data_116aim17_sq _audit_creation_date 2018-09-22 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2014/7' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C73 H64 B2 N O2 P4 Rh2, Al C16 F36 O4' _chemical_formula_sum 'C89 H64 Al B2 F36 N O6 P4 Rh2' _chemical_formula_weight 2305.71 _chemical_melting_point ? _chemical_oxdiff_formula 'Rh2 B1 P4 Al1 F36 C89 O6 H63 N1' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.2130 0.2455 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'B' 'B' 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Rh' 'Rh' 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 14.5138(2) _cell_length_b 18.5644(3) _cell_length_c 21.4620(3) _cell_angle_alpha 104.3850(10) _cell_angle_beta 102.6830(10) _cell_angle_gamma 107.5450(10) _cell_volume 5062.15(13) _cell_formula_units_Z 2 _cell_measurement_reflns_used 23761 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 75.2630 _cell_measurement_theta_min 3.9480 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 4.361 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71953 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.513 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 2300 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.03 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0477 _diffrn_reflns_av_unetI/netI 0.0473 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 59612 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.147 _diffrn_reflns_theta_min 3.988 _diffrn_ambient_temperature 150(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.4102 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -28.00 6.00 1.00 3.00 -- 42.41 -38.00 0.00 34 2 \w 102.00 128.00 1.00 3.00 -- 42.41 178.00 0.00 26 3 \w 57.00 87.00 1.00 3.00 -- 42.41 178.00 120.00 30 4 \w 100.00 129.00 1.00 3.00 -- 42.41 178.00-150.00 29 5 \w -87.00 -24.00 1.00 3.00 -- -42.41 -38.00 120.00 63 6 \w -89.00 -23.00 1.00 3.00 -- -42.41 -38.00 60.00 66 7 \w -112.00 -42.00 1.00 3.00 -- -42.41 -38.00-150.00 70 8 \w -126.00 -38.00 1.00 3.00 -- -42.41 178.00-150.00 88 9 \w 43.00 90.00 1.00 12.00 -- 111.00 -30.00-120.00 47 10 \w 79.00 177.00 1.00 12.00 -- 111.00 15.00 -90.00 98 11 \w 151.00 178.00 1.00 12.00 -- 111.00 45.00 -60.00 27 12 \w 145.00 172.00 1.00 12.00 -- 111.00 45.00-150.00 27 13 \w 94.00 177.00 1.00 12.00 -- 111.00 45.00-180.00 83 14 \w 97.00 131.00 1.00 12.00 -- 111.00 45.00 -60.00 34 15 \w 52.00 97.00 1.00 12.00 -- 111.00 -45.00 30.00 45 16 \w 94.00 132.00 1.00 12.00 -- 111.00 -77.00 60.00 38 17 \w 81.00 126.00 1.00 12.00 -- 111.00-138.00 -49.00 45 18 \w 73.00 108.00 1.00 12.00 -- 111.00 -95.00 -90.00 35 19 \w 62.00 89.00 1.00 12.00 -- 111.00 -95.00-120.00 27 20 \w 65.00 108.00 1.00 12.00 -- 111.00-125.00-120.00 43 21 \w 66.00 121.00 1.00 12.00 -- 111.00-125.00 0.00 55 22 \w 68.00 119.00 1.00 12.00 -- 111.00-125.00 90.00 51 23 \w 72.00 98.00 1.00 12.00 -- 111.00 -95.00 150.00 26 24 \w 64.00 100.00 1.00 12.00 -- 111.00 -95.00 90.00 36 25 \w 56.00 82.00 1.00 12.00 -- 111.00 -77.00 60.00 26 26 \w 47.00 98.00 1.00 12.00 -- 111.00 -45.00 90.00 51 27 \w 149.00 178.00 1.00 12.00 -- 111.00 30.00 150.00 29 28 \w 138.00 178.00 1.00 12.00 -- 111.00 30.00 120.00 40 29 \w 90.00 115.00 1.00 12.00 -- 111.00 30.00 150.00 25 30 \w 91.00 116.00 1.00 12.00 -- 111.00 30.00 120.00 25 31 \w 49.00 76.00 1.00 12.00 -- 111.00 -45.00 60.00 27 32 \w 41.00 68.00 1.00 12.00 -- 111.00 -30.00 0.00 27 33 \w 53.00 80.00 1.00 12.00 -- 111.00 -45.00 -30.00 27 34 \w 48.00 90.00 1.00 12.00 -- 111.00 -95.00 0.00 42 35 \w 44.00 110.00 1.00 12.00 -- 111.00-125.00 60.00 66 36 \w 40.00 80.00 1.00 12.00 -- 111.00-125.00 120.00 40 37 \w 40.00 67.00 1.00 12.00 -- 111.00-125.00 30.00 27 38 \w 31.00 57.00 1.00 12.00 -- 111.00 -95.00 60.00 26 39 \w 42.00 98.00 1.00 12.00 -- 111.00 -45.00 150.00 56 40 \w 43.00 135.00 1.00 12.00 -- 111.00 -61.00-120.00 92 41 \w 45.00 121.00 1.00 12.00 -- 111.00-125.00-180.00 76 42 \w 42.00 91.00 1.00 12.00 -- 111.00 -30.00-180.00 49 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0062887000 _diffrn_orient_matrix_UB_12 0.0390317000 _diffrn_orient_matrix_UB_13 0.0738816000 _diffrn_orient_matrix_UB_21 -0.1007725000 _diffrn_orient_matrix_UB_22 0.0112976000 _diffrn_orient_matrix_UB_23 -0.0255150000 _diffrn_orient_matrix_UB_31 -0.0600044000 _diffrn_orient_matrix_UB_32 -0.0830799000 _diffrn_orient_matrix_UB_33 0.0018024000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 16821 _reflns_number_total 20908 _reflns_odcompleteness_completeness 99.75 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 74.33 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. Structure factors included contributions from the .fab file. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 1.756 _refine_diff_density_min -0.938 _refine_diff_density_rms 0.111 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.027 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 1761 _refine_ls_number_reflns 20908 _refine_ls_number_restraints 2901 _refine_ls_R_factor_all 0.0717 _refine_ls_R_factor_gt 0.0579 _refine_ls_restrained_S_all 1.240 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1103P)^2^+7.3798P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1577 _refine_ls_wR_factor_ref 0.1730 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances N1A-C73A \\sim N1-C73 with sigma of 0.02 N1A-B1 \\sim N1-B1 \\sim N1A-B2 \\sim N1-B2 with sigma of 0.02 C82-C83 \\sim C82-C83A \\sim C82-C85 \\sim C82-C85A \\sim C82-C84 \\sim C82-C84A with sigma of 0.02 C83-F19 \\sim C83-F21 \\sim C83-F20 \\sim C83A-F20A \\sim C83A-F19A \\sim C83A-F21A \\sim C84-F23 ~ C84-F24 \\sim C84-F22 \\sim C84A-F23A \\sim C84A-F24A \\sim C84A-F22A \\sim C85-F27 \\sim C85-F26 ~ C85-F25 \\sim C85A-F25A \\sim C85A-F27A \\sim C85A-F26A with sigma of 0.02 F19-F21 \\sim F19-F20 \\sim F21-F20 \\sim F20A-F19A \\sim F20A-F21A \\sim F19A-F21A \\sim F23-F24 ~ F24-F22 \\sim F22-F23 \\sim F23A-F24A \\sim F24A-F22A \\sim F23A-F22A \\sim F25-F27 \\sim F25-F26 ~ F27-F26 \\sim F25A-F27A \\sim F25A-F26A \\sim F27A-F26A with sigma of 0.04 O5-C83 \\sim O5-C83A \\sim O5-C85 \\sim O5-C85A \\sim O5-C84 \\sim O5-C84A with sigma of 0.04 C83-C84 \\sim C84-C85 \\sim C85-C83 \\sim C83A-C84A \\sim C84A-C85A \\sim C85A-C83A with sigma of 0.04 C86A-C89A \\sim C86A-C87A \\sim C86A-C88A \\sim C86-C87 \\sim C86-C88 \\sim C86-C89 with sigma of 0.02 C89A-F34A \\sim C89A-F36A \\sim C89A-F35A \\sim C87-F28 \\sim C87-F29 \\sim C87-F30 \\sim C87A-F29A ~ C87A-F28A \\sim C87A-F30A \\sim C88-C86A \\sim C88-F32 \\sim C88-F33 \\sim C88-F31 \\sim C88A-F32A ~ C88A-F31A \\sim C88A-F33A \\sim C89-F34 \\sim C89-F35 \\sim C89-F36 with sigma of 0.02 F34A-F36A \\sim F34A-F35A \\sim F36A-F35A \\sim F28-F29 \\sim F28-F30 \\sim F29-F30 \\sim F29A-F28A ~ F29A-F30A \\sim F28A-F30A \\sim F32-F33 \\sim F32-F31 \\sim F33-F31 \\sim F32A-F31A \\sim F32A-F33A ~ F31A-F33A \\sim F34-F35 \\sim F34-F36 \\sim F35-F36 with sigma of 0.04 O6A-C87A \\sim O6A-C88A \\sim C89A-O6A \\sim O6-C88 \\sim O6-C89 \\sim C87-O6 with sigma of 0.04 C89A-C87A \\sim C87A-C88A \\sim C88A-C89A \\sim C87-C88 \\sim C88-C89 \\sim C89-C87 with sigma of 0.04 C74-C77 \\sim C74-C76 \\sim C74-C75 \\sim C74-C77A \\sim C74-C75A \\sim C74-C76A with sigma of 0.02 C75-F3 \\sim C75-F1 \\sim C75-F2 \\sim C75A-F3A \\sim C75A-F2A \\sim C75A-F1A \\sim C76-F5 \\sim C76-F6 ~ C76-F4 \\sim C76A-F5A \\sim C76A-F6A \\sim C76A-F4A \\sim C77-F8 \\sim C77-F9 \\sim C77-F7 \\sim C77A-F9A \\sim C77A-F8A \\sim C77A-F7A with sigma of 0.02 F3-F2 \\sim F3-F1 \\sim F2-F1 \\sim F3A-F2A \\sim F3A-F1A \\sim F2A-F1A \\sim F5-F6 \\sim F5-F4 \\sim F6-F4 ~ F5A-F6A \\sim F5A-F4A \\sim F6A-F4A \\sim F8-F9 \\sim F8-F7 \\sim F9-F7 \\sim F9A-F8A \\sim F9A-F7A \\sim F8A- F7A with sigma of 0.04 O3-C77 \\sim O3-C76 \\sim O3-C75 \\sim O3-C77A \\sim O3-C75A \\sim O3-C76A with sigma of 0.04 C75-C76 \\sim C76-C77 \\sim C77-C75 \\sim C75A-C76A \\sim C76A-C77A \\sim C77A-C75A with sigma of 0.04 C78-C81 \\sim C78-C80 \\sim C78-C79 \\sim C78-C81A \\sim C78-C80A \\sim C78-C79A with sigma of 0.02 C79-F10 \\sim C79-F12 \\sim C79-F11 \\sim C79A-F12A \\sim C79A-F10A \\sim C79A-F11A \\sim C80-F15 ~ C80-F13 \\sim C80-F14 \\sim C80A-F13A \\sim C80A-F15A \\sim C80A-F14A \\sim C81-F16 \\sim C81-F18 ~ C81-F17 \\sim C81A-F17A \\sim C81A-F16A \\sim C81A-F18A with sigma of 0.02 F10-F12 \\sim F10-F11 \\sim F12-F11 \\sim F12A-F10A \\sim F12A-F11A \\sim F10A-F11A \\sim F15-F13 ~ F15-F14 \\sim F13-F14 \\sim F13A-F15A \\sim F13A-F14A \\sim F15A-F14A \\sim F16-F18 \\sim F16-F17 ~ F18-F17 \\sim F17A-F16A \\sim F17A-F18A \\sim F16A-F18A with sigma of 0.04 O4-C81 \\sim O4-C80 \\sim O4-C79 \\sim O4-C81A \\sim O4-C80A \\sim O4-C79A with sigma of 0.04 C79-C80 \\sim C80-C81 \\sim C81-C79 \\sim C79A-C80A \\sim C80A-C81A \\sim C81A-C79A with sigma of 0.04 Al1-O3 \\sim Al1-O4 \\sim Al1-O5 \\sim Al1-O6A \\sim Al1-O6 with sigma of 0.02 O6-C86 \\sim O6A-C86A with sigma of 0.02 3. Uiso/Uaniso restraints and constraints N1A \\sim C73A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 N1 \\sim C73: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 C82 \\sim C83 \\sim C84 \\sim C85 \\sim F19 \\sim F20 \\sim F21 \\sim F22 \\sim F23 \\sim F24 \\sim F25 \\sim F26 \\sim F27: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 C82 \\sim C83A \\sim C84A \\sim C85A \\sim F19A \\sim F20A \\sim F21A \\sim F22A \\sim F23A \\sim F24A \\sim F25A \\sim F26A \\sim F27A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 Al1 \\sim O6 \\sim C86A \\sim C89A \\sim C87A \\sim C88A \\sim F35A \\sim F34A \\sim F36A \\sim F28A \\sim F29A \\sim F30A \\sim F31A \\sim F33A \\sim F32A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 Al1 \\sim O6 \\sim C86 \\sim C87 \\sim C88 \\sim C89 \\sim F28 \\sim F30 \\sim F29 \\sim F32 \\sim F33 \\sim F31 \\sim F34 \\sim F36 \\sim F35: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 C74 \\sim C75 \\sim C76 \\sim C77 \\sim F1 \\sim F2 \\sim F3 \\sim F4 \\sim F5 \\sim F6 \\sim F7 \\sim F8 \\sim F9: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 C74 \\sim C75A \\sim C76A \\sim C77A \\sim F1A \\sim F2A \\sim F3A \\sim F4A \\sim F5A \\sim F6A \\sim F7A \\sim F8A \\sim F9A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 C78 \\sim C79 \\sim C80 \\sim C81 \\sim F10 \\sim F11 \\sim F12 \\sim F13 \\sim F14 \\sim F15 \\sim F16 \\sim F17 \\sim F18: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 C78 \\sim C79A \\sim C80A \\sim C81A \\sim F10A \\sim F11A \\sim F12A \\sim F13A \\sim F14A \\sim F15A \\sim F16A \\sim F17A \\sim F18A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Rigid body (RIGU) restrains N1, C73 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 N1A, C73A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C82, C83, C84, C85, F19, F20, F21, F22, F23, F24, F25, F26, F27 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C82, C83A, C84A, C85A, F19A, F20A, F21A, F22A, F23A, F24A, F25A, F26A, F27A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 Al1, O6A, C86A, C89A, C87A, C88A, F35A, F34A, F36A, F28A, F29A, F30A, F31A, F33A, F32A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 Al1, O6, C86A, C87, C88, C89, F28, F30, F29, F32, F33, F31, F34, F36, F35 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C74, C75, C76, C77, F1, F2, F3, F4, F5, F6, F7, F8, F9 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C74, C75A, C76A, C77A, F1A, F2A, F3A, F4A, F5A, F6A, F7A, F8A, F9A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C78, C79, C80, C81, F10, F11, F12, F13, F14, F15, F16, F17, F18 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C78, C79A, C80A, C81A, F10A, F11A, F12A, F13A, F14A, F15A, F16A, F17A, F18A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Sof(C73A)=Sof(H73D)=Sof(H73E)=Sof(H73F)=Sof(N1A)=Sof(H1AA)=1-FVAR(1) Sof(N1)=Sof(H1)=Sof(C73)=Sof(H73A)=Sof(H73B)=Sof(H73C)=FVAR(1) Sof(F25A)=Sof(F27A)=Sof(F26A)=Sof(F23A)=Sof(C84A)=Sof(F24A)=Sof(F22A)= Sof(F20A)=Sof(C83A)=Sof(F19A)=Sof(F21A)=Sof(C85A)=1-FVAR(2) Sof(F19)=Sof(F21)=Sof(F27)=Sof(F20)=Sof(F23)=Sof(F26)=Sof(F24)=Sof(F25)= Sof(F22)=Sof(C83)=Sof(C84)=Sof(C85)=FVAR(2) Sof(O6A)=Sof(C86A)=Sof(C89A)=Sof(F34A)=Sof(F36A)=Sof(F35A)=Sof(C87A)= Sof(F29A)=Sof(F28A)=Sof(F30A)=Sof(C88A)=Sof(F32A)=Sof(F31A)=Sof(F33A)=1-FVAR(3) Sof(F28)=Sof(F29)=Sof(C87)=Sof(F30)=Sof(F34)=Sof(F32)=Sof(C88)=Sof(F33)= Sof(F31)=Sof(F35)=Sof(C89)=Sof(F36)=Sof(O6)=Sof(C86)=FVAR(3) Sof(F9A)=Sof(C77A)=Sof(F8A)=Sof(F7A)=Sof(F3A)=Sof(C75A)=Sof(F2A)=Sof(F1A)= Sof(C76A)=Sof(F5A)=Sof(F6A)=Sof(F4A)=1-FVAR(4) Sof(F5)=Sof(F3)=Sof(F6)=Sof(F8)=Sof(F1)=Sof(F9)=Sof(F7)=Sof(F2)=Sof(C77)= Sof(C76)=Sof(F4)=Sof(C75)=FVAR(4) Sof(F17A)=Sof(C81A)=Sof(F16A)=Sof(F18A)=Sof(C80A)=Sof(F13A)=Sof(F15A)= Sof(F14A)=Sof(F12A)=Sof(C79A)=Sof(F10A)=Sof(F11A)=1-FVAR(5) Sof(F16)=Sof(F15)=Sof(F13)=Sof(F18)=Sof(F17)=Sof(F10)=Sof(F12)=Sof(F11)= Sof(F14)=Sof(C81)=Sof(C80)=Sof(C79)=FVAR(5) 6.a Ternary CH refined with riding coordinates: N1(H1), N1A(H1AA) 6.b Aromatic/amide H refined with riding coordinates: C48(H48), C23(H23), C42(H42), C40(H40), C47(H47), C12(H12), C50(H50), C22(H22), C20(H20), C39(H39), C16(H16), C41(H41), C44(H44), C6(H6), C38(H38), C56(H56), C29(H29), C32(H32), C17(H17), C8(H8), C59(H59), C10(H10), C21(H21), C30(H30), C26(H26), C28(H28), C15(H15), C33(H33), C58(H58), C57(H57), C46(H46), C11(H11), C27(H27), C53(H53), C5(H5), C72(H72), C14(H14), C66(H66), C9(H9), C62(H62), C2(H2), C68(H68), C52(H52), C51(H51), C45(H45), C4(H4), C64(H64), C71(H71), C65(H65), C69(H69), C3(H3), C63(H63), C70(H70), C36(H36), C35(H35), C34(H34) 6.c Idealised Me refined as rotating group: C73(H73A,H73B,H73C), C73A(H73D,H73E,H73F) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh2 Rh 0.60676(2) 0.18917(2) 0.31851(2) 0.02460(9) Uani 1 1 d . . . . . Rh1 Rh 0.76460(2) 0.16336(2) 0.38273(2) 0.02666(9) Uani 1 1 d . . . . . P2 P 0.86404(7) 0.29566(6) 0.43862(5) 0.02692(19) Uani 1 1 d . . . . . P3 P 0.63704(7) 0.15681(6) 0.21706(5) 0.02463(18) Uani 1 1 d . . . . . P1 P 0.86518(8) 0.10334(6) 0.43303(5) 0.0305(2) Uani 1 1 d . . . . . P4 P 0.45087(8) 0.20272(7) 0.28055(5) 0.0317(2) Uani 1 1 d . . . . . Al1 Al 0.37751(11) 0.62959(9) 0.18604(7) 0.0382(3) Uani 1 1 d D U . . . O2 O 0.5888(2) 0.30579(18) 0.23073(14) 0.0321(6) Uani 1 1 d . . . . . O1 O 1.0057(2) 0.21674(18) 0.39345(15) 0.0331(6) Uani 1 1 d . . . . . C19 C 1.0196(3) 0.2883(3) 0.3807(2) 0.0323(8) Uani 1 1 d . . . . . C24 C 0.9582(3) 0.3316(2) 0.39703(19) 0.0301(8) Uani 1 1 d . . . . . C7 C 0.8758(3) 0.0202(2) 0.3719(2) 0.0321(8) Uani 1 1 d . . . . . C37 C 0.7202(3) 0.1003(2) 0.2094(2) 0.0289(7) Uani 1 1 d . . . . . C48 C 0.4551(3) 0.0299(3) 0.1372(2) 0.0351(9) Uani 1 1 d . . . . . H48 H 0.4611 0.0149 0.1767 0.042 Uiso 1 1 calc R . . . . C23 C 0.9698(3) 0.3995(3) 0.3775(2) 0.0357(9) Uani 1 1 d . . . . . H23 H 0.9313 0.4311 0.3889 0.043 Uiso 1 1 calc R . . . . C43 C 0.5298(3) 0.0986(2) 0.13854(19) 0.0284(7) Uani 1 1 d . . . . . O3 O 0.4745(4) 0.6002(3) 0.1719(3) 0.0735(13) Uani 1 1 d D . . . . C31 C 0.9414(3) 0.3315(2) 0.5286(2) 0.0307(8) Uani 1 1 d . . . . . C49 C 0.7041(3) 0.2460(2) 0.1982(2) 0.0298(8) Uani 1 1 d . . . . . C54 C 0.6724(3) 0.3104(2) 0.2081(2) 0.0310(8) Uani 1 1 d . . . . . C42 C 0.6896(3) 0.0265(3) 0.1584(2) 0.0346(9) Uani 1 1 d . . . . . H42 H 0.6218 0.0021 0.1279 0.042 Uiso 1 1 calc R . . . . C40 C 0.8568(4) 0.0233(3) 0.1951(2) 0.0395(10) Uani 1 1 d . . . . . H40 H 0.9038 -0.0019 0.1892 0.047 Uiso 1 1 calc R . . . . C47 C 0.3726(4) -0.0166(3) 0.0798(3) 0.0438(10) Uani 1 1 d . . . . . H47 H 0.3222 -0.0634 0.0797 0.053 Uiso 1 1 calc R . . . . C25 C 0.7985(3) 0.3666(2) 0.4410(2) 0.0296(8) Uani 1 1 d . . . . . N1 N 0.5866(7) 0.0814(6) 0.4006(5) 0.042(3) Uani 0.606(13) 1 d D U P A 1 H1 H 0.6252 0.0530 0.4226 0.051 Uiso 0.606(13) 1 calc R . P A 1 C1 C 0.8184(3) 0.0516(3) 0.4889(2) 0.0368(9) Uani 1 1 d . . . . . C12 C 0.7873(4) -0.0395(3) 0.3229(2) 0.0388(9) Uani 1 1 d . . . . . H12 H 0.7237 -0.0335 0.3188 0.047 Uiso 1 1 calc R . . . . C50 C 0.7884(4) 0.2534(3) 0.1752(2) 0.0399(10) Uani 1 1 d . . . . . H50 H 0.8105 0.2097 0.1664 0.048 Uiso 1 1 calc R . . . . C22 C 1.0359(4) 0.4216(3) 0.3419(2) 0.0425(10) Uani 1 1 d . . . . . H22 H 1.0413 0.4673 0.3284 0.051 Uiso 1 1 calc R . . . . C20 C 1.0858(4) 0.3104(3) 0.3455(2) 0.0413(10) Uani 1 1 d . . . . . H20 H 1.1258 0.2800 0.3347 0.050 Uiso 1 1 calc R . . . . C55 C 0.4929(3) 0.2682(3) 0.1816(2) 0.0316(8) Uani 1 1 d . . . . . C39 C 0.8872(3) 0.0953(3) 0.2471(2) 0.0369(9) Uani 1 1 d . . . . . H39 H 0.9547 0.1186 0.2779 0.044 Uiso 1 1 calc R . . . . C16 C 1.2009(4) 0.2682(3) 0.5561(3) 0.0460(11) Uani 1 1 d . . . . . H16 H 1.2694 0.3032 0.5811 0.055 Uiso 1 1 calc R . . . . C18 C 1.0547(3) 0.2189(3) 0.4576(2) 0.0326(8) Uani 1 1 d . . . . . C41 C 0.7579(4) -0.0115(3) 0.1519(2) 0.0407(10) Uani 1 1 d . . . . . H41 H 0.7361 -0.0619 0.1172 0.049 Uiso 1 1 calc R . . . . O4 O 0.3572(5) 0.6853(4) 0.1368(3) 0.0887(18) Uani 1 1 d D . . . . C44 C 0.5220(4) 0.1190(3) 0.0802(2) 0.0362(9) Uani 1 1 d . . . . . H44 H 0.5735 0.1645 0.0795 0.043 Uiso 1 1 calc R . . . . C6 C 0.8111(4) -0.0264(3) 0.4831(2) 0.0407(10) Uani 1 1 d . . . . . H6 H 0.8334 -0.0540 0.4497 0.049 Uiso 1 1 calc R . . . . C38 C 0.8197(3) 0.1336(3) 0.2546(2) 0.0318(8) Uani 1 1 d . . . . . H38 H 0.8412 0.1828 0.2906 0.038 Uiso 1 1 calc R . . . . C56 C 0.4740(4) 0.2840(3) 0.1217(2) 0.0392(9) Uani 1 1 d . . . . . H56 H 0.5267 0.3201 0.1122 0.047 Uiso 1 1 calc R . . . . C29 C 0.6845(4) 0.4156(3) 0.3792(2) 0.0367(9) Uani 1 1 d . . . . . H29 H 0.6427 0.4134 0.3374 0.044 Uiso 1 1 calc R . . . . C32 C 0.8943(4) 0.3058(3) 0.5738(2) 0.0398(10) Uani 1 1 d . . . . . H32 H 0.8257 0.2686 0.5573 0.048 Uiso 1 1 calc R . . . . C17 C 1.1549(4) 0.2695(3) 0.4925(2) 0.0396(9) Uani 1 1 d . . . . . H17 H 1.1918 0.3047 0.4734 0.047 Uiso 1 1 calc R . . . . C67 C 0.3346(3) 0.1213(3) 0.2728(2) 0.0408(10) Uani 1 1 d . . . . . C60 C 0.4166(3) 0.2168(3) 0.1982(2) 0.0322(8) Uani 1 1 d . . . . . O5 O 0.4160(5) 0.6840(3) 0.2706(2) 0.0814(15) Uani 1 1 d D . . . . C8 C 0.9680(4) 0.0107(3) 0.3757(2) 0.0374(9) Uani 1 1 d . . . . . H8 H 1.0293 0.0510 0.4080 0.045 Uiso 1 1 calc R . . . . C59 C 0.3195(4) 0.1791(3) 0.1503(2) 0.0429(10) Uani 1 1 d . . . . . H59 H 0.2665 0.1432 0.1597 0.051 Uiso 1 1 calc R . . . . C10 C 0.8826(5) -0.1165(3) 0.2850(3) 0.0491(12) Uani 1 1 d . . . . . H10 H 0.8851 -0.1632 0.2558 0.059 Uiso 1 1 calc R . . . . C21 C 1.0941(4) 0.3776(3) 0.3258(3) 0.0458(11) Uani 1 1 d . . . . . H21 H 1.1395 0.3929 0.3014 0.055 Uiso 1 1 calc R . . . . C30 C 0.7348(3) 0.3631(2) 0.3802(2) 0.0325(8) Uani 1 1 d . . . . . H30 H 0.7258 0.3241 0.3388 0.039 Uiso 1 1 calc R . . . . C26 C 0.8078(4) 0.4227(3) 0.5010(2) 0.0383(9) Uani 1 1 d . . . . . H26 H 0.8497 0.4255 0.5430 0.046 Uiso 1 1 calc R . . . . C28 C 0.6954(4) 0.4713(3) 0.4394(2) 0.0412(10) Uani 1 1 d . . . . . H28 H 0.6609 0.5073 0.4390 0.049 Uiso 1 1 calc R . . . . C13 C 0.9985(3) 0.1655(2) 0.4833(2) 0.0323(8) Uani 1 1 d . . . . . C15 C 1.1458(4) 0.2150(3) 0.5828(3) 0.0431(10) Uani 1 1 d . . . . . H15 H 1.1774 0.2134 0.6259 0.052 Uiso 1 1 calc R . . . . C61 C 0.4381(3) 0.2893(3) 0.3368(2) 0.0381(9) Uani 1 1 d . . . . . C33 C 0.9477(4) 0.3345(3) 0.6425(2) 0.0470(11) Uani 1 1 d . . . . . H33 H 0.9155 0.3169 0.6730 0.056 Uiso 1 1 calc R . . . . C58 C 0.2993(4) 0.1932(4) 0.0896(3) 0.0546(13) Uani 1 1 d . . . . . H58 H 0.2328 0.1669 0.0575 0.065 Uiso 1 1 calc R . . . . C57 C 0.3760(4) 0.2458(4) 0.0753(2) 0.0480(12) Uani 1 1 d . . . . . H57 H 0.3614 0.2558 0.0336 0.058 Uiso 1 1 calc R . . . . C46 C 0.3638(4) 0.0057(3) 0.0218(2) 0.0483(12) Uani 1 1 d . . . . . H46 H 0.3066 -0.0253 -0.0178 0.058 Uiso 1 1 calc R . . . . F5 F 0.5707(7) 0.5599(4) 0.0792(3) 0.095(2) Uani 0.821(5) 1 d D U P B 1 C11 C 0.7913(4) -0.1074(3) 0.2803(2) 0.0457(11) Uani 1 1 d . . . . . H11 H 0.7304 -0.1478 0.2476 0.055 Uiso 1 1 calc R . . . . B1 B 0.5956(4) 0.0766(3) 0.3274(2) 0.0326(9) Uani 1 1 d D . . . . C27 C 0.7564(4) 0.4746(3) 0.4999(2) 0.0439(10) Uani 1 1 d . . . . . H27 H 0.7632 0.5127 0.5412 0.053 Uiso 1 1 calc R . . . . C53 C 0.7257(4) 0.3815(3) 0.1994(3) 0.0429(10) Uani 1 1 d . . . . . H53 H 0.7040 0.4254 0.2082 0.051 Uiso 1 1 calc R . . . . F3 F 0.5733(7) 0.4780(5) 0.2426(4) 0.110(2) Uani 0.821(5) 1 d D U P B 1 C5 C 0.7726(4) -0.0649(3) 0.5246(3) 0.0458(11) Uani 1 1 d . . . . . H5 H 0.7670 -0.1186 0.5187 0.055 Uiso 1 1 calc R . . . . C72 C 0.3305(4) 0.0431(3) 0.2554(3) 0.0480(11) Uani 1 1 d . . . . . H72 H 0.3900 0.0331 0.2522 0.058 Uiso 1 1 calc R . . . . C14 C 1.0465(4) 0.1650(3) 0.5472(2) 0.0386(9) Uani 1 1 d . . . . . H14 H 1.0097 0.1295 0.5663 0.046 Uiso 1 1 calc R . . . . C66 C 0.4547(4) 0.2978(4) 0.4053(3) 0.0511(12) Uani 1 1 d . . . . . H66 H 0.4755 0.2606 0.4223 0.061 Uiso 1 1 calc R . . . . C9 C 0.9712(4) -0.0572(3) 0.3327(3) 0.0434(10) Uani 1 1 d . . . . . H9 H 1.0346 -0.0632 0.3360 0.052 Uiso 1 1 calc R . . . . O6A O 0.2660(12) 0.5497(11) 0.1493(8) 0.105(6) Uani 0.402(8) 1 d D U P C 2 C62 C 0.4083(4) 0.3451(3) 0.3133(3) 0.0459(11) Uani 1 1 d . . . . . H62 H 0.3965 0.3403 0.2669 0.055 Uiso 1 1 calc R . . . . C2 C 0.7851(6) 0.0901(4) 0.5388(4) 0.0617(16) Uani 1 1 d . . . . . H2 H 0.7869 0.1428 0.5436 0.074 Uiso 1 1 calc R . . . . B2 B 0.6493(4) 0.1738(3) 0.4242(2) 0.0346(10) Uani 1 1 d D . . . . C68 C 0.2479(4) 0.1351(4) 0.2802(3) 0.0572(14) Uani 1 1 d . . . . . H68 H 0.2495 0.1883 0.2939 0.069 Uiso 1 1 calc R . . . . C52 C 0.8092(4) 0.3879(3) 0.1782(3) 0.0496(12) Uani 1 1 d . . . . . H52 H 0.8459 0.4363 0.1725 0.060 Uiso 1 1 calc R . . . . C51 C 0.8404(4) 0.3234(3) 0.1651(3) 0.0465(11) Uani 1 1 d . . . . . H51 H 0.8972 0.3272 0.1492 0.056 Uiso 1 1 calc R . . . . C45 C 0.4373(4) 0.0717(3) 0.0222(2) 0.0474(11) Uani 1 1 d . . . . . H45 H 0.4312 0.0861 -0.0176 0.057 Uiso 1 1 calc R . . . . F19 F 0.3721(8) 0.8306(7) 0.2998(6) 0.108(3) Uani 0.704(6) 1 d D U P D 1 C4 C 0.7425(5) -0.0254(4) 0.5741(3) 0.0569(14) Uani 1 1 d . . . . . H4 H 0.7171 -0.0512 0.6033 0.068 Uiso 1 1 calc R . . . . C64 C 0.4107(5) 0.4141(4) 0.4249(3) 0.0605(15) Uani 1 1 d . . . . . H64 H 0.4001 0.4559 0.4547 0.073 Uiso 1 1 calc R . . . . C71 C 0.2408(5) -0.0207(4) 0.2424(3) 0.0632(16) Uani 1 1 d . . . . . H71 H 0.2390 -0.0740 0.2299 0.076 Uiso 1 1 calc R . . . . F16 F 0.2894(7) 0.7854(4) 0.0251(4) 0.110(3) Uani 0.781(6) 1 d D U P E 1 C65 C 0.4410(5) 0.3600(4) 0.4488(3) 0.0614(16) Uani 1 1 d . . . . . H65 H 0.4526 0.3651 0.4953 0.074 Uiso 1 1 calc R . . . . C74 C 0.5448(6) 0.5699(4) 0.1850(3) 0.0693(13) Uani 1 1 d D U . . . C69 C 0.1580(4) 0.0696(5) 0.2674(4) 0.072(2) Uani 1 1 d . . . . . H69 H 0.0989 0.0791 0.2725 0.086 Uiso 1 1 calc R . . . . F21 F 0.3024(7) 0.7849(6) 0.3686(4) 0.097(2) Uani 0.704(6) 1 d D U P D 1 C3 C 0.7494(7) 0.0518(5) 0.5812(5) 0.084(3) Uani 1 1 d . . . . . H3 H 0.7292 0.0794 0.6160 0.101 Uiso 1 1 calc R . . . . F6 F 0.6003(9) 0.4754(5) 0.1200(4) 0.128(3) Uani 0.821(5) 1 d D U P B 1 F27 F 0.5589(7) 0.8187(6) 0.3418(5) 0.122(3) Uani 0.704(6) 1 d D U P D 1 F8 F 0.6643(8) 0.6900(5) 0.1914(5) 0.149(3) Uani 0.821(5) 1 d D U P B 1 F15 F 0.4016(8) 0.8514(5) 0.1682(4) 0.135(3) Uani 0.781(6) 1 d D U P E 1 F13 F 0.4810(8) 0.8426(6) 0.0914(7) 0.158(4) Uani 0.781(6) 1 d D U P E 1 C63 C 0.3958(5) 0.4079(4) 0.3576(3) 0.0569(14) Uani 1 1 d . . . . . H63 H 0.3770 0.4463 0.3415 0.068 Uiso 1 1 calc R . . . . F1 F 0.4913(9) 0.5454(6) 0.2757(5) 0.143(3) Uani 0.821(5) 1 d D U P B 1 C70 C 0.1539(5) -0.0070(5) 0.2478(4) 0.0672(18) Uani 1 1 d . . . . . H70 H 0.0919 -0.0507 0.2378 0.081 Uiso 1 1 calc R . . . . F20 F 0.2546(6) 0.7202(6) 0.2622(4) 0.107(2) Uani 0.704(6) 1 d D U P D 1 F9 F 0.6441(6) 0.6888(6) 0.2781(4) 0.152(3) Uani 0.821(5) 1 d D U P B 1 F23 F 0.3783(10) 0.6938(7) 0.4272(4) 0.131(3) Uani 0.704(6) 1 d D U P D 1 C78 C 0.3718(6) 0.7233(4) 0.0933(4) 0.0742(14) Uani 1 1 d D U . . . F18 F 0.2094(7) 0.6618(5) 0.0071(5) 0.144(3) Uani 0.781(6) 1 d D U P E 1 C82 C 0.4137(6) 0.7262(5) 0.3274(4) 0.0922(17) Uani 1 1 d D U . . . F26 F 0.5641(8) 0.7366(7) 0.4050(5) 0.130(3) Uani 0.704(6) 1 d D U P D 1 F17 F 0.2212(8) 0.7481(7) 0.0966(5) 0.141(3) Uani 0.781(6) 1 d D U P E 1 F24 F 0.4005(9) 0.6044(6) 0.3577(5) 0.122(3) Uani 0.704(6) 1 d D U P D 1 F7 F 0.7184(6) 0.6087(7) 0.2313(6) 0.157(3) Uani 0.821(5) 1 d D U P B 1 F2 F 0.4372(9) 0.4571(7) 0.1982(6) 0.177(4) Uani 0.821(5) 1 d D U P B 1 C77 C 0.6481(8) 0.6407(7) 0.2229(5) 0.098(2) Uani 0.821(5) 1 d D U P B 1 C76 C 0.5475(8) 0.5190(5) 0.1173(4) 0.080(2) Uani 0.821(5) 1 d D U P B 1 F10 F 0.3770(9) 0.6904(7) -0.0204(4) 0.136(3) Uani 0.781(6) 1 d D U P E 1 C73 C 0.4827(6) 0.0616(5) 0.4073(4) 0.045(2) Uani 0.606(13) 1 d D U P A 1 H73A H 0.4434 0.0039 0.3848 0.068 Uiso 0.606(13) 1 calc GR . P A 1 H73B H 0.4482 0.0915 0.3860 0.068 Uiso 0.606(13) 1 calc GR . P A 1 H73C H 0.4881 0.0764 0.4554 0.068 Uiso 0.606(13) 1 calc GR . P A 1 F12 F 0.4971(8) 0.6828(8) 0.0552(6) 0.151(3) Uani 0.781(6) 1 d D U P E 1 F4 F 0.4550(8) 0.4710(6) 0.0757(5) 0.167(4) Uani 0.821(5) 1 d D U P B 1 F11 F 0.3464(11) 0.5949(6) 0.0207(5) 0.148(3) Uani 0.781(6) 1 d D U P E 1 F25 F 0.5018(9) 0.8308(8) 0.4305(5) 0.153(4) Uani 0.704(6) 1 d D U P D 1 F22 F 0.2587(8) 0.6179(7) 0.3303(6) 0.139(3) Uani 0.704(6) 1 d D U P D 1 C83 C 0.3386(8) 0.7670(6) 0.3178(5) 0.081(2) Uani 0.704(6) 1 d D U P D 1 C75 C 0.5252(9) 0.5191(6) 0.2304(5) 0.093(2) Uani 0.821(5) 1 d D U P B 1 C84 C 0.3633(9) 0.6608(7) 0.3623(5) 0.102(3) Uani 0.704(6) 1 d D U P D 1 F14 F 0.5213(7) 0.8037(6) 0.1799(6) 0.193(5) Uani 0.781(6) 1 d D U P E 1 C81 C 0.2746(8) 0.7317(6) 0.0574(5) 0.097(2) Uani 0.781(6) 1 d D U P E 1 C85 C 0.5155(10) 0.7816(7) 0.3794(6) 0.114(3) Uani 0.704(6) 1 d D U P D 1 C80 C 0.4495(8) 0.8073(6) 0.1338(6) 0.114(3) Uani 0.781(6) 1 d D U P E 1 C79 C 0.3975(9) 0.6729(7) 0.0361(5) 0.101(2) Uani 0.781(6) 1 d D U P E 1 C73A C 0.5567(12) 0.0263(8) 0.4252(7) 0.051(4) Uani 0.394(13) 1 d D U P A 2 H73D H 0.4995 -0.0242 0.3975 0.077 Uiso 0.394(13) 1 calc GR . P A 2 H73E H 0.5493 0.0454 0.4700 0.077 Uiso 0.394(13) 1 calc GR . P A 2 H73F H 0.6209 0.0176 0.4304 0.077 Uiso 0.394(13) 1 calc GR . P A 2 C86A C 0.1881(15) 0.4828(10) 0.1359(10) 0.142(4) Uani 0.402(8) 1 d D U P C 2 C89A C 0.0977(13) 0.4889(13) 0.0871(10) 0.157(5) Uani 0.402(8) 1 d D U P C 2 F34A F 0.108(2) 0.4815(17) 0.0246(10) 0.178(7) Uani 0.402(8) 1 d D U P C 2 F36A F 0.0145(16) 0.4269(15) 0.0784(11) 0.180(8) Uani 0.402(8) 1 d D U P C 2 F35A F 0.0987(18) 0.5627(13) 0.1133(12) 0.189(7) Uani 0.402(8) 1 d D U P C 2 C87A C 0.1534(13) 0.4644(13) 0.1941(9) 0.162(5) Uani 0.402(8) 1 d D U P C 2 F29A F 0.2357(13) 0.4968(14) 0.2498(9) 0.195(8) Uani 0.402(8) 1 d D U P C 2 F28A F 0.0693(12) 0.4748(13) 0.2066(9) 0.160(6) Uani 0.402(8) 1 d D U P C 2 F30A F 0.1106(18) 0.3815(12) 0.1737(11) 0.192(7) Uani 0.402(8) 1 d D U P C 2 C88A C 0.2078(17) 0.4118(15) 0.0959(11) 0.183(6) Uani 0.402(8) 1 d D U P C 2 F32A F 0.257(2) 0.3997(19) 0.1514(14) 0.214(8) Uani 0.402(8) 1 d D U P C 2 F31A F 0.1152(19) 0.3579(19) 0.0579(15) 0.233(9) Uani 0.402(8) 1 d D U P C 2 F33A F 0.265(2) 0.4379(18) 0.0594(14) 0.208(8) Uani 0.402(8) 1 d D U P C 2 N1A N 0.5573(10) 0.0870(6) 0.3918(6) 0.030(3) Uani 0.394(13) 1 d D U P A 2 H1AA H 0.4897 0.0925 0.3812 0.036 Uiso 0.394(13) 1 calc R . P A 2 F25A F 0.4834(16) 0.7661(12) 0.4470(7) 0.097(5) Uani 0.296(6) 1 d D U P D 2 F27A F 0.5879(16) 0.7701(16) 0.3762(12) 0.134(6) Uani 0.296(6) 1 d D U P D 2 F26A F 0.483(2) 0.6570(12) 0.3818(8) 0.118(5) Uani 0.296(6) 1 d D U P D 2 F23A F 0.322(2) 0.6884(18) 0.3846(12) 0.158(7) Uani 0.296(6) 1 d D U P D 2 C84A C 0.2989(12) 0.6932(14) 0.3231(12) 0.137(5) Uani 0.296(6) 1 d D U P D 2 F24A F 0.221(2) 0.6249(17) 0.2751(15) 0.203(9) Uani 0.296(6) 1 d D U P D 2 F22A F 0.277(2) 0.7562(16) 0.3164(15) 0.148(6) Uani 0.296(6) 1 d D U P D 2 F20A F 0.404(2) 0.837(2) 0.2888(11) 0.132(7) Uani 0.296(6) 1 d D U P D 2 C83A C 0.4403(16) 0.8209(9) 0.3456(11) 0.125(4) Uani 0.296(6) 1 d D U P D 2 F19A F 0.5419(15) 0.8754(16) 0.3792(13) 0.147(7) Uani 0.296(6) 1 d D U P D 2 F21A F 0.3885(18) 0.8443(14) 0.3901(11) 0.123(5) Uani 0.296(6) 1 d D U P D 2 C85A C 0.4975(14) 0.7325(12) 0.3889(7) 0.110(4) Uani 0.296(6) 1 d D U P D 2 F28 F 0.1096(12) 0.5058(11) 0.2212(8) 0.160(5) Uani 0.598(8) 1 d D U P C 1 F29 F 0.0022(9) 0.4705(10) 0.1109(8) 0.159(5) Uani 0.598(8) 1 d D U P C 1 C87 C 0.0938(11) 0.5082(9) 0.1578(8) 0.134(5) Uani 0.598(8) 1 d D U P C 1 F30 F 0.1113(12) 0.5873(8) 0.1705(10) 0.177(6) Uani 0.598(8) 1 d D U P C 1 F34 F 0.0810(12) 0.4061(10) 0.0207(8) 0.198(7) Uani 0.598(8) 1 d D U P C 1 F32 F 0.2252(8) 0.4173(7) 0.2092(6) 0.114(3) Uani 0.598(8) 1 d D U P C 1 C88 C 0.1747(9) 0.4089(7) 0.1449(7) 0.113(4) Uani 0.598(8) 1 d D U P C 1 F33 F 0.2236(12) 0.3740(9) 0.1055(8) 0.162(5) Uani 0.598(8) 1 d D U P C 1 F31 F 0.0770(8) 0.3553(7) 0.1202(8) 0.155(5) Uani 0.598(8) 1 d D U P C 1 F35 F 0.2403(11) 0.4827(10) 0.0421(7) 0.171(5) Uani 0.598(8) 1 d D U P C 1 C89 C 0.1563(11) 0.4750(9) 0.0612(8) 0.141(5) Uani 0.598(8) 1 d D U P C 1 F36 F 0.1243(10) 0.5336(9) 0.0478(7) 0.155(5) Uani 0.598(8) 1 d D U P C 1 F9A F 0.708(3) 0.6464(17) 0.1983(16) 0.124(7) Uani 0.179(5) 1 d D U P B 2 C77A C 0.6339(15) 0.5821(14) 0.1556(12) 0.089(4) Uani 0.179(5) 1 d D U P B 2 F8A F 0.609(3) 0.593(2) 0.0993(13) 0.090(6) Uani 0.179(5) 1 d D U P B 2 F7A F 0.668(2) 0.5247(15) 0.1443(13) 0.075(5) Uani 0.179(5) 1 d D U P B 2 F3A F 0.6626(18) 0.5410(13) 0.2725(9) 0.067(4) Uani 0.179(5) 1 d D U P B 2 C75A C 0.6045(15) 0.5796(13) 0.2582(7) 0.079(4) Uani 0.179(5) 1 d D U P B 2 F2A F 0.5566(14) 0.5740(13) 0.3006(8) 0.058(4) Uani 0.179(5) 1 d D U P B 2 F1A F 0.6710(19) 0.6497(11) 0.2894(11) 0.085(5) Uani 0.179(5) 1 d D U P B 2 C76A C 0.4908(17) 0.4756(9) 0.1601(9) 0.088(4) Uani 0.179(5) 1 d D U P B 2 F5A F 0.493(2) 0.4530(11) 0.1008(9) 0.070(4) Uani 0.179(5) 1 d D U P B 2 F6A F 0.541(2) 0.4562(17) 0.2056(12) 0.095(5) Uani 0.179(5) 1 d D U P B 2 F4A F 0.4016(17) 0.4322(13) 0.1572(12) 0.085(5) Uani 0.179(5) 1 d D U P B 2 F17A F 0.211(2) 0.6988(19) 0.0997(15) 0.124(6) Uani 0.219(6) 1 d D U P E 2 C81A C 0.2569(12) 0.6919(14) 0.0510(12) 0.111(4) Uani 0.219(6) 1 d D U P E 2 F16A F 0.245(3) 0.7467(18) 0.0236(17) 0.119(5) Uani 0.219(6) 1 d D U P E 2 F18A F 0.233(3) 0.6171(15) 0.0131(17) 0.143(8) Uani 0.219(6) 1 d D U P E 2 C80A C 0.3917(16) 0.8119(9) 0.1084(12) 0.102(4) Uani 0.219(6) 1 d D U P E 2 F13A F 0.366(2) 0.8141(18) 0.0435(12) 0.121(5) Uani 0.219(6) 1 d D U P E 2 F15A F 0.316(2) 0.8163(16) 0.1347(15) 0.106(5) Uani 0.219(6) 1 d D U P E 2 F14A F 0.4875(16) 0.8624(12) 0.1380(13) 0.089(5) Uani 0.219(6) 1 d D U P E 2 F12A F 0.5379(13) 0.7335(13) 0.1071(10) 0.083(5) Uani 0.219(6) 1 d D U P E 2 C79A C 0.4445(14) 0.7029(11) 0.0595(9) 0.076(4) Uani 0.219(6) 1 d D U P E 2 F10A F 0.4504(18) 0.7364(13) 0.0110(11) 0.080(5) Uani 0.219(6) 1 d D U P E 2 F11A F 0.4131(16) 0.6228(10) 0.0307(9) 0.063(4) Uani 0.219(6) 1 d D U P E 2 O6 O 0.2719(7) 0.5477(6) 0.1740(5) 0.077(2) Uani 0.598(8) 1 d D U P C 1 C86 C 0.1830(9) 0.4915(7) 0.1383(7) 0.096(3) Uani 0.598(8) 1 d D U P C 1 H2A H 0.664(4) 0.200(3) 0.476(3) 0.043(14) Uiso 1 1 d . . . . . H1A H 0.547(5) 0.016(4) 0.283(3) 0.055(17) Uiso 1 1 d . . . . . H2B H 0.600(5) 0.221(4) 0.407(3) 0.052(16) Uiso 1 1 d . . . . . H1B H 0.679(5) 0.069(4) 0.337(3) 0.048(16) Uiso 1 1 d . . . . . C36 C 1.0406(3) 0.3872(3) 0.5535(2) 0.0358(9) Uani 1 1 d . . . . . H36 H 1.0728 0.4061 0.5235 0.043 Uiso 1 1 calc R . . . . C35 C 1.0931(4) 0.4154(3) 0.6229(2) 0.0442(11) Uani 1 1 d . . . . . H35 H 1.1612 0.4536 0.6398 0.053 Uiso 1 1 calc R . . . . C34 C 1.0480(4) 0.3889(3) 0.6671(2) 0.0458(11) Uani 1 1 d . . . . . H34 H 1.0850 0.4075 0.7141 0.055 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh2 0.02277(14) 0.03140(15) 0.02230(14) 0.00960(11) 0.00742(10) 0.01319(11) Rh1 0.02567(15) 0.02697(15) 0.02595(15) 0.00823(11) 0.00321(10) 0.01221(11) P2 0.0289(4) 0.0282(4) 0.0237(4) 0.0089(3) 0.0067(3) 0.0119(4) P3 0.0235(4) 0.0283(4) 0.0231(4) 0.0086(3) 0.0077(3) 0.0110(4) P1 0.0282(5) 0.0309(5) 0.0316(5) 0.0113(4) 0.0028(4) 0.0142(4) P4 0.0260(5) 0.0470(6) 0.0285(5) 0.0148(4) 0.0105(4) 0.0193(4) Al1 0.0384(7) 0.0453(7) 0.0304(6) 0.0169(5) 0.0107(5) 0.0120(6) O2 0.0325(14) 0.0366(15) 0.0276(13) 0.0098(11) 0.0074(11) 0.0161(12) O1 0.0304(14) 0.0342(15) 0.0297(14) 0.0084(11) 0.0039(11) 0.0115(12) C19 0.0280(18) 0.036(2) 0.0276(18) 0.0098(16) 0.0041(15) 0.0093(16) C24 0.0285(18) 0.0321(19) 0.0233(17) 0.0053(15) 0.0044(14) 0.0087(16) C7 0.036(2) 0.0313(19) 0.032(2) 0.0139(16) 0.0069(16) 0.0161(17) C37 0.0314(19) 0.0311(19) 0.0282(18) 0.0115(15) 0.0112(15) 0.0149(16) C48 0.033(2) 0.040(2) 0.030(2) 0.0125(17) 0.0073(16) 0.0114(18) C23 0.039(2) 0.037(2) 0.031(2) 0.0123(17) 0.0089(17) 0.0145(18) C43 0.0281(18) 0.0315(19) 0.0250(17) 0.0064(15) 0.0068(14) 0.0142(16) O3 0.078(3) 0.103(4) 0.073(3) 0.043(3) 0.036(3) 0.060(3) C31 0.035(2) 0.0301(19) 0.0262(18) 0.0079(15) 0.0061(15) 0.0153(16) C49 0.0300(19) 0.0314(19) 0.0275(18) 0.0101(15) 0.0078(15) 0.0117(16) C54 0.0308(19) 0.0310(19) 0.0286(18) 0.0104(15) 0.0079(15) 0.0089(16) C42 0.035(2) 0.036(2) 0.0283(19) 0.0050(16) 0.0047(16) 0.0159(17) C40 0.044(2) 0.049(3) 0.035(2) 0.0115(19) 0.0127(18) 0.031(2) C47 0.035(2) 0.045(3) 0.040(2) 0.011(2) 0.0050(19) 0.008(2) C25 0.0289(18) 0.0285(18) 0.0285(18) 0.0086(15) 0.0065(15) 0.0095(15) N1 0.034(5) 0.052(5) 0.050(5) 0.024(4) 0.016(4) 0.020(3) C1 0.034(2) 0.042(2) 0.038(2) 0.0152(18) 0.0094(17) 0.0189(18) C12 0.043(2) 0.036(2) 0.036(2) 0.0106(18) 0.0046(18) 0.0181(19) C50 0.036(2) 0.049(3) 0.041(2) 0.020(2) 0.0183(19) 0.018(2) C22 0.045(2) 0.044(2) 0.034(2) 0.0171(19) 0.0101(19) 0.008(2) C20 0.038(2) 0.050(3) 0.037(2) 0.012(2) 0.0153(18) 0.018(2) C55 0.033(2) 0.037(2) 0.0279(19) 0.0092(16) 0.0084(16) 0.0204(17) C39 0.031(2) 0.047(2) 0.032(2) 0.0104(18) 0.0064(16) 0.0189(19) C16 0.036(2) 0.043(2) 0.046(3) 0.008(2) -0.0057(19) 0.016(2) C18 0.0264(18) 0.036(2) 0.032(2) 0.0087(16) 0.0024(15) 0.0143(16) C41 0.044(2) 0.043(2) 0.036(2) 0.0058(18) 0.0083(18) 0.026(2) O4 0.152(6) 0.100(4) 0.085(3) 0.069(3) 0.070(4) 0.088(4) C44 0.042(2) 0.037(2) 0.0257(19) 0.0096(16) 0.0065(17) 0.0146(19) C6 0.047(2) 0.041(2) 0.041(2) 0.019(2) 0.013(2) 0.022(2) C38 0.0280(19) 0.040(2) 0.0259(18) 0.0062(16) 0.0073(15) 0.0154(17) C56 0.045(2) 0.047(2) 0.034(2) 0.0189(19) 0.0138(19) 0.025(2) C29 0.040(2) 0.036(2) 0.035(2) 0.0139(17) 0.0079(17) 0.0181(18) C32 0.038(2) 0.044(2) 0.030(2) 0.0105(18) 0.0071(17) 0.0098(19) C17 0.034(2) 0.039(2) 0.044(2) 0.0129(19) 0.0067(18) 0.0172(18) C67 0.028(2) 0.063(3) 0.037(2) 0.024(2) 0.0123(17) 0.016(2) C60 0.0302(19) 0.045(2) 0.0255(18) 0.0126(16) 0.0081(15) 0.0200(18) O5 0.106(4) 0.096(4) 0.039(2) 0.008(2) 0.022(2) 0.046(3) C8 0.037(2) 0.040(2) 0.040(2) 0.0165(19) 0.0117(18) 0.0199(19) C59 0.031(2) 0.063(3) 0.038(2) 0.021(2) 0.0081(18) 0.021(2) C10 0.071(3) 0.045(3) 0.039(2) 0.014(2) 0.021(2) 0.030(3) C21 0.045(3) 0.054(3) 0.038(2) 0.016(2) 0.020(2) 0.012(2) C30 0.038(2) 0.0296(19) 0.0293(19) 0.0076(15) 0.0100(16) 0.0144(17) C26 0.043(2) 0.041(2) 0.0267(19) 0.0051(17) 0.0051(17) 0.0198(19) C28 0.042(2) 0.042(2) 0.042(2) 0.0103(19) 0.0107(19) 0.024(2) C13 0.0280(19) 0.033(2) 0.031(2) 0.0064(16) 0.0016(15) 0.0145(16) C15 0.040(2) 0.043(2) 0.041(2) 0.014(2) -0.0024(19) 0.017(2) C61 0.033(2) 0.056(3) 0.034(2) 0.0156(19) 0.0151(17) 0.024(2) C33 0.052(3) 0.052(3) 0.032(2) 0.015(2) 0.012(2) 0.013(2) C58 0.037(2) 0.079(4) 0.039(3) 0.018(3) -0.001(2) 0.020(3) C57 0.050(3) 0.069(3) 0.030(2) 0.020(2) 0.009(2) 0.029(3) C46 0.046(3) 0.047(3) 0.031(2) 0.0027(19) -0.0047(19) 0.011(2) F5 0.176(7) 0.084(4) 0.060(3) 0.033(3) 0.054(4) 0.078(4) C11 0.057(3) 0.038(2) 0.036(2) 0.0078(19) 0.005(2) 0.020(2) B1 0.031(2) 0.033(2) 0.036(2) 0.0142(19) 0.0123(18) 0.0119(18) C27 0.049(3) 0.046(3) 0.034(2) 0.0027(19) 0.0095(19) 0.026(2) C53 0.048(3) 0.033(2) 0.047(3) 0.0173(19) 0.014(2) 0.013(2) F3 0.203(7) 0.131(5) 0.084(4) 0.071(4) 0.073(4) 0.131(5) C5 0.051(3) 0.043(3) 0.048(3) 0.023(2) 0.013(2) 0.020(2) C72 0.039(2) 0.060(3) 0.042(3) 0.014(2) 0.018(2) 0.013(2) C14 0.036(2) 0.042(2) 0.036(2) 0.0152(18) 0.0011(17) 0.0180(19) C66 0.054(3) 0.075(4) 0.040(3) 0.020(2) 0.020(2) 0.040(3) C9 0.049(3) 0.050(3) 0.047(3) 0.025(2) 0.021(2) 0.030(2) O6A 0.074(7) 0.122(9) 0.062(9) 0.042(7) -0.001(6) -0.029(6) C62 0.048(3) 0.063(3) 0.041(2) 0.020(2) 0.019(2) 0.036(2) C2 0.090(5) 0.051(3) 0.080(4) 0.034(3) 0.057(4) 0.045(3) B2 0.037(2) 0.041(3) 0.029(2) 0.0142(19) 0.0130(18) 0.016(2) C68 0.039(3) 0.078(4) 0.075(4) 0.041(3) 0.028(3) 0.029(3) C52 0.043(3) 0.041(3) 0.060(3) 0.026(2) 0.016(2) 0.003(2) C51 0.038(2) 0.055(3) 0.052(3) 0.028(2) 0.021(2) 0.012(2) C45 0.060(3) 0.045(3) 0.029(2) 0.0117(19) 0.002(2) 0.017(2) F19 0.116(6) 0.133(6) 0.125(6) 0.066(5) 0.065(5) 0.080(5) C4 0.064(3) 0.065(3) 0.066(4) 0.041(3) 0.038(3) 0.030(3) C64 0.062(3) 0.078(4) 0.049(3) 0.008(3) 0.023(3) 0.042(3) C71 0.052(3) 0.070(4) 0.060(3) 0.017(3) 0.026(3) 0.010(3) F16 0.127(6) 0.073(4) 0.107(5) 0.047(3) -0.023(4) 0.037(4) C65 0.071(4) 0.092(5) 0.038(3) 0.015(3) 0.024(3) 0.053(4) C74 0.110(4) 0.075(3) 0.055(3) 0.028(2) 0.034(2) 0.067(3) C69 0.032(3) 0.108(6) 0.092(5) 0.049(4) 0.033(3) 0.028(3) F21 0.121(6) 0.137(6) 0.088(4) 0.045(4) 0.064(4) 0.094(5) C3 0.133(7) 0.081(5) 0.105(6) 0.057(5) 0.093(6) 0.069(5) F6 0.249(9) 0.129(5) 0.095(5) 0.055(4) 0.096(5) 0.148(6) F27 0.102(5) 0.114(6) 0.136(6) 0.022(5) 0.032(5) 0.041(5) F8 0.145(6) 0.093(5) 0.135(6) 0.005(4) 0.013(5) -0.004(4) F15 0.166(7) 0.079(4) 0.120(6) 0.029(4) -0.012(5) 0.037(5) F13 0.114(6) 0.126(6) 0.226(8) 0.112(7) 0.034(6) 0.007(5) C63 0.064(3) 0.070(4) 0.052(3) 0.019(3) 0.023(3) 0.045(3) F1 0.257(9) 0.163(6) 0.129(5) 0.100(5) 0.130(6) 0.151(6) C70 0.042(3) 0.088(5) 0.068(4) 0.033(4) 0.026(3) 0.008(3) F20 0.086(4) 0.149(6) 0.099(5) 0.034(4) 0.024(3) 0.074(4) F9 0.101(5) 0.177(7) 0.105(5) -0.032(5) -0.001(4) 0.043(5) F23 0.204(9) 0.160(7) 0.088(5) 0.058(5) 0.072(5) 0.119(7) C78 0.092(3) 0.080(3) 0.089(3) 0.064(3) 0.042(3) 0.045(3) F18 0.133(6) 0.096(5) 0.150(6) 0.047(4) -0.028(5) 0.019(4) C82 0.115(4) 0.133(4) 0.061(3) 0.026(3) 0.037(3) 0.089(3) F26 0.120(6) 0.195(8) 0.087(5) 0.037(5) 0.005(5) 0.104(6) F17 0.140(7) 0.169(8) 0.172(7) 0.087(6) 0.054(5) 0.109(6) F24 0.163(8) 0.138(6) 0.128(7) 0.066(5) 0.088(6) 0.094(6) F7 0.091(5) 0.221(8) 0.170(8) 0.078(7) 0.021(5) 0.077(5) F2 0.221(7) 0.168(6) 0.175(7) 0.114(5) 0.057(6) 0.074(6) C77 0.082(4) 0.126(5) 0.072(4) 0.012(4) 0.019(4) 0.043(4) C76 0.149(6) 0.065(4) 0.055(3) 0.023(3) 0.048(3) 0.065(4) F10 0.183(8) 0.217(9) 0.095(5) 0.100(5) 0.080(5) 0.128(7) C73 0.038(4) 0.052(5) 0.046(4) 0.017(4) 0.019(3) 0.012(3) F12 0.136(6) 0.253(10) 0.167(8) 0.138(7) 0.097(5) 0.121(6) F4 0.194(7) 0.138(6) 0.102(5) -0.025(5) 0.036(5) 0.034(5) F11 0.229(10) 0.122(6) 0.120(6) 0.037(5) 0.074(7) 0.093(6) F25 0.141(7) 0.171(8) 0.101(6) -0.029(6) 0.007(5) 0.079(7) F22 0.145(6) 0.170(8) 0.135(7) 0.068(6) 0.073(5) 0.069(6) C83 0.088(4) 0.119(5) 0.081(4) 0.043(4) 0.048(3) 0.075(4) C75 0.165(6) 0.094(4) 0.088(4) 0.056(4) 0.074(4) 0.095(4) C84 0.136(6) 0.133(6) 0.086(5) 0.047(4) 0.066(4) 0.089(5) F14 0.127(6) 0.123(6) 0.233(9) 0.084(6) -0.078(6) -0.005(5) C81 0.106(5) 0.080(4) 0.119(5) 0.054(4) 0.017(4) 0.053(4) C85 0.116(5) 0.138(6) 0.093(5) 0.021(4) 0.017(4) 0.079(5) C80 0.105(5) 0.079(4) 0.146(6) 0.067(4) -0.003(4) 0.027(4) C79 0.135(6) 0.134(6) 0.092(5) 0.074(4) 0.061(4) 0.081(5) C73A 0.065(9) 0.048(7) 0.050(7) 0.032(6) 0.017(6) 0.021(6) C86A 0.107(6) 0.151(6) 0.104(6) 0.062(5) 0.001(5) -0.031(5) C89A 0.114(7) 0.183(9) 0.102(8) 0.056(7) -0.008(6) -0.018(7) F34A 0.165(13) 0.196(15) 0.107(9) 0.061(9) 0.003(8) -0.001(12) F36A 0.104(9) 0.208(13) 0.124(12) 0.049(10) -0.023(8) -0.032(9) F35A 0.143(12) 0.210(11) 0.136(12) 0.050(9) -0.018(10) 0.013(9) C87A 0.119(8) 0.186(9) 0.107(7) 0.073(7) 0.006(6) -0.039(7) F29A 0.147(10) 0.205(14) 0.124(9) 0.097(9) -0.025(7) -0.063(9) F28A 0.103(8) 0.217(12) 0.082(8) 0.069(8) 0.010(6) -0.047(8) F30A 0.175(13) 0.191(10) 0.126(11) 0.085(8) 0.014(10) -0.047(8) C88A 0.161(9) 0.171(8) 0.139(9) 0.047(7) 0.001(7) -0.004(7) F32A 0.209(15) 0.186(14) 0.165(12) 0.055(11) -0.011(10) 0.018(11) F31A 0.200(12) 0.206(13) 0.178(14) 0.048(11) -0.012(10) -0.011(10) F33A 0.210(14) 0.188(15) 0.162(12) 0.051(11) 0.028(10) 0.018(11) N1A 0.035(7) 0.025(5) 0.035(6) 0.017(4) 0.017(5) 0.011(5) F25A 0.141(11) 0.123(11) 0.050(6) 0.025(6) 0.021(6) 0.089(9) F27A 0.125(9) 0.191(13) 0.112(11) 0.057(10) 0.021(7) 0.100(8) F26A 0.171(13) 0.132(9) 0.054(7) 0.019(7) 0.006(8) 0.093(8) F23A 0.161(13) 0.182(14) 0.110(9) 0.020(9) 0.053(8) 0.056(11) C84A 0.138(7) 0.167(8) 0.107(8) 0.017(7) 0.046(6) 0.078(6) F24A 0.189(13) 0.212(12) 0.158(13) 0.014(11) 0.034(11) 0.065(10) F22A 0.134(11) 0.171(10) 0.138(12) 0.020(9) 0.050(9) 0.080(8) F20A 0.169(15) 0.138(12) 0.115(9) 0.024(8) 0.047(9) 0.107(11) C83A 0.141(8) 0.139(7) 0.106(7) 0.024(5) 0.036(6) 0.083(6) F19A 0.154(10) 0.143(11) 0.131(12) 0.033(10) 0.028(8) 0.061(8) F21A 0.140(10) 0.123(10) 0.119(9) 0.016(8) 0.050(8) 0.081(8) C85A 0.139(7) 0.140(8) 0.068(6) 0.020(5) 0.026(5) 0.092(6) F28 0.146(10) 0.195(12) 0.150(9) 0.039(8) 0.059(8) 0.086(9) F29 0.079(6) 0.169(10) 0.171(10) 0.017(8) 0.019(6) 0.019(6) C87 0.094(6) 0.128(7) 0.146(8) 0.029(7) 0.028(6) 0.019(6) F30 0.144(10) 0.134(8) 0.215(12) 0.032(8) 0.026(10) 0.044(7) F34 0.170(10) 0.178(10) 0.134(10) 0.035(8) -0.013(8) -0.027(8) F32 0.120(7) 0.109(7) 0.136(7) 0.070(6) 0.066(5) 0.035(5) C88 0.100(6) 0.093(6) 0.125(6) 0.038(5) 0.050(5) -0.005(5) F33 0.154(9) 0.140(10) 0.146(9) 0.001(8) 0.056(7) 0.027(8) F31 0.111(6) 0.102(7) 0.181(10) 0.017(7) 0.049(6) -0.032(5) F35 0.164(8) 0.195(12) 0.092(7) 0.045(8) 0.019(6) 0.002(8) C89 0.114(7) 0.146(8) 0.101(7) 0.053(6) -0.003(6) -0.020(6) F36 0.134(8) 0.162(9) 0.097(7) 0.062(7) -0.019(6) -0.015(7) F9A 0.149(11) 0.110(10) 0.111(11) 0.025(9) 0.044(9) 0.055(8) C77A 0.122(7) 0.092(7) 0.076(7) 0.029(6) 0.044(6) 0.064(6) F8A 0.114(13) 0.104(14) 0.082(9) 0.039(8) 0.051(8) 0.061(10) F7A 0.101(11) 0.086(10) 0.066(10) 0.029(8) 0.044(9) 0.058(9) F3A 0.111(8) 0.073(7) 0.041(6) 0.018(6) 0.026(6) 0.066(7) C75A 0.117(7) 0.086(7) 0.053(5) 0.019(5) 0.027(5) 0.068(6) F2A 0.090(8) 0.079(8) 0.020(5) 0.007(5) 0.003(5) 0.068(7) F1A 0.126(9) 0.085(7) 0.048(7) 0.012(5) 0.013(6) 0.066(6) C76A 0.131(8) 0.077(6) 0.065(6) 0.022(5) 0.029(6) 0.056(5) F5A 0.134(11) 0.038(7) 0.057(7) 0.017(5) 0.023(7) 0.061(7) F6A 0.142(10) 0.069(8) 0.077(8) 0.025(7) 0.021(8) 0.054(7) F4A 0.136(9) 0.057(7) 0.069(9) 0.013(7) 0.031(7) 0.053(6) F17A 0.099(11) 0.125(13) 0.157(11) 0.064(10) 0.045(9) 0.038(10) C81A 0.105(6) 0.110(7) 0.129(7) 0.060(6) 0.032(5) 0.044(5) F16A 0.116(8) 0.114(8) 0.135(8) 0.062(7) 0.030(7) 0.045(6) F18A 0.134(14) 0.117(9) 0.157(12) 0.046(9) 0.014(10) 0.043(8) C80A 0.113(7) 0.094(6) 0.119(7) 0.058(5) 0.039(6) 0.047(5) F13A 0.129(8) 0.113(8) 0.126(8) 0.066(6) 0.032(7) 0.041(7) F15A 0.128(11) 0.101(11) 0.137(12) 0.074(9) 0.056(9) 0.070(9) F14A 0.105(8) 0.062(8) 0.122(11) 0.048(8) 0.034(8) 0.048(6) F12A 0.074(7) 0.109(11) 0.098(9) 0.068(8) 0.053(6) 0.034(7) C79A 0.091(6) 0.080(6) 0.090(7) 0.058(5) 0.046(5) 0.042(5) F10A 0.104(11) 0.090(10) 0.091(9) 0.066(8) 0.059(8) 0.048(8) F11A 0.093(10) 0.069(7) 0.066(8) 0.046(6) 0.049(7) 0.044(6) O6 0.056(4) 0.079(4) 0.074(5) 0.043(4) 0.008(4) -0.006(3) C86 0.074(5) 0.096(5) 0.102(5) 0.055(5) 0.028(4) -0.006(5) C36 0.036(2) 0.034(2) 0.032(2) 0.0099(17) 0.0074(17) 0.0097(17) C35 0.041(2) 0.043(2) 0.033(2) 0.0075(19) -0.0010(18) 0.008(2) C34 0.050(3) 0.050(3) 0.026(2) 0.0076(19) 0.0006(19) 0.017(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh2 Rh1 2.6421(4) . ? Rh2 P3 2.2857(9) . ? Rh2 P4 2.3414(10) . ? Rh2 B1 2.107(5) . ? Rh2 B2 2.328(5) . ? Rh2 H2B 1.88(6) . ? Rh1 P2 2.2787(10) . ? Rh1 P1 2.3290(10) . ? Rh1 B1 2.326(5) . ? Rh1 B2 2.096(5) . ? Rh1 H1B 1.70(6) . ? P2 C24 1.842(4) . ? P2 C31 1.841(4) . ? P2 C25 1.840(4) . ? P3 C37 1.829(4) . ? P3 C43 1.833(4) . ? P3 C49 1.841(4) . ? P1 C7 1.832(4) . ? P1 C1 1.833(5) . ? P1 C13 1.833(4) . ? P4 C67 1.837(5) . ? P4 C60 1.834(4) . ? P4 C61 1.840(5) . ? Al1 O3 1.716(4) . ? Al1 O4 1.692(4) . ? Al1 O5 1.712(4) . ? Al1 O6A 1.688(11) . ? Al1 O6 1.719(7) . ? O2 C54 1.390(5) . ? O2 C55 1.393(5) . ? O1 C19 1.387(5) . ? O1 C18 1.390(5) . ? C19 C24 1.411(6) . ? C19 C20 1.377(6) . ? C24 C23 1.400(6) . ? C7 C12 1.397(6) . ? C7 C8 1.390(6) . ? C37 C42 1.396(6) . ? C37 C38 1.399(6) . ? C48 H48 0.9500 . ? C48 C43 1.392(6) . ? C48 C47 1.377(6) . ? C23 H23 0.9500 . ? C23 C22 1.384(6) . ? C43 C44 1.388(6) . ? O3 C74 1.316(8) . ? C31 C32 1.400(6) . ? C31 C36 1.385(6) . ? C49 C54 1.391(6) . ? C49 C50 1.399(6) . ? C54 C53 1.395(6) . ? C42 H42 0.9500 . ? C42 C41 1.389(6) . ? C40 H40 0.9500 . ? C40 C39 1.383(7) . ? C40 C41 1.378(7) . ? C47 H47 0.9500 . ? C47 C46 1.399(7) . ? C25 C30 1.398(6) . ? C25 C26 1.391(6) . ? N1 H1 1.0000 . ? N1 B1 1.589(10) . ? N1 B2 1.565(10) . ? N1 C73 1.488(11) . ? C1 C6 1.391(6) . ? C1 C2 1.396(7) . ? C12 H12 0.9500 . ? C12 C11 1.387(7) . ? C50 H50 0.9500 . ? C50 C51 1.387(7) . ? C22 H22 0.9500 . ? C22 C21 1.380(8) . ? C20 H20 0.9500 . ? C20 C21 1.393(7) . ? C55 C56 1.377(6) . ? C55 C60 1.401(6) . ? C39 H39 0.9500 . ? C39 C38 1.387(6) . ? C16 H16 0.9500 . ? C16 C17 1.391(7) . ? C16 C15 1.397(8) . ? C18 C17 1.380(6) . ? C18 C13 1.390(6) . ? C41 H41 0.9500 . ? O4 C78 1.317(7) . ? C44 H44 0.9500 . ? C44 C45 1.402(7) . ? C6 H6 0.9500 . ? C6 C5 1.381(7) . ? C38 H38 0.9500 . ? C56 H56 0.9500 . ? C56 C57 1.392(7) . ? C29 H29 0.9500 . ? C29 C30 1.383(6) . ? C29 C28 1.382(7) . ? C32 H32 0.9500 . ? C32 C33 1.385(7) . ? C17 H17 0.9500 . ? C67 C72 1.385(8) . ? C67 C68 1.391(7) . ? C60 C59 1.394(6) . ? O5 C82 1.289(9) . ? C8 H8 0.9500 . ? C8 C9 1.385(7) . ? C59 H59 0.9500 . ? C59 C58 1.378(7) . ? C10 H10 0.9500 . ? C10 C11 1.371(8) . ? C10 C9 1.387(8) . ? C21 H21 0.9500 . ? C30 H30 0.9500 . ? C26 H26 0.9500 . ? C26 C27 1.388(7) . ? C28 H28 0.9500 . ? C28 C27 1.377(7) . ? C13 C14 1.399(6) . ? C15 H15 0.9500 . ? C15 C14 1.372(7) . ? C61 C66 1.397(7) . ? C61 C62 1.396(7) . ? C33 H33 0.9500 . ? C33 C34 1.389(8) . ? C58 H58 0.9500 . ? C58 C57 1.389(8) . ? C57 H57 0.9500 . ? C46 H46 0.9500 . ? C46 C45 1.358(8) . ? F5 C76 1.276(9) . ? C11 H11 0.9500 . ? B1 N1A 1.590(11) . ? B1 H1A 1.16(7) . ? B1 H1B 1.24(6) . ? C27 H27 0.9500 . ? C53 H53 0.9500 . ? C53 C52 1.369(8) . ? F3 C75 1.216(9) . ? C5 H5 0.9500 . ? C5 C4 1.366(8) . ? C72 H72 0.9500 . ? C72 C71 1.387(8) . ? C14 H14 0.9500 . ? C66 H66 0.9500 . ? C66 C65 1.388(8) . ? C9 H9 0.9500 . ? O6A C86A 1.318(16) . ? C62 H62 0.9500 . ? C62 C63 1.396(7) . ? C2 H2 0.9500 . ? C2 C3 1.382(8) . ? B2 N1A 1.612(11) . ? B2 H2A 1.04(6) . ? B2 H2B 1.35(6) . ? C68 H68 0.9500 . ? C68 C69 1.406(9) . ? C52 H52 0.9500 . ? C52 C51 1.390(8) . ? C51 H51 0.9500 . ? C45 H45 0.9500 . ? F19 C83 1.319(11) . ? C4 H4 0.9500 . ? C4 C3 1.374(9) . ? C64 H64 0.9500 . ? C64 C65 1.375(9) . ? C64 C63 1.382(9) . ? C71 H71 0.9500 . ? C71 C70 1.382(10) . ? F16 C81 1.343(10) . ? C65 H65 0.9500 . ? C74 C77 1.544(11) . ? C74 C76 1.540(8) . ? C74 C75 1.528(9) . ? C74 C77A 1.541(14) . ? C74 C75A 1.556(13) . ? C74 C76A 1.577(14) . ? C69 H69 0.9500 . ? C69 C70 1.357(11) . ? F21 C83 1.323(9) . ? C3 H3 0.9500 . ? F6 C76 1.274(9) . ? F27 C85 1.327(12) . ? F8 C77 1.264(11) . ? F15 C80 1.404(11) . ? F13 C80 1.329(11) . ? C63 H63 0.9500 . ? F1 C75 1.243(9) . ? C70 H70 0.9500 . ? F20 C83 1.369(11) . ? F9 C77 1.320(10) . ? F23 C84 1.313(11) . ? C78 C81 1.524(10) . ? C78 C80 1.515(11) . ? C78 C79 1.536(11) . ? C78 C81A 1.559(15) . ? C78 C80A 1.518(14) . ? C78 C79A 1.491(14) . ? F18 C81 1.364(11) . ? C82 C83 1.510(10) . ? C82 C84 1.650(12) . ? C82 C85 1.508(13) . ? C82 C84A 1.564(15) . ? C82 C83A 1.605(15) . ? C82 C85A 1.539(14) . ? F26 C85 1.384(11) . ? F17 C81 1.304(11) . ? F24 C84 1.307(11) . ? F7 C77 1.327(10) . ? F2 C75 1.330(12) . ? C76 F4 1.323(11) . ? F10 C79 1.327(9) . ? C73 H73A 0.9800 . ? C73 H73B 0.9800 . ? C73 H73C 0.9800 . ? F12 C79 1.355(11) . ? F11 C79 1.327(11) . ? F25 C85 1.335(11) . ? F22 C84 1.397(12) . ? F14 C80 1.300(10) . ? C73A H73D 0.9800 . ? C73A H73E 0.9800 . ? C73A H73F 0.9800 . ? C73A N1A 1.476(13) . ? C86A C89A 1.541(17) . ? C86A C87A 1.521(16) . ? C86A C88A 1.526(16) . ? C89A F34A 1.361(14) . ? C89A F36A 1.331(14) . ? C89A F35A 1.341(14) . ? C87A F29A 1.342(14) . ? C87A F28A 1.364(14) . ? C87A F30A 1.384(14) . ? C88A F32A 1.357(14) . ? C88A F31A 1.331(14) . ? C88A F33A 1.332(14) . ? N1A H1AA 1.0000 . ? F25A C85A 1.337(13) . ? F27A C85A 1.409(14) . ? F26A C85A 1.318(14) . ? F23A C84A 1.320(14) . ? C84A F24A 1.385(14) . ? C84A F22A 1.336(14) . ? F20A C83A 1.357(14) . ? C83A F19A 1.411(14) . ? C83A F21A 1.404(14) . ? F28 C87 1.342(13) . ? F29 C87 1.331(13) . ? C87 F30 1.357(13) . ? C87 C86 1.537(15) . ? F34 C89 1.331(13) . ? F32 C88 1.358(12) . ? C88 F33 1.381(13) . ? C88 F31 1.357(11) . ? C88 C86 1.546(14) . ? F35 C89 1.349(13) . ? C89 F36 1.374(13) . ? C89 C86 1.542(15) . ? F9A C77A 1.291(14) . ? C77A F8A 1.265(14) . ? C77A F7A 1.299(14) . ? F3A C75A 1.295(14) . ? C75A F2A 1.267(14) . ? C75A F1A 1.265(14) . ? C76A F5A 1.247(14) . ? C76A F6A 1.280(14) . ? C76A F4A 1.281(14) . ? F17A C81A 1.353(14) . ? C81A F16A 1.331(14) . ? C81A F18A 1.318(14) . ? F16A F13A 1.71(4) . ? C80A F13A 1.376(14) . ? C80A F15A 1.351(14) . ? C80A F14A 1.322(14) . ? F12A C79A 1.358(14) . ? C79A F10A 1.343(13) . ? C79A F11A 1.346(13) . ? O6 C86 1.302(13) . ? C36 H36 0.9500 . ? C36 C35 1.395(6) . ? C35 H35 0.9500 . ? C35 C34 1.371(7) . ? C34 H34 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Rh1 Rh2 H2B 80.7(19) . . ? P3 Rh2 Rh1 93.03(3) . . ? P3 Rh2 P4 98.63(4) . . ? P3 Rh2 B2 140.14(13) . . ? P3 Rh2 H2B 172.7(19) . . ? P4 Rh2 Rh1 166.53(3) . . ? P4 Rh2 H2B 88.1(19) . . ? B1 Rh2 Rh1 57.32(13) . . ? B1 Rh2 P3 92.16(13) . . ? B1 Rh2 P4 115.17(13) . . ? B1 Rh2 B2 58.65(18) . . ? B1 Rh2 H2B 87.6(19) . . ? B2 Rh2 Rh1 49.38(12) . . ? B2 Rh2 P4 117.55(13) . . ? B2 Rh2 H2B 35.3(19) . . ? Rh2 Rh1 H1B 78(2) . . ? P2 Rh1 Rh2 95.31(3) . . ? P2 Rh1 P1 100.69(4) . . ? P2 Rh1 B1 142.03(12) . . ? P2 Rh1 H1B 173(2) . . ? P1 Rh1 Rh2 162.59(3) . . ? P1 Rh1 H1B 86(2) . . ? B1 Rh1 Rh2 49.70(12) . . ? B1 Rh1 P1 112.99(12) . . ? B1 Rh1 H1B 31(2) . . ? B2 Rh1 Rh2 57.47(13) . . ? B2 Rh1 P2 91.93(14) . . ? B2 Rh1 P1 114.70(14) . . ? B2 Rh1 B1 58.82(18) . . ? B2 Rh1 H1B 84(2) . . ? C24 P2 Rh1 111.03(13) . . ? C31 P2 Rh1 121.10(14) . . ? C31 P2 C24 103.24(19) . . ? C25 P2 Rh1 116.41(13) . . ? C25 P2 C24 102.56(19) . . ? C25 P2 C31 100.13(18) . . ? C37 P3 Rh2 116.66(13) . . ? C37 P3 C43 101.34(18) . . ? C37 P3 C49 101.75(18) . . ? C43 P3 Rh2 119.75(13) . . ? C43 P3 C49 102.35(18) . . ? C49 P3 Rh2 112.51(13) . . ? C7 P1 Rh1 113.41(13) . . ? C7 P1 C1 99.5(2) . . ? C7 P1 C13 102.76(19) . . ? C1 P1 Rh1 116.96(14) . . ? C1 P1 C13 103.2(2) . . ? C13 P1 Rh1 118.41(14) . . ? C67 P4 Rh2 117.59(16) . . ? C67 P4 C61 100.6(2) . . ? C60 P4 Rh2 118.40(13) . . ? C60 P4 C67 101.7(2) . . ? C60 P4 C61 101.6(2) . . ? C61 P4 Rh2 114.20(15) . . ? O3 Al1 O6 110.4(5) . . ? O4 Al1 O3 108.1(3) . . ? O4 Al1 O5 111.8(3) . . ? O4 Al1 O6 114.6(4) . . ? O5 Al1 O3 106.9(3) . . ? O5 Al1 O6 104.7(4) . . ? O6A Al1 O3 109.1(9) . . ? O6A Al1 O4 99.4(7) . . ? O6A Al1 O5 120.9(7) . . ? C54 O2 C55 116.9(3) . . ? C19 O1 C18 119.2(3) . . ? O1 C19 C24 119.6(4) . . ? C20 C19 O1 118.3(4) . . ? C20 C19 C24 121.7(4) . . ? C19 C24 P2 120.2(3) . . ? C23 C24 P2 122.9(3) . . ? C23 C24 C19 116.9(4) . . ? C12 C7 P1 119.2(3) . . ? C8 C7 P1 122.2(3) . . ? C8 C7 C12 118.4(4) . . ? C42 C37 P3 122.5(3) . . ? C42 C37 C38 118.4(4) . . ? C38 C37 P3 119.0(3) . . ? C43 C48 H48 119.3 . . ? C47 C48 H48 119.3 . . ? C47 C48 C43 121.3(4) . . ? C24 C23 H23 119.3 . . ? C22 C23 C24 121.5(4) . . ? C22 C23 H23 119.3 . . ? C48 C43 P3 118.3(3) . . ? C44 C43 P3 122.6(3) . . ? C44 C43 C48 119.0(4) . . ? C74 O3 Al1 154.6(4) . . ? C32 C31 P2 117.9(3) . . ? C36 C31 P2 122.6(3) . . ? C36 C31 C32 119.3(4) . . ? C54 C49 P3 119.8(3) . . ? C54 C49 C50 117.4(4) . . ? C50 C49 P3 122.9(3) . . ? O2 C54 C49 119.5(4) . . ? O2 C54 C53 118.8(4) . . ? C49 C54 C53 121.6(4) . . ? C37 C42 H42 119.8 . . ? C41 C42 C37 120.4(4) . . ? C41 C42 H42 119.8 . . ? C39 C40 H40 120.3 . . ? C41 C40 H40 120.3 . . ? C41 C40 C39 119.5(4) . . ? C48 C47 H47 120.4 . . ? C48 C47 C46 119.3(5) . . ? C46 C47 H47 120.4 . . ? C30 C25 P2 118.9(3) . . ? C26 C25 P2 122.8(3) . . ? C26 C25 C30 118.3(4) . . ? B1 N1 H1 112.2 . . ? B2 N1 H1 112.2 . . ? B2 N1 B1 87.5(5) . . ? C73 N1 H1 112.2 . . ? C73 N1 B1 117.2(7) . . ? C73 N1 B2 113.4(7) . . ? C6 C1 P1 123.3(4) . . ? C6 C1 C2 117.1(5) . . ? C2 C1 P1 119.6(4) . . ? C7 C12 H12 119.6 . . ? C11 C12 C7 120.7(5) . . ? C11 C12 H12 119.6 . . ? C49 C50 H50 119.4 . . ? C51 C50 C49 121.1(5) . . ? C51 C50 H50 119.4 . . ? C23 C22 H22 119.8 . . ? C21 C22 C23 120.4(5) . . ? C21 C22 H22 119.8 . . ? C19 C20 H20 120.0 . . ? C19 C20 C21 119.9(4) . . ? C21 C20 H20 120.0 . . ? O2 C55 C60 116.2(4) . . ? C56 C55 O2 121.2(4) . . ? C56 C55 C60 122.5(4) . . ? C40 C39 H39 119.8 . . ? C40 C39 C38 120.4(4) . . ? C38 C39 H39 119.8 . . ? C17 C16 H16 120.2 . . ? C17 C16 C15 119.6(4) . . ? C15 C16 H16 120.2 . . ? C17 C18 O1 121.4(4) . . ? C17 C18 C13 122.3(4) . . ? C13 C18 O1 116.3(4) . . ? C42 C41 H41 119.6 . . ? C40 C41 C42 120.7(4) . . ? C40 C41 H41 119.7 . . ? C78 O4 Al1 157.8(5) . . ? C43 C44 H44 120.4 . . ? C43 C44 C45 119.2(4) . . ? C45 C44 H44 120.4 . . ? C1 C6 H6 119.0 . . ? C5 C6 C1 122.1(5) . . ? C5 C6 H6 119.0 . . ? C37 C38 H38 119.7 . . ? C39 C38 C37 120.6(4) . . ? C39 C38 H38 119.7 . . ? C55 C56 H56 120.8 . . ? C55 C56 C57 118.5(5) . . ? C57 C56 H56 120.8 . . ? C30 C29 H29 120.2 . . ? C28 C29 H29 120.2 . . ? C28 C29 C30 119.7(4) . . ? C31 C32 H32 120.0 . . ? C33 C32 C31 120.0(4) . . ? C33 C32 H32 120.0 . . ? C16 C17 H17 120.5 . . ? C18 C17 C16 119.0(5) . . ? C18 C17 H17 120.5 . . ? C72 C67 P4 119.4(4) . . ? C72 C67 C68 118.6(5) . . ? C68 C67 P4 121.9(4) . . ? C55 C60 P4 118.2(3) . . ? C59 C60 P4 124.3(3) . . ? C59 C60 C55 117.5(4) . . ? C82 O5 Al1 159.7(6) . . ? C7 C8 H8 119.8 . . ? C9 C8 C7 120.4(5) . . ? C9 C8 H8 119.8 . . ? C60 C59 H59 119.5 . . ? C58 C59 C60 121.0(5) . . ? C58 C59 H59 119.5 . . ? C11 C10 H10 120.3 . . ? C11 C10 C9 119.5(5) . . ? C9 C10 H10 120.3 . . ? C22 C21 C20 119.6(4) . . ? C22 C21 H21 120.2 . . ? C20 C21 H21 120.2 . . ? C25 C30 H30 119.5 . . ? C29 C30 C25 121.1(4) . . ? C29 C30 H30 119.5 . . ? C25 C26 H26 119.8 . . ? C27 C26 C25 120.4(4) . . ? C27 C26 H26 119.8 . . ? C29 C28 H28 120.0 . . ? C27 C28 C29 120.1(4) . . ? C27 C28 H28 120.0 . . ? C18 C13 P1 118.1(3) . . ? C18 C13 C14 117.7(4) . . ? C14 C13 P1 124.2(4) . . ? C16 C15 H15 119.8 . . ? C14 C15 C16 120.4(4) . . ? C14 C15 H15 119.8 . . ? C66 C61 P4 118.8(4) . . ? C62 C61 P4 122.7(4) . . ? C62 C61 C66 118.4(5) . . ? C32 C33 H33 119.8 . . ? C32 C33 C34 120.4(5) . . ? C34 C33 H33 119.8 . . ? C59 C58 H58 119.9 . . ? C59 C58 C57 120.2(5) . . ? C57 C58 H58 119.9 . . ? C56 C57 H57 119.8 . . ? C58 C57 C56 120.4(4) . . ? C58 C57 H57 119.8 . . ? C47 C46 H46 120.1 . . ? C45 C46 C47 119.8(4) . . ? C45 C46 H46 120.1 . . ? C12 C11 H11 119.8 . . ? C10 C11 C12 120.4(5) . . ? C10 C11 H11 119.8 . . ? Rh2 B1 Rh1 72.97(15) . . ? Rh2 B1 H1A 123(3) . . ? Rh2 B1 H1B 112(3) . . ? Rh1 B1 H1A 140(3) . . ? Rh1 B1 H1B 45(3) . . ? N1 B1 Rh2 106.1(4) . . ? N1 B1 Rh1 86.6(4) . . ? N1 B1 H1A 117(3) . . ? N1 B1 H1B 97(3) . . ? N1A B1 Rh2 96.7(5) . . ? N1A B1 Rh1 97.7(5) . . ? N1A B1 H1A 114(3) . . ? N1A B1 H1B 114(3) . . ? H1A B1 H1B 98(4) . . ? C26 C27 H27 119.8 . . ? C28 C27 C26 120.4(4) . . ? C28 C27 H27 119.8 . . ? C54 C53 H53 120.1 . . ? C52 C53 C54 119.8(5) . . ? C52 C53 H53 120.1 . . ? C6 C5 H5 120.1 . . ? C4 C5 C6 119.9(5) . . ? C4 C5 H5 120.1 . . ? C67 C72 H72 119.5 . . ? C67 C72 C71 121.0(5) . . ? C71 C72 H72 119.5 . . ? C13 C14 H14 119.5 . . ? C15 C14 C13 120.9(5) . . ? C15 C14 H14 119.5 . . ? C61 C66 H66 119.7 . . ? C65 C66 C61 120.6(5) . . ? C65 C66 H66 119.7 . . ? C8 C9 C10 120.6(5) . . ? C8 C9 H9 119.7 . . ? C10 C9 H9 119.7 . . ? C86A O6A Al1 164.1(15) . . ? C61 C62 H62 119.8 . . ? C61 C62 C63 120.5(5) . . ? C63 C62 H62 119.8 . . ? C1 C2 H2 119.9 . . ? C3 C2 C1 120.3(5) . . ? C3 C2 H2 119.9 . . ? Rh2 B2 H2A 145(3) . . ? Rh2 B2 H2B 54(3) . . ? Rh1 B2 Rh2 73.14(15) . . ? Rh1 B2 H2A 123(3) . . ? Rh1 B2 H2B 119(3) . . ? N1 B2 Rh2 97.5(4) . . ? N1 B2 Rh1 95.7(4) . . ? N1 B2 H2A 110(3) . . ? N1 B2 H2B 118(3) . . ? N1A B2 Rh2 87.9(4) . . ? N1A B2 Rh1 106.6(5) . . ? N1A B2 H2A 113(3) . . ? N1A B2 H2B 101(3) . . ? H2A B2 H2B 93(4) . . ? C67 C68 H68 120.3 . . ? C67 C68 C69 119.5(6) . . ? C69 C68 H68 120.3 . . ? C53 C52 H52 120.0 . . ? C53 C52 C51 120.0(4) . . ? C51 C52 H52 120.0 . . ? C50 C51 C52 120.0(5) . . ? C50 C51 H51 120.0 . . ? C52 C51 H51 120.0 . . ? C44 C45 H45 119.4 . . ? C46 C45 C44 121.3(4) . . ? C46 C45 H45 119.4 . . ? C5 C4 H4 120.3 . . ? C5 C4 C3 119.4(5) . . ? C3 C4 H4 120.3 . . ? C65 C64 H64 120.0 . . ? C65 C64 C63 120.0(5) . . ? C63 C64 H64 120.0 . . ? C72 C71 H71 119.9 . . ? C70 C71 C72 120.3(7) . . ? C70 C71 H71 119.9 . . ? C66 C65 H65 119.8 . . ? C64 C65 C66 120.4(5) . . ? C64 C65 H65 119.8 . . ? O3 C74 C77 107.6(6) . . ? O3 C74 C76 108.6(6) . . ? O3 C74 C75 112.2(6) . . ? O3 C74 C77A 123.5(9) . . ? O3 C74 C75A 123.1(8) . . ? O3 C74 C76A 108.4(10) . . ? C76 C74 C77 110.1(7) . . ? C75 C74 C77 108.0(7) . . ? C75 C74 C76 110.3(6) . . ? C77A C74 C75A 98.2(11) . . ? C77A C74 C76A 102.8(11) . . ? C75A C74 C76A 96.0(10) . . ? C68 C69 H69 119.3 . . ? C70 C69 C68 121.3(6) . . ? C70 C69 H69 119.3 . . ? C2 C3 H3 119.4 . . ? C4 C3 C2 121.3(6) . . ? C4 C3 H3 119.4 . . ? C62 C63 H63 120.0 . . ? C64 C63 C62 120.0(6) . . ? C64 C63 H63 120.0 . . ? C71 C70 H70 120.3 . . ? C69 C70 C71 119.3(6) . . ? C69 C70 H70 120.3 . . ? O4 C78 C81 111.6(7) . . ? O4 C78 C80 107.2(7) . . ? O4 C78 C79 109.5(6) . . ? O4 C78 C81A 95.6(10) . . ? O4 C78 C80A 124.1(10) . . ? O4 C78 C79A 111.6(8) . . ? C81 C78 C79 104.6(7) . . ? C80 C78 C81 107.2(6) . . ? C80 C78 C79 116.8(8) . . ? C80A C78 C81A 96.4(11) . . ? C79A C78 C81A 119.1(12) . . ? C79A C78 C80A 109.2(10) . . ? O5 C82 C83 112.4(7) . . ? O5 C82 C84 105.6(7) . . ? O5 C82 C85 116.3(7) . . ? O5 C82 C84A 104.4(11) . . ? O5 C82 C83A 120.7(10) . . ? O5 C82 C85A 112.7(8) . . ? C83 C82 C84 103.2(7) . . ? C85 C82 C83 112.8(8) . . ? C85 C82 C84 105.1(8) . . ? C84A C82 C83A 102.7(11) . . ? C85A C82 C84A 120.6(12) . . ? C85A C82 C83A 96.3(11) . . ? F8 C77 C74 111.5(8) . . ? F8 C77 F9 98.1(10) . . ? F8 C77 F7 113.3(10) . . ? F9 C77 C74 110.8(8) . . ? F9 C77 F7 116.8(10) . . ? F7 C77 C74 106.4(9) . . ? F5 C76 C74 112.9(6) . . ? F5 C76 F4 96.4(8) . . ? F6 C76 F5 109.4(8) . . ? F6 C76 C74 117.4(7) . . ? F6 C76 F4 106.6(9) . . ? F4 C76 C74 111.9(8) . . ? N1 C73 H73A 109.5 . . ? N1 C73 H73B 109.5 . . ? N1 C73 H73C 109.5 . . ? H73A C73 H73B 109.5 . . ? H73A C73 H73C 109.5 . . ? H73B C73 H73C 109.5 . . ? F19 C83 F21 109.9(9) . . ? F19 C83 F20 99.8(9) . . ? F19 C83 C82 113.2(9) . . ? F21 C83 F20 105.3(9) . . ? F21 C83 C82 115.9(8) . . ? F20 C83 C82 111.2(8) . . ? F3 C75 C74 123.4(8) . . ? F3 C75 F1 115.3(8) . . ? F3 C75 F2 94.3(9) . . ? F1 C75 C74 115.0(7) . . ? F1 C75 F2 90.9(10) . . ? F2 C75 C74 109.0(9) . . ? F23 C84 C82 113.0(10) . . ? F23 C84 F22 108.0(10) . . ? F24 C84 F23 106.1(10) . . ? F24 C84 C82 112.6(8) . . ? F24 C84 F22 103.1(11) . . ? F22 C84 C82 113.3(9) . . ? F16 C81 C78 114.3(8) . . ? F16 C81 F18 103.5(8) . . ? F18 C81 C78 111.3(8) . . ? F17 C81 F16 108.1(9) . . ? F17 C81 C78 114.2(9) . . ? F17 C81 F18 104.5(10) . . ? F27 C85 C82 100.4(9) . . ? F27 C85 F26 115.0(11) . . ? F27 C85 F25 113.5(12) . . ? F26 C85 C82 109.3(9) . . ? F25 C85 C82 109.9(10) . . ? F25 C85 F26 108.5(10) . . ? F15 C80 C78 108.3(8) . . ? F13 C80 F15 108.0(9) . . ? F13 C80 C78 109.2(9) . . ? F14 C80 F15 106.7(11) . . ? F14 C80 F13 115.1(11) . . ? F14 C80 C78 109.3(8) . . ? F10 C79 C78 112.8(8) . . ? F10 C79 F12 108.0(9) . . ? F10 C79 F11 107.7(11) . . ? F12 C79 C78 111.4(9) . . ? F11 C79 C78 111.5(8) . . ? F11 C79 F12 105.0(10) . . ? H73D C73A H73E 109.5 . . ? H73D C73A H73F 109.5 . . ? H73E C73A H73F 109.5 . . ? N1A C73A H73D 109.5 . . ? N1A C73A H73E 109.5 . . ? N1A C73A H73F 109.5 . . ? O6A C86A C89A 105.3(13) . . ? O6A C86A C87A 118.9(16) . . ? O6A C86A C88A 109.3(16) . . ? C87A C86A C89A 106.9(14) . . ? C87A C86A C88A 109.4(13) . . ? C88A C86A C89A 106.2(15) . . ? F34A C89A C86A 111.8(18) . . ? F36A C89A C86A 107.3(17) . . ? F36A C89A F34A 106.4(16) . . ? F36A C89A F35A 117.5(19) . . ? F35A C89A C86A 106.7(17) . . ? F35A C89A F34A 107.3(17) . . ? F29A C87A C86A 107.7(15) . . ? F29A C87A F28A 113.0(17) . . ? F29A C87A F30A 113.0(17) . . ? F28A C87A C86A 122.6(16) . . ? F28A C87A F30A 94.3(15) . . ? F30A C87A C86A 105.4(15) . . ? F32A C88A C86A 95(2) . . ? F31A C88A C86A 104(2) . . ? F31A C88A F32A 118(2) . . ? F31A C88A F33A 113.1(19) . . ? F33A C88A C86A 107(2) . . ? F33A C88A F32A 115(2) . . ? B1 N1A B2 85.8(5) . . ? B1 N1A H1AA 111.0 . . ? B2 N1A H1AA 111.0 . . ? C73A N1A B1 116.1(10) . . ? C73A N1A B2 119.5(11) . . ? C73A N1A H1AA 111.0 . . ? F23A C84A C82 92.4(18) . . ? F23A C84A F24A 113.5(19) . . ? F23A C84A F22A 117(2) . . ? F24A C84A C82 127(2) . . ? F22A C84A C82 98.5(17) . . ? F22A C84A F24A 107.4(18) . . ? F20A C83A C82 109.8(19) . . ? F20A C83A F19A 108.3(18) . . ? F20A C83A F21A 106.1(16) . . ? F19A C83A C82 119.9(18) . . ? F21A C83A C82 108.6(14) . . ? F21A C83A F19A 103.2(16) . . ? F25A C85A C82 110.9(13) . . ? F25A C85A F27A 119.3(17) . . ? F27A C85A C82 103.0(14) . . ? F26A C85A C82 103.4(13) . . ? F26A C85A F25A 108.7(15) . . ? F26A C85A F27A 110.3(16) . . ? F28 C87 F30 100.1(14) . . ? F28 C87 C86 103.5(12) . . ? F29 C87 F28 121.8(15) . . ? F29 C87 F30 104.3(14) . . ? F29 C87 C86 116.7(13) . . ? F30 C87 C86 108.7(14) . . ? F32 C88 F33 104.2(12) . . ? F32 C88 C86 110.9(10) . . ? F33 C88 C86 110.6(12) . . ? F31 C88 F32 114.5(11) . . ? F31 C88 F33 104.0(12) . . ? F31 C88 C86 112.2(11) . . ? F34 C89 F35 109.8(14) . . ? F34 C89 F36 104.8(14) . . ? F34 C89 C86 117.3(14) . . ? F35 C89 F36 106.1(14) . . ? F35 C89 C86 110.5(12) . . ? F36 C89 C86 107.6(12) . . ? F9A C77A C74 106(2) . . ? F9A C77A F7A 108.3(19) . . ? F8A C77A C74 110(2) . . ? F8A C77A F9A 109(2) . . ? F8A C77A F7A 105.6(18) . . ? F7A C77A C74 117.4(18) . . ? F3A C75A C74 124.5(15) . . ? F2A C75A C74 118.5(14) . . ? F2A C75A F3A 100.8(14) . . ? F1A C75A C74 111.9(17) . . ? F1A C75A F3A 97.2(16) . . ? F1A C75A F2A 99.4(16) . . ? F5A C76A C74 104.3(14) . . ? F5A C76A F6A 120(2) . . ? F5A C76A F4A 104.6(17) . . ? F6A C76A C74 103.4(17) . . ? F6A C76A F4A 97.0(17) . . ? F4A C76A C74 129.6(19) . . ? F17A C81A C78 103(2) . . ? F16A C81A C78 107(2) . . ? F16A C81A F17A 104.5(18) . . ? F18A C81A C78 106(2) . . ? F18A C81A F17A 113.7(19) . . ? F18A C81A F16A 121(2) . . ? C81A F16A F13A 104(2) . . ? F13A C80A C78 100.3(17) . . ? F15A C80A C78 99.5(15) . . ? F15A C80A F13A 109.4(18) . . ? F14A C80A C78 116.8(16) . . ? F14A C80A F13A 105.4(16) . . ? F14A C80A F15A 123.1(19) . . ? C80A F13A F16A 91.9(18) . . ? F12A C79A C78 108.1(14) . . ? F10A C79A C78 110.2(14) . . ? F10A C79A F12A 108.5(15) . . ? F10A C79A F11A 108.6(15) . . ? F11A C79A C78 110.3(13) . . ? F11A C79A F12A 111.1(16) . . ? C86 O6 Al1 153.4(9) . . ? C87 C86 C88 105.8(10) . . ? C87 C86 C89 105.8(11) . . ? C89 C86 C88 103.5(11) . . ? O6 C86 C87 113.9(12) . . ? O6 C86 C88 112.6(11) . . ? O6 C86 C89 114.2(10) . . ? C31 C36 H36 120.1 . . ? C31 C36 C35 119.8(4) . . ? C35 C36 H36 120.1 . . ? C36 C35 H35 119.5 . . ? C34 C35 C36 121.0(5) . . ? C34 C35 H35 119.5 . . ? C33 C34 H34 120.3 . . ? C35 C34 C33 119.4(4) . . ? C35 C34 H34 120.3 . . ? _smtbx_masks_special_details ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.000 0.000 738.3 175.8 '3 1,2-C6F2H4' _shelx_res_file ; 116aim17_sq.res created by SHELXL-2014/7 TITL 116aim17_a.res in P-1 CELL 1.54184 14.5138 18.5644 21.462 104.385 102.683 107.545 ZERR 2 0.0002 0.0003 0.0003 0.001 0.001 0.001 LATT 1 SFAC C H Al B F N O P Rh UNIT 178 128 2 4 72 2 12 8 4 SADI N1A C73A N1 C73 SADI N1A B1 N1 B1 N1A B2 N1 B2 SADI C82 C83 C82 C83A C82 C85 C82 C85A C82 C84 C82 C84A SADI C83 F19 C83 F21 C83 F20 C83A F20A C83A F19A C83A F21A C84 F23 C84 F24 = C84 F22 C84A F23A C84A F24A C84A F22A C85 F27 C85 F26 C85 F25 C85A F25A = C85A F27A C85A F26A SADI 0.04 F19 F21 F19 F20 F21 F20 F20A F19A F20A F21A F19A F21A F23 F24 F24 = F22 F22 F23 F23A F24A F24A F22A F23A F22A F25 F27 F25 F26 F27 F26 F25A F27A = F25A F26A F27A F26A SADI 0.04 O5 C83 O5 C83A O5 C85 O5 C85A O5 C84 O5 C84A SADI 0.04 C83 C84 C84 C85 C85 C83 C83A C84A C84A C85A C85A C83A SADI C86A C89A C86A C87A C86A C88A C86 C87 C86 C88 C86 C89 SADI C89A F34A C89A F36A C89A F35A C87 F28 C87 F29 C87 F30 C87A F29A C87A = F28A C87A F30A C88 C86A C88 F32 C88 F33 C88 F31 C88A F32A C88A F31A C88A = F33A C89 F34 C89 F35 C89 F36 SADI 0.04 F34A F36A F34A F35A F36A F35A F28 F29 F28 F30 F29 F30 F29A F28A = F29A F30A F28A F30A F32 F33 F32 F31 F33 F31 F32A F31A F32A F33A F31A F33A = F34 F35 F34 F36 F35 F36 SADI 0.04 O6A C87A O6A C88A C89A O6A O6 C88 O6 C89 C87 O6 SADI 0.04 C89A C87A C87A C88A C88A C89A C87 C88 C88 C89 C89 C87 SADI C74 C77 C74 C76 C74 C75 C74 C77A C74 C75A C74 C76A SADI C75 F3 C75 F1 C75 F2 C75A F3A C75A F2A C75A F1A C76 F5 C76 F6 C76 F4 = C76A F5A C76A F6A C76A F4A C77 F8 C77 F9 C77 F7 C77A F9A C77A F8A C77A F7A SADI 0.04 F3 F2 F3 F1 F2 F1 F3A F2A F3A F1A F2A F1A F5 F6 F5 F4 F6 F4 F5A = F6A F5A F4A F6A F4A F8 F9 F8 F7 F9 F7 F9A F8A F9A F7A F8A F7A SADI 0.04 O3 C77 O3 C76 O3 C75 O3 C77A O3 C75A O3 C76A SADI 0.04 C75 C76 C76 C77 C77 C75 C75A C76A C76A C77A C77A C75A SADI C78 C81 C78 C80 C78 C79 C78 C81A C78 C80A C78 C79A SADI C79 F10 C79 F12 C79 F11 C79A F12A C79A F10A C79A F11A C80 F15 C80 F13 = C80 F14 C80A F13A C80A F15A C80A F14A C81 F16 C81 F18 C81 F17 C81A F17A = C81A F16A C81A F18A SADI 0.04 F10 F12 F10 F11 F12 F11 F12A F10A F12A F11A F10A F11A F15 F13 F15 = F14 F13 F14 F13A F15A F13A F14A F15A F14A F16 F18 F16 F17 F18 F17 F17A F16A = F17A F18A F16A F18A SADI 0.04 O4 C81 O4 C80 O4 C79 O4 C81A O4 C80A O4 C79A SADI 0.04 C79 C80 C80 C81 C81 C79 C79A C80A C80A C81A C81A C79A SADI Al1 O3 Al1 O4 Al1 O5 Al1 O6A Al1 O6 SADI O6 C86 O6A C86A SIMU N1A C73A SIMU N1 C73 SIMU 0.01 0.02 2 C82 C83 C84 C85 F19 F20 F21 F22 F23 F24 F25 F26 F27 SIMU 0.01 0.02 2 C82 C83A C84A C85A F19A F20A F21A F22A F23A F24A F25A F26A = F27A SIMU 0.01 0.02 2 Al1 O6 C86A C89A C87A C88A F35A F34A F36A F28A F29A F30A = F31A F33A F32A SIMU 0.01 0.02 2 Al1 O6 C86 C87 C88 C89 F28 F30 F29 F32 F33 F31 F34 F36 F35 SIMU 0.01 0.02 2 C74 C75 C76 C77 F1 F2 F3 F4 F5 F6 F7 F8 F9 SIMU 0.01 0.02 2 C74 C75A C76A C77A F1A F2A F3A F4A F5A F6A F7A F8A F9A SIMU 0.01 0.02 2 C78 C79 C80 C81 F10 F11 F12 F13 F14 F15 F16 F17 F18 SIMU 0.01 0.02 2 C78 C79A C80A C81A F10A F11A F12A F13A F14A F15A F16A F17A = F18A RIGU N1 C73 RIGU N1A C73A RIGU C82 C83 C84 C85 F19 F20 F21 F22 F23 F24 F25 F26 F27 RIGU C82 C83A C84A C85A F19A F20A F21A F22A F23A F24A F25A F26A F27A RIGU Al1 O6A C86A C89A C87A C88A F35A F34A F36A F28A F29A F30A F31A F33A F32A RIGU Al1 O6 C86A C87 C88 C89 F28 F30 F29 F32 F33 F31 F34 F36 F35 RIGU C74 C75 C76 C77 F1 F2 F3 F4 F5 F6 F7 F8 F9 RIGU C74 C75A C76A C77A F1A F2A F3A F4A F5A F6A F7A F8A F9A RIGU C78 C79 C80 C81 F10 F11 F12 F13 F14 F15 F16 F17 F18 RIGU C78 C79A C80A C81A F10A F11A F12A F13A F14A F15A F16A F17A F18A L.S. 20 0 94 PLAN 20 TEMP -123(2) BOND $H list 4 fmap 2 acta ABIN OMIT 1 2 1 REM REM REM WGHT 0.110300 7.379800 FVAR 0.22246 0.60648 0.70439 0.59813 0.82074 0.78123 RH2 9 0.606762 0.189168 0.318511 11.00000 0.02277 0.03140 = 0.02230 0.00960 0.00742 0.01319 RH1 9 0.764603 0.163362 0.382727 11.00000 0.02567 0.02697 = 0.02595 0.00823 0.00321 0.01221 P2 8 0.864037 0.295658 0.438620 11.00000 0.02889 0.02821 = 0.02367 0.00889 0.00673 0.01187 P3 8 0.637036 0.156809 0.217057 11.00000 0.02351 0.02831 = 0.02307 0.00861 0.00771 0.01096 P1 8 0.865182 0.103342 0.433027 11.00000 0.02818 0.03087 = 0.03161 0.01125 0.00280 0.01423 P4 8 0.450866 0.202725 0.280554 11.00000 0.02600 0.04701 = 0.02850 0.01482 0.01052 0.01935 AL1 3 0.377505 0.629591 0.186036 11.00000 0.03842 0.04534 = 0.03036 0.01693 0.01075 0.01198 O2 7 0.588779 0.305786 0.230730 11.00000 0.03255 0.03662 = 0.02758 0.00981 0.00741 0.01613 O1 7 1.005656 0.216741 0.393451 11.00000 0.03037 0.03425 = 0.02972 0.00842 0.00389 0.01154 C19 1 1.019580 0.288292 0.380656 11.00000 0.02804 0.03594 = 0.02764 0.00979 0.00406 0.00931 C24 1 0.958211 0.331572 0.397032 11.00000 0.02846 0.03213 = 0.02330 0.00528 0.00443 0.00866 C7 1 0.875774 0.020156 0.371884 11.00000 0.03563 0.03130 = 0.03182 0.01394 0.00691 0.01614 C37 1 0.720164 0.100323 0.209396 11.00000 0.03144 0.03107 = 0.02818 0.01154 0.01123 0.01486 C48 1 0.455073 0.029926 0.137214 11.00000 0.03319 0.03988 = 0.02961 0.01252 0.00731 0.01139 AFIX 43 H48 2 0.461086 0.014874 0.176667 11.00000 -1.20000 AFIX 0 C23 1 0.969760 0.399487 0.377487 11.00000 0.03894 0.03690 = 0.03070 0.01228 0.00890 0.01449 AFIX 43 H23 2 0.931309 0.431115 0.388921 11.00000 -1.20000 AFIX 0 C43 1 0.529818 0.098600 0.138539 11.00000 0.02815 0.03149 = 0.02503 0.00643 0.00681 0.01422 O3 7 0.474542 0.600176 0.171856 11.00000 0.07788 0.10295 = 0.07346 0.04251 0.03621 0.06044 C31 1 0.941357 0.331541 0.528562 11.00000 0.03510 0.03012 = 0.02622 0.00792 0.00610 0.01528 C49 1 0.704098 0.246011 0.198199 11.00000 0.02997 0.03142 = 0.02747 0.01008 0.00778 0.01168 C54 1 0.672372 0.310397 0.208113 11.00000 0.03075 0.03099 = 0.02861 0.01037 0.00786 0.00892 C42 1 0.689637 0.026514 0.158382 11.00000 0.03544 0.03558 = 0.02834 0.00504 0.00469 0.01593 AFIX 43 H42 2 0.621819 0.002108 0.127949 11.00000 -1.20000 AFIX 0 C40 1 0.856815 0.023314 0.195080 11.00000 0.04373 0.04859 = 0.03451 0.01150 0.01267 0.03067 AFIX 43 H40 2 0.903818 -0.001949 0.189209 11.00000 -1.20000 AFIX 0 C47 1 0.372580 -0.016629 0.079842 11.00000 0.03518 0.04518 = 0.04005 0.01055 0.00498 0.00834 AFIX 43 H47 2 0.322183 -0.063363 0.079679 11.00000 -1.20000 AFIX 0 C25 1 0.798512 0.366590 0.440992 11.00000 0.02887 0.02851 = 0.02847 0.00864 0.00652 0.00952 PART 1 N1 6 0.586559 0.081388 0.400639 21.00000 0.03377 0.05222 = 0.04968 0.02418 0.01592 0.02015 AFIX 13 H1 2 0.625192 0.053013 0.422628 21.00000 -1.20000 AFIX 0 PART 0 C1 1 0.818397 0.051569 0.488883 11.00000 0.03362 0.04222 = 0.03802 0.01520 0.00937 0.01890 C12 1 0.787324 -0.039517 0.322908 11.00000 0.04255 0.03559 = 0.03568 0.01063 0.00464 0.01812 AFIX 43 H12 2 0.723743 -0.033533 0.318775 11.00000 -1.20000 AFIX 0 C50 1 0.788428 0.253386 0.175209 11.00000 0.03646 0.04936 = 0.04138 0.02032 0.01826 0.01817 AFIX 43 H50 2 0.810504 0.209724 0.166384 11.00000 -1.20000 AFIX 0 C22 1 1.035923 0.421574 0.341889 11.00000 0.04475 0.04389 = 0.03370 0.01706 0.01013 0.00812 AFIX 43 H22 2 1.041325 0.467326 0.328439 11.00000 -1.20000 AFIX 0 C20 1 1.085838 0.310430 0.345523 11.00000 0.03836 0.05006 = 0.03682 0.01179 0.01527 0.01839 AFIX 43 H20 2 1.125849 0.279968 0.334750 11.00000 -1.20000 AFIX 0 C55 1 0.492866 0.268179 0.181621 11.00000 0.03340 0.03701 = 0.02790 0.00915 0.00842 0.02037 C39 1 0.887178 0.095266 0.247068 11.00000 0.03090 0.04721 = 0.03205 0.01042 0.00636 0.01890 AFIX 43 H39 2 0.954715 0.118618 0.277860 11.00000 -1.20000 AFIX 0 C16 1 1.200911 0.268151 0.556068 11.00000 0.03607 0.04291 = 0.04564 0.00813 -0.00575 0.01566 AFIX 43 H16 2 1.269403 0.303223 0.581143 11.00000 -1.20000 AFIX 0 C18 1 1.054718 0.218863 0.457634 11.00000 0.02639 0.03607 = 0.03182 0.00873 0.00237 0.01432 C41 1 0.757861 -0.011456 0.151860 11.00000 0.04359 0.04314 = 0.03601 0.00576 0.00832 0.02629 AFIX 43 H41 2 0.736058 -0.061933 0.117231 11.00000 -1.20000 AFIX 0 O4 7 0.357239 0.685291 0.136800 11.00000 0.15167 0.09992 = 0.08497 0.06946 0.07020 0.08808 C44 1 0.522033 0.119011 0.080152 11.00000 0.04238 0.03716 = 0.02571 0.00955 0.00654 0.01460 AFIX 43 H44 2 0.573522 0.164509 0.079469 11.00000 -1.20000 AFIX 0 C6 1 0.811125 -0.026388 0.483142 11.00000 0.04694 0.04093 = 0.04095 0.01947 0.01265 0.02215 AFIX 43 H6 2 0.833363 -0.054041 0.449661 11.00000 -1.20000 AFIX 0 C38 1 0.819686 0.133560 0.254550 11.00000 0.02803 0.03980 = 0.02586 0.00616 0.00731 0.01535 AFIX 43 H38 2 0.841211 0.182780 0.290643 11.00000 -1.20000 AFIX 0 C56 1 0.474011 0.283959 0.121677 11.00000 0.04515 0.04704 = 0.03441 0.01887 0.01380 0.02460 AFIX 43 H56 2 0.526710 0.320076 0.112214 11.00000 -1.20000 AFIX 0 C29 1 0.684489 0.415601 0.379230 11.00000 0.04045 0.03628 = 0.03511 0.01393 0.00789 0.01811 AFIX 43 H29 2 0.642661 0.413363 0.337421 11.00000 -1.20000 AFIX 0 C32 1 0.894295 0.305803 0.573777 11.00000 0.03763 0.04391 = 0.03050 0.01051 0.00711 0.00978 AFIX 43 H32 2 0.825703 0.268613 0.557304 11.00000 -1.20000 AFIX 0 C17 1 1.154886 0.269466 0.492499 11.00000 0.03416 0.03936 = 0.04388 0.01288 0.00673 0.01721 AFIX 43 H17 2 1.191839 0.304670 0.473353 11.00000 -1.20000 AFIX 0 C67 1 0.334558 0.121314 0.272783 11.00000 0.02764 0.06295 = 0.03682 0.02428 0.01233 0.01646 C60 1 0.416647 0.216826 0.198156 11.00000 0.03017 0.04515 = 0.02548 0.01264 0.00806 0.01999 O5 7 0.416009 0.684029 0.270627 11.00000 0.10566 0.09565 = 0.03928 0.00796 0.02200 0.04592 C8 1 0.968045 0.010686 0.375709 11.00000 0.03737 0.04020 = 0.04006 0.01655 0.01165 0.01994 AFIX 43 H8 2 1.029327 0.051049 0.408012 11.00000 -1.20000 AFIX 0 C59 1 0.319509 0.179121 0.150296 11.00000 0.03074 0.06263 = 0.03826 0.02072 0.00806 0.02073 AFIX 43 H59 2 0.266486 0.143210 0.159672 11.00000 -1.20000 AFIX 0 C10 1 0.882599 -0.116548 0.284975 11.00000 0.07079 0.04523 = 0.03908 0.01407 0.02070 0.03006 AFIX 43 H10 2 0.885129 -0.163151 0.255773 11.00000 -1.20000 AFIX 0 C21 1 1.094112 0.377552 0.325803 11.00000 0.04494 0.05356 = 0.03848 0.01638 0.02046 0.01214 AFIX 43 H21 2 1.139550 0.392933 0.301421 11.00000 -1.20000 AFIX 0 C30 1 0.734762 0.363118 0.380182 11.00000 0.03784 0.02965 = 0.02933 0.00757 0.01000 0.01442 AFIX 43 H30 2 0.725828 0.324079 0.338845 11.00000 -1.20000 AFIX 0 C26 1 0.807841 0.422682 0.501003 11.00000 0.04341 0.04079 = 0.02666 0.00511 0.00514 0.01978 AFIX 43 H26 2 0.849720 0.425470 0.543020 11.00000 -1.20000 AFIX 0 C28 1 0.695431 0.471304 0.439414 11.00000 0.04212 0.04151 = 0.04234 0.01035 0.01074 0.02406 AFIX 43 H28 2 0.660865 0.507337 0.439027 11.00000 -1.20000 AFIX 0 C13 1 0.998536 0.165506 0.483309 11.00000 0.02798 0.03283 = 0.03143 0.00644 0.00158 0.01455 C15 1 1.145835 0.214955 0.582833 11.00000 0.03988 0.04257 = 0.04051 0.01443 -0.00240 0.01741 AFIX 43 H15 2 1.177399 0.213375 0.625950 11.00000 -1.20000 AFIX 0 C61 1 0.438114 0.289288 0.336791 11.00000 0.03304 0.05555 = 0.03418 0.01558 0.01507 0.02448 C33 1 0.947671 0.334525 0.642472 11.00000 0.05177 0.05188 = 0.03210 0.01505 0.01205 0.01263 AFIX 43 H33 2 0.915472 0.316934 0.672984 11.00000 -1.20000 AFIX 0 C58 1 0.299314 0.193198 0.089593 11.00000 0.03657 0.07885 = 0.03927 0.01819 -0.00103 0.02042 AFIX 43 H58 2 0.232788 0.166875 0.057450 11.00000 -1.20000 AFIX 0 C57 1 0.376002 0.245790 0.075284 11.00000 0.05014 0.06922 = 0.03009 0.02038 0.00931 0.02946 AFIX 43 H57 2 0.361449 0.255755 0.033586 11.00000 -1.20000 AFIX 0 C46 1 0.363812 0.005661 0.021797 11.00000 0.04560 0.04731 = 0.03148 0.00267 -0.00466 0.01054 AFIX 43 H46 2 0.306566 -0.025342 -0.017805 11.00000 -1.20000 AFIX 0 PART 1 F5 5 0.570705 0.559869 0.079236 51.00000 0.17634 0.08416 = 0.05958 0.03330 0.05351 0.07825 PART 0 C11 1 0.791312 -0.107400 0.280252 11.00000 0.05650 0.03812 = 0.03638 0.00780 0.00542 0.02014 AFIX 43 H11 2 0.730419 -0.147805 0.247562 11.00000 -1.20000 AFIX 0 B1 4 0.595620 0.076552 0.327405 11.00000 0.03108 0.03293 = 0.03589 0.01417 0.01228 0.01188 C27 1 0.756360 0.474631 0.499916 11.00000 0.04884 0.04645 = 0.03402 0.00265 0.00950 0.02645 AFIX 43 H27 2 0.763220 0.512728 0.541196 11.00000 -1.20000 AFIX 0 C53 1 0.725652 0.381521 0.199421 11.00000 0.04850 0.03304 = 0.04678 0.01729 0.01370 0.01279 AFIX 43 H53 2 0.704008 0.425425 0.208178 11.00000 -1.20000 AFIX 0 PART 1 F3 5 0.573291 0.477968 0.242622 51.00000 0.20281 0.13100 = 0.08359 0.07132 0.07308 0.13078 PART 0 C5 1 0.772595 -0.064857 0.524581 11.00000 0.05110 0.04342 = 0.04789 0.02331 0.01333 0.02004 AFIX 43 H5 2 0.767030 -0.118614 0.518660 11.00000 -1.20000 AFIX 0 C72 1 0.330473 0.043140 0.255353 11.00000 0.03870 0.06023 = 0.04158 0.01416 0.01760 0.01315 AFIX 43 H72 2 0.389997 0.033077 0.252204 11.00000 -1.20000 AFIX 0 C14 1 1.046467 0.164993 0.547240 11.00000 0.03638 0.04196 = 0.03572 0.01522 0.00109 0.01802 AFIX 43 H14 2 1.009665 0.129539 0.566262 11.00000 -1.20000 AFIX 0 C66 1 0.454674 0.297785 0.405294 11.00000 0.05354 0.07477 = 0.04037 0.01988 0.02043 0.04046 AFIX 43 H66 2 0.475521 0.260648 0.422307 11.00000 -1.20000 AFIX 0 C9 1 0.971210 -0.057242 0.332713 11.00000 0.04938 0.05031 = 0.04683 0.02480 0.02079 0.03000 AFIX 43 H9 2 1.034644 -0.063249 0.335960 11.00000 -1.20000 AFIX 0 PART 2 O6A 7 0.266045 0.549716 0.149308 -41.00000 0.07413 0.12237 = 0.06221 0.04173 -0.00113 -0.02900 PART 0 C62 1 0.408300 0.345093 0.313324 11.00000 0.04849 0.06300 = 0.04120 0.01999 0.01949 0.03551 AFIX 43 H62 2 0.396453 0.340311 0.266882 11.00000 -1.20000 AFIX 0 C2 1 0.785059 0.090062 0.538798 11.00000 0.09041 0.05125 = 0.07993 0.03368 0.05741 0.04501 AFIX 43 H2 2 0.786912 0.142800 0.543619 11.00000 -1.20000 AFIX 0 B2 4 0.649292 0.173751 0.424154 11.00000 0.03747 0.04053 = 0.02928 0.01420 0.01298 0.01596 C68 1 0.247912 0.135072 0.280220 11.00000 0.03897 0.07758 = 0.07471 0.04073 0.02752 0.02947 AFIX 43 H68 2 0.249477 0.188300 0.293879 11.00000 -1.20000 AFIX 0 C52 1 0.809210 0.387864 0.178238 11.00000 0.04313 0.04149 = 0.05998 0.02647 0.01600 0.00289 AFIX 43 H52 2 0.845898 0.436326 0.172531 11.00000 -1.20000 AFIX 0 C51 1 0.840353 0.323350 0.165079 11.00000 0.03811 0.05487 = 0.05189 0.02810 0.02098 0.01204 AFIX 43 H51 2 0.897177 0.327179 0.149156 11.00000 -1.20000 AFIX 0 C45 1 0.437318 0.071710 0.022206 11.00000 0.06005 0.04458 = 0.02880 0.01170 0.00169 0.01743 AFIX 43 H45 2 0.431209 0.086142 -0.017554 11.00000 -1.20000 AFIX 0 PART 1 F19 5 0.372090 0.830573 0.299830 31.00000 0.11631 0.13257 = 0.12541 0.06560 0.06450 0.08009 PART 0 C4 1 0.742500 -0.025443 0.574106 11.00000 0.06441 0.06510 = 0.06607 0.04084 0.03818 0.03038 AFIX 43 H4 2 0.717069 -0.051191 0.603334 11.00000 -1.20000 AFIX 0 C64 1 0.410705 0.414139 0.424895 11.00000 0.06169 0.07753 = 0.04927 0.00796 0.02342 0.04241 AFIX 43 H64 2 0.400056 0.455892 0.454669 11.00000 -1.20000 AFIX 0 C71 1 0.240765 -0.020669 0.242428 11.00000 0.05182 0.06967 = 0.05980 0.01666 0.02611 0.00986 AFIX 43 H71 2 0.239037 -0.073987 0.229856 11.00000 -1.20000 AFIX 0 PART 1 F16 5 0.289421 0.785445 0.025068 61.00000 0.12749 0.07313 = 0.10677 0.04661 -0.02257 0.03708 PART 0 C65 1 0.440969 0.359968 0.448766 11.00000 0.07121 0.09155 = 0.03761 0.01540 0.02363 0.05310 AFIX 43 H65 2 0.452567 0.365116 0.495264 11.00000 -1.20000 AFIX 0 C74 1 0.544769 0.569873 0.184973 11.00000 0.10958 0.07467 = 0.05542 0.02838 0.03406 0.06688 C69 1 0.157979 0.069581 0.267362 11.00000 0.03176 0.10848 = 0.09184 0.04897 0.03282 0.02834 AFIX 43 H69 2 0.098880 0.079115 0.272492 11.00000 -1.20000 AFIX 0 PART 1 F21 5 0.302441 0.784879 0.368556 31.00000 0.12075 0.13682 = 0.08767 0.04549 0.06400 0.09376 PART 0 C3 1 0.749368 0.051782 0.581232 11.00000 0.13272 0.08086 = 0.10473 0.05749 0.09281 0.06855 AFIX 43 H3 2 0.729187 0.079414 0.616014 11.00000 -1.20000 AFIX 0 PART 1 F6 5 0.600279 0.475394 0.120023 51.00000 0.24927 0.12868 = 0.09530 0.05541 0.09650 0.14810 F27 5 0.558932 0.818674 0.341763 31.00000 0.10193 0.11404 = 0.13600 0.02232 0.03227 0.04117 F8 5 0.664348 0.689973 0.191398 51.00000 0.14485 0.09272 = 0.13500 0.00505 0.01282 -0.00404 F15 5 0.401630 0.851412 0.168244 61.00000 0.16583 0.07852 = 0.11977 0.02892 -0.01170 0.03730 F13 5 0.481014 0.842626 0.091389 61.00000 0.11437 0.12590 = 0.22629 0.11156 0.03408 0.00742 PART 0 C63 1 0.395768 0.407880 0.357609 11.00000 0.06396 0.06993 = 0.05224 0.01890 0.02269 0.04458 AFIX 43 H63 2 0.376962 0.446332 0.341486 11.00000 -1.20000 AFIX 0 PART 1 F1 5 0.491285 0.545432 0.275657 51.00000 0.25677 0.16338 = 0.12918 0.09996 0.13041 0.15089 PART 0 C70 1 0.153879 -0.006986 0.247770 11.00000 0.04171 0.08810 = 0.06788 0.03345 0.02567 0.00750 AFIX 43 H70 2 0.091938 -0.050716 0.237832 11.00000 -1.20000 AFIX 0 PART 1 F20 5 0.254591 0.720158 0.262155 31.00000 0.08613 0.14904 = 0.09928 0.03375 0.02369 0.07431 F9 5 0.644101 0.688805 0.278129 51.00000 0.10081 0.17656 = 0.10482 -0.03224 -0.00096 0.04303 F23 5 0.378329 0.693839 0.427178 31.00000 0.20412 0.16037 = 0.08844 0.05762 0.07241 0.11917 PART 0 C78 1 0.371753 0.723259 0.093324 11.00000 0.09186 0.07974 = 0.08903 0.06386 0.04218 0.04529 PART 1 F18 5 0.209424 0.661802 0.007076 61.00000 0.13278 0.09566 = 0.14992 0.04744 -0.02845 0.01860 PART 0 C82 1 0.413663 0.726172 0.327440 11.00000 0.11492 0.13252 = 0.06107 0.02603 0.03723 0.08851 PART 1 F26 5 0.564090 0.736576 0.405038 31.00000 0.12046 0.19481 = 0.08727 0.03744 0.00490 0.10357 F17 5 0.221249 0.748146 0.096581 61.00000 0.13993 0.16926 = 0.17195 0.08728 0.05441 0.10947 F24 5 0.400480 0.604434 0.357691 31.00000 0.16277 0.13770 = 0.12838 0.06572 0.08767 0.09387 F7 5 0.718353 0.608714 0.231292 51.00000 0.09103 0.22075 = 0.17038 0.07833 0.02150 0.07669 F2 5 0.437168 0.457053 0.198233 51.00000 0.22082 0.16810 = 0.17462 0.11413 0.05749 0.07387 C77 1 0.648104 0.640675 0.222881 51.00000 0.08169 0.12647 = 0.07171 0.01207 0.01904 0.04340 C76 1 0.547528 0.518997 0.117258 51.00000 0.14876 0.06462 = 0.05482 0.02297 0.04764 0.06497 F10 5 0.377027 0.690441 -0.020380 61.00000 0.18272 0.21662 = 0.09464 0.10011 0.08028 0.12781 C73 1 0.482683 0.061630 0.407273 21.00000 0.03786 0.05243 = 0.04556 0.01720 0.01924 0.01232 AFIX 137 H73A 2 0.443368 0.003907 0.384754 21.00000 -1.50000 H73B 2 0.448202 0.091541 0.386001 21.00000 -1.50000 H73C 2 0.488073 0.076429 0.455434 21.00000 -1.50000 AFIX 0 F12 5 0.497129 0.682767 0.055178 61.00000 0.13591 0.25296 = 0.16702 0.13792 0.09749 0.12113 F4 5 0.455039 0.471050 0.075676 51.00000 0.19406 0.13752 = 0.10230 -0.02515 0.03554 0.03387 F11 5 0.346370 0.594907 0.020683 61.00000 0.22945 0.12201 = 0.11975 0.03696 0.07435 0.09285 F25 5 0.501814 0.830751 0.430501 31.00000 0.14075 0.17106 = 0.10091 -0.02919 0.00724 0.07906 F22 5 0.258713 0.617862 0.330289 31.00000 0.14458 0.17003 = 0.13478 0.06822 0.07279 0.06869 C83 1 0.338621 0.767011 0.317759 31.00000 0.08795 0.11864 = 0.08086 0.04304 0.04827 0.07511 C75 1 0.525249 0.519122 0.230408 51.00000 0.16488 0.09393 = 0.08814 0.05561 0.07417 0.09504 C84 1 0.363316 0.660816 0.362295 31.00000 0.13603 0.13348 = 0.08584 0.04735 0.06564 0.08928 F14 5 0.521329 0.803717 0.179864 61.00000 0.12663 0.12324 = 0.23261 0.08369 -0.07760 -0.00497 C81 1 0.274590 0.731679 0.057414 61.00000 0.10629 0.07999 = 0.11897 0.05360 0.01673 0.05267 C85 1 0.515456 0.781604 0.379374 31.00000 0.11565 0.13781 = 0.09337 0.02068 0.01741 0.07916 C80 1 0.449530 0.807258 0.133765 61.00000 0.10509 0.07912 = 0.14563 0.06682 -0.00260 0.02702 C79 1 0.397450 0.672898 0.036138 61.00000 0.13538 0.13393 = 0.09199 0.07415 0.06142 0.08124 PART 0 PART 2 C73A 1 0.556685 0.026347 0.425246 -21.00000 0.06460 0.04752 = 0.04955 0.03156 0.01685 0.02120 AFIX 137 H73D 2 0.499505 -0.024219 0.397459 -21.00000 -1.50000 H73E 2 0.549269 0.045380 0.470044 -21.00000 -1.50000 H73F 2 0.620859 0.017632 0.430424 -21.00000 -1.50000 AFIX 0 C86A 1 0.188102 0.482795 0.135873 -41.00000 0.10684 0.15053 = 0.10376 0.06204 0.00089 -0.03101 C89A 1 0.097657 0.488865 0.087112 -41.00000 0.11448 0.18305 = 0.10215 0.05562 -0.00761 -0.01762 F34A 5 0.108242 0.481469 0.024617 -41.00000 0.16457 0.19573 = 0.10673 0.06102 0.00349 -0.00119 F36A 5 0.014484 0.426865 0.078369 -41.00000 0.10416 0.20815 = 0.12393 0.04884 -0.02281 -0.03220 F35A 5 0.098729 0.562739 0.113340 -41.00000 0.14331 0.21035 = 0.13596 0.05033 -0.01769 0.01300 C87A 1 0.153416 0.464386 0.194053 -41.00000 0.11893 0.18593 = 0.10744 0.07294 0.00611 -0.03922 F29A 5 0.235720 0.496842 0.249811 -41.00000 0.14705 0.20498 = 0.12389 0.09651 -0.02487 -0.06316 F28A 5 0.069294 0.474759 0.206640 -41.00000 0.10326 0.21688 = 0.08173 0.06871 0.00967 -0.04700 F30A 5 0.110563 0.381521 0.173709 -41.00000 0.17499 0.19108 = 0.12558 0.08477 0.01404 -0.04740 C88A 1 0.207756 0.411753 0.095880 -41.00000 0.16079 0.17072 = 0.13911 0.04679 0.00125 -0.00374 F32A 5 0.257354 0.399698 0.151392 -41.00000 0.20926 0.18608 = 0.16479 0.05531 -0.01087 0.01792 F31A 5 0.115239 0.357891 0.057903 -41.00000 0.20041 0.20643 = 0.17804 0.04817 -0.01171 -0.01068 F33A 5 0.265111 0.437936 0.059396 -41.00000 0.20987 0.18790 = 0.16175 0.05086 0.02810 0.01845 N1A 6 0.557320 0.086979 0.391819 -21.00000 0.03546 0.02530 = 0.03502 0.01714 0.01655 0.01132 AFIX 13 H1AA 2 0.489670 0.092469 0.381190 -21.00000 -1.20000 AFIX 0 F25A 5 0.483433 0.766133 0.447031 -31.00000 0.14116 0.12294 = 0.04972 0.02543 0.02131 0.08862 F27A 5 0.587949 0.770134 0.376165 -31.00000 0.12461 0.19107 = 0.11184 0.05656 0.02088 0.10033 F26A 5 0.483415 0.656982 0.381777 -31.00000 0.17051 0.13247 = 0.05355 0.01888 0.00597 0.09268 F23A 5 0.321725 0.688392 0.384619 -31.00000 0.16118 0.18247 = 0.11031 0.02017 0.05293 0.05642 C84A 1 0.298929 0.693183 0.323144 -31.00000 0.13815 0.16746 = 0.10750 0.01713 0.04591 0.07792 F24A 5 0.221410 0.624857 0.275127 -31.00000 0.18943 0.21248 = 0.15789 0.01418 0.03370 0.06467 F22A 5 0.276681 0.756191 0.316370 -31.00000 0.13440 0.17074 = 0.13775 0.01963 0.04952 0.07954 F20A 5 0.403607 0.836722 0.288842 -31.00000 0.16916 0.13826 = 0.11453 0.02444 0.04736 0.10659 C83A 1 0.440254 0.820865 0.345603 -31.00000 0.14088 0.13873 = 0.10592 0.02444 0.03585 0.08255 F19A 5 0.541880 0.875365 0.379198 -31.00000 0.15397 0.14274 = 0.13122 0.03345 0.02847 0.06058 F21A 5 0.388524 0.844284 0.390136 -31.00000 0.13988 0.12323 = 0.11945 0.01639 0.05047 0.08131 C85A 1 0.497504 0.732503 0.388922 -31.00000 0.13890 0.14043 = 0.06804 0.02041 0.02632 0.09207 PART 0 PART 1 F28 5 0.109617 0.505816 0.221177 41.00000 0.14563 0.19503 = 0.14952 0.03941 0.05904 0.08623 F29 5 0.002184 0.470475 0.110880 41.00000 0.07949 0.16915 = 0.17136 0.01694 0.01896 0.01855 C87 1 0.093755 0.508222 0.157838 41.00000 0.09435 0.12829 = 0.14630 0.02945 0.02812 0.01889 F30 5 0.111258 0.587316 0.170451 41.00000 0.14378 0.13424 = 0.21487 0.03249 0.02570 0.04357 F34 5 0.081000 0.406083 0.020739 41.00000 0.16988 0.17850 = 0.13353 0.03503 -0.01319 -0.02705 F32 5 0.225235 0.417283 0.209175 41.00000 0.11971 0.10919 = 0.13620 0.06982 0.06620 0.03488 C88 1 0.174723 0.408933 0.144939 41.00000 0.09965 0.09346 = 0.12459 0.03806 0.05005 -0.00491 F33 5 0.223622 0.374033 0.105515 41.00000 0.15405 0.14014 = 0.14551 0.00063 0.05585 0.02734 F31 5 0.076983 0.355315 0.120220 41.00000 0.11113 0.10201 = 0.18065 0.01740 0.04878 -0.03207 F35 5 0.240317 0.482704 0.042136 41.00000 0.16399 0.19467 = 0.09211 0.04485 0.01919 0.00164 C89 1 0.156290 0.474963 0.061235 41.00000 0.11410 0.14550 = 0.10058 0.05288 -0.00281 -0.01984 F36 5 0.124287 0.533603 0.047755 41.00000 0.13368 0.16168 = 0.09744 0.06225 -0.01923 -0.01539 PART 0 PART 2 F9A 5 0.707587 0.646447 0.198329 -51.00000 0.14894 0.11036 = 0.11100 0.02454 0.04351 0.05524 C77A 1 0.633907 0.582081 0.155603 -51.00000 0.12240 0.09242 = 0.07612 0.02879 0.04370 0.06432 F8A 5 0.608709 0.592742 0.099316 -51.00000 0.11426 0.10350 = 0.08162 0.03918 0.05121 0.06112 F7A 5 0.668229 0.524659 0.144310 -51.00000 0.10131 0.08648 = 0.06580 0.02898 0.04446 0.05825 F3A 5 0.662572 0.540972 0.272505 -51.00000 0.11121 0.07256 = 0.04125 0.01764 0.02574 0.06582 C75A 1 0.604537 0.579586 0.258218 -51.00000 0.11748 0.08627 = 0.05295 0.01926 0.02690 0.06846 F2A 5 0.556609 0.573964 0.300631 -51.00000 0.09022 0.07877 = 0.01957 0.00723 0.00285 0.06842 F1A 5 0.671010 0.649686 0.289412 -51.00000 0.12584 0.08531 = 0.04823 0.01164 0.01260 0.06575 C76A 1 0.490762 0.475633 0.160078 -51.00000 0.13101 0.07689 = 0.06505 0.02203 0.02931 0.05604 F5A 5 0.492812 0.452964 0.100802 -51.00000 0.13440 0.03809 = 0.05679 0.01739 0.02324 0.06050 F6A 5 0.541005 0.456167 0.205589 -51.00000 0.14214 0.06917 = 0.07702 0.02519 0.02122 0.05396 F4A 5 0.401588 0.432244 0.157247 -51.00000 0.13599 0.05705 = 0.06876 0.01256 0.03144 0.05304 F17A 5 0.211380 0.698782 0.099733 -61.00000 0.09905 0.12462 = 0.15739 0.06434 0.04549 0.03850 C81A 1 0.256859 0.691851 0.051034 -61.00000 0.10517 0.10959 = 0.12924 0.06049 0.03233 0.04374 F16A 5 0.244876 0.746665 0.023630 -61.00000 0.11640 0.11362 = 0.13547 0.06227 0.02996 0.04550 F18A 5 0.233070 0.617064 0.013076 -61.00000 0.13418 0.11720 = 0.15688 0.04637 0.01373 0.04319 C80A 1 0.391704 0.811916 0.108406 -61.00000 0.11310 0.09380 = 0.11856 0.05798 0.03912 0.04691 F13A 5 0.365868 0.814146 0.043463 -61.00000 0.12936 0.11339 = 0.12630 0.06626 0.03246 0.04066 F15A 5 0.316322 0.816302 0.134736 -61.00000 0.12816 0.10109 = 0.13655 0.07359 0.05563 0.07011 F14A 5 0.487520 0.862432 0.138004 -61.00000 0.10499 0.06191 = 0.12210 0.04839 0.03441 0.04753 F12A 5 0.537936 0.733533 0.107090 -61.00000 0.07433 0.10939 = 0.09773 0.06814 0.05339 0.03429 C79A 1 0.444460 0.702913 0.059541 -61.00000 0.09078 0.08004 = 0.09014 0.05751 0.04611 0.04221 F10A 5 0.450427 0.736374 0.011047 -61.00000 0.10407 0.08995 = 0.09093 0.06556 0.05865 0.04814 F11A 5 0.413075 0.622838 0.030731 -61.00000 0.09295 0.06867 = 0.06558 0.04564 0.04945 0.04440 PART 0 PART 1 O6 7 0.271905 0.547664 0.173957 41.00000 0.05603 0.07938 = 0.07438 0.04314 0.00845 -0.00622 C86 1 0.182967 0.491532 0.138343 41.00000 0.07364 0.09601 = 0.10224 0.05468 0.02775 -0.00643 PART 0 H2A 2 0.663558 0.200339 0.476062 11.00000 0.04295 H1A 2 0.547006 0.016254 0.283284 11.00000 0.05482 H2B 2 0.599980 0.220527 0.407386 11.00000 0.05234 H1B 2 0.678801 0.068555 0.336933 11.00000 0.04808 C36 1 1.040631 0.387184 0.553541 11.00000 0.03598 0.03442 = 0.03185 0.00995 0.00742 0.00969 AFIX 43 H36 2 1.072847 0.406070 0.523517 11.00000 -1.20000 AFIX 0 C35 1 1.093143 0.415397 0.622910 11.00000 0.04071 0.04307 = 0.03326 0.00749 -0.00098 0.00847 AFIX 43 H35 2 1.161217 0.453551 0.639817 11.00000 -1.20000 AFIX 0 C34 1 1.047989 0.388892 0.667060 11.00000 0.05000 0.05029 = 0.02624 0.00760 0.00056 0.01690 AFIX 43 H34 2 1.084996 0.407549 0.714067 11.00000 -1.20000 AFIX 0 HKLF 4 REM 116aim17_a.res in P-1 REM R1 = 0.0579 for 16821 Fo > 4sig(Fo) and 0.0717 for all 20908 data REM 1761 parameters refined using 2901 restraints END WGHT 0.1103 7.3835 REM Highest difference peak 1.756, deepest hole -0.938, 1-sigma level 0.111 Q1 1 0.5485 0.8195 0.2786 11.00000 0.05 1.76 Q2 1 0.7428 0.6683 0.2306 11.00000 0.05 1.04 Q3 1 0.1576 0.6031 0.2256 11.00000 0.05 0.96 Q4 1 0.4415 0.7053 0.3823 11.00000 0.05 0.96 Q5 1 0.7801 0.1859 0.4359 11.00000 0.05 0.95 Q6 1 0.6066 0.7731 0.3282 11.00000 0.05 0.92 Q7 1 0.5148 0.7988 0.0539 11.00000 0.05 0.90 Q8 1 0.6177 0.7887 0.3480 11.00000 0.05 0.89 Q9 1 0.7202 0.5789 0.2019 11.00000 0.05 0.89 Q10 1 0.4788 0.7861 0.1046 11.00000 0.05 0.87 Q11 1 0.4362 0.4951 0.2315 11.00000 0.05 0.87 Q12 1 0.5578 0.7758 0.1395 11.00000 0.05 0.86 Q13 1 0.4475 0.7542 0.3265 11.00000 0.05 0.84 Q14 1 0.6890 0.6858 0.2283 11.00000 0.05 0.81 Q15 1 0.1944 0.5396 0.2699 11.00000 0.05 0.80 Q16 1 0.2405 0.7389 0.1421 11.00000 0.05 0.79 Q17 1 0.5867 0.1624 0.2594 11.00000 0.05 0.78 Q18 1 0.1415 0.6144 0.1225 11.00000 0.05 0.78 Q19 1 0.6107 0.7074 0.1793 11.00000 0.05 0.78 Q20 1 0.1646 0.5254 0.2171 11.00000 0.05 0.76 ; _shelx_res_checksum 15545 _shelx_hkl_file ; 0 0 2 878.42 11.60 0 0 3 12.83 2.37 0 0 4 1921.06 24.33 0 0 5 444.10 13.48 0 0 6 3.56 2.78 0 0 7 1.57 2.50 0 0 8 113.24 9.35 0 0 9 18.69 5.36 0 0 10 116.01 9.13 0 0 10 112.26 10.50 0 0 11 8.81 4.42 0 0 11 9.91 3.81 0 0 12 8.15 4.51 0 0 12 8.10 3.36 0 0 13 81.33 10.15 0 0 14 78.38 10.63 0 0 15 -0.54 3.03 0 0 15 3.37 2.39 0 0 15 0.27 1.86 0 0 16 240.31 18.97 0 0 16 227.77 8.95 0 0 16 262.83 11.07 0 0 17 898.74 17.10 0 0 17 920.65 20.26 0 0 17 918.33 37.28 0 0 18 137.30 6.94 0 0 18 125.69 8.03 0 0 18 130.31 7.73 0 0 19 0.15 2.73 0 0 19 2.42 1.85 0 0 19 -0.09 2.46 0 0 20 224.26 9.17 0 0 20 240.40 10.15 0 0 -21 56.54 4.83 0 0 21 47.83 4.24 0 0 21 53.16 4.93 0 0 -22 -0.39 1.85 0 0 22 -1.33 2.24 0 0 22 -0.13 1.72 0 0 23 -0.78 0.50 0 0 -23 -1.44 1.66 0 0 23 -1.20 1.70 0 0 24 4.31 1.56 0 -1 25 1.33 1.01 0 -1 24 1.26 1.59 0 1 -24 -0.81 1.16 0 -1 23 -1.98 2.05 0 1 -23 1.32 1.45 0 -1 22 13.91 3.04 0 -1 22 9.34 1.97 0 1 -22 14.12 2.65 0 -1 21 7.59 2.28 0 -1 21 8.28 3.04 0 1 -21 8.70 2.68 0 -1 20 86.23 5.31 0 -1 20 80.77 5.70 0 -1 20 84.14 6.65 0 -1 19 464.84 14.52 0 -1 19 473.57 12.39 0 -1 19 444.53 13.13 0 -1 18 274.40 10.66 0 -1 18 279.22 9.99 0 -1 18 289.41 11.78 0 -1 17 74.58 6.41 0 -1 17 73.77 5.36 0 -1 16 201.14 8.42 0 -1 16 216.25 17.63 0 -1 16 225.17 10.14 0 -1 15 81.32 10.53 0 -1 15 68.98 5.12 0 -1 15 81.84 6.20 0 -1 14 67.15 9.30 0 -1 13 256.90 16.86 0 -1 13 260.02 15.27 0 -1 12 369.20 17.36 0 -1 12 363.40 17.47 0 -1 12 372.44 19.20 0 -1 11 19.74 4.75 0 -1 11 19.82 4.94 0 -1 11 21.13 5.55 0 -1 10 103.24 8.90 0 -1 10 86.46 9.23 0 -1 9 483.63 17.27 0 -1 9 480.52 18.21 0 -1 8 11.70 3.64 0 -1 8 8.75 3.50 0 -1 7 292.99 12.40 0 -1 6 7.94 2.68 0 -1 5 281.73 10.10 0 -1 4 74.04 4.65 0 -1 3 550.21 9.80 0 -1 2 1155.94 10.48 0 -1 2 1157.51 12.75 0 -1 2 1170.72 12.75 0 1 1 3541.09 18.75 0 -1 -1 3378.20 17.52 0 1 2 1394.27 15.91 0 -1 -2 1377.62 11.89 0 1 3 869.94 16.34 0 1 3 849.95 15.21 0 1 4 389.06 12.43 0 1 5 1.77 2.61 0 1 6 585.05 17.93 0 1 7 291.21 13.82 0 1 8 150.45 11.26 0 1 9 4.20 4.88 0 1 10 0.26 4.38 0 1 11 431.86 17.88 0 1 11 450.35 22.13 0 1 12 398.77 21.90 0 1 13 82.12 10.70 0 1 14 147.12 14.66 0 1 15 264.27 9.10 0 1 15 283.25 11.07 0 1 16 200.15 9.64 0 1 16 200.54 17.94 0 1 16 194.69 7.95 0 1 17 120.11 14.37 0 1 17 126.13 6.55 0 1 17 130.55 7.98 0 1 18 147.56 8.34 0 1 18 156.85 8.59 0 1 18 153.73 6.95 0 1 19 54.38 5.33 0 1 19 55.53 5.27 0 1 20 4.45 2.67 0 1 20 3.26 2.61 0 -1 -20 4.34 2.65 0 1 21 6.65 2.44 0 1 21 8.46 2.40 0 -1 -21 9.96 2.68 0 1 22 1.86 1.83 0 -1 -22 3.99 1.91 0 1 22 1.26 1.59 0 1 23 -0.06 0.43 0 -1 -23 -3.09 1.57 0 1 24 -1.16 1.21 0 -2 25 47.47 2.89 0 2 -24 40.13 2.57 0 -2 24 49.59 3.75 0 -2 23 0.14 2.22 0 2 -23 1.69 1.50 0 -2 22 2.09 2.52 0 2 -22 -0.18 1.83 0 -2 21 50.53 5.23 0 -2 21 50.48 4.15 0 -2 20 8.88 2.57 0 -2 20 8.97 3.59 0 -2 20 11.22 2.79 0 -2 19 35.99 4.11 0 -2 19 38.10 4.27 0 -2 19 29.26 4.54 0 -2 18 481.86 15.00 0 -2 18 471.67 12.83 0 -2 18 469.82 13.51 0 -2 17 202.07 8.73 0 -2 17 213.30 9.29 0 -2 17 227.99 10.51 0 -2 16 41.66 4.94 0 -2 16 42.39 7.54 0 -2 16 36.46 4.09 0 -2 15 99.27 11.57 0 -2 15 102.99 6.94 0 -2 14 115.63 11.66 0 -2 14 122.94 11.09 0 -2 13 11.48 4.24 0 -2 13 8.76 4.11 0 -2 12 17.32 4.80 0 -2 12 6.32 3.66 0 -2 12 19.23 4.95 0 -2 11 99.41 9.27 0 -2 11 87.25 8.41 0 -2 11 92.73 9.17 0 -2 10 767.97 23.32 0 -2 10 742.02 23.02 0 -2 9 9.41 3.73 0 -2 9 10.22 3.98 0 -2 9 8.41 3.52 0 -2 8 881.64 22.16 0 -2 8 810.93 20.92 0 -2 8 836.90 20.79 0 -2 7 245.15 10.97 0 -2 7 219.41 9.76 0 -2 7 221.21 10.29 0 -2 6 31.42 4.16 0 -2 6 27.06 3.87 0 -2 6 29.28 3.58 0 -2 5 79.25 4.92 0 -2 5 71.11 5.50 0 -2 5 72.60 5.34 0 -2 4 1045.64 14.16 0 -2 4 1027.90 17.26 0 -2 4 1068.65 17.63 0 -2 3 1630.57 19.44 0 -2 3 1677.77 19.91 0 -2 3 1653.25 14.57 0 -2 2 38.68 2.80 0 -2 1 4860.49 30.31 0 -2 1 4958.98 26.95 0 -2 0 1585.51 14.06 0 -2 -1 349.49 6.73 0 2 1 375.13 7.28 0 2 2 219.85 6.89 0 -2 -2 201.05 6.24 0 -2 -3 222.90 6.72 0 2 3 231.01 8.29 0 2 4 476.38 15.07 0 2 4 459.61 13.34 0 2 5 33.05 4.27 0 2 5 38.93 5.34 0 2 6 135.73 9.82 0 2 7 14.77 4.91 0 2 8 60.77 8.63 0 2 9 6.04 4.96 0 2 10 14.22 5.39 0 2 11 144.27 13.52 0 2 12 262.52 18.73 0 2 13 123.12 13.47 0 2 14 23.90 3.80 0 2 14 22.23 6.43 0 2 15 12.59 3.35 0 2 15 10.49 2.28 0 -2 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-17 9 30.18 4.16 1 -17 9 25.92 4.07 1 -17 9 23.35 4.36 1 -17 10 0.29 2.73 1 -17 10 2.68 2.97 1 -17 10 5.00 2.77 1 -17 10 4.71 2.58 1 -17 10 2.79 2.36 1 -17 11 63.44 5.48 1 -17 11 51.64 5.11 1 -17 11 57.62 5.61 1 -17 11 65.20 5.50 1 -17 11 57.30 6.03 1 -17 12 7.81 2.77 1 -17 12 10.98 3.11 1 -17 12 9.27 2.94 1 -17 12 10.80 3.65 1 -17 13 29.90 4.30 1 -17 13 41.47 4.55 1 -17 13 42.80 4.52 1 -17 13 44.92 5.25 1 -17 13 36.24 4.32 1 -17 14 16.47 3.37 1 -17 14 23.29 3.32 1 -17 14 16.45 3.37 1 -17 14 15.50 3.42 1 -17 15 -1.27 3.24 1 -17 15 5.52 2.70 1 -17 15 6.17 1.90 1 -17 15 3.00 2.42 1 -17 16 27.63 3.82 1 -17 16 23.08 3.72 1 -17 16 23.45 3.68 1 -17 17 10.49 2.76 1 -17 17 9.01 2.88 1 -17 17 11.45 2.96 1 -17 18 146.45 6.52 1 -17 18 155.04 7.21 1 -17 18 157.35 7.28 1 -17 19 21.07 3.16 1 -17 19 26.49 2.88 1 -17 19 23.78 3.16 1 -17 20 65.40 4.24 1 -17 20 62.55 3.43 1 -17 20 63.23 4.41 1 -17 21 87.68 4.33 1 -17 21 84.11 4.47 1 -17 22 51.16 2.95 1 -17 22 49.06 3.06 1 -16 -11 15.34 1.82 1 -16 -10 12.23 1.86 1 -16 -10 11.92 2.12 1 -16 -9 0.81 1.42 1 -16 -9 -0.09 1.95 1 -16 -9 -0.29 1.86 1 -16 -8 57.73 4.34 1 -16 -8 60.99 4.87 1 -16 -8 44.93 3.76 1 -16 -8 61.83 4.62 1 -16 -8 50.97 4.58 1 -16 -7 9.28 3.34 1 -16 -7 6.90 2.11 1 -16 -7 11.96 3.10 1 -16 -7 9.25 2.53 1 -16 -7 6.95 2.67 1 -16 -6 3.37 3.49 1 -16 -6 6.05 3.11 1 -16 -6 3.37 2.59 1 -16 -6 5.74 2.52 1 -16 -6 3.71 1.96 1 -16 -5 83.26 6.42 1 -16 -5 57.85 5.78 1 -16 -5 80.30 6.96 1 -16 -5 72.78 5.37 1 -16 -5 66.42 5.13 1 -16 -4 61.32 6.01 1 -16 -4 65.80 5.15 1 -16 -4 67.55 5.92 1 -16 -4 71.73 7.06 1 -16 -4 66.19 5.23 1 -16 -3 1.29 1.86 1 -16 -3 -4.91 3.29 1 -16 -3 -6.93 4.92 1 -16 -3 -1.60 2.44 1 -16 -3 -6.10 4.44 1 -16 -2 -2.44 3.45 1 -16 -2 -3.46 3.20 1 -16 -2 -1.14 2.30 1 -16 -2 -4.89 2.61 1 -16 -2 -1.02 1.76 1 -16 -2 -3.81 4.40 1 -16 -2 -8.07 4.33 1 -16 -1 -4.37 4.16 1 -16 -1 -5.64 4.00 1 -16 -1 -2.83 4.81 1 -16 -1 -0.76 2.37 1 -16 -1 -2.30 3.51 1 -16 0 -3.33 3.69 1 -16 0 -2.73 3.12 1 -16 0 -1.61 2.59 1 -16 0 -11.61 4.96 1 -16 0 -1.50 4.45 1 -16 1 65.87 7.38 1 -16 1 61.29 6.08 1 -16 1 67.47 5.91 1 -16 1 57.96 6.08 1 -16 2 150.32 8.71 1 -16 2 167.41 10.98 1 -16 2 168.21 9.41 1 -16 2 149.87 9.64 1 -16 3 147.87 9.38 1 -16 3 155.23 10.47 1 -16 3 150.52 7.23 1 -16 3 149.88 8.96 1 -16 3 150.87 8.78 1 -16 4 22.09 3.14 1 -16 4 28.59 5.83 1 -16 4 26.37 4.20 1 -16 4 29.27 4.43 1 -16 4 21.72 4.37 1 -16 5 9.39 3.82 1 -16 5 15.87 3.70 1 -16 5 14.48 2.66 1 -16 5 18.50 5.26 1 -16 5 23.67 4.23 1 -16 6 115.17 7.48 1 -16 6 114.77 7.77 1 -16 6 108.83 7.71 1 -16 6 102.81 8.21 1 -16 6 128.67 9.13 1 -16 6 121.20 7.05 1 -16 6 129.02 9.34 1 -16 7 28.30 4.18 1 -16 7 30.44 3.92 1 -16 7 40.68 5.12 1 -16 7 19.75 4.95 1 -16 7 25.17 4.16 1 -16 7 40.17 6.25 1 -16 7 48.56 6.36 1 -16 7 23.19 4.09 1 -16 8 37.38 6.20 1 -16 8 42.86 5.04 1 -16 8 30.40 4.52 1 -16 8 29.17 3.94 1 -16 8 26.30 4.31 1 -16 8 40.30 5.84 1 -16 8 27.71 4.04 1 -16 9 20.54 3.77 1 -16 9 22.26 4.13 1 -16 9 25.86 3.83 1 -16 9 32.30 6.10 1 -16 9 25.91 5.02 1 -16 9 20.13 3.57 1 -16 9 15.73 3.34 1 -16 9 20.76 3.67 1 -16 10 13.18 3.23 1 -16 10 20.92 4.67 1 -16 10 24.17 6.12 1 -16 10 16.12 3.50 1 -16 10 13.92 3.31 1 -16 10 12.43 3.77 1 -16 10 15.81 3.50 1 -16 11 3.51 2.70 1 -16 11 1.97 3.01 1 -16 11 1.45 2.55 1 -16 11 0.25 2.47 1 -16 11 3.27 2.67 1 -16 12 77.07 6.06 1 -16 12 74.51 6.02 1 -16 12 77.70 6.35 1 -16 12 77.47 6.71 1 -16 13 3.12 2.72 1 -16 13 7.02 3.16 1 -16 13 8.28 2.59 1 -16 13 11.52 3.70 1 -16 14 59.80 5.58 1 -16 14 55.39 5.40 1 -16 14 63.08 5.02 1 -16 14 58.16 5.42 1 -16 15 40.77 4.79 1 -16 15 41.77 4.90 1 -16 15 43.41 4.76 1 -16 16 1.76 2.76 1 -16 16 -1.65 3.14 1 -16 16 -0.48 2.77 1 -16 17 -1.28 2.74 1 -16 17 0.73 2.77 1 -16 17 -2.37 2.92 1 -16 18 96.14 6.29 1 -16 18 92.86 6.20 1 -16 18 83.53 5.39 1 -16 19 151.21 7.44 1 -16 19 149.69 7.32 1 -16 19 135.89 6.05 1 -16 20 119.06 6.24 1 -16 20 126.11 6.22 1 -16 20 111.46 4.73 1 -16 21 1.26 2.09 1 -16 21 -0.84 1.70 1 -16 21 0.34 0.51 1 -16 22 83.66 4.40 1 -16 22 82.81 4.15 1 -16 23 57.89 3.16 1 -16 23 53.44 2.81 1 -15 -12 10.83 1.74 1 -15 -12 10.88 1.99 1 -15 -12 9.90 1.70 1 -15 -11 5.37 1.74 1 -15 -11 2.41 1.79 1 -15 -11 5.77 1.93 1 -15 -10 19.63 3.04 1 -15 -10 17.63 3.04 1 -15 -10 13.74 2.58 1 -15 -9 35.40 3.87 1 -15 -9 26.64 3.40 1 -15 -9 31.16 4.33 1 -15 -9 34.25 4.02 1 -15 -8 -0.63 2.67 1 -15 -8 -0.98 3.05 1 -15 -8 -1.58 2.21 1 -15 -8 -2.71 4.12 1 -15 -7 85.51 6.80 1 -15 -7 100.31 7.19 1 -15 -7 86.28 6.24 1 -15 -6 170.93 8.39 1 -15 -6 186.38 10.22 1 -15 -6 174.53 9.23 1 -15 -5 23.85 4.86 1 -15 -5 21.84 4.62 1 -15 -5 26.59 4.15 1 -15 -5 21.54 3.67 1 -15 -4 99.43 6.61 1 -15 -4 100.44 6.69 1 -15 -4 100.05 8.26 1 -15 -4 109.24 7.61 1 -15 -3 -2.26 4.53 1 -15 -3 -1.11 2.82 1 -15 -3 -2.66 2.47 1 -15 -3 1.16 2.64 1 -15 -3 -1.06 4.10 1 -15 -2 49.88 6.41 1 -15 -2 48.44 4.81 1 -15 -2 56.85 5.10 1 -15 -2 51.52 5.60 1 -15 -2 53.04 5.89 1 -15 -2 52.41 5.07 1 -15 -1 58.00 6.19 1 -15 -1 49.52 5.57 1 -15 -1 53.50 5.76 1 -15 -1 53.67 4.96 1 -15 -1 51.65 6.55 1 -15 -1 59.71 5.34 1 -15 0 15.15 3.33 1 -15 0 16.20 4.65 1 -15 0 21.52 4.50 1 -15 0 19.01 4.14 1 -15 0 28.72 7.74 1 -15 0 18.57 3.25 1 -15 1 2.10 3.27 1 -15 1 -2.77 4.53 1 -15 1 1.70 2.71 1 -15 1 1.97 2.95 1 -15 1 4.39 3.32 1 -15 2 -2.73 4.44 1 -15 2 0.39 2.74 1 -15 2 -2.92 3.08 1 -15 2 -2.35 4.47 1 -15 2 -4.14 3.84 1 -15 3 217.34 11.16 1 -15 3 179.57 9.44 1 -15 3 181.68 10.84 1 -15 3 174.74 10.07 1 -15 3 203.44 18.34 1 -15 3 179.59 7.79 1 -15 4 144.27 8.34 1 -15 4 153.91 9.52 1 -15 4 147.29 7.40 1 -15 4 148.89 15.69 1 -15 4 165.13 10.07 1 -15 4 151.92 9.88 1 -15 5 20.15 5.12 1 -15 5 15.95 5.54 1 -15 5 18.22 3.67 1 -15 5 28.31 4.63 1 -15 5 16.85 3.09 1 -15 5 23.51 5.22 1 -15 5 9.16 3.90 1 -15 5 12.68 4.41 1 -15 6 39.99 5.72 1 -15 6 31.54 5.23 1 -15 6 43.66 6.27 1 -15 6 37.02 4.52 1 -15 6 46.38 5.47 1 -15 6 35.36 4.00 1 -15 6 32.31 7.89 1 -15 6 18.07 5.53 1 -15 7 114.72 8.09 1 -15 7 125.05 8.02 1 -15 7 129.00 7.78 1 -15 7 127.11 8.91 1 -15 7 117.91 6.93 1 -15 7 118.29 7.47 1 -15 7 119.87 14.28 1 -15 7 109.32 12.43 1 -15 7 136.30 9.28 1 -15 8 136.67 7.90 1 -15 8 135.07 8.25 1 -15 8 142.22 7.76 1 -15 8 139.18 7.88 1 -15 8 144.11 8.12 1 -15 8 153.46 15.11 1 -15 8 143.54 8.58 1 -15 8 133.25 14.94 1 -15 8 143.53 9.40 1 -15 9 43.42 4.64 1 -15 9 38.26 7.66 1 -15 9 46.37 5.17 1 -15 9 45.75 4.78 1 -15 9 50.01 5.15 1 -15 9 49.67 4.99 1 -15 9 45.76 9.12 1 -15 9 52.14 5.80 1 -15 9 59.47 7.00 1 -15 10 138.54 15.17 1 -15 10 125.61 7.74 1 -15 10 145.34 9.71 1 -15 10 121.96 7.34 1 -15 10 133.52 7.73 1 -15 10 129.74 8.14 1 -15 10 121.51 7.69 1 -15 10 131.82 8.22 1 -15 10 117.83 14.07 1 -15 11 265.76 11.14 1 -15 11 260.81 10.72 1 -15 11 274.12 21.41 1 -15 11 258.72 10.95 1 -15 11 293.80 13.39 1 -15 11 268.32 11.41 1 -15 11 277.26 10.69 1 -15 11 270.43 20.68 1 -15 12 0.88 2.68 1 -15 12 2.61 3.22 1 -15 12 -1.39 2.42 1 -15 12 -0.56 2.84 1 -15 13 96.83 7.19 1 -15 13 88.33 6.91 1 -15 13 86.55 6.20 1 -15 14 3.29 2.91 1 -15 14 2.04 1.83 1 -15 15 -1.78 3.12 1 -15 15 -5.70 3.68 1 -15 15 -0.77 2.05 1 -15 16 -0.48 2.76 1 -15 16 2.05 2.00 1 -15 16 -2.40 3.18 1 -15 17 82.47 6.39 1 -15 17 76.18 5.60 1 -15 18 34.85 3.76 1 -15 18 28.05 3.54 1 -15 18 39.52 4.86 1 -15 19 22.56 3.04 1 -15 19 32.74 4.27 1 -15 19 30.30 3.34 1 -15 20 97.78 5.99 1 -15 20 100.10 6.10 1 -15 20 82.90 4.32 1 -15 21 79.16 5.11 1 -15 21 79.23 4.95 1 -15 21 66.04 4.08 1 -15 22 8.80 1.75 1 -15 22 11.68 2.42 1 -15 22 11.45 2.16 1 -15 23 52.36 3.39 1 -15 23 47.80 3.02 1 -15 24 60.76 2.92 1 -14 -14 7.82 1.43 1 -14 -13 -0.14 1.35 1 -14 -13 -2.34 1.95 1 -14 -13 -1.15 1.32 1 -14 -12 56.09 4.14 1 -14 -12 50.51 3.98 1 -14 -11 12.60 3.08 1 -14 -11 19.08 3.35 1 -14 -11 17.04 2.93 1 -14 -10 -5.40 4.13 1 -14 -10 -2.81 2.90 1 -14 -9 52.84 5.21 1 -14 -9 47.68 5.51 1 -14 -9 44.73 4.82 1 -14 -8 28.01 5.11 1 -14 -8 35.71 4.75 1 -14 -8 28.19 4.28 1 -14 -7 3.68 3.04 1 -14 -7 -2.34 3.74 1 -14 -7 -2.86 5.01 1 -14 -6 139.56 8.12 1 -14 -6 137.22 9.07 1 -14 -6 143.89 8.67 1 -14 -5 242.20 10.98 1 -14 -5 224.09 11.69 1 -14 -5 236.99 10.24 1 -14 -4 6.21 4.16 1 -14 -4 5.36 2.91 1 -14 -4 -2.59 4.61 1 -14 -3 12.54 2.94 1 -14 -3 7.29 3.91 1 -14 -3 14.88 3.58 1 -14 -3 13.72 4.36 1 -14 -3 11.29 3.19 1 -14 -2 31.05 5.08 1 -14 -2 22.98 4.65 1 -14 -2 27.43 4.53 1 -14 -2 25.29 3.69 1 -14 -2 27.29 7.35 1 -14 -2 25.56 3.90 1 -14 -2 21.64 3.55 1 -14 -1 16.72 3.16 1 -14 -1 20.23 4.34 1 -14 -1 19.75 5.67 1 -14 -1 17.19 3.17 1 -14 -1 15.20 3.91 1 -14 -1 9.47 3.99 1 -14 0 193.01 16.86 1 -14 0 160.26 10.13 1 -14 0 172.05 8.54 1 -14 0 160.77 7.94 1 -14 0 177.94 9.89 1 -14 1 24.40 4.53 1 -14 1 26.55 6.77 1 -14 1 18.35 4.51 1 -14 1 50.23 6.71 1 -14 1 23.65 3.83 1 -14 1 45.61 7.02 1 -14 2 39.88 6.72 1 -14 2 21.83 4.32 1 -14 2 33.95 5.71 1 -14 2 22.58 6.65 1 -14 2 20.97 3.60 1 -14 2 19.36 4.56 1 -14 3 55.63 6.14 1 -14 3 59.26 6.46 1 -14 3 55.82 8.20 1 -14 3 54.06 6.81 1 -14 3 46.37 5.86 1 -14 3 48.01 4.98 1 -14 3 48.50 4.17 1 -14 3 54.56 9.43 1 -14 4 148.78 7.13 1 -14 4 154.21 8.34 1 -14 4 155.32 9.62 1 -14 4 147.98 12.98 1 -14 4 149.47 9.09 1 -14 4 145.81 9.17 1 -14 4 163.80 9.38 1 -14 4 140.73 14.89 1 -14 4 171.03 8.86 1 -14 5 376.83 14.13 1 -14 5 372.46 13.42 1 -14 5 375.75 14.24 1 -14 5 381.47 21.51 1 -14 5 387.26 24.72 1 -14 5 370.74 12.64 1 -14 5 317.35 12.21 1 -14 5 350.59 10.98 1 -14 5 390.48 12.75 1 -14 6 10.78 3.04 1 -14 6 13.23 4.94 1 -14 6 11.88 3.04 1 -14 6 3.82 3.49 1 -14 6 10.83 3.80 1 -14 6 9.86 3.98 1 -14 6 13.91 4.04 1 -14 6 10.90 2.59 1 -14 7 24.93 6.76 1 -14 7 37.70 5.62 1 -14 7 33.65 3.87 1 -14 7 35.66 4.40 1 -14 7 35.27 4.25 1 -14 7 34.56 4.82 1 -14 7 34.22 4.38 1 -14 7 33.10 4.05 1 -14 7 21.98 6.15 1 -14 7 30.65 4.79 1 -14 8 30.89 3.82 1 -14 8 30.75 3.91 1 -14 8 31.17 7.43 1 -14 8 29.17 4.60 1 -14 8 39.34 5.66 1 -14 8 34.27 4.35 1 -14 8 32.74 4.16 1 -14 8 31.75 5.16 1 -14 8 26.92 3.63 1 -14 8 32.02 7.03 1 -14 9 28.29 4.19 1 -14 9 33.03 5.43 1 -14 9 27.65 6.61 1 -14 9 27.05 3.77 1 -14 9 31.03 7.04 1 -14 9 30.14 4.00 1 -14 9 30.02 4.10 1 -14 9 28.20 4.41 1 -14 10 67.36 5.89 1 -14 10 68.85 10.39 1 -14 10 76.70 7.49 1 -14 10 74.93 5.66 1 -14 10 68.68 10.50 1 -14 10 65.66 5.84 1 -14 11 348.48 23.74 1 -14 11 389.59 13.24 1 -14 11 405.60 13.60 1 -14 11 419.29 15.11 1 -14 11 413.61 24.77 1 -14 11 396.43 12.51 1 -14 11 396.67 13.18 1 -14 12 253.07 10.50 1 -14 12 254.53 10.83 1 -14 12 245.89 10.89 1 -14 12 263.75 19.63 1 -14 12 230.03 19.64 1 -14 13 5.79 3.14 1 -14 13 6.00 3.96 1 -14 13 5.79 3.00 1 -14 13 1.44 2.32 1 -14 14 1.78 2.96 1 -14 15 0.27 2.98 1 -14 15 -6.01 3.64 1 -14 15 2.33 2.43 1 -14 16 3.56 3.05 1 -14 16 3.54 2.71 1 -14 16 -1.08 2.78 1 -14 17 42.78 5.10 1 -14 17 36.43 4.11 1 -14 17 39.72 3.76 1 -14 17 34.47 4.48 1 -14 18 88.09 6.73 1 -14 18 81.89 5.45 1 -14 18 86.48 5.15 1 -14 18 72.85 5.83 1 -14 19 56.74 4.10 1 -14 19 53.02 4.15 1 -14 19 42.98 4.42 1 -14 19 53.54 5.29 1 -14 20 1.07 2.58 1 -14 20 3.19 1.67 1 -14 20 -2.92 2.49 1 -14 21 160.51 5.86 1 -14 21 161.68 7.42 1 -14 22 107.59 4.43 1 -14 22 109.17 5.59 1 -14 22 106.86 5.38 1 -14 22 93.73 4.93 1 -14 23 -0.42 1.44 1 -14 23 1.45 1.30 1 -14 23 1.74 1.68 1 -14 23 2.68 0.98 1 -14 24 17.13 1.71 1 -14 24 21.51 2.10 1 -13 -15 -0.87 1.43 1 -13 -15 2.83 1.30 1 -13 -14 2.86 1.80 1 -13 -14 4.44 1.91 -1 13 14 5.90 1.44 -1 13 13 10.65 2.06 1 -13 -13 10.55 2.58 1 -13 -12 1.20 3.37 1 -13 -12 9.78 3.07 -1 13 12 6.09 2.06 1 -13 -11 30.43 4.47 -1 13 11 30.19 3.55 1 -13 -11 41.05 4.84 1 -13 -10 2.43 3.93 1 -13 -10 1.01 3.23 -1 13 10 2.91 2.14 1 -13 -9 5.80 3.53 -1 13 9 3.35 2.30 1 -13 -9 -5.01 5.10 1 -13 -9 -5.01 3.69 1 -13 -8 129.33 8.44 1 -13 -8 140.64 8.66 1 -13 -7 422.11 14.16 1 -13 -7 446.67 14.33 1 -13 -6 16.97 4.89 1 -13 -6 24.17 4.47 -1 13 5 184.26 18.05 1 -13 -5 181.39 9.73 1 -13 -5 173.45 9.20 1 -13 -4 47.11 5.19 1 -13 -4 54.31 6.08 -1 13 3 4.82 4.25 1 -13 -3 0.67 2.75 1 -13 -3 -1.03 3.72 1 -13 -3 -0.61 2.44 1 -13 -3 2.38 3.99 1 -13 -2 -1.83 2.23 1 -13 -2 1.88 2.61 1 -13 -2 3.68 3.58 -1 13 2 -3.93 3.53 1 -13 -2 -1.16 4.03 1 -13 -2 1.12 2.83 1 -13 -1 -1.61 2.11 1 -13 -1 -0.01 3.35 -1 13 1 3.76 4.00 1 -13 -1 -0.01 2.93 1 -13 -1 10.27 5.20 1 -13 -1 2.96 2.83 1 -13 0 43.55 8.03 -1 13 0 45.05 8.15 1 -13 0 60.15 6.46 1 -13 0 44.78 5.24 1 -13 0 41.27 4.83 1 -13 0 55.82 6.73 1 -13 1 7.44 4.05 1 -13 1 10.87 4.61 1 -13 1 -2.20 3.85 1 -13 1 -0.31 3.82 1 -13 2 1.37 3.24 1 -13 2 -1.72 2.40 1 -13 2 2.17 2.44 1 -13 2 0.19 3.41 1 -13 2 5.06 3.49 1 -13 3 27.51 5.42 1 -13 3 24.26 6.31 1 -13 4 60.50 8.20 1 -13 4 55.02 9.14 1 -13 5 156.24 13.25 1 -13 5 174.97 15.96 1 -13 6 453.64 23.33 1 -13 6 454.35 25.44 1 -13 7 112.61 11.99 1 -13 7 116.52 13.05 1 -13 8 73.62 10.15 1 -13 8 95.14 7.18 1 -13 8 89.69 7.06 1 -13 8 82.97 6.01 1 -13 8 81.20 11.10 1 -13 9 164.16 15.23 1 -13 9 175.45 9.68 1 -13 9 163.75 15.45 1 -13 9 168.34 8.55 1 -13 9 168.43 7.89 1 -13 9 175.58 8.63 1 -13 10 191.09 9.14 1 -13 10 194.78 9.33 1 -13 10 199.63 10.38 1 -13 10 182.38 16.61 1 -13 10 191.80 8.48 1 -13 10 213.65 17.63 1 -13 11 15.70 5.36 1 -13 11 25.20 3.79 1 -13 11 15.09 5.11 1 -13 11 20.77 3.64 1 -13 11 21.75 3.74 1 -13 12 106.08 13.16 1 -13 12 130.92 7.57 1 -13 12 121.98 7.10 1 -13 12 125.68 7.56 1 -13 12 134.06 8.07 1 -13 12 119.77 12.90 1 -13 13 112.71 7.64 1 -13 13 119.71 7.49 1 -13 13 92.68 12.32 1 -13 13 110.23 7.14 1 -13 14 1.64 3.23 1 -13 14 5.43 3.16 1 -13 14 6.56 3.17 1 -13 15 25.99 4.14 1 -13 15 18.84 3.41 1 -13 15 24.73 4.20 1 -13 15 28.54 3.54 1 -13 16 20.28 4.07 1 -13 16 17.38 3.17 1 -13 16 20.04 3.05 1 -13 16 20.20 3.91 1 -13 17 66.77 5.13 1 -13 17 61.10 5.55 1 -13 17 70.92 5.12 1 -13 17 66.22 6.15 1 -13 18 9.70 2.49 1 -13 18 10.32 3.41 1 -13 18 9.80 3.07 1 -13 18 8.90 2.48 1 -13 19 30.63 4.00 1 -13 19 40.18 3.89 1 -13 19 38.94 4.66 1 -13 20 19.49 3.61 1 -13 20 22.91 2.94 1 -13 20 17.70 3.32 1 -13 21 5.57 2.35 1 -13 21 7.17 2.75 1 -13 21 10.08 2.29 1 -13 22 74.89 4.17 1 -13 22 78.18 5.01 1 -13 22 84.23 5.14 1 -13 23 115.92 4.50 1 -13 23 106.19 5.18 1 -13 24 0.26 0.90 1 -13 24 -0.42 1.19 1 -13 24 -0.28 1.10 1 -13 24 0.29 1.26 1 -12 -16 15.42 1.93 -1 12 16 10.51 1.55 1 -12 -16 15.34 2.07 1 -12 -15 -1.79 1.98 -1 12 15 -0.99 1.39 1 -12 -14 -1.46 2.46 -1 12 14 0.66 1.71 -1 12 13 12.54 2.68 1 -12 -13 6.52 3.34 1 -12 -13 13.80 3.38 1 -12 -12 18.76 3.90 1 -12 -12 27.31 4.49 -1 12 12 23.50 3.47 1 -12 -11 6.40 3.86 1 -12 -11 -0.17 3.98 -1 12 11 3.50 2.68 1 -12 -10 106.17 7.50 -1 12 10 100.47 6.79 1 -12 -10 119.30 7.93 1 -12 -9 114.49 8.02 1 -12 -9 126.60 8.28 1 -12 -8 93.32 7.46 1 -12 -8 115.11 8.16 1 -12 -7 105.53 7.88 -1 12 7 106.23 14.07 1 -12 -7 114.26 8.18 1 -12 -6 449.97 14.24 1 -12 -6 465.66 14.64 -1 12 6 500.52 29.48 1 -12 -5 5.81 4.35 1 -12 -5 4.19 3.16 -1 12 5 2.65 4.20 1 -12 -4 144.09 8.01 -1 12 4 149.93 15.64 1 -12 -4 162.39 8.72 1 -12 -3 175.20 8.85 1 -12 -3 159.06 8.05 -1 12 3 168.27 15.99 1 -12 -3 180.57 14.71 1 -12 -3 194.41 10.41 -1 12 2 1.15 3.32 1 -12 -2 2.43 2.89 1 -12 -1 3.30 3.69 1 -12 0 8.00 3.66 1 -12 1 23.82 5.76 1 -12 1 31.15 5.68 1 -12 2 29.32 5.32 1 -12 2 23.98 6.24 1 -12 3 1.41 3.42 1 -12 3 3.11 2.64 1 -12 4 100.32 11.48 1 -12 4 107.95 10.17 1 -12 5 0.29 2.40 -1 12 -5 -1.74 2.30 1 -12 6 746.76 28.44 1 -12 7 577.04 25.86 1 -12 8 213.78 16.34 1 -12 9 90.72 10.97 1 -12 10 80.91 10.81 1 -12 11 309.07 21.40 1 -12 11 347.02 13.06 1 -12 11 354.27 12.25 1 -12 11 340.92 11.52 1 -12 12 4.35 3.55 1 -12 12 2.06 2.67 1 -12 12 4.10 2.36 1 -12 12 3.61 2.45 1 -12 12 1.30 2.34 1 -12 13 80.92 6.37 1 -12 13 92.69 6.40 1 -12 13 91.31 6.42 1 -12 13 84.28 11.81 1 -12 14 52.46 4.47 1 -12 14 45.50 5.00 1 -12 14 57.89 5.78 1 -12 14 50.03 9.56 1 -12 15 0.72 2.82 1 -12 15 1.82 2.59 1 -12 15 -2.07 3.20 1 -12 15 1.21 1.92 1 -12 16 29.18 3.67 1 -12 16 23.80 4.21 1 -12 16 20.31 3.27 1 -12 16 22.82 3.93 1 -12 17 1.47 2.90 1 -12 17 -1.33 2.19 1 -12 17 1.62 2.28 1 -12 17 1.64 2.77 1 -12 18 15.26 3.73 1 -12 18 16.64 3.06 1 -12 18 11.50 3.32 1 -12 19 0.59 2.62 1 -12 19 -0.45 2.51 1 -12 19 0.26 2.17 1 -12 20 55.68 5.31 1 -12 20 53.28 5.04 1 -12 20 55.30 4.46 1 -12 21 52.64 4.87 1 -12 21 52.90 4.21 1 -12 21 51.04 4.75 1 -12 22 15.89 2.97 1 -12 22 15.47 2.55 1 -12 22 12.33 2.67 1 -12 23 111.05 5.43 1 -12 23 111.67 5.37 1 -12 23 117.19 4.89 1 -12 24 122.77 4.38 1 -12 24 117.84 4.78 1 -12 24 121.64 4.97 1 -12 25 5.42 1.26 1 -11 -17 -1.52 1.35 -1 11 17 2.92 1.31 -1 11 16 29.06 2.97 1 -11 -16 29.43 2.95 -1 11 15 16.96 2.83 1 -11 -15 18.12 3.02 -1 11 14 -0.24 2.37 1 -11 -14 1.25 2.64 1 -11 -13 59.71 5.59 1 -11 -13 48.26 4.99 -1 11 13 50.22 4.95 1 -11 -12 151.31 8.27 1 -11 -12 156.63 8.76 -1 11 12 148.12 8.22 1 -11 -11 44.87 5.89 1 -11 -11 41.63 5.44 1 -11 -11 40.06 5.20 -1 11 11 40.19 4.88 1 -11 -10 -4.28 4.65 1 -11 -10 6.82 4.14 1 -11 -10 -0.26 3.00 1 -11 -9 225.36 10.57 1 -11 -9 220.64 10.44 1 -11 -9 209.69 10.41 1 -11 -8 351.99 12.94 1 -11 -8 376.30 13.41 1 -11 -8 391.43 13.39 1 -11 -7 34.31 4.83 1 -11 -7 36.19 4.86 1 -11 -7 35.52 5.28 -1 11 7 39.13 9.00 1 -11 -6 172.81 8.82 1 -11 -6 187.71 9.43 1 -11 -6 167.66 8.86 -1 11 5 124.81 14.21 1 -11 -5 123.81 7.32 1 -11 -5 136.75 8.02 1 -11 -5 119.42 7.21 -1 11 4 18.28 6.12 1 -11 -4 19.65 5.33 -1 11 3 134.99 13.97 1 -11 -3 148.07 12.66 1 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-11 20 -0.08 2.00 1 -11 20 1.28 2.45 1 -11 21 45.23 4.15 1 -11 21 47.28 4.72 1 -11 21 45.75 4.73 1 -11 22 102.20 6.17 1 -11 22 110.43 5.59 1 -11 22 105.17 5.97 1 -11 23 0.47 2.02 1 -11 23 4.03 1.97 1 -11 23 4.01 1.79 1 -11 24 121.56 4.73 1 -11 24 117.63 4.82 1 -11 24 126.66 5.35 1 -11 25 134.24 4.50 1 -10 -18 27.76 2.16 -1 10 18 27.74 2.44 1 -10 -17 36.59 3.11 -1 10 17 36.89 3.30 -1 10 16 10.56 2.62 1 -10 -16 9.39 2.51 -1 10 15 0.16 2.41 1 -10 -15 1.87 2.63 1 -10 -14 0.54 2.81 1 -10 -14 -0.50 3.39 1 -10 -14 -8.24 4.16 -1 10 14 1.20 2.67 -1 10 13 1.49 2.73 1 -10 -13 3.69 3.63 1 -10 -13 -5.55 4.13 1 -10 -13 -1.33 3.56 1 -10 -12 20.09 4.48 1 -10 -12 10.60 4.09 1 -10 -12 12.29 3.78 1 -10 -11 179.28 9.68 1 -10 -11 176.65 9.16 1 -10 -11 185.20 9.54 1 -10 -10 97.26 7.24 1 -10 -10 96.93 7.30 -1 10 10 119.78 15.49 1 -10 -10 94.12 7.17 1 -10 -9 46.84 5.38 -1 10 9 51.15 10.43 1 -10 -9 48.99 6.01 1 -10 -9 46.37 5.56 -1 10 8 2.08 4.37 1 -10 -8 2.41 3.00 1 -10 -8 -1.08 3.87 1 -10 -8 4.09 2.68 1 -10 -7 233.20 10.30 1 -10 -7 229.83 10.16 1 -10 -7 222.42 9.89 1 -10 -6 13.96 3.98 1 -10 -6 7.90 2.83 -1 10 6 9.44 4.90 -1 10 5 229.43 18.19 1 -10 -5 257.30 15.35 1 -10 -4 227.75 14.63 -1 10 4 206.99 16.89 1 -10 -3 1.52 2.68 1 -10 -2 26.77 5.72 -1 10 2 28.45 4.85 1 -10 -2 29.45 5.78 1 -10 -1 490.99 22.30 1 -10 -1 473.90 21.15 -1 10 1 434.04 16.85 1 -10 0 172.45 10.44 1 -10 0 180.17 13.64 -1 10 0 184.92 10.81 1 -10 1 88.07 7.88 -1 10 -1 91.01 7.66 -1 10 -2 54.27 6.08 1 -10 2 49.96 6.20 1 -10 3 6.96 3.14 -1 10 -3 12.49 3.65 1 -10 4 23.36 4.73 1 -10 5 276.68 15.45 1 -10 6 777.45 26.49 1 -10 7 228.77 15.06 1 -10 8 144.32 12.51 1 -10 9 312.59 18.73 1 -10 10 682.70 28.89 1 -10 11 11.65 4.49 1 -10 12 108.91 12.43 1 -10 13 84.01 11.41 1 -10 13 84.46 6.16 1 -10 14 4.41 3.26 1 -10 14 0.69 2.21 1 -10 14 -1.26 2.90 1 -10 14 2.46 2.07 1 -10 15 195.38 8.47 1 -10 15 206.50 9.60 1 -10 15 216.07 18.85 1 -10 15 212.40 8.73 1 -10 16 150.93 7.64 1 -10 16 138.14 8.04 1 -10 16 144.53 15.66 1 -10 17 26.55 7.47 1 -10 17 28.09 3.90 1 -10 17 23.30 4.07 1 -10 17 20.36 4.00 1 -10 18 11.72 2.91 1 -10 18 13.22 3.39 1 -10 18 15.98 3.80 1 -10 18 14.71 3.21 1 -10 19 9.27 3.31 1 -10 19 7.76 2.55 1 -10 19 10.58 2.84 1 -10 19 5.48 2.89 1 -10 20 19.84 3.36 1 -10 20 26.00 3.60 1 -10 20 26.25 4.25 1 -10 20 23.35 4.03 1 -10 21 7.38 2.51 1 -10 21 15.17 3.31 1 -10 21 12.40 3.42 1 -10 21 11.26 2.87 1 -10 22 95.01 5.33 1 -10 22 86.90 5.46 1 -10 22 96.63 6.19 1 -10 22 86.67 5.22 1 -10 23 184.22 6.69 1 -10 23 199.52 6.93 1 -10 23 207.50 7.85 1 -10 23 187.80 6.92 1 -10 24 33.77 2.76 1 -10 24 37.19 3.32 1 -10 25 41.40 2.80 -1 9 19 96.35 4.19 -1 9 18 0.42 1.69 1 -9 -18 -0.85 1.60 1 -9 -17 5.62 2.12 -1 9 17 1.51 2.16 1 -9 -16 33.37 4.07 1 -9 -16 32.34 4.19 -1 9 16 33.77 4.25 -1 9 15 13.88 3.59 1 -9 -15 12.31 3.54 1 -9 -15 14.18 3.55 1 -9 -14 16.99 3.97 1 -9 -14 15.98 3.85 1 -9 -14 5.06 3.35 -1 9 14 18.85 4.06 1 -9 -13 45.24 5.53 1 -9 -13 41.07 5.19 1 -9 -13 42.11 5.22 1 -9 -12 38.59 5.10 1 -9 -12 41.85 5.41 1 -9 -12 34.77 4.85 1 -9 -11 77.14 6.44 1 -9 -11 91.53 7.26 1 -9 -11 76.93 6.66 -1 9 11 88.07 13.29 1 -9 -10 88.34 7.08 -1 9 10 100.24 13.97 1 -9 -10 90.28 6.87 1 -9 -10 83.26 6.72 1 -9 -9 400.28 13.49 1 -9 -9 386.85 13.34 1 -9 -9 410.06 13.07 1 -9 -8 102.01 6.94 -1 9 8 104.14 13.48 1 -9 -8 103.58 7.08 1 -9 -8 93.82 6.54 -1 9 7 0.52 4.00 -1 9 6 205.80 17.41 -1 9 5 2.84 2.98 1 -9 -5 2.48 2.84 -1 9 5 -0.79 3.94 1 -9 -4 114.84 9.93 -1 9 4 107.73 9.17 1 -9 -3 390.23 18.05 -1 9 3 376.15 16.17 1 -9 -3 393.02 17.98 1 -9 -2 42.44 6.39 -1 9 2 41.17 5.46 1 -9 -2 36.64 6.22 -1 9 1 171.87 10.15 1 -9 -1 173.36 12.10 1 -9 -1 182.64 12.86 1 -9 0 75.09 8.89 1 -9 0 79.97 6.72 -1 9 0 76.10 6.83 1 -9 1 67.04 6.46 1 -9 1 71.19 8.76 -1 9 -1 67.57 6.52 1 -9 2 29.71 4.78 -1 9 -2 30.54 4.64 1 -9 3 0.46 3.07 1 -9 4 151.74 10.61 1 -9 5 168.32 11.62 1 -9 6 209.27 13.39 1 -9 7 533.19 21.99 1 -9 8 30.98 6.28 1 -9 9 10.22 4.82 1 -9 10 79.26 9.82 1 -9 11 628.17 27.50 1 -9 12 51.08 8.53 1 -9 13 216.77 17.40 1 -9 14 199.33 8.37 1 -9 14 204.45 17.51 1 -9 14 182.08 8.83 1 -9 15 38.52 8.03 1 -9 15 38.05 4.57 1 -9 15 42.18 4.30 1 -9 16 -0.32 2.09 1 -9 16 4.84 3.81 1 -9 16 2.19 2.33 1 -9 16 0.39 2.61 1 -9 17 13.17 3.17 1 -9 17 16.50 5.49 1 -9 17 14.27 3.14 1 -9 17 14.38 3.42 1 -9 18 -0.43 2.48 1 -9 18 0.79 2.72 1 -9 18 0.66 2.43 1 -9 19 1.08 2.32 1 -9 19 2.64 2.55 1 -9 19 -0.43 2.54 1 -9 20 17.23 3.77 1 -9 20 10.79 2.99 1 -9 20 12.89 3.26 1 -9 20 12.30 3.16 1 -9 21 175.69 8.08 1 -9 21 178.89 8.83 1 -9 21 170.91 8.12 1 -9 21 173.78 7.70 1 -9 22 69.67 4.85 1 -9 22 72.62 5.53 1 -9 22 66.41 4.94 1 -9 22 61.55 4.71 1 -9 23 51.57 4.01 1 -9 23 60.09 4.63 1 -9 23 54.51 4.04 1 -9 23 50.27 3.85 1 -9 24 210.59 7.30 1 -9 24 194.78 5.90 1 -9 24 219.45 6.59 1 -9 25 33.30 2.65 -1 8 20 3.67 1.37 -1 8 19 64.60 4.11 1 -8 -19 57.35 3.16 1 -8 -18 25.34 2.94 -1 8 18 28.95 3.54 -1 8 18 26.72 2.68 -1 8 17 0.02 2.53 1 -8 -17 -3.35 2.34 1 -8 -17 -0.93 2.72 -1 8 16 14.15 3.82 1 -8 -16 7.80 2.96 1 -8 -16 9.22 3.39 1 -8 -15 42.79 4.55 -1 8 15 55.97 5.80 1 -8 -15 50.90 5.38 1 -8 -15 52.63 5.62 1 -8 -14 2.24 3.14 1 -8 -14 1.41 3.10 1 -8 -14 -1.16 3.93 1 -8 -13 1.99 3.23 1 -8 -13 1.67 3.13 1 -8 -13 3.38 3.40 1 -8 -12 2.77 3.25 -1 8 12 10.40 5.43 1 -8 -12 6.93 3.30 1 -8 -12 -3.86 4.55 1 -8 -11 74.04 6.14 1 -8 -11 71.61 6.37 1 -8 -11 84.76 6.81 -1 8 11 91.59 13.65 1 -8 -10 60.61 5.73 1 -8 -10 62.59 5.92 1 -8 -10 65.57 5.81 -1 8 10 57.15 10.40 1 -8 -9 95.70 6.71 1 -8 -9 101.41 6.90 -1 8 9 108.99 13.52 1 -8 -9 104.15 6.84 -1 8 8 407.06 24.85 -1 8 7 246.22 18.31 -1 8 6 209.55 16.48 -1 8 6 209.64 13.79 1 -8 -5 514.60 18.93 -1 8 5 480.01 19.34 -1 8 4 228.38 12.92 1 -8 -4 233.94 12.90 1 -8 -4 231.87 12.72 1 -8 -3 24.40 4.87 1 -8 -3 22.64 4.81 -1 8 3 24.99 4.44 -1 8 2 273.25 12.45 1 -8 -2 281.35 14.42 1 -8 -2 263.53 14.06 1 -8 -1 11.04 3.04 1 -8 -1 12.32 4.21 -1 8 1 13.93 3.69 1 -8 0 85.97 6.54 1 -8 0 92.79 8.93 -1 8 0 88.77 6.89 1 -8 1 29.68 6.11 1 -8 1 22.11 3.78 -1 8 -1 24.62 4.25 1 -8 2 -0.92 2.75 1 -8 3 65.62 6.51 1 -8 4 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96.26 6.36 2 -17 10 5.46 3.19 2 -17 10 4.57 2.88 2 -17 10 2.57 2.53 2 -17 10 3.20 2.28 2 -17 10 13.73 3.31 2 -17 11 22.01 4.11 2 -17 11 22.92 3.62 2 -17 11 18.62 3.69 2 -17 11 20.22 3.88 2 -17 12 1.63 3.25 2 -17 12 -0.52 2.48 2 -17 12 -0.65 2.66 2 -17 12 0.10 2.33 2 -17 13 2.55 2.94 2 -17 13 -2.69 2.52 2 -17 13 1.19 2.77 2 -17 13 -1.25 2.11 2 -17 14 0.10 2.67 2 -17 14 -2.60 2.60 2 -17 14 1.11 1.87 2 -17 15 -1.33 2.90 2 -17 15 -2.20 3.37 2 -17 15 -1.89 2.61 2 -17 16 176.72 8.17 2 -17 16 196.49 8.43 2 -17 16 191.28 8.76 2 -17 17 38.84 4.30 2 -17 17 40.66 4.22 2 -17 17 35.81 3.84 2 -17 18 67.52 5.22 2 -17 18 65.91 4.95 2 -17 18 61.69 4.24 2 -17 19 112.13 4.91 2 -17 19 123.53 6.31 2 -17 19 125.41 6.14 2 -17 20 31.95 3.13 2 -17 20 31.58 3.37 2 -17 21 10.80 1.94 2 -17 21 13.69 2.22 2 -17 22 0.49 1.02 2 -17 22 1.56 1.30 2 -16 -12 -0.08 1.01 2 -16 -11 51.58 3.57 2 -16 -11 46.67 3.15 2 -16 -10 55.04 4.24 2 -16 -10 52.61 3.81 2 -16 -9 7.19 2.44 2 -16 -9 9.01 2.43 2 -16 -9 7.61 2.30 2 -16 -8 37.48 3.99 2 -16 -8 46.11 4.32 2 -16 -8 47.07 4.72 2 -16 -7 66.32 5.10 2 -16 -7 71.24 5.88 2 -16 -7 80.33 6.07 2 -16 -6 68.45 6.13 2 -16 -6 62.51 5.16 2 -16 -6 65.60 6.05 2 -16 -6 55.15 4.90 2 -16 -5 -2.38 3.52 2 -16 -5 -2.14 2.85 2 -16 -5 1.27 3.70 2 -16 -5 0.22 2.28 2 -16 -4 19.52 3.36 2 -16 -4 25.80 3.82 2 -16 -4 26.28 4.48 2 -16 -4 26.07 4.91 2 -16 -3 3.95 2.05 2 -16 -3 3.72 2.19 2 -16 -3 3.62 3.77 2 -16 -3 -2.19 4.25 2 -16 -3 1.47 2.29 2 -16 -2 1.66 2.03 2 -16 -2 0.92 2.06 2 -16 -2 -5.93 4.34 2 -16 -2 3.82 4.01 2 -16 -2 2.46 2.80 2 -16 -2 0.94 2.11 2 -16 -1 65.13 7.40 2 -16 -1 62.22 6.16 2 -16 -1 68.55 5.55 2 -16 -1 59.44 5.52 2 -16 -1 66.19 5.57 2 -16 0 70.12 6.40 2 -16 0 83.96 8.14 2 -16 0 72.46 6.10 2 -16 0 71.11 6.36 2 -16 0 72.74 5.72 2 -16 1 105.63 6.55 2 -16 1 99.00 7.59 2 -16 1 114.92 7.84 2 -16 1 116.44 9.22 2 -16 2 96.41 7.56 2 -16 2 104.46 7.49 2 -16 2 113.48 9.19 2 -16 3 95.05 7.04 2 -16 3 87.01 7.31 2 -16 3 108.48 8.97 2 -16 4 234.17 12.47 2 -16 4 233.48 10.45 2 -16 4 222.27 11.27 2 -16 5 27.71 7.97 2 -16 5 34.48 4.03 2 -16 5 27.87 4.99 2 -16 5 39.37 6.55 2 -16 5 30.30 4.29 2 -16 6 51.86 5.21 2 -16 6 52.10 6.36 2 -16 6 48.47 4.70 2 -16 6 59.34 7.12 2 -16 7 116.79 7.33 2 -16 7 117.46 7.41 2 -16 7 134.13 9.40 2 -16 7 127.02 7.04 2 -16 7 114.01 7.79 2 -16 8 16.62 5.46 2 -16 8 9.62 2.80 2 -16 8 17.37 5.93 2 -16 8 9.08 3.03 2 -16 8 9.19 2.95 2 -16 8 9.49 2.67 2 -16 9 102.33 6.64 2 -16 9 100.58 7.30 2 -16 9 111.68 9.38 2 -16 9 90.46 6.66 2 -16 9 122.14 8.13 2 -16 9 99.42 6.56 2 -16 10 141.31 7.82 2 -16 10 152.82 8.76 2 -16 10 139.01 7.86 2 -16 10 148.34 8.54 2 -16 11 18.57 4.02 2 -16 11 16.77 3.22 2 -16 11 18.28 3.83 2 -16 11 19.21 3.74 2 -16 12 25.92 3.72 2 -16 12 33.03 4.62 2 -16 12 25.39 3.84 2 -16 12 33.02 4.70 2 -16 13 32.48 4.64 2 -16 13 19.16 3.76 2 -16 13 26.06 4.42 2 -16 13 22.87 3.47 2 -16 14 4.11 1.94 2 -16 14 5.76 3.07 2 -16 15 2.12 2.93 2 -16 15 8.07 3.27 2 -16 16 80.37 5.82 2 -16 16 89.45 6.61 2 -16 17 328.57 10.44 2 -16 17 355.06 11.99 2 -16 18 126.50 6.19 2 -16 18 136.17 7.49 2 -16 19 24.31 3.71 2 -16 19 21.62 3.38 2 -16 19 25.33 2.80 2 -16 20 88.18 5.43 2 -16 20 90.20 5.27 2 -16 21 32.09 3.23 2 -16 21 28.42 2.91 2 -16 22 3.75 1.49 2 -16 22 5.86 1.74 2 -16 23 0.24 0.92 2 -16 23 2.55 1.12 2 -15 -13 21.94 2.20 2 -15 -13 21.81 2.22 2 -15 -12 49.77 3.66 2 -15 -12 52.49 3.84 2 -15 -12 59.10 3.96 2 -15 -11 9.41 2.54 2 -15 -11 7.37 2.48 2 -15 -10 12.54 3.23 2 -15 -10 13.77 2.80 2 -15 -10 17.58 3.37 2 -15 -9 169.97 8.02 2 -15 -9 166.74 8.24 2 -15 -8 74.63 6.31 2 -15 -8 71.42 5.72 2 -15 -8 76.98 5.98 2 -15 -7 1.76 2.51 2 -15 -7 -1.47 4.23 2 -15 -7 0.54 2.93 2 -15 -7 4.71 2.91 2 -15 -6 129.76 8.20 2 -15 -6 111.17 7.39 2 -15 -6 129.82 8.66 2 -15 -6 123.52 7.42 2 -15 -5 83.69 6.47 2 -15 -5 82.38 6.52 2 -15 -5 83.52 6.74 2 -15 -5 90.92 7.77 2 -15 -4 26.15 5.20 2 -15 -4 25.18 4.02 2 -15 -4 19.86 4.37 2 -15 -4 26.51 4.01 2 -15 -3 18.82 4.16 2 -15 -3 24.13 3.77 2 -15 -3 26.37 3.58 2 -15 -3 23.78 3.92 2 -15 -3 18.92 4.84 2 -15 -2 32.25 4.05 2 -15 -2 32.75 3.96 2 -15 -2 33.69 4.42 2 -15 -2 25.50 4.52 2 -15 -2 33.66 5.55 2 -15 -1 -0.64 4.28 2 -15 -1 5.78 4.62 2 -15 -1 -0.03 4.11 2 -15 -1 3.10 3.20 2 -15 -1 5.88 2.62 2 -15 0 24.89 4.10 2 -15 0 31.51 7.68 2 -15 0 27.74 3.82 2 -15 0 23.34 5.25 2 -15 1 38.55 8.20 2 -15 1 41.11 4.45 2 -15 1 41.57 5.88 2 -15 1 37.89 4.88 2 -15 1 35.66 4.51 2 -15 2 124.04 7.84 2 -15 2 116.68 8.06 2 -15 2 134.98 9.49 2 -15 2 124.79 6.98 2 -15 2 130.94 14.90 2 -15 3 29.45 7.91 2 -15 3 29.54 4.15 2 -15 3 17.46 3.89 2 -15 3 25.18 5.19 2 -15 4 119.71 8.98 2 -15 4 96.67 12.89 2 -15 4 110.34 7.33 2 -15 4 105.69 7.89 2 -15 5 303.76 13.40 2 -15 5 295.29 22.29 2 -15 5 286.23 11.13 2 -15 5 294.13 10.07 2 -15 5 294.12 18.86 2 -15 5 297.14 12.79 2 -15 5 307.25 12.69 2 -15 6 30.19 5.50 2 -15 6 11.48 2.73 2 -15 6 21.94 5.24 2 -15 6 24.79 4.14 2 -15 6 15.45 5.09 2 -15 6 12.53 4.22 2 -15 6 13.38 3.09 2 -15 6 7.95 3.85 2 -15 7 71.44 5.95 2 -15 7 65.71 5.27 2 -15 7 71.92 11.42 2 -15 7 64.09 9.60 2 -15 7 69.93 5.72 2 -15 7 65.34 6.79 2 -15 7 75.57 6.91 2 -15 8 185.66 9.72 2 -15 8 203.14 9.68 2 -15 8 201.55 8.84 2 -15 8 188.06 8.81 2 -15 8 187.48 16.57 2 -15 8 210.80 11.23 2 -15 8 196.77 18.36 2 -15 8 190.33 9.63 2 -15 9 34.52 6.12 2 -15 9 30.65 7.88 2 -15 9 21.86 3.89 2 -15 9 28.25 4.19 2 -15 9 25.99 3.66 2 -15 9 21.74 3.51 2 -15 9 14.61 5.40 2 -15 10 0.81 2.62 2 -15 10 0.98 2.38 2 -15 10 -1.12 2.84 2 -15 10 4.92 3.85 2 -15 10 1.80 2.26 2 -15 10 -3.28 3.01 2 -15 11 90.62 12.44 2 -15 11 111.21 13.63 2 -15 11 105.05 7.34 2 -15 11 113.15 7.55 2 -15 11 112.45 6.74 2 -15 12 19.07 4.01 2 -15 12 11.46 2.86 2 -15 12 12.12 3.74 2 -15 13 10.54 2.63 2 -15 13 18.14 3.98 2 -15 13 17.01 3.85 2 -15 14 18.54 4.07 2 -15 15 131.89 8.18 2 -15 16 21.66 4.18 2 -15 16 17.62 3.20 2 -15 17 113.49 5.71 2 -15 17 111.35 7.29 2 -15 17 111.94 6.41 2 -15 18 240.68 8.39 2 -15 18 260.08 10.48 2 -15 18 253.84 8.08 2 -15 19 39.88 4.59 2 -15 19 28.69 3.20 2 -15 19 42.67 3.40 2 -15 19 39.45 3.35 2 -15 20 0.35 1.39 2 -15 20 0.60 1.26 2 -15 20 1.90 2.49 2 -15 21 28.13 2.44 2 -15 21 35.35 3.58 2 -15 22 78.32 4.29 2 -15 22 75.67 4.33 2 -15 23 -0.26 1.34 2 -15 23 -1.35 1.27 2 -14 -15 0.32 0.92 2 -14 -14 39.06 3.07 2 -14 -14 35.54 2.80 2 -14 -13 52.83 4.04 2 -14 -13 62.57 4.19 2 -14 -12 9.55 2.57 2 -14 -12 7.21 2.68 2 -14 -11 69.68 5.49 2 -14 -11 55.82 5.10 2 -14 -10 13.89 3.63 2 -14 -10 8.58 4.12 2 -14 -9 27.74 4.92 2 -14 -9 26.69 4.31 2 -14 -8 72.31 6.31 2 -14 -8 75.59 6.30 2 -14 -8 74.43 6.94 2 -14 -7 174.15 8.94 2 -14 -7 169.76 9.54 2 -14 -7 172.41 9.37 2 -14 -6 21.06 4.45 2 -14 -6 30.04 5.01 2 -14 -6 25.55 4.47 2 -14 -5 66.09 6.06 2 -14 -5 64.55 6.28 2 -14 -5 58.90 6.57 -2 14 4 -5.09 4.81 2 -14 -4 -2.61 4.85 2 -14 -4 3.04 2.88 2 -14 -4 -4.12 4.37 -2 14 3 0.12 3.04 2 -14 -3 10.39 4.74 2 -14 -3 2.29 1.89 2 -14 -3 2.03 4.28 2 -14 -3 2.54 2.46 2 -14 -3 1.81 2.71 2 -14 -3 2.06 4.17 2 -14 -2 125.57 8.97 2 -14 -2 132.43 7.63 -2 14 2 124.30 14.44 2 -14 -2 126.15 7.69 2 -14 -2 131.42 7.44 2 -14 -2 139.18 13.81 2 -14 -1 93.65 6.50 2 -14 -1 98.79 7.97 2 -14 -1 93.59 6.71 2 -14 -1 117.17 13.03 2 -14 -1 93.14 6.09 2 -14 0 2.65 2.27 2 -14 0 2.21 3.76 2 -14 0 1.19 3.40 2 -14 0 2.58 3.09 2 -14 1 0.69 3.70 2 -14 1 2.28 2.11 2 -14 1 6.56 2.99 2 -14 1 2.08 3.67 2 -14 2 -3.88 4.41 2 -14 2 -0.29 3.69 2 -14 2 0.32 3.66 2 -14 2 -1.75 2.65 2 -14 2 2.66 2.10 2 -14 3 376.92 14.19 2 -14 3 344.85 12.12 2 -14 3 335.94 12.85 2 -14 3 358.89 13.39 2 -14 3 343.46 22.89 2 -14 4 43.76 4.56 2 -14 4 42.18 5.69 2 -14 4 56.38 5.26 2 -14 4 39.38 4.93 2 -14 4 44.83 8.63 2 -14 4 41.86 6.66 2 -14 4 56.10 6.22 2 -14 5 76.16 6.73 2 -14 5 61.48 8.50 2 -14 5 64.96 6.14 2 -14 5 66.31 4.94 2 -14 5 64.88 6.62 2 -14 5 65.97 10.40 2 -14 5 67.42 5.48 2 -14 6 122.07 8.65 2 -14 6 120.72 7.91 2 -14 6 121.55 6.99 2 -14 6 118.72 8.13 2 -14 6 113.93 6.35 2 -14 6 110.99 11.82 2 -14 7 56.45 5.83 2 -14 7 62.00 6.36 2 -14 7 76.11 7.25 2 -14 7 57.99 8.92 2 -14 7 58.20 5.15 2 -14 7 62.19 5.03 2 -14 8 16.54 5.22 2 -14 8 12.87 2.93 2 -14 8 11.62 2.97 2 -14 8 18.14 4.66 2 -14 8 12.13 2.73 2 -14 9 53.28 5.18 2 -14 9 47.13 4.55 2 -14 9 58.00 5.49 2 -14 9 63.48 6.98 2 -14 9 49.62 8.78 2 -14 10 357.46 14.26 2 -14 10 310.27 21.91 2 -14 10 339.38 12.41 2 -14 10 320.66 11.88 2 -14 10 318.13 10.86 2 -14 11 0.27 3.93 2 -14 11 0.91 2.31 2 -14 11 5.33 2.47 2 -14 11 0.76 2.52 2 -14 11 -4.04 2.69 2 -14 12 7.95 3.17 2 -14 12 13.64 5.56 2 -14 12 11.36 3.26 2 -14 13 15.23 3.92 2 -14 13 20.70 3.96 2 -14 14 -1.77 2.50 2 -14 14 1.36 2.97 2 -14 15 54.70 5.17 2 -14 15 59.13 4.70 2 -14 15 63.18 6.09 2 -14 16 263.74 11.32 2 -14 16 282.21 10.38 2 -14 16 273.61 9.37 2 -14 17 129.45 6.82 2 -14 17 126.61 6.40 2 -14 17 125.27 7.81 2 -14 18 16.65 3.14 2 -14 18 24.75 4.08 2 -14 18 25.24 3.15 2 -14 18 24.45 3.15 2 -14 19 144.87 6.50 2 -14 19 149.38 7.84 2 -14 20 78.86 4.57 2 -14 20 85.74 5.77 2 -14 21 4.11 1.59 2 -14 21 6.41 2.38 2 -14 22 5.32 1.67 2 -14 22 8.94 2.21 2 -14 22 8.94 1.71 2 -14 23 67.37 3.72 2 -14 23 67.87 3.14 2 -14 23 61.40 3.53 2 -14 24 4.92 1.11 2 -13 -16 8.33 1.50 2 -13 -15 13.79 2.31 -2 13 15 14.22 1.76 2 -13 -15 15.10 2.18 2 -13 -14 10.06 2.50 -2 13 14 11.99 2.12 -2 13 13 100.65 5.32 2 -13 -13 124.74 6.45 -2 13 12 54.48 4.42 2 -13 -12 63.05 5.49 2 -13 -12 52.11 4.94 2 -13 -11 5.57 3.32 2 -13 -11 -1.95 4.34 -2 13 11 4.86 2.44 -2 13 10 57.99 5.04 2 -13 -10 73.18 6.50 2 -13 -10 64.08 6.27 2 -13 -9 84.43 6.75 2 -13 -9 87.47 7.26 2 -13 -8 6.88 3.65 2 -13 -8 3.07 2.92 2 -13 -7 55.41 5.96 2 -13 -7 65.20 6.27 2 -13 -7 50.78 5.66 2 -13 -6 48.22 5.38 2 -13 -6 42.48 5.59 -2 13 6 38.36 9.45 2 -13 -6 36.79 5.30 2 -13 -5 16.69 3.53 2 -13 -5 13.05 4.14 -2 13 5 11.97 6.07 2 -13 -4 0.47 2.59 -2 13 4 1.75 3.74 2 -13 -4 -3.81 3.99 2 -13 -4 9.64 4.03 2 -13 -3 1.41 3.43 2 -13 -3 -2.17 2.47 2 -13 -3 1.53 2.93 -2 13 3 1.38 4.05 2 -13 -3 -4.29 4.06 2 -13 -2 2.97 3.28 2 -13 -2 -2.20 4.03 2 -13 -2 0.31 3.28 2 -13 -2 1.89 2.27 2 -13 -1 40.88 7.77 2 -13 -1 32.16 4.76 2 -13 -1 38.10 4.84 2 -13 -1 40.11 4.33 2 -13 0 19.63 4.06 2 -13 0 23.97 6.17 2 -13 1 8.78 4.38 2 -13 2 24.31 6.44 2 -13 2 33.04 5.62 2 -13 3 9.11 3.56 2 -13 4 745.64 27.36 -2 13 -4 705.94 25.72 -2 13 -5 460.95 21.33 2 -13 5 461.63 22.29 2 -13 6 273.53 17.78 2 -13 7 494.92 24.63 2 -13 8 66.77 9.67 2 -13 8 70.56 5.55 2 -13 9 42.45 4.59 2 -13 9 34.84 7.15 2 -13 9 44.71 4.56 2 -13 9 52.93 6.18 2 -13 10 8.89 2.88 2 -13 10 10.80 4.27 2 -13 10 6.21 2.52 2 -13 11 174.97 8.60 2 -13 11 178.13 8.44 2 -13 11 179.28 9.11 2 -13 11 161.39 15.92 2 -13 12 5.81 2.97 2 -13 12 4.57 2.52 2 -13 12 1.05 3.58 2 -13 12 4.20 2.33 2 -13 13 29.09 3.57 2 -13 13 32.65 4.70 2 -13 13 36.12 4.53 2 -13 13 37.52 4.42 2 -13 13 25.08 6.81 2 -13 14 44.92 4.33 2 -13 14 41.15 8.84 2 -13 14 41.88 5.18 2 -13 14 42.02 4.79 2 -13 15 34.80 4.42 2 -13 15 42.22 5.25 2 -13 15 42.97 4.33 2 -13 16 11.74 3.63 2 -13 16 7.00 2.37 2 -13 16 12.63 2.93 2 -13 16 5.75 2.50 2 -13 17 107.28 6.09 2 -13 17 107.63 6.37 2 -13 17 92.82 6.49 2 -13 17 111.34 7.48 2 -13 18 2.84 2.25 2 -13 18 3.49 2.94 2 -13 18 5.05 2.24 2 -13 19 15.07 2.77 2 -13 19 16.90 3.58 2 -13 19 9.29 2.74 2 -13 20 63.03 5.20 2 -13 20 65.44 4.64 2 -13 20 56.81 4.68 2 -13 21 105.41 5.83 2 -13 21 110.53 6.11 2 -13 21 116.22 5.53 2 -13 22 -1.48 1.67 2 -13 22 3.62 1.91 2 -13 22 1.97 1.50 2 -13 23 50.99 3.42 2 -13 23 53.37 3.16 2 -13 24 40.90 2.35 2 -13 24 30.74 2.25 2 -13 24 36.79 2.43 2 -13 24 29.16 2.14 2 -12 -17 -0.24 1.12 2 -12 -16 -3.62 1.97 -2 12 16 0.32 1.37 -2 12 15 22.42 2.79 2 -12 -15 24.02 3.13 -2 12 14 65.37 4.68 2 -12 -14 65.20 5.10 -2 12 13 31.44 3.81 2 -12 -13 25.51 4.10 2 -12 -13 34.74 4.58 2 -12 -12 260.20 10.40 -2 12 12 245.00 9.80 2 -12 -12 280.24 10.98 2 -12 -11 83.70 6.78 2 -12 -11 80.12 6.75 -2 12 11 70.76 5.83 2 -12 -10 7.65 3.84 -2 12 10 7.29 2.98 2 -12 -10 3.62 4.11 -2 12 9 7.59 2.89 2 -12 -9 10.92 4.30 -2 12 8 170.70 8.90 2 -12 -8 184.89 9.61 2 -12 -7 16.34 4.25 2 -12 -7 7.41 4.47 -2 12 7 16.17 5.66 2 -12 -6 193.06 9.67 2 -12 -6 204.08 9.85 -2 12 6 206.93 19.04 2 -12 -5 90.94 6.77 2 -12 -5 91.68 7.05 -2 12 5 85.77 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16 26.03 4.12 2 -11 16 36.65 4.28 2 -11 17 7.15 2.90 2 -11 17 7.41 3.04 2 -11 17 7.40 2.71 2 -11 18 16.75 3.56 2 -11 18 14.54 3.47 2 -11 18 14.63 3.06 2 -11 19 72.27 5.82 2 -11 19 67.27 5.24 2 -11 19 72.26 5.96 2 -11 20 235.78 9.78 2 -11 20 233.83 8.75 2 -11 20 240.79 9.50 2 -11 20 243.35 9.12 2 -11 21 4.74 2.48 2 -11 21 3.30 2.33 2 -11 21 2.34 1.79 2 -11 21 3.88 2.56 2 -11 22 151.98 6.05 2 -11 22 154.14 6.72 2 -11 22 171.46 6.71 2 -11 22 162.97 7.10 2 -11 23 204.66 7.03 2 -11 23 208.10 6.59 2 -11 23 194.36 6.48 2 -11 24 34.34 2.36 2 -11 24 39.98 2.78 2 -11 24 43.23 2.84 -2 10 19 47.85 2.73 2 -10 -18 22.04 2.24 -2 10 18 23.45 2.63 2 -10 -17 2.34 1.87 -2 10 17 5.45 2.10 2 -10 -16 -1.53 2.50 -2 10 16 -1.48 2.41 -2 10 15 40.58 4.62 2 -10 -15 39.35 4.45 2 -10 -14 6.74 3.45 2 -10 -14 -0.57 4.11 2 -10 -14 6.99 3.62 -2 10 14 5.80 3.11 -2 10 13 344.81 12.57 2 -10 -13 330.06 12.16 2 -10 -13 321.41 11.64 2 -10 -13 326.78 12.74 2 -10 -12 290.45 11.34 -2 10 12 277.47 11.77 2 -10 -12 273.51 11.77 2 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1.67 -2 8 21 24.66 1.93 -2 8 20 57.85 3.60 -2 8 19 7.93 2.35 -2 8 19 7.60 1.61 2 -8 -19 5.12 1.49 -2 8 18 15.44 3.18 -2 8 18 15.27 2.53 2 -8 -18 11.40 2.36 2 -8 -17 83.11 5.46 -2 8 17 79.37 5.28 2 -8 -17 77.36 6.16 -2 8 17 88.02 6.38 2 -8 -16 -2.73 3.35 2 -8 -16 5.42 2.98 -2 8 16 2.44 3.00 2 -8 -15 0.83 2.90 -2 8 15 2.46 3.24 2 -8 -15 -1.23 3.27 2 -8 -14 69.07 5.86 2 -8 -14 80.61 6.55 2 -8 -14 85.38 6.95 -2 8 14 83.87 6.99 2 -8 -13 1.53 2.98 2 -8 -13 -4.06 4.05 2 -8 -13 1.94 3.09 2 -8 -12 5.71 3.20 -2 8 12 8.34 5.66 2 -8 -12 3.97 3.48 2 -8 -12 3.70 3.09 2 -8 -11 82.60 6.71 2 -8 -11 79.15 6.52 -2 8 11 97.55 13.18 2 -8 -11 79.03 6.24 -2 8 10 205.34 18.42 2 -8 -10 177.85 8.60 2 -8 -10 187.82 9.29 2 -8 -10 180.97 8.88 -2 8 9 112.47 13.56 -2 8 8 343.83 19.86 -2 8 8 368.61 22.80 -2 8 7 967.85 31.23 -2 8 6 26.16 5.12 2 -8 -6 31.67 4.81 2 -8 -5 1.86 2.16 -2 8 5 3.15 3.05 -2 8 4 169.11 11.11 2 -8 -4 164.52 10.53 -2 8 3 99.73 8.46 -2 8 2 159.21 10.01 -2 8 1 0.84 2.96 2 -8 -1 4.32 2.12 2 -8 0 60.56 5.54 -2 8 0 65.58 6.68 2 -8 1 1.58 2.34 -2 8 -1 1.85 2.79 2 -8 2 50.94 5.46 2 -8 3 697.24 19.80 2 -8 4 613.56 19.63 2 -8 5 67.55 7.50 2 -8 6 53.31 7.17 2 -8 7 441.14 19.67 2 -8 8 439.16 20.33 2 -8 9 94.56 10.22 2 -8 10 343.80 19.51 2 -8 11 181.94 14.94 2 -8 12 1.35 3.40 2 -8 13 440.15 24.84 2 -8 14 4.73 2.10 2 -8 14 3.14 2.06 2 -8 14 1.80 3.61 2 -8 15 61.35 9.80 -2 8 -15 60.83 5.10 2 -8 15 61.76 5.11 2 -8 15 68.51 5.70 2 -8 15 56.02 5.05 -2 8 -16 64.49 5.35 2 -8 16 74.60 5.97 2 -8 16 65.05 5.28 2 -8 16 66.60 10.24 2 -8 16 69.98 5.82 2 -8 17 110.85 6.74 2 -8 17 119.67 7.52 -2 8 -17 107.74 6.80 2 -8 17 112.94 7.04 2 -8 17 129.60 14.45 2 -8 18 4.09 2.51 2 -8 18 2.19 2.51 -2 8 -18 1.49 2.14 2 -8 18 2.24 2.57 2 -8 19 -0.11 2.14 -2 8 -19 -1.27 2.01 2 -8 19 0.22 2.39 2 -8 19 0.05 2.67 2 -8 20 46.72 4.55 2 -8 20 52.13 5.08 -2 8 -20 46.61 4.28 2 -8 20 53.52 4.69 2 -8 21 78.70 5.22 2 -8 21 84.18 5.61 2 -8 21 78.18 5.86 2 -8 22 25.61 2.86 2 -8 22 23.98 3.54 2 -8 22 26.90 3.73 2 -8 22 20.66 3.02 2 -8 23 165.76 6.27 2 -8 23 153.77 6.60 2 -8 23 158.91 6.86 2 -8 24 4.54 1.45 2 -8 24 1.12 1.56 2 -8 24 4.46 1.72 2 -8 25 16.51 1.78 -2 7 21 10.85 1.91 -2 7 20 47.79 3.37 -2 7 20 50.26 3.92 2 -7 -19 65.36 3.92 2 -7 -19 70.13 4.99 -2 7 19 71.42 5.16 -2 7 19 69.78 4.69 2 -7 -18 4.84 2.88 -2 7 18 7.06 3.07 2 -7 -18 4.24 2.10 2 -7 -17 -0.90 3.37 2 -7 -17 0.19 2.35 -2 7 17 0.20 2.92 2 -7 -16 3.50 2.66 2 -7 -16 -3.07 3.29 -2 7 16 1.99 3.01 2 -7 -15 2.34 3.00 2 -7 -15 -9.41 4.27 2 -7 -15 -0.41 3.00 -2 7 15 -1.23 3.16 2 -7 -14 6.32 3.08 2 -7 -14 8.66 3.14 2 -7 -14 -1.32 3.70 2 -7 -13 54.17 5.42 -2 7 13 63.79 11.13 2 -7 -13 56.72 5.49 2 -7 -13 64.07 6.20 -2 7 12 179.51 17.66 2 -7 -12 161.19 8.55 2 -7 -12 173.03 9.39 2 -7 -12 162.60 8.30 2 -7 -11 33.20 4.40 2 -7 -11 22.59 3.70 2 -7 -11 32.34 4.39 -2 7 11 39.19 8.82 -2 7 10 196.61 17.30 -2 7 9 668.88 30.41 -2 7 8 194.69 14.69 -2 7 8 212.76 17.06 -2 7 7 113.25 10.43 2 -7 -6 394.67 14.45 -2 7 6 364.02 17.32 -2 7 5 12.47 4.11 2 -7 -5 12.06 3.38 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105.92 6.03 2 -7 21 107.48 6.78 2 -7 22 15.64 3.18 2 -7 22 19.50 2.87 2 -7 23 90.00 4.57 2 -7 23 87.47 5.27 2 -7 23 90.22 5.30 2 -7 24 99.01 4.74 2 -7 24 102.71 4.90 2 -7 24 104.40 4.30 2 -7 25 38.47 2.49 -2 6 22 20.42 2.05 -2 6 21 62.02 4.00 -2 6 21 59.61 3.66 2 -6 -20 1.64 1.97 -2 6 20 4.96 1.94 -2 6 20 2.16 2.17 -2 6 19 75.86 5.77 2 -6 -19 71.24 5.39 2 -6 -19 63.90 4.17 2 -6 -18 72.96 5.91 2 -6 -18 63.61 4.72 -2 6 18 74.53 6.21 -2 6 17 11.73 3.85 2 -6 -17 13.23 3.59 2 -6 -17 13.22 3.20 2 -6 -16 0.83 2.80 2 -6 -16 2.78 2.75 -2 6 16 0.45 3.21 2 -6 -15 0.58 2.83 -2 6 15 0.31 3.00 2 -6 -15 1.23 2.69 2 -6 -14 13.89 3.35 -2 6 14 31.52 8.43 2 -6 -14 23.98 4.02 2 -6 -14 24.95 4.33 2 -6 -13 52.85 5.17 2 -6 -13 53.53 5.12 2 -6 -13 59.33 5.80 -2 6 13 66.00 10.82 2 -6 -12 225.28 10.17 2 -6 -12 207.81 9.04 2 -6 -12 207.68 9.14 -2 6 12 239.94 19.51 -2 6 11 247.77 19.25 -2 6 10 196.62 16.56 -2 6 9 212.66 15.36 -2 6 9 224.81 17.20 -2 6 8 2370.51 48.06 -2 6 8 2623.43 53.36 2 -6 -7 287.76 10.96 -2 6 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3 -18 -1 71.21 5.20 3 -18 -1 79.26 5.69 3 -18 -1 89.87 7.79 3 -18 0 62.68 4.92 3 -18 0 63.48 5.41 3 -18 0 63.00 5.90 3 -18 0 69.01 7.58 3 -18 1 -1.37 2.82 3 -18 1 2.69 2.24 3 -18 1 1.34 2.49 3 -18 1 7.15 4.61 3 -18 2 83.71 6.54 3 -18 2 84.85 6.64 3 -18 2 90.15 6.90 3 -18 2 89.51 5.75 3 -18 2 108.25 8.89 3 -18 3 61.44 5.56 3 -18 3 49.61 5.49 3 -18 3 70.37 6.45 3 -18 4 25.19 4.99 3 -18 4 19.06 3.70 3 -18 5 8.83 3.19 3 -18 5 13.69 3.44 3 -18 6 96.63 7.37 3 -18 6 99.45 6.54 3 -18 7 29.95 3.53 3 -18 7 25.89 3.82 3 -18 7 23.05 4.16 3 -18 7 19.74 3.40 3 -18 8 106.95 6.87 3 -18 8 113.73 6.53 3 -18 8 116.34 6.81 3 -18 8 115.92 7.93 3 -18 9 16.12 3.03 3 -18 9 15.80 3.71 3 -18 9 16.30 3.81 3 -18 9 14.67 3.36 3 -18 9 18.04 3.10 3 -18 10 43.53 5.19 3 -18 10 40.45 4.16 3 -18 10 40.10 4.68 3 -18 10 43.88 5.06 3 -18 11 42.44 4.35 3 -18 11 44.11 4.85 3 -18 11 52.51 5.38 3 -18 11 49.66 5.10 3 -18 12 70.37 6.04 3 -18 12 62.96 5.11 3 -18 12 61.14 5.62 3 -18 12 62.37 5.26 3 -18 13 62.67 5.02 3 -18 13 73.21 5.82 3 -18 13 64.69 5.32 3 -18 14 0.68 2.41 3 -18 14 -0.25 1.75 3 -18 14 0.94 2.12 3 -18 15 57.51 4.75 3 -18 15 68.42 5.20 3 -18 15 70.95 5.55 3 -18 16 140.46 6.80 3 -18 16 154.71 7.43 3 -18 17 68.97 4.65 3 -18 17 65.96 4.93 3 -18 17 69.13 4.44 3 -18 18 5.87 2.22 3 -18 18 5.52 2.05 3 -18 18 7.10 1.86 3 -18 19 37.84 3.40 3 -18 19 37.07 3.17 3 -18 19 37.04 2.45 3 -18 20 8.57 1.89 3 -18 20 6.85 1.62 3 -18 21 4.45 1.30 3 -18 21 3.86 1.18 3 -17 -11 8.64 1.42 3 -17 -11 9.18 1.63 3 -17 -10 18.07 2.44 3 -17 -10 20.04 2.30 3 -17 -9 1.64 1.65 3 -17 -9 -0.01 1.74 3 -17 -8 1.76 1.79 3 -17 -8 0.17 2.04 3 -17 -7 7.74 2.47 3 -17 -7 4.29 2.49 3 -17 -6 18.07 3.33 3 -17 -6 20.71 3.66 3 -17 -6 19.35 3.20 3 -17 -6 29.74 4.26 3 -17 -5 -0.79 2.97 3 -17 -5 -7.64 4.12 3 -17 -5 0.41 2.16 3 -17 -5 0.52 2.86 3 -17 -4 4.85 2.22 3 -17 -4 5.69 3.45 3 -17 -4 3.06 3.31 3 -17 -4 2.53 2.68 3 -17 -3 28.15 3.95 3 -17 -3 25.57 3.84 3 -17 -3 28.13 4.34 3 -17 -3 37.07 3.77 3 -17 -3 30.08 5.34 3 -17 -2 2.47 3.11 3 -17 -2 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3.57 3 -17 12 13.41 3.05 3 -17 12 10.62 2.88 3 -17 12 16.28 3.94 3 -17 13 80.49 5.74 3 -17 13 90.01 6.44 3 -17 13 66.02 5.58 3 -17 13 82.25 6.60 3 -17 14 117.76 6.29 3 -17 14 120.61 7.60 3 -17 15 27.85 4.23 3 -17 15 24.49 3.70 3 -17 15 18.99 3.33 3 -17 16 59.75 5.04 3 -17 16 56.42 4.78 3 -17 16 63.14 5.63 3 -17 17 160.47 6.96 3 -17 17 166.91 7.72 3 -17 17 176.91 8.14 3 -17 18 54.36 4.63 3 -17 18 55.19 3.82 3 -17 18 55.78 4.48 3 -17 19 -2.96 2.20 3 -17 19 -2.63 2.00 3 -17 20 0.31 1.56 3 -17 20 3.68 1.96 3 -17 21 10.00 1.80 3 -17 21 14.23 2.18 3 -17 22 2.80 1.10 3 -17 22 3.40 1.16 3 -16 -12 100.71 4.43 3 -16 -12 100.78 4.63 3 -16 -11 9.10 2.14 3 -16 -11 12.93 2.45 3 -16 -10 19.74 2.96 3 -16 -9 56.80 4.80 3 -16 -9 66.29 5.02 3 -16 -8 44.50 4.83 3 -16 -8 42.67 4.43 3 -16 -7 24.12 3.51 3 -16 -7 21.47 3.62 3 -16 -7 20.37 3.68 3 -16 -7 33.75 4.43 3 -16 -6 3.01 4.13 3 -16 -6 14.92 3.80 3 -16 -6 5.71 2.69 3 -16 -6 8.59 2.77 3 -16 -5 2.03 3.24 3 -16 -5 0.64 2.57 3 -16 -5 0.51 3.96 3 -16 -5 -2.25 3.11 3 -16 -4 -2.71 3.74 3 -16 -4 -1.91 2.83 3 -16 -4 -0.70 2.58 3 -16 -4 0.66 3.44 3 -16 -3 107.04 7.12 3 -16 -3 108.20 7.17 3 -16 -3 105.60 6.48 3 -16 -3 106.64 6.58 3 -16 -3 104.23 8.53 3 -16 -2 122.29 7.44 3 -16 -2 119.47 9.04 3 -16 -2 123.29 7.67 3 -16 -2 124.28 7.48 3 -16 -2 137.81 7.20 3 -16 -1 2.94 2.65 3 -16 -1 -1.28 3.15 3 -16 -1 5.71 4.17 3 -16 0 5.03 2.68 3 -16 0 10.76 4.79 3 -16 0 3.20 2.70 3 -16 1 135.20 7.63 3 -16 1 128.93 8.23 3 -16 1 141.41 9.84 3 -16 2 367.80 11.98 3 -16 2 355.28 13.56 3 -16 2 381.62 15.57 3 -16 2 338.79 12.92 3 -16 3 31.01 4.25 3 -16 3 31.13 4.97 3 -16 3 37.25 8.23 3 -16 3 32.72 4.11 3 -16 3 46.19 6.67 3 -16 4 170.02 8.06 3 -16 4 180.67 10.18 3 -16 4 194.83 11.52 3 -16 4 181.52 17.74 3 -16 4 174.58 9.00 3 -16 5 179.68 10.34 3 -16 5 184.39 8.21 3 -16 5 180.12 8.96 3 -16 5 184.16 18.33 3 -16 6 11.50 4.81 3 -16 6 0.97 2.14 3 -16 6 4.04 5.55 3 -16 6 0.84 1.78 3 -16 7 139.99 8.14 3 -16 7 154.25 10.08 3 -16 7 128.11 7.41 3 -16 7 130.34 15.63 3 -16 7 143.41 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2.58 3 -15 -8 3.73 2.94 3 -15 -8 -4.00 4.56 3 -15 -8 3.70 2.67 3 -15 -7 65.75 6.20 3 -15 -7 74.79 6.10 3 -15 -7 56.79 5.70 3 -15 -7 67.95 6.16 3 -15 -6 60.65 6.01 3 -15 -6 52.10 5.50 3 -15 -6 51.32 5.35 3 -15 -6 59.75 6.11 3 -15 -5 26.26 4.27 3 -15 -5 25.56 4.95 3 -15 -5 27.51 4.05 3 -15 -5 28.81 4.89 3 -15 -4 15.70 3.55 3 -15 -4 21.44 4.53 3 -15 -4 17.09 3.44 3 -15 -4 17.32 4.40 3 -15 -3 32.82 4.81 3 -15 -3 34.95 4.54 3 -15 -3 35.27 4.27 3 -15 -3 32.29 5.35 3 -15 -2 192.54 8.56 3 -15 -2 178.12 16.12 3 -15 -2 175.25 8.91 3 -15 -2 182.88 9.31 -3 15 2 158.76 16.55 3 -15 -2 175.74 10.64 3 -15 -1 334.12 11.53 3 -15 -1 362.87 12.55 3 -15 -1 364.47 14.76 3 -15 -1 387.20 23.87 3 -15 -1 377.17 11.47 3 -15 0 160.75 15.66 3 -15 0 145.87 8.07 3 -15 0 151.59 9.80 3 -15 1 37.34 8.16 3 -15 1 34.09 5.61 3 -15 1 34.56 4.23 3 -15 1 28.83 4.21 3 -15 2 4.01 2.39 3 -15 2 9.40 4.38 3 -15 2 2.88 4.17 3 -15 2 -0.27 3.99 3 -15 2 8.00 2.68 3 -15 3 534.41 14.15 3 -15 3 588.28 18.43 3 -15 3 560.44 16.87 3 -15 3 536.34 15.44 3 -15 3 547.44 29.85 3 -15 4 128.24 8.62 3 -15 4 125.30 6.92 3 -15 4 132.00 7.62 3 -15 4 133.95 9.61 3 -15 4 144.90 15.75 3 -15 5 311.18 12.89 3 -15 5 318.32 13.72 3 -15 5 294.64 10.15 3 -15 5 311.62 11.18 3 -15 6 154.35 9.79 3 -15 6 151.41 7.30 3 -15 6 160.51 8.18 3 -15 6 158.35 7.49 3 -15 6 153.34 14.06 3 -15 7 1.28 2.06 3 -15 7 8.85 4.72 3 -15 7 -1.38 4.56 3 -15 7 0.48 2.15 3 -15 8 3.30 3.38 3 -15 8 2.76 1.97 3 -15 8 1.28 2.77 3 -15 8 5.25 2.23 3 -15 9 42.15 4.84 3 -15 9 39.22 4.65 3 -15 9 37.53 7.92 3 -15 10 45.17 8.65 3 -15 10 57.07 5.57 3 -15 10 59.89 5.82 3 -15 11 5.16 2.86 3 -15 11 3.69 3.14 3 -15 11 6.44 3.20 3 -15 12 253.13 10.59 3 -15 12 264.16 11.40 3 -15 13 173.32 9.47 3 -15 13 162.30 7.99 3 -15 13 174.74 8.78 3 -15 14 24.71 4.54 3 -15 15 170.80 9.21 3 -15 15 169.93 7.39 3 -15 16 255.28 9.72 3 -15 16 278.03 9.23 3 -15 16 266.93 11.25 3 -15 17 191.70 7.50 3 -15 17 177.87 7.62 3 -15 17 189.57 9.21 3 -15 18 4.35 1.92 3 -15 18 4.00 2.73 3 -15 19 81.22 5.78 3 -15 19 86.63 4.72 3 -15 20 92.52 5.43 3 -15 20 93.55 4.56 3 -15 21 10.52 2.26 3 -15 21 7.98 1.64 3 -15 22 11.16 1.94 3 -15 22 9.53 1.48 3 -15 23 20.60 1.92 3 -15 23 23.58 1.97 3 -14 -15 37.57 2.85 3 -14 -14 14.12 2.50 3 -14 -13 159.90 6.67 3 -14 -13 133.66 6.61 3 -14 -12 12.63 3.16 3 -14 -12 12.31 3.14 3 -14 -11 13.32 3.60 3 -14 -10 95.84 6.82 3 -14 -10 89.09 6.64 3 -14 -9 65.31 6.21 3 -14 -9 73.04 6.20 3 -14 -8 31.70 5.17 3 -14 -8 29.86 4.69 3 -14 -7 1.98 2.84 3 -14 -7 -1.19 4.64 3 -14 -7 0.78 3.10 3 -14 -6 7.46 4.12 3 -14 -6 3.90 3.03 3 -14 -6 6.75 3.28 3 -14 -5 -3.65 5.12 3 -14 -5 0.71 3.00 3 -14 -5 -1.67 4.08 3 -14 -4 72.55 6.38 -3 14 4 74.77 11.70 3 -14 -4 66.21 5.79 3 -14 -4 68.21 6.10 3 -14 -4 67.03 6.77 3 -14 -3 239.71 10.59 3 -14 -3 247.30 10.04 3 -14 -3 235.31 10.05 3 -14 -3 270.00 18.74 3 -14 -3 241.24 11.85 3 -14 -2 88.82 6.46 3 -14 -2 73.37 5.94 3 -14 -2 93.54 6.28 3 -14 -2 88.89 11.12 3 -14 -2 84.53 7.57 3 -14 -1 20.94 3.48 3 -14 -1 18.42 5.85 3 -14 -1 18.25 3.46 3 -14 -1 11.39 3.26 3 -14 -1 15.95 3.96 3 -14 0 44.68 4.67 3 -14 0 39.37 7.93 3 -14 0 42.00 5.56 3 -14 1 227.63 18.49 3 -14 1 219.66 9.30 3 -14 1 239.14 11.69 3 -14 2 82.18 5.75 3 -14 2 88.91 6.28 3 -14 2 89.16 7.44 3 -14 3 28.61 4.08 3 -14 3 35.47 3.98 3 -14 3 28.40 3.73 3 -14 3 37.98 5.54 3 -14 4 268.84 16.86 -3 14 -4 256.38 17.23 3 -14 4 254.75 9.42 3 -14 4 252.95 9.89 3 -14 4 260.26 11.27 3 -14 4 280.33 12.24 -3 14 -5 124.73 12.44 3 -14 5 127.79 8.29 3 -14 5 126.21 7.05 3 -14 5 126.12 12.15 3 -14 5 154.90 9.42 3 -14 5 153.32 8.81 -3 14 -6 251.88 17.62 3 -14 6 249.82 9.48 3 -14 6 252.40 10.71 3 -14 6 263.44 11.71 3 -14 6 257.09 17.82 3 -14 7 216.59 16.97 3 -14 7 237.94 11.39 3 -14 8 -2.21 2.71 3 -14 8 -4.69 3.48 3 -14 9 0.75 2.48 3 -14 9 4.66 2.46 3 -14 9 -1.12 2.34 3 -14 10 18.14 3.54 3 -14 10 20.65 3.58 3 -14 10 21.97 5.84 3 -14 11 63.16 5.65 3 -14 11 60.09 9.99 3 -14 11 72.53 6.26 3 -14 12 39.16 4.56 3 -14 12 40.25 5.28 3 -14 12 35.10 8.37 3 -14 13 125.55 7.40 3 -14 13 119.59 7.90 3 -14 13 106.71 14.00 3 -14 14 532.29 16.22 3 -14 14 543.79 13.58 3 -14 15 341.89 12.77 3 -14 15 351.59 10.96 3 -14 16 1.25 2.77 3 -14 16 1.63 2.02 3 -14 16 0.44 1.96 3 -14 16 -3.83 2.60 3 -14 17 162.45 8.57 3 -14 17 169.02 7.50 3 -14 17 147.78 6.91 3 -14 18 34.49 4.43 3 -14 18 28.94 3.44 3 -14 18 36.28 3.83 3 -14 19 1.31 1.82 3 -14 19 -2.13 2.51 3 -14 19 -2.71 2.12 3 -14 20 9.09 2.19 3 -14 20 7.22 2.64 3 -14 21 40.85 3.65 3 -14 21 44.17 3.33 3 -14 22 24.39 2.73 3 -14 22 24.85 2.35 3 -14 23 8.88 1.40 3 -14 23 8.33 1.49 3 -13 -16 27.44 2.61 3 -13 -15 83.47 4.91 -3 13 15 51.83 3.22 -3 13 14 56.82 3.95 3 -13 -14 69.67 4.78 3 -13 -13 5.03 2.84 -3 13 13 6.23 2.24 -3 13 12 120.12 6.50 3 -13 -12 146.46 7.93 -3 13 11 48.19 4.64 3 -13 -11 44.04 5.31 3 -13 -11 56.52 5.59 3 -13 -10 -0.23 3.25 -3 13 10 -0.20 2.00 3 -13 -9 37.26 5.42 3 -13 -9 43.81 5.32 3 -13 -8 107.18 7.56 3 -13 -8 103.60 7.85 3 -13 -7 54.67 5.96 3 -13 -7 56.88 5.87 3 -13 -7 59.70 6.01 -3 13 6 36.62 8.20 3 -13 -6 34.43 4.90 3 -13 -6 35.39 5.02 3 -13 -6 36.15 5.17 -3 13 5 -0.45 4.27 3 -13 -5 0.35 2.99 3 -13 -5 -6.95 4.78 3 -13 -5 -3.78 3.74 3 -13 -4 64.58 5.96 3 -13 -4 79.07 9.92 3 -13 -4 69.60 5.79 3 -13 -4 65.31 6.80 3 -13 -3 3.52 2.45 3 -13 -3 -1.10 3.67 3 -13 -3 2.09 2.73 3 -13 -3 -0.48 3.39 3 -13 -2 65.81 9.37 3 -13 -2 53.27 5.02 3 -13 -2 59.00 4.97 3 -13 -2 47.27 4.83 3 -13 -2 55.10 5.93 3 -13 -1 23.99 6.32 3 -13 -1 20.55 3.39 3 -13 -1 25.66 4.33 -3 13 0 2.63 3.06 -3 13 -1 26.87 5.66 -3 13 -2 272.71 16.78 -3 13 -3 433.92 21.22 3 -13 3 443.75 19.99 3 -13 4 12.36 4.17 -3 13 -4 9.19 3.60 3 -13 5 489.19 22.74 -3 13 -5 481.91 23.18 3 -13 6 41.07 7.01 3 -13 7 25.85 5.80 3 -13 8 13.51 4.88 3 -13 9 10.03 2.64 3 -13 9 10.36 4.39 3 -13 10 92.87 6.18 3 -13 10 89.22 6.55 3 -13 10 91.18 11.85 3 -13 11 -0.01 2.43 3 -13 11 1.01 2.19 3 -13 11 1.27 2.91 3 -13 12 1.03 2.32 3 -13 12 -0.11 2.46 3 -13 12 0.62 1.66 3 -13 12 2.73 2.42 3 -13 13 10.37 2.80 3 -13 13 11.02 3.37 3 -13 13 11.65 2.59 3 -13 13 9.89 4.58 3 -13 14 0.78 2.71 3 -13 14 1.08 2.24 3 -13 15 170.20 8.29 3 -13 15 194.74 8.58 3 -13 15 197.58 9.77 3 -13 16 34.22 3.71 3 -13 16 31.15 4.15 3 -13 16 45.19 4.44 3 -13 16 40.29 4.95 3 -13 17 62.06 5.73 3 -13 17 49.02 4.85 3 -13 17 65.33 5.19 3 -13 18 155.04 7.36 3 -13 18 161.62 8.31 3 -13 19 58.43 4.66 3 -13 19 56.65 4.64 3 -13 19 56.40 5.10 3 -13 20 -0.17 1.89 3 -13 20 0.22 1.92 3 -13 20 1.40 2.24 3 -13 21 33.35 3.25 3 -13 21 34.96 3.64 3 -13 21 29.60 3.05 3 -13 22 58.20 3.60 3 -13 22 53.68 3.71 3 -13 23 37.69 2.63 3 -13 23 33.51 2.57 3 -13 24 0.02 0.91 3 -13 24 3.13 0.90 -3 12 17 43.69 2.73 3 -12 -17 44.85 3.24 -3 12 16 72.07 4.11 3 -12 -16 75.45 4.28 -3 12 15 7.10 2.33 3 -12 -15 4.40 2.33 -3 12 14 254.24 9.08 3 -12 -14 285.49 9.92 -3 12 13 108.23 6.65 3 -12 -13 121.62 7.24 3 -12 -12 6.72 3.47 3 -12 -12 -0.83 4.89 -3 12 12 5.87 2.71 3 -12 -11 56.95 5.86 -3 12 11 55.25 5.39 3 -12 -11 67.83 6.17 3 -12 -10 58.67 6.29 3 -12 -10 52.05 6.02 -3 12 10 52.18 5.30 -3 12 9 6.01 2.71 3 -12 -9 8.12 4.21 3 -12 -9 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7.75 3 -8 21 164.93 7.10 3 -8 22 19.09 2.74 3 -8 22 18.40 2.90 3 -8 22 16.23 3.01 3 -8 23 41.54 3.53 3 -8 23 35.02 3.12 3 -8 23 39.02 3.04 3 -8 24 58.95 2.98 3 -8 24 54.78 3.30 3 -8 24 48.82 2.89 -3 7 22 7.59 1.38 -3 7 21 25.10 2.23 -3 7 21 28.82 2.80 -3 7 20 0.39 1.49 -3 7 20 -0.39 2.27 3 -7 -19 6.79 1.81 -3 7 19 12.69 2.58 -3 7 19 11.01 3.05 3 -7 -18 25.38 3.96 -3 7 18 22.76 3.58 3 -7 -18 20.92 3.05 -3 7 18 25.72 4.23 3 -7 -17 1.35 2.82 -3 7 17 2.84 3.19 3 -7 -17 -0.72 2.42 3 -7 -16 13.20 3.61 3 -7 -16 13.86 3.36 -3 7 16 15.86 4.07 3 -7 -15 40.73 5.18 -3 7 15 46.81 5.70 3 -7 -15 41.16 4.89 3 -7 -14 77.93 5.97 -3 7 14 98.48 7.56 3 -7 -14 90.55 7.14 -3 7 14 102.22 13.70 3 -7 -14 92.19 6.82 -3 7 14 102.82 13.60 3 -7 -13 -2.33 3.92 -3 7 13 5.84 4.39 -3 7 13 5.68 3.10 3 -7 -13 7.22 3.44 3 -7 -13 6.20 3.08 3 -7 -12 273.96 11.31 3 -7 -12 268.87 10.66 -3 7 12 287.41 21.79 3 -7 -12 246.29 10.57 3 -7 -11 301.04 11.41 -3 7 11 315.56 22.36 3 -7 -11 304.74 10.80 3 -7 -11 294.31 10.72 -3 7 10 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288.73 13.31 4 -6 7 281.80 16.61 4 -6 8 628.76 20.02 4 -6 8 629.05 25.38 4 -6 9 84.05 10.50 4 -6 9 77.27 7.79 4 -6 10 9.02 3.55 4 -6 10 10.58 5.31 4 -6 11 11.48 5.50 4 -6 12 238.62 18.46 4 -6 13 35.17 7.76 -4 6 -13 27.99 3.91 4 -6 14 98.25 6.52 -4 6 -14 82.58 6.24 4 -6 14 85.62 12.05 -4 6 -14 75.32 5.82 -4 6 -15 66.44 5.52 4 -6 15 73.91 5.52 -4 6 -15 73.44 6.22 4 -6 15 78.25 6.07 4 -6 15 86.88 12.13 -4 6 -16 -1.13 2.83 4 -6 16 2.25 2.63 4 -6 16 5.03 2.54 -4 6 -16 5.02 2.84 4 -6 16 10.75 4.75 4 -6 17 82.06 5.75 -4 6 -17 83.76 6.50 4 -6 17 84.93 6.83 4 -6 18 271.46 9.74 4 -6 18 279.75 11.46 -4 6 -18 268.52 10.76 4 -6 19 22.33 3.29 -4 6 -19 19.24 3.55 4 -6 19 27.27 4.44 4 -6 20 10.47 3.18 4 -6 20 11.41 2.64 4 -6 21 148.77 6.04 4 -6 21 152.93 7.19 4 -6 22 146.59 5.25 4 -6 22 143.43 6.33 4 -6 23 14.44 1.57 4 -6 23 15.28 2.23 4 -6 24 43.47 2.54 -4 5 23 4.17 1.43 -4 5 23 4.78 1.45 -4 5 22 34.08 3.28 -4 5 22 33.78 3.29 -4 5 21 53.73 4.59 -4 5 21 51.91 4.50 4 -5 -20 -2.50 2.33 -4 5 20 2.00 2.43 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11 77.36 6.33 5 -18 11 72.97 5.68 5 -18 12 86.12 5.93 5 -18 12 66.98 4.99 5 -18 12 82.36 6.58 5 -18 13 38.80 4.69 5 -18 13 35.92 3.65 5 -18 13 25.37 3.31 5 -18 14 7.79 2.30 5 -18 14 11.63 3.25 5 -18 15 99.77 6.45 5 -18 15 96.85 5.53 5 -18 16 114.88 6.38 5 -18 16 112.84 5.35 5 -18 17 7.31 2.37 5 -18 17 5.20 1.54 5 -18 17 2.63 1.76 5 -18 18 17.23 2.30 5 -18 18 21.73 2.76 5 -18 19 3.12 1.39 5 -18 19 3.24 1.58 5 -18 20 3.13 1.30 5 -18 20 2.57 1.10 5 -17 -12 1.27 1.12 5 -17 -12 0.65 1.13 5 -17 -11 1.57 1.48 5 -17 -11 -0.58 1.58 5 -17 -10 9.92 2.41 5 -17 -9 26.45 3.44 5 -17 -8 48.19 4.62 5 -17 -7 54.09 5.12 5 -17 -6 112.66 7.11 5 -17 -5 3.39 3.04 5 -17 -4 241.48 8.99 5 -17 -4 247.40 10.72 5 -17 -3 207.29 9.88 5 -17 -2 15.14 3.77 5 -17 -2 18.05 3.72 5 -17 -1 100.22 7.02 5 -17 -1 84.89 6.64 5 -17 0 76.39 6.30 5 -17 0 73.83 6.15 5 -17 1 9.68 2.81 5 -17 1 7.95 2.90 5 -17 2 13.78 3.25 5 -17 2 12.20 3.10 5 -17 3 1.35 2.01 5 -17 3 -0.41 2.23 5 -17 4 5.81 2.59 5 -17 4 7.29 2.86 5 -17 5 2.86 2.38 5 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19 21.49 3.11 5 -11 20 16.32 2.36 5 -11 20 16.67 2.83 -5 11 -20 14.68 2.51 5 -11 20 12.50 2.40 5 -11 21 30.97 2.94 5 -11 21 37.39 3.31 5 -11 22 2.98 1.36 5 -11 22 0.23 0.50 5 -11 23 0.13 0.94 5 -10 -20 9.30 1.44 -5 10 20 11.83 1.67 5 -10 -19 109.08 4.92 -5 10 19 133.32 5.52 -5 10 18 89.59 5.32 -5 10 17 15.93 3.11 -5 10 16 106.37 6.77 5 -10 -16 114.05 6.44 -5 10 15 64.77 5.82 5 -10 -15 60.23 5.15 5 -10 -14 1.16 3.36 -5 10 14 -1.69 3.09 -5 10 13 64.58 6.19 5 -10 -13 71.29 6.09 5 -10 -12 28.72 4.53 -5 10 12 18.44 3.92 -5 10 11 11.40 5.39 5 -10 -11 8.37 3.33 -5 10 11 7.45 2.98 -5 10 10 4.20 4.54 5 -10 -10 -3.11 4.58 -5 10 10 -1.87 3.22 5 -10 -10 0.70 2.99 -5 10 10 0.64 2.72 5 -10 -9 143.94 8.06 -5 10 9 140.57 14.67 -5 10 9 142.48 8.14 5 -10 -9 148.14 8.12 5 -10 -8 45.20 4.91 -5 10 8 49.32 8.54 5 -10 -8 59.63 5.23 -5 10 7 13.98 5.28 -5 10 6 5.82 3.33 -5 10 5 28.11 5.98 -5 10 4 2.91 3.59 -5 10 3 349.20 18.68 -5 10 2 982.04 30.88 -5 10 1 109.16 10.56 -5 10 0 47.03 7.30 -5 10 -1 348.96 18.59 5 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1.94 -5 9 19 18.71 2.92 -5 9 18 123.59 5.84 -5 9 18 147.72 7.37 -5 9 17 129.91 6.64 -5 9 17 131.87 7.54 5 -9 -17 133.15 6.59 -5 9 16 0.12 1.83 5 -9 -16 -1.70 2.88 -5 9 16 -1.44 3.18 -5 9 15 95.29 6.37 -5 9 15 103.05 7.35 5 -9 -15 92.43 6.38 -5 9 14 33.88 4.95 -5 9 14 35.16 4.28 5 -9 -14 34.34 4.43 5 -9 -13 26.56 4.27 -5 9 13 23.36 4.24 -5 9 12 14.78 5.90 5 -9 -12 12.34 3.51 -5 9 12 9.71 3.23 -5 9 11 21.32 7.33 -5 9 11 30.29 7.63 5 -9 -11 20.66 3.53 5 -9 -11 29.96 4.34 -5 9 11 26.76 4.19 -5 9 10 48.71 8.95 5 -9 -10 49.00 4.98 -5 9 10 47.01 5.32 5 -9 -10 54.84 5.28 -5 9 9 14.25 4.77 -5 9 9 21.08 5.87 5 -9 -9 23.03 3.81 5 -9 -9 13.54 3.20 -5 9 8 0.55 2.62 -5 9 8 -2.22 3.52 -5 9 7 170.26 14.31 -5 9 7 158.35 12.35 -5 9 6 2.67 3.12 -5 9 6 4.20 2.39 -5 9 5 130.15 11.88 -5 9 5 117.92 9.21 -5 9 4 20.04 5.13 -5 9 3 137.45 11.63 -5 9 2 844.66 27.38 -5 9 1 1704.95 38.42 -5 9 0 1246.13 32.55 5 -9 0 1303.79 24.30 -5 9 -1 -1.40 4.67 5 -9 1 2.55 2.50 5 -9 2 612.13 19.88 5 -9 3 471.54 18.65 5 -9 4 5.94 3.63 5 -9 5 311.82 17.24 5 -9 6 176.90 13.88 5 -9 7 136.81 12.75 5 -9 8 3.33 4.16 5 -9 9 40.87 8.34 5 -9 10 8.73 4.47 5 -9 11 111.15 13.43 5 -9 12 56.64 4.95 5 -9 12 58.51 4.80 5 -9 12 56.25 10.15 5 -9 13 174.34 7.96 5 -9 13 161.33 8.12 -5 9 -13 147.36 7.52 5 -9 13 172.95 17.33 5 -9 14 22.41 3.59 -5 9 -14 20.28 3.95 -5 9 -14 16.06 3.13 5 -9 14 24.90 7.16 5 -9 15 470.79 13.18 -5 9 -15 444.88 13.07 -5 9 -15 440.89 13.94 -5 9 -16 147.23 7.57 -5 9 -16 139.38 8.11 5 -9 16 148.13 7.55 5 -9 16 145.07 7.77 -5 9 -17 39.40 4.07 5 -9 17 35.90 3.79 5 -9 17 43.94 4.56 -5 9 -17 40.93 4.86 5 -9 17 42.14 4.83 5 -9 18 7.79 2.69 -5 9 -18 10.93 3.34 5 -9 18 9.52 3.23 5 -9 19 36.38 3.70 5 -9 19 37.18 3.95 -5 9 -19 37.94 4.25 5 -9 19 43.55 4.43 5 -9 20 105.46 5.58 5 -9 20 112.66 6.18 -5 9 -20 100.88 5.80 5 -9 21 2.01 1.84 5 -9 21 -2.65 2.15 5 -9 22 25.78 2.40 5 -9 22 21.53 2.54 5 -9 23 -0.59 0.93 5 -9 23 -0.34 1.11 -5 8 22 1.41 0.97 5 -8 -21 4.96 1.30 -5 8 21 6.23 1.76 -5 8 20 69.70 4.00 -5 8 20 80.27 4.87 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100.08 9.62 -5 8 1 61.52 7.87 5 -8 -1 61.97 4.82 -5 8 0 89.02 9.46 5 -8 0 89.49 6.49 5 -8 1 373.19 14.14 5 -8 2 53.33 6.46 5 -8 3 900.50 25.22 5 -8 4 44.62 6.16 5 -8 4 41.03 6.82 5 -8 5 281.70 16.14 5 -8 5 322.99 14.70 5 -8 6 11.03 3.54 5 -8 6 9.49 4.56 5 -8 7 17.35 4.16 5 -8 7 15.38 5.20 5 -8 8 18.04 5.67 5 -8 9 63.26 9.75 5 -8 10 203.98 17.09 5 -8 11 137.44 14.62 5 -8 12 43.99 4.14 5 -8 12 48.33 9.59 5 -8 13 264.83 9.77 -5 8 -13 248.24 9.90 -5 8 -14 197.51 9.02 5 -8 14 197.94 8.70 -5 8 -14 196.63 9.40 5 -8 14 206.79 18.97 -5 8 -15 22.62 4.19 -5 8 -15 19.71 3.40 5 -8 15 30.88 4.14 5 -8 16 155.42 8.01 5 -8 16 138.43 7.48 -5 8 -16 143.05 8.27 -5 8 -16 135.84 7.50 -5 8 -17 192.16 8.71 -5 8 -17 178.86 8.98 5 -8 17 201.90 9.58 5 -8 17 192.82 8.52 5 -8 18 50.18 4.67 -5 8 -18 50.47 4.99 5 -8 18 52.55 5.35 5 -8 19 2.04 2.04 -5 8 -19 5.61 2.78 5 -8 19 4.59 2.76 5 -8 20 71.55 4.61 -5 8 -20 62.21 4.78 5 -8 20 73.87 5.35 5 -8 21 52.32 3.68 5 -8 21 48.09 4.07 5 -8 22 0.40 1.19 5 -8 22 1.62 1.60 5 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45.79 5.15 5 -7 17 51.75 5.43 5 -7 18 106.00 6.21 -5 7 -18 102.19 6.78 5 -7 18 116.76 7.34 5 -7 19 43.99 4.06 -5 7 -19 41.47 4.52 5 -7 19 43.79 4.73 5 -7 20 0.00 1.67 5 -7 20 1.32 2.46 5 -7 21 128.99 6.20 5 -7 21 126.82 5.21 5 -7 22 56.63 3.07 5 -7 22 49.59 3.65 5 -7 23 -0.97 1.28 -5 6 23 13.59 1.73 -5 6 22 31.02 2.86 -5 6 22 32.04 3.03 -5 6 21 1.22 1.76 -5 6 21 -0.52 2.04 -5 6 20 4.41 2.37 -5 6 20 9.87 3.05 -5 6 19 14.65 3.37 -5 6 19 13.11 3.59 -5 6 18 76.00 6.41 -5 6 18 72.83 6.37 5 -6 -17 126.08 7.59 -5 6 17 136.59 8.57 -5 6 17 134.24 8.49 5 -6 -17 120.05 6.54 5 -6 -16 1.04 2.68 -5 6 16 1.38 2.48 -5 6 16 -0.60 3.23 5 -6 -16 1.17 2.28 5 -6 -15 426.83 13.88 -5 6 15 458.92 28.57 -5 6 15 443.69 15.01 5 -6 -15 408.61 12.31 -5 6 15 439.50 26.78 -5 6 14 510.75 29.26 5 -6 -14 449.26 14.07 -5 6 14 502.76 15.70 5 -6 -14 433.34 12.90 -5 6 14 488.76 27.45 -5 6 13 32.54 7.86 -5 6 13 33.00 7.87 5 -6 -13 32.50 4.32 -5 6 13 33.67 4.77 5 -6 -13 30.43 3.86 -5 6 12 9.03 4.57 -5 6 12 3.29 3.64 -5 6 12 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15 83.87 11.97 -5 6 -15 71.31 5.88 5 -6 16 240.22 10.29 -5 6 -16 220.66 9.95 5 -6 16 227.63 9.27 -5 6 -16 225.38 10.24 -5 6 -17 10.91 3.45 -5 6 -17 4.40 2.41 5 -6 17 7.82 2.67 5 -6 17 11.01 3.37 5 -6 18 29.19 3.51 -5 6 -18 29.65 4.32 5 -6 18 31.66 4.54 5 -6 19 106.36 5.62 5 -6 19 112.51 7.00 -5 6 -19 116.00 6.90 5 -6 20 114.40 5.29 5 -6 20 121.06 6.70 5 -6 21 23.79 2.38 5 -6 21 22.09 3.10 5 -6 22 43.20 2.50 5 -6 22 41.92 3.40 -5 6 -23 29.11 2.08 5 -6 23 25.54 2.20 -5 5 23 16.58 2.08 -5 5 23 15.79 2.14 -5 5 22 1.32 1.73 -5 5 22 2.19 1.83 -5 5 21 0.15 2.17 -5 5 21 0.12 2.27 -5 5 20 1.96 2.53 -5 5 20 -1.13 2.94 -5 5 19 0.60 2.58 -5 5 19 -1.29 3.18 5 -5 -18 14.27 3.20 -5 5 18 21.06 4.20 -5 5 18 14.73 3.78 5 -5 -17 185.13 9.05 -5 5 17 201.14 10.47 -5 5 17 201.27 10.21 5 -5 -16 170.03 8.81 -5 5 16 188.01 10.01 5 -5 -15 4.46 2.82 -5 5 15 2.12 4.32 5 -5 -15 4.00 2.28 -5 5 15 5.99 3.03 -5 5 15 4.89 4.13 5 -5 -14 97.98 6.76 -5 5 14 109.87 13.90 -5 5 14 111.75 7.66 5 -5 -14 91.79 6.00 -5 5 14 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11 37.59 4.58 6 -19 12 56.19 4.37 6 -19 12 62.19 5.42 6 -19 12 47.46 3.61 6 -19 13 11.55 2.10 6 -19 13 16.65 3.27 6 -19 13 14.35 2.23 6 -19 14 2.74 2.35 6 -19 14 -0.59 1.44 6 -19 15 50.10 3.39 6 -19 15 62.58 3.90 6 -19 15 64.69 4.72 6 -19 16 23.39 2.94 6 -19 16 20.28 2.10 6 -19 16 16.21 2.04 6 -19 17 14.13 2.31 6 -19 17 8.52 1.57 6 -19 18 -0.05 0.79 6 -19 18 1.38 1.28 6 -18 -11 14.26 1.70 6 -18 -11 14.70 1.75 6 -18 -10 71.21 3.95 6 -18 -10 74.45 4.02 6 -18 -9 6.89 1.97 6 -18 -9 10.70 2.25 6 -18 -8 24.27 3.19 6 -18 -8 23.79 3.09 6 -18 -7 88.66 5.64 6 -18 -7 98.68 5.98 6 -18 -6 63.55 5.19 6 -18 -6 54.95 4.78 6 -18 -5 -0.40 2.37 6 -18 -5 -3.51 2.54 6 -18 -4 178.66 8.71 6 -18 -4 174.61 7.14 6 -18 -4 164.71 8.31 6 -18 -3 131.28 7.72 6 -18 -3 118.30 7.07 6 -18 -2 1.18 2.26 6 -18 -2 3.10 2.74 6 -18 -1 1.00 2.43 6 -18 -1 -0.78 2.29 6 -18 0 14.00 2.98 6 -18 0 7.96 2.95 6 -18 1 1.22 2.14 6 -18 1 -0.35 2.48 6 -18 2 9.06 2.86 6 -18 3 -1.64 2.47 6 -18 4 25.64 3.83 6 -18 5 13.13 3.15 6 -18 6 196.35 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13.24 3.09 6 -15 5 12.52 2.84 6 -15 6 74.49 5.51 -6 15 -6 66.32 10.84 6 -15 6 73.22 5.78 -6 15 -7 164.23 16.88 6 -15 7 170.59 8.09 6 -15 7 173.53 8.54 6 -15 8 34.78 4.21 6 -15 8 27.66 3.84 6 -15 8 35.33 4.14 6 -15 8 42.82 8.07 6 -15 9 355.71 11.89 6 -15 9 365.56 11.62 6 -15 10 93.02 6.19 6 -15 10 92.37 7.02 6 -15 10 96.25 6.23 6 -15 11 10.93 2.64 6 -15 11 7.54 3.12 6 -15 12 -1.31 3.33 6 -15 12 -1.24 2.08 6 -15 13 63.36 5.02 6 -15 13 62.28 5.87 6 -15 14 159.94 8.65 6 -15 15 77.67 6.19 6 -15 15 74.71 5.23 6 -15 16 83.95 5.86 6 -15 16 84.00 5.37 -6 15 -16 75.61 5.38 6 -15 17 -1.70 2.27 6 -15 17 1.00 1.94 -6 15 -17 0.23 1.73 6 -15 18 5.80 2.04 6 -15 18 6.24 2.00 -6 15 -18 6.25 1.95 6 -15 19 -1.51 1.55 6 -15 19 1.84 1.60 -6 15 -19 -1.00 1.28 6 -15 20 -0.78 1.37 6 -15 20 1.00 1.24 6 -15 21 0.20 0.95 6 -14 -16 40.80 2.90 6 -14 -15 65.86 4.23 6 -14 -14 -1.74 2.31 -6 14 14 -2.34 1.37 6 -14 -13 7.83 2.88 6 -14 -12 2.02 2.88 6 -14 -11 1.22 2.98 6 -14 -10 65.98 6.30 6 -14 -9 51.00 5.70 6 -14 -8 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2.22 -6 14 -16 -0.74 2.47 -6 14 -17 14.48 2.89 6 -14 17 8.84 2.52 6 -14 17 14.52 2.89 6 -14 18 0.13 1.89 6 -14 18 1.02 1.95 -6 14 -18 1.27 1.87 6 -14 19 0.32 1.55 6 -14 19 0.16 1.69 -6 14 -19 -0.33 1.50 6 -14 20 21.05 2.25 6 -14 20 21.68 2.46 -6 14 -20 18.71 2.08 6 -14 21 8.19 1.53 6 -14 22 4.24 1.00 6 -13 -17 29.15 2.54 6 -13 -16 1.52 1.69 -6 13 16 0.58 1.15 6 -13 -15 54.25 4.44 -6 13 15 51.41 3.71 6 -13 -14 17.90 3.34 -6 13 14 18.41 2.80 6 -13 -13 -1.50 2.92 -6 13 13 -0.07 1.96 6 -13 -12 -0.69 3.18 -6 13 12 -1.10 2.03 6 -13 -11 1.92 2.76 6 -13 -11 -2.40 3.67 -6 13 11 -0.94 2.12 6 -13 -10 9.15 3.33 6 -13 -10 10.14 3.34 6 -13 -9 8.84 3.25 6 -13 -9 9.14 3.61 6 -13 -8 152.93 9.32 6 -13 -8 170.88 8.98 -6 13 7 91.35 12.24 6 -13 -7 97.56 7.36 6 -13 -7 94.53 7.06 6 -13 -6 15.09 3.69 -6 13 6 10.04 4.83 6 -13 -6 16.60 3.61 6 -13 -5 70.48 6.30 6 -13 -5 70.18 5.73 -6 13 5 72.57 10.57 -6 13 4 286.32 20.19 6 -13 -4 315.43 12.11 -6 13 3 0.97 3.30 6 -13 -3 7.28 2.92 -6 13 2 242.10 18.47 6 -13 -2 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8 -12 3 4.93 2.43 -8 12 -3 4.82 1.85 8 -12 3 4.96 2.24 -8 12 -4 12.87 6.33 8 -12 4 9.66 2.86 -8 12 -4 13.90 2.62 8 -12 4 12.11 2.74 8 -12 5 29.28 3.90 -8 12 -5 22.94 3.14 8 -12 5 28.31 3.97 8 -12 5 30.76 7.19 8 -12 6 193.83 8.70 -8 12 -6 180.64 7.82 8 -12 6 195.14 8.85 8 -12 6 179.64 15.79 -8 12 -7 58.71 4.71 8 -12 7 60.08 5.28 8 -12 7 50.69 9.21 -8 12 -8 185.10 8.17 8 -12 8 192.38 8.68 8 -12 8 171.32 16.88 8 -12 9 248.87 10.06 -8 12 -9 249.73 9.53 8 -12 9 228.10 19.62 -8 12 -10 39.94 4.19 8 -12 10 39.98 4.53 8 -12 10 38.95 8.62 8 -12 11 -1.71 2.83 -8 12 -11 0.73 2.03 8 -12 11 -1.91 2.60 8 -12 12 6.39 2.59 8 -12 12 5.15 2.27 -8 12 -12 5.69 2.33 8 -12 13 122.45 7.04 -8 12 -13 124.21 7.01 8 -12 13 118.07 6.85 8 -12 14 4.83 2.19 -8 12 -14 1.76 1.88 -8 12 -14 0.34 3.21 8 -12 15 12.98 2.59 -8 12 -15 9.63 2.39 -8 12 -15 12.62 3.37 -8 12 -16 73.85 4.71 8 -12 16 72.69 5.12 -8 12 -16 70.31 5.53 8 -12 16 81.83 5.17 8 -12 17 91.16 5.25 -8 12 -17 83.33 5.57 8 -12 17 87.45 5.02 8 -12 18 1.34 1.72 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8 -11 5 28.74 3.59 8 -11 5 26.73 6.27 8 -11 6 16.69 3.05 8 -11 6 16.57 3.23 -8 11 -6 13.36 2.55 8 -11 6 12.80 4.63 -8 11 -7 129.35 6.75 8 -11 7 141.59 7.38 8 -11 8 101.22 6.43 -8 11 -8 99.05 6.10 8 -11 8 83.01 11.83 -8 11 -9 103.42 6.28 8 -11 9 105.07 13.50 8 -11 9 99.11 6.47 -8 11 -10 369.69 11.82 8 -11 10 381.52 12.35 8 -11 10 372.19 25.81 8 -11 10 394.74 12.31 8 -11 11 23.58 3.64 8 -11 11 18.01 3.21 -8 11 -11 19.20 3.21 -8 11 -12 94.81 6.38 8 -11 12 99.67 6.34 8 -11 12 104.80 6.61 8 -11 13 1.66 2.04 -8 11 -13 1.59 2.10 -8 11 -14 16.77 3.03 -8 11 -14 14.25 3.65 -8 11 -15 22.28 3.99 -8 11 -15 20.38 3.20 -8 11 -16 19.92 2.86 8 -11 16 19.94 3.18 -8 11 -16 21.97 3.87 8 -11 16 21.34 3.28 -8 11 -17 101.38 5.36 8 -11 17 105.06 5.57 -8 11 -17 100.37 6.26 8 -11 17 105.56 5.77 8 -11 18 202.30 6.89 -8 11 -18 188.21 7.50 8 -11 18 189.21 6.90 8 -11 19 1.26 1.34 -8 11 -19 0.27 1.62 8 -11 19 -0.75 1.56 8 -11 20 67.22 3.16 8 -11 20 2.02 0.76 -8 10 20 -1.91 1.37 -8 10 19 -0.74 1.70 8 -10 -18 40.79 3.36 -8 10 18 45.30 4.01 8 -10 -17 3.79 2.04 -8 10 17 5.43 2.64 8 -10 -16 97.90 6.09 -8 10 16 109.07 6.89 8 -10 -15 0.64 2.16 -8 10 15 0.37 1.95 -8 10 15 -1.88 2.64 8 -10 -14 31.62 4.35 -8 10 14 37.67 4.68 8 -10 -13 15.79 3.45 -8 10 13 20.19 3.93 8 -10 -12 93.29 6.86 -8 10 12 110.63 7.48 8 -10 -11 98.13 7.15 -8 10 11 115.90 7.50 -8 10 10 74.30 11.59 8 -10 -10 65.56 5.94 -8 10 10 76.51 6.27 -8 10 9 952.96 39.26 8 -10 -9 868.68 19.98 -8 10 9 918.46 19.43 -8 10 8 438.84 26.72 8 -10 -8 473.06 14.31 -8 10 8 422.11 13.12 8 -10 -7 2.50 2.21 -8 10 7 -6.56 4.72 8 -10 -6 54.11 4.97 -8 10 6 42.14 8.34 -8 10 5 350.30 22.13 -8 10 4 14.47 5.57 -8 10 3 27.66 7.20 -8 10 2 82.48 10.89 -8 10 1 34.87 7.54 -8 10 0 7.01 4.86 -8 10 -1 58.94 9.54 -8 10 -2 1.00 3.84 8 -10 3 12.50 4.29 8 -10 4 0.85 2.52 8 -10 5 134.70 13.52 8 -10 6 70.61 5.24 8 -10 6 64.99 9.96 8 -10 7 435.56 12.54 -8 10 -7 427.38 12.08 8 -10 7 408.33 24.48 8 -10 8 548.13 14.06 -8 10 -8 521.71 13.61 8 -10 8 541.52 14.90 8 -10 9 243.75 9.57 -8 10 -9 232.85 9.46 8 -10 9 240.07 10.34 8 -10 9 247.25 20.45 8 -10 10 0.67 2.26 8 -10 10 -3.11 2.60 -8 10 -10 0.18 2.16 8 -10 10 0.72 2.63 8 -10 11 185.88 8.50 -8 10 -11 177.30 8.65 8 -10 11 169.27 8.06 8 -10 11 191.21 18.78 8 -10 12 333.57 11.46 -8 10 -12 302.60 11.31 -8 10 -13 17.51 3.41 -8 10 -13 16.23 3.76 -8 10 -14 3.62 2.37 -8 10 -14 3.38 2.93 -8 10 -15 1.92 1.99 -8 10 -15 1.84 2.93 -8 10 -16 30.83 3.67 8 -10 16 34.02 3.76 -8 10 -16 36.14 4.59 -8 10 -17 -1.01 1.83 8 -10 17 0.26 1.79 -8 10 -17 1.65 2.58 8 -10 17 5.04 2.49 8 -10 18 83.15 4.55 -8 10 -18 80.80 5.24 8 -10 18 86.80 5.07 8 -10 19 102.70 4.42 -8 10 -19 107.37 5.22 8 -10 19 104.18 4.96 8 -10 20 3.21 1.10 8 -10 20 1.32 1.23 -8 9 21 16.41 1.90 -8 9 20 4.11 1.81 -8 9 19 14.34 2.73 8 -9 -18 0.67 1.56 -8 9 18 0.86 2.30 8 -9 -17 24.03 3.27 -8 9 17 24.26 3.35 -8 9 17 27.93 4.08 8 -9 -16 0.97 2.07 -8 9 16 -1.97 2.35 -8 9 16 -0.38 2.74 8 -9 -15 94.38 6.56 -8 9 15 103.44 6.82 -8 9 15 108.53 7.56 8 -9 -14 2.98 2.21 -8 9 14 -1.07 2.38 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10.81 8 -9 10 318.35 10.94 8 -9 10 295.96 11.92 8 -9 10 326.90 23.98 8 -9 11 25.66 3.62 -8 9 -11 24.53 3.83 8 -9 11 23.65 4.27 8 -9 11 26.78 7.75 -8 9 -12 75.94 6.04 8 -9 12 83.94 6.02 8 -9 12 80.71 5.94 -8 9 -13 56.29 5.35 -8 9 -13 57.81 5.85 8 -9 13 60.14 5.21 -8 9 -14 1.15 2.33 -8 9 -14 0.39 2.95 8 -9 14 2.17 2.14 8 -9 15 25.11 3.54 -8 9 -15 25.95 3.72 8 -9 15 29.15 3.85 -8 9 -15 25.26 4.31 -8 9 -16 -1.25 1.98 8 -9 16 -0.67 2.01 -8 9 -16 0.81 2.74 8 -9 16 -0.82 1.99 -8 9 -17 57.34 4.49 8 -9 17 55.69 4.19 -8 9 -17 59.98 5.22 8 -9 17 65.06 5.04 8 -9 18 -0.21 1.54 -8 9 -18 1.16 2.10 8 -9 18 2.04 2.13 8 -9 19 48.94 3.10 -8 9 -19 47.13 3.68 8 -9 19 52.79 3.79 8 -9 20 14.76 1.55 8 -9 20 13.32 1.93 -8 8 22 18.58 1.88 -8 8 21 1.67 1.49 -8 8 20 8.19 2.34 -8 8 19 94.94 5.59 -8 8 19 98.79 6.07 -8 8 18 26.35 3.65 -8 8 18 26.96 4.09 8 -8 -17 35.20 3.85 -8 8 17 40.13 4.50 -8 8 17 46.45 5.12 8 -8 -16 118.28 6.85 -8 8 16 138.72 8.05 -8 8 16 144.40 8.51 -8 8 15 0.33 2.47 -8 8 15 0.73 2.85 -8 8 14 20.07 3.74 -8 8 14 24.07 4.40 -8 8 13 99.54 7.12 -8 8 13 108.94 7.62 -8 8 13 106.24 13.36 -8 8 12 137.64 15.98 -8 8 12 155.40 16.08 -8 8 12 142.32 8.26 -8 8 12 150.83 8.70 -8 8 11 46.22 9.37 -8 8 11 34.88 8.05 -8 8 11 38.66 4.57 -8 8 11 36.96 4.83 8 -8 -10 355.76 12.08 -8 8 10 415.45 24.15 -8 8 10 400.94 25.45 -8 8 10 382.80 12.61 -8 8 10 386.44 12.93 -8 8 9 287.90 20.75 -8 8 9 268.89 10.58 -8 8 8 78.26 11.10 -8 8 7 4.32 3.74 -8 8 6 504.22 24.85 -8 8 5 15.29 5.17 -8 8 4 211.66 15.87 -8 8 3 75.28 9.56 -8 8 2 27.99 6.42 -8 8 1 11.97 4.95 -8 8 0 118.19 11.76 8 -8 0 122.04 9.66 -8 8 -1 25.15 6.08 8 -8 1 23.24 6.04 8 -8 1 20.46 4.79 8 -8 2 66.75 9.62 8 -8 2 57.77 7.98 8 -8 3 5.33 3.59 8 -8 3 1.47 3.08 8 -8 4 328.24 19.96 8 -8 4 290.20 18.65 8 -8 5 171.86 14.73 8 -8 5 163.16 15.05 8 -8 6 288.24 19.09 8 -8 6 256.45 19.14 8 -8 7 364.59 21.72 8 -8 7 358.47 23.17 8 -8 8 103.38 6.22 -8 8 -8 105.07 6.44 8 -8 8 100.98 6.73 8 -8 8 101.27 13.04 8 -8 9 46.32 4.42 -8 8 -9 48.47 4.67 8 -8 9 48.85 5.36 8 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5.98 -8 7 14 69.23 6.34 -8 7 13 -3.94 4.13 -8 7 13 1.32 2.48 -8 7 13 6.35 4.82 -8 7 13 0.56 2.83 -8 7 12 411.24 26.55 -8 7 12 419.73 26.65 -8 7 12 377.71 13.53 -8 7 12 411.77 13.86 -8 7 11 35.52 7.89 -8 7 11 33.85 4.40 -8 7 11 24.37 4.02 -8 7 11 30.01 7.68 -8 7 10 6.90 5.03 -8 7 10 5.86 4.20 -8 7 10 2.29 2.02 -8 7 10 7.04 2.68 -8 7 9 128.81 13.78 -8 7 9 145.61 14.14 -8 7 8 388.63 22.40 -8 7 7 22.76 6.28 -8 7 6 503.12 24.26 -8 7 5 534.30 24.17 -8 7 4 16.18 5.21 -8 7 3 -0.03 3.24 -8 7 2 35.58 6.62 -8 7 1 4.58 3.68 8 -7 -1 10.69 5.23 -8 7 0 16.38 5.21 8 -7 0 18.09 5.57 -8 7 -1 68.69 9.02 8 -7 1 61.57 9.08 8 -7 2 225.72 16.21 8 -7 3 2.58 3.74 8 -7 4 13.21 4.66 8 -7 5 166.98 14.76 8 -7 6 244.38 17.95 8 -7 7 6.51 4.39 -8 7 -8 109.28 6.56 8 -7 8 104.56 6.15 8 -7 8 106.51 12.69 8 -7 8 108.18 7.12 8 -7 9 23.24 3.36 -8 7 -9 21.42 3.44 8 -7 9 25.80 4.21 8 -7 9 26.27 6.36 8 -7 9 23.59 7.14 8 -7 10 0.14 1.95 -8 7 -10 3.66 2.27 8 -7 10 3.39 2.97 8 -7 10 -3.15 4.11 -8 7 -11 429.85 13.70 8 -7 11 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3.52 10 -11 11 2.58 2.30 -10 11 -11 3.83 2.41 -10 11 -12 3.45 2.30 -10 11 -12 4.58 2.99 -10 11 -13 175.43 8.09 -10 11 -13 177.68 8.96 -10 11 -14 55.28 4.51 -10 11 -14 60.93 5.31 -10 11 -15 -1.86 1.79 10 -11 15 -0.41 1.93 -10 11 -15 0.29 2.39 -10 11 -16 53.48 3.71 10 -11 16 56.45 3.62 -10 11 -16 58.69 4.48 10 -11 16 55.81 3.94 10 -11 17 21.10 2.13 -10 11 -17 22.58 2.64 10 -11 17 20.16 2.27 10 -11 18 9.01 1.27 10 -11 18 1.58 0.73 -10 10 20 0.42 0.86 -10 10 20 -1.03 1.07 -10 10 19 10.87 1.78 -10 10 19 9.51 1.97 -10 10 18 -0.50 1.89 -10 10 17 13.63 2.86 -10 10 16 114.87 6.57 -10 10 15 54.75 5.07 10 -10 -14 75.75 5.32 -10 10 14 92.22 6.53 10 -10 -13 295.78 10.57 -10 10 13 353.40 12.29 10 -10 -12 38.00 4.25 -10 10 12 44.13 4.99 10 -10 -11 8.81 2.70 -10 10 11 6.98 3.15 10 -10 -10 22.39 3.59 -10 10 10 21.84 3.82 10 -10 -9 51.28 5.00 -10 10 9 58.14 10.71 -10 10 9 60.75 5.38 -10 10 8 68.38 11.37 10 -10 -8 63.24 5.46 -10 10 8 66.72 5.76 10 -10 -7 -0.01 2.15 -10 10 7 2.31 3.11 -10 10 7 -0.37 2.33 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8.30 -10 9 8 45.22 4.84 10 -9 -7 15.43 2.95 -10 9 7 14.19 5.59 -10 9 7 16.93 3.26 -10 9 6 47.94 9.30 -10 9 6 52.94 4.61 10 -9 -6 49.56 4.64 -10 9 6 46.44 4.48 -10 9 5 3.53 3.71 10 -9 -5 -1.03 1.95 -10 9 5 0.71 2.07 -10 9 4 58.83 4.75 10 -9 -4 51.23 4.57 -10 9 4 57.82 9.81 -10 9 3 0.99 3.42 -10 9 3 0.48 1.82 -10 9 2 102.63 12.59 -10 9 2 105.33 6.11 -10 9 1 54.04 9.28 -10 9 1 49.10 4.32 -10 9 0 9.23 4.83 10 -9 0 5.54 2.13 -10 9 0 7.62 2.46 -10 9 -1 235.25 18.70 -10 9 -1 211.77 8.61 10 -9 1 205.95 8.64 10 -9 1 203.01 8.64 -10 9 -2 175.97 16.43 -10 9 -2 161.04 7.68 10 -9 2 164.47 7.85 10 -9 2 159.48 7.83 10 -9 2 174.95 17.22 -10 9 -2 154.09 7.34 10 -9 3 22.33 3.39 -10 9 -3 22.25 3.37 -10 9 -3 11.65 4.87 10 -9 3 21.68 6.62 10 -9 3 13.02 4.82 -10 9 -4 64.80 10.78 10 -9 4 62.36 5.17 -10 9 -4 60.60 4.99 10 -9 4 60.62 10.55 10 -9 4 50.10 9.07 -10 9 -5 767.08 35.00 10 -9 5 765.75 16.65 -10 9 -5 761.82 17.25 10 -9 5 744.66 35.51 10 -9 5 713.87 33.07 10 -9 6 413.40 12.55 -10 9 -6 427.11 13.04 10 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343.61 24.94 -10 6 12 348.38 12.89 -10 6 11 176.71 17.25 -10 6 11 167.54 8.23 -10 6 11 159.56 8.77 -10 6 10 4.25 3.44 -10 6 10 6.48 2.44 -10 6 10 3.92 2.56 -10 6 9 457.84 26.30 -10 6 9 439.82 13.86 -10 6 8 395.33 23.63 -10 6 8 389.38 12.52 -10 6 7 33.43 3.55 -10 6 7 30.67 7.04 -10 6 7 32.47 3.90 -10 6 6 19.70 5.60 -10 6 5 16.45 5.30 -10 6 4 54.44 8.52 -10 6 3 112.79 11.62 10 -6 -3 109.22 13.28 -10 6 2 205.64 15.44 10 -6 -2 195.13 18.03 -10 6 1 140.61 12.88 10 -6 -1 143.56 15.20 -10 6 0 -1.76 3.41 10 -6 0 -3.77 4.83 -10 6 -1 70.83 9.39 10 -6 1 59.63 10.50 -10 6 -2 178.29 14.89 -10 6 -2 179.72 7.86 10 -6 2 190.60 17.94 -10 6 -3 212.07 16.24 -10 6 -3 216.60 8.90 -10 6 -3 230.74 9.08 10 -6 3 225.20 19.53 -10 6 -3 218.53 8.93 10 -6 4 31.70 3.49 -10 6 -4 30.37 3.82 -10 6 -4 26.88 3.60 10 -6 4 33.65 8.84 -10 6 -4 30.14 3.81 10 -6 5 448.17 12.11 -10 6 -5 459.66 13.38 10 -6 5 478.63 28.77 -10 6 -5 446.88 12.89 10 -6 6 220.63 8.74 -10 6 -6 237.01 10.03 10 -6 6 219.10 20.02 10 -6 6 238.89 10.79 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21.41 2.42 -11 10 18 19.05 2.60 -11 10 17 1.77 1.71 -11 10 17 3.01 2.23 -11 10 16 86.02 5.62 -11 10 15 330.58 10.99 -11 10 14 169.57 8.38 -11 10 13 32.56 4.32 -11 10 12 80.76 6.31 -11 10 11 15.82 3.49 -11 10 10 32.40 4.38 -11 10 9 18.77 3.36 -11 10 9 21.58 3.62 11 -10 -8 17.47 3.09 -11 10 8 19.77 3.44 -11 10 8 21.23 3.67 -11 10 7 49.01 4.86 11 -10 -7 50.99 4.72 -11 10 7 50.96 9.74 -11 10 7 50.30 4.88 -11 10 6 60.46 10.26 -11 10 6 63.77 5.49 11 -10 -6 62.07 5.20 -11 10 6 67.55 5.40 11 -10 -5 1.11 2.48 -11 10 5 2.09 3.36 -11 10 5 -1.48 2.35 -11 10 4 210.15 18.74 -11 10 4 219.49 9.26 11 -10 -4 205.55 9.05 -11 10 3 25.23 3.62 -11 10 3 21.47 6.58 11 -10 -3 19.78 3.36 -11 10 2 27.86 3.73 11 -10 -2 29.65 3.89 -11 10 2 29.81 7.28 11 -10 -1 90.77 6.19 -11 10 1 107.15 6.81 11 -10 -1 95.63 6.27 -11 10 1 111.81 13.69 11 -10 0 1.43 2.27 -11 10 0 6.31 4.20 11 -10 0 3.16 2.47 -11 10 0 0.56 2.44 -11 10 -1 268.25 21.10 -11 10 -1 265.53 10.20 11 -10 1 274.69 10.42 11 -10 1 259.32 10.24 -11 10 -1 256.62 9.81 -11 10 -2 366.36 24.60 11 -10 2 358.08 11.93 -11 10 -2 359.43 11.88 -11 10 -2 345.85 11.21 -11 10 -3 90.16 12.93 11 -10 3 93.35 6.31 -11 10 -3 95.81 6.40 -11 10 -3 83.62 5.65 -11 10 -4 101.85 14.16 11 -10 4 97.55 6.58 -11 10 -4 101.16 6.66 11 -10 5 187.53 8.73 -11 10 -5 194.97 9.12 11 -10 5 201.11 9.82 11 -10 6 91.57 6.18 -11 10 -6 99.01 6.87 11 -10 6 97.75 7.24 11 -10 7 9.37 2.76 -11 10 -7 11.04 3.15 11 -10 7 8.13 3.12 11 -10 8 47.28 4.63 -11 10 -8 42.66 4.76 11 -10 8 49.37 5.38 11 -10 9 61.14 4.96 -11 10 -9 54.11 5.19 11 -10 9 55.48 5.71 11 -10 10 2.04 2.12 -11 10 -10 2.73 2.36 11 -10 10 7.54 2.99 -11 10 -10 2.05 3.03 -11 10 -11 17.63 3.38 -11 10 -11 16.23 3.71 11 -10 11 18.72 3.19 -11 10 -12 80.65 5.76 -11 10 -12 87.77 6.34 11 -10 12 85.35 5.24 -11 10 -13 20.13 3.15 -11 10 -13 19.32 3.36 -11 10 -14 3.71 1.96 11 -10 14 4.94 1.73 -11 10 -14 6.61 2.59 -11 10 -15 30.00 2.99 11 -10 15 31.48 2.60 -11 10 -15 32.88 3.41 11 -10 16 13.11 1.54 -11 10 -16 14.92 2.21 11 -10 16 14.56 2.07 11 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299.51 10.51 -11 8 0 296.31 10.51 11 -8 0 333.82 24.67 -11 8 -1 188.94 16.82 11 -8 1 202.55 8.65 -11 8 -1 203.94 8.88 -11 8 -1 205.28 8.74 11 -8 1 206.54 19.75 -11 8 -1 197.62 8.75 11 -8 2 46.70 4.39 -11 8 -2 47.38 4.66 -11 8 -2 50.43 9.43 -11 8 -2 50.67 4.71 11 -8 2 45.60 9.88 -11 8 -2 51.15 4.76 11 -8 3 19.79 3.36 -11 8 -3 7.86 4.31 -11 8 -3 14.58 3.15 -11 8 -3 19.89 3.28 11 -8 3 11.69 5.84 -11 8 -3 14.98 3.15 11 -8 4 230.38 9.21 -11 8 -4 236.93 9.90 11 -8 4 200.86 19.51 11 -8 4 203.44 18.09 -11 8 -4 235.99 9.54 11 -8 5 342.72 11.14 -11 8 -5 366.97 12.48 11 -8 5 347.99 25.80 11 -8 5 370.86 13.41 11 -8 5 338.89 24.02 -11 8 -5 357.63 11.49 11 -8 6 26.85 3.70 -11 8 -6 31.51 4.25 11 -8 6 26.77 4.50 11 -8 7 14.57 2.93 -11 8 -7 11.82 3.11 11 -8 7 11.53 3.59 11 -8 8 41.14 4.19 -11 8 -8 40.50 4.87 11 -8 8 39.54 5.45 -11 8 -8 39.30 4.74 -11 8 -9 35.98 4.65 11 -8 9 38.88 5.19 -11 8 -9 35.91 4.67 -11 8 -10 39.29 4.68 11 -8 10 40.01 5.29 -11 8 -10 40.40 4.92 -11 8 -11 66.29 5.79 -11 8 -11 72.17 5.94 11 -8 11 67.06 5.52 -11 8 -12 3.30 2.53 -11 8 -12 4.36 2.83 11 -8 12 0.80 2.30 -11 8 -13 11.31 2.72 11 -8 13 11.49 2.04 -11 8 -13 14.52 3.08 11 -8 13 14.05 2.96 -11 8 -14 132.15 6.43 11 -8 14 119.52 4.73 -11 8 -14 137.54 6.56 11 -8 14 133.25 6.02 -11 8 -15 149.09 6.24 -11 8 -15 148.42 6.15 11 -8 15 137.40 5.37 11 -8 16 7.96 1.92 11 -8 17 82.55 3.45 -11 7 22 -0.56 0.95 -11 7 21 -0.04 0.30 -11 7 21 4.88 1.68 -11 7 20 21.26 2.17 -11 7 20 23.77 3.02 -11 7 19 13.04 2.09 -11 7 19 15.05 2.93 -11 7 18 178.88 8.26 -11 7 17 55.97 5.34 -11 7 16 32.50 4.65 -11 7 15 158.80 8.76 -11 7 14 92.18 6.99 -11 7 13 -0.05 2.80 -11 7 12 86.24 6.76 -11 7 11 21.96 4.19 -11 7 10 19.47 6.64 -11 7 10 15.12 2.78 -11 7 10 13.45 3.37 -11 7 9 10.48 5.50 -11 7 9 9.46 2.58 -11 7 9 7.93 2.73 -11 7 8 9.70 4.75 -11 7 8 11.31 2.74 -11 7 8 9.06 3.01 -11 7 7 50.15 4.54 -11 7 7 49.20 8.85 -11 7 7 55.85 5.23 -11 7 6 -0.22 3.47 -11 7 6 0.32 1.87 -11 7 6 -0.15 2.18 -11 7 5 42.40 4.14 -11 7 5 26.89 6.24 -11 7 5 33.99 3.96 -11 7 5 37.55 4.34 -11 7 4 141.15 14.39 -11 7 4 136.10 7.05 -11 7 4 136.64 7.30 -11 7 3 59.37 9.27 -11 7 3 62.39 4.93 -11 7 3 64.19 5.13 11 -7 -2 30.05 3.44 -11 7 2 38.70 4.14 -11 7 2 42.77 8.05 -11 7 2 38.02 4.05 -11 7 2 30.85 3.86 -11 7 1 287.51 19.66 11 -7 -1 276.78 9.81 -11 7 1 281.83 10.09 -11 7 1 296.58 10.42 11 -7 -1 271.58 22.48 -11 7 1 277.21 9.94 -11 7 0 7.38 2.61 11 -7 0 8.12 2.26 -11 7 0 6.75 3.70 -11 7 0 10.06 2.63 -11 7 0 7.28 2.37 11 -7 0 11.44 6.10 -11 7 -1 86.48 10.85 11 -7 1 87.79 5.64 -11 7 -1 94.48 6.17 -11 7 -1 92.14 6.08 11 -7 1 91.49 13.42 -11 7 -1 85.94 6.07 11 -7 2 211.83 8.62 -11 7 -2 222.71 9.34 -11 7 -2 213.52 9.22 11 -7 2 221.29 20.22 -11 7 -2 218.56 9.22 11 -7 3 274.88 9.75 -11 7 -3 285.74 10.84 -11 7 -3 288.45 10.66 11 -7 3 293.12 23.31 -11 7 -3 288.39 10.56 11 -7 4 8.46 2.47 -11 7 -4 9.94 2.94 11 -7 4 13.71 6.54 -11 7 -4 12.84 2.88 11 -7 5 247.55 9.31 -11 7 -5 256.65 10.55 11 -7 5 243.85 21.62 11 -7 5 278.46 11.75 -11 7 -5 258.72 10.17 11 -7 6 13.47 2.58 -11 7 -6 18.69 3.58 11 -7 6 14.42 3.91 11 -7 6 22.34 8.23 11 -7 7 45.46 4.23 -11 7 -7 44.18 5.01 11 -7 7 39.31 5.35 -11 7 -7 45.87 5.09 -11 7 -8 19.74 3.92 11 -7 8 15.29 4.22 -11 7 -8 20.75 3.78 -11 7 -9 -0.43 2.78 11 -7 9 2.10 3.32 -11 7 -9 1.67 2.70 -11 7 -10 1.76 2.54 11 -7 10 7.45 3.81 -11 7 -10 2.98 2.76 -11 7 -11 36.76 4.68 -11 7 -11 35.44 4.44 11 -7 11 34.80 4.36 -11 7 -12 175.56 8.39 11 -7 12 158.44 6.20 -11 7 -12 177.18 8.34 11 -7 12 169.56 7.93 -11 7 -13 32.24 3.83 11 -7 13 32.45 2.73 -11 7 -13 39.28 4.13 11 -7 13 36.95 3.95 -11 7 -14 29.32 3.39 -11 7 -14 34.62 3.66 11 -7 14 32.15 3.43 11 -7 15 165.34 6.05 11 -7 16 157.43 5.53 11 -7 17 3.36 1.11 -11 6 22 1.21 1.16 -11 6 21 -0.78 0.45 -11 6 21 0.29 1.61 -11 6 20 14.80 1.94 -11 6 20 14.41 2.72 -11 6 19 48.98 3.60 -11 6 19 53.43 4.76 -11 6 18 14.22 3.49 -11 6 17 103.22 7.19 -11 6 16 103.43 6.11 -11 6 16 107.84 7.38 -11 6 15 2.55 2.09 -11 6 15 0.52 3.07 -11 6 14 158.68 8.27 -11 6 14 161.18 9.26 -11 6 13 102.97 6.63 -11 6 13 93.11 7.13 -11 6 12 3.75 2.36 -11 6 12 4.32 3.04 -11 6 11 56.22 10.15 -11 6 11 60.14 5.30 -11 6 11 52.44 5.47 -11 6 10 113.95 14.14 -11 6 10 119.86 6.90 -11 6 10 125.08 7.37 -11 6 10 117.04 7.64 -11 6 9 120.80 13.82 -11 6 9 122.22 6.87 -11 6 9 126.80 7.31 -11 6 9 121.87 7.66 -11 6 8 4.44 3.28 -11 6 8 5.27 2.33 -11 6 8 4.44 2.42 -11 6 8 2.80 2.51 -11 6 7 4.43 4.19 -11 6 7 5.94 2.09 -11 6 7 5.87 2.23 -11 6 7 5.41 2.51 -11 6 6 10.11 4.49 -11 6 6 7.34 2.12 -11 6 6 9.09 2.48 -11 6 6 10.59 2.88 -11 6 5 46.09 4.25 -11 6 5 39.98 7.39 -11 6 5 43.75 4.52 -11 6 5 45.32 4.60 -11 6 4 54.96 8.68 -11 6 4 58.95 4.82 -11 6 4 56.53 4.97 -11 6 3 198.55 15.93 -11 6 3 201.41 8.39 -11 6 3 190.29 8.65 -11 6 2 252.03 17.77 -11 6 2 247.73 9.35 -11 6 2 230.46 9.35 11 -6 -2 233.22 20.72 -11 6 2 241.14 9.52 -11 6 1 33.21 3.84 -11 6 1 36.81 7.44 -11 6 1 37.13 4.08 11 -6 -1 32.15 8.50 -11 6 1 34.24 4.04 -11 6 0 214.98 8.97 -11 6 0 229.39 9.33 11 -6 0 210.60 19.68 -11 6 0 218.86 9.38 -11 6 -1 27.96 3.76 -11 6 -1 23.50 3.58 11 -6 1 25.74 8.11 -11 6 -1 23.14 3.58 -11 6 -2 2.39 2.07 -11 6 -2 1.42 1.98 11 -6 2 1.71 4.34 -11 6 -2 0.75 2.12 -11 6 -3 34.09 4.13 -11 6 -3 32.94 4.14 11 -6 3 33.61 8.58 -11 6 -3 30.31 3.93 -11 6 -4 88.81 6.37 11 -6 4 83.27 13.22 -11 6 -4 86.25 6.18 11 -6 5 7.37 2.20 -11 6 -5 10.13 2.99 -11 6 -5 8.50 2.72 11 -6 5 9.94 3.47 11 -6 5 9.57 5.49 11 -6 6 299.42 10.02 -11 6 -6 306.52 11.74 -11 6 -6 312.20 9.84 11 -6 6 320.64 12.69 -11 6 -6 314.86 11.75 -11 6 -7 18.89 3.75 11 -6 7 14.45 4.00 -11 6 -7 17.15 3.51 -11 6 -8 -0.19 2.50 11 -6 8 1.06 3.31 -11 6 -8 0.94 2.75 11 -6 9 8.13 3.73 -11 6 -9 7.59 2.93 -11 6 -9 7.15 3.13 -11 6 -10 1.18 2.76 11 -6 10 1.06 3.47 -11 6 -10 2.17 2.43 -11 6 -11 24.50 3.94 -11 6 -11 24.23 3.83 11 -6 11 20.96 3.76 -11 6 -12 68.80 5.70 -11 6 -12 73.98 5.53 11 -6 12 67.83 5.43 -11 6 -13 162.92 7.60 -11 6 -13 164.24 7.21 11 -6 13 156.22 7.22 -11 6 -14 124.32 6.17 11 -6 14 123.88 5.88 11 -6 15 1.59 1.73 11 -6 16 135.07 4.92 -11 5 22 -0.12 1.36 -11 5 21 19.78 2.77 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1.25 1.88 -12 14 -11 70.98 4.51 -12 14 -11 77.33 5.40 -12 14 -12 64.57 3.93 -12 14 -12 68.81 4.79 -12 14 -13 11.07 1.64 12 -14 13 13.29 2.04 -12 14 -13 14.63 2.46 12 -14 14 -0.17 1.18 -12 14 -14 1.84 1.48 12 -14 15 64.79 2.76 -12 14 -15 66.84 3.27 -12 13 16 7.10 1.42 -12 13 15 1.35 1.28 -12 13 14 37.48 3.26 -12 13 14 30.93 2.57 -12 13 13 1.56 1.72 -12 13 13 4.28 1.61 -12 13 12 -1.13 2.22 -12 13 12 0.80 1.39 12 -13 -11 -1.66 1.74 -12 13 11 0.03 2.10 12 -13 -10 1.99 1.98 -12 13 10 0.02 2.01 12 -13 -9 -1.34 1.97 -12 13 9 -1.03 2.22 -12 13 8 70.26 5.49 12 -13 -8 60.87 5.03 -12 13 7 55.95 5.11 12 -13 -7 45.84 4.56 -12 13 6 167.13 8.27 12 -13 -6 148.92 7.84 12 -13 -5 18.43 3.47 -12 13 5 19.98 3.55 -12 13 4 241.46 9.98 12 -13 -4 232.04 9.91 -12 13 3 98.10 6.75 12 -13 -3 101.51 6.82 12 -13 -2 5.26 2.60 12 -13 -2 4.10 2.40 -12 13 2 6.98 2.73 12 -13 -1 80.18 6.42 -12 13 1 83.88 6.17 12 -13 -1 80.36 6.25 12 -13 0 145.03 8.22 -12 13 0 145.53 7.86 12 -13 0 149.71 8.19 -12 13 0 139.13 7.19 12 -13 1 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8.74 2.43 -12 12 10 5.48 2.64 -12 12 10 4.76 2.07 -12 12 9 105.92 6.72 12 -12 -9 90.82 5.83 -12 12 9 97.34 6.03 -12 12 8 51.16 5.05 12 -12 -8 45.63 4.40 12 -12 -7 1.33 2.16 -12 12 7 1.58 2.36 -12 12 6 96.95 6.52 12 -12 -6 88.28 6.13 -12 12 5 157.01 8.20 12 -12 -5 139.60 7.69 12 -12 -4 1.13 2.04 -12 12 4 0.52 2.47 -12 12 3 131.37 7.58 12 -12 -3 125.20 7.40 12 -12 -2 86.74 6.53 -12 12 2 98.09 6.66 12 -12 -2 96.42 6.52 12 -12 -1 21.38 3.88 12 -12 -1 23.55 3.86 -12 12 1 18.69 3.48 12 -12 0 195.63 9.37 -12 12 0 194.88 9.16 12 -12 0 189.55 9.02 -12 12 0 182.22 8.44 12 -12 1 180.73 9.01 -12 12 -1 181.44 8.74 -12 12 -1 180.08 8.17 12 -12 2 5.65 2.64 -12 12 -2 5.44 2.70 12 -12 3 7.92 2.95 -12 12 -3 8.24 2.73 12 -12 4 6.07 2.86 -12 12 -4 4.32 2.51 12 -12 4 5.37 2.72 12 -12 5 1.39 2.47 -12 12 -5 1.08 2.31 12 -12 5 -0.10 2.42 12 -12 6 0.68 2.21 -12 12 -6 1.97 2.47 12 -12 6 1.90 2.58 12 -12 7 186.50 8.44 -12 12 -7 200.35 8.97 12 -12 7 184.90 8.88 12 -12 8 168.15 7.73 -12 12 -8 163.79 8.15 12 -12 8 149.39 7.90 12 -12 9 4.48 2.15 -12 12 -9 3.67 2.25 -12 12 -10 36.31 4.09 -12 12 -10 35.85 4.41 -12 12 -11 80.24 5.27 -12 12 -11 87.60 5.90 -12 12 -12 13.74 2.49 -12 12 -12 14.34 2.93 -12 12 -13 1.45 1.44 12 -12 13 0.44 1.36 -12 12 -13 3.10 2.03 -12 12 -14 46.45 3.15 12 -12 14 46.67 2.90 -12 12 -14 51.75 3.68 12 -12 15 38.32 2.23 -12 12 -15 41.15 2.86 -12 11 18 51.67 2.80 -12 11 18 44.33 2.61 -12 11 17 14.94 2.04 -12 11 17 13.65 2.00 -12 11 16 7.32 1.96 -12 11 16 5.55 1.83 -12 11 15 99.70 5.34 -12 11 15 89.76 5.16 -12 11 14 101.94 5.77 -12 11 14 87.92 5.60 -12 11 13 0.84 1.91 -12 11 13 -0.03 2.03 -12 11 12 -1.85 2.19 -12 11 12 -0.25 2.27 -12 11 11 26.49 3.80 -12 11 11 23.66 3.50 -12 11 10 0.32 2.53 -12 11 10 -1.17 2.10 -12 11 9 33.98 4.29 -12 11 9 37.94 4.30 -12 11 8 16.14 3.28 -12 11 8 10.49 2.94 -12 11 7 89.34 6.47 12 -11 -7 74.20 5.50 -12 11 7 89.45 5.98 12 -11 -6 0.43 1.90 -12 11 6 0.88 2.41 -12 11 5 183.40 8.79 12 -11 -5 167.42 8.25 -12 11 4 168.32 8.60 12 -11 -4 155.59 8.04 12 -11 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11 -13 9.25 2.36 -12 11 -14 0.57 1.36 12 -11 14 2.09 1.23 -12 11 -14 2.15 1.69 12 -11 15 53.41 2.42 -12 11 -15 61.87 3.46 12 -11 15 55.53 2.89 -12 10 19 3.35 1.05 -12 10 19 2.28 1.12 -12 10 18 62.00 3.40 -12 10 18 55.40 3.53 -12 10 17 140.08 5.56 -12 10 17 131.45 5.87 -12 10 16 57.35 4.13 -12 10 16 55.67 4.35 -12 10 15 1.78 2.10 -12 10 15 -0.44 2.08 -12 10 14 42.56 4.14 -12 10 14 38.24 4.36 -12 10 13 0.39 2.03 -12 10 13 0.94 2.28 -12 10 12 6.23 2.38 -12 10 12 6.49 2.67 -12 10 11 -1.82 2.56 -12 10 11 -0.86 2.40 -12 10 10 23.15 3.71 -12 10 10 24.20 3.75 -12 10 9 11.81 3.02 -12 10 9 7.85 2.51 -12 10 8 3.04 2.27 -12 10 8 2.28 2.31 -12 10 7 1.36 2.36 -12 10 7 2.80 2.22 -12 10 6 64.00 5.53 -12 10 6 64.89 5.43 -12 10 5 38.74 4.46 -12 10 5 40.70 4.38 -12 10 4 145.67 7.97 12 -10 -4 123.88 7.02 -12 10 3 212.08 19.29 -12 10 3 223.26 9.80 12 -10 -3 212.67 9.07 -12 10 3 219.06 9.03 12 -10 -2 24.69 3.78 -12 10 2 29.19 4.24 12 -10 -2 25.32 3.63 -12 10 2 27.63 7.53 -12 10 2 21.20 3.20 -12 10 1 573.20 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7 64.38 5.54 -14 10 7 57.80 4.97 -14 10 7 59.98 4.95 14 -10 -6 20.99 3.26 -14 10 6 24.21 4.03 -14 10 6 23.95 3.50 -14 10 6 24.61 3.60 14 -10 -5 230.77 9.14 -14 10 5 253.26 10.32 -14 10 5 248.37 9.64 14 -10 -4 89.77 5.87 -14 10 4 97.32 6.57 -14 10 4 96.95 6.30 -14 10 4 94.67 6.70 -14 10 3 1.49 2.44 14 -10 -3 -0.21 2.45 -14 10 3 5.09 2.83 -14 10 3 0.11 2.03 -14 10 2 18.54 3.55 14 -10 -2 15.36 2.77 -14 10 2 19.08 3.66 -14 10 2 17.92 3.06 14 -10 -1 10.63 2.47 -14 10 1 17.57 3.52 -14 10 1 15.77 2.89 -14 10 1 15.11 3.26 14 -10 0 0.68 1.82 -14 10 0 -0.39 2.71 -14 10 0 0.26 1.97 -14 10 0 -0.31 2.03 14 -10 1 101.93 5.96 -14 10 -1 112.35 7.00 -14 10 -1 115.21 6.68 14 -10 2 126.60 6.43 -14 10 -2 140.84 7.91 14 -10 2 136.51 8.08 -14 10 -2 136.17 7.09 14 -10 3 14.86 2.69 -14 10 -3 18.85 3.53 14 -10 3 12.00 3.28 14 -10 4 -0.18 1.53 -14 10 -4 -0.07 2.71 14 -10 4 0.40 2.79 -14 10 -4 -1.78 2.27 14 -10 5 12.48 2.18 -14 10 -5 12.66 3.23 14 -10 5 9.78 3.12 -14 10 -5 5.21 2.10 -14 10 -6 142.70 7.50 14 -10 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9 4 166.69 8.98 14 -9 -3 190.46 8.07 -14 9 3 207.12 9.27 -14 9 3 189.68 8.84 -14 9 3 204.06 9.61 -14 9 2 -0.01 2.41 14 -9 -2 -1.60 2.26 -14 9 2 1.17 2.54 -14 9 2 -1.02 2.21 -14 9 1 18.61 3.47 -14 9 1 16.99 3.21 -14 9 1 18.35 3.68 -14 9 0 39.79 4.57 -14 9 0 29.82 3.90 -14 9 0 38.76 4.54 -14 9 -1 11.07 3.22 -14 9 -1 13.40 3.01 -14 9 -2 94.57 6.50 14 -9 2 86.25 6.64 -14 9 -2 84.10 5.91 -14 9 -3 29.10 4.19 14 -9 3 33.80 4.78 -14 9 -4 0.50 2.60 14 -9 4 -0.28 3.02 -14 9 -5 8.92 2.98 14 -9 5 7.65 3.11 -14 9 -6 38.11 4.32 -14 9 -6 34.79 3.54 14 -9 6 41.51 4.76 -14 9 -7 285.31 10.03 -14 9 -7 263.93 8.44 14 -9 7 277.56 10.28 -14 9 -8 36.96 3.93 -14 9 -8 21.63 2.54 -14 9 -9 20.99 2.92 14 -9 9 19.49 2.58 -14 9 -10 -1.13 0.49 14 -9 10 17.78 2.07 -14 9 -11 11.13 1.90 -14 9 -12 3.82 1.20 -14 8 19 19.92 1.88 -14 8 18 17.56 2.23 -14 8 17 -1.27 0.70 -14 8 17 2.52 1.75 -14 8 16 27.29 2.58 -14 8 16 25.34 3.13 -14 8 15 21.77 2.64 -14 8 15 26.37 3.37 -14 8 14 0.41 1.59 -14 8 14 2.37 2.36 -14 8 13 -1.39 1.71 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95.41 5.90 -15 10 6 96.37 6.50 -15 10 5 2.87 2.60 -15 10 5 0.43 2.31 -15 10 5 0.39 1.79 -15 10 4 1.59 2.25 -15 10 4 3.08 2.56 -15 10 4 2.95 1.85 -15 10 3 6.28 2.58 -15 10 3 6.85 2.14 -15 10 3 6.61 2.62 -15 10 2 7.06 2.65 -15 10 2 6.27 2.09 -15 10 2 8.03 2.71 -15 10 1 45.02 4.50 -15 10 1 44.87 4.47 -15 10 0 95.19 6.21 -15 10 0 82.69 5.63 -15 10 -1 56.25 4.95 15 -10 1 45.18 4.78 -15 10 -1 52.58 4.46 -15 10 -2 5.08 2.51 15 -10 2 2.51 2.38 -15 10 -3 42.55 4.24 15 -10 3 39.17 4.44 -15 10 -4 100.96 5.98 15 -10 4 95.73 6.17 -15 10 -5 138.03 6.75 15 -10 5 125.74 6.58 -15 10 -6 6.45 2.25 15 -10 6 6.61 2.54 -15 10 -7 148.25 6.29 15 -10 7 -0.36 0.48 -15 10 -8 7.08 1.88 -15 10 -9 55.26 3.36 -15 10 -10 60.91 3.03 -15 9 16 0.47 1.18 -15 9 16 -0.37 1.09 -15 9 16 -0.14 1.22 -15 9 15 8.64 1.52 -15 9 15 9.77 1.79 -15 9 15 8.85 1.90 -15 9 14 17.06 2.17 -15 9 14 14.16 2.18 -15 9 14 17.98 2.63 -15 9 13 -0.22 1.46 -15 9 13 0.96 1.49 -15 9 13 0.85 1.88 -15 9 12 110.42 5.52 -15 9 12 104.78 5.68 -15 9 12 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