# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_II _shelx_title ' ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 434.48 _exptl_crystal_F_000 1616 _reflns_d_resolution_high ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z+1/2' _cell_length_a 25.0809(15) _cell_length_b 6.7251(4) _cell_length_c 18.9145(10) _cell_angle_alpha 90 _cell_angle_beta 97.658(6) _cell_angle_gamma 90 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8126.05 7854.62 214.99 o 4 0 0 21342.20 20089.60 282.96 o 6 0 0 948.76 962.94 46.12 o 8 0 0 23524.90 22669.50 365.68 o 10 0 0 28511.00 28888.70 462.55 o 12 0 0 161.37 240.64 27.20 o 14 0 0 12773.30 13268.50 225.53 o 16 0 0 28940.40 29294.50 487.54 o 18 0 0 6300.68 6529.17 172.44 o 20 0 0 16.07 37.51 35.90 < 22 0 0 4165.82 3823.75 263.53 o 24 0 0 367.63 427.87 96.52 o 26 0 0 512.72 412.57 91.42 o 28 0 0 33.43 -58.31 69.41 < 30 0 0 461.85 685.51 143.22 o 32 0 0 556.60 511.49 153.63 o 1 1 0 1543.54 1409.84 29.53 o 3 1 0 24887.40 24289.00 280.87 o 5 1 0 100360.00 101526.00 1136.77 o 7 1 0 4287.15 4661.57 65.88 o 9 1 0 10783.00 10663.60 114.67 o 11 1 0 8107.36 8333.01 111.37 o 13 1 0 452.64 463.59 27.81 o 15 1 0 118.11 74.51 20.50 o 17 1 0 2498.03 2560.54 78.23 o 19 1 0 28.42 76.81 27.90 < 21 1 0 15.40 -14.60 29.20 < 23 1 0 96.11 65.91 38.71 < 25 1 0 299.57 218.63 52.51 o 27 1 0 3.93 33.60 52.81 < 29 1 0 6.84 31.90 64.71 < 31 1 0 173.54 159.92 77.71 < 0 2 0 178433.00 188772.00 3097.59 o 2 2 0 73275.40 72956.30 930.00 o 4 2 0 3418.39 3456.47 67.26 o 6 2 0 25744.80 25077.00 269.67 o 8 2 0 21164.20 21940.80 232.42 o 10 2 0 211.73 176.33 18.50 o 12 2 0 6754.83 6984.39 95.90 o 14 2 0 1360.63 1401.62 45.71 o 16 2 0 2014.57 2000.30 59.72 o 18 2 0 1370.92 1291.54 63.52 o 20 2 0 1656.90 1754.79 73.02 o 22 2 0 929.91 1118.03 81.92 o 24 2 0 2907.08 2953.52 127.44 o 26 2 0 1731.29 1713.03 135.63 o 28 2 0 466.97 579.49 97.12 o 30 2 0 242.58 68.01 91.21 < 1 3 0 3570.23 3448.34 64.65 o 3 3 0 392.45 317.56 23.50 o 5 3 0 6190.78 6054.83 94.51 o 7 3 0 1906.00 2141.09 53.72 o 9 3 0 5429.98 5460.73 95.98 o 11 3 0 2109.53 2180.46 58.42 o 13 3 0 3990.63 4040.33 81.15 o 15 3 0 1335.28 1321.95 51.51 o 17 3 0 152.35 136.12 31.90 o 19 3 0 723.09 782.35 56.31 o 21 3 0 1263.57 1325.91 81.42 o 23 3 0 1662.12 1573.90 85.32 o 25 3 0 398.43 352.86 77.91 o 27 3 0 295.68 378.66 86.81 o 29 3 0 689.37 828.15 114.32 o 0 4 0 39.41 46.71 27.10 < 2 4 0 919.13 969.54 43.31 o 4 4 0 11296.20 11258.00 168.66 o 6 4 0 180.13 182.43 25.20 o 8 4 0 12.68 4.40 19.20 < 10 4 0 3259.91 3230.74 143.87 o 12 4 0 563.49 586.11 47.41 o 14 4 0 871.93 922.80 51.21 o 16 4 0 35.42 -6.50 27.70 < 18 4 0 10.66 20.10 38.61 < 20 4 0 519.08 602.60 64.71 o 22 4 0 7.00 59.61 61.21 < 24 4 0 7.00 34.70 60.91 < 26 4 0 488.54 704.62 145.42 o 28 4 0 113.64 137.62 108.32 < 1 5 0 1822.18 1935.32 103.33 o 3 5 0 4804.53 4565.20 116.47 o 5 5 0 10.68 -18.80 26.90 < 7 5 0 3151.26 3294.02 125.35 o 9 5 0 747.39 718.95 45.51 o 11 5 0 1344.39 1525.68 57.01 o 13 5 0 1712.64 1805.99 128.93 o 15 5 0 1625.34 1762.86 89.72 o 17 5 0 519.50 615.31 68.81 o 19 5 0 535.09 797.64 113.62 o 21 5 0 1083.84 1216.15 134.33 o 23 5 0 113.65 189.53 91.81 < 25 5 0 48.26 25.00 74.81 < 0 6 0 896.43 754.36 110.62 o 2 6 0 4.64 -14.00 34.60 < 4 6 0 2.86 -32.20 32.20 < 6 6 0 15.14 -32.40 35.50 < 8 6 0 291.54 264.04 46.21 o 10 6 0 107.17 127.92 41.31 o 12 6 0 19.25 2.50 50.11 < 14 6 0 0.63 -50.91 61.31 < 16 6 0 63.08 8.40 62.51 < 18 6 0 0.22 9.90 60.61 < 20 6 0 0.02 -4.10 74.11 < 22 6 0 4.54 -68.31 82.61 < 1 7 0 489.18 426.17 83.61 o 3 7 0 253.64 205.73 75.61 < 5 7 0 2254.84 2233.15 143.64 o 7 7 0 3.87 -52.11 52.11 < 9 7 0 615.63 705.02 88.42 o 11 7 0 271.43 335.45 72.11 o 13 7 0 153.33 119.52 80.01 < 15 7 0 11.91 26.20 67.31 < 17 7 0 234.31 234.93 80.81 < 19 7 0 306.70 357.36 116.72 o 0 8 0 702.66 679.42 168.43 o 2 8 0 2.83 -78.81 78.81 < 4 8 0 233.55 127.22 101.42 < 6 8 0 100.65 148.72 80.21 < 8 8 0 41.27 33.70 74.91 < 10 8 0 185.74 167.92 76.31 < 12 8 0 17.42 45.81 93.61 < -31 1 1 492.77 524.69 102.72 o -29 1 1 569.70 670.51 97.92 o -27 1 1 230.57 310.15 71.61 o -25 1 1 344.01 324.95 55.11 o -23 1 1 1899.35 1662.37 94.33 o -21 1 1 2208.86 2278.14 94.43 o -19 1 1 1855.96 1817.97 66.32 o -17 1 1 2254.35 2082.89 61.82 o -15 1 1 1516.25 1479.58 42.71 o -13 1 1 6606.64 6573.95 101.61 o -11 1 1 4082.86 4015.93 72.46 o -9 1 1 35.25 33.00 9.10 o -7 1 1 6116.31 5879.41 76.93 o -5 1 1 26924.10 25076.30 282.88 o -3 1 1 2169.61 2032.72 34.34 o -1 1 1 11348.30 11722.80 141.43 o 1 1 1 12436.10 12629.40 142.89 o 3 1 1 5809.77 5574.59 75.69 o 5 1 1 10670.40 10399.10 141.79 o 7 1 1 387.92 478.01 18.00 o 9 1 1 8654.18 8271.58 96.58 o 11 1 1 21034.80 21283.00 236.45 o 13 1 1 5357.10 5585.06 85.08 o 15 1 1 1889.52 1901.19 47.82 o 17 1 1 2653.36 2728.34 102.54 o 19 1 1 3831.31 3754.67 98.05 o 21 1 1 2039.33 1901.29 84.83 o 23 1 1 806.26 958.49 75.92 o 25 1 1 14.04 13.70 41.81 < 27 1 1 410.89 330.45 75.21 o 29 1 1 607.16 805.54 108.02 o 31 1 1 209.45 142.32 92.71 < -30 2 1 22.11 14.50 70.51 < -28 2 1 100.15 41.71 63.01 < -26 2 1 678.76 660.62 126.42 o -24 2 1 2903.78 2728.45 122.84 o -22 2 1 13.93 36.30 34.00 < -20 2 1 1164.77 1129.77 65.82 o -18 2 1 2801.70 2764.22 87.64 o -16 2 1 1132.95 1184.10 55.21 o -14 2 1 3172.56 3305.42 66.63 o -12 2 1 5.09 1.30 14.00 < -10 2 1 13277.70 13531.90 140.41 o -8 2 1 4983.00 5089.69 64.17 o -6 2 1 198.60 219.64 16.10 o -4 2 1 3407.73 3349.55 62.96 o -2 2 1 9830.58 9738.33 137.87 o 0 2 1 24562.10 24104.50 284.69 o 2 2 1 108043.00 111531.00 1302.30 o 4 2 1 35824.80 35754.50 466.60 o 6 2 1 5414.36 5547.36 92.11 o 8 2 1 16498.70 17993.60 214.25 o 10 2 1 3120.28 3389.28 67.34 o 12 2 1 3982.27 4341.11 77.75 o 14 2 1 7740.99 7674.18 116.82 o 16 2 1 1443.99 1306.17 54.62 o 18 2 1 3.81 3.70 25.20 < 20 2 1 125.71 76.81 33.20 < 22 2 1 935.23 858.38 75.72 o 24 2 1 368.24 332.25 58.21 o 26 2 1 196.97 226.73 72.51 o 28 2 1 432.58 497.78 93.02 o 30 2 1 1.81 23.50 62.11 < -29 3 1 39.35 20.60 72.61 < -27 3 1 422.83 428.07 85.91 o -25 3 1 462.31 531.39 96.32 o -23 3 1 910.78 866.87 81.12 o -21 3 1 234.96 313.85 48.61 o -19 3 1 91.26 92.01 33.00 < -17 3 1 995.50 961.72 52.81 o -15 3 1 6131.36 6385.91 114.99 o -13 3 1 851.19 831.29 37.51 o -11 3 1 3419.02 3211.18 61.03 o -9 3 1 7921.63 8035.59 98.22 o -7 3 1 2421.88 2393.88 65.23 o -5 3 1 132.73 107.12 17.30 o -3 3 1 9382.55 9180.17 127.52 o -1 3 1 309.31 312.86 22.60 o 1 3 1 879.84 873.45 32.11 o 3 3 1 5742.05 5488.05 101.31 o 5 3 1 675.82 629.65 26.91 o 7 3 1 15977.00 16069.70 214.73 o 9 3 1 25.89 20.60 19.90 < 11 3 1 134.66 103.62 23.40 o 13 3 1 760.14 735.16 41.51 o 15 3 1 279.79 224.74 33.11 o 17 3 1 451.03 479.48 40.31 o 19 3 1 6.03 -6.10 30.70 < 21 3 1 40.36 6.10 33.30 < 23 3 1 147.20 107.12 50.11 < 25 3 1 2177.30 2223.62 243.97 o 27 3 1 377.91 516.38 91.91 o 29 3 1 17.42 95.11 72.81 < -28 4 1 122.31 124.52 108.82 < -26 4 1 670.84 647.21 99.12 o -24 4 1 6.86 -53.61 59.61 < -22 4 1 465.73 369.96 77.81 o -20 4 1 2194.16 2278.18 175.25 o -18 4 1 1513.21 1531.99 84.22 o -16 4 1 1951.09 2073.42 84.13 o -14 4 1 409.33 356.26 48.81 o -12 4 1 1446.29 1506.02 56.52 o -10 4 1 2759.38 2866.32 123.35 o -8 4 1 4852.68 4861.12 89.46 o -6 4 1 29.95 20.20 18.70 < -4 4 1 7126.86 7414.08 120.52 o -2 4 1 1585.65 1516.51 49.52 o 0 4 1 53.28 44.51 19.20 < 2 4 1 22655.60 22871.80 255.97 o 4 4 1 9563.10 9676.56 144.39 o 6 4 1 17692.50 17816.60 226.10 o 8 4 1 1803.73 2019.98 50.52 o 10 4 1 3207.55 3212.71 100.55 o 12 4 1 225.78 242.24 34.01 o 14 4 1 42.55 41.21 28.80 < 16 4 1 201.04 166.02 35.41 o 18 4 1 116.17 105.21 39.01 < 20 4 1 788.86 753.95 68.81 o 22 4 1 350.02 308.35 74.41 o 24 4 1 48.39 11.30 68.51 < 26 4 1 7.80 73.61 102.71 < 28 4 1 89.21 115.12 126.82 < -25 5 1 42.14 35.90 86.41 < -23 5 1 438.69 283.45 99.32 < -21 5 1 141.91 216.53 90.11 < -19 5 1 374.91 373.66 93.92 o -17 5 1 15.35 24.30 46.91 < -15 5 1 123.30 63.41 37.01 < -13 5 1 389.26 353.56 43.31 o -11 5 1 28.01 -15.00 28.80 < -9 5 1 250.02 200.33 35.91 o -7 5 1 428.44 378.67 42.61 o -5 5 1 626.05 623.42 51.11 o -3 5 1 1.76 46.11 29.00 < -1 5 1 157.55 155.42 34.81 o 1 5 1 1086.34 1173.09 74.52 o 3 5 1 1502.50 1430.91 67.82 o 5 5 1 933.01 1010.73 71.42 o 7 5 1 6.19 56.21 27.30 < 9 5 1 4224.06 4172.54 116.96 o 11 5 1 459.54 330.56 45.41 o 13 5 1 11.09 15.30 34.90 < 15 5 1 410.34 506.68 66.61 o 17 5 1 558.28 518.29 65.31 o 19 5 1 664.65 503.19 98.72 o 21 5 1 83.04 68.41 81.11 < 23 5 1 54.39 111.71 89.21 < 25 5 1 49.69 -82.71 82.71 < -22 6 1 105.17 94.51 87.71 < -20 6 1 104.29 45.51 80.61 < -18 6 1 265.56 340.15 79.31 o -16 6 1 358.59 229.64 71.01 o -14 6 1 2078.32 1978.15 119.53 o -12 6 1 984.83 1249.86 106.42 o -10 6 1 454.36 500.79 52.91 o -8 6 1 19.10 -10.80 33.10 < -6 6 1 1718.86 1605.34 83.02 o -4 6 1 73.80 41.91 36.51 < -2 6 1 4017.27 3959.64 196.29 o 0 6 1 3830.71 3553.60 126.96 o 2 6 1 536.82 487.99 60.01 o 4 6 1 8949.00 8739.32 258.92 o 6 6 1 858.43 680.04 64.31 o 8 6 1 5107.24 5243.77 150.68 o 10 6 1 7.37 -12.80 33.10 < 12 6 1 734.14 604.81 86.02 o 14 6 1 1620.60 1551.68 212.55 o 16 6 1 641.59 882.46 102.92 o 18 6 1 539.90 327.05 78.21 o 20 6 1 425.87 396.76 103.92 o 22 6 1 124.54 86.41 96.01 < -19 7 1 2.35 7.80 88.21 < -17 7 1 40.93 54.11 70.41 < -15 7 1 47.42 29.20 67.41 < -13 7 1 29.82 -34.60 76.31 < -11 7 1 8.34 30.50 56.81 < -9 7 1 211.23 262.24 70.01 o -7 7 1 45.28 52.11 59.51 < -5 7 1 74.67 50.11 58.11 < -3 7 1 24.67 11.20 66.11 < -1 7 1 75.77 -12.70 60.31 < 1 7 1 113.41 112.72 70.91 < 3 7 1 418.66 443.37 84.21 o 5 7 1 578.33 762.43 96.82 o 7 7 1 52.48 16.20 64.71 < 9 7 1 23.37 48.01 64.31 < 11 7 1 5.07 3.90 66.31 < 13 7 1 2.63 14.20 76.81 < 15 7 1 41.25 51.71 82.01 < 17 7 1 1.31 29.90 67.81 < 19 7 1 95.79 -3.20 108.32 < -12 8 1 47.18 -81.31 81.31 < -10 8 1 30.75 -33.80 63.51 < -8 8 1 703.06 862.95 139.73 o -6 8 1 135.18 311.55 92.31 o -4 8 1 803.42 777.04 132.22 o -2 8 1 63.08 19.80 71.21 < 0 8 1 10.49 21.50 73.71 < 2 8 1 48.97 47.31 74.71 < 4 8 1 1.95 -32.90 72.11 < 6 8 1 1088.49 888.78 117.62 o 8 8 1 133.79 181.83 94.11 < 10 8 1 1006.83 763.45 148.93 o 12 8 1 83.40 257.04 123.72 < -32 0 2 5.43 -90.11 90.11 < -30 0 2 6.07 43.31 86.31 < -28 0 2 46.87 74.51 84.31 < -26 0 2 2171.25 2348.38 231.47 o -24 0 2 608.63 485.89 87.62 o -22 0 2 2982.61 2950.34 165.76 o -20 0 2 1178.94 1193.19 87.22 o -18 0 2 3193.61 2630.24 180.99 o -16 0 2 4369.59 4052.97 130.79 o -14 0 2 5468.40 5539.85 112.90 o -12 0 2 22990.20 21499.40 306.09 o -10 0 2 15363.40 14263.90 210.47 o -8 0 2 94.34 195.43 21.40 o -6 0 2 10513.90 10006.40 176.02 o -4 0 2 23967.00 23794.50 418.21 o -2 0 2 33744.80 32030.10 595.78 o 0 0 2 890.28 763.82 18.82 o 2 0 2 53447.80 54978.50 927.53 o 4 0 2 55659.60 56348.80 949.54 o 6 0 2 1804.34 1886.15 62.34 o 8 0 2 8412.29 8467.40 157.82 o 10 0 2 12044.10 14376.30 281.56 o 12 0 2 69768.40 71733.40 1407.31 o 14 0 2 572.80 745.86 51.31 o 16 0 2 3820.29 3827.29 114.57 o 18 0 2 2809.57 2636.30 195.38 o 20 0 2 3022.25 3083.16 142.96 o 22 0 2 2154.82 2019.83 201.16 o 24 0 2 1284.54 949.12 111.63 o 26 0 2 85.56 118.32 69.81 < 28 0 2 1024.57 1300.46 224.04 o 30 0 2 193.87 292.84 116.22 < -31 1 2 1012.07 1137.32 203.54 o -29 1 2 0.36 -9.80 57.81 < -27 1 2 107.48 137.32 63.41 < -25 1 2 522.78 508.49 63.91 o -23 1 2 693.38 689.73 77.81 o -21 1 2 761.40 805.36 60.61 o -19 1 2 326.10 327.85 34.91 o -17 1 2 327.44 266.35 31.51 o -15 1 2 90.65 110.12 20.60 o -13 1 2 2408.24 2332.82 58.13 o -11 1 2 3176.40 3390.98 54.74 o -9 1 2 9849.32 9722.99 117.25 o -7 1 2 137.22 104.82 14.80 o -5 1 2 7029.08 6933.49 80.39 o -3 1 2 21826.00 21358.90 217.84 o -1 1 2 104.54 98.92 8.30 o 1 1 2 4859.71 4567.18 57.33 o 3 1 2 16052.10 15574.50 185.28 o 5 1 2 17687.30 17803.90 214.01 o 7 1 2 5460.98 5831.92 79.01 o 9 1 2 15425.30 15924.50 174.73 o 11 1 2 3185.86 3235.88 58.64 o 13 1 2 256.32 302.75 23.50 o 15 1 2 4481.22 4842.03 86.96 o 17 1 2 326.73 421.47 50.11 o 19 1 2 2807.36 2814.92 95.54 o 21 1 2 6.32 8.80 34.90 < 23 1 2 956.59 968.50 77.92 o 25 1 2 22.79 17.00 41.31 < 27 1 2 576.35 383.47 79.71 o 29 1 2 8.83 -7.90 60.61 < 31 1 2 153.35 76.71 72.21 < -30 2 2 79.89 103.71 70.31 < -28 2 2 938.60 1080.51 128.23 o -26 2 2 274.43 253.14 73.11 o -24 2 2 35.55 68.21 39.91 < -22 2 2 5924.08 6032.35 152.39 o -20 2 2 2343.94 2307.28 121.34 o -18 2 2 4194.51 4128.43 97.35 o -16 2 2 286.30 276.15 27.20 o -14 2 2 20.77 -10.10 13.80 < -12 2 2 4903.08 4866.53 69.26 o -10 2 2 3235.03 3080.48 50.03 o -8 2 2 237.83 164.63 14.00 o -6 2 2 20982.80 20238.70 224.99 o -4 2 2 10521.20 10242.00 131.64 o -2 2 2 1823.37 1655.28 39.12 o 0 2 2 8815.73 8797.28 120.18 o 2 2 2 8046.15 7999.13 110.53 o 4 2 2 4152.12 4023.24 60.96 o 6 2 2 6013.01 5885.01 90.72 o 8 2 2 212.29 316.75 23.40 o 10 2 2 31184.20 32137.20 387.75 o 12 2 2 989.34 1176.11 45.31 o 14 2 2 5931.57 6209.71 102.48 o 16 2 2 64.92 49.31 21.90 < 18 2 2 2912.19 3033.33 121.65 o 20 2 2 983.62 1075.33 70.42 o 22 2 2 230.17 194.03 49.31 o 24 2 2 12.23 50.31 44.31 < 26 2 2 1205.91 1102.04 112.62 o 28 2 2 344.64 315.85 112.82 < 30 2 2 157.65 126.72 77.61 < -29 3 2 160.35 261.04 83.31 o -27 3 2 305.35 217.03 67.01 o -25 3 2 274.31 261.34 60.01 o -23 3 2 1923.93 1833.30 113.43 o -21 3 2 18.38 37.51 35.70 < -19 3 2 984.45 992.52 60.91 o -17 3 2 1490.26 1462.60 61.42 o -15 3 2 828.53 874.29 44.81 o -13 3 2 155.74 166.93 20.20 o -11 3 2 2955.75 2860.52 51.53 o -9 3 2 613.83 628.14 28.41 o -7 3 2 6127.53 6075.89 86.89 o -5 3 2 1355.07 1159.51 38.21 o -3 3 2 1130.23 1158.98 42.01 o -1 3 2 26.48 22.50 13.30 < 1 3 2 2844.32 2800.34 54.33 o 3 3 2 28.15 8.00 12.20 < 5 3 2 4263.73 4358.86 67.65 o 7 3 2 183.60 154.12 20.50 o 9 3 2 528.63 671.44 35.71 o 11 3 2 7520.17 7834.82 134.24 o 13 3 2 533.98 632.12 38.91 o 15 3 2 1402.84 1489.70 62.32 o 17 3 2 11.03 28.40 25.70 < 19 3 2 7.37 -4.30 29.90 < 21 3 2 282.65 252.24 50.81 o 23 3 2 262.74 276.24 57.61 o 25 3 2 336.22 276.04 91.41 o 27 3 2 400.37 210.73 76.81 < 29 3 2 211.80 167.12 78.01 < -28 4 2 145.83 112.12 78.71 < -26 4 2 1.12 -7.30 66.41 < -24 4 2 1017.09 1091.52 112.72 o -22 4 2 3.67 4.80 56.61 < -20 4 2 136.19 185.13 50.21 o -18 4 2 87.46 91.91 40.41 < -16 4 2 323.86 343.86 41.11 o -14 4 2 2068.50 2236.02 69.22 o -12 4 2 205.48 204.13 26.40 o -10 4 2 238.40 204.73 26.50 o -8 4 2 7420.42 7419.28 123.92 o -6 4 2 377.01 363.17 36.51 o -4 4 2 13.04 -8.90 20.20 < -2 4 2 1320.44 1389.72 47.71 o 0 4 2 4.45 -15.90 17.70 < 2 4 2 13423.40 13722.60 184.94 o 4 4 2 217.27 150.62 22.30 o 6 4 2 5609.25 5727.41 100.48 o 8 4 2 2988.99 2803.90 75.43 o 10 4 2 32.69 6.70 21.10 < 12 4 2 2146.00 2110.02 67.22 o 14 4 2 892.19 992.41 59.81 o 16 4 2 1997.85 2081.72 79.92 o 18 4 2 34.92 21.50 37.41 < 20 4 2 675.41 621.41 60.71 o 22 4 2 330.21 359.46 131.72 < 24 4 2 620.26 486.39 120.32 o 26 4 2 5.58 -23.20 142.52 < 28 4 2 34.33 -22.20 100.01 < -25 5 2 594.87 472.18 130.42 o -23 5 2 49.99 -12.40 80.41 < -21 5 2 450.15 568.89 107.42 o -19 5 2 194.64 204.23 86.01 < -17 5 2 739.57 784.45 90.72 o -15 5 2 563.80 564.60 55.71 o -13 5 2 498.25 527.89 48.11 o -11 5 2 277.59 267.44 40.11 o -9 5 2 138.73 95.61 31.80 o -7 5 2 202.21 158.02 33.41 o -5 5 2 1500.00 1517.72 74.62 o -3 5 2 2982.50 3018.40 141.66 o -1 5 2 4808.09 5056.21 123.08 o 1 5 2 3088.19 3088.67 103.55 o 3 5 2 2525.67 2422.33 150.46 o 5 5 2 65.60 52.61 27.00 < 7 5 2 1346.74 1412.47 78.52 o 9 5 2 2203.82 2432.70 74.52 o 11 5 2 1206.21 1220.39 85.92 o 13 5 2 981.78 1107.94 80.52 o 15 5 2 972.41 1088.03 81.92 o 17 5 2 3691.37 3574.83 135.65 o 19 5 2 746.28 850.16 118.72 o 21 5 2 350.29 257.54 89.61 < 23 5 2 79.09 41.01 72.91 < 25 5 2 149.65 330.85 136.12 < -22 6 2 90.91 24.50 85.11 < -20 6 2 4.65 -22.30 80.61 < -18 6 2 0.18 13.30 58.91 < -16 6 2 299.23 241.54 70.01 o -14 6 2 174.84 86.21 56.21 < -12 6 2 188.94 197.43 61.01 o -10 6 2 40.99 -18.30 36.10 < -8 6 2 3.65 11.60 32.60 < -6 6 2 138.20 40.51 38.41 < -4 6 2 0.09 -3.20 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124.32 < -14 4 20 119.21 45.41 87.41 < -12 4 20 3.30 -74.11 74.11 < -10 4 20 17.20 11.60 78.81 < -8 4 20 432.57 317.05 152.73 < -6 4 20 12.47 97.61 108.92 < -4 4 20 138.59 62.31 99.91 < -2 4 20 602.51 760.53 152.93 o 0 4 20 179.07 -25.30 94.71 < 2 4 20 45.97 305.44 192.53 < 4 4 20 86.53 177.73 177.73 < 6 4 20 1.84 -142.52 151.82 < 8 4 20 229.72 303.64 207.33 < -5 5 20 61.66 75.71 96.41 < -3 5 20 135.44 103.71 109.22 < -1 5 20 56.06 61.11 138.82 < -19 1 21 193.50 223.23 79.81 < -17 1 21 413.46 360.56 85.41 o -15 1 21 443.13 488.78 90.61 o -13 1 21 298.33 161.73 69.91 < -11 1 21 808.43 796.35 101.82 o -9 1 21 731.15 678.62 93.32 o -7 1 21 460.61 409.47 82.01 o -5 1 21 549.34 404.47 151.23 < -3 1 21 442.56 375.46 121.52 o -1 1 21 695.09 761.84 152.53 o 1 1 21 750.39 831.05 153.63 o 3 1 21 428.82 393.56 123.02 o 5 1 21 598.22 167.03 234.14 < 7 1 21 528.26 490.98 136.82 o 9 1 21 152.82 82.51 100.82 < 11 1 21 341.46 338.25 126.22 < -18 2 21 12.23 -63.11 63.11 < -16 2 21 405.15 336.55 89.91 o 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122.42 < 0 2 23 27.85 48.21 129.62 < 2 2 23 22.24 147.42 123.12 < 4 2 23 138.19 237.43 128.22 < -7 3 23 502.64 538.69 220.34 < -5 3 23 34.28 -24.30 98.21 < -3 3 23 356.06 358.06 148.62 < -10 0 24 731.85 778.14 193.43 o -8 0 24 9.78 179.52 161.02 < -6 0 24 1698.65 1458.94 301.77 o -4 0 24 42.18 87.01 153.62 < -2 0 24 515.70 401.77 186.93 < 0 0 24 462.14 375.86 201.83 < 2 0 24 909.40 685.03 227.74 o -9 1 24 28.79 2.30 82.51 < -7 1 24 28.61 -3.70 95.51 < -5 1 24 1576.95 1918.54 248.46 o -3 1 24 22.57 15.30 158.32 < -1 1 24 446.91 324.95 138.32 < 1 1 24 20.35 159.42 119.02 <