data_mo_eo36_0m _audit_creation_date 2018-06-26 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2014/7' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C4 H12 P, I' _chemical_formula_sum 'C4 H12 I P' _chemical_formula_weight 218.01 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'tetragonal' _space_group_IT_number 129 _space_group_name_H-M_alt 'P 4/n m m' _space_group_name_Hall '-P 4a 2a' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+1/2, x, z' '-x+1/2, -y+1/2, z' 'y, -x+1/2, z' 'x+1/2, -y, -z' '-x, y+1/2, -z' 'y+1/2, x+1/2, -z' '-y, -x, -z' '-x, -y, -z' 'y-1/2, -x, -z' 'x-1/2, y-1/2, -z' '-y, x-1/2, -z' '-x-1/2, y, z' 'x, -y-1/2, z' '-y-1/2, -x-1/2, z' 'y, x, z' _cell_length_a 8.1978(10) _cell_length_b 8.1978(10) _cell_length_c 6.0037(8) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 403.47(11) _cell_formula_units_Z 2 _cell_measurement_reflns_used 5087 _cell_measurement_temperature 170.0 _cell_measurement_theta_max 31.829 _cell_measurement_theta_min 3.515 _shelx_estimated_absorpt_T_max 0.942 _shelx_estimated_absorpt_T_min 0.497 _exptl_absorpt_coefficient_mu 4.061 _exptl_absorpt_correction_T_max 0.7464 _exptl_absorpt_correction_T_min 0.3871 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1448 before and 0.0885 after correction. The Ratio of minimum to maximum transmission is 0.5186. The \l/2 correction factor is Not present.' _exptl_absorpt_special_details ? _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.794 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 208 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.015 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0702 _diffrn_reflns_av_unetI/netI 0.0253 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 7940 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.518 _diffrn_reflns_theta_min 3.393 _diffrn_ambient_temperature 170.0 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX3 Photon 100' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 399 _reflns_number_total 448 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XS (Sheldrick, 2008)' _refine_diff_density_max 2.899 _refine_diff_density_min -1.037 _refine_diff_density_rms 0.164 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.232 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 13 _refine_ls_number_reflns 448 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0501 _refine_ls_R_factor_gt 0.0423 _refine_ls_restrained_S_all 1.232 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0220P)^2^+2.5021P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0914 _refine_ls_wR_factor_ref 0.0962 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.5 times of: All C(H,H,H) groups 2. Others Fixed Sof: H1A(0.5) H1C(0.5) H1B(0.5) 3.a Idealised Me refined as rotating group: C1(H1A,H1C,H1B) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary heavy _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.2500 0.2500 0.16010(13) 0.0279(2) Uani 1 8 d S T P . . P1 P 0.2500 -0.2500 0.5000 0.0211(5) Uani 1 8 d S T P . . C1 C 0.2500 -0.0772(9) 0.6743(12) 0.064(3) Uani 1 2 d S T P . . H1A H 0.2195 0.0193 0.5875 0.096 Uiso 0.5 1 calc GR . . A -1 H1C H 0.3592 -0.0617 0.7373 0.096 Uiso 0.5 1 calc GR . . A -1 H1B H 0.1712 -0.0931 0.7952 0.096 Uiso 0.5 1 calc GR . . A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.0291(3) 0.0291(3) 0.0256(4) 0.000 0.000 0.000 P1 0.0222(7) 0.0222(7) 0.0187(11) 0.000 0.000 0.000 C1 0.136(9) 0.023(3) 0.033(3) -0.007(3) 0.000 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 C1 1.761(7) 12_556 ? P1 C1 1.761(7) 10_656 ? P1 C1 1.761(7) . ? P1 C1 1.761(7) 3_545 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 P1 C1 110.7(2) 12_556 3_545 ? C1 P1 C1 110.7(2) 10_656 . ? C1 P1 C1 107.1(5) 12_556 10_656 ? C1 P1 C1 107.1(5) 3_545 . ? C1 P1 C1 110.7(2) 3_545 10_656 ? C1 P1 C1 110.7(2) 12_556 . ? _shelx_res_file ; mo_eo36_0m.res created by SHELXL-2014/7 TITL mo_EO36_0m in P4/nmm #129 REM reset to P4/nmm #129 CELL 0.71073 8.1978 8.1978 6.0037 90 90 90 ZERR 2 0.001 0.001 0.0008 0 0 0 LATT 1 SYMM 0.5-Y,+X,+Z SYMM 0.5-X,0.5-Y,+Z SYMM +Y,0.5-X,+Z SYMM 0.5+X,-Y,-Z SYMM -X,0.5+Y,-Z SYMM 0.5+Y,0.5+X,-Z SYMM -Y,-X,-Z SFAC C H I P UNIT 8 24 2 2 L.S. 20 PLAN 20 SIZE 0.1 0.2 0.015 TEMP -103.15 BOND fmap 2 53 ACTA REM REM REM WGHT 0.022000 2.502100 FVAR 0.24484 I1 3 0.250000 0.250000 0.160101 10.12500 0.02914 0.02914 = 0.02556 0.00000 0.00000 0.00000 P1 4 0.250000 -0.250000 0.500000 10.12500 0.02224 0.02224 = 0.01867 0.00000 0.00000 0.00000 C1 1 0.250000 -0.077208 0.674346 10.50000 0.13619 0.02269 = 0.03339 -0.00698 0.00000 0.00000 PART -1 AFIX 137 H1A 2 0.219548 0.019330 0.587514 10.50000 -1.50000 H1C 2 0.359203 -0.061732 0.737306 10.50000 -1.50000 H1B 2 0.171249 -0.093078 0.795227 10.50000 -1.50000 AFIX 0 HKLF 4 REM mo_EO36_0m in P4/nmm #129 REM R1 = 0.0423 for 399 Fo > 4sig(Fo) and 0.0501 for all 448 data REM 13 parameters refined using 0 restraints END WGHT 0.0219 2.5031 REM Highest difference peak 2.899, deepest hole -1.037, 1-sigma level 0.164 Q1 1 0.2500 0.2500 0.2877 10.12500 0.05 2.90 Q2 1 0.2500 0.2500 0.0194 10.12500 0.05 1.74 Q3 1 0.2500 0.2500 0.4504 10.12500 0.05 1.28 Q4 1 0.2500 0.2500 -0.0896 10.12500 0.05 1.18 Q5 1 0.2500 0.2500 0.5865 10.12500 0.05 0.66 Q6 1 0.2500 -0.1786 0.8875 10.50000 0.05 0.65 Q7 1 0.0607 0.2500 0.1553 10.50000 0.05 0.61 Q8 1 0.2500 0.1634 0.7811 10.50000 0.05 0.60 Q9 1 0.2500 -0.1777 0.6927 10.50000 0.05 0.57 Q10 1 0.2500 0.1611 0.3318 10.50000 0.05 0.54 Q11 1 0.2500 0.1110 0.6247 10.50000 0.05 0.51 Q12 1 0.0024 -0.2500 0.8924 10.50000 0.05 0.51 Q13 1 0.2500 -0.1303 0.5580 10.50000 0.05 0.48 Q14 1 0.2500 -0.0337 0.7787 10.50000 0.05 0.47 Q15 1 0.2500 0.0916 0.4476 10.50000 0.05 0.45 Q16 1 0.1929 -0.0641 0.6380 11.00000 0.05 0.45 Q17 1 0.2500 -0.1246 1.0402 10.50000 0.05 0.44 Q18 1 0.1684 -0.2500 0.7868 10.50000 0.05 0.42 Q19 1 0.1412 0.1412 0.5616 10.50000 0.05 0.35 Q20 1 0.2500 0.0117 0.8284 10.50000 0.05 0.32 ; _shelx_res_checksum 1903 _shelx_hkl_file ; 1 -1 0 145.07 9.70 1 1 0 127.27 9.69 1 1 0 148.83 9.70 1 1 0 151.28 9.70 -1 -1 0 155.01 9.70 -1 1 0 130.70 9.68 1 -1 0 125.06 9.68 -1 -1 0 165.14 9.71 2 1 0 0.24 0.30 2 1 0 0.63 0.32 -1 2 0 0.53 0.24 1 -2 0 0.18 0.19 -2 -1 0 0.03 0.26 -2 -1 0 0.37 0.23 -2 -1 0 0.13 0.19 1 -2 0 0.60 0.28 2 1 0 0.06 0.17 -2 -1 0 0.30 0.22 -1 2 0 0.04 0.19 2 1 0 0.40 0.29 2 0 0 950.00 65.28 2 0 0 953.80 65.28 0 2 0 973.00 65.43 0 -2 0 967.67 65.42 -2 0 0 1000.00 65.32 2 -1 0 0.29 0.14 1 2 0 0.22 0.23 -1 -2 0 0.43 0.27 -2 1 0 0.02 0.15 -2 1 0 0.18 0.22 2 -1 0 0.20 0.10 -2 2 0 436.92 26.38 -2 -2 0 341.98 26.37 2 2 0 366.87 26.36 2 -2 0 349.05 26.33 2 2 0 408.93 26.37 2 2 0 399.01 26.37 -2 -2 0 451.68 26.40 -2 2 0 372.25 26.35 3 2 0 -0.08 0.25 -3 -2 0 -0.01 0.30 2 -3 0 0.58 0.42 3 2 0 0.16 0.39 3 2 0 -0.24 0.43 -3 -2 0 -0.11 0.27 2 -3 0 -0.36 0.23 -2 3 0 -0.21 0.26 -2 3 0 0.07 0.30 -3 -2 0 0.33 0.30 3 2 0 0.56 0.42 -3 -2 0 -0.24 0.33 -3 -1 0 329.48 20.28 1 -3 0 274.46 20.28 1 -3 0 327.43 20.32 -1 3 0 278.92 20.29 -1 3 0 314.90 20.32 -3 -1 0 316.75 20.27 3 1 0 291.73 20.31 3 1 0 268.90 20.25 3 1 0 301.26 20.29 3 1 0 330.36 20.30 -3 -1 0 270.25 20.28 0 -3 0 0.41 0.32 -3 0 0 -0.01 0.31 -3 0 0 0.19 0.19 0 3 0 0.00 0.27 -3 0 0 -0.06 0.28 0 3 0 0.68 0.32 0 -3 0 0.16 0.26 1 3 0 275.83 19.81 1 3 0 324.28 19.85 -1 -3 0 257.51 19.80 -3 1 0 288.83 19.76 -1 -3 0 319.00 19.84 -3 2 0 -0.02 0.36 3 -2 0 0.02 0.14 2 3 0 0.20 0.38 2 3 0 0.05 0.30 -3 2 0 0.21 0.22 2 3 0 0.27 0.39 2 3 0 -0.05 0.36 -2 -3 0 -0.09 0.28 -2 -3 0 -0.08 0.37 -3 -3 0 241.26 17.47 3 3 0 232.84 17.45 -3 3 0 264.61 17.47 3 -3 0 256.16 17.46 3 3 0 269.29 17.48 3 3 0 265.66 17.47 -3 -3 0 285.45 17.51 -3 3 0 247.73 17.44 -4 -3 0 0.48 0.45 4 3 0 0.17 0.59 4 3 0 0.47 0.62 3 -4 0 0.28 0.29 3 -4 0 0.59 0.57 -4 -3 0 0.36 0.38 4 3 0 0.35 0.56 4 3 0 0.33 0.34 -2 4 0 332.02 21.73 -2 4 0 347.20 21.76 -4 -2 0 319.41 21.69 -4 -2 0 317.58 21.72 2 -4 0 302.81 21.70 4 2 0 313.72 21.69 -4 -2 0 315.40 21.69 -4 -1 0 -0.14 0.37 4 1 0 -0.13 0.20 -4 -1 0 -0.13 0.34 1 -4 0 0.80 0.43 1 -4 0 0.19 0.31 4 1 0 -0.50 0.52 -4 -1 0 -0.18 0.30 -4 0 0 489.43 33.01 0 -4 0 508.02 33.05 -4 0 0 527.28 33.02 0 4 0 443.54 33.02 0 4 0 506.13 33.06 -4 0 0 465.16 33.01 -4 0 0 506.12 32.98 0 -4 0 467.00 33.03 -4 1 0 0.08 0.23 -1 -4 0 0.17 0.40 -1 -4 0 0.26 0.34 2 4 0 323.98 22.32 -2 -4 0 363.96 22.36 2 4 0 310.43 22.31 2 4 0 329.56 22.32 2 4 0 348.49 22.36 -2 -4 0 308.40 22.31 -4 2 0 322.95 22.26 4 -3 0 -0.07 0.18 -4 3 0 0.16 0.41 -3 -4 0 1.03 0.76 -4 3 0 0.22 0.32 -3 -4 0 0.20 0.40 4 4 0 265.45 17.25 4 4 0 273.30 17.26 4 4 0 234.74 17.29 -4 -4 0 245.84 17.24 -4 -4 0 263.85 17.29 -4 4 0 255.85 17.21 -4 4 0 257.01 17.24 4 4 0 239.52 17.22 4 -4 0 247.88 17.17 -5 -4 0 0.46 0.53 4 -5 0 0.61 0.68 3 -5 0 83.76 5.88 -5 -3 0 87.15 5.91 5 3 0 77.99 5.87 5 3 0 81.24 5.72 -3 5 0 88.85 5.83 5 3 0 73.44 5.87 5 3 0 73.68 5.87 -5 -3 0 85.05 5.78 3 -5 0 85.95 5.73 -3 5 0 92.54 5.82 -5 -2 0 0.85 0.38 -5 -2 0 0.81 0.38 -5 -2 0 -0.02 0.48 2 -5 0 1.40 0.58 -5 -1 0 88.25 6.06 -5 -1 0 94.79 6.14 5 1 0 91.46 6.00 5 1 0 78.49 6.02 1 -5 0 80.96 6.09 1 -5 0 89.02 6.16 -1 5 0 94.53 6.16 -5 -1 0 89.28 6.08 -5 -1 0 88.10 6.06 -5 0 0 -0.33 0.33 -5 0 0 -0.72 0.40 -5 0 0 -0.58 0.48 0 -5 0 0.54 0.51 1 5 0 88.50 6.35 -5 1 0 89.17 6.10 1 5 0 92.90 6.22 -1 -5 0 85.19 6.17 -5 2 0 -0.58 0.44 -5 2 0 0.39 0.30 -5 3 0 84.82 6.18 3 5 0 87.06 6.25 3 5 0 96.44 6.22 3 5 0 89.52 6.20 -3 -5 0 82.29 6.18 -5 3 0 86.34 6.11 3 5 0 92.62 6.22 -3 -5 0 90.94 6.25 -4 -5 0 0.82 0.76 5 5 0 56.08 3.77 -5 5 0 49.16 3.58 -5 -5 0 45.49 3.71 5 5 0 45.09 3.76 5 5 0 47.22 3.60 -5 5 0 50.03 3.60 -5 -5 0 44.00 3.60 5 5 0 54.84 3.73 6 5 0 1.92 1.06 -5 6 0 1.14 0.72 -6 -5 0 0.71 0.91 -5 6 0 1.06 0.67 -6 -5 0 0.90 0.71 6 5 0 3.22 1.11 5 -6 0 0.50 0.42 6 5 0 1.77 0.73 6 5 0 2.58 1.21 6 4 0 160.31 10.58 -4 6 0 165.04 10.67 -4 6 0 157.71 10.65 6 4 0 131.85 10.72 4 -6 0 156.48 10.54 -6 -4 0 159.52 10.70 -6 -4 0 164.30 10.66 6 4 0 141.33 10.74 3 -6 0 -0.01 0.48 -6 -3 0 0.04 0.52 6 3 0 -0.18 0.40 -6 -3 0 -0.09 0.62 6 3 0 -0.15 0.84 -3 6 0 1.34 0.62 3 -6 0 -0.72 0.83 -6 -2 0 209.08 16.57 -6 -2 0 209.52 16.58 6 2 0 279.98 16.61 -2 6 0 247.23 16.68 -6 -2 0 252.13 16.64 2 -6 0 230.16 16.63 -2 6 0 253.15 16.71 2 -6 0 268.59 16.77 6 2 0 243.85 16.54 -6 -2 0 255.49 16.95 -6 -1 0 -0.35 0.42 1 -6 0 0.48 0.47 -6 -1 0 -0.61 0.51 1 -6 0 1.21 0.71 -6 -1 0 -0.36 0.55 0 6 0 319.30 20.40 -6 0 0 258.62 20.29 -6 0 0 275.42 20.31 -6 0 0 337.68 20.27 0 6 0 310.43 20.36 0 -6 0 285.82 20.32 0 -6 0 299.61 20.37 -6 0 0 307.74 20.34 1 6 0 2.31 0.66 -1 -6 0 0.00 0.50 1 6 0 2.09 0.62 -1 -6 0 1.20 0.69 2 6 0 242.50 15.78 -6 2 0 244.49 15.66 2 6 0 213.83 15.78 -2 -6 0 235.63 15.75 -2 -6 0 195.62 15.81 2 6 0 233.81 15.75 -6 2 0 238.42 15.71 2 6 0 240.52 15.77 3 6 0 1.68 0.71 -3 -6 0 1.10 0.63 3 6 0 1.83 0.75 -3 -6 0 0.97 0.76 3 6 0 3.21 0.84 4 6 0 163.61 10.97 4 6 0 167.00 10.96 4 6 0 162.45 10.96 4 6 0 131.46 10.98 -6 4 0 154.35 10.87 -4 -6 0 157.37 10.95 -6 4 0 174.23 10.94 5 6 0 2.88 1.02 5 6 0 2.26 1.00 -6 5 0 1.19 0.66 5 6 0 2.51 0.95 5 6 0 2.31 0.83 -6 5 0 1.41 0.66 -5 -6 0 3.02 0.97 -6 -6 0 100.54 6.98 -6 -6 0 84.57 7.04 6 6 0 103.15 7.09 6 6 0 103.22 7.11 -6 6 0 96.14 6.93 6 6 0 99.40 6.95 -6 6 0 103.40 6.94 6 6 0 93.91 7.12 -6 7 0 -0.05 0.82 7 6 0 1.24 0.96 7 6 0 -2.16 1.39 -6 7 0 1.20 1.03 7 6 0 0.36 1.32 7 6 0 -0.01 1.49 -7 -6 0 -0.01 0.91 -7 -5 0 26.15 2.21 5 -7 0 24.75 1.90 7 5 0 23.10 2.77 -5 7 0 24.37 2.36 -5 7 0 27.15 2.23 7 5 0 19.21 2.72 -4 7 0 1.96 0.77 4 -7 0 1.35 0.59 4 -7 0 -0.70 1.20 7 4 0 2.66 1.16 7 4 0 1.02 0.58 -7 -4 0 0.37 0.68 7 4 0 0.69 1.06 -4 7 0 0.65 0.95 -7 -4 0 2.23 0.91 -3 7 0 43.22 3.16 3 -7 0 43.20 3.04 7 3 0 39.80 2.89 -7 -3 0 41.02 3.18 -7 -3 0 39.07 3.06 7 3 0 39.56 3.02 3 -7 0 33.59 3.82 -3 7 0 42.78 3.17 -7 -2 0 0.86 0.51 -2 7 0 0.99 0.75 -7 -2 0 -0.35 0.57 2 -7 0 0.13 0.62 -7 -2 0 -0.80 0.68 -7 -2 0 0.72 0.52 -2 7 0 1.10 0.71 2 -7 0 -0.43 0.91 -7 -1 0 56.16 3.73 -7 -1 0 48.27 3.53 1 -7 0 42.02 3.78 -1 7 0 48.85 3.72 -7 -1 0 51.79 3.58 1 -7 0 48.66 3.63 -7 -1 0 51.00 3.56 -1 7 0 48.32 3.70 0 -7 0 1.70 0.89 -7 0 0 0.17 0.48 0 7 0 1.32 0.77 0 7 0 0.40 0.98 -7 0 0 -0.95 0.69 0 -7 0 0.04 0.59 -7 0 0 -1.08 0.71 -7 0 0 -1.04 0.79 -1 -7 0 45.46 3.36 -7 1 0 44.66 3.36 -7 1 0 48.67 3.42 1 7 0 44.12 3.43 -1 -7 0 39.14 3.47 -7 1 0 40.18 3.31 1 7 0 45.75 3.45 1 7 0 47.68 3.52 -2 -7 0 0.68 0.71 2 7 0 2.93 0.88 2 7 0 3.83 0.98 2 7 0 2.02 0.84 2 7 0 3.75 0.96 3 7 0 46.23 3.40 -3 -7 0 44.14 3.27 3 7 0 44.31 3.35 3 7 0 45.70 3.36 -7 3 0 38.54 3.13 -7 3 0 34.93 3.23 -4 -7 0 -0.60 0.78 4 7 0 0.80 1.00 -7 4 0 0.78 0.61 4 7 0 2.50 0.96 4 7 0 2.16 1.01 -7 4 0 1.86 0.74 4 7 0 0.64 0.96 -5 -7 0 28.68 2.44 5 7 0 25.00 2.53 5 7 0 22.59 2.57 5 7 0 25.87 2.47 -7 5 0 25.36 2.26 5 7 0 26.30 2.60 -7 5 0 27.75 2.30 -6 -7 0 -0.24 0.96 -7 6 0 1.08 0.92 6 7 0 0.03 1.18 6 7 0 -0.23 1.26 6 7 0 0.91 1.15 -7 6 0 0.66 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