############################################################################## # # # This CIF contains the data in a paper accepted for publication in # # Acta Crystallographica Section E. It conforms to the requirements of # # Notes for Authors for Acta Crystallographica Section E, and has been # # peer reviewed under the auspices of the IUCr Commission on Journals. # # # # Full details of the Crystallographic Information File format # # are given in the paper "The Crystallographic Information File (CIF): # # a New Standard Archive File for Crystallography" by S. R. Hall, F. H. # # Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # # # The current version of the core CIF dictionary is obtainable from # # ftp://ftp.iucr.org/pub/cif_core.dic. # # # # Software is freely available for graphical display of the structure(s) # # in this CIF. For information consult the CIF software page # # http://www.iucr.org/resources/cif/software. # # # # This file may be used for bona fide research purposes within the # # scientific community so long as proper attribution is given to the journal # # article from which it was obtained. # # # ############################################################################## data_global _audit_creation_method 'from SHELXL-2014' _journal_date_recd_electronic 2019-01-08 _journal_date_accepted 2019-01-09 _journal_name_full 'Acta Crystallographica, Section E' _journal_year 2019 _journal_volume 75 _journal_issue 2 _journal_page_first 202 _journal_page_last 207 _journal_paper_category GO _journal_paper_doi 10.1107/S2056989019000458 _journal_coeditor_code ZL2747 loop_ _publ_contact_author_name _publ_contact_author_address _publ_contact_author_email 'Yathirajan, Hemmige S.' ; Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysuru-570 006, India ; yathirajan@hotmail.com _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_section_title ; Three closely related 1-[(1,3-benzodioxol-5-yl)methyl]-4-(halobenzoyl)piperazines: similar molecular structures but different intermolecular interactions ; loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Mahesha, Ninganayaka' . ; Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysuru-570 006, India ; 'Sagar, Belakavadi K.' . ; Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysuru-570 006, India ; 'Yathirajan, Hemmige S.' . ; Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysuru-570 006, India ; 'Furuya, Tetsundo' . ; Department of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, Japan ; 'Haraguchi, Tomoyuki' . ; Department of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, Japan ; 'Akitsu, Takashiro' . ; Department of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, Japan ; 'Glidewell, Christopher' . ; School of Chemistry, University of St Andrews, St Andrews, Fife KY16 9ST, UK ; _publ_section_synopsis ; Three 1-[(1,3-benzodioxol-5-yl)methyl]-4-(halobenzoyl)piperazines adopt very similar molecular conformations but, while the molecules of the 3-fluorobenzoyl are linked by hydrogen bonds into a three-dimensional structure, there are no hydrogen bonds in either of the 2,6-difluorobenzoyl and 2,4-dichlorobenzoyl analogues. ; data_I _database_code_depnum_ccdc_archive 'CCDC 1889708' _audit_creation_method SHELXL-2014 _chemical_name_systematic ; 1-[(1,3-Benzodioxol-5-yl)methyl]-4-(3-fluorobenzoyl)piperazine ; _chemical_name_common ? _chemical_formula_moiety 'C19 H19 F N2 O3' _chemical_formula_sum 'C19 H19 F N2 O3' _chemical_formula_iupac 'C19 H19 F N2 O3' _chemical_formula_weight 342.36 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 12.2358(16) _cell_length_b 10.3185(14) _cell_length_c 14.2310(19) _cell_angle_alpha 90 _cell_angle_beta 111.199(2) _cell_angle_gamma 90 _cell_volume 1675.2(4) _cell_formula_units_Z 4 _cell_measurement_reflns_used 3689 _cell_measurement_theta_min 1.887 _cell_measurement_theta_max 27.574 _cell_measurement_temperature 173(2) _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_size_max 0.479 _exptl_crystal_size_mid 0.293 _exptl_crystal_size_min 0.282 _exptl_crystal_density_diffrn 1.357 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 720 _exptl_absorpt_coefficient_mu 0.100 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2015) ; _exptl_absorpt_correction_T_min 0.813 _exptl_absorpt_correction_T_max 0.972 _exptl_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_source 'fine focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 0.3333 _diffrn_reflns_number 8635 _diffrn_reflns_av_R_equivalents 0.0213 _diffrn_reflns_av_unetI/netI 0.0279 _diffrn_reflns_theta_min 1.887 _diffrn_reflns_theta_max 27.573 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.946 _diffrn_measured_fraction_theta_full 0.978 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_limit_l_max 9 _diffrn_standards_number 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_decay_% 0 _refine_special_details ? _reflns_number_total 3674 _reflns_number_gt 2975 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0502 _refine_ls_R_factor_gt 0.0397 _refine_ls_wR_factor_gt 0.1084 _refine_ls_wR_factor_ref 0.1141 _refine_ls_goodness_of_fit_ref 1.096 _refine_ls_restrained_S_all 1.096 _refine_ls_number_reflns 3674 _refine_ls_number_parameters 226 _refine_ls_number_restraints 0 _refine_ls_hydrogen_treatment constr _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0476P)^2^+0.4713P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.238 _refine_diff_density_min -0.179 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX2 (Bruker, 2004) ; _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_structure_solution ; SHELXS97 (Sheldrick 2015) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick,2015) ; _computing_molecular_graphics ; PLATON (Spek, 2009) ; _computing_publication_material ; SHELXL2014 and PLATON (Spek, 2009) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N1 0.57212(10) 0.47476(11) 0.26954(9) 0.0303(3) Uani d 1 . . C C2 0.51223(13) 0.44782(14) 0.33984(11) 0.0330(3) Uani d 1 . . H H2A 0.5622 0.3918 0.3952 0.040 Uiso calc 1 . . H H2B 0.4379 0.4014 0.3043 0.040 Uiso calc 1 . . C C3 0.48694(13) 0.57400(15) 0.38272(11) 0.0356(3) Uani d 1 . . H H3A 0.4438 0.5560 0.4283 0.043 Uiso calc 1 . . H H3B 0.5616 0.6173 0.4224 0.043 Uiso calc 1 . . N N4 0.41697(11) 0.65903(12) 0.30093(9) 0.0327(3) Uani d 1 . . C C5 0.47088(13) 0.68273(14) 0.22552(11) 0.0327(3) Uani d 1 . . H H5A 0.5444 0.7325 0.2564 0.039 Uiso calc 1 . . H H5B 0.4170 0.7344 0.1691 0.039 Uiso calc 1 . . C C6 0.49704(13) 0.55452(14) 0.18609(11) 0.0313(3) Uani d 1 . . H H6A 0.4228 0.5081 0.1502 0.038 Uiso calc 1 . . H H6B 0.5368 0.5704 0.1377 0.038 Uiso calc 1 . . C C11 0.60711(14) 0.35498(14) 0.23287(12) 0.0368(3) Uani d 1 . . H H11A 0.5367 0.3124 0.1845 0.044 Uiso calc 1 . . H H11B 0.6424 0.2951 0.2903 0.044 Uiso calc 1 . . O O11 0.95161(10) 0.44449(12) 0.06543(9) 0.0460(3) Uani d 1 . . C C12 1.01387(15) 0.54464(18) 0.13322(13) 0.0450(4) Uani d 1 . . H H12A 1.0984 0.5232 0.1624 0.054 Uiso calc 1 . . H H12B 1.0049 0.6279 0.0967 0.054 Uiso calc 1 . . O O13 0.96722(10) 0.55552(12) 0.21141(9) 0.0453(3) Uani d 1 . . C C3A 0.86787(13) 0.48056(14) 0.18111(11) 0.0317(3) Uani d 1 . . C C14 0.78769(13) 0.46591(14) 0.22718(11) 0.0323(3) Uani d 1 . . H H14 0.7950 0.5118 0.2870 0.039 Uiso calc 1 . . C C15 0.69410(13) 0.37999(14) 0.18201(11) 0.0327(3) Uani d 1 . . C C16 0.68486(14) 0.31574(15) 0.09369(12) 0.0384(4) Uani d 1 . . H H16 0.6203 0.2592 0.0636 0.046 Uiso calc 1 . . C C17 0.76762(14) 0.33156(16) 0.04750(12) 0.0399(4) Uani d 1 . . H H17 0.7610 0.2869 -0.0127 0.048 Uiso calc 1 . . C C7A 0.85801(14) 0.41432(14) 0.09347(11) 0.0347(3) Uani d 1 . . C C47 0.32103(13) 0.72461(14) 0.29797(11) 0.0328(3) Uani d 1 . . O O47 0.27475(12) 0.80626(13) 0.23290(10) 0.0583(4) Uani d 1 . . C C41 0.26784(12) 0.69823(13) 0.37650(11) 0.0291(3) Uani d 1 . . C C42 0.22151(13) 0.57722(14) 0.38544(11) 0.0333(3) Uani d 1 . . H H42 0.2306 0.5049 0.3476 0.040 Uiso calc 1 . . C C43 0.16209(14) 0.56607(15) 0.45098(12) 0.0367(3) Uani d 1 . . F F43 0.11374(10) 0.44972(10) 0.45775(9) 0.0590(3) Uani d 1 . . C C44 0.14867(13) 0.66616(16) 0.50952(12) 0.0377(4) Uani d 1 . . H H44 0.1079 0.6542 0.5544 0.045 Uiso calc 1 . . C C45 0.19660(13) 0.78531(16) 0.50088(12) 0.0381(4) Uani d 1 . . H H45 0.1896 0.8563 0.5409 0.046 Uiso calc 1 . . C C46 0.25459(13) 0.80141(14) 0.43428(12) 0.0345(3) Uani d 1 . . H H46 0.2857 0.8839 0.4280 0.041 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0328(6) 0.0277(6) 0.0323(6) 0.0018(5) 0.0140(5) 0.0033(5) C2 0.0307(7) 0.0341(8) 0.0338(8) 0.0021(6) 0.0113(6) 0.0106(6) C3 0.0349(8) 0.0444(9) 0.0275(7) 0.0076(6) 0.0114(6) 0.0080(6) N4 0.0373(7) 0.0345(7) 0.0283(6) 0.0068(5) 0.0145(5) 0.0068(5) C5 0.0388(8) 0.0300(7) 0.0317(7) 0.0015(6) 0.0157(6) 0.0061(6) C6 0.0350(8) 0.0311(7) 0.0285(7) -0.0005(6) 0.0121(6) 0.0025(6) C11 0.0408(8) 0.0276(7) 0.0427(9) 0.0007(6) 0.0160(7) 0.0009(6) O11 0.0512(7) 0.0504(7) 0.0447(7) -0.0015(5) 0.0275(6) -0.0093(5) C12 0.0400(9) 0.0524(10) 0.0469(10) 0.0013(7) 0.0209(8) -0.0054(8) O13 0.0426(6) 0.0511(7) 0.0478(7) -0.0086(5) 0.0231(6) -0.0146(5) C3A 0.0325(7) 0.0279(7) 0.0318(7) 0.0059(6) 0.0082(6) -0.0006(6) C14 0.0367(8) 0.0306(7) 0.0290(7) 0.0048(6) 0.0113(6) -0.0022(6) C15 0.0351(8) 0.0273(7) 0.0344(8) 0.0064(6) 0.0108(6) 0.0013(6) C16 0.0358(8) 0.0344(8) 0.0391(8) 0.0030(6) 0.0066(7) -0.0068(6) C17 0.0465(9) 0.0388(8) 0.0324(8) 0.0077(7) 0.0117(7) -0.0073(6) C7A 0.0401(8) 0.0330(8) 0.0330(8) 0.0109(6) 0.0160(7) 0.0023(6) C47 0.0369(8) 0.0260(7) 0.0370(8) 0.0018(6) 0.0150(6) 0.0059(6) O47 0.0624(8) 0.0576(8) 0.0686(9) 0.0303(6) 0.0401(7) 0.0385(7) C41 0.0263(7) 0.0280(7) 0.0303(7) 0.0019(5) 0.0071(6) 0.0036(5) C42 0.0400(8) 0.0268(7) 0.0329(7) -0.0001(6) 0.0128(7) 0.0002(6) C43 0.0383(8) 0.0311(8) 0.0398(8) -0.0047(6) 0.0130(7) 0.0068(6) F43 0.0759(8) 0.0378(6) 0.0757(7) -0.0142(5) 0.0424(6) 0.0061(5) C44 0.0342(8) 0.0466(9) 0.0337(8) 0.0027(7) 0.0141(7) 0.0058(7) C45 0.0368(8) 0.0382(8) 0.0387(8) 0.0020(6) 0.0127(7) -0.0064(7) C46 0.0332(8) 0.0270(7) 0.0431(8) -0.0020(6) 0.0135(7) -0.0006(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N1 C6 . 1.4638(18) ? N1 C11 . 1.4645(18) ? N1 C2 . 1.4647(18) ? C2 C3 . 1.517(2) ? C2 H2A . 0.9900 ? C2 H2B . 0.9900 ? C3 N4 . 1.4619(18) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? N4 C47 . 1.3423(19) ? N4 C5 . 1.4692(17) ? C5 C6 . 1.5156(19) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C11 C15 . 1.510(2) ? C11 H11A . 0.9900 ? C11 H11B . 0.9900 ? O11 C7A . 1.3777(19) ? O11 C12 . 1.431(2) ? C12 O13 . 1.4268(19) ? C12 H12A . 0.9900 ? C12 H12B . 0.9900 ? O13 C3A . 1.3722(18) ? C3A C14 . 1.371(2) ? C3A C7A . 1.389(2) ? C14 C15 . 1.406(2) ? C14 H14 . 0.9500 ? C15 C16 . 1.389(2) ? C16 C17 . 1.402(2) ? C16 H16 . 0.9500 ? C17 C7A . 1.363(2) ? C17 H17 . 0.9500 ? C47 O47 . 1.2283(18) ? C47 C41 . 1.507(2) ? C41 C46 . 1.390(2) ? C41 C42 . 1.3960(19) ? C42 C43 . 1.379(2) ? C42 H42 . 0.9500 ? C43 F43 . 1.3572(17) ? C43 C44 . 1.374(2) ? C44 C45 . 1.387(2) ? C44 H44 . 0.9500 ? C45 C46 . 1.384(2) ? C45 H45 . 0.9500 ? C46 H46 . 0.9500 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 N1 C11 . . 111.35(11) ? C6 N1 C2 . . 109.80(11) ? C11 N1 C2 . . 111.48(11) ? N1 C2 C3 . . 109.70(12) ? N1 C2 H2A . . 109.7 ? C3 C2 H2A . . 109.7 ? N1 C2 H2B . . 109.7 ? C3 C2 H2B . . 109.7 ? H2A C2 H2B . . 108.2 ? N4 C3 C2 . . 109.93(12) ? N4 C3 H3A . . 109.7 ? C2 C3 H3A . . 109.7 ? N4 C3 H3B . . 109.7 ? C2 C3 H3B . . 109.7 ? H3A C3 H3B . . 108.2 ? C47 N4 C3 . . 125.54(12) ? C47 N4 C5 . . 120.78(12) ? C3 N4 C5 . . 113.15(11) ? N4 C5 C6 . . 109.62(11) ? N4 C5 H5A . . 109.7 ? C6 C5 H5A . . 109.7 ? N4 C5 H5B . . 109.7 ? C6 C5 H5B . . 109.7 ? H5A C5 H5B . . 108.2 ? N1 C6 C5 . . 110.19(12) ? N1 C6 H6A . . 109.6 ? C5 C6 H6A . . 109.6 ? N1 C6 H6B . . 109.6 ? C5 C6 H6B . . 109.6 ? H6A C6 H6B . . 108.1 ? N1 C11 C15 . . 111.97(12) ? N1 C11 H11A . . 109.2 ? C15 C11 H11A . . 109.2 ? N1 C11 H11B . . 109.2 ? C15 C11 H11B . . 109.2 ? H11A C11 H11B . . 107.9 ? C7A O11 C12 . . 105.29(11) ? O13 C12 O11 . . 108.48(13) ? O13 C12 H12A . . 110.0 ? O11 C12 H12A . . 110.0 ? O13 C12 H12B . . 110.0 ? O11 C12 H12B . . 110.0 ? H12A C12 H12B . . 108.4 ? C3A O13 C12 . . 105.63(12) ? C14 C3A O13 . . 128.14(13) ? C14 C3A C7A . . 122.03(14) ? O13 C3A C7A . . 109.82(13) ? C3A C14 C15 . . 117.14(13) ? C3A C14 H14 . . 121.4 ? C15 C14 H14 . . 121.4 ? C16 C15 C14 . . 120.05(14) ? C16 C15 C11 . . 120.75(14) ? C14 C15 C11 . . 119.16(13) ? C15 C16 C17 . . 122.17(15) ? C15 C16 H16 . . 118.9 ? C17 C16 H16 . . 118.9 ? C7A C17 C16 . . 116.51(14) ? C7A C17 H17 . . 121.7 ? C16 C17 H17 . . 121.7 ? C17 C7A O11 . . 128.17(14) ? C17 C7A C3A . . 122.10(14) ? O11 C7A C3A . . 109.73(14) ? O47 C47 N4 . . 121.94(13) ? O47 C47 C41 . . 118.54(13) ? N4 C47 C41 . . 119.52(12) ? C46 C41 C42 . . 119.54(13) ? C46 C41 C47 . . 118.31(12) ? C42 C41 C47 . . 121.84(13) ? C43 C42 C41 . . 117.84(13) ? C43 C42 H42 . . 121.1 ? C41 C42 H42 . . 121.1 ? F43 C43 C44 . . 118.11(14) ? F43 C43 C42 . . 118.15(14) ? C44 C43 C42 . . 123.73(14) ? C43 C44 C45 . . 117.76(14) ? C43 C44 H44 . . 121.1 ? C45 C44 H44 . . 121.1 ? C46 C45 C44 . . 120.34(14) ? C46 C45 H45 . . 119.8 ? C44 C45 H45 . . 119.8 ? C45 C46 C41 . . 120.77(14) ? C45 C46 H46 . . 119.6 ? C41 C46 H46 . . 119.6 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 N1 C2 C3 . . . . -60.96(15) ? C11 N1 C2 C3 . . . . 175.17(12) ? N1 C2 C3 N4 . . . . 57.23(15) ? C2 C3 N4 C47 . . . . 133.38(15) ? C2 C3 N4 C5 . . . . -55.00(16) ? C47 N4 C5 C6 . . . . -133.39(14) ? C3 N4 C5 C6 . . . . 54.54(16) ? C11 N1 C6 C5 . . . . -175.10(11) ? C2 N1 C6 C5 . . . . 60.95(15) ? N4 C5 C6 N1 . . . . -56.63(15) ? C6 N1 C11 C15 . . . . 71.31(15) ? C2 N1 C11 C15 . . . . -165.70(12) ? C7A O11 C12 O13 . . . . 10.19(17) ? O11 C12 O13 C3A . . . . -9.99(17) ? C12 O13 C3A C14 . . . . -175.37(15) ? C12 O13 C3A C7A . . . . 5.95(17) ? O13 C3A C14 C15 . . . . -178.36(14) ? C7A C3A C14 C15 . . . . 0.2(2) ? C3A C14 C15 C16 . . . . -0.9(2) ? C3A C14 C15 C11 . . . . 176.73(13) ? N1 C11 C15 C16 . . . . -138.33(14) ? N1 C11 C15 C14 . . . . 44.02(18) ? C14 C15 C16 C17 . . . . 1.1(2) ? C11 C15 C16 C17 . . . . -176.55(14) ? C15 C16 C17 C7A . . . . -0.4(2) ? C16 C17 C7A O11 . . . . 178.28(14) ? C16 C17 C7A C3A . . . . -0.4(2) ? C12 O11 C7A C17 . . . . 174.64(16) ? C12 O11 C7A C3A . . . . -6.53(16) ? C14 C3A C7A C17 . . . . 0.5(2) ? O13 C3A C7A C17 . . . . 179.30(14) ? C14 C3A C7A O11 . . . . -178.38(13) ? O13 C3A C7A O11 . . . . 0.39(17) ? C3 N4 C47 O47 . . . . 171.03(16) ? C5 N4 C47 O47 . . . . 0.0(2) ? C3 N4 C47 C41 . . . . -8.9(2) ? C5 N4 C47 C41 . . . . -179.92(13) ? O47 C47 C41 C46 . . . . -56.5(2) ? N4 C47 C41 C46 . . . . 123.39(16) ? O47 C47 C41 C42 . . . . 116.97(17) ? N4 C47 C41 C42 . . . . -63.11(19) ? C46 C41 C42 C43 . . . . 1.1(2) ? C47 C41 C42 C43 . . . . -172.33(13) ? C41 C42 C43 F43 . . . . 178.02(14) ? C41 C42 C43 C44 . . . . -1.7(2) ? F43 C43 C44 C45 . . . . -178.92(14) ? C42 C43 C44 C45 . . . . 0.8(2) ? C43 C44 C45 C46 . . . . 0.7(2) ? C44 C45 C46 C41 . . . . -1.3(2) ? C42 C41 C46 C45 . . . . 0.4(2) ? C47 C41 C46 C45 . . . . 174.01(13) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C42 H42 O47 2_545 0.95 2.34 3.273(2) 168 y C5 H5A Cg1 2_655 0.99 2.76 3.7310(18) 168 y C45 H45 Cg1 4_576 0.95 2.90 3.7470(18) 149 y _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.954 _shelx_estimated_absorpt_T_max 0.972 _shelx_hkl_file ; 1 0 0 0.00 0.10 1 0 0 0.00 0.10 -2 0 0 29.80 0.90 2 0 0 30.70 1.00 2 0 0 29.80 1.20 -3 0 0 -0.10 0.10 3 0 0 0.20 0.20 3 0 0 0.00 0.30 4 0 0 1675.83 44.80 4 0 0 1688.13 43.80 -4 0 0 1677.83 43.50 5 0 0 0.00 0.40 5 0 0 0.20 0.20 -5 0 0 0.10 0.20 6 0 0 22.20 1.40 -6 0 0 21.50 0.90 6 0 0 22.60 1.00 -7 0 0 0.00 0.30 7 0 0 -0.20 0.30 7 0 0 -0.20 0.50 8 0 0 60.29 2.70 8 0 0 60.39 2.10 9 0 0 0.00 0.40 9 0 0 -0.50 0.70 10 0 0 12.90 1.00 10 0 0 11.90 1.50 11 0 0 0.00 0.90 11 0 0 0.70 0.50 12 0 0 3.70 1.20 13 0 0 0.90 1.10 14 0 0 5.10 1.40 0 -1 0 -2.60 0.10 1 -1 0 54.79 1.80 -1 -1 0 51.89 1.70 -1 1 0 54.69 1.80 -2 -1 0 738.03 19.70 2 -1 0 760.12 20.00 2 -1 0 760.22 19.80 2 1 0 761.52 19.60 -2 1 0 760.52 19.80 3 -1 0 1990.40 65.79 3 -1 0 1942.31 50.69 -3 -1 0 1940.11 54.59 -3 1 0 1983.50 50.59 3 1 0 1919.01 51.79 3 1 0 1944.91 50.39 4 -1 0 98.49 3.00 4 -1 0 98.09 2.80 -4 -1 0 100.19 2.80 4 1 0 100.19 2.80 -4 1 0 100.19 2.80 4 1 0 91.89 3.20 5 -1 0 0.70 0.30 5 -1 0 0.00 0.30 -5 -1 0 0.10 0.20 -5 1 0 0.20 0.20 5 1 0 0.20 0.40 5 1 0 -0.10 0.20 6 -1 0 170.98 4.80 6 -1 0 169.08 5.20 -6 -1 0 167.98 4.70 -6 1 0 172.88 4.70 6 1 0 171.88 4.70 6 1 0 167.08 5.40 7 -1 0 28.60 1.60 -7 -1 0 28.50 1.20 7 -1 0 30.70 1.30 -7 1 0 28.10 1.20 7 1 0 27.40 1.80 7 1 0 28.30 1.20 8 -1 0 56.79 2.50 8 -1 0 53.89 2.00 -8 1 0 52.79 1.90 8 1 0 57.29 2.70 8 1 0 55.89 2.00 9 -1 0 2.60 0.60 9 -1 0 3.20 0.90 9 1 0 2.30 0.90 9 1 0 2.50 0.50 10 -1 0 -0.30 0.40 10 -1 0 0.50 0.80 10 1 0 -0.20 0.80 10 1 0 0.10 0.40 11 -1 0 313.17 9.70 11 -1 0 319.47 9.10 11 1 0 326.67 10.10 12 -1 0 55.69 3.00 12 1 0 54.09 3.20 13 -1 0 1.10 1.60 13 1 0 1.10 1.10 14 1 0 7.40 1.70 0 -2 0 1731.73 45.10 -1 -2 0 4312.57 121.99 1 -2 0 4110.69 122.69 2 -2 0 6236.88 180.28 -2 -2 0 6302.67 176.58 -2 2 0 6383.16 177.68 2 2 0 6546.85 177.38 -3 -2 0 404.16 10.40 3 -2 0 399.76 10.50 3 -2 0 394.26 10.50 3 2 0 394.86 10.40 -3 2 0 400.06 10.40 4 -2 0 25.70 1.10 4 -2 0 27.50 1.10 -4 -2 0 26.70 1.00 4 2 0 26.60 1.00 4 2 0 24.20 1.40 -4 2 0 26.40 1.00 5 -2 0 0.00 0.30 -5 -2 0 0.10 0.20 5 -2 0 0.10 0.40 5 2 0 -0.20 0.30 -5 2 0 0.10 0.20 5 2 0 -0.20 0.50 6 -2 0 152.88 4.60 6 -2 0 151.18 4.40 -6 -2 0 151.88 4.30 -6 2 0 150.08 4.30 6 2 0 149.59 5.00 6 2 0 155.68 4.30 7 -2 0 87.39 2.90 -7 -2 0 88.49 2.70 7 -2 0 88.69 3.10 7 2 0 89.99 2.70 7 2 0 85.89 3.50 -7 2 0 89.79 2.70 8 -2 0 52.39 2.00 8 -2 0 47.80 2.20 -8 2 0 49.20 1.80 8 2 0 50.39 1.80 8 2 0 48.60 2.60 9 -2 0 2.40 0.60 9 -2 0 2.20 0.80 9 2 0 2.00 0.50 9 2 0 2.90 1.10 10 -2 0 10.80 1.30 10 -2 0 11.30 1.10 10 2 0 12.30 1.70 11 -2 0 0.20 0.70 11 -2 0 0.50 0.60 11 2 0 0.80 1.00 12 -2 0 11.00 1.20 12 2 0 6.80 1.60 13 2 0 1.60 1.30 14 2 0 47.30 3.50 0 -3 0 -0.20 0.20 1 -3 0 1948.31 50.89 -1 -3 0 1925.61 50.69 -2 -3 0 112.79 3.30 -3 -3 0 369.16 9.60 3 -3 0 351.56 9.70 3 3 0 384.06 9.60 -3 3 0 349.87 9.70 4 -3 0 538.45 14.20 -4 -3 0 537.65 14.00 4 3 0 534.65 14.00 -4 3 0 534.35 14.10 -5 -3 0 2.90 0.40 5 -3 0 3.10 0.50 -5 3 0 2.90 0.40 5 3 0 3.50 0.40 5 3 0 3.10 0.80 -6 -3 0 14.60 0.80 6 -3 0 16.90 1.00 6 -3 0 16.80 1.10 6 3 0 17.10 1.50 6 3 0 15.80 0.90 -6 3 0 15.70 0.90 7 -3 0 24.40 1.40 7 -3 0 22.20 1.20 -7 3 0 22.70 1.10 7 3 0 22.80 1.80 7 3 0 25.30 1.20 8 -3 0 2.00 0.70 8 -3 0 4.20 0.70 8 3 0 3.30 1.00 -8 3 0 3.20 0.50 8 3 0 3.50 0.60 9 -3 0 0.60 0.60 9 -3 0 1.90 0.60 9 3 0 1.30 0.90 -9 3 0 0.50 0.40 10 -3 0 0.20 0.50 10 3 0 0.20 1.00 11 -3 0 11.00 1.20 11 3 0 11.30 1.80 12 -3 0 95.39 3.60 12 3 0 96.59 4.60 13 -3 0 80.49 3.40 13 3 0 92.79 4.60 14 3 0 3.10 1.60 0 -4 0 188.08 5.40 1 -4 0 66.19 2.20 -1 -4 0 65.19 2.20 -2 -4 0 1.20 0.40 2 -4 0 1.70 0.40 -3 -4 0 347.57 9.30 3 -4 0 343.27 9.40 -3 4 0 348.57 9.40 4 -4 0 70.79 2.50 -4 -4 0 77.69 2.40 -4 4 0 69.09 2.40 4 4 0 79.99 2.40 5 -4 0 85.49 2.80 -5 -4 0 80.69 2.60 5 4 0 85.49 3.30 5 4 0 81.59 2.60 -5 4 0 85.49 2.70 -6 -4 0 2.90 0.50 6 -4 0 1.60 0.50 -6 4 0 1.30 0.40 6 4 0 1.50 0.80 6 4 0 2.00 0.50 7 -4 0 27.50 1.40 -7 4 0 26.60 1.30 7 4 0 27.20 2.00 7 4 0 28.30 1.30 8 -4 0 0.00 0.50 8 4 0 0.10 0.90 -8 4 0 0.30 0.40 8 4 0 0.50 0.70 9 -4 0 8.30 1.00 9 4 0 7.30 1.40 -9 4 0 7.40 0.80 10 4 0 1.60 1.10 11 -4 0 0.00 0.60 11 4 0 -0.80 1.00 12 -4 0 0.00 0.60 12 4 0 -0.40 1.20 13 -4 0 9.00 1.30 13 4 0 12.80 2.10 0 -5 0 0.50 0.40 1 -5 0 128.39 4.00 -1 -5 0 131.39 4.00 -2 -5 0 77.59 2.70 2 -5 0 82.49 2.80 -3 -5 0 31.20 1.40 -3 5 0 28.70 1.40 4 -5 0 98.09 3.30 -4 -5 0 102.29 3.20 4 5 0 97.79 3.10 -4 5 0 95.99 3.20 -5 -5 0 2.30 0.50 5 -5 0 1.40 0.50 5 5 0 1.30 0.40 -5 5 0 1.70 0.40 5 5 0 1.50 0.80 6 -5 0 54.59 2.20 -6 -5 0 48.40 1.90 -6 5 0 49.70 2.00 6 5 0 54.69 1.90 6 5 0 51.79 2.70 7 -5 0 14.80 1.20 7 5 0 17.00 1.80 -7 5 0 15.40 1.00 7 5 0 14.40 1.00 8 -5 0 40.20 2.00 -8 5 0 39.50 1.70 8 5 0 37.90 2.60 9 -5 0 76.29 3.00 9 5 0 77.29 3.80 -9 5 0 76.89 2.80 10 -5 0 1.40 0.70 10 5 0 1.00 1.10 11 -5 0 0.50 0.70 11 5 0 0.50 1.10 12 -5 0 0.90 0.80 12 5 0 -0.20 1.20 13 -5 0 0.20 0.80 13 5 0 1.00 1.40 0 -6 0 22.60 1.30 1 -6 0 1.00 0.50 -1 -6 0 0.50 0.40 -2 -6 0 123.79 4.00 -3 -6 0 21.90 1.30 -3 6 0 20.10 1.20 -4 -6 0 29.00 1.50 -4 6 0 29.50 1.50 -5 -6 0 17.70 1.20 5 -6 0 20.00 1.30 5 6 0 19.80 1.10 -5 6 0 19.50 1.20 5 6 0 19.00 1.70 6 -6 0 245.38 7.10 -6 -6 0 225.78 7.20 -6 6 0 235.58 6.80 6 6 0 229.58 6.70 6 6 0 238.98 7.60 7 -6 0 154.98 5.00 -7 6 0 149.88 4.80 7 6 0 155.98 5.60 8 -6 0 3.70 0.80 -8 6 0 2.90 0.60 8 6 0 2.80 1.10 9 -6 0 12.40 1.30 9 6 0 10.90 1.70 -9 6 0 12.50 1.10 10 -6 0 -0.90 0.60 -10 6 0 -0.10 0.50 10 6 0 -1.10 1.00 11 -6 0 3.70 1.00 11 6 0 3.50 1.40 12 -6 0 -0.50 0.70 12 6 0 -0.20 1.20 13 -6 0 0.10 0.80 0 -7 0 1.10 0.50 -1 -7 0 59.19 2.40 1 -7 0 58.49 2.40 -2 -7 0 49.50 2.20 -3 -7 0 26.20 1.50 -3 7 0 22.80 1.40 -4 -7 0 150.28 4.70 -4 7 0 144.19 4.60 -5 -7 0 206.38 6.10 -5 7 0 196.08 6.00 5 7 0 198.78 5.90 5 7 0 200.08 6.70 6 7 0 11.20 1.50 -6 7 0 13.30 1.10 7 7 0 43.70 2.70 -7 7 0 41.50 2.00 8 -7 0 4.30 1.00 8 7 0 5.00 1.30 -8 7 0 4.20 0.80 9 -7 0 4.60 1.00 -9 7 0 6.50 0.90 9 7 0 6.20 1.50 10 -7 0 1.10 0.80 -10 7 0 0.80 0.60 10 7 0 0.30 1.10 11 -7 0 16.00 1.70 11 7 0 15.20 2.10 12 -7 0 1.50 1.00 12 7 0 2.40 1.50 0 -8 0 1321.77 34.70 -1 -8 0 78.09 3.10 1 -8 0 83.99 3.20 -2 -8 0 12.00 1.20 -3 -8 0 25.70 1.70 -3 8 0 28.80 1.60 -4 -8 0 331.87 9.70 -4 8 0 343.87 9.70 -5 -8 0 73.49 2.90 5 8 0 69.29 3.30 -5 8 0 69.69 2.80 6 8 0 15.60 1.90 -6 8 0 17.50 1.30 -7 8 0 9.00 1.00 7 8 0 8.50 1.50 8 8 0 69.99 3.70 -8 8 0 73.59 2.90 -9 8 0 0.60 0.60 9 8 0 0.20 1.00 10 8 0 8.60 1.80 -10 8 0 7.60 1.10 11 8 0 -0.30 1.10 0 -9 0 0.20 0.70 -1 -9 0 24.90 1.80 -2 -9 0 27.70 1.80 -2 9 0 31.20 1.80 -3 -9 0 180.78 5.90 -3 9 0 178.68 5.70 -4 -9 0 18.50 1.50 4 9 0 17.20 1.90 -4 9 0 19.30 1.50 -5 -9 0 15.60 1.80 -5 9 0 21.90 1.50 5 9 0 25.40 2.10 6 9 0 36.30 2.60 -6 9 0 35.40 2.00 7 9 0 29.80 2.50 -7 9 0 27.50 1.80 8 9 0 3.20 1.30 -8 9 0 2.80 0.80 -9 9 0 8.50 1.10 9 9 0 8.60 1.70 10 9 0 36.00 3.10 -10 9 0 37.60 2.20 -1 -10 0 3.40 0.90 -1 10 0 2.40 0.80 -2 -10 0 256.87 8.40 -2 10 0 292.97 8.40 -3 -10 0 5.20 1.00 -3 10 0 2.70 0.80 -4 -10 0 17.80 1.60 -4 10 0 14.90 1.50 5 10 0 3.30 1.30 -5 10 0 3.90 0.90 6 10 0 12.70 1.80 -6 10 0 13.80 1.50 7 10 0 -0.30 1.00 -7 10 0 -0.50 0.60 -8 10 0 2.40 0.80 8 10 0 1.60 1.30 -9 10 0 24.00 1.80 9 10 0 22.70 2.60 0 11 0 -0.10 0.60 -1 11 0 0.50 0.70 -2 -11 0 2.20 0.90 -2 11 0 2.60 0.80 -3 -11 0 34.30 2.30 -3 11 0 43.30 2.40 -4 -11 0 23.30 1.90 -4 11 0 27.00 1.90 -5 11 0 1.10 0.80 -6 11 0 19.60 1.70 -7 11 0 0.90 0.80 -8 11 0 1.50 0.80 8 11 0 0.90 1.30 0 12 0 27.40 2.00 1 12 0 0.50 0.70 -1 12 0 0.30 0.70 -2 12 0 -0.30 0.70 -3 12 0 0.50 0.80 -4 12 0 29.30 2.20 -5 12 0 -0.40 0.70 0 13 0 0.60 0.80 -1 13 0 -0.20 0.80 1 13 0 -0.30 0.70 -2 13 0 8.70 1.70 2 13 0 7.50 1.30 3 13 0 4.10 1.00 14 0 -1 1.40 1.10 13 0 -1 119.49 5.00 12 0 -1 -1.10 0.90 12 0 -1 0.00 0.50 11 0 -1 129.29 5.00 11 0 -1 128.59 4.20 10 0 -1 0.10 0.40 10 0 -1 -0.50 0.80 9 0 -1 12.90 1.50 9 0 -1 11.20 0.90 8 0 -1 0.20 0.60 8 0 -1 -0.10 0.30 7 0 -1 192.68 5.90 7 0 -1 189.88 5.40 -7 0 1 186.78 5.10 6 0 -1 -0.10 0.50 -6 0 1 -0.10 0.20 6 0 -1 -0.10 0.30 5 0 -1 289.07 7.70 -5 0 1 288.67 7.50 5 0 -1 283.07 8.10 -4 0 1 0.00 0.10 4 0 -1 0.10 0.30 4 0 -1 -0.10 0.20 -3 0 1 649.14 16.70 3 0 -1 647.84 17.10 2 0 -1 -2.50 0.10 1 0 -1 260.67 7.00 0 0 -1 -2.40 0.10 -1 0 -1 346.57 9.30 1 0 1 354.76 9.20 1 0 1 352.36 9.20 2 0 1 0.10 0.10 2 0 1 0.10 0.30 -2 0 -1 0.10 0.20 -3 0 -1 7481.85 205.38 3 0 1 7355.46 210.08 3 0 1 7691.63 204.68 4 0 1 -0.30 0.30 4 0 1 -0.10 0.20 -4 0 -1 -0.10 0.20 5 0 1 68.49 2.10 -5 0 -1 65.19 2.10 5 0 1 66.99 2.50 6 0 1 0.00 0.20 6 0 1 0.40 0.50 -6 0 -1 -0.10 0.30 -7 0 -1 49.90 1.80 7 0 1 51.79 1.80 7 0 1 49.60 2.30 8 0 1 -0.40 0.30 -8 0 -1 -0.20 0.30 8 0 1 -0.10 0.60 9 0 1 2.70 0.50 9 0 1 2.20 0.90 10 0 1 -0.20 0.80 10 0 1 0.00 0.40 11 0 1 6.10 1.30 12 0 1 0.80 1.10 13 0 1 3.90 1.30 14 0 1 -0.10 1.10 15 1 -1 12.10 2.00 14 1 -1 0.20 1.10 13 -1 -1 13.30 2.10 13 1 -1 12.60 1.90 12 -1 -1 4.90 0.90 12 -1 -1 4.70 1.20 12 1 -1 4.40 1.30 11 -1 -1 0.70 0.90 11 -1 -1 0.40 0.50 11 1 -1 0.60 1.00 11 1 -1 1.60 0.60 10 -1 -1 92.89 3.20 10 -1 -1 96.09 3.80 10 1 -1 91.39 4.00 10 1 -1 97.39 3.20 9 -1 -1 4.20 0.70 9 -1 -1 2.40 0.90 9 1 -1 4.00 0.60 9 1 -1 2.80 0.90 8 -1 -1 231.68 7.00 8 -1 -1 232.98 6.60 8 1 -1 238.58 6.50 8 1 -1 235.28 7.30 -8 1 1 228.08 6.40 7 -1 -1 51.49 2.20 7 -1 -1 48.80 1.80 -7 -1 1 50.39 1.60 7 1 -1 47.50 2.30 -7 1 1 51.29 1.60 7 1 -1 51.99 1.80 6 -1 -1 -0.10 0.40 6 -1 -1 -0.10 0.30 -6 -1 1 0.00 0.20 6 1 -1 0.20 0.30 6 1 -1 -0.10 0.50 -6 1 1 0.00 0.20 5 -1 -1 65.39 2.30 -5 -1 1 62.19 1.80 5 -1 -1 64.49 2.00 5 1 -1 62.49 2.00 -5 1 1 63.39 1.90 -4 -1 1 114.79 3.20 4 -1 -1 124.69 3.50 4 -1 -1 115.59 3.40 -4 1 1 121.29 3.30 4 1 -1 119.69 3.40 3 -1 -1 165.68 4.50 3 -1 -1 168.48 4.60 3 1 -1 169.48 4.60 -3 1 1 168.88 4.50 2 -1 -1 6.00 0.40 2 -1 -1 7.50 0.40 2 1 -1 6.70 0.40 0 -1 -1 11.80 0.50 0 1 1 12.50 0.50 0 1 -1 11.70 0.40 -1 -1 -1 1078.39 35.90 -1 1 -1 1102.49 29.10 1 1 1 1161.98 29.70 2 -1 1 39.80 1.60 -2 -1 -1 47.40 1.50 2 -1 1 49.00 1.50 -2 1 -1 49.99 1.50 2 1 1 48.20 1.30 2 1 1 46.70 1.70 -3 -1 -1 196.78 5.30 3 -1 1 192.48 5.20 3 -1 1 198.98 5.40 -3 1 -1 191.38 5.20 3 1 1 193.18 5.60 3 1 1 198.18 5.10 -4 -1 -1 477.75 12.70 4 -1 1 485.85 13.00 4 -1 1 485.45 12.70 4 1 1 469.65 13.10 4 1 1 511.85 12.60 -4 1 -1 491.75 12.70 5 -1 1 65.59 2.00 5 -1 1 60.69 2.30 -5 -1 -1 63.39 2.00 -5 1 -1 63.09 2.00 5 1 1 60.79 2.50 5 1 1 66.29 1.90 6 -1 1 17.60 1.20 6 -1 1 19.10 0.90 -6 -1 -1 19.30 1.00 6 1 1 18.70 0.90 6 1 1 18.00 1.40 -6 1 -1 19.80 0.90 7 -1 1 34.70 1.80 -7 -1 -1 32.00 1.40 7 -1 1 33.70 1.40 -7 1 -1 30.90 1.30 7 1 1 32.00 1.30 7 1 1 32.30 1.90 8 -1 1 24.10 1.70 8 -1 1 24.70 1.20 -8 1 -1 25.90 1.30 8 1 1 27.20 1.90 8 1 1 25.70 1.20 9 -1 1 13.80 1.50 9 -1 1 13.40 1.00 9 1 1 17.10 1.70 9 1 1 14.80 1.00 10 -1 1 15.20 1.60 10 -1 1 18.20 1.20 10 1 1 18.20 1.90 11 -1 1 32.00 2.30 11 1 1 35.90 2.60 12 -1 1 20.40 2.00 12 1 1 20.40 2.20 13 -1 1 27.50 2.40 13 1 1 29.60 2.80 14 1 1 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-15 17.80 2.10 3 7 -15 11.70 1.70 3 7 -15 13.70 1.70 2 7 -15 1.20 1.10 2 7 -15 0.00 0.90 1 7 -15 52.09 3.20 12 0 -16 4.90 1.10 11 0 -16 -0.50 0.80 10 0 -16 0.50 0.90 9 0 -16 0.60 0.80 8 0 -16 2.20 0.90 5 0 -16 -0.10 0.80 4 0 -16 1.20 0.90 3 0 -16 0.90 1.00 2 0 -16 31.30 2.50 1 0 -16 0.20 1.00 0 0 -16 26.60 2.60 -1 0 -16 -1.00 1.10 12 -1 -16 23.20 1.90 12 1 -16 15.50 1.90 11 -1 -16 3.00 1.00 11 1 -16 3.10 1.00 10 -1 -16 1.50 0.80 10 1 -16 0.60 0.90 9 -1 -16 -0.70 0.70 9 1 -16 0.20 0.80 8 1 -16 -0.20 0.80 7 1 -16 8.40 1.30 6 -1 -16 0.60 0.80 5 -1 -16 40.10 2.50 5 1 -16 36.90 2.50 4 -1 -16 0.00 0.80 4 1 -16 0.50 1.00 3 -1 -16 17.90 2.00 3 1 -16 17.20 1.90 2 -1 -16 11.80 1.70 2 1 -16 12.80 1.70 1 -1 -16 29.10 2.60 1 1 -16 31.30 2.60 0 -1 -16 0.00 1.10 0 1 -16 2.40 1.20 -1 -1 -16 19.60 2.20 -1 1 -16 20.10 2.30 12 -2 -16 3.50 1.00 11 -2 -16 1.50 0.80 11 2 -16 1.20 1.10 10 -2 -16 0.00 0.70 10 2 -16 -0.10 0.90 9 2 -16 5.50 1.20 8 2 -16 3.20 1.00 7 2 -16 1.80 0.90 6 -2 -16 2.40 0.90 5 -2 -16 0.30 0.80 5 2 -16 -0.10 0.80 4 -2 -16 0.50 0.80 4 2 -16 -0.60 0.80 3 -2 -16 2.30 1.00 3 2 -16 3.20 1.20 2 -2 -16 33.10 2.60 2 2 -16 32.20 2.60 1 -2 -16 5.90 1.40 1 2 -16 5.70 1.50 0 -2 -16 0.70 1.10 0 2 -16 0.90 1.20 -1 -2 -16 7.00 1.60 -1 2 -16 9.20 1.80 11 -3 -16 5.80 1.10 11 3 -16 3.80 1.30 10 3 -16 0.80 1.00 9 3 -16 2.20 1.10 8 3 -16 -0.30 0.90 7 3 -16 -0.70 0.90 6 -3 -16 9.70 1.40 6 3 -16 9.50 1.40 5 -3 -16 16.70 1.90 4 -3 -16 3.20 1.10 4 3 -16 0.70 1.00 3 -3 -16 1.30 0.90 3 3 -16 -0.80 0.90 2 -3 -16 3.60 1.20 2 3 -16 1.70 1.10 1 -3 -16 0.80 1.00 1 3 -16 1.50 1.10 0 -3 -16 21.70 2.30 0 3 -16 24.00 2.60 -1 3 -16 6.00 1.90 10 4 -16 5.30 1.40 9 4 -16 -1.10 0.90 8 4 -16 4.00 1.20 7 -4 -16 57.69 3.10 7 4 -16 60.79 3.20 6 -4 -16 4.70 1.10 6 4 -16 4.20 1.20 5 -4 -16 1.10 0.80 5 4 -16 -0.10 0.90 4 -4 -16 4.40 1.20 4 4 -16 4.60 1.30 3 -4 -16 1.60 1.00 3 4 -16 1.40 1.10 2 -4 -16 6.90 1.40 2 4 -16 8.60 1.50 1 -4 -16 2.40 1.20 1 4 -16 0.90 1.20 0 -4 -16 0.50 1.60 0 4 -16 -0.40 1.10 9 5 -16 2.10 1.20 8 5 -16 -0.40 1.10 7 -5 -16 5.10 1.20 7 5 -16 4.60 1.40 6 -5 -16 3.40 1.10 6 5 -16 1.30 1.10 5 -5 -16 0.10 0.80 5 5 -16 -1.00 0.90 4 -5 -16 0.90 0.90 4 5 -16 -0.40 0.90 4 5 -16 -0.20 1.40 3 -5 -16 6.30 1.30 3 5 -16 4.90 1.30 2 -5 -16 1.90 1.10 2 5 -16 1.40 1.20 1 5 -16 7.80 1.60 7 -6 -16 3.00 1.10 7 6 -16 2.00 1.20 6 -6 -16 0.50 0.90 6 6 -16 -0.60 1.00 5 -6 -16 3.40 1.20 5 6 -16 1.50 1.20 4 -6 -16 1.00 1.00 4 6 -16 1.60 1.10 3 -6 -16 10.90 2.50 3 6 -16 8.20 1.50 2 6 -16 -1.40 1.10 11 0 -17 7.80 1.30 10 0 -17 0.30 0.90 5 0 -17 14.20 1.80 4 0 -17 -0.30 0.90 3 0 -17 2.00 1.10 2 0 -17 0.70 1.10 1 0 -17 0.10 1.10 11 -1 -17 11.80 1.50 11 1 -17 12.00 1.50 10 1 -17 20.90 1.90 9 1 -17 14.30 1.60 5 -1 -17 0.70 0.90 5 1 -17 0.70 0.90 4 -1 -17 10.80 1.60 4 1 -17 10.60 1.60 3 -1 -17 4.30 1.30 3 1 -17 2.30 1.20 2 -1 -17 12.00 1.80 2 1 -17 10.30 1.70 1 -1 -17 1.10 1.10 1 1 -17 0.60 1.10 10 2 -17 7.20 1.40 9 2 -17 0.80 1.00 8 2 -17 2.70 1.10 6 -2 -17 37.70 2.50 5 -2 -17 1.20 0.90 4 -2 -17 0.90 0.90 4 2 -17 0.30 0.90 3 -2 -17 0.00 0.90 3 2 -17 1.00 1.10 2 -2 -17 10.80 1.70 2 2 -17 11.30 1.80 1 -2 -17 2.20 1.30 1 2 -17 -0.10 1.10 10 3 -17 11.90 1.80 9 3 -17 1.70 1.10 8 3 -17 3.20 1.20 7 3 -17 2.40 1.10 6 -3 -17 3.10 1.10 5 -3 -17 10.50 1.60 4 -3 -17 0.10 0.90 4 3 -17 0.40 1.10 3 -3 -17 10.90 1.70 3 3 -17 11.30 1.80 2 -3 -17 3.80 1.20 2 3 -17 1.90 1.30 1 3 -17 6.80 1.90 9 4 -17 0.10 1.10 8 4 -17 -0.70 1.10 7 4 -17 3.00 1.20 6 -4 -17 17.70 2.00 6 4 -17 10.90 1.80 5 -4 -17 8.50 1.50 4 -4 -17 25.90 2.40 4 4 -17 26.10 2.50 3 -4 -17 8.90 1.60 3 4 -17 10.50 1.70 2 4 -17 11.60 1.90 7 5 -17 20.70 2.20 6 -5 -17 25.00 2.20 6 5 -17 17.00 2.00 5 -5 -17 13.20 1.70 5 0 -18 0.50 1.00 4 0 -18 6.80 1.40 3 0 -18 -0.10 1.00 5 -1 -18 -0.10 0.90 5 1 -18 0.40 1.40 4 -1 -18 0.40 1.00 4 1 -18 1.20 1.10 3 -1 -18 2.10 1.20 3 1 -18 0.90 1.10 6 -2 -18 0.40 1.30 5 -2 -18 0.40 0.90 4 -2 -18 2.50 1.10 4 2 -18 1.30 1.20 3 2 -18 4.40 1.40 6 -3 -18 5.90 1.30 5 -3 -18 14.90 1.90 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 90666 _shelx_res_file ; TITL m1cg CELL 0.71073 12.2358 10.3185 14.2310 90.000 111.199 90.000 ZERR 4.000 0.0016 0.0014 0.0019 0.000 0.002 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O F UNIT 76 76 8 12 4 OMIT -2 180.0 L.S. 20 ACTA BOND $H CONF HTAB OMIT 12 1 6 OMIT 12 0 6 OMIT 11 1 6 OMIT 10 1 7 OMIT 10 1 8 OMIT 10 0 8 OMIT 10 1 6 OMIT 10 2 8 OMIT 9 1 7 OMIT 9 0 7 OMIT 10 2 7 OMIT 11 1 7 OMIT 11 1 5 OMIT 11 0 5 OMIT 10 0 6 FMAP 2 PLAN 20 SIZE 0.479 0.293 0.282 TEMP -100 WGHT 0.047600 0.471300 FVAR 0.56895 N1 3 0.572121 0.474757 0.269542 11.00000 0.03280 0.02768 = 0.03228 0.00332 0.01405 0.00185 C2 1 0.512231 0.447816 0.339845 11.00000 0.03066 0.03414 = 0.03382 0.01059 0.01127 0.00214 AFIX 23 H2A 2 0.562161 0.391831 0.395240 11.00000 -1.20000 H2B 2 0.437890 0.401360 0.304338 11.00000 -1.20000 AFIX 0 C3 1 0.486939 0.574002 0.382722 11.00000 0.03485 0.04444 = 0.02745 0.00798 0.01137 0.00755 AFIX 23 H3A 2 0.443830 0.555984 0.428265 11.00000 -1.20000 H3B 2 0.561595 0.617346 0.422374 11.00000 -1.20000 AFIX 0 N4 3 0.416967 0.659032 0.300927 11.00000 0.03733 0.03455 = 0.02833 0.00676 0.01448 0.00675 C5 1 0.470877 0.682728 0.225515 11.00000 0.03885 0.02997 = 0.03165 0.00606 0.01572 0.00147 AFIX 23 H5A 2 0.544371 0.732534 0.256395 11.00000 -1.20000 H5B 2 0.416951 0.734362 0.169136 11.00000 -1.20000 AFIX 0 C6 1 0.497044 0.554524 0.186093 11.00000 0.03499 0.03105 = 0.02846 0.00254 0.01213 -0.00049 AFIX 23 H6A 2 0.422788 0.508095 0.150241 11.00000 -1.20000 H6B 2 0.536760 0.570402 0.137668 11.00000 -1.20000 AFIX 0 C11 1 0.607112 0.354977 0.232875 11.00000 0.04083 0.02762 = 0.04269 0.00085 0.01603 0.00067 AFIX 23 H11A 2 0.536708 0.312427 0.184481 11.00000 -1.20000 H11B 2 0.642415 0.295113 0.290268 11.00000 -1.20000 AFIX 0 O11 4 0.951611 0.444489 0.065434 11.00000 0.05124 0.05036 = 0.04469 -0.00925 0.02748 -0.00155 C12 1 1.013873 0.544638 0.133221 11.00000 0.03998 0.05241 = 0.04694 -0.00539 0.02087 0.00131 AFIX 23 H12A 2 1.098377 0.523170 0.162415 11.00000 -1.20000 H12B 2 1.004920 0.627934 0.096668 11.00000 -1.20000 AFIX 0 O13 4 0.967225 0.555518 0.211406 11.00000 0.04256 0.05110 = 0.04778 -0.01464 0.02314 -0.00857 C3A 1 0.867869 0.480564 0.181106 11.00000 0.03251 0.02793 = 0.03175 -0.00060 0.00824 0.00593 C14 1 0.787692 0.465906 0.227177 11.00000 0.03670 0.03060 = 0.02901 -0.00220 0.01134 0.00476 AFIX 43 H14 2 0.795046 0.511809 0.287029 11.00000 -1.20000 AFIX 0 C15 1 0.694102 0.379991 0.182013 11.00000 0.03506 0.02725 = 0.03445 0.00130 0.01082 0.00637 C16 1 0.684860 0.315738 0.093690 11.00000 0.03582 0.03435 = 0.03911 -0.00677 0.00657 0.00298 AFIX 43 H16 2 0.620332 0.259210 0.063589 11.00000 -1.20000 AFIX 0 C17 1 0.767618 0.331557 0.047502 11.00000 0.04648 0.03877 = 0.03243 -0.00727 0.01175 0.00766 AFIX 43 H17 2 0.761030 0.286915 -0.012690 11.00000 -1.20000 AFIX 0 C7A 1 0.858012 0.414323 0.093465 11.00000 0.04014 0.03305 = 0.03305 0.00227 0.01596 0.01093 C47 1 0.321035 0.724612 0.297971 11.00000 0.03686 0.02604 = 0.03698 0.00594 0.01502 0.00179 O47 4 0.274752 0.806262 0.232905 11.00000 0.06241 0.05764 = 0.06863 0.03854 0.04011 0.03030 C41 1 0.267845 0.698234 0.376498 11.00000 0.02633 0.02796 = 0.03034 0.00364 0.00707 0.00192 C42 1 0.221514 0.577225 0.385443 11.00000 0.04003 0.02684 = 0.03289 0.00017 0.01284 -0.00012 AFIX 43 H42 2 0.230621 0.504904 0.347614 11.00000 -1.20000 AFIX 0 C43 1 0.162093 0.566070 0.450976 11.00000 0.03827 0.03107 = 0.03977 0.00683 0.01295 -0.00474 F43 5 0.113738 0.449716 0.457752 11.00000 0.07592 0.03784 = 0.07565 0.00611 0.04244 -0.01424 C44 1 0.148668 0.666158 0.509515 11.00000 0.03424 0.04661 = 0.03365 0.00582 0.01413 0.00275 AFIX 43 H44 2 0.107919 0.654158 0.554410 11.00000 -1.20000 AFIX 0 C45 1 0.196600 0.785313 0.500876 11.00000 0.03677 0.03820 = 0.03870 -0.00642 0.01275 0.00205 AFIX 43 H45 2 0.189600 0.856258 0.540875 11.00000 -1.20000 AFIX 0 C46 1 0.254587 0.801409 0.434279 11.00000 0.03319 0.02704 = 0.04310 -0.00062 0.01350 -0.00198 AFIX 43 H46 2 0.285689 0.883927 0.427981 11.00000 -1.20000 AFIX 0 HKLF 4 REM m1cg REM R1 = 0.0397 for 2975 Fo > 4sig(Fo) and 0.0502 for all 3674 data REM 226 parameters refined using 0 restraints END WGHT 0.0476 0.4712 REM Instructions for potential hydrogen bonds EQIV $1 -x+1/2, y-1/2, -z+1/2 HTAB C2 O47_$1 HTAB C42 O47_$1 REM Highest difference peak 0.238, deepest hole -0.179, 1-sigma level 0.038 Q1 1 0.8627 0.4553 0.1329 11.00000 0.05 0.20 Q2 1 0.3000 0.7087 0.3453 11.00000 0.05 0.20 Q3 1 0.2392 0.5622 0.4534 11.00000 0.05 0.20 Q4 1 0.1977 0.5960 0.5110 11.00000 0.05 0.19 Q5 1 0.6611 0.3645 0.2116 11.00000 0.05 0.18 Q6 1 0.4682 0.6161 0.1970 11.00000 0.05 0.18 Q7 1 0.4418 0.6729 0.2613 11.00000 0.05 0.18 Q8 1 0.7082 0.3217 0.1578 11.00000 0.05 0.18 Q9 1 0.8130 0.5010 0.1874 11.00000 0.05 0.18 Q10 1 0.5329 0.4635 0.2961 11.00000 0.05 0.17 Q11 1 0.1559 0.5828 0.3940 11.00000 0.05 0.17 Q12 1 0.6677 0.3816 0.1248 11.00000 0.05 0.17 Q13 1 0.7222 0.4602 0.1844 11.00000 0.05 0.17 Q14 1 0.8978 0.5954 0.1598 11.00000 0.05 0.16 Q15 1 0.1534 0.7353 0.4873 11.00000 0.05 0.16 Q16 1 0.2625 0.7765 0.5001 11.00000 0.05 0.16 Q17 1 0.3796 0.6971 0.3059 11.00000 0.05 0.16 Q18 1 0.6216 0.5137 0.3035 11.00000 0.05 0.15 Q19 1 0.2994 0.7386 0.4290 11.00000 0.05 0.15 Q20 1 0.5451 0.5210 0.2375 11.00000 0.05 0.15 ; _shelx_res_checksum 24443 _shelxl_version_number 2.014 data_II _database_code_depnum_ccdc_archive 'CCDC 1889709' _audit_creation_method SHELXL-2014 _chemical_name_systematic ; 1-[(1,3-Benzodioxol-5-yl)methyl]-4-(2,6-difluorobenzoyl)piperazine ; _chemical_name_common ? _chemical_formula_moiety 'C19 H18 F2 N2 O3' _chemical_formula_sum 'C19 H18 F2 N2 O3' _chemical_formula_iupac 'C19 H18 F2 N2 O3' _chemical_formula_weight 360.35 _chemical_melting_point ? _chemical_absolute_configuration unk _space_group_crystal_system orthorhombic _space_group_name_H-M_alt 'P c a 21' _space_group_name_Hall 'P 2c -2ac' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' _cell_length_a 14.2762(9) _cell_length_b 15.9821(10) _cell_length_c 7.3753(5) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1682.78(19) _cell_formula_units_Z 4 _cell_measurement_reflns_used 3743 _cell_measurement_theta_min 1.913 _cell_measurement_theta_max 27.503 _cell_measurement_temperature 173(2) _exptl_crystal_description needle _exptl_crystal_colour colourless _exptl_crystal_size_max 0.910 _exptl_crystal_size_mid 0.352 _exptl_crystal_size_min 0.168 _exptl_crystal_density_diffrn 1.422 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 752 _exptl_absorpt_coefficient_mu 0.112 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2015) ; _exptl_absorpt_correction_T_min 0.587 _exptl_absorpt_correction_T_max 0.981 _exptl_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_source 'fine focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 0.3333 _diffrn_reflns_number 9016 _diffrn_reflns_av_R_equivalents 0.0569 _diffrn_reflns_av_unetI/netI 0.0522 _diffrn_reflns_theta_min 1.913 _diffrn_reflns_theta_max 27.503 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_limit_l_max 9 _diffrn_standards_number 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_decay_% 0 _refine_special_details ? _reflns_number_total 3743 _reflns_number_gt 3449 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0560 _refine_ls_R_factor_gt 0.0535 _refine_ls_wR_factor_gt 0.1526 _refine_ls_wR_factor_ref 0.1550 _refine_ls_goodness_of_fit_ref 1.161 _refine_ls_restrained_S_all 1.161 _refine_ls_number_reflns 3743 _refine_ls_number_parameters 235 _refine_ls_number_restraints 1 _refine_ls_hydrogen_treatment constr _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0960P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.171 _refine_diff_density_min -0.215 _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 1369 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX2 (Bruker, 2004) ; _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_molecular_graphics ; PLATON (Spek, 2009) ; _computing_publication_material ; SHELXL2014 and PLATON (Spek, 2009) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N1 0.36051(17) 0.62727(15) 0.3017(3) 0.0249(5) Uani d 1 . . C C2 0.3856(2) 0.71107(18) 0.2369(5) 0.0302(6) Uani d 1 . . H H2A 0.3597 0.7197 0.1138 0.036 Uiso calc 1 . . H H2B 0.4546 0.7163 0.2299 0.036 Uiso calc 1 . . C C3 0.3470(2) 0.77682(17) 0.3641(4) 0.0302(6) Uani d 1 . . H H3A 0.3686 0.8328 0.3249 0.036 Uiso calc 1 . . H H3B 0.2777 0.7762 0.3590 0.036 Uiso calc 1 . . N N4 0.37766(17) 0.76146(14) 0.5509(4) 0.0265(5) Uani d 1 . . C C5 0.3658(2) 0.67513(15) 0.6138(4) 0.0247(5) Uani d 1 . . H H5A 0.2984 0.6633 0.6317 0.030 Uiso calc 1 . . H H5B 0.3979 0.6679 0.7317 0.030 Uiso calc 1 . . C C6 0.40582(18) 0.61456(18) 0.4776(4) 0.0243(6) Uani d 1 . . H H6A 0.4742 0.6236 0.4659 0.029 Uiso calc 1 . . H H6B 0.3953 0.5564 0.5193 0.029 Uiso calc 1 . . C C11 0.3880(2) 0.5620(2) 0.1720(4) 0.0320(7) Uani d 1 . . H H11A 0.4569 0.5628 0.1566 0.038 Uiso calc 1 . . H H11B 0.3592 0.5740 0.0526 0.038 Uiso calc 1 . . O O11 0.26117(18) 0.25056(13) 0.4272(4) 0.0445(6) Uani d 1 . . C C12 0.1638(3) 0.2617(2) 0.3896(6) 0.0426(8) Uani d 1 . . H H12A 0.1431 0.2208 0.2971 0.051 Uiso calc 1 . . H H12B 0.1266 0.2526 0.5011 0.051 Uiso calc 1 . . O O13 0.15012(16) 0.34454(15) 0.3247(4) 0.0436(6) Uani d 1 . . C C3A 0.2382(2) 0.37818(18) 0.3049(5) 0.0295(6) Uani d 1 . . C C14 0.2621(2) 0.45542(17) 0.2400(4) 0.0299(6) Uani d 1 . . H H14 0.2157 0.4937 0.1993 0.036 Uiso calc 1 . . C C15 0.35761(19) 0.47614(18) 0.2356(4) 0.0276(6) Uani d 1 . . C C16 0.4231(2) 0.4189(2) 0.2983(4) 0.0309(6) Uani d 1 . . H H16 0.4875 0.4339 0.2961 0.037 Uiso calc 1 . . C C17 0.3983(2) 0.34019(19) 0.3646(5) 0.0336(7) Uani d 1 . . H H17 0.4438 0.3015 0.4067 0.040 Uiso calc 1 . . C C7A 0.3045(2) 0.32183(18) 0.3656(4) 0.0317(6) Uani d 1 . . C C47 0.4015(2) 0.82057(17) 0.6718(4) 0.0262(6) Uani d 1 . . O O47 0.41835(17) 0.80559(13) 0.8317(3) 0.0366(5) Uani d 1 . . C C41 0.4064(2) 0.91022(16) 0.6064(5) 0.0277(6) Uani d 1 . . C C42 0.3281(2) 0.96071(19) 0.5945(6) 0.0384(8) Uani d 1 . . F F42 0.24359(14) 0.92331(12) 0.6222(4) 0.0620(8) Uani d 1 . . C C43 0.3316(3) 1.0447(2) 0.5555(7) 0.0476(9) Uani d 1 . . H H43 0.2760 1.0772 0.5492 0.057 Uiso calc 1 . . C C44 0.4181(3) 1.0804(2) 0.5258(5) 0.0432(9) Uani d 1 . . H H44 0.4221 1.1383 0.4980 0.052 Uiso calc 1 . . C C45 0.4992(2) 1.03346(19) 0.5357(5) 0.0375(8) Uani d 1 . . H H45 0.5587 1.0584 0.5158 0.045 Uiso calc 1 . . C C46 0.4913(2) 0.94955(18) 0.5754(5) 0.0303(6) Uani d 1 . . F F46 0.56966(12) 0.90206(13) 0.5843(4) 0.0464(6) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0308(11) 0.0227(11) 0.0214(11) -0.0015(9) -0.0005(9) 0.0023(9) C2 0.0356(14) 0.0296(15) 0.0254(14) -0.0041(12) -0.0029(12) 0.0090(13) C3 0.0399(14) 0.0214(12) 0.0293(16) -0.0025(11) -0.0088(12) 0.0068(12) N4 0.0347(11) 0.0173(10) 0.0274(13) -0.0015(9) -0.0039(10) 0.0052(9) C5 0.0328(12) 0.0169(11) 0.0243(13) -0.0024(10) -0.0002(11) 0.0029(11) C6 0.0267(12) 0.0220(13) 0.0241(14) 0.0012(10) 0.0000(11) 0.0044(11) C11 0.0400(15) 0.0328(15) 0.0232(14) 0.0002(13) 0.0051(12) -0.0003(12) O11 0.0469(14) 0.0305(11) 0.0563(17) 0.0005(10) -0.0008(12) 0.0081(11) C12 0.0465(19) 0.0387(17) 0.043(2) -0.0081(14) -0.0024(15) -0.0013(15) O13 0.0332(11) 0.0427(13) 0.0547(16) -0.0046(10) -0.0009(11) 0.0050(12) C3A 0.0282(13) 0.0343(14) 0.0260(14) 0.0040(12) -0.0012(11) -0.0043(12) C14 0.0338(13) 0.0308(13) 0.0252(14) 0.0072(12) -0.0048(12) -0.0008(13) C15 0.0371(14) 0.0266(13) 0.0191(12) 0.0031(11) 0.0018(11) -0.0044(11) C16 0.0283(12) 0.0336(16) 0.0307(15) 0.0059(11) 0.0018(12) -0.0063(13) C17 0.0374(14) 0.0270(14) 0.0365(17) 0.0093(12) -0.0025(13) -0.0011(13) C7A 0.0420(15) 0.0242(13) 0.0289(16) 0.0036(12) 0.0004(13) -0.0027(12) C47 0.0293(11) 0.0188(12) 0.0304(15) -0.0014(10) -0.0014(11) 0.0043(11) O47 0.0560(13) 0.0233(10) 0.0305(13) -0.0055(9) -0.0064(10) 0.0021(9) C41 0.0365(14) 0.0183(12) 0.0284(15) -0.0031(11) -0.0002(12) 0.0023(11) C42 0.0344(14) 0.0295(16) 0.051(2) -0.0016(12) 0.0038(14) 0.0095(15) F42 0.0323(9) 0.0451(11) 0.109(2) -0.0006(10) 0.0056(12) 0.0293(14) C43 0.0502(19) 0.0283(16) 0.064(3) 0.0091(14) 0.0094(18) 0.0128(16) C44 0.068(2) 0.0187(14) 0.043(2) -0.0038(14) 0.0079(17) 0.0061(13) C45 0.0461(17) 0.0282(14) 0.038(2) -0.0127(14) 0.0074(13) 0.0019(14) C46 0.0331(14) 0.0265(13) 0.0313(17) -0.0021(11) 0.0026(12) 0.0003(13) F46 0.0330(9) 0.0404(11) 0.0658(16) 0.0006(8) 0.0054(10) 0.0060(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N1 C6 . 1.464(4) ? N1 C2 . 1.466(3) ? N1 C11 . 1.469(4) ? C2 C3 . 1.513(4) ? C2 H2A . 0.9900 ? C2 H2B . 0.9900 ? C3 N4 . 1.466(4) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? N4 C47 . 1.343(4) ? N4 C5 . 1.465(3) ? C5 C6 . 1.507(4) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C11 C15 . 1.514(4) ? C11 H11A . 0.9900 ? C11 H11B . 0.9900 ? O11 C7A . 1.374(4) ? O11 C12 . 1.429(4) ? C12 O13 . 1.422(4) ? C12 H12A . 0.9900 ? C12 H12B . 0.9900 ? O13 C3A . 1.375(4) ? C3A C14 . 1.367(4) ? C3A C7A . 1.381(4) ? C14 C15 . 1.404(4) ? C14 H14 . 0.9500 ? C15 C16 . 1.388(4) ? C16 C17 . 1.395(5) ? C16 H16 . 0.9500 ? C17 C7A . 1.370(4) ? C17 H17 . 0.9500 ? C47 O47 . 1.227(4) ? C47 C41 . 1.513(4) ? C41 C42 . 1.382(4) ? C41 C46 . 1.384(4) ? C42 F42 . 1.362(3) ? C42 C43 . 1.373(4) ? C43 C44 . 1.379(5) ? C43 H43 . 0.9500 ? C44 C45 . 1.381(5) ? C44 H44 . 0.9500 ? C45 C46 . 1.377(4) ? C45 H45 . 0.9500 ? C46 F46 . 1.354(3) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 N1 C2 . . 107.9(2) ? C6 N1 C11 . . 111.2(2) ? C2 N1 C11 . . 111.8(2) ? N1 C2 C3 . . 110.1(3) ? N1 C2 H2A . . 109.6 ? C3 C2 H2A . . 109.6 ? N1 C2 H2B . . 109.6 ? C3 C2 H2B . . 109.6 ? H2A C2 H2B . . 108.2 ? N4 C3 C2 . . 111.0(2) ? N4 C3 H3A . . 109.4 ? C2 C3 H3A . . 109.4 ? N4 C3 H3B . . 109.4 ? C2 C3 H3B . . 109.4 ? H3A C3 H3B . . 108.0 ? C47 N4 C5 . . 118.8(3) ? C47 N4 C3 . . 125.6(2) ? C5 N4 C3 . . 114.9(2) ? N4 C5 C6 . . 110.5(2) ? N4 C5 H5A . . 109.6 ? C6 C5 H5A . . 109.6 ? N4 C5 H5B . . 109.6 ? C6 C5 H5B . . 109.6 ? H5A C5 H5B . . 108.1 ? N1 C6 C5 . . 109.5(2) ? N1 C6 H6A . . 109.8 ? C5 C6 H6A . . 109.8 ? N1 C6 H6B . . 109.8 ? C5 C6 H6B . . 109.8 ? H6A C6 H6B . . 108.2 ? N1 C11 C15 . . 111.4(2) ? N1 C11 H11A . . 109.3 ? C15 C11 H11A . . 109.3 ? N1 C11 H11B . . 109.3 ? C15 C11 H11B . . 109.3 ? H11A C11 H11B . . 108.0 ? C7A O11 C12 . . 105.7(2) ? O13 C12 O11 . . 108.4(3) ? O13 C12 H12A . . 110.0 ? O11 C12 H12A . . 110.0 ? O13 C12 H12B . . 110.0 ? O11 C12 H12B . . 110.0 ? H12A C12 H12B . . 108.4 ? C3A O13 C12 . . 105.9(2) ? C14 C3A O13 . . 128.2(3) ? C14 C3A C7A . . 122.1(3) ? O13 C3A C7A . . 109.7(3) ? C3A C14 C15 . . 117.6(3) ? C3A C14 H14 . . 121.2 ? C15 C14 H14 . . 121.2 ? C16 C15 C14 . . 119.4(3) ? C16 C15 C11 . . 120.5(3) ? C14 C15 C11 . . 120.0(3) ? C15 C16 C17 . . 122.6(3) ? C15 C16 H16 . . 118.7 ? C17 C16 H16 . . 118.7 ? C7A C17 C16 . . 116.3(3) ? C7A C17 H17 . . 121.8 ? C16 C17 H17 . . 121.8 ? C17 C7A O11 . . 128.3(3) ? C17 C7A C3A . . 121.9(3) ? O11 C7A C3A . . 109.8(3) ? O47 C47 N4 . . 123.4(3) ? O47 C47 C41 . . 118.8(3) ? N4 C47 C41 . . 117.8(3) ? C42 C41 C46 . . 115.6(2) ? C42 C41 C47 . . 122.4(2) ? C46 C41 C47 . . 121.6(3) ? F42 C42 C43 . . 119.5(3) ? F42 C42 C41 . . 116.8(2) ? C43 C42 C41 . . 123.7(3) ? C42 C43 C44 . . 118.0(3) ? C42 C43 H43 . . 121.0 ? C44 C43 H43 . . 121.0 ? C43 C44 C45 . . 121.2(3) ? C43 C44 H44 . . 119.4 ? C45 C44 H44 . . 119.4 ? C46 C45 C44 . . 118.1(3) ? C46 C45 H45 . . 120.9 ? C44 C45 H45 . . 120.9 ? F46 C46 C45 . . 119.2(3) ? F46 C46 C41 . . 117.4(2) ? C45 C46 C41 . . 123.3(3) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 N1 C2 C3 . . . . -63.5(3) ? C11 N1 C2 C3 . . . . 173.9(2) ? N1 C2 C3 N4 . . . . 54.5(3) ? C2 C3 N4 C47 . . . . 142.2(3) ? C2 C3 N4 C5 . . . . -48.1(3) ? C47 N4 C5 C6 . . . . -140.1(3) ? C3 N4 C5 C6 . . . . 49.5(3) ? C2 N1 C6 C5 . . . . 65.0(3) ? C11 N1 C6 C5 . . . . -172.1(2) ? N4 C5 C6 N1 . . . . -57.3(3) ? C6 N1 C11 C15 . . . . 62.1(3) ? C2 N1 C11 C15 . . . . -177.2(2) ? C7A O11 C12 O13 . . . . -6.7(4) ? O11 C12 O13 C3A . . . . 6.5(4) ? C12 O13 C3A C14 . . . . 177.4(3) ? C12 O13 C3A C7A . . . . -3.9(4) ? O13 C3A C14 C15 . . . . 179.0(3) ? C7A C3A C14 C15 . . . . 0.4(5) ? C3A C14 C15 C16 . . . . -0.8(4) ? C3A C14 C15 C11 . . . . -177.6(3) ? N1 C11 C15 C16 . . . . -107.8(3) ? N1 C11 C15 C14 . . . . 69.0(4) ? C14 C15 C16 C17 . . . . 0.8(5) ? C11 C15 C16 C17 . . . . 177.6(3) ? C15 C16 C17 C7A . . . . -0.3(5) ? C16 C17 C7A O11 . . . . -178.2(3) ? C16 C17 C7A C3A . . . . -0.2(5) ? C12 O11 C7A C17 . . . . -177.4(4) ? C12 O11 C7A C3A . . . . 4.4(4) ? C14 C3A C7A C17 . . . . 0.1(5) ? O13 C3A C7A C17 . . . . -178.7(3) ? C14 C3A C7A O11 . . . . 178.5(3) ? O13 C3A C7A O11 . . . . -0.4(4) ? C5 N4 C47 O47 . . . . 3.6(4) ? C3 N4 C47 O47 . . . . 173.0(3) ? C5 N4 C47 C41 . . . . -175.7(2) ? C3 N4 C47 C41 . . . . -6.3(4) ? O47 C47 C41 C42 . . . . -95.9(4) ? N4 C47 C41 C42 . . . . 83.4(4) ? O47 C47 C41 C46 . . . . 76.3(4) ? N4 C47 C41 C46 . . . . -104.4(4) ? C46 C41 C42 F42 . . . . 179.2(3) ? C47 C41 C42 F42 . . . . -8.2(5) ? C46 C41 C42 C43 . . . . -0.2(6) ? C47 C41 C42 C43 . . . . 172.4(4) ? F42 C42 C43 C44 . . . . -179.1(4) ? C41 C42 C43 C44 . . . . 0.3(7) ? C42 C43 C44 C45 . . . . -0.3(7) ? C43 C44 C45 C46 . . . . 0.3(6) ? C44 C45 C46 F46 . . . . 179.4(3) ? C44 C45 C46 C41 . . . . -0.3(5) ? C42 C41 C46 F46 . . . . -179.5(3) ? C47 C41 C46 F46 . . . . 7.8(5) ? C42 C41 C46 C45 . . . . 0.3(5) ? C47 C41 C46 C45 . . . . -172.4(3) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C45 H45 O47 2_674 0.95 2.58 3.204(4) 123 no _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.905 _shelx_estimated_absorpt_T_max 0.981 _shelx_hkl_file ; 0 0 -1 -0.10 0.20 0 0 -2 194.58 8.40 0 0 -3 -0.10 0.40 0 0 -4 2556.64 103.39 0 0 -5 0.00 0.60 0 0 -6 13.90 2.10 0 0 -7 -0.30 0.90 0 0 -8 29.50 3.60 1 0 -8 -0.20 1.10 1 0 -7 -0.50 0.90 1 0 -6 -0.30 0.80 1 0 -5 -0.10 0.70 1 0 -4 -0.20 0.60 1 0 -3 -0.20 0.40 1 0 -2 -0.40 0.40 1 0 -1 -1.50 0.10 1 0 -1 -1.40 0.20 1 0 0 -0.30 0.10 -1 0 -1 -1.50 0.10 -1 0 -2 -0.30 0.30 -1 0 -3 0.00 0.40 -1 0 -4 0.40 0.60 -1 0 -5 0.10 0.60 -1 0 -6 0.00 0.70 -1 0 -7 -0.40 0.80 -1 0 -8 0.30 1.00 2 0 -8 13.60 2.90 2 0 -7 21.30 3.00 2 0 -6 30.90 3.20 2 0 -5 34.60 3.10 2 0 -4 248.18 11.40 2 0 -3 925.21 36.80 2 0 -2 1023.20 41.70 2 0 -1 3236.08 120.69 2 0 -1 2903.61 124.59 2 0 0 368.76 15.50 2 0 0 377.46 14.80 2 0 1 3348.47 133.79 -2 0 -2 1049.30 41.80 2 0 2 1058.69 40.80 -2 0 -3 1008.10 40.50 -2 0 -4 248.68 10.90 -2 0 -5 34.70 2.80 -2 0 -6 31.80 3.00 -2 0 -7 22.90 2.70 3 0 -8 -0.20 1.00 3 0 -7 -0.40 0.90 3 0 -6 0.20 0.90 3 0 -5 0.20 0.60 3 0 -4 0.10 0.60 3 0 -3 -0.20 0.50 3 0 -2 -0.10 0.10 3 0 -2 -0.10 0.30 3 0 -1 -0.10 0.10 3 0 -1 -0.30 0.20 3 0 0 -0.60 0.30 3 0 1 -0.20 0.10 -3 0 -2 -0.10 0.20 3 0 2 -0.10 0.10 -3 0 -3 -0.10 0.30 3 0 3 -0.10 0.10 -3 0 -4 0.20 0.40 3 0 4 0.00 0.10 -3 0 -5 0.10 0.50 3 0 5 -0.10 0.20 -3 0 -6 -0.40 0.60 3 0 6 0.00 0.20 3 0 7 0.10 0.30 3 0 8 -0.10 1.00 4 0 -8 20.00 3.20 4 0 -7 -0.10 1.00 4 0 -6 69.39 5.20 4 0 -5 159.08 8.50 4 0 -3 135.39 5.50 4 0 -3 140.49 6.80 4 0 -2 326.67 12.90 4 0 -2 337.67 13.90 4 0 -1 82.99 3.50 4 0 -1 82.19 3.90 4 0 -1 78.89 3.30 4 0 0 4063.69 166.38 4 0 1 83.89 3.40 -4 0 -2 357.56 14.00 4 0 2 356.86 13.80 -4 0 -3 146.89 6.40 4 0 3 148.29 5.80 -4 0 -4 154.18 7.10 4 0 4 155.38 6.20 -4 0 -5 164.18 7.90 4 0 5 169.58 6.70 4 0 6 75.69 3.30 4 0 7 0.30 0.30 4 0 8 15.50 3.00 -5 0 9 0.40 0.90 5 0 -8 -0.50 0.90 5 0 -7 -0.30 1.00 5 0 -6 -0.20 0.90 5 0 -5 0.20 0.80 5 0 -4 -0.20 0.50 5 0 -3 -0.30 0.50 5 0 -3 0.00 0.20 5 0 -2 0.10 0.10 5 0 -2 -0.10 0.40 5 0 -1 -0.20 0.10 5 0 -1 0.00 0.30 -5 0 0 0.20 0.20 5 0 0 0.30 0.10 5 0 1 -0.30 0.10 5 0 2 0.10 0.10 -5 0 -3 -0.10 0.20 5 0 3 -0.10 0.10 -5 0 -4 0.10 0.40 5 0 4 -0.10 0.20 5 0 5 0.20 0.20 5 0 6 -0.20 0.20 5 0 8 -0.20 1.00 6 0 -7 4.00 1.80 6 0 -6 126.49 7.80 6 0 -5 4.80 1.50 6 0 -4 75.89 3.30 6 0 -4 72.29 4.70 6 0 -3 463.95 18.20 6 0 -3 470.95 19.70 6 0 -2 96.59 4.10 6 0 -2 100.09 5.10 6 0 -1 124.99 5.20 6 0 -1 123.89 5.80 6 0 -1 134.59 5.80 -6 0 0 1267.27 66.49 6 0 0 1308.37 50.19 6 0 1 129.99 5.20 6 0 2 98.99 4.00 -6 0 -3 489.25 19.20 6 0 3 494.85 19.00 6 0 4 76.89 3.20 6 0 5 5.40 0.50 6 0 6 121.79 5.10 6 0 8 2.30 1.60 6 0 9 1.10 1.40 7 0 -7 0.90 1.30 7 0 -6 0.70 1.10 7 0 -5 -0.40 0.70 7 0 -4 0.20 0.30 7 0 -4 0.90 0.90 7 0 -3 0.30 0.30 7 0 -3 0.20 0.60 7 0 -2 -0.30 0.20 7 0 -2 -0.20 0.10 7 0 -2 -0.10 0.50 7 0 -1 -0.20 0.30 7 0 -1 0.00 0.20 7 0 -1 -0.20 0.30 -7 0 0 0.50 0.30 7 0 0 0.50 0.20 7 0 1 -0.10 0.20 7 0 2 -0.10 0.20 7 0 3 0.20 0.20 7 0 4 0.10 0.20 7 0 5 0.20 0.20 7 0 6 0.00 0.30 7 0 8 0.00 1.10 -8 0 8 3.80 1.50 8 0 -7 20.50 3.20 8 0 -6 9.00 2.20 8 0 -5 21.50 2.70 8 0 -4 42.30 2.10 8 0 -4 40.40 3.40 8 0 -3 145.99 5.90 8 0 -3 140.59 7.30 8 0 -2 157.08 7.30 8 0 -2 144.89 6.10 -8 0 1 103.39 5.00 8 0 -1 103.19 4.30 8 0 -1 104.19 5.20 -8 0 0 1102.39 44.00 8 0 0 1106.79 42.70 -8 0 -1 108.99 4.30 8 0 1 107.79 4.50 8 0 2 147.89 6.00 8 0 3 131.59 5.30 8 0 4 37.60 1.80 8 0 5 21.10 1.20 8 0 6 11.00 0.80 8 0 8 2.00 1.70 -9 0 8 -0.30 0.90 9 0 -6 -0.10 0.90 9 0 -5 -0.60 0.30 9 0 -5 0.20 0.90 9 0 -4 -0.20 0.30 9 0 -4 0.20 0.80 9 0 -3 0.50 0.70 9 0 -3 -0.10 0.30 9 0 -2 -0.10 0.20 -9 0 1 -0.20 0.40 9 0 -1 0.30 0.50 9 0 -1 0.10 0.20 9 0 0 0.70 0.60 9 0 0 0.60 0.30 9 0 1 0.00 0.20 9 0 2 -0.20 0.20 9 0 3 0.00 0.20 9 0 4 0.00 0.20 9 0 5 0.00 0.20 9 0 6 0.20 0.30 9 0 8 -0.50 1.20 -10 0 7 1.80 1.20 10 0 -5 47.80 2.50 10 0 -4 26.50 2.80 10 0 -4 24.80 1.50 10 0 -3 23.30 1.40 -10 0 2 126.39 6.50 10 0 -2 131.99 5.50 -10 0 1 121.79 5.90 10 0 -1 122.29 5.10 10 0 0 66.49 4.40 10 0 0 67.49 3.00 10 0 1 117.19 4.90 10 0 2 127.49 5.30 10 0 3 19.80 1.10 10 0 4 21.30 1.20 10 0 5 39.20 1.90 10 0 6 61.59 3.40 10 0 7 2.40 2.00 -11 0 7 0.20 1.00 -11 0 6 0.20 0.90 -11 0 5 0.20 0.80 11 0 -5 -0.10 0.40 -11 0 4 -0.20 0.70 11 0 -4 -0.10 0.30 -11 0 3 0.00 0.70 11 0 -3 0.30 0.40 -11 0 2 0.00 0.60 11 0 -2 -0.10 0.30 11 0 -1 -0.10 0.30 11 0 1 -0.20 0.30 11 0 1 -0.20 0.60 11 0 2 0.10 0.30 11 0 3 -0.10 0.20 11 0 4 0.00 0.30 11 0 5 0.10 0.30 11 0 6 -0.60 1.00 11 0 7 -0.10 1.30 -12 0 7 5.50 1.80 -12 0 6 3.10 1.40 -12 0 5 30.50 3.20 12 0 -5 39.60 2.20 -12 0 4 58.99 4.40 12 0 -4 69.99 3.20 -12 0 3 15.30 2.10 12 0 -3 20.60 1.40 12 0 -2 25.20 1.50 12 0 -1 162.28 6.80 12 0 0 527.65 20.70 12 0 1 151.78 6.30 12 0 1 151.08 8.70 12 0 2 23.90 1.40 12 0 2 23.70 3.20 12 0 3 17.40 1.10 12 0 4 53.59 2.50 12 0 5 29.90 1.60 12 0 5 30.90 4.20 12 0 6 3.20 2.10 12 0 7 5.60 3.80 -13 0 6 0.30 0.90 -13 0 5 -0.30 0.80 13 0 -5 0.10 0.50 -13 0 4 -0.40 0.70 13 0 -4 0.50 0.50 13 0 -3 0.50 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2 -2 77.19 4.20 7 2 -2 74.99 3.20 7 2 -1 101.59 4.20 7 2 -1 101.89 4.90 7 2 0 96.09 4.00 7 2 0 97.49 4.40 7 2 1 100.79 4.10 7 2 2 74.69 3.10 7 2 3 267.87 10.50 7 2 4 70.49 3.10 7 2 5 3.60 0.50 7 2 6 3.30 0.50 7 2 7 18.00 1.20 8 2 -8 2.70 1.70 8 2 -7 25.70 3.50 8 2 -6 12.40 2.30 8 2 -5 23.90 1.40 8 2 -5 24.90 2.90 8 2 -4 8.50 1.60 8 2 -4 8.60 0.80 8 2 -3 3.60 0.50 8 2 -3 2.30 0.90 8 2 -2 82.89 4.60 8 2 -2 84.09 3.60 8 2 -1 97.99 4.80 8 2 -1 95.09 4.00 8 2 0 13.80 0.80 8 2 0 12.80 1.10 8 2 1 93.09 3.90 8 2 2 79.49 3.40 8 2 3 2.80 0.40 8 2 4 8.60 0.70 8 2 5 24.80 1.40 8 2 6 15.40 1.10 8 2 7 27.60 1.60 9 2 -8 1.10 1.50 9 2 -7 11.60 2.70 9 2 -6 7.40 2.10 9 2 -5 1.60 0.50 9 2 -5 2.60 1.30 9 2 -4 38.20 3.30 9 2 -4 41.70 2.10 9 2 -3 66.29 3.00 9 2 -3 65.69 4.30 9 2 -2 105.09 4.50 9 2 -2 109.79 5.70 9 2 -1 4.90 0.90 9 2 -1 4.00 0.50 9 2 0 20.30 1.50 9 2 0 19.80 1.10 9 2 1 4.80 0.50 9 2 2 102.69 4.30 9 2 3 62.49 2.80 9 2 4 39.50 1.90 9 2 5 1.60 0.40 9 2 6 7.20 0.80 9 2 7 13.90 1.10 10 2 -7 2.90 1.70 10 2 -6 2.10 1.40 10 2 -5 6.90 1.90 10 2 -5 7.70 0.90 10 2 -4 18.40 2.40 10 2 -4 19.50 1.30 10 2 -3 23.70 2.40 10 2 -3 26.00 1.50 10 2 -2 123.49 6.30 10 2 -2 118.89 5.10 10 2 -1 188.98 8.50 10 2 -1 186.28 7.60 10 2 0 4.40 0.50 10 2 1 180.38 7.30 10 2 2 112.79 4.70 10 2 3 20.90 1.20 10 2 4 17.00 1.10 10 2 5 6.00 0.70 10 2 6 3.30 0.60 10 2 7 4.40 0.70 11 2 -7 28.00 3.70 11 2 -6 25.10 3.30 11 2 -5 3.40 0.60 11 2 -5 3.40 1.40 11 2 -4 7.30 1.80 11 2 -4 9.50 0.90 11 2 -3 271.97 12.70 11 2 -3 278.27 11.10 11 2 -2 106.99 5.80 11 2 -2 105.79 4.60 11 2 -1 33.60 1.80 11 2 0 48.30 2.30 11 2 1 31.60 1.70 11 2 2 96.59 4.10 11 2 3 248.78 9.90 11 2 4 7.30 0.70 11 2 5 3.70 0.60 11 2 6 25.10 1.50 12 2 -6 21.30 1.60 12 2 -6 18.40 2.90 12 2 -5 25.10 1.60 12 2 -5 21.50 2.90 12 2 -4 94.89 4.20 12 2 -4 84.79 5.70 12 2 -3 8.90 1.80 12 2 -3 10.20 1.00 12 2 -2 198.58 8.20 12 2 -1 61.79 2.90 12 2 0 114.69 4.90 12 2 1 58.99 2.80 12 2 2 191.48 7.80 12 2 3 9.00 0.80 12 2 4 73.89 3.30 12 2 5 19.60 1.20 12 2 6 17.00 1.20 13 2 -6 14.20 1.30 13 2 -5 39.30 3.90 13 2 -5 42.50 2.40 13 2 -4 89.29 6.00 13 2 -4 96.29 4.30 13 2 -3 43.70 2.30 13 2 -2 61.69 3.00 13 2 -1 20.50 1.40 13 2 0 153.98 6.50 13 2 1 17.50 1.20 13 2 2 54.29 2.60 13 2 3 37.20 1.90 13 2 4 80.89 3.60 13 2 5 32.00 1.80 13 2 6 11.40 1.00 -14 -2 6 12.10 2.20 14 2 -6 16.70 1.40 -14 -2 5 5.50 1.60 14 2 -5 8.10 1.10 14 2 -4 21.70 1.60 14 2 -3 47.90 2.50 14 2 -2 0.60 0.40 14 2 -1 34.00 2.00 14 2 0 1.50 0.50 14 2 1 34.80 1.90 14 2 2 0.90 0.40 14 2 3 40.50 2.10 14 2 4 17.10 1.20 14 2 5 5.60 0.70 14 2 6 12.50 1.10 15 2 -5 2.90 0.80 15 2 -4 1.10 0.50 15 2 -3 12.30 1.10 15 2 -2 20.20 1.40 15 2 -1 6.70 0.90 15 2 0 0.50 0.40 15 2 1 5.10 0.70 15 2 2 17.90 1.30 15 2 3 10.10 0.90 15 2 4 1.30 0.50 15 2 5 1.90 0.50 16 2 -4 5.10 1.00 16 2 -3 0.00 0.50 16 2 -2 2.80 0.60 16 2 -1 4.80 0.80 16 2 0 10.20 1.00 16 2 1 4.40 0.70 16 2 2 3.10 0.60 16 2 3 0.00 1.10 16 2 3 0.40 0.40 16 2 4 4.70 0.70 16 2 4 4.90 2.20 17 2 -3 1.60 0.70 17 2 -2 2.80 0.70 17 2 -1 1.80 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5.70 -3 -3 4 143.39 6.40 3 3 -4 149.69 7.50 -3 -3 3 25.90 1.50 3 3 -3 28.00 1.20 3 3 -3 27.60 2.20 3 3 -2 123.39 5.00 3 3 -2 127.69 5.90 3 3 -1 297.57 11.30 3 3 -1 287.37 11.90 3 3 0 1621.24 62.79 3 3 0 1635.64 64.09 3 3 1 350.46 13.30 3 3 1 317.17 12.90 3 3 2 147.89 5.70 3 3 2 141.99 5.90 3 3 3 33.20 1.50 3 3 3 32.10 1.90 3 3 4 182.58 7.20 3 3 4 178.88 8.00 3 3 5 96.49 5.00 3 3 6 46.40 3.20 3 3 7 56.49 2.70 3 3 8 5.40 0.70 4 3 -9 5.80 2.30 4 3 -8 26.30 3.50 4 3 -7 7.10 1.90 4 3 -6 38.80 3.60 4 3 -5 15.20 2.10 4 3 -4 6.50 1.30 4 3 -3 25.10 1.20 4 3 -3 24.70 2.10 4 3 -2 138.79 6.60 4 3 -2 145.79 5.60 4 3 -1 546.25 22.10 4 3 -1 572.54 21.80 4 3 0 6.80 0.40 4 3 0 6.80 0.60 4 3 1 644.04 24.10 4 3 1 571.44 23.50 4 3 2 171.28 6.70 4 3 2 170.08 6.70 4 3 3 27.40 1.30 4 3 3 28.40 1.60 4 3 4 8.90 0.60 4 3 4 7.80 1.00 4 3 5 13.10 1.40 4 3 5 15.10 0.90 4 3 6 48.00 2.30 4 3 7 10.00 0.90 4 3 8 29.20 1.70 5 3 -8 16.50 3.00 5 3 -7 49.00 4.50 5 3 -6 19.10 2.60 5 3 -5 18.80 2.30 5 3 -4 160.08 8.20 5 3 -4 161.58 6.50 5 3 -2 253.17 10.90 5 3 -2 247.88 9.80 5 3 -1 3.60 0.70 5 3 -1 4.10 0.40 5 3 0 0.30 0.20 5 3 0 -0.10 0.10 5 3 1 4.30 0.40 5 3 1 4.10 0.40 5 3 2 284.47 11.50 5 3 2 303.07 11.60 5 3 3 1.80 0.30 5 3 3 1.90 0.40 5 3 4 175.78 7.00 5 3 4 172.48 7.40 5 3 5 23.40 1.30 5 3 6 24.40 1.40 5 3 7 57.69 2.80 5 3 8 15.60 1.20 6 3 -8 17.80 3.10 6 3 -7 8.50 2.30 6 3 -6 2.40 1.30 6 3 -5 22.80 2.60 6 3 -4 201.78 8.00 6 3 -4 199.68 9.80 6 3 -3 8.30 0.60 6 3 -3 9.50 1.40 6 3 -2 82.49 3.40 6 3 -2 81.29 4.40 6 3 -1 13.60 1.30 6 3 -1 16.00 0.80 6 3 0 944.61 38.10 6 3 1 14.90 0.90 6 3 1 15.50 0.80 6 3 2 90.69 3.60 6 3 2 85.89 3.50 6 3 3 8.10 0.60 6 3 4 232.68 9.20 6 3 5 24.50 1.40 6 3 6 2.10 0.50 6 3 7 8.90 0.90 6 3 8 20.10 1.40 7 3 -8 0.00 1.10 7 3 -7 8.20 2.30 7 3 -6 34.90 3.50 7 3 -5 67.49 4.90 7 3 -5 70.49 3.10 7 3 -4 137.79 5.50 7 3 -4 124.69 7.00 7 3 -3 3.00 0.40 7 3 -3 2.50 0.90 7 3 -2 138.29 6.60 7 3 -2 135.69 5.60 7 3 -1 247.38 9.50 7 3 -1 234.58 10.30 7 3 0 13.60 0.80 7 3 0 11.90 1.00 7 3 1 232.98 9.30 7 3 1 237.48 9.40 7 3 2 148.89 6.00 7 3 3 2.80 0.40 7 3 4 150.18 6.10 7 3 5 75.59 3.30 7 3 6 40.10 2.00 7 3 7 10.00 0.90 7 3 8 0.80 0.50 8 3 -8 5.50 2.30 8 3 -7 35.60 4.00 8 3 -6 25.30 3.20 8 3 -5 28.40 3.00 8 3 -5 32.20 1.70 8 3 -4 81.79 3.50 8 3 -4 74.29 4.90 8 3 -3 70.59 4.40 8 3 -3 73.19 3.20 8 3 -2 -0.10 0.20 8 3 -2 0.20 0.50 8 3 -1 358.66 14.90 8 3 -1 359.46 14.10 8 3 0 87.49 3.60 8 3 0 85.79 4.10 8 3 1 358.76 14.00 8 3 2 0.10 0.20 8 3 3 78.49 3.40 8 3 4 88.29 3.80 8 3 5 34.20 1.80 8 3 6 31.10 1.70 8 3 7 38.20 2.10 9 3 -8 30.10 5.30 9 3 -7 18.80 3.10 9 3 -6 7.00 1.90 9 3 -5 4.30 0.70 9 3 -5 2.80 1.20 9 3 -4 22.50 2.50 9 3 -4 25.40 1.40 9 3 -3 113.59 6.20 9 3 -3 116.39 4.90 9 3 -2 12.90 1.50 9 3 -1 73.39 4.00 9 3 0 127.29 5.70 9 3 0 127.49 5.30 9 3 1 69.29 3.00 9 3 2 12.20 0.80 9 3 3 113.49 4.70 9 3 4 23.40 1.30 9 3 5 3.40 0.50 9 3 6 9.90 0.90 9 3 7 19.30 1.40 10 3 -7 0.10 1.10 10 3 -6 86.29 6.10 10 3 -5 11.60 2.10 10 3 -5 11.00 1.00 10 3 -4 24.20 1.40 10 3 -4 19.90 2.40 10 3 -3 7.30 1.40 10 3 -3 6.80 0.70 10 3 -2 35.20 2.70 10 3 -2 37.60 1.90 10 3 -1 22.80 1.30 10 3 -1 21.00 1.80 10 3 0 0.20 0.20 10 3 1 22.00 1.20 10 3 2 34.10 1.70 10 3 3 5.60 0.60 10 3 4 21.30 1.20 10 3 5 10.70 0.90 10 3 6 91.59 4.10 10 3 7 0.10 0.40 11 3 -7 14.60 3.10 11 3 -6 8.50 1.00 11 3 -6 7.40 2.10 11 3 -5 62.59 2.90 11 3 -5 52.99 4.50 11 3 -4 35.00 3.30 11 3 -4 41.20 2.10 11 3 -3 47.50 2.30 11 3 -3 45.30 3.50 11 3 -2 9.30 1.50 11 3 -2 11.60 0.90 11 3 -1 51.99 2.50 11 3 0 27.80 1.50 11 3 1 50.09 2.40 11 3 2 9.40 0.70 11 3 3 43.30 2.10 11 3 4 31.00 1.60 11 3 5 56.49 2.70 11 3 6 7.60 0.90 11 3 7 14.30 1.20 12 3 -7 20.50 3.30 12 3 -6 1.60 0.60 12 3 -6 0.80 1.20 12 3 -5 6.60 1.90 12 3 -5 7.00 0.90 12 3 -4 8.80 1.90 12 3 -4 10.70 1.00 12 3 -3 1.60 1.00 12 3 -3 2.30 0.50 12 3 -2 38.10 2.00 12 3 -1 145.49 6.10 12 3 0 1.60 0.40 12 3 1 138.99 5.80 12 3 2 35.00 1.80 12 3 3 2.40 0.50 12 3 4 9.70 0.80 12 3 5 6.70 0.80 12 3 6 0.90 0.40 12 3 7 18.30 1.30 13 3 -6 12.10 2.50 13 3 -6 12.40 1.20 13 3 -5 0.80 1.10 13 3 -5 1.20 0.60 13 3 -4 23.90 1.60 13 3 -4 23.80 2.80 13 3 -3 7.20 0.90 13 3 -2 104.79 4.70 13 3 -1 17.60 1.20 13 3 0 104.29 4.60 13 3 1 19.10 1.30 13 3 2 90.39 4.00 13 3 3 5.30 0.70 13 3 4 20.70 1.30 13 3 5 0.70 0.40 13 3 6 9.70 0.90 14 3 -6 10.60 1.20 14 3 -5 3.50 0.80 14 3 -5 3.90 1.60 14 3 -4 1.00 0.50 14 3 -3 32.60 1.90 14 3 -2 5.60 0.80 14 3 -1 8.50 0.90 14 3 0 0.20 0.40 14 3 1 7.60 0.80 14 3 2 4.10 0.60 14 3 3 28.10 1.60 14 3 4 1.00 0.40 14 3 5 3.80 0.60 14 3 6 8.00 0.90 15 3 -5 7.50 1.10 15 3 -4 18.50 1.50 15 3 -3 7.70 1.00 15 3 -2 2.10 0.60 15 3 -1 1.00 0.50 15 3 0 11.40 1.00 15 3 1 1.30 0.50 15 3 2 1.70 0.50 15 3 3 8.20 0.90 15 3 4 15.20 1.20 15 3 5 6.30 0.80 16 3 -4 2.50 0.70 16 3 -3 7.40 1.00 16 3 -2 8.30 1.00 16 3 -1 1.50 0.50 16 3 0 2.90 0.60 16 3 1 1.50 0.50 16 3 2 8.80 0.90 16 3 3 7.10 0.90 16 3 4 2.60 0.60 17 3 -2 0.20 0.50 17 3 -1 3.40 0.70 17 3 0 11.80 1.10 17 3 1 3.50 0.70 17 3 2 0.30 0.40 17 3 3 5.20 0.80 18 -4 1 31.60 2.10 18 -4 0 36.20 2.30 18 -4 -1 36.90 2.70 17 -4 1 -0.10 0.40 17 -4 0 37.60 2.30 17 -4 -1 0.50 0.50 17 -4 -2 8.20 1.20 16 -4 4 7.20 2.80 16 -4 3 8.70 2.70 16 -4 2 8.80 1.00 16 -4 1 11.80 1.10 16 -4 0 12.30 1.20 16 -4 -1 12.10 1.30 16 -4 -2 10.00 1.30 16 -4 -3 9.70 1.30 16 -4 -4 11.40 2.10 15 -4 5 0.20 1.50 15 -4 4 -0.20 1.30 15 -4 3 14.30 3.10 15 -4 2 2.80 1.70 15 -4 2 4.10 0.70 15 -4 1 22.90 1.60 15 -4 0 16.10 1.30 15 -4 -1 24.20 1.70 15 -4 -2 4.40 0.80 15 -4 -3 15.60 1.40 15 -4 -4 1.00 0.60 14 -4 5 -0.60 1.30 14 -4 4 8.50 2.70 14 -4 3 20.00 3.40 14 -4 2 0.20 0.40 14 -4 2 0.40 1.20 14 -4 1 12.10 1.10 14 -4 1 10.80 2.70 14 -4 0 8.60 0.90 14 -4 -1 11.50 1.10 14 -4 -2 -0.20 0.40 14 -4 -3 20.30 1.50 14 -4 -4 13.30 1.30 -14 4 4 11.10 2.10 -14 4 5 -0.40 0.90 -14 4 6 6.60 2.10 13 -4 6 19.30 4.00 13 -4 5 8.90 3.00 13 -4 4 16.40 3.40 13 -4 3 27.40 3.90 13 -4 2 16.30 1.20 13 -4 2 13.70 2.60 13 -4 1 70.69 5.50 13 -4 1 68.39 3.30 13 -4 0 1.70 0.50 13 -4 -1 70.79 3.40 13 -4 -2 18.20 1.40 13 -4 -3 31.50 1.90 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2 39.40 1.90 10 -4 2 39.60 4.00 10 -4 1 105.49 4.40 10 -4 1 101.39 6.50 10 -4 0 9.80 1.70 10 -4 0 10.10 0.80 -10 4 0 10.20 0.90 10 -4 -1 95.69 5.20 10 -4 -1 99.49 4.30 -10 4 1 98.39 4.90 10 -4 -2 39.00 2.00 -10 4 2 40.00 2.90 10 -4 -3 3.90 0.60 -10 4 3 4.80 1.30 10 -4 -4 145.69 6.00 -10 4 4 129.29 7.50 -10 4 5 3.30 1.40 -10 4 6 12.20 2.40 -10 4 7 7.30 2.10 9 -4 8 13.00 3.60 9 -4 7 3.50 2.00 9 -4 6 8.70 2.70 9 -4 5 23.60 3.60 9 -4 4 9.10 2.50 9 -4 3 15.70 2.70 9 -4 3 14.70 0.90 9 -4 2 66.09 5.10 9 -4 2 64.09 2.80 9 -4 1 37.70 3.40 9 -4 1 37.30 1.80 -9 4 -1 37.10 1.90 9 -4 0 482.05 20.70 9 -4 0 484.05 18.90 -9 4 0 488.45 19.20 9 -4 -1 39.30 1.90 9 -4 -1 38.20 2.60 -9 4 1 36.90 2.40 9 -4 -2 68.79 3.00 -9 4 2 62.49 3.90 9 -4 -3 14.50 1.10 -9 4 3 15.80 2.00 -9 4 4 10.70 1.80 -9 4 5 22.80 2.70 -9 4 6 8.70 2.10 -9 4 7 4.00 1.60 8 -4 8 0.20 1.40 8 -4 7 30.00 4.40 8 -4 6 82.59 7.00 8 -4 5 6.90 2.20 8 -4 4 35.40 4.00 8 -4 3 3.00 0.40 8 -4 3 3.00 1.40 8 -4 2 166.88 9.30 8 -4 2 172.78 6.80 8 -4 1 35.50 3.20 8 -4 1 34.90 1.70 -8 4 -1 37.10 1.70 8 -4 0 114.19 4.70 8 -4 0 114.39 6.10 -8 4 0 113.59 5.00 8 -4 -1 34.50 2.40 8 -4 -1 39.50 1.80 -8 4 1 35.20 2.30 8 -4 -2 170.38 7.00 -8 4 2 174.38 8.10 8 -4 -3 2.70 0.50 -8 4 3 2.20 0.90 -8 4 4 34.20 3.00 -8 4 5 6.20 1.60 -8 4 6 83.49 5.70 -8 4 7 29.90 3.40 -8 4 8 0.80 1.20 7 -4 8 31.80 4.60 7 -4 7 9.40 2.80 7 -4 6 68.19 6.20 7 -4 5 26.90 3.60 7 -4 4 11.50 2.40 7 -4 3 1.30 1.10 7 -4 3 1.60 0.30 7 -4 2 28.70 1.40 7 -4 2 27.90 3.00 -7 4 -2 30.20 1.60 7 -4 1 27.20 2.60 7 -4 1 28.50 1.40 -7 4 -1 28.00 1.40 7 -4 0 62.99 2.60 7 -4 0 58.39 3.70 -7 4 0 60.99 2.90 7 -4 -1 28.80 1.40 7 -4 -1 25.60 1.90 -7 4 1 26.70 1.80 7 -4 -2 28.50 1.50 -7 4 2 29.40 2.30 7 -4 -3 2.00 0.40 -7 4 3 1.30 0.70 -7 4 4 10.20 1.70 -7 4 5 24.90 2.70 -7 4 6 62.59 4.70 -7 4 7 7.40 2.00 -7 4 8 31.90 3.60 6 -4 8 10.10 2.90 6 -4 7 39.70 4.70 6 -4 6 6.00 2.10 6 -4 5 10.70 2.40 6 -4 4 112.29 4.60 6 -4 4 126.59 7.80 -6 4 -4 108.69 5.70 6 -4 3 38.60 1.70 6 -4 3 41.60 3.80 -6 4 -3 36.40 2.30 6 -4 2 359.56 17.00 6 -4 2 390.26 14.70 -6 4 -2 389.76 15.10 6 -4 1 73.29 4.60 6 -4 1 72.99 3.10 -6 4 -1 75.69 3.20 6 -4 0 1006.70 38.80 6 -4 0 968.60 39.80 -6 4 0 1042.60 40.40 6 -4 -1 70.89 3.00 6 -4 -1 71.69 3.60 -6 4 1 72.49 3.60 6 -4 -2 371.46 14.70 -6 4 2 379.76 15.70 -6 4 3 37.70 2.90 -6 4 4 116.49 6.40 -6 4 5 9.30 1.70 -6 4 6 5.40 1.70 -6 4 7 37.50 3.70 -6 4 8 6.80 2.00 5 -4 8 7.90 2.50 5 -4 7 7.00 2.30 5 -4 6 10.80 2.50 5 -4 5 1.50 1.20 -5 4 -5 1.60 0.80 5 -4 4 5.40 0.40 5 -4 4 5.00 1.60 -5 4 -4 5.00 1.00 5 -4 3 182.98 7.10 5 -4 3 190.58 9.80 -5 4 -3 174.68 7.90 5 -4 2 85.09 3.40 5 -4 2 82.59 5.20 -5 4 -2 85.29 3.80 5 -4 1 125.39 5.00 5 -4 1 126.59 6.50 -5 4 -1 129.19 5.20 5 -4 0 207.28 9.40 5 -4 0 216.08 8.40 -5 4 0 221.38 8.70 5 -4 -1 120.99 4.90 5 -4 -1 123.49 5.40 -5 4 1 119.29 5.50 5 -4 -2 79.09 3.40 -5 4 2 83.39 4.30 -5 4 3 181.08 8.50 -5 4 4 6.30 1.50 -5 4 5 1.30 0.80 -5 4 6 10.20 2.00 -5 4 7 7.30 1.80 -5 4 8 9.50 2.30 4 -4 8 2.40 1.70 4 -4 7 11.30 2.60 4 -4 6 56.59 5.10 -4 4 -6 50.99 3.80 4 -4 5 32.00 3.50 -4 4 -5 28.40 2.50 4 -4 4 9.50 1.90 4 -4 4 8.50 0.50 -4 4 -4 6.80 1.10 4 -4 3 3.80 1.30 4 -4 3 3.60 0.30 -4 4 -3 3.50 0.80 4 -4 2 163.48 6.10 4 -4 2 155.58 7.90 -4 4 -2 150.88 6.60 4 -4 1 214.08 10.00 4 -4 1 230.88 8.70 -4 4 -1 227.78 8.90 4 -4 0 184.98 7.20 4 -4 0 180.68 8.10 -4 4 0 190.38 7.50 4 -4 -1 213.18 8.60 -4 4 1 223.38 9.10 -4 4 2 159.78 7.30 -4 4 3 3.10 0.90 -4 4 4 8.00 1.40 -4 4 5 29.30 2.80 -4 4 6 52.99 4.10 -4 4 7 10.70 2.10 -4 4 8 2.20 1.30 -4 4 9 2.10 1.40 3 -4 7 2.40 1.50 -3 4 -7 3.00 1.30 3 -4 6 120.19 7.70 -3 4 -6 109.29 6.40 3 -4 5 98.89 6.40 -3 4 -5 87.69 5.20 3 -4 4 64.49 2.60 3 -4 4 67.99 4.80 -3 4 -4 59.99 3.70 3 -4 3 65.49 4.40 3 -4 3 69.19 2.60 -3 4 -3 59.99 3.40 3 -4 2 96.29 3.60 3 -4 2 85.89 5.00 -3 4 -2 88.59 4.10 3 -4 1 29.90 2.20 3 -4 1 30.90 1.30 -3 4 -1 32.50 1.50 3 -4 0 2009.10 81.79 3 -4 0 1978.90 85.19 -3 4 0 2111.19 94.19 -3 4 1 30.70 1.80 -3 4 2 90.29 4.50 -3 4 3 64.79 3.80 -3 4 4 63.59 4.00 -3 4 5 97.59 5.70 -3 4 6 115.49 6.70 -3 4 7 2.30 1.30 -3 4 8 9.70 2.20 -3 4 9 5.30 1.70 2 -4 7 35.20 3.90 -2 4 -7 31.30 3.30 2 -4 6 44.60 4.10 -2 4 -6 40.80 3.50 2 -4 5 89.89 5.90 -2 4 -5 84.39 5.10 2 -4 4 177.18 8.90 2 -4 4 165.08 6.50 -2 4 -4 162.58 7.90 2 -4 3 390.06 16.40 2 -4 3 381.36 15.20 -2 4 -3 355.86 15.40 2 -4 2 186.98 8.70 2 -4 2 200.08 7.30 -2 4 -2 179.58 7.90 2 -4 1 12.20 0.50 2 -4 1 12.10 1.20 -2 4 -1 12.80 0.80 2 -4 0 382.26 16.40 -2 4 0 393.36 15.80 -2 4 1 12.10 0.90 -2 4 2 196.28 8.50 -2 4 3 427.16 17.70 -2 4 4 169.98 8.20 -2 4 5 88.79 5.20 -2 4 6 41.60 3.50 -2 4 7 30.60 3.10 -2 4 8 9.90 2.10 -2 4 9 32.00 3.50 -1 4 -8 24.00 3.10 -1 4 -7 88.49 5.90 1 -4 6 299.07 14.40 -1 4 -6 295.87 13.90 1 -4 5 59.89 4.40 -1 4 -5 58.49 4.00 1 -4 4 104.79 5.90 -1 4 -4 100.99 5.40 1 -4 3 1102.99 44.10 -1 4 -3 997.60 41.20 1 -4 2 1275.27 55.79 -1 4 -2 1401.06 54.79 1 -4 1 105.49 4.90 -1 4 -1 108.79 4.60 -1 4 0 114.79 4.60 -1 4 1 105.69 4.50 -1 4 2 1486.55 60.09 -1 4 3 1233.78 49.20 -1 4 4 114.49 5.90 -1 4 5 60.39 4.00 -1 4 6 313.47 14.20 -1 4 7 81.09 5.30 -1 4 8 25.20 2.90 -1 4 9 1.30 1.20 0 4 -9 0.30 1.20 0 4 -8 15.30 2.70 0 4 -7 0.70 1.00 0 -4 6 471.75 20.80 0 4 -6 475.45 20.80 0 -4 5 0.30 0.60 0 4 -5 -0.30 0.50 0 -4 4 332.97 14.50 0 4 -4 333.47 14.50 0 -4 3 0.10 0.40 0 4 -3 0.10 0.40 0 -4 2 119.69 5.50 0 4 -2 121.49 5.50 0 -4 1 -1.40 0.20 0 4 -1 -1.40 0.20 0 4 0 14.30 0.80 0 4 1 -1.50 0.20 0 4 2 137.39 6.00 0 4 3 0.20 0.40 0 4 4 402.06 16.90 0 4 5 -0.50 0.50 0 4 6 495.75 21.10 0 4 7 0.00 0.80 0 4 8 12.80 2.10 1 4 -9 2.30 1.60 1 4 -8 25.10 3.30 1 4 -7 84.29 5.90 1 4 -6 301.27 14.20 -1 -4 5 54.89 3.70 1 4 -5 57.99 4.10 -1 -4 4 92.29 5.00 1 4 -4 98.39 5.30 -1 -4 3 1006.00 40.00 1 4 -3 996.00 39.60 -1 -4 2 1219.48 50.49 1 4 -2 1270.07 48.40 1 4 -2 1286.67 51.49 1 4 -1 98.49 4.40 1 4 -1 102.89 3.90 1 4 0 119.39 4.80 1 4 0 114.49 4.60 1 4 1 105.49 4.30 1 4 2 1495.15 59.59 1 4 3 1225.08 49.90 1 4 4 113.19 5.70 1 4 5 60.39 3.80 1 4 6 313.37 14.00 1 4 7 85.59 5.30 2 4 -9 41.30 4.60 2 4 -8 11.50 2.60 2 4 -7 34.80 3.60 2 4 -6 39.00 3.60 -2 -4 5 80.39 4.50 2 4 -5 84.69 5.20 -2 -4 4 149.79 6.70 2 4 -4 143.69 7.40 -2 -4 3 316.87 13.60 2 4 -3 342.37 14.30 2 4 -3 351.16 13.00 -2 -4 2 173.78 7.00 2 4 -2 165.18 6.60 2 4 -2 171.78 7.50 2 4 -1 12.10 0.60 2 4 -1 11.60 1.00 2 4 0 386.46 15.50 2 4 0 411.66 16.30 2 4 1 11.90 0.60 2 4 1 13.20 0.70 2 4 2 187.78 7.60 2 4 3 415.86 16.80 2 4 4 182.28 8.20 2 4 5 96.49 5.10 2 4 6 40.90 3.10 2 4 7 32.40 2.90 2 4 9 39.50 2.20 3 4 -9 6.90 2.40 3 4 -8 11.10 2.60 3 4 -7 2.90 1.50 3 4 -6 106.79 6.60 3 4 -5 90.89 5.60 -3 -4 4 54.89 2.80 3 4 -4 51.09 3.60 -3 -4 3 53.99 2.60 3 4 -3 55.69 2.30 3 4 -3 54.19 3.40 3 4 -2 81.49 4.10 3 4 -2 77.99 3.20 3 4 -1 28.40 1.20 3 4 -1 27.00 1.70 3 4 0 1936.91 94.09 3 4 0 1980.80 82.79 3 4 1 30.20 1.40 3 4 1 32.30 1.40 3 4 2 87.79 3.50 3 4 2 85.49 3.60 3 4 3 65.99 3.20 3 4 3 68.29 2.80 3 4 4 69.19 3.70 3 4 4 71.09 3.00 3 4 5 100.19 5.20 3 4 6 121.29 6.30 3 4 7 3.10 0.60 3 4 8 11.50 1.00 3 4 9 7.00 0.90 4 4 -9 2.60 1.80 4 4 -8 2.20 1.50 4 4 -7 10.50 2.40 4 4 -6 49.50 4.20 4 4 -5 25.70 2.70 4 4 -4 6.70 0.50 4 4 -4 7.10 1.40 4 4 -3 3.60 1.00 4 4 -3 3.20 0.30 4 4 -2 125.99 5.10 4 4 -2 131.39 6.10 4 4 -1 202.48 7.70 4 4 -1 192.48 8.40 4 4 0 162.48 6.80 4 4 0 166.18 6.50 4 4 1 218.98 9.00 4 4 1 241.08 9.30 4 4 2 154.08 6.20 4 4 2 159.58 6.20 4 4 3 3.70 0.40 4 4 3 3.40 0.50 4 4 4 9.80 0.70 4 4 4 8.70 1.00 4 4 5 33.50 1.70 4 4 5 30.50 2.20 4 4 6 58.29 2.70 4 4 7 13.80 1.10 4 4 8 2.60 0.60 4 4 9 2.10 0.60 5 4 -8 7.90 2.30 5 4 -7 4.30 1.70 5 4 -6 8.40 2.00 5 4 -5 0.40 0.80 5 4 -4 4.80 1.30 5 4 -4 4.90 0.50 5 4 -3 157.18 6.10 5 4 -3 146.69 7.40 5 4 -2 69.59 3.80 5 4 -2 69.09 2.90 5 4 -1 102.99 4.80 5 4 -1 104.79 4.20 5 4 0 184.98 7.80 5 4 0 194.28 7.50 5 4 1 114.99 4.80 5 4 1 118.69 4.70 5 4 2 81.69 3.50 5 4 2 88.39 3.50 5 4 3 188.58 7.40 5 4 3 183.48 7.50 5 4 4 6.60 0.60 5 4 4 5.90 0.90 5 4 5 1.20 0.40 5 4 6 11.20 0.90 5 4 7 8.50 0.80 5 4 8 9.30 1.00 5 4 9 1.10 0.90 6 4 -8 10.40 2.70 6 4 -7 37.60 4.00 6 4 -6 4.80 1.50 6 4 -5 8.10 1.60 6 4 -4 102.19 4.20 6 4 -4 98.99 5.80 6 4 -3 32.10 2.60 6 4 -3 30.60 1.50 6 4 -2 306.67 13.30 6 4 -2 321.07 12.30 6 4 -1 57.09 3.20 6 4 -1 62.69 2.60 6 4 0 800.42 33.90 6 4 0 885.11 33.00 6 4 1 58.89 2.70 6 4 1 64.49 2.60 6 4 2 359.26 14.40 6 4 2 377.46 14.60 6 4 3 39.30 1.80 6 4 4 127.39 5.30 6 4 5 11.20 0.80 6 4 6 6.10 0.70 6 4 7 40.20 2.10 6 4 8 10.20 1.00 7 4 -8 31.50 4.00 7 4 -7 8.30 2.30 7 4 -6 60.69 4.90 7 4 -5 20.60 2.50 7 4 -5 24.00 1.30 7 4 -4 9.80 1.70 7 4 -4 9.70 0.70 7 4 -3 0.80 0.60 7 4 -3 1.20 0.30 7 4 -2 21.50 1.90 7 4 -2 24.40 1.20 7 4 -1 22.20 1.10 7 4 -1 21.50 1.70 7 4 0 49.10 2.60 7 4 0 50.19 2.20 7 4 1 21.00 1.20 7 4 1 22.50 1.10 7 4 2 26.30 1.30 7 4 3 1.40 0.30 7 4 4 10.80 0.80 7 4 5 27.80 1.50 7 4 6 73.89 3.40 7 4 7 9.60 0.90 7 4 8 39.00 2.20 8 4 -8 0.90 1.40 8 4 -7 29.10 3.60 8 4 -6 75.19 5.50 8 4 -5 7.70 1.80 8 4 -5 7.50 0.70 8 4 -4 27.40 2.70 8 4 -4 32.70 1.60 8 4 -3 2.00 0.90 8 4 -3 2.30 0.40 8 4 -2 137.69 6.90 8 4 -2 147.29 5.80 8 4 -1 28.90 2.10 8 4 -1 31.10 1.50 8 4 0 98.09 4.00 8 4 0 90.69 4.40 8 4 1 28.40 1.40 8 4 2 142.59 5.80 8 4 3 2.50 0.40 8 4 4 34.40 1.70 8 4 5 9.30 0.80 8 4 6 89.19 4.00 8 4 7 35.30 2.00 8 4 8 1.10 0.60 9 4 -7 4.40 1.70 9 4 -6 6.20 1.80 9 4 -5 20.00 2.60 9 4 -5 20.60 1.30 9 4 -4 10.70 0.90 9 4 -4 8.00 1.60 9 4 -3 11.50 1.70 9 4 -3 13.30 0.90 9 4 -2 54.49 2.40 9 4 -2 50.49 3.30 9 4 -1 30.00 2.20 9 4 -1 32.10 1.60 9 4 0 393.16 15.40 9 4 0 392.16 16.00 9 4 1 29.30 1.50 9 4 2 52.69 2.40 9 4 3 12.70 0.90 9 4 4 9.50 0.80 9 4 5 24.10 1.40 9 4 6 9.00 0.90 9 4 7 7.60 0.90 9 4 8 19.50 1.50 10 4 -7 6.00 2.10 10 4 -6 11.20 2.20 10 4 -5 2.50 1.20 10 4 -5 3.70 0.60 10 4 -4 105.19 6.50 10 4 -4 123.49 5.00 10 4 -3 3.20 1.10 10 4 -3 3.10 0.50 10 4 -2 32.30 1.70 10 4 -2 31.60 2.50 10 4 -1 82.39 4.40 10 4 -1 84.19 3.60 10 4 0 9.30 0.70 10 4 1 81.59 3.50 10 4 2 33.40 1.70 10 4 3 4.50 0.60 10 4 4 115.19 4.90 10 4 5 3.40 0.60 10 4 6 12.30 1.00 10 4 7 8.40 1.00 11 4 -7 36.90 4.20 11 4 -6 9.20 2.30 11 4 -6 11.50 1.10 11 4 -5 10.30 1.00 11 4 -5 10.80 2.10 11 4 -4 29.70 3.00 11 4 -4 36.40 1.90 11 4 -3 6.80 1.50 11 4 -3 6.90 0.70 11 4 -2 25.80 1.50 11 4 -2 24.50 2.30 11 4 -1 4.50 0.60 11 4 0 4.30 0.60 11 4 1 4.80 0.60 11 4 2 24.60 1.40 11 4 3 6.70 0.70 11 4 4 32.30 1.70 11 4 5 11.10 0.90 11 4 6 10.70 1.00 11 4 7 40.60 2.20 12 4 -7 6.60 2.80 12 4 -6 4.90 0.80 12 4 -6 4.20 1.60 12 4 -5 4.40 0.70 12 4 -5 3.10 1.40 12 4 -4 16.40 2.30 12 4 -4 16.60 1.30 12 4 -3 4.60 1.30 12 4 -3 5.30 0.70 12 4 -2 20.80 1.30 12 4 -1 72.69 3.30 12 4 0 9.40 0.80 12 4 1 65.39 3.00 12 4 2 16.90 1.10 12 4 3 5.20 0.70 12 4 4 15.70 1.10 12 4 5 3.70 0.60 12 4 6 3.60 0.70 12 4 7 6.00 0.80 13 4 -6 18.40 2.90 13 4 -6 20.90 1.60 13 4 -5 9.70 1.00 13 4 -5 7.30 1.90 13 4 -4 17.00 1.30 13 4 -4 14.20 2.30 13 4 -3 24.80 1.60 13 4 -2 13.70 1.10 13 4 -1 57.59 2.80 13 4 0 1.40 0.40 13 4 1 55.39 2.70 13 4 2 13.30 1.00 13 4 3 21.80 1.30 13 4 4 14.90 1.10 13 4 5 8.10 0.90 13 4 6 18.90 1.30 14 4 -6 5.00 1.80 14 4 -6 5.90 0.90 14 4 -5 -0.10 0.40 14 4 -5 -0.20 1.00 14 4 -4 10.50 1.00 14 4 -3 17.40 1.30 14 4 -2 0.30 0.40 14 4 -1 9.20 0.90 14 4 0 6.70 0.80 14 4 1 9.30 0.90 14 4 2 0.10 0.30 14 4 3 14.40 1.10 14 4 4 8.10 0.80 14 4 5 -0.10 0.30 14 4 6 5.10 0.80 15 4 -5 0.20 0.50 15 4 -4 1.00 0.50 15 4 -3 10.00 1.00 15 4 -2 3.40 0.70 15 4 -1 20.90 1.50 15 4 0 13.10 1.10 15 4 1 18.60 1.30 15 4 2 2.70 0.50 15 4 3 10.70 1.00 15 4 4 0.90 0.40 15 4 5 0.30 0.40 16 4 -4 8.80 1.20 16 4 -3 6.90 1.00 16 4 -2 5.90 0.90 16 4 -1 9.00 1.00 16 4 0 9.30 1.00 16 4 1 9.80 1.00 16 4 2 6.40 0.90 16 4 3 5.60 0.80 16 4 4 7.40 0.90 17 4 -2 6.80 1.00 17 4 -1 -0.10 0.40 17 4 0 30.70 1.90 17 4 1 0.20 0.40 17 4 2 6.30 0.90 17 4 3 0.80 0.70 18 -5 0 1.50 0.70 17 -5 3 6.70 3.00 17 -5 1 0.20 0.50 17 -5 0 2.70 0.70 17 -5 -1 -0.10 0.50 17 -5 -2 16.10 1.60 16 -5 4 5.30 2.50 16 -5 3 3.40 2.10 16 -5 1 17.50 1.40 16 -5 0 18.60 1.50 16 -5 -1 17.80 1.50 16 -5 -2 1.90 0.70 16 -5 -3 5.20 1.00 15 -5 4 1.90 1.70 15 -5 3 3.90 2.10 15 -5 2 13.10 2.80 15 -5 1 7.50 1.00 15 -5 0 21.80 1.60 15 -5 -1 7.50 1.10 15 -5 -2 15.60 1.40 15 -5 -3 3.60 0.80 15 -5 -4 2.70 0.80 14 -5 5 8.40 2.90 14 -5 4 7.30 2.70 14 -5 3 8.70 2.70 14 -5 2 49.80 5.00 14 -5 2 49.40 2.60 14 -5 1 4.90 1.80 14 -5 1 4.70 0.70 14 -5 0 0.20 0.40 14 -5 -1 5.10 0.80 14 -5 -2 50.69 2.70 14 -5 -3 10.70 1.10 14 -5 -4 7.10 1.00 -14 5 4 6.40 1.80 -14 5 5 11.70 2.50 13 -5 6 10.40 3.30 13 -5 5 5.50 2.40 13 -5 4 32.50 4.50 13 -5 3 30.00 4.00 13 -5 2 29.30 3.70 13 -5 2 30.00 1.70 13 -5 1 118.19 5.20 13 -5 1 119.49 7.70 13 -5 0 4.90 0.70 13 -5 -1 130.19 5.70 13 -5 -2 32.70 2.00 13 -5 -3 33.30 2.00 -13 5 3 34.00 3.10 13 -5 -4 40.50 2.40 -13 5 4 36.60 3.50 -13 5 5 7.60 2.10 -13 5 6 11.50 2.50 12 -5 6 7.20 2.80 12 -5 5 35.60 4.90 12 -5 4 5.10 2.20 12 -5 3 27.10 3.90 12 -5 2 88.49 4.00 12 -5 2 91.29 6.80 12 -5 1 18.40 1.20 12 -5 1 16.90 2.70 12 -5 0 21.80 1.40 12 -5 0 20.00 2.50 12 -5 -1 18.70 1.30 12 -5 -2 92.79 4.30 -12 5 2 96.09 5.30 12 -5 -3 29.20 1.80 -12 5 3 27.20 2.70 12 -5 -4 7.10 1.00 -12 5 4 6.90 1.80 -12 5 5 35.20 3.60 -12 5 6 7.50 2.10 11 -5 7 15.80 3.80 11 -5 6 42.30 5.30 11 -5 5 40.90 5.00 11 -5 4 6.30 2.40 11 -5 3 102.99 7.60 11 -5 2 7.10 2.10 11 -5 2 7.40 0.70 11 -5 1 113.39 4.90 11 -5 1 115.09 7.20 11 -5 0 73.99 3.30 11 -5 0 72.79 4.90 11 -5 -1 115.29 5.00 -11 5 1 112.19 5.50 11 -5 -2 7.60 0.90 -11 5 2 7.10 1.30 11 -5 -3 109.49 4.80 -11 5 3 107.49 6.20 -11 5 4 7.00 1.80 -11 5 5 41.50 3.90 -11 5 6 46.80 4.30 -11 5 7 15.50 2.80 10 -5 7 -0.20 1.60 10 -5 6 2.40 1.80 10 -5 5 30.40 4.30 10 -5 4 25.20 3.70 10 -5 3 37.90 4.30 10 -5 2 105.89 4.50 10 -5 2 108.29 7.20 10 -5 1 9.20 1.80 10 -5 1 9.30 0.80 10 -5 0 40.30 3.30 10 -5 0 41.10 2.10 -10 5 0 43.20 2.30 10 -5 -1 8.60 1.30 10 -5 -1 9.70 0.80 -10 5 1 9.10 1.10 10 -5 -2 109.39 4.70 -10 5 2 107.79 5.70 10 -5 -3 39.30 2.10 -10 5 3 38.30 3.10 -10 5 4 25.20 2.80 -10 5 5 32.20 3.30 -10 5 6 3.60 1.60 -10 5 7 0.40 1.20 9 -5 7 8.20 2.90 9 -5 6 38.80 4.80 9 -5 5 65.09 6.00 9 -5 3 46.20 2.20 9 -5 3 46.40 4.50 9 -5 2 43.80 4.10 9 -5 2 42.20 2.00 9 -5 1 20.80 2.50 9 -5 1 21.50 1.20 -9 5 -1 23.50 1.30 9 -5 0 7.40 1.40 9 -5 0 7.50 0.70 -9 5 0 8.30 0.80 9 -5 -1 21.30 1.90 9 -5 -1 22.00 1.30 -9 5 1 22.20 1.70 9 -5 -2 41.60 2.10 -9 5 2 40.60 2.90 9 -5 -3 49.50 2.50 -9 5 3 50.09 3.60 -9 5 4 31.40 3.00 -9 5 5 62.59 4.70 -9 5 6 40.10 3.90 -9 5 7 6.70 2.00 8 -5 8 22.20 4.10 8 -5 7 2.30 1.90 8 -5 6 17.40 3.50 8 -5 5 67.99 6.10 8 -5 4 24.20 3.30 8 -5 3 67.79 5.50 8 -5 3 68.19 2.90 8 -5 2 81.89 5.70 8 -5 2 82.49 3.50 -8 5 -2 82.39 3.80 8 -5 1 140.69 5.70 8 -5 1 133.89 7.60 -8 5 -1 145.49 5.80 8 -5 0 9.80 1.50 8 -5 0 9.50 0.70 -8 5 0 10.90 0.90 8 -5 -1 144.49 5.80 8 -5 -1 138.29 6.60 -8 5 1 138.49 6.40 8 -5 -2 82.69 3.60 -8 5 2 82.89 4.60 -8 5 3 73.29 4.50 -8 5 4 22.90 2.50 -8 5 5 58.19 4.40 -8 5 6 17.90 2.60 -8 5 7 1.00 1.10 -8 5 8 17.70 3.00 7 -5 8 15.60 3.50 7 -5 7 13.00 3.40 7 -5 6 20.30 3.50 7 -5 5 13.50 2.80 7 -5 4 22.50 3.10 7 -5 3 67.69 5.20 7 -5 3 67.29 2.80 -7 5 -3 59.79 3.30 7 -5 2 45.10 2.00 7 -5 2 44.40 3.80 -7 5 -2 45.90 2.30 7 -5 1 67.69 2.80 7 -5 1 62.89 4.40 -7 5 -1 65.89 2.90 7 -5 0 0.20 0.20 7 -5 0 0.60 0.60 -7 5 0 0.10 0.20 7 -5 -1 64.39 2.80 7 -5 -1 64.49 3.50 -7 5 1 64.59 3.40 7 -5 -2 45.00 2.10 -7 5 2 45.10 3.00 -7 5 3 68.89 4.30 -7 5 4 21.70 2.40 -7 5 5 12.80 2.00 -7 5 6 20.00 2.70 -7 5 7 13.40 2.40 -7 5 8 12.60 2.50 6 -5 8 11.70 3.20 6 -5 7 2.80 1.70 6 -5 6 96.49 7.40 6 -5 5 91.19 6.80 6 -5 4 41.30 4.10 -6 5 -4 37.80 2.60 6 -5 3 137.09 7.90 6 -5 3 131.79 5.20 -6 5 -3 121.79 5.90 6 -5 2 817.32 35.40 6 -5 2 887.41 36.50 -6 5 -2 881.01 34.80 6 -5 1 42.50 1.90 6 -5 1 41.00 3.20 -6 5 -1 43.90 2.00 6 -5 0 56.09 3.50 6 -5 0 61.79 2.60 -6 5 0 61.39 2.80 6 -5 -1 42.10 2.50 6 -5 -1 40.80 1.90 -6 5 1 43.40 2.50 6 -5 -2 893.21 35.40 -6 5 2 946.91 36.60 -6 5 3 127.99 6.60 -6 5 4 45.40 3.50 -6 5 5 95.99 5.90 -6 5 6 94.09 6.10 -6 5 7 2.00 1.20 -6 5 8 10.00 2.30 5 -5 8 1.60 1.60 5 -5 7 1.90 1.50 5 -5 6 12.40 2.60 5 -5 5 26.40 3.30 -5 5 -5 21.90 2.20 5 -5 4 6.50 1.90 -5 5 -4 5.20 1.10 5 -5 3 111.79 6.80 5 -5 3 114.79 4.40 -5 5 -3 101.99 5.10 5 -5 2 152.28 8.20 5 -5 2 162.88 6.20 -5 5 -2 157.78 6.70 5 -5 1 86.89 3.50 5 -5 1 79.69 4.80 -5 5 -1 91.49 3.70 5 -5 0 67.79 2.80 5 -5 0 65.39 3.70 -5 5 0 67.29 3.00 5 -5 -1 86.69 4.20 5 -5 -1 87.19 3.60 -5 5 1 88.79 4.20 -5 5 2 165.48 7.60 -5 5 3 114.09 6.00 -5 5 4 5.10 1.30 -5 5 5 27.20 2.70 -5 5 6 12.20 2.00 -5 5 7 2.50 1.30 -5 5 8 1.50 1.30 4 -5 8 24.60 3.80 4 -5 7 4.50 2.00 4 -5 6 72.99 5.80 -4 5 -6 63.59 4.40 4 -5 5 25.50 3.20 -4 5 -5 23.00 2.20 4 -5 4 28.20 3.10 -4 5 -4 24.90 2.10 4 -5 3 30.10 1.30 -4 5 -3 27.60 2.00 4 -5 2 23.40 1.00 4 -5 2 24.10 2.30 -4 5 -2 22.60 1.50 4 -5 1 59.99 2.40 4 -5 1 57.19 3.50 -4 5 -1 58.69 2.60 4 -5 0 21.50 1.70 4 -5 0 23.20 1.10 -4 5 0 24.40 1.30 -4 5 1 58.19 2.90 -4 5 2 24.00 1.80 -4 5 3 32.70 2.50 -4 5 4 27.50 2.50 -4 5 5 27.60 2.70 -4 5 6 73.09 5.00 -4 5 7 4.50 1.50 -4 5 8 20.60 2.80 -4 5 9 2.20 1.50 3 -5 7 35.80 4.10 -3 5 -7 32.30 3.30 3 -5 6 104.59 7.00 -3 5 -6 97.89 6.00 3 -5 5 92.29 6.10 -3 5 -5 82.09 5.00 3 -5 4 53.59 4.20 -3 5 -4 49.70 3.30 3 -5 3 262.17 9.50 3 -5 3 236.08 11.60 -3 5 -3 243.08 10.60 3 -5 2 86.59 5.00 3 -5 2 92.49 3.50 -3 5 -2 88.09 4.10 3 -5 1 6.40 1.00 3 -5 1 7.30 0.40 -3 5 -1 7.10 0.60 3 -5 0 38.10 2.30 -3 5 0 42.20 1.90 -3 5 1 7.10 0.70 -3 5 2 96.19 4.70 -3 5 3 281.87 12.30 -3 5 4 53.29 3.60 -3 5 5 94.09 5.60 -3 5 6 104.09 6.20 -3 5 7 35.60 3.40 -3 5 8 0.60 1.10 -3 5 9 6.20 1.90 2 -5 7 48.20 4.50 -2 5 -7 41.10 3.80 2 -5 6 19.60 2.80 -2 5 -6 17.90 2.30 2 -5 5 51.49 4.10 -2 5 -5 46.40 3.50 2 -5 4 21.70 2.40 -2 5 -4 19.30 1.90 2 -5 3 27.30 2.50 2 -5 3 31.20 1.20 -2 5 -3 25.90 2.00 2 -5 2 27.20 2.20 -2 5 -2 27.40 1.70 2 -5 1 155.48 7.10 -2 5 -1 164.18 6.60 2 -5 0 123.19 5.50 -2 5 0 127.49 5.10 -2 5 1 168.88 7.00 -2 5 2 30.60 2.00 -2 5 3 29.30 2.20 -2 5 4 21.30 2.10 -2 5 5 51.19 3.70 -2 5 6 17.60 2.30 -2 5 7 45.70 3.90 -2 5 8 0.70 1.00 -2 5 9 3.10 1.50 -1 5 -8 2.90 1.50 -1 5 -7 0.00 0.90 1 -5 6 79.99 5.50 -1 5 -6 70.69 5.00 1 -5 5 319.07 14.30 -1 5 -5 289.67 13.70 1 -5 4 398.86 16.70 -1 5 -4 358.06 16.10 1 -5 3 42.90 3.00 -1 5 -3 40.10 2.60 1 -5 2 53.99 3.10 -1 5 -2 51.49 2.80 1 -5 1 12.60 1.10 -1 5 -1 11.60 0.90 -1 5 0 -0.40 0.10 -1 5 1 12.20 0.90 -1 5 2 59.59 3.10 -1 5 3 48.80 3.00 -1 5 4 428.16 18.10 -1 5 5 331.77 14.70 -1 5 6 81.49 5.20 -1 5 7 0.50 0.90 -1 5 8 3.40 1.40 -1 5 9 16.60 2.50 0 5 -9 -0.10 1.00 0 5 -8 131.39 8.20 0 5 -7 0.20 0.90 0 -5 6 354.36 16.20 0 5 -6 358.46 16.30 0 5 -5 1.60 0.90 0 -5 4 95.79 5.30 0 5 -4 97.39 5.30 0 -5 3 -0.10 0.40 0 5 -3 0.00 0.40 0 -5 2 1507.75 61.69 0 5 -2 1498.15 60.79 0 -5 1 -0.10 0.20 0 5 -1 0.00 0.10 0 5 0 78.59 3.30 0 5 1 0.00 0.20 0 5 2 1732.13 69.09 0 5 3 -0.40 0.30 0 5 4 115.29 5.90 0 5 6 391.76 17.20 0 5 7 0.00 0.80 0 5 8 136.69 7.70 1 5 -9 16.00 3.00 1 5 -8 3.30 1.60 1 5 -7 0.40 0.90 1 5 -6 70.09 5.00 -1 -5 5 278.37 12.60 1 5 -5 289.97 13.20 -1 -5 4 345.27 14.50 1 5 -4 339.47 14.90 -1 -5 3 39.70 2.40 1 5 -3 39.00 2.60 -1 -5 2 51.19 2.60 1 5 -2 49.60 2.00 1 5 -1 11.50 0.90 1 5 -1 11.40 0.50 1 5 0 -0.40 0.10 1 5 0 -0.40 0.10 1 5 1 11.60 0.70 1 5 2 58.29 2.80 1 5 3 47.50 2.70 1 5 4 447.16 18.50 1 5 5 341.87 14.80 1 5 6 83.09 5.00 1 5 7 -0.50 0.80 2 5 -9 4.30 1.90 2 5 -8 1.40 1.40 2 5 -7 41.10 4.00 2 5 -6 19.00 2.60 -2 -5 5 42.70 2.90 2 5 -5 45.70 3.60 -2 -5 4 18.10 1.50 2 5 -4 19.20 2.00 -2 -5 3 23.80 1.60 2 5 -3 22.70 1.00 2 5 -3 23.00 2.00 2 5 -2 28.00 1.10 2 5 -2 24.80 1.80 2 5 -1 148.69 6.40 2 5 -1 149.09 5.80 2 5 0 121.49 5.10 2 5 0 123.19 4.80 2 5 1 167.48 6.60 2 5 1 164.48 6.50 2 5 2 29.20 1.60 2 5 3 27.70 1.80 2 5 4 23.70 1.90 2 5 5 52.69 3.40 2 5 6 20.10 2.20 2 5 7 46.70 4.20 2 5 9 2.90 0.60 3 5 -9 5.20 2.10 3 5 -8 -0.40 0.80 3 5 -7 32.10 3.50 3 5 -6 95.09 6.10 3 5 -5 81.39 5.20 -3 -5 4 45.80 2.50 3 5 -4 41.80 3.20 -3 -5 3 240.88 9.40 3 5 -3 224.08 10.20 3 5 -3 219.18 8.90 3 5 -2 77.99 4.00 3 5 -2 75.19 3.10 3 5 -1 6.70 0.80 3 5 -1 6.20 0.40 3 5 0 39.10 1.70 3 5 0 38.00 2.00 3 5 1 6.70 0.50 3 5 1 6.10 0.40 3 5 2 90.19 3.70 3 5 2 90.89 3.80 3 5 3 269.17 11.00 3 5 3 271.17 10.60 3 5 4 56.19 2.50 3 5 4 55.09 3.10 3 5 5 97.59 5.10 3 5 6 117.79 6.20 3 5 7 38.50 2.00 3 5 8 0.50 0.40 3 5 9 6.00 0.90 4 5 -8 19.40 3.10 4 5 -7 4.80 1.70 4 5 -6 58.49 4.60 4 5 -5 21.20 2.50 4 5 -4 25.70 1.20 4 5 -4 23.80 2.30 4 5 -3 26.80 1.30 4 5 -2 19.10 0.90 4 5 -2 18.50 1.60 4 5 -1 48.40 2.70 4 5 -1 51.39 2.10 4 5 0 21.00 1.30 4 5 0 19.80 1.00 4 5 1 59.19 2.50 4 5 1 55.09 2.40 4 5 2 23.40 1.20 4 5 2 22.00 1.10 4 5 3 30.70 1.50 4 5 3 31.20 1.70 4 5 4 32.50 1.60 4 5 4 31.20 2.00 4 5 5 29.20 1.50 4 5 5 26.00 2.10 4 5 6 79.59 3.60 4 5 7 5.60 0.80 4 5 8 24.20 1.60 4 5 9 3.60 0.80 5 5 -8 1.40 1.30 5 5 -7 2.10 1.30 5 5 -6 9.10 2.00 5 5 -5 20.50 2.50 5 5 -4 4.80 1.20 5 5 -4 4.40 0.50 5 5 -3 86.49 4.90 5 5 -3 88.19 3.60 5 5 -2 129.99 5.20 5 5 -2 129.29 6.20 5 5 -1 72.09 3.00 5 5 -1 70.29 3.60 5 5 0 56.39 2.80 5 5 0 58.59 2.40 5 5 1 82.79 3.40 5 5 1 82.99 3.60 5 5 2 153.18 6.40 5 5 2 167.78 6.40 5 5 3 112.89 4.60 5 5 3 112.19 4.70 5 5 4 5.60 0.60 5 5 5 29.30 1.60 5 5 6 13.30 1.00 5 5 7 3.10 0.60 5 5 8 1.40 0.50 6 5 -8 9.70 2.50 6 5 -7 1.50 1.20 6 5 -6 79.79 5.60 6 5 -5 89.39 3.70 6 5 -5 82.09 5.40 6 5 -4 38.60 1.80 6 5 -4 37.70 3.10 6 5 -3 102.59 5.60 6 5 -3 107.99 4.30 6 5 -2 728.83 27.20 6 5 -2 675.63 28.20 6 5 -1 32.80 2.10 6 5 -1 35.50 1.60 6 5 0 47.80 2.10 6 5 0 46.30 2.50 6 5 1 35.90 1.80 6 5 1 36.50 1.70 6 5 2 817.52 32.50 6 5 2 864.61 38.90 6 5 3 128.79 5.30 6 5 4 45.30 2.10 6 5 5 103.19 4.40 6 5 6 105.29 4.60 6 5 7 2.50 0.60 6 5 8 13.70 1.20 7 5 -8 11.60 2.80 7 5 -7 12.10 2.40 7 5 -6 16.20 2.50 7 5 -5 12.60 0.90 7 5 -5 10.40 1.90 7 5 -4 20.30 2.20 7 5 -4 20.20 1.20 7 5 -3 49.30 3.40 7 5 -3 54.09 2.40 7 5 -2 34.60 2.50 7 5 -2 37.50 1.70 7 5 -1 49.50 2.90 7 5 -1 52.49 2.30 7 5 0 -0.10 0.20 7 5 0 -0.10 0.20 7 5 1 52.09 2.20 7 5 1 49.00 2.40 7 5 2 38.20 1.80 7 5 3 64.79 2.90 7 5 4 23.20 1.30 7 5 5 13.40 1.00 7 5 6 21.20 1.40 7 5 7 15.60 1.20 7 5 8 15.30 1.30 8 5 -8 18.80 3.30 8 5 -7 1.50 1.40 8 5 -6 13.30 2.30 8 5 -5 49.60 4.10 8 5 -5 54.09 2.50 8 5 -4 20.20 2.30 8 5 -4 21.50 1.20 8 5 -3 51.89 3.60 8 5 -3 54.49 2.40 8 5 -2 69.69 2.90 8 5 -2 60.59 3.80 8 5 -1 106.09 5.30 8 5 -1 112.09 4.50 8 5 0 7.90 0.60 8 5 0 7.40 0.90 8 5 1 106.99 4.40 8 5 2 70.29 3.00 8 5 3 63.19 2.80 8 5 4 24.20 1.40 8 5 5 61.19 2.90 8 5 6 17.90 1.30 8 5 7 1.50 0.50 8 5 8 24.70 1.70 9 5 -7 6.00 2.00 9 5 -6 30.80 3.40 9 5 -5 51.29 4.20 9 5 -5 57.79 2.70 9 5 -4 26.90 2.70 9 5 -4 28.70 1.60 9 5 -3 41.70 2.00 9 5 -3 36.40 3.00 9 5 -2 32.50 2.50 9 5 -2 34.40 1.70 9 5 -1 16.20 1.50 9 5 -1 18.20 1.10 9 5 0 7.70 0.60 9 5 0 6.50 1.00 9 5 1 16.60 1.00 9 5 2 33.80 1.70 9 5 3 42.60 2.10 9 5 4 32.70 1.70 9 5 5 64.19 3.00 9 5 6 41.60 2.20 9 5 7 8.00 1.00 9 5 8 20.70 1.60 10 5 -7 0.00 1.10 10 5 -6 1.60 1.20 10 5 -6 2.40 0.60 10 5 -5 28.50 1.60 10 5 -5 26.00 3.00 10 5 -4 20.90 1.30 10 5 -4 17.40 2.20 10 5 -3 26.40 2.50 10 5 -3 30.50 1.60 10 5 -2 79.49 4.60 10 5 -2 86.29 3.70 10 5 -1 6.80 1.10 10 5 -1 7.20 0.70 10 5 0 31.60 1.60 10 5 1 8.10 0.70 10 5 2 77.69 3.40 10 5 3 30.60 1.60 10 5 4 22.60 1.40 10 5 5 29.00 1.70 10 5 6 2.50 0.60 10 5 7 0.40 0.40 11 5 -7 12.70 2.80 11 5 -6 42.40 2.20 11 5 -6 35.10 3.80 11 5 -5 31.70 3.30 11 5 -5 34.70 1.90 11 5 -4 5.10 1.40 11 5 -4 7.00 0.80 11 5 -3 85.59 3.70 11 5 -3 75.39 4.90 11 5 -2 5.80 0.70 11 5 -2 6.00 1.30 11 5 -1 86.99 3.80 11 5 0 58.99 2.70 11 5 1 78.29 3.40 11 5 2 4.60 0.60 11 5 3 79.09 3.50 11 5 4 5.30 0.70 11 5 5 34.50 1.90 11 5 6 41.70 2.20 11 5 7 15.50 1.30 12 5 -6 7.40 2.10 12 5 -6 7.90 1.00 12 5 -5 26.70 3.10 12 5 -5 33.20 1.90 12 5 -4 4.00 0.60 12 5 -4 3.90 1.40 12 5 -3 18.70 2.30 12 5 -3 21.60 1.40 12 5 -2 72.79 3.40 12 5 -1 13.80 1.10 12 5 0 15.90 1.10 12 5 1 13.60 1.00 12 5 2 67.29 3.10 12 5 3 19.90 1.30 12 5 4 4.30 0.60 12 5 5 29.70 1.70 12 5 6 7.10 0.90 13 5 -6 9.40 2.30 13 5 -6 11.90 1.10 13 5 -5 6.50 0.90 13 5 -5 6.60 1.80 13 5 -4 27.00 2.90 13 5 -4 31.80 1.80 13 5 -3 26.70 1.70 13 5 -2 25.20 1.50 13 5 -1 95.89 4.30 13 5 0 3.50 0.60 13 5 1 84.59 3.80 13 5 2 23.50 1.40 13 5 3 23.90 1.50 13 5 4 25.00 1.50 13 5 5 5.40 0.80 13 5 6 9.70 1.00 14 5 -5 8.20 1.00 14 5 -4 6.40 0.90 14 5 -3 8.90 0.90 14 5 -2 38.90 2.20 14 5 -1 3.70 0.70 14 5 0 0.60 0.40 14 5 1 3.80 0.60 14 5 2 36.00 2.00 14 5 3 6.70 0.80 14 5 4 4.90 0.70 14 5 5 10.10 1.00 15 5 -5 5.00 0.90 15 5 -4 1.20 0.50 15 5 -3 2.50 0.60 15 5 -2 12.00 1.10 15 5 -1 5.90 0.80 15 5 0 15.90 1.20 15 5 1 5.40 0.70 15 5 2 10.10 0.90 15 5 3 3.10 0.60 15 5 4 1.60 0.50 15 5 5 3.80 0.80 16 5 -4 4.80 0.90 16 5 -3 2.90 0.70 16 5 -2 1.10 0.50 16 5 -1 13.60 1.20 16 5 0 13.80 1.20 16 5 1 12.80 1.10 16 5 2 1.10 0.50 16 5 3 3.20 0.60 16 5 4 3.40 1.00 17 5 -2 12.60 1.20 17 5 -1 0.70 0.50 17 5 0 3.00 0.70 17 5 1 0.10 0.40 17 5 2 12.50 1.10 17 -6 0 15.40 1.50 17 -6 -1 5.80 1.10 17 -6 -2 7.70 1.20 16 -6 3 17.60 3.50 16 -6 0 18.20 1.50 16 -6 -1 2.60 0.80 16 -6 -2 5.70 1.00 16 -6 -3 19.70 1.70 15 -6 4 1.90 1.90 15 -6 3 1.40 1.60 15 -6 2 12.20 2.80 15 -6 1 8.10 1.00 15 -6 0 40.50 2.30 15 -6 -1 10.60 1.20 15 -6 -2 11.30 1.30 15 -6 -3 2.10 0.80 14 -6 5 -0.50 1.50 14 -6 4 4.70 2.40 14 -6 3 2.70 1.80 14 -6 2 3.50 1.80 14 -6 1 28.90 3.50 14 -6 1 28.80 1.80 14 -6 0 10.00 1.10 14 -6 -1 31.50 2.00 14 -6 -2 2.80 0.70 14 -6 -3 4.10 0.90 -14 6 4 4.90 1.60 -14 6 5 -0.10 1.00 13 -6 5 12.20 3.50 13 -6 4 18.70 3.70 13 -6 3 11.90 2.90 13 -6 2 21.40 3.30 13 -6 1 95.49 6.70 13 -6 1 96.59 4.30 13 -6 0 -0.90 0.30 13 -6 -1 103.59 4.70 13 -6 -2 23.70 1.70 13 -6 -3 12.10 1.30 -13 6 3 14.20 2.10 -13 6 4 25.10 2.90 -13 6 5 11.80 2.30 -13 6 6 0.10 1.20 12 -6 6 25.60 4.50 12 -6 5 25.00 4.10 12 -6 4 19.40 3.50 12 -6 3 156.28 10.10 12 -6 2 5.50 2.10 12 -6 1 52.09 2.50 12 -6 1 47.40 4.30 12 -6 0 145.49 6.10 12 -6 0 138.39 7.80 12 -6 -1 55.09 2.80 12 -6 -2 5.10 0.80 -12 6 2 5.30 1.30 12 -6 -3 165.88 7.10 -12 6 3 167.18 8.60 -12 6 4 21.40 2.70 -12 6 5 29.50 3.40 -12 6 6 25.90 3.40 11 -6 6 5.30 2.60 11 -6 5 25.10 4.00 11 -6 4 8.90 2.70 11 -6 3 43.40 4.70 11 -6 2 45.90 2.20 11 -6 2 43.90 4.40 11 -6 1 165.58 9.40 11 -6 1 173.28 7.00 11 -6 0 77.49 3.30 11 -6 0 65.69 4.70 11 -6 -1 183.68 7.50 -11 6 1 176.68 8.00 11 -6 -2 45.50 2.30 -11 6 2 42.20 3.10 11 -6 -3 48.00 2.50 -11 6 3 46.90 3.60 -11 6 4 11.20 2.10 -11 6 5 24.80 3.00 -11 6 6 5.50 1.90 10 -6 7 14.90 3.50 10 -6 6 25.00 4.20 10 -6 5 29.90 4.20 10 -6 4 67.19 6.10 10 -6 3 46.60 4.70 10 -6 2 18.70 2.80 10 -6 2 17.30 1.10 10 -6 1 6.90 1.70 10 -6 1 7.40 0.70 10 -6 0 76.99 5.00 10 -6 0 84.79 3.60 -10 6 0 80.29 3.80 10 -6 -1 7.60 1.30 10 -6 -1 7.60 0.70 -10 6 1 8.50 1.10 10 -6 -2 20.00 1.30 -10 6 2 19.50 2.00 10 -6 -3 48.50 2.50 -10 6 3 50.09 3.70 -10 6 4 66.69 4.70 -10 6 5 28.50 3.20 -10 6 6 26.30 3.30 -10 6 7 14.00 2.70 9 -6 7 11.20 3.40 9 -6 6 38.80 5.00 9 -6 5 11.30 3.00 9 -6 4 15.20 3.00 9 -6 3 3.20 1.50 9 -6 2 19.80 1.10 9 -6 2 17.90 2.60 9 -6 1 43.30 3.70 9 -6 1 43.90 2.10 -9 6 -1 44.70 2.20 9 -6 0 5.90 0.60 9 -6 0 4.30 1.20 -9 6 0 4.40 0.70 9 -6 -1 43.80 2.90 9 -6 -1 44.40 2.20 -9 6 1 43.50 2.70 9 -6 -2 18.30 1.20 -9 6 2 20.60 1.90 -9 6 3 2.30 1.00 -9 6 4 18.20 2.40 -9 6 5 19.30 2.70 -9 6 6 44.40 4.10 -9 6 7 8.90 2.20 8 -6 8 2.00 1.80 8 -6 7 8.20 2.90 8 -6 6 3.80 2.00 8 -6 5 16.80 3.30 8 -6 4 23.20 3.40 8 -6 3 110.39 7.40 8 -6 2 15.50 0.90 8 -6 2 13.90 2.30 -8 6 -2 14.20 1.10 8 -6 1 26.80 1.30 8 -6 1 25.30 2.60 -8 6 -1 25.80 1.50 8 -6 0 20.40 1.10 8 -6 0 17.70 2.00 -8 6 0 20.10 1.30 8 -6 -1 26.20 2.00 8 -6 -1 25.00 1.40 -8 6 1 26.40 1.90 8 -6 -2 14.50 1.00 -8 6 2 14.40 1.60 -8 6 3 118.89 6.40 -8 6 4 26.00 2.70 -8 6 5 18.20 2.50 -8 6 6 4.00 1.50 -8 6 7 8.90 2.20 7 -6 8 0.30 1.60 7 -6 7 15.40 3.40 7 -6 6 7.70 2.60 7 -6 5 30.40 4.00 7 -6 4 49.50 4.70 7 -6 3 195.68 10.40 -7 6 -3 169.48 7.90 7 -6 2 18.10 2.40 7 -6 2 19.00 1.00 -7 6 -2 17.60 1.30 7 -6 1 101.09 4.10 7 -6 1 99.69 5.90 -7 6 -1 101.49 4.30 7 -6 0 13.30 0.80 7 -6 0 12.10 1.50 -7 6 0 12.00 1.00 7 -6 -1 102.19 4.20 7 -6 -1 100.49 5.00 -7 6 1 102.49 4.90 -7 6 2 18.90 1.80 -7 6 3 198.88 9.50 -7 6 4 47.20 3.70 -7 6 5 31.00 3.10 -7 6 6 6.40 1.70 -7 6 7 16.40 2.70 -7 6 8 0.20 1.10 6 -6 8 0.30 1.40 6 -6 7 2.10 1.80 6 -6 6 76.39 6.50 6 -6 5 78.29 6.30 6 -6 4 51.29 4.60 -6 6 -4 45.10 3.00 -6 6 -3 26.20 1.90 6 -6 2 235.18 11.80 6 -6 2 251.87 9.60 -6 6 -2 248.78 10.10 6 -6 1 27.50 1.30 6 -6 1 27.10 2.50 -6 6 -1 28.10 1.50 6 -6 0 1175.58 45.80 6 -6 0 1151.88 49.80 -6 6 0 1226.58 51.89 6 -6 -1 28.50 1.40 6 -6 -1 28.80 2.00 -6 6 1 29.20 1.90 -6 6 2 263.37 11.40 -6 6 3 31.30 2.60 -6 6 4 51.99 3.80 -6 6 5 75.39 5.10 -6 6 6 75.59 5.30 -6 6 7 1.50 1.20 -6 6 8 0.00 1.10 5 -6 8 5.80 2.50 5 -6 7 15.30 3.10 5 -6 6 2.50 1.70 5 -6 5 106.49 7.20 -5 6 -5 92.89 5.40 5 -6 4 11.50 2.10 -5 6 -4 8.90 1.30 5 -6 3 142.79 7.90 -5 6 -3 129.79 6.20 5 -6 2 164.98 6.30 5 -6 2 153.28 8.20 -5 6 -2 160.98 6.90 5 -6 1 174.28 6.60 5 -6 1 162.88 8.10 -5 6 -1 168.78 6.90 5 -6 0 22.50 1.90 5 -6 0 23.20 1.10 -5 6 0 23.80 1.40 -5 6 1 178.38 7.70 -5 6 2 178.18 8.10 -5 6 3 145.39 7.20 -5 6 4 12.10 1.80 -5 6 5 112.49 6.50 -5 6 6 1.40 1.00 -5 6 7 14.10 2.40 -5 6 8 3.90 1.60 4 -6 8 9.80 2.80 4 -6 7 2.80 1.70 4 -6 6 26.30 3.50 -4 6 -6 22.50 2.50 4 -6 5 2.50 1.40 -4 6 -5 2.20 0.90 4 -6 4 110.79 6.80 -4 6 -4 99.49 5.40 4 -6 3 11.80 1.90 -4 6 -3 10.00 1.20 4 -6 2 247.58 9.10 4 -6 2 228.68 11.00 -4 6 -2 233.28 9.80 4 -6 1 137.59 5.40 4 -6 1 132.09 6.70 -4 6 -1 140.69 5.70 4 -6 0 343.37 14.30 -4 6 0 345.47 13.60 -4 6 1 144.89 6.30 -4 6 2 255.97 11.00 -4 6 3 11.50 1.50 -4 6 4 125.59 6.70 -4 6 5 3.10 1.20 -4 6 6 27.90 2.90 -4 6 7 3.10 1.40 -4 6 8 10.40 2.30 -3 6 -7 2.50 1.30 3 -6 6 68.69 5.50 -3 6 -6 62.89 4.50 3 -6 5 39.70 3.80 -3 6 -5 35.20 2.90 3 -6 4 193.48 9.90 -3 6 -4 183.88 8.80 3 -6 3 136.79 7.20 -3 6 -3 130.19 6.20 3 -6 2 248.18 9.60 3 -6 2 256.47 11.30 -3 6 -2 245.88 10.40 3 -6 1 332.37 14.40 -3 6 -1 353.56 14.00 3 -6 0 210.58 8.90 -3 6 0 204.78 8.40 -3 6 1 371.36 14.90 -3 6 2 274.47 11.60 -3 6 3 166.38 7.90 -3 6 4 228.78 10.60 -3 6 5 40.90 3.30 -3 6 6 76.19 5.10 -3 6 7 3.80 1.50 -3 6 8 32.90 3.50 -3 6 9 1.50 1.20 -2 6 -8 3.40 1.60 2 -6 7 45.30 4.40 -2 6 -7 43.00 3.90 2 -6 6 0.70 1.00 -2 6 -6 0.80 0.90 2 -6 5 190.68 9.70 -2 6 -5 168.28 8.80 2 -6 4 136.99 7.30 -2 6 -4 122.79 6.50 2 -6 3 158.18 7.80 -2 6 -3 153.58 7.20 2 -6 2 54.59 3.40 -2 6 -2 54.49 2.90 2 -6 1 295.27 12.20 -2 6 -1 281.47 11.50 -2 6 0 16.40 1.00 -2 6 1 296.97 11.90 -2 6 2 65.59 3.40 -2 6 3 179.88 8.30 -2 6 4 158.68 7.80 -2 6 5 205.28 10.00 -2 6 6 0.20 0.80 -2 6 7 47.00 4.00 -2 6 8 3.00 1.40 -2 6 9 7.40 2.00 -1 6 -8 16.30 2.70 -1 6 -7 3.20 1.40 1 -6 6 9.20 1.90 -1 6 -6 8.20 1.90 1 -6 5 48.10 3.80 -1 6 -5 45.00 3.50 1 -6 4 4.40 1.20 -1 6 -4 3.60 1.00 1 -6 3 51.49 3.30 -1 6 -3 49.10 3.10 1 -6 2 39.60 2.60 -1 6 -2 40.20 2.30 1 -6 1 22.20 1.60 -1 6 -1 22.10 1.30 -1 6 -1 22.30 0.90 -1 6 0 675.23 27.20 -1 6 1 22.90 1.30 -1 6 2 47.30 2.60 -1 6 3 62.19 3.50 -1 6 4 5.10 1.20 -1 6 5 53.19 3.80 -1 6 6 9.40 1.80 -1 6 7 4.70 1.50 -1 6 8 18.50 2.60 -1 6 9 5.50 1.80 0 6 -9 -0.10 1.00 0 6 -8 34.50 3.80 0 6 -7 0.00 0.80 0 -6 6 120.59 6.80 0 6 -6 108.49 6.70 0 -6 5 0.10 0.60 0 6 -5 0.20 0.60 0 -6 4 19.40 1.90 0 6 -4 17.80 1.90 0 -6 3 0.40 0.40 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298.57 11.60 2 6 2 61.69 2.60 2 6 2 60.49 2.80 2 6 3 180.88 7.70 2 6 4 159.98 7.30 2 6 5 212.68 9.70 2 6 6 0.70 0.80 2 6 9 10.90 1.10 3 6 -9 1.10 2.30 3 6 -8 29.40 3.70 3 6 -7 2.20 1.40 3 6 -6 58.49 4.60 3 6 -5 30.80 2.90 -3 -6 4 176.58 7.50 3 6 -4 170.98 8.60 3 6 -3 123.89 4.90 3 6 -2 212.18 9.30 3 6 -2 211.48 8.20 3 6 -1 306.07 11.80 3 6 -1 303.07 12.50 3 6 0 206.68 7.90 3 6 0 196.68 8.30 3 6 1 342.17 13.40 3 6 1 349.57 16.40 3 6 2 265.87 10.40 3 6 2 257.67 10.30 3 6 3 154.28 6.30 3 6 3 156.78 6.60 3 6 4 228.98 9.70 3 6 4 221.58 9.00 3 6 5 44.60 2.90 3 6 5 41.20 2.10 3 6 6 68.49 3.20 3 6 7 3.90 0.70 3 6 8 38.00 2.10 3 6 9 2.70 0.70 4 6 -8 9.30 2.50 4 6 -7 3.10 1.40 4 6 -6 23.10 2.80 4 6 -5 1.60 0.90 4 6 -4 89.59 5.30 4 6 -4 91.99 3.70 4 6 -3 9.10 0.60 4 6 -3 9.50 1.40 4 6 -2 198.08 7.80 4 6 -2 201.98 8.90 4 6 -1 121.49 4.70 4 6 -1 113.59 5.40 4 6 0 314.27 12.50 4 6 0 306.87 12.00 4 6 1 141.19 5.70 4 6 1 132.79 5.50 4 6 2 253.87 9.90 4 6 2 248.58 9.90 4 6 3 12.30 0.90 4 6 3 11.90 0.80 4 6 4 120.09 5.50 4 6 4 124.39 5.10 4 6 5 3.20 0.50 4 6 6 30.20 1.70 4 6 7 4.40 0.70 4 6 8 11.80 1.10 5 6 -8 2.90 1.60 5 6 -7 13.20 2.50 5 6 -6 1.10 1.10 5 6 -5 85.99 5.50 5 6 -4 9.40 0.60 5 6 -4 8.20 1.50 5 6 -3 111.69 4.50 5 6 -3 110.39 5.80 5 6 -2 122.89 6.10 5 6 -2 128.09 5.00 5 6 -1 137.09 6.30 5 6 -1 139.79 5.50 5 6 0 19.50 1.00 5 6 0 18.80 1.30 5 6 1 162.08 6.50 5 6 1 153.28 6.30 5 6 2 163.58 6.50 5 6 2 156.18 6.40 5 6 3 146.39 5.90 5 6 3 141.39 5.90 5 6 4 11.60 0.90 5 6 5 120.69 5.10 5 6 6 1.60 0.50 5 6 7 17.40 1.30 5 6 8 5.10 0.80 6 6 -8 0.10 1.10 6 6 -7 0.80 1.10 6 6 -6 59.49 4.70 6 6 -5 56.39 4.30 6 6 -4 44.00 2.00 6 6 -4 38.70 3.20 6 6 -3 23.10 2.20 6 6 -3 23.20 1.20 6 6 -2 186.18 8.60 6 6 -2 194.58 7.60 6 6 -1 21.20 1.70 6 6 -1 22.50 1.10 6 6 0 939.61 36.00 6 6 0 915.41 37.30 6 6 1 23.50 1.20 6 6 1 21.90 1.40 6 6 2 244.78 9.70 6 6 2 242.18 9.60 6 6 3 28.70 1.50 6 6 4 53.49 2.50 6 6 5 78.79 3.50 6 6 6 79.99 3.60 6 6 7 1.90 0.60 6 6 8 0.00 0.40 7 6 -8 -0.10 1.00 7 6 -7 9.90 2.40 7 6 -6 4.40 1.60 7 6 -5 27.40 1.40 7 6 -5 21.30 2.60 7 6 -4 38.40 1.80 7 6 -4 33.80 3.00 7 6 -3 147.99 5.90 7 6 -3 140.89 7.20 7 6 -2 13.70 0.80 7 6 -2 12.40 1.40 7 6 -1 76.09 4.00 7 6 -1 80.49 3.30 7 6 0 9.10 1.00 7 6 0 11.40 0.70 7 6 1 77.99 3.30 7 6 1 76.79 3.60 7 6 2 15.70 0.90 7 6 3 184.48 7.50 7 6 4 46.30 2.20 7 6 5 31.80 1.80 7 6 6 8.20 0.80 7 6 7 16.40 1.30 7 6 8 0.70 0.50 8 6 -7 8.60 2.30 8 6 -6 3.90 1.60 8 6 -5 13.10 2.20 8 6 -5 14.90 1.00 8 6 -4 18.10 2.20 8 6 -4 20.20 1.20 8 6 -3 89.69 3.70 8 6 -3 81.69 4.90 8 6 -2 8.60 1.30 8 6 -2 10.80 0.70 8 6 -1 21.30 1.10 8 6 -1 18.80 1.60 8 6 0 14.70 0.90 8 6 0 14.00 1.20 8 6 1 19.40 1.10 8 6 2 11.80 0.80 8 6 3 106.79 4.50 8 6 4 24.00 1.40 8 6 5 17.10 1.20 8 6 6 4.10 0.70 8 6 7 9.70 1.10 8 6 8 4.00 0.80 9 6 -7 7.20 2.10 9 6 -6 30.00 3.40 9 6 -5 8.30 1.90 9 6 -5 7.80 0.80 9 6 -4 10.70 1.80 9 6 -4 12.60 0.90 9 6 -3 1.90 0.90 9 6 -3 1.70 0.40 9 6 -2 14.10 0.90 9 6 -2 12.80 1.50 9 6 -1 29.30 2.20 9 6 -1 34.80 1.60 9 6 0 3.10 0.40 9 6 2 15.10 1.00 9 6 3 1.90 0.40 9 6 4 15.50 1.10 9 6 5 10.80 1.00 9 6 6 40.70 2.20 9 6 7 8.50 1.00 10 6 -7 11.90 2.80 10 6 -6 19.10 2.70 10 6 -5 22.40 2.80 10 6 -5 26.50 1.50 10 6 -4 56.59 2.50 10 6 -4 46.10 3.80 10 6 -3 36.70 1.80 10 6 -3 32.50 2.80 10 6 -2 12.50 1.60 10 6 -2 16.40 1.00 10 6 -1 4.60 0.90 10 6 -1 6.20 0.60 10 6 0 61.99 2.80 10 6 1 6.40 0.60 10 6 2 14.90 1.00 10 6 3 34.00 1.80 10 6 4 58.59 2.80 10 6 5 29.60 1.70 10 6 6 28.20 1.80 10 6 7 15.40 1.30 11 6 -7 2.10 1.50 11 6 -6 4.20 1.70 11 6 -5 19.50 2.60 11 6 -5 22.00 1.40 11 6 -4 9.70 0.90 11 6 -4 9.10 1.80 11 6 -3 33.30 2.90 11 6 -3 36.50 1.90 11 6 -2 30.20 2.60 11 6 -2 34.60 1.80 11 6 -1 128.89 5.40 11 6 0 50.39 2.40 11 6 1 121.79 5.10 11 6 2 32.60 1.70 11 6 3 33.60 1.80 11 6 4 9.10 0.90 11 6 5 22.50 1.50 11 6 6 4.70 0.80 11 6 7 1.70 0.60 12 6 -6 18.80 2.80 12 6 -5 22.60 1.50 12 6 -5 19.80 2.70 12 6 -4 16.40 1.20 12 6 -4 14.30 2.10 12 6 -3 104.39 6.30 12 6 -3 124.69 5.00 12 6 -2 3.80 0.60 12 6 -1 38.80 2.00 12 6 0 105.49 4.60 12 6 1 37.20 1.90 12 6 2 3.30 0.50 12 6 3 116.29 5.00 12 6 4 16.30 1.20 12 6 5 23.80 1.50 12 6 6 24.90 1.60 13 6 -6 0.40 1.00 13 6 -5 7.70 1.90 13 6 -5 9.70 1.00 13 6 -4 18.30 1.30 13 6 -3 10.30 1.00 13 6 -2 17.60 1.30 13 6 -1 72.69 3.40 13 6 0 -0.10 0.30 13 6 1 71.39 3.30 13 6 2 15.90 1.10 13 6 3 8.00 0.80 13 6 4 15.30 1.20 13 6 5 9.00 0.90 13 6 6 0.40 0.40 14 6 -5 0.40 0.50 14 6 -4 4.10 0.70 14 6 -3 1.70 0.50 14 6 -2 1.70 0.50 14 6 -1 23.20 1.50 14 6 0 7.70 0.80 14 6 1 20.10 1.30 14 6 2 2.40 0.50 14 6 3 1.60 0.50 14 6 4 3.80 0.60 14 6 5 0.10 0.40 15 6 -4 1.00 0.50 15 6 -3 1.10 0.50 15 6 -2 9.00 1.00 15 6 -1 6.10 0.80 15 6 0 28.80 1.70 15 6 1 5.50 0.80 15 6 2 8.00 0.80 15 6 3 1.70 0.50 15 6 4 1.30 0.50 16 6 -3 13.10 1.20 16 6 -2 4.30 0.80 16 6 -1 1.20 0.50 16 6 0 15.30 1.20 16 6 1 1.30 0.50 16 6 2 4.40 0.70 16 6 3 13.70 1.20 17 6 -2 5.00 1.00 17 6 -1 3.80 0.70 17 6 0 10.90 1.10 17 6 1 3.40 0.70 17 -7 0 6.90 1.70 17 -7 -1 0.30 0.60 17 -7 -2 15.30 1.60 16 -7 3 17.30 3.50 16 -7 0 6.40 1.00 16 -7 -1 2.10 0.70 16 -7 -2 20.40 1.70 16 -7 -3 23.10 1.90 15 -7 4 8.30 2.90 15 -7 3 -0.30 1.10 15 -7 2 7.70 2.50 15 -7 0 0.50 0.50 15 -7 -1 4.40 0.90 15 -7 -2 9.00 1.20 15 -7 -3 0.40 0.60 14 -7 5 13.20 3.80 14 -7 4 3.80 2.10 14 -7 3 14.10 3.20 14 -7 2 13.90 2.90 14 -7 1 2.80 1.50 14 -7 0 23.70 1.60 14 -7 -1 2.80 0.70 14 -7 -2 17.00 1.50 14 -7 -3 14.70 1.40 -14 7 4 4.10 1.60 -14 7 5 13.00 2.50 13 -7 5 4.90 2.40 13 -7 4 -0.20 1.40 13 -7 3 22.30 3.70 13 -7 2 46.10 4.80 13 -7 1 4.50 1.70 13 -7 1 4.60 0.80 13 -7 0 8.90 1.00 13 -7 -1 4.80 0.80 13 -7 -2 48.50 2.60 13 -7 -3 26.00 1.80 -13 7 3 25.30 2.70 -13 7 4 0.30 1.00 -13 7 5 5.50 1.90 -13 7 6 5.30 3.00 12 -7 6 2.20 2.00 12 -7 5 2.70 2.00 12 -7 4 17.20 3.40 12 -7 3 20.80 3.60 12 -7 2 22.50 3.30 12 -7 1 47.40 2.40 12 -7 1 43.70 4.20 12 -7 0 89.99 4.00 12 -7 0 81.99 5.50 12 -7 -1 49.80 2.60 12 -7 -2 20.90 1.50 -12 7 2 22.70 2.20 12 -7 -3 20.80 1.60 -12 7 3 21.00 2.40 -12 7 4 16.60 2.40 -12 7 5 3.20 1.40 -12 7 6 1.50 1.30 11 -7 6 -0.80 1.30 11 -7 5 19.00 3.70 11 -7 4 35.10 4.60 11 -7 3 53.19 5.30 11 -7 2 79.59 6.20 11 -7 1 50.39 4.40 11 -7 1 51.19 2.50 11 -7 0 63.69 2.90 11 -7 0 59.29 4.30 11 -7 -1 50.89 2.60 -11 7 1 55.79 3.20 11 -7 -2 82.19 3.90 -11 7 2 88.79 4.90 -11 7 3 56.39 4.00 -11 7 4 39.50 3.60 -11 7 5 22.50 3.00 -11 7 6 0.20 1.10 10 -7 7 8.40 3.10 10 -7 6 6.50 2.80 10 -7 5 14.30 3.40 10 -7 4 3.20 2.00 10 -7 3 25.40 3.60 10 -7 2 69.19 5.50 10 -7 1 3.60 1.30 10 -7 1 4.30 0.60 10 -7 0 96.29 5.80 10 -7 0 103.29 4.40 -10 7 0 102.39 4.60 10 -7 -1 4.30 1.10 10 -7 -1 5.00 0.70 -10 7 1 5.00 1.00 10 -7 -2 70.69 3.30 -10 7 2 73.29 4.30 -10 7 3 25.90 2.60 -10 7 4 4.40 1.50 -10 7 5 14.20 2.40 -10 7 6 4.90 1.70 -10 7 7 8.80 2.30 9 -7 7 3.10 2.10 9 -7 6 8.90 3.00 9 -7 5 27.80 4.10 9 -7 4 79.89 6.70 9 -7 3 12.20 2.60 9 -7 2 107.19 7.00 9 -7 1 21.00 1.20 9 -7 1 19.70 2.50 -9 7 -1 19.30 1.30 9 -7 0 47.60 2.20 9 -7 0 41.70 3.30 -9 7 0 47.80 2.50 9 -7 -1 19.10 1.20 9 -7 -1 18.70 1.80 -9 7 1 19.40 1.60 9 -7 -2 114.79 4.90 -9 7 2 113.19 5.90 -9 7 3 12.50 1.80 -9 7 4 83.59 5.40 -9 7 5 28.30 3.20 -9 7 6 9.20 2.30 -9 7 7 4.00 1.80 8 -7 8 6.00 3.10 8 -7 7 2.00 2.00 8 -7 6 16.60 3.50 8 -7 5 4.00 2.00 8 -7 4 59.79 5.40 8 -7 3 32.20 3.70 8 -7 2 7.50 1.70 -8 7 -2 7.20 0.90 8 -7 1 61.59 4.50 8 -7 1 68.99 2.90 -8 7 -1 65.19 3.10 8 -7 0 52.89 3.70 8 -7 0 55.09 2.50 -8 7 0 55.89 2.80 8 -7 -1 65.79 3.80 8 -7 -1 64.89 2.90 -8 7 1 66.09 3.50 -8 7 2 8.50 1.30 -8 7 3 32.80 2.80 -8 7 4 57.09 4.20 -8 7 5 4.30 1.50 -8 7 6 15.00 2.60 -8 7 7 2.90 1.60 7 -7 8 22.20 3.90 7 -7 7 82.79 7.20 7 -7 6 46.10 5.10 7 -7 5 35.20 4.20 7 -7 4 26.60 3.40 7 -7 3 88.49 6.10 -7 7 -3 79.29 4.20 7 -7 2 115.89 7.00 -7 7 -2 115.59 5.20 7 -7 1 38.80 1.70 7 -7 1 34.50 3.00 -7 7 -1 37.50 2.00 7 -7 0 6.90 1.20 7 -7 0 7.50 0.60 -7 7 0 7.90 0.80 7 -7 -1 38.70 2.60 7 -7 -1 38.50 1.90 -7 7 1 39.30 2.40 -7 7 2 131.89 6.40 -7 7 3 96.39 5.40 -7 7 4 29.10 2.80 -7 7 5 38.30 3.50 -7 7 6 48.40 4.30 -7 7 7 91.49 6.40 -7 7 8 21.90 4.00 6 -7 8 5.20 2.30 6 -7 7 0.80 1.40 6 -7 6 8.70 2.60 6 -7 5 1.40 1.30 6 -7 4 47.00 4.30 -6 7 -4 37.50 2.80 6 -7 3 50.29 4.20 -6 7 -3 44.80 2.80 6 -7 2 179.88 9.40 6 -7 2 187.68 7.20 -6 7 -2 181.68 7.80 6 -7 1 104.49 4.10 6 -7 1 96.89 5.70 -6 7 -1 103.39 4.40 6 -7 0 26.40 1.30 6 -7 0 27.60 2.30 -6 7 0 29.90 1.70 -6 7 1 110.39 5.10 -6 7 2 192.58 8.70 -6 7 3 54.39 3.60 -6 7 4 52.59 3.80 -6 7 5 0.80 1.00 -6 7 6 7.60 1.80 -6 7 7 1.90 1.20 -6 7 8 4.40 1.80 5 -7 8 53.59 5.70 5 -7 7 67.59 6.20 5 -7 6 5.90 2.10 5 -7 5 18.60 2.90 -5 7 -5 16.60 2.00 5 -7 4 159.68 8.90 -5 7 -4 135.49 7.00 5 -7 3 37.30 3.40 -5 7 -3 32.50 2.30 5 -7 2 140.79 7.40 5 -7 2 136.39 5.30 -5 7 -2 128.09 5.90 5 -7 1 129.39 6.70 5 -7 1 131.69 5.10 -5 7 -1 128.69 5.50 5 -7 0 573.64 24.10 -5 7 0 617.04 24.30 -5 7 1 145.29 6.40 -5 7 2 143.19 6.70 -5 7 3 41.10 3.00 -5 7 4 170.58 8.60 -5 7 5 21.10 2.60 -5 7 6 5.80 1.70 -5 7 7 59.39 4.80 -5 7 8 55.59 4.80 4 -7 8 10.30 2.90 4 -7 7 4.50 2.00 4 -7 6 8.80 2.40 -4 7 -6 6.40 1.60 4 -7 5 4.80 1.80 -4 7 -5 3.80 1.10 4 -7 4 102.99 6.40 -4 7 -4 86.69 5.00 4 -7 3 32.90 3.00 -4 7 -3 32.40 2.20 4 -7 2 281.37 12.80 4 -7 2 295.97 10.90 -4 7 -2 273.47 11.70 4 -7 1 137.59 6.80 -4 7 -1 142.39 5.90 4 -7 0 55.49 3.20 -4 7 0 58.49 2.70 -4 7 1 151.28 6.50 -4 7 2 318.07 13.40 -4 7 3 38.20 2.80 -4 7 4 119.49 6.50 -4 7 5 4.30 1.30 -4 7 6 8.80 2.00 -4 7 7 4.80 1.70 -4 7 8 8.00 2.10 3 -7 7 27.70 3.60 -3 7 -7 25.90 3.00 3 -7 6 23.60 3.20 -3 7 -6 20.60 2.50 3 -7 5 19.60 2.60 -3 7 -5 16.70 2.00 3 -7 4 41.30 3.60 -3 7 -4 38.60 2.90 3 -7 3 4.80 1.30 -3 7 -3 4.30 0.90 3 -7 2 451.85 18.50 -3 7 -2 418.56 17.50 3 -7 1 337.67 14.50 -3 7 -1 352.26 13.80 -3 7 0 50.79 2.40 -3 7 1 369.76 14.80 -3 7 2 493.75 20.00 -3 7 3 6.00 1.10 -3 7 4 49.99 3.50 -3 7 5 21.70 2.50 -3 7 6 21.90 2.60 -3 7 7 30.10 3.20 -3 7 8 1.10 1.20 -2 7 -8 4.30 1.70 2 -7 7 23.40 3.20 -2 7 -7 18.70 2.60 2 -7 6 19.90 2.70 -2 7 -6 18.60 2.40 2 -7 5 22.80 2.70 -2 7 -5 21.40 2.30 2 -7 4 8.70 1.60 -2 7 -4 6.90 1.30 2 -7 3 4.70 1.10 -2 7 -3 4.80 0.90 2 -7 2 123.89 6.10 -2 7 -2 120.69 5.60 2 -7 1 632.74 25.80 -2 7 -1 604.14 25.00 -2 7 0 158.38 6.50 -2 7 1 659.23 26.10 -2 7 2 149.09 6.70 -2 7 3 5.70 1.10 -2 7 4 9.10 1.50 -2 7 5 24.90 2.60 -2 7 6 23.40 2.70 -2 7 7 23.60 2.90 -2 7 8 5.10 1.70 -1 7 -8 24.80 3.20 -1 7 -7 6.30 1.80 1 -7 6 49.99 4.10 -1 7 -6 46.60 3.90 1 -7 5 56.89 4.10 -1 7 -5 47.90 3.70 1 -7 4 147.69 7.50 -1 7 -4 146.39 7.30 1 -7 3 31.90 2.40 -1 7 -3 29.30 2.20 1 -7 2 46.70 2.80 -1 7 -2 42.60 2.60 1 -7 1 864.21 34.70 -1 7 -1 777.12 32.50 -1 7 -1 824.52 31.60 -1 7 0 1.80 0.40 -1 7 1 917.91 36.80 -1 7 2 55.59 2.90 -1 7 3 39.80 2.60 -1 7 4 198.98 9.30 -1 7 5 68.19 4.40 -1 7 6 61.09 4.40 -1 7 7 7.00 1.80 -1 7 8 28.30 3.20 -1 7 9 4.20 1.70 0 7 -9 -0.60 0.90 0 7 -8 21.30 3.10 0 -7 6 10.70 1.80 0 7 -6 10.30 1.90 0 -7 5 0.10 0.60 0 7 -5 -0.10 0.60 0 -7 4 786.82 30.60 0 7 -4 720.53 30.60 0 -7 3 0.10 0.40 0 7 -3 0.00 0.40 0 -7 2 97.79 4.60 0 7 -2 87.29 4.50 0 7 -1 0.00 0.30 0 7 -1 -0.10 0.10 0 7 0 2756.22 123.59 0 7 1 -0.10 0.20 0 7 2 104.29 4.70 0 7 3 0.40 0.50 0 7 4 977.60 38.90 0 7 5 0.00 0.70 0 7 6 12.70 2.00 0 7 8 24.40 2.90 1 7 -9 2.50 1.70 1 7 -8 26.40 3.40 1 7 -7 6.00 1.80 1 7 -6 46.00 3.90 -1 -7 5 51.69 3.50 1 7 -5 52.49 3.90 -1 -7 4 150.38 7.00 1 7 -4 140.19 7.30 -1 -7 3 31.30 2.10 1 7 -3 29.80 2.30 1 7 -2 39.80 1.60 1 7 -2 41.80 2.50 1 7 -1 798.12 32.40 1 7 -1 789.72 32.70 1 7 0 1.40 0.20 1 7 0 1.60 0.40 1 7 1 864.41 34.50 1 7 2 53.39 2.60 1 7 3 40.40 2.40 1 7 4 192.98 8.70 1 7 5 72.29 4.30 1 7 6 58.09 4.00 1 7 7 7.60 1.80 2 7 -8 4.00 1.70 2 7 -7 20.10 2.80 2 7 -6 18.10 2.50 2 7 -5 18.60 2.20 -2 -7 4 6.60 1.00 2 7 -4 6.50 1.30 -2 -7 3 4.50 0.70 2 7 -3 4.50 0.30 2 7 -3 4.70 1.10 2 7 -2 110.29 5.30 2 7 -2 106.69 4.30 2 7 -1 561.34 22.10 2 7 -1 552.74 21.60 2 7 0 143.29 6.20 2 7 0 152.28 5.80 2 7 1 651.53 25.50 2 7 1 657.13 38.40 2 7 2 138.79 5.50 2 7 2 133.19 5.70 2 7 3 6.20 0.80 2 7 4 9.70 1.20 2 7 5 27.20 2.30 2 7 6 22.50 2.30 3 7 -8 0.90 1.10 3 7 -7 21.60 3.00 3 7 -6 16.80 2.40 3 7 -5 15.90 2.20 -3 -7 4 40.40 2.40 3 7 -3 3.20 0.90 3 7 -3 4.20 0.30 3 7 -2 363.26 14.20 3 7 -2 374.76 15.40 3 7 -1 292.47 11.50 3 7 -1 302.17 12.30 3 7 0 46.10 2.40 3 7 0 46.40 2.00 3 7 1 354.06 14.30 3 7 1 345.57 13.60 3 7 2 480.35 18.60 3 7 2 479.05 18.90 3 7 3 5.60 0.60 3 7 3 5.50 0.70 3 7 4 45.90 2.20 3 7 4 49.10 2.80 3 7 5 23.30 2.00 3 7 5 22.50 1.30 3 7 6 24.10 1.50 3 7 7 28.70 1.70 3 7 8 0.50 0.40 4 7 -8 5.70 1.90 4 7 -7 2.30 1.30 4 7 -6 7.40 1.90 4 7 -5 3.00 1.20 4 7 -4 79.29 4.90 4 7 -3 27.70 2.30 4 7 -3 26.20 1.20 4 7 -2 228.08 10.20 4 7 -2 239.78 9.10 4 7 -1 119.99 4.80 4 7 -1 122.79 5.60 4 7 0 47.20 2.50 4 7 0 48.50 2.00 4 7 1 139.69 5.60 4 7 1 141.89 5.90 4 7 2 310.27 12.10 4 7 2 302.57 12.00 4 7 3 35.20 1.80 4 7 3 36.90 1.90 4 7 4 118.39 5.30 4 7 4 112.79 4.90 4 7 5 4.80 0.60 4 7 6 10.20 1.00 4 7 7 4.10 0.70 4 7 8 9.50 1.10 5 7 -8 41.80 4.50 5 7 -7 52.89 4.70 5 7 -6 5.40 1.70 5 7 -5 14.80 2.10 5 7 -4 127.89 5.10 5 7 -4 120.39 6.70 5 7 -3 26.10 2.30 5 7 -3 27.30 1.30 5 7 -2 105.99 4.30 5 7 -2 105.09 5.30 5 7 -1 106.49 5.10 5 7 -1 108.19 4.30 5 7 0 489.45 19.30 5 7 0 479.25 18.70 5 7 1 124.79 5.30 5 7 1 122.19 5.00 5 7 2 129.79 5.40 5 7 2 137.99 5.60 5 7 3 39.10 1.90 5 7 3 40.60 2.00 5 7 4 161.48 6.60 5 7 5 23.20 1.40 5 7 6 6.20 0.80 5 7 7 66.59 3.30 5 7 8 57.09 3.00 6 7 -8 4.10 1.90 6 7 -7 1.30 1.30 6 7 -6 7.80 2.00 6 7 -5 0.20 0.80 6 7 -4 34.60 3.00 6 7 -4 36.60 1.70 6 7 -3 38.50 2.90 6 7 -3 40.70 1.80 6 7 -2 139.19 6.90 6 7 -2 153.08 5.90 6 7 -1 76.89 4.10 6 7 -1 82.19 3.30 6 7 0 22.60 1.10 6 7 0 22.50 1.60 6 7 1 84.69 3.60 6 7 1 86.09 3.90 6 7 2 188.78 7.60 6 7 2 180.68 7.40 6 7 3 51.79 2.40 6 7 4 49.60 2.40 6 7 5 1.40 0.40 6 7 6 10.20 1.00 6 7 7 1.70 0.60 6 7 8 6.80 1.00 7 7 -8 17.60 5.00 7 7 -7 60.79 5.10 7 7 -6 36.80 3.70 7 7 -5 27.80 2.90 7 7 -4 20.70 1.20 7 7 -4 19.50 2.30 7 7 -3 70.19 2.90 7 7 -3 63.49 4.10 7 7 -2 86.79 4.80 7 7 -2 94.89 3.80 7 7 -1 28.30 2.10 7 7 -1 29.80 1.40 7 7 0 6.60 0.80 7 7 0 5.60 0.50 7 7 1 31.70 1.50 7 7 1 29.80 1.80 7 7 3 88.99 3.80 7 7 4 26.40 1.50 7 7 5 39.20 2.10 7 7 6 53.39 2.70 7 7 7 95.59 4.40 7 7 8 24.70 1.70 8 7 -7 1.90 1.40 8 7 -6 10.10 2.20 8 7 -5 2.70 1.20 8 7 -4 44.90 2.10 8 7 -4 40.10 3.30 8 7 -3 24.20 1.30 8 7 -3 20.80 2.20 8 7 -2 6.00 0.60 8 7 -2 5.50 1.20 8 7 -1 43.10 2.80 8 7 -1 48.70 2.10 8 7 0 38.30 2.30 8 7 0 38.90 1.80 8 7 1 49.30 2.20 8 7 2 7.40 0.60 8 7 4 58.29 2.80 8 7 5 4.20 0.70 8 7 6 14.60 1.20 8 7 7 3.80 0.80 8 7 8 5.50 1.00 9 7 -7 2.70 1.50 9 7 -6 7.20 2.00 9 7 -5 18.40 2.50 9 7 -4 49.99 3.90 9 7 -4 59.39 2.60 9 7 -3 9.40 0.80 9 7 -3 8.30 1.50 9 7 -2 81.89 3.40 9 7 -2 71.39 4.30 9 7 -1 13.50 0.90 9 7 -1 12.30 1.40 9 7 0 32.10 1.60 9 7 1 13.90 0.90 9 7 2 85.69 3.70 9 7 3 9.80 0.80 9 7 4 70.89 3.30 9 7 5 26.10 1.60 9 7 6 7.50 1.00 9 7 7 2.80 0.70 10 7 -7 7.40 2.10 10 7 -6 3.20 1.40 10 7 -5 11.50 2.00 10 7 -4 3.30 0.50 10 7 -3 18.30 1.10 10 7 -3 15.80 2.00 10 7 -2 51.49 2.30 10 7 -2 45.60 3.20 10 7 -1 3.60 0.50 10 7 -1 2.80 1.30 10 7 0 72.29 3.20 10 7 1 3.20 0.50 10 7 2 48.80 2.30 10 7 3 18.40 1.20 10 7 4 3.10 0.50 10 7 5 14.90 1.20 10 7 6 6.30 0.90 10 7 7 9.20 1.10 11 7 -6 0.10 0.90 11 7 -5 12.30 2.10 11 7 -4 23.90 2.60 11 7 -4 26.00 1.50 11 7 -3 38.30 1.90 11 7 -3 33.50 2.90 11 7 -2 59.59 2.70 11 7 -2 51.29 3.90 11 7 -1 37.10 1.90 11 7 0 41.70 2.00 11 7 1 35.60 1.80 11 7 2 61.09 2.80 11 7 3 39.00 2.00 11 7 4 29.10 1.70 11 7 5 17.50 1.30 11 7 6 0.00 0.40 12 7 -6 1.60 1.20 12 7 -5 3.40 0.70 12 7 -5 1.90 1.10 12 7 -4 14.10 1.10 12 7 -4 10.30 1.90 12 7 -3 12.90 3.10 12 7 -3 14.20 1.10 12 7 -2 15.20 1.10 12 7 -1 35.20 1.90 12 7 0 59.89 2.80 12 7 1 32.40 1.70 12 7 2 15.80 1.10 12 7 3 14.10 1.10 12 7 4 14.00 1.10 12 7 5 2.80 0.60 12 7 6 1.10 0.50 13 7 -6 5.00 1.80 13 7 -5 3.40 0.70 13 7 -5 2.90 1.40 13 7 -4 0.20 0.40 13 7 -3 17.40 1.30 13 7 -2 34.80 1.90 13 7 -1 2.80 0.60 13 7 0 5.70 0.70 13 7 1 2.50 0.50 13 7 2 33.00 1.80 13 7 3 14.80 1.10 13 7 4 0.30 0.40 13 7 5 3.90 0.70 14 7 -5 9.90 1.10 14 7 -4 2.90 0.60 14 7 -3 11.60 1.10 14 7 -2 11.00 1.00 14 7 -1 2.90 0.60 14 7 0 16.50 1.20 14 7 1 1.70 0.50 14 7 2 9.90 0.90 14 7 3 10.00 1.00 14 7 4 2.80 0.60 14 7 5 8.20 0.90 15 7 -4 6.40 0.90 15 7 -3 -0.20 0.40 15 7 -2 5.50 0.80 15 7 -1 3.50 0.60 15 7 0 -0.10 0.30 15 7 1 3.30 0.60 15 7 2 4.70 0.70 15 7 3 -0.20 0.30 15 7 4 7.80 0.90 16 7 -3 13.00 1.20 16 7 -2 14.30 1.20 16 7 -1 1.70 0.60 16 7 0 4.10 0.70 16 7 1 1.70 0.50 16 7 2 12.10 1.10 16 7 3 12.70 1.80 17 7 -1 0.70 0.50 17 7 0 3.50 0.90 17 -8 -1 4.20 0.90 16 -8 3 4.10 2.20 16 -8 -1 47.00 2.80 16 -8 -2 0.10 0.60 15 -8 4 3.10 2.00 15 -8 3 9.20 2.90 15 -8 2 17.40 3.10 15 -8 -1 33.80 2.20 15 -8 -2 20.30 1.70 14 -8 4 7.80 2.80 14 -8 3 32.60 4.40 14 -8 2 45.10 4.80 14 -8 1 1.90 1.30 14 -8 0 9.60 1.10 14 -8 -1 1.80 0.60 14 -8 -2 46.40 2.70 -14 8 4 8.30 2.00 -14 8 5 4.70 1.80 13 -8 5 8.00 3.10 13 -8 4 0.90 1.50 13 -8 3 23.60 3.80 13 -8 2 3.30 1.80 13 -8 1 23.30 3.10 13 -8 0 -0.10 0.40 13 -8 -1 25.60 1.70 13 -8 -2 3.10 0.70 -13 8 3 26.10 2.70 -13 8 4 0.80 1.10 -13 8 5 9.20 2.20 12 -8 5 6.20 2.70 12 -8 4 56.89 5.90 12 -8 3 6.20 2.30 12 -8 2 37.60 4.20 12 -8 1 5.10 1.80 12 -8 0 22.30 1.50 12 -8 0 20.90 2.60 12 -8 -1 5.80 0.80 12 -8 -2 37.70 2.20 -12 8 2 40.50 3.00 -12 8 3 8.70 1.70 -12 8 4 62.99 4.70 -12 8 5 6.00 1.90 -12 8 6 2.60 1.60 11 -8 6 5.80 2.70 11 -8 5 22.90 4.10 11 -8 4 10.30 3.10 11 -8 3 51.59 5.20 11 -8 2 59.19 5.20 11 -8 1 19.40 2.70 11 -8 0 6.80 1.60 11 -8 0 8.60 0.90 11 -8 -1 22.70 1.50 -11 8 1 21.70 1.80 11 -8 -2 61.49 3.10 -11 8 2 62.49 3.90 -11 8 3 55.59 4.00 -11 8 4 9.70 2.00 -11 8 5 21.70 2.90 -11 8 6 5.90 2.00 10 -8 6 11.20 3.40 10 -8 5 0.80 1.60 10 -8 4 16.30 3.30 10 -8 3 0.10 1.10 10 -8 2 103.69 7.10 10 -8 1 53.79 4.30 10 -8 0 138.09 7.50 10 -8 0 146.19 5.90 -10 8 0 140.79 6.20 10 -8 -1 55.39 2.70 10 -8 -1 55.39 3.60 -10 8 1 54.79 3.20 -10 8 2 112.79 5.90 -10 8 3 0.20 0.80 -10 8 4 17.50 2.40 -10 8 5 0.50 1.00 -10 8 6 11.80 2.50 9 -8 7 3.90 2.40 9 -8 6 9.60 3.10 9 -8 5 0.50 1.40 9 -8 4 45.30 5.00 9 -8 3 24.70 3.50 9 -8 2 160.08 9.20 9 -8 1 72.39 5.10 9 -8 1 75.29 3.20 -9 8 -1 72.49 3.50 9 -8 0 18.40 1.10 9 -8 0 16.80 2.00 -9 8 0 19.30 1.40 9 -8 -1 77.69 4.60 9 -8 -1 79.19 3.60 -9 8 1 82.99 4.20 -9 8 2 171.98 8.10 -9 8 3 25.50 2.50 -9 8 4 49.60 3.90 -9 8 5 0.90 1.20 -9 8 6 7.70 2.10 -9 8 7 4.10 1.70 8 -8 7 3.50 2.10 8 -8 6 4.60 2.30 8 -8 5 19.10 3.40 8 -8 4 89.29 6.90 8 -8 3 31.40 3.70 8 -8 2 303.17 14.30 -8 8 -2 278.17 11.90 8 -8 1 89.19 5.60 8 -8 1 92.19 3.80 -8 8 -1 90.69 4.10 8 -8 0 32.00 1.60 8 -8 0 31.30 2.70 -8 8 0 34.60 2.00 -8 8 1 95.09 4.70 -8 8 2 338.77 14.50 -8 8 3 36.70 3.00 -8 8 4 96.99 5.90 -8 8 5 18.50 2.60 -8 8 6 3.50 1.60 -8 8 7 2.20 1.40 7 -8 8 10.70 3.30 7 -8 7 15.90 3.40 7 -8 6 44.50 5.10 7 -8 5 92.69 7.20 7 -8 4 115.89 7.90 7 -8 3 31.60 3.40 -7 8 -3 26.70 2.10 7 -8 2 130.19 7.40 -7 8 -2 115.59 5.50 7 -8 1 70.99 2.90 7 -8 1 68.89 4.60 -7 8 -1 67.89 3.30 7 -8 0 3.70 0.40 7 -8 0 3.50 1.00 -7 8 0 3.50 0.60 -7 8 1 74.49 3.80 -7 8 2 141.89 6.80 -7 8 3 35.30 2.80 -7 8 4 120.09 6.80 -7 8 5 103.69 6.40 -7 8 6 45.30 4.10 -7 8 7 17.60 2.90 6 -8 8 5.10 2.30 6 -8 7 10.70 3.00 6 -8 6 44.80 4.90 6 -8 5 67.49 5.80 6 -8 4 5.70 1.90 -6 8 -4 6.20 1.20 6 -8 3 31.20 3.20 -6 8 -3 27.00 2.10 6 -8 2 293.67 13.50 -6 8 -2 276.37 11.80 6 -8 1 94.39 3.70 6 -8 1 87.89 5.30 -6 8 -1 90.09 4.10 6 -8 0 63.09 3.80 -6 8 0 66.39 3.10 -6 8 1 102.99 4.90 -6 8 2 333.87 14.10 -6 8 3 35.40 2.80 -6 8 4 7.10 1.60 -6 8 5 71.09 5.00 -6 8 6 48.40 4.20 -6 8 7 9.20 2.20 -6 8 8 4.90 1.90 5 -8 8 2.70 1.90 5 -8 7 76.09 6.60 5 -8 6 44.60 4.70 5 -8 5 68.79 5.60 -5 8 -5 58.29 4.10 5 -8 4 4.70 1.70 -5 8 -4 3.30 1.00 5 -8 3 112.59 6.70 -5 8 -3 101.69 5.20 5 -8 2 208.18 10.10 -5 8 -2 201.18 8.70 5 -8 1 100.49 5.50 -5 8 -1 101.79 4.50 5 -8 0 2.50 0.80 -5 8 0 2.50 0.50 -5 8 1 112.69 5.20 -5 8 2 229.58 10.10 -5 8 3 131.29 6.70 -5 8 4 4.70 1.30 -5 8 5 74.49 5.00 -5 8 6 48.80 4.20 -5 8 7 83.49 5.90 -5 8 8 2.40 1.50 4 -8 7 14.50 2.90 4 -8 6 27.20 3.50 -4 8 -6 22.30 2.60 4 -8 5 25.40 3.20 -4 8 -5 19.30 2.20 4 -8 4 98.69 6.30 -4 8 -4 87.59 5.10 4 -8 3 32.30 3.00 -4 8 -3 28.80 2.20 4 -8 2 25.50 2.40 -4 8 -2 23.60 1.70 4 -8 1 72.89 4.20 -4 8 -1 74.29 3.40 -4 8 0 1.20 0.40 -4 8 1 79.79 3.80 -4 8 2 28.40 2.10 -4 8 3 38.50 2.80 -4 8 4 120.39 6.50 -4 8 5 27.10 2.80 -4 8 6 29.10 3.10 -4 8 7 16.20 2.60 -4 8 8 4.50 1.70 3 -8 7 33.80 3.90 -3 8 -7 24.90 3.10 3 -8 6 11.20 2.30 -3 8 -6 8.30 1.80 3 -8 5 47.20 4.10 -3 8 -5 41.50 3.30 3 -8 4 4.00 1.40 -3 8 -4 3.70 1.10 3 -8 3 47.80 3.50 -3 8 -3 40.00 2.70 3 -8 2 65.99 4.00 -3 8 -2 63.79 3.40 3 -8 1 13.40 1.50 -3 8 -1 12.80 1.00 -3 8 0 210.18 8.60 -3 8 1 14.60 1.10 -3 8 2 81.19 4.10 -3 8 3 54.79 3.40 -3 8 4 4.40 1.30 -3 8 5 57.89 4.10 -3 8 6 11.30 2.10 -3 8 7 34.80 3.50 -3 8 8 1.50 1.30 -2 8 -8 34.60 3.80 2 -8 7 5.10 2.10 -2 8 -7 5.40 1.70 2 -8 6 5.50 1.70 -2 8 -6 5.10 1.50 2 -8 5 108.69 6.50 -2 8 -5 99.59 5.90 2 -8 4 8.90 1.60 -2 8 -4 8.20 1.40 2 -8 3 4.50 1.20 -2 8 -3 2.70 0.80 2 -8 2 212.78 9.30 -2 8 -2 192.08 8.70 2 -8 1 84.39 4.30 -2 8 -1 77.09 3.70 -2 8 0 203.48 8.30 -2 8 1 85.09 3.90 -2 8 2 243.68 10.30 -2 8 3 4.50 1.00 -2 8 4 12.10 1.70 -2 8 5 138.59 7.40 -2 8 6 6.80 1.70 -2 8 7 6.80 1.80 -2 8 8 43.20 4.00 -1 8 -8 13.00 2.50 -1 8 -7 35.70 3.60 1 -8 6 10.20 2.00 -1 8 -6 11.20 2.00 1 -8 5 45.10 3.60 -1 8 -5 43.80 3.50 1 -8 4 82.29 4.90 -1 8 -4 78.09 4.70 1 -8 3 91.09 4.90 -1 8 -3 85.19 4.70 1 -8 2 159.18 7.40 -1 8 -2 159.18 7.10 -1 8 -1 277.87 10.70 -1 8 -1 277.67 11.30 -1 8 0 59.19 2.80 -1 8 1 316.77 12.70 -1 8 2 196.08 8.30 -1 8 3 121.09 5.90 -1 8 4 107.49 5.70 -1 8 5 59.99 4.10 -1 8 6 13.20 2.00 -1 8 7 47.70 4.00 -1 8 8 18.30 2.60 0 8 -8 11.60 2.60 0 8 -7 0.40 0.90 0 -8 6 27.60 3.10 0 8 -6 26.10 2.90 0 -8 5 -0.10 0.60 0 8 -5 -0.20 0.60 0 -8 4 145.49 7.00 0 8 -4 132.09 7.10 0 -8 3 0.20 0.40 0 8 -3 -0.10 0.40 0 -8 2 996.90 38.20 0 8 -2 862.01 37.80 0 8 -1 0.00 0.30 0 8 -1 0.00 0.10 0 8 0 461.25 17.70 0 8 0 455.35 18.70 0 8 1 0.20 0.20 0 8 2 1121.89 44.90 0 8 3 0.00 0.40 0 8 4 201.18 9.20 0 8 5 1.10 0.90 0 8 6 34.90 3.10 0 8 7 -0.40 0.80 0 8 8 16.20 2.40 1 8 -8 14.30 2.70 1 8 -7 32.80 3.50 1 8 -6 9.90 2.00 -1 -8 5 46.80 3.20 1 8 -5 40.60 3.40 -1 -8 4 82.69 4.30 1 8 -4 72.09 4.60 -1 -8 3 92.79 4.50 1 8 -3 82.29 4.70 1 8 -2 144.59 6.50 1 8 -2 137.39 5.50 1 8 -1 278.07 11.40 1 8 -1 274.47 10.70 1 8 0 55.49 2.70 1 8 0 54.09 2.20 1 8 1 313.57 12.20 1 8 1 311.57 12.40 1 8 2 185.08 7.70 1 8 3 116.39 5.40 1 8 4 105.99 5.40 1 8 5 58.19 3.80 1 8 6 14.00 1.90 1 8 7 46.50 3.70 2 8 -8 36.30 4.00 2 8 -7 4.50 1.60 2 8 -6 4.70 1.50 2 8 -5 92.89 5.70 -2 -8 4 9.10 1.20 2 8 -4 8.90 1.50 2 8 -3 2.30 0.80 2 8 -2 172.08 6.70 2 8 -2 175.28 7.90 2 8 -1 68.99 2.80 2 8 -1 68.49 3.50 2 8 0 191.88 8.00 2 8 0 190.78 7.50 2 8 1 82.59 3.60 2 8 1 79.19 3.30 2 8 2 234.38 9.30 2 8 2 234.38 9.50 2 8 3 3.70 0.70 2 8 4 12.10 1.40 2 8 5 135.69 6.70 2 8 6 8.40 1.60 3 8 -8 0.70 1.20 3 8 -7 26.90 3.30 3 8 -6 6.20 1.70 3 8 -5 39.20 3.40 3 8 -4 2.30 1.00 3 8 -3 38.40 2.80 3 8 -2 61.69 3.50 3 8 -2 55.49 2.40 3 8 -1 10.00 0.60 3 8 -1 11.30 1.10 3 8 0 192.88 8.00 3 8 0 186.28 7.40 3 8 1 13.60 1.00 3 8 1 13.80 0.80 3 8 2 74.39 3.20 3 8 2 74.49 3.30 3 8 3 52.79 2.40 3 8 3 50.99 2.60 3 8 4 4.10 0.60 3 8 4 4.40 0.80 3 8 5 57.09 3.40 3 8 5 55.49 2.70 3 8 6 12.10 1.00 3 8 7 31.20 1.90 3 8 8 0.80 0.50 4 8 -8 4.00 1.80 4 8 -7 10.70 2.40 4 8 -6 20.20 2.70 4 8 -5 15.80 2.20 4 8 -4 84.99 5.20 4 8 -3 26.40 1.20 4 8 -3 25.30 2.30 4 8 -2 20.70 1.80 4 8 -2 20.00 1.00 4 8 -1 62.79 3.30 4 8 -1 60.09 2.50 4 8 0 1.20 0.40 4 8 0 1.10 0.20 4 8 1 72.39 3.40 4 8 1 74.49 3.10 4 8 2 27.70 1.40 4 8 2 28.20 1.50 4 8 3 38.40 1.90 4 8 3 37.80 2.00 4 8 4 116.39 5.00 4 8 4 118.19 5.30 4 8 5 26.60 1.60 4 8 6 31.30 1.80 4 8 7 13.90 1.20 4 8 8 3.50 0.80 5 8 -8 1.60 1.30 5 8 -7 59.09 5.00 5 8 -6 35.00 3.50 5 8 -5 52.49 4.10 5 8 -4 2.50 1.10 5 8 -3 86.69 4.90 5 8 -3 85.39 3.50 5 8 -2 166.38 6.50 5 8 -2 159.38 7.60 5 8 -1 81.19 3.30 5 8 -1 77.99 4.10 5 8 0 2.00 0.50 5 8 0 1.60 0.30 5 8 1 92.39 4.10 5 8 1 89.99 3.80 5 8 2 207.78 8.50 5 8 2 217.98 8.70 5 8 3 124.09 5.10 5 8 3 116.39 5.00 5 8 4 3.70 0.50 5 8 5 77.69 3.60 5 8 6 48.90 2.50 5 8 7 79.19 3.80 5 8 8 1.70 0.70 6 8 -8 4.90 2.40 6 8 -7 6.70 2.00 6 8 -6 32.20 3.40 6 8 -5 45.80 3.80 6 8 -4 3.40 1.10 6 8 -3 22.10 2.20 6 8 -3 24.20 1.20 6 8 -2 225.78 8.80 6 8 -2 217.78 10.00 6 8 -1 69.49 3.80 6 8 -1 71.39 3.00 6 8 0 49.80 2.10 6 8 0 47.90 2.70 6 8 1 78.89 3.70 6 8 1 79.19 3.30 6 8 2 300.97 12.10 6 8 2 300.87 11.90 6 8 3 33.20 1.70 6 8 4 6.50 0.70 6 8 5 72.09 3.40 6 8 6 48.70 2.50 6 8 7 11.60 1.20 6 8 8 6.80 0.90 7 8 -7 12.10 2.70 7 8 -6 30.90 3.40 7 8 -5 70.79 5.00 7 8 -4 77.69 5.00 7 8 -3 25.50 1.30 7 8 -3 24.00 2.30 7 8 -2 86.49 4.80 7 8 -2 91.89 3.80 7 8 -1 46.60 2.90 7 8 -1 51.39 2.20 7 8 0 2.50 0.40 7 8 0 2.70 0.70 7 8 1 54.59 2.40 7 8 1 52.79 2.80 7 8 2 108.89 4.60 7 8 3 32.20 1.70 7 8 4 113.49 4.90 7 8 5 102.49 4.50 7 8 6 48.00 2.60 7 8 7 16.40 1.40 8 8 -7 3.40 1.50 8 8 -6 4.10 1.60 8 8 -5 12.90 2.10 8 8 -4 62.09 4.30 8 8 -3 25.00 1.30 8 8 -3 21.90 2.30 8 8 -2 206.58 9.80 8 8 -2 224.88 8.60 8 8 -1 62.59 2.70 8 8 -1 61.99 3.60 8 8 0 23.60 1.20 8 8 0 22.20 1.70 8 8 1 68.59 3.00 8 8 2 244.58 9.80 8 8 3 29.90 1.60 8 8 4 87.19 3.90 8 8 5 20.90 1.40 8 8 6 5.90 0.90 8 8 7 2.90 0.70 9 8 -7 3.40 1.60 9 8 -6 5.10 1.70 9 8 -5 0.40 0.80 9 8 -4 30.20 2.90 9 8 -4 34.10 1.70 9 8 -3 14.80 1.90 9 8 -3 17.60 1.10 9 8 -2 103.99 5.80 9 8 -2 117.59 4.70 9 8 -1 48.30 3.10 9 8 -1 54.49 2.40 9 8 0 13.10 0.90 9 8 1 51.89 2.40 9 8 2 119.59 5.00 9 8 3 19.80 1.20 9 8 4 38.50 2.00 9 8 5 0.10 0.40 9 8 6 9.40 1.10 9 8 7 5.20 0.90 10 8 -7 18.30 4.70 10 8 -6 8.90 2.20 10 8 -5 0.50 0.80 10 8 -4 12.80 0.90 10 8 -4 10.60 1.80 10 8 -3 0.10 0.60 10 8 -3 0.30 0.30 10 8 -2 74.39 3.20 10 8 -2 66.79 4.20 10 8 -1 38.20 1.90 10 8 0 97.39 4.20 10 8 1 37.10 1.80 10 8 2 75.49 3.30 10 8 3 0.40 0.30 10 8 4 14.60 1.10 10 8 5 0.80 0.50 10 8 6 13.60 1.20 10 8 7 27.50 2.10 11 8 -6 3.60 1.50 11 8 -5 15.80 2.40 11 8 -4 7.00 1.70 11 8 -4 8.10 0.80 11 8 -3 40.80 2.00 11 8 -3 33.20 3.00 11 8 -2 40.00 2.00 11 8 -1 14.20 1.00 11 8 0 5.10 0.60 11 8 1 15.20 1.00 11 8 2 38.90 2.00 11 8 3 36.10 1.90 11 8 4 8.10 0.90 11 8 5 17.10 1.30 11 8 6 5.00 0.80 12 8 -6 1.20 1.10 12 8 -5 3.30 1.30 12 8 -4 40.60 2.10 12 8 -4 37.00 3.40 12 8 -3 5.30 0.70 12 8 -2 24.90 1.50 12 8 -1 4.30 0.60 12 8 0 13.90 1.00 12 8 1 4.30 0.60 12 8 2 26.10 1.50 12 8 3 4.40 0.60 12 8 4 45.20 2.40 12 8 5 4.00 0.70 12 8 6 1.80 0.70 13 8 -5 5.50 1.70 13 8 -4 0.30 0.40 13 8 -3 17.30 1.20 13 8 -2 2.40 0.50 13 8 -1 17.10 1.20 13 8 0 0.10 0.30 13 8 1 17.40 1.20 13 8 2 2.40 0.50 13 8 3 15.70 1.20 13 8 4 0.80 0.40 13 8 5 5.00 0.80 14 8 -4 4.50 0.70 14 8 -3 22.70 1.50 14 8 -2 31.20 1.80 14 8 -1 1.30 0.50 14 8 0 4.90 0.70 14 8 1 0.80 0.40 14 8 2 28.60 1.70 14 8 3 21.20 1.40 14 8 4 4.30 0.70 15 8 -4 2.30 0.60 15 8 -3 5.40 0.80 15 8 -2 13.30 1.10 15 8 -1 20.40 1.40 15 8 0 0.50 0.40 15 8 1 20.40 1.40 15 8 2 11.00 1.00 15 8 3 5.30 0.80 16 8 -3 3.20 0.70 16 8 -2 -0.30 0.40 16 8 -1 28.90 1.80 16 8 0 2.70 0.60 16 8 1 27.60 1.70 16 8 2 0.60 0.40 16 -9 -2 15.40 1.60 15 -9 3 6.50 2.50 15 -9 2 1.30 1.50 15 -9 -1 12.80 1.30 15 -9 -2 0.90 0.70 14 -9 4 2.30 2.00 14 -9 3 11.00 3.10 14 -9 2 4.10 1.90 14 -9 1 43.30 4.30 14 -9 -1 48.00 2.70 14 -9 -2 4.20 0.90 -14 9 4 3.20 1.50 13 -9 5 21.70 4.70 13 -9 4 17.10 3.70 13 -9 3 33.50 4.40 13 -9 2 0.60 1.20 13 -9 1 24.60 3.20 13 -9 -1 28.10 1.80 -13 9 3 39.90 3.40 -13 9 4 17.50 2.60 -13 9 5 22.40 3.10 12 -9 5 29.10 4.50 12 -9 4 10.80 3.00 12 -9 3 3.00 1.90 12 -9 2 71.49 5.90 12 -9 1 16.80 2.60 12 -9 0 48.90 4.00 12 -9 -1 18.80 1.40 -12 9 2 73.59 4.40 -12 9 3 3.70 1.30 -12 9 4 11.50 2.20 -12 9 5 33.00 3.60 11 -9 6 5.00 2.50 11 -9 5 18.90 3.90 11 -9 4 3.70 2.20 11 -9 3 10.20 2.80 11 -9 2 26.50 3.50 11 -9 1 31.30 3.40 11 -9 0 31.80 1.70 11 -9 0 28.40 2.90 11 -9 -1 35.20 2.00 -11 9 1 33.40 2.40 -11 9 2 33.60 2.70 -11 9 3 11.60 1.90 -11 9 4 3.50 1.40 -11 9 5 18.30 2.80 -11 9 6 4.90 1.90 10 -9 6 1.00 1.60 10 -9 5 7.40 2.80 10 -9 4 14.00 3.20 10 -9 3 39.20 4.40 10 -9 2 11.60 2.30 10 -9 1 51.09 4.30 10 -9 0 9.40 1.70 10 -9 0 9.20 0.80 -10 9 0 10.10 1.10 10 -9 -1 56.09 2.80 -10 9 1 58.19 3.30 -10 9 2 13.50 1.70 -10 9 3 44.20 3.50 -10 9 4 16.40 2.40 -10 9 5 8.40 2.10 -10 9 6 1.50 1.30 9 -9 7 1.70 2.00 9 -9 6 16.20 3.60 9 -9 5 11.50 3.20 9 -9 4 7.40 2.40 9 -9 3 15.30 2.80 9 -9 2 3.50 1.50 9 -9 1 39.50 3.50 -9 9 -1 41.00 2.30 9 -9 0 141.19 7.60 9 -9 0 150.28 6.10 -9 9 0 148.49 6.50 -9 9 1 44.80 2.70 -9 9 2 4.80 1.10 -9 9 3 17.70 2.20 -9 9 4 7.40 1.80 -9 9 5 11.80 2.30 -9 9 6 16.10 2.60 8 -9 7 15.10 3.60 8 -9 6 2.60 1.80 8 -9 5 35.90 4.60 8 -9 4 9.30 2.50 8 -9 3 68.39 5.60 8 -9 2 8.10 2.10 -8 9 -2 8.00 1.00 8 -9 1 52.29 4.00 -8 9 -1 50.69 2.70 8 -9 0 19.90 2.20 -8 9 0 20.70 1.50 -8 9 1 59.49 3.30 -8 9 2 10.40 1.50 -8 9 3 78.59 4.80 -8 9 4 9.60 1.90 -8 9 5 37.20 3.60 -8 9 6 2.30 1.40 -8 9 7 16.30 2.90 7 -9 7 17.40 3.50 7 -9 6 17.20 3.30 7 -9 5 20.80 3.50 7 -9 4 85.29 6.50 7 -9 3 9.00 2.00 -7 9 -3 8.00 1.20 7 -9 2 62.69 4.60 -7 9 -2 57.89 3.20 7 -9 1 32.50 2.90 -7 9 -1 31.50 1.90 7 -9 0 340.27 15.00 -7 9 0 350.96 14.00 -7 9 1 35.80 2.30 -7 9 2 73.99 4.20 -7 9 3 10.50 1.60 -7 9 4 95.79 5.80 -7 9 5 20.90 2.80 -7 9 6 20.00 2.90 -7 9 7 15.40 2.70 6 -9 8 3.40 2.20 6 -9 7 7.40 2.60 6 -9 6 118.29 8.50 6 -9 5 123.49 8.40 6 -9 4 49.80 4.50 -6 9 -4 37.30 2.90 6 -9 3 37.10 3.60 -6 9 -3 32.50 2.40 6 -9 2 150.18 8.00 -6 9 -2 136.39 6.40 6 -9 1 135.69 7.10 -6 9 -1 131.89 5.80 6 -9 0 12.20 1.50 -6 9 0 11.10 1.00 -6 9 1 150.88 6.70 -6 9 2 175.88 8.10 -6 9 3 49.20 3.50 -6 9 4 57.49 4.20 -6 9 5 137.39 7.80 -6 9 6 120.99 7.40 -6 9 7 7.40 2.10 5 -9 8 13.70 3.20 5 -9 7 10.50 3.00 5 -9 6 24.20 3.70 5 -9 5 193.68 10.50 -5 9 -5 155.18 8.50 -5 9 -4 12.60 1.60 5 -9 3 60.39 4.40 -5 9 -3 47.80 3.10 5 -9 2 3.50 1.20 -5 9 -2 4.00 0.80 5 -9 1 74.49 4.40 -5 9 -1 69.89 3.40 -5 9 0 27.10 1.70 -5 9 1 79.39 3.90 -5 9 2 5.50 1.00 -5 9 3 62.49 3.90 -5 9 4 15.30 2.00 -5 9 5 220.08 11.00 -5 9 6 28.70 3.10 -5 9 7 11.30 2.30 -5 9 8 12.30 2.60 4 -9 7 18.90 3.10 4 -9 6 6.30 2.10 -4 9 -6 5.40 1.50 4 -9 5 9.20 2.10 -4 9 -5 6.50 1.50 4 -9 4 243.38 11.70 -4 9 -4 210.28 10.30 4 -9 3 12.60 1.90 -4 9 -3 10.00 1.30 4 -9 2 53.09 3.60 -4 9 -2 48.10 2.80 4 -9 1 76.29 4.40 -4 9 -1 74.79 3.60 -4 9 0 183.08 7.70 -4 9 1 85.99 4.10 -4 9 2 61.29 3.40 -4 9 3 16.20 1.80 -4 9 4 302.87 13.70 -4 9 5 11.70 2.00 -4 9 6 7.50 1.90 -4 9 7 21.10 2.90 -4 9 8 8.80 2.30 3 -9 7 4.40 1.80 -3 9 -7 3.00 1.40 3 -9 6 28.30 3.40 -3 9 -6 24.30 2.80 3 -9 5 96.79 6.20 -3 9 -5 84.29 5.40 3 -9 4 64.89 4.60 -3 9 -4 59.59 3.90 3 -9 3 29.80 2.70 -3 9 -3 25.20 2.10 3 -9 2 178.88 8.30 -3 9 -2 158.08 7.40 3 -9 1 148.39 7.00 -3 9 -1 141.99 6.30 -3 9 0 172.98 7.20 -3 9 1 166.88 7.10 -3 9 2 209.98 9.10 -3 9 3 39.80 2.80 -3 9 4 86.29 5.10 -3 9 5 121.09 6.80 -3 9 6 33.90 3.30 -3 9 7 4.60 1.60 -3 9 8 49.10 4.40 -2 9 -8 12.30 2.50 -2 9 -7 6.20 1.70 2 -9 6 19.40 2.70 -2 9 -6 15.90 2.30 2 -9 5 182.58 9.30 -2 9 -5 159.98 8.60 2 -9 4 11.20 1.80 -2 9 -4 9.30 1.50 2 -9 3 99.09 5.40 -2 9 -3 89.59 4.90 2 -9 2 25.20 2.10 -2 9 -1 10.30 1.00 -2 9 0 1.80 0.40 -2 9 1 11.80 1.00 -2 9 2 30.70 2.00 -2 9 3 135.19 6.50 -2 9 4 14.30 1.80 -2 9 5 232.98 11.10 -2 9 6 23.10 2.70 -2 9 7 11.40 2.20 -2 9 8 16.10 2.60 -1 9 -8 8.30 2.20 -1 9 -7 14.20 2.40 1 -9 6 9.10 1.80 -1 9 -6 9.20 1.90 1 -9 5 166.78 8.40 -1 9 -5 148.89 8.20 1 -9 4 85.79 5.00 -1 9 -4 79.79 4.80 1 -9 3 86.19 4.70 -1 9 -3 75.49 4.40 1 -9 2 71.49 3.90 -1 9 -2 60.89 3.50 -1 9 -1 243.68 9.30 -1 9 -1 240.38 10.10 -1 9 0 673.23 27.60 -1 9 1 281.17 11.40 -1 9 2 83.29 4.00 -1 9 3 110.39 5.40 -1 9 4 117.89 6.10 -1 9 5 212.38 10.20 -1 9 6 11.50 2.00 -1 9 7 21.20 2.70 -1 9 8 11.80 2.40 0 9 -8 19.70 3.00 0 9 -7 -0.10 0.90 0 9 -6 23.90 2.70 0 -9 5 0.20 0.60 0 9 -5 0.20 0.60 0 -9 4 216.58 9.60 0 9 -4 191.58 9.70 0 -9 3 0.00 0.40 0 9 -3 0.20 0.50 0 9 -2 52.69 3.10 0 9 -1 0.10 0.10 0 9 -1 -0.10 0.30 0 9 0 17.40 0.80 0 9 0 17.70 1.20 0 9 1 -0.10 0.20 0 9 2 73.99 3.60 0 9 3 -0.20 0.40 0 9 4 284.17 12.40 0 9 5 -0.10 0.70 0 9 6 35.20 3.10 0 9 7 -0.50 0.80 0 9 8 26.00 3.00 1 9 -8 8.80 2.40 1 9 -7 14.80 2.50 1 9 -6 8.50 2.00 -1 -9 5 156.18 7.40 1 9 -5 140.69 7.90 -1 -9 4 86.79 4.60 1 9 -4 78.79 4.90 1 9 -3 76.89 4.40 1 9 -2 58.79 3.30 1 9 -1 238.88 10.10 1 9 -1 239.78 9.30 1 9 0 668.03 27.20 1 9 0 653.63 29.30 1 9 1 279.37 10.80 1 9 1 274.67 11.10 1 9 2 76.49 3.60 1 9 3 108.69 5.10 1 9 4 119.79 5.90 1 9 5 209.78 9.70 1 9 6 11.50 1.90 1 9 7 19.30 2.40 2 9 -8 9.70 2.50 2 9 -7 6.10 1.90 2 9 -6 16.60 2.40 2 9 -5 150.48 8.10 2 9 -4 8.30 1.50 2 9 -3 84.49 4.80 2 9 -2 20.10 1.00 2 9 -2 21.00 1.80 2 9 -1 9.10 0.50 2 9 -1 9.60 1.00 2 9 0 1.50 0.20 2 9 0 1.30 0.40 2 9 1 12.50 0.90 2 9 1 12.00 0.70 2 9 2 27.90 1.60 2 9 2 29.10 1.40 2 9 3 124.99 5.60 2 9 4 14.30 1.40 2 9 5 226.48 10.20 2 9 6 24.20 2.40 2 9 8 13.80 1.30 3 9 -8 33.40 4.00 3 9 -7 2.30 1.40 3 9 -6 22.90 2.90 3 9 -5 79.49 5.30 3 9 -4 53.59 3.80 3 9 -3 22.90 2.10 3 9 -2 134.49 5.40 3 9 -2 141.99 6.60 3 9 -1 122.79 5.70 3 9 -1 119.39 4.80 3 9 0 159.88 6.20 3 9 0 154.48 6.80 3 9 1 145.69 6.20 3 9 1 145.09 5.80 3 9 2 183.18 7.40 3 9 2 185.88 7.60 3 9 3 34.20 2.00 3 9 3 34.50 1.70 3 9 4 81.79 4.00 3 9 4 77.89 3.60 3 9 5 112.49 5.10 3 9 5 124.49 5.90 3 9 6 32.00 1.80 3 9 7 3.90 0.80 3 9 8 42.80 2.40 4 9 -8 6.10 2.10 4 9 -7 15.00 2.50 4 9 -6 5.10 1.70 4 9 -5 6.60 1.70 4 9 -4 197.08 9.70 4 9 -3 9.50 1.50 4 9 -2 40.00 1.70 4 9 -2 39.80 2.70 4 9 -1 61.19 2.60 4 9 -1 61.79 3.40 4 9 0 151.18 6.70 4 9 0 156.28 6.10 4 9 1 75.09 3.50 4 9 1 73.69 3.10 4 9 2 52.99 2.40 4 9 2 55.69 2.60 4 9 3 13.60 1.10 4 9 3 14.50 1.00 4 9 4 281.47 11.40 4 9 4 288.77 11.80 4 9 5 8.20 0.90 4 9 6 7.70 1.00 4 9 7 21.30 1.60 4 9 8 9.90 1.20 5 9 -8 8.10 3.40 5 9 -7 7.90 2.10 5 9 -6 17.30 2.60 5 9 -5 134.09 7.60 5 9 -4 10.70 1.80 5 9 -3 38.20 3.00 5 9 -2 2.80 0.30 5 9 -2 3.70 1.00 5 9 -1 54.39 2.30 5 9 -1 52.99 3.10 5 9 0 21.60 1.10 5 9 0 21.70 1.60 5 9 1 66.19 2.80 5 9 1 65.39 3.20 5 9 2 3.30 0.50 5 9 2 4.70 0.60 5 9 3 59.09 2.80 5 9 3 57.49 2.70 5 9 4 15.10 1.10 5 9 5 207.08 8.50 5 9 6 29.30 1.80 5 9 7 10.90 1.20 5 9 8 11.40 1.30 6 9 -7 4.70 1.70 6 9 -6 81.69 5.80 6 9 -5 82.29 5.50 6 9 -4 30.90 2.90 6 9 -3 30.00 2.60 6 9 -2 115.49 4.60 6 9 -2 110.09 5.80 6 9 -1 102.79 5.10 6 9 -1 101.19 4.20 6 9 0 9.50 1.10 6 9 0 8.80 0.60 6 9 1 117.79 5.30 6 9 1 115.09 4.80 6 9 2 144.79 6.20 6 9 2 144.59 5.90 6 9 3 40.20 2.00 6 9 4 49.20 2.40 6 9 5 128.39 5.60 6 9 6 127.29 5.60 6 9 7 8.50 1.10 7 9 -7 11.90 2.70 7 9 -6 11.60 2.10 7 9 -5 11.50 2.00 7 9 -4 58.69 4.20 7 9 -3 5.70 1.30 7 9 -3 6.40 0.60 7 9 -2 45.40 3.10 7 9 -2 44.80 2.10 7 9 -1 22.10 1.90 7 9 -1 23.60 1.20 7 9 0 234.28 9.60 7 9 0 251.57 10.40 7 9 1 26.50 1.30 7 9 1 25.10 1.70 7 9 2 55.69 2.60 7 9 3 7.80 0.70 7 9 4 86.49 3.90 7 9 5 20.70 1.50 7 9 6 17.90 1.40 7 9 7 17.50 1.40 8 9 -7 9.90 2.40 8 9 -5 22.20 2.60 8 9 -4 5.70 1.50 8 9 -3 48.10 2.20 8 9 -3 44.20 3.40 8 9 -2 6.00 1.20 8 9 -2 5.80 0.60 8 9 -1 35.40 2.60 8 9 -1 36.80 1.70 8 9 0 13.00 1.30 8 9 0 14.00 0.90 8 9 1 38.30 1.80 8 9 2 7.00 0.60 8 9 3 62.49 2.90 8 9 4 9.60 1.00 8 9 5 37.20 2.10 8 9 6 3.30 0.70 8 9 7 16.10 1.50 9 9 -7 1.00 1.30 9 9 -6 11.60 2.30 9 9 -5 6.30 1.70 9 9 -4 4.20 1.40 9 9 -3 12.00 0.90 9 9 -3 9.90 1.60 9 9 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16.90 1.20 13 9 0 54.79 2.70 13 9 1 15.50 1.10 13 9 2 0.30 0.30 13 9 3 25.20 1.60 13 9 4 12.10 1.10 13 9 5 17.90 1.60 14 9 -3 7.50 0.90 14 9 -2 3.00 0.60 14 9 -1 28.20 1.70 14 9 0 10.10 0.90 14 9 1 26.30 1.60 14 9 2 2.60 0.50 14 9 3 8.00 0.90 14 9 4 2.00 0.50 15 9 -3 5.40 0.80 15 9 -2 0.50 0.40 15 9 -1 7.90 0.90 15 9 0 2.00 0.50 15 9 1 7.20 0.90 15 9 2 0.50 0.40 15 9 3 3.50 0.70 16 9 -2 8.90 1.00 16 9 -1 13.80 1.20 16 9 0 1.00 0.50 16 9 1 13.00 1.20 15 -10 3 0.10 1.30 15 -10 2 -0.20 1.30 14 -10 4 3.80 2.40 14 -10 3 0.30 1.40 14 -10 2 0.70 1.40 14 -10 1 6.20 2.00 -14 10 4 5.30 1.70 13 -10 4 11.50 3.20 13 -10 3 8.70 2.60 13 -10 2 54.79 5.20 13 -10 1 0.60 1.20 13 -10 -1 1.00 0.70 -13 10 3 10.20 2.00 -13 10 4 15.70 2.50 -13 10 5 15.10 2.70 12 -10 5 35.20 5.10 12 -10 4 8.30 2.90 12 -10 3 6.30 2.40 12 -10 2 2.60 1.60 12 -10 1 3.10 1.50 12 -10 0 0.70 1.00 -12 10 2 2.30 1.00 -12 10 3 5.80 1.50 -12 10 4 5.80 1.70 -12 10 5 38.60 3.90 11 -10 5 20.00 3.80 11 -10 4 6.40 2.50 11 -10 3 10.10 2.80 11 -10 2 40.90 4.30 11 -10 1 75.89 5.50 11 -10 0 11.90 2.00 -11 10 0 12.20 1.80 -11 10 1 83.09 4.40 -11 10 2 49.00 3.30 -11 10 3 8.30 1.70 -11 10 4 6.40 1.80 -11 10 5 23.00 3.10 10 -10 6 11.00 3.40 10 -10 5 1.00 1.50 10 -10 4 7.50 2.60 10 -10 3 20.90 3.20 10 -10 2 33.80 3.80 10 -10 1 9.30 2.00 -10 10 -1 10.40 1.30 10 -10 0 51.29 3.90 -10 10 0 52.29 2.90 -10 10 1 11.30 1.30 -10 10 2 39.10 2.90 -10 10 3 25.80 2.60 -10 10 4 11.10 2.10 -10 10 5 0.60 1.20 -10 10 6 10.30 2.50 9 -10 6 0.90 1.60 9 -10 5 7.10 2.60 9 -10 4 7.10 2.30 9 -10 3 15.10 2.80 9 -10 2 19.60 2.80 -9 10 -2 17.90 2.20 9 -10 1 18.20 2.40 -9 10 -1 17.70 1.40 9 -10 0 111.89 6.40 -9 10 0 116.19 5.30 -9 10 1 19.70 1.70 -9 10 2 22.60 2.10 -9 10 3 17.00 2.10 -9 10 4 7.00 1.70 -9 10 5 8.70 2.10 -9 10 6 2.10 1.50 8 -10 7 2.40 2.00 8 -10 6 1.80 1.80 8 -10 5 12.40 3.00 8 -10 4 27.70 3.80 8 -10 3 73.19 5.70 8 -10 2 9.10 1.90 -8 10 -2 8.60 1.10 8 -10 1 153.18 8.10 -8 10 -1 143.69 6.50 8 -10 0 297.47 13.60 -8 10 0 303.17 12.40 -8 10 1 163.38 7.40 -8 10 2 10.50 1.50 -8 10 3 88.09 5.20 -8 10 4 31.80 3.10 -8 10 5 12.60 2.30 -8 10 6 2.70 1.50 -8 10 7 4.00 2.80 7 -10 7 11.80 3.30 7 -10 6 3.30 1.90 7 -10 5 24.10 3.60 7 -10 4 45.80 4.50 7 -10 3 41.60 3.90 -7 10 -3 35.80 2.60 7 -10 2 15.60 2.30 -7 10 -2 11.90 1.30 -7 10 -1 10.10 1.00 7 -10 0 61.69 4.10 -7 10 0 61.39 3.20 -7 10 1 11.40 1.30 -7 10 2 15.50 1.70 -7 10 3 51.29 3.60 -7 10 4 53.79 4.10 -7 10 5 25.40 3.00 -7 10 6 3.00 1.50 -7 10 7 14.50 2.80 6 -10 7 1.20 1.60 6 -10 6 3.40 1.90 6 -10 5 29.70 3.80 6 -10 4 318.07 14.70 -6 10 -4 249.88 12.40 6 -10 3 25.00 3.00 -6 10 -3 21.50 1.90 6 -10 2 101.99 6.00 -6 10 -2 88.59 4.60 6 -10 1 23.80 2.40 -6 10 -1 21.50 1.60 -6 10 0 561.74 22.30 -6 10 1 26.60 1.90 -6 10 2 112.29 5.60 -6 10 3 29.50 2.50 -6 10 4 370.86 16.50 -6 10 5 36.60 3.50 -6 10 6 4.50 1.80 -6 10 7 0.40 1.20 5 -10 7 2.90 1.90 5 -10 6 14.00 2.70 5 -10 5 124.69 7.80 -5 10 -5 98.89 6.10 5 -10 4 92.39 6.10 -5 10 -4 75.89 4.70 5 -10 3 55.49 4.20 -5 10 -3 45.60 3.10 5 -10 2 96.29 5.70 -5 10 -2 91.89 4.60 5 -10 1 11.10 1.60 -5 10 -1 9.60 1.00 -5 10 0 126.89 5.60 -5 10 1 12.20 1.20 -5 10 2 117.49 5.70 -5 10 3 62.99 3.90 -5 10 4 118.19 6.60 -5 10 5 153.68 8.40 -5 10 6 15.80 2.60 -5 10 7 3.70 1.60 4 -10 7 1.90 1.50 4 -10 6 36.80 4.00 -4 10 -6 32.30 3.20 4 -10 5 52.99 4.60 -4 10 -5 43.40 3.50 4 -10 4 50.69 4.10 -4 10 -4 39.00 3.10 4 -10 3 68.49 4.60 -4 10 -3 57.69 3.60 4 -10 2 5.40 1.40 -4 10 -2 4.70 0.90 4 -10 1 51.99 3.40 -4 10 -1 47.20 2.60 -4 10 0 47.80 2.50 -4 10 1 57.29 3.00 -4 10 2 6.30 1.00 -4 10 3 85.89 4.80 -4 10 4 59.79 4.10 -4 10 5 66.19 4.70 -4 10 6 47.60 4.00 -4 10 7 3.90 1.70 -4 10 8 21.00 3.00 3 -10 7 2.30 1.50 -3 10 -7 2.40 1.30 3 -10 6 57.39 4.80 -3 10 -6 46.70 4.00 3 -10 5 28.70 3.10 -3 10 -5 21.10 2.40 3 -10 4 32.60 3.10 -3 10 -4 26.50 2.50 3 -10 3 104.99 5.80 -3 10 -3 85.79 4.90 3 -10 2 353.56 14.50 -3 10 -2 298.57 13.50 -3 10 -1 47.10 2.60 -3 10 0 29.50 1.80 -3 10 1 53.89 2.80 -3 10 2 425.16 17.40 -3 10 3 132.29 6.50 -3 10 4 42.40 3.20 -3 10 5 34.70 3.10 -3 10 6 70.49 5.10 -3 10 7 2.80 1.40 -3 10 8 9.00 2.20 -2 10 -8 3.30 1.60 -2 10 -7 11.60 2.50 2 -10 6 9.50 2.00 -2 10 -6 7.40 1.80 2 -10 5 115.39 6.70 -2 10 -5 100.79 6.20 2 -10 4 3.70 1.20 -2 10 -4 4.70 1.20 2 -10 3 59.59 3.80 -2 10 -3 49.80 3.30 2 -10 2 27.50 2.30 -2 10 -2 23.80 1.90 -2 10 -1 66.89 3.40 -2 10 0 351.46 14.10 -2 10 1 77.09 3.70 -2 10 2 31.50 2.10 -2 10 3 80.39 4.40 -2 10 4 7.00 1.50 -2 10 5 158.78 8.20 -2 10 6 13.10 2.20 -2 10 7 20.90 2.80 -2 10 8 2.90 1.50 -1 10 -8 1.50 1.30 -1 10 -7 2.40 1.30 1 -10 6 27.80 2.90 -1 10 -6 26.90 3.00 1 -10 5 49.40 3.70 -1 10 -5 44.40 3.70 1 -10 4 5.10 1.20 -1 10 -4 4.30 1.20 1 -10 3 31.10 2.50 -1 10 -3 25.90 2.20 -1 10 -2 21.30 1.70 -1 10 -1 33.00 2.00 -1 10 0 6.00 0.70 -1 10 1 37.90 2.10 -1 10 2 31.90 2.00 -1 10 3 42.50 2.70 -1 10 4 6.60 1.30 -1 10 5 69.69 4.50 -1 10 6 37.80 3.40 -1 10 7 4.30 1.50 -1 10 8 1.40 1.20 0 10 -8 22.40 3.20 0 10 -7 0.60 1.00 0 10 -6 44.30 3.90 0 -10 5 0.20 0.60 0 10 -5 0.40 0.70 0 -10 4 0.20 0.60 0 10 -4 0.10 0.60 0 -10 3 0.20 0.50 0 10 -3 -0.20 0.40 0 10 -2 51.19 3.10 0 10 -1 0.00 0.10 0 10 -1 -0.20 0.30 0 10 0 241.88 9.90 0 10 0 236.38 9.30 0 10 1 -0.10 0.30 0 10 2 68.49 3.40 0 10 3 0.00 0.40 0 10 4 0.20 0.60 0 10 5 0.00 0.70 0 10 6 67.19 4.50 0 10 7 0.40 0.90 1 10 -8 2.10 1.40 1 10 -7 2.50 1.40 1 10 -6 25.70 3.00 -1 -10 5 49.50 3.30 1 10 -5 42.00 3.60 -1 -10 4 5.20 1.10 1 10 -4 4.80 1.30 1 10 -3 25.20 2.20 1 10 -2 22.00 1.80 1 10 -1 32.70 1.40 1 10 -1 31.60 2.10 1 10 0 5.50 0.40 1 10 0 5.60 0.70 1 10 1 38.10 2.00 1 10 1 35.60 1.70 1 10 2 30.90 1.80 1 10 3 37.60 2.30 1 10 4 6.60 1.20 1 10 5 68.39 4.20 1 10 6 39.90 3.30 1 10 7 4.30 1.40 2 10 -8 2.60 1.50 2 10 -7 13.10 2.50 2 10 -6 6.90 1.80 2 10 -5 95.59 6.00 2 10 -4 4.30 1.20 2 10 -3 47.40 3.30 2 10 -2 23.00 1.90 2 10 -1 58.99 2.40 2 10 0 307.27 12.80 2 10 0 319.17 12.20 2 10 1 73.69 3.40 2 10 1 69.39 3.00 2 10 2 30.90 1.50 2 10 2 30.20 1.80 2 10 3 67.79 3.40 2 10 3 67.49 3.00 2 10 4 5.50 1.00 2 10 5 159.68 7.60 2 10 6 10.90 1.70 2 10 8 2.70 0.70 3 10 -8 6.30 2.20 3 10 -7 1.40 1.20 3 10 -6 44.60 4.00 3 10 -5 22.90 2.70 3 10 -4 24.80 2.50 3 10 -3 82.99 4.80 3 10 -2 279.67 12.20 3 10 -1 38.80 1.70 3 10 -1 40.50 2.50 3 10 0 27.30 1.30 3 10 0 25.20 1.70 3 10 1 48.30 2.50 3 10 1 46.50 2.10 3 10 2 363.16 14.20 3 10 2 363.56 14.50 3 10 3 119.19 5.30 3 10 3 115.09 4.90 3 10 4 37.70 2.00 3 10 4 38.70 2.40 3 10 5 35.30 2.50 3 10 5 30.70 1.80 3 10 6 67.89 3.30 3 10 7 2.90 0.70 3 10 8 6.90 1.10 4 10 -7 0.70 1.00 4 10 -6 29.40 3.30 4 10 -5 38.70 3.50 4 10 -4 37.40 3.20 4 10 -3 52.09 3.60 4 10 -2 4.30 1.00 4 10 -1 36.90 1.70 4 10 -1 40.20 2.50 4 10 0 40.30 1.80 4 10 0 40.20 2.40 4 10 1 46.30 2.10 4 10 1 48.20 2.50 4 10 2 5.10 0.70 4 10 2 5.10 0.50 4 10 3 72.59 3.30 4 10 3 77.79 3.60 4 10 4 55.99 3.00 4 10 4 53.89 2.70 4 10 5 60.49 3.00 4 10 6 43.40 2.40 4 10 7 3.40 0.80 5 10 -7 2.40 1.40 5 10 -6 8.80 2.10 5 10 -5 89.29 5.80 5 10 -4 66.99 4.60 5 10 -3 39.40 3.10 5 10 -2 71.49 3.00 5 10 -2 72.49 4.20 5 10 -1 7.90 0.50 5 10 -1 8.10 1.10 5 10 0 92.29 3.80 5 10 0 94.89 4.60 5 10 1 9.40 0.70 5 10 1 9.10 1.00 5 10 2 100.39 4.20 5 10 2 95.59 4.40 5 10 3 57.79 2.80 5 10 3 55.09 2.60 5 10 4 97.89 4.30 5 10 5 139.99 6.00 5 10 6 15.10 1.30 5 10 7 3.10 0.70 6 10 -7 0.80 1.20 6 10 -6 2.20 1.20 6 10 -5 20.10 2.60 6 10 -4 221.88 10.80 6 10 -3 17.10 2.00 6 10 -2 68.79 3.00 6 10 -2 70.99 4.20 6 10 -1 16.90 1.60 6 10 -1 16.00 0.90 6 10 0 406.26 16.60 6 10 0 403.96 15.80 6 10 1 17.70 1.00 6 10 1 19.40 1.50 6 10 2 98.79 4.10 6 10 2 90.19 4.30 6 10 3 26.10 1.50 6 10 4 350.86 14.00 6 10 5 35.20 2.10 6 10 6 5.60 0.90 6 10 7 0.40 0.50 7 10 -7 8.70 2.30 7 10 -6 2.00 1.20 7 10 -5 15.20 2.20 7 10 -4 29.90 2.90 7 10 -3 28.70 2.60 7 10 -2 8.70 1.40 7 10 -2 10.90 0.70 7 10 -1 6.60 1.10 7 10 -1 6.30 0.60 7 10 0 40.80 2.60 7 10 0 40.70 1.90 7 10 1 7.60 0.60 7 10 1 8.10 1.00 7 10 2 12.60 0.90 7 10 3 42.40 2.20 7 10 4 48.00 2.50 7 10 5 25.40 1.70 7 10 6 3.50 0.70 7 10 7 13.90 1.40 8 10 -7 1.60 1.50 8 10 -6 1.60 1.20 8 10 -5 7.50 1.80 8 10 -4 18.40 2.30 8 10 -3 46.70 3.50 8 10 -2 6.60 0.60 8 10 -2 6.30 1.30 8 10 -1 103.29 4.20 8 10 -1 97.89 5.30 8 10 0 203.08 8.80 8 10 0 190.88 7.90 8 10 1 108.99 4.60 8 10 2 7.50 0.70 8 10 3 68.79 3.20 8 10 4 27.70 1.70 8 10 5 13.30 1.20 8 10 6 2.50 0.70 8 10 7 3.20 0.90 9 10 -6 1.50 1.20 9 10 -5 3.30 1.30 9 10 -4 4.40 1.40 9 10 -3 8.40 1.50 9 10 -2 11.10 1.60 9 10 -2 12.70 0.90 9 10 -1 11.70 0.80 9 10 -1 11.50 1.50 9 10 0 74.39 3.30 9 10 1 11.40 0.80 9 10 2 14.00 1.00 9 10 3 12.50 1.00 9 10 4 6.60 0.90 9 10 5 7.00 1.00 9 10 6 2.70 0.70 10 10 -6 6.10 1.90 10 10 -5 -0.10 0.80 10 10 -4 4.60 1.40 10 10 -3 12.20 1.80 10 10 -2 24.00 1.30 10 10 -2 20.60 2.20 10 10 -1 6.90 0.70 10 10 0 32.90 1.70 10 10 1 7.00 0.70 10 10 2 25.90 1.50 10 10 3 18.00 1.20 10 10 4 6.80 0.80 10 10 5 0.30 0.50 10 10 6 11.50 1.30 11 10 -6 9.40 2.20 11 10 -5 12.30 2.20 11 10 -4 3.30 1.20 11 10 -3 5.70 0.70 11 10 -3 5.10 1.40 11 10 -2 27.30 1.50 11 10 -1 50.09 2.40 11 10 0 8.80 0.80 11 10 1 48.80 2.40 11 10 2 27.10 1.50 11 10 3 7.00 0.80 11 10 4 4.40 0.70 11 10 5 19.00 1.40 12 10 -5 20.30 2.70 12 10 -4 3.30 1.30 12 10 -3 3.90 0.60 12 10 -2 1.10 0.40 12 10 -1 2.90 0.50 12 10 0 0.30 0.30 12 10 1 2.30 0.50 12 10 2 1.30 0.40 12 10 3 3.10 0.60 12 10 4 4.40 0.70 12 10 5 29.10 1.90 13 10 -5 8.60 2.20 13 10 -3 6.00 0.80 13 10 -2 34.40 1.90 13 10 -1 1.10 0.40 13 10 0 25.80 1.50 13 10 1 1.20 0.40 13 10 2 34.80 1.90 13 10 3 6.30 0.80 13 10 4 11.30 1.10 14 10 -3 0.80 0.40 14 10 -2 0.30 0.40 14 10 -1 4.90 0.70 14 10 0 11.00 1.00 14 10 1 3.90 0.60 14 10 2 0.90 0.40 14 10 3 0.80 0.40 15 10 -3 -0.30 0.30 15 10 -2 0.30 0.40 15 10 -1 5.80 0.80 15 10 0 0.00 0.30 15 10 1 5.30 0.70 15 10 2 0.20 0.40 16 10 -1 4.10 0.70 16 10 0 2.20 0.70 15 -11 2 1.00 1.50 14 -11 3 1.30 1.60 14 -11 2 8.90 2.50 14 -11 1 12.20 2.50 13 -11 4 3.60 2.30 13 -11 3 2.80 2.00 13 -11 2 23.70 3.50 13 -11 1 14.60 2.60 -13 11 3 3.90 1.40 -13 11 4 3.30 1.50 12 -11 4 14.10 3.20 12 -11 3 16.50 3.10 12 -11 2 1.50 1.40 12 -11 1 22.50 3.00 12 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8 -11 2 152.28 8.40 -8 11 -2 131.99 6.50 8 -11 1 110.09 6.50 -8 11 -1 106.39 5.10 -8 11 0 4.80 0.90 -8 11 1 124.09 5.90 -8 11 2 175.08 8.20 -8 11 3 15.90 2.00 -8 11 4 16.40 2.30 -8 11 5 45.50 4.10 -8 11 6 11.30 2.50 7 -11 7 1.70 1.70 7 -11 6 2.80 1.80 7 -11 5 1.50 1.40 7 -11 4 43.00 4.30 -7 11 -4 33.10 3.10 7 -11 3 47.30 4.20 -7 11 -3 40.70 2.90 7 -11 2 97.49 6.10 -7 11 -2 85.99 4.60 7 -11 1 154.08 8.00 -7 11 -1 143.39 6.60 -7 11 0 6.10 1.00 -7 11 1 171.58 7.70 -7 11 2 116.79 5.90 -7 11 3 59.59 4.00 -7 11 4 51.69 4.00 -7 11 5 2.20 1.30 -7 11 6 1.90 1.40 -7 11 7 2.50 2.50 6 -11 7 3.70 1.90 6 -11 6 19.50 3.40 6 -11 5 6.20 2.10 6 -11 4 116.99 7.30 -6 11 -4 87.99 5.40 6 -11 3 15.30 2.40 -6 11 -3 11.60 1.50 6 -11 2 297.37 13.40 -6 11 -2 261.87 11.80 6 -11 1 12.50 1.80 -6 11 -1 11.00 1.20 -6 11 0 890.71 35.70 -6 11 1 14.50 1.40 -6 11 2 360.46 15.20 -6 11 3 18.80 2.10 -6 11 4 137.59 7.40 -6 11 5 8.00 1.90 -6 11 6 27.30 3.30 -6 11 7 4.10 1.70 5 -11 7 14.20 3.00 5 -11 6 7.20 2.30 5 -11 5 7.20 2.10 -5 11 -5 6.10 1.50 5 -11 4 63.09 4.90 -5 11 -4 47.30 3.60 -5 11 -3 11.70 1.50 5 -11 2 25.60 2.60 -5 11 -2 22.30 1.90 5 -11 1 27.30 2.50 -5 11 -1 23.40 1.70 -5 11 0 11.40 1.10 -5 11 1 28.40 2.00 -5 11 2 32.10 2.40 -5 11 3 21.20 2.20 -5 11 4 80.29 5.00 -5 11 5 10.90 2.30 -5 11 6 8.00 2.00 -5 11 7 17.70 2.90 4 -11 7 19.60 3.20 4 -11 6 15.80 2.80 -4 11 -6 11.90 2.10 4 -11 5 33.10 3.50 -4 11 -5 29.50 2.90 4 -11 4 0.40 0.90 -4 11 -4 0.40 0.70 4 -11 3 9.70 1.70 -4 11 -3 6.90 1.20 4 -11 2 3.90 1.20 -4 11 -2 3.60 0.90 -4 11 -1 80.79 4.00 -4 11 0 8.20 0.90 -4 11 1 93.79 4.50 -4 11 2 4.80 1.00 -4 11 3 11.30 1.50 -4 11 4 0.90 1.00 -4 11 5 45.20 3.80 -4 11 6 18.80 2.70 -4 11 7 24.60 3.20 3 -11 7 0.20 1.00 -3 11 -7 -0.40 0.80 3 -11 6 51.89 4.50 -3 11 -6 45.80 4.00 3 -11 5 1.30 1.00 -3 11 -5 0.60 0.80 3 -11 4 65.89 4.50 -3 11 -4 51.49 3.80 3 -11 3 2.20 1.00 -3 11 -3 1.70 0.80 3 -11 2 159.28 7.50 -3 11 -2 128.69 6.60 -3 11 -1 9.00 1.00 -3 11 0 113.69 5.10 -3 11 1 11.90 1.10 -3 11 2 177.18 7.90 -3 11 3 3.80 1.10 -3 11 4 83.79 5.00 -3 11 5 1.80 1.20 -3 11 6 71.29 5.10 -3 11 7 0.60 1.10 -2 11 -8 3.80 1.70 -2 11 -7 2.40 1.30 2 -11 6 11.50 2.20 -2 11 -6 10.40 2.00 2 -11 5 154.98 8.10 -2 11 -5 126.79 7.50 2 -11 4 48.70 3.60 -2 11 -4 39.10 3.20 2 -11 3 39.70 3.00 -2 11 -3 31.50 2.60 -2 11 -2 7.20 1.00 -2 11 -1 231.58 9.80 -2 11 0 1.20 0.40 -2 11 1 276.27 11.40 -2 11 2 9.50 1.10 -2 11 3 52.69 3.30 -2 11 4 62.19 4.00 -2 11 5 214.88 10.40 -2 11 6 16.00 2.40 -2 11 7 4.90 1.70 -2 11 8 6.00 1.90 -1 11 -8 3.10 1.60 -1 11 -7 0.60 1.00 1 -11 6 0.60 0.90 -1 11 -6 0.40 0.90 1 -11 5 30.90 2.90 -1 11 -5 22.80 2.60 1 -11 4 2.70 1.10 -1 11 -4 1.90 0.90 1 -11 3 4.30 1.10 -1 11 -3 2.90 0.90 -1 11 -2 420.36 17.40 -1 11 -1 3.50 0.70 -1 11 0 55.39 2.90 -1 11 1 4.20 0.70 -1 11 2 592.24 23.60 -1 11 3 4.80 1.00 -1 11 4 3.50 1.10 -1 11 5 39.10 3.20 -1 11 6 0.80 1.00 -1 11 7 2.10 1.30 -1 11 8 4.30 1.70 0 11 -8 1.00 1.20 0 11 -7 -0.50 0.70 0 11 -6 35.70 3.50 0 -11 5 0.10 0.60 0 11 -5 0.20 0.70 0 -11 4 33.00 2.60 0 11 -4 26.70 2.60 0 11 -3 0.00 0.40 0 11 -2 146.19 6.90 0 11 -1 0.10 0.40 0 11 0 81.69 4.00 0 11 0 84.39 3.40 0 11 1 0.00 0.30 0 11 2 215.28 9.10 0 11 3 0.20 0.40 0 11 4 44.00 3.00 0 11 5 0.50 0.80 0 11 6 63.89 4.40 0 11 7 -0.60 0.90 1 11 -8 3.40 1.70 1 11 -7 0.70 1.00 1 11 -6 0.70 0.90 -1 -11 5 29.30 2.50 1 11 -5 24.60 2.80 1 11 -4 2.60 1.00 1 11 -3 3.50 1.00 1 11 -2 403.96 16.90 1 11 -1 4.00 0.80 1 11 0 54.39 2.90 1 11 0 54.19 2.30 1 11 1 3.80 0.60 1 11 1 3.80 0.40 1 11 2 552.64 21.90 1 11 2 551.64 21.50 1 11 3 4.40 0.90 1 11 4 3.50 1.00 1 11 5 39.80 3.00 1 11 6 0.40 0.90 1 11 7 2.60 1.90 2 11 -7 2.40 1.40 2 11 -6 8.40 2.00 2 11 -5 122.29 7.10 2 11 -4 33.40 3.00 2 11 -3 29.80 2.50 2 11 -2 6.70 1.10 2 11 -1 208.88 9.20 2 11 0 0.60 0.40 2 11 0 0.60 0.20 2 11 1 234.18 9.40 2 11 1 240.78 9.90 2 11 2 8.90 0.90 2 11 2 8.10 0.70 2 11 3 42.60 2.20 2 11 3 48.00 2.60 2 11 4 51.79 2.70 2 11 4 60.39 3.30 2 11 5 212.18 9.60 2 11 6 15.90 2.00 2 11 6 10.80 1.10 2 11 7 3.50 0.70 3 11 -7 0.50 1.00 3 11 -6 38.10 3.70 3 11 -5 0.50 0.70 3 11 -4 45.50 3.50 3 11 -3 1.60 0.80 3 11 -2 117.59 6.00 3 11 -1 8.00 0.50 3 11 -1 8.00 1.10 3 11 0 100.29 4.80 3 11 0 103.19 4.10 3 11 1 10.10 0.70 3 11 1 9.70 1.00 3 11 2 155.48 6.30 3 11 2 154.78 6.70 3 11 3 3.20 0.70 3 11 3 2.10 0.40 3 11 4 80.39 4.00 3 11 4 74.99 3.60 3 11 5 1.30 0.50 3 11 5 1.60 0.80 3 11 6 61.79 3.10 3 11 7 -0.30 0.40 4 11 -7 17.30 2.80 4 11 -6 10.80 2.10 4 11 -5 25.80 2.80 4 11 -4 0.20 0.70 4 11 -3 6.30 1.40 4 11 -2 3.00 0.90 4 11 -1 61.19 2.60 4 11 -1 65.89 3.60 4 11 0 6.90 0.50 4 11 0 7.30 1.00 4 11 1 77.69 3.80 4 11 1 79.59 3.30 4 11 2 4.30 0.50 4 11 2 4.00 0.70 4 11 3 9.70 0.90 4 11 3 10.70 1.10 4 11 4 0.80 0.50 4 11 4 0.60 0.40 4 11 5 37.60 2.10 4 11 6 17.50 1.40 4 11 7 23.60 1.70 5 11 -7 9.30 2.40 5 11 -6 5.50 1.80 5 11 -5 5.30 1.60 5 11 -4 44.50 3.60 5 11 -3 11.80 1.70 5 11 -2 19.00 1.90 5 11 -1 18.80 1.70 5 11 -1 18.80 1.00 5 11 0 9.30 0.70 5 11 0 9.80 1.20 5 11 1 22.60 1.20 5 11 1 22.50 1.70 5 11 2 27.40 1.40 5 11 2 25.70 1.70 5 11 3 17.30 1.30 5 11 3 17.90 1.20 5 11 4 66.69 3.20 5 11 5 8.30 1.00 5 11 6 9.10 1.00 5 11 7 14.90 1.30 6 11 -7 2.10 1.30 6 11 -6 13.00 2.40 6 11 -5 6.40 1.80 6 11 -4 73.79 4.90 6 11 -3 11.40 1.70 6 11 -2 206.98 9.70 6 11 -1 8.20 1.20 6 11 -1 9.30 0.60 6 11 0 647.94 25.50 6 11 0 617.54 24.40 6 11 1 9.60 0.70 6 11 1 10.70 1.20 6 11 2 287.37 11.20 6 11 2 275.97 11.70 6 11 3 14.80 1.10 6 11 4 120.89 5.30 6 11 5 9.40 1.10 6 11 6 23.40 1.70 6 11 7 4.30 0.90 7 11 -6 1.50 1.20 7 11 -5 0.50 0.90 7 11 -4 30.00 3.00 7 11 -3 32.50 2.90 7 11 -2 66.19 4.10 7 11 -1 102.79 5.40 7 11 -1 104.09 4.30 7 11 0 3.40 0.50 7 11 0 4.20 0.90 7 11 1 117.19 5.60 7 11 1 115.59 4.80 7 11 2 86.19 3.80 7 11 3 49.20 2.50 7 11 4 42.40 2.30 7 11 5 2.00 0.60 7 11 6 2.40 0.70 8 11 -6 4.60 1.70 8 11 -5 25.70 3.00 8 11 -4 8.10 1.60 8 11 -3 8.60 1.60 8 11 -2 101.79 4.30 8 11 -2 92.59 5.40 8 11 -1 73.19 4.30 8 11 -1 73.99 3.20 8 11 0 2.60 0.80 8 11 0 2.30 0.40 8 11 1 77.59 3.40 8 11 2 123.09 5.20 8 11 3 12.50 1.00 8 11 4 13.30 1.10 8 11 5 43.90 2.50 8 11 6 11.10 1.30 9 11 -6 2.00 1.30 9 11 -5 14.80 2.30 9 11 -4 3.40 1.30 9 11 -3 32.50 2.90 9 11 -2 5.40 0.60 9 11 -2 6.00 1.40 9 11 -1 46.70 2.20 9 11 -1 46.60 3.20 9 11 0 46.40 2.20 9 11 1 49.50 2.30 9 11 2 8.40 0.80 9 11 3 44.50 2.30 9 11 4 6.10 0.90 9 11 5 26.10 1.80 9 11 6 2.90 0.80 10 11 -6 4.70 1.70 10 11 -5 -0.20 0.80 10 11 -4 20.10 2.50 10 11 -3 4.60 1.30 10 11 -2 12.30 1.70 10 11 -2 13.00 0.90 10 11 -1 37.20 1.90 10 11 0 3.70 0.50 10 11 1 36.20 1.80 10 11 2 13.50 1.00 10 11 3 7.70 0.80 10 11 4 33.00 1.90 10 11 5 0.50 0.50 11 11 -5 2.40 1.30 11 11 -4 2.80 1.20 11 11 -3 4.40 1.30 11 11 -2 7.60 0.70 11 11 -1 0.40 0.30 11 11 0 7.00 0.70 11 11 1 0.20 0.30 11 11 2 7.10 0.70 11 11 3 4.10 0.70 11 11 4 3.80 0.70 11 11 5 3.60 0.70 12 11 -5 1.60 1.20 12 11 -4 7.30 1.80 12 11 -2 1.30 0.40 12 11 -1 13.40 1.00 12 11 0 14.40 1.00 12 11 1 15.10 1.10 12 11 2 1.30 0.50 12 11 3 11.10 1.00 12 11 4 9.40 1.00 13 11 -2 14.80 1.10 13 11 -1 9.50 0.90 13 11 0 14.70 1.10 13 11 1 10.80 0.90 13 11 2 15.80 1.20 13 11 3 1.40 0.50 13 11 4 2.30 0.70 14 11 -2 6.70 0.80 14 11 -1 6.80 0.80 14 11 0 5.10 0.70 14 11 1 8.50 0.90 14 11 2 6.40 0.80 14 11 3 1.80 0.60 15 11 -2 0.20 0.40 15 11 -1 14.90 1.20 15 11 0 16.90 1.20 15 11 1 14.80 1.20 14 -12 2 3.50 1.80 14 -12 1 13.00 2.70 13 -12 3 6.80 2.50 13 -12 2 24.40 3.60 13 -12 1 13.20 2.60 -13 12 3 6.80 1.70 -13 12 4 20.80 2.80 12 -12 4 11.60 3.30 12 -12 3 31.70 4.30 12 -12 2 21.30 3.30 12 -12 1 1.50 1.30 -12 12 1 1.90 0.90 -12 12 2 24.80 2.40 -12 12 3 32.20 3.00 -12 12 4 12.70 2.30 11 -12 4 31.40 4.50 11 -12 3 7.30 2.50 11 -12 2 3.80 1.70 11 -12 1 36.00 3.70 -11 12 0 47.20 2.90 -11 12 1 37.60 2.60 -11 12 2 6.30 1.40 -11 12 3 7.80 1.70 -11 12 4 35.70 3.50 -11 12 5 8.20 2.10 10 -12 5 21.10 3.90 10 -12 4 4.40 2.10 10 -12 3 9.80 2.60 10 -12 2 57.49 5.00 10 -12 1 67.39 5.00 -10 12 -1 57.69 3.40 -10 12 0 1.40 0.70 -10 12 1 71.89 4.00 -10 12 2 69.39 4.20 -10 12 3 11.70 1.90 -10 12 4 6.10 1.70 -10 12 5 23.80 3.10 9 -12 6 15.70 5.40 9 -12 5 7.40 2.50 9 -12 4 69.49 6.10 9 -12 3 19.40 3.20 9 -12 2 2.40 1.30 -9 12 -2 1.50 0.70 9 -12 1 63.39 4.70 -9 12 -1 59.89 3.40 -9 12 0 55.69 3.20 -9 12 1 73.49 4.00 -9 12 2 2.40 1.00 -9 12 3 21.40 2.40 -9 12 4 81.99 5.40 -9 12 5 10.30 2.30 8 -12 6 0.90 1.50 8 -12 5 52.49 5.50 8 -12 4 68.29 5.90 8 -12 3 83.89 6.00 -8 12 -3 65.09 4.20 8 -12 2 80.09 5.60 -8 12 -2 73.59 4.10 8 -12 1 179.38 9.10 -8 12 -1 160.78 7.50 -8 12 0 5.80 1.00 -8 12 1 185.58 8.30 -8 12 2 97.09 5.20 -8 12 3 104.39 5.90 -8 12 4 77.69 5.20 -8 12 5 61.29 4.70 -8 12 6 0.30 1.20 7 -12 6 5.80 2.40 7 -12 5 37.10 4.30 7 -12 4 5.20 1.90 -7 12 -4 3.80 1.20 7 -12 3 20.10 2.80 -7 12 -3 14.70 1.70 7 -12 2 23.60 2.90 -7 12 -2 18.90 1.80 7 -12 1 240.68 11.30 -7 12 -1 215.48 9.70 -7 12 0 3.40 0.80 -7 12 1 253.97 10.90 -7 12 2 27.80 2.30 -7 12 3 22.30 2.30 -7 12 4 7.50 1.80 -7 12 5 43.30 3.80 -7 12 6 5.60 1.90 6 -12 7 2.20 1.80 6 -12 6 14.90 3.10 6 -12 5 36.40 4.00 -6 12 -5 24.00 3.20 -6 12 -4 52.39 3.70 6 -12 3 19.50 2.70 -6 12 -3 14.30 1.70 6 -12 2 277.77 12.60 -6 12 -2 234.68 11.00 6 -12 1 177.98 8.80 -6 12 -1 159.68 7.50 -6 12 0 300.17 12.50 -6 12 1 196.38 8.60 -6 12 2 319.37 13.60 -6 12 3 25.60 2.50 -6 12 4 91.59 5.60 -6 12 5 42.80 3.80 -6 12 6 18.40 2.70 5 -12 7 8.60 2.50 5 -12 6 13.20 2.70 5 -12 5 3.70 1.60 -5 12 -5 3.90 1.30 5 -12 4 45.10 4.10 -5 12 -4 35.50 3.00 5 -12 3 60.59 4.40 -5 12 -3 49.40 3.40 5 -12 2 96.99 5.70 -5 12 -2 81.89 4.60 -5 12 -1 33.40 2.20 -5 12 0 0.60 0.50 -5 12 1 39.00 2.40 -5 12 2 119.29 5.90 -5 12 3 75.29 4.50 -5 12 4 59.59 4.20 -5 12 5 6.40 1.80 -5 12 6 18.10 2.70 -5 12 7 9.10 2.20 4 -12 7 2.30 1.50 -4 12 -6 7.40 1.80 4 -12 5 19.10 2.80 -4 12 -5 14.30 2.10 -4 12 -4 42.00 3.20 4 -12 3 73.29 4.70 -4 12 -3 54.69 3.70 4 -12 2 26.40 2.60 -4 12 -2 23.40 2.00 -4 12 -1 59.99 3.30 -4 12 0 30.60 2.00 -4 12 1 72.79 3.70 -4 12 2 33.70 2.30 -4 12 3 93.49 5.10 -4 12 4 78.69 4.90 -4 12 5 24.70 2.80 -4 12 6 13.90 2.30 -4 12 7 1.80 1.40 3 -12 7 1.50 1.40 -3 12 -7 1.00 1.20 3 -12 6 17.90 2.60 -3 12 -6 15.20 2.40 3 -12 5 0.40 0.90 -3 12 -5 0.40 0.80 3 -12 4 37.20 3.40 -3 12 -4 30.60 2.80 3 -12 3 6.90 1.60 -3 12 -3 5.00 1.20 -3 12 -2 89.19 4.70 -3 12 -1 45.90 2.70 -3 12 0 2.80 0.70 -3 12 1 57.99 3.10 -3 12 2 132.09 6.20 -3 12 3 9.30 1.50 -3 12 4 51.89 3.70 -3 12 5 0.20 1.00 -3 12 6 25.20 3.00 -3 12 7 2.50 1.50 -2 12 -7 1.70 1.20 2 -12 6 2.30 1.30 -2 12 -6 3.10 1.30 2 -12 5 13.20 2.10 -2 12 -5 9.00 1.90 2 -12 4 44.20 3.40 -2 12 -4 30.40 2.90 2 -12 3 29.90 2.60 -2 12 -3 21.90 2.10 -2 12 -2 70.29 3.90 -2 12 -1 59.99 3.30 -2 12 0 14.90 1.30 -2 12 1 73.69 3.70 -2 12 2 99.79 4.90 -2 12 3 34.30 2.50 -2 12 4 58.19 3.80 -2 12 5 17.20 2.20 -2 12 6 2.90 1.40 -2 12 7 1.80 1.40 -1 12 -7 1.30 1.20 1 -12 6 1.70 1.10 -1 12 -6 1.00 1.00 1 -12 5 26.20 2.70 -1 12 -5 20.60 2.50 1 -12 4 15.30 1.90 -1 12 -4 11.50 1.70 -1 12 -3 5.50 1.30 -1 12 -2 39.30 2.70 -1 12 -1 13.60 1.40 -1 12 0 10.60 1.10 -1 12 1 15.20 1.30 -1 12 2 56.39 3.10 -1 12 3 5.60 1.00 -1 12 4 19.40 2.00 -1 12 5 36.40 3.10 -1 12 6 1.80 1.20 -1 12 7 2.10 1.30 0 12 -7 0.20 0.90 0 12 -6 1.20 1.00 0 -12 5 0.20 0.70 0 12 -5 -0.10 0.60 0 12 -4 179.88 9.00 0 12 -3 0.00 0.50 0 12 -2 51.79 3.20 0 12 -1 0.00 0.40 0 12 0 47.80 2.70 0 12 1 -0.10 0.40 0 12 1 0.00 0.20 0 12 2 80.79 4.00 0 12 3 0.20 0.50 0 12 4 309.27 13.30 0 12 5 0.00 0.70 0 12 6 2.20 1.20 0 12 7 -0.10 1.00 1 12 -7 1.60 1.20 1 12 -6 0.40 0.90 1 12 -5 19.20 2.40 1 12 -4 10.80 1.70 1 12 -3 4.10 1.10 1 12 -2 38.00 2.70 1 12 -1 11.50 1.30 1 12 0 10.90 0.60 1 12 0 11.10 1.10 1 12 1 15.70 0.90 1 12 1 14.80 1.30 1 12 2 53.89 2.90 1 12 2 52.59 2.40 1 12 3 5.70 1.00 1 12 4 19.30 1.80 1 12 5 35.80 2.80 1 12 6 2.10 1.10 2 12 -7 0.60 1.10 2 12 -6 1.40 1.10 2 12 -5 10.40 1.90 2 12 -4 31.70 2.90 2 12 -3 20.00 2.10 2 12 -2 63.89 3.80 2 12 -1 55.39 3.30 2 12 0 12.50 1.20 2 12 0 13.10 0.70 2 12 1 65.69 3.30 2 12 1 65.39 2.80 2 12 2 91.89 3.90 2 12 2 90.79 4.30 2 12 3 29.50 1.70 2 12 3 32.20 2.10 2 12 4 54.89 3.10 2 12 4 45.00 2.50 2 12 5 13.30 1.20 2 12 5 17.70 1.80 2 12 6 1.70 0.60 2 12 6 1.30 1.40 2 12 7 1.60 0.50 3 12 -7 0.80 1.10 3 12 -6 12.20 2.30 3 12 -5 0.10 0.70 3 12 -4 28.90 2.80 3 12 -3 6.60 1.40 3 12 -2 78.89 4.50 3 12 -1 39.10 2.60 3 12 0 2.30 0.30 3 12 0 2.00 0.60 3 12 1 47.80 2.20 3 12 1 49.70 2.70 3 12 2 111.69 5.10 3 12 2 113.79 4.70 3 12 3 8.10 1.00 3 12 3 8.20 0.80 3 12 4 42.00 2.30 3 12 4 47.20 2.80 3 12 5 0.30 0.50 3 12 5 0.50 0.60 3 12 6 19.90 1.50 3 12 7 2.60 0.70 4 12 -7 0.90 1.20 4 12 -6 6.40 1.80 4 12 -5 12.50 2.10 4 12 -4 43.20 3.50 4 12 -3 48.10 3.50 4 12 -2 19.00 1.90 4 12 -1 47.50 3.00 4 12 0 26.30 2.00 4 12 0 25.10 1.30 4 12 1 56.99 2.60 4 12 1 58.99 3.20 4 12 2 27.10 1.50 4 12 2 27.70 1.80 4 12 3 76.99 3.50 4 12 3 78.19 3.80 4 12 4 65.49 3.20 4 12 4 69.59 3.60 4 12 5 21.50 1.50 4 12 6 12.00 1.20 4 12 7 2.40 0.70 5 12 -7 8.10 2.30 5 12 -6 11.40 2.50 5 12 -5 3.70 1.30 5 12 -4 33.40 3.10 5 12 -3 44.10 3.40 5 12 -2 69.19 4.20 5 12 -1 26.70 2.20 5 12 0 0.60 0.50 5 12 0 0.50 0.20 5 12 1 31.20 2.10 5 12 1 32.00 1.60 5 12 2 99.19 4.20 5 12 2 94.09 4.60 5 12 3 65.19 3.00 5 12 3 63.69 3.30 5 12 4 48.10 2.50 5 12 5 7.20 1.00 5 12 6 14.40 1.30 5 12 7 11.00 1.30 6 12 -6 10.10 2.40 6 12 -5 22.60 2.80 6 12 -4 48.50 3.90 6 12 -3 13.70 1.90 6 12 -2 188.18 9.00 6 12 -1 118.19 5.90 6 12 -1 110.69 4.70 6 12 0 212.38 9.40 6 12 0 208.08 8.40 6 12 1 143.09 5.90 6 12 1 143.29 6.60 6 12 2 263.77 10.30 6 12 2 250.97 10.90 6 12 3 20.00 1.30 6 12 4 76.29 3.60 6 12 5 40.50 2.30 6 12 6 15.30 1.40 7 12 -6 4.90 1.70 7 12 -5 23.90 2.80 7 12 -4 3.50 1.30 7 12 -3 12.10 1.90 7 12 -2 15.60 1.90 7 12 -1 145.79 6.00 7 12 -1 149.49 7.30 7 12 0 1.70 0.70 7 12 0 1.70 0.30 7 12 1 175.58 7.90 7 12 1 174.58 7.10 7 12 2 19.30 1.20 7 12 3 18.40 1.30 7 12 4 6.00 0.80 7 12 5 41.10 2.40 7 12 6 4.80 0.80 8 12 -6 0.50 1.00 8 12 -5 28.10 3.10 8 12 -4 40.50 3.60 8 12 -3 51.69 3.90 8 12 -2 52.49 3.70 8 12 -1 111.89 5.90 8 12 -1 108.39 4.60 8 12 0 4.40 1.00 8 12 0 3.60 0.50 8 12 1 121.69 5.10 8 12 2 63.49 2.90 8 12 3 74.59 3.50 8 12 4 64.69 3.20 8 12 5 48.00 2.60 8 12 6 2.00 0.70 9 12 -6 8.20 2.10 9 12 -5 3.30 1.40 9 12 -4 40.10 3.60 9 12 -3 11.20 1.80 9 12 -2 1.50 0.80 9 12 -1 41.10 2.00 9 12 -1 40.10 3.00 9 12 0 33.40 1.70 9 12 1 45.20 2.20 9 12 2 1.30 0.40 9 12 3 14.60 1.10 9 12 4 65.29 3.30 9 12 5 7.90 1.10 10 12 -5 11.10 2.10 10 12 -4 2.80 1.20 10 12 -3 7.90 1.70 10 12 -2 33.10 2.90 10 12 -1 40.20 2.00 10 12 0 0.50 0.30 10 12 1 42.00 2.10 10 12 2 39.40 2.00 10 12 3 8.80 0.90 10 12 4 4.00 0.80 10 12 5 18.90 1.50 11 12 -5 2.80 1.40 11 12 -4 18.20 2.40 11 12 -3 3.60 1.30 11 12 -1 21.20 1.30 11 12 0 27.30 1.50 11 12 1 22.30 1.40 11 12 2 3.30 0.60 11 12 3 4.90 0.70 11 12 4 21.80 1.60 12 12 -1 0.70 0.40 12 12 0 1.00 0.40 12 12 1 0.50 0.40 12 12 2 13.50 1.10 12 12 3 21.20 1.40 12 12 4 8.50 1.00 13 12 -1 7.30 0.80 13 12 0 1.30 0.40 13 12 1 7.90 0.80 13 12 2 14.90 1.20 13 12 3 4.10 0.70 14 12 -1 6.90 0.80 14 12 0 0.60 0.40 14 12 1 6.80 0.80 14 12 2 3.10 0.60 15 12 -1 11.70 1.00 15 12 0 0.50 0.40 14 -13 1 13.20 2.80 13 -13 3 -0.40 2.30 13 -13 2 14.00 3.00 13 -13 1 6.60 2.10 -13 13 3 0.60 1.10 12 -13 3 12.60 3.20 12 -13 2 1.10 1.40 12 -13 1 14.70 2.70 -12 13 1 15.40 1.70 -12 13 2 1.20 0.90 -12 13 3 13.20 2.10 -12 13 4 48.00 4.00 11 -13 4 4.60 2.30 11 -13 3 11.10 2.70 11 -13 2 10.30 2.40 11 -13 1 7.60 2.10 -11 13 0 10.90 1.40 -11 13 1 8.70 1.40 -11 13 2 15.00 1.90 -11 13 3 12.30 2.00 -11 13 4 4.30 1.60 10 -13 4 11.50 2.90 10 -13 3 25.90 3.70 10 -13 2 34.10 3.80 10 -13 1 2.10 1.30 -10 13 -1 1.30 0.70 -10 13 0 36.00 2.50 -10 13 1 1.60 0.80 -10 13 2 37.50 2.90 -10 13 3 28.50 2.70 -10 13 4 10.40 2.00 -10 13 5 2.10 1.40 9 -13 5 14.90 3.40 9 -13 4 34.90 4.40 9 -13 3 15.40 2.80 9 -13 2 13.60 2.60 -9 13 -2 13.30 1.60 9 -13 1 39.00 3.60 -9 13 -1 35.40 2.50 -9 13 0 0.00 0.50 -9 13 1 42.20 2.80 -9 13 2 14.60 1.70 -9 13 3 18.20 2.30 -9 13 4 40.50 3.60 -9 13 5 19.40 2.80 8 -13 5 0.60 1.40 8 -13 4 26.90 3.80 8 -13 3 120.59 7.50 -8 13 -3 88.09 5.40 8 -13 2 26.30 3.10 -8 13 -2 22.40 2.00 8 -13 1 49.00 4.00 -8 13 -1 42.40 2.80 -8 13 0 111.89 5.40 -8 13 1 53.89 3.30 -8 13 2 30.30 2.50 -8 13 3 145.49 7.50 -8 13 4 31.80 3.20 -8 13 5 1.20 1.20 7 -13 6 0.40 1.30 7 -13 5 0.30 1.40 -7 13 -4 23.00 2.40 7 -13 3 47.60 4.30 -7 13 -3 33.70 2.80 7 -13 2 6.60 1.90 -7 13 -2 4.30 1.00 -7 13 -1 5.40 1.00 -7 13 0 9.90 1.30 -7 13 1 5.80 1.10 -7 13 2 7.70 1.30 -7 13 3 54.99 3.80 -7 13 4 40.30 3.50 -7 13 5 -0.10 1.10 -7 13 6 0.40 1.10 6 -13 6 16.70 3.10 6 -13 5 7.00 2.20 -6 13 -5 3.50 1.40 -6 13 -4 14.80 1.90 6 -13 3 30.00 3.30 -6 13 -3 22.60 2.20 6 -13 2 263.67 11.90 -6 13 -2 205.18 10.20 -6 13 -1 40.60 2.60 -6 13 0 145.99 6.70 -6 13 1 50.99 3.10 -6 13 2 279.87 12.20 -6 13 3 37.80 3.00 -6 13 4 28.20 2.90 -6 13 5 8.10 1.90 -6 13 6 20.30 3.00 5 -13 7 2.10 1.70 5 -13 6 4.90 2.00 5 -13 5 6.00 2.10 -5 13 -5 4.80 1.50 -5 13 -4 12.10 1.80 5 -13 3 26.80 3.00 -5 13 -3 19.70 2.10 5 -13 2 172.98 8.50 -5 13 -2 139.09 7.30 -5 13 -1 229.48 10.00 -5 13 0 0.00 0.50 -5 13 1 274.97 11.70 -5 13 2 204.08 9.20 -5 13 3 35.70 2.90 -5 13 4 22.60 2.60 -5 13 5 8.30 1.90 -5 13 6 7.10 2.00 4 -13 7 10.30 2.70 4 -13 6 4.70 1.80 -4 13 -6 3.70 1.40 4 -13 5 2.20 1.30 -4 13 -5 2.50 1.20 4 -13 4 45.60 3.90 -4 13 -4 33.00 3.00 4 -13 3 79.09 5.00 -4 13 -3 57.49 4.00 -4 13 -2 120.49 6.00 -4 13 -1 96.89 4.90 -4 13 0 21.30 1.70 -4 13 1 119.19 5.60 -4 13 2 169.58 7.80 -4 13 3 105.49 5.60 -4 13 4 63.09 4.30 -4 13 5 3.90 1.50 -4 13 6 7.70 2.00 -4 13 7 13.60 2.80 -3 13 -7 4.50 1.70 3 -13 6 3.00 1.50 -3 13 -6 1.80 1.10 3 -13 5 1.90 1.20 -3 13 -5 1.70 1.00 3 -13 4 66.29 4.50 -3 13 -4 49.70 3.80 -3 13 -3 9.30 1.50 -3 13 -2 41.90 2.90 -3 13 -1 189.88 8.50 -3 13 0 12.50 1.30 -3 13 1 230.98 9.90 -3 13 2 60.49 3.50 -3 13 3 20.40 2.00 -3 13 4 87.49 5.20 -3 13 5 2.70 1.30 -3 13 6 4.60 1.60 -3 13 7 9.60 2.20 -2 13 -7 8.90 2.20 2 -13 6 0.50 1.00 -2 13 -6 0.40 0.90 2 -13 5 18.40 2.50 -2 13 -5 14.10 2.20 2 -13 4 28.00 2.80 -2 13 -4 21.30 2.40 -2 13 -3 1.20 0.80 -2 13 -2 45.90 3.00 -2 13 -1 183.08 8.20 -2 13 0 147.99 6.70 -2 13 1 216.68 9.30 -2 13 2 69.39 3.70 -2 13 3 1.80 0.80 -2 13 4 35.20 2.80 -2 13 5 24.00 2.60 -2 13 6 0.40 1.10 -2 13 7 14.70 2.50 -1 13 -7 3.60 1.60 1 -13 6 13.50 2.20 -1 13 -6 9.50 2.20 1 -13 5 7.60 1.60 -1 13 -5 5.60 1.50 -1 13 -4 11.40 1.80 -1 13 -3 11.10 1.60 -1 13 -2 117.19 5.90 -1 13 -1 219.18 9.60 -1 13 0 117.49 5.50 -1 13 1 264.17 11.10 -1 13 2 168.98 7.50 -1 13 3 21.80 1.90 -1 13 4 20.10 2.10 -1 13 5 12.30 1.90 -1 13 6 18.80 2.40 -1 13 7 5.60 1.70 0 13 -7 -0.30 0.90 0 13 -6 6.30 1.80 0 13 -5 -0.30 0.70 0 13 -4 45.60 3.60 0 13 -2 17.10 1.70 0 13 -1 -0.10 0.50 0 13 0 0.50 0.50 0 13 1 0.20 0.40 0 13 1 -0.30 0.20 0 13 2 28.90 2.00 0 13 3 0.40 0.60 0 13 4 84.29 4.70 0 13 5 -0.20 0.70 0 13 6 13.20 2.10 0 13 7 0.10 1.00 1 13 -7 3.80 1.60 1 13 -6 11.00 2.20 1 13 -5 6.40 1.70 1 13 -4 10.60 1.70 1 13 -3 12.10 1.70 1 13 -2 111.49 5.80 1 13 -1 207.08 9.30 1 13 0 111.29 5.30 1 13 1 247.58 10.60 1 13 1 256.47 10.00 1 13 2 161.78 7.20 1 13 2 160.88 6.60 1 13 3 18.80 1.60 1 13 3 16.20 1.20 1 13 4 19.30 1.80 1 13 5 11.20 1.60 1 13 6 18.80 2.20 2 13 -7 10.40 2.50 2 13 -6 0.20 0.90 2 13 -5 13.50 2.10 2 13 -4 19.80 2.30 2 13 -3 1.00 0.70 2 13 -2 42.90 3.00 2 13 -1 166.88 7.70 2 13 0 133.09 6.20 2 13 1 197.28 7.80 2 13 1 194.38 8.50 2 13 2 64.89 2.90 2 13 2 62.79 3.30 2 13 3 2.10 0.70 2 13 3 2.00 0.50 2 13 4 33.10 1.90 2 13 4 36.10 2.50 2 13 5 22.40 2.10 2 13 5 20.70 1.50 2 13 6 0.30 0.40 2 13 7 14.30 1.40 3 13 -7 4.30 1.80 3 13 -6 1.70 1.20 3 13 -5 1.40 1.00 3 13 -4 46.20 3.70 3 13 -3 10.50 1.60 3 13 -2 36.40 2.80 3 13 -1 162.58 7.60 3 13 0 12.10 1.40 3 13 1 196.38 8.70 3 13 1 205.18 8.00 3 13 2 51.99 2.40 3 13 2 50.09 2.80 3 13 3 17.80 1.50 3 13 3 17.70 1.20 3 13 4 79.79 4.20 3 13 4 81.09 3.70 3 13 5 2.10 0.60 3 13 6 2.20 0.70 3 13 7 8.40 1.30 4 13 -6 4.50 1.70 4 13 -5 1.70 1.10 4 13 -4 31.00 3.00 4 13 -3 54.49 3.80 4 13 -2 99.49 5.50 4 13 -1 75.79 4.30 4 13 0 16.00 1.60 4 13 0 16.30 0.90 4 13 1 94.09 3.90 4 13 1 92.39 4.70 4 13 2 144.49 5.80 4 13 2 136.49 6.30 4 13 3 83.49 4.20 4 13 3 84.09 3.80 4 13 4 53.29 3.20 4 13 4 50.19 2.60 4 13 5 3.20 0.70 4 13 6 6.50 1.00 5 13 -6 3.70 1.40 5 13 -5 4.00 1.50 5 13 -4 11.00 1.90 5 13 -3 16.60 2.10 5 13 -2 111.69 6.00 5 13 -1 190.88 8.90 5 13 0 0.00 0.50 5 13 0 0.00 0.20 5 13 1 225.88 9.00 5 13 1 226.18 9.90 5 13 2 158.68 7.20 5 13 2 160.28 6.60 5 13 3 29.50 1.70 5 13 3 25.70 1.90 5 13 4 19.90 1.40 5 13 5 6.80 0.90 5 13 6 7.10 1.10 6 13 -6 9.60 2.30 6 13 -5 4.10 1.50 6 13 -4 15.50 2.20 6 13 -3 20.70 2.30 6 13 -2 156.08 7.90 6 13 -1 33.00 2.60 6 13 0 106.99 5.40 6 13 0 100.39 4.30 6 13 1 36.10 2.50 6 13 1 36.80 1.80 6 13 2 223.78 8.90 6 13 2 216.18 9.60 6 13 3 30.10 1.70 6 13 4 23.90 1.60 6 13 5 7.00 1.00 6 13 6 16.50 1.50 7 13 -6 0.20 0.90 7 13 -5 1.00 1.00 7 13 -4 21.70 2.60 7 13 -3 26.70 2.70 7 13 -2 3.50 1.10 7 13 -1 3.10 1.00 7 13 0 6.40 0.60 7 13 0 7.10 1.20 7 13 1 3.30 0.90 7 13 1 3.40 0.50 7 13 2 4.40 0.60 7 13 3 41.00 2.20 7 13 4 33.50 2.00 7 13 5 0.30 0.50 7 13 6 0.20 0.60 8 13 -6 9.10 3.30 8 13 -5 0.60 1.00 8 13 -4 16.10 2.30 8 13 -3 70.59 4.80 8 13 -2 17.50 2.10 8 13 -1 31.00 2.60 8 13 0 64.39 3.00 8 13 0 71.59 4.10 8 13 1 34.00 1.70 8 13 2 20.10 1.30 8 13 3 105.59 4.70 8 13 4 25.60 1.70 8 13 5 0.90 0.60 9 13 -5 8.00 2.00 9 13 -4 19.20 2.50 9 13 -3 8.20 1.70 9 13 -2 8.20 1.50 9 13 -1 22.50 2.20 9 13 0 0.10 0.20 9 13 1 24.80 1.40 9 13 2 9.70 0.90 9 13 3 11.30 1.00 9 13 4 28.60 1.80 9 13 5 14.70 1.40 10 13 -5 1.50 1.20 10 13 -4 6.20 1.70 10 13 -3 15.00 2.10 10 13 -2 20.60 2.50 10 13 -1 0.90 0.50 10 13 0 23.10 1.30 10 13 1 0.80 0.30 10 13 2 22.60 1.40 10 13 3 19.50 1.40 10 13 4 7.60 1.00 10 13 5 1.80 0.70 11 13 -4 2.50 1.30 11 13 -1 5.30 0.70 11 13 0 5.20 0.60 11 13 1 5.10 0.70 11 13 2 8.10 0.80 11 13 3 7.10 0.90 11 13 4 3.10 0.70 12 13 -1 8.70 0.80 12 13 0 18.20 1.20 12 13 1 9.30 0.90 12 13 2 1.00 0.40 12 13 3 6.80 0.90 13 13 -1 3.20 0.60 13 13 0 4.70 0.70 13 13 1 3.20 0.60 13 13 2 9.80 1.00 14 13 -1 7.50 0.80 14 13 0 3.00 0.60 14 13 1 8.00 0.90 13 -14 2 23.40 3.60 13 -14 1 3.90 1.90 12 -14 3 5.80 3.60 12 -14 2 2.70 1.80 12 -14 1 29.80 3.50 -12 14 1 27.00 2.40 -12 14 2 3.50 1.20 -12 14 3 8.60 1.90 11 -14 3 8.30 2.50 11 -14 2 10.50 2.40 -11 14 0 6.20 1.20 -11 14 1 0.90 0.80 -11 14 2 10.70 1.70 -11 14 3 9.50 1.90 -11 14 4 3.20 1.70 10 -14 4 16.50 3.40 10 -14 3 3.00 1.80 10 -14 2 6.90 2.10 -10 14 -1 21.60 1.90 -10 14 0 19.90 1.90 -10 14 1 26.40 2.20 -10 14 2 7.90 1.50 -10 14 3 4.10 1.40 -10 14 4 19.60 2.70 9 -14 4 16.10 3.30 9 -14 3 7.80 2.30 9 -14 2 3.50 1.70 -9 14 -2 2.10 0.90 -9 14 -1 15.00 1.60 -9 14 0 34.40 2.50 -9 14 1 17.90 1.80 -9 14 2 3.10 1.10 -9 14 3 9.80 1.80 -9 14 4 17.50 2.50 8 -14 5 7.60 2.50 8 -14 4 24.30 3.50 -8 14 -3 48.80 3.40 8 -14 2 8.40 2.00 -8 14 -2 6.40 1.20 -8 14 -1 1.90 0.70 -8 14 0 0.10 0.50 -8 14 1 2.20 0.80 -8 14 2 7.70 1.50 -8 14 3 85.39 5.20 -8 14 4 31.10 3.10 -8 14 5 10.50 2.30 7 -14 5 3.10 1.90 7 -14 4 2.90 1.60 -7 14 -4 1.90 0.90 7 -14 3 28.60 3.30 -7 14 -3 22.00 2.20 7 -14 2 57.09 4.60 -7 14 -2 46.80 3.30 -7 14 -1 25.30 2.10 -7 14 0 11.50 1.40 -7 14 1 30.00 2.30 -7 14 2 67.19 4.10 -7 14 3 35.30 2.90 -7 14 4 3.30 1.30 -7 14 5 4.50 1.70 6 -14 6 5.50 2.30 6 -14 5 6.50 2.10 -6 14 -5 3.60 1.40 6 -14 4 28.70 3.50 -6 14 -4 19.90 2.30 6 -14 3 9.00 2.20 -6 14 -3 6.60 1.30 -6 14 -2 48.50 3.20 -6 14 -1 52.19 3.20 -6 14 0 11.10 1.40 -6 14 1 67.99 3.80 -6 14 2 65.69 3.90 -6 14 3 10.10 1.70 -6 14 4 37.50 3.30 -6 14 5 10.10 2.20 -6 14 6 7.40 2.40 5 -14 6 11.40 2.50 5 -14 5 30.50 3.50 -5 14 -5 22.70 2.70 -5 14 -4 32.60 2.90 5 -14 3 43.80 3.80 -5 14 -3 33.30 2.80 -5 14 -2 64.99 3.90 -5 14 -1 114.59 5.70 -5 14 0 338.47 14.20 -5 14 1 133.49 6.30 -5 14 2 92.39 4.90 -5 14 3 55.79 3.80 -5 14 4 65.89 4.40 -5 14 5 39.90 3.70 -5 14 6 13.50 2.60 -4 14 -6 7.30 1.90 4 -14 5 18.60 2.80 -4 14 -5 14.30 2.20 4 -14 4 21.80 2.70 -4 14 -4 15.40 2.10 -4 14 -3 49.80 3.50 -4 14 -2 80.89 4.60 -4 14 -1 43.50 2.80 -4 14 0 1.30 0.60 -4 14 1 55.69 3.30 -4 14 2 120.69 6.00 -4 14 3 90.29 5.10 -4 14 4 29.50 2.80 -4 14 5 28.20 3.00 -4 14 6 17.60 2.70 3 -14 6 0.60 1.10 -3 14 -6 0.40 0.90 3 -14 5 9.20 2.10 -3 14 -5 6.30 1.60 3 -14 4 5.80 1.60 -3 14 -4 4.50 1.30 -3 14 -3 31.40 2.70 -3 14 -2 36.10 2.70 -3 14 -1 23.90 2.00 -3 14 0 85.29 4.40 -3 14 1 30.00 2.10 -3 14 2 55.79 3.30 -3 14 3 55.69 3.60 -3 14 4 8.70 1.70 -3 14 5 13.30 2.20 -3 14 6 0.90 1.20 -2 14 -7 0.30 1.00 2 -14 6 10.00 2.10 -2 14 -6 8.20 2.00 2 -14 5 8.00 1.80 -2 14 -5 6.10 1.60 -2 14 -4 4.60 1.40 -2 14 -3 7.00 1.40 -2 14 -2 49.40 3.30 -2 14 -1 108.09 5.40 -2 14 0 6.20 1.00 -2 14 1 134.39 6.30 -2 14 2 78.29 4.20 -2 14 3 13.00 1.60 -2 14 4 7.60 1.60 -2 14 5 11.90 2.00 -2 14 6 12.40 2.20 -2 14 7 0.90 1.30 -1 14 -7 12.20 2.40 -1 14 -6 2.50 1.40 -1 14 -5 4.00 1.40 -1 14 -4 5.50 1.40 -1 14 -3 23.90 2.30 -1 14 -2 3.70 1.00 -1 14 -1 90.89 4.80 -1 14 0 118.39 5.70 -1 14 1 107.79 5.20 -1 14 2 5.30 1.00 -1 14 3 38.40 2.70 -1 14 4 10.40 1.60 -1 14 5 5.90 1.40 -1 14 6 4.60 1.50 -1 14 7 21.70 2.90 0 14 -7 0.00 1.00 0 14 -6 15.30 2.50 0 14 -5 0.00 0.70 0 14 -4 2.30 1.00 0 14 -3 -0.20 0.40 0 14 -2 83.89 4.70 0 14 -1 -0.20 0.50 0 14 0 218.08 9.60 0 14 1 0.00 0.50 0 14 2 121.69 5.20 0 14 2 124.79 5.80 0 14 3 -0.20 0.50 0 14 4 5.20 1.20 0 14 5 0.20 0.80 0 14 6 32.30 3.10 0 14 7 0.00 1.10 1 14 -6 2.80 1.40 1 14 -5 2.50 1.20 1 14 -4 4.90 1.40 1 14 -3 22.80 2.30 1 14 -2 3.70 1.00 1 14 -1 83.99 4.60 1 14 0 117.49 5.70 1 14 1 105.69 5.10 1 14 2 4.50 0.60 1 14 2 5.20 0.90 1 14 3 36.30 2.00 1 14 3 39.10 2.50 1 14 4 7.50 0.90 1 14 4 9.20 1.40 1 14 5 5.80 1.30 1 14 5 4.50 0.80 1 14 6 4.60 1.30 1 14 6 3.50 0.70 2 14 -6 6.20 1.80 2 14 -5 4.80 1.50 2 14 -4 2.90 1.20 2 14 -3 8.10 1.50 2 14 -2 46.60 3.20 2 14 -1 90.39 4.80 2 14 0 6.90 1.10 2 14 1 111.99 5.50 2 14 1 119.29 4.80 2 14 2 65.79 3.60 2 14 2 66.69 3.00 2 14 3 11.70 1.30 2 14 3 13.20 1.00 2 14 4 7.00 1.20 2 14 4 5.10 0.80 2 14 5 8.90 1.00 2 14 5 10.10 1.50 2 14 6 12.40 1.20 3 14 -6 0.50 0.90 3 14 -5 7.10 1.80 3 14 -4 4.60 1.40 3 14 -3 26.90 2.60 3 14 -2 33.60 2.70 3 14 -1 21.30 2.00 3 14 0 75.69 4.20 3 14 1 26.00 2.00 3 14 1 26.70 1.40 3 14 2 47.10 2.30 3 14 2 45.50 2.80 3 14 3 44.10 2.30 3 14 3 45.30 2.70 3 14 4 6.60 0.90 3 14 4 7.30 1.20 3 14 5 11.50 1.20 3 14 6 0.20 0.50 4 14 -6 9.80 2.30 4 14 -5 11.80 2.10 4 14 -4 14.40 2.10 4 14 -3 46.00 3.50 4 14 -2 64.79 4.10 4 14 -1 37.10 2.80 4 14 0 0.60 0.60 4 14 1 46.70 2.20 4 14 1 45.20 2.90 4 14 2 100.69 4.20 4 14 2 92.89 4.80 4 14 3 76.09 3.50 4 14 3 74.39 4.00 4 14 4 24.20 1.60 4 14 5 19.90 1.50 4 14 6 16.10 1.50 5 14 -6 7.00 2.00 5 14 -5 19.10 2.60 5 14 -4 31.00 3.10 5 14 -3 27.90 2.70 5 14 -2 53.59 3.70 5 14 -1 84.89 4.80 5 14 0 251.47 11.10 5 14 1 107.29 4.40 5 14 1 102.79 5.30 5 14 2 73.29 4.00 5 14 2 74.19 3.30 5 14 3 45.80 2.40 5 14 4 54.69 2.80 5 14 5 30.30 2.00 5 14 6 13.90 1.40 6 14 -6 3.40 1.80 6 14 -5 4.90 1.70 6 14 -4 17.70 2.40 6 14 -3 4.90 1.40 6 14 -2 36.20 3.00 6 14 -1 37.10 2.90 6 14 0 8.10 1.30 6 14 1 45.70 3.00 6 14 1 45.90 2.20 6 14 2 49.50 2.40 6 14 2 50.09 4.30 6 14 3 8.50 0.90 6 14 4 30.30 1.90 6 14 5 8.90 1.20 6 14 6 5.90 1.10 7 14 -5 2.40 1.20 7 14 -4 2.30 1.20 7 14 -3 16.10 2.10 7 14 -2 32.70 2.90 7 14 -1 15.80 1.90 7 14 0 7.70 1.30 7 14 1 18.40 2.10 7 14 1 20.30 1.20 7 14 2 48.20 2.40 7 14 3 27.00 1.70 7 14 4 3.70 0.70 7 14 5 4.30 0.90 8 14 -5 5.80 1.80 8 14 -4 16.10 2.40 8 14 -3 39.80 3.40 8 14 -2 4.20 1.20 8 14 -1 1.90 0.90 8 14 0 0.20 0.20 8 14 0 0.20 0.60 8 14 1 1.70 0.40 8 14 2 5.10 0.70 8 14 3 60.69 3.00 8 14 4 21.60 1.60 8 14 5 10.00 1.30 9 14 -5 1.10 1.10 9 14 -4 9.40 1.90 9 14 -3 4.50 1.40 9 14 -2 1.00 0.80 9 14 0 20.50 1.20 9 14 1 10.70 0.90 9 14 2 1.70 0.50 9 14 3 6.70 0.90 9 14 4 13.40 1.20 9 14 5 1.90 1.00 10 14 -4 7.80 1.80 10 14 -3 1.60 1.00 10 14 0 10.90 0.90 10 14 1 14.40 1.00 10 14 2 4.50 0.70 10 14 3 2.60 0.60 10 14 4 13.20 1.30 11 14 -4 1.60 1.10 11 14 0 3.00 0.50 11 14 1 0.50 0.30 11 14 2 7.10 0.80 11 14 3 5.80 0.80 12 14 0 6.20 0.70 12 14 1 14.80 1.10 12 14 2 1.40 0.50 12 14 3 3.90 0.70 13 14 0 0.30 0.30 13 14 1 2.00 0.50 13 14 2 14.00 1.20 12 -15 2 18.60 3.70 -12 15 1 9.90 1.60 -12 15 2 21.60 2.30 11 -15 2 14.20 2.90 -11 15 0 9.80 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29.40 2.20 -2 15 1 48.60 3.00 -2 15 2 36.50 2.50 -2 15 3 13.20 1.70 -2 15 4 6.00 1.50 -2 15 5 42.70 3.50 -2 15 6 11.00 2.20 -1 15 -6 22.00 2.90 -1 15 -5 9.90 1.90 -1 15 -4 11.20 1.80 -1 15 -3 14.50 1.90 -1 15 -2 12.50 1.60 -1 15 -1 34.10 2.50 -1 15 0 6.10 1.00 -1 15 1 43.30 2.70 -1 15 2 17.40 1.70 -1 15 3 28.50 2.30 -1 15 4 19.10 2.10 -1 15 5 20.10 2.30 -1 15 6 47.40 3.80 0 15 -6 2.70 1.40 0 15 -5 0.20 0.80 0 15 -4 31.30 3.00 0 15 -3 -0.10 0.50 0 15 -2 97.69 5.40 0 15 -1 -0.30 0.40 0 15 0 29.00 2.20 0 15 1 0.10 0.50 0 15 2 148.19 6.90 0 15 2 149.39 6.20 0 15 3 -0.20 0.60 0 15 3 -0.20 0.30 0 15 4 59.69 3.80 0 15 5 0.10 0.80 0 15 6 5.20 1.50 1 15 -6 22.60 3.00 1 15 -5 9.70 2.00 1 15 -4 10.10 1.80 1 15 -3 15.10 1.90 1 15 -2 10.30 1.50 1 15 -1 34.00 2.60 1 15 0 5.90 1.10 1 15 1 40.00 2.60 1 15 2 16.50 1.60 1 15 2 15.90 1.10 1 15 3 22.30 1.50 1 15 3 24.50 2.00 1 15 4 20.30 2.00 1 15 4 18.10 1.40 1 15 5 14.00 1.30 1 15 5 19.70 2.10 1 15 6 45.10 3.40 1 15 6 34.90 2.30 2 15 -6 5.60 1.90 2 15 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16 -1 -0.10 0.50 0 16 0 1.40 0.70 0 16 1 0.00 0.40 0 16 2 27.30 2.20 0 16 3 -0.10 0.30 0 16 3 -0.40 0.60 0 16 4 34.20 2.10 0 16 4 40.60 3.00 0 16 5 -0.30 0.90 0 16 5 -0.30 0.40 0 16 6 98.29 5.60 0 16 6 71.99 4.30 1 16 -5 22.10 2.80 1 16 -4 1.80 1.00 1 16 -3 5.70 1.50 1 16 -2 21.30 2.20 1 16 -1 11.10 1.50 1 16 0 5.10 1.10 1 16 1 14.70 1.60 1 16 2 31.90 2.40 1 16 3 8.20 1.30 1 16 3 7.10 0.90 1 16 4 1.60 0.60 1 16 4 2.60 1.00 1 16 5 46.20 3.30 1 16 5 40.20 2.40 1 16 6 50.79 4.20 1 16 6 37.00 3.20 2 16 -5 11.70 2.20 2 16 -4 1.40 1.00 2 16 -3 5.50 1.50 2 16 -2 6.50 1.30 2 16 -1 8.40 1.40 2 16 0 24.70 2.10 2 16 1 9.60 1.30 2 16 2 10.40 1.40 2 16 3 8.70 1.30 2 16 3 8.00 0.90 2 16 4 1.70 0.90 2 16 4 1.60 0.60 2 16 5 21.60 1.70 2 16 5 24.00 2.40 3 16 -5 7.00 1.80 3 16 -4 2.90 1.30 3 16 -3 4.80 1.40 3 16 -2 27.80 2.60 3 16 -1 6.80 1.30 3 16 0 4.10 1.00 3 16 1 8.90 1.30 3 16 2 39.60 2.70 3 16 3 9.30 0.90 3 16 3 8.70 1.30 3 16 4 3.40 0.70 3 16 4 3.70 1.10 3 16 5 12.80 1.30 4 16 -5 4.80 1.70 4 16 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22.70 2.10 1 17 4 12.00 1.20 1 17 4 16.10 1.90 1 17 5 1.40 1.10 1 17 5 1.20 0.60 2 17 -5 1.30 1.70 2 17 -4 5.00 1.50 2 17 -3 2.70 1.10 2 17 -2 10.00 1.60 2 17 -1 6.20 1.20 2 17 0 2.20 0.90 2 17 1 7.00 1.30 2 17 2 14.20 1.70 2 17 3 4.30 1.10 2 17 4 11.90 1.70 2 17 4 10.70 1.10 2 17 5 1.00 0.60 2 17 5 1.80 1.50 3 17 -4 24.70 2.80 3 17 -3 3.90 1.30 3 17 -2 23.80 2.40 3 17 -1 0.90 0.70 3 17 0 9.10 1.40 3 17 1 1.50 0.80 3 17 2 34.40 2.60 3 17 3 5.40 0.80 3 17 3 5.80 1.20 3 17 4 47.00 3.20 3 17 4 45.20 2.50 3 17 5 7.50 1.10 4 17 -4 20.20 2.60 4 17 -3 27.50 2.80 4 17 -2 12.60 1.80 4 17 -1 0.40 0.60 4 17 0 2.90 1.00 4 17 1 0.30 0.60 4 17 2 16.40 1.90 4 17 3 45.00 2.40 4 17 3 42.90 3.10 4 17 4 38.60 2.30 4 17 5 2.00 0.70 5 17 -4 6.30 1.70 5 17 -3 10.90 1.90 5 17 -2 14.80 2.00 5 17 -1 4.50 1.20 5 17 0 1.20 0.80 5 17 1 4.70 1.20 5 17 2 22.10 2.20 5 17 3 13.50 1.20 5 17 4 14.10 1.30 6 17 -4 6.80 1.90 6 17 -3 1.50 1.10 6 17 -2 8.00 1.60 6 17 -1 -0.10 0.50 6 17 0 6.40 1.40 6 17 1 0.50 0.60 6 17 3 1.90 0.60 6 17 4 11.00 1.20 7 17 -3 0.70 0.90 7 17 -2 7.20 1.60 7 17 -1 12.90 1.90 7 17 0 11.90 1.80 7 17 3 0.70 0.50 7 17 4 25.70 1.90 8 17 -3 22.50 2.80 8 17 -2 0.70 0.80 8 17 -1 2.60 1.10 8 17 3 34.40 2.00 9 17 -2 2.70 1.20 -9 18 -1 15.50 2.10 -9 18 0 5.80 1.40 -8 18 -2 9.90 1.80 -8 18 -1 14.10 2.00 -8 18 0 9.30 1.70 -8 18 1 18.90 2.20 -7 18 -3 22.10 2.50 -7 18 -2 17.00 2.20 -7 18 -1 5.50 1.40 -7 18 0 0.30 0.70 -7 18 1 6.40 1.50 -7 18 2 21.50 2.40 -6 18 -3 5.60 1.50 -6 18 -2 2.30 1.10 -6 18 -1 2.70 1.00 -6 18 0 45.80 3.40 -6 18 1 2.20 1.00 -6 18 2 3.20 1.20 -6 18 3 9.70 2.90 -5 18 -4 18.20 2.40 -5 18 -3 4.90 1.40 -5 18 -2 4.40 1.30 -5 18 -1 6.40 1.50 -5 18 0 8.30 1.50 -5 18 1 8.80 1.60 -5 18 2 7.80 1.50 -5 18 3 8.00 1.70 -4 18 -4 17.10 2.40 -4 18 -3 2.90 1.20 -4 18 -2 10.90 1.80 -4 18 -1 8.60 1.60 -4 18 0 10.70 1.60 -4 18 1 10.20 1.60 -4 18 2 16.00 2.00 -4 18 3 4.50 1.50 -3 18 -4 17.00 2.40 -3 18 -3 2.60 1.10 -3 18 -2 13.00 1.90 -3 18 -1 0.30 0.70 -3 18 0 2.20 0.90 -3 18 1 0.20 0.70 -3 18 2 19.40 2.10 -3 18 3 4.20 1.30 -3 18 4 34.20 3.20 -2 18 -4 13.00 2.10 -2 18 -3 21.80 2.50 -2 18 -2 6.50 1.50 -2 18 -1 8.80 1.60 -2 18 0 0.40 0.70 -2 18 1 12.60 1.70 -2 18 2 11.40 1.70 -2 18 3 40.20 3.20 -2 18 4 26.90 2.80 -1 18 -4 1.30 1.00 -1 18 -3 0.60 0.80 -1 18 -2 1.30 0.90 -1 18 -1 5.10 1.30 -1 18 0 7.10 1.30 -1 18 1 7.00 1.40 -1 18 2 1.50 0.90 -1 18 3 0.80 0.90 -1 18 4 0.60 1.00 0 18 -4 10.40 2.00 0 18 -3 0.20 0.70 0 18 -2 0.90 0.80 0 18 -1 0.60 0.70 0 18 0 10.90 1.60 0 18 1 0.10 0.60 0 18 2 1.00 0.80 0 18 3 0.00 0.70 0 18 4 20.70 2.30 1 18 -4 0.50 0.80 1 18 -3 0.40 0.80 1 18 -2 1.10 0.80 1 18 -1 5.90 1.40 1 18 0 7.00 1.40 1 18 1 5.20 1.20 1 18 2 1.90 0.90 1 18 3 1.00 0.80 1 18 4 0.60 0.80 2 18 -4 11.10 2.10 2 18 -3 19.40 2.40 2 18 -2 5.80 1.40 2 18 -1 8.90 1.50 2 18 0 0.00 0.60 2 18 1 10.50 1.60 2 18 2 9.10 1.50 2 18 3 36.50 2.90 2 18 4 23.90 2.40 2 18 4 18.80 1.50 3 18 -4 14.70 2.70 3 18 -3 2.50 1.10 3 18 -2 10.80 1.70 3 18 -1 0.00 0.50 3 18 0 1.90 0.90 3 18 1 0.40 0.70 3 18 2 16.40 1.90 3 18 3 3.80 1.10 3 18 4 27.70 1.90 4 18 -3 1.90 1.00 4 18 -2 8.70 1.70 4 18 -1 5.90 1.40 4 18 0 9.20 1.50 4 18 1 8.00 1.50 4 18 2 12.60 1.70 4 18 3 3.20 1.20 4 18 4 29.50 2.00 5 18 -3 4.00 1.40 5 18 -2 4.80 1.40 5 18 -1 4.40 1.30 5 18 0 5.20 1.30 5 18 1 5.40 1.30 5 18 2 7.80 1.50 5 18 4 28.60 2.00 6 18 -3 4.60 1.50 6 18 -2 1.70 1.00 6 18 -1 1.50 0.90 6 18 0 30.70 2.80 6 18 1 1.80 0.90 7 18 -3 18.20 2.50 7 18 -2 11.70 2.00 7 18 -1 4.10 1.30 7 18 0 0.20 0.60 8 18 -2 6.70 1.70 8 18 -1 11.10 2.10 -7 19 -1 11.20 2.10 -7 19 0 11.90 3.00 -6 19 -2 5.50 1.50 -6 19 -1 7.40 1.60 -6 19 0 114.49 6.40 -6 19 1 7.80 1.80 -5 19 -2 6.10 1.50 -5 19 -1 2.70 1.10 -5 19 0 4.00 1.30 -5 19 1 3.60 1.20 -5 19 2 11.10 2.90 -4 19 -3 3.40 2.00 -4 19 -2 4.00 1.30 -4 19 -1 20.80 2.30 -4 19 0 10.90 1.80 -4 19 1 24.90 2.50 -4 19 2 5.20 1.40 -3 19 -3 0.80 1.00 -3 19 -2 3.60 1.30 -3 19 -1 1.90 1.00 -3 19 0 2.20 1.00 -3 19 1 2.30 1.00 -3 19 2 4.20 1.30 -3 19 3 1.10 1.70 -2 19 -3 16.40 2.30 -2 19 -2 8.60 1.70 -2 19 -1 25.90 2.60 -2 19 0 3.80 1.20 -2 19 1 31.90 2.80 -2 19 2 12.80 1.80 -2 19 3 35.40 3.10 -1 19 -3 1.20 1.00 -1 19 -2 1.00 0.90 -1 19 -1 15.60 2.10 -1 19 0 30.60 2.70 -1 19 1 18.90 2.10 -1 19 2 0.80 0.80 -1 19 3 2.40 1.10 0 19 -3 -0.20 0.60 0 19 -2 13.30 1.90 0 19 -1 0.00 0.60 0 19 0 14.80 2.00 0 19 1 0.60 0.80 0 19 2 18.90 2.20 0 19 3 0.00 0.80 1 19 -3 0.90 0.90 1 19 -2 0.40 0.80 1 19 -1 14.20 2.00 1 19 0 29.40 2.70 1 19 1 15.50 2.00 1 19 2 1.10 0.90 1 19 3 2.40 1.10 2 19 -3 17.40 2.60 2 19 -2 7.70 1.50 2 19 -1 22.80 2.50 2 19 0 3.00 1.10 2 19 1 30.20 2.70 2 19 2 12.80 1.80 2 19 3 28.30 2.60 3 19 -2 2.80 1.10 3 19 -1 1.50 0.90 3 19 0 1.60 0.90 3 19 1 2.00 1.00 3 19 2 4.90 1.40 3 19 3 1.20 0.90 4 19 -2 2.00 1.10 4 19 -1 16.50 2.10 4 19 0 10.40 1.70 4 19 1 22.20 2.30 4 19 2 4.80 1.40 5 19 -2 5.20 1.50 5 19 -1 1.90 1.00 5 19 0 2.90 1.20 5 19 1 2.50 1.00 6 19 -2 4.20 1.40 6 19 -1 5.70 1.50 6 19 0 79.39 5.10 7 19 -1 9.30 1.80 -3 20 0 29.70 4.20 -2 20 -1 40.00 4.30 -2 20 0 4.50 1.30 -2 20 1 48.70 4.10 -1 20 -1 1.20 0.90 -1 20 0 39.60 3.30 -1 20 1 2.10 1.10 0 20 -1 -0.20 0.70 0 20 0 24.50 2.60 0 20 1 0.40 0.80 0 20 2 30.10 3.20 1 20 -1 1.50 1.00 1 20 0 35.00 3.10 1 20 1 1.50 1.00 1 20 2 12.40 1.90 2 20 -1 34.90 3.20 2 20 0 3.60 1.30 2 20 1 43.60 3.50 2 20 2 3.60 1.20 3 20 -1 4.50 1.40 3 20 0 27.10 2.70 3 20 1 5.80 1.50 3 20 2 7.30 1.70 4 20 -1 8.40 2.00 4 20 0 25.70 2.70 4 20 1 9.80 1.70 5 20 0 -0.20 0.70 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 9447 _shelx_res_file ; TITL m3cg CELL 0.71073 14.2762 15.9821 7.3753 90.000 90.000 90.000 ZERR 4.000 0.0009 0.0010 0.0005 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, 1/2+Z SYMM 1/2+X, -Y, Z SYMM 1/2-X, Y, 1/2+Z SFAC C N O F H UNIT 76 8 12 8 72 OMIT -2 180.0 L.S. 20 ACTA BOND $H CONF HTAB FMAP 2 PLAN 20 SIZE 0.910 0.352 0.168 TEMP -100 WGHT 0.096000 FVAR 0.51353 N1 2 0.360510 0.627271 0.301714 11.00000 0.03077 0.02270 = 0.02135 0.00229 -0.00050 -0.00153 C2 1 0.385551 0.711071 0.236882 11.00000 0.03561 0.02963 = 0.02540 0.00898 -0.00293 -0.00410 AFIX 23 H2A 5 0.359698 0.719747 0.113754 11.00000 -1.20000 H2B 5 0.454559 0.716266 0.229906 11.00000 -1.20000 AFIX 0 C3 1 0.346990 0.776821 0.364138 11.00000 0.03986 0.02141 = 0.02933 0.00684 -0.00882 -0.00248 AFIX 23 H3A 5 0.368636 0.832813 0.324883 11.00000 -1.20000 H3B 5 0.277698 0.776204 0.358977 11.00000 -1.20000 AFIX 0 N4 2 0.377658 0.761464 0.550901 11.00000 0.03474 0.01729 = 0.02738 0.00523 -0.00388 -0.00149 C5 1 0.365802 0.675129 0.613762 11.00000 0.03278 0.01693 = 0.02429 0.00291 -0.00021 -0.00237 AFIX 23 H5A 5 0.298368 0.663280 0.631674 11.00000 -1.20000 H5B 5 0.397915 0.667881 0.731693 11.00000 -1.20000 AFIX 0 C6 1 0.405824 0.614559 0.477597 11.00000 0.02674 0.02202 = 0.02406 0.00443 -0.00005 0.00120 AFIX 23 H6A 5 0.474169 0.623555 0.465915 11.00000 -1.20000 H6B 5 0.395300 0.556431 0.519268 11.00000 -1.20000 AFIX 0 C11 1 0.387985 0.562029 0.171955 11.00000 0.03995 0.03282 = 0.02323 -0.00030 0.00508 0.00017 AFIX 23 H11A 5 0.456869 0.562794 0.156572 11.00000 -1.20000 H11B 5 0.359158 0.573978 0.052648 11.00000 -1.20000 AFIX 0 O11 3 0.261170 0.250557 0.427238 11.00000 0.04685 0.03049 = 0.05627 0.00807 -0.00076 0.00049 C12 1 0.163803 0.261684 0.389567 11.00000 0.04651 0.03867 = 0.04271 -0.00128 -0.00243 -0.00813 AFIX 23 H12A 5 0.143086 0.220765 0.297114 11.00000 -1.20000 H12B 5 0.126584 0.252620 0.501111 11.00000 -1.20000 AFIX 0 O13 3 0.150123 0.344538 0.324667 11.00000 0.03325 0.04272 = 0.05470 0.00496 -0.00089 -0.00461 C3A 1 0.238204 0.378176 0.304903 11.00000 0.02820 0.03428 = 0.02600 -0.00429 -0.00122 0.00405 C14 1 0.262068 0.455417 0.239954 11.00000 0.03381 0.03082 = 0.02520 -0.00079 -0.00481 0.00724 AFIX 43 H14 5 0.215679 0.493677 0.199274 11.00000 -1.20000 AFIX 0 C15 1 0.357610 0.476141 0.235559 11.00000 0.03715 0.02658 = 0.01913 -0.00437 0.00182 0.00308 C16 1 0.423149 0.418888 0.298316 11.00000 0.02829 0.03355 = 0.03073 -0.00629 0.00184 0.00592 AFIX 43 H16 5 0.487529 0.433889 0.296057 11.00000 -1.20000 AFIX 0 C17 1 0.398270 0.340193 0.364582 11.00000 0.03740 0.02695 = 0.03653 -0.00112 -0.00250 0.00928 AFIX 43 H17 5 0.443834 0.301468 0.406668 11.00000 -1.20000 AFIX 0 C7A 1 0.304524 0.321827 0.365630 11.00000 0.04196 0.02420 = 0.02891 -0.00269 0.00042 0.00360 C47 1 0.401462 0.820568 0.671836 11.00000 0.02927 0.01884 = 0.03038 0.00426 -0.00138 -0.00144 O47 3 0.418354 0.805591 0.831683 11.00000 0.05603 0.02330 = 0.03048 0.00206 -0.00641 -0.00554 C41 1 0.406410 0.910215 0.606413 11.00000 0.03650 0.01826 = 0.02840 0.00235 -0.00022 -0.00312 C42 1 0.328101 0.960710 0.594540 11.00000 0.03444 0.02947 = 0.05117 0.00951 0.00375 -0.00158 F42 4 0.243587 0.923307 0.622238 11.00000 0.03230 0.04514 = 0.10853 0.02933 0.00559 -0.00061 C43 1 0.331562 1.044654 0.555508 11.00000 0.05023 0.02827 = 0.06421 0.01275 0.00941 0.00908 AFIX 43 H43 5 0.275953 1.077170 0.549167 11.00000 -1.20000 AFIX 0 C44 1 0.418122 1.080361 0.525790 11.00000 0.06829 0.01875 = 0.04258 0.00610 0.00792 -0.00380 AFIX 43 H44 5 0.422070 1.138291 0.497961 11.00000 -1.20000 AFIX 0 C45 1 0.499167 1.033458 0.535740 11.00000 0.04609 0.02825 = 0.03805 0.00186 0.00740 -0.01265 AFIX 43 H45 5 0.558706 1.058363 0.515808 11.00000 -1.20000 AFIX 0 C46 1 0.491264 0.949547 0.575377 11.00000 0.03313 0.02650 = 0.03131 0.00028 0.00258 -0.00208 F46 4 0.569655 0.902060 0.584279 11.00000 0.03301 0.04044 = 0.06575 0.00595 0.00544 0.00056 HKLF 4 REM m3cg REM R1 = 0.0535 for 3449 Fo > 4sig(Fo) and 0.0560 for all 3743 data REM 235 parameters refined using 1 restraints END WGHT 0.0960 0.0000 REM Instructions for potential hydrogen bonds EQIV $1 x, y, z-1 HTAB C2 O47_$1 EQIV $2 -x+1/2, y, z-1/2 HTAB C3 F42_$2 EQIV $3 -x+1/2, y, z+1/2 HTAB C5 N1_$3 EQIV $4 -x+1, -y+2, z-1/2 HTAB C45 O47_$4 REM Highest difference peak 0.171, deepest hole -0.215, 1-sigma level 0.040 Q1 1 0.3730 0.6333 0.5398 11.00000 0.05 0.17 Q2 1 0.4970 0.9929 0.6272 11.00000 0.05 0.17 Q3 1 0.4064 0.8638 0.6308 11.00000 0.05 0.17 Q4 1 0.3817 0.4509 0.3048 11.00000 0.05 0.16 Q5 1 0.5971 1.0388 0.3303 11.00000 0.05 0.16 Q6 1 0.4033 0.6455 0.5578 11.00000 0.05 0.16 Q7 1 0.3116 0.4733 0.2829 11.00000 0.05 0.15 Q8 1 0.4588 1.0565 0.5931 11.00000 0.05 0.15 Q9 1 0.3610 0.9257 0.5408 11.00000 0.05 0.15 Q10 1 0.4368 0.9300 0.6440 11.00000 0.05 0.15 Q11 1 0.3610 0.3204 0.2934 11.00000 0.05 0.14 Q12 1 0.3314 0.9978 0.5049 11.00000 0.05 0.14 Q13 1 0.3831 0.6757 0.2850 11.00000 0.05 0.14 Q14 1 0.3665 0.5937 0.2385 11.00000 0.05 0.14 Q15 1 0.3749 0.7142 0.6049 11.00000 0.05 0.14 Q16 1 0.4963 0.9926 0.4870 11.00000 0.05 0.13 Q17 1 0.2467 0.4230 0.3104 11.00000 0.05 0.13 Q18 1 0.2576 1.0587 0.4617 11.00000 0.05 0.13 Q19 1 0.3386 1.0030 0.6527 11.00000 0.05 0.13 Q20 1 0.3797 0.9433 0.6484 11.00000 0.05 0.13 ; _shelx_res_checksum 16120 _shelxl_version_number 2.014 data_III _database_code_depnum_ccdc_archive 'CCDC 1889710' _audit_creation_method SHELXL-2014 _chemical_name_systematic ; 1-[(1,3-Benzodioxol-5-yl)methyl]-4-(2,4-dichlorobenzoyl)piperazine ; _chemical_name_common ? _chemical_formula_moiety 'C19 H18 Cl2 N2 O3' _chemical_formula_sum 'C19 H18 Cl2 N2 O3' _chemical_formula_iupac 'C19 H18 Cl2 N2 O3' _chemical_formula_weight 393.25 _chemical_melting_point ? _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 12.2889(14) _cell_length_b 12.3034(14) _cell_length_c 13.3667(15) _cell_angle_alpha 90 _cell_angle_beta 116.2950(10) _cell_angle_gamma 90 _cell_volume 1811.9(4) _cell_formula_units_Z 4 _cell_measurement_reflns_used 4054 _cell_measurement_theta_min 2.372 _cell_measurement_theta_max 27.434 _cell_measurement_temperature 173(2) _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_size_max 0.490 _exptl_crystal_size_mid 0.480 _exptl_crystal_size_min 0.375 _exptl_crystal_density_diffrn 1.442 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 816 _exptl_absorpt_coefficient_mu 0.380 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2015) ; _exptl_absorpt_correction_T_min 0.776 _exptl_absorpt_correction_T_max 0.867 _exptl_special_details ? _diffrn_ambient_temperature 173(2) _diffrn_source 'fine focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 0.3333 _diffrn_reflns_number 9718 _diffrn_reflns_av_R_equivalents 0.0174 _diffrn_reflns_av_unetI/netI 0.0203 _diffrn_reflns_theta_min 2.372 _diffrn_reflns_theta_max 27.434 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_standards_number 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_decay_% 0 _refine_special_details ? _reflns_number_total 4054 _reflns_number_gt 3545 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0363 _refine_ls_R_factor_gt 0.0312 _refine_ls_wR_factor_gt 0.0836 _refine_ls_wR_factor_ref 0.0869 _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_restrained_S_all 1.042 _refine_ls_number_reflns 4054 _refine_ls_number_parameters 235 _refine_ls_number_restraints 0 _refine_ls_hydrogen_treatment constr _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0430P)^2^+0.6034P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.371 _refine_diff_density_min -0.375 _refine_ls_extinction_method none _refine_ls_extinction_coef . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ; APEX2 (Bruker, 2004) ; _computing_cell_refinement ; SAINT (Bruker, 2013) ; _computing_data_reduction ; SAINT (Bruker, 2013) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_molecular_graphics ; PLATON (Spek, 2009) ; _computing_publication_material ; SHELXL2014 and PLATON (Spek, 2009) ; loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N N1 0.52986(10) 0.18706(10) 0.64831(10) 0.0293(3) Uani d 1 . . C C2 0.48214(12) 0.13857(13) 0.72047(12) 0.0335(3) Uani d 1 . . H H2A 0.5451 0.1407 0.7989 0.040 Uiso calc 1 . . H H2B 0.4609 0.0616 0.6993 0.040 Uiso calc 1 . . C C3 0.37079(12) 0.19934(13) 0.71033(11) 0.0321(3) Uani d 1 . . H H3A 0.3360 0.1622 0.7553 0.038 Uiso calc 1 . . H H3B 0.3939 0.2740 0.7398 0.038 Uiso calc 1 . . N N4 0.27950(10) 0.20437(11) 0.59349(9) 0.0310(3) Uani d 1 . . C C5 0.32597(13) 0.24338(15) 0.51615(12) 0.0376(3) Uani d 1 . . H H5A 0.3457 0.3217 0.5292 0.045 Uiso calc 1 . . H H5B 0.2629 0.2343 0.4384 0.045 Uiso calc 1 . . C C6 0.43884(13) 0.18029(13) 0.53272(12) 0.0342(3) Uani d 1 . . H H6A 0.4173 0.1032 0.5122 0.041 Uiso calc 1 . . H H6B 0.4723 0.2103 0.4834 0.041 Uiso calc 1 . . C C11 0.64509(13) 0.13691(12) 0.66549(15) 0.0371(3) Uani d 1 . . H H11A 0.6295 0.0625 0.6341 0.045 Uiso calc 1 . . H H11B 0.6988 0.1313 0.7465 0.045 Uiso calc 1 . . O O11 0.87114(9) 0.40074(9) 0.46855(9) 0.0362(2) Uani d 1 . . C C12 0.83867(16) 0.50226(13) 0.49898(14) 0.0407(4) Uani d 1 . . H H12A 0.7743 0.5375 0.4326 0.049 Uiso calc 1 . . H H12B 0.9100 0.5511 0.5296 0.049 Uiso calc 1 . . O O13 0.79616(10) 0.48304(9) 0.58078(10) 0.0391(3) Uani d 1 . . C C3A 0.77539(12) 0.37264(11) 0.57687(12) 0.0280(3) Uani d 1 . . C C14 0.71953(12) 0.31497(12) 0.62874(12) 0.0312(3) Uani d 1 . . H H14 0.6897 0.3498 0.6751 0.037 Uiso calc 1 . . C C15 0.70819(12) 0.20229(12) 0.61057(12) 0.0299(3) Uani d 1 . . C C16 0.75523(12) 0.15362(12) 0.54436(12) 0.0316(3) Uani d 1 . . H H16 0.7471 0.0773 0.5330 0.038 Uiso calc 1 . . C C17 0.81427(12) 0.21356(12) 0.49382(11) 0.0311(3) Uani d 1 . . H H17 0.8479 0.1795 0.4501 0.037 Uiso calc 1 . . C C7A 0.82108(11) 0.32314(12) 0.51047(11) 0.0269(3) Uani d 1 . . C C47 0.15968(12) 0.18798(11) 0.55740(11) 0.0273(3) Uani d 1 . . O O47 0.08510(9) 0.19648(11) 0.45924(8) 0.0426(3) Uani d 1 . . C C41 0.11656(11) 0.15520(11) 0.64264(10) 0.0240(3) Uani d 1 . . C C42 0.09914(11) 0.22960(10) 0.71238(10) 0.0236(3) Uani d 1 . . Cl Cl42 0.13921(3) 0.36508(3) 0.71225(3) 0.03486(11) Uani d 1 . . C C43 0.04921(11) 0.19988(11) 0.78313(11) 0.0261(3) Uani d 1 . . H H43 0.0384 0.2518 0.8306 0.031 Uiso calc 1 . . C C44 0.01549(11) 0.09273(12) 0.78272(11) 0.0276(3) Uani d 1 . . Cl Cl44 -0.04771(4) 0.05479(4) 0.87079(3) 0.04291(12) Uani d 1 . . C C45 0.02990(12) 0.01613(11) 0.71408(12) 0.0310(3) Uani d 1 . . H H45 0.0052 -0.0570 0.7143 0.037 Uiso calc 1 . . C C46 0.08095(12) 0.04794(11) 0.64495(12) 0.0291(3) Uani d 1 . . H H46 0.0920 -0.0044 0.5980 0.035 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0239(5) 0.0337(6) 0.0344(6) 0.0016(5) 0.0165(5) 0.0087(5) C2 0.0262(6) 0.0420(8) 0.0328(7) -0.0015(6) 0.0135(6) 0.0125(6) C3 0.0253(6) 0.0480(9) 0.0241(6) -0.0042(6) 0.0119(5) 0.0031(6) N4 0.0243(5) 0.0478(7) 0.0239(5) 0.0012(5) 0.0135(5) 0.0061(5) C5 0.0304(7) 0.0575(10) 0.0312(7) 0.0080(7) 0.0194(6) 0.0154(7) C6 0.0313(7) 0.0454(9) 0.0332(7) 0.0022(6) 0.0208(6) 0.0042(6) C11 0.0294(7) 0.0333(8) 0.0526(9) 0.0061(6) 0.0217(7) 0.0129(7) O11 0.0389(6) 0.0424(6) 0.0378(6) -0.0031(5) 0.0265(5) 0.0000(5) C12 0.0499(9) 0.0396(8) 0.0452(9) -0.0087(7) 0.0326(8) -0.0021(7) O13 0.0537(6) 0.0300(5) 0.0509(6) -0.0066(5) 0.0388(6) -0.0041(5) C3A 0.0256(6) 0.0292(7) 0.0320(7) 0.0002(5) 0.0153(6) -0.0009(5) C14 0.0307(7) 0.0328(7) 0.0389(8) 0.0036(6) 0.0235(6) 0.0016(6) C15 0.0214(6) 0.0319(7) 0.0377(7) 0.0051(5) 0.0143(6) 0.0062(6) C16 0.0250(6) 0.0287(7) 0.0378(8) 0.0046(5) 0.0110(6) -0.0008(6) C17 0.0255(6) 0.0386(8) 0.0291(7) 0.0053(6) 0.0120(5) -0.0041(6) C7A 0.0193(6) 0.0379(7) 0.0241(6) -0.0003(5) 0.0103(5) 0.0004(5) C47 0.0259(6) 0.0336(7) 0.0251(6) 0.0026(5) 0.0137(5) -0.0010(5) O47 0.0286(5) 0.0743(8) 0.0238(5) 0.0021(5) 0.0106(4) 0.0031(5) C41 0.0186(5) 0.0306(7) 0.0226(6) 0.0011(5) 0.0090(5) -0.0002(5) C42 0.0232(6) 0.0246(6) 0.0233(6) -0.0024(5) 0.0105(5) 0.0000(5) Cl42 0.0493(2) 0.02548(18) 0.03616(19) -0.00753(14) 0.02471(17) -0.00147(13) C43 0.0246(6) 0.0315(7) 0.0237(6) -0.0015(5) 0.0121(5) -0.0013(5) C44 0.0211(6) 0.0351(7) 0.0261(6) -0.0021(5) 0.0101(5) 0.0063(5) Cl44 0.0431(2) 0.0533(2) 0.0397(2) -0.01166(17) 0.02503(17) 0.00825(17) C45 0.0276(7) 0.0253(7) 0.0361(7) -0.0013(5) 0.0105(6) 0.0046(6) C46 0.0274(6) 0.0271(7) 0.0311(7) 0.0039(5) 0.0115(5) -0.0025(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag N1 C6 . 1.4540(19) ? N1 C2 . 1.4600(17) ? N1 C11 . 1.4665(17) ? C2 C3 . 1.512(2) ? C2 H2A . 0.9900 ? C2 H2B . 0.9900 ? C3 N4 . 1.4660(17) ? C3 H3A . 0.9900 ? C3 H3B . 0.9900 ? N4 C47 . 1.3462(17) ? N4 C5 . 1.4658(17) ? C5 C6 . 1.518(2) ? C5 H5A . 0.9900 ? C5 H5B . 0.9900 ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C11 C15 . 1.5138(19) ? C11 H11A . 0.9900 ? C11 H11B . 0.9900 ? O11 C7A . 1.3817(17) ? O11 C12 . 1.4242(19) ? C12 O13 . 1.4249(17) ? C12 H12A . 0.9900 ? C12 H12B . 0.9900 ? O13 C3A . 1.3787(17) ? C3A C14 . 1.3701(19) ? C3A C7A . 1.3839(19) ? C14 C15 . 1.404(2) ? C14 H14 . 0.9500 ? C15 C16 . 1.389(2) ? C16 C17 . 1.400(2) ? C16 H16 . 0.9500 ? C17 C7A . 1.363(2) ? C17 H17 . 0.9500 ? C47 O47 . 1.2276(17) ? C47 C41 . 1.5088(17) ? C41 C42 . 1.3890(18) ? C41 C46 . 1.3950(19) ? C42 C43 . 1.3852(17) ? C42 Cl42 . 1.7383(13) ? C43 C44 . 1.381(2) ? C43 H43 . 0.9500 ? C44 C45 . 1.380(2) ? C44 Cl44 . 1.7370(13) ? C45 C46 . 1.384(2) ? C45 H45 . 0.9500 ? C46 H46 . 0.9500 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 N1 C2 . . 109.49(11) ? C6 N1 C11 . . 112.16(12) ? C2 N1 C11 . . 111.54(11) ? N1 C2 C3 . . 110.56(11) ? N1 C2 H2A . . 109.5 ? C3 C2 H2A . . 109.5 ? N1 C2 H2B . . 109.5 ? C3 C2 H2B . . 109.5 ? H2A C2 H2B . . 108.1 ? N4 C3 C2 . . 110.58(12) ? N4 C3 H3A . . 109.5 ? C2 C3 H3A . . 109.5 ? N4 C3 H3B . . 109.5 ? C2 C3 H3B . . 109.5 ? H3A C3 H3B . . 108.1 ? C47 N4 C5 . . 120.16(11) ? C47 N4 C3 . . 125.09(11) ? C5 N4 C3 . . 114.32(11) ? N4 C5 C6 . . 110.25(12) ? N4 C5 H5A . . 109.6 ? C6 C5 H5A . . 109.6 ? N4 C5 H5B . . 109.6 ? C6 C5 H5B . . 109.6 ? H5A C5 H5B . . 108.1 ? N1 C6 C5 . . 110.42(12) ? N1 C6 H6A . . 109.6 ? C5 C6 H6A . . 109.6 ? N1 C6 H6B . . 109.6 ? C5 C6 H6B . . 109.6 ? H6A C6 H6B . . 108.1 ? N1 C11 C15 . . 111.53(11) ? N1 C11 H11A . . 109.3 ? C15 C11 H11A . . 109.3 ? N1 C11 H11B . . 109.3 ? C15 C11 H11B . . 109.3 ? H11A C11 H11B . . 108.0 ? C7A O11 C12 . . 105.00(10) ? O11 C12 O13 . . 108.54(12) ? O11 C12 H12A . . 110.0 ? O13 C12 H12A . . 110.0 ? O11 C12 H12B . . 110.0 ? O13 C12 H12B . . 110.0 ? H12A C12 H12B . . 108.4 ? C3A O13 C12 . . 105.01(11) ? C14 C3A O13 . . 128.09(13) ? C14 C3A C7A . . 122.22(13) ? O13 C3A C7A . . 109.69(12) ? C3A C14 C15 . . 117.23(13) ? C3A C14 H14 . . 121.4 ? C15 C14 H14 . . 121.4 ? C16 C15 C14 . . 119.91(13) ? C16 C15 C11 . . 121.81(13) ? C14 C15 C11 . . 118.28(13) ? C15 C16 C17 . . 122.09(14) ? C15 C16 H16 . . 119.0 ? C17 C16 H16 . . 119.0 ? C7A C17 C16 . . 116.72(13) ? C7A C17 H17 . . 121.6 ? C16 C17 H17 . . 121.6 ? C17 C7A O11 . . 128.57(12) ? C17 C7A C3A . . 121.80(13) ? O11 C7A C3A . . 109.63(12) ? O47 C47 N4 . . 123.39(13) ? O47 C47 C41 . . 118.97(12) ? N4 C47 C41 . . 117.62(11) ? C42 C41 C46 . . 117.74(12) ? C42 C41 C47 . . 122.74(12) ? C46 C41 C47 . . 119.22(12) ? C43 C42 C41 . . 122.06(12) ? C43 C42 Cl42 . . 117.72(10) ? C41 C42 Cl42 . . 120.22(10) ? C44 C43 C42 . . 118.17(12) ? C44 C43 H43 . . 120.9 ? C42 C43 H43 . . 120.9 ? C45 C44 C43 . . 121.85(12) ? C45 C44 Cl44 . . 119.64(11) ? C43 C44 Cl44 . . 118.50(11) ? C44 C45 C46 . . 118.71(13) ? C44 C45 H45 . . 120.6 ? C46 C45 H45 . . 120.6 ? C45 C46 C41 . . 121.47(13) ? C45 C46 H46 . . 119.3 ? C41 C46 H46 . . 119.3 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 N1 C2 C3 . . . . -61.31(16) ? C11 N1 C2 C3 . . . . 173.95(13) ? N1 C2 C3 N4 . . . . 55.00(16) ? C2 C3 N4 C47 . . . . 136.85(14) ? C2 C3 N4 C5 . . . . -50.77(17) ? C47 N4 C5 C6 . . . . -136.22(14) ? C3 N4 C5 C6 . . . . 50.99(18) ? C2 N1 C6 C5 . . . . 61.64(16) ? C11 N1 C6 C5 . . . . -173.97(12) ? N4 C5 C6 N1 . . . . -55.75(17) ? C6 N1 C11 C15 . . . . 69.26(16) ? C2 N1 C11 C15 . . . . -167.51(13) ? C7A O11 C12 O13 . . . . 14.03(16) ? O11 C12 O13 C3A . . . . -14.51(16) ? C12 O13 C3A C14 . . . . -170.92(15) ? C12 O13 C3A C7A . . . . 9.41(16) ? O13 C3A C14 C15 . . . . 179.33(14) ? C7A C3A C14 C15 . . . . -1.0(2) ? C3A C14 C15 C16 . . . . 1.5(2) ? C3A C14 C15 C11 . . . . -179.07(12) ? N1 C11 C15 C16 . . . . -132.47(14) ? N1 C11 C15 C14 . . . . 48.08(19) ? C14 C15 C16 C17 . . . . -0.2(2) ? C11 C15 C16 C17 . . . . -179.64(13) ? C15 C16 C17 C7A . . . . -1.5(2) ? C16 C17 C7A O11 . . . . -178.31(12) ? C16 C17 C7A C3A . . . . 2.0(2) ? C12 O11 C7A C17 . . . . 172.09(14) ? C12 O11 C7A C3A . . . . -8.17(15) ? C14 C3A C7A C17 . . . . -0.7(2) ? O13 C3A C7A C17 . . . . 178.96(13) ? C14 C3A C7A O11 . . . . 179.50(12) ? O13 C3A C7A O11 . . . . -0.81(15) ? C5 N4 C47 O47 . . . . 5.4(2) ? C3 N4 C47 O47 . . . . 177.41(14) ? C5 N4 C47 C41 . . . . -175.89(13) ? C3 N4 C47 C41 . . . . -3.9(2) ? O47 C47 C41 C42 . . . . -100.59(16) ? N4 C47 C41 C42 . . . . 80.68(17) ? O47 C47 C41 C46 . . . . 72.85(18) ? N4 C47 C41 C46 . . . . -105.88(15) ? C46 C41 C42 C43 . . . . 0.52(19) ? C47 C41 C42 C43 . . . . 174.06(12) ? C46 C41 C42 Cl42 . . . . -178.99(10) ? C47 C41 C42 Cl42 . . . . -5.46(17) ? C41 C42 C43 C44 . . . . -0.42(19) ? Cl42 C42 C43 C44 . . . . 179.11(10) ? C42 C43 C44 C45 . . . . -0.3(2) ? C42 C43 C44 Cl44 . . . . -179.77(10) ? C43 C44 C45 C46 . . . . 0.8(2) ? Cl44 C44 C45 C46 . . . . -179.70(10) ? C44 C45 C46 C41 . . . . -0.7(2) ? C42 C41 C46 C45 . . . . 0.03(19) ? C47 C41 C46 C45 . . . . -173.74(12) ? _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_T_min 0.836 _shelx_estimated_absorpt_T_max 0.871 _shelx_hkl_file ; -1 0 0 0.00 0.10 -2 0 0 0.00 0.10 -2 0 0 -0.10 0.10 -3 0 0 -0.20 0.10 -3 0 0 0.00 0.10 -4 0 0 82.99 1.70 -4 0 0 82.99 1.50 -5 0 0 0.40 0.10 -5 0 0 -0.20 0.10 -6 0 0 72.59 1.50 -6 0 0 71.39 1.70 -7 0 0 0.00 0.20 -7 0 0 -0.10 0.10 -8 0 0 0.70 0.20 -8 0 0 0.70 0.30 -9 0 0 0.20 0.30 -10 0 0 87.69 2.40 -11 0 0 -0.20 0.30 -12 0 0 70.39 2.40 -13 0 0 -0.30 0.50 -14 0 0 0.30 0.60 -14 1 0 10.10 1.40 -13 1 0 9.50 1.10 -12 1 0 0.60 0.50 -11 1 0 6.70 0.90 -10 1 0 21.50 1.20 -9 1 0 54.19 1.70 -8 1 0 0.00 0.20 -8 1 0 0.10 0.20 -7 1 0 205.38 3.90 -7 1 0 201.88 3.50 -6 1 0 207.38 3.40 -6 1 0 206.88 3.80 -5 1 0 71.49 1.60 -5 1 0 73.99 1.40 -4 1 0 421.26 6.70 -4 1 0 417.96 6.90 -3 1 0 3625.94 76.09 -3 1 0 3669.23 64.29 -2 1 0 529.35 8.30 -1 1 0 116.19 1.90 0 1 0 -3.30 0.10 -2 -1 0 486.85 13.50 -3 -1 0 3516.65 72.29 -3 -1 0 3643.44 72.09 -4 -1 0 407.26 6.60 -4 -1 0 402.76 6.70 -5 -1 0 75.19 1.50 -5 -1 0 74.09 1.60 -6 -1 0 210.28 3.60 -6 -1 0 200.98 3.70 -7 -1 0 199.38 3.50 -7 -1 0 197.28 3.70 -8 -1 0 0.00 0.20 -8 -1 0 0.20 0.20 -9 -1 0 54.49 1.50 -9 -1 0 52.69 1.70 -10 -1 0 23.80 1.20 -11 -1 0 6.70 0.80 -12 -1 0 0.00 0.40 -13 -1 0 8.70 1.10 -14 -1 0 10.00 1.20 -13 2 0 18.70 1.40 -12 2 0 3.80 0.70 -11 2 0 40.80 1.70 -10 2 0 28.20 1.40 -9 2 0 107.99 2.70 -8 2 0 0.40 0.30 -7 2 0 36.20 1.20 -7 2 0 35.40 0.90 -6 2 0 0.80 0.30 -6 2 0 1.50 0.20 -5 2 0 73.89 1.70 -5 2 0 75.09 1.30 -4 2 0 148.59 2.70 -4 2 0 149.88 2.40 -3 2 0 51.49 0.90 -2 2 0 1112.19 21.20 1 -2 0 219.88 3.60 -1 2 0 227.18 3.80 0 -2 0 2211.38 43.20 1 2 0 233.38 4.00 -2 -2 0 1045.10 16.80 -3 -2 0 48.70 1.10 -4 -2 0 143.89 2.60 -4 -2 0 144.99 2.60 -5 -2 0 71.49 1.60 -5 -2 0 73.19 1.60 -6 -2 0 0.70 0.20 -6 -2 0 0.70 0.20 -7 -2 0 32.70 1.10 -7 -2 0 34.10 1.00 -8 -2 0 0.60 0.30 -8 -2 0 0.20 0.20 -9 -2 0 106.99 2.60 -9 -2 0 107.99 2.40 -10 -2 0 26.70 1.20 -10 -2 0 25.70 1.00 -11 -2 0 39.60 1.60 -12 -2 0 4.20 0.70 -13 -2 0 18.00 1.30 -14 -2 0 -0.10 0.50 -13 3 0 1.60 0.70 -12 3 0 1.90 0.60 -11 3 0 128.29 3.40 -10 3 0 5.90 0.70 -9 3 0 10.30 0.90 -8 3 0 15.00 0.90 -7 3 0 100.39 2.40 -6 3 0 249.38 3.90 -6 3 0 248.28 4.50 -5 3 0 57.89 1.00 -5 3 0 58.69 1.50 -4 3 0 734.83 12.80 -3 3 0 199.28 3.40 2 -3 0 -0.10 0.10 -2 3 0 0.20 0.10 1 -3 0 1641.44 32.50 -1 3 0 1628.24 27.40 -1 3 0 1706.43 25.90 0 -3 0 -1.70 0.10 -1 -3 0 1555.84 38.50 1 3 0 1629.64 27.00 -3 -3 0 194.98 3.40 -4 -3 0 683.73 11.70 -4 -3 0 708.63 11.60 -5 -3 0 57.69 1.40 -5 -3 0 56.69 1.30 -6 -3 0 249.88 4.40 -6 -3 0 245.68 4.30 -7 -3 0 99.29 2.10 -7 -3 0 93.09 2.10 -8 -3 0 15.10 0.80 -8 -3 0 15.60 0.80 -9 -3 0 10.50 0.70 -9 -3 0 11.40 0.80 -10 -3 0 5.30 0.60 -10 -3 0 6.10 0.70 -11 -3 0 118.39 3.00 -11 -3 0 122.79 3.80 -12 -3 0 2.00 0.60 -13 -3 0 1.30 0.60 -14 -3 0 2.50 0.70 -13 4 0 21.50 1.60 -12 4 0 1.40 0.60 -11 4 0 19.40 1.30 -10 4 0 53.79 1.90 -9 4 0 6.80 0.80 -8 4 0 484.45 8.40 -7 4 0 6.70 0.60 -6 4 0 25.80 1.00 -5 4 0 213.08 3.90 -4 4 0 202.98 3.60 3 -4 0 427.26 6.70 -3 4 0 433.26 6.90 2 -4 0 3.30 0.20 -2 4 0 3.20 0.30 1 -4 0 367.56 6.10 -1 4 0 364.86 5.90 0 -4 0 82.99 1.60 0 4 0 83.89 1.50 0 4 0 82.49 2.00 -1 -4 0 335.57 5.50 1 4 0 347.87 6.00 -2 -4 0 3.30 0.30 2 4 0 3.90 0.50 -3 -4 0 421.06 6.80 -4 -4 0 202.78 3.60 -5 -4 0 200.48 3.50 -5 -4 0 203.08 3.70 -6 -4 0 25.20 0.80 -6 -4 0 24.20 0.90 -7 -4 0 6.60 0.50 -7 -4 0 7.00 0.60 -8 -4 0 474.65 8.00 -8 -4 0 468.45 7.90 -9 -4 0 6.00 0.60 -9 -4 0 5.90 0.60 -10 -4 0 53.09 1.70 -10 -4 0 57.79 1.70 -11 -4 0 18.70 1.00 -11 -4 0 18.30 1.10 -12 -4 0 1.90 0.50 -13 -4 0 22.10 1.40 -13 5 0 1.20 0.70 -12 5 0 31.10 1.70 -11 5 0 3.40 0.70 -10 5 0 16.90 1.20 -9 5 0 0.70 0.40 -8 5 0 200.18 4.10 -7 5 0 41.80 1.40 -6 5 0 9.70 0.70 -5 5 0 423.16 7.10 -4 5 0 71.99 1.70 3 -5 0 84.79 1.50 -3 5 0 83.39 1.80 2 -5 0 834.02 13.20 -2 5 0 808.72 14.10 -2 5 0 828.92 13.60 1 -5 0 159.78 2.80 -1 5 0 167.48 2.80 -1 5 0 158.58 3.40 0 -5 0 0.30 0.10 0 5 0 0.50 0.10 -1 -5 0 153.98 2.80 1 5 0 160.98 3.40 -2 -5 0 800.12 13.60 2 5 0 778.82 12.90 -3 -5 0 79.89 1.80 -4 -5 0 70.99 1.70 -5 -5 0 424.26 6.80 -5 -5 0 426.56 7.10 -6 -5 0 10.70 0.50 -6 -5 0 10.70 0.70 -7 -5 0 43.90 1.40 -7 -5 0 42.90 1.20 -8 -5 0 197.08 3.70 -8 -5 0 191.68 3.90 -9 -5 0 0.50 0.30 -9 -5 0 0.40 0.30 -10 -5 0 16.10 1.00 -10 -5 0 15.90 1.00 -11 -5 0 3.10 0.60 -11 -5 0 2.70 0.60 -12 -5 0 29.20 1.40 -13 6 0 5.60 1.50 -12 6 0 0.40 0.60 -11 6 0 51.69 2.10 -10 6 0 12.60 1.10 -9 6 0 0.20 0.40 -8 6 0 1.40 0.50 -7 6 0 114.69 2.70 -6 6 0 30.60 1.20 -5 6 0 240.48 4.40 -4 6 0 2.50 0.40 3 -6 0 90.49 1.70 -3 6 0 90.29 2.50 -3 6 0 91.59 1.90 2 -6 0 270.17 4.30 -2 6 0 267.47 4.50 -2 6 0 255.97 5.20 1 -6 0 555.94 8.70 -1 6 0 541.05 9.50 -1 6 0 543.05 8.70 0 -6 0 1183.98 19.70 0 6 0 1177.38 19.90 0 6 0 1189.08 18.50 -1 -6 0 528.25 8.50 1 6 0 542.35 9.40 -2 -6 0 254.57 4.50 2 6 0 261.17 5.20 -3 -6 0 85.99 1.90 -4 -6 0 2.90 0.40 -5 -6 0 232.68 4.30 -5 -6 0 233.18 3.90 -6 -6 0 28.50 0.90 -6 -6 0 29.80 1.10 -7 -6 0 111.89 2.60 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3.30 -2 8 0 183.58 3.30 -2 8 0 177.78 4.30 1 -8 0 50.19 1.30 -1 8 0 48.00 2.00 -1 8 0 52.99 1.40 0 -8 0 66.89 1.60 0 8 0 61.79 2.30 -1 -8 0 50.89 1.40 1 8 0 50.39 2.10 -2 -8 0 172.88 3.30 2 8 0 166.08 4.20 -3 -8 0 68.49 1.80 3 8 0 70.39 2.50 -4 -8 0 134.69 2.90 -5 -8 0 3.80 0.50 -6 -8 0 92.19 2.40 -7 -8 0 14.10 0.90 -8 -8 0 220.28 4.60 -9 -8 0 106.79 2.80 -10 -8 0 2.40 0.60 -11 -8 0 7.20 0.90 -12 -8 0 4.80 0.80 -11 9 0 78.79 2.80 -10 9 0 0.30 0.50 -9 9 0 5.60 0.80 -8 9 0 9.00 1.00 -7 9 0 5.90 1.10 -7 9 0 7.80 0.80 -6 9 0 358.66 6.60 -6 9 0 368.66 7.60 -5 9 0 0.50 0.70 -5 9 0 0.90 0.40 -4 9 0 1.70 0.40 -3 9 0 72.79 2.70 2 -9 0 151.38 3.00 -2 9 0 168.78 4.30 1 -9 0 83.59 1.90 -1 9 0 85.69 2.90 0 -9 0 -0.20 0.20 0 9 0 0.40 0.60 -1 -9 0 88.49 2.10 1 9 0 90.29 3.00 -2 -9 0 148.09 3.10 2 9 0 147.99 4.00 -3 -9 0 68.29 1.90 3 9 0 68.39 2.60 -4 -9 0 1.20 0.40 -5 -9 0 0.90 0.40 -6 -9 0 344.77 6.40 -7 -9 0 8.50 0.90 -8 -9 0 10.10 0.90 -9 -9 0 6.50 0.80 -10 -9 0 0.10 0.50 -11 -9 0 78.49 2.50 -11 10 0 11.60 1.40 -10 10 0 31.20 1.70 -9 10 0 9.90 1.10 -8 10 0 5.60 1.20 -7 10 0 0.20 0.80 -6 10 0 7.20 1.20 -5 10 0 216.58 5.50 -4 10 0 23.60 1.80 -3 10 0 10.10 1.30 -2 10 0 22.50 1.70 1 -10 0 30.80 1.10 -1 10 0 34.90 2.00 0 -10 0 0.90 0.30 0 10 0 0.70 0.70 -1 -10 0 29.40 1.10 1 10 0 36.70 2.00 -2 -10 0 23.10 1.00 2 10 0 23.20 1.70 -3 -10 0 11.90 0.80 3 10 0 10.90 1.40 -4 -10 0 17.80 1.00 -5 -10 0 210.18 4.30 -6 -10 0 7.30 0.80 -7 -10 0 0.20 0.40 -8 -10 0 4.80 0.70 -9 -10 0 7.60 0.90 -10 -10 0 29.90 1.60 -9 11 0 15.70 2.10 -8 11 0 25.90 2.20 -7 11 0 86.69 3.50 -6 11 0 43.10 2.40 -5 11 0 8.90 1.40 -4 11 0 66.19 2.90 -3 11 0 44.50 2.50 -2 11 0 1.50 0.90 0 -11 0 -0.20 0.30 0 11 0 -0.10 0.80 -1 -11 0 2.20 0.50 1 11 0 1.90 0.90 -2 -11 0 1.10 0.40 2 11 0 1.80 0.90 -3 -11 0 45.30 1.60 3 11 0 44.50 2.40 -4 -11 0 61.49 1.90 -5 -11 0 8.70 0.90 -6 -11 0 41.90 1.70 -7 -11 0 85.29 2.60 -8 -11 0 26.40 1.50 -9 -11 0 14.50 1.20 -10 -11 0 5.00 1.10 -9 12 0 33.10 3.80 -8 12 0 -0.30 1.00 -7 12 0 22.80 2.10 -6 12 0 1.90 1.10 -5 12 0 0.70 1.00 -4 12 0 6.10 1.30 -3 12 0 10.50 1.60 -2 12 0 0.80 0.90 -1 12 0 178.88 5.20 0 -12 0 114.69 3.00 0 12 0 108.59 4.00 -1 -12 0 171.58 3.70 1 12 0 173.68 5.10 -2 -12 0 0.20 0.30 2 12 0 0.30 0.80 -3 -12 0 9.30 0.90 3 12 0 11.50 1.70 -4 -12 0 7.50 0.80 -5 -12 0 1.80 0.50 -6 -12 0 2.60 0.60 -7 -12 0 22.30 1.40 -8 -12 0 0.20 0.50 -7 13 0 0.30 1.00 -6 13 0 108.79 4.20 -5 13 0 8.90 1.60 -4 13 0 44.10 2.70 -3 13 0 0.60 0.90 -2 13 0 64.39 3.20 -1 13 0 0.40 1.00 0 13 0 0.90 1.00 -1 -13 0 0.70 0.40 1 13 0 0.70 0.90 -2 -13 0 68.29 2.10 2 13 0 71.39 3.30 -3 -13 0 -0.20 0.40 3 13 0 -0.30 0.80 -4 -13 0 39.10 1.70 -5 -13 0 5.90 0.80 -6 -13 0 102.09 3.00 -7 -13 0 -0.10 0.50 -6 14 0 3.10 1.30 -5 14 0 7.30 1.60 -4 14 0 14.20 2.10 -3 14 0 48.50 3.00 -2 14 0 11.70 1.90 -1 14 0 17.40 2.20 0 14 0 43.30 3.00 1 14 0 16.90 2.00 -2 -14 0 8.10 0.90 2 14 0 9.40 1.70 -3 -14 0 44.80 1.80 -4 -14 0 11.20 1.10 -5 -14 0 6.70 0.90 -6 -14 0 2.20 0.60 -3 15 0 36.90 3.00 -2 15 0 3.90 1.40 -1 15 0 26.60 2.60 0 15 0 -0.50 1.00 1 15 0 27.70 2.50 2 15 0 2.40 1.20 -3 -15 0 38.30 1.80 -4 -15 0 6.70 0.90 -5 -15 1 12.00 1.20 -4 -15 1 0.00 0.40 2 15 -1 47.90 3.10 1 15 -1 11.10 1.90 0 15 -1 0.40 1.10 -1 15 -1 0.70 1.20 -2 15 -1 31.90 2.70 -3 15 -1 1.80 1.30 -6 -14 1 20.60 1.40 -5 -14 1 0.80 0.50 -4 -14 1 2.10 0.60 3 14 -1 3.90 1.30 -3 -14 1 3.30 0.60 2 14 -1 0.50 1.00 1 14 -1 21.40 2.20 0 14 -1 1.50 1.20 -1 14 -1 7.30 1.60 -2 14 -1 0.70 1.10 -3 14 -1 5.00 1.40 -4 14 -1 30.50 2.60 -5 14 -1 11.00 1.80 -8 -13 1 0.20 0.50 -7 -13 1 0.20 0.50 -6 -13 1 27.90 1.50 -5 -13 1 45.80 1.80 -4 -13 1 5.70 0.80 3 13 -1 57.29 3.00 -3 -13 1 57.79 1.90 2 13 -1 -0.10 0.90 -2 -13 1 -0.10 0.30 1 13 -1 1.50 1.00 0 13 -1 0.90 1.00 -1 13 -1 43.80 2.70 -2 13 -1 15.50 1.90 -3 13 -1 1.10 1.00 -4 13 -1 1.40 1.10 -5 13 -1 21.90 2.30 -6 13 -1 2.00 1.20 -7 13 -1 0.40 1.00 -9 -12 1 0.50 0.50 -8 -12 1 0.50 0.50 -7 -12 1 17.40 1.20 -6 -12 1 63.99 2.10 -5 -12 1 40.20 1.60 -4 -12 1 29.90 1.40 3 12 -1 10.40 1.50 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5 1.20 0.50 4 12 -5 35.60 2.40 -4 -12 5 34.50 1.40 3 12 -5 9.00 1.50 2 12 -5 9.00 1.40 1 12 -5 32.00 2.40 0 12 -5 52.89 2.80 -1 12 -5 0.00 0.90 -2 12 -5 25.00 2.10 -3 12 -5 17.10 2.00 -4 12 -5 28.50 2.30 -5 12 -5 4.90 1.30 -6 12 -5 2.50 1.10 -11 -11 5 23.70 1.90 -10 -11 5 13.50 1.20 -9 -11 5 5.00 0.80 -8 -11 5 20.20 1.30 -7 -11 5 4.20 0.70 -6 -11 5 56.89 1.90 -5 -11 5 0.20 0.40 4 11 -5 195.58 5.30 -4 -11 5 185.08 3.90 3 11 -5 0.20 0.80 -3 -11 5 0.70 0.30 2 11 -5 0.00 0.70 1 11 -5 3.60 1.10 0 11 -5 9.60 1.40 -1 11 -5 73.49 3.10 -2 11 -5 25.40 2.00 -3 11 -5 3.60 1.10 -4 11 -5 -0.70 0.90 -4 11 -5 0.40 0.90 -5 11 -5 5.40 1.00 -5 11 -5 5.10 1.20 -6 11 -5 2.50 0.90 -6 11 -5 3.80 1.20 -7 11 -5 0.60 1.00 -7 11 -5 1.70 0.80 -12 -10 5 0.70 0.80 -11 -10 5 43.30 1.90 -10 -10 5 13.80 1.10 -9 -10 5 22.50 1.30 -8 -10 5 1.00 0.50 -7 -10 5 93.59 2.60 -6 -10 5 8.70 0.80 -5 -10 5 30.20 1.30 4 10 -5 142.29 4.20 -4 -10 5 142.89 3.10 3 10 -5 49.99 2.40 -3 -10 5 52.39 1.60 2 10 -5 196.08 5.10 -2 -10 5 193.18 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15.70 1.50 -8 9 -5 2.50 0.90 -13 -8 5 25.40 1.50 -12 -8 5 3.10 0.70 -11 -8 5 15.30 1.10 -10 -8 5 15.20 1.10 -9 -8 5 22.40 1.20 -8 -8 5 21.60 1.10 -7 -8 5 47.20 1.60 -6 -8 5 70.59 2.00 -5 -8 5 890.11 14.30 4 8 -5 88.89 2.90 -4 -8 5 91.09 2.20 3 8 -5 1.00 0.60 3 8 -5 0.70 0.30 -3 -8 5 0.60 0.30 2 8 -5 6.90 0.60 2 8 -5 7.30 1.00 -2 -8 5 7.00 0.50 1 8 -5 1.00 0.40 1 8 -5 0.90 0.60 -1 -8 5 2.00 0.30 0 8 -5 132.59 3.60 0 8 -5 128.99 3.10 -1 8 -5 42.30 2.00 -1 8 -5 41.50 1.70 -2 8 -5 67.79 2.20 -2 8 -5 63.19 2.40 -3 8 -5 33.40 1.60 -3 8 -5 32.10 1.80 -4 8 -5 34.40 1.60 -4 8 -5 32.80 1.90 -5 8 -5 2.20 0.70 -5 8 -5 1.40 0.80 -6 8 -5 3.90 0.80 -7 8 -5 188.78 4.70 -8 8 -5 2.00 0.70 -9 8 -5 0.90 0.80 -14 -7 5 14.90 1.20 -13 -7 5 1.10 0.50 -12 -7 5 2.10 0.60 -11 -7 5 7.80 0.90 -10 -7 5 27.60 1.30 -9 -7 5 5.40 0.70 -8 -7 5 104.09 2.60 -7 -7 5 51.29 1.60 -6 -7 5 3.40 0.50 -5 -7 5 89.09 2.20 -4 -7 5 367.56 6.30 3 7 -5 25.30 0.90 3 7 -5 25.20 1.40 -3 -7 5 23.80 0.90 2 7 -5 105.79 2.90 2 7 -5 106.29 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-4 14 0.10 0.60 -9 -4 14 6.90 0.90 -8 -4 14 45.70 1.80 -7 -4 14 24.20 1.40 -6 -4 14 14.70 1.10 5 4 -14 4.40 0.70 -5 -4 14 3.00 0.60 4 4 -14 11.50 1.10 -4 -4 14 11.60 1.00 3 4 -14 0.90 0.60 2 4 -14 -0.20 0.50 1 4 -14 73.59 2.80 0 4 -14 3.00 1.00 -1 4 -14 9.00 1.30 -13 -3 14 -0.60 0.60 -12 -3 14 22.40 1.50 -11 -3 14 4.80 0.90 -10 -3 14 30.40 1.60 -9 -3 14 0.10 0.50 -8 -3 14 52.49 1.90 -7 -3 14 21.50 1.20 -6 -3 14 35.10 1.50 5 3 -14 38.70 1.60 -5 -3 14 39.60 1.50 4 3 -14 29.80 1.50 -4 -3 14 29.00 1.30 3 3 -14 1.00 0.60 -3 -3 14 0.10 0.40 2 3 -14 2.50 0.80 1 3 -14 3.80 0.90 0 3 -14 5.20 1.10 -1 3 -14 26.30 2.00 -2 3 -14 28.50 3.10 -13 -2 14 117.99 3.40 -12 -2 14 0.20 0.60 -11 -2 14 44.10 1.90 -10 -2 14 3.10 0.70 -9 -2 14 0.00 0.50 -8 -2 14 54.99 1.90 -7 -2 14 0.10 0.40 -6 -2 14 34.70 1.40 5 2 -14 153.38 3.60 -5 -2 14 151.28 3.30 4 2 -14 3.50 0.70 -4 -2 14 3.90 0.60 3 2 -14 70.39 2.40 2 2 -14 3.40 0.80 1 2 -14 0.60 0.70 0 2 -14 0.60 0.80 -1 2 -14 0.70 0.80 -2 2 -14 0.80 0.80 -13 -1 14 1.40 0.70 -12 -1 14 16.40 1.40 -11 -1 14 5.60 0.80 -10 -1 14 43.00 1.70 -9 -1 14 40.00 1.70 -8 -1 14 86.49 2.40 -7 -1 14 82.39 2.20 -6 -1 14 21.00 1.10 5 1 -14 24.60 1.30 4 1 -14 2.70 0.60 4 1 -14 2.70 0.50 3 1 -14 1.60 0.60 3 1 -14 1.40 0.50 2 1 -14 10.50 0.90 2 1 -14 11.00 1.10 1 1 -14 8.20 1.10 0 1 -14 8.20 1.20 -1 1 -14 3.30 1.00 -2 1 -14 23.60 1.90 -14 0 14 4.80 1.10 -13 0 14 0.30 0.60 -12 0 14 1.50 0.70 -11 0 14 -0.60 0.50 -10 0 14 27.50 1.40 -9 0 14 -0.40 0.40 -8 0 14 0.80 0.50 -7 0 14 0.30 0.40 5 0 -14 -0.30 0.40 4 0 -14 2.90 0.60 4 0 -14 2.90 0.60 3 0 -14 -0.10 0.40 3 0 -14 -0.20 0.50 2 0 -14 5.20 0.80 2 0 -14 4.80 0.70 1 0 -14 -0.30 0.60 1 0 -14 -0.60 0.40 0 0 -14 261.27 5.80 -1 0 -14 0.40 0.80 -2 0 -14 54.49 2.50 -14 1 14 0.80 0.70 -13 1 14 1.20 0.70 -12 1 14 17.90 1.40 -11 1 14 6.40 0.90 -10 1 14 46.80 1.70 -9 1 14 40.80 1.60 -8 1 14 86.09 2.30 6 -1 -14 22.00 1.20 5 -1 -14 24.00 1.20 4 -1 -14 3.20 0.60 4 -1 -14 3.90 0.60 3 -1 -14 1.80 0.50 3 -1 -14 1.50 0.50 2 -1 -14 9.60 1.00 2 -1 -14 11.70 1.10 1 -1 -14 9.50 1.00 1 -1 -14 8.10 1.00 0 -1 -14 6.40 1.00 -1 -1 -14 2.70 0.90 -2 -1 -14 19.70 1.70 -13 2 14 120.79 3.30 -12 2 14 0.70 0.60 -11 2 14 46.40 1.80 -10 2 14 4.20 0.70 -9 2 14 0.50 0.40 7 -2 -14 0.40 0.50 6 -2 -14 36.00 1.50 5 -2 -14 153.48 3.50 4 -2 -14 4.00 0.70 4 -2 -14 4.00 0.60 3 -2 -14 71.19 2.10 3 -2 -14 70.89 2.20 2 -2 -14 4.40 0.70 2 -2 -14 4.00 0.70 1 -2 -14 0.50 0.50 1 -2 -14 1.20 0.60 0 -2 -14 0.40 0.50 -13 3 14 0.10 0.60 -12 3 14 24.50 1.40 -11 3 14 5.20 0.80 -10 3 14 31.00 1.40 8 -3 -14 52.89 1.80 7 -3 -14 23.10 1.30 6 -3 -14 37.80 1.60 5 -3 -14 41.50 1.70 4 -3 -14 26.50 1.40 3 -3 -14 0.80 0.50 2 -3 -14 1.80 0.70 1 -3 -14 3.20 0.70 0 -3 -14 4.90 0.90 -1 -3 -14 24.80 1.60 -13 4 14 22.00 1.40 -12 4 14 2.30 0.70 -11 4 14 27.20 1.40 9 -4 -14 6.30 0.80 8 -4 -14 49.99 1.90 7 -4 -14 26.90 1.40 6 -4 -14 15.90 1.20 5 -4 -14 3.90 0.70 4 -4 -14 9.80 1.10 3 -4 -14 0.10 0.60 2 -4 -14 -0.60 0.60 1 -4 -14 75.09 2.60 0 -4 -14 1.70 0.70 -1 -4 -14 8.40 1.10 -12 5 14 70.19 2.20 -11 5 14 19.40 1.20 10 -5 -14 4.20 0.70 9 -5 -14 22.90 1.30 8 -5 -14 5.40 0.80 7 -5 -14 10.80 1.10 6 -5 -14 21.00 1.40 5 -5 -14 11.60 1.20 4 -5 -14 -0.40 0.50 3 -5 -14 -0.30 0.60 2 -5 -14 27.20 1.70 1 -5 -14 7.10 1.00 0 -5 -14 12.80 1.40 -1 -5 -14 -0.20 0.60 -12 6 14 31.10 1.50 10 -6 -14 20.20 1.30 9 -6 -14 36.00 1.60 8 -6 -14 21.10 1.40 7 -6 -14 4.40 0.80 6 -6 -14 43.90 1.90 5 -6 -14 36.50 1.80 4 -6 -14 1.50 0.70 3 -6 -14 2.30 0.80 2 -6 -14 1.60 0.70 1 -6 -14 3.60 0.90 0 -6 -14 11.00 1.30 10 -7 -14 2.60 0.70 9 -7 -14 21.40 1.40 8 -7 -14 3.80 0.80 7 -7 -14 7.20 1.00 6 -7 -14 31.70 1.70 5 -7 -14 1.50 0.70 4 -7 -14 0.10 0.70 3 -7 -14 61.59 2.50 2 -7 -14 39.30 2.10 1 -7 -14 10.40 1.20 10 -8 -14 -0.10 0.50 9 -8 -14 1.20 0.60 8 -8 -14 40.00 1.90 7 -8 -14 8.60 1.10 6 -8 -14 32.30 1.80 5 -8 -14 0.20 0.70 4 -8 -14 0.50 0.70 3 -8 -14 7.40 1.10 8 -9 -14 1.10 1.10 7 -9 -14 12.00 1.40 6 -9 -14 147.29 4.90 -9 -7 15 17.00 1.40 -8 -7 15 96.19 2.90 -7 -7 15 39.10 1.80 5 7 -15 0.20 0.50 -10 -6 15 39.60 1.90 -9 -6 15 1.20 0.60 -8 -6 15 0.60 0.60 -7 -6 15 10.40 1.20 -6 -6 15 18.20 1.80 5 6 -15 0.50 0.50 4 6 -15 58.39 2.30 3 6 -15 4.00 0.90 -11 -5 15 32.80 2.30 -10 -5 15 2.60 0.70 -9 -5 15 22.50 1.50 -8 -5 15 4.70 0.80 -7 -5 15 89.89 2.70 -6 -5 15 7.90 0.90 5 5 -15 70.09 2.40 4 5 -15 0.60 0.60 3 5 -15 12.60 1.30 2 5 -15 13.40 1.40 -11 -4 15 2.90 0.80 -10 -4 15 0.80 0.60 -9 -4 15 43.90 1.90 -8 -4 15 0.20 0.60 -7 -4 15 0.10 0.50 -6 -4 15 0.30 0.50 5 4 -15 25.30 1.40 -5 -4 15 25.20 1.30 4 4 -15 23.60 1.50 3 4 -15 4.30 0.80 2 4 -15 31.90 1.90 1 4 -15 3.70 1.00 -12 -3 15 5.60 1.20 -11 -3 15 0.80 0.60 -10 -3 15 22.40 1.50 -9 -3 15 1.30 0.60 -8 -3 15 22.60 1.30 -7 -3 15 7.20 0.90 -6 -3 15 44.10 1.70 5 3 -15 0.20 0.50 -5 -3 15 0.40 0.40 4 3 -15 1.80 0.60 -4 -3 15 1.60 0.50 3 3 -15 85.59 2.80 2 3 -15 1.70 0.70 1 3 -15 8.20 1.20 0 3 -15 2.60 1.00 -12 -2 15 0.50 0.70 -11 -2 15 2.90 0.80 -10 -2 15 84.99 2.60 -9 -2 15 64.49 2.20 -8 -2 15 0.50 0.50 -7 -2 15 34.40 1.50 -6 -2 15 120.39 2.90 5 2 -15 0.40 0.50 -5 -2 15 0.20 0.40 4 2 -15 1.00 0.50 -4 -2 15 0.30 0.40 3 2 -15 0.60 0.60 -3 -2 15 0.60 0.50 2 2 -15 59.49 2.40 1 2 -15 61.09 2.50 0 2 -15 0.30 0.70 -12 -1 15 37.20 1.90 -11 -1 15 1.80 0.70 -10 -1 15 39.20 1.80 -9 -1 15 11.30 1.10 -8 -1 15 4.90 0.70 -7 -1 15 0.90 0.50 -6 -1 15 93.49 2.40 5 1 -15 1.20 0.50 -5 -1 15 0.50 0.40 4 1 -15 2.80 0.60 3 1 -15 44.50 1.90 3 1 -15 47.90 1.60 2 1 -15 0.20 0.60 1 1 -15 7.40 1.10 0 1 -15 22.80 1.70 -12 0 15 -0.80 0.60 -11 0 15 33.90 1.70 -10 0 15 -0.10 0.50 -9 0 15 72.59 2.20 -8 0 15 0.00 0.40 -7 0 15 0.50 0.40 5 0 -15 19.70 1.10 4 0 -15 -0.10 0.40 4 0 -15 0.30 0.40 3 0 -15 4.20 0.80 3 0 -15 4.00 0.70 2 0 -15 0.00 0.50 2 0 -15 0.40 0.60 1 0 -15 81.79 2.80 0 0 -15 0.10 0.70 -1 0 -15 40.80 2.20 -12 1 15 38.10 1.80 -11 1 15 0.80 0.60 -10 1 15 40.80 1.70 -9 1 15 12.40 1.10 -8 1 15 5.00 0.70 6 -1 -15 97.39 2.60 5 -1 -15 0.70 0.50 4 -1 -15 1.80 0.50 4 -1 -15 1.70 0.60 3 -1 -15 45.60 1.70 3 -1 -15 45.70 1.80 2 -1 -15 -0.10 0.50 2 -1 -15 -0.60 0.40 1 -1 -15 5.90 0.90 1 -1 -15 7.10 0.90 0 -1 -15 25.90 1.70 -12 2 15 -0.90 0.50 -11 2 15 2.60 0.70 -10 2 15 91.59 2.60 -9 2 15 65.99 2.10 7 -2 -15 38.60 1.60 6 -2 -15 125.59 3.10 5 -2 -15 0.10 0.50 4 -2 -15 -0.10 0.50 4 -2 -15 1.30 0.50 3 -2 -15 0.90 0.50 3 -2 -15 0.60 0.60 2 -2 -15 55.19 2.00 1 -2 -15 61.09 2.20 -12 3 15 6.20 0.90 -11 3 15 0.70 0.60 -10 3 15 23.00 1.30 8 -3 -15 22.10 1.30 7 -3 -15 7.90 0.90 6 -3 -15 42.00 1.80 5 -3 -15 0.10 0.50 4 -3 -15 0.70 0.60 3 -3 -15 87.39 2.70 2 -3 -15 1.10 0.60 1 -3 -15 9.20 1.00 0 -3 -15 2.60 0.80 -12 4 15 69.99 2.40 -11 4 15 3.60 0.70 9 -4 -15 44.30 1.80 8 -4 -15 -0.70 0.50 7 -4 -15 -0.10 0.50 6 -4 -15 0.40 0.60 5 -4 -15 26.40 1.50 4 -4 -15 20.50 1.40 3 -4 -15 3.20 0.80 2 -4 -15 32.60 1.70 1 -4 -15 2.50 0.80 0 -4 -15 3.40 0.80 -11 5 15 29.40 1.50 10 -5 -15 2.60 0.70 9 -5 -15 24.60 1.40 8 -5 -15 5.00 0.80 7 -5 -15 91.19 2.70 6 -5 -15 9.20 1.10 5 -5 -15 69.59 2.50 4 -5 -15 1.00 0.60 3 -5 -15 9.10 1.10 2 -5 -15 10.70 1.20 1 -5 -15 0.70 0.70 10 -6 -15 40.80 1.80 9 -6 -15 1.10 0.60 8 -6 -15 0.60 0.60 7 -6 -15 9.40 1.10 6 -6 -15 16.90 1.40 5 -6 -15 -0.60 0.60 4 -6 -15 51.69 2.30 3 -6 -15 4.70 1.00 2 -6 -15 7.40 1.40 8 -7 -15 94.79 3.10 7 -7 -15 40.60 2.00 6 -7 -15 18.00 1.50 5 -7 -15 0.50 0.70 -7 -6 16 0.00 0.60 -9 -5 16 0.60 0.60 -8 -5 16 1.80 0.70 -7 -5 16 8.10 1.00 -10 -4 16 30.90 2.00 -9 -4 16 5.00 0.90 -8 -4 16 9.00 1.00 -7 -4 16 81.09 2.50 -6 -4 16 85.29 2.50 5 4 -16 2.00 0.60 4 4 -16 0.40 0.60 -10 -3 16 13.10 1.30 -9 -3 16 3.60 0.80 -8 -3 16 24.00 1.40 -7 -3 16 1.10 0.60 -6 -3 16 9.80 1.10 5 3 -16 0.80 0.60 -5 -3 16 0.60 0.50 4 3 -16 0.50 0.50 3 3 -16 56.09 2.30 -10 -2 16 50.39 2.10 -9 -2 16 1.00 0.60 -8 -2 16 5.40 0.80 -7 -2 16 -0.20 0.50 -6 -2 16 8.60 1.00 5 2 -16 31.20 1.60 -5 -2 16 30.80 1.40 4 2 -16 1.60 0.60 -4 -2 16 1.10 0.50 3 2 -16 41.40 2.00 2 2 -16 19.50 1.50 -11 -1 16 56.99 2.80 -10 -1 16 -0.10 0.60 -9 -1 16 29.70 1.60 -8 -1 16 43.60 1.80 -7 -1 16 0.60 0.50 -6 -1 16 0.30 0.50 5 1 -16 12.20 1.10 -5 -1 16 11.60 1.00 4 1 -16 2.50 0.60 3 1 -16 3.00 0.70 2 1 -16 13.00 1.30 -11 0 16 0.10 0.60 -10 0 16 -0.10 0.50 -9 0 16 -0.30 0.50 -8 0 16 99.69 2.70 -7 0 16 0.00 0.40 4 0 -16 141.49 3.30 4 0 -16 145.69 3.60 3 0 -16 0.20 0.50 3 0 -16 -0.40 0.50 2 0 -16 0.40 0.60 -11 1 16 56.99 2.50 -10 1 16 -0.50 0.50 -9 1 16 29.10 1.50 -8 1 16 42.00 1.70 6 -1 -16 0.00 0.50 5 -1 -16 10.80 1.10 4 -1 -16 2.50 0.60 4 -1 -16 3.00 0.60 3 -1 -16 2.10 0.60 3 -1 -16 3.20 0.70 2 -1 -16 12.30 1.20 2 -1 -16 10.50 1.10 -10 2 16 56.59 2.00 -9 2 16 0.00 0.50 7 -2 -16 0.10 0.50 6 -2 -16 8.50 1.00 5 -2 -16 32.00 1.50 4 -2 -16 0.80 0.60 3 -2 -16 40.10 1.80 2 -2 -16 19.40 1.40 -10 3 16 13.10 1.20 8 -3 -16 25.40 1.40 7 -3 -16 0.30 0.60 6 -3 -16 11.30 1.20 5 -3 -16 0.70 0.60 4 -3 -16 0.20 0.60 3 -3 -16 50.79 2.10 2 -3 -16 0.20 0.60 9 -4 -16 7.30 1.00 8 -4 -16 11.60 1.20 7 -4 -16 88.59 2.70 6 -4 -16 87.09 2.70 5 -4 -16 0.90 0.60 4 -4 -16 0.00 0.60 3 -4 -16 0.10 0.60 7 -5 -16 10.10 1.60 6 -5 -16 43.50 2.50 -7 -3 17 13.40 1.20 -8 -2 17 33.40 1.70 -7 -2 17 4.80 0.80 -6 -2 17 1.20 0.60 -5 -2 17 24.40 1.40 -8 -1 17 0.70 0.60 -7 -1 17 53.79 2.00 -6 -1 17 3.60 0.70 -5 -1 17 9.40 1.00 -8 0 17 -0.10 0.60 -7 0 17 34.60 1.60 -6 0 17 -0.40 0.50 5 -1 -17 8.00 0.90 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 63551 _shelx_res_file ; TITL m5cg CELL 0.71073 12.2889 12.3034 13.3667 90.000 116.295 90.000 ZERR 4.000 0.0014 0.0014 0.0015 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C N O Cl H UNIT 76 8 12 8 72 OMIT -2 180.0 L.S. 20 ACTA BOND $H CONF HTAB FMAP 2 PLAN 20 SIZE 0.490 0.480 0.375 TEMP -100 WGHT 0.043000 0.603400 FVAR 0.43879 N1 2 0.529862 0.187062 0.648306 11.00000 0.02390 0.03369 = 0.03441 0.00866 0.01653 0.00156 C2 1 0.482138 0.138574 0.720470 11.00000 0.02619 0.04200 = 0.03284 0.01254 0.01346 -0.00147 AFIX 23 H2A 5 0.545148 0.140660 0.798902 11.00000 -1.20000 H2B 5 0.460937 0.061570 0.699329 11.00000 -1.20000 AFIX 0 C3 1 0.370785 0.199344 0.710330 11.00000 0.02528 0.04799 = 0.02409 0.00312 0.01194 -0.00416 AFIX 23 H3A 5 0.336045 0.162243 0.755337 11.00000 -1.20000 H3B 5 0.393904 0.273976 0.739830 11.00000 -1.20000 AFIX 0 N4 2 0.279499 0.204371 0.593494 11.00000 0.02430 0.04778 = 0.02390 0.00612 0.01351 0.00122 C5 1 0.325971 0.243378 0.516147 11.00000 0.03038 0.05748 = 0.03122 0.01539 0.01941 0.00802 AFIX 23 H5A 5 0.345694 0.321690 0.529222 11.00000 -1.20000 H5B 5 0.262899 0.234342 0.438365 11.00000 -1.20000 AFIX 0 C6 1 0.438843 0.180287 0.532716 11.00000 0.03135 0.04538 = 0.03316 0.00417 0.02080 0.00215 AFIX 23 H6A 5 0.417331 0.103219 0.512163 11.00000 -1.20000 H6B 5 0.472344 0.210271 0.483420 11.00000 -1.20000 AFIX 0 C11 1 0.645092 0.136907 0.665490 11.00000 0.02937 0.03327 = 0.05262 0.01287 0.02171 0.00615 AFIX 23 H11A 5 0.629519 0.062463 0.634138 11.00000 -1.20000 H11B 5 0.698842 0.131274 0.746508 11.00000 -1.20000 AFIX 0 O11 3 0.871138 0.400741 0.468554 11.00000 0.03893 0.04236 = 0.03781 0.00005 0.02654 -0.00308 C12 1 0.838669 0.502258 0.498981 11.00000 0.04991 0.03963 = 0.04517 -0.00212 0.03258 -0.00865 AFIX 23 H12A 5 0.774276 0.537505 0.432555 11.00000 -1.20000 H12B 5 0.910044 0.551111 0.529649 11.00000 -1.20000 AFIX 0 O13 3 0.796157 0.483037 0.580776 11.00000 0.05365 0.03001 = 0.05086 -0.00414 0.03884 -0.00658 C3A 1 0.775391 0.372639 0.576870 11.00000 0.02556 0.02920 = 0.03196 -0.00088 0.01532 0.00020 C14 1 0.719534 0.314966 0.628743 11.00000 0.03075 0.03283 = 0.03893 0.00160 0.02347 0.00361 AFIX 43 H14 5 0.689722 0.349787 0.675084 11.00000 -1.20000 AFIX 0 C15 1 0.708187 0.202289 0.610567 11.00000 0.02140 0.03189 = 0.03773 0.00622 0.01431 0.00507 C16 1 0.755226 0.153621 0.544361 11.00000 0.02500 0.02874 = 0.03783 -0.00083 0.01098 0.00462 AFIX 43 H16 5 0.747084 0.077250 0.533002 11.00000 -1.20000 AFIX 0 C17 1 0.814270 0.213557 0.493824 11.00000 0.02547 0.03859 = 0.02908 -0.00407 0.01203 0.00526 AFIX 43 H17 5 0.847924 0.179515 0.450085 11.00000 -1.20000 AFIX 0 C7A 1 0.821084 0.323142 0.510474 11.00000 0.01930 0.03793 = 0.02410 0.00040 0.01030 -0.00030 C47 1 0.159676 0.187976 0.557399 11.00000 0.02588 0.03358 = 0.02506 -0.00096 0.01367 0.00255 O47 3 0.085101 0.196477 0.459236 11.00000 0.02860 0.07429 = 0.02377 0.00312 0.01062 0.00212 C41 1 0.116561 0.155203 0.642641 11.00000 0.01859 0.03058 = 0.02260 -0.00020 0.00905 0.00110 C42 1 0.099142 0.229600 0.712380 11.00000 0.02323 0.02456 = 0.02328 0.00001 0.01049 -0.00242 CL42 4 0.139211 0.365083 0.712250 11.00000 0.04931 0.02548 = 0.03616 -0.00147 0.02471 -0.00753 C43 1 0.049209 0.199876 0.783126 11.00000 0.02456 0.03150 = 0.02370 -0.00134 0.01212 -0.00149 AFIX 43 H43 5 0.038447 0.251764 0.830623 11.00000 -1.20000 AFIX 0 C44 1 0.015494 0.092726 0.782719 11.00000 0.02115 0.03512 = 0.02610 0.00629 0.01011 -0.00215 CL44 4 -0.047707 0.054794 0.870792 11.00000 0.04308 0.05334 = 0.03968 0.00825 0.02503 -0.01166 C45 1 0.029897 0.016126 0.714078 11.00000 0.02759 0.02528 = 0.03606 0.00458 0.01052 -0.00129 AFIX 43 H45 5 0.005236 -0.057018 0.714296 11.00000 -1.20000 AFIX 0 C46 1 0.080949 0.047945 0.644952 11.00000 0.02737 0.02712 = 0.03114 -0.00247 0.01150 0.00389 AFIX 43 H46 5 0.091996 -0.004417 0.598017 11.00000 -1.20000 AFIX 0 HKLF 4 REM m5cg REM R1 = 0.0312 for 3545 Fo > 4sig(Fo) and 0.0363 for all 4054 data REM 235 parameters refined using 0 restraints END WGHT 0.0429 0.6033 REM Instructions for potential hydrogen bonds EQIV $1 x+1, y, z HTAB C11 Cl44_$1 EQIV $2 -x+1, -y+1, -z+1 HTAB C12 Cl42_$2 EQIV $3 -x+1/2, y+1/2, -z+3/2 HTAB C14 Cl44_$3 REM Highest difference peak 0.371, deepest hole -0.375, 1-sigma level 0.042 Q1 1 -0.0377 0.0038 0.8321 11.00000 0.05 0.37 Q2 1 0.1450 0.1720 0.6054 11.00000 0.05 0.34 Q3 1 0.7767 0.3432 0.5325 11.00000 0.05 0.29 Q4 1 0.0458 0.0561 0.7594 11.00000 0.05 0.26 Q5 1 0.3802 0.2045 0.5272 11.00000 0.05 0.25 Q6 1 0.0323 0.0410 0.6683 11.00000 0.05 0.25 Q7 1 0.1196 0.1885 0.6824 11.00000 0.05 0.24 Q8 1 0.0856 0.0235 0.7054 11.00000 0.05 0.24 Q9 1 0.6824 0.1728 0.6381 11.00000 0.05 0.23 Q10 1 0.3222 0.2083 0.6469 11.00000 0.05 0.23 Q11 1 0.4183 0.1601 0.7088 11.00000 0.05 0.23 Q12 1 0.0452 0.1387 0.7902 11.00000 0.05 0.23 Q13 1 0.5086 0.1688 0.6764 11.00000 0.05 0.23 Q14 1 0.2212 0.2136 0.5830 11.00000 0.05 0.23 Q15 1 0.1013 0.2029 0.7636 11.00000 0.05 0.22 Q16 1 0.7154 0.3468 0.5746 11.00000 0.05 0.22 Q17 1 0.7197 0.1833 0.5677 11.00000 0.05 0.22 Q18 1 0.5797 0.1619 0.6552 11.00000 0.05 0.21 Q19 1 0.1048 0.1000 0.6469 11.00000 0.05 0.21 Q20 1 0.7183 0.2515 0.6240 11.00000 0.05 0.21 ; _shelx_res_checksum 20592 _shelxl_version_number 2.014