data_007b-17101 _vrf_PLAT411_007b-17101 ; PROBLEM: Short Inter H...H Contact RESPONSE: The short H...H contacts in this structure arise from the disordered THF. The hydrogen positions associated with THF were generated geometrically and may not represent their true locations. ; _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C20 H23 Cl N3 Rh, 0.5(C4 H8 O)' _chemical_formula_sum 'C22 H27 Cl N3 O0.50 Rh' _chemical_formula_weight 479.82 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Rh' 'Rh' 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 2/c' _space_group_name_Hall '-C 2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 29.4841(9) _cell_length_b 9.3563(2) _cell_length_c 14.9795(5) _cell_angle_alpha 90 _cell_angle_beta 91.787(3) _cell_angle_gamma 90 _cell_volume 4130.3(2) _cell_formula_units_Z 8 _cell_measurement_temperature 93(2) _cell_measurement_reflns_used 21170 _cell_measurement_theta_min 4.9470 _cell_measurement_theta_max 66.5730 _exptl_crystal_description Plate _exptl_crystal_colour Red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.543 _exptl_crystal_F_000 1968 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.100 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.010 _exptl_absorpt_coefficient_mu 7.981 _shelx_estimated_absorpt_T_min 0.502 _shelx_estimated_absorpt_T_max 0.924 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.54567 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.16b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _diffrn_ambient_temperature 93(2) _diffrn_radiation_wavelength 1.54184 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_detector_area_resol_mean 22.2 _diffrn_reflns_number 8567 _diffrn_reflns_av_unetI/netI 0.0204 _diffrn_reflns_av_R_equivalents 0.0951 _diffrn_reflns_limit_h_min -35 _diffrn_reflns_limit_h_max 35 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_theta_min 2.999 _diffrn_reflns_theta_max 67.115 _diffrn_reflns_theta_full 67.115 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measured_fraction_theta_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_point_group_measured_fraction_full 0.993 _reflns_number_total 8567 _reflns_number_gt 7343 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_cell_refinement 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ; Dolomanov, O.V.; Bourhis, L.J.; Gildea, R.J.; Howard, J.A.K.; Puschmann, H., OLEX2: A complete structure solution, refinement and analysis program (2009). J. Appl. Cryst., 42, 339-341. ; _computing_publication_material 'CIFTAB-2014/2 (Sheldrick, 2014)' _refine_special_details ; Refined as a 2-component twin. The fractional volume contributions of the second twin component is 0.4728(16). Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The hydrogen atoms were first found in the difference map, then generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) for CH, NH and CH2 groups and Uiso(H) = 1.5 times Ueq(C) for CH3 groups. The only exception were the THF hydrogens, which were not found in the difference map, but generated geometrically and refined as riding atoms with C-H distances = 0.95 - 0.99 angstroms and Uiso(H) = 1.2 times Ueq(C) CH2 groups. The THF molecule is disordered across crystallographic glide plane. The special position constraints were suppressed and the THF model extends past the asymmetric unit with all atoms at half occupancy. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1100P)^2^+13.2571P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary SHELXT _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 8567 _refine_ls_number_parameters 277 _refine_ls_number_restraints 34 _refine_ls_R_factor_all 0.0672 _refine_ls_R_factor_gt 0.0583 _refine_ls_wR_factor_ref 0.1636 _refine_ls_wR_factor_gt 0.1572 _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_restrained_S_all 1.062 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh1 Rh 0.63381(2) 0.70182(5) 0.60596(3) 0.0273(2) Uani 1 1 d . . . . . Cl1 Cl 0.65440(6) 0.77451(15) 0.45941(10) 0.0318(4) Uani 1 1 d . . . . . N1 N 0.56691(18) 0.7639(5) 0.5820(4) 0.0281(11) Uani 1 1 d . . . . . N2 N 0.49852(18) 0.6906(5) 0.5411(4) 0.0331(12) Uani 1 1 d . . . . . H2 H 0.4762 0.6348 0.5219 0.040 Uiso 1 1 calc R U . . . N3 N 0.56161(18) 0.5237(5) 0.5319(4) 0.0314(12) Uani 1 1 d . . . . . C1 C 0.6054(2) 0.5248(6) 0.5499(4) 0.0281(13) Uani 1 1 d . . . . . C2 C 0.5421(2) 0.6542(6) 0.5516(4) 0.0300(14) Uani 1 1 d . . . . . C3 C 0.4950(2) 0.8313(7) 0.5659(5) 0.0332(14) Uani 1 1 d . . . . . H3 H 0.4680 0.8870 0.5656 0.040 Uiso 1 1 calc R U . . . C4 C 0.5371(2) 0.8754(7) 0.5908(5) 0.0325(14) Uani 1 1 d . . . . . H4 H 0.5449 0.9687 0.6111 0.039 Uiso 1 1 calc R U . . . C5 C 0.6305(2) 0.3955(6) 0.5265(4) 0.0273(13) Uani 1 1 d . . . . . C6 C 0.6126(2) 0.2598(7) 0.5438(4) 0.0295(13) Uani 1 1 d . . . . . H6 H 0.5850 0.2513 0.5744 0.035 Uiso 1 1 calc R U . . . C7 C 0.6350(2) 0.1385(7) 0.5167(4) 0.0325(14) Uani 1 1 d . . . . . H7 H 0.6230 0.0468 0.5295 0.039 Uiso 1 1 calc R U . . . C8 C 0.6750(2) 0.1503(7) 0.4705(5) 0.0350(15) Uani 1 1 d . . . . . H8 H 0.6899 0.0669 0.4502 0.042 Uiso 1 1 calc R U . . . C9 C 0.6933(2) 0.2847(7) 0.4542(5) 0.0328(14) Uani 1 1 d . . . . . H9 H 0.7208 0.2930 0.4231 0.039 Uiso 1 1 calc R U . . . C10 C 0.6714(2) 0.4061(7) 0.4831(4) 0.0311(14) Uani 1 1 d . . . . . H10 H 0.6844 0.4975 0.4733 0.037 Uiso 1 1 calc R U . . . C11 C 0.6925(2) 0.8117(7) 0.6794(4) 0.0334(15) Uani 1 1 d . . . . . C12 C 0.6529(2) 0.8399(7) 0.7263(4) 0.0325(14) Uani 1 1 d . . . . . C13 C 0.6332(2) 0.7029(7) 0.7479(4) 0.0333(14) Uani 1 1 d . . . . . C14 C 0.6628(2) 0.5921(7) 0.7221(4) 0.0328(14) Uani 1 1 d . . . . . C15 C 0.6982(2) 0.6580(7) 0.6742(4) 0.0303(14) Uani 1 1 d . . . . . C16 C 0.7242(2) 0.9180(8) 0.6398(5) 0.0415(17) Uani 1 1 d . . . . . H16A H 0.7307 0.8895 0.5785 0.062 Uiso 1 1 calc R U . . . H16B H 0.7525 0.9211 0.6757 0.062 Uiso 1 1 calc R U . . . H16C H 0.7101 1.0128 0.6392 0.062 Uiso 1 1 calc R U . . . C17 C 0.6335(3) 0.9831(8) 0.7481(5) 0.0434(17) Uani 1 1 d . . . . . H17A H 0.6457 1.0554 0.7081 0.065 Uiso 1 1 calc R U . . . H17B H 0.6416 1.0077 0.8101 0.065 Uiso 1 1 calc R U . . . H17C H 0.6004 0.9798 0.7403 0.065 Uiso 1 1 calc R U . . . C18 C 0.5905(3) 0.6850(8) 0.8003(5) 0.0409(17) Uani 1 1 d . . . . . H18A H 0.5680 0.7562 0.7804 0.061 Uiso 1 1 calc R U . . . H18B H 0.5977 0.6984 0.8640 0.061 Uiso 1 1 calc R U . . . H18C H 0.5782 0.5889 0.7903 0.061 Uiso 1 1 calc R U . . . C19 C 0.6574(2) 0.4364(7) 0.7420(5) 0.0374(15) Uani 1 1 d . . . . . H19A H 0.6254 0.4097 0.7349 0.056 Uiso 1 1 calc R U . . . H19B H 0.6681 0.4171 0.8034 0.056 Uiso 1 1 calc R U . . . H19C H 0.6754 0.3803 0.7006 0.056 Uiso 1 1 calc R U . . . C20 C 0.7391(2) 0.5868(8) 0.6381(5) 0.0379(16) Uani 1 1 d . . . . . H20A H 0.7328 0.4850 0.6289 0.057 Uiso 1 1 calc R U . . . H20B H 0.7648 0.5979 0.6806 0.057 Uiso 1 1 calc R U . . . H20C H 0.7465 0.6309 0.5810 0.057 Uiso 1 1 calc R U . . . C21 C 0.5284(7) 0.158(2) 0.7151(17) 0.077(6) Uani 0.5 1 d D U P A -1 H21A H 0.5483 0.1919 0.6675 0.093 Uiso 0.5 1 calc R U P A -1 H21B H 0.5371 0.0588 0.7307 0.093 Uiso 0.5 1 calc R U P A -1 O1 O 0.4836(7) 0.162(3) 0.6853(17) 0.121(7) Uani 0.5 1 d D U P A -1 C22 C 0.5339(11) 0.250(3) 0.794(2) 0.096(12) Uani 0.5 1 d D U P A -1 H22A H 0.5647 0.2919 0.7983 0.115 Uiso 0.5 1 calc R U P A -1 H22B H 0.5281 0.1966 0.8495 0.115 Uiso 0.5 1 calc R U P A -1 C23 C 0.4991(8) 0.362(2) 0.7774(13) 0.075(6) Uani 0.5 1 d D U P A -1 H23A H 0.4832 0.3850 0.8327 0.090 Uiso 0.5 1 calc R U P A -1 H23B H 0.5129 0.4500 0.7539 0.090 Uiso 0.5 1 calc R U P A -1 C24 C 0.4683(15) 0.298(4) 0.711(3) 0.15(2) Uani 0.5 1 d D U P A -1 H24A H 0.4378 0.2886 0.7365 0.175 Uiso 0.5 1 calc R U P A -1 H24B H 0.4657 0.3606 0.6583 0.175 Uiso 0.5 1 calc R U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1 0.0219(3) 0.0300(3) 0.0301(3) -0.00102(18) 0.00153(18) -0.00019(18) Cl1 0.0340(9) 0.0300(7) 0.0318(8) 0.0006(6) 0.0053(6) -0.0023(6) N1 0.022(3) 0.025(2) 0.038(3) 0.001(2) 0.003(2) -0.001(2) N2 0.019(3) 0.032(3) 0.048(3) -0.001(2) 0.001(2) -0.004(2) N3 0.024(3) 0.030(3) 0.040(3) 0.000(2) 0.001(2) 0.001(2) C1 0.027(3) 0.031(3) 0.027(3) 0.003(2) 0.003(2) -0.002(3) C2 0.025(3) 0.024(3) 0.041(4) 0.002(3) 0.005(3) -0.002(2) C3 0.029(4) 0.027(3) 0.043(4) 0.001(3) 0.001(3) 0.003(3) C4 0.022(3) 0.030(3) 0.046(4) 0.001(3) 0.003(3) 0.002(3) C5 0.025(3) 0.029(3) 0.028(3) 0.000(2) -0.002(2) -0.001(2) C6 0.024(3) 0.033(3) 0.032(3) 0.002(3) 0.001(3) 0.001(3) C7 0.030(3) 0.030(3) 0.037(3) 0.002(3) -0.001(3) -0.002(3) C8 0.035(4) 0.029(3) 0.041(4) -0.004(3) -0.001(3) 0.008(3) C9 0.027(3) 0.034(3) 0.038(4) -0.001(3) 0.004(3) 0.004(3) C10 0.025(3) 0.029(3) 0.039(4) 0.002(3) 0.001(3) 0.001(3) C11 0.025(3) 0.044(4) 0.031(3) -0.004(3) -0.007(3) -0.003(3) C12 0.033(4) 0.039(3) 0.025(3) -0.008(3) -0.005(3) -0.002(3) C13 0.026(3) 0.044(4) 0.030(3) 0.000(3) 0.001(3) -0.002(3) C14 0.026(3) 0.044(4) 0.028(3) 0.003(3) -0.001(3) 0.000(3) C15 0.025(3) 0.039(3) 0.027(3) 0.000(3) -0.004(3) 0.000(3) C16 0.034(4) 0.043(4) 0.048(4) 0.002(3) -0.004(3) -0.011(3) C17 0.048(5) 0.044(4) 0.037(4) -0.010(3) -0.004(3) 0.006(3) C18 0.032(4) 0.059(5) 0.031(4) -0.002(3) 0.006(3) 0.003(3) C19 0.039(4) 0.037(4) 0.035(4) 0.006(3) -0.001(3) -0.004(3) C20 0.026(3) 0.050(4) 0.038(4) 0.000(3) 0.003(3) 0.005(3) C21 0.064(10) 0.061(10) 0.107(15) -0.049(11) 0.006(9) 0.021(8) O1 0.084(11) 0.117(13) 0.163(18) -0.047(12) 0.010(10) 0.012(9) C22 0.095(16) 0.078(15) 0.113(17) -0.053(15) -0.002(15) 0.035(16) C23 0.084(13) 0.054(8) 0.088(16) -0.017(8) 0.024(13) 0.018(10) C24 0.12(2) 0.13(2) 0.18(3) -0.07(2) -0.04(2) 0.054(17) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1 C1 2.027(6) . ? Rh1 N1 2.077(5) . ? Rh1 C13 2.126(7) . ? Rh1 C15 2.168(6) . ? Rh1 C14 2.172(6) . ? Rh1 C11 2.268(6) . ? Rh1 C12 2.274(6) . ? Rh1 Cl1 2.3945(16) . ? N1 C2 1.331(8) . ? N1 C4 1.373(8) . ? N2 C2 1.335(8) . ? N2 C3 1.373(8) . ? N2 H2 0.8800 . ? N3 C1 1.310(8) . ? N3 C2 1.385(8) . ? C1 C5 1.467(9) . ? C3 C4 1.352(9) . ? C3 H3 0.9500 . ? C4 H4 0.9500 . ? C5 C10 1.391(9) . ? C5 C6 1.402(9) . ? C6 C7 1.380(9) . ? C6 H6 0.9500 . ? C7 C8 1.391(10) . ? C7 H7 0.9500 . ? C8 C9 1.393(10) . ? C8 H8 0.9500 . ? C9 C10 1.383(9) . ? C9 H9 0.9500 . ? C10 H10 0.9500 . ? C11 C12 1.406(10) . ? C11 C15 1.450(9) . ? C11 C16 1.500(10) . ? C12 C13 1.449(10) . ? C12 C17 1.497(10) . ? C13 C14 1.416(10) . ? C13 C18 1.513(10) . ? C14 C15 1.427(9) . ? C14 C19 1.496(9) . ? C15 C20 1.493(9) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 O1 1.38(2) . ? C21 C22 1.47(2) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? O1 C24 1.40(3) . ? C22 C23 1.48(2) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C23 C24 1.45(2) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Rh1 N1 77.2(2) . . ? C1 Rh1 C13 113.7(2) . . ? N1 Rh1 C13 97.7(2) . . ? C1 Rh1 C15 112.7(3) . . ? N1 Rh1 C15 161.4(2) . . ? C13 Rh1 C15 64.2(3) . . ? C1 Rh1 C14 95.3(2) . . ? N1 Rh1 C14 128.2(2) . . ? C13 Rh1 C14 38.5(3) . . ? C15 Rh1 C14 38.4(2) . . ? C1 Rh1 C11 150.6(3) . . ? N1 Rh1 C11 131.6(2) . . ? C13 Rh1 C11 62.8(3) . . ? C15 Rh1 C11 38.1(2) . . ? C14 Rh1 C11 63.3(2) . . ? C1 Rh1 C12 151.9(2) . . ? N1 Rh1 C12 100.9(2) . . ? C13 Rh1 C12 38.3(3) . . ? C15 Rh1 C12 62.7(2) . . ? C14 Rh1 C12 63.4(3) . . ? C11 Rh1 C12 36.1(3) . . ? C1 Rh1 Cl1 88.01(17) . . ? N1 Rh1 Cl1 91.65(16) . . ? C13 Rh1 Cl1 157.75(19) . . ? C15 Rh1 Cl1 104.04(18) . . ? C14 Rh1 Cl1 139.83(18) . . ? C11 Rh1 Cl1 96.00(18) . . ? C12 Rh1 Cl1 120.10(18) . . ? C2 N1 C4 105.8(5) . . ? C2 N1 Rh1 110.6(4) . . ? C4 N1 Rh1 143.4(4) . . ? C2 N2 C3 107.1(5) . . ? C2 N2 H2 126.4 . . ? C3 N2 H2 126.4 . . ? C1 N3 C2 111.2(5) . . ? N3 C1 C5 116.5(5) . . ? N3 C1 Rh1 118.9(4) . . ? C5 C1 Rh1 124.6(4) . . ? N1 C2 N2 111.1(5) . . ? N1 C2 N3 121.7(6) . . ? N2 C2 N3 127.1(6) . . ? C4 C3 N2 106.8(6) . . ? C4 C3 H3 126.6 . . ? N2 C3 H3 126.6 . . ? C3 C4 N1 109.1(6) . . ? C3 C4 H4 125.5 . . ? N1 C4 H4 125.5 . . ? C10 C5 C6 119.2(6) . . ? C10 C5 C1 120.3(5) . . ? C6 C5 C1 120.5(6) . . ? C7 C6 C5 120.3(6) . . ? C7 C6 H6 119.9 . . ? C5 C6 H6 119.9 . . ? C6 C7 C8 120.1(6) . . ? C6 C7 H7 119.9 . . ? C8 C7 H7 119.9 . . ? C7 C8 C9 119.9(6) . . ? C7 C8 H8 120.0 . . ? C9 C8 H8 120.0 . . ? C10 C9 C8 119.9(6) . . ? C10 C9 H9 120.0 . . ? C8 C9 H9 120.0 . . ? C9 C10 C5 120.5(6) . . ? C9 C10 H10 119.7 . . ? C5 C10 H10 119.7 . . ? C12 C11 C15 108.2(6) . . ? C12 C11 C16 127.6(6) . . ? C15 C11 C16 124.1(6) . . ? C12 C11 Rh1 72.2(4) . . ? C15 C11 Rh1 67.2(3) . . ? C16 C11 Rh1 125.7(5) . . ? C11 C12 C13 106.9(6) . . ? C11 C12 C17 127.4(7) . . ? C13 C12 C17 125.7(6) . . ? C11 C12 Rh1 71.7(4) . . ? C13 C12 Rh1 65.3(4) . . ? C17 C12 Rh1 126.5(5) . . ? C14 C13 C12 109.4(6) . . ? C14 C13 C18 126.1(6) . . ? C12 C13 C18 124.1(6) . . ? C14 C13 Rh1 72.5(4) . . ? C12 C13 Rh1 76.4(4) . . ? C18 C13 Rh1 123.5(5) . . ? C13 C14 C15 106.7(6) . . ? C13 C14 C19 126.1(6) . . ? C15 C14 C19 127.2(6) . . ? C13 C14 Rh1 69.0(4) . . ? C15 C14 Rh1 70.7(4) . . ? C19 C14 Rh1 125.4(5) . . ? C14 C15 C11 108.3(6) . . ? C14 C15 C20 127.0(6) . . ? C11 C15 C20 124.0(6) . . ? C14 C15 Rh1 70.9(4) . . ? C11 C15 Rh1 74.7(4) . . ? C20 C15 Rh1 128.2(5) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? O1 C21 C22 109.0(18) . . ? O1 C21 H21A 109.9 . . ? C22 C21 H21A 109.9 . . ? O1 C21 H21B 109.9 . . ? C22 C21 H21B 109.9 . . ? H21A C21 H21B 108.3 . . ? C21 O1 C24 104(2) . . ? C21 C22 C23 102.7(19) . . ? C21 C22 H22A 111.2 . . ? C23 C22 H22A 111.2 . . ? C21 C22 H22B 111.2 . . ? C23 C22 H22B 111.2 . . ? H22A C22 H22B 109.1 . . ? C24 C23 C22 103.8(19) . . ? C24 C23 H23A 111.0 . . ? C22 C23 H23A 111.0 . . ? C24 C23 H23B 111.0 . . ? C22 C23 H23B 111.0 . . ? H23A C23 H23B 109.0 . . ? O1 C24 C23 111(2) . . ? O1 C24 H24A 109.4 . . ? C23 C24 H24A 109.4 . . ? O1 C24 H24B 109.4 . . ? C23 C24 H24B 109.4 . . ? H24A C24 H24B 108.0 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 N3 C1 C5 -176.2(5) . . . . ? C2 N3 C1 Rh1 3.3(7) . . . . ? C4 N1 C2 N2 -0.2(8) . . . . ? Rh1 N1 C2 N2 176.3(4) . . . . ? C4 N1 C2 N3 177.7(6) . . . . ? Rh1 N1 C2 N3 -5.8(8) . . . . ? C3 N2 C2 N1 0.1(8) . . . . ? C3 N2 C2 N3 -177.7(6) . . . . ? C1 N3 C2 N1 2.0(9) . . . . ? C1 N3 C2 N2 179.6(6) . . . . ? C2 N2 C3 C4 0.0(8) . . . . ? N2 C3 C4 N1 -0.1(8) . . . . ? C2 N1 C4 C3 0.2(8) . . . . ? Rh1 N1 C4 C3 -174.2(6) . . . . ? N3 C1 C5 C10 134.6(6) . . . . ? Rh1 C1 C5 C10 -44.9(8) . . . . ? N3 C1 C5 C6 -42.4(8) . . . . ? Rh1 C1 C5 C6 138.1(5) . . . . ? C10 C5 C6 C7 -1.1(9) . . . . ? C1 C5 C6 C7 175.9(6) . . . . ? C5 C6 C7 C8 -1.1(10) . . . . ? C6 C7 C8 C9 2.0(10) . . . . ? C7 C8 C9 C10 -0.6(10) . . . . ? C8 C9 C10 C5 -1.7(10) . . . . ? C6 C5 C10 C9 2.6(10) . . . . ? C1 C5 C10 C9 -174.5(6) . . . . ? C15 C11 C12 C13 -1.8(7) . . . . ? C16 C11 C12 C13 177.8(6) . . . . ? Rh1 C11 C12 C13 56.0(4) . . . . ? C15 C11 C12 C17 179.9(6) . . . . ? C16 C11 C12 C17 -0.5(11) . . . . ? Rh1 C11 C12 C17 -122.4(7) . . . . ? C15 C11 C12 Rh1 -57.7(4) . . . . ? C16 C11 C12 Rh1 121.8(7) . . . . ? C11 C12 C13 C14 5.6(7) . . . . ? C17 C12 C13 C14 -176.0(6) . . . . ? Rh1 C12 C13 C14 65.6(5) . . . . ? C11 C12 C13 C18 178.6(6) . . . . ? C17 C12 C13 C18 -3.0(11) . . . . ? Rh1 C12 C13 C18 -121.4(7) . . . . ? C11 C12 C13 Rh1 -60.0(5) . . . . ? C17 C12 C13 Rh1 118.4(6) . . . . ? C12 C13 C14 C15 -7.2(7) . . . . ? C18 C13 C14 C15 -180.0(6) . . . . ? Rh1 C13 C14 C15 61.0(4) . . . . ? C12 C13 C14 C19 172.7(6) . . . . ? C18 C13 C14 C19 -0.1(11) . . . . ? Rh1 C13 C14 C19 -119.2(7) . . . . ? C12 C13 C14 Rh1 -68.2(5) . . . . ? C18 C13 C14 Rh1 119.1(7) . . . . ? C13 C14 C15 C11 6.0(7) . . . . ? C19 C14 C15 C11 -173.8(6) . . . . ? Rh1 C14 C15 C11 65.9(4) . . . . ? C13 C14 C15 C20 176.1(6) . . . . ? C19 C14 C15 C20 -3.8(11) . . . . ? Rh1 C14 C15 C20 -124.0(6) . . . . ? C13 C14 C15 Rh1 -59.9(4) . . . . ? C19 C14 C15 Rh1 120.2(7) . . . . ? C12 C11 C15 C14 -2.6(7) . . . . ? C16 C11 C15 C14 177.8(6) . . . . ? Rh1 C11 C15 C14 -63.5(4) . . . . ? C12 C11 C15 C20 -173.1(6) . . . . ? C16 C11 C15 C20 7.3(10) . . . . ? Rh1 C11 C15 C20 126.1(6) . . . . ? C12 C11 C15 Rh1 60.8(5) . . . . ? C16 C11 C15 Rh1 -118.7(6) . . . . ? C22 C21 O1 C24 29(4) . . . . ? O1 C21 C22 C23 -30(4) . . . . ? C21 C22 C23 C24 19(5) . . . . ? C21 O1 C24 C23 -16(5) . . . . ? C22 C23 C24 O1 -3(6) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N2 H2 N3 0.88 2.01 2.871(7) 165.4 5_666 _refine_diff_density_max 3.775 _refine_diff_density_min -1.248 _refine_diff_density_rms 0.132 _shelx_res_file ; 007b-17101.res created by SHELXL-2014/7 TITL 007b-17101 CELL 1.54184 29.4841 9.3563 14.9795 90 91.787 90 ZERR 8 0.0009 0.0002 0.0005 0 0.003 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Cl N O Rh UNIT 176 216 8 24 4 8 SADI C23 C22 C21 C22 C24 C23 SADI O1 C24 O1 C21 RIGU O1 C21 C22 > C24 L.S. 10 PLAN 20 SIZE 0.1 0.05 0.01 TEMP -180 BOND $H CONF MORE -1 ACTA EQIV $1 -x+1, -y+1, -z+1 HTAB N2 N3_$1 WGHT 0.110000 13.257100 BASF 0.47279 FVAR 1.81076 RH1 6 0.633813 0.701816 0.605960 11.00000 0.02186 0.02995 = 0.03006 -0.00102 0.00153 -0.00019 CL1 3 0.654404 0.774509 0.459407 11.00000 0.03399 0.02996 = 0.03183 0.00063 0.00528 -0.00228 N1 4 0.566914 0.763868 0.582014 11.00000 0.02184 0.02454 = 0.03805 0.00110 0.00273 -0.00138 N2 4 0.498517 0.690590 0.541110 11.00000 0.01942 0.03155 = 0.04821 -0.00133 0.00094 -0.00365 AFIX 43 H2 2 0.476240 0.634847 0.521906 11.00000 -1.20000 AFIX 0 N3 4 0.561611 0.523746 0.531948 11.00000 0.02449 0.03000 = 0.03964 0.00033 0.00093 0.00055 C1 1 0.605395 0.524817 0.549855 11.00000 0.02681 0.03082 = 0.02688 0.00311 0.00344 -0.00157 C2 1 0.542138 0.654224 0.551641 11.00000 0.02528 0.02411 = 0.04074 0.00199 0.00475 -0.00178 C3 1 0.494952 0.831309 0.565876 11.00000 0.02920 0.02717 = 0.04305 0.00088 0.00060 0.00349 AFIX 43 H3 2 0.468007 0.887004 0.565580 11.00000 -1.20000 AFIX 0 C4 1 0.537138 0.875432 0.590768 11.00000 0.02191 0.02957 = 0.04618 0.00118 0.00270 0.00220 AFIX 43 H4 2 0.544930 0.968707 0.611067 11.00000 -1.20000 AFIX 0 C5 1 0.630527 0.395475 0.526514 11.00000 0.02468 0.02927 = 0.02793 0.00036 -0.00163 -0.00130 C6 1 0.612616 0.259798 0.543836 11.00000 0.02367 0.03338 = 0.03152 0.00249 0.00064 0.00066 AFIX 43 H6 2 0.584993 0.251339 0.574403 11.00000 -1.20000 AFIX 0 C7 1 0.634960 0.138525 0.516655 11.00000 0.03008 0.03016 = 0.03702 0.00173 -0.00077 -0.00158 AFIX 43 H7 2 0.622974 0.046802 0.529479 11.00000 -1.20000 AFIX 0 C8 1 0.675018 0.150345 0.470495 11.00000 0.03544 0.02881 = 0.04051 -0.00404 -0.00063 0.00803 AFIX 43 H8 2 0.689864 0.066885 0.450157 11.00000 -1.20000 AFIX 0 C9 1 0.693316 0.284726 0.454151 11.00000 0.02651 0.03363 = 0.03829 -0.00143 0.00382 0.00448 AFIX 43 H9 2 0.720812 0.292990 0.423138 11.00000 -1.20000 AFIX 0 C10 1 0.671414 0.406101 0.483118 11.00000 0.02533 0.02930 = 0.03854 0.00161 0.00101 0.00121 AFIX 43 H10 2 0.684398 0.497470 0.473299 11.00000 -1.20000 AFIX 0 C11 1 0.692507 0.811685 0.679397 11.00000 0.02500 0.04359 = 0.03110 -0.00370 -0.00729 -0.00288 C12 1 0.652920 0.839926 0.726262 11.00000 0.03337 0.03902 = 0.02485 -0.00797 -0.00459 -0.00236 C13 1 0.633183 0.702913 0.747851 11.00000 0.02588 0.04394 = 0.03010 -0.00009 0.00117 -0.00171 C14 1 0.662762 0.592059 0.722094 11.00000 0.02614 0.04429 = 0.02774 0.00324 -0.00133 -0.00015 C15 1 0.698239 0.658011 0.674211 11.00000 0.02482 0.03916 = 0.02674 -0.00027 -0.00368 -0.00045 C16 1 0.724212 0.917971 0.639769 11.00000 0.03368 0.04259 = 0.04799 0.00234 -0.00426 -0.01052 AFIX 137 H16A 2 0.730745 0.889503 0.578536 11.00000 -1.50000 H16B 2 0.752541 0.921091 0.675716 11.00000 -1.50000 H16C 2 0.710066 1.012762 0.639164 11.00000 -1.50000 AFIX 0 C17 1 0.633465 0.983085 0.748072 11.00000 0.04839 0.04398 = 0.03737 -0.00970 -0.00410 0.00614 AFIX 137 H17A 2 0.645706 1.055396 0.708078 11.00000 -1.50000 H17B 2 0.641600 1.007731 0.810110 11.00000 -1.50000 H17C 2 0.600355 0.979834 0.740303 11.00000 -1.50000 AFIX 0 C18 1 0.590491 0.685046 0.800256 11.00000 0.03210 0.05931 = 0.03149 -0.00151 0.00605 0.00269 AFIX 137 H18A 2 0.567988 0.756238 0.780357 11.00000 -1.50000 H18B 2 0.597680 0.698441 0.864022 11.00000 -1.50000 H18C 2 0.578158 0.588888 0.790323 11.00000 -1.50000 AFIX 0 C19 1 0.657444 0.436353 0.741963 11.00000 0.03937 0.03728 = 0.03529 0.00596 -0.00102 -0.00424 AFIX 137 H19A 2 0.625392 0.409662 0.734895 11.00000 -1.50000 H19B 2 0.668058 0.417122 0.803440 11.00000 -1.50000 H19C 2 0.675398 0.380285 0.700567 11.00000 -1.50000 AFIX 0 C20 1 0.739093 0.586849 0.638090 11.00000 0.02569 0.05050 = 0.03763 0.00010 0.00341 0.00462 AFIX 137 H20A 2 0.732801 0.484965 0.628920 11.00000 -1.50000 H20B 2 0.764788 0.597949 0.680616 11.00000 -1.50000 H20C 2 0.746517 0.630907 0.581017 11.00000 -1.50000 AFIX 0 PART -1 C21 1 0.528378 0.158077 0.715127 10.50000 0.06367 0.06123 = 0.10725 -0.04942 0.00570 0.02077 AFIX 23 H21A 2 0.548289 0.191860 0.667479 10.50000 -1.20000 H21B 2 0.537089 0.058754 0.730679 10.50000 -1.20000 AFIX 0 O1 5 0.483578 0.162127 0.685270 10.50000 0.08371 0.11730 = 0.16297 -0.04740 0.01017 0.01161 C22 1 0.533869 0.250155 0.794032 10.50000 0.09526 0.07767 = 0.11345 -0.05317 -0.00152 0.03513 AFIX 23 H22A 2 0.564708 0.291944 0.798306 10.50000 -1.20000 H22B 2 0.528064 0.196650 0.849538 10.50000 -1.20000 AFIX 0 C23 1 0.499130 0.361774 0.777367 10.50000 0.08372 0.05382 = 0.08836 -0.01662 0.02417 0.01832 AFIX 23 H23A 2 0.483188 0.385036 0.832720 10.50000 -1.20000 H23B 2 0.512949 0.450011 0.753897 10.50000 -1.20000 AFIX 0 C24 1 0.468313 0.297591 0.711289 10.50000 0.12197 0.13203 = 0.17991 -0.07136 -0.03723 0.05366 AFIX 23 H24A 2 0.437808 0.288550 0.736514 10.50000 -1.20000 H24B 2 0.465728 0.360552 0.658257 10.50000 -1.20000 AFIX 0 HKLF 5 REM 007b-17101 REM R1 = 0.0583 for 7343 Fo > 4sig(Fo) and 0.0672 for all 8567 data REM 277 parameters refined using 34 restraints END WGHT 0.1103 13.1873 REM Highest difference peak 3.775, deepest hole -1.248, 1-sigma level 0.132 Q1 1 0.6336 0.8059 0.6037 11.00000 0.05 3.78 Q2 1 0.6296 0.7024 0.5372 11.00000 0.05 1.33 Q3 1 0.6357 0.7015 0.6740 11.00000 0.05 1.31 Q4 1 0.5000 0.1117 0.7500 10.50000 0.05 0.89 Q5 1 0.6557 0.7082 0.4586 11.00000 0.05 0.89 Q6 1 0.6594 0.7857 0.5356 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193.308 1 7 -9 -6 717.023 203.479 1 7 -9 -5 1245.52 201.308 1 7 -9 -4 7409.90 296.293 1 7 -9 -4 15409.5 557.203 -2 -7 -9 4 15409.5 557.203 1 7 -9 -3 16651.5 295.729 1 7 -9 -3 33509.2 610.869 -2 -7 -9 3 33509.2 610.869 1 7 -9 -2 3069.61 404.768 1 7 -9 -2 5547.79 476.726 -2 -7 -9 2 5547.79 476.726 1 7 9 -2 29787.3 486.582 -2 -7 9 1 29787.3 486.582 1 7 -9 -1 50736.8 503.822 -2 -7 -9 1 50736.8 503.822 1 7 9 -1 29591.3 952.812 -2 -7 9 0 29591.3 952.812 1 7 -9 0 5249.09 435.854 -2 -7 -9 0 5249.09 435.854 1 -7 -9 0 2547.72 419.389 -2 7 -9 1 2547.72 419.389 1 7 -9 1 844.463 366.703 -2 -7 -9 -1 844.463 366.703 1 -7 9 -2 775.886 574.654 1 -7 -9 -1 1962.69 493.093 -2 7 -9 2 1962.69 493.093 1 7 -9 2 1276.64 335.269 -2 -7 -9 -2 1276.64 335.269 1 7 -9 3 20064.2 362.768 1 7 -9 3 42038.3 407.125 -2 -7 -9 -3 42038.3 407.125 1 7 -9 4 1220.34 352.149 1 7 -9 4 2907.39 354.677 -2 -7 -9 -4 2907.39 354.677 1 7 9 5 4986.80 274.874 1 7 -9 5 11525.9 419.999 -2 -7 -9 -5 11525.9 419.999 1 -7 -9 -6 1815.41 239.637 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1 -8 -2 8 179.713 128.463 1 -8 -2 7 13970.7 117.051 1 -8 -2 6 91216.9 157.248 1 8 2 -5 228.590 121.085 1 -8 -2 4 29293.3 159.914 1 8 -2 -3 52015.4 145.671 1 8 -2 -3 110477. 1270.01 -2 -8 -2 3 110477. 1270.01 1 8 -2 -2 64965.8 147.080 1 8 -2 -2 137012. 1416.54 -2 -8 -2 2 137012. 1416.54 1 8 -2 -1 3484.20 124.161 1 8 -2 -1 6758.50 1229.37 -2 -8 -2 1 6758.50 1229.37 1 -8 2 0 66372.2 269.466 1 -8 2 0 107575. 374.059 -2 8 2 0 107575. 374.059 1 -8 2 -1 31091.4 250.090 1 8 -2 1 52357.4 323.086 -2 -8 -2 -1 52357.4 323.086 1 -8 2 -2 3309.67 214.083 1 8 -2 2 6143.12 359.881 -2 -8 -2 -2 6143.12 359.881 1 -8 2 -3 9576.56 192.443 1 8 -2 3 20316.3 1494.67 -2 -8 -2 -3 20316.3 1494.67 1 -8 2 -4 14047.1 214.656 1 8 -2 4 24480.3 1645.72 -2 -8 -2 -4 24480.3 1645.72 1 -8 2 -5 10617.1 151.585 1 8 -2 5 24383.3 1722.56 -2 -8 -2 -5 24383.3 1722.56 1 8 2 6 2220.18 121.505 1 8 -2 7 26049.3 124.253 1 8 2 8 59608.4 156.722 1 8 2 9 621.496 132.083 1 -8 -2 -10 15863.7 163.845 1 -8 2 -11 9530.06 163.573 1 -8 -2 -12 9584.51 174.010 1 8 2 13 1137.70 188.851 1 -8 2 -14 17390.2 198.565 1 8 -2 15 1228.09 163.804 1 8 -2 16 1492.40 157.401 1 8 -4 -16 254.034 177.975 1 -8 -4 15 1124.17 190.681 1 -8 -4 14 2047.09 185.773 1 -8 -4 13 26164.0 209.024 1 -8 -4 12 1002.83 186.720 1 -8 4 11 6975.35 191.246 1 -8 -4 10 139.645 176.060 1 -8 -4 9 7098.21 170.145 1 -8 -4 8 45.1133 159.665 1 -8 4 7 23786.0 164.357 1 8 4 -6 44365.9 146.963 1 8 -4 -5 10132.4 129.167 1 8 -4 -5 19529.2 908.147 -2 -8 -4 5 19529.2 908.147 1 -8 -4 4 16631.9 134.990 1 8 -4 -4 31834.5 371.195 -2 -8 -4 4 31834.5 371.195 1 -8 4 3 47144.2 180.847 1 8 -4 -3 85623.8 271.663 -2 -8 -4 3 85623.8 271.663 1 -8 4 2 6417.41 153.229 1 -8 4 2 11326.1 244.620 -2 8 4 -2 11326.1 244.620 1 8 -4 -1 8003.55 172.946 1 8 -4 -1 14411.5 274.521 -2 -8 -4 1 14411.5 274.521 1 8 -4 0 2911.72 462.580 1 -8 -4 1 8894.05 270.619 -2 8 -4 0 8894.05 270.619 1 8 -4 0 4843.15 245.338 -2 -8 -4 0 4843.15 245.338 1 -8 4 -1 104766. 1025.63 1 8 4 0 96835.2 348.271 -2 -8 4 -1 96835.2 348.271 1 8 -4 1 172661. 426.745 -2 -8 -4 -1 172661. 426.745 1 -8 4 -2 164.528 173.863 1 8 -4 2 486.469 266.458 -2 -8 -4 -2 486.469 266.458 1 8 -4 3 24634.0 178.683 1 8 -4 3 45430.8 256.421 -2 -8 -4 -3 45430.8 256.421 1 -8 4 -4 88.8858 142.138 1 8 -4 4 474.896 279.685 -2 -8 -4 -4 474.896 279.685 1 -8 -4 -5 8024.34 142.587 1 8 -4 5 15970.2 361.946 -2 -8 -4 -5 15970.2 361.946 1 -8 -4 -6 8475.77 125.358 1 8 4 7 30194.0 153.775 1 -8 4 -8 3968.13 144.614 1 8 4 9 5262.90 156.321 1 -8 4 -10 2826.81 169.981 1 -8 -4 -11 39315.2 206.307 1 8 -4 12 1432.74 191.805 1 8 4 13 7797.68 209.689 1 8 4 14 5596.59 198.205 1 -8 4 -15 3728.85 172.449 1 8 -4 16 231.126 204.443 1 -8 -6 14 469.297 171.997 1 -8 -6 13 4799.61 207.044 1 -8 6 12 446.824 188.980 1 -8 -6 11 229.337 182.322 1 -8 6 10 5852.29 201.595 1 -8 -6 9 20631.2 208.991 1 -8 -6 8 1774.57 181.429 1 -8 -6 7 23521.4 198.216 1 -8 6 6 4752.28 179.980 1 8 6 -5 5748.68 182.383 1 8 -6 -5 11610.6 1124.31 -2 -8 -6 5 11610.6 1124.31 1 -8 6 4 894.452 155.769 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22940.7 192.335 1 10 6 6 25864.4 1160.31 -2 -8 6 -7 25864.4 1160.31 1 8 -6 8 208.696 179.720 1 8 -6 9 1767.04 206.451 1 8 -6 10 396.571 196.915 1 8 -6 11 25750.3 235.613 1 8 -6 12 34.1706 189.322 1 8 -6 13 3026.95 187.098 1 8 -6 14 211.284 188.462 1 -8 -8 11 277.273 203.848 1 -8 -8 10 7316.49 199.410 1 8 -8 -9 6830.38 214.058 1 -8 -8 8 638.823 206.727 1 -8 -8 7 7423.29 218.122 1 -8 8 6 7148.38 219.307 1 8 -8 -5 1599.25 219.741 1 8 -8 -4 6410.16 246.180 1 -8 8 4 11886.2 609.471 -2 8 8 -4 11886.2 609.471 1 8 -8 -3 28202.8 354.265 1 8 -8 -3 58803.4 469.144 -2 -8 -8 3 58803.4 469.144 1 8 -8 -2 11129.7 282.284 1 -8 -8 3 28223.8 1217.66 -2 8 -8 -2 28223.8 1217.66 1 8 -8 -2 21292.1 477.674 -2 -8 -8 2 21292.1 477.674 1 -8 -8 2 26049.0 364.547 -2 8 -8 -1 26049.0 364.547 1 8 -8 -1 26728.6 484.694 -2 -8 -8 1 26728.6 484.694 1 8 8 -1 29136.0 405.040 -2 -8 8 0 29136.0 405.040 1 8 -8 0 30384.9 383.848 -2 -8 -8 0 30384.9 383.848 1 8 8 0 21906.4 435.022 -2 -8 8 -1 21906.4 435.022 1 8 -8 1 9976.88 344.270 -2 -8 -8 -1 9976.88 344.270 1 -8 8 -2 457.314 662.892 1 8 8 1 5683.34 424.684 -2 -8 8 -2 5683.34 424.684 1 8 -8 2 431.357 353.757 -2 -8 -8 -2 431.357 353.757 1 8 -8 3 290.186 326.419 1 8 -8 3 1200.21 366.761 -2 -8 -8 -3 1200.21 366.761 1 8 -8 4 20531.2 354.189 1 -8 8 -4 39521.0 417.637 -2 8 8 4 39521.0 417.637 1 8 -8 5 4892.72 327.804 1 -8 8 -5 10260.7 386.965 -2 8 8 5 10260.7 386.965 1 -8 -8 -6 8359.03 310.785 1 8 -8 6 14247.1 834.134 -2 -8 -8 -6 14247.1 834.134 1 10 8 5 13190.3 566.315 -2 -8 8 -6 13190.3 566.315 1 8 8 7 13315.1 276.127 1 -10 -8 -6 24608.1 708.001 -2 8 -8 7 24608.1 708.001 1 8 -8 8 4494.92 207.546 1 8 -8 9 444.025 189.292 1 -8 -8 -10 1416.71 178.801 1 -8 -8 -11 2283.87 169.100 1 -8 -10 6 7717.25 216.350 1 -8 -10 5 461.272 206.661 1 8 -10 -4 4744.55 264.941 1 8 -10 -4 8866.82 543.902 -2 -8 -10 4 8866.82 543.902 1 8 -10 -3 1764.64 271.301 1 8 -10 -3 4372.44 587.445 -2 -8 -10 3 4372.44 587.445 1 -8 10 2 5672.72 384.274 1 -8 -10 3 7395.98 592.220 -2 8 -10 -2 7395.98 592.220 1 8 -10 -2 10910.9 707.645 -2 -8 -10 2 10910.9 707.645 1 8 10 -2 9919.89 558.669 -2 -8 10 1 9919.89 558.669 1 -8 10 1 6305.77 523.526 -2 8 10 -1 6305.77 523.526 1 8 10 -1 21145.7 581.909 -2 -8 10 0 21145.7 581.909 1 -8 10 0 35437.2 477.212 -2 8 10 0 35437.2 477.212 1 8 10 0 21618.7 695.208 -2 -8 10 -1 21618.7 695.208 1 -8 10 -1 3130.49 356.284 -2 8 10 1 3130.49 356.284 1 -8 -10 -1 2016.03 432.907 -2 8 -10 2 2016.03 432.907 1 8 -10 2 1427.21 359.896 -2 -8 -10 -2 1427.21 359.896 1 8 -10 3 175.970 302.695 1 8 -10 3 608.935 368.469 -2 -8 -10 -3 608.935 368.469 1 -8 10 -4 11655.7 466.903 1 8 -10 4 23890.2 400.903 -2 -8 -10 -4 23890.2 400.903 1 -8 10 -5 301.707 271.491 1 8 -10 5 1452.95 366.316 -2 -8 -10 -5 1452.95 366.316 1 8 10 6 1492.26 260.715 1 8 -10 6 3729.57 531.461 -2 -8 -10 -6 3729.57 531.461 1 -10 -10 -5 3668.97 527.014 -2 8 -10 6 3668.97 527.014 1 9 -1 -17 2284.65 159.222 1 -9 -1 16 961.656 165.068 1 -9 1 15 3158.61 195.762 1 -9 -1 14 1549.17 195.788 1 -9 1 13 29619.8 225.149 1 -9 1 12 262.782 189.252 1 -9 1 11 790.414 184.998 1 -9 -1 10 2238.13 171.760 1 -9 1 9 34073.7 188.223 1 9 -1 -8 3935.65 124.852 1 9 -1 -7 1646.45 117.442 1 9 -1 -6 5370.16 100.854 1 -9 -1 5 59926.9 129.602 1 9 -1 -4 2627.06 166.727 1 9 -1 -3 57024.0 182.905 1 9 -1 -2 30759.3 157.358 1 9 -1 -1 92581.0 281.708 1 9 -1 -1 199392. 1610.08 -2 -9 -1 1 199392. 1610.08 1 -9 -1 0 1010.19 107.095 1 9 -1 0 234.425 1389.48 -2 -9 -1 0 234.425 1389.48 1 9 1 1 199274. 241.709 1 9 -1 1 381770. 2078.42 -2 -9 -1 -1 381770. 2078.42 1 -9 -1 -2 5463.12 157.646 1 9 -1 2 15325.7 1338.17 -2 -9 -1 -2 15325.7 1338.17 1 9 -1 3 106.703 168.218 1 -9 1 -4 11605.1 211.925 1 9 1 5 89574.8 300.761 1 -9 -1 -6 1452.05 122.501 1 -9 1 -7 11154.5 122.389 1 -9 -1 -8 31.0359 122.005 1 9 1 9 51947.9 163.075 1 -9 -1 -10 82.9042 136.113 1 -9 -1 -11 1726.88 149.176 1 -9 -1 -12 3744.97 156.500 1 9 1 13 22054.0 194.937 1 -9 1 -14 167.790 171.139 1 -9 -1 -15 36117.9 208.120 1 9 -1 16 118.412 156.664 1 9 1 17 706.110 226.988 1 -9 -3 16 14399.0 175.379 1 -9 3 15 6979.69 172.817 1 -9 3 14 9951.55 203.362 1 -9 -3 13 23304.4 216.313 1 -9 -3 12 7496.98 214.073 1 -9 -3 11 8301.34 200.753 1 -9 -3 10 4180.33 180.090 1 -9 -3 9 4318.82 158.192 1 -9 3 8 2289.15 145.873 1 -9 -3 7 4090.25 152.539 1 -9 -3 6 13782.1 142.424 1 9 -3 -5 32261.3 121.822 1 -9 3 4 32826.3 133.947 1 9 -3 -4 68532.7 534.101 -2 -9 -3 4 68532.7 534.101 1 -9 -3 3 797.690 122.598 1 9 -3 -3 1810.40 373.271 -2 -9 -3 3 1810.40 373.271 1 9 -3 -2 85238.2 214.002 1 9 -3 -2 187301. 1824.58 -2 -9 -3 2 187301. 1824.58 1 -9 3 1 32543.5 293.528 1 -9 3 1 57400.1 365.787 -2 9 3 -1 57400.1 365.787 1 -9 3 0 47600.3 481.557 1 -9 -3 1 79186.7 966.953 -2 9 -3 0 79186.7 966.953 1 9 -3 0 84193.1 376.569 -2 -9 -3 0 84193.1 376.569 1 -9 3 -1 71758.2 356.774 1 -9 3 -1 127357. 435.072 -2 9 3 1 127357. 435.072 1 9 -3 2 56136.0 294.259 1 9 -3 2 104232. 614.865 -2 -9 -3 -2 104232. 614.865 1 -9 3 -3 7264.00 175.010 1 9 -3 3 14699.9 404.369 -2 -9 -3 -3 14699.9 404.369 1 -9 3 -4 14370.9 140.178 1 9 -3 4 28624.3 496.089 -2 -9 -3 -4 28624.3 496.089 1 9 -3 5 562.598 122.536 1 9 -3 5 477.821 334.691 -2 -9 -3 -5 477.821 334.691 1 -9 -3 -6 3602.89 116.316 1 9 3 7 592.107 120.877 1 9 3 8 20634.2 146.907 1 9 -3 9 15516.8 158.202 1 9 3 10 759.048 156.045 1 -9 -3 -11 8518.15 187.264 1 -9 -3 -12 19312.5 220.134 1 -9 3 -13 4734.87 206.138 1 9 -3 14 1375.33 185.124 1 -9 3 -15 8922.46 179.554 1 9 -3 16 1990.59 150.952 1 9 5 -15 192.741 173.672 1 -9 -5 14 2409.45 191.498 1 -9 -5 13 418.810 177.162 1 -9 -5 12 10209.8 203.542 1 -9 -5 11 28.3483 208.152 1 -9 -5 10 2349.16 193.918 1 -9 -5 9 4475.03 193.793 1 -9 -5 8 13707.0 186.598 1 -9 -5 7 384.047 163.363 1 -9 -5 6 24674.4 170.168 1 -9 -5 5 125.829 170.120 1 9 -5 -5-633.813 1005.76 -2 -9 -5 5-633.813 1005.76 1 -9 5 4 14133.7 147.885 1 9 -5 -4 29511.3 450.609 -2 -9 -5 4 29511.3 450.609 1 9 -5 -3 916.211 155.615 1 9 -5 -3 1996.37 231.004 -2 -9 -5 3 1996.37 231.004 1 -9 5 2 108322. 229.742 1 9 -5 -2 196959. 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15467.4 199.171 2 -8 -2 -15 1187.54 172.535 2 8 2 16 1392.28 151.669 2 -8 2 -17 367.136 559.570 2 -8 -4 16 338.202 176.554 2 -8 4 15 1228.43 188.725 2 -8 4 14 1876.62 196.902 2 8 -4 -13 24663.3 234.279 2 8 -4 -12 1038.34 211.737 2 8 -4 -11 6112.77 224.816 2 8 -4 -10-8.07112 217.159 2 8 -4 -9 6643.00 188.266 2 8 -4 -8-17.2874 159.525 2 8 -4 -7 21964.0 167.134 2 8 -4 -6 42640.4 169.042 2 -8 -4 5 9386.96 126.453 2 -8 -4 4 14492.8 133.341 2 -8 -4 3 41572.8 184.528 2 -8 -4 2 5246.45 153.441 2 -8 -4 1 7255.68 482.987 2 -8 -4 0 2196.40 732.547 2 8 4 1 86523.4 240.131 2 8 4 2 230.864 170.474 2 8 4 3 20583.7 181.525 2 8 4 4 210.661 140.702 2 -8 -4 -5 7309.30 140.289 2 -8 4 -6 8047.04 131.834 2 8 4 7 28349.4 159.224 2 -8 4 -8 3542.43 151.607 2 -8 4 -9 5158.04 168.505 2 8 -4 10 2803.34 179.932 2 -8 4 -11 37487.0 214.444 2 8 4 12 1539.83 196.703 2 -8 -4 -13 6937.12 203.130 2 -8 -4 -14 5265.53 211.121 2 -8 -4 -15 3241.04 187.526 2 8 4 16 290.369 213.023 2 8 -6 -14 121.714 182.619 2 8 -6 -13 4348.05 191.302 2 8 -6 -12 494.282 200.303 2 8 -6 -11 227.403 203.910 2 8 -6 -10 6066.67 206.838 2 8 -6 -9 20159.0 224.178 2 8 -6 -8 1553.61 193.896 2 8 -6 -7 21905.4 211.025 2 8 -6 -6 4418.96 179.835 2 -8 -6 5 5407.84 177.773 2 -8 -6 4 790.022 171.801 2 -8 -6 3 66755.9 243.581 2 -8 -6 2 5330.51 431.517 2 -8 -6 -1 28608.0 274.952 2 -8 -6 -2 3773.04 212.882 2 -8 -6 -3 3338.36 206.015 2 -8 -6 -4 4297.96 203.339 2 8 6 5 15513.1 209.908 2 8 -6 6 10507.5 177.212 2 -8 -6 -7 21060.5 191.010 2 -8 -6 -8 287.960 176.713 2 -8 -6 -9 1575.63 219.463 2 -8 -6 -10 192.252 214.480 2 -8 -6 -11 24548.8 245.901 2 -8 -6 -12 65.6070 197.383 2 -8 -6 -13 3414.91 180.496 2 -8 -6 -14 145.024 183.993 2 8 -8 -11 137.771 190.785 2 8 -8 -10 7249.75 201.328 2 8 -8 -9 7244.13 213.216 2 8 -8 -8 516.929 213.623 2 8 -8 -7 7497.45 223.058 2 8 -8 -6 7306.94 228.424 2 8 -8 -5 1679.72 203.329 2 -8 -8 4 5517.37 257.383 2 -8 -8 3 27548.9 349.916 2 8 8 1 4589.30 644.862 2 -8 -8 -2 200.198 284.624 2 -8 -8 -3 147.192 328.348 2 -8 -8 -4 19166.5 357.953 2 -8 -8 -5 4306.77 400.265 2 -8 -8 -6 7535.64 232.915 2 -8 -8 -7 12993.8 238.563 2 -8 -8 -8 4413.94 239.624 2 -8 -8 -9 515.209 198.301 2 -8 -8 -10 1279.76 192.129 2 -8 -8 -11 2004.34 176.905 2 8 -10 -6 8046.17 222.486 2 8 -10 -5 230.796 216.153 2 -8 -10 4 4003.50 276.898 2 8 10 -3 1569.10 377.966 2 -8 -10 -2 862.235 312.196 2 8 10 3 7.36852 381.791 2 8 10 4 11400.7 341.195 2 -8 10 -5-101.367 306.663 2 8 -10 6 1554.69 245.012 2 -9 -1 17 2102.47 154.383 2 -9 1 16 1254.80 186.066 2 -9 1 15 2759.93 199.262 2 9 1 -14 1252.81 201.739 2 9 1 -13 25122.3 234.784 2 9 1 -12 248.777 198.900 2 9 1 -11 911.256 190.437 2 9 1 -10 2066.15 176.453 2 9 1 -9 29932.4 180.783 2 9 1 -8 3769.37 150.321 2 -9 -1 7 1525.00 117.159 2 9 1 -6 5432.49 127.965 2 -9 -1 5 68685.1 232.341 2 -9 -1 4 2689.06 145.934 2 -9 -1 3 50702.5 183.505 2 -9 -1 2 27670.2 169.489 2 9 -1 -1 85524.2 115.958 2 9 -1 0 934.409 118.918 2 -9 1 -1 198041. 255.536 2 9 -1 2 5325.77 171.528 2 9 -1 3 203.914 182.431 2 -9 1 -4 11004.2 208.386 2 -9 1 -5 84881.4 301.615 2 -9 1 -6 1356.37 128.770 2 9 -1 7 10886.4 128.188 2 9 -1 8 121.820 125.303 2 9 -1 9 48245.6 170.380 2 9 -1 10 76.3443 149.481 2 9 -1 11 1517.80 161.689 2 9 -1 12 3463.15 174.298 2 9 -1 13 20134.2 213.169 2 9 -1 14 155.873 178.322 2 9 -1 15 32894.4 198.218 2 9 -1 16 349.675 170.715 2 9 1 17 375.562 236.477 2 -9 -3 16 13461.8 185.980 2 -9 3 15 6039.56 188.438 2 -9 3 14 9209.34 213.848 2 -9 3 13 20185.0 236.732 2 9 -3 -12 6416.69 205.581 2 9 -3 -11 7199.62 194.334 2 9 -3 -10 3988.09 198.746 2 9 -3 -9 3883.12 189.457 2 9 -3 -8 2147.79 158.581 2 9 -3 -7 3737.96 144.464 2 9 -3 -6 12672.5 144.435 2 9 -3 -5 32696.0 153.235 2 9 -3 -4 29106.9 125.520 2 -9 -3 3 721.799 124.853 2 -9 -3 2 80128.4 226.164 2 -9 -3 1 27077.8 442.267 2 9 3 0 41476.6 317.763 2 9 3 1 63416.1 359.837 2 9 3 2 52545.6 300.001 2 9 3 3 6712.23 165.269 2 9 3 4 13147.7 143.962 2 9 3 5 572.336 129.631 2 9 3 6 3466.98 125.563 2 9 3 7 379.758 128.722 2 -9 3 -8 19928.5 158.345 2 9 -3 9 14821.8 161.967 2 -9 3 -10 558.276 159.754 2 9 -3 11 8010.35 174.234 2 9 -3 12 16916.6 205.564 2 -9 -3 -13 4481.42 190.445 2 -9 -3 -14 1313.09 186.216 2 -9 -3 -15 8372.62 186.374 2 -9 -3 -16 2014.69 163.992 2 -9 -5 15 23.4576 170.221 2 9 -5 -14 2313.78 182.931 2 9 -5 -13 396.542 203.424 2 9 -5 -12 9433.87 222.534 2 9 -5 -11 128.313 216.507 2 9 -5 -10 1995.75 224.860 2 9 -5 -9 3810.74 217.572 2 9 -5 -8 13598.8 195.285 2 9 -5 -7 438.938 170.874 2 9 -5 -6 22834.8 181.090 2 -9 -5 5 30.3388 156.165 2 -9 -5 4 13915.5 162.888 2 -9 -5 3 881.422 163.440 2 -9 -5 2 100264. 410.812 2 -9 -5 -1 6603.59 178.846 2 9 5 2 46204.1 211.108 2 9 5 3 195.597 172.374 2 -9 -5 -4 15024.9 181.088 2 9 -5 5 3789.01 165.729 2 9 -5 6 5134.46 155.331 2 9 -5 7 1373.49 167.281 2 9 5 8 20385.6 188.084 2 -9 5 -9 1089.87 180.823 2 -9 -5 -10 432.612 190.280 2 -9 -5 -11 129.163 201.613 2 -9 -5 -12 28627.3 224.167 2 -9 -5 -13 599.972 184.654 2 -9 -5 -14 1184.58 187.457 2 -9 -5 -15 714.225 180.354 2 9 -7 -13 1776.39 191.914 2 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0 16 644.239 228.379 2 10 0 -14 9474.12 324.434 2 10 0 -12 46862.8 388.454 2 10 0 -10 6922.10 242.952 2 10 0 -8 55020.2 245.745 2 10 0 -6 4360.82 212.918 2 10 0 -2 118820. 1186.52 2 10 0 0 151213. 259.499 2 10 0 2 193699. 413.732 2 10 0 4 40891.7 348.867 2 10 0 6 102222. 270.159 2 10 0 8 17656.2 185.357 2 10 0 10 53940.6 263.835 2 10 0 12 19963.5 268.277 2 10 0 14 6818.50 255.805 2 10 0 16 24415.5 272.125 2 -10 -2 16 3789.42 178.235 2 -10 2 15 1806.67 198.714 2 -10 2 14 4257.08 195.049 2 -10 2 13 1283.16 209.264 2 10 2 -12 28462.8 240.764 2 10 2 -11 8294.79 209.297 2 10 -2 -10 1128.34 178.845 2 10 -2 -9 10411.7 170.599 2 10 -2 -8 22050.5 172.829 2 10 2 -7 3411.91 127.900 2 10 -2 -6 2443.65 127.763 2 -10 -2 5 9413.92 130.001 2 -10 -2 4 49767.3 204.146 2 -10 -2 3 5548.41 200.732 2 10 -2 -2 5162.63 90.9878 2 -10 -2 1 18422.3 259.066 2 10 2 0 8674.51 230.436 2 10 2 1 6534.27 167.845 2 10 2 2 72320.8 243.150 2 10 2 3 28896.2 227.053 2 -10 2 -4 325.969 191.056 2 -10 -2 -5 10356.1 131.370 2 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5458.43 209.944 2 -10 -8 4 5948.80 277.273 2 -10 -8 3 1271.40 337.549 2 -10 -8 -2 4126.29 331.671 2 -10 -8 -3 2566.65 323.008 2 -10 -8 -4 919.574 327.760 2 10 -8 5 6225.69 445.015 2 10 8 6 18412.1 318.105 2 -10 -8 -7 938.210 225.303 2 -10 -8 -8 330.285 212.601 2 -10 -8 -9 1856.73 187.589 2 -10 -8 -10 2035.02 182.122 2 -10 -8 -11 163.962 189.293 2 -10 -10 6 1723.67 281.349 2 10 -10 -5 229.513 190.901 2 -10 -10 4 9960.93 237.689 2 10 10 -3 537.999 417.795 2 -10 -10 -2 10141.6 324.382 2 10 10 3 262.903 325.469 2 10 10 4 717.497 362.057 2 10 -10 5 1856.14 332.708 2 -10 10 -6 7386.68 616.366 2 -11 -1 17 2585.94 170.273 2 -11 -1 16-26.9586 174.497 2 -11 1 15 2669.93 204.019 2 11 1 -14 1399.47 220.081 2 11 1 -13 13597.6 232.269 2 11 1 -12 665.356 190.342 2 11 1 -11 48920.4 241.615 2 11 1 -10 4551.89 177.824 2 11 1 -9 313.342 159.192 2 11 1 -8 1504.68 154.841 2 11 1 -7 116641. 207.795 2 11 1 -6 991.526 139.580 2 11 -1 -5 24452.4 218.017 2 -11 -1 4 7896.51 114.612 2 -11 -1 3 2784.34 110.106 2 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52642.5 180.065 2 11 3 4 39763.2 146.960 2 -11 3 -5 169.421 115.427 2 -11 3 -6 38732.2 148.346 2 11 3 7 31330.3 155.832 2 -11 3 -8 2646.77 147.949 2 -11 3 -9 12828.0 176.198 2 11 -3 10 7195.12 183.103 2 11 -3 11 3215.38 192.083 2 11 -3 12 425.549 209.238 2 -11 -3 -13 5097.39 211.011 2 11 3 14 5965.25 195.941 2 -11 -3 -15 1094.40 176.072 2 11 3 16 475.675 181.201 2 11 -5 -15 1134.36 186.787 2 -11 5 14 8470.22 186.094 2 11 -5 -13 4125.87 202.850 2 11 -5 -12 1213.50 206.535 2 11 -5 -11 564.571 212.927 2 11 -5 -10 30395.9 261.456 2 11 -5 -9 4669.15 227.346 2 11 -5 -8 47552.1 276.246 2 11 -5 -7 392.058 202.547 2 11 -5 -6 2750.01 171.628 2 -11 -5 5 978.047 170.588 2 11 -5 -4 35045.6 188.990 2 -11 -5 3 1371.61 169.004 2 11 5 -2 46.5056 983.510 2 -11 -5 -1 15195.0 213.014 2 11 5 2 2644.15 156.308 2 11 5 3 2733.14 151.448 2 -11 -5 -4 52530.8 209.175 2 -11 5 -5 408.211 180.493 2 11 5 6 42552.8 197.672 2 -11 5 -7-50.9305 168.401 2 -11 5 -8 620.340 177.557 2 11 -5 9 2030.42 180.161 2 11 -5 10 22204.9 229.528 2 11 -5 11-169.119 197.820 2 -11 -5 -12 116.681 193.503 2 -11 -5 -13 201.756 191.795 2 -11 -5 -14 4592.69 179.575 2 11 -7 -12 152.902 185.075 2 11 -7 -11 2206.55 214.131 2 11 -7 -10 15672.0 249.366 2 11 -7 -9 136.852 221.265 2 11 -7 -8 21996.1 255.337 2 11 -7 -7 9936.27 222.320 2 11 -7 -6 1441.27 209.761 2 11 -7 -5 209.346 183.148 2 -11 -7 4 15652.8 219.643 2 -11 -7 3 3332.81 239.809 2 -11 -7 -1 421.871 937.930 2 -11 -7 -2 1410.21 244.789 2 -11 -7 -3 3255.94 224.881 2 -11 -7 -4 12003.7 209.939 2 -11 7 -5 371.930 238.417 2 11 -7 6 24965.7 253.770 2 11 -7 7 4253.73 217.758 2 -11 -7 -8 2032.36 206.797 2 -11 -7 -9 1337.16 203.988 2 -11 -7 -10 9244.02 203.267 2 -11 -7 -11 4434.62 201.898 2 -11 -7 -12 2909.76 198.341 2 11 -9 -9-297.803 266.983 2 11 -9 -8 3847.11 243.593 2 11 -9 -7 12035.1 215.741 2 11 -9 -6 983.422 209.917 2 11 -9 -5 3126.30 222.808 2 -11 -9 4 832.909 243.532 2 11 9 -3 12981.8 527.472 2 -11 -9 -2 1470.70 310.558 2 -11 -9 -3 9184.33 312.856 2 11 9 4 3801.59 318.415 2 11 9 5 531.613 352.387 2 11 -9 6 3368.55 253.850 2 11 -9 7 10220.2 227.947 2 11 -9 8 441.760 175.193 2 -12 0 16 916.130 245.420 2 12 0 -14 5809.52 290.051 2 12 0 -12 18780.6 353.568 2 12 0 -10 69664.9 357.675 2 12 0 -8 733.566 229.885 2 12 0 -6 81745.0 238.294 2 12 0 -2 92478.6 1265.16 2 12 0 0 43430.5 201.278 2 12 0 2 54252.3 309.778 2 12 0 4 133963. 338.443 2 12 0 6 161.135 167.341 2 12 0 8 86262.6 264.287 2 12 0 10 2520.57 235.336 2 12 0 12 2559.10 247.714 2 12 0 14 37942.9 288.381 2 12 0 16 73.5165 234.195 2 -12 -2 16 1442.58 162.841 2 -12 2 15 1084.44 195.028 2 -12 2 14 3440.38 192.114 2 -12 2 13 6981.37 217.856 2 12 2 -12 7567.41 217.205 2 12 2 -11 1125.82 214.775 2 12 2 -10 14762.2 216.129 2 12 -2 -9 11820.7 197.791 2 12 -2 -8 5093.91 180.735 2 12 -2 -7 15841.5 170.526 2 12 -2 -6 57623.5 178.028 2 12 -2 -5 5464.91 134.843 2 12 -2 -4 13661.0 125.486 2 -12 -2 3 13902.6 153.106 2 -12 -2 2 4294.29 165.112 2 -12 2 1 64.2201 119.343 2 -12 2 0 23583.2 218.407 2 12 2 1 19035.6 191.307 2 12 -2 2 26854.7 174.062 2 -12 2 -3 1284.38 127.196 2 -12 2 -4 48645.1 136.812 2 12 -2 5 6152.59 116.377 2 12 -2 6 1960.03 128.177 2 12 -2 7 7111.71 133.791 2 12 -2 8 88070.2 202.644 2 12 -2 9 2175.29 154.826 2 12 -2 10 21517.3 186.834 2 12 -2 11 6945.61 176.683 2 12 -2 12 2173.15 191.618 2 12 -2 13-3.19418 188.758 2 12 -2 14 7627.08 185.191 2 12 2 15 4324.68 183.544 2 12 2 16 531.365 185.591 2 -12 4 15 228.006 177.788 2 -12 4 14 297.713 190.027 2 -12 4 13 14406.2 240.782 2 12 -4 -12 1568.19 228.551 2 12 -4 -11 441.783 226.195 2 12 -4 -10 10.9234 236.584 2 12 -4 -9 12489.8 241.401 2 12 -4 -8 1478.87 234.352 2 12 -4 -7 33126.2 232.738 2 12 -4 -6 23289.5 175.316 2 12 -4 -5 11278.6 156.892 2 -12 -4 4 2000.53 140.999 2 12 -4 -3 65604.3 199.310 2 12 -4 -2 2806.98 374.735 2 12 -4 -1 4531.54 1271.85 2 12 4 1 56051.0 186.984 2 12 4 2 9828.05 141.794 2 12 -4 3 3803.00 135.008 2 12 -4 4 123.008 139.980 2 12 4 5 20775.4 173.526 2 -12 4 -6 1826.90 152.907 2 12 4 7 26262.5 173.230 2 -12 4 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127.605 2 13 -1 1 88222.5 224.778 2 13 -1 2 126.815 144.481 2 13 -1 3 3090.74 123.353 2 13 -1 4 3546.17 118.396 2 13 -1 5 58338.2 140.674 2 13 -1 6 2464.10 125.770 2 13 -1 7 685.105 130.672 2 13 -1 8 96.6445 140.521 2 13 -1 9 42455.0 184.194 2 13 -1 10 2011.97 161.695 2 13 -1 11 9765.89 178.920 2 13 -1 12 10605.7 204.560 2 13 -1 13 3789.79 196.356 2 13 -1 14 323.601 182.335 2 13 -1 15 26125.7 188.198 2 13 1 16 747.248 174.667 2 -13 -3 16 5673.14 171.283 2 -13 3 15 1744.06 187.533 2 13 3 -14 432.248 203.580 2 13 3 -13 1018.83 222.056 2 13 3 -12 6992.22 234.633 2 13 -3 -11 368.065 230.537 2 13 -3 -10 61.1699 209.758 2 13 -3 -9 2530.67 305.753 2 13 -3 -8 21603.8 256.272 2 13 -3 -7 10000.7 196.342 2 13 -3 -6 29265.2 180.195 2 13 -3 -5 24630.0 170.292 2 13 -3 -4 4849.23 128.015 2 13 -3 -3 16458.8 137.314 2 13 -3 -2 59869.9 263.211 2 13 -3 -1 25811.0 429.291 2 13 -3 0 7550.98 193.965 2 13 3 1 29271.6 131.888 2 13 -3 2 26385.3 125.208 2 -13 3 -3 2395.98 112.498 2 13 3 4 484.616 111.983 2 -13 3 -5 25782.5 134.171 2 -13 3 -6 11659.6 164.032 2 13 -3 7 223.632 151.887 2 13 -3 8 20421.7 182.607 2 13 -3 9 30970.3 196.935 2 13 -3 10 5012.49 186.190 2 13 -3 11 6767.00 210.111 2 13 -3 12 12229.0 218.499 2 13 3 13 4739.65 204.271 2 -13 -3 -14 14.9350 177.596 2 -13 -3 -15 3330.99 179.552 2 13 5 -14-25.6567 174.765 2 13 -5 -13 519.799 193.870 2 13 -5 -12 7214.30 210.942 2 13 -5 -11 353.324 208.177 2 13 -5 -10 918.722 228.257 2 13 -5 -9 162.806 289.035 2 13 -5 -8 25050.1 316.428 2 13 -5 -7 101.795 235.973 2 13 -5 -6 41721.3 236.497 2 -13 -5 5 8872.06 195.135 2 -13 -5 4 5226.36 179.501 2 13 -5 -3 674.908 174.207 2 13 -5 -2 76189.5 1822.67 2 13 -5 -1 370.414 534.682 2 13 -5 0 11223.7 1540.34 2 13 -5 1 667.357 227.199 2 -13 -5 -2 26138.3 185.167 2 13 -5 3 118.943 143.609 2 13 -5 4 850.679 161.044 2 -13 5 -5 1488.64 176.132 2 -13 -5 -6 7501.49 195.163 2 -13 5 -7 459.445 192.829 2 -13 5 -8 16787.2 201.356 2 13 -5 9 2897.41 203.953 2 -13 -5 -10 6209.15 206.006 2 -13 -5 -11 540.599 202.607 2 13 -5 12 15107.0 209.498 2 -13 -5 -13 79.5274 166.810 2 -13 -5 -14 172.982 175.460 2 13 -7 -12 4114.62 179.943 2 13 -7 -11 419.746 194.970 2 13 -7 -10 1384.77 223.574 2 13 -7 -9 5125.71 266.792 2 13 -7 -8 6502.58 278.690 2 13 -7 -7-206.170 238.027 2 -13 -7 6 8798.52 223.840 2 13 -7 -5 611.290 205.477 2 -13 -7 4 5257.41 211.854 2 -13 -7 3 876.422 232.274 2 -13 -7 -1 7087.74 796.761 2 -13 -7 -2 3711.28 252.140 2 -13 -7 -3 2151.38 230.335 2 13 -7 4 5110.18 252.123 2 13 7 5 6966.51 309.005 2 13 -7 6 3940.38 239.909 2 13 -7 7 109.427 241.038 2 13 -7 8 4510.04 225.524 2 -13 -7 -9 3207.51 195.892 2 -13 -7 -10 2741.46 186.515 2 -13 -7 -11-16.6102 183.168 2 13 7 12 11555.6 237.660 2 13 -9 -8 964.121 230.654 2 13 -9 -7 434.282 222.392 2 13 -9 -6 927.536 192.426 2 -13 -9 5 8708.94 215.038 2 -13 -9 4 4074.71 228.059 2 -13 9 3 1162.45 379.394 2 -13 -9 -2 297.904 290.887 2 -13 -9 -3 3088.16 315.970 2 13 9 4 133.780 272.761 2 13 9 5 9569.26 373.678 2 13 -9 6 966.580 254.682 2 13 -9 7 303.044 220.672 2 13 9 8 27.6094 277.960 2 -14 0 16 3002.88 259.919 2 14 0 -14 13014.4 282.080 2 14 0 -12 45850.6 388.832 2 14 0 -10 2649.65 306.010 2 14 0 -8 15366.2 301.469 2 14 0 -6 33551.2 197.887 2 14 0 -4 88940.8 265.881 2 14 0 -2 77280.9 1370.55 2 14 0 0 90223.1 251.933 2 14 0 2 132095. 265.638 2 14 0 4 5223.29 159.517 2 14 0 6 21552.9 205.296 2 14 0 8 11607.9 229.478 2 14 0 10 15465.4 262.214 2 14 0 12 46144.5 341.073 2 14 0 14 11543.5 261.611 2 -14 0 -16 13820.7 308.588 2 -14 -2 16 2415.24 168.936 2 -14 2 15 5309.37 203.349 2 -14 2 14 3944.76 206.414 2 14 2 -13 443.758 215.343 2 14 2 -12 10533.8 226.958 2 14 2 -11 10959.3 227.562 2 14 2 -10 1585.37 261.958 2 14 2 -9 1889.94 309.569 2 14 2 -8 13430.0 279.252 2 14 2 -7 3270.38 178.387 2 14 -2 -6 6465.55 148.715 2 14 -2 -5 4045.23 132.750 2 14 -2 -4 48073.6 164.082 2 14 -2 -3 4921.99 142.358 2 14 -2 -2 20237.5 185.806 2 14 -2 -1 30643.7 1290.16 2 14 -2 0 53486.6 235.960 2 -14 2 -1 6976.22 118.018 2 14 2 2 133894. 178.468 2 -14 2 -3 23080.7 128.170 2 14 -2 4 3127.68 111.128 2 14 -2 5 2416.47 117.613 2 14 -2 6 32802.6 161.447 2 14 -2 7 4266.36 194.604 2 14 -2 8 925.119 159.266 2 14 -2 9 7436.76 169.351 2 14 -2 10 13745.5 180.549 2 14 2 11 1611.78 177.249 2 14 -2 12 4633.69 198.291 2 14 2 13 13902.2 216.393 2 14 2 14 6533.56 201.008 2 -14 -2 -15 117.936 164.832 2 14 4 -15 11003.9 216.938 2 -14 4 14 1505.65 179.816 2 -14 4 13 143.303 211.777 2 14 -4 -12 85.2940 208.165 2 14 -4 -11 13542.1 243.182 2 14 -4 -10-351.085 322.098 2 14 4 -9 20435.4 396.406 2 14 -4 -8 4056.56 274.796 2 14 -4 -7 12359.0 235.130 2 14 -4 -6 2579.14 181.114 2 14 4 -5 11547.4 192.518 2 14 -4 -4 10333.6 155.238 2 14 -4 -3 5670.06 143.512 2 14 -4 -2 1102.62 216.600 2 14 -4 -1 73277.4 672.743 2 14 -4 0 17018.9 577.235 2 -14 4 -1 668.565 151.431 2 14 -4 2 16143.8 129.360 2 14 -4 3 47657.0 150.397 2 -14 4 -4-8.63400 126.780 2 14 -4 5 11776.7 145.883 2 14 -4 6 6328.93 181.981 2 14 -4 7 3808.10 190.634 2 14 -4 8 374.578 187.457 2 14 -4 9 5322.29 180.794 2 14 -4 10 5511.70 213.450 2 14 -4 11 4279.64 206.520 2 -14 -4 -12 336.292 186.443 2 14 -4 13 17968.0 201.277 2 -14 -4 -14 1980.33 168.860 2 14 6 -13 646.693 177.279 2 14 -6 -12 223.779 181.953 2 14 -6 -11 7660.75 206.733 2 14 -6 -10 923.134 248.745 2 14 -6 -9 10504.9 299.484 2 14 -6 -8 4549.55 298.454 2 14 -6 -7 6926.93 243.606 2 14 -6 -6 796.601 220.986 2 -14 -6 5 8789.49 244.725 2 -14 -6 4 804.409 207.222 2 -14 -6 3 7458.84 206.657 2 14 -6 -2 5555.15 668.515 2 14 -6 -1 51567.4 2050.51 2 14 -6 0 1388.06 621.253 2 14 -6 1 2218.34 576.700 2 14 -6 2 2522.78 196.325 2 -14 -6 -3 15513.7 205.925 2 -14 6 -4 1968.28 179.789 2 -14 6 -5 10796.1 208.941 2 -14 6 -6 2941.04 210.337 2 14 -6 7 2378.15 260.312 2 14 -6 8 113.254 245.491 2 -14 -6 -9 6066.87 203.929 2 -14 -6 -10 427.799 208.543 2 -14 -6 -11 3887.91 203.972 2 -14 -6 -12 83.8781 186.408 2 14 6 13 8448.97 230.886 2 14 -8 -10 1455.02 255.998 2 14 -8 -9 529.180 287.248 2 14 -8 -8 9923.52 312.045 2 14 -8 -7 2360.91 242.948 2 14 -8 -6 314.074 223.966 2 14 -8 -5 1919.06 229.424 2 -14 -8 4 5373.07 281.640 2 -14 8 3 3736.69 389.478 2 -14 8 2 1440.24 650.208 2 -14 -8 -2 7821.60 356.799 2 14 -8 3 3600.56 267.139 2 -14 -8 -4 3876.63 292.088 2 14 8 5 10578.8 296.712 2 14 -8 6 15731.5 264.844 2 14 -8 7 2446.09 267.352 2 14 -8 8 1227.80 248.356 2 -14 -8 -9 2302.16 173.972 2 -14 8 -10 675.153 400.312 2 14 10 -3 1965.37 599.916 2 14 10 2 6859.01 359.665 2 14 -10 3 76.6030 294.142 2 -15 -1 16 1324.12 187.004 2 -15 1 15 3285.53 190.826 2 15 1 -14 2143.68 212.824 2 15 1 -13 24782.9 255.618 2 15 1 -12-400.331 220.627 2 15 1 -11 29019.9 254.776 2 15 1 -10 1360.39 296.374 2 15 1 -9 2313.97 314.563 2 15 1 -8 31.3347 252.337 2 15 1 -7 32566.8 174.507 2 15 1 -6 1162.36 133.404 2 15 -1 -5 236.649 112.997 2 15 -1 -4 8259.68 106.190 2 15 -1 -3 28880.5 154.365 2 15 -1 -2 738.477 207.389 2 -15 -1 1 16883.8 350.967 2 15 -1 1 117272. 170.036 2 15 -1 2 8024.28 121.340 2 15 -1 3 126680. 174.660 2 15 -1 4 6622.07 113.545 2 15 -1 5 2229.02 115.478 2 15 -1 6 206.687 134.694 2 15 -1 7 33673.5 226.933 2 15 -1 8 1402.26 201.657 2 15 -1 9 6447.22 169.487 2 -15 -1 -10 5054.21 175.620 2 15 -1 11 771.800 179.948 2 15 -1 12 900.097 186.092 2 15 1 13 4183.83 189.765 2 15 -1 14 4315.94 187.506 2 15 1 15 22418.5 200.766 2 -15 3 15 251.835 180.852 2 15 3 -14 18156.8 216.613 2 15 3 -13 10283.7 230.729 2 15 3 -12-11.5814 219.805 2 15 3 -11 25067.8 275.894 2 15 -3 -10 3487.75 355.149 2 15 3 -9 3219.08 378.935 2 15 3 -8 15416.9 329.321 2 15 -3 -7 3149.84 193.988 2 15 -3 -6 19512.5 188.309 2 15 -3 -5 5506.99 161.690 2 15 -3 -4 8756.58 154.174 2 15 -3 -3 31963.4 169.876 2 15 -3 -2 1417.46 304.208 2 15 -3 -1 14618.8 1327.54 2 15 -3 0 73043.1 1706.02 2 -15 3 -1 76082.3 152.819 2 -15 3 -2 86.2439 113.333 2 -15 3 -3 83385.0 163.355 2 -15 3 -4 24924.1 136.988 2 15 -3 5 2826.16 126.523 2 -15 3 -6 16726.2 171.943 2 15 -3 7 9814.84 224.474 2 15 -3 8 4663.52 247.782 2 15 -3 9 1097.19 188.121 2 15 -3 10 7097.03 192.834 2 15 -3 11 2951.63 198.570 2 15 -3 12 863.928 192.983 2 15 3 13 366.635 187.554 2 15 3 14 11859.6 189.665 2 -15 -3 -15 1767.01 162.487 2 15 5 -14 12690.7 187.565 2 15 5 -13 2551.97 207.482 2 15 -5 -12 993.467 199.878 2 15 -5 -11 2278.39 248.157 2 15 -5 -10 11785.9 431.618 2 15 5 -9 5243.77 469.033 2 15 -5 -8 23697.2 311.833 2 15 -5 -7 148.705 238.702 2 15 -5 -6 8510.28 229.164 2 15 -5 -5 7074.82 217.293 2 15 -5 -4 9146.38 202.367 2 15 -5 -3-11.9466 158.996 2 15 -5 -2 12095.3 313.121 2 15 -5 -1 2986.46 551.072 2 15 -5 0 55772.7 762.098 2 15 -5 1 8771.19 256.365 2 15 -5 2 983.921 156.020 2 -15 5 -3 5396.47 141.186 2 -15 5 -4 19424.9 166.596 2 -15 5 -5 5988.35 162.577 2 15 -5 6 9462.87 201.080 2 15 -5 7 79.6569 221.878 2 15 -5 8 5210.99 297.729 2 15 -5 9 269.339 231.980 2 15 -5 10 8357.31 242.757 2 15 -5 11 23.7295 213.482 2 -15 -5 -12 1224.50 199.785 2 -15 -5 -13-160.796 168.426 2 15 -7 -11 747.151 205.815 2 15 -7 -10 6642.09 239.974 2 15 -7 -9 826.624 293.218 2 15 -7 -8 7402.00 290.510 2 15 -7 -7 6947.69 240.940 2 15 -7 -6 824.005 219.210 2 15 -7 -5 289.263 204.034 2 -15 -7 4 2750.27 231.740 2 15 7 -3 10710.4 300.606 2 -15 7 2 8832.49 752.156 2 15 -7 -1 18320.1 2225.69 2 15 -7 0 17583.9 2260.13 2 15 -7 1 1083.93 431.426 2 -15 -7 -2 1616.60 302.627 2 15 -7 3 1243.13 280.092 2 15 -7 4 16086.0 251.652 2 15 -7 5 798.471 238.849 2 15 -7 6 21847.5 276.747 2 15 -7 7 2728.92 249.971 2 15 -7 8 1144.98 237.146 2 15 -7 9 1526.05 202.938 2 -15 -7 -10 832.376 186.582 2 -15 -7 -11 3678.73 184.092 2 15 -9 -7 7867.64 203.094 2 15 -9 -6 175.637 208.174 2 15 -9 -5 162.002 195.676 2 -15 -9 4-14.9279 211.010 2 -15 9 3 9948.39 320.205 2 15 9 1 4303.58 802.354 2 -15 -9 -2-37.4021 314.463 2 -15 -9 -3 10376.3 330.203 2 15 9 4 2876.70 323.641 2 15 9 5 279.365 294.369 2 15 -9 6 4670.63 258.609 2 15 -9 7 5137.24 231.645 2 -16 0 16 2236.08 261.733 2 16 0 -14 365.153 309.605 2 16 0 -12 53566.7 350.758 2 16 0 -10 26183.8 366.228 2 16 0 -8 3277.56 248.063 2 16 0 -6 50830.6 240.312 2 16 0 -4 12281.3 176.581 2 16 0 -2 91008.1 390.883 2 16 0 0 44205.9 439.948 2 16 0 2 738.897 154.882 2 16 0 4 31127.6 191.559 2 16 0 6 7440.77 193.449 2 16 0 8 44756.3 327.480 2 16 0 10 2976.05 261.688 2 16 0 12 19568.7 306.021 2 16 0 14 30374.7 263.642 2 16 2 -15 514.033 190.842 2 16 2 -14 421.963 206.040 2 -16 2 13 3908.70 204.204 2 16 2 -12 19639.1 236.220 2 16 2 -11 1704.56 285.994 2 16 2 -10 15224.9 402.145 2 16 2 -9 6728.94 337.896 2 16 2 -8 4183.09 245.717 2 16 -2 -7 20767.0 191.269 2 16 -2 -6 69287.3 210.166 2 16 -2 -5 4681.77 152.273 2 16 -2 -4 15368.6 150.071 2 16 -2 -3 15942.9 151.541 2 16 -2 -2 32174.8 379.810 2 16 -2 1 16241.8 136.254 2 16 -2 2 37108.0 130.633 2 16 -2 3 1132.13 115.183 2 16 -2 4 37861.1 136.777 2 16 -2 5 20512.1 136.796 2 16 2 6 722.104 142.453 2 16 -2 7 9243.87 251.766 2 16 -2 8 35560.2 407.472 2 16 -2 9 8475.81 291.387 2 16 2 10 4055.04 179.112 2 16 -2 11 11506.6 210.944 2 16 2 12 1735.47 206.959 2 16 2 13 580.034 189.826 2 -16 -2 -14 3317.16 192.823 2 -16 -2 -15 2016.38 156.821 2 16 4 -14 56.9210 178.715 2 -16 4 13 9290.69 209.220 2 -16 4 12 1624.92 208.578 2 16 -4 -11 410.135 341.995 2 16 4 -10 2094.87 548.605 2 16 4 -9 17621.5 512.402 2 16 4 -8 3969.73 341.164 2 16 -4 -7 18899.8 236.489 2 16 -4 -6 32022.3 229.861 2 16 -4 -5 18901.7 212.022 2 16 -4 -4 4103.89 170.064 2 16 -4 -3 24000.7 185.033 2 16 -4 -2 439.617 329.307 2 16 -4 -1 1916.66 1480.77 2 16 -4 0 3167.58 1497.44 2 16 -4 1 23224.0 233.994 2 16 -4 2 7860.05 139.099 2 16 -4 3 318.563 131.080 2 -16 4 -4 2609.95 136.601 2 -16 4 -5 26221.6 161.375 2 16 -4 6 298.813 178.426 2 16 -4 7 19654.1 261.286 2 16 -4 8 17303.9 278.402 2 16 -4 9 6638.87 283.698 2 16 -4 10 3991.42 203.238 2 16 -4 11 11950.5 204.472 2 16 -4 12 396.386 175.054 2 -16 -4 -13-42.5971 176.482 2 -16 -4 -14-4.88604 176.683 2 16 -6 -12-146.918 180.321 2 16 -6 -11 119.083 282.132 2 16 6 -10 204.370 491.498 2 16 6 -9 10492.4 452.637 2 16 -6 -8-34.7086 267.251 2 16 -6 -7 12809.4 255.259 2 16 -6 -6 1375.20 237.126 2 16 -6 -5 12336.4 249.748 2 16 -6 -4 234.580 212.561 2 16 -6 -3 14802.0 231.343 2 16 -6 -2 5873.46 528.902 2 16 -6 -1-357.886 1844.76 2 16 -6 0 6931.52 669.314 2 16 -6 1 16706.9 326.468 2 16 -6 2 253.118 171.640 2 16 -6 3-4.88355 180.427 2 16 -6 4 618.012 173.466 2 16 -6 5 17133.3 187.124 2 16 -6 6 334.093 210.959 2 16 -6 7 11739.2 248.501 2 16 -6 8 644.718 274.283 2 16 -6 9 8679.69 269.752 2 -16 -6 -10 1428.29 211.256 2 -16 -6 -11 6328.73 193.043 2 -16 -6 -12 548.948 167.064 2 16 -8 -9 5399.48 327.204 2 16 -8 -8 1767.33 240.939 2 16 -8 -7 6154.71 231.473 2 16 -8 -6 8427.38 237.329 2 16 -8 -5 477.947 243.020 2 -16 -8 4 834.655 210.402 2 -16 8 3 1915.79 341.359 2 -16 -8 -2 1531.64 264.652 2 16 -8 3 624.096 266.068 2 -16 -8 -4 8863.11 248.101 2 16 8 5 9809.00 236.566 2 16 -8 6 280.581 208.116 2 16 -8 7 6761.62 242.098 2 16 -8 8 3368.25 242.932 2 16 -8 9 202.438 231.768 2 -17 1 15 5810.21 195.072 2 17 1 -14 252.319 206.798 2 17 1 -13 1870.56 223.782 2 17 1 -12 1134.40 254.242 2 17 -1 -11 30068.0 494.983 2 17 -1 -10-212.043 422.444 2 17 1 -9 14723.8 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3 7461.51 136.669 2 17 -3 4 57.5128 124.175 2 17 -3 5 9065.22 140.253 2 17 -3 6 17098.2 164.451 2 17 -3 7 236.744 270.800 2 17 -3 8 22619.7 405.419 2 17 -3 9 9930.66 399.397 2 17 -3 10 2561.31 253.064 2 17 -3 11 2485.43 194.473 2 17 -3 12 7686.74 191.240 2 17 3 13 944.562 182.496 2 -17 -3 -14 290.613 162.699 2 17 5 -13 617.253 189.733 2 17 5 -12 4759.59 241.948 2 17 -5 -11 839.332 710.115 2 17 5 -10-51.2654 722.362 2 17 5 -9 1434.86 555.061 2 -17 -5 8 42546.5 325.449 2 17 -5 -7 291.461 244.661 2 17 -5 -6 18844.4 245.138 2 17 -5 -5 2214.44 218.583 2 17 -5 -4 5781.04 206.865 2 17 -5 -3 150.130 211.426 2 17 -5 -2 27964.6 542.139 2 17 -5 -1 1106.89 1638.82 2 17 -5 0 1316.21 1692.13 2 17 -5 1 2837.13 288.555 2 17 -5 2 10505.0 180.011 2 17 -5 3 236.185 164.027 2 17 -5 4 913.123 155.308 2 17 -5 5 342.876 169.686 2 17 -5 6 27856.7 225.404 2 17 -5 7 262.753 285.709 2 17 -5 8 20152.5 387.940 2 17 -5 9 1004.00 424.521 2 17 -5 10 8236.65 246.680 2 -17 -5 -11 275.193 197.669 2 -17 -5 -12 12686.7 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0 -2 60520.6 356.918 2 18 0 0 46053.8 347.908 2 18 0 2 8812.65 171.687 2 18 0 4 9617.98 175.893 2 18 0 6 28674.4 231.282 2 18 0 8 6104.51 314.723 2 18 0 10 58632.3 452.118 2 18 0 12 22380.2 315.041 2 18 0 14 16486.1 278.641 2 18 2 -15 3217.70 199.275 2 18 2 -14 5747.74 199.634 2 18 2 -13-323.294 209.005 2 18 -2 -12 3955.04 419.921 2 18 -2 -11 2270.23 689.137 2 18 2 -10 7240.79 529.297 2 18 2 -9 2157.70 344.980 2 18 2 -8 17839.2 219.555 2 18 -2 -7 10703.1 195.480 2 18 -2 -6 3508.56 177.891 2 18 -2 -5 13399.1 176.366 2 18 -2 -4 56215.5 193.626 2 18 -2 -3 2869.30 148.782 2 18 -2 1 629.895 163.572 2 18 -2 2 19331.1 150.538 2 18 -2 3 13201.5 136.698 2 18 -2 4 1118.88 128.060 2 18 -2 5 942.063 129.763 2 18 -2 6 7123.62 142.444 2 18 -2 7 6506.54 240.169 2 18 -2 8 537.127 498.709 2 18 -2 11 1016.12 187.611 2 18 2 12 2945.74 207.268 2 18 2 13 2552.56 187.631 2 18 2 14 5886.11 172.662 2 18 4 -14 366.568 191.516 2 18 4 -13 37.7241 202.194 2 18 4 -12 927.486 411.917 2 18 4 -10 1076.62 762.738 2 18 4 -9 1168.50 398.004 2 18 -4 -8 4572.73 241.582 2 18 -4 -7 18493.3 235.693 2 18 -4 -6 11202.5 228.982 2 18 -4 -5 1876.59 204.026 2 18 -4 -4 16893.4 197.820 2 18 -4 -3 17683.0 211.410 2 18 -4 -2 23222.8 1651.46 2 -18 -4 -1 256.888 232.962 2 18 -4 2 2650.95 156.618 2 18 -4 3 19302.3 171.987 2 18 -4 4 999.879 164.444 2 18 -4 5 6359.38 165.207 2 -18 4 -6 242.263 166.290 2 18 -4 7 7869.23 244.796 2 18 -4 8 1323.97 481.269 2 18 -4 9 8239.68 619.609 2 18 -4 10 1906.79 374.126 2 18 -4 11 5728.99 186.380 2 -18 -4 -12 1092.96 162.047 2 18 4 13 10928.8 206.764 2 18 6 -12 363.583 321.947 2 18 -6 -11 3195.93 456.450 2 18 6 -10 771.522 482.142 2 -18 -6 9-33.1014 334.473 2 18 -6 -8 5528.41 249.269 2 18 -6 -7 22356.8 271.030 2 18 -6 -6 2721.42 246.632 2 18 -6 -5 5895.12 239.506 2 18 -6 -4 453.605 210.733 2 18 -6 -3 10649.9 295.623 2 18 -6 -2 301.575 804.814 2 18 -6 -1 35997.9 2195.71 2 18 -6 0 6654.06 2024.12 2 18 -6 1 518.403 290.662 2 18 -6 2 3813.33 178.565 2 18 -6 3 11450.3 198.630 2 18 -6 4 3541.56 199.442 2 -18 -6 -5 480.898 176.344 2 18 -6 6 2669.45 188.678 2 18 -6 7 17735.8 282.519 2 18 -6 8 857.386 317.918 2 18 -6 9 5112.52 442.722 2 18 -6 10 373.853 301.560 2 -18 -6 -11 3562.44 166.677 2 18 -8 -8 3737.28 212.664 2 18 -8 -7 5559.69 214.460 2 18 -8 -6 404.853 198.877 2 18 -8 -5 3248.90 218.065 2 18 -8 -4 5800.63 224.124 2 18 -8 -3 3458.00 306.618 2 18 -8 -2 1211.24 471.874 2 18 -8 -1 9304.06 802.175 2 18 -8 1 338.150 317.069 2 18 -8 2 2996.64 219.032 2 18 -8 3 6236.48 197.584 2 -18 -8 -4 4559.74 209.160 2 18 -8 5 1314.64 185.359 2 18 -8 6 7794.65 194.213 2 18 -8 7 3606.71 272.904 2 18 -8 8 484.681 271.591 2 19 1 -15 978.038 208.467 2 -19 1 14 739.135 181.726 2 19 1 -13 19320.1 322.101 2 19 -1 -12-1775.57 645.448 2 19 -1 -11 12755.9 719.163 2 19 -1 -10 2587.08 410.416 2 19 1 -9 745.421 249.270 2 19 1 -8 1991.50 189.846 2 19 1 -7 25697.0 197.428 2 19 1 -6 3197.79 156.115 2 19 -1 -5 606.180 145.084 2 19 -1 -4 9339.19 148.049 2 19 -1 -3 46271.2 182.810 2 19 -1 1 78110.2 413.867 2 19 -1 2 326.516 164.988 2 19 1 3 53530.1 190.655 2 19 -1 4 11415.1 145.991 2 19 -1 5 967.780 132.220 2 19 -1 6 1014.37 143.348 2 19 -1 7 29074.6 189.426 2 19 -1 8 912.534 918.622 2 19 1 11 11581.1 344.003 2 19 1 12 296.433 188.430 2 19 1 13 1916.23 179.314 2 19 1 14 330.745 160.937 2 19 3 -14 7055.80 202.725 2 19 3 -13 6032.21 261.097 2 19 -3 -11 17119.4 675.433 2 19 3 -10 4752.01 786.044 2 19 3 -9-33.5213 305.601 2 19 -3 -8 6778.50 229.588 2 19 -3 -7 1632.65 211.264 2 19 -3 -6 30225.4 237.190 2 19 -3 -5 5297.96 192.841 2 19 -3 -4 2008.50 182.695 2 19 -3 -3 34525.6 198.569 2 19 -3 1 15999.8 655.021 2 19 -3 2 67.0703 154.874 2 19 -3 3 17363.5 166.855 2 19 3 4 19031.1 166.625 2 19 3 5 2673.48 154.127 2 -19 3 -6 9386.50 159.445 2 19 -3 7 310.045 190.510 2 19 -3 8 4262.27 572.192 2 19 -3 11 4164.46 266.558 2 19 -3 12 1530.36 173.013 2 -19 -3 -13 237.472 168.184 2 19 5 -13 350.849 254.198 2 19 -5 -12 303.664 640.262 2 -19 5 11 463.028 728.712 2 19 5 -10 11934.9 779.964 2 -19 -5 9 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20 -2 8 12183.8 582.820 2 -20 2 -11 119.952 740.573 2 20 2 12 3921.88 188.540 2 20 2 13 57.9156 164.146 2 -20 2 -14 450.273 247.073 2 20 -4 -13 7384.86 470.356 2 20 -4 -12 2486.67 646.042 2 -20 -4 10 3880.45 348.216 2 20 -4 -9 22871.2 296.937 2 20 -4 -8 1782.75 238.745 2 20 -4 -7 8322.58 238.766 2 20 -4 -6 13782.2 231.755 2 20 -4 -5 5636.90 219.273 2 20 -4 -4 8713.52 216.071 2 20 -4 -3 3079.57 212.646 2 20 -4 1 42579.0 1610.06 2 20 -4 2 6634.18 188.859 2 20 -4 3 71.4079 168.522 2 20 -4 4 1342.77 169.727 2 20 -4 5 31438.8 206.112 2 -20 -4 -6 247.101 179.548 2 20 -4 7 16545.7 217.808 2 -20 4 -11 2490.37 449.832 2 20 -4 12 706.005 169.886 2 -20 -6 11 464.675 308.083 2 -20 -6 10-190.444 340.084 2 20 -6 -9 19390.6 262.424 2 20 -6 -8 816.988 229.506 2 20 -6 -7 5361.00 240.624 2 20 -6 -6 1021.92 232.787 2 20 -6 -5 7988.58 234.185 2 20 -6 -4 182.311 227.404 2 20 -6 -3 7017.45 279.166 2 20 6 1 17270.5 618.758 2 20 -6 2 1215.21 182.408 2 20 -6 3 900.239 188.184 2 20 -6 4 265.051 198.779 2 20 -6 5 37386.4 256.307 2 20 -6 6 23.6169 192.654 2 -20 -6 -7 9629.89 250.223 2 20 -6 8 3027.61 575.205 2 20 -8 -7 1344.62 206.356 2 20 -8 -6 6131.34 201.648 2 20 -8 -5 2074.08 205.283 2 20 -8 -4 78.7950 212.501 2 20 -8 -3 217.122 243.475 2 -20 -8 -1 6132.58 307.135 2 20 -8 2 6086.68 197.851 2 20 -8 3 57.9618 180.311 2 20 -8 4 5837.77 185.664 2 20 -8 5 8782.82 193.285 2 20 -8 6 875.625 201.064 2 21 1 -14-681.625 304.289 2 21 -1 -12 1999.86 589.340 2 21 1 -11 14464.5 413.622 2 21 1 -10 226.004 265.170 2 21 1 -9 20870.7 250.822 2 21 1 -8 2400.56 212.787 2 21 1 -7 678.945 201.572 2 21 1 -6 3172.22 210.849 2 21 -1 -5 58874.8 225.314 2 21 -1 -4 4159.64 168.601 2 21 -1 -3 631.403 163.520 2 21 -1 1 1974.28 1482.53 2 21 -1 2 625.518 177.723 2 21 -1 3 41977.3 239.081 2 21 -1 4 2283.29 188.470 2 21 -1 5 65450.0 233.356 2 21 1 6 3378.28 168.904 2 21 1 7 221.692 169.943 2 21 1 8 2286.55 290.434 2 -21 1 -12 40.0004 326.181 2 21 1 13 3398.04 172.673 2 21 -3 -13 426.802 617.560 2 -21 -3 10 1441.91 310.096 2 21 3 -9 12945.7 249.965 2 21 -3 -8 8914.31 236.354 2 21 -3 -7 366.497 223.250 2 21 -3 -6 2077.69 216.917 2 21 -3 -5 2404.97 214.553 2 21 -3 -4 12666.2 212.374 2 21 -3 -3 96.0209 186.673 2 21 3 1 2740.96 940.606 2 21 -3 2 18418.5 203.729 2 21 -3 3 3795.90 186.811 2 21 -3 4 2340.72 177.149 2 21 -3 5 6681.44 170.563 2 21 3 6 12633.7 177.149 2 21 -3 7 306.015 174.544 2 21 3 8 4484.86 259.328 2 -21 -3 -11 81.9437 594.153 2 21 -3 12 2110.85 193.056 2 -21 -3 -13 2671.38 175.529 2 -21 -5 12 5713.46 623.936 2 -21 -5 11 1707.55 392.677 2 -21 -5 10 690.890 328.034 2 21 -5 -9 4489.86 224.495 2 21 -5 -8 29348.3 271.656 2 21 -5 -7 289.499 232.789 2 21 -5 -6 14323.3 242.504 2 21 -5 -5 979.695 236.167 2 21 -5 -4 3078.53 219.875 2 21 -5 -3 3474.49 252.462 2 -21 -5 -1-2352.07 3048.55 2 21 -5 2 28182.6 218.467 2 21 -5 3 1497.31 182.193 2 21 -5 4 196.017 182.653 2 21 -5 5 485.161 186.854 2 21 -5 6 37587.8 239.835 2 21 -5 7 459.933 195.912 2 21 5 8 12699.4 342.632 2 21 -7 -9 1011.61 183.016 2 21 -7 -8 13163.0 236.054 2 21 -7 -7-250.921 222.430 2 21 -7 -6 5080.90 231.406 2 21 -7 -5 2499.42 225.970 2 21 -7 -4 6271.96 218.100 2 21 -7 -3 864.566 225.266 2 21 7 1-802.921 513.257 2 21 -7 2 11851.9 196.358 2 21 -7 3 769.827 196.642 2 21 -7 4 280.523 208.108 2 21 -7 5 5534.74 207.994 2 21 -7 6 14674.5 205.612 2 21 -7 7 122.262 194.938 2 21 -7 8 3208.96 264.139 2 22 0 -14 4817.49 436.662 2 22 0 -12 1689.13 359.343 2 22 0 -10 18715.2 327.898 2 22 0 -8 32026.3 336.538 2 22 0 -6 6593.77 271.410 2 22 0 -4 75650.4 321.959 2 22 0 -2 1288.14 319.161 2 22 0 0 48481.9 428.174 2 22 0 2 14873.4 256.560 2 22 0 4 7124.34 261.063 2 22 0 6 19031.2 257.268 2 22 0 8 5324.49 255.296 2 22 0 10 33177.6 548.332 2 -22 0 -12 1541.38 328.138 2 22 2 -12 1010.24 596.703 2 22 2 -11 1968.33 498.779 2 22 2 -10 6573.91 276.296 2 22 2 -9 42.9565 223.538 2 22 2 -8 5643.69 245.765 2 22 2 -7 16833.9 266.027 2 22 -2 -6 12555.3 238.531 2 22 -2 -5 265.817 208.304 2 22 -2 -4 54590.5 236.072 2 22 -2 -3 3304.53 185.315 2 -22 -2 -1 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