data_amx-f05-100k-me _audit_creation_date 2017-07-27 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5337) ; _shelx_SHELXL_version_number '2014/7' _publ_contact_author_address 'Department of Chemical Science, IISER Mohali' _publ_contact_author_email angshurc@iisermohali.ac.in _publ_contact_author_id_orcid ? _publ_contact_author_name 'Angshuman Roy Choudhury' _publ_contact_author_phone 8054001404 _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C17 H17 Cl N3 O)+, (C4 H3 O4)-, (C2 H O2)-, 2(H2 O)' _chemical_formula_sum 'C40 H42 Cl2 N6 O10' _chemical_formula_weight 837.69 _chemical_melting_point ? _chemical_oxdiff_formula 'C21 H20 O5 N3 Cl1' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.2238(2) _cell_length_b 12.4815(2) _cell_length_c 17.0725(3) _cell_angle_alpha 86.2850(10) _cell_angle_beta 89.375(2) _cell_angle_gamma 82.224(2) _cell_volume 1943.33(6) _cell_formula_units_Z 2 _cell_measurement_reflns_used 16018 _cell_measurement_temperature 100.0(2) _cell_measurement_theta_max 33.0250 _cell_measurement_theta_min 2.5720 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 0.235 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.95865 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.7f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.432 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 876 _exptl_crystal_preparation ? _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.25 _exptl_crystal_size_min 0.05 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0249 _diffrn_reflns_av_unetI/netI 0.0259 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.952 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 43941 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.952 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 32.848 _diffrn_reflns_theta_min 2.531 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.952 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -69.00 118.20 0.30 20.00 -- 29.89 54.00 120.00 624 2 \w -69.00 118.20 0.30 20.00 -- 29.89 54.00-150.00 624 3 \w -69.00 118.20 0.30 20.00 -- 29.89 54.00 0.00 624 4 \w -69.00 59.10 0.30 20.00 -- 29.89 54.00 30.00 427 5 \w -69.00 118.20 0.30 20.00 -- 29.89 54.00 -90.00 624 ; _diffrn_measurement_device 'two-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Mini (ROW)' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0232778000 _diffrn_orient_matrix_UB_12 0.0558666000 _diffrn_orient_matrix_UB_13 0.0042036000 _diffrn_orient_matrix_UB_21 0.0491894000 _diffrn_orient_matrix_UB_22 -0.0009392000 _diffrn_orient_matrix_UB_23 0.0317604000 _diffrn_orient_matrix_UB_31 0.0553387000 _diffrn_orient_matrix_UB_32 0.0134613000 _diffrn_orient_matrix_UB_33 -0.0265895000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 11488 _reflns_number_total 13758 _reflns_odcompleteness_completeness 99.88 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 25.01 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.39.7f (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.7f (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.7f (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _refine_diff_density_max 0.605 _refine_diff_density_min -0.298 _refine_diff_density_rms 0.063 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 530 _refine_ls_number_reflns 13758 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0519 _refine_ls_R_factor_gt 0.0418 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0611P)^2^+0.5281P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1095 _refine_ls_wR_factor_ref 0.1188 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H,H) groups At 1.5 times of: All O(H) groups, All O(H,H) groups 2.a Free rotating group: O9(H9A,H9B), O10(H10A,H10B) 2.b Secondary CH2 refined with riding coordinates: N3(H3A,H3B), N6(H6A,H6B), C15(H15A,H15B), C17(H17A,H17B), C16(H16A,H16B), C32(H32A,H32B), C14(H14A,H14B), C34(H34A,H34B), C31(H31A,H31B), C33(H33A,H33B) 2.c Aromatic/amide H refined with riding coordinates: C4(H4), C9(H9), C40(H40), C36(H36), C12(H12), C21(H21), C37(H37), C6(H6), C29(H29), C23(H23), C26(H26), C7(H7), C27(H27), C11(H11), C10(H10), C24(H24), C28(H28) 2.d Idealised tetrahedral OH refined as rotating group: O4(H4A) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.12497(3) -0.10624(2) -0.24370(2) 0.02477(6) Uani 1 1 d . . . . . Cl2 Cl 0.36223(3) 0.14355(3) 0.73499(2) 0.02856(7) Uani 1 1 d . . . . . O1 O 0.45558(8) -0.11184(6) 0.04797(4) 0.01727(13) Uani 1 1 d . . . . . O6 O 0.84676(8) -0.48997(6) 0.87453(4) 0.01916(14) Uani 1 1 d . . . . . O2 O 0.04116(8) 0.11447(6) 0.44437(4) 0.01910(14) Uani 1 1 d . . . . . O5 O 0.69860(8) -0.42627(7) 0.97025(4) 0.02106(15) Uani 1 1 d . . . . . O7 O 0.24747(8) -0.44303(7) 0.52813(5) 0.02245(15) Uani 1 1 d . . . . . O9 O 0.08229(9) -0.43953(7) 0.27552(5) 0.02300(15) Uani 1 1 d . . . . . H9A H 0.0067 -0.4656 0.2925 0.035 Uiso 1 1 d G . . . . H9B H 0.1027 -0.4601 0.2297 0.035 Uiso 1 1 d G . . . . O10 O 0.31803(9) -0.48590(7) 0.37557(5) 0.02426(16) Uani 1 1 d . . . . . H10A H 0.2471 -0.4774 0.3434 0.036 Uiso 1 1 d G . . . . H10B H 0.2867 -0.4696 0.4208 0.036 Uiso 1 1 d G . . . . O4 O 0.37482(8) -0.46823(7) 0.74197(4) 0.02361(16) Uani 1 1 d . . . . . H4A H 0.3031 -0.4777 0.7145 0.035 Uiso 1 1 calc GR . . . . O8 O 0.16346(9) -0.49328(7) 0.64609(4) 0.02566(17) Uani 1 1 d . . . . . O3 O 0.21340(8) -0.48043(7) 0.84023(5) 0.02472(16) Uani 1 1 d . . . . . N1 N 0.20364(9) 0.02387(7) 0.10269(5) 0.01622(15) Uani 1 1 d . . . . . N3 N 0.05172(9) 0.37244(6) -0.04452(5) 0.01576(15) Uani 1 1 d . . . . . H3A H -0.0120 0.4273 -0.0673 0.019 Uiso 1 1 calc R . . . . H3B H 0.1284 0.4014 -0.0253 0.019 Uiso 1 1 calc R . . . . N2 N 0.13863(9) 0.14760(6) -0.00091(5) 0.01541(15) Uani 1 1 d . . . . . N4 N 0.29509(10) -0.02621(7) 0.39816(5) 0.01754(15) Uani 1 1 d . . . . . N5 N 0.36003(9) -0.13802(7) 0.50752(5) 0.01702(15) Uani 1 1 d . . . . . N6 N 0.47976(9) -0.34779(7) 0.57125(5) 0.01853(16) Uani 1 1 d . . . . . H6A H 0.4076 -0.3882 0.5617 0.022 Uiso 1 1 calc R . . . . H6B H 0.5541 -0.3920 0.5962 0.022 Uiso 1 1 calc R . . . . C1 C 0.20333(10) 0.04544(7) 0.02772(6) 0.01447(16) Uani 1 1 d . . . . . C8 C 0.25274(11) -0.07923(7) 0.13765(6) 0.01591(16) Uani 1 1 d . . . . . C19 C 0.24363(10) 0.04569(8) 0.52932(6) 0.01576(16) Uani 1 1 d . . . . . C13 C 0.37493(10) -0.14739(8) 0.11201(6) 0.01594(16) Uani 1 1 d . . . . . C25 C 0.24792(11) 0.07379(8) 0.35830(6) 0.01732(17) Uani 1 1 d . . . . . C2 C 0.25227(10) -0.03260(7) -0.03285(5) 0.01470(16) Uani 1 1 d . . . . . C15 C 0.21118(11) 0.20362(8) -0.06526(6) 0.01656(17) Uani 1 1 d . . . . . H15A H 0.2480 0.1514 -0.1045 0.020 Uiso 1 1 calc R . . . . H15B H 0.2958 0.2338 -0.0445 0.020 Uiso 1 1 calc R . . . . C38 C 0.72195(10) -0.45700(7) 0.90246(6) 0.01533(16) Uani 1 1 d . . . . . C4 C 0.17347(10) -0.03238(8) -0.10260(6) 0.01605(17) Uani 1 1 d . . . . . H4 H 0.0869 0.0172 -0.1119 0.019 Uiso 1 1 calc R . . . . C3 C 0.37609(10) -0.10909(8) -0.02065(6) 0.01603(17) Uani 1 1 d . . . . . C18 C 0.29512(10) -0.03920(8) 0.47378(6) 0.01544(16) Uani 1 1 d . . . . . C35 C 0.33652(11) -0.47090(8) 0.81731(6) 0.01672(17) Uani 1 1 d . . . . . C9 C 0.18329(11) -0.11331(8) 0.20630(6) 0.01900(18) Uani 1 1 d . . . . . H9 H 0.1025 -0.0678 0.2265 0.023 Uiso 1 1 calc R . . . . C20 C 0.11607(11) 0.11732(8) 0.51388(6) 0.01703(17) Uani 1 1 d . . . . . C5 C 0.22357(11) -0.10567(8) -0.15796(6) 0.01747(17) Uani 1 1 d . . . . . C17 C 0.08188(11) 0.22294(8) 0.05826(6) 0.01657(17) Uani 1 1 d . . . . . H17A H 0.1643 0.2517 0.0827 0.020 Uiso 1 1 calc R . . . . H17B H 0.0305 0.1839 0.1000 0.020 Uiso 1 1 calc R . . . . C40 C 0.02172(10) -0.51484(8) 0.53653(6) 0.01670(17) Uani 1 1 d . . . . . H40 H -0.0346 -0.5598 0.5677 0.020 Uiso 1 1 calc R . . . . C36 C 0.45888(10) -0.46240(8) 0.87164(6) 0.01669(17) Uani 1 1 d . . . . . H36 H 0.4388 -0.4615 0.9263 0.020 Uiso 1 1 calc R . . . . C12 C 0.42190(11) -0.24752(8) 0.14998(6) 0.01932(18) Uani 1 1 d . . . . . H12 H 0.5029 -0.2932 0.1301 0.023 Uiso 1 1 calc R . . . . C21 C 0.32050(11) 0.05558(8) 0.59837(6) 0.01760(17) Uani 1 1 d . . . . . H21 H 0.4101 0.0103 0.6095 0.021 Uiso 1 1 calc R . . . . C37 C 0.59520(10) -0.45599(7) 0.84729(6) 0.01565(16) Uani 1 1 d . . . . . H37 H 0.6135 -0.4505 0.7924 0.019 Uiso 1 1 calc R . . . . C30 C 0.12615(11) 0.14523(8) 0.38043(6) 0.01764(17) Uani 1 1 d . . . . . C6 C 0.34845(12) -0.18042(8) -0.14578(6) 0.02061(19) Uani 1 1 d . . . . . H6 H 0.3813 -0.2291 -0.1848 0.025 Uiso 1 1 calc R . . . . C16 C -0.02292(11) 0.31615(8) 0.02102(6) 0.01757(17) Uani 1 1 d . . . . . H16A H -0.1096 0.2882 0.0006 0.021 Uiso 1 1 calc R . . . . H16B H -0.0566 0.3681 0.0610 0.021 Uiso 1 1 calc R . . . . C32 C 0.30155(11) -0.18523(8) 0.57977(6) 0.01899(18) Uani 1 1 d . . . . . H32A H 0.2215 -0.2266 0.5670 0.023 Uiso 1 1 calc R . . . . H32B H 0.2611 -0.1269 0.6136 0.023 Uiso 1 1 calc R . . . . C14 C 0.10551(11) 0.29415(8) -0.10420(6) 0.01735(17) Uani 1 1 d . . . . . H14A H 0.1553 0.3315 -0.1475 0.021 Uiso 1 1 calc R . . . . H14B H 0.0220 0.2642 -0.1265 0.021 Uiso 1 1 calc R . . . . C34 C 0.41532(11) -0.22227(8) 0.45451(6) 0.01837(18) Uani 1 1 d . . . . . H34A H 0.4554 -0.1886 0.4064 0.022 Uiso 1 1 calc R . . . . H34B H 0.3342 -0.2610 0.4391 0.022 Uiso 1 1 calc R . . . . C39 C 0.15485(10) -0.48130(8) 0.57264(6) 0.01656(17) Uani 1 1 d . . . . . C29 C 0.08352(12) 0.24358(8) 0.33903(7) 0.02191(19) Uani 1 1 d . . . . . H29 H 0.0029 0.2918 0.3565 0.026 Uiso 1 1 calc R . . . . C23 C 0.13430(12) 0.20026(9) 0.63616(6) 0.0227(2) Uani 1 1 d . . . . . H23 H 0.0965 0.2506 0.6731 0.027 Uiso 1 1 calc R . . . . C22 C 0.26478(12) 0.13202(9) 0.65034(6) 0.02004(18) Uani 1 1 d . . . . . C26 C 0.32070(12) 0.10138(9) 0.28902(6) 0.01993(18) Uani 1 1 d . . . . . H26 H 0.4004 0.0529 0.2708 0.024 Uiso 1 1 calc R . . . . C7 C 0.42442(11) -0.18299(8) -0.07587(6) 0.01998(18) Uani 1 1 d . . . . . H7 H 0.5086 -0.2347 -0.0658 0.024 Uiso 1 1 calc R . . . . C27 C 0.27732(13) 0.19908(9) 0.24663(6) 0.0228(2) Uani 1 1 d . . . . . H27 H 0.3284 0.2170 0.2000 0.027 Uiso 1 1 calc R . . . . C11 C 0.34984(12) -0.28060(8) 0.21728(6) 0.02141(19) Uani 1 1 d . . . . . H11 H 0.3815 -0.3488 0.2439 0.026 Uiso 1 1 calc R . . . . C10 C 0.23084(12) -0.21304(8) 0.24545(6) 0.02106(19) Uani 1 1 d . . . . . H10 H 0.1817 -0.2351 0.2917 0.025 Uiso 1 1 calc R . . . . C31 C 0.42193(12) -0.25968(8) 0.62289(6) 0.02111(19) Uani 1 1 d . . . . . H31A H 0.5015 -0.2183 0.6364 0.025 Uiso 1 1 calc R . . . . H31B H 0.3830 -0.2912 0.6721 0.025 Uiso 1 1 calc R . . . . C33 C 0.53424(11) -0.30198(8) 0.49525(7) 0.02079(19) Uani 1 1 d . . . . . H33A H 0.5661 -0.3615 0.4607 0.025 Uiso 1 1 calc R . . . . H33B H 0.6198 -0.2648 0.5051 0.025 Uiso 1 1 calc R . . . . C24 C 0.06070(12) 0.19288(9) 0.56658(6) 0.02157(19) Uani 1 1 d . . . . . H24 H -0.0276 0.2396 0.5550 0.026 Uiso 1 1 calc R . . . . C28 C 0.16011(13) 0.27084(9) 0.27159(7) 0.0244(2) Uani 1 1 d . . . . . H28 H 0.1324 0.3381 0.2428 0.029 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.02380(12) 0.03354(14) 0.01721(11) -0.00964(9) -0.00194(9) -0.00083(10) Cl2 0.02916(14) 0.03877(15) 0.01906(12) -0.01141(10) -0.00156(10) -0.00464(11) O1 0.0142(3) 0.0204(3) 0.0168(3) 0.0005(2) -0.0010(2) -0.0014(2) O6 0.0148(3) 0.0233(3) 0.0182(3) 0.0003(3) -0.0018(2) 0.0013(3) O2 0.0156(3) 0.0226(3) 0.0189(3) -0.0011(3) -0.0018(3) -0.0018(3) O5 0.0188(3) 0.0296(4) 0.0158(3) -0.0045(3) -0.0013(3) -0.0055(3) O7 0.0200(3) 0.0305(4) 0.0190(3) -0.0031(3) -0.0005(3) -0.0106(3) O9 0.0233(4) 0.0281(4) 0.0183(3) -0.0011(3) 0.0006(3) -0.0067(3) O10 0.0205(4) 0.0309(4) 0.0192(4) 0.0000(3) -0.0002(3) 0.0037(3) O4 0.0182(3) 0.0390(4) 0.0149(3) 0.0000(3) -0.0033(3) -0.0094(3) O8 0.0208(4) 0.0428(5) 0.0151(3) -0.0018(3) -0.0042(3) -0.0101(3) O3 0.0162(3) 0.0361(4) 0.0231(4) -0.0023(3) -0.0001(3) -0.0077(3) N1 0.0183(4) 0.0143(3) 0.0153(4) -0.0009(3) -0.0008(3) 0.0003(3) N3 0.0157(3) 0.0142(3) 0.0168(4) -0.0007(3) -0.0023(3) 0.0004(3) N2 0.0173(4) 0.0138(3) 0.0143(3) -0.0011(3) 0.0016(3) 0.0011(3) N4 0.0197(4) 0.0172(4) 0.0153(4) -0.0014(3) -0.0011(3) -0.0009(3) N5 0.0198(4) 0.0149(3) 0.0153(4) -0.0007(3) 0.0017(3) 0.0012(3) N6 0.0162(4) 0.0163(4) 0.0230(4) 0.0003(3) -0.0045(3) -0.0025(3) C1 0.0137(4) 0.0137(4) 0.0157(4) -0.0015(3) -0.0003(3) -0.0007(3) C8 0.0177(4) 0.0149(4) 0.0149(4) -0.0017(3) -0.0021(3) -0.0008(3) C19 0.0166(4) 0.0155(4) 0.0152(4) -0.0020(3) 0.0004(3) -0.0017(3) C13 0.0162(4) 0.0162(4) 0.0155(4) -0.0006(3) -0.0017(3) -0.0027(3) C25 0.0190(4) 0.0171(4) 0.0159(4) -0.0014(3) -0.0038(3) -0.0021(3) C2 0.0146(4) 0.0144(4) 0.0150(4) -0.0024(3) 0.0009(3) -0.0014(3) C15 0.0173(4) 0.0163(4) 0.0151(4) 0.0002(3) 0.0015(3) 0.0004(3) C38 0.0155(4) 0.0151(4) 0.0155(4) 0.0010(3) -0.0024(3) -0.0029(3) C4 0.0155(4) 0.0171(4) 0.0155(4) -0.0029(3) -0.0001(3) -0.0007(3) C3 0.0150(4) 0.0159(4) 0.0166(4) -0.0009(3) 0.0011(3) -0.0004(3) C18 0.0148(4) 0.0156(4) 0.0160(4) -0.0023(3) -0.0003(3) -0.0016(3) C35 0.0164(4) 0.0166(4) 0.0172(4) -0.0002(3) -0.0019(3) -0.0027(3) C9 0.0204(4) 0.0195(4) 0.0166(4) -0.0007(3) 0.0001(3) -0.0012(3) C20 0.0162(4) 0.0171(4) 0.0177(4) -0.0019(3) -0.0002(3) -0.0016(3) C5 0.0184(4) 0.0196(4) 0.0148(4) -0.0037(3) 0.0005(3) -0.0028(3) C17 0.0192(4) 0.0151(4) 0.0150(4) -0.0028(3) 0.0019(3) 0.0002(3) C40 0.0144(4) 0.0198(4) 0.0167(4) -0.0028(3) -0.0012(3) -0.0044(3) C36 0.0167(4) 0.0183(4) 0.0151(4) -0.0011(3) -0.0027(3) -0.0021(3) C12 0.0196(4) 0.0162(4) 0.0214(5) -0.0001(3) -0.0019(4) 0.0001(3) C21 0.0179(4) 0.0192(4) 0.0158(4) -0.0025(3) 0.0008(3) -0.0020(3) C37 0.0161(4) 0.0157(4) 0.0151(4) -0.0008(3) -0.0024(3) -0.0016(3) C30 0.0177(4) 0.0179(4) 0.0174(4) -0.0012(3) -0.0036(3) -0.0027(3) C6 0.0214(5) 0.0205(4) 0.0198(4) -0.0061(3) 0.0032(4) -0.0002(4) C16 0.0153(4) 0.0157(4) 0.0211(4) -0.0014(3) 0.0025(3) 0.0000(3) C32 0.0219(4) 0.0174(4) 0.0168(4) 0.0000(3) 0.0023(3) -0.0004(3) C14 0.0201(4) 0.0165(4) 0.0148(4) -0.0018(3) -0.0008(3) 0.0003(3) C34 0.0202(4) 0.0164(4) 0.0177(4) -0.0020(3) 0.0016(3) 0.0008(3) C39 0.0149(4) 0.0182(4) 0.0167(4) -0.0035(3) -0.0030(3) -0.0013(3) C29 0.0240(5) 0.0174(4) 0.0237(5) -0.0001(4) -0.0046(4) -0.0006(4) C23 0.0237(5) 0.0229(5) 0.0221(5) -0.0078(4) 0.0040(4) -0.0027(4) C22 0.0217(5) 0.0226(4) 0.0168(4) -0.0050(3) 0.0012(3) -0.0047(4) C26 0.0210(4) 0.0231(5) 0.0159(4) -0.0009(3) -0.0031(3) -0.0034(4) C7 0.0185(4) 0.0195(4) 0.0210(5) -0.0038(3) 0.0016(3) 0.0022(3) C27 0.0266(5) 0.0254(5) 0.0174(4) 0.0025(4) -0.0039(4) -0.0081(4) C11 0.0246(5) 0.0160(4) 0.0232(5) 0.0023(3) -0.0017(4) -0.0026(4) C10 0.0248(5) 0.0196(4) 0.0187(4) 0.0016(3) 0.0006(4) -0.0041(4) C31 0.0275(5) 0.0182(4) 0.0177(4) -0.0012(3) -0.0047(4) -0.0027(4) C33 0.0175(4) 0.0173(4) 0.0268(5) 0.0001(4) 0.0022(4) -0.0006(3) C24 0.0194(4) 0.0206(4) 0.0240(5) -0.0049(4) 0.0023(4) 0.0012(4) C28 0.0305(5) 0.0191(4) 0.0235(5) 0.0027(4) -0.0064(4) -0.0047(4) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C5 1.7327(10) . ? Cl2 C22 1.7342(11) . ? O1 C13 1.3980(12) . ? O1 C3 1.3849(12) . ? O6 C38 1.2678(12) . ? O2 C20 1.3845(12) . ? O2 C30 1.4007(12) . ? O5 C38 1.2501(12) . ? O7 C39 1.2589(12) . ? O9 H9A 0.8498 . ? O9 H9B 0.8498 . ? O10 H10A 0.8504 . ? O10 H10B 0.8491 . ? O4 H4A 0.8400 . ? O4 C35 1.3297(12) . ? O8 C39 1.2554(12) . ? O3 C35 1.2157(12) . ? N1 C1 1.2906(12) . ? N1 C8 1.4022(12) . ? N3 H3A 0.9100 . ? N3 H3B 0.9100 . ? N3 C16 1.4939(13) . ? N3 C14 1.4920(12) . ? N2 C1 1.3930(12) . ? N2 C15 1.4680(12) . ? N2 C17 1.4687(12) . ? N4 C25 1.3999(13) . ? N4 C18 1.2906(13) . ? N5 C18 1.3882(12) . ? N5 C32 1.4618(13) . ? N5 C34 1.4674(12) . ? N6 H6A 0.9100 . ? N6 H6B 0.9100 . ? N6 C31 1.4926(13) . ? N6 C33 1.4935(14) . ? C1 C2 1.4911(13) . ? C8 C13 1.4012(13) . ? C8 C9 1.3991(14) . ? C19 C18 1.4939(13) . ? C19 C20 1.3945(13) . ? C19 C21 1.4030(13) . ? C13 C12 1.3873(13) . ? C25 C30 1.4010(14) . ? C25 C26 1.4002(14) . ? C2 C4 1.4016(13) . ? C2 C3 1.3941(13) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C14 1.5124(13) . ? C38 C37 1.5074(13) . ? C4 H4 0.9500 . ? C4 C5 1.3899(13) . ? C3 C7 1.3895(13) . ? C35 C36 1.4878(13) . ? C9 H9 0.9500 . ? C9 C10 1.3927(14) . ? C20 C24 1.3890(14) . ? C5 C6 1.3892(14) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C17 C16 1.5184(13) . ? C40 C40 1.3284(19) 2_546 ? C40 H40 0.9500 . ? C40 C39 1.5007(13) . ? C36 H36 0.9500 . ? C36 C37 1.3311(13) . ? C12 H12 0.9500 . ? C12 C11 1.3888(15) . ? C21 H21 0.9500 . ? C21 C22 1.3889(14) . ? C37 H37 0.9500 . ? C30 C29 1.3871(14) . ? C6 H6 0.9500 . ? C6 C7 1.3870(15) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C32 C31 1.5127(14) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C34 C33 1.5194(14) . ? C29 H29 0.9500 . ? C29 C28 1.3919(16) . ? C23 H23 0.9500 . ? C23 C22 1.3909(15) . ? C23 C24 1.3890(15) . ? C26 H26 0.9500 . ? C26 C27 1.3895(15) . ? C7 H7 0.9500 . ? C27 H27 0.9500 . ? C27 C28 1.3893(17) . ? C11 H11 0.9500 . ? C11 C10 1.3920(15) . ? C10 H10 0.9500 . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C24 H24 0.9500 . ? C28 H28 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 O1 C13 110.34(7) . . ? C20 O2 C30 110.26(8) . . ? H9A O9 H9B 109.5 . . ? H10A O10 H10B 109.5 . . ? C35 O4 H4A 109.5 . . ? C1 N1 C8 122.94(8) . . ? H3A N3 H3B 108.2 . . ? C16 N3 H3A 109.7 . . ? C16 N3 H3B 109.7 . . ? C14 N3 H3A 109.7 . . ? C14 N3 H3B 109.7 . . ? C14 N3 C16 109.99(7) . . ? C1 N2 C15 118.60(8) . . ? C1 N2 C17 116.14(8) . . ? C15 N2 C17 111.06(7) . . ? C18 N4 C25 122.33(9) . . ? C18 N5 C32 120.86(8) . . ? C18 N5 C34 117.52(8) . . ? C32 N5 C34 111.12(8) . . ? H6A N6 H6B 108.0 . . ? C31 N6 H6A 109.4 . . ? C31 N6 H6B 109.4 . . ? C31 N6 C33 110.95(8) . . ? C33 N6 H6A 109.4 . . ? C33 N6 H6B 109.4 . . ? N1 C1 N2 117.94(8) . . ? N1 C1 C2 126.08(8) . . ? N2 C1 C2 115.67(8) . . ? C13 C8 N1 124.20(9) . . ? C9 C8 N1 118.29(9) . . ? C9 C8 C13 117.31(9) . . ? C20 C19 C18 120.46(9) . . ? C20 C19 C21 118.03(9) . . ? C21 C19 C18 121.50(9) . . ? O1 C13 C8 119.09(8) . . ? C12 C13 O1 118.77(9) . . ? C12 C13 C8 122.10(9) . . ? N4 C25 C30 124.11(9) . . ? N4 C25 C26 118.18(9) . . ? C26 C25 C30 117.57(9) . . ? C4 C2 C1 120.92(8) . . ? C3 C2 C1 120.66(8) . . ? C3 C2 C4 118.40(8) . . ? N2 C15 H15A 109.6 . . ? N2 C15 H15B 109.6 . . ? N2 C15 C14 110.41(8) . . ? H15A C15 H15B 108.1 . . ? C14 C15 H15A 109.6 . . ? C14 C15 H15B 109.6 . . ? O6 C38 C37 115.27(8) . . ? O5 C38 O6 125.17(9) . . ? O5 C38 C37 119.55(8) . . ? C2 C4 H4 120.4 . . ? C5 C4 C2 119.16(9) . . ? C5 C4 H4 120.4 . . ? O1 C3 C2 119.73(8) . . ? O1 C3 C7 118.20(8) . . ? C7 C3 C2 122.06(9) . . ? N4 C18 N5 117.60(9) . . ? N4 C18 C19 126.05(9) . . ? N5 C18 C19 116.12(8) . . ? O4 C35 C36 113.84(8) . . ? O3 C35 O4 123.46(9) . . ? O3 C35 C36 122.70(9) . . ? C8 C9 H9 119.5 . . ? C10 C9 C8 120.97(9) . . ? C10 C9 H9 119.5 . . ? O2 C20 C19 119.99(8) . . ? O2 C20 C24 118.20(9) . . ? C24 C20 C19 121.81(9) . . ? C4 C5 Cl1 119.09(8) . . ? C6 C5 Cl1 118.92(7) . . ? C6 C5 C4 121.97(9) . . ? N2 C17 H17A 109.5 . . ? N2 C17 H17B 109.5 . . ? N2 C17 C16 110.55(8) . . ? H17A C17 H17B 108.1 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C40 C40 H40 118.2 2_546 . ? C40 C40 C39 123.68(11) 2_546 . ? C39 C40 H40 118.2 . . ? C35 C36 H36 118.4 . . ? C37 C36 C35 123.11(9) . . ? C37 C36 H36 118.4 . . ? C13 C12 H12 120.2 . . ? C13 C12 C11 119.59(9) . . ? C11 C12 H12 120.2 . . ? C19 C21 H21 120.2 . . ? C22 C21 C19 119.60(9) . . ? C22 C21 H21 120.2 . . ? C38 C37 H37 118.4 . . ? C36 C37 C38 123.27(9) . . ? C36 C37 H37 118.4 . . ? O2 C30 C25 119.00(9) . . ? C29 C30 O2 118.89(9) . . ? C29 C30 C25 122.05(10) . . ? C5 C6 H6 120.5 . . ? C7 C6 C5 119.06(9) . . ? C7 C6 H6 120.5 . . ? N3 C16 C17 109.94(8) . . ? N3 C16 H16A 109.7 . . ? N3 C16 H16B 109.7 . . ? C17 C16 H16A 109.7 . . ? C17 C16 H16B 109.7 . . ? H16A C16 H16B 108.2 . . ? N5 C32 H32A 109.7 . . ? N5 C32 H32B 109.7 . . ? N5 C32 C31 109.67(8) . . ? H32A C32 H32B 108.2 . . ? C31 C32 H32A 109.7 . . ? C31 C32 H32B 109.7 . . ? N3 C14 C15 108.90(8) . . ? N3 C14 H14A 109.9 . . ? N3 C14 H14B 109.9 . . ? C15 C14 H14A 109.9 . . ? C15 C14 H14B 109.9 . . ? H14A C14 H14B 108.3 . . ? N5 C34 H34A 109.7 . . ? N5 C34 H34B 109.7 . . ? N5 C34 C33 109.81(8) . . ? H34A C34 H34B 108.2 . . ? C33 C34 H34A 109.7 . . ? C33 C34 H34B 109.7 . . ? O7 C39 C40 118.53(9) . . ? O8 C39 O7 125.22(9) . . ? O8 C39 C40 116.24(9) . . ? C30 C29 H29 120.3 . . ? C30 C29 C28 119.32(10) . . ? C28 C29 H29 120.3 . . ? C22 C23 H23 120.8 . . ? C24 C23 H23 120.8 . . ? C24 C23 C22 118.31(9) . . ? C21 C22 Cl2 118.84(8) . . ? C21 C22 C23 122.06(10) . . ? C23 C22 Cl2 119.09(8) . . ? C25 C26 H26 119.7 . . ? C27 C26 C25 120.57(10) . . ? C27 C26 H26 119.7 . . ? C3 C7 H7 120.3 . . ? C6 C7 C3 119.31(9) . . ? C6 C7 H7 120.3 . . ? C26 C27 H27 119.6 . . ? C28 C27 C26 120.78(10) . . ? C28 C27 H27 119.6 . . ? C12 C11 H11 120.2 . . ? C12 C11 C10 119.51(9) . . ? C10 C11 H11 120.2 . . ? C9 C10 H10 119.8 . . ? C11 C10 C9 120.46(10) . . ? C11 C10 H10 119.8 . . ? N6 C31 C32 108.79(8) . . ? N6 C31 H31A 109.9 . . ? N6 C31 H31B 109.9 . . ? C32 C31 H31A 109.9 . . ? C32 C31 H31B 109.9 . . ? H31A C31 H31B 108.3 . . ? N6 C33 C34 110.78(8) . . ? N6 C33 H33A 109.5 . . ? N6 C33 H33B 109.5 . . ? C34 C33 H33A 109.5 . . ? C34 C33 H33B 109.5 . . ? H33A C33 H33B 108.1 . . ? C20 C24 C23 120.08(10) . . ? C20 C24 H24 120.0 . . ? C23 C24 H24 120.0 . . ? C29 C28 H28 120.2 . . ? C27 C28 C29 119.57(10) . . ? C27 C28 H28 120.2 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 C5 C6 C7 -177.51(8) . . . . ? O1 C13 C12 C11 175.10(9) . . . . ? O1 C3 C7 C6 -178.67(9) . . . . ? O6 C38 C37 C36 155.06(9) . . . . ? O2 C20 C24 C23 -178.46(9) . . . . ? O2 C30 C29 C28 -174.72(9) . . . . ? O5 C38 C37 C36 -25.09(14) . . . . ? O4 C35 C36 C37 -1.92(14) . . . . ? O3 C35 C36 C37 177.43(10) . . . . ? N1 C1 C2 C4 138.71(10) . . . . ? N1 C1 C2 C3 -39.98(14) . . . . ? N1 C8 C13 O1 0.54(14) . . . . ? N1 C8 C13 C12 178.04(9) . . . . ? N1 C8 C9 C10 -177.44(9) . . . . ? N2 C1 C2 C4 -34.67(13) . . . . ? N2 C1 C2 C3 146.64(9) . . . . ? N2 C15 C14 N3 59.55(10) . . . . ? N2 C17 C16 N3 -56.61(10) . . . . ? N4 C25 C30 O2 -2.71(15) . . . . ? N4 C25 C30 C29 -179.98(9) . . . . ? N4 C25 C26 C27 179.26(9) . . . . ? N5 C32 C31 N6 -60.17(11) . . . . ? N5 C34 C33 N6 55.08(11) . . . . ? C1 N1 C8 C13 39.46(15) . . . . ? C1 N1 C8 C9 -145.96(10) . . . . ? C1 N2 C15 C14 162.67(8) . . . . ? C1 N2 C17 C16 -163.32(8) . . . . ? C1 C2 C4 C5 179.32(8) . . . . ? C1 C2 C3 O1 -0.80(13) . . . . ? C1 C2 C3 C7 179.92(9) . . . . ? C8 N1 C1 N2 173.69(9) . . . . ? C8 N1 C1 C2 0.44(15) . . . . ? C8 C13 C12 C11 -2.41(15) . . . . ? C8 C9 C10 C11 0.60(16) . . . . ? C19 C20 C24 C23 1.41(16) . . . . ? C19 C21 C22 Cl2 -179.54(8) . . . . ? C19 C21 C22 C23 -0.25(16) . . . . ? C13 O1 C3 C2 69.01(11) . . . . ? C13 O1 C3 C7 -111.69(10) . . . . ? C13 C8 C9 C10 -2.48(15) . . . . ? C13 C12 C11 C10 0.38(16) . . . . ? C25 N4 C18 N5 -172.54(9) . . . . ? C25 N4 C18 C19 1.58(15) . . . . ? C25 C30 C29 C28 2.56(16) . . . . ? C25 C26 C27 C28 -0.66(16) . . . . ? C2 C4 C5 Cl1 179.33(7) . . . . ? C2 C4 C5 C6 0.98(15) . . . . ? C2 C3 C7 C6 0.61(15) . . . . ? C15 N2 C1 N1 138.77(9) . . . . ? C15 N2 C1 C2 -47.28(12) . . . . ? C15 N2 C17 C16 57.19(10) . . . . ? C4 C2 C3 O1 -179.52(8) . . . . ? C4 C2 C3 C7 1.20(14) . . . . ? C4 C5 C6 C7 0.84(16) . . . . ? C3 O1 C13 C8 -70.60(11) . . . . ? C3 O1 C13 C12 111.82(10) . . . . ? C3 C2 C4 C5 -1.96(14) . . . . ? C18 N4 C25 C30 -40.31(15) . . . . ? C18 N4 C25 C26 144.09(10) . . . . ? C18 N5 C32 C31 -154.34(9) . . . . ? C18 N5 C34 C33 156.12(9) . . . . ? C18 C19 C20 O2 -4.01(14) . . . . ? C18 C19 C20 C24 176.12(9) . . . . ? C18 C19 C21 C22 -176.73(9) . . . . ? C35 C36 C37 C38 -174.58(9) . . . . ? C9 C8 C13 O1 -174.08(8) . . . . ? C9 C8 C13 C12 3.41(14) . . . . ? C20 O2 C30 C25 72.23(11) . . . . ? C20 O2 C30 C29 -110.41(10) . . . . ? C20 C19 C18 N4 41.75(14) . . . . ? C20 C19 C18 N5 -144.05(9) . . . . ? C20 C19 C21 C22 2.84(14) . . . . ? C5 C6 C7 C3 -1.62(16) . . . . ? C17 N2 C1 N1 2.44(13) . . . . ? C17 N2 C1 C2 176.39(8) . . . . ? C17 N2 C15 C14 -58.95(10) . . . . ? C40 C40 C39 O7 -15.66(18) 2_546 . . . ? C40 C40 C39 O8 163.74(13) 2_546 . . . ? C12 C11 C10 C9 0.50(16) . . . . ? C21 C19 C18 N4 -138.69(11) . . . . ? C21 C19 C18 N5 35.51(13) . . . . ? C21 C19 C20 O2 176.41(9) . . . . ? C21 C19 C20 C24 -3.46(15) . . . . ? C30 O2 C20 C19 -65.68(11) . . . . ? C30 O2 C20 C24 114.19(10) . . . . ? C30 C25 C26 C27 3.37(15) . . . . ? C30 C29 C28 C27 0.31(16) . . . . ? C16 N3 C14 C15 -59.35(10) . . . . ? C32 N5 C18 N4 -145.39(9) . . . . ? C32 N5 C18 C19 39.89(13) . . . . ? C32 N5 C34 C33 -58.68(11) . . . . ? C14 N3 C16 C17 58.15(10) . . . . ? C34 N5 C18 N4 -3.72(13) . . . . ? C34 N5 C18 C19 -178.44(8) . . . . ? C34 N5 C32 C31 61.79(11) . . . . ? C22 C23 C24 C20 1.25(16) . . . . ? C26 C25 C30 O2 172.91(9) . . . . ? C26 C25 C30 C29 -4.36(15) . . . . ? C26 C27 C28 C29 -1.24(17) . . . . ? C31 N6 C33 C34 -55.56(11) . . . . ? C33 N6 C31 C32 57.53(11) . . . . ? C24 C23 C22 Cl2 177.45(8) . . . . ? C24 C23 C22 C21 -1.83(16) . . . . ? _shelx_res_file ; amx-f05-100k-me.res created by SHELXL-2014/7 TITL amx-f05-100k-me_a.res in P-1 REM Old TITL AMX-F05-100K-Me in P-1 REM SHELXT solution in P-1 REM R1 0.110, Rweak 0.002, Alpha 0.021, Orientation as input REM Formula found by SHELXT: C40 N6 O10 Cl2 CELL 0.71073 9.2238 12.4815 17.0725 86.285 89.375 82.224 ZERR 2 0.0002 0.0002 0.0003 0.001 0.002 0.002 LATT 1 SFAC C H Cl N O UNIT 80 84 4 12 20 L.S. 10 PLAN 20 TEMP -173.1(2) BOND $H list 4 conf htab fmap 2 acta 50 OMIT -3 -5 20 OMIT 1 0 1 OMIT -2 2 8 OMIT -2 -1 8 OMIT -4 3 4 OMIT 3 -4 3 OMIT -4 -5 12 OMIT 5 0 1 OMIT 4 -4 2 OMIT -2 3 8 OMIT -2 9 10 REM REM REM WGHT 0.061100 0.528100 FVAR 0.50600 CL1 3 0.124968 -0.106237 -0.243703 11.00000 0.02380 0.03354 = 0.01721 -0.00964 -0.00194 -0.00083 CL2 3 0.362229 0.143554 0.734990 11.00000 0.02916 0.03877 = 0.01906 -0.01141 -0.00156 -0.00464 O1 5 0.455585 -0.111836 0.047971 11.00000 0.01415 0.02038 = 0.01682 0.00051 -0.00104 -0.00143 O6 5 0.846756 -0.489972 0.874525 11.00000 0.01478 0.02327 = 0.01821 0.00029 -0.00180 0.00126 O2 5 0.041164 0.114467 0.444371 11.00000 0.01561 0.02259 = 0.01889 -0.00108 -0.00178 -0.00178 O5 5 0.698598 -0.426268 0.970251 11.00000 0.01881 0.02957 = 0.01583 -0.00452 -0.00133 -0.00545 O7 5 0.247473 -0.443033 0.528130 11.00000 0.02003 0.03053 = 0.01897 -0.00308 -0.00050 -0.01058 AFIX 6 O9 5 0.082285 -0.439528 0.275525 11.00000 0.02333 0.02815 = 0.01834 -0.00113 0.00063 -0.00666 H9A 2 0.006655 -0.465646 0.292547 11.00000 -1.50000 H9B 2 0.102704 -0.460104 0.229736 11.00000 -1.50000 AFIX 6 O10 5 0.318034 -0.485900 0.375567 11.00000 0.02055 0.03089 = 0.01916 -0.00004 -0.00023 0.00373 H10A 2 0.247073 -0.477400 0.343377 11.00000 -1.50000 H10B 2 0.286665 -0.469594 0.420798 11.00000 -1.50000 AFIX 0 O4 5 0.374821 -0.468233 0.741967 11.00000 0.01823 0.03903 = 0.01495 -0.00005 -0.00331 -0.00942 AFIX 147 H4A 2 0.303129 -0.477716 0.714544 11.00000 -1.50000 AFIX 0 O8 5 0.163459 -0.493280 0.646093 11.00000 0.02082 0.04277 = 0.01508 -0.00183 -0.00419 -0.01010 O3 5 0.213397 -0.480434 0.840234 11.00000 0.01622 0.03606 = 0.02310 -0.00233 -0.00009 -0.00770 N1 4 0.203640 0.023874 0.102689 11.00000 0.01833 0.01430 = 0.01534 -0.00092 -0.00080 0.00035 N3 4 0.051718 0.372444 -0.044519 11.00000 0.01566 0.01416 = 0.01681 -0.00070 -0.00233 0.00039 AFIX 23 H3A 2 -0.011997 0.427346 -0.067332 11.00000 -1.20000 H3B 2 0.128374 0.401434 -0.025309 11.00000 -1.20000 AFIX 0 N2 4 0.138627 0.147601 -0.000907 11.00000 0.01726 0.01377 = 0.01432 -0.00112 0.00161 0.00107 N4 4 0.295088 -0.026210 0.398164 11.00000 0.01971 0.01717 = 0.01534 -0.00138 -0.00112 -0.00085 N5 4 0.360028 -0.138015 0.507522 11.00000 0.01979 0.01494 = 0.01531 -0.00071 0.00168 0.00115 N6 4 0.479765 -0.347793 0.571252 11.00000 0.01623 0.01627 = 0.02304 0.00031 -0.00447 -0.00248 AFIX 23 H6A 2 0.407623 -0.388240 0.561710 11.00000 -1.20000 H6B 2 0.554051 -0.391964 0.596164 11.00000 -1.20000 AFIX 0 C1 1 0.203329 0.045443 0.027722 11.00000 0.01374 0.01368 = 0.01575 -0.00149 -0.00030 -0.00072 C8 1 0.252744 -0.079231 0.137654 11.00000 0.01775 0.01490 = 0.01485 -0.00169 -0.00209 -0.00084 C19 1 0.243627 0.045690 0.529321 11.00000 0.01661 0.01549 = 0.01517 -0.00204 0.00036 -0.00169 C13 1 0.374926 -0.147388 0.112011 11.00000 0.01621 0.01623 = 0.01549 -0.00056 -0.00168 -0.00267 C25 1 0.247921 0.073791 0.358298 11.00000 0.01904 0.01707 = 0.01588 -0.00143 -0.00382 -0.00213 C2 1 0.252270 -0.032601 -0.032849 11.00000 0.01464 0.01445 = 0.01503 -0.00239 0.00088 -0.00137 C15 1 0.211184 0.203621 -0.065262 11.00000 0.01731 0.01632 = 0.01512 0.00023 0.00154 0.00038 AFIX 23 H15A 2 0.248014 0.151371 -0.104456 11.00000 -1.20000 H15B 2 0.295850 0.233778 -0.044497 11.00000 -1.20000 AFIX 0 C38 1 0.721947 -0.456997 0.902456 11.00000 0.01547 0.01507 = 0.01548 0.00098 -0.00238 -0.00292 C4 1 0.173475 -0.032378 -0.102604 11.00000 0.01547 0.01705 = 0.01547 -0.00285 -0.00006 -0.00070 AFIX 43 H4 2 0.086918 0.017240 -0.111928 11.00000 -1.20000 AFIX 0 C3 1 0.376091 -0.109089 -0.020646 11.00000 0.01505 0.01593 = 0.01661 -0.00094 0.00111 -0.00044 C18 1 0.295124 -0.039203 0.473780 11.00000 0.01476 0.01562 = 0.01601 -0.00231 -0.00027 -0.00161 C35 1 0.336518 -0.470905 0.817311 11.00000 0.01640 0.01664 = 0.01717 -0.00016 -0.00194 -0.00271 C9 1 0.183287 -0.113310 0.206297 11.00000 0.02038 0.01954 = 0.01661 -0.00074 0.00009 -0.00122 AFIX 43 H9 2 0.102506 -0.067755 0.226490 11.00000 -1.20000 AFIX 0 C20 1 0.116073 0.117325 0.513879 11.00000 0.01618 0.01709 = 0.01774 -0.00190 -0.00016 -0.00157 C5 1 0.223575 -0.105670 -0.157963 11.00000 0.01844 0.01958 = 0.01478 -0.00370 0.00049 -0.00280 C17 1 0.081883 0.222937 0.058265 11.00000 0.01918 0.01508 = 0.01497 -0.00277 0.00194 0.00019 AFIX 23 H17A 2 0.164301 0.251670 0.082664 11.00000 -1.20000 H17B 2 0.030467 0.183906 0.100000 11.00000 -1.20000 AFIX 0 C40 1 0.021722 -0.514843 0.536533 11.00000 0.01441 0.01979 = 0.01671 -0.00283 -0.00118 -0.00437 AFIX 43 H40 2 -0.034640 -0.559830 0.567674 11.00000 -1.20000 AFIX 0 C36 1 0.458880 -0.462395 0.871641 11.00000 0.01667 0.01826 = 0.01514 -0.00109 -0.00270 -0.00215 AFIX 43 H36 2 0.438766 -0.461494 0.926304 11.00000 -1.20000 AFIX 0 C12 1 0.421904 -0.247518 0.149980 11.00000 0.01957 0.01620 = 0.02142 -0.00014 -0.00190 0.00007 AFIX 43 H12 2 0.502870 -0.293177 0.130066 11.00000 -1.20000 AFIX 0 C21 1 0.320502 0.055576 0.598372 11.00000 0.01786 0.01919 = 0.01578 -0.00247 0.00080 -0.00204 AFIX 43 H21 2 0.410124 0.010252 0.609510 11.00000 -1.20000 AFIX 0 C37 1 0.595205 -0.455985 0.847289 11.00000 0.01608 0.01568 = 0.01509 -0.00083 -0.00245 -0.00160 AFIX 43 H37 2 0.613536 -0.450500 0.792409 11.00000 -1.20000 AFIX 0 C30 1 0.126147 0.145230 0.380431 11.00000 0.01771 0.01791 = 0.01744 -0.00120 -0.00360 -0.00266 C6 1 0.348447 -0.180422 -0.145775 11.00000 0.02139 0.02052 = 0.01976 -0.00609 0.00322 -0.00025 AFIX 43 H6 2 0.381341 -0.229095 -0.184772 11.00000 -1.20000 AFIX 0 C16 1 -0.022919 0.316150 0.021022 11.00000 0.01530 0.01570 = 0.02109 -0.00145 0.00246 0.00001 AFIX 23 H16A 2 -0.109647 0.288215 0.000622 11.00000 -1.20000 H16B 2 -0.056559 0.368069 0.060990 11.00000 -1.20000 AFIX 0 C32 1 0.301547 -0.185233 0.579768 11.00000 0.02194 0.01740 = 0.01682 0.00001 0.00232 -0.00043 AFIX 23 H32A 2 0.221480 -0.226561 0.567010 11.00000 -1.20000 H32B 2 0.261099 -0.126857 0.613606 11.00000 -1.20000 AFIX 0 C14 1 0.105509 0.294145 -0.104196 11.00000 0.02014 0.01649 = 0.01479 -0.00179 -0.00084 0.00026 AFIX 23 H14A 2 0.155258 0.331488 -0.147496 11.00000 -1.20000 H14B 2 0.022035 0.264157 -0.126454 11.00000 -1.20000 AFIX 0 C34 1 0.415316 -0.222268 0.454512 11.00000 0.02022 0.01642 = 0.01766 -0.00204 0.00164 0.00076 AFIX 23 H34A 2 0.455393 -0.188569 0.406356 11.00000 -1.20000 H34B 2 0.334247 -0.260970 0.439113 11.00000 -1.20000 AFIX 0 C39 1 0.154845 -0.481296 0.572639 11.00000 0.01491 0.01819 = 0.01671 -0.00352 -0.00295 -0.00134 C29 1 0.083520 0.243576 0.339032 11.00000 0.02396 0.01741 = 0.02367 -0.00012 -0.00461 -0.00056 AFIX 43 H29 2 0.002878 0.291828 0.356532 11.00000 -1.20000 AFIX 0 C23 1 0.134303 0.200257 0.636162 11.00000 0.02374 0.02293 = 0.02213 -0.00776 0.00398 -0.00269 AFIX 43 H23 2 0.096487 0.250627 0.673129 11.00000 -1.20000 AFIX 0 C22 1 0.264782 0.132025 0.650343 11.00000 0.02173 0.02257 = 0.01678 -0.00499 0.00125 -0.00475 C26 1 0.320698 0.101376 0.289017 11.00000 0.02096 0.02306 = 0.01591 -0.00092 -0.00315 -0.00340 AFIX 43 H26 2 0.400426 0.052876 0.270837 11.00000 -1.20000 AFIX 0 C7 1 0.424423 -0.182993 -0.075870 11.00000 0.01848 0.01948 = 0.02095 -0.00378 0.00156 0.00222 AFIX 43 H7 2 0.508627 -0.234741 -0.065849 11.00000 -1.20000 AFIX 0 C27 1 0.277316 0.199075 0.246628 11.00000 0.02658 0.02535 = 0.01740 0.00255 -0.00393 -0.00806 AFIX 43 H27 2 0.328411 0.217009 0.200026 11.00000 -1.20000 AFIX 0 C11 1 0.349835 -0.280597 0.217285 11.00000 0.02455 0.01601 = 0.02321 0.00234 -0.00173 -0.00263 AFIX 43 H11 2 0.381517 -0.348825 0.243901 11.00000 -1.20000 AFIX 0 C10 1 0.230840 -0.213041 0.245454 11.00000 0.02484 0.01957 = 0.01870 0.00157 0.00055 -0.00407 AFIX 43 H10 2 0.181725 -0.235116 0.291707 11.00000 -1.20000 AFIX 0 C31 1 0.421925 -0.259683 0.622887 11.00000 0.02747 0.01817 = 0.01767 -0.00123 -0.00469 -0.00266 AFIX 23 H31A 2 0.501490 -0.218343 0.636449 11.00000 -1.20000 H31B 2 0.383009 -0.291250 0.672147 11.00000 -1.20000 AFIX 0 C33 1 0.534244 -0.301982 0.495248 11.00000 0.01747 0.01735 = 0.02681 0.00006 0.00217 -0.00056 AFIX 23 H33A 2 0.566124 -0.361522 0.460718 11.00000 -1.20000 H33B 2 0.619841 -0.264750 0.505126 11.00000 -1.20000 AFIX 0 C24 1 0.060697 0.192880 0.566578 11.00000 0.01942 0.02064 = 0.02395 -0.00492 0.00226 0.00125 AFIX 43 H24 2 -0.027633 0.239571 0.555016 11.00000 -1.20000 AFIX 0 C28 1 0.160109 0.270842 0.271586 11.00000 0.03048 0.01915 = 0.02349 0.00267 -0.00639 -0.00473 AFIX 43 H28 2 0.132415 0.338091 0.242805 11.00000 -1.20000 AFIX 0 HKLF 4 REM amx-f05-100k-me_a.res in P-1 REM R1 = 0.0418 for 11488 Fo > 4sig(Fo) and 0.0519 for all 13758 data REM 530 parameters refined using 0 restraints END WGHT 0.0611 0.5281 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y-1, -z+1 HTAB O9 O8_$1 EQIV $2 -x+1, -y-1, -z+1 HTAB O9 O6_$2 HTAB O10 O9 HTAB O10 O7 HTAB O4 O8 EQIV $3 x-1, y+1, z-1 HTAB N3 O6_$3 EQIV $4 -x+1, -y, -z+1 HTAB N3 O5_$4 HTAB N6 O7 HTAB N6 O10_$2 EQIV $5 x, y, z-1 HTAB C15 Cl2_$5 EQIV $6 -x+1, -y, -z HTAB C15 O1_$6 EQIV $7 -x, -y, -z HTAB C9 Cl1_$7 EQIV $8 -x+1, -y-1, -z+2 HTAB C36 O5_$8 EQIV $9 -x, -y, -z+1 HTAB C16 O3_$9 HTAB C32 O2_$9 EQIV $10 x, y, z+1 HTAB C32 Cl1_$10 EQIV $11 x, y+1, z-1 HTAB C14 O3_$11 HTAB C31 O4 REM Highest difference peak 0.605, deepest hole -0.298, 1-sigma level 0.063 Q1 1 0.2679 0.0071 0.5029 11.00000 0.05 0.47 Q2 1 0.0857 0.1565 0.5369 11.00000 0.05 0.45 Q3 1 0.2026 -0.0688 -0.1317 11.00000 0.05 0.45 Q4 1 0.1545 0.2468 -0.0812 11.00000 0.05 0.42 Q5 1 0.3197 -0.1131 0.1261 11.00000 0.05 0.41 Q6 1 0.2139 -0.0917 0.1701 11.00000 0.05 0.41 Q7 1 0.1065 0.1956 0.3616 11.00000 0.05 0.41 Q8 1 0.2962 -0.2445 0.2284 11.00000 0.05 0.40 Q9 1 0.4047 -0.1950 0.1368 11.00000 0.05 0.40 Q10 1 0.2983 0.0951 0.6246 11.00000 0.05 0.40 Q11 1 0.2241 0.2330 0.2588 11.00000 0.05 0.39 Q12 1 0.0931 -0.4981 0.5569 11.00000 0.05 0.39 Q13 1 0.3976 -0.1441 -0.0491 11.00000 0.05 0.39 Q14 1 0.1788 0.0712 0.5211 11.00000 0.05 0.38 Q15 1 0.2936 0.0784 0.3241 11.00000 0.05 0.38 Q16 1 0.3030 -0.0789 -0.0229 11.00000 0.05 0.38 Q17 1 0.2243 0.0043 -0.0055 11.00000 0.05 0.37 Q18 1 0.2177 -0.1578 0.2287 11.00000 0.05 0.37 Q19 1 0.1850 0.1047 0.3689 11.00000 0.05 0.36 Q20 1 0.1748 0.0976 0.0127 11.00000 0.05 0.35 ; _shelx_res_checksum 86384 _shelx_hkl_file ; 0 0 3 114.35 2.37 0 0 3 119.42 2.25 0 0 3 119.42 2.66 0 0 -3 114.14 2.24 0 0 -3 118.49 2.68 0 0 -3 122.62 2.41 0 0 -4 188.88 4.00 0 0 -4 183.51 3.60 0 0 4 183.18 3.40 0 0 4 184.59 3.98 0 0 5 28.92 1.01 0 0 -5 29.31 1.37 0 0 -5 29.41 1.14 0 0 5 27.56 1.36 0 0 -6 670.30 11.85 0 0 6 646.16 11.82 0 0 -6 669.38 11.17 0 0 6 649.57 10.81 0 0 -7 149.31 3.55 0 0 7 144.68 4.07 0 0 -7 140.96 4.01 0 0 7 148.27 3.26 0 0 8 2551.53 39.02 0 0 -8 2538.40 40.53 0 0 -8 2545.13 39.52 0 0 8 2501.47 40.48 0 0 9 131.35 3.25 0 0 -9 129.81 4.23 0 0 9 132.41 4.23 0 0 -9 133.30 3.61 0 0 -10 1303.47 22.79 0 0 10 1289.47 20.86 0 0 10 1283.60 22.69 0 0 -10 1283.49 21.50 0 0 -11 76.27 3.41 0 0 11 76.45 3.42 0 0 -11 80.33 2.90 0 0 11 82.59 2.55 0 0 -12 0.58 0.37 0 0 12 -0.06 0.28 0 0 -12 0.35 0.35 0 0 12 0.30 0.18 0 0 -13 206.08 5.48 0 0 13 194.13 4.74 0 0 13 190.27 6.30 0 0 -13 207.68 6.50 0 0 14 25.18 2.20 0 0 -14 26.84 2.23 0 0 14 26.56 1.47 0 0 -14 29.78 1.90 0 0 15 11.50 1.52 0 0 15 13.04 1.05 0 0 -15 14.70 1.36 0 0 -15 13.99 1.66 0 0 16 2.10 0.81 0 0 -16 1.41 0.59 0 0 -16 2.52 0.60 0 0 -17 17.73 1.70 0 0 17 19.84 2.17 0 0 -17 20.02 2.17 0 0 18 22.76 2.49 0 0 -18 22.56 1.92 0 0 -18 27.47 2.64 0 0 19 59.60 4.11 0 0 -19 53.84 3.90 0 0 20 19.07 2.44 0 0 -20 16.25 2.20 0 0 21 1.32 0.64 0 0 -21 -1.33 1.04 0 0 22 43.42 3.90 0 0 -22 46.03 3.95 0 0 22 44.07 3.99 0 0 -23 7.32 1.53 0 0 23 5.83 1.62 0 0 23 5.91 1.57 0 0 24 15.47 2.56 0 0 -24 17.45 2.67 0 0 24 12.98 2.42 0 0 -25 0.14 0.81 0 0 25 0.35 0.96 0 0 25 0.65 1.24 0 -1 25 20.61 3.00 0 -1 24 30.13 3.44 0 -1 24 35.75 3.80 0 -1 23 100.70 6.41 0 -1 23 92.66 5.93 0 1 -23 96.74 6.06 0 1 -22 6.66 1.57 0 -1 22 10.43 1.92 0 -1 22 7.38 1.75 0 1 -21 1.32 1.02 0 -1 21 1.37 0.88 0 -1 21 0.71 0.69 0 -1 20 5.05 1.19 0 1 -20 2.21 0.89 0 -1 20 5.35 1.32 0 -1 19 1.13 0.78 0 -1 19 1.42 0.97 0 1 -19 1.21 0.67 0 1 -19 0.30 0.51 0 -1 18 26.93 2.59 0 1 -18 23.02 2.05 0 -1 18 29.30 2.77 0 1 -18 21.57 2.40 0 1 -17 93.35 4.06 0 1 -17 99.97 5.01 0 -1 17 87.38 4.65 0 -1 16 -0.62 0.53 0 1 -16 0.52 0.56 0 1 -16 0.23 0.33 0 -1 15 4.87 1.03 0 1 -15 4.34 0.94 0 1 -15 5.04 0.93 0 1 -14 51.03 3.13 0 -1 14 51.57 3.09 0 1 -14 49.83 2.64 0 1 -13 129.24 4.32 0 -1 13 115.31 3.07 0 -1 13 126.92 4.85 0 1 -13 132.47 5.00 0 1 -12 49.88 2.84 0 -1 12 45.75 1.65 0 1 -12 53.20 2.52 0 -1 12 50.10 2.79 0 -1 11 159.54 5.10 0 1 -11 156.80 5.17 0 1 -11 165.76 4.68 0 -1 11 151.49 3.46 0 1 -10 166.84 5.15 0 1 -10 164.88 4.58 0 -1 10 168.84 5.05 0 -1 10 163.83 3.52 0 -1 9 7.21 0.88 0 1 -9 9.38 0.91 0 1 -9 8.85 1.03 0 -1 9 8.97 0.58 0 1 -8 466.06 9.52 0 1 -8 470.79 8.93 0 -1 8 442.24 7.65 0 -1 8 462.25 9.33 0 -1 7 81.25 2.77 0 1 -7 82.73 2.88 0 1 -7 81.37 2.59 0 -1 7 74.70 1.80 0 1 -6 58.35 2.00 0 -1 6 53.93 2.08 0 1 -6 55.61 2.16 0 -1 6 53.54 1.33 0 1 -5 -0.23 0.16 0 1 -5 -0.02 0.17 0 1 -5 -0.06 0.07 0 -1 5 -0.12 0.09 0 -1 5 0.35 0.24 0 1 -4 582.68 10.13 0 -1 4 619.31 10.21 0 1 -4 593.02 10.39 0 -1 3 441.46 7.99 0 1 -3 443.42 7.93 0 -1 3 459.28 7.74 0 1 -3 473.81 7.86 0 -1 2 1.22 0.21 0 1 -2 1.05 0.17 0 1 -2 1.33 0.21 0 -1 2 0.25 0.08 0 -1 -2 583.22 9.55 0 1 2 606.12 9.58 0 1 2 598.67 9.49 0 -1 -2 628.59 9.59 0 1 3 21.77 0.99 0 1 3 24.54 0.93 0 -1 -3 21.12 0.98 0 -1 -3 22.00 0.97 0 -1 -4 400.97 6.52 0 1 4 390.91 6.51 0 1 4 387.91 6.98 0 -1 -4 410.54 7.34 0 -1 -4 414.88 7.39 0 1 4 400.59 7.37 0 -1 -5 17.33 1.05 0 -1 -5 18.03 1.08 0 1 5 16.45 1.06 0 -1 -5 17.22 0.72 0 1 5 18.88 0.95 0 1 6 958.95 16.46 0 -1 -6 973.96 16.43 0 -1 -6 958.88 15.31 0 -1 -6 952.46 16.37 0 1 6 948.87 15.73 0 1 7 170.50 3.92 0 -1 -7 163.59 3.59 0 1 7 164.87 4.48 0 -1 -7 163.62 4.39 0 1 8 13.59 1.19 0 -1 -8 14.41 0.87 0 1 8 13.68 0.95 0 -1 -8 13.86 1.16 0 -1 -9 1.58 0.32 0 1 9 1.69 0.38 0 -1 -9 1.58 0.40 0 1 9 1.05 0.32 0 -1 -10 3.84 0.67 0 -1 -10 3.99 0.54 0 1 10 3.99 0.55 0 1 10 4.00 0.80 0 -1 -11 0.86 0.32 0 1 11 0.01 0.27 0 1 11 0.82 0.32 0 -1 -11 0.31 0.31 0 -1 -12 60.57 2.40 0 1 12 59.81 2.42 0 1 12 55.91 3.05 0 -1 -12 60.06 3.09 0 -1 -13 25.15 2.07 0 1 13 27.62 1.62 0 1 13 24.66 2.12 0 -1 -13 27.22 1.65 0 -1 -14 432.72 9.21 0 1 14 424.17 10.91 0 -1 -14 447.83 11.00 0 1 14 449.41 9.19 0 -1 -15 0.98 0.48 0 1 15 2.35 0.58 0 1 15 3.03 0.89 0 -1 -15 2.49 0.58 0 1 16 2.19 0.49 0 1 16 3.64 1.00 0 -1 -16 3.34 0.90 0 -1 -16 2.54 0.63 0 -1 -17 67.97 3.13 0 1 17 78.62 4.36 0 -1 -17 79.34 4.41 0 -1 -18 30.59 2.77 0 1 18 36.85 3.12 0 -1 -19 12.30 1.91 0 1 19 10.49 1.76 0 1 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0 -2 12 266.65 7.74 0 -2 12 278.21 7.44 0 2 -12 269.29 7.59 0 2 -12 264.03 6.97 0 -2 11 -0.50 0.53 0 2 -11 0.46 0.27 0 -2 11 -0.07 0.27 0 2 -11 -0.30 0.37 0 -2 10 28.09 1.95 0 2 -10 28.67 1.78 0 2 -10 28.36 1.95 0 -2 10 30.02 1.87 0 -2 10 16.51 0.67 0 -2 9 30.02 1.80 0 -2 9 31.71 2.04 0 2 -9 29.65 1.91 0 2 -9 32.52 1.84 0 2 -8 209.62 5.55 0 2 -8 207.21 5.25 0 -2 8 206.11 5.26 0 -2 8 213.63 5.69 0 2 -7 43.00 1.95 0 2 -7 44.83 2.12 0 -2 7 41.65 1.90 0 -2 7 41.74 2.13 0 -2 6 311.73 6.93 0 -2 6 317.97 6.47 0 2 -6 318.23 6.67 0 2 -6 315.25 6.84 0 -2 5 4.83 0.62 0 2 -5 4.06 0.54 0 -2 5 3.97 0.47 0 -2 4 99.00 2.87 0 -2 4 96.67 2.46 0 2 -4 101.12 2.77 0 -2 3 835.68 12.78 0 -2 3 792.11 13.37 0 2 -3 781.50 13.24 0 2 -2 120.89 2.33 0 -2 2 118.83 2.25 0 2 -2 119.37 2.23 0 -2 2 120.80 2.88 0 -2 2 126.53 2.89 0 -2 2 117.20 2.32 0 2 -2 124.63 2.86 0 2 -1 3.64 0.38 0 2 -1 3.35 0.29 0 -2 1 4.13 0.40 0 -2 1 2.94 0.27 0 -2 1 4.12 0.44 0 2 0 1502.85 23.32 0 -2 0 1513.43 23.44 0 2 0 1575.65 23.32 0 -2 0 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4.33 0 -3 18 20.40 2.29 0 3 -18 18.04 1.99 0 -3 18 19.21 2.40 0 -3 17 15.70 1.92 0 3 -17 17.31 1.93 0 -3 17 16.82 2.11 0 3 -16 478.18 11.82 0 -3 16 495.65 12.99 0 -3 16 511.65 12.50 0 -3 15 49.96 3.40 0 -3 15 54.39 3.27 0 3 -15 46.71 2.92 0 -3 14 207.79 6.68 0 -3 14 208.06 7.14 0 3 -14 211.44 6.56 0 -3 13 55.96 3.09 0 3 -13 54.38 2.96 0 -3 13 53.17 3.25 0 -3 12 0.56 0.36 0 -3 12 -0.03 0.40 0 3 -12 0.02 0.31 0 -3 11 399.97 9.19 0 -3 11 391.70 9.73 0 3 -11 392.66 9.20 0 -3 10 1874.32 31.35 0 -3 10 1930.45 32.29 0 3 -10 1851.50 31.55 0 -3 9 438.04 9.84 0 -3 9 435.22 9.15 0 3 -9 429.35 9.42 0 3 -8 500.39 10.46 0 -3 8 537.28 10.25 0 -3 8 518.22 10.88 0 3 -7 19.29 1.36 0 -3 7 19.36 1.46 0 -3 7 19.16 1.26 0 3 -6 50.15 2.21 0 -3 6 52.43 2.36 0 -3 6 54.46 2.01 0 3 -5 85.11 2.84 0 -3 5 86.38 2.97 0 -3 5 84.91 2.45 0 -3 4 216.22 4.92 0 -3 4 227.16 4.23 0 -3 4 209.93 4.93 0 3 -4 190.56 3.53 0 3 -4 211.46 4.85 0 -3 3 273.10 4.79 0 3 -3 263.35 5.60 0 -3 3 262.06 5.68 0 -3 3 263.83 5.65 0 3 -3 258.78 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82.60 4.92 0 -8 16 80.55 5.01 0 -8 16 80.95 5.03 0 8 -15 4.55 1.21 0 -8 15 4.53 1.21 0 -8 15 6.87 1.43 0 -8 14 12.34 1.81 0 8 -14 9.86 1.65 0 -8 14 9.66 1.68 0 8 -13 93.58 4.95 0 -8 13 93.47 5.00 0 -8 13 95.93 5.08 0 -8 12 16.06 1.92 0 8 -12 15.84 1.96 0 -8 12 14.72 1.91 0 -8 11 136.28 5.59 0 8 -11 130.70 5.48 0 -8 11 142.97 5.82 0 -8 10 54.33 2.43 0 -8 10 67.31 3.86 0 -8 10 66.55 3.77 0 8 -10 62.40 3.70 0 -8 9 5.46 1.03 0 8 -9 4.65 0.96 0 -8 9 5.24 1.06 0 -8 9 3.94 0.59 0 -8 8 5.72 1.08 0 -8 8 3.07 0.88 0 8 -8 3.52 0.87 0 -8 8 3.28 0.56 0 -8 7 13.76 1.60 0 8 -7 15.10 1.70 0 8 -7 12.88 0.98 0 -8 7 9.24 0.81 0 -8 7 14.19 1.59 0 8 -6 209.02 6.57 0 -8 6 209.26 6.65 0 -8 6 210.75 6.55 0 8 -6 191.67 4.83 0 8 -5 0.73 0.27 0 -8 5 0.23 0.37 0 -8 5 0.15 0.31 0 8 -5 -0.41 0.44 0 8 -4 124.92 4.67 0 -8 4 122.84 4.66 0 -8 4 131.56 4.85 0 8 -4 122.12 3.77 0 8 -3 162.93 4.48 0 -8 3 138.83 4.93 0 8 -3 144.04 4.95 0 -8 3 135.08 5.02 0 8 -2 106.63 3.57 0 -8 2 109.37 4.15 0 8 -2 106.85 3.98 0 -8 2 113.44 4.33 0 -8 2 88.38 2.21 0 8 -1 666.08 11.51 0 8 -1 721.16 13.98 0 -8 1 725.71 14.27 0 -8 1 744.76 14.56 0 8 -1 738.02 13.61 0 -8 0 244.21 6.83 0 8 0 226.23 6.15 0 -8 0 239.44 6.61 0 8 0 237.10 6.28 0 8 0 232.11 4.75 0 8 1 344.33 6.61 0 8 1 330.13 7.80 0 8 1 337.77 8.11 0 -8 -1 332.92 8.49 0 -8 -1 338.76 8.42 0 -8 -2 34.27 2.23 0 8 2 33.40 1.57 0 8 2 34.95 2.19 0 -8 -2 33.87 2.29 0 8 2 33.93 1.94 0 -8 -3 56.58 2.93 0 8 3 54.40 2.20 0 8 3 50.89 2.34 0 8 3 51.17 2.73 0 -8 -3 52.86 2.81 0 8 4 156.39 4.31 0 8 4 151.26 4.25 0 -8 -4 146.12 5.14 0 -8 -4 139.71 4.97 0 8 4 147.45 5.07 0 8 5 50.22 2.83 0 -8 -5 48.23 2.80 0 -8 -5 47.48 2.74 0 8 5 48.13 2.14 0 8 5 51.29 2.37 0 -8 -6 107.18 4.32 0 8 6 108.45 3.27 0 8 6 103.24 4.29 0 8 6 105.54 3.76 0 -8 -6 99.37 4.17 0 -8 -7 225.64 6.76 0 8 7 227.80 6.86 0 8 7 218.39 6.10 0 8 7 217.78 5.03 0 -8 -7 221.04 6.73 0 -8 -7 203.81 4.89 0 -8 -8 50.87 3.00 0 8 8 46.63 2.91 0 -8 -8 42.49 1.72 0 8 8 47.78 2.65 0 -8 -8 43.89 2.82 0 -8 -9 5.51 1.01 0 -8 -9 3.85 0.92 0 8 9 6.26 1.07 0 8 9 4.24 0.80 0 8 10 60.38 3.28 0 -8 -10 64.31 3.59 0 8 10 57.66 3.45 0 -8 -10 69.43 3.71 0 8 11 108.06 4.84 0 -8 -11 108.01 4.88 0 8 11 108.42 4.70 0 -8 -11 111.06 4.92 0 -8 -12 0.54 0.48 0 -8 -12 0.56 0.42 0 8 12 1.83 0.70 0 8 12 1.52 0.70 0 -8 -13 25.17 2.36 0 8 13 28.38 2.53 0 -8 -13 28.72 2.60 0 8 13 27.80 2.51 0 -8 -14 76.69 4.45 0 8 14 80.95 4.43 0 8 14 79.13 4.36 0 -8 -14 77.10 4.39 0 -8 -15 -0.82 0.74 0 -8 -15 1.22 0.75 0 8 15 -0.18 0.42 0 8 15 0.23 0.49 0 -8 -16 24.32 2.63 0 -8 -16 23.40 2.47 0 8 16 21.30 2.43 0 8 16 24.47 2.49 0 8 17 0.98 0.51 0 8 17 1.96 0.83 0 -8 -17 0.93 0.59 0 -8 -17 2.37 0.71 0 8 18 179.91 7.33 0 -8 -18 172.12 7.59 0 8 18 180.76 7.85 0 -8 -18 186.05 7.93 0 8 19 10.57 1.95 0 8 19 9.32 1.76 0 -8 -19 8.55 1.80 0 -8 -19 7.70 1.55 0 8 20 127.43 6.31 0 -8 -20 136.50 7.02 0 8 20 128.22 6.93 0 8 21 51.17 4.44 0 -8 -21 48.00 4.26 0 -8 -22 2.73 1.18 0 8 22 3.81 1.39 0 8 23 10.26 2.17 0 -8 -23 9.88 2.13 0 8 24 82.39 6.21 0 -9 21 13.67 2.54 0 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209.99 5.62 0 -9 3 50.84 3.06 0 9 -3 51.12 2.93 0 9 -3 47.56 2.44 0 -9 3 46.56 2.87 0 9 -2 34.65 2.34 0 9 -2 32.35 2.00 0 -9 2 33.23 2.35 0 -9 2 32.16 2.38 0 9 -1 37.13 2.25 0 -9 1 35.19 2.41 0 9 -1 39.07 2.41 0 -9 1 33.84 2.48 0 9 0 104.65 4.01 0 -9 0 106.98 4.35 0 9 0 116.66 4.24 0 9 0 100.66 2.71 0 -9 0 113.74 4.56 0 -9 -1 0.30 0.31 0 -9 -1 0.01 0.36 0 9 1 0.31 0.33 0 9 1 0.97 0.50 0 9 1 0.39 0.20 0 -9 -2 170.66 5.68 0 9 2 163.77 5.02 0 -9 -2 168.97 5.75 0 9 2 166.23 4.19 0 9 2 159.88 5.37 0 9 3 244.32 6.30 0 9 3 238.48 5.69 0 -9 -3 247.78 7.24 0 9 3 245.20 7.07 0 -9 -3 235.06 7.03 0 9 4 513.36 9.81 0 -9 -4 465.81 11.09 0 9 4 453.77 9.79 0 -9 -4 425.37 10.84 0 9 4 491.62 11.20 0 9 5 84.47 3.12 0 -9 -5 86.63 4.00 0 9 5 81.12 3.88 0 9 5 83.05 3.22 0 -9 -5 86.23 3.97 0 -9 -6 6.48 1.15 0 -9 -6 6.01 1.04 0 9 6 6.22 0.86 0 9 6 5.12 0.71 0 9 6 6.77 1.20 0 -9 -7 3.25 0.73 0 9 7 4.14 0.93 0 9 7 3.12 0.54 0 -9 -7 4.22 0.94 0 9 7 3.64 0.73 0 -9 -8 0.41 0.35 0 9 8 0.93 0.47 0 9 8 1.14 0.53 0 -9 -8 0.71 0.56 0 9 9 89.60 4.40 0 -9 -9 87.84 4.34 0 9 9 90.41 4.00 0 -9 -9 87.53 4.31 0 9 10 234.63 7.23 0 -9 -10 220.98 7.51 0 -9 -10 229.36 7.58 0 9 10 239.22 7.75 0 -9 -11 6.47 1.25 0 9 11 8.60 1.37 0 9 11 8.50 1.41 0 -9 -11 6.65 1.20 0 -9 -12 1.45 0.79 0 -9 -12 1.83 0.79 0 9 12 2.40 0.78 0 9 12 1.80 0.63 0 9 13 68.90 4.02 0 9 13 69.75 4.19 0 -9 -13 71.09 4.22 0 -9 -13 69.42 4.21 0 9 14 47.96 3.51 0 -9 -14 47.67 3.50 0 9 14 46.54 3.41 0 -9 -14 48.32 3.57 0 -9 -15 3.10 0.95 0 9 15 5.43 1.23 0 -9 -15 3.60 1.03 0 9 15 5.30 1.29 0 9 16 112.24 5.78 0 -9 -16 113.67 5.93 0 -9 -16 108.88 5.71 0 9 16 112.92 5.70 0 9 17 0.77 0.69 0 -9 -17 -0.28 0.58 0 9 17 -0.42 0.59 0 -9 -17 -1.09 1.07 0 9 18 16.30 2.32 0 -9 -18 14.73 2.28 0 9 18 14.84 2.13 0 -9 -18 13.77 2.11 0 -9 -19 144.77 7.18 0 9 19 148.94 7.35 0 9 19 143.37 6.88 0 -9 -19 148.01 7.42 0 9 20 190.94 8.66 0 9 20 172.80 7.71 0 -9 -20 179.27 8.26 0 -9 -21 3.91 1.55 0 9 21 5.53 1.33 0 -9 -22 57.78 4.81 0 9 22 64.33 5.17 0 9 23 56.42 5.01 0 -10 20 1.69 1.02 0 -10 20 1.08 1.11 0 -10 19 22.81 3.09 0 -10 19 21.86 2.97 0 10 -19 16.20 2.63 0 -10 18 13.08 2.31 0 -10 18 11.47 2.13 0 10 -18 7.64 1.76 0 10 -17 2.23 0.91 0 -10 17 0.72 0.95 0 -10 17 -0.16 0.84 0 -10 16 34.87 3.45 0 -10 16 36.46 3.63 0 10 -16 35.25 3.48 0 -10 15 131.99 6.67 0 -10 15 133.20 6.84 0 10 -15 128.18 6.63 0 -10 14 160.37 7.27 0 -10 14 168.60 7.53 0 10 -14 147.91 7.06 0 -10 13 24.77 2.71 0 10 -13 23.57 2.55 0 -10 13 24.08 2.72 0 -10 12 0.42 0.57 0 -10 12 0.24 0.71 0 10 -12 0.29 0.51 0 -10 11 4.63 1.19 0 -10 11 2.08 0.78 0 10 -11 1.96 0.79 0 10 -10 14.51 1.95 0 -10 10 16.84 2.15 0 -10 10 16.36 2.03 0 -10 9 31.56 2.82 0 -10 9 36.92 2.99 0 10 -9 27.31 2.64 0 -10 8 39.37 3.04 0 -10 8 38.23 2.99 0 10 -8 41.81 3.13 0 -10 7 2.45 0.69 0 10 -7 4.19 1.02 0 -10 7 2.53 0.82 0 10 -6 4.97 1.11 0 10 -6 5.86 0.84 0 -10 6 8.93 1.41 0 -10 6 7.58 1.32 0 -10 5 116.47 5.16 0 10 -5 118.39 5.05 0 -10 5 114.28 5.00 0 10 -5 111.68 3.94 0 10 -4 34.77 2.12 0 -10 4 33.94 2.66 0 -10 4 36.72 2.71 0 10 -4 34.95 2.60 0 -10 3 14.04 1.77 0 10 -3 13.94 1.66 0 10 -3 14.37 1.37 0 -10 3 16.26 1.77 0 -10 2 1.76 0.72 0 -10 2 1.45 0.65 0 10 -2 0.96 0.55 0 10 -1 49.07 2.89 0 -10 1 48.20 2.97 0 10 -1 55.48 2.86 0 -10 1 40.74 2.89 0 -10 0 1.68 0.71 0 -10 0 1.72 0.69 0 10 0 0.77 0.42 0 10 0 0.49 0.32 0 10 1 165.00 5.41 0 -10 -1 160.47 5.99 0 10 1 160.58 5.49 0 -10 -1 166.74 5.92 0 10 2 55.79 3.11 0 -10 -2 58.17 3.29 0 -10 -2 56.50 3.31 0 10 2 57.16 2.90 0 10 2 55.84 2.19 0 -10 -3 57.63 3.36 0 10 3 55.05 3.15 0 10 3 51.42 2.69 0 -10 -3 58.93 3.33 0 10 3 54.17 2.30 0 -10 -4 24.82 2.20 0 10 4 24.65 1.77 0 10 4 24.92 1.62 0 -10 -4 26.70 2.25 0 10 4 24.06 2.12 0 -10 -5 1.75 0.64 0 10 5 2.98 0.66 0 10 5 3.26 0.84 0 10 5 2.48 0.60 0 -10 -5 2.43 0.77 0 10 6 166.12 5.14 0 -10 -6 164.40 6.07 0 10 6 160.08 5.99 0 -10 -6 169.29 6.14 0 10 6 163.22 4.84 0 10 7 199.06 6.97 0 -10 -7 208.24 7.06 0 10 7 219.01 6.28 0 10 7 201.13 5.39 0 -10 -7 197.76 6.91 0 -10 -8 1.03 0.60 0 10 8 1.82 0.53 0 -10 -8 0.93 0.43 0 10 8 1.97 0.63 0 -10 -9 16.38 1.93 0 -10 -9 16.89 1.95 0 10 9 16.12 1.96 0 10 9 13.96 1.59 0 10 10 376.76 10.55 0 -10 -10 357.00 10.29 0 10 10 357.90 9.63 0 -10 -10 356.89 10.35 0 10 11 317.99 9.17 0 -10 -11 322.12 9.79 0 -10 -11 315.12 9.70 0 10 11 316.51 9.73 0 -10 -12 3.64 0.99 0 10 12 5.00 1.07 0 -10 -12 3.09 0.89 0 10 12 4.86 1.20 0 10 13 4.10 1.03 0 -10 -13 1.96 0.82 0 -10 -13 6.20 1.41 0 10 13 4.43 1.19 0 10 14 29.83 2.76 0 10 14 32.76 2.99 0 -10 -14 26.18 2.71 0 -10 -14 34.01 3.09 0 -10 -15 61.19 4.26 0 10 15 62.75 4.24 0 -10 -15 62.46 4.33 0 10 15 58.51 4.03 0 -10 -16 153.38 7.11 0 10 16 157.57 7.10 0 -10 -16 170.81 7.61 0 10 16 168.77 7.31 0 -10 -17 104.57 5.96 0 10 17 104.57 5.77 0 10 17 106.10 5.87 0 -10 -17 105.93 5.93 0 10 18 10.87 1.94 0 10 18 11.59 1.92 0 -10 -18 14.57 2.33 0 -10 -18 10.70 1.94 0 10 19 61.14 4.54 0 10 19 71.67 5.07 0 -10 -19 62.84 4.67 0 -10 -19 68.67 5.01 0 -10 -20 93.69 6.05 0 10 20 95.00 6.12 0 10 20 81.45 5.40 0 -10 -20 91.58 5.82 0 10 21 1.04 0.89 0 -10 -21 1.48 1.15 0 10 22 67.72 5.42 0 -10 -22 65.20 5.25 0 -11 20 1.70 1.43 0 11 -19 -1.43 1.32 0 -11 19 2.01 1.46 0 -11 19 1.25 1.22 0 11 -18 -0.41 1.10 0 -11 18 1.70 1.12 0 -11 18 0.63 0.96 0 -11 17 -0.15 0.77 0 11 -17 -0.22 1.01 0 -11 17 1.16 0.95 0 -11 16 2.42 0.85 0 11 -16 3.36 1.05 0 -11 16 1.78 1.01 0 -11 15 14.78 2.36 0 11 -15 13.05 2.11 0 -11 15 11.97 2.08 0 -11 14 102.29 6.01 0 11 -14 113.08 6.23 0 -11 14 108.85 6.10 0 11 -13 67.02 4.70 0 -11 13 65.29 4.63 0 -11 13 72.63 4.80 0 -11 12 59.04 4.21 0 11 -12 57.56 4.24 0 -11 12 62.35 4.41 0 11 -11 99.29 5.48 0 -11 11 102.66 5.51 0 -11 11 114.55 5.90 0 11 -10 5.38 1.14 0 -11 10 5.70 1.25 0 -11 10 7.33 1.52 0 11 -9 0.81 0.75 0 -11 9 -0.27 0.56 0 -11 9 0.22 0.53 0 -11 8 11.98 1.83 0 -11 8 14.71 1.90 0 11 -8 12.61 1.84 0 -11 7 13.40 1.86 0 11 -7 10.65 1.63 0 -11 7 11.86 1.69 0 -11 6 451.60 11.87 0 -11 6 439.50 12.01 0 11 -6 422.12 9.61 0 11 -6 428.67 11.66 0 11 -5 -0.06 0.51 0 -11 5 1.52 0.78 0 -11 5 0.14 0.42 0 11 -5 0.79 0.52 0 11 -4 51.80 2.79 0 11 -4 45.67 3.15 0 -11 4 47.93 3.34 0 -11 4 47.76 3.28 0 -11 3 295.44 9.12 0 11 -3 306.68 7.97 0 11 -3 288.13 8.68 0 -11 3 308.12 9.05 0 11 -2 2.07 0.54 0 11 -2 2.17 0.70 0 -11 2 2.29 0.73 0 -11 2 1.55 0.74 0 -11 1 227.48 7.49 0 11 -1 221.13 7.11 0 11 -1 238.12 6.97 0 -11 1 221.75 7.64 0 -11 0 17.09 1.93 0 11 0 18.18 1.80 0 -11 0 16.78 1.92 0 11 0 17.19 1.75 0 -11 -1 13.29 1.70 0 11 1 11.61 1.48 0 -11 -1 13.96 1.75 0 11 1 11.18 1.38 0 11 2 753.81 16.03 0 11 2 748.98 15.40 0 -11 -2 762.77 16.68 0 -11 -2 745.56 16.41 0 -11 -3 18.16 1.93 0 11 3 20.46 1.77 0 -11 -3 16.81 1.87 0 11 3 20.18 1.99 0 11 4 15.53 1.34 0 -11 -4 15.64 1.79 0 -11 -4 15.76 1.90 0 11 4 18.80 1.95 0 11 4 15.33 1.52 0 -11 -5 0.24 0.43 0 11 5 0.09 0.33 0 11 5 0.11 0.32 0 11 5 0.66 0.50 0 -11 -5 0.03 0.55 0 -11 -6 46.85 3.22 0 11 6 54.43 3.45 0 -11 -6 49.52 3.33 0 11 6 50.57 2.66 0 11 6 47.19 2.53 0 -11 -7 233.79 7.85 0 11 7 224.76 6.57 0 11 7 214.72 5.96 0 -11 -7 225.35 7.70 0 11 7 225.04 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15 387.16 11.01 2 -5 -14 243.70 8.09 -2 5 14 241.13 7.60 -2 5 14 251.18 8.21 2 -5 -14 243.55 7.93 2 -5 -13 19.59 2.01 -2 5 13 15.25 1.67 2 -5 -13 15.23 1.79 -2 5 13 16.97 1.94 2 -5 -12 60.43 3.41 2 -5 -12 58.70 3.42 -2 5 12 54.77 3.12 -2 5 12 54.43 3.30 2 -5 -11 10.97 1.40 2 -5 -11 12.14 1.53 -2 5 11 12.04 1.38 -2 5 11 13.82 1.62 2 -5 -10 173.98 5.87 -2 5 10 162.99 5.53 -2 5 10 167.84 5.78 2 -5 -10 169.96 5.66 2 -5 -9 25.84 1.99 -2 5 9 27.38 2.07 2 -5 -9 25.09 2.02 -2 5 9 28.85 2.05 -2 5 8 71.24 3.31 -2 5 8 75.76 3.35 2 -5 -8 68.62 3.31 2 -5 -8 71.14 3.18 -2 5 7 9.11 1.10 2 -5 -7 8.69 1.05 2 -5 -7 10.43 1.23 -2 5 7 10.12 1.18 -2 5 6 13.55 0.62 2 -5 -6 18.99 1.58 2 -5 -6 21.92 1.56 -2 5 6 19.21 1.56 -2 5 6 19.40 1.54 2 -5 -6 17.32 1.46 -2 5 5 68.33 2.89 2 -5 -5 70.62 3.10 -2 5 5 72.54 3.04 -2 5 5 66.30 1.81 2 -5 -5 69.35 2.93 2 -5 -5 66.09 2.74 -2 5 4 54.69 1.76 -2 5 4 62.65 2.75 2 -5 -4 57.26 2.41 2 -5 -4 55.19 2.62 2 -5 -4 56.29 2.52 2 -5 -3 0.97 0.36 -2 5 3 0.52 0.25 2 -5 -3 0.50 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0.79 -2 -4 15 2.93 0.96 -2 -4 15 2.77 0.72 -2 -4 14 14.79 1.81 2 4 -14 16.64 1.69 -2 -4 14 16.12 1.67 2 4 -13 471.61 11.20 -2 -4 13 478.18 10.91 -2 -4 13 484.75 12.11 2 4 -12 21.44 1.87 -2 -4 12 21.64 1.75 -2 -4 12 19.57 1.98 2 4 -11 9.98 1.25 -2 -4 11 11.09 1.42 -2 -4 11 11.25 1.20 2 4 -10 114.73 4.26 -2 -4 10 119.60 4.65 -2 -4 10 111.71 2.84 -2 -4 10 114.83 3.86 2 4 -9 55.68 2.77 -2 -4 9 56.94 2.97 -2 -4 9 51.97 1.79 -2 -4 9 56.57 2.42 -2 -4 8 245.69 6.67 2 4 -8 239.07 6.33 -2 -4 8 232.83 5.55 2 4 -8 238.25 5.07 2 4 -7 4.95 0.79 -2 -4 7 5.04 0.81 2 4 -7 5.65 0.59 -2 -4 7 5.74 0.63 2 4 -6 3.54 0.64 -2 -4 6 3.75 0.67 -2 -4 6 3.00 0.66 -2 -4 6 3.80 0.50 2 4 -6 3.06 0.42 2 4 -5 362.18 8.06 2 4 -5 371.61 7.18 -2 -4 5 375.97 6.85 -2 -4 5 359.58 8.13 -2 -4 5 370.44 8.07 -2 -4 4 578.67 11.24 -2 -4 4 587.18 11.46 -2 -4 4 599.14 9.89 2 4 -4 594.95 11.39 2 4 -4 591.06 10.56 -2 -4 3 111.11 3.32 -2 -4 3 104.85 3.40 2 4 -3 109.01 2.39 2 4 -3 107.34 3.02 -2 -4 3 109.01 2.37 2 4 -3 110.72 3.46 -2 -4 2 28.31 1.54 2 4 -2 27.24 1.38 2 4 -2 26.61 1.53 2 4 -2 25.92 0.88 -2 -4 2 27.05 1.43 -2 -4 1 10.21 0.81 2 4 -1 9.32 0.88 -2 -4 1 9.35 0.84 2 4 -1 10.61 0.86 2 4 -1 7.95 0.47 -2 -4 0 96.50 2.76 -2 -4 0 98.67 3.03 2 4 0 98.11 3.01 2 4 0 98.66 2.23 2 4 0 101.69 3.09 2 4 1 212.73 5.07 2 4 1 215.43 4.27 -2 -4 -1 224.59 4.76 2 4 1 220.04 5.10 -2 -4 -1 210.81 5.01 2 4 2 198.30 4.98 -2 -4 -2 212.16 4.64 -2 -4 -2 219.27 5.05 2 4 2 215.42 4.48 2 4 2 210.61 4.96 -2 -4 -3 2.31 0.38 2 4 3 1.95 0.41 2 4 3 1.96 0.40 -2 -4 -3 3.10 0.49 -2 -4 -3 3.14 0.54 2 4 3 3.57 0.48 -2 -4 -4 8.63 0.79 2 4 4 5.93 0.73 -2 -4 -4 8.22 0.73 2 4 4 7.67 0.77 -2 -4 -4 7.26 0.80 2 4 5 734.59 13.40 2 4 5 730.90 13.21 -2 -4 -5 722.18 12.73 -2 -4 -5 718.24 13.29 -2 -4 -5 710.31 12.71 2 4 6 888.54 15.92 2 4 6 880.20 15.85 -2 -4 -6 886.98 15.35 -2 -4 -6 862.33 15.80 -2 -4 -6 881.37 15.12 2 4 7 111.73 3.78 -2 -4 -7 118.87 3.62 -2 -4 -7 118.68 3.36 2 4 7 118.80 3.92 -2 -4 -7 114.45 3.85 -2 -4 -8 28.72 1.70 -2 -4 -8 26.85 1.46 2 4 8 27.33 1.85 2 4 8 24.72 1.69 -2 -4 -8 24.63 1.72 -2 -4 -9 2.38 0.60 -2 -4 -9 2.36 0.51 2 4 9 2.77 0.67 2 4 9 2.29 0.54 -2 -4 -9 2.40 0.48 -2 -4 -10 91.27 3.05 2 4 10 98.21 3.68 -2 -4 -10 90.56 3.52 2 4 10 88.29 3.82 -2 -4 -10 90.97 3.77 -2 -4 -11 29.33 2.14 -2 -4 -11 30.09 1.70 2 4 11 29.78 2.22 -2 -4 -11 27.88 1.96 2 4 11 29.79 1.98 2 4 12 252.09 6.86 -2 -4 -12 250.93 7.01 2 4 12 246.63 7.49 -2 -4 -12 250.82 6.05 -2 -4 -12 246.75 7.32 2 4 13 2.85 0.72 -2 -4 -13 1.83 0.63 2 4 13 1.90 0.64 -2 -4 -13 1.62 0.68 -2 -4 -13 2.14 0.52 -2 -4 -14 270.15 7.83 -2 -4 -14 266.08 6.58 -2 -4 -14 268.51 8.14 2 4 14 267.72 8.44 2 4 14 272.25 7.51 -2 -4 -15 264.22 7.94 2 4 15 271.24 7.55 2 4 15 265.37 8.58 -2 -4 -15 244.96 6.48 -2 -4 -16 408.85 10.79 2 4 16 407.01 11.53 2 4 16 395.21 9.97 2 4 17 6.59 1.12 -2 -4 -17 9.38 1.51 2 4 17 5.81 1.29 2 4 18 186.08 6.40 -2 -4 -18 197.06 7.33 2 4 18 190.08 7.78 -2 -4 -19 11.72 1.87 2 4 19 10.53 1.97 -2 -4 -20 261.56 9.24 2 4 20 255.73 9.80 -2 -4 -21 -0.58 0.76 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31.26 1.49 -2 -5 8 42.05 2.53 2 5 -7 65.81 3.03 -2 -5 7 64.06 3.11 2 5 -7 68.27 2.27 -2 -5 7 67.93 3.14 -2 -5 7 66.25 2.24 -2 -5 6 774.67 15.01 -2 -5 6 793.34 13.08 2 5 -6 769.73 14.94 -2 -5 6 764.18 15.12 2 5 -6 774.89 13.46 2 5 -5 2.61 0.48 2 5 -5 2.93 0.65 -2 -5 5 2.71 0.60 -2 -5 5 1.82 0.47 -2 -5 5 2.31 0.31 -2 -5 4 773.96 12.42 2 5 -4 803.82 14.76 -2 -5 4 795.24 14.79 -2 -5 4 784.32 14.51 2 5 -4 782.70 13.67 -2 -5 3 100.93 3.40 -2 -5 3 76.30 1.71 -2 -5 3 93.66 3.18 2 5 -3 100.40 2.96 2 5 -3 97.96 3.37 2 5 -2 1.72 0.41 2 5 -2 2.40 0.53 -2 -5 2 1.84 0.50 -2 -5 2 2.17 0.47 -2 -5 1 7.33 0.80 -2 -5 1 8.57 1.05 2 5 -1 6.48 0.75 2 5 -1 6.92 0.81 2 5 0 29.15 1.64 -2 -5 0 29.40 1.67 -2 -5 0 29.73 1.54 2 5 0 25.98 0.92 2 5 0 27.55 1.56 2 5 1 1.48 0.43 2 5 1 2.29 0.47 -2 -5 -1 2.18 0.47 2 5 1 1.56 0.26 -2 -5 -1 1.87 0.44 2 5 2 76.88 2.90 -2 -5 -2 82.56 2.74 -2 -5 -2 82.53 2.98 2 5 2 83.09 2.85 2 5 2 84.53 2.35 -2 -5 -3 32.81 1.83 -2 -5 -3 32.97 1.63 2 5 3 37.32 1.60 2 5 3 34.95 1.76 2 5 3 32.82 1.85 2 5 4 842.58 15.35 -2 -5 -4 821.23 14.66 2 5 4 853.82 14.70 -2 -5 -4 859.07 14.75 -2 -5 -4 815.68 15.21 -2 -5 -5 274.77 6.06 -2 -5 -5 274.24 6.19 2 5 5 272.26 6.27 2 5 5 269.56 6.63 -2 -5 -5 276.89 6.66 -2 -5 -6 111.85 3.30 2 5 6 105.21 3.75 -2 -5 -6 114.31 3.56 2 5 6 108.79 3.63 -2 -5 -6 111.59 3.85 2 5 7 341.47 8.06 -2 -5 -7 341.15 8.11 -2 -5 -7 335.80 7.63 2 5 7 355.17 8.02 -2 -5 -7 350.48 7.21 2 5 8 9.83 1.13 -2 -5 -8 10.65 1.10 -2 -5 -8 8.92 0.85 2 5 8 12.19 1.26 -2 -5 -8 9.93 1.14 2 5 9 1.72 0.57 -2 -5 -9 1.23 0.42 -2 -5 -9 1.27 0.37 -2 -5 -9 1.41 0.51 2 5 9 1.97 0.61 -2 -5 -10 176.52 5.38 2 5 10 183.31 5.62 -2 -5 -10 177.97 4.62 2 5 10 177.17 5.77 -2 -5 -10 170.60 5.61 -2 -5 -11 63.19 2.51 -2 -5 -11 63.98 3.12 2 5 11 68.56 3.27 2 5 11 71.40 3.54 -2 -5 -11 61.20 3.28 -2 -5 -12 889.29 15.87 -2 -5 -12 892.40 17.54 2 5 12 902.20 18.27 2 5 12 882.91 17.45 -2 -5 -12 903.60 18.13 -2 -5 -13 29.26 2.24 2 5 13 29.71 2.44 -2 -5 -13 27.72 2.31 -2 -5 -13 26.10 1.63 2 5 13 29.49 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30.16 2.37 -4 7 5 28.24 2.26 4 -7 -5 26.17 2.19 4 -7 -5 26.57 1.87 4 -7 -4 837.66 16.95 -4 7 4 827.14 15.10 -4 7 4 821.81 16.99 4 -7 -4 826.19 16.88 4 -7 -4 865.89 15.93 4 -7 -3 15.65 1.36 4 -7 -3 14.03 1.51 4 -7 -3 14.34 1.51 -4 7 3 12.36 1.14 -4 7 3 16.86 1.70 4 -7 -2 0.68 0.41 4 -7 -2 1.01 0.56 -4 7 2 1.18 0.59 4 -7 -2 0.27 0.27 -4 7 2 0.03 0.28 4 -7 -1 105.40 3.66 -4 7 1 100.73 4.16 4 -7 -1 101.25 4.20 -4 7 1 101.85 3.76 4 -7 -1 100.04 4.14 4 -7 0 1232.75 21.26 -4 7 0 1214.05 22.26 4 -7 0 1218.16 22.55 -4 7 0 1191.79 21.74 4 -7 0 1233.24 22.39 4 -7 1 40.08 2.14 4 -7 1 44.45 2.60 -4 7 -1 41.29 2.48 4 -7 1 43.81 2.68 -4 7 -1 43.67 2.49 -4 7 -2 10.24 1.22 4 -7 2 8.36 1.11 4 -7 2 8.31 1.22 -4 7 -2 7.34 1.05 4 -7 2 11.10 1.12 4 -7 3 40.40 2.19 -4 7 -3 37.18 2.25 -4 7 -3 36.93 2.43 4 -7 3 37.66 2.52 4 -7 3 37.24 2.40 4 -7 4 14.53 1.48 4 -7 4 10.84 1.22 -4 7 -4 12.82 1.49 -4 7 -4 12.50 1.28 4 -7 4 13.24 1.56 4 -7 5 2.37 0.59 4 -7 5 3.69 0.76 -4 7 -5 4.94 0.79 -4 7 -5 2.51 0.60 4 -7 5 3.14 0.79 4 -7 6 33.64 2.17 -4 7 -6 32.91 1.94 -4 7 -6 27.33 2.29 4 -7 6 33.35 2.43 4 -7 6 29.12 2.17 -4 7 -7 185.58 5.13 -4 7 -7 186.21 6.62 4 -7 7 195.33 6.52 4 -7 7 185.14 6.09 4 -7 7 198.03 5.92 4 -7 8 91.45 4.12 4 -7 8 97.09 4.02 -4 7 -8 86.51 4.41 4 -7 8 98.52 4.44 4 -7 9 284.55 7.83 -4 7 -9 269.24 8.58 4 -7 9 287.63 8.45 4 -7 9 260.18 7.84 4 -7 10 24.43 2.10 4 -7 10 23.13 2.07 4 -7 10 24.96 2.36 -4 7 -10 22.93 2.39 4 -7 11 26.11 2.23 -4 7 -11 26.21 2.58 4 -7 11 26.37 2.28 4 -7 11 27.74 2.44 4 -7 12 83.85 4.27 -4 7 -12 91.10 4.96 4 -7 12 87.95 4.63 4 -7 12 83.22 4.33 -4 7 -13 12.55 1.84 4 -7 13 15.20 1.97 4 -7 13 16.87 1.95 4 -7 13 13.33 1.83 4 -7 14 2.38 0.90 4 -7 14 1.52 0.65 4 -7 14 2.27 1.18 -4 7 -14 1.94 0.89 4 -7 15 3.79 1.16 4 -7 15 4.24 1.10 -4 7 -15 3.72 1.21 4 -7 15 2.99 0.84 4 -7 16 24.46 2.56 -4 7 -16 26.98 2.97 4 -7 16 28.45 2.74 4 -7 16 27.22 2.77 4 -7 17 83.22 5.02 -4 7 -17 83.52 5.38 4 -7 17 77.23 4.74 4 -7 17 92.46 5.39 4 -7 18 7.01 1.78 -4 7 -18 9.07 1.88 4 -7 19 29.50 3.33 -4 7 -19 29.44 3.34 -4 7 -20 0.26 1.01 4 -6 -23 6.41 1.87 -4 6 23 8.71 2.18 4 -6 -22 7.38 2.02 -4 6 22 2.36 1.12 4 -6 -21 20.96 2.97 -4 6 21 18.54 2.73 4 -6 -20 94.50 6.01 -4 6 20 87.74 5.29 -4 6 20 89.65 5.89 4 -6 -19 29.19 3.25 -4 6 19 30.17 3.00 -4 6 19 29.02 3.29 4 -6 -18 3.49 1.22 -4 6 18 5.31 1.41 -4 6 18 4.54 1.42 4 -6 -17 15.20 2.25 -4 6 17 15.94 2.14 -4 6 17 16.52 2.28 4 -6 -16 52.28 3.95 -4 6 16 52.63 3.74 -4 6 16 54.25 4.04 4 -6 -15 3.96 0.96 -4 6 15 5.11 1.28 -4 6 15 3.15 0.99 4 -6 -14 61.25 4.04 -4 6 14 60.48 3.82 -4 6 14 59.49 4.03 4 -6 -13 18.20 2.07 -4 6 13 19.03 2.11 -4 6 13 19.26 2.22 4 -6 -13 21.95 2.20 4 -6 -12 0.85 0.58 -4 6 12 -1.32 0.78 -4 6 12 -1.19 0.78 4 -6 -12 0.69 0.52 4 -6 -11 5.62 1.09 4 -6 -11 6.94 1.31 -4 6 11 5.51 1.04 -4 6 11 5.11 1.03 -4 6 10 95.96 4.65 4 -6 -10 94.92 4.56 -4 6 10 101.39 4.65 4 -6 -10 97.68 4.29 4 -6 -9 46.62 3.18 4 -6 -9 47.41 3.13 -4 6 9 49.79 3.23 -4 6 9 53.29 3.25 4 -6 -9 51.77 2.96 -4 6 8 100.32 4.54 4 -6 -8 103.35 4.56 -4 6 8 98.74 4.47 4 -6 -8 102.63 4.60 4 -6 -8 104.93 4.15 4 -6 -7 29.51 2.31 -4 6 7 33.05 2.43 4 -6 -7 31.86 2.42 4 -6 -7 27.76 1.99 4 -6 -6 125.88 4.85 -4 6 6 121.67 4.82 -4 6 6 117.67 3.21 4 -6 -6 121.67 4.84 4 -6 -6 128.63 4.32 -4 6 5 7.66 0.75 4 -6 -5 6.12 0.83 -4 6 5 7.46 1.15 4 -6 -5 5.92 1.02 4 -6 -5 7.37 1.13 4 -6 -4 113.38 4.47 4 -6 -4 111.22 4.37 -4 6 4 107.15 4.37 -4 6 4 110.24 3.37 4 -6 -4 108.96 3.71 4 -6 -3 64.86 2.66 4 -6 -3 63.58 3.14 -4 6 3 64.17 3.23 -4 6 3 62.59 2.53 4 -6 -3 67.70 3.30 -4 6 2 1.67 0.46 4 -6 -2 1.56 0.50 4 -6 -2 0.92 0.47 4 -6 -2 0.37 0.27 -4 6 2 0.68 0.34 4 -6 -1 64.17 3.15 4 -6 -1 68.18 3.17 -4 6 1 68.31 3.18 -4 6 1 60.89 2.71 4 -6 -1 67.83 2.61 4 -6 0 95.53 3.22 -4 6 0 98.67 3.64 4 -6 0 95.71 3.82 -4 6 0 96.94 3.82 4 -6 0 96.09 3.90 4 -6 1 1.00 0.36 4 -6 1 -0.16 0.27 -4 6 -1 -0.14 0.44 4 -6 1 0.46 0.26 -4 6 -1 1.46 0.54 4 -6 2 138.38 4.05 -4 6 -2 130.97 4.60 -4 6 -2 146.10 4.65 4 -6 2 137.95 4.78 4 -6 2 144.14 4.93 4 -6 3 23.09 1.47 -4 6 -3 21.71 1.60 4 -6 3 21.67 1.83 -4 6 -3 23.64 1.83 4 -6 3 22.28 1.79 4 -6 4 297.70 6.89 -4 6 -4 297.03 7.17 4 -6 4 280.86 7.63 -4 6 -4 311.12 8.02 4 -6 4 289.32 7.68 4 -6 5 74.49 3.01 -4 6 -5 82.29 3.14 4 -6 5 82.05 3.63 -4 6 -5 74.93 3.63 4 -6 5 73.21 3.44 4 -6 6 1.71 0.55 4 -6 6 2.88 0.86 -4 6 -6 1.48 0.43 -4 6 -6 2.76 0.79 4 -6 6 1.46 0.43 -4 6 -7 1.47 0.39 4 -6 7 2.51 0.60 4 -6 7 1.39 0.55 4 -6 7 1.74 0.59 -4 6 -7 2.96 0.77 4 -6 8 -0.05 0.39 4 -6 8 0.68 0.38 4 -6 8 -0.74 0.63 -4 6 -8 0.01 0.28 -4 6 -8 0.89 0.45 4 -6 9 31.25 2.20 -4 6 -9 29.70 2.52 4 -6 9 35.74 2.55 4 -6 9 34.38 2.50 4 -6 10 145.70 5.21 -4 6 -10 138.89 5.74 4 -6 10 130.88 5.24 4 -6 10 137.40 5.41 4 -6 11 48.64 3.14 -4 6 -11 52.48 3.47 4 -6 11 50.45 3.25 4 -6 11 51.41 3.07 4 -6 12 259.74 7.84 -4 6 -12 250.05 8.52 4 -6 12 248.25 8.04 4 -6 12 251.15 7.99 4 -6 13 15.73 1.94 -4 6 -13 15.56 2.02 4 -6 13 15.34 1.86 4 -6 13 16.03 1.92 4 -6 14 2.44 0.88 4 -6 14 0.97 0.58 4 -6 14 1.56 0.63 -4 6 -14 0.88 0.61 4 -6 15 53.50 3.64 -4 6 -15 52.64 3.90 4 -6 15 58.28 3.91 4 -6 15 53.97 3.70 -4 6 -16 3.56 1.15 4 -6 16 2.41 0.78 4 -6 16 0.92 0.73 4 -6 16 4.03 1.14 -4 6 -17 30.05 3.07 4 -6 17 29.57 2.88 4 -6 17 32.29 3.13 4 -6 17 32.18 3.03 4 -6 18 46.01 3.77 4 -6 18 52.30 4.06 4 -6 18 49.07 3.82 -4 6 -18 44.63 3.87 4 -6 19 51.28 4.09 -4 6 -19 56.91 4.45 4 -6 19 55.25 4.26 -4 6 -20 22.00 2.89 4 -5 -24 54.09 5.08 -4 5 24 54.04 5.03 -4 5 23 4.02 1.62 4 -5 -23 3.59 1.37 4 -5 -22 65.66 5.20 -4 5 22 68.27 5.35 4 -5 -21 11.63 2.10 -4 5 21 5.78 1.62 4 -5 -20 144.93 7.41 -4 5 20 129.99 6.35 -4 5 20 147.52 7.42 4 -5 -19 -0.09 0.62 -4 5 19 1.24 0.87 -4 5 19 -0.64 0.95 4 -5 -18 4.39 1.34 -4 5 18 7.22 1.52 -4 5 18 6.26 1.48 4 -5 -17 69.20 4.64 -4 5 17 66.33 4.10 -4 5 17 61.19 4.40 4 -5 -16 311.25 10.28 -4 5 16 310.30 9.59 -4 5 16 309.61 10.34 4 -5 -15 92.70 5.08 -4 5 15 97.06 4.82 -4 5 15 93.13 5.13 4 -5 -14 775.75 17.81 -4 5 14 800.15 17.35 -4 5 14 757.05 17.92 4 -5 -13 51.86 3.54 -4 5 13 54.48 3.42 -4 5 13 55.90 3.71 4 -5 -12 199.68 7.12 -4 5 12 198.32 7.20 -4 5 12 196.39 6.83 4 -5 -11 115.27 5.07 -4 5 11 108.39 4.82 -4 5 11 116.81 5.20 4 -5 -11 111.32 4.65 4 -5 -10 13.19 1.57 -4 5 10 18.68 1.88 -4 5 10 13.29 1.62 4 -5 -10 15.67 1.59 4 -5 -9 72.90 3.70 -4 5 9 71.58 3.65 -4 5 9 69.52 3.73 4 -5 -9 64.36 3.66 4 -5 -9 68.57 3.31 4 -5 -8 389.09 10.11 4 -5 -8 391.13 9.21 4 -5 -8 375.55 9.71 -4 5 8 395.04 9.89 -4 5 8 386.91 10.00 4 -5 -7 84.76 3.82 -4 5 7 84.62 3.86 -4 5 7 75.01 2.16 4 -5 -7 80.54 3.86 4 -5 -7 83.64 3.41 4 -5 -6 215.15 6.43 -4 5 6 211.27 6.50 4 -5 -6 207.97 6.56 -4 5 6 216.08 4.65 4 -5 -6 217.76 5.81 4 -5 -5 263.56 7.10 -4 5 5 264.31 7.29 4 -5 -5 254.00 7.28 -4 5 5 251.24 5.50 4 -5 -5 261.48 6.33 4 -5 -4 224.57 6.37 4 -5 -4 229.14 6.66 -4 5 4 216.45 6.45 -4 5 4 227.94 5.31 4 -5 -4 243.55 5.74 4 -5 -3 107.80 3.96 -4 5 3 106.21 4.10 4 -5 -3 103.80 4.12 -4 5 3 108.30 3.35 4 -5 -3 102.89 3.28 4 -5 -2 22.49 1.71 -4 5 2 23.20 1.78 -4 5 2 21.98 1.44 4 -5 -2 23.48 1.83 4 -5 -2 23.47 1.37 4 -5 -1 85.21 3.60 4 -5 -1 91.05 3.50 -4 5 1 87.43 3.55 -4 5 1 83.11 3.16 4 -5 -1 89.62 2.82 4 -5 0 119.31 3.37 4 -5 0 114.31 4.01 -4 5 0 121.86 4.21 4 -5 0 124.29 4.38 -4 5 0 123.34 4.10 -4 5 -1 -0.15 0.36 4 -5 1 0.12 0.20 4 -5 1 1.05 0.47 4 -5 1 0.38 0.34 -4 5 -1 1.10 0.53 4 -5 2 229.71 5.21 4 -5 2 221.09 6.09 -4 5 -2 229.11 5.99 4 -5 2 222.40 6.32 -4 5 -2 219.51 6.11 4 -5 3 108.29 3.24 4 -5 3 105.10 3.89 -4 5 -3 109.78 3.76 -4 5 -3 109.78 4.06 4 -5 3 103.92 4.02 4 -5 4 0.40 0.26 -4 5 -4 0.92 0.38 -4 5 -4 -0.55 0.54 4 -5 4 0.56 0.41 4 -5 4 0.04 0.26 4 -5 5 190.45 4.96 -4 5 -5 191.63 5.08 4 -5 5 195.99 5.67 -4 5 -5 172.14 5.76 4 -5 5 184.64 5.75 4 -5 6 22.82 1.54 -4 5 -6 21.49 1.42 4 -5 6 19.74 1.70 -4 5 -6 20.45 1.83 4 -5 6 20.76 1.74 4 -5 7 4.67 0.86 4 -5 7 2.72 0.65 -4 5 -7 4.24 0.63 4 -5 7 3.58 0.68 -4 5 -7 4.14 0.93 -4 5 -8 137.80 5.29 -4 5 -8 138.20 3.87 4 -5 8 133.93 4.98 4 -5 8 132.36 4.45 4 -5 8 132.10 4.83 4 -5 9 101.15 3.92 -4 5 -9 87.34 2.92 -4 5 -9 104.42 4.59 4 -5 9 97.51 4.14 4 -5 9 100.21 4.30 4 -5 10 75.95 3.51 -4 5 -10 66.77 3.76 4 -5 10 75.85 3.81 4 -5 10 73.26 3.64 4 -5 11 32.59 2.34 4 -5 11 36.71 2.64 4 -5 11 37.62 2.66 -4 5 -11 37.32 2.83 4 -5 12 82.17 4.03 -4 5 -12 97.68 4.77 4 -5 12 95.83 4.45 4 -5 12 98.63 4.58 4 -5 13 31.67 2.53 4 -5 13 30.08 2.53 4 -5 13 30.93 2.60 -4 5 -13 29.91 2.66 4 -5 14 63.77 3.75 4 -5 14 67.72 3.97 -4 5 -14 68.81 4.22 4 -5 14 70.34 4.07 4 -5 15 2.66 0.85 -4 5 -15 1.39 0.83 4 -5 15 0.58 0.63 4 -5 15 1.48 0.65 4 -5 16 6.54 1.39 4 -5 16 3.45 0.94 4 -5 16 3.86 1.04 -4 5 -16 4.29 1.23 4 -5 17 1.18 0.77 4 -5 17 1.64 0.99 4 -5 17 1.97 0.87 -4 5 -17 1.17 0.86 4 -5 18 28.05 2.86 -4 5 -18 32.13 3.19 4 -5 18 29.66 3.00 4 -5 18 31.82 3.02 4 -5 19 33.26 3.24 4 -5 19 34.98 3.39 4 -5 19 37.14 3.50 -4 5 -19 34.54 3.39 4 -5 20 18.32 2.45 4 -5 20 12.84 2.06 -4 5 -20 14.16 2.21 -4 5 -21 6.47 1.61 4 -4 -24 48.12 4.79 -4 4 24 53.68 4.89 -4 4 23 25.75 3.33 4 -4 -23 25.03 3.36 4 -4 -22 3.23 1.03 -4 4 22 3.91 1.57 4 -4 -21 3.77 1.25 -4 4 21 1.98 0.93 4 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0.79 4 -4 -5 4.07 0.82 4 -4 -5 3.67 0.58 4 -4 -4 634.01 12.71 -4 4 4 639.42 13.08 -4 4 4 640.80 11.58 4 -4 -4 655.17 11.83 4 -4 -4 641.58 13.36 4 -4 -3 10.71 1.12 4 -4 -3 11.37 1.23 -4 4 3 11.95 1.02 -4 4 3 11.06 1.21 4 -4 -3 11.77 0.90 4 -4 -2 514.87 10.42 -4 4 2 506.45 10.81 4 -4 -2 499.02 10.95 -4 4 2 502.76 9.93 4 -4 -2 515.92 9.33 4 -4 -1 62.06 2.63 -4 4 1 68.26 2.95 4 -4 -1 60.37 2.90 -4 4 1 58.35 2.48 4 -4 -1 62.95 2.06 -4 4 0 3.04 0.61 4 -4 0 1.84 0.35 4 -4 0 1.66 0.46 -4 4 0 1.50 0.40 4 -4 0 1.46 0.44 4 -4 1 172.73 3.88 4 -4 1 170.12 5.21 4 -4 1 181.72 4.87 -4 4 -1 169.96 4.94 -4 4 -1 157.24 4.83 4 -4 2 8.39 0.69 -4 4 -2 6.22 0.96 4 -4 2 9.18 0.99 4 -4 2 10.39 1.14 -4 4 -2 8.02 0.94 4 -4 3 1.77 0.38 -4 4 -3 1.95 0.47 -4 4 -3 0.99 0.35 4 -4 3 2.31 0.60 4 -4 3 2.66 0.63 4 -4 4 75.53 2.99 -4 4 -4 71.74 2.81 4 -4 4 74.44 3.25 -4 4 -4 69.29 3.15 4 -4 4 74.68 2.46 4 -4 5 52.33 2.15 -4 4 -5 50.02 2.71 4 -4 5 54.07 2.77 4 -4 5 54.01 2.53 -4 4 -5 54.96 2.36 4 -4 6 309.28 6.89 -4 4 -6 316.60 6.95 4 -4 6 315.05 8.01 4 -4 6 317.32 7.55 -4 4 -6 302.19 8.12 4 -4 7 111.21 4.36 4 -4 7 113.64 3.73 -4 4 -7 113.37 4.57 4 -4 7 114.72 4.09 -4 4 -7 123.88 3.64 4 -4 8 450.37 9.60 -4 4 -8 428.92 10.60 4 -4 8 452.21 10.08 4 -4 8 451.42 10.58 -4 4 -8 444.40 8.83 4 -4 9 453.76 10.39 4 -4 9 454.22 9.99 4 -4 9 458.83 10.91 -4 4 -9 447.37 8.81 -4 4 -9 461.11 11.21 -4 4 -10 384.80 10.07 4 -4 10 385.98 9.44 4 -4 10 377.37 9.79 4 -4 10 381.34 9.12 4 -4 11 8.38 1.20 4 -4 11 9.14 1.33 4 -4 12 196.60 6.82 -4 4 -12 197.35 6.95 4 -4 12 203.21 6.60 4 -4 13 7.37 1.22 4 -4 13 6.33 1.23 -4 4 -13 6.64 1.26 4 -4 14 33.95 2.79 4 -4 14 29.36 2.49 -4 4 -14 28.93 2.62 4 -4 15 26.47 2.46 4 -4 15 25.54 2.49 -4 4 -15 25.09 2.53 4 -4 16 50.59 3.69 -4 4 -16 46.20 3.50 4 -4 16 49.71 3.52 4 -4 17 6.21 1.40 4 -4 17 3.52 1.29 -4 4 -17 6.64 1.37 4 -4 18 24.38 2.62 4 -4 18 27.80 2.86 -4 4 -18 28.83 2.92 -4 4 -19 7.96 1.60 4 -4 19 9.78 1.99 4 -4 19 7.59 1.72 4 -4 20 3.81 1.28 -4 4 -20 3.88 1.23 4 -4 20 4.48 1.24 4 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5.01 -4 -11 -11 92.54 4.21 -4 -11 -12 7.27 1.51 4 11 12 9.82 1.89 -4 -11 -12 7.32 1.38 4 11 12 5.33 1.15 4 11 13 1.81 0.95 -4 -11 -13 1.65 0.79 4 11 13 0.33 0.62 -4 -11 -13 0.60 0.61 4 11 14 49.71 3.97 4 11 14 48.16 3.66 -4 -11 -14 46.81 3.42 -4 -11 -14 49.10 3.90 4 11 15 6.63 1.61 -4 -11 -15 8.32 1.47 4 11 15 7.05 1.54 -4 -11 -15 8.07 1.66 4 11 16 0.79 0.64 -4 -11 -16 0.99 0.72 4 11 16 2.81 0.96 -4 -11 -16 2.45 1.12 4 11 17 3.19 1.22 4 11 17 3.01 1.19 -4 -11 -17 1.04 0.70 4 11 18 13.62 2.26 4 11 18 10.49 1.88 -4 -11 -18 14.94 2.37 4 11 19 0.14 0.77 -4 -11 -19 1.23 1.07 -4 -11 -20 4.73 1.61 -4 -12 18 3.94 1.55 -4 -12 18 3.94 1.97 -4 -12 17 0.28 1.05 4 12 -17 0.93 0.93 -4 -12 17 1.37 1.29 -4 -12 16 76.57 5.67 -4 -12 16 70.10 5.40 4 12 -16 69.39 5.33 4 12 -15 24.48 3.09 -4 -12 15 27.11 3.29 -4 -12 15 26.71 3.28 4 12 -14 -0.36 1.08 -4 -12 14 0.96 1.06 -4 -12 14 2.20 1.14 4 12 -13 3.60 0.88 -4 -12 13 3.48 0.99 -4 -12 13 5.43 1.47 -4 -12 12 27.30 3.10 4 12 -12 26.17 3.01 -4 -12 12 26.58 3.10 4 12 -11 7.63 1.67 -4 -12 11 5.46 1.37 -4 -12 11 4.83 1.40 4 12 -10 -1.24 0.86 -4 -12 10 -1.53 1.11 -4 -12 10 0.53 0.81 4 12 -9 8.39 1.67 -4 -12 9 10.74 1.81 -4 -12 9 9.00 1.73 4 12 -8 -1.06 0.84 -4 -12 8 0.54 0.58 -4 -12 8 0.25 0.59 -4 -12 7 210.49 8.20 -4 -12 7 203.68 7.82 4 12 -7 218.06 8.41 4 12 -6 4.17 0.92 4 12 -6 4.80 1.18 -4 -12 6 4.50 1.15 -4 -12 6 4.98 1.09 4 12 -5 2.71 0.92 4 12 -5 1.30 0.64 -4 -12 5 2.97 1.00 -4 -12 5 3.40 1.01 4 12 -4 29.80 2.89 4 12 -4 27.11 2.37 -4 -12 4 32.24 2.89 -4 -12 4 31.26 2.76 4 12 -3 15.87 2.01 -4 -12 3 16.17 1.96 4 12 -3 10.43 1.58 -4 -12 3 14.18 1.85 -4 -12 2 259.54 8.78 -4 -12 2 263.02 8.42 4 12 -2 263.43 8.32 4 12 -2 257.44 8.81 4 12 -1 26.41 2.57 -4 -12 1 28.87 2.65 4 12 -1 27.87 2.56 -4 -12 1 29.55 2.53 4 12 0 2.43 0.89 -4 -12 0 3.56 1.09 4 12 0 1.19 0.70 -4 -12 0 1.37 0.68 -4 -12 -1 9.97 1.72 4 12 1 10.94 1.57 -4 -12 -1 11.64 1.62 4 12 1 11.32 1.67 -4 -12 -2 -0.57 0.72 4 12 2 0.18 0.53 -4 -12 -2 0.39 0.47 4 12 2 -0.38 0.73 -4 -12 -3 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0.99 4 13 -4 6.59 1.38 -4 -13 4 4.00 1.15 -4 -13 4 3.55 1.07 4 13 -3 5.55 1.31 -4 -13 3 7.06 1.46 4 13 -3 4.74 1.13 -4 -13 3 3.41 1.13 4 13 -2 4.75 1.16 -4 -13 2 2.11 0.85 4 13 -2 4.21 1.07 -4 -13 2 3.34 1.11 4 13 -1 70.70 4.21 -4 -13 1 76.26 4.65 -4 -13 1 77.88 4.40 4 13 -1 73.80 4.52 4 13 0 9.65 1.64 -4 -13 0 8.88 1.61 4 13 0 9.63 1.56 -4 -13 0 13.25 1.76 4 13 1 121.68 5.73 -4 -13 -1 117.72 5.48 -4 -13 -1 131.56 6.17 4 13 1 123.39 5.84 -4 -13 -2 39.10 3.27 4 13 2 43.36 3.40 -4 -13 -2 41.76 3.14 4 13 2 40.49 3.25 -4 -13 -3 -0.25 0.65 4 13 3 1.12 0.65 -4 -13 -3 0.09 0.53 4 13 3 0.26 0.63 4 13 4 53.19 3.79 -4 -13 -4 45.75 3.29 -4 -13 -4 48.89 3.39 4 13 4 48.23 3.45 -4 -13 -4 44.09 3.45 -4 -13 -5 73.73 4.59 4 13 5 80.02 4.80 -4 -13 -5 85.65 4.51 -4 -13 -5 80.73 4.39 4 13 5 78.53 4.44 4 13 6 50.44 3.75 -4 -13 -6 44.24 3.23 -4 -13 -6 50.02 3.40 -4 -13 -6 47.85 3.67 4 13 7 114.18 5.92 -4 -13 -7 117.62 5.26 -4 -13 -7 117.52 5.43 -4 -13 -7 116.36 5.90 -4 -13 -8 27.51 2.78 -4 -13 -8 21.52 2.20 4 13 8 29.85 3.01 -4 -13 -8 25.54 2.51 -4 -13 -9 105.39 5.24 4 13 9 107.49 5.91 -4 -13 -9 103.50 5.68 4 13 10 5.72 1.47 -4 -13 -10 2.21 0.89 -4 -13 -10 3.74 1.24 -4 -13 -11 31.25 3.18 4 13 11 29.60 3.18 -4 -13 -11 24.01 2.53 -4 -13 -12 15.46 2.25 4 13 12 15.11 2.36 -4 -13 -12 12.20 1.90 4 13 13 9.49 1.89 -4 -13 -13 7.40 1.58 -4 -13 -13 8.95 1.87 4 13 14 1.22 1.06 -4 -13 -14 -1.83 1.25 4 13 15 29.46 3.35 -4 -13 -15 29.55 3.35 4 13 16 31.43 3.51 -4 -13 -16 27.74 3.17 4 13 17 12.66 2.23 -4 -13 -17 13.50 2.43 4 13 18 19.72 2.94 -4 -13 -18 17.97 2.89 -4 -13 -19 71.30 5.67 4 14 -15 2.03 1.25 -4 -14 15 -0.52 1.30 -4 -14 15 0.87 1.37 4 14 -14 -1.05 1.07 -4 -14 14 -0.46 0.93 -4 -14 14 0.09 0.93 4 14 -13 2.83 1.29 -4 -14 13 4.49 1.60 -4 -14 13 2.99 1.47 -4 -14 12 139.32 7.56 -4 -14 12 127.82 7.16 4 14 -12 129.85 7.34 4 14 -11 -0.04 0.84 -4 -14 11 -1.48 1.20 -4 -14 11 0.58 0.81 4 14 -10 13.88 2.35 -4 -14 10 14.28 2.35 -4 -14 10 13.63 2.25 4 14 -9 3.01 1.21 -4 -14 9 2.32 1.13 -4 -14 9 0.70 0.73 4 14 -8 2.84 1.10 -4 -14 8 4.79 1.44 -4 -14 8 2.87 1.10 -4 -14 7 30.62 3.34 -4 -14 7 32.67 3.24 4 14 -7 35.40 3.52 -4 -14 6 4.55 1.28 -4 -14 6 3.58 1.14 4 14 -6 1.60 0.77 -4 -14 5 59.15 4.41 -4 -14 5 58.80 4.21 4 14 -5 63.61 4.57 4 14 -4 -0.38 0.83 4 14 -4 -0.08 0.68 -4 -14 4 1.00 0.98 -4 -14 4 0.36 0.63 4 14 -3 2.06 1.09 -4 -14 3 4.71 1.36 4 14 -3 0.78 0.54 -4 -14 3 2.41 0.92 4 14 -2 1.77 0.83 -4 -14 2 2.01 0.96 4 14 -2 2.70 1.04 -4 -14 2 0.82 0.68 4 14 -1 34.52 3.20 -4 -14 1 34.28 3.25 4 14 -1 36.04 3.14 -4 -14 1 40.91 3.36 4 14 0 0.60 0.70 -4 -14 0 -0.50 0.69 4 14 0 -0.08 0.59 -4 -14 0 0.76 0.81 -4 -14 -1 51.99 3.99 4 14 1 57.27 3.97 -4 -14 -1 51.15 3.68 4 14 1 56.46 4.00 -4 -14 -2 84.69 5.09 4 14 2 85.19 4.94 -4 -14 -2 76.66 4.52 4 14 2 89.10 5.00 -4 -14 -3 21.50 2.56 4 14 3 23.93 2.60 -4 -14 -3 24.59 2.53 4 14 3 22.69 2.48 -4 -14 -4 0.88 0.81 4 14 4 3.41 1.20 -4 -14 -4 3.53 1.15 -4 -14 -4 3.68 1.06 4 14 4 2.31 0.95 -4 -14 -5 4.28 1.31 4 14 5 6.38 1.36 -4 -14 -5 3.45 1.01 4 14 5 2.53 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46.22 4.33 -5 13 12 56.56 4.76 5 -13 -11 -0.31 1.03 -5 13 11 0.42 1.11 5 -13 -10 44.76 4.12 -5 13 10 41.45 4.00 -5 13 9 0.06 0.84 5 -13 -9 -1.37 1.08 -5 13 8 38.32 3.69 5 -13 -8 37.67 3.73 -5 13 7 146.02 7.21 5 -13 -7 129.33 6.86 -5 13 6 158.33 7.41 5 -13 -6 137.79 7.11 -5 13 5 10.43 1.94 5 -13 -5 8.79 1.86 -5 13 4 11.54 2.09 5 -13 -4 8.27 1.78 -5 13 3 40.93 3.57 5 -13 -3 36.05 3.44 -5 13 2 81.88 5.00 5 -13 -2 83.40 5.19 -5 13 1 61.15 4.25 5 -13 -1 73.68 4.87 -5 13 0 10.11 1.71 -5 13 0 6.51 1.40 5 -13 0 6.54 1.60 -5 13 -1 222.03 8.29 -5 13 -1 245.63 8.68 5 -13 1 256.24 9.58 -5 13 -2 10.74 1.78 5 -13 2 10.47 1.84 -5 13 -3 19.73 2.40 5 -13 3 19.76 2.61 -5 13 -4 74.44 4.91 5 -13 4 84.03 5.35 -5 13 -5 31.20 3.32 5 -13 5 31.14 3.21 -5 13 -6 1.69 0.99 5 -13 6 0.14 0.99 -5 13 -7 16.34 2.41 5 -13 7 23.18 2.92 -5 13 -8 11.97 2.16 5 -13 8 11.53 2.04 -5 13 -9 3.20 1.20 5 -13 9 4.76 1.51 -5 13 -10 6.63 1.73 5 -13 10 8.35 1.79 -5 13 -11 18.14 2.78 -5 13 -12 8.44 1.90 -5 13 -13 4.73 1.60 5 -12 -17 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7 -14 13.89 2.06 -7 -7 13 46.20 3.71 -7 -7 13 49.34 3.76 7 7 -13 42.38 3.54 -7 -7 12 50.67 3.80 -7 -7 12 49.93 3.18 7 7 -12 52.82 3.88 -7 -7 12 54.00 3.70 -7 -7 11 56.32 3.83 -7 -7 11 58.19 3.78 7 7 -11 44.29 3.28 7 7 -11 55.18 3.90 -7 -7 10 4.05 1.05 -7 -7 10 3.88 0.97 7 7 -10 2.37 0.77 7 7 -10 5.07 1.34 -7 -7 9 0.78 0.57 -7 -7 9 1.38 0.76 -7 -7 9 0.33 0.51 7 7 -9 -0.12 0.55 7 7 -9 0.35 0.68 -7 -7 8 30.05 2.56 7 7 -8 27.44 2.07 -7 -7 8 30.32 2.41 -7 -7 8 30.39 2.14 7 7 -8 27.59 2.52 7 7 -8 32.20 2.88 -7 -7 7 239.27 7.68 -7 -7 7 255.26 8.30 7 7 -7 218.21 6.56 -7 -7 7 239.16 7.20 7 7 -7 241.07 8.30 7 7 -7 235.29 7.84 -7 -7 6 1.50 0.58 -7 -7 6 2.03 0.55 7 7 -6 1.02 0.47 -7 -7 6 2.15 0.54 7 7 -6 2.05 0.71 7 7 -6 1.93 0.71 -7 -7 5 327.15 8.94 -7 -7 5 332.58 9.72 7 7 -5 327.71 8.20 -7 -7 5 315.52 8.16 7 7 -5 330.89 9.88 7 7 -5 313.86 9.36 -7 -7 4 30.34 2.58 -7 -7 4 28.95 2.24 7 7 -4 27.41 1.95 -7 -7 4 29.12 1.97 7 7 -4 27.50 2.52 7 7 -4 27.63 2.43 -7 -7 3 344.57 8.93 -7 -7 3 324.30 7.84 7 7 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645.47 16.66 8 -4 -7 0.11 0.57 -8 4 7 0.90 0.46 8 -4 -7 1.28 0.77 -8 4 7 0.45 0.67 -8 4 6 239.08 6.89 8 -4 -6 242.81 7.43 -8 4 6 237.01 8.33 8 -4 -6 253.28 8.96 8 -4 -5 15.22 1.66 -8 4 5 16.58 1.68 8 -4 -5 18.44 2.20 -8 4 5 15.56 2.01 8 -4 -4 1.41 0.60 -8 4 4 2.15 0.77 8 -4 -4 0.15 0.70 -8 4 4 0.86 0.58 8 -4 -3 23.92 1.92 -8 4 3 23.97 2.05 8 -4 -3 24.69 2.58 -8 4 3 24.77 2.42 -8 4 2 151.98 5.57 8 -4 -2 151.59 5.11 -8 4 2 150.59 6.23 8 -4 -2 151.94 6.58 8 -4 -1 25.10 1.88 -8 4 1 26.51 2.26 8 -4 -1 27.30 2.67 -8 4 1 25.96 2.45 8 -4 0 729.10 14.56 -8 4 0 748.35 16.75 8 -4 0 755.26 17.44 -8 4 0 752.99 16.11 -8 4 -1 11.41 1.54 8 -4 1 8.46 1.02 8 -4 1 9.77 1.64 -8 4 -1 13.34 1.74 -8 4 -2 75.30 4.12 8 -4 2 69.73 4.31 -8 4 -2 65.61 3.83 -8 4 -3 2.66 0.90 8 -4 3 2.05 0.68 -8 4 -3 2.47 0.82 -8 4 -4 14.91 1.93 8 -4 4 16.02 2.07 -8 4 -4 16.29 1.91 -8 4 -5 87.41 4.35 8 -4 5 84.12 4.80 -8 4 -5 81.96 4.57 -8 4 -6 24.68 2.56 8 -4 6 22.14 2.49 -8 4 -6 27.91 2.40 -8 4 -7 16.23 2.12 8 -4 7 15.56 2.08 -8 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9 23.14 2.28 -8 -2 -10 287.07 9.20 8 2 10 277.34 9.49 8 2 10 284.28 9.01 -8 -2 -11 3.13 1.01 8 2 11 2.32 0.85 8 2 11 1.58 0.73 -8 -2 -12 169.68 6.96 8 2 12 176.58 7.51 8 2 12 161.88 6.55 -8 -2 -13 27.32 2.80 8 2 13 29.32 3.01 8 2 13 29.94 2.66 8 2 14 62.29 4.54 8 2 14 54.12 3.67 -8 -2 -14 62.61 4.21 8 2 15 182.28 8.24 -8 -2 -15 193.01 7.90 -8 -2 -16 3.13 1.09 8 2 16 1.52 0.99 -8 -2 -17 18.67 2.44 8 2 17 16.34 2.51 8 2 18 164.86 8.31 -8 -2 -18 168.27 7.75 8 2 19 11.47 2.25 8 2 20 3.35 1.32 8 2 21 1.54 1.20 8 3 -18 10.91 2.04 -8 -3 18 7.25 1.78 -8 -3 17 5.91 1.67 8 3 -17 6.80 1.57 -8 -3 17 8.81 1.84 -8 -3 17 5.92 1.49 -8 -3 16 77.35 4.90 8 3 -16 81.25 5.02 -8 -3 16 88.24 5.32 -8 -3 16 84.73 5.09 -8 -3 15 3.94 1.23 8 3 -15 5.65 1.54 -8 -3 15 2.91 0.89 -8 -3 15 3.78 1.18 -8 -3 15 4.55 1.23 -8 -3 14 2.18 0.82 8 3 -14 3.78 1.11 -8 -3 14 3.28 0.91 -8 -3 14 4.22 1.13 -8 -3 14 4.70 1.30 -8 -3 13 1.30 0.60 8 3 -13 2.41 0.88 -8 -3 13 1.76 0.86 -8 -3 13 0.56 0.47 -8 -3 13 1.18 0.83 -8 -3 13 1.89 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2.89 -8 -4 -4 6.95 1.28 8 4 4 5.64 1.21 8 4 4 4.51 1.09 8 4 5 -0.28 0.53 -8 -4 -5 1.24 0.72 8 4 5 -0.55 0.63 8 4 6 0.65 0.52 -8 -4 -6 1.70 0.72 8 4 6 1.34 0.70 8 4 7 3.05 0.90 -8 -4 -7 4.12 1.08 8 4 7 3.02 0.91 -8 -4 -8 212.95 7.50 8 4 8 204.50 7.57 8 4 8 202.07 7.49 8 4 9 -0.09 0.68 8 4 9 -0.25 0.64 -8 -4 -9 -0.71 0.70 8 4 10 1.32 0.72 8 4 10 1.77 0.79 -8 -4 -10 1.60 0.71 8 4 11 3.98 1.02 8 4 11 3.73 1.13 -8 -4 -11 5.58 1.33 8 4 12 21.49 2.39 -8 -4 -12 28.48 2.74 8 4 12 26.14 2.77 8 4 13 11.22 1.73 -8 -4 -13 10.19 1.70 8 4 13 12.00 1.88 8 4 14 7.36 1.45 -8 -4 -14 7.64 1.36 8 4 14 6.25 1.43 8 4 15 0.48 0.56 -8 -4 -15 0.14 0.64 8 4 15 0.14 0.56 8 4 16 55.33 4.45 -8 -4 -16 58.44 4.24 -8 -4 -17 1.24 0.78 8 4 17 2.04 1.23 8 4 18 180.56 8.72 8 4 19 4.49 1.63 8 4 20 7.87 2.01 8 4 21 6.01 1.99 -8 -5 17 0.66 0.96 -8 -5 17 -0.74 0.90 -8 -5 16 13.94 2.15 -8 -5 16 16.27 2.40 -8 -5 15 3.59 1.28 -8 -5 15 5.00 1.30 -8 -5 14 0.98 0.74 -8 -5 14 0.03 0.64 -8 -5 14 1.28 0.77 -8 -5 14 1.67 0.79 -8 -5 13 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4.31 -8 -7 4 103.65 5.14 8 7 -4 99.21 5.12 -8 -7 3 70.05 3.55 -8 -7 3 74.67 4.33 8 7 -3 69.65 3.53 8 7 -3 67.38 4.15 -8 -7 2 0.38 0.41 -8 -7 2 0.96 0.62 8 7 -2 0.37 0.39 8 7 -2 -0.22 0.41 8 7 -1 17.72 2.13 -8 -7 1 17.00 2.00 -8 -7 1 18.49 1.71 8 7 -1 17.34 1.70 -8 -7 0 93.34 3.97 -8 -7 0 91.56 4.77 8 7 0 87.03 4.10 8 7 0 89.84 4.84 8 7 1 0.24 0.51 -8 -7 -1 -0.24 0.50 8 7 1 0.42 0.41 -8 -7 -1 1.11 0.75 -8 -7 -2 821.20 16.23 -8 -7 -2 814.01 18.18 8 7 2 796.00 17.01 8 7 2 838.72 18.71 8 7 3 18.84 2.23 -8 -7 -3 20.15 1.78 -8 -7 -3 21.60 2.31 8 7 3 20.09 1.98 8 7 4 18.22 2.26 -8 -7 -4 20.92 1.79 -8 -7 -4 22.09 2.28 8 7 4 20.31 2.08 -8 -7 -5 6.62 0.94 8 7 5 6.93 1.47 8 7 5 7.64 1.29 -8 -7 -5 4.49 1.03 -8 -7 -6 15.50 1.55 8 7 6 17.00 2.18 8 7 6 13.93 1.79 -8 -7 -6 17.88 2.08 8 7 7 31.98 2.95 -8 -7 -7 35.39 2.96 8 7 7 33.64 2.80 -8 -7 -7 36.28 2.51 8 7 8 23.09 2.61 -8 -7 -8 27.29 2.61 8 7 8 24.64 2.48 -8 -7 -8 20.24 1.90 8 7 9 32.35 3.08 -8 -7 -9 31.95 2.89 8 7 9 29.74 2.76 -8 -7 -9 28.41 2.30 -8 -7 -10 171.85 6.81 8 7 10 160.72 6.75 8 7 10 165.51 7.06 8 7 11 2.78 1.06 -8 -7 -11 2.16 0.97 8 7 11 1.00 0.49 -8 -7 -11 0.29 0.51 8 7 12 3.28 1.12 8 7 12 1.81 0.95 -8 -7 -12 3.33 1.07 -8 -7 -12 0.61 0.50 8 7 13 25.18 2.81 8 7 13 23.84 2.74 -8 -7 -13 26.87 2.70 8 7 14 5.19 1.40 -8 -7 -14 5.58 1.37 8 7 14 6.88 1.67 8 7 15 4.13 1.28 -8 -7 -15 6.94 1.64 8 7 15 5.55 1.56 8 7 16 14.40 2.26 8 7 16 22.11 2.77 8 7 17 0.15 0.93 8 7 18 157.28 8.15 8 7 19 3.30 1.46 -8 -8 16 14.37 2.32 -8 -8 15 0.73 0.94 -8 -8 15 -0.77 1.25 -8 -8 14 58.81 4.43 -8 -8 14 61.83 4.42 -8 -8 14 58.83 4.36 8 8 -14 58.14 4.55 -8 -8 13 63.55 4.49 -8 -8 13 67.91 4.66 -8 -8 13 53.52 4.01 8 8 -13 64.96 4.68 -8 -8 12 32.60 3.12 -8 -8 12 30.86 2.94 8 8 -12 26.96 3.01 -8 -8 12 34.38 3.21 -8 -8 11 5.38 1.46 -8 -8 11 4.72 1.21 -8 -8 11 4.14 1.25 8 8 -11 4.92 1.40 -8 -8 10 0.77 0.73 -8 -8 10 -1.20 0.89 8 8 -10 -0.09 0.55 -8 -8 10 0.64 0.70 8 8 -10 0.91 0.72 -8 -8 9 41.34 3.23 -8 -8 9 41.04 3.40 -8 -8 9 35.58 2.81 8 8 -9 41.96 3.32 8 8 -9 35.72 3.28 -8 -8 8 229.00 8.08 -8 -8 8 247.57 8.85 -8 -8 8 237.85 7.63 8 8 -8 241.52 8.98 8 8 -8 233.13 8.42 -8 -8 7 173.30 7.13 -8 -8 7 163.81 6.44 -8 -8 7 150.49 5.71 8 8 -7 153.74 6.92 8 8 -7 149.71 6.56 -8 -8 6 126.41 5.46 -8 -8 6 123.23 4.86 8 8 -6 124.32 6.10 8 8 -6 121.46 5.80 -8 -8 6 130.12 6.08 -8 -8 5 78.99 4.16 -8 -8 5 75.71 3.59 8 8 -5 78.82 4.62 -8 -8 5 82.98 4.77 -8 -8 4 9.98 1.47 -8 -8 4 11.80 1.78 8 8 -4 10.79 1.77 -8 -8 3 79.84 4.03 8 8 -3 79.10 3.75 -8 -8 3 84.70 4.76 8 8 -3 84.12 4.72 8 8 -2 5.63 1.26 -8 -8 2 5.46 1.09 -8 -8 2 6.14 1.36 8 8 -2 6.49 1.06 -8 -8 1 44.78 2.87 -8 -8 1 43.58 3.37 8 8 -1 40.81 2.67 8 8 -1 43.07 3.37 -8 -8 0 193.89 6.36 -8 -8 0 195.20 7.38 8 8 0 173.16 6.05 8 8 0 185.36 7.44 -8 -8 -1 116.86 4.67 -8 -8 -1 101.39 5.19 8 8 1 97.77 4.37 8 8 1 103.99 5.41 8 8 2 0.91 0.56 -8 -8 -2 -1.24 0.73 8 8 2 0.36 0.41 -8 -8 -2 0.17 0.47 8 8 3 16.92 2.13 -8 -8 -3 19.76 1.88 -8 -8 -3 22.30 2.36 8 8 3 16.36 1.79 -8 -8 -4 85.68 4.70 8 8 4 76.18 3.96 8 8 4 80.63 4.78 -8 -8 -4 75.54 3.76 -8 -8 -5 20.14 1.88 8 8 5 24.12 2.66 -8 -8 -5 20.21 2.27 8 8 5 21.23 2.12 -8 -8 -6 23.64 2.05 8 8 6 23.81 2.60 8 8 6 26.35 2.42 -8 -8 -6 26.80 2.58 -8 -8 -7 3.85 0.97 8 8 7 4.90 1.32 8 8 7 4.43 1.02 -8 -8 -7 4.94 1.25 -8 -8 -8 1.25 0.53 8 8 8 2.02 0.98 -8 -8 -8 1.07 0.49 8 8 8 0.18 0.55 8 8 9 20.97 2.57 -8 -8 -9 19.81 2.28 8 8 9 19.65 2.28 -8 -8 -9 18.50 1.88 8 8 10 14.99 2.16 -8 -8 -10 14.27 2.02 8 8 10 13.47 1.86 -8 -8 -10 14.24 1.75 8 8 11 8.69 1.64 -8 -8 -11 9.60 1.64 8 8 11 8.45 1.62 -8 -8 -11 8.85 1.48 -8 -8 -12 258.75 8.98 8 8 12 254.59 9.20 -8 -8 -12 225.75 7.95 8 8 12 267.64 9.69 8 8 13 3.04 1.19 8 8 13 1.33 0.86 -8 -8 -13 2.93 0.91 -8 -8 -13 0.89 0.65 -8 -8 -14 110.96 5.70 8 8 14 100.51 5.83 8 8 14 98.01 5.79 8 8 15 38.86 3.62 -8 -8 -15 36.31 3.29 8 8 15 37.37 3.61 8 8 16 14.62 2.34 8 8 16 17.31 2.64 8 8 17 11.68 2.27 8 8 18 16.77 2.79 -8 -9 15 0.12 1.01 -8 -9 14 0.32 0.86 8 9 -14 0.19 0.88 -8 -9 13 0.82 0.88 8 9 -13 0.02 0.87 -8 -9 12 2.34 0.96 -8 -9 12 2.52 1.04 8 9 -12 2.69 0.95 -8 -9 11 2.18 1.09 -8 -9 11 4.37 1.31 -8 -9 11 1.69 0.71 8 9 -11 2.20 1.14 -8 -9 10 -0.86 1.06 -8 -9 10 0.81 0.85 -8 -9 10 0.68 0.69 8 9 -10 0.05 0.96 -8 -9 9 4.40 1.26 -8 -9 9 3.11 1.31 -8 -9 9 3.39 1.02 8 9 -9 3.58 1.29 8 9 -9 3.08 1.02 -8 -9 8 90.46 4.96 -8 -9 8 99.17 5.52 -8 -9 8 89.34 4.55 8 9 -8 97.26 5.68 8 9 -8 98.06 5.23 -8 -9 7 9.35 1.55 -8 -9 7 7.51 1.65 -8 -9 7 7.79 1.38 8 9 -7 7.68 1.62 8 9 -7 5.92 1.30 -8 -9 6 1.57 0.80 -8 -9 6 0.50 0.44 -8 -9 6 0.59 0.73 8 9 -6 0.20 0.56 8 9 -6 0.93 0.71 -8 -9 5 24.91 2.42 -8 -9 5 22.20 2.51 8 9 -5 23.84 2.67 8 9 -5 24.11 2.57 -8 -9 4 10.81 1.57 -8 -9 4 9.15 1.57 8 9 -4 8.17 1.57 -8 -9 3 200.89 7.01 -8 -9 3 203.81 7.93 8 9 -3 190.57 7.61 -8 -9 2 58.46 3.53 -8 -9 2 66.70 4.31 8 9 -2 64.41 4.17 -8 -9 1 77.34 4.08 -8 -9 1 84.74 4.83 8 9 -1 75.54 4.62 8 9 0 3.06 1.13 -8 -9 0 5.81 1.14 -8 -9 0 4.21 1.13 -8 -9 -1 24.94 2.53 8 9 1 27.86 2.87 -8 -9 -1 27.58 2.33 8 9 2 11.38 1.84 -8 -9 -2 9.37 1.34 8 9 2 8.16 1.24 -8 -9 -2 9.03 1.54 8 9 3 21.90 2.57 -8 -9 -3 23.92 2.16 -8 -9 -3 27.26 2.70 8 9 3 20.34 1.98 -8 -9 -4 153.44 6.60 8 9 4 122.57 5.29 8 9 4 153.69 6.85 -8 -9 -4 153.46 5.81 -8 -9 -5 21.11 2.06 8 9 5 22.67 2.56 -8 -9 -5 25.49 2.61 8 9 5 18.08 1.98 8 9 6 174.49 6.61 -8 -9 -6 203.87 7.72 8 9 6 188.79 7.77 -8 -9 -6 189.29 6.70 8 9 7 53.41 3.56 -8 -9 -7 61.57 4.11 8 9 7 57.51 4.17 -8 -9 -7 61.83 3.64 8 9 8 62.94 3.98 -8 -9 -8 73.32 4.44 -8 -9 -8 65.11 3.79 8 9 8 55.45 4.16 -8 -9 -9 2.10 0.83 8 9 9 1.18 0.81 -8 -9 -9 1.61 0.87 8 9 9 1.46 0.87 -8 -9 -10 105.81 5.47 8 9 10 84.16 4.91 -8 -9 -10 94.26 4.79 8 9 10 92.71 5.55 8 9 11 12.44 2.05 -8 -9 -11 12.75 1.92 8 9 11 11.29 1.85 -8 -9 -11 10.35 1.68 -8 -9 -12 217.98 8.28 8 9 12 191.46 7.97 -8 -9 -12 190.28 7.38 8 9 12 216.85 8.78 8 9 13 26.40 2.97 8 9 13 29.00 3.06 -8 -9 -13 28.93 2.80 -8 -9 -13 29.79 2.93 -8 -9 -14 288.87 9.86 8 9 14 274.89 10.31 8 9 14 287.93 10.65 8 9 15 31.85 3.40 8 9 15 38.62 3.74 8 9 16 1.34 0.99 8 9 16 2.34 1.27 8 9 17 7.91 1.81 -8 -10 14 21.46 2.88 8 10 -14 23.81 3.15 -8 -10 13 11.72 2.15 8 10 -13 10.14 2.20 -8 -10 12 24.05 2.94 8 10 -12 22.94 2.98 -8 -10 11 0.86 0.74 8 10 -11 1.17 0.88 -8 -10 10 -0.61 0.96 8 10 -10 0.14 0.82 -8 -10 9 0.86 0.70 -8 -10 9 -0.47 0.86 8 10 -9 0.57 0.64 -8 -10 8 28.63 2.87 -8 -10 8 33.36 3.23 8 10 -8 31.61 3.29 8 10 -8 29.88 2.89 -8 -10 7 5.07 1.26 -8 -10 7 7.56 1.61 8 10 -7 5.42 1.48 8 10 -7 4.77 1.27 -8 -10 6 11.75 1.72 -8 -10 6 10.92 1.85 8 10 -6 8.28 1.80 8 10 -6 9.43 1.66 -8 -10 5 3.53 1.07 -8 -10 5 2.75 1.13 8 10 -5 2.18 0.87 8 10 -5 1.90 0.90 -8 -10 4 16.23 1.94 -8 -10 4 15.14 2.17 8 10 -4 15.44 2.27 8 10 -4 15.25 2.09 -8 -10 3 44.14 3.26 -8 -10 3 47.48 3.74 8 10 -3 43.87 3.57 8 10 -2 -0.87 0.80 -8 -10 2 -0.83 0.81 -8 -10 2 0.89 0.64 -8 -10 1 52.19 3.49 -8 -10 1 44.21 3.59 8 10 -1 48.57 3.78 8 10 0 18.97 2.34 -8 -10 0 22.27 2.26 -8 -10 0 17.01 2.14 -8 -10 -1 140.29 5.83 -8 -10 -1 140.35 6.49 8 10 1 143.42 6.68 -8 -10 -2 89.94 4.55 -8 -10 -2 93.00 5.16 8 10 2 88.59 5.21 8 10 3 20.44 2.51 -8 -10 -3 16.28 1.89 -8 -10 -3 22.95 2.54 -8 -10 -4 1.17 0.69 8 10 4 2.54 1.24 -8 -10 -4 1.21 0.85 -8 -10 -5 9.91 1.58 8 10 5 7.76 1.51 -8 -10 -5 10.90 1.80 -8 -10 -6 1.97 0.94 8 10 6 3.24 1.15 -8 -10 -6 3.31 1.08 -8 -10 -7 4.53 1.03 -8 -10 -7 5.99 1.40 8 10 7 4.63 1.18 8 10 7 5.02 1.17 8 10 8 36.97 3.49 8 10 8 34.19 2.90 -8 -10 -8 39.96 3.31 -8 -10 -8 40.33 3.11 -8 -10 -9 5.83 1.31 8 10 9 6.64 1.66 -8 -10 -9 4.21 1.19 8 10 9 4.34 1.09 8 10 10 18.70 2.61 -8 -10 -10 17.02 2.28 8 10 10 16.79 2.17 -8 -10 -10 16.28 2.06 -8 -10 -11 58.31 4.13 8 10 11 51.77 3.89 -8 -10 -11 51.93 3.80 8 10 11 58.84 4.49 8 10 12 43.60 3.96 -8 -10 -12 44.66 3.58 8 10 12 39.15 3.46 -8 -10 -12 43.24 3.51 -8 -10 -13 34.23 3.16 8 10 13 41.68 3.88 8 10 13 39.20 3.53 8 10 14 143.00 7.09 8 10 14 159.96 7.83 8 10 15 4.15 1.47 8 10 16 32.44 3.54 -8 -11 13 3.43 1.28 8 11 -13 4.01 1.58 -8 -11 12 18.81 2.57 8 11 -12 16.34 2.58 -8 -11 11 22.52 2.84 8 11 -11 18.07 2.73 -8 -11 10 176.94 7.95 8 11 -10 179.25 8.45 -8 -11 9 71.69 4.83 8 11 -9 70.55 5.11 -8 -11 8 28.21 2.96 -8 -11 8 25.07 2.98 8 11 -8 28.53 3.25 -8 -11 7 4.73 1.25 -8 -11 7 4.52 1.29 8 11 -7 4.49 1.38 8 11 -7 2.60 1.08 -8 -11 6 18.39 2.30 -8 -11 6 16.89 2.45 8 11 -6 14.12 2.25 8 11 -6 16.98 2.25 -8 -11 5 0.30 0.69 -8 -11 5 0.81 0.83 8 11 -5 1.64 1.13 8 11 -5 -0.11 0.77 8 11 -4 22.89 2.56 -8 -11 4 20.66 2.34 -8 -11 4 22.15 2.65 8 11 -4 27.64 3.10 8 11 -3 -0.51 0.66 -8 -11 3 -0.66 0.98 -8 -11 3 0.71 0.71 8 11 -3 -1.01 1.04 -8 -11 2 144.60 6.38 -8 -11 2 153.20 7.09 8 11 -2 150.02 6.90 8 11 -1 9.08 1.70 -8 -11 1 11.30 1.74 -8 -11 1 10.76 1.85 8 11 0 17.44 2.30 -8 -11 0 22.44 2.34 -8 -11 0 15.45 2.08 -8 -11 -1 41.76 3.18 8 11 1 37.13 3.39 -8 -11 -1 40.96 3.49 8 11 2 1.54 0.97 -8 -11 -2 0.84 0.54 -8 -11 -2 1.10 0.64 -8 -11 -3 3.78 0.83 8 11 3 1.52 0.88 -8 -11 -3 4.11 1.21 -8 -11 -4 18.58 2.14 8 11 4 18.12 2.54 -8 -11 -4 20.90 2.53 -8 -11 -5 5.77 1.25 8 11 5 6.01 1.50 -8 -11 -5 5.18 1.40 -8 -11 -6 98.55 5.52 8 11 6 93.44 5.69 -8 -11 -6 101.89 5.16 -8 -11 -7 3.71 1.01 8 11 7 8.34 1.76 -8 -11 -7 4.18 1.26 -8 -11 -8 40.21 3.27 8 11 8 42.87 3.85 -8 -11 -8 37.16 3.36 -8 -11 -9 5.81 1.33 8 11 9 6.76 1.53 -8 -11 -9 5.37 1.29 -8 -11 -10 1.97 0.68 8 11 10 4.61 1.41 -8 -11 -10 3.77 1.16 8 11 11 4.94 1.38 -8 -11 -11 3.90 1.39 -8 -11 -11 4.11 1.26 8 11 12 0.05 0.76 -8 -11 -12 1.20 0.83 -8 -11 -12 -0.58 0.93 8 11 13 6.05 1.64 8 11 14 3.94 1.44 8 11 15 0.08 0.80 8 11 16 20.63 2.98 8 12 -13 5.91 2.04 -8 -12 12 2.36 0.94 8 12 -12 4.04 1.66 -8 -12 11 14.49 2.24 8 12 -11 13.53 2.41 -8 -12 10 185.37 8.44 8 12 -10 196.97 9.19 -8 -12 9 39.55 3.65 8 12 -9 40.63 4.09 -8 -12 8 2.65 1.08 -8 -12 8 3.05 1.24 8 12 -8 3.95 1.49 -8 -12 7 0.89 0.89 -8 -12 7 -1.05 0.98 8 12 -7 1.95 1.00 -8 -12 6 10.38 1.94 -8 -12 6 6.97 1.47 8 12 -6 8.68 1.96 8 12 -6 8.87 1.68 -8 -12 5 40.97 3.48 -8 -12 5 44.03 3.90 8 12 -5 43.88 3.93 8 12 -5 38.18 3.47 8 12 -4 29.78 3.18 -8 -12 4 37.11 3.33 8 12 -4 36.27 3.62 -8 -12 4 36.20 3.56 -8 -12 3 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1.66 10 3 6 3.83 1.17 10 3 6 1.78 0.82 -10 -3 -6 3.86 1.17 10 3 7 3.50 1.29 -10 -3 -7 3.48 1.03 10 3 7 1.57 0.82 10 3 8 8.56 1.68 -10 -3 -8 14.07 2.09 10 3 8 12.91 2.07 -10 -3 -9 79.52 4.94 10 3 9 75.57 5.02 10 3 9 77.67 4.95 -10 -3 -10 23.59 2.63 10 3 10 18.24 2.44 10 3 10 18.24 2.44 -10 -3 -11 43.46 3.74 10 3 11 38.73 3.76 10 3 11 38.23 3.52 -10 -3 -12 81.33 5.21 10 3 12 77.92 5.42 10 3 12 71.12 4.86 -10 -3 -13 25.82 3.05 10 3 13 23.70 3.07 10 3 13 24.60 2.87 -10 -3 -14 29.87 3.24 10 3 14 28.90 3.45 -10 -3 -15 -0.10 1.04 10 3 15 1.28 1.18 10 3 16 80.82 5.98 -10 -3 -16 88.53 5.86 10 3 17 74.55 5.86 10 3 18 1.41 0.91 -10 -4 13 1.28 0.92 10 4 -12 29.93 3.30 -10 -4 12 40.50 3.52 -10 -4 12 40.33 3.52 -10 -4 11 2.69 1.00 10 4 -11 2.46 0.88 -10 -4 11 1.31 0.72 -10 -4 11 4.61 1.31 -10 -4 10 0.55 0.87 10 4 -10 1.78 0.93 -10 -4 10 1.22 0.58 10 4 -10 0.47 0.76 -10 -4 9 0.64 0.61 10 4 -9 1.13 0.73 -10 -4 9 1.75 0.79 10 4 -9 1.72 0.74 -10 -4 8 -0.32 0.51 10 4 -8 0.90 0.79 -10 -4 8 -1.21 1.00 10 4 -8 -0.42 0.78 -10 -4 7 3.28 1.00 10 4 -7 3.58 1.16 10 4 -7 3.58 1.22 -10 -4 6 -1.47 0.91 10 4 -6 0.27 0.61 10 4 -6 -0.42 0.74 -10 -4 5 3.15 0.93 10 4 -5 1.87 0.74 10 4 -5 3.03 1.00 -10 -4 4 -0.99 0.82 10 4 -4 1.30 0.91 10 4 -4 0.40 0.55 10 4 -3 1.39 0.74 10 4 -3 1.71 0.77 -10 -4 3 0.95 0.68 10 4 -2 128.75 6.08 -10 -4 2 130.47 6.07 10 4 -2 124.95 6.34 10 4 -1 2.68 1.07 -10 -4 1 3.74 1.13 10 4 -1 2.27 0.82 -10 -4 0 9.62 1.59 10 4 0 10.85 1.74 10 4 0 11.18 1.90 -10 -4 -1 1.31 0.53 10 4 1 1.82 0.89 10 4 1 -0.18 0.74 -10 -4 -2 93.88 5.13 10 4 2 76.15 4.71 10 4 2 88.72 5.28 -10 -4 -3 71.35 4.46 10 4 3 64.98 4.29 10 4 3 69.64 4.63 -10 -4 -4 51.88 3.82 10 4 4 50.30 3.81 10 4 4 50.10 3.91 -10 -4 -5 -1.12 0.85 10 4 5 0.25 0.58 10 4 5 -0.71 0.92 -10 -4 -6 38.22 3.36 10 4 6 37.51 3.40 10 4 6 39.17 3.49 -10 -4 -7 3.36 0.98 10 4 7 3.27 1.11 10 4 7 3.08 0.99 -10 -4 -8 188.12 7.83 10 4 8 176.64 7.71 10 4 8 174.27 7.75 -10 -4 -9 126.76 6.33 10 4 9 115.25 6.24 10 4 9 117.33 6.25 -10 -4 -10 133.88 6.60 10 4 10 128.62 6.72 10 4 10 119.90 6.38 -10 -4 -11 0.83 0.97 10 4 11 -1.12 0.93 10 4 11 0.20 0.67 -10 -4 -12 88.32 5.45 10 4 12 79.90 5.45 10 4 12 80.70 5.20 -10 -4 -13 6.43 1.52 10 4 13 6.16 1.66 10 4 13 5.49 1.40 -10 -4 -14 2.41 1.19 10 4 14 0.72 0.79 -10 -4 -15 12.95 2.31 10 4 15 11.31 2.22 -10 -4 -16 19.95 2.83 10 4 16 18.24 2.79 10 4 17 48.11 4.76 10 4 18 3.37 1.39 -10 -5 12 41.76 3.63 -10 -5 11 2.25 1.10 -10 -5 11 2.35 0.98 10 5 -11 1.30 0.91 -10 -5 10 60.69 4.25 -10 -5 10 59.78 4.30 10 5 -10 53.77 4.30 10 5 -9 13.75 1.95 -10 -5 9 14.24 1.98 -10 -5 9 13.54 2.11 10 5 -9 12.18 1.99 -10 -5 8 26.41 2.74 10 5 -8 22.61 2.48 10 5 -8 23.53 2.75 -10 -5 7 -0.56 0.78 10 5 -7 -0.41 0.69 10 5 -7 1.10 0.87 -10 -5 6 0.92 0.69 10 5 -6 0.26 0.55 10 5 -6 -1.28 0.98 -10 -5 5 0.10 0.55 10 5 -5 -0.57 0.50 10 5 -5 -0.35 0.66 10 5 -4 178.82 7.18 10 5 -4 172.87 7.73 -10 -5 4 182.82 7.46 -10 -5 3 24.90 2.66 10 5 -3 25.04 2.64 10 5 -3 25.11 2.86 10 5 -2 392.76 11.55 10 5 -2 378.71 12.22 -10 -5 2 428.39 12.12 10 5 -1 6.52 1.31 -10 -5 1 6.76 1.40 10 5 -1 6.34 1.41 10 5 0 80.41 4.63 -10 -5 0 79.05 4.74 10 5 0 77.90 4.99 10 5 1 1.56 0.63 -10 -5 -1 0.73 0.61 10 5 1 0.17 0.60 -10 -5 -2 24.62 2.64 10 5 2 22.70 2.54 10 5 2 24.16 2.72 -10 -5 -3 4.10 1.23 10 5 3 3.76 1.07 10 5 3 2.89 1.13 -10 -5 -4 0.26 0.53 10 5 4 0.45 0.63 10 5 4 0.99 0.71 -10 -5 -5 25.31 2.77 10 5 5 20.68 2.43 10 5 5 24.20 2.73 -10 -5 -6 11.74 1.87 10 5 6 14.28 2.14 10 5 6 13.36 2.06 -10 -5 -7 31.30 3.05 10 5 7 27.20 2.89 10 5 7 29.73 3.06 -10 -5 -8 -0.01 0.73 10 5 8 0.44 0.70 10 5 8 -0.04 0.56 10 5 9 4.92 1.40 -10 -5 -9 4.01 1.11 10 5 9 5.96 1.42 10 5 10 29.53 3.19 -10 -5 -10 31.09 3.13 10 5 10 31.18 3.22 10 5 11 4.78 1.43 -10 -5 -11 4.01 1.38 10 5 11 5.59 1.42 -10 -5 -12 14.97 2.33 10 5 12 13.16 2.33 10 5 12 11.64 1.99 -10 -5 -13 82.65 5.32 10 5 13 72.65 5.29 10 5 13 70.36 4.98 -10 -5 -14 28.85 3.23 10 5 14 25.92 3.31 10 5 14 27.47 3.20 -10 -5 -15 1.15 1.18 10 5 15 2.16 0.91 10 5 16 49.63 4.72 10 5 17 19.01 2.93 -10 -6 12 -1.22 0.99 -10 -6 11 2.04 0.65 10 6 -11 0.37 0.70 -10 -6 11 0.26 0.80 -10 -6 10 -0.90 0.85 10 6 -10 -0.13 0.91 -10 -6 10 0.67 0.83 10 6 -9 3.40 1.20 -10 -6 9 7.10 1.56 -10 -6 8 69.51 4.63 10 6 -8 71.01 4.91 10 6 -7 32.44 2.92 -10 -6 7 40.04 3.44 10 6 -7 37.42 3.54 10 6 -6 8.89 1.59 -10 -6 6 11.28 1.85 10 6 -6 12.24 2.04 -10 -6 5 4.81 1.34 10 6 -5 5.37 1.35 10 6 -5 5.71 1.42 -10 -6 4 0.69 0.54 10 6 -4 0.53 0.57 10 6 -4 1.05 0.68 -10 -6 3 1.16 0.82 10 6 -3 -0.07 0.65 10 6 -3 0.95 0.72 -10 -6 2 15.67 2.16 10 6 -2 15.71 2.01 10 6 -2 14.31 2.14 -10 -6 1 13.00 1.96 10 6 -1 11.60 1.75 10 6 -1 12.35 1.95 -10 -6 0 20.55 2.49 10 6 0 17.73 2.17 10 6 0 19.69 2.52 10 6 1 89.96 4.94 -10 -6 -1 90.89 5.19 10 6 1 88.12 5.35 10 6 2 129.73 6.12 -10 -6 -2 133.43 6.39 10 6 2 129.85 6.62 -10 -6 -3 12.97 1.97 10 6 3 12.34 1.91 10 6 3 12.61 2.05 -10 -6 -4 9.06 1.71 10 6 4 10.70 1.72 10 6 4 10.36 1.93 -10 -6 -5 25.29 2.81 10 6 5 25.61 2.75 10 6 5 26.01 2.97 -10 -6 -6 1.01 0.70 10 6 6 -0.01 0.68 10 6 6 0.97 0.75 -10 -6 -7 58.36 4.20 10 6 7 45.25 3.67 10 6 7 45.56 3.92 -10 -6 -8 -0.72 0.86 10 6 8 -0.26 0.73 10 6 8 -0.89 0.84 -10 -6 -9 -0.98 0.87 10 6 9 0.18 0.70 10 6 9 -0.71 0.90 10 6 10 -0.17 0.75 -10 -6 -10 -1.16 0.72 10 6 10 0.49 0.91 10 6 11 0.09 0.61 10 6 11 0.01 0.76 -10 -6 -11 -0.49 0.91 -10 -6 -12 124.50 6.55 10 6 12 118.56 6.64 10 6 12 121.72 6.69 10 6 13 17.69 2.65 -10 -6 -13 16.15 2.44 10 6 13 18.04 2.73 -10 -6 -14 41.83 3.80 10 6 14 38.94 3.93 10 6 14 33.58 3.52 -10 -6 -15 42.20 3.94 10 6 15 46.24 4.40 10 6 16 47.34 4.58 -10 -7 12 25.39 3.07 -10 -7 11 18.95 2.48 -10 -7 10 3.37 1.13 10 7 -10 3.84 1.31 -10 -7 9 0.66 0.73 10 7 -9 0.59 0.91 10 7 -8 18.46 2.58 -10 -7 8 20.73 2.54 10 7 -7 -1.14 0.86 -10 -7 7 -0.32 0.76 -10 -7 6 16.13 2.26 10 7 -6 13.02 2.13 -10 -7 5 2.20 0.95 10 7 -5 0.89 0.85 -10 -7 4 74.91 4.84 10 7 -4 73.80 4.99 -10 -7 3 2.60 0.96 10 7 -3 2.50 0.94 10 7 -3 1.75 0.90 -10 -7 2 23.79 2.65 10 7 -2 20.63 2.41 10 7 -2 25.84 2.95 -10 -7 1 25.81 2.84 10 7 -1 18.98 2.23 10 7 -1 20.18 2.62 -10 -7 0 33.20 3.16 10 7 0 26.15 2.60 10 7 0 33.10 3.29 10 7 1 47.22 3.48 10 7 1 46.61 3.98 -10 -7 -1 52.63 4.02 10 7 2 40.79 3.23 -10 -7 -2 48.56 3.78 10 7 2 29.61 3.09 10 7 3 14.28 2.01 -10 -7 -3 14.49 2.17 10 7 3 12.19 2.00 -10 -7 -4 15.70 2.28 10 7 4 15.55 2.10 10 7 4 13.01 2.13 -10 -7 -5 -0.17 0.56 10 7 5 -0.21 0.63 10 7 5 -0.30 0.95 -10 -7 -6 53.80 4.11 10 7 6 51.10 3.94 10 7 6 52.28 4.27 10 7 7 0.35 0.77 -10 -7 -7 0.62 0.73 10 7 7 0.12 0.78 10 7 8 27.55 3.09 -10 -7 -8 33.37 3.23 10 7 8 25.32 2.90 10 7 9 2.06 1.02 -10 -7 -9 3.42 1.08 10 7 9 4.26 1.27 -10 -7 -10 157.23 7.27 10 7 10 140.62 7.08 10 7 10 138.68 7.26 10 7 11 6.82 1.71 10 7 11 9.27 1.89 -10 -7 -11 9.67 1.87 10 7 12 25.52 3.15 10 7 12 20.67 2.78 -10 -7 -12 26.50 2.98 10 7 13 57.32 4.61 -10 -7 -13 52.36 4.24 10 7 13 55.59 4.60 10 7 14 1.12 1.04 -10 -7 -14 0.74 0.78 10 7 14 0.37 0.87 10 7 15 67.06 5.28 -10 -8 12 21.33 2.77 -10 -8 11 10.82 2.12 -10 -8 10 0.44 0.75 -10 -8 9 1.02 0.82 10 8 -9 0.59 0.80 -10 -8 8 6.05 1.40 10 8 -8 5.60 1.54 -10 -8 7 2.35 1.01 10 8 -7 2.98 1.25 -10 -8 6 18.02 2.45 10 8 -6 20.61 2.72 -10 -8 5 0.42 0.71 10 8 -5 -0.34 0.63 -10 -8 4 6.74 1.55 10 8 -4 7.65 1.58 -10 -8 3 -0.48 0.77 10 8 -3 0.86 1.02 -10 -8 2 35.55 3.35 10 8 -2 40.02 3.64 -10 -8 1 29.00 3.02 10 8 -1 33.01 3.37 -10 -8 0 77.91 5.01 10 8 0 70.28 4.91 10 8 1 182.27 7.19 10 8 1 207.64 8.72 -10 -8 -1 205.13 8.36 -10 -8 -2 3.73 1.31 10 8 2 3.68 1.12 10 8 2 3.39 1.21 10 8 3 14.68 1.93 -10 -8 -3 14.59 2.22 10 8 3 14.48 2.22 10 8 4 5.79 1.46 10 8 4 3.55 1.07 -10 -8 -4 6.92 1.45 10 8 5 37.62 3.61 -10 -8 -5 35.74 3.43 10 8 5 31.13 3.01 10 8 6 21.82 2.78 -10 -8 -6 24.82 2.84 10 8 6 25.88 2.82 10 8 7 6.32 1.57 -10 -8 -7 9.49 1.79 10 8 7 4.36 1.29 10 8 8 0.71 0.93 -10 -8 -8 0.78 0.97 10 8 8 -0.39 0.73 10 8 9 2.41 1.06 -10 -8 -9 2.60 0.90 10 8 9 2.98 1.01 10 8 10 4.92 1.38 -10 -8 -10 4.77 1.37 10 8 10 6.28 1.56 -10 -8 -11 -1.37 1.28 10 8 11 1.12 1.04 10 8 11 0.15 0.93 -10 -8 -12 197.51 8.42 10 8 12 139.63 7.48 10 8 12 176.31 8.49 10 8 13 7.80 1.83 10 8 13 7.68 1.86 -10 -8 -13 6.85 1.72 10 8 14 96.77 6.27 -10 -9 11 0.35 0.83 -10 -9 10 23.26 2.93 -10 -9 9 31.24 3.30 -10 -9 8 5.79 1.59 10 9 -8 4.38 1.41 -10 -9 7 1.95 1.01 10 9 -7 -0.01 0.89 -10 -9 6 1.40 0.80 10 9 -6 2.74 1.22 -10 -9 5 1.48 0.79 10 9 -5 1.96 0.97 -10 -9 4 6.87 1.71 10 9 -4 6.69 1.48 -10 -9 3 17.69 2.53 10 9 -3 14.91 2.32 -10 -9 2 76.01 5.10 10 9 -2 66.32 4.90 -10 -9 1 1.21 0.92 10 9 -1 3.05 1.24 -10 -9 0 0.53 0.70 10 9 0 0.77 0.89 -10 -9 -1 41.18 3.72 10 9 1 47.68 4.13 10 9 2 83.44 5.48 -10 -9 -2 99.96 5.77 10 9 3 5.35 1.48 -10 -9 -3 4.98 1.46 10 9 4 43.69 4.02 -10 -9 -4 41.90 3.70 10 9 5 2.66 1.08 -10 -9 -5 2.33 1.00 -10 -9 -6 85.50 5.38 10 9 6 93.04 5.88 10 9 7 -0.06 0.81 -10 -9 -7 -0.71 0.95 10 9 8 1.78 1.09 -10 -9 -8 1.89 1.18 10 9 9 10.21 2.05 -10 -9 -9 8.15 1.66 10 9 10 0.71 1.06 -10 -9 -10 -2.34 1.42 10 9 11 15.90 2.70 -10 -9 -11 13.29 2.03 10 9 12 16.13 2.70 -10 -9 -12 16.69 2.31 10 9 13 1.85 1.12 10 9 14 26.78 3.36 -10 -10 11 31.55 3.55 -10 -10 10 5.66 1.56 -10 -10 9 2.37 1.25 -10 -10 8 2.40 1.28 -10 -10 7 1.08 1.01 10 10 -7 -0.25 1.01 -10 -10 6 4.76 1.45 10 10 -6 2.21 0.94 -10 -10 5 50.24 4.28 10 10 -5 47.59 4.25 -10 -10 4 180.76 8.26 10 10 -4 169.35 8.02 10 10 -3 13.23 2.15 -10 -10 3 12.82 2.15 -10 -10 2 26.86 3.07 10 10 -2 20.11 2.86 -10 -10 1 12.89 2.23 10 10 -1 10.53 2.10 -10 -10 0 -0.44 0.79 10 10 0 -0.43 0.68 10 10 1 1.92 1.01 -10 -10 -1 1.11 0.68 10 10 2 -1.33 1.04 -10 -10 -2 0.75 0.80 10 10 3 1.43 0.95 -10 -10 -3 3.19 1.16 10 10 4 0.91 0.87 -10 -10 -4 -0.18 0.64 10 10 5 9.91 2.01 -10 -10 -5 11.59 1.98 10 10 6 1.80 0.89 -10 -10 -6 5.59 1.63 10 10 7 -1.91 1.26 -10 -10 -7 8.63 2.04 10 10 8 33.99 3.69 -10 -10 -8 32.96 3.48 10 10 9 23.49 3.11 -10 -10 -9 24.88 2.99 10 10 10 19.65 2.83 -10 -10 -10 25.07 2.96 10 10 11 11.41 2.36 -10 -10 -11 11.13 2.10 10 10 12 33.40 3.77 10 10 13 4.11 1.53 -10 -11 10 5.70 1.72 -10 -11 9 3.24 1.41 -10 -11 8 21.62 2.96 -10 -11 7 43.94 4.15 -10 -11 6 4.50 1.26 -10 -11 5 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12 5 2 31.54 3.61 -12 -5 -3 60.58 4.64 12 5 3 58.86 4.56 12 5 3 53.20 4.68 -12 -5 -4 69.33 5.03 12 5 4 69.69 5.09 12 5 4 62.63 5.03 -12 -5 -5 -1.61 1.27 12 5 5 0.43 0.82 12 5 5 0.69 0.83 12 5 6 33.21 3.59 12 5 6 30.30 3.58 -12 -5 -6 35.35 3.63 12 5 7 1.20 1.02 -12 -5 -7 2.10 0.98 12 5 7 1.63 1.20 -12 -5 -8 61.66 4.90 12 5 8 49.03 4.48 12 5 8 59.29 4.99 12 5 9 7.60 1.95 -12 -5 -9 8.79 1.97 12 5 9 7.62 1.89 12 5 10 5.94 1.82 -12 -5 -10 9.52 2.28 12 5 10 8.37 1.91 -12 -5 -11 13.08 2.49 12 5 11 11.93 2.55 -12 -5 -12 8.83 2.09 -12 -6 8 2.72 1.15 12 6 -8 1.38 0.91 12 6 -7 19.01 2.86 -12 -6 7 16.97 2.54 12 6 -6 2.82 1.59 -12 -6 6 2.79 1.02 -12 -6 5 1.97 1.03 12 6 -5 3.63 1.46 -12 -6 4 -0.43 1.09 12 6 -4 2.60 1.35 -12 -6 3 7.37 1.68 12 6 -3 5.09 1.55 -12 -6 2 0.66 0.97 12 6 -2 0.08 0.85 -12 -6 1 8.96 1.91 12 6 -1 9.17 1.93 -12 -6 0 7.53 1.71 12 6 0 6.17 1.88 -12 -6 -1 -0.79 1.09 12 6 1 -0.35 0.81 12 6 1 1.24 1.13 -12 -6 -2 25.51 3.00 12 6 2 19.31 2.74 12 6 2 20.45 2.97 -12 -6 -3 -0.22 0.96 12 6 3 0.70 0.76 12 6 3 0.48 0.94 -12 -6 -4 20.35 2.74 12 6 4 21.31 2.76 12 6 4 21.40 3.07 -12 -6 -5 8.39 1.73 12 6 5 7.58 1.72 12 6 5 9.09 2.08 -12 -6 -6 63.55 4.91 12 6 6 50.96 4.49 12 6 6 56.28 4.79 -12 -6 -7 -1.13 1.27 12 6 7 -1.32 1.30 12 6 7 1.27 1.03 12 6 8 15.74 2.52 -12 -6 -8 15.70 2.50 12 6 8 15.87 2.65 12 6 9 9.74 2.05 -12 -6 -9 12.01 2.28 12 6 9 10.28 2.26 -12 -6 -10 52.10 4.61 12 6 10 51.32 4.69 -12 -6 -11 44.69 4.35 -12 -6 -12 -1.45 1.46 -12 -7 7 4.78 1.58 12 7 -7 6.98 1.99 -12 -7 6 10.77 2.06 12 7 -6 10.39 2.46 -12 -7 5 1.23 1.01 12 7 -5 1.87 1.26 12 7 -4 14.65 2.77 -12 -7 4 12.01 2.08 -12 -7 3 4.95 1.41 12 7 -3 5.00 1.42 -12 -7 2 2.29 1.12 12 7 -2 2.44 1.42 -12 -7 1 -0.40 1.10 12 7 -1 1.51 1.04 -12 -7 0 46.93 4.16 12 7 0 47.80 4.47 -12 -7 -1 12.37 2.14 12 7 1 6.85 1.95 -12 -7 -2 20.55 2.75 12 7 2 23.62 3.24 -12 -7 -3 0.24 0.82 12 7 3 0.07 0.77 -12 -7 -4 67.89 5.08 12 7 4 65.14 5.39 -12 -7 -5 2.51 1.21 12 7 5 3.74 1.62 -12 -7 -6 12.30 2.13 12 7 6 12.29 2.27 -12 -7 -7 -0.27 0.91 12 7 7 -0.19 1.14 -12 -7 -8 22.10 3.05 12 7 8 18.82 2.92 -12 -7 -9 4.00 1.18 12 7 9 6.89 1.72 -12 -7 -10 9.35 2.04 12 7 10 7.64 2.19 -12 -7 -11 4.84 1.80 -12 -8 7 12.89 2.39 -12 -8 6 4.09 1.48 12 8 -6 -0.64 1.21 -12 -8 5 16.67 2.55 12 8 -5 15.47 2.70 -12 -8 4 11.61 2.28 12 8 -4 6.88 1.81 -12 -8 3 5.75 1.61 12 8 -3 6.33 1.99 12 8 -2 99.50 6.54 -12 -8 2 108.54 6.54 -12 -8 1 0.04 0.84 12 8 -1 -0.26 1.12 -12 -8 0 1.45 0.76 12 8 0 0.22 0.96 -12 -8 -1 22.83 3.03 12 8 1 24.44 3.23 -12 -8 -2 16.64 2.65 12 8 2 12.29 2.41 -12 -8 -3 23.44 2.97 12 8 3 22.34 2.98 -12 -8 -4 7.65 1.87 12 8 4 6.46 1.83 -12 -8 -5 4.39 1.36 12 8 5 1.40 1.16 -12 -8 -6 27.09 3.33 12 8 6 21.62 3.08 -12 -8 -7 -2.08 1.33 12 8 7 1.63 1.19 -12 -8 -8 28.66 3.41 12 8 8 27.12 3.48 -12 -8 -9 -0.95 1.35 12 8 9 -0.45 1.07 -12 -8 -10 7.14 1.98 12 8 10 4.76 1.55 -12 -9 6 2.71 1.08 -12 -9 5 0.74 1.07 12 9 -5 -0.48 0.93 -12 -9 4 1.14 1.21 12 9 -4 0.13 0.95 -12 -9 3 6.83 1.83 12 9 -3 5.00 1.91 -12 -9 2 2.27 1.26 12 9 -2 -1.26 1.16 12 9 -1 12.08 2.42 -12 -9 1 15.52 2.47 -12 -9 0 71.29 5.37 12 9 0 62.35 5.23 -12 -9 -1 1.47 1.27 12 9 1 -0.20 0.89 -12 -9 -2 4.77 1.30 12 9 2 2.91 1.15 -12 -9 -3 13.03 2.29 12 9 3 9.08 2.08 -12 -9 -4 0.21 0.95 12 9 4 0.04 0.90 -12 -9 -5 12.95 2.38 12 9 5 9.23 2.24 -12 -9 -6 36.77 3.90 12 9 6 34.90 3.94 -12 -9 -7 4.38 1.44 12 9 7 3.63 1.27 -12 -9 -8 7.18 1.82 12 9 8 5.94 1.46 -12 -9 -9 1.60 0.95 12 9 9 2.01 0.95 -12 -10 5 -0.40 1.15 -12 -10 4 7.80 2.03 -12 -10 3 -1.78 1.24 12 10 -3 0.22 1.06 -12 -10 2 14.60 2.49 12 10 -2 12.94 2.49 -12 -10 1 4.55 1.62 12 10 -1 3.92 1.53 12 10 0 18.62 2.98 -12 -10 0 22.58 3.06 -12 -10 -1 -0.79 0.99 12 10 1 1.00 1.11 -12 -10 -2 2.69 1.45 12 10 2 -0.45 1.11 -12 -10 -3 22.20 3.14 12 10 3 25.39 3.49 -12 -10 -4 5.01 1.77 12 10 4 1.60 0.87 -12 -10 -5 0.12 1.02 12 10 5 -1.20 1.33 -12 -10 -6 0.32 1.05 12 10 6 -0.10 1.09 -12 -10 -7 6.33 1.94 12 10 7 7.85 1.94 12 10 8 5.69 2.05 -12 -11 4 22.68 3.12 -12 -11 3 14.28 2.71 -12 -11 2 0.19 0.99 -12 -11 1 0.50 1.12 -12 -11 0 0.85 1.02 12 11 0 1.06 1.21 12 11 1 0.53 0.98 -12 -11 -1 1.99 1.40 -12 -11 -2 4.72 1.51 12 11 2 4.11 1.81 -12 -11 -3 37.32 4.01 12 11 3 31.77 3.89 -12 -11 -4 -1.02 1.41 12 11 4 -1.02 1.35 -12 -11 -5 13.74 2.63 12 11 5 14.06 2.59 12 11 6 1.80 0.98 12 11 7 2.12 1.49 -12 -12 0 60.99 5.39 -12 -12 -1 -0.35 1.29 13 -4 -4 0.56 1.03 13 -4 -3 21.58 3.34 -13 4 3 24.22 3.40 13 -4 -2 35.32 4.20 13 -4 -1 210.90 10.48 13 -4 0 69.81 5.99 13 -4 1 31.01 3.91 13 -4 2 2.76 1.28 13 -4 3 12.40 2.54 13 -4 4 21.17 3.26 13 -3 -6 2.78 1.31 -13 3 6 1.56 1.20 13 -3 -5 -1.01 1.41 -13 3 5 1.85 1.29 13 -3 -4 10.57 2.46 -13 3 4 9.50 2.19 13 -3 -3 20.46 3.12 -13 3 3 18.48 2.85 13 -3 -2 4.48 1.76 -13 3 2 5.20 1.83 -13 3 1 137.96 7.77 13 -3 -1 126.83 7.94 13 -3 0 -1.10 1.38 -13 3 0 -2.14 1.37 13 -3 1 14.97 2.80 13 -3 2 2.60 1.27 13 -3 3 6.13 1.92 13 -3 4 3.48 1.38 13 -3 5 1.45 1.53 13 -3 6 0.34 1.07 -13 2 8 19.84 3.17 13 -2 -7 15.33 2.87 -13 2 7 16.94 2.89 13 -2 -6 2.26 1.28 -13 2 6 0.44 1.00 13 -2 -5 0.21 1.03 -13 2 5 0.37 1.06 13 -2 -4 3.71 1.55 -13 2 4 4.35 1.56 13 -2 -3 16.43 2.88 -13 2 3 17.96 2.71 13 -2 -2 34.38 3.96 -13 2 2 37.74 4.00 13 -2 -1 1.06 0.93 -13 2 1 -0.52 0.96 13 -2 0 43.99 4.55 -13 2 0 54.81 4.78 13 -2 1 13.16 2.61 -13 2 -1 14.03 2.51 13 -2 2 0.61 1.11 -13 2 -2 -2.11 1.37 13 -2 3 8.98 2.10 -13 2 -4 5.01 1.78 13 -2 4 1.15 0.99 -13 2 -5 3.34 1.48 13 -2 5 3.46 1.52 13 -2 6 0.58 1.22 13 -2 7 29.64 3.87 -13 1 8 41.75 4.34 13 -1 -7 25.19 3.42 -13 1 7 23.38 3.27 13 -1 -6 3.86 1.69 -13 1 6 2.25 1.06 13 -1 -5 2.02 1.35 -13 1 5 2.39 1.17 13 -1 -4 5.61 1.46 -13 1 4 7.63 1.99 13 -1 -3 34.50 3.96 -13 1 3 39.91 4.17 13 -1 -2 3.45 1.59 -13 1 2 1.04 1.02 13 -1 -1 2.35 1.36 -13 1 1 4.48 1.66 13 -1 0 63.67 5.44 -13 1 0 66.00 5.14 -13 1 -1 -0.45 0.95 13 -1 1 1.03 1.24 -13 1 -1 0.70 0.82 -13 1 -2 1.88 1.31 13 -1 2 3.04 1.54 -13 1 -2 1.74 1.16 -13 1 -3 5.67 1.77 13 -1 3 3.31 1.41 -13 1 -3 3.41 1.38 -13 1 -4 -0.02 0.91 13 -1 4 -1.14 1.11 -13 1 -4 1.44 1.05 -13 1 -5 18.84 2.89 13 -1 5 20.24 3.13 -13 1 -6 11.30 2.21 13 -1 6 8.60 2.10 -13 1 -7 2.40 1.39 13 -1 7 -0.41 1.10 -13 1 -8 0.34 0.97 13 -1 8 -0.15 1.24 -13 0 8 30.88 3.72 -13 0 7 1.97 1.02 13 0 -6 0.16 0.95 -13 0 6 -0.71 1.02 13 0 -5 1.44 1.07 -13 0 5 1.75 1.17 13 0 -4 0.24 1.07 -13 0 4 -1.42 1.25 13 0 -3 16.56 2.76 -13 0 3 21.75 3.05 13 0 -2 9.13 2.23 -13 0 2 5.53 1.60 13 0 -1 19.17 3.00 -13 0 1 15.24 2.46 -13 0 1 17.89 2.69 13 0 0 -1.26 1.22 -13 0 0 -1.05 1.18 -13 0 0 -0.66 0.87 13 0 0 1.21 1.01 -13 0 -1 31.30 3.44 13 0 1 28.03 3.57 -13 0 -1 30.88 3.55 13 0 1 28.87 3.57 -13 0 -2 3.55 1.29 13 0 2 2.06 1.18 -13 0 -2 3.69 1.60 13 0 2 1.55 1.08 -13 0 -3 153.82 7.88 13 0 3 149.41 8.28 -13 0 -3 169.16 8.33 13 0 3 145.91 8.14 -13 0 -4 3.69 1.60 13 0 4 4.96 1.74 -13 0 -4 6.92 1.67 13 0 4 2.21 1.20 -13 0 -5 1.27 1.27 13 0 5 1.11 0.89 -13 0 -5 -0.29 1.00 13 0 5 1.57 0.92 -13 0 -6 1.17 0.89 13 0 6 1.05 1.09 -13 0 -7 44.15 4.32 13 0 7 46.88 4.69 -13 0 -8 29.16 3.56 13 0 8 23.39 3.56 -13 0 -9 22.39 3.25 13 0 9 16.81 2.98 -13 -1 8 61.31 5.17 -13 -1 7 30.70 3.71 13 1 -6 4.15 1.61 -13 -1 6 2.99 0.84 13 1 -5 17.48 2.98 -13 -1 5 19.31 2.77 13 1 -4 -0.82 0.86 -13 -1 4 -0.94 1.04 13 1 -3 0.18 1.19 -13 -1 3 -0.38 0.76 13 1 -2 1.42 1.21 -13 -1 2 6.11 1.56 -13 -1 2 5.13 1.53 13 1 -2 4.18 1.78 13 1 -1 17.45 2.88 -13 -1 1 13.29 2.44 -13 -1 1 12.56 2.19 13 1 -1 10.03 2.18 13 1 0 10.48 2.23 -13 -1 0 10.56 2.00 -13 -1 0 13.15 2.34 13 1 0 12.06 2.34 13 1 1 0.33 1.12 -13 -1 -1 0.76 0.82 -13 -1 -1 -0.24 0.94 13 1 1 2.52 1.34 13 1 2 30.68 3.88 -13 -1 -2 35.90 3.68 -13 -1 -2 31.04 3.69 13 1 2 26.52 3.39 13 1 3 39.65 4.23 -13 -1 -3 45.34 4.13 -13 -1 -3 48.72 4.49 13 1 3 38.46 4.12 -13 -1 -4 2.47 1.36 13 1 4 1.97 1.37 13 1 4 1.49 0.85 -13 -1 -5 10.10 2.16 13 1 5 11.01 2.36 13 1 5 10.89 2.08 -13 -1 -6 5.67 1.68 13 1 6 5.32 1.85 13 1 6 3.50 1.45 -13 -1 -7 6.39 1.72 13 1 7 6.61 1.80 -13 -1 -8 10.74 2.26 13 1 8 8.31 2.29 -13 -1 -9 3.87 1.49 13 1 9 -0.05 0.93 -13 -2 8 59.43 5.03 -13 -2 7 12.82 2.49 -13 -2 6 -0.01 0.83 13 2 -5 69.22 5.46 -13 -2 5 72.77 5.58 13 2 -4 25.10 3.24 -13 -2 4 26.96 3.31 13 2 -4 26.85 3.54 -13 -2 3 80.00 5.42 13 2 -3 84.16 6.01 -13 -2 3 90.18 6.14 13 2 -3 98.43 6.68 13 2 -2 5.15 1.54 -13 -2 2 3.40 1.43 13 2 -2 1.47 0.89 -13 -2 2 3.95 1.23 13 2 -1 2.11 1.24 -13 -2 1 3.44 1.20 13 2 -1 1.13 0.99 -13 -2 1 1.82 1.03 13 2 0 4.34 1.51 -13 -2 0 7.68 1.85 13 2 0 4.85 1.46 -13 -2 0 5.09 1.31 13 2 1 6.26 1.89 -13 -2 -1 8.90 1.94 13 2 1 6.47 1.85 13 2 2 11.09 2.08 -13 -2 -2 9.08 1.98 13 2 2 14.87 2.67 13 2 3 49.55 4.58 -13 -2 -3 50.03 4.38 13 2 3 46.00 4.73 13 2 4 14.96 2.57 -13 -2 -4 14.09 2.46 13 2 4 10.51 2.12 -13 -2 -5 103.04 6.40 13 2 5 96.24 6.57 13 2 5 91.14 6.41 -13 -2 -6 0.22 0.84 13 2 6 1.11 1.20 13 2 6 0.11 1.00 -13 -2 -7 31.31 3.59 13 2 7 31.85 3.75 -13 -2 -8 -0.91 1.22 13 2 8 0.52 1.21 -13 -2 -9 2.65 1.45 13 2 9 2.61 1.52 -13 -2 -10 -0.51 1.13 -13 -3 8 17.70 2.85 -13 -3 7 -1.06 1.30 -13 -3 6 5.21 1.37 13 3 -6 3.07 1.38 -13 -3 5 77.85 5.69 13 3 -5 70.60 5.76 -13 -3 4 9.89 2.24 13 3 -4 11.28 2.46 -13 -3 3 16.24 2.48 13 3 -3 14.75 2.43 -13 -3 3 14.72 2.40 13 3 -3 16.08 2.67 -13 -3 2 -0.96 1.18 13 3 -2 -1.09 1.26 13 3 -2 -0.54 0.92 -13 -3 1 94.72 5.93 13 3 -1 86.87 6.01 13 3 -1 86.51 6.30 -13 -3 0 4.69 1.27 13 3 0 4.73 1.68 13 3 0 5.46 1.70 13 3 1 38.45 4.05 13 3 1 39.18 4.10 -13 -3 -1 47.81 4.17 13 3 2 2.41 1.30 13 3 2 1.73 1.28 -13 -3 -2 -0.96 1.19 13 3 3 0.01 0.90 -13 -3 -3 -1.67 1.25 13 3 3 -0.74 1.05 13 3 4 3.38 1.47 -13 -3 -4 1.88 1.14 13 3 4 1.35 0.94 13 3 5 16.87 2.81 -13 -3 -5 20.99 2.90 13 3 5 19.96 2.92 13 3 6 1.67 1.24 -13 -3 -6 -1.02 1.29 13 3 6 0.85 0.92 13 3 7 45.40 4.57 -13 -3 -7 50.57 4.60 13 3 7 35.30 3.92 -13 -3 -8 0.54 1.19 13 3 8 2.79 1.42 -13 -3 -9 -1.29 1.09 -13 -3 -10 6.42 1.85 -13 -4 7 -2.01 1.48 13 4 -7 0.18 1.05 -13 -4 6 0.23 1.01 13 4 -6 -0.15 0.97 -13 -4 5 71.81 5.50 13 4 -5 64.24 5.40 -13 -4 4 2.11 1.23 13 4 -4 -0.15 0.97 -13 -4 3 5.66 1.64 13 4 -3 4.29 1.49 -13 -4 2 -2.94 1.50 13 4 -2 -1.80 1.15 -13 -4 1 6.10 1.44 13 4 -1 5.04 1.62 -13 -4 0 -1.25 1.09 13 4 0 0.57 1.06 -13 -4 -1 1.87 0.93 13 4 1 3.65 1.53 13 4 1 5.40 1.76 -13 -4 -2 7.40 1.77 13 4 2 9.26 2.12 13 4 2 6.65 1.84 13 4 3 -0.75 1.05 13 4 3 2.21 1.24 -13 -4 -3 2.77 1.29 13 4 4 -0.25 1.03 13 4 4 1.95 1.38 -13 -4 -4 0.47 0.93 13 4 5 43.21 4.30 -13 -4 -5 54.58 4.73 13 4 5 37.60 4.18 13 4 6 -0.06 1.05 -13 -4 -6 -2.29 1.45 13 4 6 0.10 0.87 -13 -4 -7 9.86 2.11 13 4 7 7.56 2.07 -13 -4 -8 0.05 0.92 -13 -4 -9 71.78 5.54 -13 -4 -10 0.23 0.93 -13 -5 6 2.66 1.10 13 5 -6 1.22 0.92 13 5 -5 -1.11 1.28 -13 -5 4 8.07 1.83 13 5 -4 6.95 1.82 -13 -5 3 17.25 2.58 13 5 -3 16.83 2.87 -13 -5 2 1.22 1.27 13 5 -2 -0.77 0.88 -13 -5 1 1.93 1.32 13 5 -1 -0.84 1.27 -13 -5 0 10.58 1.98 13 5 0 5.67 1.80 -13 -5 -1 9.99 1.95 13 5 1 13.19 2.60 -13 -5 -2 -0.78 1.37 13 5 2 0.48 1.18 -13 -5 -3 73.08 5.44 13 5 3 70.29 5.73 -13 -5 -4 -0.17 1.15 13 5 4 3.20 1.42 13 5 5 1.69 1.15 -13 -5 -5 0.54 1.04 -13 -5 -6 -1.29 1.11 13 5 6 0.42 1.15 -13 -5 -7 100.64 6.48 13 5 7 79.77 6.19 -13 -5 -8 -0.43 0.96 -13 -5 -9 40.72 4.17 13 6 -5 1.84 1.39 -13 -6 4 4.44 1.61 13 6 -4 4.36 1.61 -13 -6 3 19.13 2.67 13 6 -3 15.94 2.79 -13 -6 2 1.05 0.84 13 6 -2 0.12 1.15 -13 -6 1 5.48 1.65 13 6 -1 4.30 1.67 -13 -6 0 21.35 3.05 13 6 0 25.46 3.53 -13 -6 -1 54.97 4.58 13 6 1 46.99 4.67 -13 -6 -2 -3.14 1.55 13 6 2 0.18 0.93 -13 -6 -3 6.83 1.78 13 6 3 7.77 2.03 -13 -6 -4 12.57 2.28 13 6 4 10.26 2.32 -13 -6 -5 6.49 1.76 13 6 5 3.24 1.61 13 6 6 11.86 2.56 -13 -6 -6 17.16 2.69 -13 -6 -7 -1.71 1.36 13 6 7 -1.18 1.28 -13 -6 -8 0.12 1.16 -13 -6 -9 65.75 5.41 -13 -7 4 3.86 1.35 13 7 -4 4.36 1.61 -13 -7 3 2.41 1.39 13 7 -3 0.53 1.01 -13 -7 2 8.46 2.20 13 7 -2 6.54 2.14 -13 -7 1 14.94 2.39 13 7 -1 13.03 2.73 -13 -7 0 -0.80 1.26 13 7 0 -0.27 1.02 -13 -7 -1 77.55 5.59 13 7 1 70.55 5.81 -13 -7 -2 42.40 4.20 13 7 2 43.73 4.61 -13 -7 -3 155.80 8.16 13 7 3 145.67 8.52 -13 -7 -4 93.89 6.27 13 7 4 85.40 6.47 -13 -7 -5 28.86 3.49 13 7 5 23.34 3.39 -13 -7 -6 8.42 2.18 13 7 6 8.02 2.02 13 7 7 24.02 3.50 -13 -7 -7 31.38 3.73 -13 -7 -8 1.98 1.13 -13 -8 3 2.52 1.38 13 8 -3 1.43 1.38 -13 -8 2 -0.05 0.96 13 8 -2 1.29 1.30 -13 -8 1 136.22 7.68 13 8 -1 109.99 7.56 -13 -8 0 -0.21 0.92 13 8 0 0.08 1.13 -13 -8 -1 96.43 6.47 13 8 1 95.53 6.73 -13 -8 -2 33.89 3.71 13 8 2 24.64 3.54 -13 -8 -3 209.17 9.71 13 8 3 178.03 9.55 -13 -8 -4 3.56 1.43 13 8 4 2.07 1.57 -13 -8 -5 51.16 4.67 13 8 5 44.24 4.68 -13 -8 -6 1.96 1.05 13 8 6 4.88 2.06 -13 -9 1 150.84 8.33 -13 -9 0 0.98 0.89 13 9 0 -2.10 1.38 -13 -9 -1 7.28 1.98 13 9 1 6.50 2.01 -13 -9 -2 1.24 1.20 13 9 2 0.35 1.09 -13 -9 -3 116.44 7.29 13 9 3 101.36 7.12 -13 -9 -4 1.53 1.40 13 9 4 1.28 1.62 -14 -2 2 57.76 5.09 14 2 -2 51.70 5.08 -14 -2 1 7.43 1.96 14 2 -1 4.94 1.82 -14 -2 0 9.09 2.27 14 2 0 6.41 2.09 14 2 1 0.73 1.45 -14 -3 2 -0.94 1.36 14 3 -2 1.46 1.08 -14 -3 1 2.57 0.93 14 3 -1 1.21 1.46 -14 -3 0 -1.11 1.43 14 3 0 -0.24 1.22 14 3 1 2.79 2.43 14 4 0 0.19 1.12 14 4 1 18.63 3.18 0 0 0 0.00 0.00 TITL AMX-F05-100K-Me in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 9.223750 12.481487 17.072455 86.2851 89.3749 82.2235 ZERR 4.00 0.000171 0.000218 0.000300 0.0014 0.0015 0.0015 LATT 1 SFAC C H N O Cl UNIT 84.00 80.00 12.00 20.00 4.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 3330 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.124 _oxdiff_exptl_absorpt_empirical_full_min 0.934