10 -3 100.39 5.30 5 10 3 95.99 5.40 -5 10 -3 98.59 5.00 -5 10 -3 98.39 5.10 5 -10 -3 87.89 5.60 -6 10 3 3.10 2.00 -6 10 3 4.50 1.60 -6 10 3 4.20 2.00 -6 10 3 2.00 1.40 6 -10 3 2.00 1.50 6 -10 3 2.70 1.60 6 10 -3 2.10 1.70 -6 10 -3 3.40 1.80 6 10 3 2.30 1.90 6 -10 -3 3.80 1.90 6 -10 -3 3.60 3.40 6 -10 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3 0.70 1.80 0 11 3 7.60 2.20 0 11 3 2.70 2.10 0 11 -3 5.60 2.00 0 11 3 3.50 1.90 0 11 -3 2.40 1.70 0 -11 -3 0.10 2.10 0 -11 3 6.40 3.60 0 -11 -3 5.20 4.20 0 11 -3 2.90 1.90 0 -11 -3 1.50 1.80 0 -11 -3 8.20 4.00 -1 11 3 30.70 3.20 -1 -11 -3 20.40 3.00 -1 11 3 30.90 3.20 -1 11 3 39.60 3.70 1 -11 3 29.60 3.40 1 -11 3 39.20 5.50 1 -11 3 28.80 3.30 -1 11 3 30.00 3.40 -1 -11 -3 30.90 3.70 1 11 -3 25.60 3.00 1 11 -3 28.20 3.00 -1 -11 -3 35.70 7.50 1 11 -3 29.50 3.30 -1 -11 -3 25.60 3.40 1 -11 3 29.00 4.10 -1 -11 3 33.90 5.50 1 -11 -3 29.30 3.60 1 11 3 30.00 3.00 1 11 3 35.50 3.10 1 11 3 28.90 3.40 1 11 3 27.50 3.40 1 -11 -3 32.70 3.60 -1 -11 3 29.90 4.30 -1 11 -3 25.20 3.20 -1 11 -3 29.40 3.30 -1 -11 3 30.00 3.20 1 -11 -3 32.30 5.70 -1 11 -3 27.20 3.20 2 11 -3 33.50 3.10 2 -11 3 37.90 5.00 -2 11 3 36.80 3.50 -2 -11 -3 30.80 3.30 -2 11 3 37.10 3.40 2 -11 3 36.20 3.40 2 -11 3 32.30 3.60 2 11 -3 34.50 2.80 2 11 -3 36.20 3.40 -2 -11 -3 32.80 3.20 -2 11 3 39.60 3.70 -2 -11 -3 32.50 3.70 -2 11 -3 31.10 3.20 -2 11 -3 34.00 3.40 -2 -11 3 37.70 3.40 2 -11 -3 41.60 3.60 2 11 3 30.70 3.30 2 11 3 31.70 2.80 2 11 3 35.20 3.70 2 -11 -3 42.40 5.30 -2 11 -3 31.90 2.80 2 11 3 32.10 3.10 -2 11 -3 41.70 3.50 -2 11 -3 36.80 3.50 2 -11 -3 44.20 5.70 2 -11 -3 32.10 3.60 -2 11 -3 32.50 3.20 -3 11 3 9.30 2.00 -3 11 3 10.80 2.20 3 11 -3 13.30 2.30 -3 11 3 10.50 1.90 3 -11 3 7.40 2.50 -3 -11 -3 5.10 2.40 3 -11 3 10.90 1.90 3 -11 3 7.20 1.90 -3 -11 -3 8.60 2.00 -3 11 3 10.70 2.10 3 11 -3 8.20 1.30 3 11 -3 9.00 1.80 -3 11 3 16.00 2.50 -3 -11 -3 11.20 1.80 3 -11 -3 8.60 2.10 -3 11 -3 17.10 2.80 3 11 3 11.00 1.90 3 11 3 13.60 2.40 3 11 3 7.80 2.00 3 -11 -3 10.20 2.50 3 -11 -3 16.00 3.40 3 11 3 8.90 1.40 -3 11 -3 14.50 2.20 -3 11 -3 9.70 1.90 -3 11 -3 7.90 1.90 3 11 3 11.20 1.80 -3 11 -3 10.10 2.10 3 -11 -3 14.50 2.40 4 -11 3 88.09 5.50 4 11 -3 89.09 4.90 -4 11 3 91.09 4.40 4 -11 3 90.99 4.80 -4 11 3 86.09 4.90 4 -11 3 87.09 4.80 -4 11 3 91.19 5.10 -4 11 3 90.69 5.20 4 11 -3 89.69 4.40 -4 11 3 87.79 4.90 -4 11 -3 82.09 4.90 4 11 3 81.09 5.30 4 -11 -3 96.89 5.00 4 11 3 92.69 4.70 -4 11 -3 91.79 4.30 4 11 3 86.99 5.00 -4 11 -3 96.59 5.10 -4 11 -3 85.39 4.70 -4 11 -3 88.09 5.50 4 -11 -3 85.89 4.70 4 -11 -3 84.29 5.70 -5 11 3 7.70 2.20 -5 11 3 10.60 2.20 5 -11 3 14.90 2.50 5 11 -3 12.10 1.70 -5 11 3 12.90 2.40 5 -11 3 15.40 2.30 -5 11 3 15.30 2.30 5 -11 3 17.20 2.70 -5 11 3 12.90 2.60 5 11 -3 12.10 2.20 5 -11 -3 17.00 3.60 5 11 3 11.30 2.70 5 -11 -3 6.20 2.50 5 -11 -3 13.90 1.90 -5 11 -3 10.20 1.80 -5 11 -3 11.60 2.20 -5 11 -3 13.40 2.20 5 11 3 11.70 1.90 -5 11 -3 17.50 3.40 -5 11 -3 18.50 3.00 5 -11 -3 14.00 2.10 -6 11 3 21.80 3.00 6 -11 3 27.60 2.70 -6 11 3 31.40 2.90 6 -11 3 24.40 2.60 6 11 -3 30.60 2.80 -6 11 3 31.70 2.90 -6 11 3 26.40 3.30 -6 11 3 29.80 2.50 6 11 3 33.10 3.10 -6 11 -3 28.50 2.80 -6 11 -3 30.60 2.40 6 11 3 27.00 2.70 -6 11 -3 30.00 3.30 -6 11 -3 24.10 2.70 6 -11 -3 27.10 2.80 6 -11 -3 33.70 3.30 -6 11 -3 27.40 4.10 -7 11 3 9.10 1.70 7 11 -3 7.80 1.50 -7 11 3 7.60 1.70 7 -11 3 4.40 1.30 -7 11 3 4.40 1.20 -7 11 3 8.20 1.90 -7 11 -3 5.10 2.00 7 -11 -3 9.20 1.50 -7 11 -3 6.40 1.20 7 11 3 6.10 1.70 -7 11 -3 5.90 1.40 -7 11 -3 7.80 1.50 -8 11 3 16.00 1.60 8 -11 3 14.80 1.70 -8 11 3 15.60 1.90 -8 11 3 11.50 1.70 8 11 -3 12.80 1.80 -8 11 -3 11.30 1.80 -8 11 -3 14.20 2.20 8 11 3 11.40 1.80 -8 11 -3 13.40 1.50 8 -11 -3 11.00 1.70 -9 11 3 2.80 1.20 -9 11 3 0.20 0.80 9 -11 3 1.50 0.90 9 -11 3 0.70 0.80 9 -11 -3 -0.70 0.90 -9 11 -3 0.50 0.70 -9 11 -3 0.30 0.90 0 -12 3 31.30 3.70 0 12 3 31.30 3.10 0 12 3 34.80 3.10 0 12 3 40.80 4.20 0 12 -3 34.20 3.00 0 -12 -3 35.50 3.30 0 12 3 34.10 3.50 0 -12 3 40.10 3.20 0 -12 -3 28.90 3.50 0 12 -3 34.50 3.00 1 -12 3 26.40 3.20 1 -12 3 29.90 3.20 1 12 -3 22.10 2.60 -1 -12 -3 29.70 2.70 1 12 -3 30.80 2.60 -1 12 3 25.50 2.90 1 -12 3 36.80 6.40 1 12 -3 24.00 2.90 -1 12 3 31.90 3.10 -1 12 3 21.80 3.00 -1 -12 -3 32.30 3.40 -1 12 -3 18.60 2.80 1 -12 -3 17.90 3.70 1 12 3 18.80 2.90 -1 12 -3 25.10 2.90 1 12 3 27.40 3.20 1 -12 -3 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74.19 5.20 5 -8 -4 71.79 4.50 5 -8 -4 72.89 4.30 5 8 4 74.09 4.50 5 8 4 71.69 4.40 -5 8 -4 76.49 5.20 6 8 -4 68.09 4.40 -6 8 4 74.19 4.60 -6 8 4 73.59 4.30 -6 8 4 72.99 5.20 6 -8 4 67.29 4.00 6 -8 4 70.19 4.40 -6 8 4 67.89 5.00 -6 8 4 67.69 3.70 6 -8 4 75.79 4.40 6 -8 4 57.99 4.20 6 8 -4 66.69 3.90 -6 8 4 66.49 5.40 -6 8 -4 69.99 4.20 6 -8 -4 70.59 4.10 6 8 4 76.79 4.80 6 -8 -4 70.99 4.40 6 -8 -4 67.19 4.50 6 8 4 70.89 4.30 -6 8 -4 70.49 4.50 -6 8 -4 62.49 5.70 -6 8 -4 68.89 3.60 6 -8 -4 67.59 4.10 -6 8 -4 67.69 5.60 -6 8 -4 66.09 5.30 -7 8 4 138.79 8.20 7 -8 4 151.68 6.90 7 8 -4 145.39 6.90 7 -8 4 152.78 6.90 -7 8 4 139.99 7.90 7 8 -4 156.48 6.70 -7 8 4 157.88 7.10 -7 8 4 156.78 6.90 -7 8 4 148.19 7.90 -7 8 4 158.08 6.40 7 -8 -4 144.19 6.60 7 8 4 151.08 6.90 -7 8 -4 158.98 6.80 -7 8 -4 154.48 6.40 7 8 4 159.98 7.30 7 -8 -4 156.18 6.90 7 -8 -4 156.88 7.00 -7 8 -4 137.79 8.00 -7 8 -4 154.88 7.00 7 -8 -4 138.89 6.10 7 -8 -4 157.78 7.30 -7 8 -4 155.08 8.40 8 8 -4 39.80 4.90 -8 8 4 48.50 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5.60 0 -9 -4 113.89 5.40 0 -9 4 107.29 6.80 0 -9 4 112.59 6.40 0 -9 4 110.49 5.80 0 9 4 102.59 5.90 0 -9 -4 110.99 7.10 0 9 4 111.09 6.80 0 9 4 121.59 5.80 0 9 -4 120.09 5.70 0 -9 4 111.39 5.50 0 9 -4 118.39 5.50 1 9 -4 11.40 2.00 1 9 -4 13.70 2.20 1 -9 4 9.60 2.00 1 9 -4 12.40 2.30 -1 9 4 12.40 2.20 -1 9 4 16.50 2.50 -1 9 4 10.90 1.90 1 -9 4 12.10 2.90 -1 -9 -4 13.50 2.90 -1 9 4 11.20 2.30 1 9 -4 11.40 2.00 -1 9 4 18.30 2.90 1 9 -4 12.80 2.00 1 -9 4 10.90 2.50 1 9 4 13.10 2.20 -1 9 -4 8.80 1.90 -1 9 -4 14.20 2.30 -1 -9 4 18.70 4.40 -1 -9 4 11.20 3.20 1 9 4 12.20 2.10 1 9 4 9.10 1.90 -1 9 -4 15.00 2.10 -1 -9 4 10.70 2.80 1 -9 -4 15.50 2.60 -1 9 -4 12.40 2.10 -1 9 -4 14.00 2.50 1 -9 -4 15.20 3.10 -1 9 -4 9.90 1.80 1 -9 -4 9.30 2.10 -1 -9 4 11.80 1.90 -1 9 -4 15.30 2.50 1 -9 -4 12.50 1.80 1 9 4 11.40 2.20 2 -9 4 124.89 5.90 -2 9 4 119.69 5.30 2 -9 4 124.99 6.50 -2 9 4 117.59 5.70 -2 9 4 125.99 5.60 2 -9 4 128.99 7.00 -2 9 4 120.49 6.00 2 9 -4 123.09 5.60 2 9 -4 123.39 5.80 -2 9 4 120.09 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4 -9 13.50 4.50 1 -4 -9 15.50 22.40 -1 4 -9 8.50 16.40 1 -4 -9 9.80 5.00 -1 -4 9 10.40 4.30 1 -4 -9 13.90 4.20 -1 -4 9 13.40 3.20 -1 -4 9 14.00 2.60 -1 -4 9 15.80 2.30 -1 -4 9 9.00 2.30 1 4 9 11.60 5.30 -1 -4 9 13.60 5.40 1 -4 -9 13.50 3.50 1 -4 -9 13.20 2.10 -1 4 -9 7.60 5.40 1 -4 -9 9.00 2.60 1 -4 -9 10.00 7.60 1 4 9 9.80 3.50 -1 4 -9 19.50 2.60 -1 4 -9 10.80 3.90 1 -4 -9 11.00 1.50 1 4 9 -8.40 12.30 -1 -4 9 0.90 12.50 1 -4 -9 13.90 3.90 -1 4 -9 8.10 2.90 -1 4 -9 19.40 2.70 -2 4 9 645.44 30.30 2 4 -9 656.33 28.30 -2 4 9 647.14 52.49 2 4 -9 572.84 55.39 -2 -4 -9 612.44 24.10 -2 4 9 640.14 27.40 2 -4 9 658.33 26.00 2 4 -9 656.53 25.60 -2 -4 -9 631.64 35.10 -2 -4 -9 638.24 24.80 -2 4 9 658.23 31.40 -2 4 9 651.83 24.20 2 4 -9 665.53 24.00 -2 -4 -9 642.14 25.40 -2 4 9 634.24 28.90 2 4 -9 623.04 26.50 2 -4 9 644.84 29.50 2 -4 9 625.44 29.20 2 4 -9 605.94 27.20 2 -4 9 655.73 44.40 2 -4 9 670.33 27.00 2 4 -9 638.54 28.10 -2 -4 -9 616.44 27.20 2 -4 9 683.73 24.40 -2 -4 -9 659.13 26.40 -2 4 9 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3 4 -9 103.89 11.70 3 -4 9 102.19 7.80 3 4 -9 89.99 19.70 3 -4 9 104.99 9.40 3 -4 9 97.69 4.50 3 4 -9 94.39 6.70 -3 4 9 100.89 9.40 -3 -4 -9 86.69 14.20 3 -4 9 94.89 14.40 -3 -4 -9 89.09 4.40 -3 4 9 94.39 13.30 -3 4 -9 98.89 13.60 -3 4 -9 96.39 10.40 -3 4 -9 94.09 13.30 -3 -4 9 105.49 7.50 3 4 9 94.89 6.20 3 -4 -9 87.49 10.20 -3 -4 9 100.99 10.70 3 -4 -9 96.89 11.30 -3 4 -9 110.69 36.20 3 4 9 93.89 7.10 3 -4 -9 66.29 22.30 -3 -4 9 93.99 18.20 3 -4 -9 108.49 7.90 3 -4 -9 100.09 12.90 3 -4 -9 97.79 4.50 -3 4 -9 77.99 6.40 3 -4 -9 95.59 4.30 3 4 9 99.19 11.20 3 -4 -9 85.29 8.80 -3 4 -9 96.49 7.70 -3 -4 9 90.79 5.30 3 4 9 86.99 10.50 -3 -4 9 92.69 10.20 -3 -4 9 92.29 4.50 3 -4 -9 100.79 7.20 -3 4 -9 94.99 5.00 -3 -4 9 104.09 6.40 3 4 9 70.59 16.00 4 4 -9 293.97 11.50 -4 -4 -9 285.57 12.80 4 -4 9 280.57 11.40 -4 -4 -9 260.07 12.30 -4 4 9 276.27 11.50 -4 -4 -9 307.47 26.30 4 4 -9 289.17 17.40 -4 4 9 278.27 17.40 -4 4 9 322.87 11.70 -4 -4 -9 290.77 14.00 4 4 -9 269.17 14.70 4 4 -9 291.47 40.20 4 -4 9 268.87 14.20 4 -4 9 316.17 11.50 4 -4 9 276.07 16.40 -4 -4 -9 281.27 12.00 4 -4 9 310.17 11.20 -4 -4 -9 281.77 29.10 -4 -4 -9 297.67 14.50 -4 -4 -9 280.97 14.60 4 4 -9 303.47 11.40 4 -4 9 287.27 11.50 -4 4 9 252.97 28.20 4 -4 9 289.37 11.40 -4 4 9 300.47 19.20 -4 4 9 296.47 11.20 -4 4 9 305.87 11.70 -4 4 9 273.27 11.40 4 -4 9 329.27 52.49 -4 4 9 294.77 17.50 -4 -4 -9 288.47 17.40 -4 4 9 293.47 29.50 4 -4 -9 282.77 11.70 -4 -4 9 273.77 19.40 4 -4 -9 305.07 14.50 -4 4 -9 279.37 11.30 4 -4 -9 312.87 11.20 4 -4 -9 294.97 16.70 -4 4 -9 296.37 21.10 -4 -4 9 301.57 14.30 -4 4 -9 324.47 11.90 4 -4 -9 290.27 11.60 -4 4 -9 307.37 17.80 4 -4 -9 285.77 14.30 4 4 9 280.77 11.70 4 -4 -9 328.67 52.09 4 -4 -9 305.67 19.70 -4 4 -9 282.17 15.00 -4 -4 9 224.18 38.10 -4 4 -9 303.47 22.10 4 -4 -9 287.07 20.50 -4 -4 9 291.17 13.30 -4 4 -9 307.87 12.00 4 -4 -9 305.47 11.30 -4 -4 9 290.27 11.60 4 4 9 293.27 11.50 4 4 9 280.77 11.60 -4 -4 9 294.67 16.90 4 4 9 297.27 11.60 4 -4 -9 283.87 11.50 -4 4 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68.79 4.10 2 -5 -9 58.29 3.40 2 -5 -9 71.29 6.60 2 -5 -9 83.69 27.60 2 -5 -9 55.29 8.90 2 -5 -9 61.59 9.70 -2 -5 9 52.59 6.10 -2 5 -9 64.99 8.50 -2 -5 9 63.19 4.30 -2 5 -9 122.49 39.50 -2 5 -9 53.99 9.70 -2 -5 9 78.79 22.20 -3 5 9 227.88 28.80 -3 5 9 186.78 7.60 -3 5 9 185.38 8.00 3 -5 9 208.78 8.20 -3 -5 -9 173.18 12.10 -3 5 9 189.98 7.90 -3 -5 -9 200.08 8.90 3 5 -9 179.58 7.70 3 -5 9 186.38 7.90 -3 5 9 171.58 13.10 3 -5 9 120.59 35.40 -3 5 9 197.18 7.90 3 -5 9 193.38 15.50 -3 -5 -9 142.29 26.90 3 5 -9 190.88 7.90 -3 -5 -9 175.88 11.60 3 -5 9 187.68 12.60 -3 -5 -9 203.18 11.70 -3 5 9 193.38 8.00 3 -5 9 189.58 8.00 -3 5 9 193.78 15.90 3 -5 9 200.28 8.00 3 5 -9 195.38 7.80 3 5 -9 184.18 16.10 -3 5 -9 209.08 8.50 3 -5 -9 197.18 7.80 3 -5 -9 194.28 8.00 3 -5 -9 197.88 11.50 -3 5 -9 182.88 19.10 -3 -5 9 167.98 13.90 -3 5 -9 197.18 7.70 -3 -5 9 201.98 8.20 -3 -5 9 169.18 18.80 -3 5 -9 189.68 12.20 3 -5 -9 166.48 8.80 3 -5 -9 191.38 17.20 -3 5 -9 208.18 8.30 -3 5 -9 190.38 7.90 3 -5 -9 158.78 36.90 3 5 9 193.38 8.00 3 5 9 203.68 9.00 -3 5 -9 103.29 34.50 3 5 9 191.28 8.20 -3 5 -9 189.88 15.40 3 -5 -9 224.68 19.30 3 -5 -9 186.88 8.00 3 -5 -9 189.98 7.60 3 -5 -9 189.88 8.00 3 -5 -9 169.78 14.40 3 -5 -9 189.18 12.70 -3 5 -9 198.58 20.00 3 5 9 192.08 8.20 -3 -5 9 190.98 39.10 4 -5 9 40.90 2.70 4 -5 9 47.10 3.20 -4 -5 -9 46.50 4.50 4 5 -9 43.30 2.70 4 5 -9 43.40 3.10 -4 5 9 35.70 4.80 4 -5 9 16.40 13.90 -4 5 9 42.10 3.40 4 5 -9 39.60 4.70 4 -5 9 41.50 3.30 4 5 -9 43.70 2.80 4 -5 9 43.50 3.30 -4 5 9 45.30 3.20 -4 -5 -9 48.30 6.30 -4 -5 -9 64.99 21.10 -4 5 9 39.30 2.70 -4 -5 -9 40.20 4.90 4 -5 9 39.50 3.10 -4 5 9 43.60 3.30 -4 5 9 43.70 3.50 -4 -5 -9 37.20 6.50 -4 5 -9 49.99 4.10 -4 5 -9 47.10 7.70 4 5 9 45.10 3.20 -4 5 -9 39.20 3.00 -4 5 -9 43.90 2.90 4 -5 -9 42.40 2.70 4 -5 -9 49.70 13.60 -4 5 -9 74.39 16.50 4 5 9 40.10 3.40 4 -5 -9 23.80 10.90 4 -5 -9 100.39 62.29 4 -5 -9 39.90 3.70 -4 -5 9 46.30 4.20 4 -5 -9 41.70 2.80 4 5 9 49.99 3.60 4 -5 -9 46.30 3.00 4 -5 -9 41.80 3.30 4 -5 -9 48.30 3.40 -4 5 -9 41.40 3.60 4 -5 -9 19.20 18.50 4 5 9 41.10 3.50 -5 5 9 38.20 5.30 5 -5 9 48.00 2.90 -5 5 9 44.10 5.40 -5 5 9 46.00 3.40 5 5 -9 40.20 3.10 5 -5 9 43.10 3.30 -5 5 9 45.10 2.90 -5 5 9 42.90 3.30 5 -5 9 44.60 3.20 5 5 -9 47.90 3.20 5 -5 9 40.70 3.10 5 5 -9 45.60 2.70 -5 5 9 45.30 3.60 -5 5 -9 46.30 4.50 5 -5 -9 44.10 2.90 5 5 9 40.70 3.70 5 5 9 45.80 3.20 5 -5 -9 44.10 3.80 -5 5 -9 45.00 3.00 5 5 9 43.50 3.50 5 -5 -9 45.60 3.50 5 -5 -9 45.40 3.50 5 -5 -9 41.90 2.60 -5 5 -9 41.40 3.10 5 5 9 44.60 3.60 -5 5 -9 46.40 4.00 -6 5 9 553.94 21.30 6 -5 9 556.54 21.00 -6 5 9 543.45 20.90 -6 5 9 556.04 20.60 6 -5 9 558.34 20.80 6 5 -9 552.94 20.90 6 -5 9 543.65 20.20 -6 5 9 561.54 21.50 -6 5 9 548.55 20.90 6 -5 9 520.85 21.10 6 -5 9 542.75 20.80 -6 5 -9 536.15 21.90 6 -5 -9 558.64 21.10 6 -5 -9 559.34 20.90 6 5 9 566.64 21.00 6 5 9 552.84 21.10 -6 5 -9 539.45 21.30 6 -5 -9 517.35 20.80 6 -5 -9 562.14 20.60 -6 5 -9 537.65 21.60 -6 5 -9 564.64 20.70 -7 5 9 28.40 4.10 -7 5 9 41.50 5.00 -7 5 9 31.70 3.80 7 -5 9 36.90 4.10 -7 5 9 33.50 3.50 7 5 -9 39.10 3.10 7 -5 9 39.40 3.30 7 5 -9 32.50 3.20 7 -5 9 32.40 3.40 -7 5 9 35.80 3.00 7 -5 9 41.80 3.70 -7 5 -9 37.60 3.10 7 -5 -9 34.90 3.70 7 5 9 40.30 3.70 -7 5 -9 24.80 4.90 -7 5 -9 28.70 4.30 7 -5 -9 37.10 3.90 -7 5 -9 36.00 2.90 7 5 9 40.10 3.40 7 5 9 33.10 3.80 7 -5 -9 36.70 3.70 -8 5 9 31.50 4.90 8 -5 9 28.70 3.10 8 -5 9 30.90 3.50 -8 5 9 29.70 2.80 8 -5 9 32.80 3.80 -8 5 9 25.60 3.40 -8 5 9 22.80 4.00 8 5 -9 27.40 3.00 8 -5 -9 24.80 4.00 8 5 9 27.50 3.60 8 5 9 29.80 3.70 8 5 9 29.90 3.30 -8 5 -9 28.80 3.00 8 -5 -9 28.90 3.30 8 -5 -9 22.60 3.60 -8 5 -9 26.20 2.90 9 -5 9 32.00 2.90 9 -5 9 29.80 3.30 -9 5 9 30.30 2.70 -9 5 9 24.90 3.30 9 -5 9 25.60 3.70 9 -5 9 23.80 3.40 9 -5 9 30.80 3.00 9 5 -9 29.90 2.90 9 5 9 30.50 3.50 -9 5 -9 33.60 2.80 9 -5 -9 22.00 3.20 9 -5 -9 23.70 3.20 9 5 9 31.50 3.30 9 5 9 31.60 3.70 -9 5 -9 31.10 3.00 -10 5 9 3.50 1.60 10 -5 9 1.60 1.80 10 5 -9 3.20 1.40 10 -5 9 2.70 1.70 10 -5 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7.10 13.20 2 -6 -9 28.90 2.80 -2 6 -9 33.60 2.70 2 -6 -9 35.80 5.70 2 -6 -9 80.09 40.70 -2 6 -9 43.70 12.10 2 6 9 30.70 2.80 2 -6 -9 25.80 3.00 2 6 9 33.30 3.30 2 -6 -9 28.50 3.00 -3 6 9 174.48 7.00 3 -6 9 184.08 7.60 -3 6 9 180.08 7.50 3 -6 9 191.38 20.00 -3 6 9 179.48 7.60 3 6 -9 176.18 7.30 3 6 -9 175.68 7.20 3 -6 9 181.88 7.50 3 -6 9 266.87 69.19 3 -6 9 170.78 7.40 3 6 -9 176.28 7.60 -3 6 9 170.48 8.00 3 6 -9 177.58 7.40 -3 -6 -9 163.88 14.30 3 -6 9 154.98 25.20 -3 6 9 165.28 8.90 -3 6 9 171.68 7.40 3 -6 9 177.28 22.00 3 6 9 167.68 7.70 -3 6 -9 171.78 7.70 3 6 9 167.28 7.70 3 -6 -9 176.88 7.10 3 -6 -9 205.68 27.80 -3 6 -9 182.18 7.10 3 -6 -9 188.98 7.70 3 -6 -9 168.48 7.50 3 6 9 172.18 7.80 -3 6 -9 184.18 8.20 3 6 9 177.28 7.70 3 6 9 177.28 7.50 3 -6 -9 186.88 14.00 3 -6 -9 183.28 7.40 3 6 9 167.18 7.40 3 -6 -9 167.68 7.50 -3 6 -9 195.58 8.20 3 -6 -9 131.79 16.90 -3 6 -9 173.88 7.30 -3 6 -9 186.08 7.80 4 6 -9 157.58 6.60 -4 6 9 158.58 7.80 -4 6 9 155.78 7.00 4 -6 9 159.38 7.00 -4 6 9 169.78 7.40 -4 6 9 160.58 7.20 4 6 -9 161.48 6.90 -4 6 9 165.98 6.60 -4 6 9 160.48 7.20 4 -6 9 165.58 7.10 4 6 -9 163.78 7.20 4 -6 9 166.18 6.90 4 -6 9 168.28 7.30 4 6 -9 169.28 7.00 4 6 9 159.68 7.10 4 -6 -9 158.68 7.20 -4 6 -9 160.58 7.30 4 -6 -9 154.58 7.10 4 6 9 166.98 7.30 4 -6 -9 168.18 7.10 4 -6 -9 165.48 6.90 -4 6 -9 166.28 7.60 -4 6 -9 162.28 6.60 -4 6 -9 162.18 7.90 -4 6 -9 163.68 6.90 -4 6 -9 176.78 8.00 4 6 9 150.38 7.30 4 6 9 166.38 7.50 4 -6 -9 155.08 7.10 4 -6 -9 163.58 6.60 4 6 9 164.48 7.30 -5 6 9 165.48 7.70 -5 6 9 161.88 6.80 5 6 -9 163.08 7.40 5 -6 9 162.58 7.40 5 -6 9 167.38 6.70 -5 6 9 152.88 7.40 -5 6 9 167.78 8.30 5 6 -9 154.88 6.70 5 6 -9 180.58 7.30 -5 6 9 171.28 7.40 5 6 -9 178.98 7.60 5 -6 9 166.78 7.40 5 -6 9 171.08 7.20 5 -6 9 174.48 7.30 5 6 -9 171.88 7.40 -5 6 9 168.78 7.60 -5 6 -9 170.88 7.00 5 6 9 171.58 7.50 5 6 9 164.88 7.50 5 6 9 162.38 7.40 5 -6 -9 170.48 7.20 5 -6 -9 157.28 7.40 -5 6 -9 159.48 7.50 -5 6 -9 157.08 7.80 -5 6 -9 166.98 8.00 5 -6 -9 168.38 7.40 5 -6 -9 174.58 7.00 -5 6 -9 177.78 8.40 5 6 9 162.58 7.50 -5 6 -9 150.08 8.40 5 -6 -9 157.68 7.70 5 6 9 169.28 7.60 6 -6 9 240.88 10.10 6 6 -9 252.27 10.20 6 6 -9 245.48 10.10 6 -6 9 249.97 10.20 -6 6 9 244.58 10.40 -6 6 9 257.87 10.90 6 -6 9 251.97 10.40 -6 6 9 254.87 10.30 -6 6 9 244.38 10.70 -6 6 9 228.18 11.50 6 -6 9 252.07 9.80 -6 6 9 257.87 9.90 6 -6 -9 254.37 10.50 6 6 9 257.07 10.60 -6 6 -9 241.08 10.50 -6 6 -9 257.57 9.90 6 -6 -9 239.28 10.20 -6 6 -9 243.08 11.10 -6 6 -9 254.57 11.70 6 6 9 238.88 10.40 6 6 9 256.07 10.30 -6 6 -9 253.67 10.10 6 -6 -9 251.57 10.30 6 -6 -9 263.37 10.00 7 -6 9 22.90 4.10 -7 6 9 28.00 3.40 -7 6 9 31.70 2.80 -7 6 9 27.00 4.60 7 -6 9 29.00 3.60 7 -6 9 22.60 3.10 -7 6 9 30.10 3.70 -7 6 9 32.20 4.10 7 -6 9 31.20 3.20 7 6 -9 35.10 3.00 7 6 -9 32.00 3.00 -7 6 -9 20.90 3.70 -7 6 -9 32.20 4.60 -7 6 -9 26.70 2.80 7 6 9 29.30 3.30 7 6 9 21.30 3.60 7 -6 -9 32.80 3.60 7 -6 -9 24.80 3.50 -7 6 -9 23.90 3.00 7 6 9 30.80 3.70 8 -6 9 13.20 2.70 -8 6 9 13.40 3.30 -8 6 9 12.80 5.10 8 -6 9 16.70 2.50 -8 6 9 15.30 2.30 8 6 -9 17.10 2.70 8 -6 9 12.30 1.90 -8 6 9 15.40 1.80 8 6 9 18.50 2.90 -8 6 -9 11.90 1.80 8 -6 -9 17.50 2.20 8 6 9 24.30 3.30 8 -6 -9 19.30 2.60 -8 6 -9 11.40 1.70 8 -6 -9 15.70 2.40 -8 6 -9 11.40 4.40 8 6 9 17.60 2.50 -9 6 9 19.10 2.40 9 -6 9 21.90 2.70 9 -6 9 15.00 2.00 9 -6 9 19.00 2.50 9 -6 9 20.80 2.50 9 6 -9 23.70 3.20 9 -6 -9 17.80 3.00 9 6 9 17.80 3.30 9 -6 -9 19.00 2.50 -9 6 -9 20.80 3.00 9 -6 -9 14.10 2.90 -9 6 -9 13.30 1.80 -10 6 9 32.00 2.80 10 -6 9 32.90 2.60 10 6 -9 36.20 2.60 10 -6 9 31.90 2.60 10 -6 9 32.50 3.40 -10 6 9 32.70 2.90 -10 6 9 30.30 2.40 10 6 9 28.90 3.10 10 6 9 33.70 3.00 10 -6 -9 30.60 3.30 -10 6 -9 32.50 2.30 10 -6 -9 31.00 3.30 10 -6 -9 30.00 2.80 10 6 9 31.90 3.20 -10 6 -9 28.00 2.40 11 -6 9 1.90 1.10 -11 6 9 2.40 1.30 11 -6 9 3.50 2.00 -11 6 9 1.30 0.90 11 6 -9 2.60 1.10 11 -6 9 2.30 1.10 -11 6 9 2.00 1.20 -11 6 -9 2.10 0.90 11 6 9 5.10 1.60 11 6 9 -1.20 1.60 11 -6 -9 1.50 1.10 -11 6 -9 1.80 1.20 11 6 9 -1.80 1.50 11 -6 -9 2.50 1.50 -12 6 9 4.40 0.70 12 -6 9 3.30 0.90 12 6 -9 3.80 1.00 -12 6 -9 5.10 0.80 12 -6 -9 3.20 1.10 0 -7 -9 81.99 4.60 0 -7 -9 85.99 4.20 0 7 9 86.09 3.80 0 7 -9 86.79 4.40 0 7 9 86.09 4.60 0 -7 -9 72.59 4.70 0 7 9 87.49 4.60 0 7 9 82.49 4.90 0 7 9 83.69 4.40 0 7 -9 76.29 4.30 0 7 -9 79.09 4.20 0 -7 -9 92.19 5.40 0 7 -9 91.19 4.30 0 -7 -9 74.39 4.60 0 7 -9 84.89 4.30 0 7 -9 84.89 3.80 0 7 -9 86.99 4.40 0 7 9 79.39 4.90 0 -7 9 85.89 4.90 0 7 9 73.89 4.50 0 -7 9 87.99 5.20 -1 7 9 412.86 16.20 1 7 -9 428.06 16.10 1 7 -9 437.06 16.10 -1 7 9 384.76 16.90 1 7 -9 421.56 16.10 -1 7 9 433.66 16.20 1 7 -9 433.26 16.10 -1 -7 -9 371.56 16.20 1 -7 9 376.56 16.10 -1 -7 -9 409.56 16.30 -1 7 9 423.66 15.70 -1 7 9 415.26 16.20 -1 -7 -9 402.36 16.20 1 -7 9 438.86 16.60 1 -7 9 432.86 16.40 -1 7 9 401.16 16.10 -1 7 9 399.46 16.00 -1 7 9 433.06 15.90 -1 7 9 425.96 16.30 -1 -7 -9 416.26 16.80 1 7 -9 427.26 15.90 -1 -7 -9 398.26 15.90 -1 7 -9 419.86 15.90 -1 -7 9 441.16 16.50 1 7 9 414.46 16.20 -1 7 -9 421.76 16.20 1 7 9 399.56 16.20 1 7 9 417.56 16.30 1 7 9 407.66 16.30 -1 7 -9 432.66 16.20 1 7 9 433.56 16.20 1 7 9 418.26 16.20 -1 7 -9 418.66 16.10 -1 7 -9 432.16 16.00 1 -7 -9 430.16 16.30 -1 7 -9 427.26 16.30 1 -7 -9 411.06 16.10 1 -7 -9 423.36 16.40 -1 -7 9 434.76 16.90 1 -7 -9 415.96 15.80 1 -7 -9 400.56 16.10 2 7 -9 43.90 2.90 -2 -7 -9 41.20 4.20 -2 7 9 42.60 3.10 2 7 -9 38.90 2.90 2 7 -9 39.40 3.10 -2 7 9 35.60 3.20 -2 7 9 36.80 3.80 -2 7 9 40.60 3.50 -2 7 9 45.20 3.30 -2 -7 -9 49.30 4.40 2 7 -9 42.10 2.80 2 -7 9 36.90 3.50 -2 7 9 40.40 2.80 2 -7 9 41.20 3.30 -2 7 9 37.10 3.20 2 -7 9 38.70 3.60 -2 7 9 37.10 3.20 2 -7 9 43.50 4.00 -2 -7 -9 35.00 3.70 2 7 9 38.60 3.50 -2 7 -9 34.70 3.50 -2 -7 9 36.10 3.80 -2 7 -9 42.70 3.60 2 -7 -9 38.40 3.30 -2 7 -9 40.50 3.20 -2 7 -9 38.10 3.30 2 7 9 44.00 3.50 -2 -7 9 36.00 5.00 2 7 9 39.00 3.20 -2 7 -9 41.10 2.50 2 7 9 41.40 3.20 -2 7 -9 39.10 2.90 2 7 9 39.00 3.40 2 -7 -9 38.50 3.30 2 -7 -9 36.90 2.80 2 -7 -9 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11 -5 -10 24.30 2.80 11 5 10 24.90 2.40 11 -5 -10 21.10 3.00 -11 5 -10 26.70 2.40 -12 5 10 3.60 1.30 12 5 -10 2.50 1.00 -12 5 10 3.00 0.80 12 -5 10 3.60 1.00 -12 5 -10 2.20 0.90 12 -5 -10 2.40 1.20 0 -6 -10 64.29 3.80 0 6 -10 66.09 3.40 0 6 -10 71.79 3.90 0 -6 -10 60.69 10.80 0 6 -10 42.40 10.60 0 6 -10 65.59 3.70 0 -6 -10 64.89 7.30 0 6 10 62.19 3.90 0 -6 -10 57.89 4.00 0 6 10 67.49 4.30 0 6 10 66.69 4.00 0 6 -10 64.39 3.60 0 -6 10 67.29 4.00 0 6 10 64.29 3.20 0 -6 10 62.19 4.30 0 -6 -10 63.29 4.10 0 6 -10 63.29 3.80 0 -6 10 49.20 12.30 0 -6 -10 61.29 4.10 0 -6 -10 61.39 3.60 0 6 10 63.79 3.80 0 6 -10 77.79 11.70 0 -6 -10 67.19 11.30 0 6 -10 61.69 3.60 0 6 -10 66.99 3.80 1 -6 10 62.29 3.70 1 -6 10 48.70 8.60 -1 6 10 59.79 3.30 1 -6 10 60.79 3.80 1 6 -10 41.20 7.70 1 -6 10 77.79 18.60 -1 6 10 56.69 3.70 -1 -6 -10 53.79 9.30 -1 6 10 58.89 4.00 1 6 -10 54.19 3.50 -1 6 10 60.09 3.10 1 6 -10 62.19 3.30 -1 -6 -10 59.29 3.80 1 6 -10 58.69 3.60 1 6 -10 26.60 10.60 -1 6 10 54.69 3.70 1 6 -10 58.09 3.50 -1 6 10 62.69 3.70 1 6 -10 56.89 3.40 1 -6 10 60.09 4.10 -1 -6 -10 49.30 4.40 -1 -6 -10 49.99 4.10 1 -6 -10 55.79 3.80 -1 6 -10 65.19 3.90 -1 -6 10 60.29 3.90 -1 6 -10 57.19 3.10 1 -6 -10 53.89 3.70 1 -6 -10 54.19 8.50 -1 6 -10 53.99 3.70 1 -6 -10 68.19 9.40 -1 6 -10 64.59 10.10 -1 -6 10 34.50 13.80 1 -6 -10 62.79 3.60 1 6 10 53.29 3.60 -1 6 -10 67.49 13.50 1 -6 -10 57.29 3.30 1 6 10 57.19 3.80 1 6 10 52.39 3.90 -1 6 -10 60.99 3.60 1 6 10 51.69 4.00 -1 6 -10 57.99 3.70 1 -6 -10 34.60 37.50 -1 6 -10 51.79 9.10 -1 6 -10 55.49 3.40 1 6 10 55.69 4.00 1 -6 -10 59.09 3.80 -1 6 -10 60.49 3.80 1 -6 -10 63.69 11.50 -2 6 10 90.69 4.30 2 6 -10 87.99 4.40 2 -6 10 93.39 4.60 2 6 -10 84.49 4.30 -2 6 10 85.29 4.50 2 6 -10 93.99 4.60 -2 -6 -10 88.29 4.80 2 6 -10 87.19 4.30 2 -6 10 91.89 5.00 -2 6 10 79.19 4.90 -2 6 10 88.39 4.70 -2 6 10 87.99 4.90 -2 -6 -10 92.59 11.20 2 -6 10 90.39 4.80 2 -6 10 94.59 4.70 -2 6 10 82.29 4.50 -2 6 10 79.39 4.00 2 -6 -10 103.79 16.10 -2 6 -10 94.09 5.00 2 -6 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10 88.79 4.50 -5 6 10 81.89 4.90 5 6 -10 84.19 4.50 5 6 -10 87.79 4.60 -5 6 10 79.89 5.70 -5 6 10 90.99 5.30 -5 6 -10 71.99 6.10 -5 6 -10 87.99 5.50 5 -6 -10 81.29 4.50 -5 6 -10 86.19 4.40 -5 6 -10 76.89 5.00 5 6 10 83.29 4.70 -5 6 -10 91.39 5.90 5 6 10 79.29 5.00 -5 6 -10 86.09 4.20 5 6 10 85.89 4.80 5 -6 -10 81.99 4.20 5 -6 -10 84.59 4.80 5 -6 -10 83.59 4.90 6 -6 10 98.59 5.10 -6 6 10 104.49 6.10 -6 6 10 104.59 5.40 -6 6 10 94.69 5.40 6 -6 10 100.69 4.50 -6 6 10 86.49 7.00 6 -6 10 107.79 5.30 6 6 -10 110.89 5.20 -6 6 10 103.29 5.80 6 6 -10 104.29 5.20 6 -6 10 109.79 5.50 -6 6 10 107.59 4.90 6 6 10 105.59 5.60 6 -6 -10 105.49 4.90 -6 6 -10 101.29 6.50 -6 6 -10 109.59 5.20 6 6 10 107.29 5.80 6 6 10 106.69 5.40 6 -6 -10 105.59 5.40 -6 6 -10 111.99 5.00 6 -6 -10 100.89 5.40 -6 6 -10 98.19 7.00 6 -6 -10 108.89 5.70 -7 6 10 25.70 4.30 7 -6 10 30.70 3.10 -7 6 10 30.70 4.40 7 -6 10 30.30 3.60 7 6 -10 28.90 2.90 7 6 -10 28.90 3.00 7 -6 10 26.20 4.70 -7 6 10 32.90 2.80 -7 6 10 32.80 3.40 -7 6 10 31.20 4.70 7 -6 10 28.00 3.60 7 6 10 30.40 3.70 7 -6 -10 28.60 3.60 -7 6 -10 28.40 3.00 -7 6 -10 24.20 2.90 -7 6 -10 24.80 4.60 7 6 10 27.30 3.60 7 -6 -10 32.20 3.70 7 6 10 30.00 3.30 8 6 -10 51.19 3.50 8 -6 10 51.29 3.90 -8 6 10 45.00 3.20 8 -6 10 43.40 3.60 -8 6 10 42.80 6.20 -8 6 10 48.40 3.70 -8 6 10 53.29 4.10 8 -6 10 47.20 4.40 -8 6 10 51.29 5.80 8 -6 10 47.30 3.60 -8 6 -10 46.40 3.10 -8 6 -10 38.80 5.60 -8 6 -10 47.40 3.40 8 6 10 52.89 3.80 8 6 10 45.70 4.00 8 6 10 45.00 4.00 8 -6 -10 47.70 3.90 8 -6 -10 42.40 3.80 -9 6 10 2.40 1.60 9 -6 10 1.70 2.50 9 6 -10 4.70 2.10 9 -6 10 1.50 2.20 9 -6 10 1.80 1.80 9 6 10 2.60 2.00 9 6 10 1.10 1.60 9 -6 -10 0.20 2.40 9 6 10 3.60 1.90 -9 6 -10 3.70 1.50 -9 6 -10 2.10 1.60 -10 6 10 7.40 1.70 10 -6 10 11.10 1.90 10 -6 10 9.00 2.20 -10 6 10 9.10 1.30 -10 6 10 10.90 1.60 10 6 -10 9.50 1.50 10 -6 10 10.10 1.60 -10 6 -10 11.20 1.40 -10 6 -10 6.80 1.20 10 6 10 8.70 1.90 10 -6 -10 11.30 2.10 10 6 10 10.80 1.70 -10 6 -10 8.00 1.60 10 6 10 9.60 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10 22.40 3.70 -1 -7 -10 22.60 2.70 1 7 -10 27.30 2.60 -1 7 10 21.60 2.90 -1 -7 -10 20.70 3.20 -1 7 10 21.60 2.30 -1 7 10 21.10 3.00 -1 7 10 31.00 3.00 1 7 -10 27.10 2.70 -1 -7 -10 21.40 3.10 -1 7 -10 24.10 2.80 -1 7 -10 25.90 2.60 1 7 10 22.90 2.80 1 7 10 25.80 2.80 1 -7 -10 22.20 2.90 1 7 10 20.70 2.50 -1 -7 10 26.30 3.40 1 -7 -10 19.60 2.90 -1 7 -10 24.00 3.00 -1 7 -10 20.50 2.40 1 -7 -10 24.00 2.60 1 7 10 26.50 3.10 -1 7 -10 26.10 2.70 -1 -7 10 25.30 4.40 -1 7 -10 23.40 2.90 1 -7 -10 23.90 3.40 1 7 10 24.50 3.00 1 -7 -10 23.90 3.00 1 7 10 18.80 3.30 -2 7 10 45.50 3.70 -2 7 10 46.60 3.40 -2 -7 -10 45.10 4.00 -2 7 10 51.49 3.80 -2 -7 -10 44.70 3.60 -2 7 10 42.90 3.00 -2 7 10 40.20 3.40 -2 7 10 42.50 3.20 2 -7 10 42.80 3.70 -2 7 10 45.70 3.30 2 7 -10 47.00 3.30 -2 7 10 38.60 3.10 2 -7 10 49.50 4.10 2 -7 10 42.50 3.40 2 7 -10 40.90 2.90 -2 -7 -10 41.60 4.20 2 7 -10 40.80 3.10 2 -7 10 44.50 3.50 2 7 -10 43.30 3.00 2 7 10 43.00 3.20 2 7 10 42.30 3.30 -2 7 -10 42.50 3.50 -2 -7 10 47.20 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4 14 71.59 4.10 3 4 14 74.79 4.30 3 -4 -14 74.09 4.30 3 -4 -14 78.99 10.60 -3 4 -14 69.39 4.70 -3 4 -14 66.59 4.90 3 4 14 73.79 4.30 4 -4 14 125.59 5.80 -4 4 14 129.89 5.50 -4 4 14 130.69 5.90 4 4 -14 132.89 6.00 -4 4 14 142.49 6.40 4 -4 14 135.69 5.90 -4 4 14 126.49 5.80 4 -4 14 133.69 5.40 -4 4 14 134.89 6.20 4 -4 14 127.09 5.80 4 4 -14 124.09 5.60 -4 4 -14 129.09 5.60 4 4 14 122.09 6.10 4 4 14 131.89 6.30 4 -4 -14 120.89 6.10 -4 4 -14 129.99 6.50 -4 -4 14 125.99 6.50 -4 4 -14 130.79 5.80 4 -4 -14 125.69 5.90 4 -4 -14 125.99 5.70 -4 4 -14 141.59 7.20 4 -4 -14 125.89 6.10 4 -4 -14 127.79 5.50 4 4 14 131.59 6.10 4 4 14 127.69 6.00 -4 4 -14 137.59 6.10 4 -4 -14 136.39 5.90 4 4 14 130.99 6.20 5 4 -14 97.69 4.80 5 4 -14 102.19 4.90 -5 4 14 98.39 4.90 5 -4 14 97.99 4.30 5 -4 14 89.79 4.90 -5 4 14 93.59 5.40 5 -4 14 93.89 4.90 5 -4 14 95.89 4.80 -5 4 14 99.29 4.50 -5 4 14 92.79 4.80 -5 4 14 104.29 5.70 5 -4 -14 91.89 5.10 5 4 14 97.09 5.30 5 4 14 100.49 5.20 -5 4 -14 94.89 6.30 -5 4 -14 91.89 5.90 5 -4 -14 97.59 4.70 -5 -4 14 99.59 7.00 -5 4 -14 88.99 4.90 5 4 14 98.59 5.10 5 -4 -14 90.49 4.40 5 4 14 96.49 5.30 5 -4 -14 89.79 4.90 5 4 14 100.89 5.00 -5 4 -14 95.49 4.60 5 -4 -14 88.39 5.20 6 4 -14 246.08 9.80 6 4 -14 257.27 10.10 -6 4 14 246.78 10.20 -6 4 14 240.78 10.10 6 -4 14 245.28 10.00 6 4 -14 249.97 10.20 6 -4 14 228.78 10.50 6 -4 14 255.17 10.00 -6 4 14 250.67 9.80 -6 4 14 258.07 11.00 -6 4 14 244.48 10.80 6 -4 14 249.97 10.20 -6 -4 14 243.48 10.00 6 4 14 246.98 10.30 6 -4 -14 247.08 10.40 -6 4 -14 253.07 9.90 -6 4 -14 261.27 10.10 -6 4 -14 234.08 11.30 6 4 14 253.07 10.50 -6 4 -14 245.18 10.30 -6 4 -14 238.08 12.00 6 -4 -14 246.38 10.40 6 4 14 249.78 10.50 6 -4 -14 251.87 9.80 6 4 14 256.47 10.40 6 -4 -14 227.08 10.20 7 -4 14 1.90 1.70 -7 4 14 0.10 2.50 7 4 -14 3.40 1.90 7 -4 14 3.60 1.60 -7 4 14 1.30 1.40 7 4 -14 3.70 1.40 7 4 -14 2.20 1.70 -7 4 14 2.50 1.90 7 -4 14 1.80 2.30 7 -4 14 1.90 1.70 -7 4 14 1.80 2.00 -7 4 14 6.70 2.80 -7 4 -14 2.20 1.50 -7 4 -14 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145.39 5.90 -2 5 -14 153.38 6.90 2 5 14 138.99 6.40 2 -5 -14 143.19 6.30 2 5 14 134.79 6.50 2 -5 -14 146.39 6.30 -2 5 -14 133.29 6.00 -2 5 -14 130.79 6.50 -2 5 -14 123.79 6.70 -2 5 -14 144.49 6.40 2 -5 -14 136.09 6.30 2 5 14 151.28 6.70 2 5 14 150.88 6.50 2 5 14 142.29 6.50 2 -5 -14 130.99 6.90 -2 5 -14 141.69 5.80 -2 5 -14 147.09 6.60 -3 5 14 1.60 2.00 -3 5 14 -0.30 1.50 3 -5 14 2.60 1.40 3 5 -14 -1.10 1.30 -3 5 14 2.40 1.10 3 5 -14 2.70 1.40 -3 5 14 4.00 1.50 -3 -5 -14 -0.40 2.20 -3 -5 -14 0.60 2.00 3 -5 14 0.30 1.50 3 -5 14 5.00 1.70 3 5 -14 1.80 1.20 -3 5 14 2.50 1.70 -3 5 14 -0.40 1.30 -3 -5 -14 2.20 2.20 3 -5 14 1.00 1.60 3 5 14 1.20 1.60 -3 5 -14 0.20 1.30 -3 5 -14 1.80 1.80 3 -5 -14 1.80 1.40 -3 5 -14 3.30 1.20 3 -5 -14 3.40 2.10 3 5 14 -2.10 2.40 -3 5 -14 0.40 1.80 3 -5 -14 2.80 1.50 3 5 14 3.10 1.80 3 5 14 2.50 1.80 3 -5 -14 2.40 1.40 -3 -5 14 3.20 1.90 3 5 14 0.80 1.60 -3 -5 14 1.20 3.00 -3 5 -14 0.60 2.00 3 -5 -14 3.60 1.20 -3 5 -14 -0.80 1.70 3 -5 -14 -0.10 1.50 4 -5 14 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14 80.19 4.00 -6 5 14 76.79 5.50 6 -5 14 79.29 4.40 6 5 -14 76.49 4.30 6 -5 14 71.69 4.20 6 5 -14 69.29 3.80 -6 5 14 73.59 5.20 -6 5 14 64.69 6.50 -6 5 14 84.99 4.60 6 5 -14 85.49 4.50 6 5 14 81.79 4.90 -6 5 -14 78.39 6.70 -6 5 -14 80.59 4.70 -6 5 -14 84.09 4.10 -6 5 -14 75.49 4.30 -6 5 -14 65.39 6.10 6 -5 -14 74.59 4.00 6 5 14 84.29 5.00 6 -5 -14 65.49 4.60 6 5 14 77.19 5.00 6 -5 -14 68.19 4.70 6 5 14 76.49 4.60 -7 5 14 247.88 9.70 7 -5 14 245.88 10.00 -7 5 14 244.38 10.20 7 5 -14 243.28 10.00 7 -5 14 229.78 10.60 7 -5 14 256.77 10.40 -7 5 14 227.38 11.00 7 -5 14 241.68 10.00 -7 5 14 246.28 10.20 7 5 -14 243.68 10.20 -7 5 14 237.88 11.10 -7 5 -14 253.27 10.30 7 5 14 260.47 10.30 7 5 14 246.48 10.50 -7 5 -14 260.67 10.00 7 5 14 250.77 10.50 -7 5 -14 215.88 12.10 -7 5 -14 245.08 9.70 7 -5 -14 241.48 10.40 8 5 -14 50.09 3.40 8 -5 14 48.00 3.50 8 -5 14 48.20 3.70 -8 5 14 44.20 3.80 -8 5 14 51.69 3.80 -8 5 14 40.50 4.90 8 -5 14 55.79 5.70 8 -5 14 46.70 3.40 -8 5 14 53.09 3.30 -8 5 -14 47.80 3.20 8 5 14 49.80 4.00 8 -5 -14 46.30 3.90 -8 5 -14 47.40 3.30 -8 5 -14 45.30 3.70 8 5 14 52.39 3.80 8 5 14 52.49 4.20 9 -5 14 20.00 3.30 9 -5 14 23.50 2.80 9 -5 14 18.50 2.80 9 -5 14 19.70 2.50 -9 5 14 21.90 2.60 9 -5 14 19.10 2.50 9 5 -14 20.00 2.60 -9 5 14 23.80 3.00 -9 5 14 22.90 2.40 -9 5 -14 18.00 2.70 9 5 14 24.20 3.10 9 5 14 20.80 2.90 9 -5 -14 21.50 2.90 -9 5 -14 24.10 2.50 -9 5 -14 21.30 2.30 9 5 14 24.90 3.30 10 -5 14 6.00 1.30 -10 5 14 8.00 1.50 10 -5 14 8.40 1.90 -10 5 14 5.70 1.20 10 5 -14 4.80 1.30 10 -5 14 6.60 1.30 10 -5 14 5.60 2.20 10 -5 -14 8.20 1.50 10 5 14 7.90 1.80 10 5 14 8.40 1.60 -10 5 -14 7.70 1.20 10 -5 -14 7.50 1.80 -10 5 -14 6.70 1.40 -10 5 -14 6.70 1.20 -11 5 14 2.00 1.10 11 -5 14 0.70 1.00 -11 5 14 1.70 1.20 11 5 -14 1.60 1.00 -11 5 14 1.30 0.80 11 5 14 2.40 1.20 -11 5 -14 1.90 2.40 -11 5 -14 4.10 1.30 11 -5 -14 0.80 1.20 -11 5 -14 0.70 0.80 11 5 14 0.80 1.50 11 5 14 3.10 1.50 11 -5 -14 1.40 1.30 0 6 14 172.78 6.80 0 6 14 159.68 7.20 0 -6 -14 156.68 7.10 0 -6 -14 159.28 6.80 0 -6 -14 173.38 7.30 0 6 -14 163.18 6.80 0 6 14 159.38 7.20 0 6 -14 175.58 7.50 0 -6 14 165.28 7.60 0 6 -14 165.48 7.20 0 -6 14 167.68 7.20 0 6 14 157.68 7.20 0 6 14 163.58 7.30 0 6 -14 156.28 7.10 0 -6 14 167.08 7.80 0 -6 -14 158.58 7.10 0 6 -14 169.28 7.10 0 6 -14 166.48 7.10 0 -6 -14 161.68 7.60 1 6 -14 132.69 6.10 1 -6 14 131.69 6.20 -1 6 14 139.79 5.70 1 -6 14 150.48 6.90 -1 -6 -14 137.09 5.90 1 6 -14 136.39 6.20 1 6 -14 140.39 6.10 -1 6 14 136.39 6.30 -1 6 14 129.39 6.30 -1 6 14 134.39 6.30 -1 -6 -14 136.19 7.00 -1 6 14 138.09 6.10 -1 -6 -14 136.29 6.30 1 -6 14 143.59 6.70 1 6 -14 129.19 5.90 -1 6 14 136.99 6.10 1 6 -14 139.89 6.20 -1 -6 -14 139.39 6.40 -1 6 -14 134.59 6.40 1 -6 -14 145.49 6.60 -1 6 -14 128.79 5.90 -1 6 -14 144.49 6.30 -1 6 -14 140.39 6.70 1 -6 -14 133.09 6.20 -1 -6 14 141.29 6.80 1 6 14 137.39 6.20 -1 -6 14 133.79 6.30 1 6 14 128.79 6.30 -1 6 -14 146.79 6.20 1 6 14 143.99 6.40 1 6 14 128.99 6.50 -1 6 -14 132.99 6.30 1 -6 -14 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3.10 1.60 6 5 -22 3.30 1.60 -6 -5 -22 7.70 1.50 -6 5 22 8.70 2.90 -6 5 -22 5.60 1.50 6 -5 -22 8.00 2.00 -6 5 -22 2.70 1.20 6 5 22 5.20 2.00 6 5 22 3.80 1.70 6 5 22 7.30 2.00 6 5 22 5.50 2.00 -6 5 -22 6.30 6.00 -6 5 -22 4.40 1.60 -6 -5 22 4.20 1.40 -6 -5 22 6.20 1.50 7 -5 22 3.50 1.40 -7 -5 -22 4.90 1.30 -7 5 22 6.40 1.50 7 5 -22 7.00 1.50 -7 5 22 3.40 1.10 -7 5 22 3.80 1.50 7 5 22 6.70 1.90 -7 -5 22 6.00 1.70 -7 5 -22 4.00 1.10 7 5 22 5.10 1.60 7 5 22 7.10 1.90 -7 5 -22 6.40 1.30 -7 5 -22 4.70 1.60 7 -5 -22 6.00 1.60 -7 -5 22 4.00 1.40 -7 -5 22 4.80 1.00 -8 5 22 4.80 1.20 -8 -5 -22 5.00 1.30 -8 5 22 5.30 1.30 8 -5 22 5.00 1.30 -8 5 22 5.70 1.10 8 -5 22 1.80 1.20 -8 5 22 5.60 1.40 8 5 -22 4.90 1.20 8 5 22 2.10 1.20 -8 -5 22 3.70 0.90 -8 5 -22 4.50 1.10 -8 -5 22 3.80 1.60 8 5 22 6.60 1.60 8 -5 -22 6.90 1.40 8 5 22 5.80 1.60 -8 5 -22 4.30 0.90 -9 5 22 30.80 2.20 -9 5 22 27.60 2.70 9 5 -22 31.70 2.00 9 -5 22 31.30 2.10 -9 5 22 37.70 2.40 -9 -5 22 35.30 1.80 9 -5 -22 30.00 2.20 9 -5 -22 36.30 2.50 -9 5 -22 36.30 2.00 9 5 22 33.20 2.10 9 5 22 31.90 2.60 9 5 22 39.50 2.70 -9 5 -22 34.50 2.00 0 6 22 48.40 3.60 0 -6 -22 34.80 3.90 0 -6 22 36.00 3.30 0 -6 -22 41.40 5.10 0 -6 22 37.60 5.10 0 6 -22 36.40 3.40 0 6 22 39.90 3.80 0 6 22 40.80 3.60 0 -6 22 33.60 4.50 0 -6 -22 36.50 3.20 0 6 -22 42.10 3.40 0 -6 -22 35.80 3.80 0 -6 -22 42.50 5.40 0 -6 22 40.20 3.10 0 6 -22 35.10 3.00 -1 6 22 125.39 6.20 -1 -6 -22 128.99 6.20 1 -6 22 126.09 7.00 1 6 -22 123.69 6.00 -1 6 22 126.49 6.20 1 -6 22 109.89 6.90 -1 6 22 122.39 5.90 1 6 -22 127.79 5.70 -1 -6 -22 127.59 5.70 1 6 -22 124.19 6.00 1 -6 22 122.69 5.80 -1 -6 -22 102.99 7.90 -1 -6 -22 130.09 6.20 1 -6 22 126.89 6.00 1 -6 -22 137.79 7.60 1 6 22 124.39 5.90 1 6 22 132.09 6.30 -1 -6 22 115.69 7.30 1 -6 -22 132.79 7.40 1 -6 -22 115.39 7.10 -1 6 -22 103.89 6.70 -1 6 -22 131.29 6.00 1 -6 -22 131.39 6.30 -1 -6 22 119.69 5.80 1 6 22 129.99 6.30 -1 -6 22 126.69 5.80 -1 6 -22 130.59 6.20 1 -6 -22 123.49 5.60 -1 6 -22 122.49 6.80 -1 -6 22 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-27 25.50 1.50 2 9 -27 22.50 1.60 2 9 -27 25.10 1.50 -2 9 27 24.20 1.80 -2 9 -27 24.50 1.60 2 -9 -27 23.10 1.80 -2 -9 27 23.40 1.70 2 -9 -27 24.10 1.80 -2 -9 27 23.10 1.60 -2 9 -27 27.50 1.80 -2 9 -27 23.80 2.30 -3 -9 -27 8.10 1.00 3 9 -27 5.60 0.90 -3 9 27 4.40 1.00 -3 -9 27 4.80 0.90 -3 -9 27 5.70 0.90 0 0 -28 5.90 2.10 0 0 -28 -0.60 1.70 0 0 -28 3.70 2.00 0 0 28 7.70 2.20 0 0 28 3.30 2.00 0 0 -28 1.60 1.20 0 0 28 0.50 1.70 0 0 28 3.60 1.60 0 0 -28 0.30 2.50 -1 0 -28 0.80 2.70 1 0 -28 1.00 2.00 -1 0 -28 0.80 1.30 1 0 28 3.40 1.80 -1 0 -28 3.90 2.20 1 0 28 2.80 1.80 -1 0 28 2.10 2.20 -1 0 28 0.50 1.70 1 0 -28 -4.40 2.30 1 0 -28 2.70 1.80 1 0 28 0.30 2.30 -1 0 28 0.30 1.70 2 0 -28 14.50 2.20 2 0 28 13.00 2.10 -2 0 -28 10.80 2.10 2 0 28 9.80 2.00 2 0 -28 14.90 2.00 -2 0 -28 11.80 3.60 2 0 28 12.70 2.30 -2 0 28 12.70 2.00 -2 0 28 18.30 2.60 2 0 -28 8.50 2.60 2 0 -28 8.40 2.00 -2 0 28 12.00 2.10 -2 0 -28 11.00 1.50 -2 0 28 13.20 2.70 3 0 -28 0.10 1.70 3 0 28 -0.90 1.60 3 0 28 -0.20 1.70 -3 0 -28 1.90 1.20 3 0 -28 0.70 1.80 -3 0 28 2.50 1.60 -3 0 28 -2.10 1.50 -3 0 28 2.20 2.60 -3 0 -28 1.30 1.40 -3 0 -28 4.60 4.20 -3 0 28 0.60 1.40 3 0 -28 -1.90 1.70 3 0 28 0.70 1.70 3 0 -28 -5.60 3.30 4 0 -28 6.00 1.70 -4 0 -28 6.30 1.30 -4 0 28 5.50 1.60 4 0 28 6.60 1.70 -4 0 28 4.80 1.60 4 0 28 5.90 1.70 -4 0 28 6.60 1.10 -4 0 28 4.50 1.50 -4 0 -28 3.80 1.50 4 0 28 5.20 1.80 -5 0 28 2.40 1.40 -5 0 28 0.00 1.60 5 0 -28 2.30 1.50 -5 0 28 0.10 1.30 5 0 28 0.20 1.40 5 0 28 -0.10 1.40 -5 0 -28 -0.70 1.10 -5 0 -28 1.70 1.30 5 0 28 2.00 1.70 -5 0 28 -0.40 0.90 6 0 28 173.48 7.10 -6 0 -28 167.68 6.70 -6 0 -28 171.58 7.00 6 0 28 171.18 7.20 -6 0 28 167.38 7.00 6 0 -28 170.98 7.10 -6 0 28 172.48 7.00 -6 0 28 175.78 6.60 7 0 28 14.90 1.90 -7 0 -28 17.90 1.90 -7 0 28 20.00 1.50 -7 0 28 18.30 1.80 -7 0 28 21.90 2.00 -7 0 -28 16.90 1.50 8 0 28 -0.10 1.10 -8 0 -28 0.60 0.70 -8 0 28 0.90 0.90 -8 0 28 2.20 1.00 0 -1 28 5.70 2.10 0 -1 -28 5.40 2.70 0 -1 -28 7.10 2.70 0 1 -28 0.00 2.40 0 1 28 5.20 1.70 0 -1 -28 4.90 1.30 0 -1 -28 5.60 2.30 0 -1 28 6.10 1.60 0 1 -28 6.50 2.20 0 -1 28 8.60 2.00 0 1 28 4.00 2.20 0 -1 -28 9.60 3.00 0 1 -28 10.10 2.00 0 -1 28 4.90 2.00 0 1 28 9.90 2.20 0 1 28 3.00 2.00 -1 1 28 22.90 2.90 1 -1 28 28.30 3.60 1 1 -28 28.40 3.40 -1 1 28 29.90 2.90 -1 -1 -28 26.20 3.80 1 -1 28 37.40 3.40 -1 1 28 22.80 3.60 -1 -1 -28 28.60 3.40 -1 -1 -28 27.60 2.70 1 -1 28 26.80 2.90 1 1 -28 24.90 4.00 1 1 -28 32.00 3.50 1 1 -28 30.00 3.40 1 -1 -28 21.70 3.20 -1 1 -28 32.50 3.90 -1 1 -28 25.00 3.40 -1 -1 28 26.00 3.60 1 -1 -28 29.30 3.80 1 -1 -28 30.60 3.30 1 1 28 30.50 3.50 -1 1 -28 29.40 2.30 -1 -1 28 28.60 3.00 2 1 -28 32.30 3.10 -2 -1 -28 22.70 4.20 -2 1 28 37.60 3.00 -2 1 28 29.60 4.10 -2 -1 -28 41.80 3.30 2 1 -28 34.90 3.40 -2 1 28 32.80 3.40 -2 1 28 36.80 3.20 2 -1 28 33.50 3.50 2 -1 28 36.70 3.20 -2 -1 -28 37.10 2.70 2 1 -28 29.80 3.60 2 -1 28 32.80 3.30 -2 -1 28 34.40 3.10 2 -1 -28 26.80 3.30 -2 1 -28 33.00 4.60 -2 1 -28 33.90 2.50 2 -1 -28 36.20 3.70 2 -1 -28 34.40 4.10 2 1 28 28.10 3.30 -2 -1 28 34.30 3.00 -2 -1 28 29.60 4.30 -2 -1 28 38.90 3.20 -2 1 -28 33.70 4.20 -2 1 -28 35.50 3.10 2 -1 -28 33.70 3.30 2 1 28 38.60 3.60 -3 1 28 59.99 4.70 -3 -1 -28 51.79 3.10 -3 -1 -28 57.79 3.60 3 1 -28 49.70 3.70 3 -1 28 51.19 3.50 3 -1 28 58.19 3.80 3 1 -28 49.60 3.90 3 -1 28 55.29 3.60 -3 1 28 55.69 3.60 -3 1 28 51.19 3.60 -3 1 28 51.89 3.50 3 -1 -28 53.69 3.70 -3 -1 28 50.99 3.40 3 1 28 54.39 3.90 3 -1 -28 40.80 4.60 3 -1 -28 47.30 3.50 -3 -1 28 49.90 3.40 3 1 28 50.39 3.70 -3 1 -28 56.29 3.00 -3 -1 28 49.20 5.40 -3 -1 28 52.99 2.70 3 1 28 48.90 3.80 -3 1 -28 42.90 6.50 -3 -1 28 55.89 3.40 -3 1 -28 54.19 3.40 4 -1 28 41.50 3.20 -4 -1 -28 46.20 2.80 4 -1 28 36.70 3.20 -4 1 28 38.20 3.20 -4 1 28 40.00 3.20 4 -1 28 47.30 3.40 -4 1 28 43.00 3.10 4 1 -28 43.90 3.40 -4 -1 -28 45.00 3.10 4 -1 -28 45.50 3.70 4 1 28 41.60 3.30 -4 -1 28 43.00 3.00 -4 -1 28 44.90 2.40 -4 1 -28 39.30 2.70 -4 -1 28 42.10 3.00 4 1 28 45.20 3.50 -4 1 -28 44.70 3.10 4 1 28 41.10 3.40 4 -1 -28 45.00 3.40 -4 -1 28 42.80 3.00 -5 -1 -28 13.40 1.70 5 1 -28 8.10 1.70 -5 1 28 11.40 1.90 5 -1 28 10.30 2.00 -5 1 28 7.40 1.50 -5 1 28 11.30 1.70 -5 -1 -28 9.80 1.30 -5 1 28 9.60 1.70 5 -1 28 8.00 1.70 5 -1 28 6.90 1.60 5 1 28 11.10 1.90 5 1 28 9.50 1.80 -5 -1 28 10.30 1.60 -5 -1 28 7.90 1.60 -5 -1 28 8.60 1.10 5 1 28 9.00 1.80 -5 1 -28 8.60 1.30 -5 -1 28 10.70 1.60 -5 1 -28 6.60 1.40 5 -1 -28 9.70 1.80 6 -1 28 4.70 1.50 6 -1 28 1.40 1.30 -6 1 28 2.00 1.50 6 1 -28 3.60 1.30 -6 1 28 4.80 1.40 -6 -1 -28 5.50 1.10 -6 -1 -28 4.50 1.30 -6 1 28 6.40 1.30 6 -1 -28 2.90 1.40 -6 1 -28 5.30 1.20 -6 -1 28 4.80 0.90 -6 1 -28 5.20 1.10 -6 -1 28 3.20 1.30 -6 -1 28 4.20 1.30 6 1 28 4.10 1.50 -7 1 28 8.10 1.30 7 -1 28 6.90 1.30 -7 -1 -28 7.80 1.00 7 -1 28 7.40 1.40 -7 1 28 6.90 1.20 -7 -1 -28 7.30 1.30 7 1 28 7.30 1.70 -7 -1 28 6.20 1.20 -7 -1 28 5.80 1.10 -7 -1 28 8.30 1.20 -7 1 -28 6.60 1.20 -7 1 -28 5.90 0.90 8 -1 28 47.60 2.30 -8 1 28 43.90 2.30 -8 -1 -28 45.30 2.10 -8 1 28 43.40 2.30 -8 1 -28 42.10 2.00 -8 -1 28 41.20 2.30 -8 -1 28 41.30 2.20 8 1 28 42.70 2.30 0 2 28 53.79 3.90 0 2 28 55.59 4.70 0 2 28 60.59 4.00 0 -2 -28 57.79 4.60 0 -2 -28 56.89 5.80 0 -2 28 77.19 5.60 0 2 -28 53.69 4.00 0 -2 -28 64.59 3.20 0 2 -28 57.89 4.20 0 -2 28 61.09 4.70 0 -2 -28 67.89 4.10 0 -2 28 60.79 3.70 0 2 -28 59.09 5.20 0 -2 -28 58.69 4.90 0 -2 28 62.29 4.40 0 2 -28 63.79 3.70 -1 2 28 5.90 1.90 1 2 -28 8.20 2.00 1 2 -28 3.80 1.70 -1 2 28 4.40 1.80 1 -2 28 5.90 1.90 1 -2 28 6.50 2.20 1 -2 28 7.70 1.90 -1 -2 -28 5.10 1.40 1 -2 28 7.60 1.60 -1 2 28 9.00 1.70 -1 -2 -28 5.20 1.80 -1 -2 -28 2.50 3.10 1 2 -28 4.20 1.80 1 2 -28 5.20 2.50 -1 -2 28 4.80 1.50 -1 2 -28 4.40 1.60 1 -2 -28 3.30 1.90 1 2 28 5.50 2.00 -1 -2 28 5.10 1.90 -1 2 -28 8.00 2.70 -1 2 -28 4.80 1.50 1 -2 -28 5.00 1.80 -1 -2 28 7.20 1.90 -1 2 -28 4.70 1.80 1 -2 -28 7.80 1.90 1 -2 -28 4.70 2.70 2 -2 28 7.70 1.80 -2 2 28 7.70 1.80 2 -2 28 11.10 1.90 -2 2 28 8.10 1.90 2 2 -28 6.30 1.80 -2 -2 -28 8.40 4.10 2 -2 28 13.80 2.00 2 2 -28 8.90 1.90 -2 2 28 10.70 2.50 2 2 -28 12.30 1.90 -2 2 28 11.40 1.80 2 2 -28 9.00 2.80 -2 -2 -28 12.30 2.00 -2 -2 -28 8.60 1.50 -2 -2 28 10.80 1.80 -2 2 -28 8.50 1.70 -2 -2 28 10.60 2.90 2 -2 -28 11.50 2.10 2 -2 -28 10.00 2.70 -2 2 -28 12.40 1.90 -2 -2 28 8.20 1.60 -2 2 -28 11.00 3.10 2 -2 -28 14.80 2.00 -2 2 -28 12.70 2.50 2 -2 -28 10.70 2.10 -2 -2 28 11.20 1.90 2 2 28 11.40 2.10 -3 2 28 8.00 1.70 3 -2 28 13.10 1.90 3 2 -28 11.70 2.20 3 -2 28 13.20 2.00 -3 -2 -28 12.80 1.50 3 2 -28 13.60 2.10 -3 -2 -28 11.60 1.80 -3 2 28 15.00 2.00 3 -2 28 14.90 1.90 -3 2 28 14.50 2.40 -3 2 28 9.70 2.70 3 -2 -28 11.80 2.00 -3 -2 28 13.90 1.80 3 2 28 15.40 2.40 3 -2 -28 13.80 1.90 -3 -2 28 12.30 1.70 -3 2 -28 13.70 4.60 -3 -2 28 13.90 1.90 -3 -2 28 12.30 3.20 3 -2 -28 11.80 2.20 -3 -2 28 12.00 1.80 3 2 28 12.00 1.90 3 -2 -28 12.80 2.80 -3 2 -28 10.50 1.70 -3 2 -28 15.70 1.90 -4 2 28 21.00 2.70 4 -2 28 22.50 2.50 4 2 -28 19.10 2.70 -4 -2 -28 19.80 2.50 -4 -2 -28 17.30 2.20 -4 2 28 20.80 2.40 4 -2 28 21.00 2.70 4 -2 28 17.50 2.00 -4 2 28 16.20 2.40 4 -2 -28 19.70 2.90 4 -2 -28 22.30 2.70 -4 -2 28 19.90 2.40 4 -2 -28 21.20 2.70 -4 -2 28 19.50 1.70 -4 2 -28 17.20 2.40 4 2 28 21.30 2.80 4 2 28 20.20 2.70 -4 2 -28 17.30 2.00 -4 -2 28 19.00 2.40 -4 -2 28 19.30 2.40 -5 -2 -28 22.70 2.40 5 -2 28 22.30 2.40 -5 -2 -28 25.00 2.10 -5 2 28 22.70 2.40 -5 2 28 26.20 2.50 5 2 -28 22.30 2.50 5 -2 28 22.00 2.60 -5 -2 28 26.40 1.80 -5 -2 28 21.20 2.30 -5 -2 28 28.00 2.50 5 2 28 29.10 2.80 5 -2 -28 23.30 2.90 -5 2 -28 25.30 2.00 -5 -2 28 26.60 2.40 5 2 28 28.60 2.60 5 -2 -28 20.90 2.70 -5 2 -28 22.00 2.30 -6 -2 -28 20.10 1.70 6 -2 28 16.20 2.10 6 2 -28 20.70 2.10 -6 2 28 21.90 2.10 -6 -2 -28 18.90 2.10 6 -2 28 17.60 2.30 -6 2 28 16.40 2.00 6 2 28 16.50 2.20 -6 2 -28 18.10 1.90 -6 2 -28 19.70 1.70 -6 -2 28 19.20 1.50 -6 -2 28 17.30 2.00 6 -2 -28 18.50 2.30 -6 -2 28 17.50 1.90 -7 -2 -28 5.90 1.40 -7 2 28 5.90 1.20 -7 2 28 4.20 1.30 7 -2 28 2.50 1.40 7 -2 28 5.30 1.60 -7 2 -28 4.30 1.00 7 2 28 6.30 1.30 -7 -2 28 3.80 1.10 -7 -2 28 4.50 0.80 -7 -2 28 3.80 1.30 -7 2 -28 4.40 1.00 -8 2 28 8.60 1.00 -8 2 28 10.90 1.40 -8 -2 -28 9.80 1.10 8 -2 28 8.70 1.40 8 2 28 7.20 1.60 -8 -2 28 11.30 1.30 -8 2 -28 8.70 1.10 0 -3 -28 5.30 2.80 0 -3 28 0.60 1.50 0 3 -28 1.90 1.70 0 3 28 4.40 1.80 0 -3 -28 2.20 1.90 0 -3 -28 2.90 1.80 0 -3 -28 4.60 2.80 0 -3 28 2.90 1.40 0 3 -28 3.40 1.50 0 -3 28 1.60 1.90 0 -3 28 3.00 2.30 0 -3 -28 1.40 1.20 0 3 -28 0.70 2.60 0 3 -28 2.20 1.70 0 3 28 -1.10 1.80 1 3 -28 18.10 3.00 -1 -3 -28 19.60 3.00 1 -3 28 23.20 3.80 1 -3 28 25.10 2.60 1 3 -28 22.30 2.70 -1 3 28 25.20 3.00 1 -3 28 24.80 2.80 -1 3 28 21.50 3.00 -1 -3 -28 20.30 3.00 1 3 -28 21.30 2.90 1 3 -28 23.90 2.80 1 -3 28 23.70 3.00 -1 -3 -28 35.30 5.70 -1 -3 -28 25.90 2.40 -1 3 28 28.70 2.90 -1 -3 28 20.10 3.10 1 -3 -28 23.80 3.10 -1 3 -28 28.20 3.10 -1 -3 28 22.30 2.80 -1 -3 28 17.00 2.70 1 -3 -28 22.20 3.90 -1 -3 28 22.40 2.40 -1 3 -28 23.90 3.00 1 -3 -28 23.70 3.30 -1 3 -28 19.00 3.20 -1 3 -28 24.00 2.60 1 3 28 20.60 3.10 1 -3 -28 21.00 3.10 1 -3 -28 20.80 2.30 -2 3 28 11.90 1.80 2 -3 28 18.30 3.00 2 -3 28 11.50 1.90 -2 3 28 14.00 2.00 -2 3 28 13.90 2.50 -2 -3 -28 15.00 1.60 2 -3 28 14.90 2.00 -2 -3 -28 13.50 1.90 2 3 -28 12.10 1.80 -2 3 28 13.00 1.90 2 3 -28 8.70 1.70 2 -3 28 17.10 2.60 2 3 -28 14.20 2.10 2 -3 -28 14.90 2.10 -2 -3 28 13.90 1.90 2 -3 -28 12.00 2.40 2 -3 -28 11.40 2.90 -2 -3 28 10.10 1.80 -2 3 -28 11.90 1.70 -2 3 -28 11.90 3.30 2 3 28 11.30 1.90 -2 3 -28 9.10 1.90 -2 -3 28 10.80 1.60 2 -3 -28 11.00 2.00 -2 3 -28 11.30 1.30 3 -3 28 22.80 2.60 3 3 -28 24.60 2.70 -3 3 28 24.50 2.70 -3 -3 -28 21.00 2.30 -3 3 28 24.70 2.70 3 -3 28 25.70 2.90 -3 3 28 25.00 2.70 3 3 -28 24.70 2.50 3 -3 28 26.60 2.80 -3 -3 -28 22.00 2.70 -3 -3 28 25.70 1.90 3 3 28 21.90 3.40 -3 -3 28 24.40 2.50 3 -3 -28 24.20 2.80 -3 3 -28 24.90 2.50 3 3 28 25.30 2.90 -3 -3 28 27.00 2.40 -3 3 -28 22.60 2.00 -3 3 -28 23.70 3.90 3 -3 -28 26.90 2.90 3 -3 -28 26.60 3.30 4 -3 28 16.40 2.30 -4 3 28 20.40 2.50 -4 -3 -28 19.00 2.00 4 3 -28 15.00 2.40 -4 3 28 18.30 2.50 -4 3 28 16.90 2.70 4 -3 28 19.20 2.60 -4 -3 -28 15.70 2.40 -4 3 -28 18.80 2.30 4 -3 -28 18.50 2.50 -4 -3 28 16.10 2.20 -4 -3 28 16.60 2.30 4 3 28 12.50 2.10 4 -3 -28 15.40 1.90 -4 -3 28 13.30 1.70 4 -3 -28 11.80 1.90 4 3 28 18.60 2.60 -4 3 -28 16.80 1.80 -5 3 28 32.40 4.50 -5 3 28 29.40 2.60 5 -3 28 28.30 2.40 5 3 -28 31.20 2.50 -5 3 28 36.60 2.60 -5 -3 -28 29.90 2.60 5 -3 28 31.00 2.70 -5 -3 -28 34.70 2.20 -5 3 -28 34.90 2.40 -5 -3 28 31.00 2.40 -5 3 -28 29.30 2.00 -5 -3 28 29.40 1.90 5 -3 -28 31.50 2.70 5 -3 -28 32.20 2.90 -5 -3 28 30.30 2.40 5 3 28 31.00 2.80 5 3 28 30.20 2.60 -6 -3 -28 28.60 1.90 6 -3 28 25.40 2.20 -6 3 28 23.20 2.10 6 -3 28 28.20 2.40 6 3 -28 28.20 2.10 -6 3 28 29.60 2.20 -6 -3 -28 30.30 2.40 6 -3 -28 23.20 2.50 -6 3 -28 23.40 1.80 -6 3 -28 29.10 2.00 6 3 28 27.40 2.70 -6 -3 28 25.10 2.10 -6 -3 28 27.60 2.10 -6 -3 28 27.50 1.80 -7 3 28 0.50 1.00 -7 -3 -28 -0.10 0.80 7 -3 28 1.40 1.20 7 -3 28 0.80 1.10 -7 3 28 -0.30 1.00 7 3 28 0.90 1.30 -7 3 -28 1.20 0.90 -7 -3 28 -1.00 0.90 -7 -3 28 -0.20 0.70 -7 -3 28 -1.50 1.10 -7 3 -28 0.50 0.70 0 -4 -28 54.79 3.70 0 4 -28 56.79 3.30 0 -4 -28 56.49 3.70 0 4 -28 49.50 5.00 0 -4 28 50.89 3.40 0 4 28 52.09 3.70 0 -4 28 54.09 3.20 0 4 28 50.99 3.70 0 -4 -28 55.19 3.00 0 -4 28 51.89 3.90 0 4 -28 47.80 3.30 0 -4 28 52.89 4.90 0 4 -28 58.29 3.70 -1 -4 -28 2.60 1.70 1 4 -28 4.40 1.60 1 -4 28 1.80 1.50 -1 -4 -28 1.40 1.20 -1 4 28 1.60 1.60 1 4 -28 1.20 1.50 1 -4 28 2.90 1.60 1 4 -28 3.30 1.50 -1 4 28 0.90 1.60 1 -4 28 2.70 1.30 -1 -4 -28 1.40 1.60 1 -4 -28 2.00 1.70 1 -4 -28 3.60 1.80 -1 -4 28 2.60 2.80 -1 4 -28 1.60 1.40 1 4 28 1.10 1.50 1 -4 -28 0.40 2.30 -1 -4 28 0.90 1.50 1 -4 -28 0.30 1.20 -1 4 -28 1.90 1.60 -1 4 -28 2.10 1.40 1 -4 -28 2.80 2.90 -1 -4 28 0.50 1.30 -1 4 -28 3.80 2.90 2 -4 28 3.30 1.40 2 -4 28 1.30 1.50 2 4 -28 -0.10 1.30 2 -4 28 2.60 1.50 -2 4 28 1.50 1.50 -2 -4 -28 0.40 1.70 -2 -4 -28 0.80 1.50 -2 -4 -28 0.10 1.20 -2 4 28 -1.70 1.50 2 4 -28 0.30 1.40 -2 4 28 -0.20 1.50 -2 -4 28 -0.30 1.10 -2 4 -28 1.70 1.50 2 -4 -28 -0.30 1.70 -2 4 -28 0.90 1.30 2 -4 -28 2.20 1.60 2 4 28 -0.40 1.60 -2 -4 28 0.30 1.30 -2 4 -28 -0.20 1.60 -2 -4 28 1.70 1.40 2 -4 -28 -0.60 1.90 -3 -4 -28 41.70 2.70 3 -4 28 38.60 2.90 3 4 -28 41.40 2.90 -3 4 28 38.90 3.00 3 -4 28 39.00 3.00 -3 -4 -28 42.70 3.20 -3 4 28 43.80 3.10 3 4 -28 38.00 3.00 3 -4 28 40.90 3.10 -3 4 28 42.20 3.00 -3 -4 28 41.30 2.80 3 -4 -28 39.70 3.20 3 -4 -28 48.80 3.80 3 -4 -28 43.20 3.10 -3 -4 28 39.70 2.20 -3 -4 28 40.30 2.80 -3 4 -28 43.50 2.80 3 4 28 41.10 3.20 -3 4 -28 43.70 3.80 -4 4 28 52.09 3.20 4 4 -28 51.39 3.20 -4 4 28 57.99 3.20 4 4 -28 53.59 3.20 -4 -4 -28 58.59 3.30 -4 4 28 57.49 3.60 -4 -4 -28 56.19 2.90 4 -4 28 56.99 3.30 4 -4 28 51.29 3.20 4 -4 28 51.49 3.50 -4 -4 28 57.99 3.10 -4 -4 28 55.49 3.10 4 -4 -28 47.90 3.30 -4 4 -28 59.19 3.10 -4 4 -28 50.39 2.60 4 4 28 54.99 3.40 -4 -4 28 55.59 2.60 4 4 28 49.30 4.20 4 -4 -28 52.49 3.70 4 -4 -28 53.39 3.40 -5 -4 -28 8.80 1.20 -5 -4 -28 8.70 1.50 -5 4 28 11.00 1.60 5 4 -28 10.40 1.90 5 -4 28 7.30 1.40 -5 4 28 10.50 1.40 -5 4 28 12.50 2.30 5 -4 28 11.40 1.60 5 4 28 7.20 1.60 -5 -4 28 11.00 1.40 -5 4 -28 10.70 1.80 5 -4 -28 10.70 1.60 -5 -4 28 11.80 1.50 -5 -4 28 10.30 1.40 5 4 28 6.30 2.00 -5 4 -28 12.90 1.70 -6 4 28 0.40 1.10 -6 4 28 1.10 1.20 6 -4 28 1.40 1.10 -6 -4 -28 1.00 0.90 6 -4 28 0.80 1.10 -6 -4 -28 3.90 1.70 6 4 -28 -0.50 1.00 -6 -4 28 0.90 1.00 6 4 28 2.70 1.40 -6 4 -28 0.90 0.80 -6 4 -28 0.00 0.90 -6 -4 28 0.40 1.10 -6 -4 28 0.90 1.00 6 -4 -28 1.20 1.30 -7 4 28 19.10 1.60 -7 -4 -28 17.50 1.60 -7 4 28 22.70 1.70 -7 -4 -28 20.40 1.50 7 -4 28 17.10 1.60 7 -4 28 18.80 1.80 -7 -4 28 19.70 1.80 -7 4 -28 20.50 1.50 -7 -4 28 19.00 1.30 -7 -4 28 18.60 1.50 0 5 -28 54.59 3.40 0 5 -28 56.29 3.50 0 5 -28 57.09 3.20 0 -5 28 50.69 3.20 0 5 -28 53.99 3.30 0 -5 -28 53.19 2.90 0 -5 -28 54.29 3.60 0 -5 28 52.99 3.70 0 5 28 48.20 3.50 0 -5 -28 53.09 3.50 0 -5 28 58.09 3.20 0 5 28 50.79 3.50 -1 -5 -28 13.20 1.90 1 5 -28 16.30 2.40 -1 5 28 19.00 2.60 1 5 -28 16.70 2.50 1 5 -28 15.50 2.20 1 -5 28 12.50 2.10 -1 -5 -28 14.20 1.90 1 -5 28 17.20 2.50 1 -5 28 14.40 2.20 -1 -5 -28 14.60 2.00 -1 5 28 16.90 2.50 1 -5 -28 17.70 2.70 1 -5 -28 20.50 2.70 -1 -5 28 15.70 2.10 -1 -5 28 11.80 1.70 -1 5 -28 14.50 1.70 1 -5 -28 15.20 1.80 1 -5 -28 14.40 3.00 -1 5 -28 16.90 2.10 -1 5 -28 15.90 2.10 1 5 28 13.90 1.90 2 5 -28 2.80 1.50 -2 -5 -28 3.10 1.20 2 5 -28 2.20 1.40 2 -5 28 1.70 1.40 -2 -5 -28 1.70 1.50 -2 5 28 0.30 1.50 2 -5 28 1.50 1.40 -2 5 28 1.40 1.50 2 5 -28 2.90 1.30 -2 -5 -28 3.90 1.60 2 -5 28 3.00 1.30 2 -5 -28 2.80 1.50 2 -5 -28 4.40 1.70 -2 5 -28 1.10 1.40 -2 -5 28 2.80 1.30 -2 5 -28 2.70 1.60 -2 -5 28 1.30 1.30 -2 5 -28 3.50 1.20 2 5 28 2.40 1.60 2 -5 -28 3.30 2.00 -3 -5 -28 2.30 1.40 3 -5 28 1.90 1.40 3 5 -28 -0.20 1.60 -3 -5 -28 2.30 1.10 -3 -5 -28 1.70 1.40 3 5 -28 1.30 1.20 -3 5 28 1.40 1.40 3 -5 28 1.80 1.30 -3 5 28 1.50 1.50 -3 5 28 2.40 1.40 3 5 -28 1.00 1.30 -3 5 -28 -0.60 1.70 3 -5 -28 2.40 1.50 -3 -5 28 0.70 0.80 3 5 28 2.40 1.50 -3 -5 28 0.20 1.10 3 -5 -28 0.10 1.50 -3 5 -28 2.40 1.20 -3 5 -28 2.10 1.70 -3 -5 28 1.40 1.20 4 5 -28 10.20 1.40 -4 5 28 12.50 2.00 4 5 -28 7.80 1.60 -4 -5 -28 11.80 1.80 -4 -5 -28 10.50 1.50 4 -5 28 10.80 1.50 4 -5 28 8.90 1.50 -4 5 28 7.50 1.50 -4 5 28 9.20 1.40 -4 -5 -28 10.70 1.60 4 5 -28 11.50 1.90 -4 -5 28 11.00 1.80 -4 5 -28 10.90 1.80 4 -5 -28 10.10 2.10 4 5 28 12.50 1.70 -4 -5 28 9.80 1.30 4 -5 -28 12.00 1.70 -4 -5 28 6.80 1.20 -5 5 28 6.10 1.40 5 -5 28 4.30 1.20 -5 -5 -28 5.70 1.20 -5 -5 -28 4.20 1.00 5 5 -28 4.40 1.10 -5 -5 -28 5.60 1.40 -5 5 28 4.90 1.20 5 -5 28 2.90 1.10 -5 5 28 3.50 1.80 -5 5 -28 5.40 1.10 -5 -5 28 4.90 0.80 -5 -5 28 8.30 1.60 5 5 28 3.10 1.50 -5 -5 28 5.60 1.10 5 5 28 5.00 1.90 5 -5 -28 3.80 1.30 6 -5 28 10.10 1.50 -6 5 28 11.80 1.70 -6 -5 -28 12.80 1.40 6 -5 28 10.70 1.80 -6 5 28 7.60 1.20 -6 -5 -28 8.70 1.20 -6 5 -28 11.20 1.40 -6 -5 28 11.20 1.50 6 -5 -28 10.80 1.60 -6 -5 28 12.10 1.70 -6 -5 28 11.40 1.20 0 6 28 1.00 1.40 0 6 -28 -0.50 1.20 0 6 -28 2.00 1.40 0 -6 28 0.80 1.90 0 6 28 -0.30 1.60 0 -6 -28 1.30 1.40 0 6 -28 2.60 1.20 0 -6 -28 2.00 1.20 0 -6 -28 2.50 1.50 0 -6 28 1.10 1.10 0 -6 28 1.80 1.20 1 6 -28 12.10 2.00 -1 6 28 14.70 2.40 -1 -6 -28 10.30 1.70 1 6 -28 14.20 2.10 -1 6 28 12.40 1.70 1 6 -28 12.60 2.10 -1 6 28 14.90 2.50 -1 -6 -28 15.00 1.80 -1 -6 -28 11.90 1.70 1 -6 28 12.50 2.30 1 -6 28 14.10 1.90 1 -6 28 12.20 2.00 1 6 28 15.70 2.30 1 -6 -28 12.30 1.80 1 -6 -28 15.70 2.40 -1 -6 28 14.60 1.90 -1 6 -28 12.10 1.40 -1 6 -28 13.20 2.20 -1 -6 28 12.50 1.60 1 6 28 8.10 1.60 -1 6 -28 12.50 2.00 2 -6 28 35.40 3.30 2 6 -28 42.00 2.60 -2 6 28 42.00 3.00 -2 6 28 45.30 3.30 -2 6 28 40.80 2.90 -2 -6 -28 45.60 3.00 -2 -6 -28 47.10 2.60 2 6 -28 44.00 2.70 -2 -6 -28 45.30 2.90 2 -6 28 43.40 2.80 2 -6 28 40.50 2.70 2 6 -28 40.90 2.70 -2 6 -28 37.50 2.70 2 6 28 42.70 3.00 2 6 28 43.10 2.80 -2 -6 28 41.60 2.60 -2 6 -28 39.10 2.90 -2 6 -28 41.10 2.50 2 -6 -28 46.70 3.00 2 -6 -28 41.70 3.00 -2 -6 28 45.70 2.60 3 -6 28 15.70 1.80 -3 6 28 22.40 2.70 3 6 -28 13.60 2.10 3 6 -28 14.80 1.80 -3 6 28 16.30 2.50 -3 6 28 14.80 2.10 3 -6 28 16.50 2.10 -3 -6 -28 15.90 2.10 3 6 -28 14.50 2.00 -3 -6 -28 14.30 1.80 -3 -6 -28 18.50 2.30 -3 -6 28 15.50 1.90 -3 6 -28 14.70 2.30 -3 -6 28 14.60 1.70 3 -6 -28 15.90 2.20 -3 6 -28 18.10 2.80 3 -6 -28 16.90 2.20 3 6 28 15.00 2.20 -3 6 -28 16.30 1.80 -3 -6 28 15.80 1.80 3 6 28 14.20 2.20 4 -6 28 11.50 1.80 -4 6 28 14.40 2.20 4 6 -28 11.20 1.50 4 -6 28 13.00 1.90 -4 6 28 14.60 1.80 -4 -6 -28 12.50 1.80 -4 -6 -28 12.80 1.60 4 6 -28 12.40 1.80 4 6 -28 11.60 1.60 -4 -6 -28 11.70 1.60 4 6 28 10.80 1.50 4 -6 -28 13.20 2.00 -4 -6 28 10.60 1.70 -4 -6 28 12.50 1.30 4 -6 -28 17.10 2.80 -4 -6 28 13.50 1.70 -4 6 -28 12.80 1.60 5 -6 28 1.60 1.00 5 -6 28 1.80 1.10 -5 -6 -28 2.00 1.10 -5 -6 -28 3.30 0.90 -5 6 28 2.80 1.20 -5 6 28 2.80 1.60 -5 -6 28 4.00 1.10 -5 -6 28 3.50 1.00 -5 -6 28 3.00 0.70 -5 6 -28 3.10 0.90 5 -6 -28 0.50 1.10 6 -6 28 19.20 1.70 -6 -6 -28 18.70 1.50 -6 6 28 15.70 1.50 -6 -6 28 17.10 1.60 -6 -6 28 23.50 2.10 6 -6 -28 20.20 2.00 -6 6 -28 18.70 1.40 0 7 28 8.50 1.50 0 7 28 12.60 1.80 0 -7 -28 9.10 1.50 0 -7 -28 11.40 1.70 0 7 -28 10.30 1.40 0 7 -28 10.20 1.80 0 -7 28 11.80 1.70 0 -7 -28 11.60 1.60 0 7 28 12.40 2.10 0 7 -28 11.90 1.90 0 -7 28 9.10 1.40 -1 7 28 26.70 2.50 1 7 -28 27.80 2.50 1 -7 28 29.00 2.40 -1 7 28 26.60 3.10 -1 -7 -28 29.30 2.50 -1 7 28 23.20 2.40 -1 -7 -28 25.70 1.90 1 7 -28 25.80 2.10 1 -7 28 24.20 2.10 1 7 -28 23.50 2.10 1 -7 28 23.30 2.30 -1 -7 -28 26.80 2.30 1 -7 -28 24.20 2.20 1 -7 -28 25.90 2.30 1 7 28 25.30 2.20 -1 -7 28 26.00 2.00 -1 7 -28 22.10 2.10 1 7 28 24.30 2.40 -1 -7 28 27.30 2.10 -1 7 -28 25.10 2.20 2 7 -28 22.70 1.90 2 7 -28 23.80 1.90 -2 -7 -28 22.20 2.30 -2 7 28 22.60 2.10 -2 7 28 25.10 2.40 -2 7 28 26.30 2.50 -2 -7 -28 25.00 1.80 2 -7 28 24.90 3.00 2 -7 28 30.30 2.20 2 7 -28 24.20 2.00 -2 -7 -28 22.50 2.20 2 -7 -28 21.20 2.20 -2 -7 28 24.20 2.00 -2 7 -28 20.80 2.10 -2 7 -28 27.30 3.00 2 7 28 21.90 2.10 -2 7 -28 20.40 2.20 2 -7 -28 26.20 2.10 -2 -7 28 26.80 1.90 2 7 28 27.10 2.40 3 7 -28 0.30 1.10 3 7 -28 1.60 0.90 3 -7 28 1.00 1.50 -3 -7 -28 1.80 1.20 -3 7 28 1.40 1.20 -3 -7 -28 2.00 0.90 -3 7 28 1.90 1.40 3 7 -28 0.80 1.00 -3 -7 -28 0.20 1.20 -3 7 -28 0.80 1.00 3 -7 -28 1.40 1.20 -3 -7 28 0.70 0.90 -3 7 -28 0.90 1.30 3 7 28 1.70 1.20 -3 -7 28 1.30 1.00 3 -7 -28 1.20 1.10 -3 7 -28 1.50 1.20 -4 -7 -28 3.20 0.80 -4 7 28 3.00 1.10 4 -7 28 5.70 1.10 4 -7 28 2.00 1.20 4 7 -28 2.10 1.00 -4 7 28 3.20 1.30 -4 -7 -28 2.50 1.10 4 7 -28 2.40 0.90 -4 -7 28 3.00 1.00 -4 7 -28 3.60 0.90 -4 -7 28 1.80 0.90 4 -7 -28 5.40 1.20 -5 -7 -28 2.90 0.80 5 -7 28 1.30 1.10 5 -7 28 1.80 1.00 5 -7 -28 0.50 1.00 -5 -7 28 2.00 0.90 0 -8 -28 26.60 2.00 0 8 -28 29.90 2.50 0 -8 28 25.00 1.80 0 8 -28 24.70 1.80 0 8 28 21.00 1.70 0 8 -28 24.30 1.80 0 -8 -28 23.70 2.30 0 -8 28 19.60 1.70 1 -8 28 11.50 1.70 1 8 -28 11.30 1.60 1 8 -28 10.50 1.50 1 -8 28 16.50 1.80 -1 -8 -28 13.30 1.90 -1 8 28 9.30 1.50 -1 8 28 12.20 1.80 -1 -8 -28 11.50 1.70 -1 -8 -28 12.30 1.40 1 8 -28 13.80 1.80 -1 8 -28 11.30 1.60 -1 -8 28 13.10 1.60 -1 8 -28 13.20 1.70 -1 -8 28 12.20 1.60 1 8 28 11.50 1.70 1 -8 -28 13.10 2.00 1 -8 -28 9.70 1.40 -1 8 -28 10.80 1.50 2 8 -28 11.20 1.50 2 8 -28 10.80 1.30 2 -8 28 11.60 1.80 -2 8 28 9.20 1.30 2 8 -28 11.90 1.40 -2 -8 -28 9.70 1.30 -2 -8 -28 11.50 1.90 -2 -8 -28 10.90 1.70 -2 8 28 11.20 1.60 2 -8 -28 15.40 1.70 -2 8 -28 13.80 1.50 2 -8 -28 11.30 1.30 -2 -8 28 11.50 1.60 -2 -8 28 9.40 1.10 -2 8 -28 11.30 1.70 3 8 -28 2.60 1.30 -3 -8 -28 6.20 1.60 3 -8 28 2.70 1.10 -3 8 28 1.70 1.10 -3 8 28 2.10 1.10 3 8 -28 2.00 0.90 -3 -8 -28 2.50 0.80 3 -8 -28 1.90 1.00 -3 -8 28 1.20 0.80 4 -8 -28 6.60 1.50 0 9 -28 21.20 1.70 0 9 -28 22.00 1.50 0 -9 -28 24.00 1.70 -1 -9 -28 5.50 1.50 1 9 -28 2.20 1.20 1 9 -28 3.40 1.20 -1 9 -28 5.80 0.90 1 -9 -28 3.90 1.30 0 0 -29 1.10 2.70 0 0 29 2.80 2.70 0 0 -29 -0.80 1.70 0 0 29 0.70 1.70 0 0 -29 -0.80 1.70 0 0 -29 -0.80 1.50 0 0 29 2.30 1.50 1 0 -29 1.50 1.90 1 0 -29 1.40 1.70 -1 0 -29 -1.90 2.00 1 0 29 1.20 1.60 1 0 -29 -2.10 2.50 1 0 29 2.70 1.80 -1 0 -29 1.60 1.60 1 0 -29 1.20 1.50 -1 0 29 2.10 1.70 -1 0 29 0.30 1.60 -1 0 -29 1.60 3.10 -1 0 -29 1.10 1.10 -1 0 29 0.90 1.50 2 0 -29 3.70 1.90 2 0 29 0.90 1.60 -2 0 29 0.40 1.60 2 0 29 0.40 1.60 2 0 -29 0.40 1.60 -2 0 -29 -2.10 1.00 -2 0 29 2.00 1.60 -2 0 -29 -1.10 4.00 -2 0 29 2.80 1.40 -2 0 -29 1.30 1.50 2 0 -29 0.00 1.70 2 0 -29 -0.30 2.60 -2 0 29 0.70 2.40 -3 0 29 33.70 2.70 3 0 -29 22.90 2.90 3 0 -29 29.20 3.10 -3 0 -29 28.70 2.20 -3 0 29 31.30 2.70 3 0 -29 25.60 2.90 3 0 29 26.60 3.10 3 0 29 26.40 2.90 -3 0 -29 28.20 2.70 -3 0 29 34.20 2.80 3 0 29 30.60 3.10 -4 0 29 1.60 1.40 -4 0 -29 1.90 1.10 -4 0 -29 0.60 1.30 -4 0 29 2.80 1.50 4 0 29 2.70 1.50 -4 0 29 1.10 1.30 4 0 -29 1.10 1.60 4 0 29 2.00 1.60 4 0 29 -0.60 1.50 -5 0 -29 16.30 1.80 -5 0 -29 15.50 2.10 5 0 -29 16.00 2.30 5 0 29 17.50 2.50 5 0 29 8.30 2.40 -5 0 29 16.30 2.10 5 0 29 14.90 2.20 -5 0 29 15.10 2.10 -6 0 29 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2.40 1.10 3 3 -33 1.90 1.00 -3 -3 -33 0.20 1.00 -3 -3 -33 -0.30 0.90 -3 -3 33 0.50 0.90 3 3 33 1.10 1.20 -3 3 -33 1.70 1.00 0 -4 33 30.00 2.00 0 -4 -33 29.40 2.00 0 4 33 27.00 2.00 0 -4 -33 23.80 1.90 0 4 -33 28.40 2.30 0 4 33 26.10 2.00 -1 4 33 19.10 1.90 -1 -4 -33 18.90 1.60 -1 -4 -33 19.20 1.70 1 -4 33 17.80 1.80 -1 4 33 20.40 1.90 1 4 -33 14.80 1.70 1 4 33 18.80 1.70 1 -4 -33 16.60 2.10 -1 -4 33 19.00 1.80 1 -4 -33 18.00 1.70 1 4 33 16.50 1.80 -2 -4 -33 3.40 1.00 2 4 -33 3.60 1.00 -2 -4 -33 2.80 1.00 -2 4 33 2.70 1.20 -2 -4 33 3.20 1.10 2 4 33 3.20 1.00 0 -5 -33 1.20 1.60 0 0 34 1.70 1.10 1 0 -34 11.90 2.30 -1 0 34 7.90 1.20 -1 0 -34 8.40 1.20 1 0 34 7.10 1.30 -2 0 -34 0.70 1.00 2 0 34 -0.10 1.10 -2 0 34 -0.10 1.00 3 0 -34 12.10 2.20 0 -1 34 10.40 1.70 0 1 34 11.90 1.80 0 -1 -34 10.50 1.30 -1 -1 -34 15.80 1.80 -1 1 34 16.00 2.00 1 -1 34 16.80 1.70 -1 -1 34 19.70 1.80 -1 1 -34 19.90 2.50 1 1 34 16.10 1.80 -2 -1 -34 8.50 1.20 2 -1 34 7.80 1.30 -2 1 34 10.70 1.70 2 1 -34 13.90 2.00 -2 1 -34 10.40 1.60 -2 -1 34 11.40 1.60 2 1 34 11.80 1.60 -3 -1 -34 -0.20 0.90 3 1 -34 -1.60 1.10 0 -2 -34 89.49 4.10 0 -2 34 94.99 4.00 0 2 34 93.09 4.00 -1 -2 -34 5.40 1.10 -1 2 34 3.70 1.00 1 -2 34 5.20 1.10 1 2 34 4.00 1.10 -1 -2 34 6.10 1.10 -2 2 34 5.20 1.50 -2 -2 -34 6.30 1.00 -2 -2 34 7.10 1.30 2 2 34 6.70 1.20 0 3 34 1.80 1.00 0 -3 34 1.70 0.90 0 3 34 1.40 1.00 -1 3 34 5.70 1.20 1 3 34 7.70 1.10 -1 -3 34 5.50 1.10 1 3 34 10.20 1.80 0 0 35 -0.30 1.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 11772 _shelx_SHELXL_version_number '2014/7' _olex2_submission_special_instructions 'No special instructions were received'