data_pentapeptide # data_tom12h # structure Linda JW Simon, WIS # Tom Guterman Ehud Gazit TAU _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C30 H47 N6 O8, H2 O' _chemical_formula_sum 'C30 H50 N6 O9' _chemical_formula_weight 638.76 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 1 _space_group_name_H-M_alt 'P 1' _space_group_name_Hall 'P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' _cell_length_a 4.9205(10) _cell_length_b 11.812(2) _cell_length_c 14.637(3) _cell_angle_alpha 99.369(7) _cell_angle_beta 93.376(7) _cell_angle_gamma 98.820(7) _cell_volume 826.4(3) _cell_formula_units_Z 1 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 3755 _cell_measurement_theta_min 2.03 _cell_measurement_theta_max 29.09 _exptl_crystal_description needle _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.284 _exptl_crystal_F_000 344 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.050 _exptl_absorpt_coefficient_mu 0.095 _shelx_estimated_absorpt_T_min 0.986 _shelx_estimated_absorpt_T_max 0.995 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.991 _exptl_absorpt_correction_T_max 0.995 _exptl_absorpt_process_details 'EDNA' _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.700 _diffrn_radiation_type 'synchrotron' _diffrn_source 'ESRF ID29' _diffrn_measurement_device_type 'Pilatus 6M' _diffrn_measurement_method 'phi scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 13647 _diffrn_reflns_av_unetI/netI 0.0438 _diffrn_reflns_av_R_equivalents ? _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 2.035 _diffrn_reflns_theta_max 29.099 _diffrn_reflns_theta_full 24.835 _diffrn_measured_fraction_theta_max 0.814 _diffrn_measured_fraction_theta_full 0.898 _diffrn_reflns_Laue_measured_fraction_max 0.814 _diffrn_reflns_Laue_measured_fraction_full 0.898 _diffrn_reflns_point_group_measured_fraction_max 0.407 _diffrn_reflns_point_group_measured_fraction_full 0.449 _reflns_number_total 3773 _reflns_number_gt 3755 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max 0.000 _reflns_Friedel_fraction_full 0.000 _reflns_special_details ; Data were apparently pre-merged, so _diffrn_reflns_number etc. will have to be added later. Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'MXCube' _computing_cell_refinement 'EDNA' _computing_data_reduction 'EDNA' _computing_structure_solution 'SHELXT-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0794P)^2^+0.3805P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; No quotients, so Flack parameter determined by classical intensity fit ; _chemical_absolute_configuration 'syn' _refine_ls_number_reflns 3773 _refine_ls_number_parameters 448 _refine_ls_number_restraints 18 _refine_ls_R_factor_all 0.0472 _refine_ls_R_factor_gt 0.0470 _refine_ls_wR_factor_ref 0.1257 _refine_ls_wR_factor_gt 0.1255 _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_restrained_S_all 1.090 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.2561(5) 0.23393(18) -0.05702(14) 0.0159(4) Uani 1 1 d . . . . . H1A H 0.220(9) 0.156(3) -0.092(3) 0.024 Uiso 1 1 d . U . . . H1B H 0.124(9) 0.276(4) -0.071(3) 0.024 Uiso 1 1 d . U . . . H1C H 0.434(9) 0.265(4) -0.071(3) 0.024 Uiso 1 1 d . U . . . C1 C 0.2139(5) 0.2252(2) 0.04152(16) 0.0133(4) Uani 1 1 d . . . . . H1D H 0.0118 0.2081 0.0490 0.016 Uiso 1 1 calc R U . . . C2 C 0.3551(6) 0.1263(2) 0.06864(17) 0.0181(5) Uani 1 1 d . . . . . H2A H 0.2894 0.0544 0.0229 0.022 Uiso 1 1 calc R U . . . H2B H 0.5569 0.1469 0.0659 0.022 Uiso 1 1 calc R U . . . C3 C 0.2992(6) 0.1029(2) 0.16430(17) 0.0175(5) Uani 1 1 d . . . . . C4 C 0.4727(8) 0.1586(3) 0.2426(2) 0.0289(6) Uani 1 1 d . . . . . H4A H 0.6310 0.2131 0.2365 0.035 Uiso 1 1 calc R U . . . C5 C 0.4129(10) 0.1339(4) 0.3301(2) 0.0437(10) Uani 1 1 d . . . . . H5A H 0.5310 0.1721 0.3834 0.052 Uiso 1 1 calc R U . . . C6 C 0.1850(11) 0.0549(4) 0.3398(3) 0.0445(10) Uani 1 1 d . . . . . H6A H 0.1464 0.0386 0.3996 0.053 Uiso 1 1 calc R U . . . C7 C 0.0103(9) -0.0014(3) 0.2616(3) 0.0401(9) Uani 1 1 d . . . . . H7A H -0.1471 -0.0564 0.2679 0.048 Uiso 1 1 calc R U . . . C8 C 0.0684(7) 0.0235(3) 0.1748(2) 0.0274(6) Uani 1 1 d . . . . . H8A H -0.0512 -0.0143 0.1217 0.033 Uiso 1 1 calc R U . . . C9 C 0.3419(5) 0.3386(2) 0.10570(16) 0.0131(4) Uani 1 1 d . . . . . O1 O 0.5904(4) 0.37353(17) 0.10713(13) 0.0184(4) Uani 1 1 d . . . . . N2 N 0.1704(4) 0.38781(17) 0.16167(13) 0.0119(4) Uani 1 1 d . . . . . H2C H -0.0057 0.3571 0.1560 0.014 Uiso 1 1 calc R U . . . C10 C 0.2680(5) 0.4904(2) 0.23133(16) 0.0143(4) Uani 1 1 d . . . . . H10A H 0.4742 0.5027 0.2400 0.017 Uiso 1 1 calc R U . . . C11 C 0.1744(6) 0.5986(2) 0.20160(17) 0.0199(5) Uani 1 1 d . . . . . H11A H -0.0315 0.5860 0.1908 0.024 Uiso 1 1 calc R U . . . C12 C 0.2730(9) 0.7064(3) 0.2743(2) 0.0355(8) Uani 1 1 d . . . . . H12A H 0.2122 0.7739 0.2534 0.053 Uiso 1 1 calc R U . . . H12B H 0.4750 0.7194 0.2835 0.053 Uiso 1 1 calc R U . . . H12C H 0.1956 0.6956 0.3331 0.053 Uiso 1 1 calc R U . . . O2 O 0.2943(5) 0.61779(17) 0.11870(13) 0.0226(4) Uani 1 1 d . . . . . H2D H 0.2179 0.5663 0.0743 0.034 Uiso 1 1 calc R U . . . C13 C 0.1500(5) 0.4727(2) 0.32331(15) 0.0138(4) Uani 1 1 d . . . . . O3 O -0.1015(4) 0.45734(19) 0.32905(13) 0.0205(4) Uani 1 1 d . . . . . N3 N 0.3402(5) 0.48102(19) 0.39497(14) 0.0159(4) Uani 1 1 d . . . . . H3A H 0.5163 0.4882 0.3852 0.019 Uiso 1 1 calc R U . . . C14 C 0.2575(6) 0.4782(2) 0.48892(16) 0.0150(4) Uani 1 1 d . . . . . H14A H 0.0591 0.4867 0.4924 0.018 Uiso 1 1 calc R U . A 1 C15A C 0.314(5) 0.361(2) 0.5212(9) 0.020(3) Uani 0.457(6) 1 d D . P B 1 H15A H 0.1801 0.2952 0.4853 0.024 Uiso 0.457(6) 1 calc R U P B 1 H15B H 0.5012 0.3475 0.5051 0.024 Uiso 0.457(6) 1 calc R U P B 1 C16A C 0.296(2) 0.3579(7) 0.6227(5) 0.0391(10) Uani 0.457(6) 1 d D . P B 1 H16A H 0.0948 0.3258 0.6107 0.047 Uiso 0.457(6) 1 calc R U P B 1 C17A C 0.2628(17) 0.3996(5) 0.6941(4) 0.0293(12) Uani 0.457(6) 1 d D . P B 1 H17A H 0.3688 0.3679 0.7398 0.044 Uiso 0.457(6) 1 calc R U P B 1 H17B H 0.0661 0.3840 0.7036 0.044 Uiso 0.457(6) 1 calc R U P B 1 H17C H 0.3243 0.4838 0.7017 0.044 Uiso 0.457(6) 1 calc R U P B 1 C18A C 0.3544(16) 0.2399(5) 0.6465(4) 0.0293(12) Uani 0.457(6) 1 d D . P B 1 H18A H 0.5342 0.2257 0.6260 0.044 Uiso 0.457(6) 1 calc R U P B 1 H18B H 0.2098 0.1771 0.6146 0.044 Uiso 0.457(6) 1 calc R U P B 1 H18C H 0.3558 0.2425 0.7138 0.044 Uiso 0.457(6) 1 calc R U P B 1 C15B C 0.250(4) 0.3600(18) 0.5127(8) 0.020(3) Uani 0.543(6) 1 d D . P B 2 H15C H 0.4430 0.3462 0.5215 0.024 Uiso 0.543(6) 1 calc R U P B 2 H15D H 0.1581 0.3022 0.4589 0.024 Uiso 0.543(6) 1 calc R U P B 2 C16B C 0.1060(18) 0.3373(6) 0.5986(5) 0.0391(10) Uani 0.543(6) 1 d D . P B 2 H16B H 0.2806 0.3483 0.6400 0.047 Uiso 0.543(6) 1 calc R U P B 2 C17B C -0.0098(17) 0.3725(6) 0.6512(5) 0.0391(10) Uani 0.543(6) 1 d D . P B 2 H17D H 0.0684 0.3618 0.7118 0.059 Uiso 0.543(6) 1 calc R U P B 2 H17E H -0.2017 0.3326 0.6402 0.059 Uiso 0.543(6) 1 calc R U P B 2 H17F H -0.0037 0.4557 0.6507 0.059 Uiso 0.543(6) 1 calc R U P B 2 C18B C 0.039(2) 0.2057(6) 0.5964(5) 0.057(2) Uani 0.543(6) 1 d D U P B 2 H18D H -0.0246 0.1908 0.6562 0.085 Uiso 0.543(6) 1 calc R U P B 2 H18E H 0.2044 0.1708 0.5847 0.085 Uiso 0.543(6) 1 calc R U P B 2 H18F H -0.1071 0.1712 0.5467 0.085 Uiso 0.543(6) 1 calc R U P B 2 C19 C 0.4453(5) 0.5789(2) 0.55217(15) 0.0137(4) Uani 1 1 d . . . . . O4 O 0.6984(4) 0.58488(17) 0.55698(13) 0.0196(4) Uani 1 1 d . . . . . N4 N 0.3131(5) 0.65876(18) 0.59837(14) 0.0149(4) Uani 1 1 d . . . . . H4B H 0.1318 0.6491 0.5905 0.018 Uiso 1 1 calc R U . . . C20 C 0.4620(5) 0.7613(2) 0.66140(16) 0.0154(5) Uani 1 1 d . . . . . H20A H 0.6651 0.7637 0.6579 0.018 Uiso 1 1 calc R U . . . C21 C 0.3814(6) 0.8744(2) 0.63730(18) 0.0181(5) Uani 1 1 d . . . . . H21A H 0.1849 0.8750 0.6509 0.022 Uiso 1 1 calc R U . . . C22 C 0.5573(7) 0.9791(3) 0.7004(2) 0.0245(6) Uani 1 1 d . . . . . H22A H 0.5072 1.0510 0.6844 0.037 Uiso 1 1 calc R U . . . H22B H 0.7529 0.9777 0.6920 0.037 Uiso 1 1 calc R U . . . H22C H 0.5245 0.9756 0.7654 0.037 Uiso 1 1 calc R U . . . C23 C 0.3995(6) 0.8818(3) 0.5340(2) 0.0222(5) Uani 1 1 d . . . . . H23A H 0.2652 0.8174 0.4968 0.027 Uiso 1 1 calc R U . . . H23B H 0.3430 0.9557 0.5229 0.027 Uiso 1 1 calc R U . . . C24 C 0.6841(7) 0.8759(3) 0.4984(2) 0.0273(6) Uani 1 1 d . . . . . H24A H 0.6759 0.8820 0.4323 0.041 Uiso 1 1 calc R U . . . H24B H 0.7398 0.8017 0.5064 0.041 Uiso 1 1 calc R U . . . H24C H 0.8190 0.9402 0.5336 0.041 Uiso 1 1 calc R U . . . C25 C 0.3886(6) 0.7483(2) 0.75963(17) 0.0147(4) Uani 1 1 d . . . . . O5 O 0.1529(4) 0.75566(19) 0.78231(14) 0.0224(4) Uani 1 1 d . . . . . N5 N 0.5861(5) 0.72615(17) 0.81684(14) 0.0132(4) Uani 1 1 d . . . . . H5B H 0.7503 0.7211 0.7973 0.016 Uiso 1 1 calc R U . . . C26 C 0.5356(5) 0.71015(19) 0.91111(15) 0.0129(4) Uani 1 1 d . . . . . H26A H 0.3440 0.6666 0.9097 0.015 Uiso 1 1 calc R U . . . C27 C 0.7367(5) 0.6367(2) 0.94743(16) 0.0141(4) Uani 1 1 d . . . . . H27A H 0.9289 0.6767 0.9476 0.017 Uiso 1 1 calc R U . . . H27B H 0.7023 0.6280 1.0121 0.017 Uiso 1 1 calc R U . . . C28 C 0.6997(6) 0.5170(2) 0.88637(17) 0.0170(5) Uani 1 1 d . . . . . H28A H 0.7454 0.5270 0.8229 0.020 Uiso 1 1 calc R U . . . H28B H 0.5029 0.4811 0.8823 0.020 Uiso 1 1 calc R U . . . C29 C 0.8751(6) 0.4335(2) 0.92015(16) 0.0154(4) Uani 1 1 d . . . . . O6 O 0.7848(4) 0.32542(16) 0.89583(13) 0.0202(4) Uani 1 1 d . . . . . O7 O 1.1021(4) 0.47277(17) 0.96523(13) 0.0193(4) Uani 1 1 d . . . . . C30 C 0.5511(6) 0.8286(2) 0.97342(17) 0.0167(5) Uani 1 1 d . . . . . N6 N 0.4547(6) 0.8257(2) 1.05669(16) 0.0204(5) Uani 1 1 d . . . . . H6B H 0.388(9) 0.763(4) 1.071(3) 0.019(8) Uiso 1 1 d . . . . . H6C H 0.459(9) 0.896(4) 1.093(3) 0.024(9) Uiso 1 1 d . . . . . O8 O 0.6429(6) 0.92003(18) 0.94893(16) 0.0320(6) Uani 1 1 d . . . . . O9 O 1.0791(5) 1.00154(18) 0.85711(16) 0.0255(4) Uani 1 1 d . . . . . H9A H 1.163(14) 0.946(6) 0.841(4) 0.059(16) Uiso 1 1 d . . . . . H9B H 0.939(13) 0.969(5) 0.882(4) 0.047(14) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0181(13) 0.0185(10) 0.0127(9) 0.0036(7) 0.0015(7) 0.0067(8) C1 0.0127(13) 0.0156(10) 0.0127(10) 0.0041(8) 0.0013(8) 0.0040(7) C2 0.0238(16) 0.0196(11) 0.0146(11) 0.0059(8) 0.0052(9) 0.0106(9) C3 0.0226(16) 0.0197(11) 0.0137(11) 0.0057(8) 0.0039(9) 0.0105(9) C4 0.035(2) 0.0348(15) 0.0188(13) 0.0055(11) -0.0017(11) 0.0112(12) C5 0.066(3) 0.058(2) 0.0140(13) 0.0068(14) -0.0002(14) 0.035(2) C6 0.065(3) 0.057(2) 0.0279(16) 0.0276(16) 0.0201(16) 0.036(2) C7 0.044(2) 0.0429(19) 0.045(2) 0.0269(16) 0.0226(16) 0.0172(15) C8 0.0295(19) 0.0265(13) 0.0294(15) 0.0096(11) 0.0075(12) 0.0082(11) C9 0.0109(13) 0.0172(10) 0.0127(10) 0.0042(8) 0.0017(7) 0.0050(7) O1 0.0111(11) 0.0255(9) 0.0175(8) -0.0001(7) 0.0029(6) 0.0030(6) N2 0.0082(11) 0.0167(9) 0.0109(8) 0.0024(7) 0.0024(6) 0.0025(6) C10 0.0147(14) 0.0185(10) 0.0094(9) 0.0013(8) 0.0032(8) 0.0018(8) C11 0.0295(17) 0.0184(11) 0.0136(11) 0.0047(9) 0.0078(9) 0.0054(9) C12 0.065(3) 0.0191(12) 0.0202(13) -0.0023(10) 0.0107(13) 0.0051(13) O2 0.0345(13) 0.0191(8) 0.0133(8) 0.0043(6) 0.0062(7) -0.0011(7) C13 0.0120(14) 0.0199(11) 0.0104(10) 0.0035(8) 0.0022(8) 0.0042(8) O3 0.0114(11) 0.0367(10) 0.0136(8) 0.0052(7) 0.0034(6) 0.0032(7) N3 0.0101(12) 0.0274(11) 0.0110(9) 0.0039(7) 0.0026(7) 0.0043(7) C14 0.0159(14) 0.0201(11) 0.0096(9) 0.0027(8) 0.0041(7) 0.0029(8) C15A 0.025(9) 0.0205(13) 0.016(2) 0.005(2) 0.001(4) 0.007(5) C16A 0.047(3) 0.044(2) 0.033(2) 0.0208(17) 0.0086(16) 0.0099(18) C17A 0.040(3) 0.031(2) 0.020(2) 0.0135(17) 0.0026(17) 0.0020(18) C18A 0.040(3) 0.031(2) 0.020(2) 0.0135(17) 0.0026(17) 0.0020(18) C15B 0.025(9) 0.0205(13) 0.016(2) 0.005(2) 0.001(4) 0.007(5) C16B 0.047(3) 0.044(2) 0.033(2) 0.0208(17) 0.0086(16) 0.0099(18) C17B 0.047(3) 0.044(2) 0.033(2) 0.0208(17) 0.0086(16) 0.0099(18) C18B 0.095(6) 0.036(3) 0.027(3) 0.017(3) -0.018(3) -0.032(3) C19 0.0140(14) 0.0200(11) 0.0092(9) 0.0056(8) 0.0025(7) 0.0057(8) O4 0.0130(12) 0.0265(9) 0.0196(9) 0.0012(7) 0.0025(6) 0.0066(7) N4 0.0101(12) 0.0206(10) 0.0139(9) 0.0011(7) 0.0007(7) 0.0044(7) C20 0.0127(14) 0.0220(11) 0.0118(10) 0.0030(8) 0.0025(8) 0.0038(8) C21 0.0158(14) 0.0237(12) 0.0169(11) 0.0058(9) 0.0035(8) 0.0060(9) C22 0.0276(17) 0.0243(13) 0.0205(12) 0.0038(10) 0.0023(10) 0.0011(10) C23 0.0193(16) 0.0298(13) 0.0202(12) 0.0104(10) 0.0021(9) 0.0061(10) C24 0.0236(18) 0.0396(16) 0.0216(12) 0.0129(11) 0.0068(10) 0.0046(12) C25 0.0125(14) 0.0188(10) 0.0136(10) 0.0037(8) 0.0024(8) 0.0038(8) O5 0.0127(11) 0.0385(11) 0.0203(9) 0.0115(8) 0.0064(7) 0.0087(7) N5 0.0102(11) 0.0183(9) 0.0129(9) 0.0049(7) 0.0041(6) 0.0047(7) C26 0.0134(13) 0.0155(10) 0.0122(10) 0.0061(8) 0.0047(7) 0.0044(7) C27 0.0142(14) 0.0157(10) 0.0143(10) 0.0041(8) 0.0029(8) 0.0057(8) C28 0.0176(15) 0.0171(11) 0.0182(11) 0.0051(8) 0.0012(8) 0.0067(8) C29 0.0166(14) 0.0194(11) 0.0132(10) 0.0051(8) 0.0072(8) 0.0076(8) O6 0.0242(12) 0.0177(8) 0.0203(9) 0.0046(7) 0.0046(7) 0.0064(7) O7 0.0194(12) 0.0229(9) 0.0169(8) 0.0043(7) 0.0011(6) 0.0073(7) C30 0.0211(15) 0.0168(10) 0.0151(10) 0.0045(8) 0.0076(9) 0.0083(8) N6 0.0304(15) 0.0166(10) 0.0160(10) 0.0046(8) 0.0106(8) 0.0049(8) O8 0.0569(17) 0.0148(9) 0.0290(11) 0.0071(8) 0.0240(10) 0.0101(9) O9 0.0299(13) 0.0191(9) 0.0264(10) 0.0003(7) 0.0044(8) 0.0036(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C1 1.487(3) . ? N1 H1A 0.97(4) . ? N1 H1B 0.91(4) . ? N1 H1C 0.94(4) . ? C1 C9 1.528(3) . ? C1 C2 1.540(3) . ? C1 H1D 1.0000 . ? C2 C3 1.503(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C8 1.391(4) . ? C3 C4 1.394(4) . ? C4 C5 1.396(4) . ? C4 H4A 0.9500 . ? C5 C6 1.375(7) . ? C5 H5A 0.9500 . ? C6 C7 1.398(7) . ? C6 H6A 0.9500 . ? C7 C8 1.385(4) . ? C7 H7A 0.9500 . ? C8 H8A 0.9500 . ? C9 O1 1.227(3) . ? C9 N2 1.341(3) . ? N2 C10 1.449(3) . ? N2 H2C 0.8800 . ? C10 C13 1.530(3) . ? C10 C11 1.542(4) . ? C10 H10A 1.0000 . ? C11 O2 1.416(3) . ? C11 C12 1.516(4) . ? C11 H11A 1.0000 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? O2 H2D 0.8400 . ? C13 O3 1.232(3) . ? C13 N3 1.345(3) . ? N3 C14 1.461(3) . ? N3 H3A 0.8800 . ? C14 C15B 1.489(19) . ? C14 C19 1.526(3) . ? C14 C15A 1.60(2) . ? C14 H14A 1.0000 . ? C15A C16A 1.500(12) . ? C15A H15A 0.9900 . ? C15A H15B 0.9900 . ? C16A C17A 1.113(9) . ? C16A C18A 1.553(8) . ? C16A H16A 1.0000 . ? C17A H17A 0.9800 . ? C17A H17B 0.9800 . ? C17A H17C 0.9800 . ? C18A H18A 0.9800 . ? C18A H18B 0.9800 . ? C18A H18C 0.9800 . ? C15B C16B 1.522(11) . ? C15B H15C 0.9900 . ? C15B H15D 0.9900 . ? C16B C17B 1.054(10) . ? C16B C18B 1.534(9) . ? C16B H16B 1.0000 . ? C17B H17D 0.9800 . ? C17B H17E 0.9800 . ? C17B H17F 0.9800 . ? C18B H18D 0.9800 . ? C18B H18E 0.9800 . ? C18B H18F 0.9800 . ? C19 O4 1.234(4) . ? C19 N4 1.342(3) . ? N4 C20 1.463(3) . ? N4 H4B 0.8800 . ? C20 C25 1.529(3) . ? C20 C21 1.538(3) . ? C20 H20A 1.0000 . ? C21 C22 1.529(4) . ? C21 C23 1.536(4) . ? C21 H21A 1.0000 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 C24 1.530(4) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 O5 1.237(4) . ? C25 N5 1.329(3) . ? N5 C26 1.453(3) . ? N5 H5B 0.8800 . ? C26 C30 1.529(3) . ? C26 C27 1.538(3) . ? C26 H26A 1.0000 . ? C27 C28 1.524(3) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 C29 1.527(3) . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C29 O7 1.246(3) . ? C29 O6 1.270(3) . ? C30 O8 1.223(3) . ? C30 N6 1.337(3) . ? N6 H6B 0.82(4) . ? N6 H6C 0.91(4) . ? O9 H9A 0.83(7) . ? O9 H9B 0.87(6) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 H1A 107(2) . . ? C1 N1 H1B 102(3) . . ? H1A N1 H1B 112(3) . . ? C1 N1 H1C 118(2) . . ? H1A N1 H1C 105(3) . . ? H1B N1 H1C 113(4) . . ? N1 C1 C9 110.58(18) . . ? N1 C1 C2 109.10(19) . . ? C9 C1 C2 108.5(2) . . ? N1 C1 H1D 109.6 . . ? C9 C1 H1D 109.6 . . ? C2 C1 H1D 109.6 . . ? C3 C2 C1 112.9(2) . . ? C3 C2 H2A 109.0 . . ? C1 C2 H2A 109.0 . . ? C3 C2 H2B 109.0 . . ? C1 C2 H2B 109.0 . . ? H2A C2 H2B 107.8 . . ? C8 C3 C4 119.1(3) . . ? C8 C3 C2 119.1(2) . . ? C4 C3 C2 121.8(3) . . ? C3 C4 C5 119.8(3) . . ? C3 C4 H4A 120.1 . . ? C5 C4 H4A 120.1 . . ? C6 C5 C4 120.7(4) . . ? C6 C5 H5A 119.6 . . ? C4 C5 H5A 119.6 . . ? C5 C6 C7 119.9(3) . . ? C5 C6 H6A 120.0 . . ? C7 C6 H6A 120.0 . . ? C8 C7 C6 119.4(4) . . ? C8 C7 H7A 120.3 . . ? C6 C7 H7A 120.3 . . ? C7 C8 C3 121.0(3) . . ? C7 C8 H8A 119.5 . . ? C3 C8 H8A 119.5 . . ? O1 C9 N2 125.1(2) . . ? O1 C9 C1 119.2(2) . . ? N2 C9 C1 115.5(2) . . ? C9 N2 C10 121.6(2) . . ? C9 N2 H2C 119.2 . . ? C10 N2 H2C 119.2 . . ? N2 C10 C13 109.22(19) . . ? N2 C10 C11 110.7(2) . . ? C13 C10 C11 108.8(2) . . ? N2 C10 H10A 109.4 . . ? C13 C10 H10A 109.4 . . ? C11 C10 H10A 109.4 . . ? O2 C11 C12 107.3(2) . . ? O2 C11 C10 108.6(2) . . ? C12 C11 C10 111.2(2) . . ? O2 C11 H11A 109.9 . . ? C12 C11 H11A 109.9 . . ? C10 C11 H11A 109.9 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C11 O2 H2D 109.5 . . ? O3 C13 N3 124.6(2) . . ? O3 C13 C10 120.5(2) . . ? N3 C13 C10 114.8(2) . . ? C13 N3 C14 120.7(2) . . ? C13 N3 H3A 119.7 . . ? C14 N3 H3A 119.7 . . ? N3 C14 C15B 110.9(5) . . ? N3 C14 C19 106.22(19) . . ? C15B C14 C19 117.3(7) . . ? N3 C14 C15A 110.0(6) . . ? C19 C14 C15A 107.5(9) . . ? N3 C14 H14A 111.0 . . ? C19 C14 H14A 111.0 . . ? C15A C14 H14A 111.0 . . ? C16A C15A C14 115.2(15) . . ? C16A C15A H15A 108.5 . . ? C14 C15A H15A 108.5 . . ? C16A C15A H15B 108.5 . . ? C14 C15A H15B 108.5 . . ? H15A C15A H15B 107.5 . . ? C17A C16A C15A 151.3(12) . . ? C17A C16A C18A 97.7(5) . . ? C15A C16A C18A 111.0(11) . . ? C17A C16A H16A 90.2 . . ? C15A C16A H16A 90.2 . . ? C18A C16A H16A 90.2 . . ? C16A C17A H17A 109.5 . . ? C16A C17A H17B 109.5 . . ? H17A C17A H17B 109.5 . . ? C16A C17A H17C 109.5 . . ? H17A C17A H17C 109.5 . . ? H17B C17A H17C 109.5 . . ? C16A C18A H18A 109.5 . . ? C16A C18A H18B 109.5 . . ? H18A C18A H18B 109.5 . . ? C16A C18A H18C 109.5 . . ? H18A C18A H18C 109.5 . . ? H18B C18A H18C 109.5 . . ? C14 C15B C16B 116.2(12) . . ? C14 C15B H15C 108.2 . . ? C16B C15B H15C 108.2 . . ? C14 C15B H15D 108.2 . . ? C16B C15B H15D 108.2 . . ? H15C C15B H15D 107.4 . . ? C17B C16B C15B 144.6(10) . . ? C17B C16B C18B 103.8(7) . . ? C15B C16B C18B 109.2(10) . . ? C17B C16B H16B 94.8 . . ? C15B C16B H16B 94.8 . . ? C18B C16B H16B 94.8 . . ? C16B C17B H17D 109.5 . . ? C16B C17B H17E 109.5 . . ? H17D C17B H17E 109.5 . . ? C16B C17B H17F 109.5 . . ? H17D C17B H17F 109.5 . . ? H17E C17B H17F 109.5 . . ? C16B C18B H18D 109.5 . . ? C16B C18B H18E 109.5 . . ? H18D C18B H18E 109.5 . . ? C16B C18B H18F 109.5 . . ? H18D C18B H18F 109.5 . . ? H18E C18B H18F 109.5 . . ? O4 C19 N4 124.4(2) . . ? O4 C19 C14 120.9(2) . . ? N4 C19 C14 114.7(2) . . ? C19 N4 C20 121.8(2) . . ? C19 N4 H4B 119.1 . . ? C20 N4 H4B 119.1 . . ? N4 C20 C25 107.1(2) . . ? N4 C20 C21 111.7(2) . . ? C25 C20 C21 109.9(2) . . ? N4 C20 H20A 109.4 . . ? C25 C20 H20A 109.4 . . ? C21 C20 H20A 109.4 . . ? C22 C21 C23 111.9(2) . . ? C22 C21 C20 109.6(2) . . ? C23 C21 C20 112.5(2) . . ? C22 C21 H21A 107.5 . . ? C23 C21 H21A 107.5 . . ? C20 C21 H21A 107.5 . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C24 C23 C21 115.3(2) . . ? C24 C23 H23A 108.4 . . ? C21 C23 H23A 108.4 . . ? C24 C23 H23B 108.4 . . ? C21 C23 H23B 108.4 . . ? H23A C23 H23B 107.5 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? O5 C25 N5 122.8(2) . . ? O5 C25 C20 120.3(2) . . ? N5 C25 C20 116.9(2) . . ? C25 N5 C26 121.2(2) . . ? C25 N5 H5B 119.4 . . ? C26 N5 H5B 119.4 . . ? N5 C26 C30 109.77(18) . . ? N5 C26 C27 110.59(19) . . ? C30 C26 C27 112.6(2) . . ? N5 C26 H26A 107.9 . . ? C30 C26 H26A 107.9 . . ? C27 C26 H26A 107.9 . . ? C28 C27 C26 110.4(2) . . ? C28 C27 H27A 109.6 . . ? C26 C27 H27A 109.6 . . ? C28 C27 H27B 109.6 . . ? C26 C27 H27B 109.6 . . ? H27A C27 H27B 108.1 . . ? C27 C28 C29 114.8(2) . . ? C27 C28 H28A 108.6 . . ? C29 C28 H28A 108.6 . . ? C27 C28 H28B 108.6 . . ? C29 C28 H28B 108.6 . . ? H28A C28 H28B 107.5 . . ? O7 C29 O6 123.3(2) . . ? O7 C29 C28 119.7(2) . . ? O6 C29 C28 116.9(2) . . ? O8 C30 N6 122.0(2) . . ? O8 C30 C26 122.6(2) . . ? N6 C30 C26 115.4(2) . . ? C30 N6 H6B 121(3) . . ? C30 N6 H6C 116(3) . . ? H6B N6 H6C 123(4) . . ? H9A O9 H9B 103(6) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C2 C3 -174.2(2) . . . . ? C9 C1 C2 C3 65.3(3) . . . . ? C1 C2 C3 C8 89.0(3) . . . . ? C1 C2 C3 C4 -91.1(3) . . . . ? C8 C3 C4 C5 0.0(5) . . . . ? C2 C3 C4 C5 -179.8(3) . . . . ? C3 C4 C5 C6 0.2(5) . . . . ? C4 C5 C6 C7 -0.1(6) . . . . ? C5 C6 C7 C8 -0.3(6) . . . . ? C6 C7 C8 C3 0.6(5) . . . . ? C4 C3 C8 C7 -0.4(4) . . . . ? C2 C3 C8 C7 179.4(3) . . . . ? N1 C1 C9 O1 -59.9(3) . . . . ? C2 C1 C9 O1 59.7(3) . . . . ? N1 C1 C9 N2 124.7(2) . . . . ? C2 C1 C9 N2 -115.7(2) . . . . ? O1 C9 N2 C10 -0.1(4) . . . . ? C1 C9 N2 C10 175.0(2) . . . . ? C9 N2 C10 C13 -133.6(2) . . . . ? C9 N2 C10 C11 106.6(2) . . . . ? N2 C10 C11 O2 -62.6(3) . . . . ? C13 C10 C11 O2 177.4(2) . . . . ? N2 C10 C11 C12 179.5(2) . . . . ? C13 C10 C11 C12 59.5(3) . . . . ? N2 C10 C13 O3 -61.3(3) . . . . ? C11 C10 C13 O3 59.6(3) . . . . ? N2 C10 C13 N3 121.8(2) . . . . ? C11 C10 C13 N3 -117.3(2) . . . . ? O3 C13 N3 C14 -3.3(4) . . . . ? C10 C13 N3 C14 173.5(2) . . . . ? C13 N3 C14 C15B 98.8(8) . . . . ? C13 N3 C14 C19 -132.7(2) . . . . ? C13 N3 C14 C15A 111.2(10) . . . . ? N3 C14 C15A C16A 167.4(12) . . . . ? C15B C14 C15A C16A -96(5) . . . . ? C19 C14 C15A C16A 52.2(17) . . . . ? C14 C15A C16A C17A -1(4) . . . . ? C14 C15A C16A C18A 179.9(12) . . . . ? N3 C14 C15B C16B -166.5(9) . . . . ? C19 C14 C15B C16B 71.3(14) . . . . ? C15A C14 C15B C16B 106(5) . . . . ? C14 C15B C16B C17B 5(3) . . . . ? C14 C15B C16B C18B 162.7(10) . . . . ? N3 C14 C19 O4 -58.6(3) . . . . ? C15B C14 C19 O4 66.0(7) . . . . ? C15A C14 C19 O4 59.2(7) . . . . ? N3 C14 C19 N4 119.9(2) . . . . ? C15B C14 C19 N4 -115.5(7) . . . . ? C15A C14 C19 N4 -122.4(7) . . . . ? O4 C19 N4 C20 -1.2(4) . . . . ? C14 C19 N4 C20 -179.6(2) . . . . ? C19 N4 C20 C25 -112.8(2) . . . . ? C19 N4 C20 C21 126.8(2) . . . . ? N4 C20 C21 C22 -175.9(2) . . . . ? C25 C20 C21 C22 65.4(3) . . . . ? N4 C20 C21 C23 -50.7(3) . . . . ? C25 C20 C21 C23 -169.4(2) . . . . ? C22 C21 C23 C24 65.0(3) . . . . ? C20 C21 C23 C24 -59.0(3) . . . . ? N4 C20 C25 O5 -69.2(3) . . . . ? C21 C20 C25 O5 52.3(3) . . . . ? N4 C20 C25 N5 109.2(2) . . . . ? C21 C20 C25 N5 -129.3(2) . . . . ? O5 C25 N5 C26 -0.5(4) . . . . ? C20 C25 N5 C26 -178.9(2) . . . . ? C25 N5 C26 C30 -79.6(3) . . . . ? C25 N5 C26 C27 155.6(2) . . . . ? N5 C26 C27 C28 -60.4(2) . . . . ? C30 C26 C27 C28 176.4(2) . . . . ? C26 C27 C28 C29 -175.8(2) . . . . ? C27 C28 C29 O7 -29.5(3) . . . . ? C27 C28 C29 O6 154.2(2) . . . . ? N5 C26 C30 O8 -12.3(4) . . . . ? C27 C26 C30 O8 111.4(3) . . . . ? N5 C26 C30 N6 167.1(2) . . . . ? C27 C26 C30 N6 -69.2(3) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N1 H1A O9 0.97(4) 1.86(4) 2.809(3) 167(4) 1_444 N1 H1B O6 0.91(4) 1.91(5) 2.801(3) 165(4) 1_454 N1 H1B O7 0.91(4) 2.32(4) 3.004(3) 132(3) 1_454 N1 H1C O6 0.94(4) 1.88(4) 2.829(3) 178(4) 1_554 C2 H2A O9 0.99 2.52 3.318(3) 137.3 1_444 N2 H2C O1 0.88 2.12 2.890(3) 145.7 1_455 C10 H10A O3 1.00 2.57 3.443(3) 146.0 1_655 O2 H2D O7 0.84 1.79 2.622(3) 168.0 1_454 N3 H3A O3 0.88 2.15 3.003(3) 161.8 1_655 C14 H14A O4 1.00 2.42 3.336(3) 151.8 1_455 N4 H4B O4 0.88 2.15 3.013(3) 166.6 1_455 N5 H5B O5 0.88 1.99 2.843(3) 161.9 1_655 C28 H28B O7 0.99 2.37 3.222(4) 143.2 1_455 N6 H6B O2 0.82(4) 1.96(4) 2.774(3) 170(4) 1_556 O9 H9A O5 0.83(7) 2.27(7) 3.017(3) 149(6) 1_655 O9 H9B O8 0.87(6) 1.87(6) 2.733(3) 171(5) . _refine_diff_density_max 0.709 _refine_diff_density_min -0.784 _refine_diff_density_rms 0.066 _shelxl_version_number 2013-4 _shelx_res_file ; TITL tom12_a.res in P1 measured ID29 REM Old TITL tom12 in P1 REM SHELXT solution in P1 REM R1 0.128, Rweak 0.057, Alpha 0.000, Orientation as input REM Flack x = -1.976 ( 1.300 ) from Parsons' quotients REM Formula found by SHELXT: C31 N5 O9 CELL 0.7000 4.9205 11.8123 14.6371 99.369 93.376 98.820 ZERR 1.000 0.0010 0.0023 0.0028 0.007 0.007 0.007 LATT -1 SFAC C H N O UNIT 30 50 6 9 TEMP -173.000 L.S. 10 BOND $H size 0.15 0.08 0.05 rem tom gazit group rem colorless elongated plate rem measured ID29 ESRF 0.7Ang wavelength omit 0 -1 0 omit 0 1 0 omit 0 0 1 omit 0 4 5 omit 0 3 -19 omit 2 5 -15 omit 1 1 7 omit 1 -1 8 acta REM Instructions for potential hydrogen bonds EQIV $1 x-1, y-1, z-1 HTAB N1 O9_$1 EQIV $2 x-1, y, z-1 HTAB N1 O6_$2 HTAB N1 O7_$2 EQIV $3 x, y, z-1 HTAB N1 O6_$3 HTAB C2 O9_$1 EQIV $4 x-1, y, z HTAB N2 O1_$4 EQIV $5 x+1, y, z HTAB C10 O3_$5 HTAB O2 O7_$2 HTAB N3 O3_$5 HTAB C14 O4_$4 HTAB N4 O4_$4 HTAB N5 O5_$5 EQIV $6 x, y, z+1 HTAB C28 O7_$4 HTAB N6 O2_$6 HTAB O9 O5_$5 HTAB O9 O8 conf wpdb -2 rem dfix 0.9 N1 H1a N1 H1b N1 H1c dfix 1.5 0.02 c16a c17a c16a c18a dang 2.06 0.005 c17a c18a isor 0.005 c18b rem isor 0.001 c17a eadp c18a c17a eadp c16b c17b free c17a c18a LIST 6 FMAP 2 PLAN 30 rem residue 1 PHE WGHT 0.079400 0.380500 FVAR 1.22430 0.45737 N1 3 0.256082 0.233926 -0.057025 11.00000 0.01807 0.01845 = 0.01274 0.00365 0.00146 0.00672 H1A 2 0.219544 0.155668 -0.091901 11.00000 -1.50000 H1B 2 0.124025 0.275707 -0.071143 11.00000 -1.50000 H1C 2 0.433831 0.265127 -0.071361 11.00000 -1.50000 C1 1 0.213938 0.225217 0.041520 11.00000 0.01275 0.01556 = 0.01267 0.00405 0.00128 0.00404 AFIX 13 H1D 2 0.011848 0.208146 0.049005 11.00000 -1.20000 AFIX 0 C2 1 0.355121 0.126310 0.068644 11.00000 0.02385 0.01960 = 0.01458 0.00588 0.00518 0.01059 AFIX 23 H2A 2 0.289378 0.054396 0.022866 11.00000 -1.20000 H2B 2 0.556863 0.146866 0.065856 11.00000 -1.20000 AFIX 0 C3 1 0.299188 0.102932 0.164301 11.00000 0.02258 0.01971 = 0.01372 0.00573 0.00388 0.01052 C4 1 0.472678 0.158572 0.242632 11.00000 0.03460 0.03476 = 0.01881 0.00554 -0.00166 0.01122 AFIX 43 H4A 2 0.631005 0.213082 0.236541 11.00000 -1.20000 AFIX 0 C5 1 0.412940 0.133908 0.330063 11.00000 0.06638 0.05826 = 0.01399 0.00680 -0.00020 0.03452 AFIX 43 H5A 2 0.531046 0.172118 0.383408 11.00000 -1.20000 AFIX 0 C6 1 0.185014 0.054912 0.339797 11.00000 0.06539 0.05728 = 0.02795 0.02759 0.02010 0.03579 AFIX 43 H6A 2 0.146358 0.038648 0.399602 11.00000 -1.20000 AFIX 0 C7 1 0.010257 -0.001433 0.261597 11.00000 0.04409 0.04288 = 0.04532 0.02691 0.02258 0.01715 AFIX 43 H7A 2 -0.147086 -0.056359 0.267870 11.00000 -1.20000 AFIX 0 C8 1 0.068403 0.023485 0.174849 11.00000 0.02952 0.02653 = 0.02937 0.00957 0.00747 0.00823 AFIX 43 H8A 2 -0.051213 -0.014278 0.121734 11.00000 -1.20000 AFIX 0 C9 1 0.341869 0.338569 0.105703 11.00000 0.01090 0.01725 = 0.01270 0.00422 0.00174 0.00504 O1 4 0.590422 0.373529 0.107130 11.00000 0.01106 0.02545 = 0.01752 -0.00008 0.00289 0.00298 rem residue 2 THR N2 3 0.170385 0.387812 0.161675 11.00000 0.00824 0.01672 = 0.01094 0.00240 0.00243 0.00245 AFIX 43 H2C 2 -0.005692 0.357106 0.155962 11.00000 -1.20000 AFIX 0 C10 1 0.268039 0.490362 0.231333 11.00000 0.01466 0.01855 = 0.00939 0.00131 0.00321 0.00181 AFIX 13 H10A 2 0.474217 0.502720 0.239994 11.00000 -1.20000 AFIX 0 C11 1 0.174359 0.598648 0.201604 11.00000 0.02955 0.01838 = 0.01360 0.00468 0.00782 0.00536 AFIX 13 H11A 2 -0.031461 0.585956 0.190788 11.00000 -1.20000 AFIX 0 C12 1 0.273005 0.706409 0.274338 11.00000 0.06533 0.01912 = 0.02023 -0.00228 0.01066 0.00510 AFIX 33 H12A 2 0.212189 0.773883 0.253415 11.00000 -1.50000 H12B 2 0.475014 0.719415 0.283531 11.00000 -1.50000 H12C 2 0.195589 0.695598 0.333091 11.00000 -1.50000 AFIX 0 O2 4 0.294286 0.617794 0.118698 11.00000 0.03452 0.01913 = 0.01326 0.00429 0.00618 -0.00110 AFIX 83 H2D 2 0.217917 0.566301 0.074322 11.00000 -1.50000 AFIX 0 C13 1 0.149980 0.472667 0.323308 11.00000 0.01203 0.01986 = 0.01041 0.00346 0.00217 0.00418 O3 4 -0.101455 0.457336 0.329055 11.00000 0.01142 0.03674 = 0.01362 0.00522 0.00338 0.00323 rem residue 3 Leu N3 3 0.340204 0.481017 0.394970 11.00000 0.01008 0.02742 = 0.01104 0.00387 0.00263 0.00433 AFIX 43 H3A 2 0.516277 0.488238 0.385170 11.00000 -1.20000 AFIX 0 C14 1 0.257542 0.478223 0.488919 11.00000 0.01588 0.02007 = 0.00959 0.00274 0.00411 0.00295 AFIX 13 H14A 2 0.059127 0.486717 0.492380 11.00000 -1.20000 AFIX 0 part 1 eadp c15b c15a eadp c16b c16a same c15b > c18b C15A 1 0.314500 0.360633 0.521155 21.00000 0.02497 0.02052 = 0.01571 0.00498 0.00080 0.00692 AFIX 23 H15A 2 0.180121 0.295216 0.485304 21.00000 -1.20000 H15B 2 0.501151 0.347530 0.505066 21.00000 -1.20000 AFIX 0 C16A 1 0.296295 0.357884 0.622700 21.00000 0.04682 0.04407 = 0.03255 0.02076 0.00864 0.00995 AFIX 13 H16A 2 0.094828 0.325765 0.610675 21.00000 -1.20000 AFIX 0 C17A 1 0.262850 0.399626 0.694077 21.00000 0.03981 0.03054 = 0.01959 0.01353 0.00256 0.00204 AFIX 137 H17A 2 0.368760 0.367854 0.739770 21.00000 -1.50000 H17B 2 0.066094 0.383962 0.703613 21.00000 -1.50000 H17C 2 0.324251 0.483811 0.701685 21.00000 -1.50000 AFIX 0 C18A 1 0.354376 0.239943 0.646480 21.00000 0.03981 0.03054 = 0.01959 0.01353 0.00256 0.00204 AFIX 137 H18A 2 0.534150 0.225740 0.626048 21.00000 -1.50000 H18B 2 0.209798 0.177131 0.614626 21.00000 -1.50000 H18C 2 0.355830 0.242535 0.713772 21.00000 -1.50000 AFIX 0 part 2 C15B 1 0.250497 0.360008 0.512654 -21.00000 0.02497 0.02052 = 0.01571 0.00498 0.00080 0.00692 AFIX 23 H15C 2 0.442977 0.346201 0.521481 -21.00000 -1.20000 H15D 2 0.158085 0.302248 0.458856 -21.00000 -1.20000 AFIX 0 C16B 1 0.106049 0.337315 0.598599 -21.00000 0.04682 0.04407 = 0.03255 0.02076 0.00864 0.00995 AFIX 13 H16B 2 0.280602 0.348323 0.639960 -21.00000 -1.20000 AFIX 0 C17B 1 -0.009767 0.372479 0.651248 -21.00000 0.04682 0.04407 = 0.03255 0.02076 0.00864 0.00995 AFIX 137 H17D 2 0.068392 0.361834 0.711807 -21.00000 -1.50000 H17E 2 -0.201675 0.332617 0.640201 -21.00000 -1.50000 H17F 2 -0.003688 0.455675 0.650682 -21.00000 -1.50000 AFIX 0 C18B 1 0.038587 0.205654 0.596358 -21.00000 0.09473 0.03583 = 0.02676 0.01672 -0.01768 -0.03243 AFIX 137 H18D 2 -0.024558 0.190829 0.656224 -21.00000 -1.50000 H18E 2 0.204371 0.170818 0.584690 -21.00000 -1.50000 H18F 2 -0.107146 0.171214 0.546727 -21.00000 -1.50000 AFIX 0 part 0 C19 1 0.445302 0.578943 0.552169 11.00000 0.01405 0.01997 = 0.00922 0.00564 0.00246 0.00566 O4 4 0.698416 0.584882 0.556979 11.00000 0.01302 0.02649 = 0.01956 0.00118 0.00251 0.00658 rem residue 4 IsoLeu N4 3 0.313067 0.658758 0.598373 11.00000 0.01006 0.02059 = 0.01394 0.00105 0.00073 0.00436 AFIX 43 H4B 2 0.131779 0.649128 0.590526 11.00000 -1.20000 AFIX 0 C20 1 0.461999 0.761294 0.661402 11.00000 0.01270 0.02203 = 0.01180 0.00295 0.00250 0.00376 AFIX 13 H20A 2 0.665127 0.763740 0.657931 11.00000 -1.20000 AFIX 0 C21 1 0.381448 0.874422 0.637300 11.00000 0.01575 0.02366 = 0.01686 0.00583 0.00345 0.00595 AFIX 13 H21A 2 0.184851 0.875038 0.650924 11.00000 -1.20000 AFIX 0 C22 1 0.557291 0.979088 0.700420 11.00000 0.02763 0.02429 = 0.02050 0.00379 0.00227 0.00108 AFIX 33 H22A 2 0.507229 1.051032 0.684376 11.00000 -1.50000 H22B 2 0.752927 0.977697 0.691976 11.00000 -1.50000 H22C 2 0.524452 0.975637 0.765375 11.00000 -1.50000 AFIX 0 C23 1 0.399505 0.881802 0.533963 11.00000 0.01926 0.02976 = 0.02024 0.01043 0.00211 0.00612 AFIX 23 H23A 2 0.265195 0.817391 0.496813 11.00000 -1.20000 H23B 2 0.343008 0.955685 0.522919 11.00000 -1.20000 AFIX 0 C24 1 0.684138 0.875919 0.498367 11.00000 0.02359 0.03960 = 0.02158 0.01293 0.00681 0.00457 AFIX 33 H24A 2 0.675946 0.882045 0.432324 11.00000 -1.50000 H24B 2 0.739785 0.801719 0.506408 11.00000 -1.50000 H24C 2 0.818962 0.940224 0.533573 11.00000 -1.50000 AFIX 0 C25 1 0.388555 0.748271 0.759627 11.00000 0.01246 0.01876 = 0.01358 0.00367 0.00244 0.00378 O5 4 0.152881 0.755656 0.782308 11.00000 0.01267 0.03849 = 0.02030 0.01153 0.00641 0.00870 rem residue 5 glu N5 3 0.586089 0.726150 0.816841 11.00000 0.01021 0.01829 = 0.01292 0.00485 0.00411 0.00471 AFIX 43 H5B 2 0.750255 0.721106 0.797288 11.00000 -1.20000 AFIX 0 C26 1 0.535634 0.710155 0.911105 11.00000 0.01336 0.01551 = 0.01218 0.00609 0.00469 0.00442 AFIX 13 H26A 2 0.343952 0.666610 0.909681 11.00000 -1.20000 AFIX 0 C27 1 0.736735 0.636677 0.947428 11.00000 0.01421 0.01570 = 0.01426 0.00411 0.00295 0.00570 AFIX 23 H27A 2 0.928923 0.676703 0.947586 11.00000 -1.20000 H27B 2 0.702318 0.627995 1.012088 11.00000 -1.20000 AFIX 0 C28 1 0.699714 0.516992 0.886370 11.00000 0.01764 0.01709 = 0.01819 0.00507 0.00122 0.00673 AFIX 23 H28A 2 0.745394 0.526961 0.822880 11.00000 -1.20000 H28B 2 0.502918 0.481096 0.882310 11.00000 -1.20000 AFIX 0 C29 1 0.875054 0.433510 0.920146 11.00000 0.01663 0.01942 = 0.01319 0.00511 0.00721 0.00756 O6 4 0.784846 0.325425 0.895828 11.00000 0.02424 0.01769 = 0.02029 0.00458 0.00462 0.00643 O7 4 1.102056 0.472773 0.965230 11.00000 0.01943 0.02292 = 0.01689 0.00431 0.00110 0.00729 C30 1 0.551127 0.828577 0.973423 11.00000 0.02106 0.01680 = 0.01509 0.00452 0.00764 0.00827 N6 3 0.454666 0.825680 1.056685 11.00000 0.03044 0.01662 = 0.01601 0.00464 0.01065 0.00488 H6B 2 0.388025 0.763450 1.071170 11.00000 0.01880 H6C 2 0.459330 0.895856 1.093450 11.00000 0.02423 O8 4 0.642901 0.920029 0.948934 11.00000 0.05692 0.01485 = 0.02900 0.00706 0.02404 0.01010 mole 2 O9 4 1.079115 1.001537 0.857114 11.00000 0.02993 0.01906 = 0.02638 0.00031 0.00443 0.00357 H9A 2 1.163192 0.946460 0.840928 11.00000 0.05901 H9B 2 0.938871 0.968966 0.882443 11.00000 0.04673 HKLF 4 REM tom12_a.res in P1 measured ID29 REM R1 = 0.0470 for 3755 Fo > 4sig(Fo) and 0.0472 for all 3773 data REM 448 parameters refined using 18 restraints END WGHT 0.0765 0.3260 REM Highest difference peak 0.709, deepest hole -0.784, 1-sigma level 0.066 Q1 1 0.4394 0.8153 0.6488 11.00000 0.05 0.33 Q2 1 0.2142 0.5417 0.2170 11.00000 0.05 0.28 Q3 1 -0.0762 0.2179 0.6000 11.00000 0.05 0.27 Q4 1 0.1085 0.6989 0.7608 11.00000 0.05 0.27 Q5 1 0.4004 0.7071 0.6209 11.00000 0.05 0.26 Q6 1 0.1358 0.1973 0.5955 11.00000 0.05 0.26 Q7 1 0.7968 0.4831 0.9058 11.00000 0.05 0.26 Q8 1 0.3087 0.1803 0.0566 11.00000 0.05 0.25 Q9 1 0.2748 0.2815 0.0785 11.00000 0.05 0.25 Q10 1 0.7740 0.3795 0.8857 11.00000 0.05 0.24 Q11 1 0.4738 0.3609 0.7149 11.00000 0.05 0.24 Q12 1 0.3300 0.3350 0.4004 11.00000 0.05 0.23 Q13 1 0.2450 0.4197 0.5050 11.00000 0.05 0.23 Q14 1 0.3277 0.4511 0.6825 11.00000 0.05 0.23 Q15 1 -0.1528 0.3680 0.3357 11.00000 0.05 0.22 Q16 1 0.6991 0.5737 0.9168 11.00000 0.05 0.22 Q17 1 0.7554 0.3777 0.9100 11.00000 0.05 0.22 Q18 1 0.1917 0.4407 0.2007 11.00000 0.05 0.22 Q19 1 0.6650 0.6753 0.9401 11.00000 0.05 0.22 Q20 1 0.3402 0.5283 0.5388 11.00000 0.05 0.21 Q21 1 0.1365 -0.1337 0.1592 11.00000 0.05 0.21 Q22 1 0.3748 0.2703 0.6784 11.00000 0.05 0.20 Q23 1 0.4705 0.3043 0.3959 11.00000 0.05 0.20 Q24 1 0.2186 0.7825 0.1742 11.00000 0.05 0.20 Q25 1 0.3873 0.6211 0.5858 11.00000 0.05 0.20 Q26 1 0.9035 0.2803 0.9000 11.00000 0.05 0.20 Q27 1 0.5808 0.7729 0.9534 11.00000 0.05 0.20 Q28 1 0.5684 0.2138 0.7140 11.00000 0.05 0.20 Q29 1 0.3244 0.7374 0.5822 11.00000 0.05 0.20 Q30 1 -0.0588 0.5219 0.3503 11.00000 0.05 0.19 ; _shelx_res_checksum 8319 _shelx_hkl_file ; 0 0 1 1151.00 46.30 0 0 2 714.40 29.00 0 0 3 3772.00 151.70 0 0 4 578.80 23.30 0 0 5 2368.00 134.90 0 0 6 156.30 6.30 0 0 7 1252.00 50.60 0 0 8 107.10 4.40 0 0 9 5.30 0.40 0 0 10 46.30 2.20 0 0 11 352.90 14.30 0 0 12 18.00 0.80 0 0 13 230.10 9.40 0 0 14 312.90 12.70 0 0 15 29.10 1.30 0 0 16 7.40 0.50 0 0 17 24.80 1.10 0 1 -19 54.90 2.40 0 1 -18 30.20 1.30 0 1 -17 2.00 0.30 0 1 -16 6.90 0.40 0 1 -15 1.20 0.30 0 1 -14 473.10 19.20 0 1 -13 170.90 9.80 0 1 -12 22.20 1.00 0 1 -11 157.10 6.40 0 1 -10 238.70 9.70 0 1 -9 272.70 15.60 0 1 -8 191.60 7.80 0 1 -7 374.50 15.10 0 1 -6 1342.00 54.20 0 1 -5 3056.00 173.80 0 1 -4 1620.00 65.20 0 1 -3 383.20 17.90 0 1 -2 158.10 6.40 0 1 -1 2669.00 108.10 0 1 0 1685.00 78.60 0 1 1 1126.00 45.30 0 1 2 830.40 33.40 0 1 3 917.10 37.00 0 1 4 1866.00 75.20 0 1 5 95.40 3.90 0 1 6 108.40 4.40 0 1 7 272.30 11.00 0 1 8 100.80 4.10 0 1 9 715.20 40.80 0 1 10 775.60 31.30 0 1 11 340.30 13.80 0 1 12 364.00 14.70 0 1 13 42.50 1.80 0 1 14 23.50 1.10 0 1 15 71.70 4.30 0 1 16 7.60 0.50 0 1 17 152.50 6.30 0 2 -19 121.40 3.70 0 2 -18 8.80 0.50 0 2 -17 12.00 0.60 0 2 -16 16.10 0.80 0 2 -15 69.50 2.90 0 2 -14 101.80 4.20 0 2 -13 371.20 21.30 0 2 -12 36.20 1.50 0 2 -11 48.90 2.00 0 2 -10 89.40 3.70 0 2 -9 610.00 34.80 0 2 -8 79.70 3.30 0 2 -7 1717.00 69.40 0 2 -6 4348.00 175.50 0 2 -5 2962.00 168.40 0 2 -4 604.20 24.40 0 2 -3 662.20 26.60 0 2 -2 54.60 2.20 0 2 -1 1587.00 63.90 0 2 0 635.90 25.70 0 2 1 3983.00 160.50 0 2 2 2336.00 94.00 0 2 3 330.50 13.30 0 2 4 1162.00 66.10 0 2 5 230.70 9.30 0 2 6 264.40 10.70 0 2 7 193.90 7.80 0 2 8 1231.00 49.60 0 2 9 102.20 4.20 0 2 10 69.00 2.80 0 2 11 165.80 6.70 0 2 13 345.10 14.00 0 2 14 7.40 0.50 0 2 15 193.40 7.90 0 2 16 59.00 2.50 0 2 17 201.80 8.20 0 3 -19 49.10 1.70 0 3 -18 0.90 0.30 0 3 -17 27.90 1.20 0 3 -16 79.70 3.30 0 3 -15 55.40 2.30 0 3 -14 41.10 1.70 0 3 -13 156.10 6.40 0 3 -12 66.70 2.80 0 3 -11 72.10 3.00 0 3 -10 96.70 4.00 0 3 -8 267.40 10.80 0 3 -7 2221.00 89.60 0 3 -6 1894.00 76.50 0 3 -5 225.80 9.10 0 3 -4 638.80 36.40 0 3 -3 254.40 10.30 0 3 -2 7479.00 300.70 0 3 -1 1787.00 72.00 0 3 0 559.30 22.50 0 3 1 237.10 9.60 0 3 2 875.50 49.80 0 3 3 4058.00 230.70 0 3 4 1510.00 60.80 0 3 5 374.60 15.10 0 3 6 106.60 4.30 0 3 7 214.90 8.70 0 3 8 25.40 1.50 0 3 9 155.20 6.30 0 3 10 490.30 19.80 0 3 11 788.70 31.90 0 3 13 7.00 0.50 0 3 14 2.30 0.30 0 3 15 29.40 1.30 0 3 16 105.10 4.30 0 3 17 140.60 5.80 0 4 -19 179.20 8.50 0 4 -18 66.40 2.80 0 4 -17 0.80 0.30 0 4 -16 68.60 2.90 0 4 -15 32.50 1.40 0 4 -14 51.50 2.20 0 4 -13 88.90 3.70 0 4 -12 10.80 0.60 0 4 -11 263.60 10.70 0 4 -10 401.10 16.20 0 4 -9 314.70 12.80 0 4 -8 31.60 1.30 0 4 -7 27.90 1.20 0 4 -6 600.90 24.20 0 4 -5 651.60 26.30 0 4 -4 1089.00 43.90 0 4 -3 1888.00 75.90 0 4 -2 5765.00 327.70 0 4 -1 585.60 33.30 0 4 0 301.70 17.20 0 4 1 644.80 26.00 0 4 2 6611.00 265.80 0 4 3 579.80 23.40 0 4 4 241.40 9.80 0 4 5 1872.00 75.40 0 4 6 312.20 12.60 0 4 7 133.40 7.60 0 4 8 120.60 4.90 0 4 9 445.30 18.00 0 4 10 140.30 5.70 0 4 11 278.30 13.00 0 4 12 155.30 6.30 0 4 13 19.30 0.90 0 4 14 11.00 0.60 0 4 15 16.00 0.80 0 4 16 14.00 0.90 0 4 17 20.70 1.00 0 5 -18 9.20 0.60 0 5 -17 13.80 0.70 0 5 -16 75.20 3.10 0 5 -15 196.20 11.30 0 5 -14 53.50 2.30 0 5 -13 63.90 2.70 0 5 -12 359.70 20.60 0 5 -11 582.50 23.50 0 5 -10 8.50 0.50 0 5 -9 449.10 18.20 0 5 -8 512.90 29.30 0 5 -7 896.70 36.20 0 5 -6 44.80 1.90 0 5 -5 75.40 3.10 0 5 -4 242.90 9.80 0 5 -3 756.50 30.50 0 5 -2 651.50 26.20 0 5 -1 824.70 33.20 0 5 0 34.30 1.50 0 5 1 129.90 5.30 0 5 2 4027.00 162.00 0 5 3 1412.00 56.80 0 5 4 102.10 4.20 0 5 5 163.00 6.60 0 5 6 493.20 28.20 0 5 7 117.80 4.80 0 5 8 63.60 2.60 0 5 9 220.00 8.90 0 5 10 255.00 14.60 0 5 11 19.90 0.90 0 5 12 126.80 5.20 0 5 14 68.60 2.90 0 5 15 12.50 0.70 0 5 16 85.60 3.60 0 6 -18 61.30 2.60 0 6 -17 58.20 2.50 0 6 -16 55.80 2.40 0 6 -15 1.60 0.30 0 6 -14 32.90 1.50 0 6 -13 40.00 1.70 0 6 -12 171.10 7.00 0 6 -11 1291.00 52.00 0 6 -10 433.40 17.50 0 6 -9 81.80 3.40 0 6 -8 2525.00 101.80 0 6 -7 104.50 6.10 0 6 -6 64.00 2.70 0 6 -5 651.60 26.30 0 6 -4 42.70 1.80 0 6 -3 42.00 1.80 0 6 -2 520.10 21.00 0 6 -1 533.00 21.50 0 6 0 150.00 6.10 0 6 1 191.60 7.80 0 6 2 154.20 6.30 0 6 3 600.00 24.20 0 6 5 748.70 30.20 0 6 6 127.10 5.20 0 6 7 95.70 3.90 0 6 8 113.70 4.70 0 6 9 90.70 5.30 0 6 10 102.90 4.20 0 6 11 65.90 2.70 0 6 12 61.00 3.70 0 6 13 32.50 1.40 0 6 14 101.50 4.20 0 6 15 180.20 7.40 0 6 16 8.10 0.80 0 7 -18 74.40 3.10 0 7 -17 14.30 0.80 0 7 -16 91.20 3.80 0 7 -15 11.20 0.80 0 7 -14 108.80 4.50 0 7 -13 268.00 10.90 0 7 -12 94.90 3.90 0 7 -11 866.50 49.50 0 7 -10 83.00 3.40 0 7 -9 399.10 16.20 0 7 -8 170.70 6.90 0 7 -7 232.40 9.40 0 7 -6 204.90 8.30 0 7 -5 298.40 17.10 0 7 -4 258.70 14.80 0 7 -3 248.90 10.10 0 7 -2 798.00 32.20 0 7 -1 176.90 7.20 0 7 0 635.40 25.60 0 7 1 269.10 15.40 0 7 2 169.40 9.70 0 7 3 136.00 5.60 0 7 4 150.60 6.10 0 7 5 125.40 5.10 0 7 6 195.40 7.90 0 7 7 151.70 6.20 0 7 8 196.20 9.20 0 7 9 269.80 10.90 0 7 10 89.80 3.70 0 7 11 47.10 2.90 0 7 12 78.10 3.20 0 7 13 25.00 1.10 0 7 14 425.70 17.20 0 7 15 10.50 0.60 0 8 -17 233.50 9.50 0 8 -16 12.90 0.90 0 8 -15 43.90 2.20 0 8 -14 173.60 7.10 0 8 -13 13.80 0.80 0 8 -12 59.10 2.50 0 8 -11 145.20 5.90 0 8 -10 92.20 4.40 0 8 -9 62.00 2.60 0 8 -8 229.30 9.30 0 8 -7 129.40 5.30 0 8 -6 88.20 3.60 0 8 -5 9.00 0.50 0 8 -4 144.30 5.90 0 8 -3 376.20 15.20 0 8 -2 556.00 22.40 0 8 -1 14.60 0.70 0 8 0 1632.00 65.70 0 8 1 43.80 1.90 0 8 2 170.10 6.90 0 8 3 255.40 10.40 0 8 4 66.30 2.80 0 8 5 86.40 3.60 0 8 6 131.70 7.60 0 8 7 123.80 5.10 0 8 8 74.80 3.10 0 8 9 65.40 2.70 0 8 11 18.40 0.90 0 8 12 100.30 4.10 0 8 13 109.40 4.50 0 8 14 173.60 7.10 0 9 -17 157.00 7.50 0 9 -16 17.50 0.90 0 9 -15 50.40 2.20 0 9 -14 78.80 3.30 0 9 -13 178.20 7.30 0 9 -12 105.10 4.30 0 9 -11 1.30 0.30 0 9 -10 26.40 1.20 0 9 -9 173.00 7.10 0 9 -7 242.30 9.80 0 9 -6 0.90 0.30 0 9 -5 179.20 7.30 0 9 -4 7.40 0.40 0 9 -3 179.50 7.30 0 9 -2 141.30 5.80 0 9 -1 357.50 14.50 0 9 0 284.30 11.50 0 9 1 741.70 29.90 0 9 2 179.80 7.30 0 9 3 122.80 5.00 0 9 5 15.60 0.80 0 9 6 12.70 0.70 0 9 7 73.70 3.10 0 9 8 43.90 1.90 0 9 9 41.20 1.80 0 9 10 21.30 1.00 0 9 11 8.50 0.50 0 9 12 72.50 3.00 0 9 13 16.70 0.80 0 10 -16 45.80 2.00 0 10 -15 10.40 0.70 0 10 -14 9.60 0.60 0 10 -13 112.80 4.70 0 10 -12 1.30 0.30 0 10 -11 39.10 1.70 0 10 -10 35.40 1.60 0 10 -9 117.20 4.80 0 10 -8 150.20 6.20 0 10 -7 447.00 18.10 0 10 -6 452.50 18.30 0 10 -4 14.00 1.00 0 10 -3 210.80 8.60 0 10 -2 166.10 6.80 0 10 -1 439.90 17.80 0 10 1 1202.00 68.50 0 10 2 77.20 3.20 0 10 3 122.80 5.00 0 10 4 98.80 4.10 0 10 5 20.70 1.00 0 10 6 17.10 0.80 0 10 8 6.80 0.50 0 10 9 64.00 2.70 0 10 10 28.20 1.30 0 10 11 25.40 1.20 0 10 12 50.10 2.50 0 11 -15 16.90 0.90 0 11 -14 43.40 1.90 0 11 -13 45.70 2.00 0 11 -12 19.60 1.00 0 11 -11 88.10 3.70 0 11 -10 347.20 14.10 0 11 -9 248.50 10.10 0 11 -8 11.30 0.70 0 11 -7 112.50 4.60 0 11 -6 288.10 11.70 0 11 -5 384.10 15.60 0 11 -4 14.80 0.70 0 11 -3 37.20 1.60 0 11 -2 63.10 2.70 0 11 -1 89.10 3.70 0 11 0 45.50 1.90 0 11 1 31.10 1.40 0 11 2 32.20 1.40 0 11 3 60.30 2.50 0 11 4 26.20 1.20 0 11 5 102.20 6.00 0 11 6 51.70 2.20 0 11 7 15.60 0.80 0 11 8 120.50 5.00 0 11 9 45.60 2.00 0 11 10 85.20 3.50 0 12 -14 16.80 0.90 0 12 -13 2.20 0.30 0 12 -11 33.30 1.50 0 12 -10 191.80 7.80 0 12 -9 20.40 1.00 0 12 -8 75.50 3.20 0 12 -7 49.30 4.30 0 12 -6 135.50 5.60 0 12 -5 66.20 2.80 0 12 -4 13.80 0.70 0 12 -3 15.30 0.80 0 12 -2 29.10 1.30 0 12 -1 84.50 3.50 0 12 0 86.70 3.60 0 12 1 68.70 4.10 0 12 2 73.00 4.30 0 12 3 174.40 7.10 0 12 4 69.20 2.90 0 12 5 53.20 2.30 0 12 6 69.70 2.90 0 12 7 1.70 0.40 0 12 8 23.40 1.10 0 12 9 77.10 3.20 0 13 -12 35.20 1.60 0 13 -11 30.90 1.40 0 13 -10 49.10 3.10 0 13 -9 47.00 2.00 0 13 -8 33.40 1.50 0 13 -7 18.10 0.90 0 13 -6 71.20 3.00 0 13 -5 22.50 1.10 0 13 -4 69.10 2.90 0 13 -3 27.00 1.20 0 13 -2 91.30 3.80 0 13 -1 225.30 9.20 0 13 0 10.80 0.60 0 13 1 36.40 1.60 0 13 2 43.10 1.90 0 13 3 113.50 4.70 0 13 5 13.40 0.70 0 13 6 80.40 3.40 0 13 7 10.90 0.60 0 14 -10 98.10 4.10 0 14 -9 56.80 2.40 0 14 -8 43.90 1.90 0 14 -7 55.00 2.40 0 14 -5 4.60 0.60 0 14 -4 34.30 1.50 0 14 -3 35.80 1.60 0 14 -2 70.60 3.00 0 14 -1 15.00 1.10 0 14 1 23.70 1.10 0 14 2 24.90 1.20 0 14 3 216.30 8.80 0 14 4 5.30 0.40 0 15 -7 61.50 3.00 0 15 -6 3.20 0.40 0 15 -5 22.10 1.10 0 15 -4 7.00 0.50 0 15 -3 21.80 1.10 0 15 -2 5.00 0.40 0 15 -1 5.00 0.40 0 15 0 0.20 0.30 1 -15 -2 32.50 1.50 1 -15 -1 39.00 1.70 1 -15 0 231.70 9.40 1 -15 1 9.80 0.60 1 -15 2 11.70 0.70 1 -15 3 8.80 0.50 1 -15 4 17.90 0.90 1 -15 5 21.80 1.10 1 -15 6 5.50 0.70 1 -15 7 28.10 1.90 1 -15 8 93.70 5.50 1 -14 -5 141.10 5.80 1 -14 -4 192.20 7.90 1 -14 -3 0.80 0.30 1 -14 -2 13.30 1.00 1 -14 -1 6.10 0.40 1 -14 0 48.90 2.10 1 -14 1 225.80 9.20 1 -14 2 39.50 1.70 1 -14 3 105.00 4.40 1 -14 4 99.00 4.10 1 -14 5 20.90 1.00 1 -14 6 10.80 0.60 1 -14 7 29.20 1.90 1 -14 8 176.70 7.30 1 -14 9 92.80 4.50 1 -14 10 165.40 7.80 1 -14 11 26.40 1.70 1 -13 -7 59.80 2.50 1 -13 -6 15.50 0.80 1 -13 -4 39.80 1.70 1 -13 -3 26.70 1.20 1 -13 -2 75.20 3.10 1 -13 -1 16.20 0.80 1 -13 0 100.00 4.10 1 -13 1 27.60 1.30 1 -13 2 31.80 1.40 1 -13 3 52.10 2.20 1 -13 4 4.70 0.40 1 -13 5 7.40 0.50 1 -13 6 35.50 1.60 1 -13 7 130.90 5.40 1 -13 8 53.30 2.30 1 -13 9 104.50 4.30 1 -13 10 61.20 2.60 1 -13 11 24.90 1.40 1 -13 12 33.90 2.20 1 -13 13 52.40 3.20 1 -12 -9 23.00 1.10 1 -12 -8 4.70 0.40 1 -12 -7 1.90 0.30 1 -12 -6 11.10 0.60 1 -12 -5 14.20 0.70 1 -12 -4 38.50 1.70 1 -12 -2 44.60 1.90 1 -12 -1 3.90 0.30 1 -12 0 86.20 3.60 1 -12 1 14.20 0.70 1 -12 2 55.50 2.40 1 -12 3 286.60 11.60 1 -12 4 17.30 0.90 1 -12 5 63.60 2.70 1 -12 6 35.60 1.60 1 -12 7 14.30 0.70 1 -12 8 227.90 13.20 1 -12 9 8.60 0.50 1 -12 10 143.70 5.90 1 -12 11 108.70 4.50 1 -12 12 180.20 7.40 1 -12 13 30.20 1.90 1 -11 -11 72.20 3.00 1 -11 -10 101.70 4.20 1 -11 -9 5.30 0.40 1 -11 -8 27.70 1.30 1 -11 -7 34.90 1.50 1 -11 -6 200.00 11.50 1 -11 -5 11.60 0.60 1 -11 -4 7.70 0.50 1 -11 -3 5.40 0.40 1 -11 -2 115.10 4.70 1 -11 -1 178.20 7.30 1 -11 0 176.30 7.20 1 -11 1 111.80 4.60 1 -11 2 24.70 1.10 1 -11 3 100.30 4.20 1 -11 4 64.30 2.70 1 -11 5 8.00 0.50 1 -11 6 27.90 1.30 1 -11 7 364.90 14.80 1 -11 8 191.30 7.80 1 -11 9 8.10 0.50 1 -11 11 95.90 4.00 1 -11 12 223.10 9.10 1 -11 13 370.20 15.00 1 -11 14 20.50 1.40 1 -11 15 6.00 0.80 1 -10 -12 92.10 3.80 1 -10 -11 115.80 4.80 1 -10 -10 57.50 2.40 1 -10 -9 16.00 0.80 1 -10 -8 6.80 0.50 1 -10 -7 54.00 2.30 1 -10 -6 74.80 3.10 1 -10 -5 63.00 2.60 1 -10 -4 46.70 2.00 1 -10 -3 126.10 5.20 1 -10 -2 620.30 35.40 1 -10 -1 322.00 13.10 1 -10 0 37.60 1.60 1 -10 1 789.10 31.80 1 -10 2 226.80 9.20 1 -10 3 249.70 10.10 1 -10 4 186.30 7.60 1 -10 5 147.70 6.00 1 -10 6 113.00 6.60 1 -10 7 49.00 2.10 1 -10 8 259.80 10.60 1 -10 9 82.50 3.40 1 -10 10 85.80 3.60 1 -10 11 32.50 1.40 1 -10 12 211.60 8.60 1 -10 13 15.80 0.80 1 -10 14 15.80 0.80 1 -10 15 15.80 1.20 1 -10 16 34.60 2.20 1 -9 -13 4.40 0.40 1 -9 -11 41.40 1.80 1 -9 -10 38.10 1.60 1 -9 -9 83.60 3.50 1 -9 -8 2.00 0.30 1 -9 -7 91.10 3.80 1 -9 -6 262.70 10.70 1 -9 -4 262.80 10.70 1 -9 -3 59.80 2.50 1 -9 -2 1247.00 50.20 1 -9 -1 43.90 1.90 1 -9 0 557.80 22.50 1 -9 1 704.50 28.40 1 -9 2 26.60 1.20 1 -9 3 151.30 6.20 1 -9 4 190.00 7.70 1 -9 5 330.70 13.40 1 -9 6 154.30 6.30 1 -9 7 15.50 0.80 1 -9 8 87.20 3.60 1 -9 9 119.40 4.90 1 -9 10 43.20 1.90 1 -9 11 68.00 2.90 1 -9 12 139.90 5.70 1 -9 13 64.70 2.70 1 -9 14 114.50 4.70 1 -9 15 15.00 0.90 1 -9 16 130.70 7.60 1 -9 17 19.00 1.10 1 -8 -14 48.00 2.10 1 -8 -12 20.50 1.00 1 -8 -11 14.40 0.70 1 -8 -10 0.90 0.30 1 -8 -9 12.70 0.60 1 -8 -8 34.90 1.50 1 -8 -7 471.90 27.00 1 -8 -6 67.60 2.80 1 -8 -5 32.40 1.40 1 -8 -4 70.40 2.90 1 -8 -3 457.70 18.50 1 -8 -2 62.00 2.60 1 -8 -1 140.30 5.70 1 -8 0 787.80 31.80 1 -8 1 48.50 2.90 1 -8 2 70.30 4.10 1 -8 3 45.10 1.90 1 -8 4 109.60 4.50 1 -8 5 278.00 11.30 1 -8 6 75.40 3.10 1 -8 7 169.50 6.90 1 -8 8 54.70 2.30 1 -8 9 281.90 11.40 1 -8 10 492.60 28.20 1 -8 11 696.50 28.10 1 -8 12 19.30 1.10 1 -8 13 26.50 1.40 1 -8 14 47.10 2.30 1 -8 15 22.80 1.10 1 -8 16 118.00 6.90 1 -7 -15 207.90 8.50 1 -7 -13 16.80 0.80 1 -7 -12 160.40 6.50 1 -7 -11 29.50 1.30 1 -7 -10 114.90 4.70 1 -7 -9 130.90 5.40 1 -7 -8 879.30 50.10 1 -7 -7 303.70 12.30 1 -7 -6 23.50 1.10 1 -7 -5 111.20 4.60 1 -7 -4 147.10 6.00 1 -7 -3 382.10 21.80 1 -7 -2 196.60 11.30 1 -7 -1 66.00 2.70 1 -7 0 521.20 21.00 1 -7 1 209.60 8.50 1 -7 2 153.80 6.30 1 -7 3 69.80 2.90 1 -7 4 91.10 3.70 1 -7 5 162.70 9.40 1 -7 6 221.70 12.70 1 -7 7 197.40 8.00 1 -7 8 95.80 3.90 1 -7 9 506.20 20.50 1 -7 10 379.50 15.40 1 -7 11 930.90 53.30 1 -7 12 184.30 7.50 1 -7 13 88.20 3.70 1 -7 14 108.20 4.50 1 -7 15 64.60 2.70 1 -7 16 62.90 2.70 1 -7 17 46.40 2.80 1 -7 18 5.00 0.50 1 -6 -16 41.60 1.80 1 -6 -15 70.20 3.00 1 -6 -14 52.10 2.20 1 -6 -13 20.70 1.00 1 -6 -12 60.00 2.50 1 -6 -11 169.90 6.90 1 -6 -10 71.20 3.00 1 -6 -9 83.80 3.50 1 -6 -8 502.90 20.30 1 -6 -7 52.60 2.20 1 -6 -6 22.00 1.00 1 -6 -5 23.90 1.50 1 -6 -4 262.80 10.60 1 -6 -3 529.20 21.30 1 -6 -2 443.10 17.90 1 -6 -1 69.60 2.90 1 -6 0 156.20 6.30 1 -6 1 1447.00 58.20 1 -6 2 299.40 12.10 1 -6 3 1903.00 76.60 1 -6 4 286.10 11.60 1 -6 5 199.80 8.10 1 -6 6 512.90 20.70 1 -6 8 337.90 13.70 1 -6 9 38.50 1.60 1 -6 10 1752.00 70.60 1 -6 11 56.50 2.40 1 -6 12 202.90 8.30 1 -6 13 35.80 1.60 1 -6 14 7.50 0.50 1 -6 15 89.60 3.70 1 -6 16 28.60 1.30 1 -6 18 49.80 3.10 1 -5 -17 45.60 4.00 1 -5 -16 1.00 0.30 1 -5 -15 4.70 0.40 1 -5 -14 10.80 0.70 1 -5 -13 235.10 9.60 1 -5 -12 106.20 4.40 1 -5 -11 53.70 2.20 1 -5 -10 12.20 0.60 1 -5 -9 259.00 10.50 1 -5 -8 148.40 6.10 1 -5 -7 198.00 8.00 1 -5 -6 24.00 1.50 1 -5 -5 307.40 12.40 1 -5 -4 1144.00 46.00 1 -5 -3 64.00 2.60 1 -5 -2 435.80 17.60 1 -5 -1 446.40 18.00 1 -5 0 1680.00 67.60 1 -5 1 1369.00 55.20 1 -5 2 28.40 1.20 1 -5 3 2039.00 82.00 1 -5 4 515.30 20.80 1 -5 5 515.50 20.80 1 -5 6 135.00 5.50 1 -5 7 239.50 9.70 1 -5 9 285.80 11.60 1 -5 10 171.40 7.00 1 -5 11 61.10 2.60 1 -5 12 309.10 17.80 1 -5 13 72.10 3.00 1 -5 14 152.10 6.20 1 -5 16 19.50 0.90 1 -5 17 3.30 0.30 1 -4 -17 23.30 1.10 1 -4 -16 28.80 1.30 1 -4 -15 33.40 1.50 1 -4 -13 331.80 13.40 1 -4 -12 291.40 11.80 1 -4 -11 199.00 11.50 1 -4 -10 919.30 37.10 1 -4 -9 205.00 8.30 1 -4 -8 190.70 7.70 1 -4 -7 353.20 20.20 1 -4 -6 57.70 2.40 1 -4 -5 490.50 19.80 1 -4 -4 128.60 5.20 1 -4 -3 226.20 9.10 1 -4 -2 780.00 44.40 1 -4 -1 639.10 36.40 1 -4 0 1092.00 62.10 1 -4 1 2152.00 122.40 1 -4 2 2784.00 223.80 1 -4 3 970.10 55.20 1 -4 4 2816.00 113.70 1 -4 5 270.70 10.90 1 -4 6 816.60 33.00 1 -4 7 263.80 10.70 1 -4 8 651.40 26.40 1 -4 9 289.80 11.80 1 -4 10 41.30 1.80 1 -4 11 799.30 32.30 1 -4 12 122.10 5.00 1 -4 13 224.30 9.10 1 -4 14 23.50 1.10 1 -4 15 177.20 7.20 1 -4 16 70.50 2.90 1 -4 17 117.60 4.80 1 -4 18 117.30 6.80 1 -3 -18 96.50 5.70 1 -3 -17 24.50 1.10 1 -3 -16 19.00 0.90 1 -3 -15 32.20 1.40 1 -3 -14 64.00 2.70 1 -3 -13 282.00 11.50 1 -3 -12 791.60 32.00 1 -3 -11 554.80 22.40 1 -3 -10 2200.00 88.60 1 -3 -9 191.80 7.80 1 -3 -8 5.70 0.70 1 -3 -7 176.60 7.20 1 -3 -6 250.90 10.10 1 -3 -5 1184.00 47.80 1 -3 -4 1209.00 48.70 1 -3 -3 63.90 3.70 1 -3 -2 149.40 6.00 1 -3 -1 415.40 16.70 1 -3 0 2647.00 106.60 1 -3 1 473.80 19.10 1 -3 2 1836.00 73.90 1 -3 3 1456.00 58.70 1 -3 4 401.80 22.90 1 -3 5 86.60 3.50 1 -3 6 603.80 24.40 1 -3 7 405.80 16.40 1 -3 8 1070.00 43.20 1 -3 9 314.20 18.00 1 -3 10 562.30 22.70 1 -3 11 348.40 14.10 1 -3 12 36.40 1.60 1 -3 13 567.30 22.90 1 -3 14 7.60 0.50 1 -3 15 86.10 3.60 1 -3 16 8.20 0.50 1 -3 17 23.20 1.10 1 -3 18 108.50 6.30 1 -2 -18 25.50 1.20 1 -2 -16 23.50 1.10 1 -2 -15 205.10 11.80 1 -2 -14 46.20 2.00 1 -2 -13 411.60 16.70 1 -2 -12 217.50 12.50 1 -2 -11 72.60 3.00 1 -2 -10 3.30 0.40 1 -2 -9 159.50 6.50 1 -2 -8 352.80 14.30 1 -2 -7 45.90 2.20 1 -2 -6 1464.00 59.00 1 -2 -5 326.80 13.20 1 -2 -4 782.20 44.50 1 -2 -3 53.70 2.20 1 -2 -2 1923.00 77.40 1 -2 -1 7117.00 286.20 1 -2 0 3336.00 134.40 1 -2 1 817.20 32.90 1 -2 2 2030.00 81.70 1 -2 3 1466.00 59.30 1 -2 4 264.10 10.70 1 -2 5 560.10 31.90 1 -2 6 78.90 3.20 1 -2 7 1022.00 41.30 1 -2 8 253.70 10.30 1 -2 9 29.80 1.80 1 -2 10 35.40 1.50 1 -2 11 31.00 1.30 1 -2 12 1523.00 61.50 1 -2 13 225.30 9.20 1 -2 14 141.60 5.80 1 -2 15 76.20 3.20 1 -2 16 3.60 0.30 1 -2 17 74.50 3.10 1 -2 18 28.90 1.90 1 -1 -18 118.90 4.90 1 -1 -17 61.40 2.60 1 -1 -16 144.90 5.90 1 -1 -15 48.60 2.10 1 -1 -14 16.00 0.80 1 -1 -13 227.00 9.20 1 -1 -12 68.40 2.80 1 -1 -11 12.30 0.60 1 -1 -10 85.00 3.50 1 -1 -8 10.60 0.50 1 -1 -7 1204.00 48.60 1 -1 -6 769.80 31.10 1 -1 -5 219.00 12.50 1 -1 -4 616.30 24.80 1 -1 -3 528.30 21.30 1 -1 -2 404.80 16.30 1 -1 -1 653.40 26.30 1 -1 0 2237.00 90.30 1 -1 1 883.10 35.80 1 -1 2 3691.00 149.20 1 -1 3 1834.00 73.90 1 -1 4 1550.00 62.60 1 -1 5 67.10 3.90 1 -1 6 224.30 9.10 1 -1 7 308.10 12.50 1 -1 8 33.10 1.40 1 -1 9 669.60 38.20 1 -1 10 132.60 5.40 1 -1 11 537.20 21.80 1 -1 12 48.40 2.00 1 -1 13 392.80 15.90 1 -1 14 187.00 7.60 1 -1 15 69.00 2.90 1 -1 16 39.60 1.70 1 -1 17 20.80 1.00 1 -1 18 12.70 1.10 1 0 -18 21.60 1.00 1 0 -17 214.00 8.70 1 0 -16 160.60 6.60 1 0 -15 64.60 2.70 1 0 -14 20.30 0.90 1 0 -13 10.70 0.60 1 0 -12 242.90 9.90 1 0 -11 199.20 8.10 1 0 -10 12.80 0.70 1 0 -9 315.40 18.00 1 0 -8 255.60 10.30 1 0 -7 2485.00 100.10 1 0 -6 418.60 16.90 1 0 -5 1371.00 77.90 1 0 -4 133.10 5.40 1 0 -3 835.50 33.70 1 0 -2 898.00 36.20 1 0 -1 3664.00 170.60 1 0 0 8527.00 343.30 1 0 1 1291.00 52.00 1 0 2 7454.00 299.80 1 0 3 1004.00 40.50 1 0 4 202.10 8.20 1 0 5 358.00 14.50 1 0 6 698.10 28.20 1 0 7 561.90 22.80 1 0 8 11.40 0.60 1 0 9 187.00 10.70 1 0 10 113.90 4.70 1 0 11 399.40 16.20 1 0 12 116.70 4.80 1 0 13 91.80 3.80 1 0 14 33.20 1.40 1 0 16 29.20 1.30 1 0 17 25.50 1.20 1 1 -19 6.60 0.40 1 1 -18 16.60 0.80 1 1 -17 4.20 0.40 1 1 -16 34.60 1.70 1 1 -15 92.50 3.80 1 1 -14 79.40 3.30 1 1 -13 85.70 5.00 1 1 -12 239.60 9.70 1 1 -11 103.40 4.20 1 1 -10 362.60 14.70 1 1 -9 641.10 36.60 1 1 -7 2853.00 115.20 1 1 -6 551.20 22.30 1 1 -5 875.20 49.90 1 1 -4 4085.00 164.90 1 1 -3 5714.00 230.60 1 1 -2 3416.00 137.70 1 1 -1 3451.00 139.10 1 1 0 1846.00 74.30 1 1 1 1257.00 50.60 1 1 2 873.20 35.10 1 1 3 398.70 16.10 1 1 4 1953.00 111.40 1 1 5 454.60 18.30 1 1 6 1820.00 73.30 1 1 7 18.80 0.80 1 1 8 186.20 7.50 1 1 9 501.40 20.20 1 1 10 882.00 35.60 1 1 11 1118.00 45.20 1 1 13 95.20 3.90 1 1 14 80.40 3.30 1 1 15 1.50 0.30 1 1 16 67.10 2.80 1 1 17 38.40 1.70 1 2 -19 16.90 0.80 1 2 -18 8.40 0.50 1 2 -17 78.60 3.30 1 2 -16 3.20 0.30 1 2 -15 10.90 0.60 1 2 -14 45.00 1.90 1 2 -13 48.20 2.90 1 2 -12 22.70 1.00 1 2 -11 83.20 3.40 1 2 -10 492.20 19.90 1 2 -9 587.50 33.60 1 2 -8 501.10 20.20 1 2 -7 644.90 26.00 1 2 -6 2461.00 99.30 1 2 -5 213.50 8.70 1 2 -4 123.10 7.00 1 2 -3 591.00 23.80 1 2 -2 454.40 18.30 1 2 -1 370.80 14.90 1 2 0 779.50 36.50 1 2 1 479.20 19.30 1 2 2 155.60 6.30 1 2 3 907.90 51.70 1 2 4 660.30 26.60 1 2 5 200.50 8.10 1 2 6 452.60 18.20 1 2 7 384.90 15.50 1 2 8 259.50 14.80 1 2 9 460.60 18.60 1 2 10 400.00 16.20 1 2 11 1.00 0.30 1 2 12 232.90 9.50 1 2 13 12.60 0.60 1 2 14 13.40 0.70 1 2 15 45.00 1.90 1 2 16 8.40 0.50 1 2 17 21.00 1.00 1 3 -19 16.20 0.80 1 3 -18 48.50 2.10 1 3 -17 27.00 1.20 1 3 -16 7.80 0.50 1 3 -15 199.30 8.10 1 3 -14 43.00 1.80 1 3 -13 55.30 2.30 1 3 -12 142.90 5.80 1 3 -11 28.50 1.20 1 3 -10 213.90 8.70 1 3 -9 169.00 9.70 1 3 -8 53.60 2.20 1 3 -7 350.30 14.20 1 3 -6 254.30 10.30 1 3 -5 1934.00 77.80 1 3 -4 98.50 4.00 1 3 -3 560.50 31.90 1 3 -2 129.10 5.20 1 3 -1 1366.00 55.00 1 3 0 37.40 1.60 1 3 1 249.50 14.20 1 3 2 89.30 5.10 1 3 3 531.60 21.40 1 3 4 572.70 23.10 1 3 5 1827.00 73.50 1 3 6 513.50 20.70 1 3 7 308.50 17.60 1 3 8 87.40 3.60 1 3 9 5.20 0.30 1 3 10 94.50 3.90 1 3 12 345.10 14.00 1 3 13 55.50 2.30 1 3 14 18.90 0.90 1 3 15 127.10 5.20 1 3 17 31.30 2.00 1 4 -19 82.60 4.90 1 4 -18 30.20 1.40 1 4 -17 8.50 0.50 1 4 -16 9.40 0.60 1 4 -15 1.00 0.40 1 4 -14 99.90 4.10 1 4 -13 114.20 4.70 1 4 -12 7.70 0.50 1 4 -11 57.00 2.40 1 4 -10 173.20 7.10 1 4 -9 104.10 4.30 1 4 -8 260.40 15.00 1 4 -7 177.30 7.20 1 4 -6 431.30 17.40 1 4 -5 123.50 5.00 1 4 -4 269.10 10.90 1 4 -3 447.50 18.00 1 4 -2 508.40 20.50 1 4 -1 97.80 4.00 1 4 0 1043.00 42.00 1 4 1 280.70 11.30 1 4 2 3187.00 128.10 1 4 3 316.30 12.80 1 4 4 2265.00 91.10 1 4 5 175.60 7.10 1 4 6 251.40 14.40 1 4 7 345.40 14.00 1 4 8 57.70 2.40 1 4 9 181.50 7.40 1 4 10 34.80 2.20 1 4 11 549.10 22.20 1 4 12 78.30 3.20 1 4 13 151.20 6.20 1 4 14 72.60 3.00 1 4 15 49.20 2.10 1 4 16 12.40 0.90 1 5 -18 21.70 1.00 1 5 -17 36.10 1.60 1 5 -16 27.10 1.20 1 5 -14 257.80 10.50 1 5 -13 218.30 8.90 1 5 -11 49.50 2.10 1 5 -10 98.30 4.00 1 5 -9 275.50 11.20 1 5 -8 623.00 25.20 1 5 -7 202.70 11.60 1 5 -6 112.60 4.60 1 5 -5 491.00 19.80 1 5 -4 94.30 3.90 1 5 -3 537.30 25.00 1 5 -2 924.60 37.20 1 5 -1 529.40 21.30 1 5 0 483.90 19.50 1 5 1 706.50 28.50 1 5 2 277.70 11.20 1 5 3 362.30 14.60 1 5 4 126.00 5.10 1 5 5 218.80 12.50 1 5 6 50.20 2.10 1 5 7 112.80 4.60 1 5 8 28.60 1.20 1 5 9 96.90 4.00 1 5 10 41.50 1.80 1 5 11 18.00 0.90 1 5 12 132.50 5.40 1 5 13 112.00 4.60 1 5 14 58.20 2.50 1 5 15 20.80 1.00 1 5 16 50.80 3.10 1 6 -18 63.60 2.70 1 6 -16 15.00 0.80 1 6 -15 5.60 0.50 1 6 -14 7.20 0.50 1 6 -13 50.80 2.20 1 6 -12 185.40 7.60 1 6 -11 513.80 29.30 1 6 -10 17.50 0.80 1 6 -9 242.60 9.90 1 6 -8 129.70 5.30 1 6 -7 312.50 12.70 1 6 -5 217.90 8.80 1 6 -4 34.40 1.50 1 6 -3 435.40 17.60 1 6 -2 264.90 10.70 1 6 -1 222.50 9.00 1 6 0 35.00 1.50 1 6 1 579.00 23.30 1 6 2 181.10 7.40 1 6 4 165.40 6.70 1 6 5 184.80 7.50 1 6 6 79.60 3.30 1 6 7 67.80 2.80 1 6 8 216.20 12.40 1 6 9 232.80 9.50 1 6 10 51.60 2.20 1 6 11 7.20 0.50 1 6 12 30.40 1.30 1 6 13 48.40 2.10 1 6 15 50.30 2.20 1 7 -18 60.40 2.60 1 7 -17 32.50 1.50 1 7 -16 98.40 4.10 1 7 -15 7.10 0.60 1 7 -13 32.50 1.50 1 7 -12 326.60 13.30 1 7 -11 135.60 5.60 1 7 -10 382.90 15.50 1 7 -9 727.90 29.40 1 7 -8 498.70 20.10 1 7 -7 250.80 10.20 1 7 -6 16.10 0.80 1 7 -5 122.10 5.00 1 7 -4 276.60 12.90 1 7 -3 513.10 29.30 1 7 -2 35.20 2.20 1 7 -1 545.80 31.20 1 7 0 34.50 2.10 1 7 1 477.80 19.30 1 7 2 217.70 8.80 1 7 3 16.90 0.80 1 7 4 153.60 6.30 1 7 5 50.80 2.10 1 7 6 26.40 1.30 1 7 7 63.40 3.70 1 7 8 24.20 1.10 1 7 9 6.30 0.40 1 7 10 20.70 1.00 1 7 11 55.90 2.40 1 7 12 7.10 0.50 1 7 14 133.00 5.50 1 8 -17 130.10 5.40 1 8 -15 100.00 4.80 1 8 -14 34.00 1.70 1 8 -13 39.50 2.40 1 8 -12 329.80 13.40 1 8 -11 70.20 3.00 1 8 -10 107.00 4.40 1 8 -9 242.00 19.60 1 8 -8 305.40 12.40 1 8 -7 22.80 1.00 1 8 -6 15.00 0.70 1 8 -5 16.60 0.80 1 8 -4 57.70 2.40 1 8 -3 82.30 3.40 1 8 -2 201.30 8.20 1 8 -1 108.80 4.50 1 8 0 576.60 23.30 1 8 1 622.90 25.10 1 8 2 75.40 3.10 1 8 3 321.30 13.00 1 8 4 264.80 10.70 1 8 5 97.70 5.70 1 8 6 23.20 1.10 1 8 7 33.70 1.50 1 8 8 114.10 4.70 1 8 9 121.40 5.00 1 8 10 63.60 2.70 1 8 11 86.60 3.60 1 8 13 144.80 5.90 1 9 -16 24.40 1.20 1 9 -15 48.50 2.90 1 9 -14 27.30 1.30 1 9 -13 5.60 0.40 1 9 -12 56.50 3.40 1 9 -11 8.70 0.50 1 9 -10 68.80 2.90 1 9 -9 201.50 8.20 1 9 -8 5.50 0.40 1 9 -6 494.00 20.00 1 9 -5 149.80 6.10 1 9 -4 123.00 5.10 1 9 -3 9.60 0.50 1 9 -2 1.30 0.20 1 9 -1 49.40 2.10 1 9 0 -0.10 0.20 1 9 1 353.40 14.30 1 9 2 84.00 3.50 1 9 3 41.50 2.50 1 9 4 85.10 3.50 1 9 5 72.30 3.00 1 9 6 28.00 1.30 1 9 7 5.20 0.40 1 9 8 39.40 2.40 1 9 9 133.80 5.50 1 9 10 9.10 0.50 1 9 11 5.50 0.40 1 9 12 13.80 0.70 1 10 -16 118.20 5.70 1 10 -15 30.80 1.40 1 10 -14 49.60 3.00 1 10 -13 105.90 4.40 1 10 -12 62.90 2.70 1 10 -11 124.60 7.30 1 10 -10 51.60 2.20 1 10 -9 10.30 0.60 1 10 -8 168.00 6.90 1 10 -7 114.20 4.70 1 10 -6 190.10 7.80 1 10 -5 121.00 5.00 1 10 -4 100.40 4.20 1 10 -3 45.30 2.00 1 10 -2 29.40 1.30 1 10 -1 46.50 2.00 1 10 0 113.10 4.70 1 10 1 288.00 11.70 1 10 2 293.30 11.90 1 10 3 246.80 10.00 1 10 4 161.30 6.60 1 10 5 8.50 0.50 1 10 7 28.70 1.30 1 10 8 3.60 0.40 1 10 9 37.80 1.70 1 10 10 7.00 0.50 1 10 11 47.50 2.00 1 11 -15 46.80 2.90 1 11 -14 12.30 0.80 1 11 -13 60.20 3.70 1 11 -12 59.70 2.50 1 11 -11 16.10 0.80 1 11 -10 125.60 5.20 1 11 -9 156.70 9.10 1 11 -8 264.40 10.80 1 11 -7 501.50 20.30 1 11 -6 92.00 3.80 1 11 -5 112.90 4.70 1 11 -4 72.20 3.00 1 11 -3 31.20 1.40 1 11 -2 42.70 1.80 1 11 -1 129.10 5.30 1 11 0 59.50 2.50 1 11 1 30.90 1.40 1 11 2 3.00 0.30 1 11 3 200.70 9.50 1 11 4 17.30 1.00 1 11 5 37.00 1.60 1 11 6 12.70 0.70 1 11 7 0.80 0.30 1 11 8 21.10 1.00 1 11 9 37.10 1.60 1 12 -13 26.40 1.20 1 12 -12 35.20 1.60 1 12 -10 28.80 1.30 1 12 -9 52.00 2.20 1 12 -8 17.00 0.90 1 12 -7 47.70 2.10 1 12 -6 48.20 2.10 1 12 -5 16.00 1.20 1 12 -1 9.90 0.80 1 12 0 12.80 0.70 1 12 1 15.80 0.80 1 12 2 122.50 5.00 1 12 3 29.70 1.30 1 12 4 20.30 1.00 1 12 5 141.50 5.80 1 12 6 23.50 1.10 1 12 7 2.20 0.30 1 12 8 56.20 2.80 1 13 -12 28.00 1.90 1 13 -11 1.20 0.30 1 13 -10 116.50 4.80 1 13 -9 5.40 0.50 1 13 -8 48.00 2.10 1 13 -7 20.00 1.00 1 13 -6 4.00 0.40 1 13 -5 14.10 0.70 1 13 -4 48.50 2.10 1 13 -3 0.50 0.30 1 13 -2 10.70 0.60 1 13 -1 122.90 5.10 1 13 0 42.60 1.90 1 13 1 4.80 0.40 1 13 2 2.30 0.30 1 13 3 65.00 2.70 1 13 4 115.60 4.80 1 13 5 29.80 1.40 1 14 -9 10.80 0.60 1 14 -8 102.30 4.30 1 14 -7 33.10 1.50 1 14 -6 24.10 1.10 1 14 -5 123.30 5.10 1 14 -4 43.70 1.90 1 14 -3 13.20 0.70 1 14 -2 10.70 0.60 1 14 -1 1.80 0.30 1 14 0 26.60 1.20 1 14 1 12.40 0.70 1 14 2 1.60 0.30 2 -15 -3 2.00 0.40 2 -15 -2 17.30 0.90 2 -15 -1 21.50 1.00 2 -15 0 31.20 1.40 2 -15 1 1.30 0.30 2 -15 2 22.00 1.20 2 -15 3 59.50 2.50 2 -15 4 70.40 3.00 2 -15 5 9.50 0.60 2 -15 6 3.40 0.40 2 -15 7 19.50 1.00 2 -15 8 6.10 0.50 2 -14 -6 39.20 1.70 2 -14 -5 21.20 1.00 2 -14 -4 90.10 3.80 2 -14 -3 174.40 7.10 2 -14 -2 28.00 1.30 2 -14 -1 21.50 1.00 2 -14 0 6.40 0.40 2 -14 1 249.00 10.10 2 -14 2 40.40 1.80 2 -14 3 230.50 9.40 2 -14 4 83.90 3.50 2 -14 5 55.50 2.40 2 -14 6 53.00 2.30 2 -14 7 9.30 0.70 2 -14 9 15.00 0.80 2 -14 10 133.40 5.50 2 -14 11 34.10 1.50 2 -13 -8 9.70 0.60 2 -13 -7 53.20 2.30 2 -13 -6 23.10 1.10 2 -13 -5 44.50 1.90 2 -13 -4 16.10 0.80 2 -13 -3 47.20 2.00 2 -13 -2 33.00 1.50 2 -13 -1 58.10 2.50 2 -13 0 208.70 8.50 2 -13 1 73.50 6.20 2 -13 4 67.00 5.70 2 -13 5 7.20 0.50 2 -13 6 26.80 1.20 2 -13 7 10.10 0.60 2 -13 8 20.90 1.00 2 -13 9 39.40 1.70 2 -13 10 34.90 1.50 2 -13 11 80.50 3.40 2 -13 12 155.30 6.40 2 -12 -10 36.40 2.30 2 -12 -9 125.30 5.20 2 -12 -8 15.60 1.60 2 -12 -7 33.10 1.50 2 -12 -6 0.50 0.30 2 -12 -5 29.80 1.30 2 -12 -4 121.80 7.10 2 -12 -3 26.30 1.20 2 -12 -2 18.80 0.90 2 -12 -1 60.10 2.50 2 -12 0 3.00 0.30 2 -12 1 16.70 0.80 2 -12 2 0.80 0.20 2 -12 3 1.90 0.30 2 -12 4 18.70 0.90 2 -12 5 80.80 3.40 2 -12 6 74.30 3.10 2 -12 7 29.60 1.30 2 -12 8 35.80 2.20 2 -12 9 24.70 1.10 2 -12 10 72.10 3.00 2 -12 11 45.30 2.00 2 -12 12 39.20 1.70 2 -12 13 7.40 0.60 2 -12 14 42.00 1.90 2 -11 -11 1.50 0.30 2 -11 -10 5.50 0.40 2 -11 -9 65.40 2.70 2 -11 -8 33.30 1.50 2 -11 -7 40.60 1.80 2 -11 -6 17.70 1.30 2 -11 -5 9.60 0.50 2 -11 -4 11.80 0.60 2 -11 -3 41.00 1.80 2 -11 -2 5.10 0.40 2 -11 -1 115.20 4.70 2 -11 0 280.00 11.40 2 -11 1 412.40 19.30 2 -11 2 44.90 2.70 2 -11 3 39.40 2.00 2 -11 4 6.90 0.50 2 -11 5 49.20 2.10 2 -11 6 71.30 3.00 2 -11 7 43.70 1.90 2 -11 8 7.90 0.50 2 -11 9 25.90 1.20 2 -11 10 32.70 2.00 2 -11 11 30.40 1.40 2 -11 12 3.30 0.40 2 -11 13 316.50 12.80 2 -11 14 58.00 2.50 2 -11 15 132.80 5.50 2 -10 -12 54.60 2.30 2 -10 -10 68.40 2.90 2 -10 -9 147.30 6.00 2 -10 -8 6.00 1.10 2 -10 -7 8.40 0.60 2 -10 -6 40.70 1.80 2 -10 -5 194.60 7.90 2 -10 -4 110.60 4.60 2 -10 -3 151.10 8.80 2 -10 -2 112.70 4.60 2 -10 -1 702.70 28.30 2 -10 0 158.70 6.50 2 -10 1 5.60 0.40 2 -10 2 135.30 5.50 2 -10 3 124.00 5.10 2 -10 4 80.90 3.40 2 -10 5 207.70 8.50 2 -10 6 54.90 2.30 2 -10 7 2.10 0.50 2 -10 8 12.80 0.70 2 -10 9 71.60 3.00 2 -10 10 23.20 1.10 2 -10 11 20.40 1.00 2 -10 12 123.60 5.10 2 -10 13 35.50 1.60 2 -10 14 26.70 1.20 2 -10 15 31.20 1.40 2 -10 16 55.00 2.40 2 -9 -13 0.80 0.30 2 -9 -12 79.00 3.30 2 -9 -11 307.60 12.50 2 -9 -10 46.30 2.00 2 -9 -9 30.40 1.30 2 -9 -8 81.80 3.40 2 -9 -7 42.40 1.80 2 -9 -6 121.70 5.00 2 -9 -5 232.30 9.40 2 -9 -4 471.10 19.00 2 -9 -3 117.70 4.80 2 -9 -2 71.50 3.00 2 -9 -1 341.20 13.80 2 -9 0 215.40 8.80 2 -9 1 116.60 4.80 2 -9 2 56.30 2.40 2 -9 3 96.20 4.00 2 -9 4 65.20 2.70 2 -9 5 227.40 9.20 2 -9 6 44.00 1.90 2 -9 7 169.90 6.90 2 -9 8 8.40 0.50 2 -9 9 222.90 12.90 2 -9 10 10.90 0.70 2 -9 11 63.00 2.70 2 -9 12 31.60 1.40 2 -9 13 13.20 0.70 2 -9 14 57.00 2.40 2 -9 15 29.20 1.30 2 -9 16 17.40 1.00 2 -8 -14 2.60 0.50 2 -8 -13 32.20 1.40 2 -8 -12 74.30 3.10 2 -8 -11 8.50 0.60 2 -8 -10 181.50 7.40 2 -8 -9 103.80 4.30 2 -8 -8 152.90 6.20 2 -8 -7 116.00 6.80 2 -8 -6 5.90 0.40 2 -8 -5 87.00 3.60 2 -8 -4 122.50 5.00 2 -8 -3 83.40 3.40 2 -8 -2 380.70 15.40 2 -8 -1 276.00 15.80 2 -8 1 403.30 23.00 2 -8 2 25.30 1.60 2 -8 3 7.40 0.60 2 -8 4 210.50 12.10 2 -8 5 68.50 2.90 2 -8 6 15.50 0.70 2 -8 7 109.80 4.50 2 -8 8 149.70 6.10 2 -8 9 16.80 0.80 2 -8 11 288.60 11.70 2 -8 12 11.50 0.70 2 -8 13 69.80 3.40 2 -8 14 5.10 0.70 2 -8 15 8.20 0.70 2 -8 17 66.00 2.80 2 -7 -15 10.20 0.60 2 -7 -14 59.50 2.50 2 -7 -13 53.00 2.30 2 -7 -12 46.10 2.70 2 -7 -11 74.10 3.10 2 -7 -10 155.40 6.30 2 -7 -9 85.40 3.50 2 -7 -8 461.00 18.60 2 -7 -7 209.00 8.50 2 -7 -6 79.80 3.30 2 -7 -5 243.40 9.90 2 -7 -4 112.30 6.50 2 -7 -3 57.40 3.40 2 -7 -2 162.50 6.60 2 -7 -1 43.30 1.80 2 -7 0 770.30 31.00 2 -7 1 188.90 7.70 2 -7 2 146.10 5.90 2 -7 3 1055.00 42.50 2 -7 4 51.90 2.20 2 -7 5 12.20 0.60 2 -7 6 34.50 2.10 2 -7 7 84.20 3.50 2 -7 8 52.90 2.20 2 -7 9 296.00 12.00 2 -7 10 351.90 14.30 2 -7 11 425.50 24.50 2 -7 12 22.80 1.10 2 -7 13 10.20 0.60 2 -7 14 86.90 7.20 2 -7 15 42.60 1.90 2 -7 16 23.00 1.10 2 -7 17 1.80 0.40 2 -6 -16 35.70 1.60 2 -6 -14 50.50 2.20 2 -6 -13 19.60 0.90 2 -6 -12 126.20 5.20 2 -6 -11 87.60 3.60 2 -6 -10 192.90 7.80 2 -6 -9 260.50 10.60 2 -6 -8 86.30 3.60 2 -6 -7 78.00 3.20 2 -6 -6 165.40 6.70 2 -6 -5 21.00 1.30 2 -6 -4 94.70 3.90 2 -6 -3 62.50 2.60 2 -6 -2 187.60 7.60 2 -6 -1 901.40 36.30 2 -6 0 702.20 28.30 2 -6 1 1075.00 43.20 2 -6 2 0.90 0.20 2 -6 3 935.30 37.60 2 -6 4 275.50 11.10 2 -6 5 251.30 10.20 2 -6 6 284.20 11.50 2 -6 7 187.30 10.80 2 -6 8 105.90 4.40 2 -6 9 60.80 2.50 2 -6 10 231.00 9.40 2 -6 11 84.90 3.50 2 -6 12 71.00 3.00 2 -6 13 52.90 2.20 2 -6 14 9.50 0.60 2 -6 15 51.50 2.20 2 -6 16 14.40 0.80 2 -6 17 120.90 5.00 2 -6 18 72.20 3.00 2 -5 -17 11.00 1.00 2 -5 -16 19.30 1.10 2 -5 -15 25.10 1.20 2 -5 -14 0.90 0.30 2 -5 -13 57.80 2.40 2 -5 -12 239.30 9.70 2 -5 -11 51.80 2.20 2 -5 -10 168.10 6.80 2 -5 -9 71.30 2.90 2 -5 -8 125.10 5.10 2 -5 -7 8.60 0.50 2 -5 -6 148.30 6.00 2 -5 -5 103.60 4.20 2 -5 -4 164.70 6.70 2 -5 -3 46.70 1.90 2 -5 -2 171.20 6.90 2 -5 -1 816.00 32.80 2 -5 0 729.00 29.40 2 -5 1 256.70 14.70 2 -5 2 691.00 27.90 2 -5 3 11.80 0.50 2 -5 4 298.90 12.10 2 -5 5 521.60 21.00 2 -5 6 92.30 3.80 2 -5 7 95.20 3.90 2 -5 9 201.90 8.20 2 -5 10 469.40 19.00 2 -5 11 318.30 12.90 2 -5 12 15.10 1.60 2 -5 13 256.80 10.40 2 -5 14 41.10 1.80 2 -5 15 64.10 2.70 2 -5 16 23.30 1.10 2 -5 18 73.50 3.10 2 -4 -17 9.80 0.70 2 -4 -16 9.40 0.60 2 -4 -15 1.50 0.30 2 -4 -14 1.40 0.70 2 -4 -13 39.50 1.70 2 -4 -12 156.00 6.40 2 -4 -11 204.20 9.60 2 -4 -10 235.90 9.60 2 -4 -9 208.90 8.50 2 -4 -8 2.90 0.30 2 -4 -7 260.20 10.50 2 -4 -6 153.80 6.30 2 -4 -5 9.80 0.50 2 -4 -4 113.30 4.60 2 -4 -3 276.50 11.20 2 -4 -2 714.30 40.70 2 -4 -1 993.30 40.00 2 -4 0 851.10 34.30 2 -4 1 76.20 3.60 2 -4 2 21.70 0.90 2 -4 3 589.40 33.60 2 -4 4 1280.00 51.60 2 -4 5 439.60 17.80 2 -4 6 38.60 1.60 2 -4 7 27.30 1.20 2 -4 8 0.30 0.20 2 -4 9 241.40 9.80 2 -4 10 7.60 0.50 2 -4 11 446.80 18.10 2 -4 12 175.90 10.10 2 -4 13 7.70 0.50 2 -4 14 72.40 3.00 2 -4 16 20.40 1.00 2 -4 17 27.70 1.80 2 -4 18 68.00 2.90 2 -3 -17 56.80 2.40 2 -3 -16 35.50 1.60 2 -3 -15 66.20 2.80 2 -3 -14 21.80 1.00 2 -3 -13 215.70 8.80 2 -3 -12 134.70 7.80 2 -3 -11 37.60 1.60 2 -3 -10 37.10 1.60 2 -3 -9 195.20 7.90 2 -3 -8 317.00 18.10 2 -3 -7 290.60 11.80 2 -3 -6 1113.00 44.80 2 -3 -5 83.10 3.40 2 -3 -4 72.20 4.20 2 -3 -3 560.00 22.50 2 -3 -2 966.10 38.90 2 -3 -1 342.70 13.80 2 -3 0 73.80 3.00 2 -3 1 1243.00 50.00 2 -3 2 1098.00 44.20 2 -3 3 2009.00 81.20 2 -3 4 238.00 13.60 2 -3 5 248.20 10.00 2 -3 6 63.00 2.60 2 -3 7 29.60 1.20 2 -3 8 14.60 0.70 2 -3 9 30.60 1.90 2 -3 10 63.00 2.60 2 -3 11 355.30 14.30 2 -3 12 40.80 1.70 2 -3 13 693.80 28.10 2 -3 14 85.00 3.50 2 -3 16 64.70 2.70 2 -3 17 69.40 2.90 2 -3 18 14.60 0.80 2 -2 -18 88.60 3.70 2 -2 -16 35.50 1.60 2 -2 -14 43.50 1.90 2 -2 -13 179.00 7.30 2 -2 -12 466.00 18.90 2 -2 -11 339.10 13.70 2 -2 -10 642.30 25.90 2 -2 -9 260.40 14.90 2 -2 -8 834.60 33.70 2 -2 -7 71.30 2.90 2 -2 -6 348.50 14.10 2 -2 -5 236.80 9.60 2 -2 -4 283.30 11.40 2 -2 -3 880.60 35.50 2 -2 -2 669.10 27.00 2 -2 -1 1491.00 60.00 2 -2 0 521.90 21.00 2 -2 1 216.60 8.80 2 -2 2 764.90 35.60 2 -2 3 134.20 5.50 2 -2 4 72.10 2.90 2 -2 5 29.60 1.70 2 -2 6 135.20 5.50 2 -2 7 225.00 9.10 2 -2 8 214.50 8.70 2 -2 9 289.20 16.60 2 -2 10 128.40 5.20 2 -2 11 34.80 1.70 2 -2 12 362.90 14.80 2 -2 13 27.40 1.20 2 -2 14 51.50 2.20 2 -2 16 36.80 1.60 2 -2 18 5.30 0.50 2 -1 -18 21.00 1.00 2 -1 -17 3.40 0.40 2 -1 -16 7.30 0.50 2 -1 -15 13.80 0.70 2 -1 -14 101.80 4.20 2 -1 -13 47.10 2.00 2 -1 -12 24.10 1.10 2 -1 -11 44.70 1.90 2 -1 -10 15.70 0.70 2 -1 -9 82.20 4.70 2 -1 -8 723.90 29.30 2 -1 -7 474.70 19.20 2 -1 -6 54.40 2.20 2 -1 -5 709.70 40.40 2 -1 -4 779.10 31.50 2 -1 -3 337.20 13.60 2 -1 -2 1613.00 65.20 2 -1 1 605.70 24.40 2 -1 2 2027.00 81.50 2 -1 3 79.60 3.20 2 -1 4 302.70 12.30 2 -1 5 50.00 2.90 2 -1 6 897.80 36.40 2 -1 7 135.30 5.50 2 -1 8 70.90 2.90 2 -1 9 134.10 7.70 2 -1 10 40.00 1.70 2 -1 11 90.30 3.70 2 -1 12 70.00 4.10 2 -1 13 13.40 0.70 2 -1 14 7.00 0.50 2 -1 15 7.30 0.70 2 -1 16 34.50 1.50 2 -1 17 205.10 9.70 2 -1 18 3.20 0.40 2 0 -18 117.70 4.90 2 0 -17 60.70 2.60 2 0 -16 18.00 0.90 2 0 -15 62.40 2.60 2 0 -14 32.10 1.40 2 0 -13 115.10 4.70 2 0 -12 109.60 4.50 2 0 -11 59.70 2.50 2 0 -10 426.70 17.30 2 0 -9 60.40 3.50 2 0 -8 432.50 17.60 2 0 -7 311.40 12.60 2 0 -6 230.00 9.30 2 0 -4 153.50 6.20 2 0 -3 789.00 31.80 2 0 -2 1224.00 49.40 2 0 -1 1217.00 49.20 2 0 0 761.30 30.70 2 0 1 491.30 19.80 2 0 2 6.10 0.40 2 0 3 583.30 23.50 2 0 4 459.40 26.20 2 0 5 914.20 36.90 2 0 6 434.40 17.50 2 0 7 104.10 4.20 2 0 8 237.30 9.60 2 0 9 122.00 5.00 2 0 10 18.30 0.80 2 0 11 179.10 7.30 2 0 13 154.10 6.30 2 0 14 37.30 1.60 2 0 15 253.80 10.30 2 0 16 20.00 1.00 2 0 17 32.30 1.40 2 1 -18 24.70 1.10 2 1 -17 8.10 0.50 2 1 -16 23.30 1.10 2 1 -15 75.00 3.10 2 1 -14 46.50 2.00 2 1 -13 123.10 7.10 2 1 -12 233.40 9.50 2 1 -11 79.00 3.20 2 1 -10 376.40 15.20 2 1 -9 191.50 11.00 2 1 -8 522.70 21.10 2 1 -7 599.70 24.20 2 1 -6 362.10 14.60 2 1 -5 85.40 4.90 2 1 -4 145.00 5.90 2 1 -3 546.50 22.10 2 1 -2 687.30 27.70 2 1 -1 714.60 28.80 2 1 0 1858.00 74.80 2 1 1 763.70 30.80 2 1 2 1152.00 46.30 2 1 3 341.00 13.80 2 1 4 79.50 4.60 2 1 5 101.20 4.10 2 1 6 20.70 0.90 2 1 7 2.40 0.20 2 1 8 203.70 11.70 2 1 9 42.90 1.80 2 1 10 104.50 4.30 2 1 11 303.00 12.30 2 1 12 188.90 7.70 2 1 13 106.00 4.40 2 1 14 19.20 0.90 2 1 15 36.60 1.60 2 1 16 58.30 2.50 2 1 17 2.50 0.40 2 2 -19 27.40 1.80 2 2 -18 55.30 2.40 2 2 -17 18.40 0.90 2 2 -16 26.10 1.20 2 2 -15 110.00 4.50 2 2 -14 39.70 1.70 2 2 -13 49.50 2.10 2 2 -12 110.60 4.50 2 2 -11 250.20 10.10 2 2 -10 236.60 9.60 2 2 -9 685.60 39.20 2 2 -8 338.90 13.80 2 2 -7 618.30 25.00 2 2 -6 1225.00 49.40 2 2 -5 48.70 2.00 2 2 -4 310.30 17.70 2 2 -3 284.70 11.50 2 2 -2 178.00 7.20 2 2 -1 272.20 11.00 2 2 0 25.50 1.10 2 2 1 718.90 28.90 2 2 2 53.60 3.10 2 2 3 204.50 11.70 2 2 4 338.90 13.70 2 2 5 698.40 28.20 2 2 6 198.80 8.10 2 2 7 52.00 2.20 2 2 8 2.10 0.30 2 2 9 18.70 0.90 2 2 10 107.50 4.40 2 2 11 46.30 2.80 2 2 12 346.30 14.00 2 2 13 44.10 1.90 2 2 14 13.20 0.70 2 2 15 68.80 2.90 2 2 16 18.80 1.10 2 2 17 3.70 0.60 2 3 -18 35.20 1.50 2 3 -17 63.40 2.70 2 3 -16 56.20 2.40 2 3 -15 33.30 1.50 2 3 -14 60.00 2.50 2 3 -13 132.40 5.40 2 3 -12 62.90 2.60 2 3 -11 182.90 7.50 2 3 -10 163.50 6.70 2 3 -9 169.00 9.80 2 3 -8 190.90 7.80 2 3 -7 493.50 19.90 2 3 -6 398.80 16.10 2 3 -5 130.70 5.30 2 3 -4 99.00 4.00 2 3 -3 10.30 0.70 2 3 -2 152.40 8.80 2 3 -1 94.30 5.40 2 3 1 211.60 12.10 2 3 2 194.50 7.90 2 3 3 12.10 0.60 2 3 4 698.90 28.10 2 3 5 155.50 6.30 2 3 6 272.70 11.00 2 3 7 1.80 0.20 2 3 8 134.10 5.50 2 3 9 26.40 1.20 2 3 10 152.60 6.20 2 3 11 310.90 12.60 2 3 12 76.00 3.20 2 3 13 9.50 0.60 2 3 14 53.70 2.30 2 3 15 80.50 3.40 2 3 16 30.80 1.40 2 4 -18 13.30 0.70 2 4 -17 12.70 0.80 2 4 -16 4.60 0.40 2 4 -15 148.80 8.60 2 4 -14 43.80 1.90 2 4 -13 50.10 2.10 2 4 -12 268.20 15.40 2 4 -11 73.00 3.00 2 4 -10 45.60 1.90 2 4 -9 314.20 12.70 2 4 -7 121.10 5.00 2 4 -6 203.60 8.30 2 4 -5 82.10 3.40 2 4 -4 283.70 11.50 2 4 -3 141.20 5.70 2 4 -2 125.20 5.10 2 4 -1 414.90 16.70 2 4 0 344.40 13.90 2 4 1 530.60 21.40 2 4 2 242.70 9.80 2 4 3 115.70 4.70 2 4 4 393.30 15.90 2 4 5 206.80 8.40 2 4 6 142.00 5.80 2 4 7 78.10 3.20 2 4 8 35.50 1.50 2 4 9 94.00 3.90 2 4 10 64.80 2.70 2 4 11 128.10 5.20 2 4 12 17.40 0.90 2 4 13 19.90 1.00 2 4 14 10.60 0.60 2 4 15 19.40 1.00 2 4 16 16.80 0.90 2 5 -18 85.80 3.60 2 5 -16 31.80 1.40 2 5 -15 25.20 1.40 2 5 -14 7.40 0.60 2 5 -13 16.10 0.80 2 5 -12 0.60 0.30 2 5 -11 399.50 16.10 2 5 -10 117.90 4.80 2 5 -9 471.10 19.10 2 5 -8 240.40 9.80 2 5 -7 145.30 8.40 2 5 -6 108.20 4.40 2 5 -5 56.80 2.40 2 5 -4 116.10 4.70 2 5 -3 53.80 2.20 2 5 -2 18.70 0.80 2 5 -1 36.10 1.50 2 5 0 333.40 13.50 2 5 1 122.00 5.00 2 5 2 298.50 12.10 2 5 3 299.90 12.10 2 5 4 209.70 17.00 2 5 5 224.30 9.10 2 5 6 310.00 12.50 2 5 7 112.10 4.60 2 5 8 14.50 0.70 2 5 9 112.30 4.60 2 5 10 202.60 8.20 2 5 11 79.40 3.30 2 5 12 25.80 1.20 2 5 13 59.60 2.50 2 5 15 26.20 1.20 2 6 -18 198.70 8.10 2 6 -17 6.30 0.50 2 6 -16 39.50 1.70 2 6 -15 24.70 1.20 2 6 -14 29.10 1.30 2 6 -13 0.90 0.30 2 6 -12 304.10 12.40 2 6 -11 107.10 6.30 2 6 -10 311.20 12.60 2 6 -9 297.50 12.10 2 6 -8 156.50 6.40 2 6 -7 391.20 15.80 2 6 -6 5.50 0.40 2 6 -5 43.30 3.70 2 6 -4 207.10 11.90 2 6 -3 44.40 1.90 2 6 -2 20.70 0.90 2 6 -1 60.30 2.50 2 6 0 52.70 2.20 2 6 1 52.40 3.10 2 6 2 27.50 1.70 2 6 3 269.10 10.90 2 6 4 591.10 23.80 2 6 5 222.50 9.00 2 6 6 41.80 1.80 2 6 7 16.70 0.80 2 6 8 4.60 0.30 2 6 9 12.80 0.60 2 6 10 110.40 4.50 2 6 11 28.50 1.30 2 6 12 177.50 7.20 2 6 13 52.30 2.20 2 6 14 57.30 2.40 2 7 -17 85.70 3.60 2 7 -16 7.00 0.90 2 7 -15 24.80 1.30 2 7 -14 1.00 0.30 2 7 -13 5.40 0.40 2 7 -12 58.90 2.50 2 7 -11 13.30 0.70 2 7 -10 204.60 11.80 2 7 -9 193.70 7.90 2 7 -8 331.50 13.40 2 7 -7 260.00 10.60 2 7 -6 22.70 1.00 2 7 -5 209.60 8.50 2 7 -4 98.70 4.10 2 7 -3 76.60 3.20 2 7 -2 39.70 1.70 2 7 -1 91.30 3.80 2 7 0 410.70 16.60 2 7 1 183.40 7.50 2 7 2 166.70 6.80 2 7 3 60.90 2.50 2 7 4 67.80 2.80 2 7 5 219.40 8.90 2 7 6 173.40 14.10 2 7 7 13.20 0.70 2 7 8 42.80 1.80 2 7 9 22.70 1.00 2 7 10 46.10 2.00 2 7 11 3.90 0.40 2 7 12 26.70 1.20 2 7 13 61.70 2.60 2 8 -17 165.90 6.80 2 8 -16 183.20 7.50 2 8 -15 14.00 0.80 2 8 -14 40.00 1.80 2 8 -13 54.50 2.30 2 8 -12 28.10 1.30 2 8 -11 185.60 7.60 2 8 -10 25.00 1.10 2 8 -9 92.20 3.80 2 8 -8 70.60 4.10 2 8 -7 82.80 3.50 2 8 -6 20.50 1.00 2 8 -5 266.30 10.80 2 8 -4 30.70 1.40 2 8 -3 75.30 3.10 2 8 -2 78.60 3.30 2 8 -1 220.70 9.00 2 8 0 75.50 3.10 2 8 1 261.50 10.60 2 8 2 34.10 1.50 2 8 3 352.20 14.20 2 8 4 46.70 2.80 2 8 5 0.50 0.20 2 8 6 22.00 1.00 2 8 7 14.50 0.70 2 8 8 47.20 2.00 2 8 9 1.30 0.30 2 8 10 5.10 0.40 2 8 11 0.70 0.70 2 8 12 7.30 0.50 2 9 -16 7.50 0.60 2 9 -15 33.40 1.50 2 9 -14 34.20 1.50 2 9 -13 40.20 1.80 2 9 -12 42.60 1.90 2 9 -11 33.60 1.50 2 9 -10 2.60 0.30 2 9 -9 68.60 2.90 2 9 -8 51.10 2.20 2 9 -7 200.40 8.20 2 9 -6 175.60 10.10 2 9 -5 27.80 2.50 2 9 -4 21.00 1.40 2 9 -3 49.80 2.10 2 9 -2 201.20 8.20 2 9 -1 199.80 8.10 2 9 0 119.00 6.90 2 9 1 194.20 11.20 2 9 2 27.80 1.20 2 9 3 48.10 2.10 2 9 4 17.50 0.80 2 9 5 98.90 4.10 2 9 6 7.60 0.50 2 9 7 2.70 0.30 2 9 8 20.90 1.00 2 9 9 1.90 0.30 2 9 10 31.00 1.40 2 9 11 35.80 1.60 2 10 -15 36.20 1.60 2 10 -14 61.80 2.60 2 10 -13 26.20 1.20 2 10 -12 20.40 1.10 2 10 -11 5.60 0.50 2 10 -10 7.70 0.60 2 10 -9 41.00 1.80 2 10 -8 36.60 1.60 2 10 -7 73.80 3.10 2 10 -6 88.50 3.70 2 10 -5 156.70 6.40 2 10 -4 10.80 0.60 2 10 -3 82.20 3.40 2 10 -2 38.00 1.70 2 10 -1 86.20 3.60 2 10 0 32.00 1.40 2 10 1 78.00 3.30 2 10 2 33.40 1.50 2 10 3 4.90 0.40 2 10 4 35.20 1.50 2 10 5 90.00 3.70 2 10 6 37.90 1.70 2 10 7 69.50 2.90 2 10 8 17.70 1.00 2 10 9 9.40 0.60 2 10 10 23.00 1.10 2 11 -14 19.90 1.00 2 11 -13 7.10 0.50 2 11 -11 43.90 1.90 2 11 -10 9.40 0.60 2 11 -9 101.60 4.20 2 11 -8 16.10 0.90 2 11 -6 370.40 15.00 2 11 -5 200.80 8.20 2 11 -4 94.90 3.90 2 11 -3 0.90 0.30 2 11 -2 77.80 3.30 2 11 -1 148.20 6.10 2 11 0 34.60 1.50 2 11 2 0.30 0.20 2 11 3 10.40 0.60 2 11 4 10.80 0.60 2 11 5 25.90 1.20 2 11 6 91.90 3.80 2 11 7 82.50 3.50 2 11 8 2.00 0.40 2 12 -12 18.30 0.90 2 12 -11 14.70 0.80 2 12 -10 126.30 6.00 2 12 -9 69.20 2.90 2 12 -8 18.80 0.90 2 12 -7 23.70 1.10 2 12 -6 139.50 5.70 2 12 -5 13.30 0.70 2 12 -4 8.10 0.50 2 12 -3 1.60 0.30 2 12 -2 11.80 0.60 2 12 -1 22.30 1.00 2 12 0 13.30 0.70 2 12 1 20.40 1.00 2 12 2 25.20 1.20 2 12 3 116.00 4.80 2 12 4 25.10 1.20 2 12 5 35.70 1.60 2 12 6 66.00 2.80 2 13 -10 32.40 1.50 2 13 -9 4.60 0.40 2 13 -8 121.30 5.00 2 13 -7 33.40 1.50 2 13 -6 25.50 2.40 2 13 -4 0.50 0.30 2 13 -3 18.10 0.90 2 13 -2 8.40 0.60 2 13 0 0.90 0.30 2 13 1 21.50 1.00 2 13 2 33.30 1.50 2 13 3 26.70 1.20 2 13 4 37.60 1.70 2 14 -6 3.00 0.40 2 14 -5 10.20 0.60 2 14 -4 3.80 0.40 2 14 -3 38.20 1.70 2 14 -2 20.30 1.00 2 14 -1 39.30 1.70 3 -15 -2 14.20 0.70 3 -15 -1 113.60 4.70 3 -15 0 79.60 3.30 3 -15 1 24.10 1.10 3 -15 2 29.20 1.30 3 -15 3 174.20 7.10 3 -15 4 12.40 0.70 3 -15 5 5.80 0.50 3 -15 6 56.00 2.40 3 -15 7 31.70 2.10 3 -14 -6 11.20 0.60 3 -14 -5 0.70 0.30 3 -14 -4 13.60 0.70 3 -14 -2 3.90 0.40 3 -14 -1 15.60 0.80 3 -14 0 40.20 1.80 3 -14 1 216.90 8.90 3 -14 2 23.20 1.10 3 -14 3 96.60 4.00 3 -14 4 37.60 1.70 3 -14 5 6.50 0.50 3 -14 6 12.40 0.70 3 -14 7 97.20 4.00 3 -14 9 42.00 1.80 3 -14 10 45.90 2.90 3 -13 -8 50.70 2.20 3 -13 -7 102.70 4.30 3 -13 -5 27.50 1.30 3 -13 -4 24.30 1.10 3 -13 -3 2.20 0.30 3 -13 -2 4.30 0.40 3 -13 -1 17.50 0.90 3 -13 1 96.60 5.70 3 -13 2 212.00 8.70 3 -13 3 173.10 8.20 3 -13 4 78.10 6.60 3 -13 5 76.70 4.60 3 -13 6 34.40 1.50 3 -13 7 17.40 0.90 3 -13 8 5.30 0.40 3 -13 9 14.90 0.80 3 -13 10 38.20 1.70 3 -13 11 76.80 3.20 3 -13 12 148.20 8.70 3 -12 -10 17.30 0.90 3 -12 -9 2.20 0.30 3 -12 -7 11.00 0.60 3 -12 -6 64.60 2.70 3 -12 -5 54.00 2.30 3 -12 -4 13.00 1.00 3 -12 -3 17.60 0.90 3 -12 -2 37.80 1.70 3 -12 -1 40.40 1.80 3 -12 0 3.40 0.30 3 -12 1 52.30 2.20 3 -12 2 50.30 2.20 3 -12 3 32.40 1.40 3 -12 4 62.50 2.60 3 -12 5 11.10 0.60 3 -12 6 47.00 2.00 3 -12 7 47.90 2.10 3 -12 8 34.00 2.10 3 -12 9 186.50 7.60 3 -12 10 37.00 1.60 3 -12 11 159.00 6.50 3 -12 13 15.20 0.90 3 -11 -11 136.70 5.60 3 -11 -10 66.30 2.80 3 -11 -9 20.60 1.00 3 -11 -8 66.10 2.80 3 -11 -7 5.20 0.40 3 -11 -6 39.50 1.70 3 -11 -5 52.80 2.30 3 -11 -4 73.20 3.10 3 -11 -3 35.70 1.60 3 -11 -2 31.00 1.40 3 -11 -1 107.50 4.40 3 -11 0 67.10 5.70 3 -11 1 48.60 4.20 3 -11 2 40.00 2.50 3 -11 4 5.10 0.60 3 -11 5 54.30 2.30 3 -11 6 20.90 1.00 3 -11 7 10.60 0.60 3 -11 8 77.70 3.20 3 -11 9 10.50 0.60 3 -11 10 81.00 4.70 3 -11 11 25.20 1.20 3 -11 12 41.70 1.80 3 -11 13 66.30 2.80 3 -11 14 20.70 1.20 3 -10 -12 3.50 0.40 3 -10 -11 73.80 4.50 3 -10 -10 99.20 4.10 3 -10 -9 51.80 2.20 3 -10 -8 54.60 2.30 3 -10 -7 24.20 1.10 3 -10 -6 95.50 4.00 3 -10 -5 19.90 0.90 3 -10 -4 50.80 4.30 3 -10 -3 76.10 3.20 3 -10 -2 393.40 15.90 3 -10 -1 305.50 12.40 3 -10 0 14.40 0.70 3 -10 1 20.30 0.90 3 -10 2 101.70 4.20 3 -10 3 41.50 1.80 3 -10 4 63.50 2.70 3 -10 5 194.20 7.90 3 -10 6 99.30 4.10 3 -10 7 60.50 5.10 3 -10 8 4.30 0.40 3 -10 9 23.10 1.10 3 -10 10 6.00 0.40 3 -10 11 98.20 4.10 3 -10 12 57.00 2.40 3 -10 13 44.20 1.90 3 -10 14 38.10 1.70 3 -10 15 26.70 1.50 3 -9 -13 13.40 0.70 3 -9 -12 13.90 0.70 3 -9 -11 159.30 6.50 3 -9 -10 70.50 3.40 3 -9 -9 130.20 5.30 3 -9 -8 369.80 15.00 3 -9 -7 56.90 2.40 3 -9 -6 17.10 1.80 3 -9 -5 107.20 4.40 3 -9 -4 47.60 2.00 3 -9 -3 101.40 4.20 3 -9 -2 206.50 8.40 3 -9 -1 90.30 3.70 3 -9 0 67.50 2.80 3 -9 1 162.80 6.60 3 -9 2 60.90 2.50 3 -9 3 88.40 3.70 3 -9 4 24.60 1.10 3 -9 5 87.80 3.60 3 -9 6 120.70 4.90 3 -9 7 88.20 3.70 3 -9 8 5.60 0.40 3 -9 9 51.50 3.20 3 -9 10 54.80 2.30 3 -9 11 129.20 5.30 3 -9 12 60.00 2.60 3 -9 13 108.30 4.50 3 -9 14 83.40 3.50 3 -9 16 17.40 1.80 3 -8 -14 57.10 2.40 3 -8 -13 38.20 1.70 3 -8 -12 150.80 6.20 3 -8 -10 224.20 9.10 3 -8 -9 102.90 4.20 3 -8 -8 143.60 5.90 3 -8 -7 161.90 6.60 3 -8 -6 9.90 0.50 3 -8 -5 162.60 6.60 3 -8 -4 8.20 0.50 3 -8 -3 3.30 0.30 3 -8 -2 29.10 1.80 3 -8 -1 182.70 10.50 3 -8 0 576.60 23.20 3 -8 1 10.00 0.50 3 -8 2 172.50 7.00 3 -8 3 28.00 1.20 3 -8 4 9.70 0.70 3 -8 5 145.40 6.80 3 -8 6 138.90 5.70 3 -8 7 27.80 1.20 3 -8 8 55.80 2.30 3 -8 9 5.30 0.40 3 -8 11 0.10 0.30 3 -8 12 44.00 1.90 3 -8 13 149.70 6.20 3 -8 14 13.40 0.90 3 -8 15 6.70 0.60 3 -8 16 15.40 0.80 3 -7 -15 58.30 2.50 3 -7 -14 5.70 0.50 3 -7 -13 16.40 0.80 3 -7 -11 3.80 0.40 3 -7 -10 78.90 3.30 3 -7 -9 253.60 14.50 3 -7 -8 53.60 2.20 3 -7 -7 155.70 6.40 3 -7 -6 93.80 3.90 3 -7 -5 53.00 2.20 3 -7 -4 258.60 14.80 3 -7 -3 39.10 1.70 3 -7 -2 165.50 6.70 3 -7 -1 4.60 0.30 3 -7 0 282.30 11.40 3 -7 1 194.00 7.90 3 -7 2 28.20 1.20 3 -7 3 148.40 6.00 3 -7 4 6.00 0.40 3 -7 5 47.30 2.00 3 -7 6 1.60 0.30 3 -7 7 90.90 3.70 3 -7 8 62.80 2.60 3 -7 9 21.80 1.00 3 -7 10 428.00 17.30 3 -7 11 118.40 7.00 3 -7 12 30.80 1.40 3 -7 13 69.10 3.40 3 -7 14 12.10 0.70 3 -7 15 38.40 1.70 3 -7 17 38.70 2.40 3 -6 -16 55.50 2.40 3 -6 -14 59.30 2.50 3 -6 -13 37.50 1.60 3 -6 -12 24.80 1.10 3 -6 -11 11.60 0.60 3 -6 -10 114.60 6.60 3 -6 -9 347.50 14.10 3 -6 -8 239.00 9.70 3 -6 -7 52.40 2.20 3 -6 -6 87.50 5.10 3 -6 -5 21.30 0.90 3 -6 -4 391.40 15.80 3 -6 -3 126.10 5.10 3 -6 -2 380.30 15.40 3 -6 -1 525.20 21.20 3 -6 0 35.90 1.50 3 -6 1 1404.00 56.60 3 -6 2 126.20 5.10 3 -6 3 213.00 8.60 3 -6 4 284.90 11.50 3 -6 5 37.20 1.60 3 -6 6 3.60 0.30 3 -6 7 216.20 10.10 3 -6 8 84.90 3.50 3 -6 9 188.60 7.70 3 -6 10 114.30 4.70 3 -6 11 33.00 1.50 3 -6 12 37.90 1.60 3 -6 13 27.80 1.20 3 -6 14 23.20 1.10 3 -6 15 19.40 0.90 3 -6 16 46.50 2.00 3 -6 17 25.70 1.80 3 -5 -16 1.40 0.40 3 -5 -15 28.00 1.50 3 -5 -14 16.30 1.00 3 -5 -13 5.20 0.40 3 -5 -12 63.20 2.70 3 -5 -11 131.50 5.40 3 -5 -10 355.00 14.40 3 -5 -9 21.50 1.00 3 -5 -8 111.00 4.50 3 -5 -7 290.10 23.50 3 -5 -6 165.10 6.70 3 -5 -5 33.00 1.40 3 -5 -4 104.10 4.20 3 -5 -3 27.60 1.20 3 -5 -2 42.40 2.50 3 -5 -1 141.40 8.10 3 -5 0 312.20 17.80 3 -5 1 85.90 4.90 3 -5 2 88.80 5.10 3 -5 3 16.30 1.00 3 -5 4 199.70 8.10 3 -5 5 29.40 1.30 3 -5 6 29.70 1.30 3 -5 7 110.80 4.50 3 -5 8 230.00 13.20 3 -5 9 17.70 0.80 3 -5 10 55.00 2.30 3 -5 11 49.80 2.10 3 -5 12 119.00 4.90 3 -5 13 33.10 1.40 3 -5 14 13.00 0.70 3 -5 15 45.20 2.00 3 -5 16 80.80 3.40 3 -5 17 24.00 1.10 3 -4 -17 21.60 1.00 3 -4 -16 39.60 2.50 3 -4 -15 8.50 0.60 3 -4 -14 4.20 0.90 3 -4 -13 65.10 2.70 3 -4 -12 171.10 7.00 3 -4 -11 142.00 5.80 3 -4 -10 254.80 10.30 3 -4 -9 385.80 15.60 3 -4 -8 53.30 3.10 3 -4 -7 14.50 0.70 3 -4 -6 561.90 22.60 3 -4 -5 1.20 0.20 3 -4 -4 128.70 5.20 3 -4 -3 114.60 6.60 3 -4 -2 109.10 4.40 3 -4 -1 37.90 1.60 3 -4 0 37.10 1.50 3 -4 1 191.70 7.70 3 -4 2 328.70 13.30 3 -4 3 514.30 20.80 3 -4 4 205.20 11.80 3 -4 5 254.10 10.30 3 -4 6 348.00 14.10 3 -4 7 235.60 9.60 3 -4 8 360.10 14.60 3 -4 9 132.80 5.40 3 -4 10 248.20 10.10 3 -4 11 28.60 1.30 3 -4 13 157.20 6.40 3 -4 14 27.00 1.20 3 -4 15 106.60 4.40 3 -4 16 23.80 1.10 3 -4 17 3.80 0.40 3 -3 -17 108.70 4.50 3 -3 -16 35.80 1.60 3 -3 -15 73.20 3.10 3 -3 -14 2.20 0.40 3 -3 -13 37.20 1.60 3 -3 -12 72.20 4.20 3 -3 -11 309.80 12.60 3 -3 -10 149.80 6.10 3 -3 -9 101.20 4.20 3 -3 -8 95.20 3.90 3 -3 -7 46.70 1.90 3 -3 -6 632.40 25.50 3 -3 -5 49.30 2.00 3 -3 -4 18.40 1.10 3 -3 -3 101.10 4.10 3 -3 -2 628.30 25.30 3 -3 -1 113.00 4.60 3 -3 0 187.50 7.60 3 -3 1 633.50 25.60 3 -3 2 257.70 10.40 3 -3 3 1243.00 50.10 3 -3 4 312.30 12.60 3 -3 5 323.60 18.50 3 -3 6 145.80 5.90 3 -3 7 110.70 4.50 3 -3 8 145.80 5.90 3 -3 9 29.70 1.80 3 -3 10 95.30 3.90 3 -3 11 261.20 10.60 3 -3 13 159.80 6.50 3 -3 14 121.80 5.00 3 -3 15 106.70 4.40 3 -3 16 68.90 2.90 3 -3 17 4.00 0.40 3 -2 -18 143.10 5.90 3 -2 -17 68.00 2.90 3 -2 -16 25.20 1.20 3 -2 -15 3.40 0.50 3 -2 -14 12.00 0.60 3 -2 -13 403.50 16.30 3 -2 -12 90.70 3.80 3 -2 -11 41.30 1.80 3 -2 -10 47.50 2.00 3 -2 -8 38.80 1.60 3 -2 -7 697.50 28.10 3 -2 -6 91.90 3.80 3 -2 -5 139.70 8.00 3 -2 -4 118.50 4.80 3 -2 -3 201.60 9.40 3 -2 -2 342.20 13.80 3 -2 2 298.30 12.00 3 -2 3 79.60 3.20 3 -2 4 80.90 3.30 3 -2 5 49.50 2.90 3 -2 6 124.30 5.00 3 -2 7 360.30 14.50 3 -2 8 42.00 1.80 3 -2 9 213.30 12.30 3 -2 10 97.90 4.00 3 -2 11 150.20 6.10 3 -2 13 8.20 0.50 3 -2 14 7.90 0.60 3 -2 15 16.60 0.80 3 -2 16 1.40 0.40 3 -2 17 9.70 0.60 3 -1 -18 47.30 2.00 3 -1 -17 202.30 8.30 3 -1 -16 33.80 1.50 3 -1 -15 1.30 0.50 3 -1 -14 4.00 0.40 3 -1 -13 49.60 2.10 3 -1 -12 419.20 17.00 3 -1 -11 139.30 5.70 3 -1 -10 424.40 17.20 3 -1 -9 53.10 3.10 3 -1 -8 464.60 18.80 3 -1 -7 328.90 13.30 3 -1 -6 283.00 11.50 3 -1 -5 196.00 11.20 3 -1 -4 85.30 3.50 3 -1 -3 184.60 7.40 3 -1 2 570.60 23.00 3 -1 3 709.00 28.50 3 -1 4 223.20 9.00 3 -1 5 110.80 6.40 3 -1 6 66.20 2.70 3 -1 7 148.20 6.00 3 -1 8 54.90 2.30 3 -1 9 99.20 4.10 3 -1 10 54.10 2.30 3 -1 11 228.10 9.30 3 -1 12 44.10 2.70 3 -1 13 23.00 1.10 3 -1 14 4.30 0.40 3 -1 15 16.00 0.80 3 -1 16 29.00 1.30 3 -1 17 34.80 1.80 3 0 -18 50.60 2.20 3 0 -17 301.20 12.20 3 0 -16 108.60 4.50 3 0 -15 10.80 0.60 3 0 -14 36.30 1.60 3 0 -13 9.20 0.50 3 0 -12 127.60 5.20 3 0 -11 56.40 2.30 3 0 -10 295.00 12.00 3 0 -9 904.00 36.70 3 0 -8 545.70 22.00 3 0 -7 547.30 22.10 3 0 -6 21.50 0.90 3 0 -5 31.70 1.80 3 0 -4 11.30 0.50 3 0 -3 292.10 11.80 3 0 -2 322.00 13.00 3 0 1 65.70 2.70 3 0 2 594.30 24.10 3 0 3 4.70 0.30 3 0 4 138.10 7.90 3 0 5 94.40 3.90 3 0 6 403.60 16.30 3 0 7 67.70 2.80 3 0 8 29.80 1.80 3 0 9 49.30 2.10 3 0 10 393.60 15.90 3 0 11 63.70 2.70 3 0 12 6.10 0.40 3 0 13 27.20 1.20 3 0 15 53.20 2.30 3 0 17 8.20 1.20 3 1 -18 22.90 1.10 3 1 -17 32.70 1.50 3 1 -16 17.10 0.80 3 1 -15 200.80 8.20 3 1 -14 33.70 1.50 3 1 -13 44.90 1.90 3 1 -12 31.60 1.40 3 1 -11 1.50 0.30 3 1 -10 201.00 8.20 3 1 -9 457.00 26.00 3 1 -8 182.60 7.40 3 1 -7 922.50 37.30 3 1 -6 179.50 7.30 3 1 -5 110.60 6.40 3 1 -4 422.00 17.00 3 1 -3 348.60 14.10 3 1 -2 784.40 31.70 3 1 -1 238.10 9.60 3 1 0 251.90 10.20 3 1 1 45.40 1.80 3 1 2 41.80 1.70 3 1 3 292.70 16.70 3 1 4 79.40 3.20 3 1 5 601.30 24.30 3 1 6 106.50 4.40 3 1 7 143.70 5.90 3 1 8 188.20 8.80 3 1 9 13.30 0.70 3 1 10 385.00 15.60 3 1 11 32.00 2.90 3 1 12 99.20 4.10 3 1 13 104.70 4.30 3 1 14 101.00 4.20 3 1 15 82.90 3.50 3 1 16 41.70 1.80 3 2 -18 9.30 0.60 3 2 -17 52.20 2.20 3 2 -16 84.70 3.50 3 2 -15 42.10 1.80 3 2 -14 45.90 2.00 3 2 -13 109.20 4.50 3 2 -12 91.20 3.80 3 2 -11 115.20 4.70 3 2 -10 79.70 3.30 3 2 -9 415.60 33.60 3 2 -8 1271.00 51.30 3 2 -7 365.80 14.80 3 2 -6 153.30 7.20 3 2 -5 51.30 2.10 3 2 -3 471.30 19.00 3 2 -2 196.10 7.90 3 2 -1 709.70 28.60 3 2 0 141.00 5.70 3 2 1 266.70 10.80 3 2 2 90.80 5.20 3 2 3 25.00 1.10 3 2 4 253.80 10.30 3 2 5 613.20 24.70 3 2 6 46.70 2.00 3 2 8 67.40 2.80 3 2 9 53.10 2.20 3 2 10 220.80 9.00 3 2 11 48.70 2.10 3 2 12 82.50 3.40 3 2 13 62.00 3.80 3 2 14 11.50 0.70 3 2 15 2.40 0.40 3 2 16 22.20 1.10 3 3 -18 12.80 0.70 3 3 -17 19.40 0.90 3 3 -16 41.70 1.80 3 3 -15 33.00 2.80 3 3 -14 23.50 1.10 3 3 -13 17.70 1.00 3 3 -12 5.60 0.50 3 3 -11 186.40 7.60 3 3 -10 148.00 6.00 3 3 -9 116.20 4.80 3 3 -8 122.00 5.00 3 3 -7 524.20 21.20 3 3 -6 348.00 14.10 3 3 -5 142.00 5.80 3 3 -4 227.70 9.20 3 3 -3 43.70 1.80 3 3 -2 120.60 6.90 3 3 -1 11.10 0.70 3 3 0 427.20 24.30 3 3 1 197.30 8.00 3 3 2 97.00 4.00 3 3 3 228.50 9.20 3 3 4 391.70 15.80 3 3 5 162.00 6.60 3 3 7 47.10 2.00 3 3 8 30.90 1.30 3 3 9 61.40 2.60 3 3 10 52.40 3.10 3 3 11 12.60 0.70 3 3 12 7.50 0.50 3 3 13 30.50 1.40 3 3 14 27.30 1.30 3 3 15 30.40 1.40 3 4 -18 55.80 2.40 3 4 -16 109.50 4.50 3 4 -15 241.40 9.80 3 4 -14 87.60 3.60 3 4 -13 38.20 1.70 3 4 -12 113.10 6.60 3 4 -11 65.60 2.80 3 4 -10 178.40 7.30 3 4 -9 500.70 20.20 3 4 -8 454.70 26.00 3 4 -7 385.10 15.60 3 4 -6 17.70 0.80 3 4 -5 210.10 8.50 3 4 -4 20.40 0.90 3 4 -3 187.10 7.60 3 4 -2 16.00 0.70 3 4 -1 15.20 0.70 3 4 0 668.70 26.90 3 4 1 373.20 15.10 3 4 2 276.30 11.20 3 4 3 191.60 7.80 3 4 4 504.90 20.40 3 4 5 317.30 18.10 3 4 6 56.60 2.40 3 4 7 60.40 2.50 3 4 8 74.30 3.10 3 4 10 15.20 0.80 3 4 11 6.50 0.50 3 4 12 30.60 1.40 3 4 13 3.80 0.40 3 4 15 55.70 2.80 3 5 -18 43.40 2.20 3 5 -17 38.50 1.70 3 5 -16 56.50 2.40 3 5 -15 57.30 2.50 3 5 -14 240.00 9.80 3 5 -13 46.80 2.00 3 5 -12 64.30 2.70 3 5 -11 21.10 1.40 3 5 -10 122.00 5.00 3 5 -9 1099.00 44.30 3 5 -8 169.50 6.90 3 5 -7 56.20 2.30 3 5 -6 31.10 1.90 3 5 -5 321.10 13.00 3 5 -4 61.20 2.50 3 5 -3 42.70 1.80 3 5 -2 22.50 1.00 3 5 -1 177.60 7.20 3 5 0 12.80 0.60 3 5 1 202.40 8.20 3 5 2 299.10 12.10 3 5 3 506.40 28.90 3 5 4 95.20 3.90 3 5 5 226.30 9.20 3 5 6 56.00 2.30 3 5 7 68.90 2.90 3 5 8 8.00 0.60 3 5 9 34.70 1.50 3 5 10 10.70 0.60 3 5 11 33.40 3.00 3 5 12 75.00 3.10 3 5 13 15.50 0.80 3 5 14 35.70 1.60 3 6 -17 24.80 1.20 3 6 -16 11.10 0.80 3 6 -15 23.30 1.30 3 6 -14 23.50 1.10 3 6 -13 38.20 1.70 3 6 -12 109.20 4.50 3 6 -11 39.70 1.70 3 6 -10 114.40 6.60 3 6 -9 93.70 3.90 3 6 -8 68.90 2.90 3 6 -7 6.80 0.40 3 6 -6 142.30 5.80 3 6 -5 189.80 7.70 3 6 -4 67.60 4.00 3 6 -3 85.40 5.00 3 6 -1 123.60 10.10 3 6 0 116.00 6.70 3 6 1 194.00 7.90 3 6 2 121.10 5.00 3 6 3 104.60 4.30 3 6 4 21.40 1.00 3 6 5 9.30 0.50 3 6 6 12.00 0.60 3 6 7 126.80 5.20 3 6 8 1.10 0.30 3 6 9 3.00 0.30 3 6 11 12.40 0.70 3 6 12 29.20 1.30 3 6 13 65.10 2.80 3 7 -17 129.00 5.30 3 7 -16 29.10 1.30 3 7 -15 131.20 5.40 3 7 -14 69.80 3.00 3 7 -13 15.70 1.30 3 7 -12 45.00 1.90 3 7 -11 59.80 2.50 3 7 -10 120.80 5.00 3 7 -9 102.20 8.50 3 7 -8 87.80 3.60 3 7 -7 103.10 4.20 3 7 -6 196.40 8.00 3 7 -5 167.90 6.90 3 7 -4 178.60 7.30 3 7 -3 344.80 14.00 3 7 -2 220.20 8.90 3 7 -1 114.90 4.70 3 7 0 307.40 12.40 3 7 1 175.60 7.20 3 7 2 310.30 12.60 3 7 3 75.80 3.20 3 7 4 178.50 7.30 3 7 5 85.20 5.00 3 7 6 23.90 1.10 3 7 7 75.50 3.10 3 7 8 41.70 1.80 3 7 9 9.80 0.60 3 7 10 61.30 2.60 3 7 11 25.30 1.40 3 7 12 69.30 2.90 3 8 -16 149.30 6.20 3 8 -15 68.70 2.90 3 8 -14 76.10 3.20 3 8 -13 26.20 1.20 3 8 -12 21.60 1.50 3 8 -11 12.60 0.80 3 8 -10 16.70 0.80 3 8 -9 50.20 2.10 3 8 -8 46.90 2.00 3 8 -7 174.80 10.10 3 8 -6 103.40 4.30 3 8 -5 27.50 1.20 3 8 -4 54.30 2.30 3 8 -3 207.80 8.50 3 8 -2 21.60 1.00 3 8 -1 131.70 5.40 3 8 0 17.20 0.80 3 8 1 43.90 1.90 3 8 2 344.90 28.00 3 8 3 172.40 7.00 3 8 4 27.50 1.20 3 8 5 1.30 0.30 3 8 6 112.20 4.60 3 8 7 90.80 7.60 3 8 8 41.00 1.80 3 8 9 92.80 3.90 3 8 10 11.40 1.30 3 8 11 23.40 1.10 3 9 -15 10.00 0.60 3 9 -14 15.10 0.80 3 9 -13 3.80 0.40 3 9 -12 78.40 3.30 3 9 -11 57.40 2.40 3 9 -10 34.50 1.80 3 9 -9 89.10 3.70 3 9 -8 91.40 3.80 3 9 -7 515.30 20.90 3 9 -6 40.00 1.70 3 9 -5 3.90 0.40 3 9 -4 6.00 0.50 3 9 -3 10.20 0.60 3 9 -2 22.40 1.00 3 9 -1 33.20 1.50 3 9 0 146.40 6.00 3 9 1 39.20 1.70 3 9 2 3.30 0.30 3 9 3 92.80 3.90 3 9 4 26.00 1.20 3 9 5 21.60 1.50 3 9 6 38.50 1.70 3 9 7 27.60 1.30 3 9 8 19.50 0.90 3 9 9 8.60 0.50 3 9 10 14.60 0.90 3 10 -14 9.50 0.60 3 10 -13 36.20 1.60 3 10 -12 4.70 0.70 3 10 -11 5.00 0.40 3 10 -10 116.00 4.80 3 10 -9 11.70 0.70 3 10 -7 231.90 9.40 3 10 -6 116.30 4.80 3 10 -5 0.10 0.30 3 10 -4 231.30 9.50 3 10 -3 30.80 1.40 3 10 -2 22.00 1.00 3 10 -1 30.00 1.40 3 10 0 12.50 0.70 3 10 1 3.60 0.30 3 10 2 33.40 1.70 3 10 3 52.00 2.20 3 10 4 5.40 0.40 3 10 5 76.80 3.20 3 10 6 11.40 0.60 3 10 7 18.80 0.90 3 10 8 4.80 0.40 3 11 -13 58.30 3.60 3 11 -12 24.40 1.20 3 11 -11 38.40 1.70 3 11 -10 13.10 0.70 3 11 -9 172.50 7.10 3 11 -8 10.40 0.60 3 11 -7 9.40 0.60 3 11 -6 170.90 7.00 3 11 -5 29.20 1.30 3 11 -4 84.00 3.50 3 11 -3 80.70 3.40 3 11 -2 23.90 1.10 3 11 -1 8.00 0.50 3 11 0 18.10 0.90 3 11 1 18.20 0.90 3 11 2 16.30 0.80 3 11 3 2.40 0.30 3 11 4 35.10 1.60 3 11 5 77.80 3.30 3 11 6 56.80 2.40 3 12 -11 4.10 0.70 3 12 -10 47.80 2.10 3 12 -9 74.50 3.10 3 12 -8 18.00 0.90 3 12 -7 87.90 7.40 3 12 -6 9.90 0.60 3 12 -5 3.80 0.50 3 12 -4 46.60 2.00 3 12 -3 21.80 1.20 3 12 -2 16.20 1.00 3 12 -1 7.70 0.50 3 12 0 69.00 2.90 3 12 1 62.10 5.30 3 12 2 18.00 0.90 3 12 3 45.90 2.00 3 12 4 71.00 3.00 3 13 -8 1.10 0.50 3 13 -7 14.50 0.80 3 13 -6 32.00 1.50 3 13 -5 21.20 1.00 3 13 -4 2.70 0.40 3 13 -3 11.00 0.60 3 13 -2 16.20 0.80 3 13 -1 2.20 0.30 3 13 0 49.40 2.10 4 -14 -2 73.40 3.10 4 -14 -1 36.70 1.60 4 -14 0 4.40 0.40 4 -14 1 12.20 0.70 4 -14 2 82.60 3.50 4 -14 3 26.10 1.20 4 -14 4 10.70 0.60 4 -14 5 16.50 0.90 4 -14 6 24.40 1.10 4 -13 -5 16.80 0.80 4 -13 -4 1.90 0.30 4 -13 -3 12.50 0.70 4 -13 -2 44.00 1.90 4 -13 0 154.80 6.40 4 -13 1 88.60 3.70 4 -13 2 32.00 1.40 4 -13 3 2.80 0.30 4 -13 4 65.80 2.80 4 -13 6 119.10 4.90 4 -13 7 93.00 3.90 4 -13 8 133.00 5.50 4 -13 9 126.60 5.20 4 -12 -8 66.10 5.80 4 -12 -7 63.00 2.70 4 -12 -6 20.50 1.00 4 -12 -5 0.80 0.30 4 -12 -4 71.90 3.00 4 -12 -3 22.50 1.10 4 -12 -2 47.80 2.10 4 -12 -1 85.50 3.60 4 -12 0 8.90 0.50 4 -12 1 264.00 10.80 4 -12 2 143.50 5.90 4 -12 3 33.40 1.50 4 -12 4 73.80 3.10 4 -12 5 26.30 1.20 4 -12 6 60.10 2.50 4 -12 7 17.90 0.90 4 -12 8 20.00 1.00 4 -12 9 62.60 2.70 4 -12 10 188.60 7.70 4 -12 11 216.20 8.80 4 -11 -9 142.00 5.80 4 -11 -8 36.90 1.60 4 -11 -7 24.00 2.20 4 -11 -6 2.50 0.30 4 -11 -5 0.70 0.30 4 -11 -4 32.10 1.40 4 -11 -3 6.30 0.50 4 -11 -2 25.20 1.60 4 -11 -1 16.80 1.20 4 -11 0 181.20 7.40 4 -11 1 79.40 3.30 4 -11 2 38.70 1.70 4 -11 3 22.80 1.10 4 -11 4 13.60 0.80 4 -11 6 8.30 0.50 4 -11 7 15.60 0.80 4 -11 8 42.10 1.80 4 -11 9 50.00 2.10 4 -11 10 92.40 7.70 4 -11 11 80.90 3.40 4 -11 12 0.10 0.40 4 -10 -11 97.20 5.80 4 -10 -10 2.50 0.40 4 -10 -9 224.90 9.20 4 -10 -8 16.10 0.80 4 -10 -7 18.60 0.90 4 -10 -6 35.30 1.50 4 -10 -5 18.80 1.20 4 -10 -4 8.20 0.60 4 -10 -3 12.10 1.20 4 -10 -2 204.30 9.60 4 -10 -1 15.10 0.70 4 -10 0 124.60 5.10 4 -10 1 7.10 0.40 4 -10 2 77.00 3.20 4 -10 3 141.30 6.70 4 -10 4 68.00 5.70 4 -10 5 179.40 8.40 4 -10 6 3.30 0.30 4 -10 7 2.40 0.30 4 -10 8 23.80 1.30 4 -10 9 29.10 1.30 4 -10 10 12.50 0.70 4 -10 11 57.80 2.50 4 -10 12 125.20 5.20 4 -10 13 28.00 1.30 4 -9 -12 12.30 0.70 4 -9 -11 73.30 3.10 4 -9 -9 118.90 4.90 4 -9 -8 141.30 5.80 4 -9 -7 74.60 3.10 4 -9 -6 59.70 3.60 4 -9 -5 9.10 0.50 4 -9 -4 39.30 1.70 4 -9 -3 29.80 1.30 4 -9 -2 5.30 0.30 4 -9 -1 334.00 13.50 4 -9 0 14.50 1.00 4 -9 1 39.20 3.40 4 -9 2 35.60 2.20 4 -9 3 86.30 5.00 4 -9 4 476.30 19.20 4 -9 5 30.80 1.30 4 -9 6 23.00 1.20 4 -9 7 105.80 6.20 4 -9 8 202.80 8.30 4 -9 10 135.30 5.60 4 -9 11 49.70 2.10 4 -9 12 23.60 1.10 4 -9 13 93.60 3.90 4 -9 14 67.30 2.90 4 -8 -13 3.30 0.50 4 -8 -12 70.30 3.00 4 -8 -11 48.40 4.30 4 -8 -10 124.60 5.10 4 -8 -9 119.40 4.90 4 -8 -8 87.40 7.40 4 -8 -7 21.30 1.00 4 -8 -6 80.40 3.30 4 -8 -5 15.30 0.70 4 -8 -4 61.80 3.00 4 -8 -3 35.50 2.20 4 -8 -2 75.40 3.10 4 -8 -1 30.20 1.30 4 -8 0 119.00 4.90 4 -8 1 145.20 5.90 4 -8 2 107.40 4.40 4 -8 3 228.20 9.20 4 -8 4 4.90 0.30 4 -8 5 10.40 0.70 4 -8 6 41.70 2.50 4 -8 7 42.90 1.80 4 -8 8 160.30 9.30 4 -8 9 31.10 1.40 4 -8 10 29.00 2.60 4 -8 11 179.30 7.30 4 -8 12 10.90 0.60 4 -8 14 104.70 4.40 4 -7 -14 57.20 5.10 4 -7 -13 20.00 1.00 4 -7 -11 7.30 0.50 4 -7 -10 9.20 0.60 4 -7 -8 183.50 7.50 4 -7 -7 247.30 10.00 4 -7 -6 162.90 6.60 4 -7 -5 2.20 0.40 4 -7 -4 55.80 2.30 4 -7 -3 14.80 0.70 4 -7 -2 233.90 9.50 4 -7 -1 22.50 1.00 4 -7 0 183.20 7.40 4 -7 1 654.70 26.50 4 -7 2 288.00 11.60 4 -7 3 243.40 9.90 4 -7 4 19.00 0.90 4 -7 5 40.70 1.70 4 -7 6 75.20 3.10 4 -7 8 35.00 1.50 4 -7 9 4.30 0.80 4 -7 10 126.60 5.20 4 -7 11 89.80 5.30 4 -7 12 47.50 2.00 4 -7 13 5.70 0.40 4 -7 14 32.00 1.40 4 -7 15 2.30 0.40 4 -6 -14 1.60 0.60 4 -6 -13 21.30 1.20 4 -6 -12 94.00 3.90 4 -6 -11 87.10 3.60 4 -6 -10 33.10 3.00 4 -6 -9 7.80 0.60 4 -6 -8 46.80 2.00 4 -6 -7 396.30 18.50 4 -6 -6 44.40 1.90 4 -6 -5 42.80 1.80 4 -6 -4 43.00 1.80 4 -6 -3 70.00 2.90 4 -6 -2 132.40 7.60 4 -6 -1 25.60 1.50 4 -6 0 288.60 11.70 4 -6 1 181.10 7.30 4 -6 2 697.90 39.80 4 -6 3 290.00 16.60 4 -6 4 103.30 4.20 4 -6 5 105.80 4.30 4 -6 6 62.60 2.60 4 -6 7 46.50 2.00 4 -6 8 59.60 3.60 4 -6 9 135.90 5.60 4 -6 10 73.20 3.10 4 -6 11 16.70 0.90 4 -6 12 22.00 1.00 4 -6 13 8.00 0.80 4 -6 15 46.60 2.00 4 -5 -15 25.10 1.40 4 -5 -14 36.90 1.60 4 -5 -13 26.30 1.20 4 -5 -12 29.70 1.30 4 -5 -10 130.30 5.30 4 -5 -9 287.80 11.70 4 -5 -8 136.60 5.60 4 -5 -7 261.40 10.60 4 -5 -6 362.00 14.60 4 -5 -5 313.70 12.70 4 -5 -4 15.20 0.70 4 -5 -3 210.80 8.50 4 -5 -2 91.10 4.30 4 -5 -1 53.80 2.20 4 -5 0 159.20 6.40 4 -5 1 316.00 12.80 4 -5 2 138.80 5.60 4 -5 3 348.70 14.10 4 -5 4 125.50 7.20 4 -5 5 457.70 18.50 4 -5 6 41.80 1.80 4 -5 7 44.00 1.80 4 -5 8 91.50 3.80 4 -5 9 24.40 1.30 4 -5 11 1.20 0.30 4 -5 12 19.20 1.40 4 -5 13 3.40 0.40 4 -5 15 134.80 5.60 4 -4 -16 64.20 3.20 4 -4 -15 1.50 0.30 4 -4 -13 5.60 0.50 4 -4 -11 74.80 3.10 4 -4 -10 38.20 1.70 4 -4 -9 141.00 5.80 4 -4 -8 35.30 1.50 4 -4 -7 102.10 4.20 4 -4 -6 161.80 6.60 4 -4 -5 16.70 1.00 4 -4 -4 415.20 16.80 4 -4 -3 73.00 3.00 4 -4 3 136.20 5.50 4 -4 4 37.60 1.50 4 -4 5 362.60 20.80 4 -4 6 31.60 1.30 4 -4 7 37.10 1.60 4 -4 8 64.50 2.70 4 -4 9 131.80 7.70 4 -4 10 3.30 0.50 4 -4 11 0.90 0.30 4 -4 12 5.90 0.40 4 -4 13 67.40 2.80 4 -4 14 101.50 4.20 4 -4 15 56.70 2.40 4 -3 -16 16.10 0.80 4 -3 -15 25.50 1.20 4 -3 -14 57.30 2.40 4 -3 -13 4.00 0.40 4 -3 -11 76.10 3.20 4 -3 -10 66.90 2.80 4 -3 -9 215.80 17.50 4 -3 -8 247.80 10.10 4 -3 -7 125.50 5.10 4 -3 -6 211.00 8.60 4 -3 -5 49.30 2.00 4 -3 -4 488.40 19.70 4 -3 4 301.40 12.10 4 -3 5 380.10 15.30 4 -3 6 3.70 0.40 4 -3 7 132.20 5.40 4 -3 8 45.00 1.90 4 -3 9 68.20 4.00 4 -3 10 71.60 3.50 4 -3 11 108.80 4.50 4 -3 12 140.60 8.20 4 -3 13 18.00 0.90 4 -3 14 199.00 8.20 4 -3 15 22.10 1.10 4 -2 -16 16.70 0.90 4 -2 -15 53.20 2.30 4 -2 -14 39.80 1.70 4 -2 -13 76.60 4.50 4 -2 -12 35.40 1.50 4 -2 -11 32.40 1.40 4 -2 -10 159.10 6.50 4 -2 -9 362.10 14.70 4 -2 -8 169.00 6.90 4 -2 -7 80.10 3.30 4 -2 -6 329.00 18.80 4 -2 -5 542.90 21.90 4 -2 4 256.80 10.40 4 -2 5 252.70 10.20 4 -2 6 40.10 1.70 4 -2 7 47.50 2.00 4 -2 8 67.50 2.80 4 -2 9 37.20 2.30 4 -2 10 180.40 8.50 4 -2 11 168.70 6.90 4 -2 12 39.70 1.70 4 -2 13 78.30 3.30 4 -2 15 9.90 0.60 4 -1 -16 16.20 0.80 4 -1 -15 69.00 5.90 4 -1 -14 51.00 2.20 4 -1 -13 24.60 1.60 4 -1 -12 4.40 0.40 4 -1 -11 25.60 1.10 4 -1 -10 49.70 2.10 4 -1 -9 113.50 4.60 4 -1 -8 363.60 14.70 4 -1 -7 272.70 11.00 4 -1 -6 80.20 4.60 4 -1 -5 64.70 2.60 4 -1 4 59.60 2.40 4 -1 5 137.00 7.90 4 -1 6 129.90 5.30 4 -1 7 146.90 6.00 4 -1 8 93.10 3.80 4 -1 9 81.30 3.40 4 -1 10 152.00 8.80 4 -1 11 77.30 3.20 4 -1 12 41.20 1.80 4 -1 13 54.20 2.30 4 -1 14 9.50 0.60 4 -1 15 3.60 0.50 4 0 -17 6.10 1.20 4 0 -16 1.20 0.40 4 0 -15 163.20 13.40 4 0 -14 97.60 4.10 4 0 -13 137.20 8.00 4 0 -12 20.10 0.90 4 0 -11 20.60 0.90 4 0 -10 364.10 14.70 4 0 -9 487.00 19.70 4 0 -8 61.80 2.60 4 0 -7 198.20 8.00 4 0 -6 375.20 21.40 4 0 -5 151.70 6.10 4 0 -4 2.90 0.20 4 0 3 204.50 8.20 4 0 4 692.20 27.90 4 0 5 162.80 6.60 4 0 6 26.60 1.20 4 0 7 99.90 4.10 4 0 8 233.50 13.40 4 0 9 47.30 2.00 4 0 10 129.70 10.60 4 0 11 11.80 1.00 4 0 12 45.80 2.00 4 0 13 5.40 0.50 4 0 14 2.00 0.40 4 0 15 2.60 0.40 4 1 -16 19.10 0.90 4 1 -15 87.40 7.30 4 1 -14 138.10 5.70 4 1 -13 126.30 7.40 4 1 -12 56.90 2.40 4 1 -11 75.30 3.10 4 1 -10 269.80 10.90 4 1 -9 143.60 5.90 4 1 -8 34.40 1.50 4 1 -7 456.60 18.50 4 1 -6 406.00 18.90 4 1 -5 204.80 8.30 4 1 -4 56.00 2.30 4 1 -3 104.40 4.20 4 1 2 382.90 15.50 4 1 3 331.20 13.40 4 1 4 88.60 5.10 4 1 5 130.80 5.30 4 1 6 48.60 2.00 4 1 7 68.20 2.80 4 1 8 264.20 10.70 4 1 9 53.80 2.60 4 1 10 56.30 2.40 4 1 11 18.40 0.90 4 1 12 48.60 2.10 4 1 14 54.30 2.40 4 2 -17 17.40 1.10 4 2 -16 16.20 0.80 4 2 -15 310.20 17.90 4 2 -14 31.50 1.40 4 2 -13 82.20 6.90 4 2 -12 28.50 1.30 4 2 -11 285.30 11.60 4 2 -10 46.00 2.00 4 2 -8 235.90 9.60 4 2 -7 128.30 5.20 4 2 -6 261.60 10.60 4 2 -5 2.70 0.30 4 2 -4 23.10 1.00 4 2 -3 20.30 0.90 4 2 -2 29.70 1.20 4 2 -1 143.90 5.80 4 2 0 154.00 6.20 4 2 1 61.80 2.50 4 2 2 148.70 8.50 4 2 3 191.10 7.70 4 2 4 274.90 11.10 4 2 5 46.60 2.00 4 2 6 18.30 0.80 4 2 7 150.90 8.70 4 2 8 16.60 0.80 4 2 9 221.50 18.00 4 2 11 1.20 0.30 4 2 12 121.70 5.00 4 2 13 97.10 4.10 4 2 14 25.00 1.20 4 3 -16 157.10 6.40 4 3 -15 62.90 2.70 4 3 -14 2.70 0.40 4 3 -13 36.10 1.80 4 3 -11 188.40 8.90 4 3 -10 29.50 1.30 4 3 -9 68.00 2.80 4 3 -8 16.00 0.80 4 3 -7 17.90 0.80 4 3 -6 304.70 12.40 4 3 -5 165.80 7.80 4 3 -4 36.30 1.50 4 3 -3 125.70 7.20 4 3 -2 41.30 2.40 4 3 0 63.40 3.70 4 3 1 84.60 3.40 4 3 2 336.50 13.60 4 3 3 488.00 19.70 4 3 4 135.00 5.50 4 3 5 518.20 20.90 4 3 6 26.80 1.60 4 3 7 68.40 2.90 4 3 8 96.80 8.00 4 3 9 0.60 0.40 4 3 10 80.70 3.40 4 3 11 3.30 0.40 4 3 12 1.70 0.40 4 3 13 32.10 1.50 4 4 -16 80.30 3.40 4 4 -15 78.50 3.30 4 4 -14 50.80 2.20 4 4 -13 57.40 2.40 4 4 -12 137.30 8.00 4 4 -11 31.70 1.40 4 4 -10 46.30 2.00 4 4 -9 281.00 11.40 4 4 -8 123.50 5.10 4 4 -7 85.70 5.00 4 4 -6 0.50 0.20 4 4 -5 108.10 4.40 4 4 -4 40.00 1.70 4 4 -3 133.90 5.50 4 4 -2 77.00 3.20 4 4 -1 52.00 2.20 4 4 0 75.60 3.10 4 4 1 45.50 1.90 4 4 2 387.80 15.70 4 4 3 123.70 5.00 4 4 4 28.70 1.80 4 4 5 143.90 5.90 4 4 6 319.10 12.90 4 4 7 -0.20 0.50 4 4 8 59.10 3.60 4 4 9 4.40 0.40 4 4 10 17.20 0.90 4 4 12 28.50 1.30 4 5 -15 33.30 1.70 4 5 -14 19.30 1.00 4 5 -13 45.00 2.70 4 5 -12 199.00 9.40 4 5 -11 40.70 2.10 4 5 -10 94.10 3.90 4 5 -9 69.80 2.90 4 5 -8 516.70 20.90 4 5 -7 126.30 5.20 4 5 -6 47.60 2.90 4 5 -5 123.00 5.00 4 5 -4 32.20 1.40 4 5 -3 503.70 20.30 4 5 -2 39.20 1.70 4 5 -1 49.90 2.10 4 5 0 36.60 1.60 4 5 1 85.10 3.50 4 5 2 32.70 2.00 4 5 3 17.20 0.80 4 5 4 121.00 4.90 4 5 5 44.50 1.90 4 5 6 111.20 6.50 4 5 8 17.10 0.80 4 5 9 14.40 0.80 4 5 11 61.30 2.60 4 6 -15 79.00 3.30 4 6 -14 6.40 0.50 4 6 -12 19.20 0.90 4 6 -11 26.00 1.40 4 6 -10 101.90 4.90 4 6 -9 56.90 2.40 4 6 -8 195.10 8.00 4 6 -7 2.50 0.30 4 6 -6 37.80 1.60 4 6 -5 60.40 2.50 4 6 -4 115.90 4.80 4 6 -3 201.20 8.20 4 6 -2 18.60 0.90 4 6 -1 1.90 0.20 4 6 0 265.10 10.80 4 6 1 22.20 1.00 4 6 2 16.10 0.80 4 6 3 33.30 1.40 4 6 4 44.20 2.20 4 6 5 40.50 2.50 4 6 6 42.70 1.80 4 6 7 27.90 1.20 4 6 8 46.40 2.00 4 6 9 16.40 1.20 4 6 10 5.70 0.50 4 7 -14 90.20 3.80 4 7 -13 37.20 1.70 4 7 -12 9.60 1.10 4 7 -11 25.90 1.20 4 7 -10 17.30 0.90 4 7 -9 160.10 9.30 4 7 -7 88.80 3.70 4 7 -6 50.20 2.10 4 7 -5 131.80 5.40 4 7 -4 31.20 1.40 4 7 -3 37.00 1.60 4 7 -2 100.30 4.10 4 7 -1 151.60 6.20 4 7 0 85.50 3.50 4 7 1 106.60 4.40 4 7 2 0.70 0.30 4 7 3 20.30 1.90 4 7 4 83.20 3.50 4 7 5 149.20 6.10 4 7 6 16.10 0.80 4 7 7 7.60 0.80 4 7 8 20.00 1.00 4 7 9 16.60 0.80 4 8 -14 177.00 7.30 4 8 -13 2.90 0.40 4 8 -12 19.80 1.00 4 8 -11 0.50 0.40 4 8 -10 61.10 2.60 4 8 -9 78.00 3.30 4 8 -8 48.80 2.10 4 8 -7 317.00 18.30 4 8 -6 54.20 4.60 4 8 -5 41.70 3.60 4 8 -4 84.80 7.00 4 8 -3 103.80 8.60 4 8 -2 8.90 1.10 4 8 1 4.60 0.40 4 8 2 84.80 3.50 4 8 3 20.40 1.00 4 8 4 284.10 11.60 4 8 5 27.10 1.20 4 8 6 16.20 0.80 4 8 7 36.50 1.60 4 8 8 110.00 4.60 4 9 -12 16.20 0.90 4 9 -11 8.90 0.60 4 9 -10 73.40 3.10 4 9 -9 69.00 5.90 4 9 -8 41.80 1.80 4 9 -7 291.30 11.80 4 9 -6 91.00 3.80 4 9 -5 69.80 2.90 4 9 -4 4.60 0.40 4 9 -3 69.60 2.90 4 9 -2 20.00 1.00 4 9 -1 23.50 1.10 4 9 0 27.00 1.20 4 9 1 3.00 0.30 4 9 2 18.80 0.90 4 9 3 73.70 3.60 4 9 4 11.70 0.60 4 9 5 4.00 0.40 4 9 6 1.20 0.30 4 10 -11 59.90 3.00 4 10 -10 34.20 1.50 4 10 -9 6.50 0.50 4 10 -8 73.10 3.10 4 10 -7 13.20 0.70 4 10 -6 91.60 3.80 4 10 -4 16.90 1.20 4 10 -3 48.50 3.00 4 10 -2 66.80 4.00 4 10 0 27.60 1.30 4 10 1 22.60 1.10 4 10 2 16.20 0.80 4 10 3 99.10 4.10 4 10 4 14.30 0.80 4 11 -7 13.90 0.80 4 11 -6 68.30 2.90 4 11 -5 9.30 0.60 4 11 -4 4.20 0.40 4 11 -3 72.30 3.10 4 11 -2 30.70 1.40 4 11 -1 23.00 1.10 4 11 0 18.70 0.90 4 11 1 34.80 1.60 5 -12 -3 6.70 0.40 5 -12 -2 64.80 3.90 5 -12 -1 27.90 1.80 5 -12 0 100.10 8.30 5 -12 1 20.20 1.90 5 -12 3 53.50 4.60 5 -12 4 142.80 8.30 5 -12 5 122.40 10.10 5 -11 -6 10.00 0.80 5 -11 -5 1.40 0.30 5 -11 -4 17.40 1.10 5 -11 -3 17.10 0.90 5 -11 -2 44.20 2.20 5 -11 -1 5.90 0.50 5 -11 0 16.00 0.90 5 -11 1 95.70 5.60 5 -11 2 42.70 2.60 5 -11 3 24.20 1.50 5 -11 4 15.40 0.90 5 -11 7 59.90 5.20 5 -10 -8 51.10 2.60 5 -10 -7 15.10 0.80 5 -10 -5 5.50 0.40 5 -10 -4 4.20 0.30 5 -10 -3 94.50 5.50 5 -10 -2 20.40 0.90 5 -10 -1 4.40 0.30 5 -10 0 0.90 0.30 5 -10 3 27.90 2.40 5 -10 4 48.40 2.40 5 -10 5 58.20 3.50 5 -10 6 70.40 5.90 5 -10 7 23.90 2.30 5 -10 9 35.90 3.30 5 -9 -9 33.60 1.80 5 -9 -8 108.40 4.50 5 -9 -7 24.80 1.10 5 -9 -6 51.40 2.20 5 -9 -5 98.60 4.10 5 -9 -4 69.20 4.00 5 -9 -3 58.60 2.40 5 -9 0 43.10 3.60 5 -9 1 42.10 3.50 5 -9 5 76.60 6.40 5 -9 7 2.10 0.50 5 -9 8 2.70 0.50 5 -9 10 66.30 5.70 5 -8 -10 47.00 2.10 5 -8 -8 79.80 3.90 5 -8 -7 14.00 0.70 5 -8 -6 28.30 1.30 5 -8 -5 127.60 6.10 5 -8 -2 107.90 8.80 5 -8 -1 8.80 0.90 5 -8 7 10.40 0.60 5 -8 8 40.30 2.00 5 -8 9 3.40 0.50 5 -8 11 19.60 1.40 5 -7 -11 45.00 2.00 5 -7 -9 30.00 1.40 5 -7 -8 12.10 0.70 5 -7 -4 46.90 2.80 5 -7 8 89.80 3.70 5 -7 9 17.00 1.20 5 -7 10 17.50 1.20 5 -7 12 7.70 1.00 5 -6 -12 14.30 0.80 5 -6 -11 18.10 0.90 5 -6 -10 95.40 4.00 5 -6 -9 2.30 0.30 5 -6 -8 27.90 2.70 5 -6 -7 222.40 12.70 5 -6 -6 48.00 2.80 5 -6 10 24.90 2.40 5 -6 12 15.80 1.70 5 -5 -13 4.30 0.50 5 -5 -12 8.00 0.80 5 -5 -11 6.90 0.50 5 -5 -10 159.10 6.50 5 -5 -9 63.30 3.70 5 -5 -8 46.80 2.80 5 -5 -7 103.90 6.00 5 -5 -6 73.80 6.10 5 -5 7 53.00 4.40 5 -5 9 41.70 2.50 5 -5 10 33.00 1.70 5 -5 11 41.00 3.70 5 -5 12 76.50 6.50 5 -4 -13 27.50 1.30 5 -4 -11 22.10 1.00 5 -4 -10 126.70 5.20 5 -4 -9 283.60 13.30 5 -4 -8 73.30 4.30 5 -4 -7 1.70 0.40 5 -4 9 19.30 1.80 5 -4 10 60.20 3.00 5 -4 11 30.20 2.70 5 -3 -14 8.40 0.70 5 -3 -13 65.30 3.20 5 -3 -12 24.10 1.10 5 -3 -11 10.30 0.60 5 -3 -10 2.60 0.50 5 -3 -9 71.50 3.40 5 -3 -8 107.50 6.20 5 -3 9 119.60 9.80 5 -3 10 24.70 1.20 5 -3 11 23.50 2.20 5 -2 -14 2.50 0.40 5 -2 -13 11.90 0.70 5 -2 -12 21.80 1.00 5 -2 -11 111.50 4.60 5 -2 -10 7.00 0.90 5 -2 -9 83.40 4.90 5 -2 9 25.20 2.30 5 -2 10 10.20 0.80 5 -2 11 96.50 8.00 5 -2 12 4.60 0.60 5 -1 -14 7.60 0.60 5 -1 -13 20.10 1.40 5 -1 -12 2.10 0.40 5 -1 -11 37.10 1.60 5 -1 -10 80.10 3.90 5 -1 -9 118.40 5.60 5 -1 7 24.00 2.10 5 -1 9 56.80 3.40 5 -1 10 19.70 1.90 5 -1 12 42.60 3.70 5 0 -14 38.90 1.70 5 0 -13 1.60 0.50 5 0 -12 4.60 0.40 5 0 -11 164.00 6.70 5 0 -10 156.10 7.40 5 0 -9 34.10 2.10 5 0 8 28.20 1.80 5 0 9 14.00 0.80 5 0 10 18.20 1.20 5 0 11 6.00 1.00 5 0 12 10.10 0.90 5 1 -14 11.20 0.70 5 1 -13 55.10 2.40 5 1 -12 37.00 1.90 5 1 -11 25.10 1.20 5 1 -10 44.50 2.70 5 1 -9 34.70 2.10 5 1 -8 5.90 0.50 5 1 -7 99.80 8.10 5 1 9 38.50 2.00 5 1 10 8.30 1.20 5 1 11 18.90 1.30 5 2 -14 38.80 1.70 5 2 -13 39.40 1.70 5 2 -12 14.80 0.80 5 2 -11 13.30 0.70 5 2 -10 19.90 1.10 5 2 -9 55.60 2.70 5 2 -8 79.70 4.60 5 2 -6 43.30 3.60 5 2 7 106.20 6.20 5 2 8 2.20 0.40 5 2 9 73.60 4.30 5 2 10 20.50 1.90 5 2 11 1.20 0.50 5 3 -14 22.90 1.10 5 3 -13 43.20 1.90 5 3 -12 43.70 2.60 5 3 -11 31.10 1.40 5 3 -10 39.70 1.70 5 3 -9 10.40 1.10 5 3 -8 11.70 0.70 5 3 -7 135.90 7.80 5 3 -5 229.40 18.50 5 3 3 116.60 6.70 5 3 6 0.70 0.40 5 3 7 24.60 1.30 5 3 8 11.30 0.70 5 3 10 11.60 1.20 5 4 -13 22.10 1.10 5 4 -12 11.10 0.60 5 4 -11 16.70 0.80 5 4 -10 12.60 0.70 5 4 -9 114.20 4.70 5 4 -8 26.00 2.30 5 4 -7 12.10 0.70 5 4 -6 87.70 5.10 5 4 -5 22.80 1.40 5 4 -2 7.60 0.80 5 4 0 37.00 2.20 5 4 1 30.70 2.60 5 4 4 204.40 9.60 5 4 5 3.20 0.40 5 4 6 26.60 1.40 5 4 7 29.50 1.50 5 4 9 16.40 1.20 5 5 -13 16.80 0.90 5 5 -12 0.50 0.30 5 5 -11 75.80 3.70 5 5 -10 1.20 0.40 5 5 -9 28.90 1.30 5 5 -8 159.40 6.50 5 5 -7 16.00 0.90 5 5 -6 157.90 12.80 5 5 -5 125.80 5.90 5 5 -4 33.60 1.70 5 5 -3 106.80 6.20 5 5 -2 12.80 0.90 5 5 -1 141.10 11.50 5 5 0 9.30 0.70 5 5 1 15.80 1.00 5 5 2 20.70 1.30 5 5 3 61.90 3.60 5 5 4 95.20 3.90 5 5 5 3.80 0.30 5 5 6 20.10 1.30 5 5 7 7.10 0.60 5 5 8 28.80 1.30 5 6 -12 35.70 1.90 5 6 -11 59.10 2.50 5 6 -10 54.90 2.40 5 6 -9 78.60 3.30 5 6 -8 15.90 0.80 5 6 -7 11.80 0.60 5 6 -6 41.90 1.80 5 6 -5 39.20 1.70 5 6 -4 23.80 1.10 5 6 -3 31.80 2.00 5 6 -2 61.50 3.60 5 6 -1 17.50 1.10 5 6 0 71.30 3.00 5 6 1 30.10 1.30 5 6 2 21.50 1.00 5 6 3 74.30 3.10 5 6 4 53.50 2.30 5 6 6 15.80 1.10 5 7 -11 48.20 3.00 5 7 -10 12.30 0.70 5 7 -9 17.00 1.00 5 7 -8 29.00 1.60 5 7 -7 18.60 0.90 5 7 -6 2.00 0.30 5 7 -5 16.80 0.90 5 7 -4 36.80 1.60 5 7 -3 24.20 1.10 5 7 -2 37.40 1.60 5 7 -1 19.90 0.90 5 7 0 4.70 0.40 5 7 1 25.90 1.30 5 7 2 29.90 1.30 5 7 3 24.70 1.50 5 7 4 9.60 0.70 5 7 5 34.10 1.80 5 8 -9 20.50 1.00 5 8 -8 35.20 1.60 5 8 -7 25.00 1.20 5 8 -6 61.50 3.00 5 8 -5 4.80 0.50 5 8 -4 41.20 1.80 5 8 -3 16.00 1.10 5 8 -2 8.40 0.70 5 8 -1 8.90 0.50 5 8 0 2.10 0.40 5 8 1 41.60 1.80 5 8 2 50.30 2.50 5 8 3 5.60 0.60 5 9 -5 67.30 2.80 5 9 -4 58.60 2.50 5 9 -3 24.40 1.10 5 9 -2 14.30 0.70 5 9 -1 3.30 0.30 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 63292 # start Validation Reply Form _vrf_PLAT029_pentapeptide ; PROBLEM: _diffrn_measured_fraction_theta_full Low ....... 0.898 Note RESPONSE: hese very weakly diffracting peptide crystals required very strong beam intensity and were collected on a single phi axis goniostat at ESRF station ISD29; ; # end Validation Reply Form