data_lp_mjy-zh_160822 _audit_creation_date 2016-09-12 _audit_creation_method ; Olex2 1.2 (compiled 2016.08.25 svn.r3337 for OlexSys, GUI svn.r5221) ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Bourhis, L.J., Dolomanov, O.V., Gildea, R.J., Howard, J.A.K., Puschmann, H. (2015). Acta Cryst. A71, 59-75. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_formula_moiety 'C21 H32 N2 O' _chemical_formula_sum 'C21 H32 N2 O' _chemical_formula_weight 328.50 _chemical_absolute_configuration unk loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.01920 0.00962 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.05239 0.03377 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.03256 0.01839 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' _space_group_crystal_system 'orthorhombic' _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall ' P 2ac 2ab' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y+1/2,-z 3 -x,y+1/2,-z+1/2 4 -x+1/2,-y,z+1/2 _symmetry_Int_Tables_number 19 _cell_length_a 7.45094(6) _cell_length_b 9.21543(8) _cell_length_c 26.7264(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1835.14(3) _cell_formula_units_Z 4 _cell_measurement_temperature 103(2) _cell_measurement_reflns_used 12690 _cell_measurement_theta_max 72.2590 _cell_measurement_theta_min 3.2990 _exptl_absorpt_coefficient_mu 0.558 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.20605 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.1889 _exptl_crystal_F_000 721.9652 _exptl_crystal_description 'block' _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.2 _diffrn_reflns_av_R_equivalents 0.0278 _diffrn_reflns_av_unetI/netI 0.0238 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 13373 _diffrn_reflns_theta_full 72.2345 _diffrn_reflns_theta_max 72.23 _diffrn_reflns_theta_min 3.31 _diffrn_ambient_temperature 103(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.2417 _diffrn_detector_type Onyx _diffrn_measured_fraction_theta_full 0.9846 _diffrn_measured_fraction_theta_max 0.9846 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -126.00 -79.00 1.00 3.00 -- -44.40 -99.00 -90.00 47 2 \w -126.00 -79.00 1.00 3.00 -- -44.40 -99.00 0.00 47 3 \w 19.00 114.00 1.00 3.00 -- 44.40 57.00 -60.00 95 4 \w 73.00 118.00 1.00 3.00 -- 44.40 125.00 30.00 45 5 \w 73.00 118.00 1.00 3.00 -- 44.40 125.00 60.00 45 6 \w 76.00 171.00 1.00 8.00 -- 100.00 45.00-150.00 95 7 \w 68.00 174.00 1.00 8.00 -- 100.00 77.00-120.00 106 8 \w 17.00 109.00 1.00 8.00 -- 100.00 -94.00 120.00 92 9 \w 68.00 174.00 1.00 8.00 -- 100.00 77.00 -60.00 106 10 \w 17.00 109.00 1.00 8.00 -- 100.00 -94.00 -60.00 92 11 \w 73.00 173.00 1.00 8.00 -- 100.00 30.00 -60.00 100 12 \w 26.00 121.00 1.00 8.00 -- 100.00-125.00 -90.00 95 13 \w 29.00 124.00 1.00 8.00 -- 100.00 -45.00-150.00 95 14 \w 78.00 173.00 1.00 8.00 -- 100.00 30.00 120.00 95 15 \w 78.00 140.00 1.00 8.00 -- 100.00 45.00-180.00 62 16 \w 58.00 84.00 1.00 8.00 -- 100.00 -94.00 30.00 26 17 \w 26.00 120.00 1.00 8.00 -- 100.00-125.00 -60.00 94 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Onyx, Nova' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.1588724000 _diffrn_orient_matrix_UB_12 0.0818785000 _diffrn_orient_matrix_UB_13 -0.0237385000 _diffrn_orient_matrix_UB_21 -0.1241156000 _diffrn_orient_matrix_UB_22 -0.0547941000 _diffrn_orient_matrix_UB_23 0.0420427000 _diffrn_orient_matrix_UB_31 0.0459392000 _diffrn_orient_matrix_UB_32 0.1350158000 _diffrn_orient_matrix_UB_33 0.0315012000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'Nova (Cu) X-ray Source' _reflns_Friedel_coverage 0.982 _reflns_limit_h_max 9 _reflns_limit_h_min -9 _reflns_limit_k_max 11 _reflns_limit_k_min -11 _reflns_limit_l_max 32 _reflns_limit_l_min -32 _reflns_number_gt 3563 _reflns_number_total 3577 _reflns_odcompleteness_completeness 98.60 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 71.98 _reflns_threshold_expression I>=2u(I) _computing_cell_refinement 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'XS (Sheldrick, 2008)' _refine_diff_density_max 0.2391 _refine_diff_density_min -0.1393 _refine_diff_density_rms 0.0355 _refine_ls_abs_structure_details 'Flack, H. D. (1983). Acta Cryst. A39, 876-881.' _refine_ls_abs_structure_Flack 0.2(2) _refine_ls_d_res_high 0.8095 _refine_ls_d_res_low 13.3632 _refine_ls_goodness_of_fit_ref 1.0500 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 49 _refine_ls_number_parameters 221 _refine_ls_number_reflns 3577 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0302 _refine_ls_R_factor_gt 0.0298 _refine_ls_restrained_S_all 1.0500 _refine_ls_shift/su_max 0.0003 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0375P)^2^+0.3990P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0737 _refine_ls_wR_factor_ref 0.0738 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C2(H2), C8(H8) 2.b Secondary CH2 refined with riding coordinates: C6(H6a,H6b), C9(H9a,H9b), C10(H10a,H10b), C14(H14a,H14b), C15(H15a,H15b), C17(H17a,H17b), C20(H20a,H20b) 2.c Aromatic/amide H refined with riding coordinates: N3(H3), C13(H13), C24(H24) 2.d Idealised Me refined as rotating group: C5(H5a,H5b,H5c), C18(H18a,H18b,H18c), C22(H22a,H22b,H22c), C23(H23a,H23b,H23c) 2.e Idealised tetrahedral OH refined as rotating group: O1(H1) ; _atom_sites_solution_primary direct loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn O1 O 0.14204(11) 0.93989(8) 0.06460(3) 0.02141(18) Uani 1.000000 . C2 C 0.30724(15) 0.84477(11) 0.15327(4) 0.0152(2) Uani 1.000000 . N3 N -0.11330(14) 1.64152(11) 0.05169(4) 0.0228(2) Uani 1.000000 . N4 N 0.33679(14) 1.59990(12) 0.01843(4) 0.0284(2) Uani 1.000000 . C5 C 0.22107(15) 1.08762(12) 0.19487(4) 0.0186(2) Uani 1.000000 . C6 C 0.49999(14) 0.89535(13) 0.14440(4) 0.0194(2) Uani 1.000000 . C7 C 0.17567(14) 0.97745(11) 0.15342(4) 0.0142(2) Uani 1.000000 . C8 C 0.38586(15) 1.09864(12) 0.08873(4) 0.0189(2) Uani 1.000000 . C9 C -0.03478(16) 0.82261(13) 0.20735(4) 0.0217(2) Uani 1.000000 . C10 C -0.01736(14) 0.92216(13) 0.16186(4) 0.0190(2) Uani 1.000000 . C11 C -0.01713(15) 1.44543(12) 0.09367(4) 0.0180(2) Uani 1.000000 . C12 C 0.19005(15) 1.05190(12) 0.10022(4) 0.0161(2) Uani 1.000000 . C13 C -0.25604(16) 1.58657(14) 0.07614(5) 0.0260(3) Uani 1.000000 . C14 C 0.05713(15) 1.17889(12) 0.09178(4) 0.0181(2) Uani 1.000000 . C15 C 0.10187(16) 1.32878(11) 0.11415(4) 0.0195(2) Uani 1.000000 . C16 C 0.28716(15) 0.73286(12) 0.19689(4) 0.0178(2) Uani 1.000000 . C17 C 0.51493(15) 0.97050(13) 0.09372(4) 0.0216(2) Uani 1.000000 . C18 C 0.36111(17) 0.78088(13) 0.24804(4) 0.0245(3) Uani 1.000000 . C19 C 0.20167(16) 1.58205(12) 0.03846(4) 0.0212(2) Uani 1.000000 . C20 C 0.08814(16) 0.69145(12) 0.20186(4) 0.0205(2) Uani 1.000000 . C21 C 0.03415(15) 1.55713(12) 0.06187(4) 0.0188(2) Uani 1.000000 . C22 C 0.40639(18) 1.16913(14) 0.03704(5) 0.0264(3) Uani 1.000000 . C23 C 0.39058(17) 0.59412(13) 0.18244(4) 0.0238(2) Uani 1.000000 . C24 C -0.20197(16) 1.46594(13) 0.10242(5) 0.0232(2) Uani 1.000000 . H1 H 0.0766(17) 0.9744(4) 0.0430(3) 0.0321(3) Uiso 1.000000 GR H2 H 0.27581(15) 0.79018(11) 0.12305(4) 0.0182(3) Uiso 1.000000 R H3 H -0.11433(14) 1.71707(11) 0.03280(4) 0.0273(3) Uiso 1.000000 R H5a H 0.2383(12) 1.03731(16) 0.22595(8) 0.0279(3) Uiso 1.000000 GR H5b H 0.3290(7) 1.1386(7) 0.18621(17) 0.0279(3) Uiso 1.000000 GR H5c H 0.1242(6) 1.1556(6) 0.1983(2) 0.0279(3) Uiso 1.000000 GR H6a H 0.53533(14) 0.96205(13) 0.17069(4) 0.0233(3) Uiso 1.000000 R H6b H 0.58033(14) 0.81258(13) 0.14537(4) 0.0233(3) Uiso 1.000000 R H8 H 0.42044(15) 1.17105(12) 0.11379(4) 0.0227(3) Uiso 1.000000 R H9a H -0.00326(16) 0.87578(13) 0.23741(4) 0.0260(3) Uiso 1.000000 R H9b H -0.15815(16) 0.79033(13) 0.21056(4) 0.0260(3) Uiso 1.000000 R H10a H -0.09645(14) 1.00482(13) 0.16620(4) 0.0228(3) Uiso 1.000000 R H10b H -0.05642(14) 0.86992(13) 0.13229(4) 0.0228(3) Uiso 1.000000 R H13 H -0.37192(16) 1.62401(14) 0.07538(5) 0.0312(3) Uiso 1.000000 R H14a H 0.04266(15) 1.19114(12) 0.05596(4) 0.0217(3) Uiso 1.000000 R H14b H -0.05849(15) 1.14933(12) 0.10498(4) 0.0217(3) Uiso 1.000000 R H15a H 0.22598(16) 1.35244(11) 0.10683(4) 0.0234(3) Uiso 1.000000 R H15b H 0.08842(16) 1.32480(11) 0.15022(4) 0.0234(3) Uiso 1.000000 R H17a H 0.63694(15) 1.00475(13) 0.08918(4) 0.0260(3) Uiso 1.000000 R H17b H 0.48976(15) 0.90073(13) 0.06747(4) 0.0260(3) Uiso 1.000000 R H18a H 0.4793(6) 0.8205(10) 0.24382(7) 0.0368(4) Uiso 1.000000 GR H18b H 0.2836(7) 0.8534(8) 0.26214(17) 0.0368(4) Uiso 1.000000 GR H18c H 0.3665(12) 0.6987(3) 0.27008(12) 0.0368(4) Uiso 1.000000 GR H20a H 0.07341(16) 0.62910(12) 0.23081(4) 0.0246(3) Uiso 1.000000 R H20b H 0.05228(16) 0.63667(12) 0.17252(4) 0.0246(3) Uiso 1.000000 R H22a H 0.3606(13) 1.1047(5) 0.01188(6) 0.0396(4) Uiso 1.000000 GR H22b H 0.3405(12) 1.2586(6) 0.03622(13) 0.0396(4) Uiso 1.000000 GR H22c H 0.5310(2) 1.1882(10) 0.03069(17) 0.0396(4) Uiso 1.000000 GR H23a H 0.3624(10) 0.5682(6) 0.14854(12) 0.0357(4) Uiso 1.000000 GR H23b H 0.51720(17) 0.6114(3) 0.1854(3) 0.0357(4) Uiso 1.000000 GR H23c H 0.3565(9) 0.5164(3) 0.2044(2) 0.0357(4) Uiso 1.000000 GR H24 H -0.27464(16) 1.40803(13) 0.12246(5) 0.0278(3) Uiso 1.000000 R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0297(4) 0.0170(4) 0.0176(4) 0.0014(3) -0.0071(3) -0.0023(3) C2 0.0155(5) 0.0147(5) 0.0154(5) 0.0010(4) -0.0012(4) -0.0001(4) N3 0.0254(5) 0.0168(4) 0.0261(5) 0.0037(4) -0.0036(4) 0.0038(4) N4 0.0266(5) 0.0286(5) 0.0301(5) -0.0031(4) 0.0028(4) 0.0075(5) C5 0.0233(5) 0.0182(5) 0.0142(5) 0.0018(4) -0.0000(4) -0.0007(4) C6 0.0141(5) 0.0203(5) 0.0239(5) 0.0014(4) 0.0006(4) 0.0013(4) C7 0.0128(5) 0.0150(5) 0.0149(5) 0.0000(4) -0.0004(4) 0.0005(4) C8 0.0202(5) 0.0184(5) 0.0181(5) -0.0011(5) 0.0039(4) 0.0006(4) C9 0.0170(5) 0.0239(6) 0.0240(5) -0.0012(5) 0.0032(4) 0.0046(5) C10 0.0135(5) 0.0203(5) 0.0233(5) 0.0005(4) 0.0001(4) 0.0036(4) C11 0.0213(5) 0.0159(5) 0.0168(5) 0.0002(4) -0.0006(4) -0.0021(4) C12 0.0183(5) 0.0145(5) 0.0154(5) -0.0004(4) -0.0015(4) -0.0011(4) C13 0.0204(5) 0.0241(6) 0.0335(7) 0.0045(5) -0.0002(5) -0.0021(5) C14 0.0180(5) 0.0176(5) 0.0188(5) 0.0000(4) -0.0030(4) 0.0025(4) C15 0.0231(5) 0.0160(5) 0.0195(5) 0.0010(4) -0.0026(4) 0.0013(4) C16 0.0181(5) 0.0167(5) 0.0184(5) 0.0020(4) -0.0015(4) 0.0028(4) C17 0.0172(5) 0.0225(5) 0.0252(6) 0.0012(5) 0.0062(4) 0.0006(5) C18 0.0295(6) 0.0242(6) 0.0198(5) 0.0012(5) -0.0065(5) 0.0032(5) C19 0.0256(6) 0.0169(5) 0.0210(5) -0.0011(5) -0.0036(5) 0.0024(4) C20 0.0216(6) 0.0188(5) 0.0210(5) -0.0020(4) 0.0017(4) 0.0045(4) C21 0.0207(5) 0.0163(5) 0.0195(5) 0.0009(4) -0.0017(4) -0.0009(4) C22 0.0319(6) 0.0238(6) 0.0235(6) 0.0016(5) 0.0092(5) 0.0045(5) C23 0.0251(6) 0.0184(5) 0.0280(6) 0.0033(5) -0.0007(5) 0.0024(5) C24 0.0219(6) 0.0211(5) 0.0266(6) -0.0001(5) 0.0046(5) -0.0003(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C12 1.4491(13) . ? O1 H1 0.8200 . ? C2 C6 1.5285(15) . ? C2 C7 1.5672(14) . ? C2 C16 1.5636(15) . ? C2 H2 0.9800 . ? N3 C13 1.3471(17) . ? N3 C21 1.3732(15) . ? N3 H3 0.8600 . ? N4 C19 1.1522(17) . ? C5 C7 1.5403(15) . ? C5 H5a 0.9600 . ? C5 H5b 0.9600 . ? C5 H5c 0.9600 . ? C6 C17 1.5252(15) . ? C6 H6a 0.9700 . ? C6 H6b 0.9700 . ? C7 C10 1.5424(14) . ? C7 C12 1.5825(14) . ? C8 C12 1.5519(15) . ? C8 C17 1.5288(16) . ? C8 C22 1.5342(15) . ? C8 H8 0.9800 . ? C9 C10 1.5286(15) . ? C9 C20 1.5235(16) . ? C9 H9a 0.9700 . ? C9 H9b 0.9700 . ? C10 H10a 0.9700 . ? C10 H10b 0.9700 . ? C11 C15 1.4972(15) . ? C11 C21 1.3884(16) . ? C11 C24 1.4097(16) . ? C12 C14 1.5496(15) . ? C13 C24 1.3753(18) . ? C13 H13 0.9300 . ? C14 C15 1.5417(15) . ? C14 H14a 0.9700 . ? C14 H14b 0.9700 . ? C15 H15a 0.9700 . ? C15 H15b 0.9700 . ? C16 C18 1.5391(16) . ? C16 C20 1.5370(16) . ? C16 C23 1.5419(15) . ? C17 H17a 0.9700 . ? C17 H17b 0.9700 . ? C18 H18a 0.9600 . ? C18 H18b 0.9600 . ? C18 H18c 0.9600 . ? C19 C21 1.4149(17) . ? C20 H20a 0.9700 . ? C20 H20b 0.9700 . ? C22 H22a 0.9600 . ? C22 H22b 0.9600 . ? C22 H22c 0.9600 . ? C23 H23a 0.9600 . ? C23 H23b 0.9600 . ? C23 H23c 0.9600 . ? C24 H24 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1 O1 C12 109.5 . . ? C7 C2 C6 110.50(9) . . ? C16 C2 C6 114.00(9) . . ? C16 C2 C7 116.93(9) . . ? H2 C2 C6 104.66(6) . . ? H2 C2 C7 104.66(5) . . ? H2 C2 C16 104.66(6) . . ? C21 N3 C13 108.83(9) . . ? H3 N3 C13 125.59(7) . . ? H3 N3 C21 125.59(6) . . ? H5a C5 C7 109.5 . . ? H5b C5 C7 109.5 . . ? H5b C5 H5a 109.5 . . ? H5c C5 C7 109.5 . . ? H5c C5 H5a 109.5 . . ? H5c C5 H5b 109.5 . . ? C17 C6 C2 110.17(9) . . ? H6a C6 C2 109.62(6) . . ? H6a C6 C17 109.62(6) . . ? H6b C6 C2 109.62(6) . . ? H6b C6 C17 109.62(6) . . ? H6b C6 H6a 108.1 . . ? C5 C7 C2 112.26(9) . . ? C10 C7 C2 109.02(9) . . ? C10 C7 C5 108.50(9) . . ? C12 C7 C2 107.08(8) . . ? C12 C7 C5 110.22(8) . . ? C12 C7 C10 109.74(8) . . ? C17 C8 C12 111.08(9) . . ? C22 C8 C12 112.92(10) . . ? C22 C8 C17 110.05(9) . . ? H8 C8 C12 107.52(6) . . ? H8 C8 C17 107.52(6) . . ? H8 C8 C22 107.52(6) . . ? C20 C9 C10 110.40(9) . . ? H9a C9 C10 109.57(6) . . ? H9a C9 C20 109.57(6) . . ? H9b C9 C10 109.57(6) . . ? H9b C9 C20 109.57(6) . . ? H9b C9 H9a 108.1 . . ? C9 C10 C7 113.18(9) . . ? H10a C10 C7 108.94(6) . . ? H10a C10 C9 108.94(6) . . ? H10b C10 C7 108.94(6) . . ? H10b C10 C9 108.94(6) . . ? H10b C10 H10a 107.8 . . ? C21 C11 C15 126.38(10) . . ? C24 C11 C15 127.89(11) . . ? C24 C11 C21 105.73(10) . . ? C7 C12 O1 105.35(8) . . ? C8 C12 O1 107.45(9) . . ? C8 C12 C7 111.21(8) . . ? C14 C12 O1 106.53(8) . . ? C14 C12 C7 114.52(9) . . ? C14 C12 C8 111.25(9) . . ? C24 C13 N3 108.68(10) . . ? H13 C13 N3 125.66(7) . . ? H13 C13 C24 125.66(7) . . ? C15 C14 C12 118.81(9) . . ? H14a C14 C12 107.61(6) . . ? H14a C14 C15 107.61(6) . . ? H14b C14 C12 107.61(6) . . ? H14b C14 C15 107.61(6) . . ? H14b C14 H14a 107.0 . . ? C14 C15 C11 111.92(9) . . ? H15a C15 C11 109.23(6) . . ? H15a C15 C14 109.23(6) . . ? H15b C15 C11 109.23(6) . . ? H15b C15 C14 109.23(6) . . ? H15b C15 H15a 107.9 . . ? C18 C16 C2 116.00(9) . . ? C20 C16 C2 108.69(9) . . ? C20 C16 C18 109.88(9) . . ? C23 C16 C2 108.20(9) . . ? C23 C16 C18 106.38(9) . . ? C23 C16 C20 107.34(9) . . ? C8 C17 C6 112.48(9) . . ? H17a C17 C6 109.10(6) . . ? H17a C17 C8 109.10(6) . . ? H17b C17 C6 109.10(6) . . ? H17b C17 C8 109.10(6) . . ? H17b C17 H17a 107.8 . . ? H18a C18 C16 109.5 . . ? H18b C18 C16 109.5 . . ? H18b C18 H18a 109.5 . . ? H18c C18 C16 109.5 . . ? H18c C18 H18a 109.5 . . ? H18c C18 H18b 109.5 . . ? C21 C19 N4 178.22(13) . . ? C16 C20 C9 113.04(9) . . ? H20a C20 C9 108.97(6) . . ? H20a C20 C16 108.97(6) . . ? H20b C20 C9 108.97(6) . . ? H20b C20 C16 108.97(6) . . ? H20b C20 H20a 107.8 . . ? C11 C21 N3 108.72(10) . . ? C19 C21 N3 121.75(10) . . ? C19 C21 C11 129.33(10) . . ? H22a C22 C8 109.5 . . ? H22b C22 C8 109.5 . . ? H22b C22 H22a 109.5 . . ? H22c C22 C8 109.5 . . ? H22c C22 H22a 109.5 . . ? H22c C22 H22b 109.5 . . ? H23a C23 C16 109.5 . . ? H23b C23 C16 109.5 . . ? H23b C23 H23a 109.5 . . ? H23c C23 C16 109.5 . . ? H23c C23 H23a 109.5 . . ? H23c C23 H23b 109.5 . . ? C13 C24 C11 108.05(11) . . ? H24 C24 C11 125.98(7) . . ? H24 C24 C13 125.98(7) . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 0 2 199417 1134.8 2 0 0 3 239.196 25.9198 1 0 0 3 315.707 44.7515 3 0 0 5 396.232 40.8925 1 0 0 5 256.253 60.2334 3 0 0 5 186.503 64.6557 2 0 0 7 263.943 41.0078 1 0 0 7 133.894 59.91 3 0 0 9 273.175 100.866 2 0 0 9 276.87 85.4063 3 0 0 10 88083.9 1339.85 3 0 0 10 89793.9 1523.02 2 0 0 11 213.748 84.4742 3 0 0 11 48.4904 84.9834 2 0 0 12 47861.1 1244.8 2 0 0 12 48529.9 1110.3 3 0 0 13 20.8602 65.1706 2 0 0 13 242.037 93.4166 3 0 0 14 73989.6 1704.41 2 0 0 14 70657.4 1493.5 3 0 0 15 5.71972 71.639 2 0 0 16 199395 3020.65 2 0 0 17 80.8091 88.4881 2 0 0 17 101.147 80.719 7 0 0 18 125014 2592.84 2 0 0 18 131208 1757.4 7 0 0 18 129024 1699.92 8 0 0 19 944.068 159.158 8 0 0 19 195.25 92.6375 7 0 0 20 737590 4352.39 8 0 0 20 744526 4509.48 7 0 0 21 1091.12 197.147 7 0 0 21 1027 182.469 8 0 0 22 60892.2 1327.08 8 0 0 22 63743.6 1390.73 7 0 0 23 43.4492 63.448 8 0 0 23 154.235 111.598 7 0 0 24 28978.5 948.394 8 0 0 24 30367.4 1002.58 7 0 0 25 49.9571 85.9652 7 0 0 25 -9.26188 71.0011 8 0 0 26 3260.36 324.304 8 0 0 26 3039.16 319.972 7 0 0 27 1987.94 259.261 7 0 0 27 57.7846 80.7708 8 0 0 28 25233.3 869.401 7 0 0 28 25259 851.767 8 0 0 29 119.179 82.1219 8 0 0 29 0.93168 71.164 7 0 0 30 9927.47 481.976 8 0 0 30 10014.3 496.006 7 0 0 31 105.147 76.5003 7 0 0 31 57.2152 59.648 8 0 0 32 53975.9 917.627 8 0 1 0 60.8197 30.8168 5 0 -1 0 173.337 34.609 3 0 -1 6 358033 2366.88 3 0 -1 7 43764.9 877.92 3 0 -1 7 47201.3 1330.16 2 0 -1 8 3140.27 108.392 1 0 -1 8 2852.6 330.895 2 0 -1 9 845104 5528.09 2 0 -1 10 152942 1910.63 3 0 1 10 148807 1959.73 2 0 -1 11 266418 3132.13 2 0 -1 11 247781 2548.61 3 0 -1 12 231457 2609.15 3 0 -1 12 249321 3089.72 2 0 -1 13 94756.8 1737.22 3 0 -1 13 98319 1997.8 2 0 -1 14 217748 3046.86 2 0 -1 14 205040 2688.77 3 0 -1 15 482314 4302.98 3 0 -1 15 497708 4696.07 2 0 -1 16 59888.9 1704.37 2 0 1 16 62602.1 1151.41 7 0 -1 16 59004 1570.51 3 0 1 16 61903.1 1125.87 8 0 -1 17 4628.35 314.945 7 0 -1 17 4329.55 289.194 11 0 1 17 4402.16 320.97 7 0 -1 17 4379.25 478.673 2 0 1 17 4855.93 330.066 8 0 -1 17 4735.88 464.336 3 0 -1 18 204772 2167.37 7 0 -1 18 200099 1976.78 11 0 1 18 202488 2193.1 8 0 -1 18 200435 3316.01 2 0 1 18 200225 2233.95 7 0 -1 19 16794.4 595.269 11 0 1 19 14853.1 629.259 7 0 1 19 14537.6 614.916 8 0 -1 19 16812.6 646.279 7 0 -1 19 14547.6 547.918 9 0 -1 19 15950.5 973.589 2 0 -1 19 15635 598.653 8 0 1 20 446.244 126.427 8 0 -1 20 1263.43 195.104 7 0 -1 20 1283.32 175.589 11 0 -1 20 453.176 172.594 2 0 1 20 849.622 165.778 7 0 -1 20 602.403 131.383 8 0 1 21 11740.6 591.672 7 0 -1 21 11536.5 545.798 8 0 -1 21 10884.3 851.733 2 0 -1 21 11625.5 514.328 11 0 1 21 11522.1 582.563 8 0 -1 21 11941.4 583.921 7 0 -1 22 19942.3 1174.78 2 0 1 22 17523.6 738.583 8 0 -1 22 20316.7 777.813 7 0 1 22 17606 744.576 7 0 -1 22 19258.2 728.202 8 0 -1 22 18205.2 652.589 11 0 -1 23 90115.4 1656.15 7 0 -1 23 86673.2 1436.21 11 0 1 23 84617.4 1647.46 8 0 1 23 86115.7 1670.78 7 0 -1 23 86214.9 1566.02 8 0 -1 24 15935.7 683.695 8 0 1 24 17662.6 760.677 8 0 -1 24 17306.9 644.16 11 0 -1 24 16797.8 724.185 7 0 1 24 17372.1 763.736 7 0 -1 25 4971.66 399.414 7 0 1 25 5081.49 418.216 7 0 1 25 4796.92 403.909 8 0 -1 25 4904.71 341.31 11 0 -1 25 4591.02 372.52 8 0 -1 26 4439.4 379.336 7 0 1 26 4729.23 401.044 7 0 -1 26 4491.01 365.61 8 0 -1 26 4596.05 321.919 11 0 1 26 4327.37 378.949 8 0 1 27 7822.14 505.783 7 0 -1 27 8598.54 513.211 7 0 1 27 8531.13 522.78 8 0 -1 27 8184.76 477.758 8 0 1 28 2868.97 300.555 8 0 1 28 2468.34 282.679 7 0 -1 28 2591.01 282.354 7 0 -1 28 2198.2 244.678 8 0 1 29 976.058 177.519 8 0 -1 29 973.792 169.425 7 0 -1 29 850.406 147.679 8 0 1 29 855.525 167.531 7 0 1 30 38070.3 966.841 7 0 1 30 37216.2 950.557 8 0 -1 30 38955.8 955.548 7 0 -1 30 37326.7 880.136 8 0 1 31 14431.2 552.09 8 0 -1 31 13896.6 525.39 7 0 1 32 1480.14 166.528 8 0 -2 -1 2175.95 151.811 3 0 2 -1 2606.88 180.006 4 0 -2 1 2316.38 174.511 3 0 -2 3 280779 2081.86 3 0 2 -3 284413 1882.9 4 0 2 -6 184789 2044.25 4 0 -2 6 124018 1605.01 3 0 -2 8 151191 1963.88 3 0 -2 9 539158 3863.59 3 0 -2 10 101.467 81.7214 3 0 -2 10 317.573 193.585 2 0 -2 11 501959 4039.33 3 0 -2 11 538440 5558.61 2 0 -2 12 560307 4424.36 3 0 -2 12 590294 5795.96 2 0 -2 13 85668.9 1780.04 3 0 -2 13 89912.8 2222.37 2 0 -2 14 13934.7 870.611 2 0 -2 14 14189.3 751.748 3 0 -2 15 76945.3 2058.92 2 0 -2 15 71441.4 1764.59 3 0 2 15 75853.2 1264.95 8 0 2 16 115351 1618.35 8 0 2 16 118852 1644.6 7 0 -2 16 114182 2324.45 3 0 -2 16 119370 1545.58 11 0 -2 16 119302 1519.56 7 0 -2 16 120158 2598.9 2 0 2 17 56737.8 1182.46 8 0 -2 17 60335.1 1858.56 2 0 -2 17 59764.8 1114.63 11 0 -2 17 60205.4 1121.67 7 0 -2 17 58152.4 1725.34 3 0 -2 17 55436 1073.56 9 0 2 17 58131.9 1193.3 7 0 -2 18 77406.6 2152.44 2 0 2 18 76341.3 1417.75 7 0 -2 18 74593.3 1287.19 11 0 -2 18 74658.5 2018.17 3 0 -2 18 73667.1 1280.49 9 0 -2 18 79076.3 1342.12 7 0 2 18 76421.1 1419.3 8 0 -2 19 49162.5 1103.21 7 0 -2 19 49192.4 1760.58 2 0 -2 19 47759.6 1023.69 8 0 2 19 47066 1152.31 8 0 -2 19 48405.3 1679.65 3 0 2 19 48176.1 1166.53 7 0 -2 19 47326 1046.28 11 0 -2 19 48647.9 1054.92 9 0 -2 20 1293.49 281.404 3 0 -2 20 1234.36 182.718 7 0 -2 20 1300.28 287.344 2 0 -2 20 1376.81 182.564 8 0 2 20 1376.12 211.191 7 0 2 20 1168.08 198.455 8 0 -2 20 1317.75 184.151 11 0 -2 20 1056.98 166.088 9 0 2 21 147618 2175.07 8 0 -2 21 151330 1943.22 11 0 -2 21 152683 2054.02 7 0 -2 21 152451 1933.87 9 0 -2 21 152957 3268.8 2 0 -2 21 152216 1943.19 8 0 2 21 148767 2155.4 7 0 2 22 29781.5 995.46 8 0 -2 22 31393 880.81 9 0 -2 22 30728.4 886.1 11 0 -2 22 31421.4 1504.56 2 0 -2 22 30892 894.593 8 0 2 22 28986.6 982.875 7 0 -2 22 30591.8 938.024 7 0 -2 23 36188.1 978.512 8 0 -2 23 36290.8 1045.38 7 0 2 23 35766.9 1104.45 8 0 -2 23 38551.7 1685.48 2 0 -2 23 36330 968.471 11 0 2 23 36389.1 1114.1 7 0 -2 23 38145.6 964.624 9 0 -2 24 134732 1903.68 8 0 2 24 130605 2119.62 7 0 -2 24 133860 1850.07 11 0 2 24 129172 2106.7 8 0 -2 24 134582 2011.64 7 0 2 25 13471.7 683.249 8 0 -2 25 14635.5 626.624 8 0 -2 25 14643.8 661.693 7 0 2 25 13735.7 687.465 7 0 -2 25 15542 630.026 11 0 -2 26 15931.3 645.178 8 0 2 26 15020.2 707.201 7 0 2 26 15108.5 718.981 8 0 -2 26 16068.5 688.162 7 0 -2 26 14951.2 599.935 11 0 -2 27 23843.6 729.779 11 0 2 27 22865.9 848.64 7 0 -2 27 24071.6 821.418 7 0 2 27 23176.1 869.999 8 0 -2 27 24821.9 785.734 8 0 -2 28 1066.97 177.408 7 0 2 28 959.914 182.113 8 0 2 28 817.164 161.985 7 0 -2 28 1071.05 152.163 11 0 -2 28 1125.06 164.483 8 0 -2 29 9441.61 436.456 8 0 -2 29 9398.97 474.291 7 0 2 29 9773.2 516.783 8 0 2 29 9429.87 498.938 7 0 -2 30 16734.8 586.717 7 0 2 30 17641.9 652.946 8 0 -2 31 5497.73 305.542 7 0 2 31 6034.44 357.565 8 0 2 32 39226.8 808.512 8 0 3 0 405.055 129.964 5 0 -3 0 275.21 92.6254 3 0 -3 -2 2445.26 193.044 3 0 3 -2 2254.83 249.365 5 0 -3 2 2167.61 210.389 3 0 3 -3 293055 2912.38 5 0 3 -3 275208 2244.66 4 0 -3 3 287851 2486.24 3 0 -3 -3 273003 1986.48 3 0 3 -4 139.892 56.5687 4 0 -3 4 272.985 91.7154 3 0 3 -4 309.792 105.414 5 0 3 -5 17570.1 584.982 4 0 -3 5 18551.1 685.761 3 0 -3 -5 16272.5 473.62 3 0 3 -6 5761.02 345.216 4 0 -3 6 5774.28 398.703 3 0 -3 -6 5831.01 286.41 3 0 -3 7 148174 2097.7 3 0 3 -7 147786 1820.92 4 0 -3 8 17198.5 738.118 3 0 3 -8 20077.4 707.635 4 0 -3 10 26551.7 991.475 3 0 3 -10 32730.9 1003.94 4 0 -3 11 467904 4335.11 3 0 3 -11 593967 4468.52 4 0 3 -12 503.229 155.677 4 0 -3 12 507.418 164.618 3 0 -3 13 348665 5219.41 2 0 -3 13 336471 3873.39 3 0 -3 14 56889.3 1059.6 11 0 -3 14 56548.2 1632.53 3 0 -3 14 56426.9 2075.23 2 0 3 14 55410.3 1122.63 8 0 -3 15 5873.32 659.808 2 0 -3 15 5994.28 354.602 11 0 3 15 7058.02 409.328 7 0 3 15 6584.48 347.366 10 0 3 15 5359.21 363.615 8 0 -3 15 4994.44 328.289 9 0 -3 16 30903.7 1465.34 2 0 3 16 31154.7 885.696 7 0 3 16 29048.1 870.441 8 0 -3 16 30139.2 1284.12 3 0 -3 16 28409.6 750.921 7 0 -3 16 29688.3 813.574 11 0 3 16 29873.3 764.34 10 0 -3 16 29273.3 804.203 9 0 3 16 30513 674.57 12 0 -3 17 126559 1725.72 11 0 -3 17 127481 2975.35 2 0 3 17 129127 1635.73 10 0 -3 17 120224 1686.73 9 0 -3 17 123819 2677.41 3 0 3 17 122593 1853.06 8 0 -3 17 122060 1604.04 7 0 3 17 123480 1815.38 7 0 3 17 124283 1368.86 12 0 -3 18 64133.6 1253.78 11 0 -3 18 62427.1 1230.68 9 0 -3 18 65069.6 2125.31 2 0 -3 18 61200.4 1181.42 7 0 -3 18 66873.9 2034.28 3 0 3 18 65407.7 1373.86 7 0 3 18 64380.3 1381.59 8 0 3 19 4208.45 364.54 7 0 -3 19 5221.83 609.22 2 0 3 19 3954 356.78 8 0 -3 19 4288.9 540.075 3 0 -3 19 4690.05 340.495 7 0 -3 19 3883.22 322.055 9 0 -3 19 4648.69 347.74 11 0 3 20 55097.9 1328.77 7 0 -3 20 55948.8 1207.1 9 0 -3 20 60264.8 1155.55 8 0 -3 20 60272.3 2077.76 2 0 3 20 54492.6 1346.19 8 0 -3 20 58544.9 1222.06 7 0 -3 20 56792.3 1978.63 3 0 -3 20 57249.9 1232.45 11 0 -3 21 141771 1810.29 8 0 -3 21 137208 1925.91 11 0 -3 21 131462 1848.68 9 0 -3 21 135245 1901.43 7 0 3 21 134338 2108.78 7 0 -3 21 136153 3113.51 3 0 -3 21 142404 3209.03 2 0 3 21 131008 2122.39 8 0 -3 22 11351.1 545.539 9 0 -3 22 12298.5 582.999 7 0 -3 22 12143.9 954.641 2 0 -3 22 12403.3 546.201 8 0 3 22 11080.2 612.274 7 0 3 22 11873.4 652.376 8 0 -3 22 12340.7 586.703 11 0 -3 23 5265.35 383.619 11 0 3 23 4516.9 395.64 7 0 -3 23 5323.3 389.692 7 0 3 23 4799.89 419.651 8 0 -3 23 5006.34 362.382 9 0 3 24 4885.16 410.521 7 0 3 24 4460.88 405.674 8 0 -3 24 4510.75 353.406 11 0 -3 24 4531.22 358.077 7 0 -3 24 4922.74 353.913 9 0 3 25 20495.7 825.166 7 0 -3 25 21623.6 770.743 7 0 3 25 20087.8 842.986 8 0 -3 25 20588.7 687.951 9 0 -3 25 21002.2 743.011 11 0 3 26 2124.54 260.004 7 0 -3 26 1924.54 230.39 7 0 -3 26 2578.43 255.139 11 0 3 26 1829.48 262.027 8 0 -3 27 61424.8 1186.06 11 0 3 27 60368 1376.55 8 0 -3 27 61042.7 1223.07 7 0 -3 28 5030.21 337.746 7 0 3 28 5074.46 389.283 8 0 -3 28 4800.96 313.486 11 0 3 29 742.787 149.704 8 0 -3 29 651.767 116.817 11 0 -3 29 480.312 102.58 7 0 -3 30 1870.56 173.726 7 0 -3 30 1835.4 160.318 11 0 3 31 12061.3 473.822 8 0 -4 0 649524 3966.91 3 0 -4 1 10079.6 508.734 3 0 4 -1 9157.42 563.538 5 0 -4 -1 10392 487.221 3 0 -4 2 169455 2150.1 3 0 4 -2 165202 2436 5 0 -4 -2 166054 1887.69 3 0 -4 -3 218813 2129.36 3 0 -4 3 225306 2548.28 3 0 4 -3 223799 2910.02 5 0 4 -4 59.1753 63.6463 5 0 -4 -4 95.5062 51.8036 3 0 -4 -5 1619.3 173.598 3 0 -4 5 1543.24 232.104 3 0 4 -5 1624.93 269.382 5 0 -4 -6 113199 1414.52 3 0 -4 6 113616 1991.07 3 0 4 -7 7630.69 619.61 5 0 -4 -7 7167.86 348.49 3 0 -4 7 7123.84 514.834 3 0 4 -7 6620.56 427.879 4 0 4 -8 42203.7 1093.59 4 0 -4 8 43756.3 1314.64 3 0 -4 9 50939.2 1468.99 3 0 4 -9 50471.3 1219.56 4 0 -4 10 74009.4 1831.24 3 0 4 -10 75501.5 1529.78 4 0 -4 11 51757.6 1581.07 3 0 4 -11 52373.1 1297.79 4 0 4 12 12457.2 443.019 12 0 4 -12 14979.8 1140.86 5 0 -4 12 14179 572.767 9 0 -4 12 11766.4 486.977 11 0 -4 12 12061.4 783.27 3 0 4 12 12033.6 463.786 10 0 -4 13 2466.56 232.679 11 0 -4 13 2236.58 352.875 3 0 4 13 2463.77 201.635 12 0 4 -13 2020.62 177.169 13 0 4 13 2340.3 242.096 8 0 4 13 2294.3 213.43 10 0 -4 13 2777.6 560.732 2 0 4 -13 2713.19 531.341 5 0 4 -14 7533.77 345.712 13 0 -4 14 6963.46 394.041 11 0 -4 14 6735.29 846.049 2 0 4 14 7133.29 377.958 10 0 -4 14 6378.98 387.21 9 0 4 14 7306.83 442.879 8 0 4 14 7305.67 349.919 12 0 -4 14 6493.51 606.733 3 0 4 14 6933.73 423.17 7 0 4 15 24943.6 660.213 12 0 4 15 23051.5 773.1 7 0 -4 15 35644.1 1845.87 2 0 4 -15 22486.3 610.774 13 0 4 15 25253.8 729.862 10 0 4 -15 35078.9 1964.46 5 0 -4 15 24239.2 751.764 11 0 -4 15 35603.4 1458.67 3 0 -4 15 23199.5 753.06 9 0 4 15 23616.4 814.138 8 0 4 16 435.106 129.644 8 0 -4 16 476.058 119.872 9 0 4 -16 690.824 110.948 13 0 4 -16 1041.86 376.205 5 0 4 16 443.289 117.539 10 0 4 16 220.076 67.9066 12 0 -4 16 657.364 220.231 3 0 -4 16 1342.13 376.842 2 0 -4 16 318.862 101.139 11 0 -4 17 83036.4 2391.99 3 0 4 -17 85988.6 1235.13 13 0 4 17 83233.3 1552.82 7 0 -4 17 82495.6 1478.95 9 0 4 17 83916.9 1633.55 8 0 -4 17 90273.2 2783.53 2 0 4 17 88987.2 1263.42 12 0 -4 17 86319.5 1488.09 11 0 4 17 87545 1410.72 10 0 -4 18 2260.92 403.89 3 0 4 18 2498.46 250.452 10 0 4 18 2160.53 258.671 7 0 4 18 2217.5 206.792 12 0 4 -18 2584.37 590.258 5 0 -4 18 2134.05 248.626 9 0 4 18 2365.93 286.191 8 0 -4 18 2119.34 243.674 11 0 -4 18 2494.88 457.503 2 0 -4 19 22459.3 732.167 7 0 4 19 23084.8 648.751 12 0 4 19 22552.7 843.812 7 0 -4 19 22459.7 1289.67 3 0 4 19 22071.6 875.048 8 0 -4 19 21125.7 767.62 9 0 -4 19 23435 1381.42 2 0 -4 19 21849.7 781.184 11 0 -4 20 29038.3 1518.31 2 0 -4 20 26690.3 865.104 9 0 4 20 26201.3 972.103 8 0 -4 20 27571.1 1449.43 3 0 -4 20 28185.7 825.011 7 0 4 20 26465.6 924.915 7 0 4 20 29605.6 723.059 12 0 -4 20 26763.8 873.159 11 0 4 21 78.0288 79.7921 8 0 4 -21 97.6152 146.498 5 0 -4 21 115.85 86.9052 11 0 4 21 127.89 79.8717 7 0 -4 21 427.447 205.109 3 0 -4 21 -29.5158 102.49 2 0 -4 21 101.733 83.2717 9 0 -4 22 15057.9 642.968 9 0 -4 22 15450.2 621.935 7 0 4 22 14981 745.894 8 0 -4 22 14995.2 658.73 11 0 4 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3 0 5 -7 22065.4 582.729 13 0 5 -7 18953.5 1067.5 5 0 -5 7 20087.6 962.447 3 0 5 -8 75375 2180.58 5 0 5 8 78295.4 1183.64 10 0 5 -8 78207.8 1111.61 13 0 -5 8 74102.3 1904.53 3 0 5 8 77871.1 1128.62 12 0 5 9 132759 1566.15 10 0 -5 9 131959 2614.16 3 0 5 -9 138062 3069.75 5 0 5 9 134929 1510.87 12 0 5 -9 133997 1483.47 13 0 -5 9 127898 1571.97 11 0 5 10 8856.29 392.629 12 0 5 -10 8807.11 805.089 5 0 -5 10 8959.74 425.516 11 0 5 10 7937.75 447.127 8 0 -5 10 9690.77 738.658 3 0 5 -10 8915.33 388.836 13 0 -5 10 9396.82 478.723 9 0 5 10 8750.1 410.967 10 0 5 11 9516.11 501.738 8 0 5 -11 8985.77 843.525 5 0 5 -11 8042.99 402.876 10 0 5 11 8783.96 396.372 12 0 5 11 8278.19 411.43 10 0 5 -11 8431.62 384.479 13 0 -5 11 8603.54 432.199 11 0 -5 11 9589.68 745.139 3 0 -5 11 9039.46 470.752 9 0 5 12 589.079 124.377 10 0 -5 12 432.4 179.445 3 0 5 12 380.677 118.717 8 0 5 -12 361.542 87.9917 13 0 5 12 669.373 122.86 12 0 -5 12 419.433 101.755 11 0 5 -12 697.711 130.108 10 0 5 -12 368.268 153.584 5 0 5 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968.703 8 0 -5 25 28366.9 832.202 11 0 5 25 28467.7 943.438 8 0 -5 25 28694.8 785.011 9 0 -5 26 1441.1 169.475 9 0 5 26 1367.09 209.549 8 0 -5 26 1586.46 197.301 11 0 5 27 9582.52 492.336 8 0 -5 27 9559.18 433.872 11 0 -5 28 2863.48 221.327 11 0 5 28 2765.57 250.28 8 0 5 29 1240.42 152.95 8 0 -5 29 1223.34 132.4 11 0 6 0 95140.7 1183.25 13 0 6 0 93492 1348.26 10 0 -6 0 92291.8 1917.14 3 0 6 -1 57833.1 1060.62 10 0 -6 1 57167.4 1549.61 3 0 6 1 57471.2 904.218 13 0 6 1 58304.3 956.885 12 0 6 1 60378.7 1078.09 10 0 6 -1 59944.7 960.749 13 0 -6 -1 59926.3 1507.48 3 0 6 2 20743.8 580.717 12 0 6 -2 20743.6 637.225 10 0 6 -2 20243.8 564.815 13 0 -6 2 19536.1 932.707 3 0 6 2 20316.8 629.474 10 0 6 -3 96490.6 1375.87 10 0 6 3 98783.1 1396.56 10 0 6 3 102221 1308.37 12 0 6 -3 101068 1281.63 13 0 -6 3 95411.5 2111.68 3 0 6 4 29278.4 765.393 10 0 6 4 29425.8 716.473 12 0 -6 4 27739.2 1162.82 3 0 6 -4 27755.5 739.958 10 0 6 -4 28602.7 694.286 13 0 6 -5 75488.5 1225.18 10 0 6 -5 78456.2 1168.61 13 0 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2797.76 281.527 11 0 6 -16 77822.6 1303.19 13 0 6 16 79906.4 1426.98 10 0 6 -16 75535.8 2782.45 5 0 -6 16 78655.7 1571.04 9 0 -6 16 81142.9 1513.6 11 0 6 16 80829.9 1688.75 8 0 6 16 78305.1 1285.51 12 0 -6 17 1069.18 184.747 9 0 6 17 937.532 153.567 12 0 6 -17 1163.79 169.795 13 0 6 17 1304.62 202.805 10 0 6 17 1093.68 210.361 8 0 6 -17 795.858 288.888 5 0 -6 17 593.008 225.722 3 0 6 18 52253.1 1373.17 8 0 6 -18 51631.3 1051.8 13 0 6 18 53497.4 1043.14 12 0 6 18 54179.9 1183.66 10 0 -6 18 51212.4 1258.46 9 0 -6 18 53144.6 1234.27 11 0 6 19 771.94 178.605 8 0 -6 19 765.352 171.224 9 0 6 19 648.408 140.974 10 0 -6 19 828.829 169.349 11 0 6 -19 720.616 131.294 13 0 6 19 612.862 129.858 12 0 -6 20 25544.9 849.814 11 0 6 20 25412.3 688.114 12 0 6 -20 27084.1 743.284 13 0 6 20 25114.5 940.509 8 0 -6 20 24534.4 855.926 9 0 6 21 1531.08 235.005 8 0 -6 21 1620.06 218.906 11 0 -6 21 1404.4 207.077 9 0 6 -21 1703.66 183.239 13 0 6 22 924.496 185.438 8 0 -6 22 868.221 164.529 11 0 -6 22 1015.23 176.336 9 0 6 23 447.949 130.052 8 0 -6 23 653.05 138.702 11 0 -6 23 413.368 111.07 9 0 -6 24 18207.3 645.205 11 0 6 24 17544.4 700.616 8 0 -6 24 18785.3 629.484 9 0 -6 25 22428.1 638.398 9 0 -6 25 22583.6 685.429 11 0 6 25 21683.7 731.495 8 0 -6 26 1992.94 196.096 11 0 6 26 2041.57 213.496 8 0 -6 26 2043.51 179.367 9 0 6 27 678.952 116.752 8 0 -6 27 831.625 121.555 11 0 -6 28 708.4 99.7442 11 0 7 0 130.646 60.0324 12 0 7 0 345.547 103.793 10 0 7 0 396.49 98.7174 13 0 7 1 113606 1436.95 12 0 7 -1 117639 1452.42 13 0 7 -1 112917 1614.58 10 0 7 1 114717 1623.96 10 0 7 1 114825 1389.41 13 0 7 2 4368.42 285.549 12 0 7 2 4487.87 272.07 13 0 7 -2 5073.07 313.664 13 0 7 2 4440.88 326.738 10 0 7 -2 4734.88 334.492 10 0 7 -3 6068.01 377.685 10 0 7 3 6855.06 402.186 10 0 7 3 6709.47 358.83 12 0 7 -3 6723.56 361.091 13 0 -7 3 6819.03 635.85 3 0 7 4 6960.39 374.042 12 0 -7 4 7383.18 667.439 3 0 7 -4 7642.31 389.404 13 0 7 -4 6929.03 405.747 10 0 7 4 6785.84 399.939 10 0 -7 5 40267.8 1581.25 3 0 7 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8798.68 527.937 8 -1 1 25 7943.45 501.574 7 1 -1 25 8123.63 448.081 9 1 -1 25 8007.5 446.598 11 1 -1 25 8172.96 526.142 7 1 -1 25 7644.86 482.349 8 -1 1 24 33752.6 1030.91 8 1 -1 24 36509.5 961.515 9 1 -1 24 37448.3 1121.45 7 -1 1 24 33616.9 1024.07 7 1 -1 24 35082.4 1031.98 8 1 -1 24 37352.6 976.541 11 1 -1 23 25555 816.252 9 1 -1 23 24517.7 856.133 8 -1 1 23 24031.2 856.465 8 -1 1 23 23674.5 854.687 7 1 -1 23 24448.4 800.931 11 1 -1 23 25842.6 921.512 7 -1 1 22 40281.7 1097.12 7 1 -1 22 44364.5 1077.77 9 1 -1 22 41780.5 1157.93 7 -1 1 22 39387.7 1072.21 8 1 -1 22 41442.2 1095.8 8 1 -1 22 42823.4 1763.08 2 1 -1 22 42499.7 1052.24 11 -1 1 21 152250 2057.66 8 1 -1 21 151784 2063.85 8 -1 1 21 157146 2107.56 7 1 -1 21 161733 2227.82 7 1 -1 21 159806 3349.21 2 1 -1 21 160352 2030.1 9 1 -1 21 160196 2017 11 1 -1 20 131449 1820.21 9 1 -1 20 131748 2953.98 2 1 -1 20 126614 1814.46 8 1 -1 20 131576 1954.91 7 -1 1 20 126825 1826.06 8 -1 1 20 132015 1879.17 7 1 -1 20 131062 1774.62 11 1 -1 19 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7 -1 -1 24 35692.2 883.974 11 1 1 25 7778.37 522.64 8 -1 -1 25 8129.46 496.45 7 -1 -1 25 7893.82 408.961 11 1 1 25 7630.69 524.257 7 -1 -1 25 8102.35 485.364 8 1 1 26 20709.4 839.653 8 -1 -1 26 20759.6 764.581 8 1 1 26 21719.4 867.61 7 -1 -1 26 22146.7 812.555 7 1 1 27 3044.39 321.478 7 -1 -1 27 3210.15 310.061 7 -1 -1 27 3223.57 299.847 8 1 1 27 3036.35 319.353 8 -1 -1 28 13588.3 609.475 7 1 1 28 12539.9 616.718 8 1 1 28 12831.9 624.619 7 -1 -1 28 12458.8 565.242 8 -1 -1 29 173.289 71.267 8 1 1 29 246.226 105.18 8 -1 -1 29 353.189 109.904 7 1 1 30 8279.98 446.043 8 -1 -1 30 8286.83 434.15 7 -1 -1 30 8218.73 414.584 8 -1 -1 31 971.611 138.034 8 -1 -1 31 938.896 145.031 7 1 1 31 946.652 145.933 8 -1 -1 32 27028.8 648.72 7 1 1 32 22291.9 582.382 8 -1 2 32 1705.44 169.077 8 -1 2 31 16394.4 563.884 8 -1 2 30 4398.42 310.039 7 -1 2 30 4819.48 334.612 8 -1 2 29 6042.93 388.368 7 1 -2 29 5847.3 319.352 11 -1 2 29 6071.28 399.523 8 1 -2 29 5318.12 345.855 7 1 -2 28 529.763 126.441 7 -1 2 28 470.537 131.911 7 -1 2 28 444.101 131.079 8 1 -2 28 468.553 109.291 11 1 -2 27 25111.2 765.992 11 -1 2 27 25780.6 872.265 7 1 -2 27 26129.6 851.753 7 -1 2 27 25239.8 878.241 8 1 -2 27 25349.2 729.932 9 1 -2 26 15313.2 599.112 9 -1 2 26 14750.3 678.783 7 1 -2 26 15023.7 617.447 11 1 -2 26 14883.5 665.318 7 -1 2 26 14781.2 690.16 8 1 -2 25 24619 815.526 11 -1 2 25 23270.2 857.664 7 -1 2 25 23651.4 881.968 8 1 -2 25 23389 771.821 9 1 -2 25 24691.1 876.583 7 -1 2 24 18673.5 771.152 7 -1 2 24 17422.3 751.978 8 1 -2 24 18861.7 725.489 11 1 -2 24 18854.6 707.957 9 1 -2 24 19381 779.051 7 1 -2 23 14964.6 639.264 8 1 -2 23 14330.7 634.656 11 -1 2 23 13675 662.52 8 1 -2 23 14515.9 628.738 9 1 -2 23 14464 675.371 7 -1 2 23 13752 663.9 7 1 -2 23 15083.4 1078.64 2 1 -2 22 22190.2 791.929 11 -1 2 22 20295.7 793.304 7 -1 2 22 19943.2 791.52 8 1 -2 22 21448.3 769.393 9 1 -2 22 22698.1 781.817 8 1 -2 22 21450.8 1266.34 2 1 -2 22 22082.8 824.783 7 -1 2 21 76403.2 1511.08 8 1 -2 21 80570 1476.08 9 1 -2 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24328.6 807.552 10 2 -6 16 12967.7 656.619 9 2 6 -16 11822.6 495.997 13 2 -6 16 11578.8 600.011 11 -2 6 16 12204.9 606.233 10 2 6 -16 11748.9 570.6 10 2 -6 15 6692.76 472.691 9 2 -6 15 6664.1 1030.53 2 2 6 -15 6587.02 376.589 13 2 -6 15 6233.56 442.402 11 2 6 -15 6542.02 852.616 5 -2 6 15 6898.76 456.861 10 2 6 -15 6336.91 423.742 10 2 -6 14 15631.6 714.116 9 -2 6 14 14948 660.755 10 2 6 -14 14986.7 651 10 2 -6 14 13764.6 647.978 11 2 6 -14 15565.4 1291.87 5 2 6 -14 13324 536.198 13 2 6 -13 53048.3 2353.82 5 2 -6 13 50767.2 1272.34 9 2 6 -13 48685.2 1021.38 13 2 -6 13 46054.9 1168.68 11 -2 6 13 50161.6 1190.6 10 2 6 -13 44494.4 1764.31 4 2 6 -13 49222.2 1180.33 10 2 -6 12 159132 3432.2 3 2 -6 12 164199 2262.62 9 2 6 -12 161810 1860.56 13 2 -6 12 153705 2090.49 11 2 6 -12 164656 4122.4 5 -2 6 12 166311 2132.47 10 2 6 -12 152646 3272.78 4 2 6 -12 165845 2145.15 10 2 -6 11 153066 3310.12 3 2 -6 11 157205 2190.76 9 2 6 -11 158187 1833.53 13 2 6 -11 148171 3224.39 4 2 -6 11 149120 2028.11 11 2 6 -11 159477 3955.77 5 -2 6 11 159915 2071.2 10 2 6 -11 155665 2080.61 10 2 -6 10 173937 3436.26 3 2 -6 10 179044 2306.34 9 -2 6 10 178011 2145.2 10 2 -6 10 169702 2120.95 11 2 6 -10 184892 4173.94 5 2 6 -10 175212 1916.44 13 2 6 -10 171661 3397.53 4 2 6 -10 179323 2208.53 10 2 6 -9 141306 1941.99 10 2 -6 9 133975 1966.98 9 2 -6 9 132297 2920.92 3 2 6 -9 137176 1689.26 13 2 -6 9 136273 1871.29 11 2 6 -9 134548 3506.14 5 -2 6 9 138308 1868.02 10 2 6 -9 130584 2957.09 4 2 -6 8 102806 1685.96 9 2 -6 8 99243.9 2463.56 3 2 6 -8 101219 1439.18 13 2 -6 8 97526.9 1557.55 11 2 6 -8 101395 2970.03 5 -2 6 8 100203 1552.06 10 2 6 -8 102473 1631.04 10 -2 6 7 35323.2 910.802 10 2 -6 7 35642.9 973.317 9 2 6 -7 35547.6 1716.41 5 2 6 -7 35479.9 846.68 13 -2 -6 -7 38056.4 1640.9 3 2 6 -7 35117 951.684 10 2 -6 6 76599.9 2021.17 3 2 -6 6 74985.7 1393.35 9 2 6 -6 76922.7 2475.68 5 -2 6 6 77639.7 1323.6 10 2 6 -6 80950.8 1422.49 10 2 6 -6 78638.8 1249.53 13 2 -6 5 3577.05 415.734 3 2 -6 5 2933.57 276.555 9 -2 -6 -5 3351.02 475.263 3 -2 6 5 2633.38 245.926 10 2 6 -5 2401.97 437.036 5 2 6 -5 2960.52 272.557 10 2 6 -5 2697.1 234.867 13 2 -6 4 93297.8 1492.34 9 2 6 -4 104029 1575.75 10 -2 -6 -4 109808 2634.75 3 2 6 -4 105342 1410.2 13 2 6 -4 100111 2741.07 5 -2 6 4 101191 1464.48 10 2 6 -3 74949.7 1175.54 13 -2 6 3 75203.3 1246.96 10 2 6 -3 76781.7 1337.68 10 2 6 -2 37907.6 821.37 13 -2 -6 -2 35933.4 1487.39 3 -2 6 2 34499.3 838.473 10 2 6 -2 35121.6 762.563 12 2 6 -2 36510.9 913.701 10 2 6 -1 2944.51 232.411 13 -2 6 1 2784.76 230.811 13 -2 -6 -1 2412.85 390.646 3 2 6 -1 2747.7 222.258 12 2 6 -1 2680.21 248.346 10 -2 6 0 122673 1527.34 13 2 6 0 117302 1411.25 13 2 6 0 112626 1418.89 12 -2 6 0 112108 1485.92 10 2 6 0 115299 1600.82 10 -2 -6 0 120859 2698.34 3 2 6 1 3135.9 228.72 13 2 6 1 2850.95 230.862 12 -2 -6 1 3092.31 442.324 3 -2 6 -1 2785.32 237.013 13 -2 6 -1 2907.29 235.795 10 2 6 1 2602.36 240.742 10 2 6 2 35558.4 812.336 12 -2 6 -2 37067 863.259 13 2 6 2 34486.8 732.258 13 -2 -6 2 35853.2 1471.18 3 -2 6 -2 34139.1 802.467 10 2 6 2 35754.4 877.761 10 -2 6 -3 75199.9 1240.08 13 2 6 3 72766.2 1058.33 13 2 6 3 73410.5 1251.9 10 -2 -6 3 76146.5 2159.93 3 2 6 3 75318.2 1197.11 12 -2 6 -3 72312.7 1161.71 10 -2 6 -4 105978 1483.28 13 2 6 4 101898 1412.41 12 2 6 4 98786.2 1454.78 10 -2 -6 4 101718 2515.8 3 -2 -6 5 2768.31 253.45 11 -2 6 -5 3856.98 292.827 13 2 6 5 3727 276.916 12 2 6 5 2674.61 244.941 10 -2 -6 5 2563.76 407.912 3 2 6 5 1623.39 227.892 8 -2 6 -6 78571.1 1317.29 13 2 6 6 80559.7 1279.55 12 -2 -6 6 77862.7 2234.46 3 2 6 6 79530.6 1288.62 10 2 6 7 38102.9 1189.98 8 -2 -6 7 35997.2 1543.77 3 2 6 7 35533.4 855.14 12 -2 6 -7 36703.6 909.415 13 2 6 7 34882.4 859.379 10 2 6 8 99603 1454.83 12 -2 6 -8 100607 1519.47 13 2 6 8 102739 1960.67 8 -2 -6 8 98264.6 1553.97 11 -2 -6 8 101943 2622.56 3 2 6 8 98508.9 1432 10 -2 -6 9 137108 1856.17 11 -2 6 -9 137498 1801.94 13 2 6 9 138328 1699.97 10 -2 -6 9 141972 3138.38 3 2 6 9 133761 1690.65 12 -2 -6 10 175834 2125.44 11 -2 -6 10 182337 3611.73 3 2 6 10 179050 1937.1 10 -2 6 -10 178496 2075.12 13 2 6 10 174845 1947.3 12 2 6 11 155167 1838.82 12 -2 -6 11 155837 2045.2 11 -2 6 -11 157693 1970.89 13 2 6 11 159710 1823.7 10 -2 -6 11 162841 3468.55 3 -2 -6 12 159200 2080.9 11 -2 -6 12 168919 3562.74 3 2 6 12 163027 1852.61 10 2 6 12 160581 1878.46 12 2 6 12 167907 2632.6 8 -2 6 -12 157492 1997.76 13 2 6 13 49256.8 1045.4 12 -2 6 -13 47253.7 1090.81 13 -2 -6 13 48736 1157.66 11 2 6 13 49839.7 1027.91 10 2 6 13 50647 1454.37 8 -2 6 -14 13817.1 593.187 13 -2 -6 14 14836.5 660.074 9 2 6 14 14283.9 563.357 12 2 6 14 14318.6 782.327 8 -2 -6 14 13588.4 616.609 11 2 6 14 14486.5 554.237 10 -2 -6 14 15876.1 1128.61 3 -2 -6 15 6874.14 454.326 9 2 6 15 6339.4 372.841 12 -2 -6 15 7317.39 769.109 3 -2 -6 15 6605.18 430.925 11 2 6 15 6460.26 366.976 10 2 6 15 6688.26 539.228 8 -2 -6 16 12625.6 608.508 9 2 6 16 12052.1 720.508 8 2 6 16 11635.4 499.88 12 -2 -6 16 12135.6 587 11 -2 -6 17 25191.7 850.571 9 2 6 17 24482.4 1019.16 8 2 6 17 23546.1 699.071 12 -2 -6 17 23862.9 818.587 11 -2 -6 18 66974.4 1351.58 9 -2 -6 18 66460.2 1350.83 11 2 6 18 65750.9 1136.56 12 2 6 18 64139.5 1633.57 8 -2 -6 19 32422.1 923.138 9 2 6 19 31367.5 1128.77 8 -2 -6 19 32946.3 937.668 11 2 6 19 32340.4 776.944 12 -2 -6 20 7386.73 427.317 9 2 6 20 7452.31 361.675 12 -2 -6 20 7698.72 446.568 11 2 6 20 7273.04 541.067 8 -2 -6 21 9569.58 484.198 11 -2 -6 21 9206.93 458.3 9 2 6 21 9146.48 582.751 8 2 6 21 9026.95 376.412 12 -2 -6 22 4341.15 297.944 9 2 6 22 4342.58 391.027 8 2 6 22 4203.54 241.227 12 -2 -6 22 4345.56 316.086 11 2 6 23 216.482 106.915 8 -2 -6 23 431.891 112.923 11 2 6 23 416.061 79.4403 12 2 6 24 50347.7 1189.41 8 -2 -6 24 51136.1 984.211 11 2 6 25 13298.8 574.233 8 -2 -6 25 14660.5 496.302 11 2 6 26 10441.4 466.252 8 -2 -6 26 10676.8 394.138 11 -2 -6 27 13472.1 398.356 11 2 6 27 12331.8 452.556 8 2 -7 24 51233.9 882.806 9 2 -7 24 49929.7 865.822 11 2 -7 23 7169.51 364.517 9 2 -7 23 6846.48 349.761 11 2 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782.071 10 2 7 -13 21374 682.386 13 2 -7 13 21398.5 793.205 11 2 7 -13 21930.7 777.332 10 2 -7 12 24465.6 884.417 9 2 7 -12 23474.2 722.426 13 2 -7 12 23766.9 834.903 11 -2 7 12 24043.5 829.108 10 2 7 -12 23890.4 815.224 10 2 -7 11 22265.2 839.759 9 2 -7 11 22734.3 810.599 11 2 7 -11 21241.8 1478.58 5 -2 7 11 22373.8 794.287 10 2 7 -11 22876.3 800.976 10 2 7 -11 22243.3 709.462 13 2 -7 10 14774.8 682.839 9 2 7 -10 15195.8 585.652 13 -2 7 10 14745.5 638.455 10 2 7 -10 15149.8 1233.04 5 2 7 -10 15624 665.422 10 2 -7 9 49402.1 1232.95 9 2 7 -9 53457.7 2283.73 5 2 7 -9 51463.5 1078.78 13 -2 7 9 50595.6 1170 10 2 7 -9 51433.9 1201.15 10 2 -7 8 134390 2001.27 9 2 7 -8 133524 1732.39 13 2 7 -8 139615 3638.85 5 -2 7 8 134147 1876.96 10 2 7 -8 137606 1970.44 10 2 -7 7 95049.1 1664.77 9 2 7 -7 99549.3 1482.94 13 2 7 -7 99147.1 1664.69 10 -2 7 7 100820 1606.82 10 2 -7 6 57250.8 1264.13 9 -2 7 6 57914.7 1215.72 10 2 7 -6 57963.2 1115.21 13 2 7 -6 58274.5 1269.87 10 2 -7 5 28284.7 877.216 9 -2 7 5 29859.2 862.88 10 2 7 -5 28690.8 888.859 10 2 7 -5 29925.3 795.8 13 2 -7 4 54138.3 1189.34 9 2 7 -4 55211.6 1075.55 13 -2 7 4 55991 1162.73 10 2 7 -4 55439.2 1220.18 10 2 7 -3 32763.5 933.967 10 -2 7 3 30641.2 857.261 10 2 7 -3 32512.2 812.759 13 -2 -7 -3 32461.7 1554.37 3 -2 -7 -2 1240.7 317.488 3 2 7 -2 1264.42 163.328 13 -2 7 2 1337.75 186.504 10 2 7 -2 1397.3 201.996 10 2 7 -1 3979.48 323.233 10 2 7 -1 4062.05 275.616 12 2 7 -1 4320.69 291.726 13 2 7 0 42468.6 885.011 13 2 7 0 41758.7 890.855 12 -2 -7 0 42805.8 1747.75 3 2 7 0 41860 1027.87 10 -2 7 0 39292.9 939.597 10 2 7 1 4752.48 294.51 13 2 7 1 3749.05 275.332 12 -2 7 -1 4013.85 303.937 13 -2 -7 1 3885.56 536.901 3 -2 7 -1 3682.96 286.401 10 2 7 1 3396.65 297.315 10 -2 -7 2 883.852 258.915 3 2 7 2 1411.31 165.84 13 2 7 2 1656.51 190.986 12 -2 7 -2 1232.03 166.763 10 -2 7 -2 1221.41 176.966 13 2 7 2 1488.63 195.933 10 2 7 3 35846.5 1107.49 8 2 7 3 31352.7 881.955 10 2 7 3 31930 728.03 13 -2 7 -3 32370.2 871.705 13 2 7 3 32445.6 822.705 12 -2 -7 3 32141.2 1525.78 3 -2 7 -3 31995.3 819.378 10 -2 7 -4 56233.3 1171.39 13 2 7 4 54945.6 1084.74 12 -2 -7 4 57272.3 2030.82 3 2 7 4 57448 1178.12 10 -2 7 -5 29338.7 842.118 13 2 7 5 30134.1 809.571 12 -2 -7 5 29075.6 1465.04 3 2 7 5 29680.7 847.11 10 -2 -7 6 58879.3 2107.52 3 2 7 6 62113 1522.13 8 2 7 6 60796.3 1167.64 12 2 7 6 57741 1169.93 10 -2 7 -6 58135 1201.65 13 -2 7 -7 100257 1595.63 13 2 7 7 107351 2011.54 8 -2 -7 7 99596.3 2759.83 3 -2 -7 7 106155 1669.36 11 2 7 7 99768.2 1525.37 10 2 7 7 100871 1501.48 12 -2 -7 8 142283 1948.75 11 -2 -7 8 141668 3309.13 3 -2 7 -8 130731 1843.22 13 2 7 8 144017 2353.95 8 2 7 8 135829 1755.61 12 2 7 8 134470 1768.29 10 2 7 9 54635 1468.45 8 2 7 9 49946.3 1064.85 12 -2 -7 9 52065.9 2021.99 3 -2 7 -9 52153.9 1177.98 13 -2 -7 9 53135.1 1207.96 11 2 7 9 49905.6 1073.32 10 2 7 10 15816.3 799.18 8 -2 7 -10 15376.8 646.661 13 2 7 10 15137.6 594.334 12 -2 -7 10 15255.7 1106.21 3 -2 -7 10 15287.9 648.866 11 2 7 10 15081.1 585.757 10 -2 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8 -7 137534 1722.78 13 -2 8 7 140498 1923.76 10 2 8 -7 137673 1962.47 10 2 -8 6 5611.56 394.341 9 2 8 -6 6585.52 382.136 13 -2 8 6 5746.11 391.931 10 2 8 -6 6101.25 419.618 10 2 -8 5 15312.8 644.135 9 -2 8 5 14813.2 617.899 10 2 8 -5 15661.7 579.994 13 2 8 -5 15333 657.692 10 2 8 -4 6445.17 370.949 13 2 8 -4 6044.64 411.378 10 -2 8 4 5516.81 381.725 10 2 8 -3 17887.4 607.66 13 -2 8 3 16617.5 646.128 10 2 8 -3 16856.8 683.462 10 2 8 -2 4813.83 316.169 13 -2 8 2 4699.2 343.437 10 2 8 -2 4829.44 368.212 10 2 8 -1 152067 1720.54 13 2 8 -1 151784 2040.09 10 2 8 0 46899.3 939.483 13 2 8 0 49153.7 953.998 12 -2 8 0 46713.3 1052.8 10 2 8 0 48926.7 1147.37 10 2 8 1 151218 1646.58 13 2 8 1 152792 1717.33 12 -2 8 -1 151488 1868.32 10 2 8 1 151031 2000.53 10 2 8 2 4889.97 291.027 13 2 8 2 4857.08 315.855 12 -2 8 -2 4701.84 329.879 10 2 8 2 5054.76 371.149 10 2 8 3 17481.1 602.633 12 -2 8 -3 17888.8 632.34 10 2 8 3 16818.3 667.139 10 2 8 4 5847.82 354.841 12 -2 8 -4 5774.71 353.273 10 2 8 4 5872.69 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2 3 5871.4 347.094 12 -8 -2 3 5728.71 336.005 7 -8 -2 4 4471.5 290.668 6 -8 2 -4 4702.16 352.061 6 8 2 4 5154.69 318.744 12 -8 -2 4 4864.59 307.597 7 -8 -2 5 11636.5 458.977 6 -8 2 -5 12251.6 559.675 6 8 2 5 12354.6 482.697 12 -8 -2 5 12784.2 486.524 7 -8 -2 6 1344.04 158.584 6 -8 2 -6 1453.3 201.493 6 8 2 6 1746.33 183.413 12 -8 -2 6 1646.68 179.515 7 -8 -2 7 12746.5 460.287 6 -8 2 -7 13793.1 584.418 6 8 2 7 13521.2 479.392 12 -8 -2 7 13929.8 491.358 7 -8 -2 8 25537.4 635.49 6 -8 2 -8 27727.9 813.193 6 8 2 8 26518.5 652.705 12 -8 -2 8 27710.4 676.699 7 -8 -2 9 4654.22 267.014 6 -8 2 -9 5059.88 346.616 6 8 2 9 5128.25 279.36 12 -8 -2 9 5414.97 293.685 7 -8 -2 10 9362.9 363.723 6 -8 2 -10 10401 482.181 6 8 2 10 9957.89 373.137 12 -8 -2 10 10690.8 430.049 11 -8 -2 10 10893.8 398.543 7 -8 2 -11 6028.17 357.828 6 8 2 11 5563.1 261.046 12 -8 -2 11 6212.94 312.251 11 -8 -2 11 6155 289.373 7 -8 2 -12 6969.67 369.78 6 8 2 12 6238.55 254.264 12 -8 -2 12 6836.45 306.003 11 -8 -2 12 6868.3 292.217 7 -8 -2 13 6330.38 274.096 11 -8 -2 13 6501.98 268.712 7 -8 2 -14 15303.7 497.352 6 -8 2 -15 3313.24 219.575 6 -8 3 12 73.3029 47.9927 6 -8 3 11 10073.2 370.54 6 -8 -3 -11 9395.3 370.117 7 -8 3 10 3437.59 225.646 6 8 3 -10 2873.23 188.184 13 -8 -3 -10 3359.31 234.566 7 -8 3 9 6868.08 327.871 6 8 3 -9 6689.28 296.239 13 -8 -3 -9 6837.28 346.53 7 -8 3 8 16001.2 514.549 6 8 3 -8 16355.2 477.551 13 -8 -3 -8 16513.7 550.47 7 -8 3 7 1656.47 173.852 6 8 3 -7 2152.83 182.693 13 8 3 -7 1618.17 149.613 12 -8 -3 -7 1883.29 195.002 7 -8 3 6 13446.7 494.456 6 8 3 -6 13969 464.256 13 8 3 -6 12856.5 430.331 12 -8 -3 -6 13790.9 522.786 7 -8 3 5 1638.97 181.417 6 8 3 -5 1910.69 177.311 13 8 3 -5 1590.47 161.294 12 8 -3 5 1568.48 154.021 12 -8 -3 -5 1692.32 190.818 7 -8 3 4 13221.1 507.576 6 8 3 -4 14097.9 479.261 13 8 3 -4 13543.4 470.878 12 8 -3 4 13638 465.606 12 -8 -3 -4 13131.3 520.769 7 -8 3 3 29772.2 769.128 6 8 3 -3 29568.6 708.684 12 -8 -3 -3 29932.1 786.548 7 -8 3 2 13524.4 524.44 6 8 3 -2 13286.2 486.084 12 -8 -3 -2 13415.9 531.121 7 -8 3 1 9994.65 458.545 6 8 3 -1 9010.98 406.526 12 -8 -3 -1 9620.96 446.382 7 -8 3 0 4717.61 319.978 6 8 3 0 4745.95 297.67 12 -8 -3 0 5173.98 325.946 7 -8 3 -1 9998.08 461.053 6 8 3 1 9241.17 410.081 12 -8 -3 1 9584.57 440.487 7 -8 3 -2 13999 547.624 6 8 3 2 14191.9 505.339 12 -8 -3 2 13931.3 525.691 7 -8 3 -3 30306 803.908 6 8 3 3 29024.8 715.933 12 -8 -3 3 30261.3 765.569 7 -8 3 -4 14123.2 549.613 6 8 3 4 13333.9 483.888 12 -8 -3 4 13623.6 511.911 7 -8 3 -5 1543.92 189.601 6 8 3 5 1759.83 181.997 12 -8 -3 5 1622.58 182.705 7 -8 3 -6 13989.9 543.191 6 8 3 6 13282.9 467.859 12 -8 -3 6 14098.9 502.117 7 -8 3 -7 1923.15 207.834 6 8 3 7 1811.67 176.014 12 -8 -3 7 2082.2 195.554 7 -8 3 -8 16579.2 573.423 6 8 3 8 16540.4 490.893 12 -8 -3 8 16056.6 535.629 11 -8 -3 8 16684.7 522.109 7 -8 3 -9 6685.53 358.471 6 8 3 9 6631.3 301.55 12 -8 -3 9 6816.26 339.027 11 -8 -3 9 6860.45 326.414 7 -8 3 -10 3500.94 253.128 6 8 3 10 3243.17 201.226 12 -8 -3 10 3281.1 229.479 11 -8 -3 10 3424.62 224.497 7 -8 3 -11 10415.9 416.535 6 8 3 11 10009.1 329.567 12 -8 -3 11 10339.8 381.128 11 -8 -3 11 11002.2 381.004 7 8 3 12 112.032 43.4006 12 -8 3 -12 45.9357 53.2903 6 -8 -3 12 110.467 54.2427 11 -8 -3 12 128.015 52.7666 7 8 4 -10 19785.2 430.866 13 -8 -4 -10 20051.3 512.983 7 8 4 -9 13814.5 381.079 13 -8 -4 -9 13183.4 435.313 7 8 4 -8 6489.41 276.669 13 -8 -4 -8 6146.43 308.726 7 -8 4 7 6596.4 285.473 6 8 4 -7 7550.47 308.272 13 -8 -4 -7 6846.03 335.254 7 -8 4 6 6763.35 298.218 6 8 4 -6 7147.97 309.227 13 -8 -4 -6 6657.67 337.264 7 -8 4 5 3432.05 220.161 6 8 4 -5 3728.62 228.85 13 8 4 -5 3176.16 192.283 12 -8 -4 -5 3546.52 250.323 7 -8 4 4 24031.7 585.535 6 8 4 -4 24080.3 574.416 13 -8 -4 -4 23237.4 642.932 7 -8 4 3 15272.2 476.272 6 8 4 -3 15140.6 459.657 13 8 4 -3 13523 428.149 12 -8 -4 -3 14290 509.312 7 -8 4 2 9930.26 388.125 6 8 4 -2 10328.1 381.708 13 8 4 -2 9005.01 359.022 12 -8 -4 -2 9615.25 421.465 7 -8 4 1 8593.58 364.923 6 8 4 -1 8508.64 345.045 13 8 4 -1 8056.7 345.168 12 -8 -4 -1 8371.32 391.04 7 -8 4 0 26764.8 643.02 6 8 4 0 27020 607.923 13 8 4 0 26460.5 630.185 12 -8 -4 0 26839.9 693.661 7 -8 4 -1 9086.42 378.566 6 8 4 1 8524.81 337.403 13 8 4 1 8224.74 357.443 12 -8 -4 1 8546.21 391.985 7 -8 4 -2 10028.2 403.858 6 8 4 2 10101.4 361.067 13 8 4 2 9748.95 388.627 12 -8 -4 2 9905.26 417.58 7 -8 4 -3 15225.2 487.854 6 8 4 3 15055.4 428.855 13 8 4 3 14817.2 475.439 12 -8 -4 3 14378.8 497.241 7 -8 4 -4 24697 616.595 6 8 4 4 23363.7 513.463 13 8 4 4 23780 592.704 12 -8 -4 4 24167.8 635.494 7 -8 4 -5 4012.54 247.296 6 8 4 5 3364.92 187.44 13 8 4 5 3547.76 227.309 12 -8 -4 5 3781.68 252.792 11 -8 4 -6 7120.87 322.704 6 8 4 6 6955.24 310.42 12 -8 -4 6 7207.35 340.309 11 -8 -4 6 7212.23 337.428 7 -8 4 -7 6780.79 307.874 6 8 4 7 6839.5 299.793 12 -8 -4 7 6909.16 326.445 11 -8 -4 7 7084.32 328.605 7 -8 4 -8 5814.83 277.851 6 8 4 8 6281.19 276.491 12 -8 -4 8 6489.5 308.738 11 -8 -4 8 6123.4 294.421 7 8 4 9 13613.4 392.786 12 -8 -4 9 13909.3 432.259 11 -8 -4 9 14663.1 440.532 7 8 4 10 20455.6 456.829 12 -8 -4 10 20977.7 509.598 11 -8 -4 11 3368.93 195.525 11 -8 -4 11 3399.44 196.118 7 8 5 -7 5180.71 217.563 13 -8 -5 -7 4741.89 237.99 7 8 5 -6 7946.53 278.011 13 -8 -5 -6 7652.39 310.575 7 8 5 -5 31001.4 557.921 13 -8 -5 -5 27940.3 602.168 7 8 5 -4 1317.08 121.165 13 -8 -5 -4 964.737 119.86 7 8 5 -3 9152.84 311.068 13 -8 -5 -3 9239.11 356.336 7 8 5 -2 16870.7 422.16 13 -8 -5 -2 16501.4 477.922 7 8 5 -1 10534.5 332.238 13 8 5 -1 9691.24 314.68 12 -8 -5 -1 9131.86 337.298 11 -8 -5 -1 10903.3 390.711 7 8 5 0 22338.6 472.696 13 -8 -5 0 22482.3 559.199 7 8 5 1 10632.2 319.374 13 8 5 1 10704 342.331 12 -8 -5 1 11079.7 392.812 7 8 5 2 14950.9 365.011 13 8 5 2 16233.4 424.331 12 -8 -5 2 14677 432.631 11 -8 -5 2 17037.7 484.368 7 8 5 3 9601.87 325.896 12 -8 -5 3 9067.11 349.597 7 8 5 4 963.389 109.402 12 -8 -5 4 1202.79 124.092 11 -8 -5 4 1218 130.021 7 8 5 5 29433.6 563.361 12 -8 -5 5 30881.3 620.578 7 8 5 6 7746.11 283.992 12 -8 -5 6 7189.86 285.358 11 -8 -5 6 7899.78 308.68 7 8 5 7 5116.37 224.376 12 -8 -5 7 4563.63 220.068 11 -8 -5 7 5064.36 239.879 7 9 0 0 183.487 71.5954 12 -9 0 0 57.6701 92.1644 6 -9 0 1 16969.6 483.607 6 -9 0 -1 17133.4 488.379 6 9 0 1 18447.7 490.486 12 9 0 -1 19038.4 518.086 12 -9 0 2 91833.7 1111.59 6 -9 0 -2 89809.6 1105.48 6 9 0 2 102858 1117.09 12 9 0 -2 103334 1202.98 12 -9 0 3 4492.3 246.412 6 -9 0 -3 4961.66 265.49 6 9 0 3 5251.9 247.755 12 9 0 -3 5541.41 277.963 12 -9 0 4 21139.7 515.95 6 -9 0 -4 20275.8 516.328 6 9 0 4 21808.9 483.815 12 9 0 -4 21911.6 539.02 12 -9 0 5 6308.88 276.087 6 -9 0 -5 6535.59 289.99 6 9 0 -5 6755.98 291.42 12 -9 0 6 922.109 110.32 6 -9 0 -6 944.777 111.63 6 -9 1 6 7583.36 298.556 6 -9 1 5 47767.8 765.676 6 -9 1 4 53244.8 831.925 6 9 1 -4 52549.6 761.634 12 -9 1 3 4284.03 243.152 6 9 1 -3 4723.05 235.839 12 9 -1 3 4742.3 234.808 12 -9 1 2 4737.99 262.104 6 9 1 -2 5045.67 248.3 12 9 -1 2 5305.23 255.117 12 -9 1 1 68970.7 987.016 6 9 1 -1 70936.8 924.23 12 -9 1 0 15939.9 477.998 6 9 1 0 16647.9 449.902 12 9 -1 0 17465.3 473.693 12 -9 1 -1 69293.5 991.924 6 9 1 1 71415.5 921.612 12 9 -1 -1 70066.9 962.496 12 -9 1 -2 5260.5 280.417 6 9 1 2 5257.21 250.393 12 9 -1 -2 4688.25 246.597 12 -9 1 -3 4421.33 255.259 6 9 1 3 4787.62 234.367 12 9 -1 -3 4219.32 232.146 12 -9 1 -4 54378.8 857.795 6 9 1 4 55353.1 770.93 12 -9 1 -5 48050.6 790.426 6 9 1 5 48989 697.261 12 -9 1 -6 7358.8 305.377 6 -9 2 3 23495.9 523.404 6 9 2 -3 19078.9 417.368 13 9 2 -2 123.279 47.0775 13 9 2 -2 71.7591 38.5827 12 -9 2 2 136.059 51.6293 6 -9 2 1 841.87 106.73 6 9 2 -1 740.539 89.7764 13 9 2 -1 925.185 103.049 12 9 2 0 226.467 60.5443 13 9 -2 0 212.017 60.9664 12 -9 2 0 281.308 64.0147 6 -9 2 -1 840.702 107.231 6 9 2 1 720.184 90.994 13 9 2 1 852.731 103.323 12 9 -2 -1 663.752 93.581 12 9 2 2 64.6557 41.996 12 9 -2 -2 56.5967 47.2316 12 -9 2 -2 105.383 48.7369 6 -9 2 -3 23274.4 532.658 6 9 2 3 24518.1 497.024 12 _iucr_refine_fcf_details ; data_lp_mjy-zh_160822 _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y+1/2,-z 3 -x,y+1/2,-z+1/2 4 -x+1/2,-y,z+1/2 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall ' P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _symmetry_space_group_name_Hall ' P 2ac 2ab' _symmetry_Int_Tables_number 19 _cell_length_a 7.45094(6) _cell_length_b 9.21543(8) _cell_length_c 26.7264(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1835.14(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -9 -2 -3 118.407 107.655 11.312 3.944 o -9 -2 -2 0.363 0.548 0.132 4050.120 o -9 -2 -1 3.966 4.270 0.293 437.896 o -9 -1 -6 34.131 38.841 1.529 41.271 o -9 -1 -5 223.213 244.661 3.922 4.168 o -9 -1 -4 259.726 270.788 2.877 3.594 o -9 -1 -3 22.026 23.556 0.703 74.344 o -9 -1 -2 23.087 25.842 0.754 69.214 o -9 -1 -1 310.342 358.696 5.035 2.482 o -8 -5 -7 27.879 25.561 1.124 57.840 o -8 -5 -6 39.349 40.045 1.061 39.660 o -8 -5 -5 138.649 151.947 7.839 5.147 o -8 -5 -4 4.678 5.973 0.902 262.446 o -8 -5 -3 44.262 47.072 1.200 33.934 o -8 -5 -2 74.091 85.591 1.621 17.945 o -8 -5 -1 54.455 51.451 1.933 26.076 o -8 -4 -10 102.835 101.906 1.690 12.952 o -8 -4 -9 66.879 69.391 1.616 21.018 o -8 -4 -8 32.359 32.479 1.055 48.873 o -8 -4 -7 40.911 35.892 1.347 38.623 o -8 -4 -6 39.324 35.193 0.928 42.070 o -8 -4 -5 16.331 17.680 0.563 102.367 o -8 -4 -4 110.679 122.031 1.771 11.279 o -8 -4 -3 69.551 74.540 1.922 19.325 o -8 -4 -2 55.223 49.811 1.211 28.303 o -8 -4 -1 43.067 42.934 0.922 36.778 o -8 -3 -12 0.639 0.375 0.246 2701.050 o -8 -3 -11 52.843 49.916 1.736 27.584 o -8 -3 -10 16.353 16.372 0.878 98.821 o -8 -3 -9 38.138 34.778 0.951 43.087 o -8 -3 -8 88.045 83.419 1.513 16.023 o -8 -3 -7 10.940 9.344 0.563 164.084 o -8 -3 -6 69.723 69.091 1.214 21.061 o -8 -3 -5 10.676 8.599 0.393 177.287 o -8 -3 -4 71.951 69.430 1.116 20.645 o -8 -3 -3 141.319 152.352 2.225 8.209 o -8 -3 -2 79.935 68.649 1.516 18.563 o -8 -3 -1 53.854 48.749 1.312 28.774 o -8 -2 -15 14.839 14.721 0.949 106.619 o -8 -2 -14 75.167 78.189 2.282 17.329 o -8 -2 -13 37.711 33.929 1.586 40.069 o -8 -2 -12 35.752 23.166 1.825 43.777 o -8 -2 -11 26.015 23.117 0.741 66.374 o -8 -2 -10 48.344 46.976 1.098 32.217 o -8 -2 -9 25.841 24.833 0.647 65.893 o -8 -2 -8 130.345 138.239 1.525 9.449 o -8 -2 -7 67.037 70.850 1.279 21.390 o -8 -2 -6 8.504 8.757 0.535 198.694 o -8 -2 -5 54.398 63.080 1.308 25.982 o -8 -2 -4 23.392 24.319 0.715 70.496 o -8 -2 -3 31.981 29.735 0.808 52.353 o -8 -2 -2 54.451 50.881 1.537 27.473 o -8 -2 -1 17.029 20.248 0.996 87.421 o -8 -1 -16 131.452 132.920 2.839 8.902 o -8 -1 -15 107.131 110.056 8.328 5.883 o -8 -1 -14 1.024 1.609 0.282 1335.100 o -8 -1 -13 65.970 59.323 5.514 12.321 o -8 -1 -12 0.567 0.782 0.250 2386.890 o -8 -1 -11 8.654 6.510 0.652 205.982 o -8 -1 -10 18.105 18.321 0.636 93.381 o -8 -1 -9 43.430 40.165 1.140 36.609 o -8 -1 -8 22.177 24.959 0.786 71.632 o -8 -1 -7 65.300 58.708 2.090 21.578 o -8 -1 -6 7.306 8.372 0.499 223.845 o -8 -1 -5 88.385 90.747 1.592 15.383 o -8 -1 -4 109.955 106.720 1.742 12.009 o -8 -1 -3 177.446 170.855 2.396 6.380 o -8 -1 -2 5.523 7.284 0.492 277.602 o -8 -1 -1 24.384 23.207 0.852 68.273 o -7 -7 -6 125.122 126.933 2.374 9.718 o -7 -7 -5 113.669 111.404 6.300 7.386 o -7 -7 -4 65.371 66.606 1.953 20.979 o -7 -7 -3 49.991 50.467 2.120 27.045 o -7 -7 -2 24.848 20.704 1.141 66.294 o -7 -7 -1 5.017 5.108 0.729 293.840 o -7 -6 -11 167.691 181.254 2.995 6.351 o -7 -6 -10 204.636 216.365 3.463 4.849 o -7 -6 -9 326.643 340.855 4.509 2.470 o -7 -6 -8 100.024 108.067 2.125 12.570 o -7 -6 -7 138.698 142.622 6.931 5.768 o -7 -6 -6 77.489 72.825 2.843 16.311 o -7 -6 -5 184.169 194.680 5.862 4.776 o -7 -6 -4 154.642 142.251 2.424 7.754 o -7 -6 -3 51.197 44.593 1.718 29.308 o -7 -6 -2 20.095 22.531 0.877 77.985 o -7 -6 -1 74.665 78.712 1.685 18.363 o -7 -5 -14 139.633 125.097 5.759 6.741 o -7 -5 -13 41.112 38.895 1.583 36.272 o -7 -5 -12 51.878 51.862 2.886 23.115 o -7 -5 -11 17.461 16.568 1.009 91.590 o -7 -5 -10 13.398 11.170 0.727 130.696 o -7 -5 -9 95.489 94.796 6.238 8.456 o -7 -5 -8 0.493 1.862 0.319 1574.260 o -7 -5 -7 1.884 1.995 0.476 759.941 o -7 -5 -6 67.654 67.328 1.994 20.306 o -7 -5 -5 23.401 25.142 0.840 68.425 o -7 -5 -4 97.417 102.056 2.258 12.994 o -7 -5 -3 114.421 125.879 2.290 10.519 o -7 -5 -2 99.070 92.897 1.516 13.980 o -7 -5 -1 2.323 2.966 0.312 677.877 o -7 -4 -17 112.875 96.155 2.477 11.641 o -7 -4 -16 61.996 52.121 4.598 15.349 o -7 -4 -15 48.303 43.412 1.831 30.290 o -7 -4 -14 74.609 78.231 1.660 18.455 o -7 -4 -13 77.374 87.473 1.515 17.362 o -7 -4 -12 12.213 11.615 0.587 141.993 o -7 -4 -11 67.433 69.019 1.440 21.250 o -7 -4 -10 50.586 54.745 1.308 28.892 o -7 -4 -9 38.710 41.530 1.249 38.707 o -7 -4 -8 41.208 44.068 1.204 36.510 o -7 -4 -7 104.309 109.078 1.883 12.316 o -7 -4 -6 14.663 14.412 0.708 114.613 o -7 -4 -5 57.797 54.939 1.392 26.004 o -7 -4 -4 225.773 234.163 3.893 4.216 o -7 -4 -3 57.634 55.374 1.475 25.777 o -7 -4 -2 19.398 28.380 1.296 66.999 o -7 -4 -1 158.692 160.850 2.629 7.136 o -7 -3 -18 29.130 27.865 1.376 52.274 o -7 -3 -17 39.890 42.367 4.407 19.959 o -7 -3 -16 79.993 76.434 7.458 7.916 o -7 -3 -15 96.330 91.220 1.810 14.141 o -7 -3 -14 7.074 9.748 0.657 205.057 o -7 -3 -13 44.849 42.206 2.371 29.299 o -7 -3 -12 54.925 60.033 1.702 25.277 o -7 -3 -11 5.756 6.538 0.502 280.504 o -7 -3 -10 158.413 149.855 2.941 7.239 o -7 -3 -9 10.098 10.553 0.543 167.342 o -7 -3 -8 45.053 44.809 1.486 32.978 o -7 -3 -7 3.310 3.719 0.421 483.276 o -7 -3 -6 4.021 6.286 0.535 341.094 o -7 -3 -5 326.966 334.739 4.712 2.474 o -7 -3 -4 58.438 50.643 2.199 24.076 o -7 -3 -3 221.518 225.234 4.932 4.144 o -7 -3 -2 20.394 19.734 1.468 70.378 o -7 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810.076 o 0 4 17 463.490 439.850 4.136 1.545 o 0 4 18 10.735 11.635 0.481 157.805 o 0 4 19 111.856 114.399 1.516 11.643 o 0 4 20 165.587 141.766 2.056 7.428 o 0 4 21 1.244 0.556 0.186 1719.600 o 0 4 22 72.414 77.061 1.532 19.173 o 0 4 23 89.481 76.952 1.677 16.106 o 0 4 24 1.262 5.536 0.460 586.237 o 0 4 25 42.254 29.286 0.993 41.797 o 0 4 26 76.453 71.561 1.743 18.602 o 0 4 27 0.028 2.995 1.224 398.066 o 0 4 28 2.689 2.295 0.418 629.478 o 0 4 29 445.418 438.687 4.595 1.599 o 0 4 30 160.232 144.540 9.627 4.027 o 0 5 1 695.343 674.065 7.390 0.762 o 0 5 2 64.647 72.740 2.116 20.102 o 0 5 3 103.668 85.464 2.265 13.195 o 0 5 4 974.827 940.970 13.773 0.403 o 0 5 5 0.817 2.166 0.560 923.219 o 0 5 6 567.115 566.544 8.394 1.013 o 0 5 7 94.549 108.323 5.038 9.628 o 0 5 8 369.082 397.155 3.768 2.068 o 0 5 9 704.305 680.258 5.487 0.766 o 0 5 10 39.966 45.407 0.839 38.246 o 0 5 11 22.470 44.496 0.788 55.091 o 0 5 12 3.272 2.606 0.245 587.985 o 0 5 13 8.065 11.339 0.450 190.840 o 0 5 14 415.118 393.431 3.884 1.841 o 0 5 15 130.076 143.245 2.221 9.026 o 0 5 16 92.866 114.789 1.751 13.269 o 0 5 17 178.555 177.311 2.737 6.155 o 0 5 18 7.000 12.779 0.505 193.054 o 0 5 19 192.760 182.546 2.906 5.641 o 0 5 20 44.963 54.260 1.197 31.785 o 0 5 21 323.928 326.519 4.177 2.567 o 0 5 22 149.522 180.601 3.059 6.950 o 0 5 23 50.069 54.553 1.657 28.027 o 0 5 24 128.058 144.496 2.602 8.907 o 0 5 25 130.023 146.085 2.502 8.812 o 0 5 26 8.898 7.533 0.561 200.429 o 0 5 27 56.255 49.013 1.667 26.760 o 0 5 28 17.509 14.451 0.849 98.712 o 0 5 29 7.746 6.304 0.513 234.370 o 0 6 0 444.807 481.758 4.132 1.537 o 0 6 1 326.475 300.767 2.448 2.757 o 0 6 2 104.548 104.592 1.464 12.800 o 0 6 3 482.979 509.246 6.161 1.320 o 0 6 4 131.759 146.937 1.778 9.019 o 0 6 5 356.868 400.058 3.759 2.129 o 0 6 6 6.096 6.528 0.388 281.419 o 0 6 7 32.224 29.145 0.791 52.512 o 0 6 8 618.052 613.036 4.442 0.948 o 0 6 9 12.858 15.332 0.550 125.878 o 0 6 10 0.258 0.807 0.319 2725.110 o 0 6 11 117.891 124.889 1.408 10.790 o 0 6 12 406.597 393.159 2.665 1.920 o 0 6 13 469.103 468.732 2.818 1.503 o 0 6 14 12.441 11.885 0.496 141.813 o 0 6 15 14.483 15.324 0.558 116.517 o 0 6 16 454.292 405.311 3.194 1.667 o 0 6 17 5.858 5.409 0.377 307.636 o 0 6 18 304.507 269.959 2.454 3.112 o 0 6 19 1.135 3.671 0.313 848.645 o 0 6 20 152.473 131.409 1.834 8.319 o 0 6 21 4.711 8.111 0.534 284.594 o 0 6 22 7.158 4.800 0.517 264.554 o 0 6 23 3.938 2.611 0.369 489.787 o 0 6 24 83.717 93.405 1.941 15.447 o 0 6 25 111.313 114.065 2.017 11.393 o 0 6 26 10.242 10.380 0.576 165.378 o 0 6 27 3.251 3.892 0.431 478.364 o 0 6 28 2.108 3.628 0.511 577.219 o 0 7 1 590.012 588.171 3.423 1.031 o 0 7 2 26.593 23.648 0.695 65.236 o 0 7 3 40.822 33.903 0.918 41.447 o 0 7 4 48.395 36.481 0.963 35.392 o 0 7 5 215.649 200.662 2.941 4.888 o 0 7 6 19.792 22.867 0.782 79.607 o 0 7 7 161.442 154.148 2.029 7.353 o 0 7 8 63.055 65.905 1.230 23.112 o 0 7 9 221.885 210.393 2.964 4.662 o 0 7 10 12.556 13.379 0.510 135.170 o 0 7 11 52.906 45.748 0.947 30.773 o 0 7 12 58.045 64.296 1.174 24.902 o 0 7 13 294.140 287.492 2.864 3.101 o 0 7 14 67.153 66.617 1.328 21.794 o 0 7 15 700.201 681.986 3.921 0.782 o 0 7 16 189.739 197.753 2.104 5.690 o 0 7 17 14.007 19.697 0.666 106.147 o 0 7 18 82.640 87.586 1.362 16.674 o 0 7 19 105.699 112.829 1.652 12.176 o 0 7 20 110.274 118.570 2.253 11.127 o 0 7 21 55.292 54.619 1.520 26.565 o 0 7 22 28.226 24.884 0.984 59.161 o 0 7 23 15.907 16.300 0.753 103.487 o 0 7 24 26.742 26.455 1.075 59.309 o 0 7 25 63.371 59.122 3.188 18.828 o 0 7 26 7.797 10.804 0.833 175.807 o 0 8 0 1546.230 1494.930 9.110 0.190 o 0 8 1 628.177 627.896 5.975 0.901 o 0 8 2 109.872 104.208 1.508 12.279 o 0 8 3 217.975 216.356 2.515 4.752 o 0 8 4 91.305 91.155 1.649 14.915 o 0 8 5 78.366 74.943 1.377 18.452 o 0 8 6 547.252 530.551 3.686 1.180 o 0 8 7 44.478 43.551 1.064 35.275 o 0 8 8 226.537 230.834 2.432 4.461 o 0 8 9 628.253 609.791 4.299 0.935 o 0 8 10 206.783 201.909 2.635 5.123 o 0 8 11 349.198 349.678 2.959 2.371 o 0 8 12 0.186 1.018 0.322 2627.490 o 0 8 13 155.956 137.190 1.875 8.002 o 0 8 14 4.789 6.814 0.500 306.829 o 0 8 15 199.668 200.423 3.154 5.196 o 0 8 16 17.644 19.567 0.685 92.088 o 0 8 17 10.384 12.833 0.624 150.620 o 0 8 18 33.293 39.808 1.040 44.609 o 0 8 19 58.607 53.593 1.728 25.059 o 0 8 20 33.783 36.394 1.366 43.632 o 0 8 21 10.972 14.183 0.891 130.687 o 0 8 22 74.369 77.710 1.732 18.438 o 0 8 23 2.935 3.096 0.477 529.437 o 0 9 1 3.063 4.109 0.423 487.125 o 0 9 2 8.902 8.598 0.461 197.862 o 0 9 3 9.697 8.971 0.476 183.868 o 0 9 4 19.781 18.359 0.671 87.386 o 0 9 5 81.548 80.272 1.388 17.413 o 0 9 6 385.158 399.690 3.084 2.000 o 0 9 7 0.116 0.493 0.217 5282.730 o 0 9 8 32.582 29.926 0.847 51.322 o 0 9 9 2.654 3.664 0.324 578.540 o 0 9 10 4.527 7.176 0.429 318.208 o 0 9 11 0.920 2.161 0.255 1264.430 o 0 9 12 51.245 49.235 1.169 30.160 o 0 9 13 11.633 14.463 0.755 130.527 o 0 9 14 1.560 2.606 0.341 858.864 o 0 9 15 1.307 2.858 0.351 885.993 o 0 9 16 18.137 21.145 0.815 86.026 o 0 9 17 19.081 30.141 1.735 59.139 o 0 9 18 6.902 6.990 0.817 216.639 o 0 9 19 24.130 26.282 1.431 59.112 o 0 9 20 6.255 8.473 0.766 220.018 o 0 10 0 5.737 10.172 1.052 186.881 o 0 10 1 49.711 53.515 2.143 26.528 o 0 10 2 181.987 189.779 2.639 5.900 o 0 10 3 103.388 101.201 1.605 12.994 o 0 10 4 100.545 103.282 1.614 13.174 o 0 10 5 86.235 83.010 1.439 16.397 o 0 10 6 289.640 292.683 2.664 3.135 o 0 10 7 19.340 18.927 0.715 87.256 o 0 10 8 6.174 4.861 0.349 308.686 o 0 10 9 2.188 1.872 0.229 852.771 o 0 10 10 43.865 47.370 1.205 34.049 o 0 10 11 5.429 9.246 0.671 237.926 o 0 10 12 1.137 3.114 0.538 750.910 o 0 10 13 201.444 211.045 6.212 4.233 o 0 10 14 4.891 6.659 1.212 205.049 o 0 10 15 10.786 11.118 0.915 141.704 o 0 11 1 0.047 0.423 0.193 7149.800 o 0 11 2 55.131 56.294 1.692 25.839 o 0 11 3 30.385 30.526 2.548 38.037 o 0 11 4 0.524 0.727 0.321 2235.530 o 0 11 5 0.280 0.449 0.257 3788.030 o 0 11 6 21.089 19.756 1.120 75.152 o 0 11 7 69.172 75.056 2.122 18.959 o 0 11 8 28.620 30.450 1.319 51.931 o 1 0 4 1790.950 1544.620 9.908 0.155 o 1 0 5 652.964 598.977 3.914 0.907 o 1 0 7 2.893 1.252 0.207 768.675 o 1 0 8 1265.940 1285.310 26.483 0.217 o 1 0 9 3138.980 3228.010 21.173 0.048 o 1 0 10 75.885 74.838 1.730 18.426 o 1 0 11 1.000 0.504 0.154 2119.040 o 1 0 12 1088.590 1104.840 14.546 0.325 o 1 0 13 1839.060 1639.210 10.889 0.145 o 1 0 14 18.469 16.251 1.214 84.365 o 1 0 15 136.481 128.884 3.000 8.648 o 1 0 16 299.637 296.733 3.001 2.989 o 1 0 17 1021.050 1090.570 6.053 0.382 o 1 0 18 163.495 187.266 2.660 6.492 o 1 0 19 342.047 320.705 2.980 2.525 o 1 0 20 21.446 22.811 0.782 75.647 o 1 0 21 1103.890 1142.830 6.640 0.338 o 1 0 22 562.428 563.030 5.097 1.090 o 1 0 23 47.468 40.920 1.236 33.732 o 1 0 24 511.633 489.680 4.487 1.309 o 1 0 25 32.987 32.059 1.155 47.770 o 1 0 26 0.015 0.446 0.218 6833.530 o 1 0 27 0.289 0.455 0.225 4026.460 o 1 0 28 19.239 16.570 0.789 90.100 o 1 0 29 478.779 463.568 3.930 1.458 o 1 0 30 173.168 178.264 3.004 6.226 o 1 0 31 25.299 25.974 1.167 60.859 o 1 0 32 12.981 14.443 0.786 121.408 o 1 1 2 359.880 319.534 5.758 2.229 o 1 1 7 787.787 853.450 9.847 0.565 o 1 1 8 757.859 682.457 5.973 0.700 o 1 1 9 959.955 923.618 11.821 0.426 o 1 1 10 79.065 76.734 2.314 16.773 o 1 1 11 169.543 165.390 4.292 6.053 o 1 1 12 1149.850 1161.580 15.560 0.294 o 1 1 13 56.088 52.437 1.266 27.347 o 1 1 14 870.217 874.483 7.813 0.513 o 1 1 15 137.687 138.739 5.871 6.518 o 1 1 16 31.167 35.252 0.992 49.081 o 1 1 17 457.894 459.592 3.394 1.547 o 1 1 18 94.876 86.752 1.317 15.029 o 1 1 19 26.052 30.447 0.808 59.729 o 1 1 20 677.453 673.705 5.762 0.801 o 1 1 21 838.264 810.919 6.224 0.567 o 1 1 22 211.195 212.210 2.488 4.939 o 1 1 23 128.217 125.933 1.934 9.792 o 1 1 24 177.410 179.717 2.324 6.259 o 1 1 25 38.157 40.562 1.103 40.136 o 1 1 26 111.486 109.256 2.096 11.520 o 1 1 27 18.091 16.060 0.800 94.628 o 1 1 28 68.603 65.850 1.543 21.164 o 1 1 29 1.107 1.264 0.266 1416.580 o 1 1 30 42.289 42.308 1.275 36.085 o 1 1 31 4.130 4.883 0.422 388.240 o 1 1 32 136.944 126.168 12.131 3.365 o 1 2 0 586.898 577.123 3.848 1.043 o 1 2 1 881.069 875.029 4.299 0.521 o 1 2 2 9.550 13.634 0.951 139.788 o 1 2 3 206.626 215.782 8.034 3.610 o 1 2 4 156.421 172.030 21.499 1.346 o 1 2 6 878.060 765.446 6.733 0.552 o 1 2 7 205.889 212.077 2.446 5.063 o 1 2 8 726.243 722.774 5.029 0.719 o 1 2 9 2663.610 2755.120 126.009 0.028 o 1 2 10 1023.980 1070.670 57.019 0.146 o 1 2 11 2873.160 2864.550 93.874 0.035 o 1 2 12 570.179 658.251 13.783 0.811 o 1 2 13 1753.290 1802.200 52.502 0.096 o 1 2 14 210.648 218.920 7.502 3.690 o 1 2 15 509.221 523.618 5.731 1.244 o 1 2 16 63.505 62.515 1.204 23.501 o 1 2 17 569.918 565.090 4.389 1.083 o 1 2 18 23.712 24.018 0.841 68.908 o 1 2 19 226.468 240.121 2.582 4.360 o 1 2 20 540.296 518.821 3.884 1.208 o 1 2 21 387.835 406.776 3.516 1.953 o 1 2 22 107.628 107.349 1.933 12.055 o 1 2 23 68.240 71.880 1.482 20.667 o 1 2 24 102.899 96.384 1.713 13.213 o 1 2 25 120.183 120.680 1.904 10.530 o 1 2 26 85.098 72.936 1.560 17.232 o 1 2 27 121.770 126.642 2.025 10.145 o 1 2 28 1.922 1.945 0.276 890.700 o 1 2 29 28.725 30.075 1.097 54.010 o 1 2 30 23.186 23.608 1.219 65.615 o 1 2 31 79.527 81.910 1.956 16.872 o 1 2 32 8.872 8.198 0.828 178.858 o 1 3 0 184.354 181.401 2.660 5.946 o 1 3 1 885.259 809.311 5.926 0.535 o 1 3 2 132.981 126.106 2.177 9.373 o 1 3 3 888.233 870.804 4.621 0.516 o 1 3 4 1441.390 1352.770 9.526 0.219 o 1 3 5 425.816 441.359 7.878 1.531 o 1 3 6 260.065 274.607 10.550 2.402 o 1 3 7 2080.870 2317.580 254.061 0.011 o 1 3 8 276.028 325.311 53.388 0.246 o 1 3 9 3068.690 3735.130 835.700 0.001 o 1 3 10 1572.410 1959.710 548.720 0.002 o 1 3 11 1889.590 1979.380 84.890 0.058 o 1 3 12 1648.070 1677.730 48.901 0.110 o 1 3 13 96.019 76.055 3.295 13.132 o 1 3 14 83.844 70.856 1.493 17.699 o 1 3 15 17.198 23.056 0.759 86.841 o 1 3 16 231.678 240.763 2.122 4.317 o 1 3 17 371.261 379.882 2.785 2.142 o 1 3 18 174.369 175.634 2.005 6.496 o 1 3 19 592.105 569.462 3.687 1.042 o 1 3 20 285.525 293.979 2.691 3.170 o 1 3 21 31.161 34.594 0.944 49.736 o 1 3 22 168.456 161.235 2.291 6.876 o 1 3 23 200.862 194.680 2.429 5.385 o 1 3 24 275.846 256.944 3.036 3.463 o 1 3 25 256.719 261.947 3.193 3.658 o 1 3 26 68.835 63.225 1.446 21.594 o 1 3 27 402.867 399.691 3.661 1.892 o 1 3 28 8.451 7.640 0.469 211.937 o 1 3 29 45.653 44.544 1.220 33.794 o 1 3 30 111.256 106.763 2.706 11.142 o 1 3 31 58.875 51.109 2.187 23.926 o 1 4 0 894.218 836.359 6.536 0.516 o 1 4 1 630.183 647.142 8.236 0.852 o 1 4 2 135.364 125.580 7.129 5.921 o 1 4 3 230.276 235.801 3.369 4.219 o 1 4 4 62.137 70.633 2.501 19.897 o 1 4 5 434.824 444.402 6.407 1.561 o 1 4 6 38.021 50.622 8.396 8.442 o 1 4 7 819.707 789.465 9.147 0.571 o 1 4 8 161.631 163.170 4.290 6.315 o 1 4 9 582.474 628.300 12.590 0.843 o 1 4 10 75.489 64.631 2.924 17.045 o 1 4 11 98.989 107.303 3.602 11.129 o 1 4 12 2425.250 2564.070 50.429 0.063 o 1 4 13 445.763 414.918 4.608 1.642 o 1 4 14 264.533 272.661 2.463 3.557 o 1 4 15 1264.340 1301.630 12.343 0.257 o 1 4 16 24.380 32.039 0.969 59.687 o 1 4 17 54.752 63.233 1.064 26.360 o 1 4 18 49.490 55.724 0.998 29.960 o 1 4 19 54.900 52.419 1.069 28.266 o 1 4 20 72.977 76.610 1.298 19.431 o 1 4 21 230.846 225.785 2.745 4.387 o 1 4 22 11.479 7.887 0.478 169.301 o 1 4 23 42.779 37.456 1.263 37.319 o 1 4 24 20.949 17.164 0.922 81.983 o 1 4 25 170.183 177.436 2.849 6.378 o 1 4 26 110.362 115.711 2.216 11.260 o 1 4 27 15.504 15.607 0.787 105.940 o 1 4 28 240.536 229.101 4.641 3.892 o 1 4 29 44.121 42.259 1.397 34.520 o 1 4 30 7.715 7.209 0.866 197.458 o 1 5 0 0.865 4.356 1.295 304.322 o 1 5 1 394.055 382.771 9.062 1.677 o 1 5 2 166.385 169.343 5.956 5.354 o 1 5 3 496.319 496.439 10.370 1.163 o 1 5 4 165.295 147.195 4.061 6.554 o 1 5 5 901.303 877.957 15.407 0.442 o 1 5 6 536.062 529.445 8.646 1.101 o 1 5 7 171.104 182.763 2.309 6.414 o 1 5 8 1233.960 1248.160 12.720 0.269 o 1 5 9 1.996 3.105 0.362 700.360 o 1 5 10 956.707 973.137 5.427 0.442 o 1 5 11 79.280 92.943 1.327 16.816 o 1 5 12 743.359 735.822 6.315 0.685 o 1 5 13 351.779 373.532 3.424 2.255 o 1 5 14 468.985 504.964 4.120 1.419 o 1 5 15 414.105 405.514 3.147 1.841 o 1 5 16 211.449 196.711 2.203 5.149 o 1 5 17 230.238 245.697 3.964 4.043 o 1 5 18 342.436 299.163 3.156 2.595 o 1 5 19 25.569 27.766 0.840 62.299 o 1 5 20 395.480 392.468 3.946 1.935 o 1 5 21 176.450 174.573 2.396 6.352 o 1 5 22 9.663 13.718 0.671 151.207 o 1 5 23 93.101 90.915 2.077 14.262 o 1 5 24 200.356 197.608 2.930 5.262 o 1 5 25 22.354 20.110 0.904 75.127 o 1 5 26 113.344 109.033 2.601 10.985 o 1 5 27 12.691 11.923 0.831 129.222 o 1 5 28 125.388 131.497 2.467 9.507 o 1 5 29 3.170 3.433 0.380 519.616 o 1 6 0 0.029 1.996 0.497 1455.220 o 1 6 1 375.094 367.738 3.445 2.131 o 1 6 2 33.863 39.008 0.803 45.630 o 1 6 3 135.743 146.966 1.794 8.793 o 1 6 4 115.804 128.261 1.754 10.654 o 1 6 5 171.377 176.581 2.228 6.527 o 1 6 6 1167.460 1127.900 9.872 0.312 o 1 6 7 209.011 213.578 2.053 5.036 o 1 6 8 33.383 37.708 1.333 43.640 o 1 6 9 237.284 224.767 2.812 4.276 o 1 6 10 229.480 230.957 2.356 4.416 o 1 6 11 367.141 351.410 2.962 2.247 o 1 6 12 451.055 418.781 3.876 1.636 o 1 6 13 170.942 173.512 3.271 6.279 o 1 6 14 308.750 298.633 2.571 2.921 o 1 6 15 46.314 47.704 0.996 33.358 o 1 6 16 20.666 28.285 0.770 71.487 o 1 6 17 155.002 161.190 1.912 7.506 o 1 6 18 125.707 122.280 1.647 10.215 o 1 6 19 263.318 257.058 2.810 3.644 o 1 6 20 80.331 77.807 1.605 17.562 o 1 6 21 140.441 133.126 2.042 8.815 o 1 6 22 121.417 130.248 1.936 10.095 o 1 6 23 21.442 20.529 0.943 76.212 o 1 6 24 98.550 96.629 1.910 13.494 o 1 6 25 49.030 51.575 1.939 27.921 o 1 6 26 67.770 72.162 1.885 19.998 o 1 6 27 16.587 20.246 1.074 87.126 o 1 7 0 16.274 15.323 0.545 108.012 o 1 7 1 100.051 95.551 1.355 13.833 o 1 7 2 34.913 34.087 0.812 46.908 o 1 7 3 47.667 51.120 0.994 31.840 o 1 7 4 572.699 560.913 4.221 1.083 o 1 7 5 56.377 52.989 1.282 27.104 o 1 7 6 1929.520 1824.830 6.924 0.130 o 1 7 7 30.027 37.595 1.004 48.972 o 1 7 8 714.928 721.721 6.366 0.722 o 1 7 9 255.443 271.558 3.098 3.622 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318.140 15.640 1.509 o 2 3 11 149.562 142.629 5.752 6.199 o 2 3 12 277.878 311.289 7.506 2.623 o 2 3 13 132.207 129.869 1.527 9.591 o 2 3 14 77.893 84.611 1.259 17.806 o 2 3 15 60.916 63.428 1.025 24.420 o 2 3 16 112.393 121.367 1.567 11.281 o 2 3 17 125.465 139.851 1.706 9.630 o 2 3 18 29.316 24.509 0.755 59.677 o 2 3 19 232.350 219.138 2.782 4.414 o 2 3 20 35.163 39.985 1.152 42.369 o 2 3 21 491.445 492.131 5.011 1.351 o 2 3 22 33.786 34.859 1.343 44.434 o 2 3 23 530.030 518.732 5.114 1.212 o 2 3 24 62.069 60.800 1.733 23.018 o 2 3 25 182.955 182.974 2.480 6.007 o 2 3 26 0.396 0.833 0.228 2827.000 o 2 3 27 38.705 41.041 1.087 39.645 o 2 3 28 61.107 61.252 1.239 24.309 o 2 3 29 35.957 32.624 1.022 45.531 o 2 3 30 26.672 23.089 1.013 62.656 o 2 4 0 229.646 246.980 4.964 3.858 o 2 4 1 2089.400 2067.630 20.626 0.103 o 2 4 2 585.344 602.452 11.115 0.891 o 2 4 3 1283.990 1319.820 16.590 0.240 o 2 4 4 625.765 627.129 11.503 0.812 o 2 4 5 12.854 13.167 1.096 114.767 o 2 4 6 430.729 450.599 6.541 1.559 o 2 4 7 50.325 51.055 2.260 26.259 o 2 4 8 86.137 80.381 2.924 14.548 o 2 4 9 422.729 472.338 6.996 1.530 o 2 4 10 530.018 552.794 10.357 1.041 o 2 4 11 2.443 2.994 0.469 593.499 o 2 4 12 254.480 266.150 4.833 3.441 o 2 4 13 1116.350 1133.070 10.323 0.326 o 2 4 14 129.170 140.477 2.016 9.252 o 2 4 15 361.210 342.720 2.798 2.320 o 2 4 16 935.802 931.947 4.680 0.467 o 2 4 17 188.771 198.922 2.186 5.685 o 2 4 18 99.847 90.867 1.484 14.033 o 2 4 19 751.962 717.347 7.523 0.675 o 2 4 20 121.310 110.925 1.636 10.953 o 2 4 21 127.224 142.461 2.703 8.951 o 2 4 22 21.019 23.482 1.100 71.588 o 2 4 23 10.126 12.235 0.965 139.990 o 2 4 24 20.124 21.783 0.854 79.151 o 2 4 25 83.167 80.353 1.566 16.938 o 2 4 26 31.356 32.516 0.954 50.580 o 2 4 27 103.879 103.805 1.913 12.583 o 2 4 28 42.960 43.307 1.300 35.295 o 2 4 29 154.471 142.175 10.601 3.714 o 2 4 30 36.340 31.354 1.616 41.805 o 2 5 0 1078.940 1156.510 16.988 0.310 o 2 5 1 426.088 398.867 9.982 1.485 o 2 5 2 732.254 709.653 13.385 0.628 o 2 5 3 483.943 499.013 5.667 1.346 o 2 5 4 423.742 431.348 4.816 1.689 o 2 5 5 562.521 551.905 14.172 0.878 o 2 5 6 417.216 406.979 3.103 1.824 o 2 5 7 375.435 364.601 2.714 2.165 o 2 5 8 1300.090 1347.520 6.823 0.252 o 2 5 9 54.774 46.547 0.892 29.898 o 2 5 10 418.916 395.216 2.771 1.853 o 2 5 11 277.097 281.998 3.087 3.296 o 2 5 12 622.990 609.686 5.144 0.934 o 2 5 13 28.327 24.878 0.708 61.237 o 2 5 14 442.385 422.979 4.269 1.650 o 2 5 15 670.863 685.544 4.132 0.816 o 2 5 16 28.128 25.175 0.801 60.627 o 2 5 17 349.428 335.553 3.360 2.399 o 2 5 18 380.920 358.174 5.058 2.046 o 2 5 19 203.045 205.299 2.339 5.222 o 2 5 20 70.687 70.699 1.354 20.459 o 2 5 21 167.334 165.714 2.083 6.892 o 2 5 22 109.077 115.798 1.631 11.756 o 2 5 23 71.730 71.073 2.392 18.297 o 2 5 24 165.509 167.174 3.713 6.381 o 2 5 25 75.069 67.013 1.572 19.585 o 2 5 26 10.794 12.482 0.856 139.256 o 2 5 27 50.577 57.379 1.673 27.269 o 2 5 28 122.169 134.838 2.311 9.692 o 2 6 0 619.530 595.793 7.941 0.910 o 2 6 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2.609 5.088 o 2 7 1 17.908 20.288 0.754 88.997 o 2 7 2 9.525 7.048 0.465 199.893 o 2 7 3 162.340 166.099 1.736 7.158 o 2 7 4 321.084 288.184 3.213 2.815 o 2 7 5 149.018 151.967 2.339 7.820 o 2 7 6 325.472 304.460 3.891 2.662 o 2 7 7 528.658 523.783 6.696 1.174 o 2 7 8 716.921 702.689 10.284 0.687 o 2 7 9 271.342 264.631 3.361 3.438 o 2 7 10 78.770 78.314 1.426 18.014 o 2 7 11 128.958 115.934 1.728 10.172 o 2 7 12 123.233 122.135 1.886 10.273 o 2 7 13 108.404 108.310 1.842 12.008 o 2 7 14 68.822 61.868 1.307 22.005 o 2 7 15 28.811 29.298 0.891 56.033 o 2 7 16 101.171 95.613 1.569 13.551 o 2 7 17 23.244 20.069 0.829 74.128 o 2 7 18 33.779 31.123 0.993 48.511 o 2 7 19 117.908 118.382 1.854 10.809 o 2 7 20 4.587 7.580 0.466 304.637 o 2 7 21 44.166 48.196 1.073 34.126 o 2 7 22 123.137 122.796 1.582 10.405 o 2 7 23 30.268 35.245 1.303 47.790 o 2 7 24 226.673 248.505 9.735 2.861 o 2 7 25 195.656 193.971 3.389 5.308 o 2 8 0 254.468 245.412 3.303 3.788 o 2 8 1 791.340 776.861 4.592 0.629 o 2 8 2 29.211 24.945 0.828 58.975 o 2 8 3 80.986 89.269 1.870 16.212 o 2 8 4 28.740 29.857 1.081 54.263 o 2 8 5 87.183 74.269 2.110 16.072 o 2 8 6 27.237 30.157 1.347 53.441 o 2 8 7 753.391 721.499 6.633 0.679 o 2 8 8 202.361 198.490 3.412 5.098 o 2 8 9 68.888 65.962 1.696 20.800 o 2 8 10 137.337 134.473 2.392 8.787 o 2 8 11 76.507 71.334 1.377 19.150 o 2 8 12 196.844 210.289 2.686 5.246 o 2 8 13 65.367 71.147 1.335 21.666 o 2 8 14 208.971 219.054 2.281 4.945 o 2 8 15 111.534 118.035 1.820 11.341 o 2 8 16 135.031 127.310 1.632 9.456 o 2 8 17 30.264 36.288 0.983 49.541 o 2 8 18 17.108 16.494 0.639 100.393 o 2 8 19 72.765 82.545 1.333 18.846 o 2 8 20 50.304 42.604 1.000 32.615 o 2 8 21 92.617 87.245 5.935 9.130 o 2 9 0 0.010 0.509 0.206 6733.800 o 2 9 1 93.632 98.475 1.531 14.279 o 2 9 2 253.826 238.970 2.910 3.891 o 2 9 3 501.662 503.811 4.129 1.324 o 2 9 4 92.841 87.626 2.151 14.404 o 2 9 5 689.040 696.848 8.930 0.737 o 2 9 6 81.989 83.002 2.088 16.224 o 2 9 7 451.716 447.284 4.772 1.555 o 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77.725 2.108 17.536 o 2 11 2 193.155 194.618 3.288 5.385 o 2 11 3 213.080 214.299 3.424 4.709 o 2 11 4 422.211 434.672 4.776 1.690 o 3 0 1 294.137 268.303 20.556 1.165 o 3 0 2 742.797 780.721 6.226 0.663 o 3 0 3 2088.800 2115.310 84.188 0.054 o 3 0 4 2108.810 2259.610 9.360 0.101 o 3 0 5 57.343 62.980 4.487 15.575 o 3 0 6 32.266 41.682 3.539 26.693 o 3 0 7 118.566 148.296 3.861 8.484 o 3 0 8 886.969 1036.520 27.656 0.320 o 3 0 9 0.075 3.374 0.773 710.535 o 3 0 10 219.431 214.253 5.864 4.035 o 3 0 11 0.008 0.939 0.363 2930.590 o 3 0 12 26.252 19.315 0.814 68.811 o 3 0 13 732.416 707.548 4.261 0.726 o 3 0 14 76.067 86.626 1.387 17.806 o 3 0 15 296.018 304.365 3.945 2.912 o 3 0 16 0.574 1.976 0.222 1626.170 o 3 0 17 426.923 428.438 3.274 1.730 o 3 0 18 465.739 418.246 3.304 1.596 o 3 0 19 18.471 24.225 0.855 80.252 o 3 0 20 3.045 1.845 0.347 639.786 o 3 0 21 3.946 3.602 0.355 452.716 o 3 0 22 135.497 133.804 2.271 8.963 o 3 0 23 243.411 237.261 3.901 3.920 o 3 0 24 1.129 2.648 0.318 1000.990 o 3 0 25 370.755 356.745 3.543 2.184 o 3 0 26 70.110 85.020 1.911 18.256 o 3 0 27 51.429 49.204 2.041 27.079 o 3 0 28 5.284 6.981 0.541 283.568 o 3 0 29 34.100 34.751 1.329 44.313 o 3 0 30 48.656 52.654 1.516 29.442 o 3 0 31 166.504 157.525 2.344 6.999 o 3 1 0 1421.920 1531.240 165.439 0.025 o 3 1 1 2095.520 2178.300 212.914 0.014 o 3 1 2 1971.640 1781.350 94.532 0.051 o 3 1 3 2026.940 1927.070 109.793 0.041 o 3 1 4 2603.050 2390.300 41.659 0.064 o 3 1 5 217.563 240.126 3.933 4.295 o 3 1 6 331.797 344.439 9.141 2.014 o 3 1 7 177.940 172.045 6.660 4.796 o 3 1 8 3.093 5.059 0.518 425.127 o 3 1 9 249.558 247.752 6.252 3.361 o 3 1 10 597.987 561.410 9.447 0.941 o 3 1 11 468.896 460.730 8.662 1.338 o 3 1 12 290.461 292.372 3.145 3.092 o 3 1 13 347.745 344.185 3.160 2.390 o 3 1 14 12.114 12.906 0.461 141.309 o 3 1 15 322.373 322.879 4.520 2.566 o 3 1 16 103.372 98.260 1.364 13.312 o 3 1 17 591.281 602.914 3.652 1.012 o 3 1 18 31.466 30.472 0.837 52.352 o 3 1 19 144.738 140.370 1.814 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1456.140 7.487 0.198 o 4 4 9 69.991 85.263 1.902 18.271 o 4 4 10 406.180 410.432 4.188 1.832 o 4 4 11 25.150 25.748 0.934 63.780 o 4 4 12 1056.440 1048.690 9.399 0.366 o 4 4 13 2101.240 2008.820 20.993 0.104 o 4 4 14 190.238 187.351 2.506 5.736 o 4 4 15 45.422 45.067 1.231 33.738 o 4 4 16 20.496 20.810 1.073 76.089 o 4 4 17 100.143 101.009 1.904 13.101 o 4 4 18 293.541 284.128 3.127 3.104 o 4 4 19 91.083 90.785 1.731 14.886 o 4 4 20 340.789 340.600 3.224 2.449 o 4 4 21 80.297 84.295 2.536 15.677 o 4 4 22 154.946 150.484 3.084 7.301 o 4 4 23 151.981 144.743 2.398 7.826 o 4 4 24 39.398 39.225 1.189 39.319 o 4 4 25 150.566 148.532 1.833 8.002 o 4 4 26 69.011 69.490 1.240 21.143 o 4 4 27 10.237 9.602 0.798 158.695 o 4 5 0 30.019 40.510 1.149 46.601 o 4 5 1 64.848 59.719 1.391 23.166 o 4 5 2 8.422 13.520 0.754 159.620 o 4 5 3 69.876 64.451 1.587 20.953 o 4 5 4 709.810 697.501 7.607 0.729 o 4 5 5 33.902 34.824 0.892 47.132 o 4 5 6 407.867 413.598 6.247 1.728 o 4 5 7 96.293 90.117 2.021 13.998 o 4 5 8 978.440 970.008 7.718 0.424 o 4 5 9 150.744 147.204 2.266 7.877 o 4 5 10 746.324 726.763 6.785 0.682 o 4 5 11 83.774 90.407 1.783 15.837 o 4 5 12 8.439 8.482 0.566 199.921 o 4 5 13 172.457 173.010 2.513 6.474 o 4 5 14 8.889 10.866 0.990 154.201 o 4 5 15 62.820 65.550 1.560 22.588 o 4 5 16 124.558 123.965 2.109 10.002 o 4 5 17 76.427 70.967 1.567 18.934 o 4 5 18 25.414 23.259 0.879 66.036 o 4 5 19 46.100 45.463 1.180 33.464 o 4 5 20 38.232 42.520 1.095 39.424 o 4 5 21 7.207 8.023 0.458 231.729 o 4 5 22 180.166 183.420 2.614 6.049 o 4 5 23 127.735 143.780 2.190 9.158 o 4 5 24 2.583 4.693 0.323 530.044 o 4 5 25 58.899 54.326 1.180 26.228 o 4 6 0 319.111 361.966 4.205 2.469 o 4 6 1 232.221 229.644 3.379 4.236 o 4 6 2 50.417 38.332 1.157 33.152 o 4 6 3 189.166 183.760 2.879 5.726 o 4 6 4 194.286 179.800 2.035 5.823 o 4 6 5 412.053 397.148 2.857 1.878 o 4 6 6 255.223 261.482 4.006 3.580 o 4 6 7 110.082 105.718 1.924 11.915 o 4 6 8 73.528 73.313 1.604 19.213 o 4 6 9 187.340 174.196 2.745 5.942 o 4 6 10 229.110 236.272 2.983 4.293 o 4 6 11 450.440 437.498 4.044 1.599 o 4 6 12 414.428 413.722 3.909 1.797 o 4 6 13 125.692 119.837 2.081 10.079 o 4 6 14 91.701 86.745 1.546 15.251 o 4 6 15 211.660 209.195 2.339 4.985 o 4 6 16 124.162 123.712 1.752 10.223 o 4 6 17 138.217 134.935 2.011 8.900 o 4 6 18 10.748 13.702 0.632 143.785 o 4 6 19 27.413 26.323 0.826 60.655 o 4 6 20 54.323 59.391 1.225 26.832 o 4 6 21 130.125 128.267 2.446 9.334 o 4 6 22 63.178 66.146 1.799 21.899 o 4 6 23 9.120 9.570 0.650 178.796 o 4 6 24 52.778 55.555 2.681 23.213 o 4 7 0 84.724 60.940 1.521 18.384 o 4 7 1 90.178 84.409 1.584 15.579 o 4 7 2 119.149 105.052 1.745 11.296 o 4 7 3 25.352 30.328 0.936 59.809 o 4 7 4 888.890 866.534 4.963 0.516 o 4 7 5 137.845 140.678 2.097 8.729 o 4 7 6 43.133 48.539 1.356 33.543 o 4 7 7 34.743 34.494 1.017 45.813 o 4 7 8 188.581 186.389 2.181 5.863 o 4 7 9 175.769 165.944 2.389 6.516 o 4 7 10 176.683 182.861 2.937 6.072 o 4 7 11 4.033 4.888 0.417 394.373 o 4 7 12 132.880 137.881 2.085 9.082 o 4 7 13 316.262 333.645 4.331 2.587 o 4 7 14 47.266 57.095 1.147 30.244 o 4 7 15 20.464 21.105 0.679 81.435 o 4 7 16 0.433 1.599 0.336 1716.860 o 4 7 17 146.288 153.540 2.260 7.937 o 4 7 18 15.391 17.590 0.735 103.325 o 4 7 19 4.820 6.701 0.438 315.062 o 4 7 20 5.715 4.250 0.379 334.488 o 4 7 21 261.012 285.919 11.507 2.218 o 4 8 0 34.392 39.219 1.131 43.422 o 4 8 1 19.672 15.650 0.723 91.261 o 4 8 2 50.777 53.072 1.299 29.179 o 4 8 3 8.260 10.022 0.568 191.402 o 4 8 4 10.728 14.560 0.874 131.757 o 4 8 5 415.763 431.238 7.900 1.581 o 4 8 6 60.332 67.216 1.809 22.452 o 4 8 7 16.204 19.115 1.708 74.472 o 4 8 8 20.145 16.029 0.895 86.301 o 4 8 9 58.171 65.234 3.550 18.099 o 4 8 10 46.185 47.171 3.360 23.055 o 4 8 11 7.808 9.132 0.573 204.131 o 4 8 12 101.835 109.215 2.527 11.980 o 4 8 13 34.576 39.007 1.083 43.622 o 4 8 14 28.568 33.510 0.965 53.139 o 4 8 15 64.626 67.541 1.566 21.869 o 4 8 16 99.633 107.296 3.600 11.084 o 4 8 17 17.590 18.467 0.732 93.397 o 4 8 18 11.680 10.084 0.691 148.682 o 4 9 0 4.249 10.510 0.637 253.634 o 4 9 1 60.559 61.214 2.351 21.684 o 4 9 2 20.498 16.818 1.037 81.660 o 4 9 3 26.222 24.657 0.962 62.635 o 4 9 4 94.570 87.134 1.941 14.460 o 4 9 5 171.107 180.797 4.299 5.798 o 4 9 6 33.876 33.343 1.077 46.807 o 4 9 7 21.523 20.028 0.821 78.305 o 4 9 8 85.427 100.414 3.269 13.016 o 4 9 9 62.654 70.355 2.839 18.927 o 4 9 10 12.259 11.373 0.960 128.616 o 4 9 11 105.553 110.633 1.944 12.085 o 4 9 12 36.988 39.153 1.130 41.388 o 4 9 13 113.907 115.194 4.216 9.273 o 4 9 14 15.792 16.737 0.891 99.990 o 4 10 0 8.646 10.600 0.773 171.220 o 4 10 1 12.281 11.688 0.799 133.867 o 4 10 3 376.019 420.874 5.888 1.869 o 4 10 4 31.032 34.466 1.656 44.518 o 4 10 5 49.858 57.035 2.051 26.247 o 4 10 6 19.083 21.471 1.218 76.061 o 5 0 1 26.719 28.009 1.252 56.440 o 5 0 2 569.837 564.776 6.418 1.050 o 5 0 3 55.961 65.032 1.977 23.453 o 5 0 4 17.337 13.753 0.734 103.233 o 5 0 5 77.158 84.384 1.492 17.686 o 5 0 6 25.492 16.925 0.680 74.242 o 5 0 7 9.000 4.352 0.414 235.371 o 5 0 8 28.605 22.362 0.923 61.041 o 5 0 9 92.915 107.994 2.187 13.222 o 5 0 10 23.605 24.901 0.835 68.316 o 5 0 11 2.564 1.147 0.221 852.545 o 5 0 12 4.354 5.159 0.440 366.701 o 5 0 13 875.037 813.536 7.616 0.532 o 5 0 14 594.530 577.660 5.303 1.010 o 5 0 15 19.427 21.371 0.821 81.974 o 5 0 16 127.594 123.281 1.934 9.917 o 5 0 17 382.080 359.569 4.222 2.079 o 5 0 18 1.091 1.585 0.338 1227.960 o 5 0 19 91.370 84.642 2.030 14.911 o 5 0 20 122.527 115.751 2.328 10.282 o 5 0 21 158.402 150.028 2.605 7.367 o 5 0 22 3.680 4.716 0.486 406.671 o 5 0 23 0.843 0.655 0.233 2070.170 o 5 0 24 14.457 14.506 0.727 114.938 o 5 0 25 9.916 9.915 0.568 171.681 o 5 0 26 17.860 19.635 0.727 90.605 o 5 0 27 96.581 101.550 1.845 13.500 o 5 1 0 253.903 257.478 3.467 3.693 o 5 1 1 271.702 288.243 3.572 3.276 o 5 1 2 420.807 409.840 5.339 1.724 o 5 1 3 4.799 6.861 0.468 309.541 o 5 1 4 104.684 93.474 1.770 13.133 o 5 1 5 289.707 331.870 3.808 2.856 o 5 1 6 206.463 223.309 2.759 4.877 o 5 1 7 16.767 21.144 0.788 90.721 o 5 1 8 126.660 114.492 1.655 10.416 o 5 1 9 22.741 17.139 0.664 80.831 o 5 1 10 459.632 440.474 3.805 1.566 o 5 1 11 61.207 62.988 1.283 23.942 o 5 1 12 4.492 3.727 0.368 409.775 o 5 1 13 86.514 95.132 1.565 15.366 o 5 1 14 91.746 88.983 1.809 14.836 o 5 1 15 63.614 54.870 1.229 24.532 o 5 1 16 237.877 226.362 2.617 4.277 o 5 1 17 32.662 36.204 1.139 46.211 o 5 1 18 536.934 531.521 4.295 1.195 o 5 1 19 57.263 52.279 1.332 26.789 o 5 1 20 187.619 190.269 2.457 5.778 o 5 1 21 83.466 81.341 1.913 16.374 o 5 1 22 334.814 326.312 4.528 2.462 o 5 1 23 63.523 63.742 2.152 21.245 o 5 1 24 17.682 16.861 1.572 77.045 o 5 1 25 230.285 241.360 2.719 4.266 o 5 1 26 38.938 40.811 1.281 38.639 o 5 1 27 54.363 55.493 1.365 27.163 o 5 2 0 532.438 526.577 4.793 1.203 o 5 2 1 1063.990 1063.730 6.776 0.368 o 5 2 2 702.169 702.553 5.126 0.758 o 5 2 3 424.878 422.221 4.376 1.719 o 5 2 4 452.254 484.173 4.264 1.504 o 5 2 5 141.732 129.485 1.588 9.017 o 5 2 6 20.059 23.044 0.721 79.470 o 5 2 7 324.655 317.304 2.646 2.693 o 5 2 8 32.786 38.462 1.123 45.169 o 5 2 9 346.232 349.512 3.417 2.370 o 5 2 10 166.870 167.369 2.093 6.877 o 5 2 11 192.188 177.358 2.182 5.888 o 5 2 12 14.382 15.613 0.720 112.716 o 5 2 13 37.141 39.869 1.040 41.442 o 5 2 14 219.782 205.657 2.149 4.877 o 5 2 15 40.009 40.451 0.993 39.340 o 5 2 16 21.692 18.944 0.679 81.050 o 5 2 17 110.090 107.863 1.821 11.893 o 5 2 18 153.165 150.419 2.119 7.750 o 5 2 19 398.348 384.087 5.010 1.895 o 5 2 20 3.330 5.219 0.405 429.460 o 5 2 21 300.116 296.744 3.069 2.980 o 5 2 22 80.376 82.404 1.541 17.253 o 5 2 23 32.468 35.592 1.064 47.161 o 5 2 24 67.656 79.824 2.788 17.385 o 5 2 25 52.179 53.663 1.528 27.825 o 5 2 26 195.184 189.281 2.277 5.626 o 5 2 27 114.899 110.445 2.401 10.973 o 5 3 0 15.406 14.957 1.418 90.011 o 5 3 1 628.501 622.301 4.212 0.925 o 5 3 2 578.518 559.356 4.186 1.074 o 5 3 3 111.767 110.294 1.870 11.611 o 5 3 4 790.398 768.108 6.835 0.621 o 5 3 5 47.244 52.121 1.192 31.234 o 5 3 6 431.046 434.863 5.828 1.615 o 5 3 7 1271.660 1291.760 12.924 0.255 o 5 3 8 620.810 628.607 4.145 0.933 o 5 3 9 234.207 240.322 2.375 4.250 o 5 3 10 18.167 20.965 0.721 87.642 o 5 3 11 7.580 7.163 0.457 232.962 o 5 3 12 134.609 130.791 2.161 9.150 o 5 3 13 653.509 638.949 5.009 0.866 o 5 3 14 280.201 269.928 2.582 3.372 o 5 3 15 92.367 80.482 1.399 15.725 o 5 3 16 83.570 87.035 1.437 16.498 o 5 3 17 118.406 118.543 1.642 10.881 o 5 3 18 104.243 101.552 1.483 12.973 o 5 3 19 95.274 99.196 2.194 13.429 o 5 3 20 56.445 57.118 1.608 25.522 o 5 3 21 14.812 15.405 1.010 103.538 o 5 3 22 209.241 211.483 3.992 4.688 o 5 3 23 40.769 41.520 1.492 36.184 o 5 3 24 273.853 260.442 15.276 1.712 o 5 3 25 157.160 174.484 2.173 7.082 o 5 3 26 6.527 5.992 0.450 271.617 o 5 4 0 282.442 305.352 3.353 3.091 o 5 4 1 3.534 4.213 0.601 403.115 o 5 4 2 29.300 28.376 1.252 52.965 o 5 4 3 124.378 133.821 3.268 8.981 o 5 4 4 163.832 160.279 3.043 6.809 o 5 4 5 102.902 103.847 1.941 12.652 o 5 4 6 116.434 114.568 2.043 10.951 o 5 4 7 90.647 100.547 1.922 14.150 o 5 4 8 607.135 594.283 6.458 0.956 o 5 4 9 820.763 800.509 5.433 0.589 o 5 4 10 195.329 185.528 2.623 5.601 o 5 4 11 244.270 233.082 2.929 4.078 o 5 4 12 130.108 132.142 2.113 9.396 o 5 4 13 77.468 78.552 1.581 18.024 o 5 4 14 26.656 26.724 0.923 60.684 o 5 4 15 43.286 47.766 1.211 34.233 o 5 4 16 236.158 238.226 2.708 4.195 o 5 4 17 269.494 273.453 2.748 3.466 o 5 4 18 315.482 307.439 4.133 2.713 o 5 4 19 59.832 57.950 1.173 25.339 o 5 4 20 80.316 87.646 1.675 16.681 o 5 4 21 251.152 254.793 3.481 3.747 o 5 4 22 104.220 105.785 1.647 12.652 o 5 4 23 137.053 135.875 4.677 7.386 o 5 4 24 4.589 5.775 0.447 341.166 o 5 4 25 62.501 61.923 1.925 22.287 o 5 5 0 193.328 194.502 2.646 5.532 o 5 5 1 26.761 27.717 0.986 59.213 o 5 5 2 186.032 188.930 3.089 5.687 o 5 5 3 92.731 88.355 2.104 14.427 o 5 5 4 143.198 142.322 2.338 8.314 o 5 5 5 223.767 209.060 3.829 4.477 o 5 5 6 303.456 315.088 3.169 2.856 o 5 5 7 31.354 34.972 1.062 48.585 o 5 5 8 1968.820 1880.930 12.122 0.122 o 5 5 9 69.688 62.779 1.401 21.521 o 5 5 10 33.681 27.324 0.932 51.025 o 5 5 11 514.006 519.429 5.208 1.249 o 5 5 12 852.029 829.260 7.169 0.545 o 5 5 13 139.863 152.843 2.314 8.231 o 5 5 14 11.565 12.260 0.677 141.482 o 5 5 15 105.571 100.351 1.846 12.638 o 5 5 16 44.270 43.459 1.185 34.975 o 5 5 17 35.651 32.277 0.986 46.171 o 5 5 18 150.519 152.990 2.035 7.838 o 5 5 19 48.978 47.460 1.078 31.854 o 5 5 20 21.867 20.248 0.659 79.139 o 5 5 21 13.979 15.707 0.710 114.752 o 5 5 22 195.065 205.031 2.681 5.351 o 5 5 23 39.550 40.726 1.099 39.115 o 5 6 0 169.098 148.770 2.380 7.055 o 5 6 1 630.366 636.271 5.884 0.893 o 5 6 2 398.930 362.510 3.288 2.019 o 5 6 3 140.477 124.897 1.915 9.094 o 5 6 4 491.969 519.465 5.578 1.298 o 5 6 5 12.401 18.404 0.764 114.518 o 5 6 6 120.627 111.072 1.830 10.894 o 5 6 7 127.708 138.176 2.512 9.151 o 5 6 8 4.558 4.390 0.491 367.116 o 5 6 9 112.475 101.052 2.109 11.772 o 5 6 10 92.812 95.699 1.857 14.246 o 5 6 11 36.594 37.464 1.152 42.231 o 5 6 12 16.491 16.004 0.747 101.821 o 5 6 13 180.025 173.123 2.761 6.167 o 5 6 14 206.354 211.328 2.530 5.047 o 5 6 15 75.836 82.270 1.527 18.057 o 5 6 16 42.479 39.871 1.035 37.715 o 5 6 17 112.910 117.831 1.971 11.144 o 5 6 18 209.480 210.323 2.114 5.053 o 5 6 19 17.337 20.380 0.619 92.728 o 5 6 20 94.651 93.355 2.019 14.003 o 5 6 21 1.506 2.317 0.420 852.340 o 5 7 0 4.990 1.182 0.349 466.403 o 5 7 1 51.262 63.128 1.628 26.178 o 5 7 2 7.745 14.673 0.632 166.564 o 5 7 3 318.049 284.781 2.937 2.876 o 5 7 4 104.180 106.011 1.716 12.596 o 5 7 5 38.211 42.666 2.077 33.902 o 5 7 6 56.547 54.577 1.751 25.482 o 5 7 7 19.609 18.136 0.849 85.566 o 5 7 8 22.498 19.979 0.875 75.340 o 5 7 9 76.899 84.874 2.025 16.948 o 5 7 10 71.643 78.196 1.644 19.042 o 5 7 11 171.665 170.426 2.374 6.581 o 5 7 12 127.256 127.124 1.718 9.916 o 5 7 13 52.049 50.260 1.440 28.806 o 5 7 14 45.707 43.417 1.078 34.573 o 5 7 15 36.519 42.562 1.274 39.735 o 5 7 16 273.152 286.414 3.115 3.314 o 5 7 17 170.552 155.997 2.149 6.934 o 5 7 18 75.448 84.081 5.978 10.030 o 5 8 0 18.958 18.235 0.679 90.058 o 5 8 1 293.516 310.236 4.194 2.886 o 5 8 2 7.963 7.610 0.393 224.931 o 5 8 3 81.401 71.378 1.373 18.229 o 5 8 4 4.929 3.859 0.590 344.371 o 5 8 5 80.191 81.626 2.573 15.813 o 5 8 6 7.691 8.556 0.867 188.408 o 5 8 7 61.415 54.827 2.091 23.028 o 5 8 8 68.080 66.761 2.280 19.635 o 5 8 9 6.724 8.529 0.643 222.292 o 5 8 10 7.989 6.526 0.421 233.368 o 5 8 11 10.486 9.658 0.610 165.162 o 5 8 12 12.263 12.587 1.912 86.107 o 5 8 13 106.200 93.870 12.395 3.628 o 5 8 14 9.689 13.190 0.838 145.870 o 5 8 15 5.970 7.271 0.583 256.897 o 5 9 0 24.619 19.971 1.056 68.522 o 5 9 1 38.654 31.255 1.271 42.377 o 5 9 4 56.386 48.628 1.463 27.400 o 5 9 5 46.648 40.565 1.359 33.781 o 5 9 6 16.095 16.733 1.284 88.924 o 5 9 7 56.968 50.776 1.164 27.575 o 5 9 8 97.070 88.991 1.970 14.026 o 6 0 0 339.171 350.721 6.336 2.214 o 6 0 1 294.877 299.481 4.201 2.922 o 6 0 2 8.537 4.712 0.598 227.805 o 6 0 3 379.221 347.969 3.768 2.150 o 6 0 4 104.124 91.905 1.883 13.178 o 6 0 5 22.042 19.838 0.822 77.263 o 6 0 6 80.760 71.701 1.561 18.075 o 6 0 7 97.457 91.775 1.774 14.011 o 6 0 8 270.700 270.659 2.673 3.475 o 6 0 9 144.360 131.212 1.870 8.725 o 6 0 10 347.852 325.684 2.983 2.464 o 6 0 11 6.367 5.252 0.388 292.451 o 6 0 12 484.840 466.784 4.338 1.424 o 6 0 13 34.145 34.837 0.992 46.348 o 6 0 14 79.501 82.071 1.554 17.409 o 6 0 15 172.406 158.942 2.117 6.823 o 6 0 16 330.269 320.214 3.817 2.567 o 6 0 17 0.404 0.236 0.230 3953.120 o 6 0 18 24.692 23.044 0.904 67.298 o 6 0 19 182.632 195.679 2.523 5.826 o 6 0 20 186.810 179.577 2.701 5.892 o 6 0 21 327.168 317.522 2.979 2.654 o 6 0 22 48.487 50.963 1.105 31.186 o 6 0 23 188.990 194.545 3.393 5.460 o 6 0 24 220.719 229.718 5.396 4.017 o 6 1 0 125.637 133.348 2.949 9.140 o 6 1 1 219.449 226.847 3.523 4.455 o 6 1 2 688.261 665.584 6.006 0.790 o 6 1 3 25.442 20.416 0.866 68.770 o 6 1 4 136.544 134.124 2.353 8.858 o 6 1 5 131.789 135.966 1.936 9.266 o 6 1 6 146.995 153.729 2.062 7.971 o 6 1 7 1284.890 1211.540 6.161 0.273 o 6 1 8 133.279 128.280 1.884 9.429 o 6 1 9 205.640 186.917 2.279 5.390 o 6 1 10 495.834 445.554 4.169 1.427 o 6 1 11 485.213 492.279 4.938 1.370 o 6 1 12 349.272 321.912 3.075 2.462 o 6 1 13 708.852 667.914 4.382 0.777 o 6 1 14 224.094 222.440 2.268 4.606 o 6 1 15 143.305 135.441 1.739 8.717 o 6 1 16 156.679 152.596 2.087 7.563 o 6 1 17 70.526 70.795 1.389 20.430 o 6 1 18 161.306 161.894 2.022 7.207 o 6 1 19 411.639 415.992 3.683 1.812 o 6 1 20 102.743 104.239 1.784 12.773 o 6 1 21 2.499 2.982 0.323 645.073 o 6 1 22 48.745 49.304 1.303 30.840 o 6 1 23 94.279 96.907 1.647 14.197 o 6 1 24 60.308 52.525 1.120 26.180 o 6 2 0 1063.650 1022.120 7.358 0.375 o 6 2 1 862.382 852.110 5.660 0.537 o 6 2 2 2000.060 1921.840 8.895 0.119 o 6 2 3 305.785 330.241 4.288 2.686 o 6 2 4 524.486 501.678 4.905 1.251 o 6 2 5 219.411 218.943 2.814 4.651 o 6 2 6 232.368 254.653 2.930 4.096 o 6 2 7 79.328 71.500 1.645 18.232 o 6 2 8 7.244 6.331 0.635 234.053 o 6 2 9 144.116 150.874 2.462 8.016 o 6 2 10 137.042 144.632 2.085 8.673 o 6 2 11 324.242 307.606 3.027 2.716 o 6 2 12 14.750 16.585 0.660 109.953 o 6 2 13 115.249 107.817 1.639 11.565 o 6 2 14 1.710 2.967 0.371 763.568 o 6 2 15 188.371 185.054 1.911 5.938 o 6 2 16 219.389 213.915 1.995 4.818 o 6 2 17 61.419 60.303 1.275 24.287 o 6 2 18 161.228 166.236 2.191 7.079 o 6 2 19 384.685 388.653 4.537 1.974 o 6 2 20 175.398 179.353 2.472 6.290 o 6 2 21 6.384 6.263 0.624 254.791 o 6 2 22 35.402 34.373 1.309 43.509 o 6 2 23 35.383 39.759 1.299 41.452 o 6 2 24 26.891 25.401 0.758 62.747 o 6 3 0 61.550 62.599 1.506 23.439 o 6 3 1 209.979 218.045 3.588 4.700 o 6 3 2 53.802 54.905 1.533 26.997 o 6 3 3 40.930 34.552 1.275 39.445 o 6 3 4 184.760 192.969 3.529 5.547 o 6 3 5 280.014 293.714 3.500 3.163 o 6 3 6 27.009 29.783 1.009 57.193 o 6 3 7 148.541 146.641 2.205 8.012 o 6 3 8 132.729 125.975 2.128 9.416 o 6 3 9 73.997 72.606 1.611 19.180 o 6 3 10 30.023 30.693 1.044 52.499 o 6 3 11 103.346 101.648 1.740 12.876 o 6 3 12 198.668 179.581 2.559 5.605 o 6 3 13 43.040 39.149 0.970 37.830 o 6 3 14 231.118 229.570 2.283 4.408 o 6 3 15 67.262 69.278 1.225 21.607 o 6 3 16 3.093 4.410 0.324 495.127 o 6 3 17 267.943 273.284 2.253 3.526 o 6 3 18 14.123 13.090 0.650 122.573 o 6 3 19 52.855 55.818 1.429 27.473 o 6 3 20 52.183 60.159 1.394 27.030 o 6 3 21 54.955 56.159 1.252 27.117 o 6 3 22 61.518 64.909 1.642 22.832 o 6 3 23 169.204 187.144 3.443 6.070 o 6 4 0 126.864 137.669 3.100 8.858 o 6 4 1 158.312 154.808 3.291 7.004 o 6 4 2 230.661 216.715 3.916 4.275 o 6 4 3 189.915 192.139 3.803 5.353 o 6 4 4 133.483 131.796 3.742 8.253 o 6 4 5 206.329 201.227 3.184 5.032 o 6 4 6 401.530 396.339 4.440 1.877 o 6 4 7 276.569 271.727 3.656 3.305 o 6 4 8 74.883 79.790 1.974 17.775 o 6 4 9 54.131 59.541 1.695 25.629 o 6 4 10 231.765 226.200 3.269 4.290 o 6 4 11 291.350 276.533 3.112 3.168 o 6 4 12 45.980 48.226 1.282 32.465 o 6 4 13 224.879 234.045 2.950 4.390 o 6 4 14 85.025 87.221 1.522 16.177 o 6 4 15 23.956 24.313 0.786 68.702 o 6 4 16 6.665 6.403 0.570 251.937 o 6 4 17 0.928 2.499 0.274 1154.160 o 6 4 18 46.234 56.213 1.393 30.130 o 6 4 19 84.600 94.528 1.680 15.550 o 6 4 20 23.894 27.267 1.504 57.777 o 6 4 21 95.225 96.189 4.324 10.886 o 6 4 22 79.450 84.700 2.229 16.259 o 6 5 0 89.700 100.840 1.990 14.173 o 6 5 1 129.755 128.568 2.798 9.139 o 6 5 2 2.985 2.265 0.297 635.269 o 6 5 3 98.621 94.585 1.793 13.704 o 6 5 4 27.066 28.912 0.956 58.173 o 6 5 5 108.525 104.779 1.782 12.199 o 6 5 6 50.923 53.494 1.258 29.151 o 6 5 7 16.679 11.862 0.598 113.343 o 6 5 8 86.687 82.399 1.645 16.153 o 6 5 9 240.525 226.663 2.993 4.181 o 6 5 10 88.659 97.311 1.739 14.772 o 6 5 11 49.874 46.589 1.185 31.319 o 6 5 12 227.582 233.986 3.254 4.297 o 6 5 13 105.467 108.590 1.975 12.162 o 6 5 14 2.568 2.068 0.375 685.349 o 6 5 15 176.773 176.376 2.332 6.329 o 6 5 16 261.511 257.446 3.123 3.632 o 6 5 17 63.894 66.050 1.280 22.780 o 6 5 18 61.069 64.046 1.571 23.227 o 6 5 19 5.352 5.631 0.456 313.122 o 6 5 20 46.202 47.275 1.158 33.021 o 6 6 0 176.370 159.959 4.056 6.032 o 6 6 1 92.361 81.058 1.735 15.352 o 6 6 2 129.864 136.716 2.390 9.136 o 6 6 3 47.252 49.566 1.185 31.851 o 6 6 4 184.332 187.341 2.264 5.953 o 6 6 5 56.800 64.325 1.306 25.014 o 6 6 6 22.920 23.920 0.980 68.945 o 6 6 7 4.476 5.200 0.483 353.330 o 6 6 8 150.813 147.815 2.343 7.831 o 6 6 9 50.021 49.392 1.335 30.158 o 6 6 10 19.959 21.782 1.307 72.173 o 6 6 11 8.434 6.757 0.495 218.267 o 6 6 12 64.086 65.150 1.412 22.607 o 6 6 13 95.075 91.042 1.610 14.487 o 6 6 14 64.275 62.069 1.265 23.240 o 6 6 15 31.913 35.986 0.919 48.379 o 6 6 16 10.736 12.107 0.508 154.773 o 6 6 17 4.824 5.254 0.410 347.205 o 6 6 18 20.996 17.585 0.970 80.511 o 6 7 0 4.622 5.394 0.414 352.459 o 6 7 1 52.535 46.139 1.138 30.360 o 6 7 2 1.587 3.164 0.331 791.021 o 6 7 3 67.874 66.319 1.181 21.885 o 6 7 4 86.025 80.827 2.456 15.271 o 6 7 5 44.907 44.400 1.163 34.443 o 6 7 6 44.709 42.115 1.122 35.344 o 6 7 7 76.419 74.343 1.457 18.769 o 6 7 8 10.888 10.133 0.538 161.605 o 6 7 9 56.980 56.343 1.473 25.835 o 6 7 10 72.262 68.603 1.292 20.433 o 6 7 11 26.679 28.371 0.804 60.375 o 6 7 12 10.324 7.535 0.401 188.043 o 6 7 13 16.386 16.115 0.685 103.261 o 6 7 14 8.246 8.730 0.478 205.977 o 6 8 0 4.555 4.920 0.375 372.243 o 6 8 1 22.811 17.622 1.046 74.866 o 6 8 2 22.796 22.338 0.765 73.334 o 6 8 3 43.050 38.167 1.368 36.440 o 6 8 4 10.984 12.299 0.796 141.090 o 6 8 5 17.330 17.774 0.959 91.120 o 6 8 6 46.065 42.163 1.458 33.253 o 6 8 7 18.344 19.105 0.977 85.590 o 6 8 8 42.011 37.501 1.329 37.473 o 6 8 9 59.341 55.525 1.565 24.977 o 7 0 1 128.479 131.932 3.395 8.728 o 7 0 2 5.730 4.907 0.520 304.736 o 7 0 3 9.157 7.078 0.611 196.901 o 7 0 4 392.767 393.145 4.131 1.939 o 7 0 5 9.554 7.349 0.546 193.182 o 7 0 6 2.358 3.556 0.382 603.421 o 7 0 7 225.852 227.294 2.765 4.460 o 7 0 8 503.434 462.669 4.091 1.379 o 7 0 9 1.655 3.504 0.381 716.150 o 7 0 10 22.083 21.494 0.760 75.957 o 7 0 11 288.614 319.164 2.809 3.001 o 7 0 12 600.805 566.593 4.793 1.015 o 7 0 13 265.401 260.067 2.512 3.624 o 7 0 14 14.833 15.672 0.700 110.856 o 7 0 15 2.953 1.942 0.270 673.459 o 7 0 16 5.814 5.774 0.412 299.609 o 7 0 17 11.194 13.154 0.721 139.317 o 7 0 18 8.976 6.534 0.621 202.978 o 7 0 19 358.004 343.626 9.366 1.876 o 7 0 20 50.059 54.491 1.522 28.495 o 7 0 21 6.552 5.237 0.680 256.721 o 7 1 0 51.293 58.700 1.769 26.475 o 7 1 1 4.267 4.392 0.445 390.210 o 7 1 2 313.482 314.945 3.434 2.750 o 7 1 3 481.075 468.209 4.164 1.438 o 7 1 4 257.251 242.468 4.000 3.677 o 7 1 5 157.237 168.595 2.514 7.084 o 7 1 6 68.675 64.663 1.520 21.328 o 7 1 7 43.536 42.891 1.238 35.341 o 7 1 8 243.622 249.432 2.961 3.958 o 7 1 9 260.499 249.570 2.912 3.721 o 7 1 10 164.633 173.466 2.380 6.769 o 7 1 11 153.943 145.831 2.131 7.813 o 7 1 12 13.015 11.413 0.597 136.525 o 7 1 13 4.022 6.038 0.381 370.032 o 7 1 14 65.753 63.099 1.143 22.906 o 7 1 15 10.722 12.734 0.594 149.277 o 7 1 16 27.779 26.621 0.809 60.002 o 7 1 17 108.168 111.378 1.915 11.842 o 7 1 18 11.929 13.208 0.640 136.556 o 7 1 19 38.787 40.510 1.039 39.992 o 7 1 20 107.291 19.416 55.048 0.247 o 7 1 21 234.032 240.371 4.395 3.950 o 7 2 0 275.353 276.032 4.246 3.229 o 7 2 1 329.758 324.700 4.763 2.486 o 7 2 2 14.516 17.399 0.819 105.591 o 7 2 3 92.787 80.714 1.719 15.334 o 7 2 4 4.418 4.821 0.447 370.750 o 7 2 5 179.726 176.111 2.951 6.078 o 7 2 6 64.112 55.797 1.659 23.322 o 7 2 7 134.176 120.313 2.049 9.539 o 7 2 8 136.398 139.010 2.161 8.823 o 7 2 9 40.436 38.064 1.123 39.313 o 7 2 10 122.989 120.540 1.958 10.307 o 7 2 11 265.637 260.437 3.330 3.538 o 7 2 12 79.393 79.058 1.366 17.911 o 7 2 13 2.438 3.845 0.314 597.080 o 7 2 14 66.893 61.299 1.121 22.876 o 7 2 15 2.254 2.077 0.219 814.814 o 7 2 16 60.347 64.182 1.454 23.667 o 7 2 17 64.103 65.554 1.272 22.803 o 7 2 18 1.537 1.426 0.181 1195.090 o 7 2 19 172.652 172.975 2.598 6.445 o 7 2 20 89.462 12.789 43.907 0.387 o 7 3 0 40.566 50.128 1.332 34.589 o 7 3 1 36.389 25.809 0.955 48.793 o 7 3 2 20.957 22.159 0.883 76.278 o 7 3 3 221.571 227.920 2.770 4.532 o 7 3 4 59.633 56.771 1.384 25.135 o 7 3 5 326.193 341.740 3.346 2.546 o 7 3 6 4.143 5.412 0.492 362.286 o 7 3 7 3.397 4.765 0.475 425.179 o 7 3 8 44.898 44.492 1.173 34.388 o 7 3 9 10.466 10.551 0.571 162.481 o 7 3 10 158.232 155.581 2.109 7.430 o 7 3 11 5.798 6.860 0.412 283.245 o 7 3 12 55.776 59.442 1.612 25.355 o 7 3 13 44.548 42.594 1.063 35.512 o 7 3 14 7.151 10.374 0.513 208.363 o 7 3 15 97.069 106.322 1.524 13.447 o 7 3 16 80.172 89.315 1.651 16.604 o 7 3 17 40.258 49.045 1.156 35.788 o 7 3 18 28.727 29.023 1.007 55.417 o 7 3 19 26.017 29.112 1.325 55.856 o 7 4 0 162.840 141.365 2.777 7.297 o 7 4 1 158.637 157.199 2.605 7.217 o 7 4 2 18.822 28.511 1.122 70.608 o 7 4 3 57.592 55.176 1.547 25.631 o 7 4 4 225.321 239.369 3.194 4.299 o 7 4 5 57.728 57.144 1.545 25.279 o 7 4 6 14.110 13.920 0.771 117.091 o 7 4 7 104.046 105.750 1.834 12.535 o 7 4 8 41.569 44.341 1.057 36.792 o 7 4 9 38.661 39.647 1.075 40.230 o 7 4 10 50.536 52.465 1.203 29.679 o 7 4 11 67.138 69.341 1.407 21.337 o 7 4 12 12.141 11.410 0.620 142.275 o 7 4 13 77.860 90.377 1.427 17.144 o 7 4 14 74.555 85.057 1.321 18.291 o 7 4 15 48.044 50.206 0.956 31.976 o 7 4 16 62.081 65.841 2.149 21.345 o 7 4 17 113.062 126.959 2.441 10.474 o 7 4 18 1.558 1.099 0.299 1161.930 o 7 5 0 358.818 372.190 3.304 2.220 o 7 5 1 2.372 3.682 0.343 606.993 o 7 5 2 99.829 95.330 1.527 13.746 o 7 5 3 114.076 122.779 1.717 11.011 o 7 5 4 96.314 99.499 1.764 13.713 o 7 5 5 23.409 25.536 0.769 68.740 o 7 5 6 67.158 64.824 1.086 22.394 o 7 5 7 1.933 2.303 0.328 812.079 o 7 5 8 0.493 2.115 0.358 1397.960 o 7 5 9 95.385 97.816 1.860 13.824 o 7 5 10 13.720 12.379 0.621 127.894 o 7 5 11 17.584 18.479 0.720 93.598 o 7 5 12 50.812 54.957 1.184 29.103 o 7 5 13 41.370 44.017 1.007 37.205 o 7 5 14 139.172 147.670 2.292 8.400 o 7 5 15 133.624 142.349 4.669 7.399 o 7 6 0 2.675 2.642 0.258 665.551 o 7 6 1 74.291 80.445 1.266 18.836 o 7 6 2 19.949 22.373 0.670 81.227 o 7 6 3 51.452 44.379 0.921 31.827 o 7 6 4 154.368 141.560 1.993 7.936 o 7 6 5 185.216 194.307 3.430 5.546 o 7 6 6 76.442 71.003 1.375 19.199 o 7 6 7 138.696 141.963 2.053 8.669 o 7 6 8 101.496 109.038 2.801 11.746 o 7 6 9 326.562 338.998 3.364 2.552 o 7 6 10 203.312 216.709 3.449 4.876 o 7 6 11 169.323 181.460 2.056 6.555 o 7 6 12 53.386 53.690 1.074 28.598 o 7 7 0 48.715 43.675 1.659 30.789 o 7 7 1 5.061 4.796 0.580 322.034 o 7 7 2 24.986 21.427 1.141 65.403 o 7 7 3 49.881 46.706 1.103 31.532 o 7 7 4 65.050 66.068 2.425 19.965 o 7 7 5 113.126 103.460 2.180 11.561 o 7 7 6 125.639 112.684 2.247 10.225 o 8 0 0 54.752 44.933 2.957 22.975 o 8 0 1 32.527 38.912 1.109 45.286 o 8 0 2 1.585 3.624 0.377 720.627 o 8 0 3 27.912 24.239 0.873 61.100 o 8 0 4 0.079 0.299 0.203 7444.570 o 8 0 5 174.803 201.590 2.433 5.984 o 8 0 6 121.947 134.080 1.964 9.918 o 8 0 7 25.327 27.554 0.887 62.452 o 8 0 8 49.462 49.470 1.142 30.976 o 8 0 9 242.096 231.110 3.649 4.025 o 8 0 10 31.642 32.412 0.893 50.706 o 8 0 11 1.549 1.936 0.228 1045.580 o 8 0 12 80.283 82.036 3.209 14.651 o 8 0 13 27.422 26.088 1.094 58.404 o 8 0 14 25.109 22.084 0.966 66.720 o 8 0 15 6.001 7.169 0.535 262.110 o 8 0 16 148.947 132.204 2.989 7.978 o 8 1 0 5.622 6.309 0.440 294.389 o 8 1 1 24.602 24.209 0.937 66.034 o 8 1 2 5.451 7.531 0.482 277.107 o 8 1 3 177.378 177.894 2.514 6.241 o 8 1 4 110.713 114.065 1.786 11.595 o 8 1 5 87.488 92.245 1.575 15.420 o 8 1 6 7.085 8.595 0.491 226.431 o 8 1 7 64.517 58.832 1.208 23.727 o 8 1 8 21.952 25.782 0.788 71.223 o 8 1 9 43.927 43.124 0.984 35.994 o 8 1 10 17.864 20.735 0.689 89.404 o 8 1 11 8.702 7.561 0.407 211.661 o 8 1 12 0.565 0.827 0.204 2506.470 o 8 1 13 65.698 60.513 1.615 22.379 o 8 1 14 0.996 1.713 0.313 1278.970 o 8 1 15 106.579 108.143 4.426 9.666 o 8 1 16 130.651 129.154 3.051 8.915 o 8 2 0 29.233 34.438 0.983 51.694 o 8 2 1 16.922 18.639 0.725 95.559 o 8 2 2 54.086 49.823 1.162 28.873 o 8 2 3 31.751 29.245 0.890 52.406 o 8 2 4 23.777 24.591 0.807 68.573 o 8 2 5 54.287 62.758 1.263 26.178 o 8 2 6 8.484 7.957 0.458 209.410 o 8 2 7 66.380 68.970 1.275 21.782 o 8 2 8 130.419 137.191 2.501 9.033 o 8 2 9 26.131 25.923 0.749 63.650 o 8 2 10 48.297 52.380 1.249 30.528 o 8 2 11 26.251 30.551 0.766 59.663 o 8 2 12 35.880 34.193 0.802 45.994 o 8 2 13 37.576 32.877 0.983 44.200 o 8 2 14 75.037 78.384 2.547 16.841 o 8 2 15 15.120 16.970 1.125 96.098 o 8 3 0 34.693 24.983 0.928 51.228 o 8 3 1 53.789 49.111 1.288 28.795 o 8 3 2 80.501 71.946 1.554 18.109 o 8 3 3 140.701 152.753 2.245 8.221 o 8 3 4 71.610 70.004 1.517 20.080 o 8 3 5 10.414 8.449 0.546 175.316 o 8 3 6 70.314 70.505 1.483 20.360 o 8 3 7 11.115 9.920 0.567 159.364 o 8 3 8 88.769 84.365 1.352 16.005 o 8 3 9 37.735 34.553 0.844 43.998 o 8 3 10 16.761 17.167 0.576 101.460 o 8 3 11 52.325 53.375 0.955 29.356 o 8 3 12 0.593 0.511 0.129 3123.910 o 8 4 0 126.987 137.137 1.643 9.645 o 8 4 1 43.416 44.010 0.934 36.201 o 8 4 2 55.153 50.983 1.001 28.596 o 8 4 3 68.599 76.274 1.204 20.517 o 8 4 4 109.355 122.634 1.494 11.517 o 8 4 5 16.823 18.646 0.652 97.143 o 8 4 6 39.678 36.457 0.838 41.667 o 8 4 7 40.725 35.333 0.807 41.409 o 8 4 8 32.130 31.617 0.739 51.472 o 8 4 9 66.393 71.905 1.424 21.184 o 8 4 10 103.392 105.979 1.742 12.655 o 8 4 11 16.982 17.334 0.709 98.025 o 8 5 0 119.173 114.724 1.849 10.855 o 8 5 1 54.071 55.198 1.028 28.139 o 8 5 2 73.678 80.138 2.693 16.631 o 8 5 3 44.629 47.945 1.369 32.879 o 8 5 4 4.721 5.757 0.403 341.678 o 8 5 5 138.414 154.194 3.707 7.575 o 8 5 6 38.946 38.978 1.021 40.508 o 8 5 7 28.123 25.183 0.845 60.279 o 9 0 1 89.178 91.685 2.501 14.157 o 9 0 2 453.137 497.209 18.148 0.920 o 9 0 3 26.047 25.951 0.990 61.595 o 9 0 4 92.922 109.142 1.704 13.606 o 9 0 5 27.357 33.448 0.844 55.545 o 9 0 6 4.021 4.781 0.402 400.697 o 9 1 0 70.772 85.586 1.916 18.081 o 9 1 1 311.398 360.186 2.871 2.615 o 9 1 2 23.524 25.946 0.922 66.578 o 9 1 3 21.838 22.999 0.769 74.685 o 9 1 4 260.357 281.304 2.937 3.513 o 9 1 5 222.186 248.836 2.678 4.346 o 9 1 6 33.989 37.691 1.564 41.566 o 9 2 0 1.432 1.240 0.183 1303.240 o 9 2 1 3.985 3.934 0.251 454.540 o 9 2 2 0.412 0.383 0.135 4238.830 o 9 2 3 118.426 122.696 3.185 9.701 o ; _iucr_refine_instructions_details ; TITL lp_mjy-zh_160822 in P212121 #19 REM reset to P212121 #19 CELL 1.54184 7.450944 9.215433 26.726438 90 90 90 ZERR 4 0.000062 0.000084 0.00023 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,-Z SYMM -X,0.5+Y,0.5-Z SFAC C H O N UNIT 92 132 4 1 L.S. 4 PLAN 20 SIZE 0.4 0.3 0.2 BOND $h htab conf acta FMAP 2 WGHT 0.037514 0.399042 FVAR 13.972852 REM REM REM O1 3 0.14204 0.93989 0.06460 11.00000 0.02972 0.01697 0.01756 = -0.00225 -0.00714 0.00140 AFIX 147 H1 2 0.07663 0.97439 0.04298 11.00000 -1.50000 AFIX 0 C2 1 0.30724 0.84477 0.15327 11.00000 0.01546 0.01469 0.01538 = -0.00014 -0.00116 0.00096 AFIX 13 H2 2 0.27581 0.79018 0.12305 11.00000 -1.20000 AFIX 0 N3 4 -0.11330 1.64152 0.05169 11.00000 0.02538 0.01682 0.02612 = 0.00376 -0.00359 0.00374 AFIX 43 H3 2 -0.11433 1.71707 0.03280 11.00000 -1.20000 AFIX 0 N4 4 0.33679 1.59990 0.01843 11.00000 0.02657 0.02864 0.03010 = 0.00751 0.00281 -0.00305 C5 1 0.22107 1.08762 0.19487 11.00000 0.02334 0.01818 0.01419 = -0.00074 -0.00000 0.00182 AFIX 137 H5a 2 0.23828 1.03731 0.22595 11.00000 -1.50000 H5b 2 0.32902 1.13864 0.18621 11.00000 -1.50000 H5c 2 0.12420 1.15559 0.19829 11.00000 -1.50000 AFIX 0 C6 1 0.49999 0.89535 0.14440 11.00000 0.01405 0.02030 0.02394 = 0.00131 0.00060 0.00141 AFIX 23 H6a 2 0.53533 0.96205 0.17069 11.00000 -1.20000 H6b 2 0.58033 0.81258 0.14537 11.00000 -1.20000 AFIX 0 C7 1 0.17567 0.97745 0.15342 11.00000 0.01275 0.01496 0.01486 = 0.00053 -0.00042 0.00002 C8 1 0.38586 1.09864 0.08873 11.00000 0.02017 0.01844 0.01813 = 0.00060 0.00390 -0.00107 AFIX 13 H8 2 0.42044 1.17105 0.11379 11.00000 -1.20000 AFIX 0 C9 1 -0.03478 0.82261 0.20735 11.00000 0.01696 0.02395 0.02405 = 0.00465 0.00317 -0.00122 AFIX 23 H9a 2 -0.00326 0.87578 0.23741 11.00000 -1.20000 H9b 2 -0.15815 0.79033 0.21056 11.00000 -1.20000 AFIX 0 C10 1 -0.01736 0.92216 0.16186 11.00000 0.01346 0.02027 0.02332 = 0.00359 0.00005 0.00046 AFIX 23 H10a 2 -0.09645 1.00482 0.16620 11.00000 -1.20000 H10b 2 -0.05642 0.86992 0.13229 11.00000 -1.20000 AFIX 0 C11 1 -0.01713 1.44543 0.09367 11.00000 0.02131 0.01595 0.01683 = -0.00209 -0.00057 0.00024 C12 1 0.19005 1.05190 0.10022 11.00000 0.01832 0.01451 0.01537 = -0.00108 -0.00149 -0.00042 C13 1 -0.25604 1.58657 0.07614 11.00000 0.02042 0.02413 0.03351 = -0.00209 -0.00021 0.00451 AFIX 43 H13 2 -0.37192 1.62401 0.07538 11.00000 -1.20000 AFIX 0 C14 1 0.05713 1.17889 0.09178 11.00000 0.01798 0.01761 0.01876 = 0.00252 -0.00300 0.00001 AFIX 23 H14a 2 0.04266 1.19114 0.05596 11.00000 -1.20000 H14b 2 -0.05849 1.14933 0.10498 11.00000 -1.20000 AFIX 0 C15 1 0.10187 1.32878 0.11415 11.00000 0.02305 0.01601 0.01948 = 0.00134 -0.00256 0.00097 AFIX 23 H15a 2 0.22598 1.35244 0.10683 11.00000 -1.20000 H15b 2 0.08842 1.32480 0.15022 11.00000 -1.20000 AFIX 0 C16 1 0.28716 0.73286 0.19689 11.00000 0.01814 0.01673 0.01843 = 0.00281 -0.00146 0.00196 C17 1 0.51493 0.97050 0.09372 11.00000 0.01721 0.02248 0.02519 = 0.00062 0.00616 0.00123 AFIX 23 H17a 2 0.63694 1.00475 0.08918 11.00000 -1.20000 H17b 2 0.48976 0.90073 0.06747 11.00000 -1.20000 AFIX 0 C18 1 0.36111 0.78088 0.24804 11.00000 0.02953 0.02420 0.01979 = 0.00319 -0.00654 0.00119 AFIX 137 H18a 2 0.47931 0.82048 0.24382 11.00000 -1.50000 H18b 2 0.28361 0.85338 0.26214 11.00000 -1.50000 H18c 2 0.36652 0.69874 0.27008 11.00000 -1.50000 AFIX 0 C19 1 0.20167 1.58205 0.03846 11.00000 0.02562 0.01692 0.02101 = 0.00241 -0.00363 -0.00114 C20 1 0.08814 0.69145 0.20186 11.00000 0.02160 0.01879 0.02099 = 0.00451 0.00174 -0.00199 AFIX 23 H20a 2 0.07341 0.62910 0.23081 11.00000 -1.20000 H20b 2 0.05228 0.63667 0.17252 11.00000 -1.20000 AFIX 0 C21 1 0.03415 1.55713 0.06187 11.00000 0.02069 0.01628 0.01946 = -0.00091 -0.00174 0.00093 C22 1 0.40639 1.16913 0.03704 11.00000 0.03194 0.02379 0.02350 = 0.00450 0.00919 0.00158 AFIX 137 H22a 2 0.36056 1.10468 0.01188 11.00000 -1.50000 H22b 2 0.34048 1.25860 0.03622 11.00000 -1.50000 H22c 2 0.53099 1.18821 0.03069 11.00000 -1.50000 AFIX 0 C23 1 0.39058 0.59412 0.18244 11.00000 0.02505 0.01836 0.02799 = 0.00240 -0.00069 0.00331 AFIX 137 H23a 2 0.36242 0.56822 0.14854 11.00000 -1.50000 H23b 2 0.51720 0.61136 0.18539 11.00000 -1.50000 H23c 2 0.35649 0.51641 0.20439 11.00000 -1.50000 AFIX 0 C24 1 -0.20197 1.46594 0.10242 11.00000 0.02191 0.02106 0.02657 = -0.00028 0.00461 -0.00011 AFIX 43 H24 2 -0.27464 1.40803 0.12246 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.125 1.1 0.1 11 0.05 0.24 Q2 1 0.25 0.9 0.155556 11 0.05 0.23 Q3 1 0.291667 0.8 0.177778 11 0.05 0.21 Q4 1 0.291667 1.066667 0.088889 11 0.05 0.21 Q5 1 0.083333 0.966667 0.155556 11 0.05 0.19 Q6 1 0.041667 1.4 0.1 11 0.05 0.18 Q7 1 -0.291667 1.366667 0.133333 11 0.05 0.18 Q8 1 0 1.5 0.077778 11 0.05 0.18 Q9 1 0.208333 0.733333 0.2 11 0.05 0.18 Q10 1 0.458333 1.033333 0.088889 11 0.05 0.17 Q11 1 0.416667 0.866667 0.144444 11 0.05 0.16 Q12 1 0.166667 1.033333 0.133333 11 0.05 0.16 Q13 1 0.333333 0.666667 0.188889 11 0.05 0.14 Q14 1 0.041667 0.766667 0.2 11 0.05 0.14 Q15 1 0.5 0.933333 0.122222 11 0.05 0.14 Q16 1 0.208333 1.033333 0.177778 11 0.05 0.13 Q17 1 0.416667 1.133333 0.066667 11 0.05 0.12 Q18 1 -0.208333 1.533333 0.1 11 0.05 0.12 Q19 1 -0.041667 0.866667 0.188889 11 0.05 0.11 Q20 1 -0.041667 1.6 0.055556 11 0.05 0.11 REM The information below was added by Olex2. REM REM R1 = 0.0298 for 3563 Fo > 4sig(Fo) and 0.0302 for all 3577 data REM 221 parameters refined using 0 restraints REM Highest difference peak 0.2391, deepest hole -0.1393 REM Mean Shift 0.0001, Max Shift 0.0003. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0302 REM R1_gt = 0.0298 REM wR_ref = 0.0738 REM GOOF = 1.0500 REM Shift_max = 0.0003 REM Shift_mean = 0.0001 REM Reflections_all = 3577 REM Reflections_gt = 3563 REM Parameters = 221 REM Hole = -0.1393 REM Peak = 0.2391 REM Flack = 0.2(2) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.489 _oxdiff_exptl_absorpt_empirical_full_min 0.637