data_stahl226 _audit_creation_date 2016-04-28 _audit_creation_method ; Olex2 1.2-dev (compiled 2016.04.27 svn.r3289 for OlexSys, GUI svn.r5176) ; loop_ _publ_author_name _publ_author_email _publ_author_address 'Guzei, I.A.' iguzei@chem.wisc.edu ; 1101 University Ave Madison, WI USA ; _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Bruker-AXS (2014). APEX2. Version 2014.11-0. Madison, Wisconsin, USA. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. "OLEX2: a complete structure solution, refinement and analysis program". (2009), J. Appl. Cryst. 42, 339-341. Krause, L., Herbst-Irmer, R., Sheldrick, G. M. & Stalke, D. (2015). J. Appl. Crystallogr. 48. Pages TBD. doi:10.1107/S1600576714024121 Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015a). "SHELXT - Integrated space-group and crystal-structure determination". Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015b). "Crystal structure refinement with SHELXL". Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C12 H13 N3 O2 Pd' _chemical_formula_sum 'C12 H13 N3 O2 Pd' _chemical_formula_weight 337.65 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pd' 'Pd' 0.1215 3.9337 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.0503(8) _cell_length_b 8.7166(5) _cell_length_c 15.0873(9) _cell_angle_alpha 90 _cell_angle_beta 91.120(3) _cell_angle_gamma 90 _cell_volume 1321.46(15) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9887 _cell_measurement_temperature 100 _cell_measurement_theta_max 73.373 _cell_measurement_theta_min 4.400 _shelx_estimated_absorpt_T_max 0.422 _shelx_estimated_absorpt_T_min 0.144 _exptl_absorpt_coefficient_mu 11.325 _exptl_absorpt_correction_T_max 0.4338 _exptl_absorpt_correction_T_min 0.1208 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'SADABS-2014/5 (Krause et al., 2015) was used for absorption correction.' _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.697 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 672 _exptl_crystal_size_max 0.279 _exptl_crystal_size_mid 0.19 _exptl_crystal_size_min 0.092 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0233 _diffrn_reflns_av_unetI/netI 0.0124 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 18978 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 67.000 _diffrn_reflns_theta_max 73.210 _diffrn_reflns_theta_min 5.863 _diffrn_ambient_temperature 100.0 _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker SMART APEX2 area detector' _diffrn_measurement_method '0.7\ \w and 0.7\ \f scans' _diffrn_radiation_collimation '0.5 mm double-pinhole' _diffrn_radiation_monochromator 'equatorially mounted graphite' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source 'sealed X-ray tube' _diffrn_source_type 'Siemens, K FFCU 2K 90' _diffrn_standards_number . _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2614 _reflns_number_total 2623 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT+ Ver. 2015.9-0 (Bruker-AXS, 2015)' _computing_data_collection 'APEX3 Ver. 2015.9-0 (Bruker-AXS, 2015)' _computing_data_reduction 'SAINT+ Ver. 2015.9-0 (Bruker-AXS, 2015)' _computing_molecular_graphics 'OLEX2 (Dolomanov et al., 2009)' _computing_publication_material 'OLEX2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2015b)' _computing_structure_solution 'XT (Sheldrick, 2015a)' _refine_diff_density_max 0.289 _refine_diff_density_min -0.325 _refine_diff_density_rms 0.059 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.131 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 215 _refine_ls_number_reflns 2623 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0158 _refine_ls_R_factor_gt 0.0156 _refine_ls_restrained_S_all 1.131 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0170P)^2^+1.0337P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0387 _refine_ls_wR_factor_ref 0.0387 _refine_special_details ? _olex2_refinement_description ; ; _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.98801(2) 0.08045(2) 0.39003(2) 0.01152(5) Uani 1 1 d . . . . . N3 N 0.85366(13) 0.24150(16) 0.41159(9) 0.0141(3) Uani 1 1 d . . . . . O4 O 0.88455(12) 0.38420(13) 0.45126(8) 0.0154(2) Uani 1 1 d . . . . . N5 N 1.11039(14) -0.10021(16) 0.36915(10) 0.0162(3) Uani 1 1 d . . . . . N6 N 1.15123(14) 0.20026(16) 0.44774(9) 0.0162(3) Uani 1 1 d . . . . . O7 O 0.63054(11) 0.30661(14) 0.40758(8) 0.0181(2) Uani 1 1 d . . . . . C8 C 0.72424(16) 0.21768(19) 0.39324(10) 0.0140(3) Uani 1 1 d . . . . . C9 C 0.82835(16) -0.01785(18) 0.33616(10) 0.0126(3) Uani 1 1 d . . . . . C10 C 0.71015(17) 0.06484(18) 0.34862(11) 0.0136(3) Uani 1 1 d . . . . . C12 C 1.24263(16) 0.25695(19) 0.47983(11) 0.0151(3) Uani 1 1 d . . . . . C13 C 0.58362(18) -0.1204(2) 0.26427(11) 0.0174(3) Uani 1 1 d . . . . . C14 C 0.58873(17) 0.01355(19) 0.31458(11) 0.0154(3) Uani 1 1 d . . . . . C17 C 1.27864(18) -0.3257(2) 0.37522(12) 0.0185(3) Uani 1 1 d . . . . . C19 C 0.69970(18) -0.2030(2) 0.25108(11) 0.0176(3) Uani 1 1 d . . . . . C20 C 1.36029(17) 0.3270(2) 0.52058(12) 0.0178(3) Uani 1 1 d . . . . . C21 C 0.92418(19) 0.4883(2) 0.38365(12) 0.0193(3) Uani 1 1 d . . . . . C22 C 0.82157(17) -0.15381(19) 0.28726(11) 0.0153(3) Uani 1 1 d . . . . . C23 C 1.18356(16) -0.1993(2) 0.37106(10) 0.0154(3) Uani 1 1 d . . . . . H13 H 0.504(2) -0.154(2) 0.2370(14) 0.021(5) Uiso 1 1 d . . . . . H14 H 0.515(2) 0.071(2) 0.3229(14) 0.016(5) Uiso 1 1 d . . . . . H20A H 1.344(2) 0.427(3) 0.5357(15) 0.022(6) Uiso 1 1 d . . . . . H20B H 1.430(2) 0.328(3) 0.4789(16) 0.025(6) Uiso 1 1 d . . . . . H21A H 0.853(2) 0.504(3) 0.3408(15) 0.025(6) Uiso 1 1 d . . . . . H19 H 0.699(2) -0.292(3) 0.2190(14) 0.018(5) Uiso 1 1 d . . . . . H22 H 0.901(2) -0.213(2) 0.2741(14) 0.020(5) Uiso 1 1 d . . . . . H21B H 0.952(2) 0.579(3) 0.4154(16) 0.022(6) Uiso 1 1 d . . . . . H17A H 1.304(2) -0.347(3) 0.4335(18) 0.035(6) Uiso 1 1 d . . . . . H17B H 1.356(3) -0.298(3) 0.3438(17) 0.037(7) Uiso 1 1 d . . . . . H20C H 1.386(2) 0.267(3) 0.5698(17) 0.031(6) Uiso 1 1 d . . . . . H17C H 1.238(3) -0.414(3) 0.3496(18) 0.037(7) Uiso 1 1 d . . . . . H21C H 0.996(2) 0.452(3) 0.3510(16) 0.024(6) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.00940(7) 0.01253(7) 0.01261(7) 0.00007(4) 0.00005(4) 0.00036(4) N3 0.0125(7) 0.0119(6) 0.0178(7) -0.0027(5) -0.0008(5) -0.0004(5) O4 0.0176(6) 0.0130(5) 0.0156(6) -0.0035(4) 0.0012(4) -0.0024(5) N5 0.0143(7) 0.0175(7) 0.0168(7) -0.0008(5) 0.0003(5) 0.0002(6) N6 0.0135(7) 0.0182(7) 0.0170(7) 0.0008(5) 0.0004(5) 0.0006(6) O7 0.0135(6) 0.0199(6) 0.0210(6) -0.0039(5) 0.0003(4) 0.0027(5) C8 0.0153(8) 0.0156(8) 0.0111(7) 0.0027(6) 0.0006(6) -0.0007(6) C9 0.0131(8) 0.0139(8) 0.0109(7) 0.0030(6) -0.0003(5) -0.0022(6) C10 0.0144(8) 0.0152(8) 0.0113(7) 0.0031(6) 0.0007(6) -0.0008(6) C12 0.0148(8) 0.0162(8) 0.0144(7) 0.0026(6) 0.0031(6) 0.0032(6) C13 0.0177(9) 0.0187(8) 0.0157(8) 0.0037(7) -0.0024(6) -0.0064(7) C14 0.0145(8) 0.0165(8) 0.0153(8) 0.0044(6) 0.0001(6) -0.0003(6) C17 0.0187(9) 0.0196(9) 0.0171(8) -0.0004(7) 0.0020(7) 0.0052(7) C19 0.0228(9) 0.0149(8) 0.0153(8) -0.0001(7) 0.0013(6) -0.0049(7) C20 0.0134(8) 0.0206(9) 0.0195(8) 0.0001(7) -0.0003(6) -0.0021(7) C21 0.0221(9) 0.0156(8) 0.0204(8) -0.0007(7) 0.0033(7) -0.0025(7) C22 0.0174(8) 0.0142(8) 0.0145(7) 0.0021(6) 0.0024(6) -0.0005(6) C23 0.0137(8) 0.0194(8) 0.0131(7) -0.0016(6) 0.0004(6) -0.0024(7) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 N3 1.9791(14) . ? Pd1 N5 2.0265(14) . ? Pd1 N6 2.1175(14) . ? Pd1 C9 1.9796(16) . ? N3 O4 1.4124(17) . ? N3 C8 1.341(2) . ? O4 C21 1.428(2) . ? N5 C23 1.135(2) . ? N6 C12 1.142(2) . ? O7 C8 1.242(2) . ? C8 C10 1.498(2) . ? C9 C10 1.405(2) . ? C9 C22 1.397(2) . ? C10 C14 1.389(2) . ? C12 C20 1.456(2) . ? C13 C14 1.393(2) . ? C13 C19 1.389(3) . ? C13 H13 0.93(2) . ? C14 H14 0.91(2) . ? C17 C23 1.459(2) . ? C17 H17A 0.93(3) . ? C17 H17B 0.95(3) . ? C17 H17C 0.95(3) . ? C19 C22 1.398(2) . ? C19 H19 0.91(2) . ? C20 H20A 0.92(2) . ? C20 H20B 0.95(2) . ? C20 H20C 0.94(3) . ? C21 H21A 0.96(2) . ? C21 H21B 0.96(2) . ? C21 H21C 0.94(3) . ? C22 H22 0.97(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 Pd1 N5 174.16(6) . . ? N3 Pd1 N6 96.21(6) . . ? N3 Pd1 C9 79.88(6) . . ? N5 Pd1 N6 88.82(6) . . ? C9 Pd1 N5 95.13(6) . . ? C9 Pd1 N6 175.97(6) . . ? O4 N3 Pd1 123.32(10) . . ? C8 N3 Pd1 121.23(11) . . ? C8 N3 O4 115.35(13) . . ? N3 O4 C21 108.60(12) . . ? C23 N5 Pd1 169.37(14) . . ? C12 N6 Pd1 176.08(14) . . ? N3 C8 C10 108.26(14) . . ? O7 C8 N3 127.11(15) . . ? O7 C8 C10 124.60(15) . . ? C10 C9 Pd1 113.81(12) . . ? C22 C9 Pd1 127.94(12) . . ? C22 C9 C10 118.24(15) . . ? C9 C10 C8 116.32(14) . . ? C14 C10 C8 121.82(15) . . ? C14 C10 C9 121.63(15) . . ? N6 C12 C20 179.10(18) . . ? C14 C13 H13 121.4(13) . . ? C19 C13 C14 119.37(16) . . ? C19 C13 H13 119.1(13) . . ? C10 C14 C13 119.61(16) . . ? C10 C14 H14 119.1(13) . . ? C13 C14 H14 121.2(13) . . ? C23 C17 H17A 111.2(16) . . ? C23 C17 H17B 109.0(16) . . ? C23 C17 H17C 108.2(16) . . ? H17A C17 H17B 108(2) . . ? H17A C17 H17C 109(2) . . ? H17B C17 H17C 111(2) . . ? C13 C19 C22 121.14(16) . . ? C13 C19 H19 121.1(13) . . ? C22 C19 H19 117.8(13) . . ? C12 C20 H20A 110.6(15) . . ? C12 C20 H20B 109.0(14) . . ? C12 C20 H20C 107.6(15) . . ? H20A C20 H20B 107(2) . . ? H20A C20 H20C 113(2) . . ? H20B C20 H20C 110(2) . . ? O4 C21 H21A 111.1(14) . . ? O4 C21 H21B 104.5(14) . . ? O4 C21 H21C 113.1(14) . . ? H21A C21 H21B 114.6(19) . . ? H21A C21 H21C 105.3(19) . . ? H21B C21 H21C 109(2) . . ? C9 C22 C19 119.97(16) . . ? C9 C22 H22 121.6(12) . . ? C19 C22 H22 118.3(12) . . ? N5 C23 C17 178.86(18) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Pd1 N3 O4 C21 86.91(14) . . . . ? Pd1 N3 C8 O7 176.42(13) . . . . ? Pd1 N3 C8 C10 -5.53(17) . . . . ? Pd1 C9 C10 C8 4.78(18) . . . . ? Pd1 C9 C10 C14 179.39(12) . . . . ? Pd1 C9 C22 C19 -177.47(12) . . . . ? N3 C8 C10 C9 0.25(19) . . . . ? N3 C8 C10 C14 -174.35(15) . . . . ? O4 N3 C8 O7 -0.2(2) . . . . ? O4 N3 C8 C10 177.84(12) . . . . ? O7 C8 C10 C9 178.36(15) . . . . ? O7 C8 C10 C14 3.8(2) . . . . ? C8 N3 O4 C21 -96.53(16) . . . . ? C8 C10 C14 C13 172.17(15) . . . . ? C9 C10 C14 C13 -2.1(2) . . . . ? C10 C9 C22 C19 1.0(2) . . . . ? C13 C19 C22 C9 -1.3(2) . . . . ? C14 C13 C19 C22 -0.1(2) . . . . ? C19 C13 C14 C10 1.8(2) . . . . ? C22 C9 C10 C8 -173.88(14) . . . . ? C22 C9 C10 C14 0.7(2) . . . . ? _shelx_res_file ; stahl226.res created by SHELXL-2014/7 TITL STAHL226 IN P21/C #14 REM RESET TO P21/C #14 REM FCF_FILTER (MSL, UW-MADISON) INSERTED 6 OMIT INSTRUCTIONS REM FOR OUTLIER REFLECTIONS WITH THE CUTOFF VALUE OF 4.95581. REM REM REM REM ============ UPDATED INSTRUCTIONS ============ REM ================================================ REM The weighting scheme has been updated. CELL 1.54178 10.05033 8.71656 15.08735 90 91.1196 90 ZERR 4 0.00075 0.00048 0.00091 0 0.0032 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O Pd UNIT 48 52 12 8 4 L.S. 12 PLAN 5 SIZE 0.092 0.19 0.279 TEMP -173.15 MORE -1 BOND $H CONF BOND $H HTAB LIST 4 fmap 2 acta 134 OMIT 1 0 0 OMIT -2 2 18 OMIT 1 0 4 OMIT 0 0 4 OMIT -3 1 4 OMIT -3 3 1 REM REM REM WGHT 0.017000 1.033700 FVAR 0.48851 PD1 5 0.988015 0.080451 0.390030 11.00000 0.00940 0.01253 = 0.01261 0.00007 0.00005 0.00036 N3 3 0.853656 0.241496 0.411587 11.00000 0.01251 0.01192 = 0.01780 -0.00266 -0.00076 -0.00044 O4 4 0.884545 0.384204 0.451260 11.00000 0.01764 0.01305 = 0.01561 -0.00346 0.00120 -0.00241 N5 3 1.110394 -0.100209 0.369154 11.00000 0.01426 0.01754 = 0.01684 -0.00075 0.00027 0.00022 N6 3 1.151230 0.200256 0.447741 11.00000 0.01351 0.01822 = 0.01700 0.00076 0.00037 0.00060 O7 4 0.630537 0.306607 0.407575 11.00000 0.01348 0.01988 = 0.02100 -0.00393 0.00029 0.00265 C8 1 0.724243 0.217679 0.393241 11.00000 0.01533 0.01561 = 0.01113 0.00269 0.00059 -0.00067 C9 1 0.828348 -0.017847 0.336155 11.00000 0.01312 0.01386 = 0.01090 0.00303 -0.00031 -0.00218 C10 1 0.710148 0.064838 0.348620 11.00000 0.01438 0.01517 = 0.01128 0.00306 0.00068 -0.00081 C12 1 1.242630 0.256949 0.479832 11.00000 0.01483 0.01619 = 0.01437 0.00261 0.00306 0.00315 C13 1 0.583616 -0.120421 0.264275 11.00000 0.01766 0.01868 = 0.01568 0.00373 -0.00245 -0.00637 C14 1 0.588728 0.013547 0.314577 11.00000 0.01450 0.01650 = 0.01525 0.00437 0.00013 -0.00028 C17 1 1.278643 -0.325697 0.375223 11.00000 0.01873 0.01963 = 0.01711 -0.00035 0.00199 0.00518 C19 1 0.699704 -0.203001 0.251081 11.00000 0.02283 0.01485 = 0.01525 -0.00011 0.00129 -0.00489 C20 1 1.360291 0.326984 0.520578 11.00000 0.01344 0.02058 = 0.01947 0.00014 -0.00033 -0.00208 C21 1 0.924184 0.488279 0.383645 11.00000 0.02212 0.01555 = 0.02037 -0.00072 0.00331 -0.00249 C22 1 0.821568 -0.153814 0.287255 11.00000 0.01741 0.01420 = 0.01448 0.00207 0.00236 -0.00055 C23 1 1.183565 -0.199346 0.371061 11.00000 0.01366 0.01943 = 0.01309 -0.00158 0.00039 -0.00240 H13 2 0.504495 -0.153597 0.236989 11.00000 0.02101 H14 2 0.514873 0.071162 0.322942 11.00000 0.01638 H20A 2 1.343610 0.426767 0.535687 11.00000 0.02198 H20B 2 1.429733 0.327930 0.478946 11.00000 0.02494 H21A 2 0.853275 0.504489 0.340830 11.00000 0.02545 H19 2 0.698856 -0.291503 0.219027 11.00000 0.01789 H22 2 0.900976 -0.212931 0.274139 11.00000 0.01963 H21B 2 0.951986 0.579151 0.415351 11.00000 0.02234 H17A 2 1.304036 -0.347315 0.433515 11.00000 0.03468 H17B 2 1.355860 -0.297638 0.343766 11.00000 0.03658 H20C 2 1.385530 0.266550 0.569752 11.00000 0.03059 H17C 2 1.237574 -0.413676 0.349622 11.00000 0.03677 H21C 2 0.995932 0.452294 0.351010 11.00000 0.02431 HKLF 4 REM STAHL226 IN P21/C #14 REM R1 = 0.0156 for 2614 Fo > 4sig(Fo) and 0.0158 for all 2623 data REM 215 parameters refined using 0 restraints END WGHT 0.0169 1.0461 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+1, -z+1 HTAB C20 O7_$1 EQIV $2 x+1, y, z HTAB C20 O7_$2 HTAB C21 O4_$1 EQIV $3 -x+2, -y, -z+1 HTAB C17 O4_$3 HTAB C17 O7_$3 REM Highest difference peak 0.289, deepest hole -0.325, 1-sigma level 0.059 Q1 1 0.9032 0.0927 0.3784 11.00000 0.05 0.29 Q2 1 0.7181 0.1401 0.3673 11.00000 0.05 0.26 Q3 1 0.8976 0.0226 0.3573 11.00000 0.05 0.24 Q4 1 0.7672 0.0101 0.3568 11.00000 0.05 0.22 Q5 1 1.0689 0.0460 0.4162 11.00000 0.05 0.22 ; _shelx_res_checksum 87691 _shelx_hkl_file ; 1 0 0 7013.87 159.437 3 2 0 0 971.708 25.1607 3 3 0 0 3627.07 83.1112 2 3 0 0 3504.22 84.2730 3 4 0 0 723.875 20.4797 1 4 0 0 702.899 19.5612 2 4 0 0 706.632 20.4845 3 5 0 0 2655.40 64.8556 1 5 0 0 2603.13 67.0066 6 6 0 0 2754.19 68.2588 1 6 0 0 2714.78 66.6935 7 6 0 0 2764.64 70.7775 6 7 0 0 3799.43 95.2073 1 7 0 0 4015.63 98.2499 6 7 0 0 3913.88 93.6751 7 8 0 0 1994.85 48.1986 12 8 0 0 2029.78 51.0230 7 8 0 0 2030.49 55.3202 6 8 0 0 1890.74 45.2458 15 9 0 0 399.067 17.5404 6 9 0 0 410.947 14.5991 7 9 0 0 396.523 11.9226 12 10 0 0 962.642 24.4481 12 10 0 0 959.195 30.7826 6 10 0 0 979.786 27.3220 7 11 0 0 1089.59 26.5618 12 0 -1 0 2.31222 0.53852 4 0 1 0 3.70903 0.59453 4 0 1 0 3.59315 0.87239 3 1 -1 0 277.867 7.82615 4 -1 1 0 292.255 7.73654 3 1 1 0 293.245 9.32267 3 -1 1 0 295.386 8.22923 4 2 1 0 393.083 12.1039 2 2 1 0 383.278 13.1539 3 -2 1 0 405.498 10.4351 4 -2 1 0 407.580 10.3231 3 3 -1 0 188.076 7.68807 1 -3 1 0 194.814 6.29379 3 3 1 0 198.183 7.81508 2 3 1 0 182.324 9.02040 3 -3 1 0 197.373 5.20754 4 4 -1 0 494.265 15.8261 1 4 -1 0 439.726 16.9781 6 4 1 0 506.027 15.5259 2 4 1 0 497.659 15.3311 1 4 1 0 497.961 17.2907 3 5 -1 0 34.9826 3.85251 1 5 -1 0 37.1240 5.44302 6 5 -1 0 33.4678 3.54154 7 5 1 0 32.0264 3.57269 1 5 1 0 20.0786 3.82154 3 5 1 0 36.8663 3.73706 2 5 1 0 40.2782 5.46684 6 6 -1 0 4.90621 1.88929 7 6 -1 0 6.64562 3.06390 6 6 -1 0 10.4537 2.74420 1 6 1 0 9.79149 3.33026 6 6 1 0 15.4911 2.68694 7 6 1 0 6.61154 2.29615 1 7 -1 0 12.8749 3.90498 6 7 -1 0 16.2451 3.54858 1 7 -1 0 23.7438 3.67095 7 7 1 0 14.4937 4.06499 6 7 1 0 18.3778 3.13317 7 7 1 0 15.8796 3.36806 1 8 -1 0 184.257 5.31197 15 8 -1 0 193.783 11.4325 6 8 -1 0 186.906 9.02882 7 8 -1 0 179.838 7.19783 11 8 -1 0 170.229 6.72525 12 8 1 0 193.034 11.1413 6 8 1 0 185.531 11.6255 7 9 -1 0 222.878 8.16311 11 9 -1 0 225.101 7.86474 12 9 -1 0 226.500 12.6557 6 9 -1 0 232.153 10.3380 7 10 -1 0 64.1158 6.80660 6 10 -1 0 56.9570 3.32240 12 10 -1 0 63.6179 4.97288 7 10 -1 0 56.1332 3.49164 11 11 -1 0 482.443 13.0052 12 12 -1 0 382.748 9.83920 12 0 -2 0 28.0064 2.13069 4 0 2 0 34.8218 2.51865 2 0 2 0 28.0888 1.76062 4 0 2 0 25.7230 2.52231 3 -1 -2 0 2636.86 59.5211 4 1 -2 0 2585.08 60.3224 4 -1 2 0 2620.84 60.7512 3 1 2 0 2528.95 61.5344 2 -1 2 0 2541.94 60.6717 4 1 2 0 2596.64 62.6764 3 2 -2 0 5371.78 137.046 1 -2 2 0 6030.62 137.368 4 -2 2 0 6248.78 135.978 3 2 2 0 6102.01 140.030 3 2 2 0 6051.87 138.453 2 3 -2 0 1327.96 34.8238 1 -3 2 0 1327.14 32.1331 3 -3 2 0 1408.84 34.5604 4 3 2 0 1353.12 37.8980 3 3 2 0 1282.54 33.6820 1 3 2 0 1348.55 35.6873 2 4 -2 0 1240.79 37.6802 6 4 -2 0 1338.33 35.5476 1 4 2 0 1351.30 38.7761 3 4 2 0 1309.34 35.5589 2 4 2 0 1303.40 34.4081 1 -4 2 0 1335.98 34.6139 4 5 -2 0 868.510 28.1128 6 5 -2 0 857.831 26.2571 1 5 -2 0 845.390 24.3902 7 5 2 0 890.606 26.2723 2 5 2 0 887.492 25.5445 1 -5 2 0 848.144 24.9442 4 5 2 0 896.319 28.8381 3 6 -2 0 221.806 10.8496 1 6 -2 0 225.134 12.1277 6 6 -2 0 212.143 9.41472 7 6 2 0 222.107 11.9169 3 6 2 0 221.608 10.2032 1 6 2 0 227.780 10.6409 2 -6 2 0 220.790 9.81166 4 7 -2 0 359.487 13.5996 7 7 -2 0 359.015 16.5349 6 7 -2 0 382.967 15.3052 1 -7 2 0 369.167 14.1572 4 8 -2 0 88.6718 6.19394 7 8 -2 0 107.322 6.51889 13 8 -2 0 84.7808 4.80687 11 8 -2 0 89.5281 4.57409 12 8 -2 0 93.6629 3.51137 15 8 -2 0 101.685 8.46764 6 9 -2 0 510.450 14.4868 12 9 -2 0 514.511 12.8776 15 9 -2 0 507.926 20.6396 6 9 -2 0 513.727 17.4505 7 9 -2 0 492.847 14.7451 11 10 -2 0 565.612 17.8885 7 10 -2 0 519.892 20.4375 6 10 -2 0 574.420 15.1631 12 10 -2 0 535.287 15.1672 11 10 -2 0 541.948 13.1104 15 11 -2 0 89.6799 3.81641 12 11 -2 0 88.4071 3.77392 11 12 -2 0 230.386 6.36663 12 0 -3 0 -1.1138 1.14861 1 0 -3 0 -0.8080 1.07010 4 0 3 0 -0.9490 1.63007 3 0 3 0 0.23244 0.88685 4 -1 -3 0 252.717 8.71820 4 -1 -3 0 260.792 9.10887 1 1 -3 0 256.157 9.31222 1 1 -3 0 258.192 8.61999 2 1 -3 0 256.050 8.92562 4 1 3 0 274.881 10.1376 2 -1 3 0 263.250 8.94788 4 1 3 0 266.987 11.1743 3 -1 3 0 267.820 10.0250 3 -2 -3 0 605.423 15.8383 4 2 -3 0 582.380 17.6631 1 2 -3 0 576.972 15.6806 2 -2 -3 0 595.847 17.0860 1 -2 3 0 599.267 17.7405 4 2 3 0 591.905 20.3244 3 -2 3 0 563.307 16.8196 5 -2 3 0 582.734 17.1675 3 2 3 0 595.321 18.6843 2 3 -3 0 220.122 9.50653 1 3 -3 0 223.240 10.8850 6 -3 3 0 242.499 10.1018 4 -3 3 0 219.660 9.13885 5 3 3 0 226.867 9.00727 1 3 3 0 238.482 12.2267 3 3 3 0 230.031 10.5540 2 4 -3 0 1174.97 32.9838 7 4 -3 0 1220.44 37.5269 6 4 -3 0 1345.05 35.4273 1 -4 3 0 1221.62 34.1259 5 4 3 0 1267.30 35.8043 2 4 3 0 1278.01 33.8378 1 4 3 0 1301.63 39.4730 3 -4 3 0 1239.26 35.3860 4 5 -3 0 802.242 25.1157 1 5 -3 0 708.047 22.3062 7 5 -3 0 765.786 26.8471 6 5 3 0 764.144 24.8335 2 5 3 0 754.798 23.5582 1 -5 3 0 790.900 25.6146 4 5 3 0 813.170 28.4961 3 6 -3 0 91.8723 4.56580 8 6 -3 0 88.2038 8.22064 6 6 -3 0 101.505 7.58956 1 6 -3 0 93.7783 6.05858 7 6 3 0 102.793 8.94936 3 6 3 0 95.6453 7.26486 2 -6 3 0 105.948 7.70486 4 6 3 0 106.241 7.06828 1 7 -3 0 194.822 10.7465 1 7 -3 0 193.575 11.9119 6 7 -3 0 188.593 7.04549 8 7 -3 0 182.895 9.15558 7 -7 3 0 177.911 10.3729 4 7 3 0 193.435 10.8201 2 8 -3 0 295.825 9.32318 13 8 -3 0 295.371 8.73835 15 8 -3 0 292.558 14.8001 1 8 -3 0 302.280 15.3466 6 8 -3 0 290.487 9.71989 12 8 -3 0 347.482 10.6402 11 8 -3 0 296.617 12.3763 7 9 -3 0 660.704 16.1179 15 9 -3 0 625.593 16.7039 13 9 -3 0 642.796 20.4727 7 9 -3 0 640.361 23.8629 6 9 -3 0 619.318 17.2954 12 9 -3 0 620.349 17.6371 11 10 -3 0 994.074 23.4165 15 10 -3 0 982.448 27.7630 7 10 -3 0 968.682 36.0272 6 10 -3 0 1010.41 24.9455 12 10 -3 0 982.573 25.0621 11 11 -3 0 978.431 23.6294 12 11 -3 0 947.515 23.5214 11 0 -4 0 276.237 10.5268 2 0 -4 0 271.414 10.0340 5 0 -4 0 286.315 10.5640 4 0 -4 0 293.663 10.7618 1 0 4 0 282.159 12.6087 3 -1 -4 0 733.423 21.3645 1 1 -4 0 709.863 20.2369 5 -1 -4 0 736.683 21.3572 4 1 -4 0 744.809 21.2149 4 -1 -4 0 719.873 20.8288 5 1 -4 0 739.314 21.7128 1 1 4 0 754.497 25.0458 3 -1 4 0 720.219 19.3958 5 -1 4 0 744.935 23.4847 3 1 4 0 764.433 22.5471 2 -2 -4 0 1635.47 41.6553 1 2 -4 0 1618.64 42.1491 1 2 -4 0 1557.53 41.5775 6 -2 -4 0 1644.93 41.1498 4 2 -4 0 1606.11 39.1921 5 -2 4 0 1650.43 42.9603 3 -2 4 0 1553.68 40.2153 5 2 4 0 1580.35 46.2569 3 2 4 0 1544.92 43.1774 2 -2 4 0 1658.24 41.7795 4 3 -4 0 758.174 23.4678 1 3 -4 0 768.335 24.1427 6 -3 -4 0 737.046 22.4432 1 -3 -4 0 764.937 21.6021 4 -3 4 0 742.379 22.0894 5 3 4 0 760.803 27.7328 3 -3 4 0 747.826 23.5213 4 3 4 0 718.717 24.4389 2 -4 -4 0 305.801 10.7627 4 4 -4 0 282.975 14.1400 6 4 -4 0 291.517 11.5211 7 4 -4 0 304.975 13.1231 1 -4 -4 0 318.509 12.5992 1 4 4 0 299.120 16.4094 3 -4 4 0 311.347 12.6441 5 -4 4 0 292.381 13.3082 4 4 4 0 283.792 13.5712 2 5 -4 0 198.335 9.37336 7 5 -4 0 214.680 11.3700 1 -5 -4 0 230.484 10.9610 1 5 -4 0 206.473 7.42689 8 5 -4 0 216.075 13.0151 6 -5 4 0 201.879 11.7042 4 -5 4 0 217.868 11.3992 5 5 4 0 207.324 13.7229 3 5 4 0 209.477 11.5536 2 -6 -4 0 312.331 13.7935 1 6 -4 0 304.840 14.6217 1 6 -4 0 309.266 15.8570 6 6 -4 0 308.953 10.0669 8 6 -4 0 303.645 12.3772 7 -6 4 0 297.222 14.0894 5 -6 4 0 290.557 14.6291 4 6 4 0 297.410 17.0214 3 6 4 0 318.785 14.8705 2 7 -4 0 234.482 10.6298 7 7 -4 0 226.651 7.42742 15 7 -4 0 225.822 8.07705 12 7 -4 0 218.479 8.51238 11 7 -4 0 241.633 8.37775 8 7 -4 0 216.133 12.1908 1 7 -4 0 232.205 7.75396 13 7 -4 0 220.699 13.1881 6 7 4 0 226.125 7.89361 10 7 4 0 231.809 12.4482 2 -7 4 0 234.588 12.0679 5 7 4 0 220.604 7.87104 9 8 -4 0 327.684 9.97183 13 8 -4 0 342.055 16.5428 6 8 -4 0 331.561 10.5693 8 8 -4 0 321.375 15.7422 1 8 -4 0 332.368 13.1920 7 8 -4 0 329.629 9.61713 15 8 -4 0 328.359 10.3883 12 8 -4 0 316.612 10.8317 11 9 -4 0 549.387 14.1514 15 9 -4 0 542.076 15.0350 12 9 -4 0 526.614 14.5024 13 9 -4 0 519.532 17.7348 7 9 -4 0 552.153 21.2812 6 9 -4 0 561.419 15.5505 11 10 -4 0 339.164 9.12275 13 10 -4 0 310.609 11.6434 7 10 -4 0 318.491 8.62333 15 10 -4 0 332.730 9.83160 11 10 -4 0 331.905 9.62600 12 11 -4 0 140.604 4.66260 11 11 -4 0 145.693 4.65865 12 0 -5 0 -0.2989 1.31712 2 0 -5 0 0.82945 1.74817 1 0 -5 0 1.86635 1.57164 4 0 -5 0 0.17239 1.54525 5 0 5 0 -0.4497 2.49214 3 -1 -5 0 73.1195 5.81793 2 1 -5 0 80.8709 5.94672 1 -1 -5 0 77.1311 5.83506 4 -1 -5 0 86.7106 6.06602 1 -1 -5 0 75.2973 5.68602 5 1 -5 0 76.4748 5.01867 5 1 -5 0 64.0849 4.87753 2 -1 5 0 83.4251 7.64882 3 1 5 0 87.9839 8.28932 3 2 -5 0 7.18983 1.90281 5 -2 -5 0 7.11159 2.45095 4 -2 -5 0 9.14013 2.64120 1 2 -5 0 7.54727 2.54456 1 2 5 0 8.06019 4.10490 3 -2 5 0 5.26609 1.76888 5 2 5 0 9.69021 3.01095 2 3 -5 0 179.184 6.59279 8 3 -5 0 182.657 10.0230 1 -3 -5 0 184.788 9.73197 4 -3 -5 0 183.080 9.49623 1 3 5 0 195.970 13.7647 3 -3 5 0 190.576 8.79703 5 3 5 0 187.749 10.9270 2 -4 -5 0 20.2221 3.95992 4 4 -5 0 24.8730 4.74217 1 4 -5 0 18.3492 2.32240 8 4 -5 0 21.6093 3.82703 7 -4 -5 0 19.9836 4.02219 1 -4 5 0 21.4411 4.73308 4 -4 5 0 29.0445 4.47549 5 4 5 0 26.3831 6.87806 3 5 -5 0 28.7029 2.78225 8 5 -5 0 25.7836 4.81290 1 5 -5 0 37.2238 6.81084 6 -5 -5 0 31.9409 5.13504 4 -5 -5 0 37.3184 5.74914 1 5 -5 0 36.1345 4.86093 7 5 5 0 40.8625 5.41891 2 5 5 0 27.3408 7.06870 3 -5 5 0 35.5556 5.29694 5 -5 5 0 40.0255 6.65707 4 6 -5 0 128.933 7.63969 7 6 -5 0 120.981 6.24970 11 6 -5 0 124.207 5.38409 13 6 -5 0 141.867 10.9102 6 6 -5 0 128.522 5.65428 15 6 -5 0 120.067 5.69766 8 6 -5 0 124.889 9.40634 1 6 5 0 117.485 9.24832 2 -6 5 0 131.177 9.09297 5 6 5 0 121.589 5.54750 10 6 5 0 125.135 4.08116 15 6 5 0 117.165 5.50022 9 7 -5 0 287.968 9.80789 8 7 -5 0 287.211 9.18003 13 7 -5 0 307.490 15.8152 6 7 -5 0 295.784 14.5693 1 7 -5 0 278.924 10.1903 11 7 -5 0 289.609 9.52370 12 7 -5 0 282.631 12.0265 7 7 -5 0 274.517 9.05371 15 -7 5 0 292.995 13.5454 5 7 5 0 281.453 7.10229 15 7 5 0 282.048 9.37726 10 7 5 0 287.876 9.42900 9 8 -5 0 350.453 13.4465 7 8 -5 0 357.935 10.4204 15 8 -5 0 359.604 10.8657 12 8 -5 0 358.513 10.5388 13 8 -5 0 363.545 11.1390 8 8 -5 0 360.608 11.5272 11 8 5 0 356.562 10.7459 10 -8 5 0 333.748 16.6453 6 -8 5 0 338.855 14.3594 5 8 5 0 357.152 10.6032 9 9 -5 0 91.5140 4.51281 11 9 -5 0 91.0989 3.97200 13 9 -5 0 98.9212 6.05416 7 9 -5 0 90.6321 3.73004 15 9 -5 0 99.7812 4.30082 12 10 -5 0 123.850 4.41459 12 10 -5 0 122.652 3.92123 15 10 -5 0 122.678 4.13610 13 10 -5 0 123.544 4.65820 11 0 -6 0 1991.34 53.2410 1 0 -6 0 2030.76 51.3704 5 0 -6 0 1984.07 47.5189 8 0 -6 0 1921.07 52.2134 2 0 -6 0 1962.95 52.9562 4 0 6 0 1950.17 59.6675 3 -1 -6 0 3338.32 81.1817 5 -1 -6 0 3344.89 82.4117 1 1 -6 0 3275.64 82.2355 1 -1 -6 0 3157.66 82.2055 4 -1 -6 0 3229.98 82.5955 2 1 -6 0 3133.53 76.1267 8 -1 -6 0 3253.40 76.3239 8 1 -6 0 3336.89 79.2453 5 1 6 0 3184.10 89.6501 3 2 -6 0 2246.31 55.4556 8 -2 -6 0 2408.76 61.2043 5 2 -6 0 2385.41 56.7755 5 -2 -6 0 2273.28 61.9310 4 -2 -6 0 2375.97 61.5623 1 2 -6 0 2368.97 61.9547 1 -2 -6 0 2363.18 55.8429 8 -2 -6 0 2244.63 62.5452 2 2 6 0 2279.02 69.4458 3 -3 -6 0 1732.61 50.1350 4 -3 -6 0 1783.36 43.8156 8 3 -6 0 1831.01 50.2499 1 3 -6 0 1799.42 43.4512 8 -3 -6 0 1853.73 49.7644 1 -3 -6 0 1764.63 51.4558 2 3 6 0 1689.76 56.9350 3 -3 6 0 1772.26 45.4673 5 4 -6 0 2347.42 56.4722 14 4 -6 0 2458.27 64.5791 1 -4 -6 0 2253.97 65.6793 2 -4 -6 0 2572.84 64.4966 1 4 -6 0 2385.84 56.3027 13 -4 -6 0 2314.12 64.4792 4 4 -6 0 2437.81 57.0192 8 4 -6 0 2339.83 57.4984 11 4 6 0 2356.70 55.9958 15 4 6 0 2322.84 71.5318 3 4 6 0 2332.40 57.0411 10 4 6 0 2281.62 57.7099 9 -4 6 0 2420.10 60.6736 5 5 -6 0 905.960 23.6835 13 5 -6 0 903.775 25.0416 11 -5 -6 0 951.846 30.7908 1 5 -6 0 935.967 31.2834 1 -5 -6 0 876.987 31.5736 2 5 -6 0 938.122 22.6276 14 5 -6 0 940.376 24.5003 8 5 6 0 917.104 24.3762 10 5 6 0 883.200 24.5280 9 -5 6 0 939.474 28.6349 5 5 6 0 901.261 22.8387 15 6 -6 0 1058.79 32.1366 7 6 -6 0 941.050 32.2246 1 6 -6 0 985.417 26.5832 11 6 -6 0 976.844 25.8056 8 6 -6 0 985.894 25.0688 13 -6 6 0 968.991 30.2929 5 6 6 0 964.993 23.5304 15 6 6 0 960.772 25.4096 10 6 6 0 933.679 25.4231 9 7 -6 0 1583.41 39.0938 11 7 -6 0 1592.24 41.4556 7 7 -6 0 1511.92 37.6889 13 7 -6 0 1564.08 38.0500 15 7 -6 0 1550.49 38.5238 8 -7 6 0 1430.18 48.2183 6 7 6 0 1525.68 38.0216 9 7 6 0 1595.93 35.6082 15 7 6 0 1582.46 38.1405 10 8 -6 0 1360.73 33.5873 8 8 -6 0 1382.23 33.0671 13 8 -6 0 1348.35 36.2170 7 8 -6 0 1384.60 34.0677 11 8 -6 0 1366.45 33.1245 15 8 6 0 1362.13 33.2951 10 8 6 0 1334.89 33.1586 9 9 -6 0 1184.81 28.5255 13 9 -6 0 1226.22 28.5558 15 9 6 0 1156.45 28.5004 10 10 -6 0 467.139 11.7253 13 10 -6 0 493.222 11.6952 15 -10 6 0 474.371 12.2451 11 0 -7 0 0.22378 1.91263 1 0 -7 0 -0.1187 1.36579 13 0 -7 0 12.3802 2.23917 8 0 -7 0 3.36176 2.31091 5 0 7 0 3.07242 1.06941 14 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28.6624 8 -5 6 4 1114.44 29.5568 11 5 6 -4 1078.40 26.8688 15 5 6 -4 1080.87 28.0778 10 5 6 -4 1081.60 27.7052 13 -5 6 4 1109.82 32.8744 5 4 -6 -4 1369.48 40.5391 1 4 -6 -4 1389.84 34.8663 8 4 -6 -4 1368.02 33.9060 13 -4 -6 4 1363.51 42.9728 2 4 -6 -4 1350.83 33.7469 14 4 6 -4 1361.93 34.6927 8 4 6 -4 1295.31 34.0331 10 4 6 -4 1346.16 33.4677 15 4 6 -4 1318.48 33.6231 13 -4 6 4 1439.94 42.9781 6 4 6 -4 1334.23 34.5249 9 -4 6 4 1404.76 37.8517 5 -4 6 4 1357.76 35.2153 11 3 -6 -4 973.466 25.9410 14 -3 -6 4 974.672 31.5176 4 3 -6 -4 1047.59 31.5677 1 -3 -6 4 925.706 32.4836 2 3 -6 -4 980.710 25.8825 8 3 6 -4 947.031 36.1530 3 -3 6 4 965.858 31.6613 6 3 6 -4 957.298 25.3339 15 -3 6 4 987.477 27.1529 5 3 6 -4 1013.67 25.7925 8 -3 6 4 996.145 26.2233 11 3 6 -4 931.342 24.9695 13 3 6 -4 967.311 26.1773 9 2 -6 -4 949.756 25.3020 8 -2 -6 4 925.001 30.5421 4 -2 -6 4 1003.33 29.9339 5 -2 -6 4 917.825 31.4952 2 2 -6 -4 994.767 30.2634 1 2 6 -4 967.301 35.8883 3 2 6 -4 942.313 24.9170 8 1 -6 -4 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1559.00 39.1081 12 7 -2 5 1532.92 39.5115 11 7 -2 5 1622.32 45.9995 1 7 -2 5 1668.25 43.1850 7 7 2 5 1562.83 37.2210 15 7 2 5 1547.39 39.9168 11 7 2 5 1618.54 48.7616 6 7 2 5 1551.61 45.6869 2 7 2 5 1655.17 46.3210 1 7 2 5 1521.60 38.6337 10 8 -2 5 942.092 24.2743 12 8 -2 5 969.734 31.8508 6 8 -2 5 937.883 22.9083 15 8 -2 5 932.412 24.6713 11 8 -2 5 909.474 27.4311 7 8 -2 5 901.484 30.0838 1 8 2 5 950.757 32.4082 6 8 2 5 945.426 22.0013 15 8 2 5 884.513 23.6951 10 8 2 5 938.092 25.0706 11 8 2 5 893.525 29.9482 1 9 -2 5 394.230 12.0541 12 9 -2 5 421.967 12.6740 11 9 -2 5 428.141 14.9978 7 9 -2 5 396.091 17.5900 6 9 -2 5 416.873 10.8632 15 9 2 5 406.783 11.8171 10 9 2 5 407.322 17.9452 6 9 2 5 409.745 12.6935 11 10 -2 5 1152.99 31.7572 7 10 -2 5 1209.34 29.8280 11 10 -2 5 1225.31 29.4599 12 10 -2 5 1192.94 27.7613 15 10 2 5 1199.55 29.8131 11 11 -2 5 610.707 15.5565 11 11 -2 5 608.128 15.3054 12 11 2 5 599.101 15.3740 11 11 -3 -5 12.7576 1.23825 13 11 -3 -5 12.8428 1.40227 12 10 -3 -5 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63.1133 4.46571 4 -5 -3 5 71.0382 7.72016 3 5 -3 -5 65.2921 5.40834 7 -5 3 5 51.5834 6.09501 4 -5 3 5 58.6839 8.35719 6 5 3 -5 65.3027 4.78547 7 -5 3 5 59.7811 6.35717 5 5 3 -5 57.0063 3.75669 8 4 -3 -5 34.4976 3.14030 8 -4 -3 5 36.3210 3.41810 4 4 -3 -5 31.8949 3.72760 7 -4 -3 5 31.6921 6.38238 3 -4 -3 5 36.9806 5.18172 2 -4 3 5 30.8163 4.39782 5 -4 3 5 36.7206 6.00518 6 -4 3 5 39.0383 5.78040 3 4 3 -5 37.5041 2.87678 8 4 3 -5 37.9744 3.56580 7 -4 3 5 35.5124 4.79374 4 -3 -3 5 1.99598 2.12935 2 -3 -3 5 3.39225 1.67868 4 -3 3 5 7.96900 3.06515 6 -3 3 5 0.61030 1.75844 4 -3 3 5 6.28842 2.95682 3 -3 3 5 2.80909 1.89824 5 3 3 -5 2.86873 3.07747 3 2 -3 -5 32.2583 2.62041 5 -2 -3 5 32.0114 4.18208 2 -2 3 5 35.8359 4.87005 6 2 3 -5 36.0842 6.50609 3 -2 3 5 35.0146 3.42670 5 -2 3 5 30.0594 4.58742 3 -2 3 5 37.7242 3.85544 4 -1 -3 5 1.03948 1.27412 4 -1 -3 5 2.86332 1.71563 5 -1 -3 5 3.01589 1.92350 2 1 -3 -5 8.55453 2.34253 4 -1 3 5 2.56722 1.43057 4 -1 3 5 2.94247 1.34620 5 -1 3 5 1.20223 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143.817 7.75159 2 3 -3 5 131.995 6.70164 7 3 -3 5 149.464 9.34299 6 3 3 5 155.730 9.20062 2 3 3 5 148.359 8.12063 1 3 3 5 156.002 8.49302 6 3 3 5 150.200 8.99924 3 -3 3 -5 143.279 7.74481 5 -3 3 -5 156.724 8.69593 4 4 -3 5 198.599 8.87374 7 -4 -3 -5 198.618 9.61887 4 4 -3 5 187.852 11.2119 6 4 -3 5 210.091 11.2824 1 4 -3 5 214.577 9.80941 2 4 3 5 206.413 11.5360 3 4 3 5 253.934 12.0838 6 -4 3 -5 192.159 10.5925 4 -4 3 -5 206.863 10.1988 5 4 3 5 196.082 11.0381 2 4 3 5 198.628 10.5739 1 5 -3 5 2.22636 2.47734 1 5 -3 5 3.98364 2.91699 6 5 -3 5 1.96944 1.65688 7 -5 -3 -5 2.64845 1.88874 4 -5 3 -5 1.15579 2.22663 4 5 3 5 1.07550 2.12331 2 5 3 5 4.00487 3.19148 6 5 3 5 5.57864 3.41527 3 5 3 5 3.27026 2.36790 1 -5 3 -5 1.56928 2.25499 5 6 -3 5 20.2275 5.07134 6 6 -3 5 13.6605 3.13012 7 6 -3 5 16.7308 4.11581 1 -6 -3 -5 18.0909 3.37086 4 6 3 5 16.0940 5.38014 6 -6 3 -5 19.1381 4.08534 5 -6 3 -5 26.3097 4.91045 4 6 3 5 15.6511 3.96417 1 6 3 5 17.7024 4.31500 2 7 -3 5 36.7002 4.50520 7 7 -3 5 30.7248 5.17621 1 7 -3 5 32.4743 3.21117 11 7 -3 5 35.7855 2.49121 15 7 -3 5 37.6614 6.47378 6 7 -3 5 40.2027 3.16133 12 7 3 5 40.6590 7.14938 6 7 3 5 36.1671 2.03385 15 -7 3 -5 40.6884 5.68934 5 7 3 5 36.1040 2.92390 10 7 3 5 43.8284 5.84306 1 7 3 5 39.0646 4.22975 11 7 3 5 44.3181 5.99499 2 8 -3 5 3.19603 0.92137 15 8 -3 5 4.15793 2.65141 1 8 -3 5 2.96433 1.98418 7 8 -3 5 5.09555 3.19908 6 8 -3 5 2.86914 1.39673 12 8 3 5 1.34511 1.40708 11 8 3 5 2.63974 0.61749 15 8 3 5 11.2418 2.01249 10 8 3 5 3.05144 2.51691 1 9 -3 5 104.956 5.01082 11 9 -3 5 105.719 4.72354 12 9 -3 5 107.094 3.93643 15 9 -3 5 95.9474 6.36029 7 9 -3 5 109.806 8.57963 6 9 3 5 105.718 5.14466 11 9 3 5 101.564 4.52901 10 10 -3 5 0.91868 0.52879 15 10 -3 5 5.11122 1.22496 12 10 -3 5 1.53084 0.95117 11 10 3 5 2.35346 1.18285 11 11 -3 5 2.35614 0.75466 12 11 -3 5 3.62024 0.90541 11 11 -4 -5 260.142 6.80961 13 11 -4 -5 260.509 7.01051 12 10 -4 -5 218.913 6.96126 12 10 -4 -5 230.712 6.14216 15 10 -4 -5 216.385 7.05740 8 10 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29.3516 1.83024 15 -6 4 5 34.9916 6.22138 5 6 4 -5 30.3109 3.02972 8 -6 4 5 33.1316 7.29963 6 6 4 -5 30.5898 2.74724 9 6 4 -5 31.5598 3.08679 13 -5 -4 5 37.9048 7.08827 3 5 -4 -5 41.1079 3.35395 8 5 -4 -5 43.7543 5.68067 7 -5 -4 5 48.4190 4.93979 4 -5 -4 5 46.1791 6.81273 2 -5 4 5 33.1567 5.30247 5 -5 4 5 39.3982 7.26100 6 -5 4 5 33.8152 5.93645 4 5 4 -5 40.9605 3.26718 8 -4 -4 5 93.6113 8.05155 2 4 -4 -5 89.1833 4.77213 8 -4 -4 5 94.9677 6.36991 4 4 4 -5 93.1502 9.15567 3 -4 4 5 84.3922 7.70216 4 -4 4 5 90.3634 6.86484 5 4 4 -5 103.113 4.88503 8 -4 4 5 96.2553 8.34943 6 -3 -4 5 109.219 8.11834 2 -3 -4 5 110.035 6.71142 4 3 -4 -5 99.8128 6.50783 1 3 -4 -5 98.4619 4.86408 8 3 4 -5 99.2389 4.61764 8 -3 4 5 104.624 7.85818 6 -3 4 5 98.6954 6.36736 5 -3 4 5 99.9300 7.96134 3 3 4 -5 102.005 9.26636 3 2 -4 -5 353.023 10.9660 5 2 -4 -5 358.942 13.1628 1 -2 -4 5 355.892 12.8014 5 -2 -4 5 345.697 14.8898 2 -2 -4 5 371.172 13.7473 4 -2 4 5 364.107 12.2920 5 -2 4 5 345.537 14.2536 6 -2 4 5 344.697 15.2386 3 2 4 -5 369.286 18.3706 3 -1 -4 5 127.819 6.71016 5 1 -4 -5 122.677 6.28104 5 -1 -4 5 129.818 7.27598 4 -1 -4 5 120.412 7.83277 2 1 -4 -5 125.279 6.80078 1 -1 -4 5 125.103 6.31775 7 -1 4 5 137.651 8.80466 3 -1 4 5 123.560 7.36070 6 1 4 -5 117.836 9.60719 3 -1 4 5 130.168 5.63728 5 0 -4 5 345.967 13.8879 2 0 -4 5 358.688 12.3484 5 0 -4 5 328.055 11.5247 7 0 -4 -5 354.958 12.5620 5 0 -4 -5 360.991 12.9622 1 0 -4 -5 358.495 13.7137 4 0 -4 5 356.003 13.2099 4 0 -4 5 355.551 13.6320 1 0 4 -5 365.693 15.6510 3 0 4 5 352.777 13.1732 2 0 4 5 355.297 15.1489 3 0 4 5 361.260 13.5662 6 1 -4 5 524.576 16.6246 5 1 -4 5 554.007 19.8333 4 1 -4 5 541.005 16.6137 7 -1 -4 -5 558.692 19.0222 4 -1 -4 -5 567.571 18.2898 1 1 -4 5 569.885 18.9188 2 -1 -4 -5 556.617 18.1693 5 1 -4 5 560.211 19.2054 1 1 4 5 561.117 18.4434 6 1 4 5 567.342 19.4194 2 1 4 5 563.912 20.6468 3 -1 4 -5 546.639 15.3929 5 -2 -4 -5 95.1605 6.48466 1 2 -4 5 96.7251 4.87764 5 -2 -4 -5 98.2171 7.11914 4 2 -4 5 98.6976 6.52955 2 2 -4 5 95.6791 7.15929 1 -2 -4 -5 104.710 6.83517 5 2 -4 5 98.9243 5.68961 7 2 4 5 103.209 7.83784 3 -2 4 -5 99.6784 5.68936 5 2 4 5 92.7330 7.32129 2 2 4 5 101.239 6.70615 6 3 -4 5 606.358 21.6399 1 3 -4 5 571.812 18.4205 7 -3 -4 -5 583.790 20.6634 4 3 -4 5 611.607 19.6658 2 3 4 5 575.858 22.4713 3 -3 4 -5 591.183 20.9327 4 3 4 5 590.421 20.5138 6 3 4 5 601.438 22.2975 2 -3 4 -5 596.834 19.0360 5 -4 -4 -5 780.556 25.4039 4 4 -4 5 747.039 23.0620 7 4 -4 5 782.072 26.7706 1 -4 4 -5 773.494 24.1797 5 4 4 5 747.459 26.5341 2 4 4 5 747.795 25.9165 6 -4 4 -5 742.099 25.9465 4 4 4 5 730.232 27.5428 3 4 4 5 795.443 26.0708 1 5 -4 5 733.434 26.0754 1 -5 -4 -5 741.264 24.1863 4 5 -4 5 745.273 26.0896 6 5 -4 5 722.588 23.1177 7 5 4 5 749.398 26.2762 1 -5 4 -5 757.173 24.5871 5 5 4 5 709.550 28.5449 3 -5 4 -5 690.740 26.0071 4 5 4 5 727.266 26.3592 2 6 -4 5 1198.96 31.8771 11 6 -4 5 1215.51 30.9591 15 6 -4 5 1232.79 38.5501 1 6 -4 5 1291.72 38.9019 6 6 -4 5 1270.77 35.6514 7 6 -4 5 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422.350 16.2127 2 -2 2 -6 425.341 14.9155 4 2 2 6 417.001 14.7910 6 2 2 6 398.554 14.7656 3 2 2 6 437.042 14.3933 1 -2 2 -6 421.525 13.9869 5 3 -2 6 233.887 13.0591 6 3 -2 6 230.395 9.12367 7 -3 -2 -6 234.210 10.3682 4 3 -2 6 233.048 11.7308 1 3 -2 6 244.972 10.7364 2 3 2 6 266.377 12.2995 2 -3 2 -6 248.761 10.5040 5 3 2 6 237.106 10.8262 1 -3 2 -6 246.338 11.1455 4 3 2 6 241.342 10.9107 3 3 2 6 234.036 11.0427 6 4 -2 6 188.005 11.7849 6 -4 -2 -6 201.114 9.53630 4 4 -2 6 191.104 8.54514 7 4 -2 6 197.437 9.78265 2 4 -2 6 204.403 10.9179 1 4 2 6 187.505 10.6612 2 4 2 6 202.537 11.1755 6 4 2 6 193.762 10.1251 3 -4 2 -6 205.360 10.0871 5 -4 2 -6 184.215 10.1110 4 4 2 6 195.948 10.6239 1 5 -2 6 24.3162 3.83177 7 5 -2 6 28.2456 5.75927 6 -5 -2 -6 25.6597 3.99473 4 5 -2 6 24.2463 4.16868 2 5 -2 6 30.1119 5.21990 1 -5 2 -6 26.2938 4.49392 5 5 2 6 24.5969 5.54540 6 5 2 6 29.0084 5.08788 2 5 2 6 23.6959 4.56453 1 -5 2 -6 18.2334 3.75189 4 6 -2 6 110.272 7.07510 7 6 -2 6 109.372 8.31138 1 -6 -2 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11 10 2 6 4.10558 1.34928 11 11 -2 6 42.5766 2.29902 11 11 -2 6 42.4847 2.16003 12 11 2 6 39.5722 2.23196 11 11 -3 -6 10.2629 1.06693 13 11 -3 -6 9.49387 1.09224 12 10 -3 -6 30.6004 1.52968 15 10 -3 -6 31.4034 2.44446 8 10 -3 -6 36.6952 2.22523 13 10 -3 -6 30.6820 2.29586 12 10 3 -6 37.9265 2.20445 13 9 -3 -6 97.7022 4.75031 8 9 -3 -6 101.097 3.83048 15 9 -3 -6 101.616 4.32762 13 9 -3 -6 105.115 4.72999 12 9 -3 -6 99.4099 6.35580 7 9 3 -6 104.266 4.35012 9 -9 3 6 92.5982 8.46360 6 9 3 -6 101.095 4.23650 13 9 3 -6 97.3461 4.64790 8 8 -3 -6 136.534 5.64283 13 8 -3 -6 149.546 6.38080 8 8 -3 -6 154.143 6.33163 12 8 -3 -6 147.332 8.27661 7 8 -3 -6 143.634 5.35550 15 8 3 -6 153.488 5.93608 9 -8 3 6 135.705 10.6958 6 8 3 -6 151.709 5.77923 13 8 3 -6 154.070 6.32825 8 7 -3 -6 174.459 6.63354 13 7 -3 -6 185.113 6.59406 15 7 -3 -6 196.858 9.81653 7 7 -3 -6 188.804 7.46984 8 7 -3 -6 186.517 7.43656 12 -7 3 6 176.371 12.6754 6 7 3 -6 187.120 5.40958 15 7 3 -6 183.905 6.80332 13 7 3 -6 193.482 7.09924 9 7 3 -6 188.712 7.40509 8 6 -3 -6 722.481 21.7064 12 -6 -3 6 758.177 29.3112 3 6 -3 -6 789.126 21.1291 8 -6 -3 6 791.076 24.1204 4 6 -3 -6 790.231 24.3801 7 6 -3 -6 748.484 20.1404 13 6 -3 -6 800.255 20.6773 15 6 3 -6 769.787 20.9944 8 6 3 -6 776.314 23.5600 7 -6 3 6 783.372 30.2608 6 6 3 -6 731.514 20.3976 13 6 3 -6 755.392 18.9306 15 -6 3 6 807.952 26.6845 5 -6 3 6 743.977 27.6626 4 6 3 -6 757.667 20.8528 9 -5 -3 6 1926.87 52.0658 2 5 -3 -6 1812.83 45.4436 8 -5 -3 6 1870.90 55.9284 3 5 -3 -6 1893.21 49.2947 7 -5 -3 6 1882.73 48.4076 4 5 3 -6 1809.66 45.5542 8 -5 3 6 1948.40 50.8118 5 -5 3 6 1880.99 54.7970 6 -5 3 6 1790.38 52.0786 4 5 3 -6 1844.73 47.7958 7 4 -3 -6 1942.94 49.2533 7 -4 -3 6 1917.34 49.2001 4 -4 -3 6 1886.70 56.5954 3 4 -3 -6 1837.87 46.4114 8 -4 -3 6 2015.80 53.6129 2 4 3 -6 1929.31 48.3945 7 -4 3 6 1953.10 52.1383 4 -4 3 6 1932.22 53.8069 6 -4 3 6 1909.12 54.0453 3 4 3 -6 1841.05 46.2467 8 -4 3 6 1958.63 50.2756 5 -3 -3 6 1862.36 49.7564 2 -3 -3 6 1782.08 53.8980 3 -3 -3 6 1745.53 45.0066 7 3 -3 -6 1767.52 45.2234 7 -3 -3 6 1818.87 46.5509 4 -3 3 6 1804.39 47.8638 4 -3 3 6 1816.27 49.4245 6 -3 3 6 1821.61 50.5003 3 -3 3 6 1805.56 46.2829 5 -2 -3 6 1035.33 27.7521 7 -2 -3 6 1081.22 31.5521 2 -2 -3 6 1065.58 29.4712 4 -2 -3 6 987.394 28.0279 5 -2 -3 6 1066.32 35.6387 3 -2 3 6 1063.31 28.2271 5 -2 3 6 1045.55 29.4818 4 -2 3 6 1059.02 32.2109 3 -2 3 6 1063.92 30.7913 6 -1 -3 6 3144.26 77.0742 5 1 -3 -6 3165.79 76.7350 5 -1 -3 6 3299.93 83.4065 3 -1 -3 6 3211.84 78.5771 4 -1 -3 6 3345.15 80.5724 2 -1 -3 6 3007.30 76.7853 7 -1 3 6 3367.84 79.6342 6 -1 3 6 3291.37 81.5527 3 -1 3 6 3265.29 76.2305 5 0 -3 6 2570.49 62.9739 4 0 -3 -6 2517.32 61.8026 1 0 -3 6 2378.50 60.7545 7 0 -3 -6 2540.32 63.2589 4 0 -3 6 2554.27 65.0676 3 0 -3 6 2551.36 64.2391 2 0 -3 -6 2563.10 61.9985 5 0 -3 6 2579.95 61.5443 5 0 3 6 2510.03 65.2485 3 0 3 6 2586.26 63.6950 6 0 3 6 2569.73 63.6811 2 1 -3 6 1125.24 33.2166 1 -1 -3 -6 1138.32 31.2232 5 -1 -3 -6 1161.43 31.2280 1 -1 -3 -6 1203.17 32.7252 4 1 -3 6 1193.01 30.0999 5 1 -3 6 1086.34 29.8919 7 1 -3 6 1143.75 31.0979 4 1 -3 6 1180.84 32.7904 2 1 3 6 1178.30 34.0708 2 1 3 6 1148.39 32.2663 6 -1 3 -6 1131.17 29.5614 5 1 3 6 1157.03 33.7563 3 -2 -3 -6 2708.27 67.4724 4 2 -3 6 2674.33 69.0456 1 2 -3 6 2675.48 67.2860 2 -2 -3 -6 2659.63 66.1535 5 2 -3 6 2624.65 64.7201 7 2 -3 6 2568.95 62.8719 5 -2 3 -6 2698.56 65.6337 5 2 3 6 2686.60 67.3312 6 2 3 6 2716.37 66.6720 1 2 3 6 2693.93 69.4488 2 -2 3 -6 2717.19 67.2774 4 2 3 6 2711.45 68.8865 3 3 -3 6 2825.98 72.0546 2 3 -3 6 2883.58 70.0920 7 3 -3 6 2776.51 74.1207 1 -3 -3 -6 2935.56 72.6490 4 3 3 6 2934.91 74.2609 3 3 3 6 2953.19 72.7902 1 3 3 6 2821.71 73.0527 6 -3 3 -6 2874.05 71.4031 5 -3 3 -6 2909.29 73.2357 4 3 3 6 2894.90 74.7194 2 -4 -3 -6 4091.19 98.4344 4 4 -3 6 4197.60 98.3818 2 4 -3 6 4008.30 96.1865 7 4 -3 6 3828.80 100.060 1 4 -3 6 3972.91 100.728 6 4 3 6 4074.59 100.985 2 -4 3 -6 3838.24 97.6570 5 4 3 6 4137.60 100.680 6 -4 3 -6 3817.02 99.3530 4 4 3 6 4143.01 101.218 3 4 3 6 3966.84 99.6656 1 -5 -3 -6 3210.37 78.9793 4 5 -3 6 3187.74 82.2664 6 5 -3 6 3067.27 81.2852 1 5 -3 6 3257.58 78.2121 7 5 3 6 3155.48 82.2856 1 5 3 6 3256.36 83.9871 6 5 3 6 3125.64 81.9919 2 -5 3 -6 3013.61 80.8947 4 -5 3 -6 3123.06 79.5428 5 6 -3 6 2671.88 65.6481 7 6 -3 6 2581.55 61.1218 12 -6 -3 -6 2643.60 65.4813 4 6 -3 6 2469.10 60.1748 15 6 -3 6 2595.09 69.1618 6 6 -3 6 2458.52 61.2410 11 6 -3 6 2582.47 68.3528 1 6 3 6 2620.19 69.1391 2 6 3 6 2483.02 60.6417 10 -6 3 -6 2612.07 66.2939 5 6 3 6 2476.20 59.2519 15 -6 3 -6 2439.09 67.2668 4 6 3 6 2585.18 72.6922 6 6 3 6 2544.89 68.8867 1 6 3 6 2558.72 62.3838 11 7 -3 6 2332.43 59.1938 7 7 -3 6 2268.51 54.8470 12 7 -3 6 2140.25 53.8144 15 7 -3 6 2285.48 62.2839 1 7 -3 6 2295.20 55.3967 11 7 -3 6 2399.96 63.4296 6 7 3 6 2228.73 62.3456 1 7 3 6 2275.72 53.0575 15 -7 3 -6 2390.16 60.3002 5 7 3 6 2254.36 54.6217 10 7 3 6 2305.26 65.5411 6 7 3 6 2237.59 62.5765 2 7 3 6 2295.49 56.2220 11 8 -3 6 744.196 26.5831 6 8 -3 6 794.270 20.7671 11 8 -3 6 685.325 25.3215 1 8 -3 6 765.647 23.6594 7 8 -3 6 776.830 19.2925 15 8 -3 6 754.192 20.2221 12 8 3 6 774.137 21.2212 11 -8 3 -6 772.373 24.6767 5 8 3 6 714.290 25.7425 1 8 3 6 740.917 19.9311 10 8 3 6 768.780 18.1715 15 9 -3 6 786.326 20.1074 12 9 -3 6 780.396 20.4924 11 9 -3 6 787.979 19.0932 15 9 -3 6 709.410 25.9957 6 9 -3 6 743.018 22.8227 7 9 3 6 780.623 20.7383 11 9 3 6 776.285 19.8568 10 10 -3 6 930.822 21.7893 15 10 -3 6 931.259 22.9239 12 10 -3 6 927.290 23.1773 11 10 3 6 908.798 22.5042 10 10 3 6 927.473 23.2477 11 11 -3 6 973.930 22.9701 12 11 -3 6 957.382 23.1094 11 10 -4 -6 308.725 7.65984 15 10 -4 -6 300.841 8.25211 13 10 -4 -6 293.080 8.47286 12 10 -4 -6 279.019 10.1513 8 9 -4 -6 194.473 6.12009 15 9 -4 -6 205.804 6.93876 12 9 -4 -6 200.055 8.91327 7 9 -4 -6 200.407 6.51145 13 9 -4 -6 189.021 6.96882 8 9 4 -6 184.725 6.67257 8 9 4 -6 201.550 6.50037 9 9 4 -6 191.729 6.24751 13 8 -4 -6 209.029 6.99995 15 8 -4 -6 203.554 9.83728 7 8 -4 -6 215.847 7.21035 13 8 -4 -6 213.831 7.87739 8 8 -4 -6 208.081 7.66937 12 -8 4 6 205.583 11.0406 5 8 4 -6 217.315 7.67691 8 8 4 -6 202.143 7.00557 13 -8 4 6 201.834 13.0643 6 8 4 -6 214.350 7.30877 9 7 -4 -6 505.935 17.9157 7 7 -4 -6 483.490 14.0354 13 7 -4 -6 500.319 15.0105 12 7 -4 -6 492.301 14.0765 15 7 -4 -6 498.638 14.9202 8 7 4 -6 507.158 14.3799 9 7 4 -6 499.512 14.0508 13 -7 4 6 498.930 19.5475 5 -7 4 6 501.925 22.9567 6 7 4 -6 501.171 12.4491 15 7 4 -6 497.035 14.7952 8 6 -4 -6 323.747 11.4515 12 6 -4 -6 347.042 10.4223 13 6 -4 -6 339.521 13.9780 7 6 -4 -6 326.830 10.9855 8 6 -4 -6 304.366 10.3462 15 -6 4 6 343.088 12.0036 11 6 4 -6 318.487 10.5392 9 6 4 -6 323.185 10.2517 13 6 4 -6 336.910 11.0890 8 -6 4 6 346.405 16.0429 5 -6 4 6 327.388 18.7224 6 5 -4 -6 753.774 20.5941 8 5 -4 -6 748.671 24.0010 7 -5 -4 6 675.298 28.3724 3 -5 -4 6 761.848 26.6774 2 -5 -4 6 752.298 24.4538 4 -5 4 6 678.067 26.9514 4 5 4 -6 734.263 20.5350 8 -5 4 6 750.604 29.1693 6 -5 4 6 770.532 25.5314 5 5 4 -6 803.426 24.6815 9 5 4 -6 752.499 19.8324 15 -4 -4 6 223.352 10.7462 4 -4 -4 6 211.433 12.2097 2 -4 -4 6 198.644 13.5411 3 4 -4 -6 215.516 8.03678 8 -4 4 6 206.415 12.5246 3 4 4 -6 205.981 7.73268 8 -4 4 6 227.729 13.3071 6 -4 4 6 207.268 10.6649 5 -3 -4 6 43.4580 4.69903 4 3 -4 -6 38.2074 3.12344 8 -3 -4 6 39.9178 5.23076 2 -3 -4 6 36.4808 7.19202 3 -3 -4 6 38.1276 3.71219 7 3 4 -6 43.8144 2.99173 8 -3 4 6 45.2397 6.80323 3 -3 4 6 47.2196 4.49044 5 -3 4 6 39.6820 6.24181 6 -2 -4 6 9.02229 2.89464 2 -2 -4 6 10.2657 2.73482 4 -2 -4 6 5.41181 2.30506 5 -2 -4 6 3.59469 3.05991 3 -2 -4 6 4.52021 1.61693 7 2 -4 -6 8.72652 2.40181 1 -2 4 6 6.96890 3.15136 3 -2 4 6 7.62815 2.72926 6 2 4 -6 3.58287 1.27994 8 -2 4 6 4.93681 1.73009 5 1 -4 -6 130.017 7.02064 1 -1 -4 6 141.361 8.75771 2 -1 -4 6 128.027 7.62233 4 1 -4 -6 126.845 6.53646 5 -1 -4 6 124.752 6.23687 7 -1 -4 6 131.480 9.88080 3 -1 -4 6 137.009 7.16749 5 -1 4 6 125.909 5.75724 5 -1 4 6 125.088 7.84240 6 -1 4 6 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6.98421 5 3 4 6 119.254 8.90700 2 -4 -4 -6 123.953 8.96882 4 4 -4 6 138.045 7.70840 7 4 -4 6 135.335 9.23677 2 4 -4 6 124.801 9.23191 1 4 4 6 116.339 10.0098 3 -4 4 -6 132.904 9.98948 4 4 4 6 118.220 9.16529 6 -4 4 -6 140.527 8.28618 5 4 4 6 134.563 9.23153 1 4 4 6 118.287 9.14564 2 5 -4 6 129.724 7.72820 7 5 -4 6 120.817 9.31577 1 -5 -4 -6 130.470 8.82146 4 5 4 6 119.644 9.47799 2 -5 4 -6 121.024 9.82364 4 5 4 6 130.834 11.3387 3 5 4 6 122.993 4.79317 15 5 4 6 116.413 5.59651 10 -5 4 -6 126.904 8.52325 5 5 4 6 129.234 6.26352 11 5 4 6 133.839 9.83761 1 5 4 6 133.375 10.7897 6 6 -4 6 93.2651 4.47781 15 6 -4 6 104.439 8.37812 1 6 -4 6 96.2884 8.70366 6 6 -4 6 97.4998 4.87666 12 6 -4 6 92.7483 5.14903 11 6 -4 6 99.8738 7.12092 7 -6 4 -6 99.3372 7.52038 5 6 4 6 87.7314 4.72490 10 6 4 6 83.8857 8.07014 1 6 4 6 85.3159 3.70344 15 6 4 6 79.8776 8.03881 2 6 4 6 87.6993 5.51582 11 7 -4 6 29.7524 3.08009 11 7 -4 6 23.3176 2.24426 15 7 -4 6 27.5600 5.43122 6 7 -4 6 28.7488 2.70125 12 7 -4 6 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738.508 19.6022 10 8 -5 6 610.296 16.1735 12 8 -5 6 622.966 16.0029 15 8 -5 6 628.636 16.6679 11 8 -5 6 601.869 19.1731 7 8 5 6 590.913 16.2875 10 8 5 6 601.125 17.0587 11 9 -5 6 411.351 11.4345 11 9 -5 6 413.442 10.7946 15 9 -5 6 412.242 11.0887 12 9 5 6 414.854 11.5344 11 9 5 6 407.495 11.2031 10 10 -5 6 414.960 10.8089 12 10 -5 6 431.760 10.4198 15 10 -5 6 447.660 11.0856 11 9 -6 -6 757.550 18.8693 15 9 -6 -6 793.947 18.9540 13 9 6 -6 791.666 18.9562 9 8 -6 -6 1339.92 31.6677 15 8 -6 -6 1298.64 32.1175 8 8 -6 -6 1308.97 31.3622 13 8 6 -6 1309.79 31.5454 9 -8 6 6 1318.45 31.8825 11 8 6 -6 1269.87 31.6344 8 7 -6 -6 1484.56 36.5222 8 7 -6 -6 1449.18 35.5649 13 7 -6 -6 1516.07 36.2756 15 7 6 -6 1462.65 33.8250 15 7 6 -6 1428.50 36.1225 8 7 6 -6 1488.30 35.4063 13 -7 6 6 1466.62 36.6366 11 7 6 -6 1467.52 35.7860 9 6 -6 -6 1402.55 33.9025 13 6 -6 -6 1398.86 34.8781 8 6 6 -6 1404.89 33.8560 13 6 6 -6 1407.92 34.7793 8 -6 6 6 1348.47 35.6058 11 6 6 -6 1351.78 34.1477 9 -6 6 6 1310.79 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57.0631 7.01962 1 -4 -6 -6 53.8965 6.66865 1 -4 -6 -6 61.5297 8.55797 5 4 -6 6 55.6686 3.34518 14 4 -6 6 57.1008 5.49295 7 4 6 6 62.0109 4.56992 9 4 6 6 57.4242 4.03900 10 -4 6 -6 57.6115 4.13043 10 4 6 6 57.9997 4.15875 11 4 6 6 56.0903 3.43503 15 4 6 6 54.3447 7.30673 2 -5 -6 -6 96.6106 8.90045 1 5 -6 6 106.151 4.68892 13 5 -6 6 105.817 3.35309 14 5 -6 6 96.2014 8.62123 1 5 -6 6 109.349 7.28394 7 -5 6 -6 100.893 6.72287 5 5 6 6 91.2703 5.46216 11 5 6 6 104.874 4.47623 15 5 6 6 103.943 5.19937 10 5 6 6 100.149 5.27077 9 6 -6 6 37.5796 2.74759 13 6 -6 6 36.3496 4.39532 7 6 -6 6 45.5174 3.37525 11 -6 6 -6 35.0087 4.53660 5 6 6 6 31.5733 2.94498 9 6 6 6 28.6286 3.36825 11 6 6 6 33.0717 2.22760 15 6 6 6 24.6608 2.74089 10 7 -6 6 8.54223 1.72920 11 7 -6 6 10.6495 2.46167 7 7 6 6 9.93770 1.82278 9 7 6 6 10.2570 2.07636 11 7 6 6 12.5564 1.22463 15 7 6 6 9.80953 1.70549 10 8 -6 6 67.0536 3.11130 15 8 -6 6 72.2947 3.44471 11 8 6 6 71.6130 3.45300 10 8 6 6 70.9172 3.72029 11 9 -6 6 25.4431 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403.814 12.8666 11 4 7 6 393.373 12.3442 10 -5 -7 -6 415.704 25.5889 5 5 -7 6 410.256 11.8510 13 5 7 6 417.247 12.5061 10 5 7 6 420.770 13.2771 11 5 7 6 406.503 12.7260 9 -5 7 -6 415.072 13.3377 14 5 7 6 430.820 11.7405 15 6 -7 6 73.9131 3.58253 13 -6 7 -6 83.8877 4.54688 14 6 7 6 78.2761 4.56904 11 6 7 6 84.6734 3.31835 15 6 7 6 79.9128 4.06509 9 6 7 6 80.3895 4.07935 10 7 7 6 366.235 10.6312 11 7 7 6 354.558 10.3069 10 -7 7 -6 382.365 12.9343 14 7 7 6 354.128 9.97960 9 7 7 6 360.699 8.72211 15 8 -7 6 79.0090 3.05962 15 8 7 6 83.2195 3.20151 10 -7 8 6 112.628 4.10957 14 7 8 -6 107.117 3.68605 9 -7 8 6 104.127 3.85491 11 6 -8 -6 154.009 6.18340 8 -6 -8 6 147.839 5.91465 13 6 -8 -6 162.472 5.07149 13 -6 8 6 153.865 5.81195 11 6 8 -6 162.624 5.35910 9 6 8 -6 161.968 4.28502 15 6 8 -6 157.285 5.27843 10 -6 8 6 154.294 5.93284 14 5 -8 -6 244.024 8.31033 8 -5 -8 6 240.601 8.29299 8 5 8 -6 245.494 8.01249 10 5 8 -6 258.042 7.97290 9 5 8 -6 256.716 7.32658 15 -5 8 6 260.660 9.05687 11 -5 8 6 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15 6 -3 7 234.189 11.0467 7 6 3 7 220.783 7.14267 15 6 3 7 219.395 9.16355 11 6 3 7 222.992 13.1108 1 6 3 7 221.481 13.0589 2 6 3 7 224.618 8.21610 10 6 3 7 238.611 15.6831 6 -6 3 -7 248.793 12.0721 5 7 -3 7 87.8059 6.57450 7 7 -3 7 84.5838 7.59771 1 7 -3 7 83.5345 4.75546 11 7 -3 7 88.6401 8.23294 6 7 -3 7 85.2929 4.04389 15 7 -3 7 92.2658 4.75230 12 7 3 7 91.9312 4.65443 10 7 3 7 82.4156 7.70358 1 7 3 7 83.9750 5.22629 11 7 3 7 87.7135 3.67674 15 -7 3 -7 89.8393 7.36091 5 7 3 7 85.9592 9.68660 6 8 -3 7 81.9750 3.62934 15 8 -3 7 79.7010 4.41435 11 8 -3 7 85.2136 4.29773 12 8 -3 7 84.4640 6.21273 7 8 -3 7 73.2998 7.47363 6 8 3 7 75.9039 4.76492 11 8 3 7 87.4993 9.00422 6 8 3 7 78.8037 4.13569 10 -8 3 -7 72.7016 6.65654 5 8 3 7 79.3821 3.03140 15 9 -3 7 6.90667 1.11352 15 9 -3 7 2.36161 1.68524 7 9 -3 7 0.94510 0.97982 12 9 -3 7 3.33500 1.32900 11 9 3 7 1.07155 1.20438 11 9 3 7 2.53626 1.16190 10 10 -3 7 0.11482 0.74455 12 10 -3 7 1.84701 0.52880 15 10 -3 7 2.16315 0.93201 11 10 3 7 1.68438 0.84161 10 10 3 7 3.75703 1.11162 11 10 -4 -7 621.343 15.7659 12 10 -4 -7 640.385 15.5987 13 10 -4 -7 621.452 14.8860 15 9 -4 -7 576.855 14.8179 13 9 -4 -7 534.744 20.8378 7 9 -4 -7 565.323 15.1930 12 9 -4 -7 564.032 14.4365 15 9 -4 -7 564.977 15.4186 8 9 4 -7 576.542 14.6077 13 9 4 -7 563.874 15.1374 8 9 4 -7 572.267 14.8033 9 8 -4 -7 1022.52 28.9474 7 8 -4 -7 1023.08 25.9867 8 8 -4 -7 1015.67 25.1575 13 8 -4 -7 1024.22 25.0342 15 8 -4 -7 1003.60 25.8840 12 8 4 -7 1011.00 25.0535 13 8 4 -7 1008.84 25.7492 8 -8 4 7 951.678 29.8004 5 8 4 -7 986.872 25.2450 9 -8 4 7 960.510 33.2520 6 7 -4 -7 501.555 14.9870 12 7 -4 -7 505.219 17.9546 7 7 -4 -7 500.904 14.8668 8 7 -4 -7 504.728 14.0162 13 7 -4 -7 500.495 14.1823 15 7 4 -7 495.404 14.2321 9 -7 4 7 463.002 22.1052 6 -7 4 7 478.530 19.0639 5 7 4 -7 507.003 14.8151 8 7 4 -7 507.041 14.0570 13 7 4 -7 486.689 12.4960 15 6 -4 -7 1298.67 33.9167 12 6 -4 -7 1336.49 33.5797 8 6 -4 -7 1363.54 33.1281 15 6 -4 -7 1283.51 32.4373 13 6 -4 -7 1329.20 37.6577 7 6 4 -7 1267.39 33.3332 8 -6 4 7 1347.90 39.8517 5 6 4 -7 1255.95 32.4201 13 6 4 -7 1306.00 31.3367 15 6 4 -7 1267.03 32.8030 9 -6 4 7 1344.58 44.6866 6 -5 -4 7 2850.04 77.0151 2 5 -4 -7 2907.51 69.7120 12 5 -4 -7 2995.79 69.7374 8 -5 -4 7 2947.67 85.5137 3 5 -4 -7 2864.52 68.6079 13 -5 4 7 3073.23 75.6044 5 5 4 -7 2886.11 67.8771 15 -5 4 7 2794.96 78.7089 4 5 4 -7 2791.02 69.0580 9 -5 4 7 3088.13 81.2273 6 5 4 -7 2855.29 68.5853 13 5 4 -7 2983.59 69.7544 8 -4 -4 7 1639.07 45.0303 4 -4 -4 7 1626.58 47.7122 2 -4 -4 7 1622.39 42.1084 7 -4 -4 7 1535.96 50.2313 3 4 -4 -7 1585.21 39.9012 8 -4 4 7 1662.56 44.2096 5 -4 4 7 1542.82 48.0057 3 -4 4 7 1603.77 48.2085 6 4 4 -7 1592.11 39.6777 8 -3 -4 7 1623.51 51.7973 3 -3 -4 7 1648.69 45.7137 4 -3 -4 7 1668.27 42.9000 7 -3 -4 7 1721.54 48.5380 2 3 -4 -7 1619.38 40.9389 8 -3 4 7 1731.25 48.1609 6 -3 4 7 1701.53 43.7444 5 3 4 -7 1581.11 40.3112 8 -3 4 7 1606.49 48.9289 3 -2 -4 7 1939.19 54.0272 2 -2 -4 7 1955.84 52.1150 4 -2 -4 7 1909.74 50.2437 5 -2 -4 7 1956.21 49.1486 7 -2 -4 7 1990.60 58.0744 3 -2 4 7 1981.85 53.4533 6 -2 4 7 1949.46 48.9995 5 2 4 -7 1941.60 46.8068 8 -2 4 7 1944.45 55.4440 3 -1 -4 7 1695.40 46.7591 4 1 -4 -7 1790.38 46.9880 1 -1 -4 7 1729.89 44.2095 7 -1 -4 7 1748.81 45.2884 5 -1 -4 7 1664.08 50.2225 3 -1 -4 7 1708.08 48.4074 2 1 -4 -7 1752.63 44.1377 5 -1 4 7 1757.93 42.6624 5 -1 4 7 1740.09 50.0552 3 1 4 -7 1730.35 41.6659 8 -1 4 7 1770.64 47.8482 6 0 -4 -7 3006.51 73.6134 1 0 -4 7 2913.41 74.3114 4 0 -4 7 3038.16 72.7577 5 0 -4 7 2876.99 71.9887 7 0 4 -7 2961.24 69.2972 8 0 4 7 2952.37 77.9576 3 0 4 7 3086.31 75.7820 6 1 -4 7 2712.59 66.6939 5 -1 -4 -7 2836.13 68.9227 5 1 -4 7 2687.10 67.0205 7 -1 -4 -7 2774.40 70.8375 4 1 -4 7 2723.59 70.5033 2 -1 -4 -7 2687.41 68.7363 1 1 4 7 2736.13 72.8874 3 1 4 7 2710.75 70.2178 6 1 4 7 2796.51 71.5006 2 -2 -4 -7 1985.30 53.4065 1 2 -4 7 2000.31 53.9681 2 2 -4 7 2018.90 55.5645 1 -2 -4 -7 1974.49 54.8862 4 2 -4 7 2003.51 51.1960 7 -2 -4 -7 2021.90 53.2986 5 2 4 7 2075.38 56.8767 2 2 4 7 1999.17 54.3164 6 2 4 7 2056.55 56.9493 3 -2 4 -7 2026.57 50.2594 5 3 -4 7 2055.32 51.3394 7 3 -4 7 2016.03 53.6731 2 -3 -4 -7 1949.44 54.9587 4 -3 -4 -7 1952.28 53.8061 1 3 -4 7 1935.32 55.0582 1 -3 -4 -7 2004.18 53.5730 5 3 4 7 1979.05 56.2562 2 -3 4 -7 1989.29 51.0925 5 3 4 7 1926.86 56.5383 3 3 4 7 2039.81 55.0013 6 4 -4 7 353.465 13.7579 7 -4 -4 -7 347.407 16.2350 4 4 -4 7 347.514 16.2727 1 4 -4 7 353.897 15.2116 2 4 4 7 360.886 17.1302 2 4 4 7 383.637 16.8253 1 -4 4 -7 344.479 14.2032 5 4 4 7 327.263 17.3812 3 4 4 7 364.548 17.0533 6 5 -4 7 1082.90 34.5186 1 5 -4 7 1069.45 27.9294 12 5 -4 7 1125.58 31.9280 7 5 -4 7 1050.89 25.1714 14 5 4 7 1093.41 35.8888 1 5 4 7 1069.62 26.8084 15 5 4 7 1076.06 28.8546 11 5 4 7 1049.17 35.2930 2 -5 4 -7 1074.00 27.7393 10 -5 4 -7 1100.91 32.6130 5 5 4 7 1105.32 37.0067 6 5 4 7 1048.27 27.7225 10 6 -4 7 2687.92 66.0023 15 6 -4 7 2670.68 72.9994 1 6 -4 7 2972.46 71.0803 7 6 -4 7 2737.01 66.1675 11 6 -4 7 2735.06 65.7294 12 6 4 7 2663.10 74.2546 2 6 4 7 2754.61 74.9516 1 6 4 7 2858.95 78.3418 6 6 4 7 2789.90 65.8106 10 6 4 7 2847.31 67.6131 11 -6 4 -7 2805.88 70.9083 5 6 4 7 2727.03 64.4724 15 7 -4 7 780.820 20.0132 15 7 -4 7 762.365 24.1164 7 7 -4 7 761.204 20.4091 12 7 -4 7 753.524 20.7588 11 7 -4 7 730.705 26.2751 1 7 4 7 732.611 27.0370 1 7 4 7 789.294 20.5161 10 7 4 7 800.387 19.1478 15 7 4 7 787.985 21.9363 11 -7 4 -7 736.945 24.1959 5 8 -4 7 587.994 16.0847 12 8 -4 7 618.835 15.6403 15 8 -4 7 609.005 16.4328 11 8 -4 7 599.480 19.2396 7 8 4 7 582.297 16.0340 10 8 4 7 598.121 14.3350 15 8 4 7 592.747 17.0873 11 -8 4 -7 532.836 19.4110 5 9 -4 7 555.808 14.7166 12 9 -4 7 550.836 14.1201 15 9 -4 7 567.988 14.9645 11 9 4 7 548.460 15.2655 11 9 4 7 555.319 14.6989 10 10 -4 7 128.106 3.66812 15 10 -4 7 132.056 4.30010 12 10 -4 7 131.341 4.42784 11 10 4 7 128.720 4.17236 10 10 4 7 129.173 4.43951 11 10 -5 -7 220.086 6.03184 13 10 -5 -7 226.935 5.55469 15 9 -5 -7 60.4211 2.77235 13 9 -5 -7 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7 8 -3 -8 1039.71 26.0531 15 8 -3 -8 1087.91 27.2213 12 8 -3 -8 1102.01 27.3566 8 8 -3 -8 1022.27 26.3009 13 -8 3 8 1028.48 31.3988 5 -8 3 8 1033.55 34.2608 6 8 3 -8 1041.49 26.5438 9 8 3 -8 1055.71 24.4543 15 8 3 -8 1081.12 26.4117 13 8 3 -8 1059.12 27.1875 8 7 -3 -8 936.992 24.5823 13 7 -3 -8 970.962 29.0936 7 7 -3 -8 976.132 25.7199 12 7 -3 -8 977.236 25.5577 8 7 -3 -8 944.194 24.5474 15 -7 -3 8 1003.70 28.8952 7 7 3 -8 945.611 24.9625 9 -7 3 8 926.232 33.6205 6 7 3 -8 970.789 23.2985 15 7 3 -8 992.404 25.5425 8 -7 3 8 964.619 30.4313 5 7 3 -8 956.359 24.6328 13 6 -3 -8 1485.81 40.9690 7 -6 -3 8 1493.27 40.4107 7 6 -3 -8 1435.88 36.9364 12 6 -3 -8 1436.94 35.5851 13 6 -3 -8 1425.49 36.5435 8 6 -3 -8 1434.57 35.8001 15 -6 3 8 1464.68 46.7208 6 6 3 -8 1409.12 34.5898 15 6 3 -8 1460.41 36.1594 9 -6 3 8 1507.32 42.6103 5 6 3 -8 1404.61 35.6397 13 6 3 -8 1419.70 36.4705 8 5 -3 -8 2089.48 50.5587 13 5 -3 -8 2071.89 51.0494 8 5 -3 -8 2060.79 51.1314 12 -5 -3 8 2104.69 56.5079 4 5 -3 -8 2168.36 55.1647 7 -5 -3 8 2226.94 54.8171 7 -5 -3 8 2034.32 62.1159 3 5 3 -8 2009.35 49.5246 15 -5 3 8 2187.58 60.9889 6 -5 3 8 1992.64 59.7291 3 5 3 -8 2123.95 51.2066 8 -5 3 8 2202.02 56.6032 5 5 3 -8 1998.79 50.1030 13 5 3 -8 2097.14 50.8996 9 -4 -3 8 3105.48 75.2819 7 4 -3 -8 3169.48 75.5574 7 4 -3 -8 2990.52 72.3843 8 -4 -3 8 3129.49 81.0191 2 -4 -3 8 2995.30 77.4246 4 -4 -3 8 2930.50 84.2392 3 -4 3 8 3006.48 82.8176 3 -4 3 8 3144.34 76.6114 5 -4 3 8 2999.84 78.7665 4 -4 3 8 3116.22 80.7905 6 4 3 -8 2989.58 72.1030 8 -3 -3 8 1375.28 45.7424 3 -3 -3 8 1359.04 38.6379 4 3 -3 -8 1302.90 33.9918 8 -3 -3 8 1326.49 40.8426 2 -3 -3 8 1355.66 36.3859 7 -3 -3 8 1377.24 37.1295 5 -3 3 8 1421.93 37.0720 5 3 3 -8 1359.39 33.6756 8 -3 3 8 1391.61 39.3170 4 -3 3 8 1296.11 42.2011 3 -3 3 8 1368.90 40.4990 6 -2 -3 8 1977.16 52.2115 4 -2 -3 8 1918.27 57.3269 3 -2 -3 8 1940.50 54.3365 2 -2 -3 8 1954.17 49.5550 7 -2 -3 8 1956.63 50.2620 5 -2 3 8 2035.45 49.7213 5 2 3 -8 1907.28 46.8326 8 -2 3 8 1972.47 55.8712 3 -2 3 8 2014.51 53.5667 6 -1 -3 8 1785.79 45.1105 7 -1 -3 8 1772.54 47.5549 4 -1 -3 8 1805.89 49.6228 2 1 -3 -8 1792.84 44.4515 5 -1 -3 8 1752.49 45.5945 5 -1 -3 8 1725.13 50.6692 3 -1 3 8 1794.77 48.6000 6 -1 3 8 1834.01 44.3883 5 -1 3 8 1741.03 50.6266 3 0 -3 8 490.464 17.8400 4 0 -3 8 537.541 19.7396 2 0 -3 8 518.365 16.4754 7 0 -3 -8 533.863 17.2966 5 0 -3 8 536.911 16.7584 5 0 3 8 548.375 19.2980 6 0 3 8 529.395 20.5071 3 1 -3 8 1351.65 35.7613 5 -1 -3 -8 1414.87 39.9943 4 -1 -3 -8 1393.22 37.5415 1 1 -3 8 1349.53 36.3939 7 1 -3 8 1430.83 40.1484 2 -1 -3 -8 1404.17 37.9673 5 1 3 8 1384.30 39.5298 6 1 3 8 1391.91 41.0464 3 -1 3 -8 1376.65 34.8426 5 1 3 8 1404.92 41.7126 2 -2 -3 -8 951.933 30.3134 4 2 -3 8 948.135 27.0069 7 2 -3 8 958.861 30.1375 2 2 3 8 954.169 30.9881 3 2 3 8 974.611 28.9972 1 2 3 8 1010.50 30.6307 6 2 3 8 938.178 31.7391 2 -2 3 -8 971.917 27.2150 5 -3 -3 -8 660.456 24.3286 4 3 -3 8 677.949 23.6487 2 3 -3 8 680.082 21.1021 7 -3 -3 -8 672.697 22.9225 5 3 -3 8 672.934 24.3309 1 3 3 8 695.926 25.4342 2 3 3 8 690.375 23.3432 1 3 3 8 662.055 24.4679 3 -3 3 -8 693.666 21.9750 5 3 3 8 719.439 24.8816 6 -4 -3 -8 453.319 18.1832 5 4 -3 8 430.033 18.2125 1 4 -3 8 435.103 15.6638 7 -4 -3 -8 402.400 18.0363 4 4 -3 8 444.141 17.9037 2 4 3 8 437.208 19.2584 6 -4 3 -8 430.760 16.7241 5 4 3 8 429.157 19.0277 2 4 3 8 448.414 18.5915 1 -4 3 -8 395.751 18.7616 4 5 -3 8 328.476 11.1456 12 5 -3 8 359.990 17.0664 6 5 -3 8 353.284 16.2184 1 5 -3 8 361.821 14.0113 7 5 -3 8 331.371 15.3738 2 -5 3 -8 351.478 15.0317 5 5 3 8 338.538 10.2937 15 5 3 8 347.824 18.0534 6 5 3 8 353.729 17.1941 1 5 3 8 341.671 12.0005 11 -5 3 -8 320.762 16.2230 4 5 3 8 336.799 10.9361 10 5 3 8 337.604 16.6441 2 6 -3 8 151.580 10.8204 6 6 -3 8 131.333 8.15922 7 6 -3 8 141.977 6.34727 11 6 -3 8 125.636 6.08510 12 6 -3 8 139.084 5.74309 15 6 -3 8 133.753 9.63426 1 6 3 8 146.945 6.20470 10 6 3 8 145.229 12.7092 6 6 3 8 136.310 10.2774 1 6 3 8 136.087 10.2631 2 6 3 8 142.439 7.11323 11 6 3 8 135.381 5.26620 15 -6 3 -8 144.074 9.06383 5 7 -3 8 10.3700 2.96110 7 7 -3 8 9.85230 1.62477 15 7 -3 8 9.63368 1.92032 12 7 -3 8 12.7630 4.37004 6 7 -3 8 8.52747 3.38948 1 7 -3 8 7.47212 1.80929 11 -7 3 -8 11.3809 1.95442 10 -7 3 -8 10.0970 3.25501 5 7 3 8 9.43561 4.92644 6 7 3 8 9.67941 1.96293 10 7 3 8 22.6083 4.93884 1 7 3 8 11.2373 1.50758 15 7 3 8 7.83493 2.08160 11 8 -3 8 79.8612 4.31611 11 8 -3 8 79.7718 7.58672 6 8 -3 8 78.7562 4.10532 12 8 -3 8 80.4050 3.61131 15 8 -3 8 76.4757 5.85618 7 8 3 8 83.0868 4.78182 11 -8 3 -8 75.0019 6.49133 5 8 3 8 78.6569 4.10775 10 8 3 8 80.3699 3.11285 15 8 3 8 79.9499 9.31637 6 9 -3 8 29.6416 2.33809 12 9 -3 8 30.3535 4.12941 7 9 -3 8 35.0296 2.62259 11 9 -3 8 34.6421 1.96203 15 9 3 8 32.2730 2.79468 11 9 3 8 36.3668 2.50882 10 10 -3 8 10.5714 0.78963 15 10 -3 8 7.87865 1.16230 11 10 -3 8 6.08003 1.01239 12 10 3 8 7.78352 1.12241 10 10 3 8 7.42883 1.21943 11 10 -4 -8 8.27888 1.03293 13 10 -4 -8 8.40121 0.66739 15 10 -4 -8 9.26804 1.13205 12 9 -4 -8 76.5130 3.34038 13 9 -4 -8 76.0899 3.08389 15 9 -4 -8 78.6666 3.76463 8 9 -4 -8 79.5096 3.66323 12 9 4 -8 79.2890 3.40290 9 9 4 -8 78.0484 3.28066 13 9 4 -8 75.8884 3.59861 8 8 -4 -8 5.45647 1.55868 12 8 -4 -8 4.63965 1.32526 13 8 -4 -8 6.51741 2.44576 7 8 -4 -8 7.10801 1.32257 15 8 -4 -8 5.24889 1.53826 8 8 4 -8 4.91420 1.33077 13 8 4 -8 4.91757 1.27717 9 8 4 -8 6.37103 1.56721 8 7 -4 -8 10.0312 2.23293 12 7 -4 -8 8.71557 2.83551 7 7 -4 -8 11.2540 2.07517 8 7 -4 -8 10.8159 1.78889 13 7 -4 -8 8.71471 1.58754 15 7 4 -8 11.4124 1.21162 15 7 4 -8 9.28365 1.89757 8 -7 4 8 10.2112 4.32532 6 -7 4 8 12.4042 3.98841 5 7 4 -8 10.9925 1.80547 9 7 4 -8 10.0305 1.86813 13 6 -4 -8 4.04952 2.66851 7 6 -4 -8 6.59367 1.92558 8 6 -4 -8 6.42045 1.66723 13 6 -4 -8 5.84191 1.67857 15 6 -4 -8 4.03759 1.88560 12 6 4 -8 5.80962 1.20023 15 6 4 -8 4.08953 1.57187 8 6 4 -8 6.75333 1.82180 13 -6 4 8 5.72125 3.31133 5 -6 4 8 4.56455 4.10197 6 6 4 -8 5.52955 1.72502 9 -5 -4 8 227.291 13.4740 2 -5 -4 8 253.555 11.1837 7 5 -4 -8 251.383 8.48367 13 5 -4 -8 249.643 9.21201 8 5 -4 -8 248.217 9.27260 12 -5 4 8 253.600 15.4448 6 5 4 -8 257.866 9.25549 8 5 4 -8 242.586 8.44209 13 5 4 -8 243.503 8.79094 9 -5 4 8 263.811 12.8458 5 5 4 -8 247.127 7.93791 15 -4 -4 8 111.564 6.93309 7 -4 -4 8 118.602 8.64677 4 4 -4 -8 117.106 4.72463 14 -4 -4 8 121.420 9.82005 2 4 -4 -8 122.072 5.82014 8 -4 -4 8 94.9287 10.2751 3 4 -4 -8 107.197 7.70819 9 -4 4 8 120.358 7.83898 5 4 4 -8 120.310 5.62292 9 4 4 -8 112.475 5.49548 8 -4 4 8 118.354 10.0987 6 4 4 -8 114.499 4.98454 15 -4 4 8 98.6911 9.91719 3 4 4 -8 107.910 4.88729 13 3 -4 -8 106.917 5.38070 8 -3 -4 8 105.966 9.02017 2 -3 -4 8 95.9728 10.5528 3 -3 -4 8 119.730 7.76308 5 -3 -4 8 100.643 7.74317 4 -3 -4 8 113.923 6.62238 7 -3 4 8 103.754 6.89280 5 -3 4 8 105.437 8.71181 6 -3 4 8 110.367 9.91757 3 3 4 -8 109.811 5.04931 8 -2 -4 8 424.804 17.3124 4 -2 -4 8 427.732 20.7733 3 -2 -4 8 446.423 18.9746 2 -2 -4 8 458.916 16.2931 5 -2 -4 8 440.721 15.1377 7 -2 4 8 461.268 14.9566 5 -2 4 8 417.462 19.7205 3 -2 4 8 458.896 18.7795 6 2 4 -8 462.814 13.0511 8 -1 -4 8 182.902 9.03625 5 -1 -4 8 187.460 10.2319 4 1 -4 -8 183.418 8.09251 5 -1 -4 8 178.285 8.36093 7 -1 -4 8 168.209 11.6076 3 -1 -4 8 183.867 11.1204 2 1 4 -8 175.598 6.48172 8 -1 4 8 172.919 10.3720 6 -1 4 8 184.231 11.8883 3 0 -4 -8 284.420 15.1003 1 0 -4 8 296.498 11.6344 5 0 -4 8 286.255 11.3673 7 0 -4 8 295.885 14.1065 2 0 -4 -8 318.224 12.4269 5 0 4 -8 301.017 9.15618 8 0 4 8 287.749 13.6238 6 0 4 8 302.320 15.4083 3 -1 -4 -8 11.2966 3.26348 5 1 -4 8 11.9668 3.53296 2 1 -4 8 11.5105 2.50611 5 -1 -4 -8 9.50303 2.79768 1 -1 -4 -8 15.2257 4.13406 4 1 -4 8 10.2610 2.50441 7 1 4 8 10.8185 3.61805 2 1 4 8 9.99065 3.78089 3 1 4 8 6.48534 3.00401 6 2 -4 8 330.561 12.8481 7 -2 -4 -8 351.534 14.7136 5 2 -4 8 341.938 15.0517 2 -2 -4 -8 343.325 16.2439 4 -2 -4 -8 349.257 14.6938 1 2 4 8 337.604 16.8081 3 -2 4 -8 348.484 11.8685 5 2 4 8 349.977 16.8797 2 2 4 8 335.162 15.4800 6 -3 -4 -8 319.977 14.6774 5 3 -4 8 313.265 15.1732 1 3 -4 8 303.949 12.4410 7 -3 -4 -8 292.834 15.2302 4 -3 -4 -8 296.394 14.1574 1 3 -4 8 279.671 13.8392 2 3 4 8 288.493 15.8102 3 3 4 8 301.493 15.1436 6 -3 4 -8 319.487 12.2813 5 3 4 8 321.823 16.1675 2 4 -4 8 21.1077 3.61989 7 4 -4 8 22.2637 4.42076 2 4 -4 8 24.5835 5.01832 1 4 -4 8 22.2979 2.11201 14 -4 -4 -8 26.3874 5.49578 5 -4 -4 -8 19.7143 4.61166 1 4 -4 8 24.1233 3.01939 12 -4 4 -8 28.4867 3.13009 10 4 4 8 23.2324 5.58814 6 4 4 8 24.2384 5.43111 2 4 4 8 24.0965 3.18415 11 4 4 8 22.7223 2.53615 15 -4 4 -8 22.5384 4.09032 5 4 4 8 26.0055 6.39518 3 4 4 8 26.0091 3.17996 10 4 4 8 25.9954 3.23547 9 5 -4 8 558.177 16.5215 12 5 -4 8 581.960 22.3101 1 5 -4 8 604.680 20.2417 7 5 4 8 584.720 24.8099 6 5 4 8 569.952 15.6910 15 -5 4 -8 577.562 16.4592 10 -5 4 -8 569.408 20.3456 5 5 4 8 574.480 16.4913 10 5 4 8 576.415 23.4561 2 5 4 8 574.830 23.7425 1 5 4 8 574.992 17.6193 11 6 -4 8 425.203 13.0029 12 6 -4 8 417.559 18.1411 1 6 -4 8 432.316 13.9912 11 6 4 8 419.840 19.5185 1 6 4 8 439.760 14.5267 11 6 4 8 417.264 12.9270 10 -6 4 -8 449.423 12.9057 10 -6 4 -8 418.636 16.4238 5 6 4 8 446.326 12.1616 15 6 4 8 447.286 22.1993 6 7 -4 8 774.418 20.0368 15 7 -4 8 759.190 20.5577 11 7 -4 8 766.710 24.0032 7 7 -4 8 773.241 20.4130 12 7 4 8 780.654 19.3154 15 -7 4 -8 747.944 23.8973 5 7 4 8 769.375 20.4189 10 8 -4 8 313.087 9.64151 11 8 -4 8 300.328 11.9443 7 8 -4 8 312.132 9.03879 15 8 -4 8 308.752 9.47149 12 8 4 8 315.331 10.3900 11 8 4 8 314.737 9.55377 10 8 4 8 300.875 8.01297 15 9 -4 8 45.9983 2.55305 12 9 -4 8 41.9104 2.11406 15 9 -4 8 38.3481 2.49813 11 9 4 8 42.6439 2.52233 10 9 4 8 43.2902 2.89542 11 10 -4 8 160.893 4.59367 12 10 4 8 138.232 5.62966 11 9 -5 -8 197.699 5.91797 13 9 -5 -8 205.893 5.84444 15 9 -5 -8 205.234 6.08993 12 9 5 -8 198.499 5.75458 13 9 5 -8 199.989 5.95687 9 8 -5 -8 182.564 6.13789 15 8 -5 -8 190.246 6.44100 12 8 -5 -8 182.632 6.63561 8 8 -5 -8 193.492 6.13109 13 8 5 -8 187.456 6.02980 13 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5.37536 2 3 4 9 35.1493 6.41359 6 -3 4 -9 29.7097 3.26247 10 3 4 9 30.4928 3.26678 15 3 4 9 31.6037 3.55161 10 3 4 9 29.8321 3.28724 9 4 -4 9 293.816 14.9684 1 4 -4 9 301.492 15.0156 2 -4 -4 -9 330.104 15.6327 5 4 -4 9 314.940 10.5632 12 -4 -4 -9 324.286 15.9700 1 4 -4 9 346.966 13.6406 7 4 -4 9 320.281 9.51367 14 4 4 9 319.024 17.0434 6 -4 4 -9 323.040 10.7060 10 4 4 9 309.327 16.5412 2 -4 4 -9 328.648 13.1906 5 4 4 9 314.904 10.2272 15 4 4 9 318.329 10.6574 10 4 4 9 319.744 11.3435 11 4 4 9 296.696 10.3346 9 -5 -4 -9 40.7974 6.40817 5 -5 -4 -9 26.6807 5.51671 1 5 -4 9 35.1577 3.19880 12 5 -4 9 31.9102 5.61922 1 5 -4 9 29.5330 4.32644 7 5 4 9 33.2289 3.90370 11 5 4 9 25.3787 6.20823 6 -5 4 -9 35.3930 5.19652 5 5 4 9 35.0342 3.28414 10 5 4 9 36.1511 2.74850 15 -5 4 -9 28.8965 3.09194 10 6 -4 9 289.302 14.2223 1 6 -4 9 302.285 12.9661 7 -6 -4 -9 272.129 15.1592 1 6 4 9 295.790 9.05848 15 -6 4 -9 292.638 9.49229 10 6 4 9 280.403 17.8322 6 6 4 9 289.287 10.9930 11 -6 4 -9 295.656 12.6709 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58.7502 6 2 0 10 2181.92 59.6613 2 -2 0 -10 2204.24 55.8947 5 2 0 10 2098.33 53.7412 7 -3 0 -10 1244.99 36.1568 5 3 0 10 1278.38 39.7399 6 3 0 10 1222.27 38.7709 2 3 0 10 1239.48 33.7349 7 -3 0 -10 1264.61 38.6219 4 -4 0 -10 537.345 22.5982 4 4 0 10 579.074 24.5871 6 4 0 10 624.306 23.9898 1 4 0 10 559.394 22.8089 2 -4 0 -10 576.855 21.2088 5 5 0 10 985.333 26.8634 11 5 0 10 1011.01 34.1925 1 5 0 10 1009.02 26.3496 12 5 0 10 1000.13 26.2022 15 5 0 10 947.183 26.0912 10 5 0 10 1087.67 38.1835 6 5 0 10 969.501 33.7020 2 -5 0 -10 1025.29 31.4508 5 -6 0 -10 163.409 10.1615 5 6 0 10 172.170 7.46190 11 6 0 10 178.545 16.9802 2 6 0 10 184.139 13.8308 6 6 0 10 171.516 7.20817 12 6 0 10 176.095 11.7007 1 6 0 10 167.210 6.68081 15 6 0 10 178.502 7.00757 10 7 0 10 18.1744 2.09454 15 7 0 10 17.3305 2.55411 11 7 0 10 20.8977 4.92705 1 7 0 10 17.6752 2.54436 12 7 0 10 24.1375 5.86917 6 7 0 10 30.9651 2.83324 10 -7 0 -10 20.5249 4.33396 5 8 0 10 372.751 10.9799 10 8 0 10 387.120 11.6646 11 8 0 10 378.653 11.1595 12 8 0 10 373.147 10.3811 15 8 0 10 326.577 16.6332 6 9 0 10 61.0730 3.35201 11 9 0 10 47.8714 2.76952 10 9 0 10 53.8967 2.19792 15 9 0 10 49.9362 2.81099 12 10 0 10 5.18950 0.98601 11 10 -1 -10 1.08507 0.72688 12 10 -1 -10 1.67315 0.76952 13 10 1 -10 3.29000 0.80550 13 9 -1 -10 -0.1948 1.01342 8 9 -1 -10 1.37892 1.52486 7 9 -1 -10 0.17045 0.87178 13 9 -1 -10 1.09018 0.54157 15 9 -1 -10 0.35467 0.89189 12 9 1 -10 0.73812 0.89794 13 9 1 -10 1.12997 1.01045 12 9 1 -10 1.93951 1.11555 8 9 1 -10 0.09993 0.95188 9 8 -1 -10 43.2020 3.09293 12 8 -1 -10 42.1791 2.88864 13 8 -1 -10 39.9526 4.50244 7 8 -1 -10 40.3130 2.37139 15 8 -1 -10 39.5768 3.17694 8 8 1 -10 37.7818 3.12040 8 8 1 -10 43.7693 4.43032 7 8 1 -10 47.2235 3.06115 9 8 1 -10 44.1342 2.85762 13 8 1 -10 41.6739 2.13144 15 8 1 -10 40.5158 2.91426 12 7 -1 -10 0.14894 1.81348 7 7 -1 -10 6.34731 1.82026 8 7 -1 -10 1.95285 1.49164 9 7 -1 -10 4.92556 1.24658 15 7 -1 -10 4.84672 1.46497 13 7 -1 -10 1.79696 1.34686 12 7 1 -10 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20.4051 6 6 2 -10 419.042 12.0809 15 5 -2 -10 685.337 19.6104 9 5 -2 -10 666.113 18.3546 13 5 -2 -10 698.820 22.7865 7 5 -2 -10 669.824 18.9363 15 -5 -2 10 693.939 22.8055 7 5 -2 -10 660.049 19.1214 12 5 -2 -10 691.917 19.2861 8 5 2 -10 680.594 19.3654 8 -5 2 10 682.512 23.3804 5 5 2 -10 678.945 19.2372 9 5 2 -10 687.960 18.5214 13 5 2 -10 712.969 20.2642 12 5 2 -10 660.106 18.1805 15 -5 2 10 688.316 26.3211 6 -4 -2 10 591.273 22.8931 4 4 -2 -10 649.796 18.1449 8 -4 -2 10 688.875 21.4424 7 4 -2 -10 655.500 20.8973 7 4 -2 -10 630.554 17.7599 12 -4 -2 10 656.000 21.7463 5 -4 -2 10 605.008 28.7912 3 4 -2 -10 631.545 18.2155 9 -4 2 10 597.204 23.3067 4 4 2 -10 585.150 18.0212 9 4 2 -10 659.540 17.9760 8 4 2 -10 618.943 17.0392 13 -4 2 10 605.981 27.5629 3 -4 2 10 624.841 24.1616 6 4 2 -10 618.214 17.4157 15 -4 2 10 649.428 21.6542 5 -3 -2 10 391.821 18.6798 2 3 -2 -10 378.138 13.7075 7 -3 -2 10 377.650 14.2374 7 -3 -2 10 351.173 15.9240 4 -3 -2 10 354.940 14.3924 5 -3 -2 10 351.562 19.9792 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7 2 -2 10 476.446 19.8334 2 2 2 10 476.649 19.7155 3 -2 2 -10 483.541 16.6275 5 2 2 10 509.945 21.6785 2 2 2 10 487.916 19.8966 6 3 -2 10 392.345 14.4747 7 -3 -2 -10 388.203 17.9891 4 -3 -2 -10 394.981 16.5112 5 3 -2 10 384.103 17.3409 2 3 2 10 393.742 16.5622 1 3 2 10 377.434 18.4458 2 3 2 10 389.229 18.0325 6 -3 2 -10 394.222 15.3943 5 4 -2 10 146.816 10.1968 2 4 -2 10 146.882 6.38369 12 4 -2 10 146.307 12.0682 6 4 -2 10 169.958 12.8421 1 4 -2 10 157.003 6.70861 10 -4 -2 -10 155.446 10.2687 5 4 -2 10 156.864 5.15428 14 4 -2 10 151.892 8.47530 7 -4 2 -10 153.315 9.58698 5 4 2 10 159.841 6.85258 10 4 2 10 154.818 11.7762 6 4 2 10 142.214 6.42273 15 4 2 10 137.253 7.20023 11 4 2 10 167.545 11.2336 1 4 2 10 145.850 10.9989 2 5 -2 10 81.3719 6.44688 7 -5 -2 -10 75.4327 7.54581 5 5 -2 10 85.5248 8.07676 2 5 -2 10 82.6723 4.67465 12 5 -2 10 80.4544 4.72452 10 5 -2 10 86.2891 8.06415 1 5 -2 10 88.7345 9.31007 6 5 2 10 82.1485 11.0677 6 5 2 10 101.843 9.63888 1 5 2 10 88.7351 4.53425 15 5 2 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7 6 -3 -10 24.8333 2.61609 15 6 -3 -10 27.1735 3.15617 8 6 -3 -10 23.6488 3.12980 12 6 -3 -10 20.5755 2.86994 9 6 -3 -10 24.6653 2.64067 13 -6 -3 10 31.3868 4.94681 7 -6 3 10 24.4975 5.04070 5 6 3 -10 28.6836 2.83045 13 6 3 -10 27.7758 3.18160 8 6 3 -10 30.4664 3.13736 9 -6 3 10 22.3232 5.73132 6 6 3 -10 28.4029 2.17981 15 5 -3 -10 33.5037 4.89949 7 5 -3 -10 47.9349 3.77421 12 5 -3 -10 38.8506 3.65442 9 -5 -3 10 44.5107 5.02168 7 5 -3 -10 46.5622 3.65391 8 -5 3 10 43.2463 6.14796 5 -5 3 10 36.9981 7.01753 6 5 3 -10 42.4871 3.53938 9 5 3 -10 38.3696 3.08387 13 5 3 -10 50.0292 3.07961 15 5 3 -10 41.6665 3.58582 8 4 -3 -10 250.886 9.55475 9 -4 -3 10 281.878 13.0766 5 4 -3 -10 282.843 9.89609 8 -4 -3 10 290.411 12.3124 7 4 -3 -10 268.512 7.76317 14 4 -3 -10 283.658 9.74981 12 4 3 -10 288.446 9.80555 8 -4 3 10 292.591 15.8007 6 -4 3 10 293.437 12.9796 5 4 3 -10 268.135 9.61739 9 4 3 -10 273.651 9.26402 15 4 3 -10 274.597 8.99842 13 3 -3 -10 265.784 9.37669 9 -3 -3 10 250.496 13.4187 4 -3 -3 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5 3 10 1802.55 55.4907 6 5 3 10 1787.31 44.0272 10 -5 3 -10 1815.48 44.1224 10 5 3 10 1786.68 43.6430 15 5 3 10 1743.00 45.5264 11 5 3 10 1803.95 53.6938 1 -6 -3 -10 2790.45 72.9116 5 6 -3 10 2932.15 67.5382 12 6 -3 10 2700.42 73.7341 1 6 -3 10 2824.85 66.8417 15 6 -3 10 2955.08 71.7832 7 6 3 10 2748.59 76.2141 1 -6 3 -10 2847.09 66.9117 10 6 3 10 2817.35 67.0422 10 -6 3 -10 2730.79 71.4506 5 6 3 10 2873.93 66.5007 15 6 3 10 2847.54 68.5610 11 6 3 10 2841.36 80.5904 6 7 -3 10 1187.32 29.7497 11 7 -3 10 1175.53 33.2550 7 7 -3 10 1184.95 29.7723 12 7 -3 10 1185.54 29.2393 15 -7 3 -10 1145.66 33.1955 5 7 3 10 1195.59 28.9175 15 7 3 10 1217.64 29.7214 10 7 3 10 1167.43 39.5489 6 7 3 10 1150.77 30.6000 11 -7 3 -10 1186.59 29.3891 10 8 -3 10 645.427 16.8890 11 8 -3 10 644.151 16.3783 15 8 -3 10 624.481 20.5955 7 8 -3 10 647.285 16.9530 12 8 3 10 639.523 17.6414 11 8 3 10 643.583 16.8659 10 -8 3 -10 641.908 16.4615 10 8 3 10 635.026 15.7855 15 9 -3 10 602.453 14.6507 15 9 -3 10 594.432 15.1832 12 9 -3 10 597.041 15.1063 11 9 3 10 588.906 15.1420 10 9 3 10 600.420 15.6812 11 9 -4 -10 129.705 3.96522 15 9 -4 -10 127.188 4.13778 13 9 -4 -10 127.815 4.35251 12 9 4 -10 126.357 4.16154 9 9 4 -10 135.322 4.20123 13 8 -4 -10 212.023 6.60849 15 8 -4 -10 205.199 6.49573 13 8 -4 -10 211.052 7.08519 8 8 -4 -10 219.571 7.12981 12 8 4 -10 206.686 6.69279 9 8 4 -10 208.106 6.54716 13 8 4 -10 209.780 7.03288 8 7 -4 -10 193.411 6.87621 15 7 -4 -10 193.269 7.23202 8 7 -4 -10 195.142 7.39600 12 7 -4 -10 207.815 6.67709 13 7 4 -10 193.886 6.65674 13 7 4 -10 196.787 7.26752 8 7 4 -10 188.190 5.72128 15 7 4 -10 197.167 6.88441 9 6 -4 -10 889.683 23.1420 13 -6 -4 10 956.603 28.4203 7 6 -4 -10 917.131 24.0804 15 6 -4 -10 892.556 24.5804 12 6 -4 -10 933.305 24.2453 8 -6 4 10 927.054 33.8423 6 6 4 -10 882.383 24.0801 8 6 4 -10 898.837 22.5922 15 6 4 -10 909.227 23.6842 9 6 4 -10 906.483 23.4094 13 -5 -4 10 334.075 13.6232 7 5 -4 -10 335.394 11.1131 9 5 -4 -10 333.764 11.2526 12 5 -4 -10 326.719 11.0183 8 5 4 -10 334.738 10.0332 15 5 4 -10 324.595 10.9670 8 5 4 -10 326.574 10.6634 9 -5 4 10 336.459 18.1748 6 5 4 -10 331.733 10.3500 13 -5 4 10 305.104 14.3535 5 -4 -4 10 98.9751 6.86536 7 4 -4 -10 96.5088 5.18862 12 -4 -4 10 97.4902 7.95062 5 4 -4 -10 102.968 5.35980 9 -4 -4 10 91.9625 9.48356 2 4 4 -10 94.3757 4.97141 9 4 4 -10 94.5581 4.69553 15 -4 4 10 99.6322 9.82461 6 4 4 -10 101.159 5.16274 8 -4 4 10 94.2254 7.37800 5 4 4 -10 106.042 4.76965 13 3 -4 -10 255.118 9.28882 9 3 -4 -10 271.092 9.26356 14 -3 -4 10 246.047 15.0736 2 -3 -4 10 266.625 12.5838 5 -3 -4 10 283.827 11.9603 7 3 4 -10 255.344 8.57265 13 -3 4 10 279.689 15.5455 6 3 4 -10 274.336 9.52613 9 3 4 -10 268.969 9.21735 8 3 4 -10 270.187 9.36693 15 2 -4 -10 114.037 5.59860 9 2 -4 -10 111.993 6.07221 14 -2 -4 10 117.823 7.91649 5 -2 -4 10 115.134 9.82417 2 -2 -4 10 118.922 7.31893 7 2 4 -10 114.874 4.96128 13 2 4 -10 123.897 5.90949 9 -2 4 10 125.072 7.17246 14 2 4 -10 114.026 5.26494 8 -2 4 10 123.288 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2064.47 58.4519 6 2 4 -11 2096.55 48.9315 8 -2 4 11 2020.59 50.1355 14 2 4 -11 2016.77 48.5997 10 -1 -4 11 2140.24 53.8007 7 -1 -4 11 1992.73 53.1156 5 1 -4 -11 2062.18 50.1364 9 1 -4 -11 1999.32 51.6240 14 -1 -4 11 1940.65 58.0296 2 1 4 -11 2043.95 49.3818 10 -1 4 11 2039.73 50.0591 14 1 4 -11 2107.84 48.7503 13 1 4 -11 2084.05 47.9895 14 -1 4 11 2069.42 58.6162 6 0 -4 11 982.417 28.1670 5 0 -4 11 964.151 33.5529 2 0 -4 -11 982.767 26.2477 9 0 -4 11 1042.79 29.6787 7 0 4 -11 990.599 25.6077 14 0 4 -11 983.440 25.6970 10 0 4 11 979.186 33.3960 6 0 4 11 996.266 25.6416 14 1 -4 11 1408.09 44.3579 2 -1 -4 -11 1481.01 37.0238 9 1 -4 11 1569.28 38.5600 14 1 -4 11 1514.66 40.4889 7 -1 -4 -11 1480.69 40.5201 5 -1 4 -11 1410.94 37.1939 14 1 4 11 1428.98 35.3481 14 1 4 11 1444.91 37.2022 11 1 4 11 1466.05 45.0477 6 -1 4 -11 1438.57 36.5230 10 2 -4 11 1308.70 35.7003 7 -2 -4 -11 1291.19 36.9873 5 -2 -4 -11 1230.19 32.0410 9 2 -4 11 1222.05 31.5217 12 2 -4 11 1191.67 38.8528 2 2 -4 11 1213.76 32.4133 14 -2 4 -11 1249.90 33.1616 14 2 4 11 1274.61 40.6119 6 2 4 11 1221.88 32.4891 11 -2 4 -11 1243.36 31.7763 10 3 -4 11 858.172 22.5134 14 -3 -4 -11 848.842 23.2747 9 3 -4 11 846.480 22.9415 12 3 -4 11 898.651 26.8259 7 -3 -4 -11 852.590 28.5579 5 3 4 11 856.205 31.6373 6 3 4 11 821.265 23.8782 11 -3 4 -11 849.334 23.0023 10 -3 4 -11 862.465 24.7077 14 4 -4 11 766.164 20.7038 12 4 -4 11 777.718 24.2624 7 4 -4 11 748.209 18.6949 14 -4 -4 -11 743.580 26.2991 5 4 4 11 741.813 20.5606 15 4 4 11 746.402 21.8008 11 4 4 11 755.349 20.7898 10 4 4 11 748.334 29.5752 6 -4 4 -11 757.174 20.7392 10 5 -4 11 1837.65 44.3034 12 5 -4 11 1761.27 48.0443 7 -5 -4 -11 1788.74 49.9352 5 5 4 11 1843.37 44.2846 10 5 4 11 1825.56 45.7760 11 -5 4 -11 1834.85 44.1615 10 5 4 11 1738.62 55.3632 6 5 4 11 1821.88 43.9223 15 6 -4 11 1970.13 47.4778 12 6 -4 11 1935.22 51.3420 7 6 4 11 1978.22 47.5033 10 -6 4 -11 2017.40 47.3696 10 6 4 11 2041.85 47.1727 15 6 4 11 1922.48 48.6991 11 7 -4 11 689.564 18.0150 12 7 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11.0540 10 -2 8 11 409.384 11.7819 11 2 8 -11 382.809 11.0116 15 1 -8 -11 573.208 15.1110 9 1 -8 -11 553.123 14.9780 14 -1 -8 11 574.126 14.4907 13 -1 -8 11 578.566 15.7722 14 1 8 -11 565.223 14.8644 10 -1 8 11 563.429 15.6370 11 0 -8 11 563.100 14.1232 13 0 -8 -11 548.913 14.9696 9 0 -8 -11 550.549 15.6591 14 0 -8 11 556.482 15.0682 14 0 8 -11 543.465 14.5735 10 0 8 11 556.186 15.4472 11 1 -8 11 510.785 13.1894 13 1 -8 11 528.369 13.8072 14 -1 -8 -11 499.449 14.2047 9 -1 -8 -11 529.431 15.6602 14 1 8 11 518.710 14.5687 11 -1 8 -11 535.965 13.9005 10 2 -8 11 621.288 15.1490 13 2 -8 11 611.215 14.8748 14 -2 -8 -11 622.917 17.3903 14 -2 -8 -11 600.133 16.3942 9 -2 8 -11 621.972 15.8532 10 2 8 11 619.874 16.6461 11 -3 -8 -11 551.903 14.4986 9 3 8 11 569.586 14.9331 11 -3 8 -11 573.138 13.9249 10 3 8 11 506.275 14.0830 15 9 0 -12 61.8977 2.74179 12 9 0 -12 61.3393 2.62890 13 -8 0 12 35.1877 5.33076 7 8 0 -12 37.2707 2.56043 9 8 0 -12 38.6979 2.59845 12 8 0 -12 37.6043 2.81234 8 8 0 -12 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23.7506 9 2 7 13 919.986 23.6726 11 -2 7 -13 958.028 23.1067 10 -3 -7 -13 380.277 10.2490 9 -3 7 -13 377.617 10.0691 10 3 7 13 369.245 10.5980 11 8 0 -14 494.449 12.3871 13 8 0 -14 458.205 11.7674 9 -8 0 14 452.467 11.8881 12 8 0 -14 466.472 11.2667 15 7 0 -14 757.549 18.6089 15 7 0 -14 745.983 18.5050 13 -7 0 14 750.079 19.2020 12 7 0 -14 757.852 19.1222 9 -6 0 14 766.009 24.5614 7 6 0 -14 839.454 21.4805 9 6 0 -14 829.292 20.9266 15 -6 0 14 845.486 21.6576 12 5 0 -14 2032.13 49.0383 9 -5 0 14 1977.84 52.7436 7 5 0 -14 2026.13 48.5027 15 4 0 -14 1663.18 41.3445 9 -4 0 14 1603.61 44.3118 5 -4 0 14 1696.91 40.8988 12 -4 0 14 1617.68 44.6496 7 -3 0 14 1715.86 46.2535 5 -3 0 14 1712.21 46.9605 7 -3 0 14 1862.07 43.5497 12 3 0 -14 1728.80 44.2298 9 -2 0 14 1652.10 44.6891 7 2 0 -14 1652.48 38.9570 14 -2 0 14 1672.66 40.9434 12 2 0 -14 1615.42 41.9643 9 1 0 -14 400.347 13.6757 9 -1 0 14 412.332 12.6871 12 1 0 -14 401.495 12.6441 14 -1 0 14 414.195 15.4335 7 -1 0 14 398.955 13.4988 14 0 0 14 2089.03 49.4038 12 0 0 14 2009.43 52.7600 7 0 0 14 1997.76 49.8539 14 0 0 -14 2001.84 50.4575 14 1 0 14 2186.36 53.1320 12 -1 0 -14 2132.33 55.1718 14 1 0 14 2227.60 56.5714 7 1 0 14 2251.33 53.1274 14 -2 0 -14 1254.01 31.1068 10 2 0 14 1256.47 41.7765 6 -2 0 -14 1208.16 33.8476 14 2 0 14 1216.58 31.3025 12 2 0 14 1217.04 30.2036 14 3 0 14 1651.35 52.5119 6 3 0 14 1642.72 40.6828 12 4 0 14 670.631 18.2097 10 4 0 14 651.348 28.2456 6 -4 0 -14 616.660 20.5509 5 4 0 14 656.297 18.1798 12 5 0 14 215.497 7.80371 10 5 0 14 220.858 7.89800 12 6 0 14 361.181 10.8788 12 6 0 14 366.812 10.7576 15 7 0 14 868.460 21.5543 15 7 0 14 874.138 21.7174 12 -7 0 -14 903.654 21.8649 10 -8 0 -14 811.173 19.9242 10 8 0 14 856.893 19.5656 15 8 -1 -14 53.8261 2.00205 15 8 1 -14 53.2814 2.15883 13 -8 1 14 55.2402 2.46765 12 8 1 -14 50.3927 2.30665 9 8 1 -14 51.9506 1.66732 15 -7 -1 14 8.48885 1.38858 12 7 -1 -14 6.79209 1.11848 15 7 -1 -14 6.23070 1.27954 9 7 1 -14 5.62647 1.17786 9 7 1 -14 8.19293 1.25309 13 7 1 -14 7.97588 1.06973 15 -7 1 14 6.97385 1.37500 12 6 -1 -14 17.5445 1.99964 15 -6 -1 14 11.4263 2.78430 7 -6 -1 14 12.7356 1.91109 12 6 -1 -14 15.7894 2.21395 9 6 1 -14 19.5976 1.96575 15 6 1 -14 15.5181 1.85100 13 -6 1 14 11.7824 3.06482 7 6 1 -14 20.7033 2.31530 9 5 -1 -14 8.37918 1.76122 15 -5 -1 14 12.2849 3.02654 7 5 -1 -14 7.70469 1.96506 9 -5 -1 14 9.68778 2.02478 12 5 1 -14 9.72891 1.93682 9 5 1 -14 8.58914 1.70557 15 -5 1 14 11.2684 3.10220 7 4 -1 -14 21.0386 3.10700 9 -4 -1 14 15.5561 3.28770 7 -4 -1 14 20.6987 3.99565 5 -4 -1 14 18.2211 2.66266 12 -4 1 14 15.9142 2.36177 12 4 1 -14 17.0337 2.54985 9 -4 1 14 14.6670 3.65008 5 -4 1 14 15.0331 3.39856 7 4 1 -14 18.0432 2.95566 15 -3 -1 14 0.99680 2.48336 5 -3 -1 14 1.61686 1.32026 12 -3 -1 14 1.23826 1.86343 7 3 -1 -14 1.21053 1.74112 9 -3 1 14 2.38023 2.02159 7 -3 1 14 0.85207 1.22229 12 -3 1 14 2.10759 2.54693 5 3 1 -14 1.95176 1.66590 9 2 -1 -14 54.3055 3.21800 14 -2 -1 14 56.8523 5.44263 7 -2 -1 14 59.2956 5.69766 5 -2 -1 14 55.4584 3.84836 12 2 -1 -14 56.4336 4.52799 9 -2 1 14 55.1282 3.85624 12 -2 1 14 57.3764 5.55983 7 2 1 -14 55.9580 4.31952 9 -1 -1 14 5.66737 2.53018 7 1 -1 -14 7.06798 1.83700 14 -1 -1 14 5.39340 1.72733 12 -1 -1 14 9.16811 2.32398 14 1 -1 -14 9.24035 2.53253 9 -1 1 14 14.0945 2.68735 14 1 1 -14 8.92697 2.52171 9 -1 1 14 7.17805 1.73414 12 -1 1 14 8.68188 4.50414 6 1 1 -14 9.00765 1.65479 14 0 -1 14 7.07322 2.62040 7 0 -1 -14 6.19398 2.30237 9 0 -1 -14 6.14423 2.10667 14 0 -1 14 5.19254 1.86188 14 0 -1 14 4.87458 1.73090 12 0 1 -14 6.31570 1.73847 14 0 1 14 8.17282 1.88421 12 0 1 14 10.7087 4.94599 6 0 1 14 7.04547 1.81000 14 1 -1 14 33.2657 3.49915 12 1 -1 14 29.2036 4.34393 7 -1 -1 -14 29.0493 4.14840 14 1 -1 14 32.9876 2.99589 14 1 1 14 39.0560 7.43613 6 1 1 14 22.2682 2.70787 12 1 1 14 26.3561 2.61885 14 -1 1 -14 29.8691 3.72164 14 2 -1 14 259.108 11.3877 7 2 -1 14 248.468 8.35715 14 2 -1 14 258.671 9.05803 12 -2 -1 -14 268.238 12.0930 14 2 1 14 239.695 15.4345 6 2 1 14 255.955 8.93132 12 2 1 14 250.948 7.65092 14 -2 1 -14 251.395 8.81272 10 -2 1 -14 238.837 10.3781 14 3 -1 14 75.2683 4.30960 12 3 -1 14 66.0483 5.85062 7 -3 1 -14 72.1161 5.43025 14 3 1 14 69.3151 4.12274 12 3 1 14 75.2477 4.38701 10 3 1 14 66.4836 9.80352 6 -3 1 -14 71.2485 4.27006 10 -4 -1 -14 20.9633 4.13833 5 4 -1 14 12.7608 2.19150 12 4 1 14 11.4189 5.37185 6 -4 1 -14 8.37430 1.83014 10 4 1 14 11.9678 2.05591 12 4 1 14 18.3537 2.50165 10 5 -1 14 107.569 5.09428 12 -5 1 -14 101.993 4.86758 10 5 1 14 109.684 5.02493 10 5 1 14 104.446 4.95449 12 5 1 14 98.1040 5.01201 15 6 -1 14 143.866 5.50685 15 6 -1 14 143.161 5.72406 12 6 1 14 143.812 5.54596 12 6 1 14 156.338 5.63563 10 -6 1 -14 143.827 5.51615 10 6 1 14 145.198 5.53396 15 7 -1 14 95.9278 3.87702 12 7 -1 14 97.7749 3.65975 15 7 1 14 96.8569 3.64826 15 -7 1 -14 95.5541 3.80824 10 7 1 14 97.1228 3.85824 10 8 -1 14 86.7480 2.92651 15 -8 -1 -14 94.5573 3.20225 10 8 1 14 90.1570 2.69388 15 8 -2 -14 202.192 5.30609 15 8 2 -14 194.698 5.55174 9 -8 2 14 197.126 5.77094 12 7 -2 -14 157.659 5.15542 15 7 -2 -14 153.931 5.25479 9 7 2 -14 164.276 4.75773 15 7 2 -14 160.492 5.02073 13 7 2 -14 156.263 5.29674 9 -7 2 14 157.297 5.57113 12 6 -2 -14 332.337 10.0987 9 6 -2 -14 336.540 9.84046 15 -6 -2 14 324.878 9.52985 12 6 2 -14 322.818 9.25170 15 6 2 -14 310.422 9.69440 8 6 2 -14 333.369 9.33575 13 6 2 -14 327.564 9.75795 9 5 -2 -14 333.028 11.0620 9 -5 -2 14 349.118 10.4993 12 -5 -2 14 329.924 13.3791 7 5 2 -14 332.246 10.1051 15 5 2 -14 332.176 9.78483 13 5 2 -14 339.910 10.4970 9 -4 -2 14 189.630 9.86358 7 -4 -2 14 202.510 7.42941 12 4 -2 -14 214.125 8.29969 9 -4 -2 14 168.121 9.70790 5 4 2 -14 200.767 7.44121 15 -4 2 14 185.100 7.55898 12 4 2 -14 198.478 7.42712 9 -3 -2 14 449.250 16.9213 7 -3 -2 14 464.257 13.7758 12 -3 -2 14 440.220 16.6702 5 3 -2 -14 463.483 14.6208 9 -3 2 14 452.271 20.3508 6 3 2 -14 469.149 13.9303 9 -3 2 14 464.092 13.9382 12 2 -2 -14 630.255 19.4585 9 -2 -2 14 694.352 18.8218 12 -2 -2 14 655.977 22.0895 7 2 -2 -14 692.981 18.1431 14 -2 2 14 677.355 18.8085 12 -2 2 14 667.140 25.9856 6 2 2 -14 684.605 19.0472 9 -2 2 14 671.116 19.6377 14 -1 -2 14 767.695 24.1929 7 -1 -2 14 779.988 20.7231 12 1 -2 -14 737.304 21.4900 9 1 -2 -14 743.506 21.3713 14 -1 2 14 758.715 28.3732 6 -1 2 14 746.479 20.5400 12 1 2 -14 760.031 19.1065 14 -1 2 14 743.679 21.0757 14 0 -2 14 337.727 10.9476 12 0 -2 -14 344.362 11.8041 9 0 -2 -14 354.058 12.6357 14 0 -2 14 333.512 13.7389 7 0 -2 14 327.384 11.4874 14 0 2 14 331.114 10.8619 14 0 2 14 334.120 17.5036 6 0 2 -14 323.866 10.7221 14 0 2 14 337.259 10.8807 12 1 -2 14 251.988 9.03320 14 -1 -2 -14 260.079 10.9875 14 1 -2 14 272.035 9.13774 12 1 -2 14 235.191 11.1900 7 -1 -2 -14 250.529 9.67929 9 1 2 14 251.381 15.1933 6 -1 2 -14 236.717 9.33861 14 -1 2 -14 239.560 8.54291 10 1 2 14 257.532 8.25570 14 1 2 14 243.503 8.69727 12 2 -2 14 607.680 17.0928 12 2 -2 14 599.918 20.1258 7 2 -2 14 609.797 17.0137 14 -2 2 -14 607.477 18.3989 14 2 2 14 584.749 16.7794 12 2 2 14 595.243 25.1581 6 -2 2 -14 590.361 16.7681 10 3 -2 14 24.4092 2.92571 12 3 -2 14 27.8183 4.39249 7 -3 -2 -14 29.1336 4.66529 5 -3 2 -14 19.2417 2.43120 10 -3 2 -14 19.2490 2.92228 14 3 2 14 26.7738 6.37303 6 3 2 14 23.6526 2.81270 12 4 -2 14 143.281 8.10995 7 4 -2 14 146.438 6.21402 12 4 2 14 135.737 5.94937 12 4 2 14 137.414 6.06842 10 -4 2 -14 143.092 6.88347 14 4 2 14 160.217 12.7549 6 -4 2 -14 150.383 6.14662 10 5 -2 14 715.901 22.6718 7 5 -2 14 786.135 20.4505 12 5 2 14 746.688 20.2360 15 5 2 14 802.059 20.1700 10 -5 2 -14 744.159 19.9994 10 6 -2 14 144.747 5.59436 12 6 2 14 147.896 5.41316 15 -6 2 -14 153.086 5.45195 10 6 2 14 144.957 5.45167 10 6 2 14 140.167 6.87850 11 7 -2 14 68.8398 2.86950 15 7 -2 14 74.1601 3.14336 12 7 2 14 73.7330 3.10076 10 -7 2 -14 72.4412 3.03999 10 7 2 14 69.9166 2.83388 15 7 2 14 67.9560 3.03092 11 7 -3 -14 94.1309 3.85068 9 7 -3 -14 98.9220 3.57831 15 7 3 -14 98.6861 2.99476 15 7 3 -14 96.5199 3.39826 13 7 3 -14 100.903 3.61197 9 -7 3 14 93.9050 3.74006 12 6 -3 -14 109.896 4.57239 9 6 -3 -14 105.084 4.35138 15 6 3 -14 110.294 3.87423 15 6 3 -14 103.730 3.97963 13 6 3 -14 107.697 4.20432 9 -6 3 14 91.4808 4.49873 12 -5 -3 14 10.8854 2.68681 7 5 -3 -14 6.63510 1.79079 9 5 3 -14 8.11853 1.41788 15 5 3 -14 6.98249 1.49204 9 5 3 -14 11.6215 1.63921 13 -5 3 14 7.77745 1.87917 12 -4 -3 14 7.32063 2.66379 7 4 -3 -14 3.85143 1.75940 9 4 3 -14 3.97259 1.38603 15 -4 3 14 4.51021 1.56945 12 4 3 -14 4.29281 1.36941 13 4 3 -14 6.51545 1.59338 9 -3 -3 14 20.9786 2.60829 12 -3 -3 14 16.8045 3.72398 5 -3 -3 14 22.2145 3.85013 7 3 -3 -14 18.4210 2.88824 9 -3 3 14 20.5001 5.64054 6 -3 3 14 22.5917 2.81874 12 3 3 -14 21.3199 2.56038 9 -3 3 14 21.5638 3.08713 14 -2 -3 14 1.43299 1.42175 12 -2 -3 14 2.07080 2.33121 5 2 -3 -14 2.24741 1.74310 9 2 -3 -14 1.09889 1.09119 14 -2 -3 14 1.24361 1.85892 7 -2 3 14 3.31224 1.53724 14 -2 3 14 6.73742 1.77207 12 -2 3 14 5.86329 3.92184 6 -1 -3 14 60.0354 3.85580 12 -1 -3 14 56.5436 5.43754 7 1 -3 -14 59.8718 4.29067 14 1 -3 -14 61.0660 4.43424 9 -1 3 14 53.4435 3.75508 14 -1 3 14 56.6219 3.76874 12 -1 3 14 52.2638 7.73392 6 0 -3 14 303.603 10.0441 12 0 -3 14 310.806 10.8043 14 0 -3 -14 305.407 10.8577 9 0 -3 14 315.216 13.0044 7 0 3 -14 299.419 9.17149 14 0 3 -14 302.236 9.69028 10 0 3 14 300.637 9.69421 14 0 3 14 286.999 16.2104 6 0 3 14 294.405 9.88582 12 1 -3 14 95.5482 5.46530 14 1 -3 14 110.617 5.30350 12 -1 -3 -14 111.294 6.95917 14 1 -3 14 114.106 7.37693 7 -1 -3 -14 109.523 5.86155 9 1 3 14 100.673 10.0060 6 -1 3 -14 108.601 5.26079 14 -1 3 -14 108.512 5.06700 10 1 3 14 114.508 4.24888 14 2 -3 14 209.777 10.0907 7 -2 -3 -14 205.902 8.09551 9 2 -3 14 205.516 7.69777 12 2 -3 14 195.103 7.42512 14 -2 3 -14 208.292 8.22644 14 2 3 14 195.891 13.5638 6 -2 3 -14 209.664 7.62052 10 3 -3 14 220.533 10.2942 7 3 -3 14 202.702 7.77794 12 -3 3 -14 205.237 7.65178 10 3 3 14 210.600 14.1058 6 -3 3 -14 214.938 8.51064 14 4 -3 14 172.432 8.88386 7 4 -3 14 186.564 7.01432 12 4 3 14 189.556 6.93516 10 -4 3 -14 177.688 6.89388 10 -4 3 -14 190.724 7.60899 14 5 -3 14 517.381 14.2073 12 -5 3 -14 509.267 14.0012 10 5 3 14 523.089 13.9983 10 5 3 14 495.647 14.1010 15 5 3 14 493.610 14.1915 11 -5 3 -14 484.579 14.6439 14 6 -3 14 457.141 12.2446 12 6 3 14 441.883 12.2559 11 -6 3 -14 440.785 12.0877 10 6 3 14 453.315 12.1110 15 6 3 14 461.928 12.1697 10 -6 3 -14 436.107 12.6866 14 7 -3 14 535.419 13.2933 12 7 3 14 531.323 12.9203 15 -7 3 -14 512.865 13.1157 10 7 3 14 527.328 13.2236 10 7 4 -14 263.011 7.18297 9 6 -4 -14 134.338 4.74832 9 6 4 -14 144.665 4.66831 9 -6 4 14 133.806 4.92074 12 -6 4 14 133.180 5.37860 14 6 4 -14 137.827 4.25986 15 6 4 -14 145.989 4.55461 13 5 -4 -14 23.2891 2.43005 9 5 4 -14 16.3137 1.77946 9 -5 4 14 25.6475 2.63932 14 5 4 -14 23.6523 2.08277 13 -5 4 14 24.0628 2.54345 12 4 -4 -14 100.204 5.03784 9 -4 -4 14 93.8358 6.71305 7 4 4 -14 101.849 4.13776 13 4 4 -14 104.288 4.44467 9 -4 4 14 107.772 5.37129 14 -4 4 14 96.2330 4.73667 12 4 4 -14 103.741 4.47233 15 -3 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10 -4 5 -15 118.259 4.07623 10 2 -6 -15 31.2078 2.29703 9 1 -6 -15 6.32166 1.39466 9 0 -6 -15 31.4025 2.52665 9 0 -6 -15 30.6122 1.90133 14 0 6 -15 27.9039 1.81850 10 1 -6 15 13.0401 0.86702 14 -1 -6 -15 12.7762 1.71091 14 -1 -6 -15 13.1493 1.68852 9 -1 6 -15 13.3230 1.44815 10 -2 -6 -15 8.52150 1.48971 14 -2 6 -15 9.08227 1.16238 10 6 0 -16 208.468 6.14167 15 -6 0 16 218.416 6.46896 12 6 0 -16 210.744 6.35286 9 -5 0 16 475.246 12.9484 12 5 0 -16 464.936 12.6779 9 5 0 -16 456.833 12.5495 15 4 0 -16 64.2535 3.64471 9 -4 0 16 61.0230 3.61517 12 -3 0 16 60.5859 7.32244 7 -3 0 16 61.1350 3.71004 12 -3 0 16 64.4996 4.27730 14 3 0 -16 63.1068 3.88342 9 -2 0 16 9.77476 2.15234 14 -2 0 16 9.39064 1.84140 12 2 0 -16 11.2784 2.10927 9 -2 0 16 10.0662 2.90893 7 -1 0 16 16.6299 2.25802 12 -1 0 16 21.1742 2.68436 14 1 0 -16 20.2051 2.72810 9 0 0 16 8.86046 1.70892 14 0 0 -16 8.67997 1.58799 14 0 0 16 8.80210 1.76217 12 1 0 16 126.107 4.76761 14 -1 0 -16 125.220 5.74173 14 1 0 16 123.624 5.50409 12 -2 0 -16 166.412 7.16374 14 2 0 16 170.302 6.47991 12 3 0 16 117.157 5.02687 12 -3 0 -16 109.282 4.63280 10 -3 0 -16 115.856 5.63263 14 -4 0 -16 147.007 6.13753 14 4 0 16 134.972 5.48245 12 -4 0 -16 151.776 5.41967 10 -5 0 -16 274.890 8.79456 14 5 0 16 277.574 8.25477 12 -5 0 -16 271.298 8.00138 10 -6 0 -16 37.7942 1.92413 10 -6 -1 16 344.964 9.38363 12 6 -1 -16 367.277 9.64332 9 6 -1 -16 355.841 9.47723 15 -6 1 16 360.061 9.75944 12 6 1 -16 352.560 9.28540 15 6 1 -16 358.858 9.50879 9 5 -1 -16 212.903 6.88916 9 5 -1 -16 208.379 6.90363 15 -5 -1 16 207.519 6.72544 12 5 1 -16 206.383 6.54169 15 5 1 -16 208.305 6.65485 9 -5 1 16 208.700 7.00270 12 4 -1 -16 75.1830 4.00861 9 -4 -1 16 67.4306 3.69192 12 -4 1 16 69.6338 4.34725 14 -4 1 16 67.8749 3.78024 12 4 1 -16 74.2136 3.68025 9 -3 -1 16 136.233 7.63356 7 -3 -1 16 141.566 5.76832 12 3 -1 -16 143.484 6.08643 9 -3 1 16 139.971 5.86385 12 -3 1 16 138.706 6.31462 14 3 1 -16 137.268 5.57081 9 -2 -1 16 385.930 12.2750 14 -2 -1 16 381.918 11.4814 12 2 -1 -16 379.895 12.0217 9 -2 -1 16 341.522 13.7711 7 -2 1 16 364.289 11.8868 14 2 1 -16 360.712 11.2279 9 -2 1 16 382.545 11.5341 12 -1 -1 16 387.273 14.8670 7 1 -1 -16 407.242 10.9421 14 -1 -1 16 430.550 12.9960 14 -1 -1 16 426.826 12.5637 12 1 -1 -16 418.453 13.1271 9 -1 1 16 411.815 12.6025 14 -1 1 16 415.699 12.5161 12 0 -1 16 426.333 15.7299 7 0 -1 -16 440.282 13.2437 14 0 -1 16 474.552 13.5411 12 0 -1 16 471.827 13.5080 14 0 -1 -16 457.109 14.3726 9 0 1 16 464.016 12.9863 14 0 1 16 444.407 13.3294 12 0 1 -16 460.824 12.3509 14 1 -1 16 386.409 11.6704 12 -1 -1 -16 379.599 12.2281 14 1 -1 16 360.790 13.7818 7 -1 1 -16 369.787 11.4102 14 1 1 16 384.519 10.1143 14 1 1 16 386.518 11.5630 12 -2 -1 -16 107.527 5.71310 14 2 -1 16 106.992 4.96510 12 2 1 16 109.733 4.84195 12 -2 1 -16 100.434 5.13457 14 3 -1 16 235.831 8.04926 12 -3 -1 -16 234.542 8.80282 14 -3 1 -16 239.429 7.63831 10 3 1 16 233.014 7.86906 12 -3 1 -16 228.656 8.40429 14 -4 -1 -16 188.303 7.16796 14 -4 -1 -16 172.077 6.04906 10 4 -1 16 183.935 6.47825 12 4 1 16 176.851 6.24861 12 -4 1 -16 177.397 6.73251 14 -4 1 -16 182.738 6.20704 10 5 -1 16 63.1843 3.17617 12 -5 -1 -16 59.5129 2.89233 10 -5 -1 -16 75.1904 4.70076 14 -5 1 -16 60.2122 3.28799 14 -5 1 -16 61.4273 2.94748 10 5 1 16 57.6121 2.89113 12 6 -1 16 163.129 5.01878 12 -6 1 -16 168.810 5.00295 10 6 -2 -16 146.952 4.60280 9 6 2 -16 144.182 4.26964 15 -6 2 16 141.425 4.70116 12 6 2 -16 150.581 4.53441 9 -5 -2 16 24.9127 1.83328 12 5 -2 -16 26.1508 2.14810 9 -5 2 16 23.0016 2.19327 14 5 2 -16 28.0986 1.90240 9 5 2 -16 22.9301 1.74424 15 -5 2 16 24.0028 2.10548 12 4 -2 -16 43.9137 3.15938 9 -4 -2 16 47.1836 2.86609 12 -4 2 16 46.2553 3.42165 14 4 2 -16 48.5815 2.76843 9 -4 2 16 46.4297 3.05950 12 4 2 -16 47.5518 2.93350 15 -3 -2 16 116.791 4.89642 12 3 -2 -16 111.941 5.40898 9 -3 2 16 113.506 5.35242 14 -3 2 16 115.316 5.11780 12 3 2 -16 115.321 4.73604 9 2 -2 -16 3.27039 1.67904 9 -2 -2 16 2.53601 1.23445 12 -2 -2 16 2.96205 1.50692 14 -2 -2 16 0.35269 1.70306 7 -2 2 16 2.98084 1.39357 12 -2 2 16 2.52604 1.33722 14 1 -2 -16 9.73740 2.18457 9 -1 -2 16 8.10196 2.49753 7 1 -2 -16 7.79578 1.29803 14 -1 -2 16 9.56510 1.90410 14 -1 -2 16 8.09270 1.77358 12 -1 2 16 6.81600 1.58459 14 -1 2 16 6.50835 1.58351 12 0 -2 16 8.48790 1.83134 12 0 -2 16 10.1656 1.84855 14 0 -2 -16 7.90242 1.64599 14 0 -2 -16 9.50918 2.26189 9 0 -2 16 8.71378 2.50656 7 0 2 16 7.66584 1.64425 12 0 2 16 11.4677 1.61942 14 -1 -2 -16 5.05687 1.63297 14 1 -2 16 2.63805 1.32529 14 1 -2 16 5.72870 1.48462 12 1 -2 16 6.50065 2.34028 7 -1 2 -16 6.62668 1.32844 14 1 2 16 4.37593 1.46521 12 2 -2 16 188.987 6.86560 12 -2 -2 -16 186.976 7.82398 14 -2 2 -16 189.362 6.42774 10 2 2 16 182.022 6.62083 12 -2 2 -16 179.623 6.70656 14 3 -2 16 186.543 6.84321 12 -3 -2 -16 200.400 7.77546 14 -3 2 -16 186.865 6.47169 10 3 2 16 191.028 6.64220 12 -3 2 -16 195.099 7.04991 14 4 -2 16 8.61567 1.55259 12 -4 -2 -16 9.57025 1.84746 14 -4 2 -16 10.0967 1.56292 10 -4 2 -16 6.42771 1.36808 14 5 -2 16 8.48778 1.34133 12 -5 -2 -16 10.1037 1.72818 10 -5 2 -16 7.35001 1.25156 14 5 2 16 8.02124 1.29705 15 -5 2 -16 7.18180 1.16860 10 5 -3 -16 456.255 11.7440 9 -5 3 16 430.421 11.7196 12 5 3 -16 444.997 11.2344 9 -5 3 16 429.483 11.9898 14 4 -3 -16 749.618 18.8849 9 -4 3 16 692.495 18.5847 12 4 3 -16 721.507 18.2057 15 4 3 -16 716.769 17.9223 9 -4 3 16 737.518 19.1668 14 3 -3 -16 1169.97 29.1274 9 -3 3 16 1175.25 28.9878 14 -3 3 16 1113.83 28.4916 12 2 -3 -16 1319.69 33.8043 9 -2 -3 16 1340.24 32.8818 12 -2 -3 16 1412.85 34.3634 14 -2 3 16 1352.99 33.1880 12 -2 3 16 1336.09 33.1794 14 1 -3 -16 1609.80 37.4937 14 1 -3 -16 1607.52 39.5924 9 -1 -3 16 1590.70 38.5955 12 -1 3 16 1548.97 38.5998 12 -1 3 16 1634.87 38.2310 14 0 -3 -16 1087.71 27.5385 9 0 -3 16 910.836 27.0204 14 0 -3 16 1105.13 26.6665 12 0 -3 -16 1118.02 27.0551 14 0 3 16 1086.54 26.5757 12 1 -3 16 1092.04 27.5422 12 -1 -3 -16 1114.07 28.0501 9 -1 -3 -16 1117.51 28.7045 14 -1 3 -16 1092.50 26.9948 10 -2 -3 -16 854.841 22.9135 14 2 -3 16 871.316 21.6248 12 -2 3 -16 815.615 21.0144 10 -2 3 -16 808.488 20.6158 14 3 -3 16 486.859 13.2913 12 -3 -3 -16 480.615 14.2591 14 -3 3 -16 487.450 13.0342 14 -3 3 -16 478.057 12.9799 10 -4 -3 -16 691.390 18.4588 14 4 -3 16 715.890 17.6660 12 -4 3 -16 688.672 17.4621 10 -4 3 -16 673.771 17.4812 14 5 -3 16 823.485 19.7190 12 -5 3 -16 805.202 19.7282 14 -5 3 -16 809.292 19.6614 10 4 -4 -16 6.35132 1.16990 9 -4 4 16 6.34030 1.25308 14 4 4 -16 6.56611 0.96506 15 3 -4 -16 136.771 5.31611 9 -3 4 16 136.723 4.90943 14 2 -4 -16 24.9110 2.60758 9 -2 -4 16 13.7178 2.25418 14 -2 4 16 22.7291 1.75835 14 1 -4 -16 22.4244 2.53735 9 -1 -4 16 14.3147 2.11490 14 0 -4 16 3.85300 1.22850 14 0 -4 -16 7.74735 1.76654 9 0 -4 -16 5.61454 1.29513 14 -1 -4 -16 6.58280 1.58354 14 -1 -4 -16 7.05870 1.64211 9 -1 4 -16 7.14894 1.28603 10 -2 -4 -16 5.51043 1.52595 14 2 -4 16 6.53848 1.38463 12 -2 4 -16 6.25426 1.19585 10 3 -4 16 61.6069 2.84947 12 -3 -4 -16 59.7008 3.46129 14 -3 4 -16 59.2712 2.83868 10 -4 4 -16 5.23389 0.91803 10 -4 4 -16 7.23076 1.03966 14 3 -5 -16 438.258 11.9091 9 -2 -5 16 257.273 8.62835 14 2 -5 -16 345.886 9.05600 9 1 -5 -16 112.020 4.47790 9 -1 -5 16 91.8913 3.94444 14 0 -5 -16 133.408 3.93616 14 0 -5 -16 140.070 5.29307 9 -1 -5 -16 329.363 9.41856 9 -1 -5 -16 327.994 9.28911 14 -1 5 -16 320.854 8.72856 10 -2 -5 -16 428.719 11.9064 14 -2 5 -16 436.150 11.1651 10 5 0 -17 -0.1881 0.61241 9 -5 0 17 -0.3793 0.58547 12 4 0 -17 1.95150 0.87024 9 -4 0 17 1.36425 1.02674 14 -4 0 17 1.21423 0.92193 12 3 0 -17 1.23807 0.95098 9 -3 0 17 1.03055 1.11277 14 -3 0 17 -0.1204 0.83966 12 -2 0 17 1.86902 1.09978 12 2 0 -17 2.50439 1.17845 9 -2 0 17 0.10022 1.02799 14 -1 0 17 0.17439 0.90047 14 -1 0 17 2.86188 1.21297 12 0 0 17 4.50262 1.11652 14 0 0 17 1.65750 1.17564 12 1 0 17 1.08580 1.02225 12 -1 0 -17 2.34148 0.98514 14 2 0 17 3.30982 1.19586 12 -2 0 -17 2.44847 1.10449 14 -3 0 -17 1.48559 0.96448 14 3 0 17 0.78566 0.98116 12 -4 0 -17 0.84791 0.82635 14 4 0 17 0.02642 0.81188 12 5 -1 -17 311.677 8.29904 9 -5 1 17 294.271 8.38083 12 5 1 -17 305.453 8.10851 9 4 -1 -17 102.786 4.03382 9 -4 -1 17 95.9591 4.33806 14 -4 -1 17 102.596 4.00835 12 -4 1 17 101.541 4.15846 12 4 1 -17 99.2769 3.77205 9 -4 1 17 94.9262 4.32887 14 -3 -1 17 239.274 8.17002 14 3 -1 -17 239.746 7.69103 9 -3 -1 17 252.941 7.72992 12 3 1 -17 233.920 7.28064 9 -3 1 17 228.438 7.94761 14 -3 1 17 244.927 7.78317 12 -2 -1 17 203.709 6.93698 12 -2 -1 17 203.356 7.25325 14 2 -1 -17 194.625 6.95607 9 2 1 -17 207.437 8.81752 9 -2 1 17 209.254 7.03774 12 -2 1 17 191.721 6.94142 14 -1 -1 17 111.794 4.91092 12 1 -1 -17 115.674 5.05448 9 -1 -1 17 121.957 5.04765 14 -1 1 17 121.811 4.73652 14 -1 1 17 120.818 5.04623 12 0 -1 -17 340.001 8.98658 14 0 -1 17 342.453 10.3521 12 0 1 17 340.556 10.2804 12 -1 -1 -17 315.134 9.45712 14 1 -1 17 324.254 9.74219 12 -1 1 -17 312.323 8.59874 14 1 1 17 318.439 9.64151 12 -2 -1 -17 719.514 19.1300 14 2 -1 17 726.738 18.8684 12 -2 1 -17 717.387 18.4541 14 2 1 17 731.604 18.7535 12 3 -1 17 374.591 10.6418 12 -3 -1 -17 367.412 10.8973 14 3 1 17 360.112 10.3828 12 -3 1 -17 379.125 10.6096 14 -4 -1 -17 345.373 9.82317 14 4 -1 17 339.611 9.58228 12 -4 1 -17 343.704 9.12820 10 4 1 17 336.540 9.28745 12 -4 1 -17 331.677 9.51527 14 4 -2 -17 549.462 13.8693 9 -4 2 17 528.646 14.1389 14 -4 2 17 525.533 13.9210 12 4 2 -17 517.493 13.2350 9 -3 -2 17 428.021 11.6818 12 3 -2 -17 448.790 12.1174 9 -3 -2 17 433.598 12.4960 14 3 2 -17 433.302 11.7828 9 -3 2 17 431.672 12.1236 14 -3 2 17 417.836 11.9557 12 2 -2 -17 456.443 13.0406 9 -2 -2 17 471.138 12.7428 12 -2 -2 17 480.602 13.3639 14 -2 2 17 449.899 12.7844 12 -2 2 17 461.200 12.7114 14 -1 -2 17 328.842 9.85900 12 1 -2 -17 345.678 10.3415 9 -1 2 17 329.931 9.18785 14 -1 2 17 327.713 9.87486 12 0 -2 17 350.981 10.4050 12 0 -2 -17 362.281 9.38597 14 0 -2 -17 364.595 10.7411 9 0 2 17 344.653 10.3470 12 1 -2 17 489.739 13.3266 12 -1 -2 -17 486.078 13.1910 14 1 2 17 462.083 12.9586 12 2 -2 17 207.948 6.76953 12 -2 -2 -17 197.761 6.94910 14 2 2 17 188.485 6.31302 12 -2 2 -17 187.222 5.55997 14 -3 -2 -17 240.477 7.67553 14 3 -2 17 238.126 7.32042 12 -3 2 -17 231.712 6.79950 10 -3 2 -17 227.970 6.78392 14 4 -2 17 275.963 7.79898 12 -4 -2 -17 265.270 8.02090 14 -4 2 -17 274.449 7.46847 14 4 -3 -17 1.60918 0.78425 9 -4 3 17 1.43991 0.79539 14 -3 -3 17 0.55675 1.08909 14 3 -3 -17 2.20422 0.98770 9 -3 3 17 2.47365 0.99239 12 -3 3 17 0.92939 0.81880 14 -2 -3 17 3.73971 1.39619 14 2 -3 -17 2.77286 1.13061 9 -2 3 17 6.02305 1.02547 14 -2 3 17 5.98833 1.20578 12 -1 -3 17 2.74015 1.18680 14 1 -3 -17 1.60919 1.14856 9 -1 -3 17 4.85905 1.20635 12 -1 3 17 0.86574 1.05622 12 0 -3 17 3.95416 1.02935 14 0 -3 17 9.31821 1.45743 12 0 -3 -17 7.10821 1.57401 9 1 -3 17 13.6794 1.74235 12 -1 -3 -17 12.0825 1.54899 14 2 -3 17 5.00952 1.14819 12 -2 -3 -17 5.31937 1.28605 14 -2 3 -17 5.53148 1.07384 10 3 -3 17 12.3209 1.44053 12 -3 -3 -17 11.5572 1.51268 14 2 -4 -17 575.702 14.8879 9 1 -4 -17 293.457 8.63820 9 0 -4 -17 302.552 9.36976 9 -1 -4 -17 304.233 7.84668 14 -2 -4 -17 276.974 7.76042 14 -3 0 18 829.943 20.4395 12 -3 0 18 832.033 20.5105 14 -2 0 18 495.206 12.6722 14 -2 0 18 473.775 12.8409 12 -1 0 18 561.029 14.7513 12 0 0 18 806.829 20.2671 12 1 0 18 2016.30 47.3847 12 2 0 18 1330.67 31.8028 12 -3 0 -18 272.552 7.28025 14 -3 -1 18 4.50108 0.96118 14 -3 -1 18 7.26197 1.33081 12 -3 1 18 6.63294 1.09978 12 -3 1 18 8.86876 1.18104 14 -2 -1 18 16.2612 1.60879 14 -2 -1 18 15.5896 1.65710 12 2 -1 -18 15.0706 1.92690 9 -2 1 18 13.5064 1.32633 14 -2 1 18 15.7256 1.70269 12 -1 -1 18 4.60685 1.07441 14 -1 -1 18 8.53484 1.35964 12 -1 1 18 7.33706 1.32151 12 0 -1 18 138.678 4.95347 12 0 1 18 133.337 4.82292 12 1 -1 18 0.90076 0.84085 12 1 1 18 1.12119 0.77765 12 2 -1 18 10.0235 1.39134 12 -2 -1 -18 9.76735 1.05573 14 2 1 18 9.48806 1.30439 12 -3 -1 -18 20.1291 1.95697 14 3 -1 18 17.8789 2.23052 12 -2 -2 18 71.1588 3.22606 14 -1 -2 18 449.549 11.5114 12 -1 2 18 420.496 11.4027 12 0 -2 18 405.498 11.0833 12 0 2 18 428.386 12.5566 12 1 -2 18 157.802 5.19691 12 2 -2 18 179.378 5.94195 12 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_max 0.4338 _exptl_absorpt_correction_T_min 0.1208 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54183 10.048 8.714 15.080 90.000 91.095 90.002 ) ; _shelx_hkl_checksum 81429 _shelx_SHELXL_version_number '2014/7' _olex2_submission_special_instructions 'No special instructions were received' _vrf_PLAT911_stahl226 ; PROBLEM: Missing # FCF Refl Between THmin & STh/L= 0.600 73 Report RESPONSE: We believe that there is a good reason to use statistical analysis and if some reflections are outliers they harm rather than improve the refinement. The statistical analysis was conducted with program G4_fcf_filter published on my web site http://xray.chem.wisc.edu/Resources.html. It uses the approach described by Prince, E., Nicholson, W.L. (1983) Acta Cryst A39, 407-410. For the suggested value for the outlier cutoff see Rollett J.S. (1988) Crystallographic Computing 4, 149-166, Oxford University Press. ;