This PDF file includes:

• Fig. S1. TEM characterization of CNCs and latex NPs.
• Fig. S2. Optical microscopy images of the Ch-CNC/NP droplets generated in the MF flow-focusing droplet generator.
• Fig. S3. Characterization of the Ch-CNC droplets loaded with latex NPs.
• Fig. S4. Characterization of the NP-free Ch-CNC droplets.
• Fig. S5. Phase separation of mixtures of Ch-CNC suspension and latex NPs.
• Fig. S6. Schematic of the flat-ellipsoidal droplet structure of the Ch-CNC droplets.
• Fig. S7. TEM images of magnetic Fe₃O₄ NPs.
• Fig. S8. Characterization of the Ch-CNC droplets loaded with magnetic NPs.
• Fig. S9. 3D assemblies of the Ch-CNC droplets loaded with Fe₃O₄ NPs.
• Fig. S10. Characterization of the Ch-CNC droplets with the layers of magnetic NP.
• Fig. S11. Two models of assembly of the Ch-CNC droplets laden with Fe₃O₄ NPs under the magnetic field.

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