# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 229.70 _exptl_crystal_F_000 628 _reflns_d_resolution_high ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 9.0154(18) _cell_length_b 7.6122(15) _cell_length_c 17.138(3) _cell_angle_alpha 90 _cell_angle_beta 104.38(3) _cell_angle_gamma 90 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3546.25 3624.08 43.12 o 3 0 0 39.47 37.01 3.71 o 4 0 0 2302.69 2235.57 28.28 o 5 0 0 2637.16 2799.90 38.61 o 6 0 0 724.60 761.10 14.04 o 7 0 0 1117.72 1214.71 76.42 o 8 0 0 2636.68 2892.77 133.69 o 9 0 0 179.90 174.81 11.13 o 10 0 0 51.02 231.87 20.36 o 11 0 0 297.71 419.41 26.58 o 1 1 0 1344.36 1168.28 24.57 o 1 -1 0 1245.10 1155.14 51.35 o 2 1 0 6162.19 6726.15 102.70 o 2 -1 0 6477.10 7047.28 85.35 o 3 1 0 2618.28 2564.12 40.52 o 3 -1 0 2598.52 2503.04 31.39 o 4 1 0 7560.96 8144.46 131.98 o 4 -1 0 7562.62 8109.56 125.56 o 5 1 0 2570.65 2554.29 42.02 o 5 -1 0 2493.80 2455.40 32.49 o 6 1 0 976.91 1106.80 102.90 o 6 -1 0 1026.37 1091.96 21.76 o 7 1 0 423.00 436.36 12.74 o 7 -1 0 398.71 421.92 14.14 o 8 1 0 164.78 178.42 8.32 o 8 -1 0 166.46 170.09 8.93 o 9 1 0 164.45 167.79 15.24 o 9 -1 0 137.32 127.97 13.54 o 10 1 0 689.43 898.80 81.54 o 10 -1 0 734.85 946.94 139.10 o 11 1 0 221.55 246.91 30.09 o 11 -1 0 216.61 235.28 16.05 o 0 -2 0 1234.52 1208.80 26.68 o 1 2 0 6859.90 7423.47 163.17 o 1 -2 0 6925.20 7507.11 110.62 o 2 2 0 4052.85 4030.56 88.56 o 2 -2 0 4174.66 4269.35 65.99 o 3 2 0 2473.37 2392.62 83.94 o 3 -2 0 2449.48 2495.02 43.02 o 4 2 0 204.99 203.49 9.13 o 4 -2 0 205.99 216.53 5.11 o 5 2 0 91.77 105.10 5.22 o 5 -2 0 84.22 95.07 7.32 o 6 2 0 1069.59 1048.93 17.25 o 6 -2 0 1110.26 1097.37 17.95 o 7 2 0 2004.21 2029.67 32.09 o 7 -2 0 2011.07 2021.05 27.58 o 8 2 0 1155.60 1168.08 18.85 o 8 -2 0 1201.81 1285.92 45.03 o 9 2 0 1362.68 1429.74 31.69 o 9 -2 0 1280.60 1321.22 50.35 o 10 2 0 438.15 433.86 25.98 o 10 -2 0 403.90 508.27 69.90 o 11 2 0 17.97 15.95 8.32 < 11 -2 0 11.79 99.79 93.27 < 1 -3 0 1560.13 1694.00 16.05 o 2 3 0 1971.24 2002.09 47.64 o 2 -3 0 2127.19 2176.19 38.31 o 3 3 0 3334.67 3269.26 83.84 o 3 -3 0 3418.59 3408.06 58.87 o 4 3 0 904.54 871.82 34.50 o 4 -3 0 1008.43 1003.10 23.27 o 5 3 0 2175.92 2243.59 27.28 o 5 -3 0 2049.84 2093.35 28.48 o 6 3 0 994.88 958.37 14.24 o 6 -3 0 946.37 912.14 13.94 o 7 3 0 220.12 210.31 6.12 o 7 -3 0 216.12 228.06 17.95 o 8 3 0 168.06 165.88 5.72 o 8 -3 0 164.70 228.66 36.81 o 9 3 0 31.10 37.91 6.62 o 9 -3 0 21.73 25.98 20.96 < 10 -3 0 488.70 586.80 61.38 o 0 -4 0 7059.79 7183.58 92.27 o 1 -4 0 5512.61 5742.21 51.15 o 2 -4 0 2184.91 2337.16 21.56 o 3 -4 0 89.07 103.90 5.11 o 4 -4 0 410.66 415.00 9.13 o 5 -4 0 454.14 428.74 15.95 o 6 -4 0 494.47 874.53 139.00 o 7 -4 0 1419.71 1438.36 39.51 o 8 -4 0 628.42 815.06 54.16 o 9 -4 0 912.33 914.45 28.48 o 10 -4 0 550.40 603.55 48.64 o 1 -5 0 453.66 446.79 6.52 o 2 -5 0 870.68 872.32 9.43 o 3 -5 0 569.45 548.29 10.03 o 4 -5 0 597.03 585.59 10.63 o 5 -5 0 299.06 299.07 14.54 o 6 -5 0 1753.52 1685.47 54.06 o 7 -5 0 675.09 746.96 100.89 o 8 -5 0 17.22 401.16 25.67 o 9 -5 0 321.70 365.16 28.08 o 0 -6 0 545.73 525.02 10.73 o 1 -6 0 1917.02 1887.76 20.06 o 2 -6 0 1535.80 1525.21 16.35 o 3 -6 0 1423.08 1420.71 30.29 o 4 -6 0 152.05 145.72 9.03 o 5 -6 0 221.48 280.21 57.87 o 6 -6 0 546.87 587.00 55.16 o 7 -6 0 916.04 927.48 29.59 o 8 -6 0 723.98 663.12 33.60 o 9 -6 0 485.07 523.72 49.24 o 1 -7 0 703.72 688.49 10.73 o 2 -7 0 124.62 120.95 4.31 o 3 -7 0 1098.01 1123.25 19.06 o 4 -7 0 888.67 909.43 16.55 o 5 -7 0 785.01 725.90 26.48 o 6 -7 0 901.28 946.04 30.29 o 7 -7 0 758.24 828.20 82.14 o 8 -7 0 38.17 31.69 12.24 < 0 -8 0 1940.68 1939.51 30.99 o 1 -8 0 1546.70 1518.49 18.95 o 2 -8 0 589.33 578.37 8.73 o 3 -8 0 31.44 32.39 4.91 o 4 -8 0 50.94 45.13 4.71 o 5 -8 0 15.87 18.05 8.73 < 6 -8 0 371.95 386.02 20.06 o 1 -9 0 267.51 278.71 15.95 o 2 -9 0 799.61 808.14 17.75 o 3 -9 0 807.57 846.95 18.55 o 4 -9 0 625.85 637.14 21.66 o -11 0 1 1368.84 1397.84 120.85 o -10 0 1 726.48 739.94 17.75 o -9 0 1 1.56 1.91 5.11 < -8 0 1 250.95 273.49 13.94 o -7 0 1 69.87 373.68 229.96 < -6 0 1 19.58 25.17 8.32 o -5 0 1 1700.78 1660.70 23.07 o -4 0 1 4434.60 4476.65 58.57 o -3 0 1 5038.77 5183.09 56.76 o -2 0 1 385.77 453.31 7.52 o 2 0 1 1853.60 1908.02 22.67 o 3 0 1 14.99 21.06 2.51 o 4 0 1 2712.80 2789.67 30.19 o 5 0 1 2662.91 2597.81 29.28 o 6 0 1 4497.64 4678.73 55.66 o 7 0 1 1840.70 1893.38 35.30 o 8 0 1 1659.78 1817.16 90.06 o 9 0 1 29.45 85.95 67.19 < 10 0 1 286.45 396.85 78.93 o 11 0 1 154.02 168.19 13.24 o -11 -1 1 91.24 221.44 25.27 o -10 1 1 301.43 522.31 44.83 o -10 -1 1 274.31 768.32 51.55 o -9 1 1 212.17 279.81 49.14 o -9 -1 1 243.26 256.84 9.33 o -8 1 1 1090.10 1049.44 23.97 o -8 -1 1 1104.84 1106.90 21.66 o -7 1 1 1069.45 1055.65 22.36 o -7 -1 1 1121.48 1111.01 19.26 o -6 1 1 1933.31 1866.70 37.11 o -6 -1 1 1858.35 1816.96 33.20 o -5 1 1 2206.20 2208.29 39.82 o -5 -1 1 2192.42 2158.44 28.38 o -4 1 1 1112.58 1120.24 21.16 o -4 -1 1 1215.81 1244.80 18.25 o -3 1 1 972.60 1049.34 21.06 o -3 -1 1 957.81 1024.66 12.44 o -2 1 1 5050.38 5133.85 65.69 o -2 -1 1 4906.49 4979.00 63.38 o -1 1 1 4030.57 4133.25 51.55 o -1 -1 1 4106.28 4310.47 49.54 o 1 1 1 2655.71 2780.54 47.64 o 1 -1 1 2359.31 2367.05 45.33 o 2 1 1 2539.96 2524.80 65.39 o 2 -1 1 2339.65 2331.54 43.93 o 3 1 1 2537.01 2585.58 34.20 o 3 -1 1 2493.96 2584.88 67.70 o 4 1 1 2035.73 2167.07 23.17 o 4 -1 1 1953.82 2055.75 27.28 o 5 1 1 1596.83 1577.16 22.47 o 5 -1 1 1603.37 1590.80 19.16 o 6 1 1 107.05 102.80 4.91 o 6 -1 1 99.00 105.71 5.42 o 7 1 1 589.66 614.48 21.46 o 7 -1 1 590.32 673.95 51.85 o 8 1 1 579.64 586.30 27.58 o 8 -1 1 586.39 614.18 15.65 o 9 1 1 2377.67 2485.29 58.27 o 9 -1 1 2260.56 2350.90 83.94 o 10 1 1 944.13 973.22 26.28 o 10 -1 1 890.52 937.01 58.27 o 11 1 1 378.48 385.11 15.14 o 11 -1 1 395.41 412.09 25.07 o -11 2 1 932.82 850.26 23.67 o -11 -2 1 973.50 972.71 32.09 o -10 2 1 1083.63 1093.26 46.33 o -10 -2 1 1144.10 1292.34 57.77 o -9 2 1 376.24 527.93 63.58 o -9 -2 1 418.35 435.46 13.24 o -8 2 1 668.61 660.41 13.94 o -8 -2 1 688.44 691.30 18.15 o -7 2 1 2.78 2.71 3.51 < -7 -2 1 2.23 11.33 4.41 < -6 2 1 594.86 596.42 14.14 o -6 -2 1 597.44 607.56 12.74 o -5 2 1 603.66 578.17 16.55 o -5 -2 1 612.61 580.48 10.63 o -4 2 1 5133.18 5316.48 110.52 o -4 -2 1 5253.83 5409.45 70.60 o -3 2 1 7163.12 7594.87 115.93 o -3 -2 1 7115.83 7452.35 115.63 o -2 2 1 3953.61 3984.42 107.21 o -2 -2 1 3964.08 4031.36 52.75 o -1 2 1 1957.00 1889.26 28.98 o -1 -2 1 1828.93 1754.17 23.17 o 0 2 1 2993.46 2977.51 41.72 o 0 -2 1 2857.72 2835.30 36.00 o 1 -2 1 99.13 99.09 4.61 o 2 -2 1 42.18 44.03 3.51 o 3 2 1 3375.49 3569.22 53.05 o 3 -2 1 3289.99 3387.90 83.84 o 4 2 1 10918.00 12355.90 160.56 o 4 -2 1 10846.20 11217.70 563.33 o 5 2 1 8267.79 9125.79 120.05 o 5 -2 1 8105.84 8759.64 103.30 o 6 2 1 2191.98 2238.98 37.21 o 6 -2 1 2102.05 2222.33 86.65 o 7 2 1 1066.89 1075.81 21.26 o 7 -2 1 1171.15 1223.94 74.11 o 8 2 1 34.88 40.32 6.22 o 8 -2 1 20.60 19.86 7.92 < 9 -2 1 145.00 478.68 29.99 o 10 2 1 59.98 124.66 12.24 o 10 -2 1 59.10 91.16 21.46 o -10 -3 1 195.88 445.69 116.94 o -9 3 1 310.27 289.74 11.73 o -9 -3 1 262.77 267.67 20.96 o -8 3 1 584.38 583.99 12.94 o -8 -3 1 597.71 607.26 14.74 o -7 3 1 1839.75 1847.74 27.88 o -7 -3 1 1783.15 1773.13 32.19 o -6 3 1 1591.55 1564.93 21.76 o -6 -3 1 1604.96 1559.01 23.07 o -5 3 1 1866.37 1675.15 98.08 o -5 -3 1 1840.03 1793.09 28.18 o -4 3 1 1128.31 1137.39 18.05 o -4 -3 1 1133.17 1195.26 40.52 o -3 3 1 121.18 132.58 17.45 o -3 -3 1 129.06 154.65 8.62 o -2 3 1 931.22 944.73 32.29 o -2 -3 1 935.80 944.93 12.94 o -1 3 1 2208.60 2206.18 48.34 o -1 -3 1 2060.50 2043.61 27.38 o 0 -3 1 4259.01 4276.57 45.23 o 1 -3 1 3359.81 3281.79 37.61 o 2 -3 1 3353.08 3545.35 60.68 o 3 -3 1 2329.06 2460.32 30.79 o 4 -3 1 1044.80 982.64 18.25 o 5 3 1 457.00 493.73 7.82 o 5 -3 1 470.53 516.99 14.34 o 6 3 1 4.36 4.01 3.01 < 6 -3 1 3.66 8.62 7.62 < 7 3 1 662.90 678.56 13.84 o 7 -3 1 651.13 776.45 124.76 o 8 3 1 288.38 303.98 10.23 o 8 -3 1 337.45 358.24 13.64 o 9 3 1 550.92 545.78 13.04 o 9 -3 1 509.72 528.73 20.86 o 10 -3 1 373.25 396.65 16.45 o -10 -4 1 318.06 520.10 137.40 o -9 -4 1 512.84 517.90 43.33 o -8 -4 1 155.94 376.59 175.41 < -7 4 1 175.53 191.96 18.45 o -7 -4 1 183.41 168.99 6.42 o -6 4 1 112.32 133.69 24.17 o -6 -4 1 130.07 117.64 9.93 o -5 4 1 486.24 519.30 32.69 o -5 -4 1 415.80 415.50 20.96 o -4 4 1 2865.13 2843.42 80.63 o -4 -4 1 2951.00 2941.51 73.91 o -3 4 1 5538.85 5562.09 140.01 o -3 -4 1 5418.72 5482.76 98.69 o -2 4 1 3891.45 4025.54 93.17 o -2 -4 1 3837.61 3941.30 50.75 o -1 -4 1 7298.98 8160.20 92.97 o 0 -4 1 97.19 111.42 4.61 o 1 -4 1 304.27 312.20 5.62 o 2 -4 1 368.26 375.39 4.11 o 3 -4 1 1738.27 1750.46 21.26 o 4 -4 1 1520.10 1530.33 28.58 o 5 -4 1 1397.82 1428.83 29.49 o 6 -4 1 3562.04 3547.56 60.78 o 7 -4 1 1517.93 1510.97 29.28 o 8 -4 1 357.60 440.77 35.80 o 9 -4 1 61.35 369.67 113.23 o 10 -4 1 50.70 122.55 45.43 < -9 -5 1 173.88 445.29 184.63 < -8 -5 1 213.41 228.66 22.06 o -7 -5 1 1196.27 1273.48 145.52 o -6 -5 1 685.46 560.82 39.31 o -5 -5 1 2892.63 2828.08 40.42 o -4 -5 1 865.99 863.90 15.55 o -3 -5 1 37.25 55.26 7.12 o -2 -5 1 431.40 461.33 6.62 o -1 -5 1 1689.84 1742.24 18.85 o 0 -5 1 1619.76 1554.70 15.55 o 1 -5 1 2870.54 2838.01 26.98 o 2 -5 1 2696.14 2730.10 25.27 o 3 -5 1 3257.56 3347.58 39.71 o 4 -5 1 617.88 624.31 9.93 o 5 -5 1 423.73 432.95 17.55 o 6 -5 1 38.17 36.81 8.52 o 7 -5 1 391.06 468.36 41.72 o 8 -5 1 1382.97 1367.96 36.51 o 9 -5 1 368.33 405.37 29.89 o -9 -6 1 465.03 471.96 35.20 o -8 -6 1 3.49 147.13 133.69 < -7 -6 1 9.56 4.61 12.44 < -6 -6 1 133.48 154.65 31.99 o -5 -6 1 646.69 642.66 17.55 o -4 -6 1 297.61 291.94 13.34 o -3 -6 1 1230.31 1296.15 30.09 o -2 -6 1 3324.41 3418.79 33.80 o -1 -6 1 1171.93 1135.58 13.34 o 0 -6 1 324.20 328.55 6.72 o 1 -6 1 579.14 560.42 8.83 o 2 -6 1 235.61 256.84 5.11 o 3 -6 1 2785.00 2924.16 40.62 o 4 -6 1 1162.07 1173.09 17.55 o 5 -6 1 2890.38 2867.19 52.75 o 6 -6 1 1472.90 1496.03 39.92 o 7 -6 1 323.11 388.92 42.92 o 8 -6 1 17.98 14.04 12.74 < -8 -7 1 128.34 177.31 42.32 o -7 -7 1 856.74 926.38 44.33 o -6 -7 1 1262.13 1346.70 46.63 o -5 -7 1 744.67 775.24 15.34 o -4 -7 1 962.73 934.50 28.38 o -3 -7 1 162.22 153.04 8.02 o -2 -7 1 529.60 529.33 8.12 o -1 -7 1 1328.69 1322.42 16.25 o 0 -7 1 961.58 992.67 13.54 o 1 -7 1 1051.67 1074.21 13.74 o 2 -7 1 884.29 904.72 10.83 o 3 -7 1 1165.81 1205.99 20.76 o 4 -7 1 64.10 84.34 5.62 o 5 -7 1 30.93 35.80 10.03 o 6 -7 1 276.93 282.32 17.45 o 7 -7 1 352.73 363.45 20.66 o -6 -8 1 39.82 103.40 59.17 < -5 -8 1 283.74 301.77 22.87 o -4 -8 1 1259.64 1291.84 23.87 o -3 -8 1 917.51 935.41 18.05 o -2 -8 1 1202.73 1185.83 14.64 o -1 -8 1 304.35 313.61 7.82 o 0 -8 1 164.69 166.08 5.92 o 1 -8 1 264.41 236.99 7.02 o 2 -8 1 42.10 46.33 3.41 o 3 -8 1 210.75 208.40 8.93 o 4 -8 1 379.20 380.10 14.74 o 5 -8 1 161.14 159.26 19.86 o 6 -8 1 1178.81 1237.78 36.91 o -4 -9 1 433.68 440.37 21.06 o -3 -9 1 211.94 230.07 15.24 o -2 -9 1 57.20 58.77 9.93 o -1 -9 1 76.42 92.17 5.62 o 0 -9 1 530.87 542.57 10.53 o 1 -9 1 412.93 433.95 13.44 o 2 -9 1 463.36 487.71 14.74 o 3 -9 1 426.52 424.23 17.45 o 4 -9 1 238.58 221.74 19.06 o -11 0 2 1344.00 1425.12 81.94 o -10 0 2 0.69 0.70 4.31 < -9 0 2 303.61 308.89 15.24 o -8 0 2 1570.88 1536.34 30.89 o -7 0 2 3518.27 3485.08 64.09 o -6 0 2 1732.26 1658.10 39.11 o -5 0 2 4932.29 5022.33 83.04 o -4 0 2 156.14 133.89 6.82 o -3 0 2 999.47 980.64 14.24 o -2 0 2 472.36 436.16 20.76 o 1 0 2 1003.12 942.33 13.84 o 2 0 2 860.07 849.46 12.24 o 3 0 2 8162.26 8479.43 131.98 o 4 0 2 2791.31 2604.63 42.12 o 5 0 2 1366.14 1314.80 18.95 o 6 0 2 339.72 360.84 10.33 o 7 0 2 65.90 64.89 6.22 o 8 0 2 2073.75 2176.09 51.55 o 9 0 2 1746.32 1762.20 39.92 o 10 0 2 1024.58 1010.42 33.60 o 11 0 2 645.99 634.23 23.67 o -11 1 2 477.41 457.72 17.05 o -11 -1 2 485.49 569.65 27.68 o -10 1 2 821.01 880.45 53.05 o -10 -1 2 907.82 945.73 42.02 o -9 1 2 778.73 812.05 27.98 o -9 -1 2 798.35 789.78 28.78 o -8 1 2 1852.38 1826.78 42.22 o -8 -1 2 1813.65 1818.06 48.64 o -7 1 2 977.25 959.38 20.96 o -7 -1 2 945.41 922.57 19.96 o -6 1 2 1226.65 1323.03 24.87 o -6 -1 2 1198.09 1286.82 24.17 o -5 1 2 349.99 363.75 11.83 o -5 -1 2 365.97 371.88 7.02 o -4 1 2 2869.66 2815.74 38.81 o -4 -1 2 2810.23 2734.71 30.99 o -3 1 2 1229.45 1219.83 21.06 o -3 -1 2 1154.56 1142.91 19.76 o -2 1 2 3725.09 3776.12 48.74 o -2 -1 2 3900.80 3894.36 51.15 o -1 1 2 8749.88 9303.71 119.14 o -1 -1 2 8837.57 9355.36 115.63 o 0 1 2 923.55 834.41 12.24 o 0 -1 2 1056.05 932.50 13.74 o 1 1 2 4096.92 4074.79 127.27 o 1 -1 2 4295.09 4339.95 64.19 o 2 1 2 995.42 913.14 20.96 o 2 -1 2 976.52 915.75 13.64 o 3 1 2 431.70 436.16 7.62 o 3 -1 2 444.19 453.01 12.03 o 4 1 2 5631.73 6249.58 92.37 o 4 -1 2 5476.32 5908.69 96.78 o 5 1 2 1095.29 1043.32 14.94 o 5 -1 2 1146.88 1098.68 22.06 o 6 1 2 3117.95 3257.32 43.53 o 6 -1 2 3244.66 3290.92 47.44 o 7 1 2 1215.76 1247.71 25.77 o 7 -1 2 1340.40 1387.21 25.87 o 8 1 2 680.24 714.37 22.26 o 8 -1 2 734.22 755.39 18.25 o 9 1 2 1357.59 1414.29 35.60 o 9 -1 2 1344.18 1332.45 38.51 o 10 1 2 309.16 358.34 19.56 o 10 -1 2 310.53 306.69 12.34 o 11 1 2 1.47 -0.80 5.52 < 11 -1 2 1.02 2.81 11.03 < -11 2 2 320.65 323.43 34.80 o -11 -2 2 286.24 595.72 59.67 o -10 2 2 13.49 79.23 46.03 < -10 -2 2 18.10 20.96 9.93 < -9 2 2 1.69 0.30 7.02 < -9 -2 2 3.31 4.21 5.22 < -8 2 2 131.42 149.13 11.33 o -8 -2 2 144.99 161.27 10.23 o -7 2 2 1485.62 1499.64 31.59 o -7 -2 2 1449.27 1468.15 34.10 o -6 2 2 4135.25 4119.52 71.31 o -6 -2 2 4179.84 4152.01 58.47 o -5 2 2 680.38 628.22 18.05 o -5 -2 2 643.73 572.56 10.03 o -4 2 2 1716.38 1690.39 27.38 o -4 -2 2 1807.14 1762.70 25.47 o -3 2 2 3038.87 2925.66 38.31 o -3 -2 2 3022.44 2870.70 37.91 o -2 2 2 264.93 247.92 6.92 o -2 -2 2 255.83 237.09 8.32 o -1 2 2 59.08 55.46 3.71 o -1 -2 2 57.04 56.76 5.72 o 0 2 2 1391.19 1354.72 16.75 o 0 -2 2 1498.42 1449.29 18.75 o 1 2 2 8095.35 8572.70 104.70 o 1 -2 2 8063.46 8379.74 103.40 o 2 2 2 9968.52 10415.40 221.04 o 2 -2 2 10240.40 10931.50 163.17 o 3 2 2 1319.72 1133.78 23.87 o 3 -2 2 1337.51 1207.49 23.67 o 4 2 2 1713.04 1638.14 23.77 o 4 -2 2 1668.70 1565.73 28.18 o 5 2 2 168.82 182.93 7.12 o 5 -2 2 168.37 170.59 9.03 o 6 2 2 50.25 60.27 6.52 o 6 -2 2 41.20 59.77 21.26 < 7 2 2 240.51 236.08 10.83 o 7 -2 2 231.81 265.97 47.44 o 8 2 2 14.85 17.05 5.72 < 8 -2 2 25.10 20.16 8.12 < 9 2 2 1122.64 1111.11 22.16 o 9 -2 2 1094.77 1060.77 24.67 o 10 2 2 665.90 679.77 22.16 o 10 -2 2 641.32 693.21 22.97 o -11 -3 2 488.81 537.35 68.10 o -10 3 2 649.59 683.48 31.99 o -10 -3 2 603.62 649.38 33.40 o -9 3 2 1366.95 1307.28 23.27 o -9 -3 2 1452.51 1403.66 68.30 o -8 3 2 1581.14 1569.94 25.67 o -8 -3 2 1599.03 1595.92 28.58 o -7 3 2 972.26 988.26 26.38 o -7 -3 2 969.75 1022.96 71.01 o -6 3 2 499.75 519.60 14.94 o -6 -3 2 486.51 475.88 9.93 o -5 3 2 59.51 64.39 9.63 o -5 -3 2 55.54 50.85 10.33 o -4 3 2 1234.90 1219.23 32.90 o -4 -3 2 1341.94 1362.14 22.57 o -3 3 2 2615.33 2633.32 38.61 o -3 -3 2 2689.39 2737.62 37.01 o -2 3 2 1765.64 1677.35 26.78 o -2 -3 2 1721.49 1601.43 22.47 o -1 3 2 9841.62 10831.00 141.41 o -1 -3 2 9630.84 10555.40 140.61 o 0 3 2 6450.77 6707.00 103.50 o 0 -3 2 6388.91 6645.92 83.94 o 1 3 2 8982.97 9758.22 206.50 o 1 -3 2 8830.20 9550.42 107.01 o 2 -3 2 1689.12 1818.36 24.07 o 3 -3 2 1160.11 1242.69 25.67 o 4 -3 2 732.22 769.33 20.06 o 5 3 2 3672.36 3842.01 53.96 o 5 -3 2 3609.24 3718.35 53.86 o 6 3 2 2239.78 2194.15 40.72 o 6 -3 2 2192.82 2179.10 35.30 o 7 3 2 1296.88 1275.39 21.86 o 7 -3 2 1307.97 1329.24 32.49 o 8 3 2 997.78 979.13 19.56 o 8 -3 2 1003.59 1039.91 24.67 o 9 3 2 264.61 245.21 10.53 o 9 -3 2 295.70 307.49 15.75 o 10 -3 2 176.70 173.60 20.26 o -10 -4 2 53.48 47.94 18.15 < -9 4 2 15.51 18.15 13.84 < -9 -4 2 16.69 22.36 14.54 < -8 4 2 762.98 644.46 38.61 o -8 -4 2 779.84 755.39 35.90 o -7 4 2 2600.52 2315.70 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