data_20 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic 20 _chemical_name_common 20 _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C27 H25 N3 O4' _chemical_formula_weight 455.50 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_H-M_alt 'P 21' _space_group_name_Hall 'P 2yb' _diffrn_refln_scan_width 2.0 _diffrn_refln_scan_rate 30 _space_group.centring_type primitive _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 13.777(6) _cell_length_b 5.073(2) _cell_length_c 15.860(6) _cell_angle_alpha 90 _cell_angle_beta 103.272(7) _cell_angle_gamma 90 _cell_volume 1078.9(8) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 2861 _cell_measurement_theta_min 3.30 _cell_measurement_theta_max 50.09 _exptl_crystal_description needle _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.402 _exptl_crystal_F_000 480 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.040 _exptl_crystal_size_mid 0.010 _exptl_crystal_size_min 0.010 _exptl_absorpt_coefficient_mu 0.775 _shelx_estimated_absorpt_T_min 0.970 _shelx_estimated_absorpt_T_max 0.992 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.784 _exptl_absorpt_correction_T_max 0.929 _exptl_absorpt_process_details SADABS _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source 'microfocus rotating anode' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 8.366 _diffrn_reflns_number 9062 _diffrn_reflns_av_unetI/netI 0.0750 _diffrn_reflns_av_R_equivalents 0.0871 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -4 _diffrn_reflns_limit_k_max 4 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 2.862 _diffrn_reflns_theta_max 50.420 _diffrn_reflns_theta_full 50.000 _diffrn_measured_fraction_theta_max 0.976 _diffrn_measured_fraction_theta_full 0.981 _diffrn_reflns_Laue_measured_fraction_max 0.976 _diffrn_reflns_Laue_measured_fraction_full 0.981 _diffrn_reflns_point_group_measured_fraction_max 0.959 _diffrn_reflns_point_group_measured_fraction_full 0.965 _reflns_number_total 2151 _reflns_number_gt 1709 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.711 _reflns_Friedel_fraction_max 0.936 _reflns_Friedel_fraction_full 0.944 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXT-2014' _computing_structure_refinement 'SHELXL-2014' _computing_molecular_graphics 'ORTEP-32' _computing_publication_material 'WinGX' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0392P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 563 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.3(4) _chemical_absolute_configuration ad _refine_ls_number_reflns 2151 _refine_ls_number_parameters 309 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0650 _refine_ls_R_factor_gt 0.0394 _refine_ls_wR_factor_ref 0.0875 _refine_ls_wR_factor_gt 0.0774 _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_restrained_S_all 1.024 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.2654(4) 0.6225(15) 0.2139(3) 0.0193(16) Uani 1 1 d . . . . . H1 H 0.2272 0.4549 0.1986 0.023 Uiso 1 1 calc R U . . . C2 C 0.2090(5) 0.8453(15) 0.1593(4) 0.0234(18) Uani 1 1 d . . . . . C3 C 0.1124(4) 0.9357(15) 0.1561(4) 0.0257(18) Uani 1 1 d . . . . . H3 H 0.0733 0.8603 0.1920 0.031 Uiso 1 1 calc R U . . . C4 C 0.0745(4) 1.1403(16) 0.0985(4) 0.0277(18) Uani 1 1 d . . . . . H4 H 0.0094 1.2062 0.0961 0.033 Uiso 1 1 calc R U . . . C5 C 0.1309(5) 1.2477(14) 0.0451(4) 0.0271(19) Uani 1 1 d . . . . . H5 H 0.1042 1.3870 0.0067 0.033 Uiso 1 1 calc R U . . . C6 C 0.2262(4) 1.1530(15) 0.0473(4) 0.0241(17) Uani 1 1 d . . . . . H6 H 0.2646 1.2252 0.0103 0.029 Uiso 1 1 calc R U . . . C7 C 0.2637(4) 0.9533(15) 0.1040(4) 0.0216(17) Uani 1 1 d . . . . . C8 C 0.3571(5) 0.8079(15) 0.1164(4) 0.0251(18) Uani 1 1 d . . . . . C9 C 0.4436(5) 0.7757(16) 0.0906(4) 0.028(2) Uani 1 1 d . . . . . H9 H 0.4665 0.8787 0.0490 0.033 Uiso 1 1 calc R U . . . C10 C 0.4380(5) 0.4698(15) 0.1889(4) 0.0237(18) Uani 1 1 d . . . . . H10 H 0.4552 0.3251 0.2275 0.028 Uiso 1 1 calc R U . . . C11 C 0.2895(4) 0.6567(14) 0.3133(3) 0.0210(17) Uani 1 1 d . . . . . H11 H 0.3393 0.5187 0.3390 0.025 Uiso 1 1 calc R U . . . C12 C 0.3333(4) 0.9244(15) 0.3459(4) 0.0239(18) Uani 1 1 d . . . . . H12 H 0.2823 1.0596 0.3200 0.029 Uiso 1 1 calc R U . . . C13 C 0.3474(4) 0.9450(14) 0.4443(4) 0.0199(17) Uani 1 1 d . . . . . C14 C 0.4154(4) 1.1261(15) 0.4907(4) 0.0233(17) Uani 1 1 d . . . . . H14 H 0.4525 1.2303 0.4595 0.028 Uiso 1 1 calc R U . . . C15 C 0.3792(5) 1.0135(15) 0.6192(4) 0.026(2) Uani 1 1 d . . . . . H15 H 0.3882 1.0399 0.6799 0.031 Uiso 1 1 calc R U . . . C16 C 0.3124(4) 0.8233(15) 0.5804(4) 0.0258(18) Uani 1 1 d . . . . . H16 H 0.2790 0.7170 0.6141 0.031 Uiso 1 1 calc R U . . . C17 C 0.2942(4) 0.7880(14) 0.4903(4) 0.0207(17) Uani 1 1 d . . . . . C18 C 0.2192(4) 0.5826(14) 0.4460(3) 0.0216(18) Uani 1 1 d . . . . . H18A H 0.1569 0.6019 0.4666 0.026 Uiso 1 1 calc R U . . . H18B H 0.2463 0.4045 0.4625 0.026 Uiso 1 1 calc R U . . . C19 C 0.1950(4) 0.6083(16) 0.3472(3) 0.0246(17) Uani 1 1 d . . . . . H19A H 0.1479 0.7563 0.3294 0.029 Uiso 1 1 calc R U . . . H19B H 0.1620 0.4449 0.3209 0.029 Uiso 1 1 calc R U . . . C20 C 0.8454(4) -0.0129(15) 0.2478(4) 0.0234(18) Uani 1 1 d . . . . . C21 C 0.9264(4) 0.1504(15) 0.2781(4) 0.0270(18) Uani 1 1 d . . . . . H21 H 0.9412 0.2889 0.2427 0.032 Uiso 1 1 calc R U . . . C22 C 0.9867(4) 0.1103(16) 0.3616(4) 0.0293(18) Uani 1 1 d . . . . . H22 H 1.0425 0.2218 0.3823 0.035 Uiso 1 1 calc R U . . . C23 C 0.9661(5) -0.0858(14) 0.4130(4) 0.0271(19) Uani 1 1 d . . . . . H23 H 1.0069 -0.1097 0.4695 0.033 Uiso 1 1 calc R U . . . C24 C 0.8853(5) -0.2516(14) 0.3829(4) 0.031(2) Uani 1 1 d . . . . . H24 H 0.8710 -0.3895 0.4187 0.038 Uiso 1 1 calc R U . . . C25 C 0.8258(5) -0.2156(14) 0.3007(4) 0.0260(18) Uani 1 1 d . . . . . H25 H 0.7710 -0.3304 0.2802 0.031 Uiso 1 1 calc R U . . . C26 C 0.7762(4) 0.0280(14) 0.1602(4) 0.0262(19) Uani 1 1 d . . . . . H26 H 0.7546 -0.1492 0.1352 0.031 Uiso 1 1 calc R U . . . C27 C 0.6821(4) 0.1830(16) 0.1674(4) 0.026(2) Uani 1 1 d . . . . . N1 N 0.4920(4) 0.5649(11) 0.1365(3) 0.0244(16) Uani 1 1 d . . . . . H1A H 0.5501 0.5024 0.1317 0.029 Uiso 1 1 calc R U . . . N2 N 0.3554(4) 0.6141(12) 0.1776(3) 0.0214(14) Uani 1 1 d . . . . . N3 N 0.4318(3) 1.1627(12) 0.5768(3) 0.0248(15) Uani 1 1 d . . . . . O1 O 0.4218(3) 0.9906(10) 0.3193(2) 0.0255(12) Uani 1 1 d . . . . . H1A H 0.4700 0.9057 0.3491 0.038 Uiso 1 1 calc R U . . . O2 O 0.8254(3) 0.1604(11) 0.1024(2) 0.0350(13) Uani 1 1 d . . . . . H2 H 0.7897 0.2857 0.0783 0.053 Uiso 1 1 calc R U . . . O3 O 0.6635(3) 0.3913(10) 0.1200(3) 0.0316(13) Uani 1 1 d . . . . . O4 O 0.6311(3) 0.1015(11) 0.2168(3) 0.0348(13) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.016(3) 0.019(5) 0.021(3) 0.000(3) 0.001(3) 0.002(4) C2 0.021(4) 0.029(5) 0.017(4) -0.005(3) -0.003(3) -0.002(4) C3 0.022(4) 0.034(6) 0.020(4) -0.004(4) 0.000(3) -0.005(4) C4 0.014(3) 0.041(6) 0.023(4) -0.005(4) -0.007(3) 0.005(4) C5 0.029(4) 0.029(6) 0.020(4) -0.008(3) -0.002(3) 0.004(4) C6 0.021(4) 0.033(5) 0.017(4) -0.009(4) 0.002(3) 0.002(4) C7 0.019(4) 0.027(5) 0.016(4) -0.002(4) -0.001(3) 0.005(4) C8 0.030(5) 0.032(5) 0.009(4) -0.001(4) -0.004(3) 0.002(4) C9 0.019(4) 0.045(6) 0.018(4) -0.001(4) 0.004(3) 0.003(4) C10 0.024(4) 0.028(5) 0.016(4) -0.004(4) -0.001(3) -0.005(4) C11 0.017(3) 0.025(5) 0.020(4) 0.003(4) 0.003(3) -0.001(4) C12 0.018(4) 0.031(6) 0.022(4) -0.003(4) 0.002(3) -0.010(4) C13 0.016(4) 0.020(5) 0.021(4) -0.001(4) 0.001(3) 0.004(4) C14 0.019(4) 0.023(5) 0.025(4) 0.002(4) 0.000(3) 0.000(4) C15 0.020(4) 0.038(6) 0.018(4) -0.002(4) 0.001(3) 0.007(4) C16 0.021(4) 0.033(5) 0.022(4) 0.006(4) 0.002(3) 0.004(4) C17 0.012(3) 0.026(5) 0.022(4) -0.001(4) 0.000(3) 0.007(4) C18 0.019(4) 0.020(5) 0.027(4) 0.002(3) 0.007(3) -0.001(3) C19 0.026(4) 0.025(5) 0.022(4) -0.008(4) 0.003(3) -0.001(4) C20 0.018(4) 0.029(5) 0.021(4) -0.004(4) 0.001(3) 0.003(4) C21 0.028(4) 0.030(5) 0.026(4) 0.002(4) 0.011(3) 0.006(4) C22 0.022(4) 0.039(6) 0.028(4) -0.001(4) 0.007(3) -0.006(4) C23 0.021(4) 0.035(6) 0.023(4) -0.003(4) 0.001(3) -0.002(4) C24 0.036(4) 0.034(6) 0.023(4) 0.003(4) 0.004(3) -0.001(4) C25 0.026(4) 0.024(5) 0.025(4) -0.004(4) -0.001(3) -0.002(4) C26 0.025(4) 0.032(6) 0.023(4) 0.001(3) 0.009(3) 0.001(4) C27 0.017(4) 0.037(6) 0.023(4) -0.015(4) 0.000(3) -0.008(4) N1 0.016(3) 0.033(5) 0.023(3) 0.000(3) 0.001(3) 0.006(3) N2 0.015(3) 0.030(4) 0.017(3) -0.005(3) 0.001(2) 0.004(3) N3 0.019(3) 0.035(4) 0.018(3) 0.000(3) -0.002(2) 0.002(3) O1 0.020(2) 0.034(4) 0.021(2) 0.006(2) 0.0003(19) -0.006(2) O2 0.032(3) 0.046(4) 0.027(3) 0.009(3) 0.006(2) 0.012(3) O3 0.028(3) 0.035(4) 0.030(3) 0.008(3) 0.003(2) 0.006(3) O4 0.024(3) 0.050(4) 0.031(3) 0.004(3) 0.008(2) 0.005(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N2 1.483(7) . ? C1 C2 1.524(9) . ? C1 C11 1.545(8) . ? C1 H1 1.0000 . ? C2 C7 1.393(9) . ? C2 C3 1.397(8) . ? C3 C4 1.401(9) . ? C3 H3 0.9500 . ? C4 C5 1.386(9) . ? C4 H4 0.9500 . ? C5 C6 1.391(8) . ? C5 H5 0.9500 . ? C6 C7 1.374(9) . ? C6 H6 0.9500 . ? C7 C8 1.457(9) . ? C8 C9 1.356(8) . ? C8 N2 1.386(8) . ? C9 N1 1.376(8) . ? C9 H9 0.9500 . ? C10 N1 1.328(7) . ? C10 N2 1.330(8) . ? C10 H10 0.9500 . ? C11 C12 1.527(9) . ? C11 C19 1.537(8) . ? C11 H11 1.0000 . ? C12 O1 1.420(7) . ? C12 C13 1.531(8) . ? C12 H12 1.0000 . ? C13 C14 1.396(8) . ? C13 C17 1.396(9) . ? C14 N3 1.344(7) . ? C14 H14 0.9500 . ? C15 N3 1.333(8) . ? C15 C16 1.378(9) . ? C15 H15 0.9500 . ? C16 C17 1.404(8) . ? C16 H16 0.9500 . ? C17 C18 1.521(9) . ? C18 C19 1.532(8) . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C20 C21 1.385(8) . ? C20 C25 1.393(9) . ? C20 C26 1.508(8) . ? C21 C22 1.408(8) . ? C21 H21 0.9500 . ? C22 C23 1.357(9) . ? C22 H22 0.9500 . ? C23 C24 1.389(9) . ? C23 H23 0.9500 . ? C24 C25 1.384(8) . ? C24 H24 0.9500 . ? C25 H25 0.9500 . ? C26 O2 1.428(7) . ? C26 C27 1.542(9) . ? C26 H26 1.0000 . ? C27 O4 1.237(8) . ? C27 O3 1.288(8) . ? N1 H1A 0.8800 . ? O1 H1A 0.8400 . ? O2 H2 0.8400 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 C1 C2 99.4(5) . . ? N2 C1 C11 113.4(4) . . ? C2 C1 C11 117.3(6) . . ? N2 C1 H1 108.7 . . ? C2 C1 H1 108.7 . . ? C11 C1 H1 108.7 . . ? C7 C2 C3 119.7(6) . . ? C7 C2 C1 111.7(6) . . ? C3 C2 C1 128.4(6) . . ? C2 C3 C4 118.4(6) . . ? C2 C3 H3 120.8 . . ? C4 C3 H3 120.8 . . ? C5 C4 C3 120.8(6) . . ? C5 C4 H4 119.6 . . ? C3 C4 H4 119.6 . . ? C4 C5 C6 120.4(7) . . ? C4 C5 H5 119.8 . . ? C6 C5 H5 119.8 . . ? C7 C6 C5 118.8(6) . . ? C7 C6 H6 120.6 . . ? C5 C6 H6 120.6 . . ? C6 C7 C2 121.7(6) . . ? C6 C7 C8 130.5(6) . . ? C2 C7 C8 107.7(6) . . ? C9 C8 N2 106.5(6) . . ? C9 C8 C7 146.2(7) . . ? N2 C8 C7 107.3(6) . . ? C8 C9 N1 106.7(6) . . ? C8 C9 H9 126.7 . . ? N1 C9 H9 126.7 . . ? N1 C10 N2 107.5(6) . . ? N1 C10 H10 126.3 . . ? N2 C10 H10 126.3 . . ? C12 C11 C19 108.9(5) . . ? C12 C11 C1 114.9(5) . . ? C19 C11 C1 109.7(4) . . ? C12 C11 H11 107.7 . . ? C19 C11 H11 107.7 . . ? C1 C11 H11 107.7 . . ? O1 C12 C11 114.2(5) . . ? O1 C12 C13 111.8(5) . . ? C11 C12 C13 110.7(5) . . ? O1 C12 H12 106.6 . . ? C11 C12 H12 106.6 . . ? C13 C12 H12 106.6 . . ? C14 C13 C17 118.0(5) . . ? C14 C13 C12 119.7(6) . . ? C17 C13 C12 122.3(6) . . ? N3 C14 C13 124.2(6) . . ? N3 C14 H14 117.9 . . ? C13 C14 H14 117.9 . . ? N3 C15 C16 123.8(6) . . ? N3 C15 H15 118.1 . . ? C16 C15 H15 118.1 . . ? C15 C16 C17 119.3(6) . . ? C15 C16 H16 120.3 . . ? C17 C16 H16 120.3 . . ? C13 C17 C16 117.8(6) . . ? C13 C17 C18 122.2(5) . . ? C16 C17 C18 120.0(6) . . ? C17 C18 C19 112.3(5) . . ? C17 C18 H18A 109.1 . . ? C19 C18 H18A 109.1 . . ? C17 C18 H18B 109.1 . . ? C19 C18 H18B 109.1 . . ? H18A C18 H18B 107.9 . . ? C18 C19 C11 111.6(5) . . ? C18 C19 H19A 109.3 . . ? C11 C19 H19A 109.3 . . ? C18 C19 H19B 109.3 . . ? C11 C19 H19B 109.3 . . ? H19A C19 H19B 108.0 . . ? C21 C20 C25 119.0(5) . . ? C21 C20 C26 121.8(6) . . ? C25 C20 C26 119.2(6) . . ? C20 C21 C22 119.6(6) . . ? C20 C21 H21 120.2 . . ? C22 C21 H21 120.2 . . ? C23 C22 C21 120.8(7) . . ? C23 C22 H22 119.6 . . ? C21 C22 H22 119.6 . . ? C22 C23 C24 119.9(6) . . ? C22 C23 H23 120.1 . . ? C24 C23 H23 120.1 . . ? C25 C24 C23 119.9(6) . . ? C25 C24 H24 120.0 . . ? C23 C24 H24 120.0 . . ? C24 C25 C20 120.7(6) . . ? C24 C25 H25 119.7 . . ? C20 C25 H25 119.7 . . ? O2 C26 C20 111.3(5) . . ? O2 C26 C27 109.8(6) . . ? C20 C26 C27 111.5(5) . . ? O2 C26 H26 108.0 . . ? C20 C26 H26 108.0 . . ? C27 C26 H26 108.0 . . ? O4 C27 O3 125.3(6) . . ? O4 C27 C26 119.0(7) . . ? O3 C27 C26 115.6(6) . . ? C10 N1 C9 109.9(5) . . ? C10 N1 H1A 125.1 . . ? C9 N1 H1A 125.1 . . ? C10 N2 C8 109.5(5) . . ? C10 N2 C1 136.8(6) . . ? C8 N2 C1 113.7(5) . . ? C15 N3 C14 116.8(6) . . ? C12 O1 H1A 109.5 . . ? C26 O2 H2 109.5 . . ? _refine_diff_density_max 0.190 _refine_diff_density_min -0.194 _refine_diff_density_rms 0.048 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL gene639_0m in P2(1) CELL 1.54178 13.7766 5.0731 15.8603 90.000 103.272 90.000 ZERR 2.00 0.0055 0.0021 0.0063 0.000 0.007 0.000 LATT -1 SYMM - X, 1/2 + Y, - Z SFAC C H N O UNIT 54 50 6 8 MERG 2 FMAP 2 PLAN 20 SIZE 0.010 0.010 0.040 ACTA 100.00 BOND $H LIST 4 WPDB -2 L.S. 10 TEMP -173.00 WGHT 0.039200 FVAR 1.18707 C1 1 0.265381 0.622541 0.213889 11.00000 0.01619 0.01907 = 0.02088 0.00031 0.00069 0.00184 AFIX 13 H1 2 0.227199 0.454939 0.198565 11.00000 -1.20000 AFIX 0 C2 1 0.208950 0.845316 0.159286 11.00000 0.02111 0.02868 = 0.01670 -0.00520 -0.00312 -0.00217 C3 1 0.112357 0.935732 0.156064 11.00000 0.02150 0.03375 = 0.01984 -0.00441 0.00031 -0.00528 AFIX 43 H3 2 0.073284 0.860295 0.192025 11.00000 -1.20000 AFIX 0 C4 1 0.074515 1.140268 0.098543 11.00000 0.01368 0.04112 = 0.02260 -0.00523 -0.00732 0.00452 AFIX 43 H4 2 0.009388 1.206155 0.096142 11.00000 -1.20000 AFIX 0 C5 1 0.130870 1.247746 0.045088 11.00000 0.02926 0.02880 = 0.01991 -0.00797 -0.00150 0.00429 AFIX 43 H5 2 0.104227 1.387034 0.006677 11.00000 -1.20000 AFIX 0 C6 1 0.226152 1.153048 0.047306 11.00000 0.02093 0.03312 = 0.01734 -0.00913 0.00227 0.00194 AFIX 43 H6 2 0.264638 1.225174 0.010293 11.00000 -1.20000 AFIX 0 C7 1 0.263651 0.953349 0.103965 11.00000 0.01899 0.02713 = 0.01607 -0.00208 -0.00143 0.00465 C8 1 0.357103 0.807927 0.116401 11.00000 0.03005 0.03151 = 0.00933 -0.00071 -0.00445 0.00203 C9 1 0.443649 0.775747 0.090644 11.00000 0.01906 0.04478 = 0.01843 -0.00080 0.00364 0.00343 AFIX 43 H9 2 0.466462 0.878743 0.049036 11.00000 -1.20000 AFIX 0 C10 1 0.437960 0.469797 0.188948 11.00000 0.02417 0.02815 = 0.01597 -0.00353 -0.00099 -0.00538 AFIX 43 H10 2 0.455151 0.325136 0.227526 11.00000 -1.20000 AFIX 0 C11 1 0.289455 0.656725 0.313333 11.00000 0.01719 0.02519 = 0.02002 0.00250 0.00308 -0.00102 AFIX 13 H11 2 0.339326 0.518662 0.339010 11.00000 -1.20000 AFIX 0 C12 1 0.333288 0.924378 0.345948 11.00000 0.01778 0.03076 = 0.02204 -0.00276 0.00221 -0.01037 AFIX 13 H12 2 0.282331 1.059616 0.320030 11.00000 -1.20000 AFIX 0 C13 1 0.347400 0.944961 0.444342 11.00000 0.01635 0.02036 = 0.02139 -0.00073 0.00097 0.00410 C14 1 0.415402 1.126134 0.490742 11.00000 0.01887 0.02305 = 0.02541 0.00242 -0.00014 0.00027 AFIX 43 H14 2 0.452495 1.230348 0.459496 11.00000 -1.20000 AFIX 0 C15 1 0.379164 1.013525 0.619244 11.00000 0.01981 0.03820 = 0.01778 -0.00165 0.00134 0.00744 AFIX 43 H15 2 0.388219 1.039937 0.679852 11.00000 -1.20000 AFIX 0 C16 1 0.312387 0.823270 0.580357 11.00000 0.02115 0.03266 = 0.02243 0.00624 0.00250 0.00430 AFIX 43 H16 2 0.279003 0.716992 0.614142 11.00000 -1.20000 AFIX 0 C17 1 0.294176 0.788046 0.490286 11.00000 0.01229 0.02632 = 0.02174 -0.00147 0.00018 0.00725 C18 1 0.219172 0.582608 0.446041 11.00000 0.01871 0.02022 = 0.02694 0.00189 0.00727 -0.00065 AFIX 23 H18A 2 0.156938 0.601922 0.466644 11.00000 -1.20000 H18B 2 0.246345 0.404482 0.462520 11.00000 -1.20000 AFIX 0 C19 1 0.194969 0.608261 0.347157 11.00000 0.02577 0.02463 = 0.02224 -0.00813 0.00342 -0.00102 AFIX 23 H19A 2 0.147923 0.756346 0.329367 11.00000 -1.20000 H19B 2 0.161996 0.444865 0.320893 11.00000 -1.20000 AFIX 0 C20 1 0.845392 -0.012888 0.247770 11.00000 0.01779 0.02943 = 0.02141 -0.00438 0.00099 0.00314 C21 1 0.926418 0.150438 0.278081 11.00000 0.02789 0.02995 = 0.02551 0.00184 0.01078 0.00611 AFIX 43 H21 2 0.941245 0.288856 0.242692 11.00000 -1.20000 AFIX 0 C22 1 0.986701 0.110261 0.361619 11.00000 0.02212 0.03878 = 0.02772 -0.00074 0.00738 -0.00600 AFIX 43 H22 2 1.042482 0.221824 0.382253 11.00000 -1.20000 AFIX 0 C23 1 0.966129 -0.085819 0.413036 11.00000 0.02087 0.03549 = 0.02298 -0.00289 0.00089 -0.00179 AFIX 43 H23 2 1.006907 -0.109719 0.469550 11.00000 -1.20000 AFIX 0 C24 1 0.885345 -0.251571 0.382912 11.00000 0.03564 0.03401 = 0.02292 0.00277 0.00360 -0.00140 AFIX 43 H24 2 0.870997 -0.389488 0.418710 11.00000 -1.20000 AFIX 0 C25 1 0.825785 -0.215602 0.300704 11.00000 0.02550 0.02413 = 0.02522 -0.00395 -0.00058 -0.00247 AFIX 43 H25 2 0.770965 -0.330369 0.280171 11.00000 -1.20000 AFIX 0 C26 1 0.776163 0.028037 0.160222 11.00000 0.02544 0.03198 = 0.02282 0.00061 0.00912 0.00146 AFIX 13 H26 2 0.754600 -0.149178 0.135188 11.00000 -1.20000 AFIX 0 C27 1 0.682072 0.182965 0.167398 11.00000 0.01664 0.03727 = 0.02273 -0.01547 -0.00049 -0.00765 N1 3 0.492019 0.564932 0.136474 11.00000 0.01560 0.03333 = 0.02274 -0.00018 0.00096 0.00617 AFIX 43 H1A 2 0.550114 0.502443 0.131727 11.00000 -1.20000 AFIX 0 N2 3 0.355377 0.614091 0.177600 11.00000 0.01520 0.03039 = 0.01730 -0.00480 0.00122 0.00387 N3 3 0.431796 1.162673 0.576791 11.00000 0.01876 0.03507 = 0.01756 -0.00034 -0.00191 0.00213 O1 4 0.421805 0.990629 0.319281 11.00000 0.01978 0.03407 = 0.02052 0.00608 0.00031 -0.00606 AFIX 147 H1A 2 0.470006 0.905689 0.349051 11.00000 -1.50000 AFIX 0 O2 4 0.825385 0.160432 0.102364 11.00000 0.03175 0.04604 = 0.02689 0.00925 0.00590 0.01152 AFIX 147 H2 2 0.789677 0.285704 0.078270 11.00000 -1.50000 AFIX 0 O3 4 0.663497 0.391277 0.119980 11.00000 0.02797 0.03478 = 0.03024 0.00789 0.00274 0.00614 O4 4 0.631139 0.101549 0.216827 11.00000 0.02447 0.04988 = 0.03108 0.00374 0.00821 0.00511 HKLF 4 REM gene639_0m in P2(1) REM R1 = 0.0394 for 1709 Fo > 4sig(Fo) and 0.0650 for all 2151 data REM 309 parameters refined using 1 restraints END WGHT 0.0394 0.0000 REM Highest difference peak 0.190, deepest hole -0.194, 1-sigma level 0.048 Q1 1 0.3524 0.2143 0.1512 11.00000 0.05 0.19 Q2 1 0.5953 0.1593 0.0714 11.00000 0.05 0.18 Q3 1 0.3400 0.2879 0.3465 11.00000 0.05 0.17 Q4 1 0.5605 0.6262 0.0538 11.00000 0.05 0.16 Q5 1 1.0000 0.5585 0.2254 11.00000 0.05 0.16 Q6 1 0.3077 1.0807 0.3065 11.00000 0.05 0.16 Q7 1 0.3420 0.4530 0.1356 11.00000 0.05 0.16 Q8 1 -0.0735 1.2833 0.0803 11.00000 0.05 0.16 Q9 1 -0.0421 0.5738 0.1456 11.00000 0.05 0.16 Q10 1 0.4366 0.8494 0.2001 11.00000 0.05 0.15 Q11 1 1.0012 -0.4016 0.3859 11.00000 0.05 0.15 Q12 1 0.5052 0.9602 0.2544 11.00000 0.05 0.15 Q13 1 0.2138 0.7208 0.2060 11.00000 0.05 0.15 Q14 1 0.6430 0.4552 0.2047 11.00000 0.05 0.15 Q15 1 0.8390 0.3282 0.1843 11.00000 0.05 0.15 Q16 1 0.0794 0.9575 0.3030 11.00000 0.05 0.15 Q17 1 0.4936 0.7744 0.0297 11.00000 0.05 0.15 Q18 1 0.8501 -0.3934 0.4240 11.00000 0.05 0.15 Q19 1 0.5088 0.7054 0.2396 11.00000 0.05 0.14 Q20 1 0.3610 0.4652 0.2768 11.00000 0.05 0.14 ; _shelx_res_checksum 98923 _shelx_hkl_file ; 1 0 0 2199.15 75.9324 17 1 0 0 2205.39 71.6170 13 1 0 0 2041.75 70.0342 13 1 0 0 2359.18 101.740 14 1 0 0 2177.75 69.8543 15 1 0 0 2109.91 70.6953 17 -1 0 0 2336.29 98.4177 14 -1 0 0 2210.31 69.8840 15 -1 0 0 2194.95 70.6571 17 -1 0 0 2041.28 76.5548 17 -1 0 0 2181.85 70.5679 13 -1 0 0 2197.10 71.4569 13 -2 0 0 4785.77 154.671 13 2 0 0 4863.83 153.729 15 -2 0 0 4829.79 156.982 13 2 0 0 4676.34 156.875 13 -2 0 0 5262.86 221.830 14 -2 0 0 4825.11 154.118 15 -2 0 0 4692.50 155.350 17 2 0 0 4860.20 165.920 17 2 0 0 4706.76 154.888 17 -3 0 0 564.509 35.9885 15 -3 0 0 815.727 230.845 14 3 0 0 633.246 65.2327 15 3 0 0 526.020 83.4942 17 -3 0 0 532.015 37.1026 13 -3 0 0 582.186 46.9220 13 3 0 0 540.447 33.4954 15 3 0 0 459.843 47.8906 13 -3 0 0 486.136 42.0093 17 -4 0 0 1004.09 56.8591 17 -4 0 0 961.698 55.6909 13 -4 0 0 1352.76 276.394 14 -4 0 0 963.849 50.7970 15 -4 0 0 943.137 54.6595 13 4 0 0 981.056 50.2642 15 4 0 0 1025.86 102.573 17 -5 0 0 301.168 247.520 14 5 0 0 360.617 74.1845 17 -5 0 0 377.109 44.6013 13 -5 0 0 234.853 100.370 18 5 0 0 278.058 34.7541 15 5 0 0 261.982 39.5973 9 6 0 0 322.794 72.9143 17 6 0 0 187.462 39.6901 9 -6 0 0 165.506 34.4811 13 -6 0 0 256.000 108.092 18 7 0 0 16.3284 22.2231 6 -7 0 0 87.5592 36.0341 5 7 0 0 54.3030 34.9472 9 -7 0 0 14.6581 113.909 18 7 0 0 71.4643 22.0980 4 -8 0 0 241.537 134.662 18 8 0 0 259.132 34.6566 4 8 0 0 202.442 32.8274 6 -8 0 0 268.253 48.7727 5 8 0 0 241.118 44.3894 9 -9 0 0 615.715 49.6806 8 9 0 0 510.493 53.7408 9 9 0 0 411.928 67.9290 11 -9 0 0 350.258 140.074 18 -9 0 0 391.712 50.5441 5 9 0 0 564.005 42.2940 4 9 0 0 507.861 37.6822 6 10 0 0 32.1345 28.8501 6 10 0 0 44.1648 45.7383 9 -10 0 0 62.0072 36.7314 8 10 0 0 45.7005 50.9174 11 10 0 0 53.6467 25.3048 4 -10 0 0 -122.59 161.028 18 11 0 0 -4.5488 24.5765 4 11 0 0 21.4199 32.5630 6 -11 0 0 42.1952 33.0245 8 11 0 0 -33.726 48.1176 9 -11 0 0 41.7373 324.118 18 12 0 0 45.7284 34.2564 6 -12 0 0 39.4972 32.2233 8 -12 0 0 7.97815 21.5485 1 -13 0 0 113.737 23.6946 1 0 -1 0 -25.468 20.9352 17 0 -1 0 10.9911 11.8378 15 0 1 0 412.962 174.090 14 0 1 0 2.81059 12.5333 15 0 1 0 10.0382 13.0474 17 0 1 0 -4.0967 13.3407 16 1 -1 0 6792.62 212.187 13 1 -1 0 6780.28 212.836 15 1 -1 0 6994.82 212.969 13 -1 -1 0 6239.96 258.205 14 1 -1 0 6767.89 226.129 17 1 -1 0 6608.12 215.105 16 1 1 0 6680.07 210.047 17 -1 1 0 6784.23 233.862 17 -1 1 0 6785.79 214.632 13 -1 1 0 6836.56 213.974 17 1 1 0 6180.13 269.584 14 -1 1 0 6805.96 212.879 15 1 1 0 6946.00 215.930 17 1 1 0 6828.35 209.766 15 -1 1 0 6954.45 217.018 16 -1 1 0 6666.59 327.085 14 2 -1 0 8197.59 261.202 16 2 -1 0 8203.07 259.384 13 2 -1 0 8031.87 256.591 13 2 -1 0 8042.38 274.280 17 2 -1 0 7723.34 256.577 15 2 1 0 8067.04 254.753 17 2 1 0 8235.25 254.721 17 2 1 0 8078.57 253.341 15 -2 1 0 8161.51 258.657 17 -2 1 0 8051.67 258.803 13 -2 1 0 7900.82 403.895 14 -2 1 0 8227.99 257.095 15 3 -1 0 3086.75 114.198 13 3 -1 0 3030.09 140.732 17 3 -1 0 3123.49 116.377 16 3 -1 0 2931.95 133.727 15 3 -1 0 3126.94 107.512 15 -3 1 0 3258.91 112.955 17 3 1 0 3136.70 113.713 17 3 1 0 2944.46 108.378 15 -3 1 0 3046.93 329.879 14 4 -1 0 2541.28 136.498 17 -4 -1 0 2566.28 130.223 18 4 -1 0 2897.87 191.651 18 4 1 0 2793.62 110.780 17 -4 1 0 2642.64 103.733 17 -4 1 0 2275.38 340.463 14 -5 -1 0 803.378 110.789 18 5 -1 0 526.271 159.413 18 5 -1 0 742.937 97.8737 17 5 -1 0 831.969 52.0882 9 5 1 0 773.102 71.4806 17 -5 1 0 763.451 96.5937 9 -5 1 0 855.413 59.1311 17 -5 1 0 697.778 332.738 14 5 1 0 812.649 43.9911 9 -5 1 0 843.747 135.799 18 6 -1 0 495.483 94.9037 17 -6 -1 0 651.471 122.230 18 -6 -1 0 484.728 31.8797 8 6 -1 0 532.965 29.8660 5 6 -1 0 587.187 51.5378 9 6 -1 0 452.905 34.4515 6 -6 1 0 599.619 62.2761 5 6 1 0 503.120 43.2044 9 -6 1 0 230.346 277.224 14 6 1 0 573.733 73.8855 17 -7 -1 0 1505.37 147.789 18 -7 -1 0 1466.40 55.6648 8 7 -1 0 1510.28 60.2886 6 7 -1 0 1245.28 96.3822 9 7 -1 0 1443.88 56.9138 5 7 1 0 1478.66 57.6855 6 7 1 0 1423.93 60.7997 4 7 1 0 1477.09 68.4987 9 -7 1 0 1538.99 81.8988 5 -8 -1 0 622.520 151.951 18 8 -1 0 359.565 36.4372 6 -8 -1 0 375.385 32.2327 8 8 1 0 332.972 46.9468 9 -8 1 0 311.890 69.0117 2 -8 1 0 305.113 72.5588 5 8 1 0 329.614 31.8053 6 8 1 0 356.476 37.2674 4 9 -1 0 266.667 37.1402 6 -9 -1 0 311.876 48.5524 8 -9 -1 0 386.467 140.976 18 9 1 0 294.187 39.7905 4 -9 1 0 389.852 75.8201 5 -9 1 0 360.126 52.2724 8 9 1 0 332.273 35.5737 6 9 1 0 343.161 51.7590 9 -9 1 0 294.407 49.9444 2 10 -1 0 479.111 46.0884 2 10 -1 0 468.251 43.7195 6 -10 -1 0 632.442 181.411 18 -10 1 0 286.446 69.0896 2 10 1 0 469.424 45.7423 4 -10 1 0 467.467 75.0715 5 10 1 0 501.993 40.3247 6 -10 1 0 414.180 56.5474 8 10 1 0 408.380 57.4204 9 11 -1 0 188.055 45.2730 2 11 -1 0 139.550 36.8719 6 11 1 0 145.325 39.8808 4 -11 1 0 108.007 44.1684 8 11 1 0 95.3698 45.2869 9 11 1 0 165.546 39.9894 6 -11 1 0 161.174 52.5556 5 12 -1 0 78.8480 30.0962 2 -12 1 0 31.5960 26.6866 1 12 1 0 44.7070 26.6754 4 12 1 0 40.3502 32.1330 6 13 -1 0 44.1086 26.2407 2 -13 1 0 37.1503 25.2840 1 0 -2 0 2392.35 147.165 18 0 -2 0 2466.27 82.6804 10 0 2 0 2566.22 89.0399 17 0 2 0 2616.04 108.916 9 0 2 0 2521.21 117.041 11 1 -2 0 806.523 34.5018 10 -1 -2 0 809.123 30.3446 10 -1 -2 0 633.947 91.5854 18 1 -2 0 671.897 138.897 18 -1 2 0 879.439 291.834 14 -1 2 0 685.694 82.1876 9 1 2 0 838.437 36.6524 17 -1 2 0 675.312 75.1463 11 -1 2 0 837.740 46.0986 17 2 -2 0 113.606 26.0232 13 -2 -2 0 137.320 12.2472 10 2 -2 0 274.056 108.761 18 2 -2 0 129.916 17.7427 8 2 -2 0 155.255 25.6397 13 -2 -2 0 55.3874 57.2570 18 2 -2 0 158.461 22.7468 10 2 2 0 160.128 20.1390 17 -2 2 0 145.480 259.682 14 -2 2 0 143.561 81.8176 9 -2 2 0 197.265 63.7617 11 -2 2 0 116.136 27.0274 17 3 -2 0 353.318 36.6844 13 3 -2 0 303.493 20.7083 8 3 -2 0 476.483 144.867 18 -3 -2 0 231.305 62.5206 18 3 -2 0 295.954 28.6369 10 -3 2 0 259.553 280.156 14 -3 2 0 263.373 46.0146 17 -3 2 0 494.750 88.7863 9 -3 2 0 409.274 75.3202 11 4 -2 0 139.582 19.1834 5 4 -2 0 121.362 18.6699 8 4 -2 0 228.696 145.162 18 4 -2 0 125.640 18.2562 5 -4 -2 0 121.922 66.4308 18 4 -2 0 91.8498 27.8368 13 -4 2 0 109.362 72.9144 6 -4 2 0 154.249 82.5004 9 -4 2 0 122.047 75.2284 11 -5 -2 0 1012.92 99.2054 18 5 -2 0 1058.46 41.1795 8 5 -2 0 1094.60 189.288 18 5 -2 0 1020.53 41.7944 5 -5 2 0 1043.17 108.042 4 -5 2 0 1035.63 90.0804 6 5 2 0 784.855 69.9942 9 -5 2 0 903.221 103.206 9 -5 2 0 1102.29 102.819 11 -6 -2 0 328.100 90.7311 18 6 -2 0 218.501 161.274 18 6 -2 0 415.516 26.2828 8 6 -2 0 406.156 30.6311 5 -6 2 0 279.595 88.7209 4 -6 2 0 323.983 95.8394 9 -6 2 0 396.604 74.6343 6 6 2 0 396.745 37.3618 9 -7 -2 0 279.883 99.1107 18 7 -2 0 220.760 31.7971 2 7 -2 0 274.042 27.7187 5 7 -2 0 245.752 25.3817 8 -7 2 0 170.144 81.4632 6 -7 2 0 270.228 55.4040 2 7 2 0 305.531 39.7010 9 -7 2 0 283.068 67.1386 5 8 -2 0 249.944 31.8350 1 8 -2 0 294.451 35.7772 2 -8 -2 0 437.820 126.279 18 8 -2 0 383.241 35.1958 5 8 2 0 326.059 46.3192 9 -8 2 0 461.613 76.3612 5 -8 2 0 320.522 56.2239 2 9 -2 0 353.987 38.8919 2 -9 -2 0 201.333 110.348 18 9 -2 0 286.178 33.8106 5 9 -2 0 276.019 34.4751 1 -9 2 0 380.244 94.3953 2 9 2 0 286.124 48.7997 9 -9 2 0 296.900 69.4959 5 9 2 0 335.010 40.6303 4 10 -2 0 175.441 38.7254 2 10 -2 0 190.435 33.0613 5 10 -2 0 217.117 31.6321 1 -10 2 0 197.963 60.7523 2 -10 2 0 178.914 63.9482 5 10 2 0 43.4379 38.7369 9 10 2 0 237.880 43.4922 4 11 -2 0 87.5603 24.4870 1 11 -2 0 45.8037 28.1916 2 11 -2 0 33.0762 28.1595 5 -11 2 0 29.8174 61.6953 5 11 2 0 30.7589 28.5870 4 -11 2 0 36.9930 29.2809 1 -11 2 0 73.1748 51.9939 2 12 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92.7901 9 -2 4 -1 571.865 102.937 11 3 -4 1 410.111 33.8606 10 -3 4 -1 108.046 53.1367 7 -3 4 -1 434.054 115.044 11 -3 4 -1 210.728 79.2173 9 -3 4 -1 362.952 109.136 4 -3 4 -1 198.377 67.7195 6 4 -4 1 23.9264 24.5144 10 -4 4 -1 54.9457 66.6468 6 -4 4 -1 104.549 84.2972 9 -4 4 -1 138.861 92.2194 11 -4 4 -1 85.6178 82.8331 4 -4 4 -1 3.88814 58.9280 7 -5 4 -1 37.0704 82.5738 4 -5 4 -1 -90.750 69.4954 6 -5 4 -1 7.72933 68.7470 7 6 -4 1 26.1295 21.3093 1 -6 4 -1 -70.609 77.8476 4 -6 4 -1 44.5150 71.4429 6 7 -4 1 238.177 28.1602 1 8 -4 1 26.1097 17.5517 1 -8 4 -1 13.8979 57.7666 2 12 0 -2 71.8538 34.6149 6 -12 0 2 -11.578 36.5181 8 -11 0 2 83.3730 38.7738 8 11 0 -2 18.5725 25.7168 4 11 0 -2 38.6227 30.5538 6 11 0 -2 23.7070 41.7006 9 -11 0 2 135.852 165.487 18 10 0 -2 -49.972 22.7280 4 10 0 -2 -57.427 37.1631 9 10 0 -2 26.3530 26.9925 6 -10 0 2 -31.531 37.8554 5 -10 0 2 195.322 159.176 18 9 0 -2 1532.33 81.4820 9 -9 0 2 1483.65 75.4859 5 -9 0 2 1292.54 175.325 18 9 0 -2 1460.67 64.2924 4 9 0 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22.0442 13 1 0 2 84.1232 17.7683 15 -1 0 -2 65.4214 16.2821 15 -1 0 -2 79.3898 22.0504 13 1 0 2 75.8260 22.4473 13 -2 0 -2 465.468 39.0632 13 -2 0 -2 608.751 189.163 14 2 0 2 601.014 76.2130 17 2 0 2 438.467 40.0097 13 2 0 2 394.812 28.5832 15 2 0 2 471.609 38.9446 16 -2 0 -2 463.629 41.3766 13 -2 0 -2 529.486 28.7755 15 -2 0 -2 432.729 31.1696 17 3 0 2 4492.30 179.811 17 -3 0 -2 4096.19 142.059 13 -3 0 -2 4284.77 143.943 13 -3 0 -2 4133.54 138.287 15 -3 0 -2 3992.73 139.442 17 3 0 2 4025.32 144.899 16 -3 0 -2 4772.31 334.457 14 3 0 2 4173.00 139.525 15 -4 0 -2 100.215 47.0156 13 -4 0 -2 152.398 82.7935 18 4 0 2 136.195 66.6896 17 -4 0 -2 11.8093 223.111 14 -4 0 -2 117.844 33.1481 13 4 0 2 153.121 28.0052 15 4 0 2 144.925 33.8587 9 5 0 2 1981.68 77.2423 9 -5 0 -2 1923.98 301.532 14 5 0 2 1833.63 125.119 17 -5 0 -2 1938.74 83.0897 13 -5 0 -2 1925.02 130.880 18 -5 0 -2 1916.08 71.7741 8 6 0 2 38.1528 19.9680 6 6 0 2 6.69445 39.9133 11 -6 0 -2 18.2555 47.3499 13 -6 0 -2 32.1403 28.5931 8 -6 0 -2 56.0350 35.1336 5 6 0 2 15.1344 34.6239 9 -6 0 -2 25.5140 100.033 18 -7 0 -2 1570.53 141.080 18 7 0 2 1422.18 82.1413 11 7 0 2 1473.99 58.6286 6 7 0 2 1446.44 76.0362 9 -7 0 -2 1487.72 65.0504 8 7 0 2 1503.18 60.4144 4 -7 0 -2 1471.75 67.9228 5 -8 0 -2 50.6049 116.048 18 8 0 2 -17.128 25.5709 6 8 0 2 11.5043 22.1631 4 8 0 2 39.7502 41.3128 11 -8 0 -2 5.64365 28.8928 8 8 0 2 33.4191 39.1832 9 -9 0 -2 -76.402 121.502 18 9 0 2 33.5790 23.6242 4 9 0 2 147.800 33.3085 6 -9 0 -2 49.2109 19.0887 1 9 0 2 73.6881 45.1401 11 9 0 2 82.0068 46.3074 9 -9 0 -2 -26.048 28.6609 8 -10 0 -2 132.149 30.0441 1 10 0 2 116.596 49.8223 9 -10 0 -2 199.705 40.3881 8 10 0 2 159.041 37.7590 6 -10 0 -2 182.482 166.937 18 10 0 2 138.782 30.0601 4 10 0 2 83.9183 49.6461 11 -11 0 -2 584.592 38.5129 1 -11 0 -2 469.566 41.5032 8 11 0 2 524.932 48.8445 4 11 0 2 504.554 101.072 9 11 0 2 579.967 49.4089 6 12 0 2 277.472 49.1492 6 12 0 2 238.782 54.9290 4 13 -1 -2 457.518 50.1464 2 13 1 -2 437.835 46.4956 4 12 -1 -2 423.440 46.2259 2 -12 1 2 549.264 70.8349 5 -12 1 2 402.162 56.3660 8 12 1 -2 467.456 46.8183 4 12 1 -2 486.278 44.7245 6 11 1 -2 301.561 41.0708 6 -11 1 2 311.938 58.3498 8 11 1 -2 299.725 46.7822 4 -11 1 2 357.706 77.3496 5 11 1 -2 184.579 51.3265 9 10 -1 -2 521.473 37.7575 5 10 -1 -2 463.959 53.0790 6 -10 -1 2 524.941 163.869 18 -10 -1 2 521.895 39.8262 8 -10 1 2 639.379 79.3506 2 10 1 -2 514.276 56.1862 9 10 1 -2 596.577 49.0555 4 10 1 -2 561.789 44.0311 6 -10 1 2 590.532 81.8584 5 9 -1 -2 277.920 35.1100 6 -9 -1 2 256.828 137.055 18 9 -1 -2 215.953 28.4071 5 9 1 -2 292.856 39.4293 4 -9 1 2 317.623 61.3857 5 9 1 -2 279.420 54.6127 9 -9 1 2 293.680 73.2999 2 9 1 -2 193.491 34.7350 6 8 -1 -2 151.465 30.1129 6 -8 -1 2 235.346 127.514 18 8 -1 -2 124.066 28.9496 5 -8 1 2 145.086 51.2354 2 8 1 -2 195.443 31.3848 6 -8 1 2 123.295 51.3878 5 8 1 -2 157.423 42.6107 9 8 1 -2 188.569 40.1874 4 7 -1 -2 749.169 40.1409 6 -7 -1 2 672.871 157.081 18 -7 -1 2 754.522 50.5678 12 7 -1 -2 750.070 37.0724 5 7 1 -2 814.607 53.9706 9 7 1 -2 762.452 39.4910 6 -7 1 2 693.685 67.3985 5 7 1 -2 764.418 43.8791 4 -6 -1 2 757.501 29.8219 13 6 -1 -2 719.072 36.0746 5 -6 -1 2 869.831 125.008 18 -6 -1 2 736.415 28.8853 13 -6 -1 2 836.450 49.8250 12 6 1 -2 746.250 68.2744 17 6 1 -2 753.409 48.1558 9 -6 1 2 763.390 322.091 14 -6 1 2 738.539 70.8342 17 -6 1 2 615.049 112.993 9 6 1 -2 717.178 39.3114 6 5 -1 -2 580.723 170.799 18 -5 -1 2 583.263 31.7096 13 -5 -1 2 572.197 111.062 18 5 -1 -2 608.267 76.1803 17 -5 -1 2 584.458 43.8851 12 -5 -1 2 569.536 29.0370 13 -5 1 2 401.310 110.097 11 -5 1 2 488.149 107.155 9 5 1 -2 714.664 61.4854 17 5 1 -2 547.248 46.9578 9 -5 1 2 636.186 268.405 14 -5 1 2 633.948 56.6656 17 -4 -1 2 1485.43 64.2164 12 -4 -1 2 1541.15 54.7100 13 4 -1 -2 1289.40 166.403 18 4 -1 -2 1527.75 96.3659 17 4 -1 -2 1646.30 81.0955 13 -4 -1 2 1686.66 126.856 18 -4 -1 2 1513.39 87.5728 15 -4 -1 2 1568.28 56.7313 13 4 1 -2 1471.13 68.3683 9 -4 1 2 1516.57 74.7041 17 4 1 -2 1429.42 75.9113 17 -4 1 2 1569.19 289.512 14 -3 -1 2 4122.31 149.373 15 3 -1 -2 4219.53 141.251 15 3 -1 -2 4342.50 153.732 15 3 -1 -2 4239.84 147.621 13 -3 -1 2 4267.99 135.366 13 -3 -1 2 4178.62 136.509 13 3 -1 -2 4095.75 153.553 17 -3 -1 2 4148.23 164.528 18 3 -1 -2 4222.94 140.354 13 3 -1 -2 4379.57 220.185 18 3 1 -2 4166.46 143.531 17 -3 1 2 4379.18 362.604 14 -3 1 2 4355.95 146.232 17 2 -1 -2 1812.19 79.0703 15 -2 -1 2 1921.22 68.3834 13 2 -1 -2 1973.83 76.2987 13 2 -1 -2 1953.00 69.8640 15 2 -1 -2 2042.06 82.2244 17 2 -1 -2 2018.75 69.9885 13 -2 -1 2 2003.65 66.7841 13 -2 -1 2 1716.75 91.5318 17 2 1 -2 1900.77 71.8696 15 2 1 -2 1875.38 73.8091 17 -2 1 2 1987.83 95.7036 15 -2 1 2 2273.58 296.504 14 -2 1 2 1861.29 72.6231 13 2 1 -2 1854.37 88.3915 17 -2 1 2 1955.76 74.5473 15 -2 1 2 1991.03 74.8934 17 -1 -1 2 393.137 28.7820 13 -1 -1 2 385.761 70.7974 17 -1 -1 2 386.496 31.2419 13 1 -1 -2 365.401 23.1275 13 1 -1 -2 376.031 25.9330 15 1 -1 -2 406.857 19.9211 13 -1 -1 2 387.090 29.7730 15 1 -1 -2 404.311 34.0251 15 1 -1 -2 340.004 28.6398 16 1 1 -2 749.194 189.749 14 1 1 -2 391.085 30.4951 17 1 1 -2 400.896 27.9985 15 -1 1 2 421.413 53.4426 15 1 1 -2 324.301 38.7640 13 -1 1 2 297.864 197.075 14 1 1 -2 416.136 34.5085 16 -1 1 2 390.047 51.3230 17 -1 1 2 393.127 30.4291 15 -1 1 2 380.982 32.1032 17 1 1 -2 394.607 59.9211 17 0 -1 2 2442.64 85.1259 13 0 -1 2 2407.85 82.1976 15 0 -1 -2 2382.87 74.2523 15 0 -1 2 2294.94 85.2489 16 0 -1 2 2426.35 83.2856 13 0 -1 2 2234.65 113.165 17 0 -1 -2 2449.92 74.3364 15 0 1 -2 2375.43 88.6946 13 0 1 2 2379.58 78.7039 15 0 1 -2 2327.73 81.9534 15 0 1 -2 2430.00 83.6927 17 0 1 2 2362.02 78.4387 17 0 1 2 1716.74 235.197 14 0 1 2 2514.53 83.1617 15 0 1 2 2296.28 81.1910 17 0 1 -2 2513.66 88.2787 16 0 1 -2 1831.90 246.935 14 1 -1 2 9783.23 311.713 13 1 -1 2 9877.39 310.892 13 1 -1 2 9873.80 309.802 15 1 -1 2 9677.10 312.489 16 1 -1 2 9777.86 311.459 13 1 1 2 9789.99 303.734 16 1 1 2 9942.41 303.771 15 -1 1 -2 9660.43 314.444 16 1 1 2 9772.68 304.609 17 -1 1 -2 9695.35 453.007 14 -1 1 -2 9768.82 309.901 15 -1 1 -2 9878.46 311.085 17 -1 1 -2 9860.03 313.360 13 1 1 2 9752.79 364.453 14 1 1 2 9732.86 303.565 17 2 -1 2 8359.58 271.573 16 2 -1 2 8418.30 266.748 15 2 -1 2 8259.38 268.428 13 2 -1 2 8225.44 296.933 17 -2 1 -2 9160.77 442.543 14 -2 1 -2 7976.00 268.384 17 2 1 2 8695.44 267.001 17 2 1 2 8370.50 260.921 16 -2 1 -2 8067.93 273.252 16 -2 1 -2 8472.18 277.716 13 2 1 2 8078.71 263.846 15 2 1 2 8276.40 260.470 17 -3 -1 -2 883.275 79.3712 18 3 -1 2 864.524 55.5597 16 3 -1 2 800.449 105.440 17 -3 1 -2 1080.88 308.644 14 -3 1 -2 886.739 54.4990 17 3 1 2 867.683 73.8551 17 4 -1 2 509.196 188.714 18 4 -1 2 189.711 74.8592 17 -4 -1 -2 215.597 64.1386 18 4 1 2 242.007 28.6263 9 -4 1 -2 228.241 43.8461 17 4 1 2 238.085 55.8037 17 -4 1 -2 322.459 90.2135 18 -4 1 -2 36.8112 245.196 14 5 -1 2 191.655 44.4784 9 -5 -1 -2 226.839 74.9237 18 5 -1 2 164.882 71.3873 17 -5 1 -2 243.917 57.3820 5 -5 1 -2 213.144 40.4897 8 -5 1 -2 333.760 99.9807 18 -5 1 -2 138.370 270.889 14 5 1 2 237.459 58.4614 17 5 1 2 239.166 31.7056 9 6 -1 2 1019.48 49.7373 6 6 -1 2 924.784 60.1136 9 -6 -1 -2 911.896 109.201 18 6 -1 2 906.887 44.0736 5 -6 1 -2 1097.47 144.540 18 -6 1 -2 1023.57 53.7761 8 6 1 2 941.367 40.1476 6 -6 1 -2 881.517 69.0222 5 6 1 2 964.152 50.0887 9 7 -1 2 158.627 37.2279 6 7 -1 2 211.553 42.9711 9 -7 -1 -2 224.571 94.4193 18 -7 1 -2 315.445 52.6975 5 7 1 2 209.787 31.6571 4 -7 1 -2 163.787 127.926 18 7 1 2 213.062 39.9885 9 7 1 2 174.170 27.0081 6 -7 1 -2 216.365 43.0815 8 8 -1 2 419.396 39.2978 6 8 -1 2 397.179 37.9640 2 -8 -1 -2 450.738 136.523 18 8 -1 2 434.436 54.5128 9 8 1 2 437.876 38.6973 4 -8 1 -2 445.238 49.5498 8 -8 1 -2 244.717 65.9379 2 8 1 2 449.410 34.0809 6 8 1 2 418.176 47.3581 9 -8 1 -2 370.888 70.4492 5 9 -1 2 34.8973 32.6661 6 -9 -1 -2 1.36920 125.962 18 9 -1 2 32.5996 24.4755 2 9 1 2 73.9396 40.7177 9 9 1 2 30.2813 24.6579 6 -9 1 -2 36.4989 21.4732 1 9 1 2 36.6659 23.2647 4 -9 1 -2 33.6498 51.8002 5 -9 1 -2 41.4710 39.4108 8 -10 -1 -2 -9.0516 137.715 18 10 -1 2 84.4823 37.2234 6 10 -1 2 62.1480 29.8755 2 -10 1 -2 65.2443 39.3217 8 10 1 2 28.8062 25.1311 4 -10 1 -2 109.905 27.3298 1 10 1 2 42.2583 29.8916 6 10 1 2 31.3126 45.8922 9 -10 1 -2 63.6454 45.9862 5 10 1 2 32.2512 50.7552 11 11 -1 2 97.7769 36.2369 6 11 -1 2 64.1124 28.3854 2 -11 1 -2 36.4919 28.8296 1 -11 1 -2 53.0220 35.4144 8 11 1 2 73.3061 32.8002 6 11 1 2 54.6106 26.0620 4 12 -1 2 263.423 46.8333 2 12 1 2 253.812 42.9856 4 -12 1 -2 250.394 41.8543 1 12 -2 -2 35.2313 22.4655 1 12 -2 -2 0.86372 27.7958 2 -12 2 2 18.3046 49.1260 2 12 2 -2 35.2734 29.2509 4 11 -2 -2 1254.60 55.0709 1 11 -2 -2 1264.74 59.3605 2 11 -2 -2 1252.29 57.2938 5 11 2 -2 1231.68 66.4460 4 -11 2 2 984.788 106.852 2 11 2 -2 1234.43 59.9344 6 -11 2 2 1103.12 100.748 5 10 -2 -2 333.478 36.3526 1 10 -2 -2 269.946 42.0387 2 10 -2 -2 284.232 37.4418 5 10 2 -2 246.133 39.4932 6 -10 2 2 260.932 67.7372 5 -10 2 2 314.995 64.0297 2 10 2 -2 321.176 56.1131 9 10 2 -2 273.735 45.1327 4 9 -2 -2 518.251 39.9668 5 9 -2 -2 577.307 35.7927 8 9 -2 -2 538.160 42.0929 2 9 -2 -2 530.103 34.8528 1 -9 -2 2 393.084 130.455 18 -9 2 2 541.868 91.9577 5 -9 2 2 494.082 92.2216 2 9 2 -2 590.888 40.6729 6 9 2 -2 527.639 49.1784 4 9 2 -2 538.946 55.0261 9 -8 -2 2 600.878 149.843 18 8 -2 -2 727.215 45.0308 2 8 -2 -2 812.737 39.9131 1 8 -2 -2 794.652 43.5252 5 8 -2 -2 769.997 40.1529 8 -8 2 2 824.413 115.181 6 -8 2 2 873.933 83.7058 2 8 2 -2 733.704 45.7292 6 8 2 -2 836.945 57.5407 9 8 2 -2 869.671 53.6800 4 7 -2 -2 315.397 161.342 18 7 -2 -2 546.086 35.9022 2 7 -2 -2 537.805 35.5178 5 -7 -2 2 576.716 39.0283 3 -7 -2 2 273.161 111.481 18 7 -2 -2 555.995 31.1422 8 7 2 -2 544.010 50.9543 9 7 2 -2 559.492 48.1904 4 -7 2 2 484.029 94.8433 6 -7 2 2 481.027 90.2987 2 -7 2 2 357.623 106.654 9 -6 -2 2 345.788 106.945 18 6 -2 -2 229.830 23.8284 8 -6 -2 2 236.362 32.9545 3 6 -2 -2 185.225 152.232 18 6 -2 -2 272.425 27.6512 5 -6 2 2 254.738 79.2611 6 -6 2 2 324.365 90.9644 4 -6 2 2 341.498 112.469 9 -6 2 2 181.119 81.2461 11 6 2 -2 253.840 45.0577 9 -5 -2 2 608.971 124.032 18 5 -2 -2 540.330 28.0561 8 5 -2 -2 555.110 29.4132 5 5 -2 -2 470.174 146.227 18 -5 2 2 501.301 115.640 4 -5 2 2 639.501 90.4686 6 -5 2 2 688.972 110.585 11 -5 2 2 600.420 110.569 9 5 2 -2 608.482 52.4925 9 -4 -2 2 1114.70 41.9049 10 -4 -2 2 960.561 125.403 18 -4 -2 2 1102.51 54.9204 12 4 -2 -2 833.006 161.073 18 4 -2 -2 1054.42 46.8392 10 4 -2 -2 1035.89 39.7487 5 4 -2 -2 1099.39 39.7346 8 -4 2 2 1224.28 93.4176 6 -4 2 2 1260.35 119.436 11 4 2 -2 1024.96 53.6110 17 4 2 -2 1086.30 69.9517 9 -4 2 2 1120.47 113.779 9 3 -2 -2 427.483 22.0490 8 -3 -2 2 458.895 25.0772 10 3 -2 -2 440.728 31.3875 10 -3 -2 2 468.578 112.078 18 3 -2 -2 578.914 137.190 18 3 -2 -2 428.125 32.4432 13 3 -2 -2 466.203 31.9985 13 -3 2 2 534.745 96.1957 9 3 2 -2 469.290 37.2371 17 -3 2 2 582.171 99.0208 11 -3 2 2 406.221 43.0616 17 -3 2 2 603.815 274.696 14 3 2 -2 421.903 55.0893 9 2 -2 -2 310.660 25.4476 10 -2 -2 2 245.364 21.0685 10 2 -2 -2 262.161 17.0789 8 -2 -2 2 266.529 89.2132 18 2 -2 -2 256.648 111.493 18 2 2 -2 217.210 53.1908 9 -2 2 2 359.776 86.4153 9 -2 2 2 269.221 214.663 14 -2 2 2 432.114 41.2552 17 2 2 -2 242.619 36.0900 17 2 2 -2 200.809 43.5984 11 -2 2 2 199.236 64.6978 11 1 -2 -2 247.279 21.1329 10 -1 -2 2 251.263 22.3158 10 1 -2 -2 215.552 98.1749 18 -1 -2 2 329.502 93.6045 18 -1 -2 2 230.391 18.3042 8 -1 2 2 127.788 201.929 14 -1 2 2 218.076 34.1244 17 1 2 -2 324.730 59.2624 9 -1 2 2 290.089 78.3975 9 1 2 -2 263.414 54.2181 11 1 2 -2 275.899 34.9294 17 -1 2 2 232.515 52.3939 11 0 -2 -2 1586.10 52.1025 10 0 -2 2 1551.34 56.3264 10 0 -2 -2 1493.03 107.438 18 0 -2 2 1619.63 141.633 18 0 -2 2 1464.22 51.6907 8 0 -2 2 1572.04 53.9655 13 0 -2 2 1510.18 53.3948 13 0 2 -2 1329.52 78.2923 11 0 2 2 1799.99 85.7132 9 0 2 -2 1636.48 67.3071 17 0 2 -2 1569.42 84.8662 9 0 2 2 1670.11 58.8218 17 0 2 -2 1491.52 296.866 14 -1 -2 -2 1988.07 61.5282 10 1 -2 2 1930.90 72.4400 13 1 -2 2 1890.59 155.540 18 1 -2 2 1979.01 70.5678 10 1 -2 2 2030.06 65.1198 8 -1 2 -2 1837.41 338.269 14 -1 2 -2 2175.43 103.830 9 -1 2 -2 1973.21 98.9375 11 -1 2 -2 2055.24 79.5253 17 -1 2 -2 1775.35 95.9712 7 2 -2 2 1422.51 60.7818 13 2 -2 2 1359.51 53.4315 10 2 -2 2 1354.27 46.8286 8 2 -2 2 1237.14 169.412 18 -2 2 -2 1246.17 64.8628 17 -2 2 -2 1312.29 308.064 14 -2 2 -2 1189.45 90.5663 11 -2 2 -2 1336.19 94.0298 9 3 -2 2 4705.08 149.597 5 3 -2 2 5126.19 224.668 18 3 -2 2 4821.75 149.588 8 3 -2 2 4696.95 162.116 13 -3 2 -2 4014.50 425.283 14 -3 2 -2 4791.32 171.646 6 -3 2 -2 4042.99 182.129 9 -3 2 -2 5042.49 174.883 11 4 -2 2 591.080 29.9652 8 4 -2 2 573.097 29.7665 5 4 -2 2 896.856 167.390 18 -4 2 -2 518.869 73.1131 6 -4 2 -2 675.575 117.012 4 -4 2 -2 608.749 70.0018 11 -4 2 -2 542.470 87.7566 9 5 -2 2 534.456 30.3864 8 5 -2 2 563.523 30.8168 5 5 -2 2 677.832 168.149 18 -5 2 -2 601.496 91.1807 9 -5 2 -2 533.352 137.500 4 -5 2 -2 495.640 72.3121 6 6 -2 2 148.652 26.9002 8 6 -2 2 186.218 31.6111 2 6 -2 2 142.882 26.1774 5 -6 2 -2 152.124 48.2229 2 -6 2 -2 251.274 58.6866 5 -6 2 -2 151.139 57.2131 6 7 -2 2 468.453 36.5425 5 7 -2 2 427.751 34.5806 2 7 -2 2 416.231 31.0170 1 -7 2 -2 452.025 82.3987 2 -7 2 -2 373.173 73.8570 5 8 -2 2 150.294 34.2870 5 8 -2 2 156.040 23.5028 1 8 -2 2 176.475 33.8532 2 -8 2 -2 162.254 53.8449 2 -8 2 -2 176.619 35.9185 1 -8 2 -2 233.481 63.1346 5 9 -2 2 172.557 34.7834 1 9 -2 2 180.495 32.3086 5 9 -2 2 181.162 28.5916 2 -9 2 -2 91.0565 60.1884 5 9 2 2 162.420 37.1447 4 -9 2 -2 178.903 30.2018 1 -9 2 -2 131.462 54.7416 2 10 -2 2 256.845 34.7304 5 10 -2 2 353.889 45.1086 2 -10 2 -2 313.068 77.5422 2 -10 2 -2 384.883 40.2180 1 -10 2 -2 276.390 65.9257 5 10 2 2 346.835 41.0356 4 11 -2 2 63.1124 28.4767 2 -11 2 -2 23.0717 29.1929 1 11 2 2 69.7920 25.6079 4 11 -3 -2 15.2688 20.4846 1 -11 3 2 11.2320 56.2511 2 10 -3 -2 -22.755 20.5070 1 -10 3 2 7.64433 62.5882 2 10 3 -2 50.5990 30.9991 4 9 -3 -2 587.255 34.9324 1 9 -3 -2 482.856 37.4665 8 9 3 -2 644.294 49.4999 4 -9 3 2 486.051 119.266 6 -9 3 2 618.512 103.874 2 8 -3 -2 1476.98 57.0129 1 8 -3 -2 1529.50 56.8080 8 -8 3 2 1415.97 113.407 2 -8 3 2 1048.45 143.087 9 -8 3 2 1139.92 122.266 6 7 -3 -2 235.088 27.1311 8 7 -3 -2 9.30715 167.307 18 -7 -3 2 299.916 45.4304 3 7 -3 -2 209.835 28.2243 1 -7 3 2 107.847 103.473 9 -7 3 2 214.189 96.6633 4 -7 3 2 174.970 89.3155 6 -6 -3 2 46.2167 26.3156 3 6 -3 -2 -7.9393 160.087 18 6 -3 -2 65.2909 18.6961 8 6 -3 -2 59.9595 16.9336 1 -6 3 2 63.3591 84.9249 6 -6 3 2 72.0204 93.6556 9 -6 3 2 108.595 91.8533 4 -6 3 2 19.3483 86.2548 11 -5 -3 2 242.618 33.8819 3 5 -3 -2 290.215 24.8494 8 5 -3 -2 272.198 31.8982 10 5 -3 -2 53.4632 153.876 18 5 -3 -2 259.352 23.1726 1 -5 -3 2 -29.714 181.639 18 -5 3 2 280.905 99.2879 9 -5 3 2 138.925 86.8213 4 -5 3 2 394.427 95.5947 6 -5 3 2 224.477 89.1892 11 4 -3 -2 235.568 29.7129 10 4 -3 -2 108.331 126.761 18 4 -3 -2 225.175 18.8766 8 -4 -3 2 183.384 37.7621 3 -4 3 2 205.694 82.6466 6 -4 3 2 201.172 86.2725 4 4 3 -2 206.048 54.7861 9 -4 3 2 169.922 103.010 9 -4 3 2 217.841 83.0948 11 3 -3 -2 486.663 31.1410 10 3 -3 -2 391.038 20.7489 8 -3 -3 2 468.937 33.3007 3 3 -3 -2 308.397 136.023 18 -3 -3 2 437.463 23.4683 10 -3 -3 2 455.495 114.998 18 -3 3 2 451.665 105.357 9 -3 3 2 321.876 82.3604 4 3 3 -2 387.552 58.1045 9 -3 3 2 375.451 92.0216 6 -3 3 2 349.182 85.3026 11 2 -3 -2 599.096 153.125 18 2 -3 -2 338.653 25.3093 10 -2 -3 2 311.015 22.9946 10 -2 -3 2 368.771 33.1279 3 -2 -3 2 241.757 99.8576 18 -2 3 2 381.678 83.6756 6 -2 3 2 316.467 73.5287 4 2 3 -2 307.096 54.8653 9 2 3 -2 365.304 70.2127 11 -2 3 2 371.918 89.4861 9 -2 3 2 387.010 92.8046 11 -1 -3 2 2147.87 160.666 18 1 -3 -2 1975.27 67.4513 10 -1 -3 2 2011.37 69.0410 10 1 -3 -2 1763.14 150.955 18 1 3 -2 1891.18 93.7969 4 1 3 -2 2064.24 101.101 9 1 3 -2 1994.10 102.259 11 -1 3 2 1883.44 109.036 9 0 -3 2 989.014 155.214 18 0 -3 -2 954.208 33.9962 10 0 -3 2 976.242 41.3085 10 0 -3 -2 619.485 126.517 18 0 3 -2 1062.53 85.2198 9 0 3 -2 1015.65 71.1582 6 0 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844.945 50.1554 12 5 -1 -3 831.942 169.629 18 -5 -1 3 852.687 44.1059 13 -5 -1 3 947.943 118.634 18 -5 1 3 936.427 65.5172 17 5 1 -3 858.292 56.8370 9 5 1 -3 860.406 61.6250 17 -5 1 3 671.717 291.510 14 -5 1 3 685.964 120.531 11 -5 1 3 626.414 113.890 9 -4 -1 3 3173.75 112.734 12 -4 -1 3 3277.44 109.546 13 -4 -1 3 3450.22 164.700 18 4 -1 -3 3308.06 194.068 18 -4 -1 3 3195.58 110.630 10 4 -1 -3 3312.76 126.014 13 -4 -1 3 3286.37 113.937 13 -4 1 3 3326.02 147.203 11 -4 1 3 2920.67 158.551 9 4 1 -3 3206.16 121.187 9 4 1 -3 3376.90 120.227 17 -4 1 3 3249.53 124.541 17 -4 1 3 2698.37 355.052 14 -4 1 3 3223.07 149.050 15 3 -1 -3 360.858 48.7378 15 -3 -1 3 367.657 111.115 18 -3 -1 3 262.428 54.3153 15 -3 -1 3 310.372 36.7497 12 -3 -1 3 309.291 38.1523 13 3 -1 -3 331.713 119.096 18 3 -1 -3 309.548 53.0153 17 -3 -1 3 308.211 34.7454 13 3 -1 -3 299.595 52.6033 13 -3 1 3 246.926 66.5477 15 -3 1 3 444.829 274.176 14 3 1 -3 332.835 43.1448 17 -3 1 3 323.822 46.3645 17 2 -1 -3 3910.44 131.694 15 2 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30.4486 10 -5 -3 9 122.688 25.9249 1 5 3 -9 111.773 56.6165 4 -5 3 9 181.555 110.615 4 5 3 -9 176.938 47.9426 6 -5 3 9 286.135 130.392 9 -5 3 9 14.0789 98.7592 6 -5 3 9 -100.35 115.195 11 5 3 -9 207.395 79.5511 9 -4 -3 9 215.679 37.8696 3 4 -3 -9 176.139 28.9662 10 -4 -3 9 233.297 32.5118 1 -4 3 9 -2.8323 111.443 9 -4 3 9 112.168 97.4649 4 4 3 -9 176.066 85.7996 9 -4 3 9 81.3626 103.666 11 4 3 -9 104.045 57.0127 4 4 3 -9 271.184 58.6817 6 -4 3 9 211.292 94.2970 6 3 -3 -9 138.509 115.689 18 -3 -3 9 55.7792 26.5423 3 -3 -3 9 35.1055 22.3820 8 -3 -3 9 141.648 235.283 18 3 -3 -9 34.5482 18.7760 10 -3 -3 9 69.2157 20.6718 1 -3 3 9 37.0673 113.062 9 -3 3 9 112.039 85.5382 6 3 3 -9 56.5871 56.8742 4 -3 3 9 49.1773 101.409 11 3 3 -9 14.5915 56.6107 6 3 3 -9 -28.631 87.6998 9 -3 3 9 54.7643 87.4923 4 2 -3 -9 434.263 118.368 18 -2 -3 9 146.380 162.842 18 -2 -3 9 599.855 46.7156 3 -2 -3 9 534.988 35.0989 1 2 -3 -9 459.877 28.0077 10 -2 -3 9 462.167 35.1628 8 -2 3 9 272.912 104.086 11 2 3 -9 381.836 81.8334 4 -2 3 9 416.260 115.179 4 2 3 -9 593.314 79.1211 6 2 3 -9 485.416 114.171 7 -2 3 9 156.008 108.553 9 1 -3 -9 278.712 19.2408 10 -1 -3 9 -52.965 149.000 18 -1 -3 9 309.211 29.9359 8 -1 -3 9 317.071 47.2107 3 -1 -3 9 337.394 33.1059 1 1 3 -9 220.678 84.9421 9 -1 3 9 249.032 69.5396 4 -1 3 9 288.462 95.8169 11 1 3 -9 257.326 89.0436 7 1 3 -9 324.350 81.5527 6 0 -3 9 123.870 30.3598 3 0 -3 9 108.580 22.8646 1 0 -3 9 163.464 29.1164 8 0 3 9 107.596 87.9546 11 0 3 -9 54.1615 85.4504 9 0 3 -9 189.402 86.4269 7 0 3 -9 130.332 46.8618 2 0 3 -9 109.332 62.2797 6 1 -3 9 669.194 40.1159 1 1 -3 9 663.296 48.3590 3 1 -3 9 681.435 39.0719 8 1 -3 9 580.347 42.1865 5 -1 3 -9 708.108 80.5430 6 -1 3 -9 801.633 115.853 7 -1 3 -9 620.761 74.2954 2 2 -3 9 405.486 34.0401 8 2 -3 9 388.294 38.1766 5 2 -3 9 449.614 43.5966 3 2 -3 9 373.784 35.6373 1 -2 3 -9 419.899 95.6266 7 -2 3 -9 375.742 60.6464 2 -2 3 -9 376.038 78.1189 6 3 -3 9 1845.16 67.8371 1 3 -3 9 1663.16 67.7727 8 3 -3 9 1754.49 75.3912 3 3 -3 9 1691.78 68.3327 5 -3 3 -9 1760.71 89.1458 2 4 -3 9 568.678 38.5523 5 4 -3 9 584.374 40.8599 1 -4 3 -9 697.228 68.5173 2 -4 3 -9 480.040 67.9734 5 5 -3 9 174.868 31.9968 1 -5 3 -9 121.393 39.8139 2 -4 -4 9 392.680 45.4244 3 -3 -4 9 104.362 31.4968 3 3 4 -9 -57.394 71.1257 4 -3 4 9 9.23998 145.866 4 -2 -4 9 158.755 36.0598 3 2 4 -9 -13.009 68.7471 4 -1 -4 9 139.499 30.4549 3 0 -4 9 14.6857 38.3860 3 1 -4 9 15.6714 22.4340 1 -1 4 -9 -21.578 54.1066 2 -12 0 10 45.8721 36.9058 1 11 0 -10 814.807 54.6815 5 -11 0 10 924.400 66.9129 1 -11 0 10 1021.79 77.9415 5 -10 0 10 172.437 37.5539 1 -10 0 10 287.664 72.4418 2 -10 0 10 129.129 59.7158 5 10 0 -10 166.713 37.8684 5 -9 0 10 796.508 62.0270 1 9 0 -10 886.516 53.4368 5 -9 0 10 532.229 70.5328 12 -9 0 10 846.303 85.9044 2 -9 0 10 962.315 81.8462 5 8 0 -10 219.548 42.4299 5 8 0 -10 235.869 29.9185 1 -8 0 10 261.946 58.7801 5 -8 0 10 167.810 47.8901 2 -8 0 10 121.484 33.3980 1 -8 0 10 284.277 61.1560 12 7 0 -10 102.908 22.1232 1 7 0 -10 128.827 28.5002 5 -7 0 10 130.118 45.8188 5 -7 0 10 14.9339 43.4264 12 -7 0 10 91.7820 30.7251 1 -7 0 10 90.1289 44.5417 2 6 0 -10 563.751 41.8400 5 6 0 -10 486.737 32.1622 1 -6 0 10 508.717 60.7612 2 -6 0 10 583.824 50.6461 5 5 0 -10 36.4566 26.9972 1 5 0 -10 52.3257 27.3838 5 -5 0 10 45.5423 34.0757 5 -5 0 10 9.71839 74.3336 6 5 0 -10 20.0780 22.2195 8 -5 0 10 47.2439 36.1495 2 -4 0 10 -76.293 75.0595 6 4 0 -10 58.7156 26.6372 5 4 0 -10 74.0198 22.6221 8 -4 0 10 44.0215 34.0614 2 -3 0 10 22.1826 29.8705 2 3 0 -10 76.4011 26.7953 5 -3 0 10 113.827 63.3636 6 3 0 -10 21.0335 109.200 18 3 0 -10 46.1382 23.6136 8 -3 0 10 2.90759 110.644 9 2 0 -10 547.682 136.085 18 2 0 -10 641.482 34.9608 8 -2 0 10 555.842 95.9790 4 -2 0 10 575.585 75.7670 6 2 0 -10 594.509 39.3374 5 -2 0 10 670.201 115.675 9 1 0 -10 84.1098 20.9467 8 -1 0 10 137.811 53.8761 4 -1 0 10 28.1517 56.8638 6 1 0 -10 122.475 101.312 18 1 0 -10 122.688 29.5408 5 -1 0 10 69.4310 88.0629 9 -1 0 10 109.997 83.3843 11 0 0 10 73.6219 83.7783 9 0 0 -10 146.032 25.9852 8 0 0 10 120.721 77.3731 11 0 0 10 158.163 51.0019 6 0 0 -10 95.4680 23.1966 5 0 0 10 163.401 50.3134 4 0 0 -10 43.2142 99.5270 18 -1 0 -10 249.486 24.9697 1 -1 0 -10 228.031 30.7502 8 -1 0 -10 255.486 28.7208 5 1 0 10 123.695 74.0125 11 1 0 10 141.693 80.5176 9 1 0 10 251.136 67.2884 4 1 0 10 303.865 56.4439 6 -1 0 -10 49.1914 86.8651 18 -2 0 -10 10.4949 21.0013 8 2 0 10 -35.918 47.7859 6 -2 0 -10 -12.082 92.4789 18 2 0 10 55.0524 43.4798 4 -2 0 -10 41.7546 16.4513 1 2 0 10 14.0508 71.4668 11 2 0 10 2.16298 75.4798 9 3 0 10 637.918 95.7430 9 -3 0 -10 715.094 35.1655 1 -3 0 -10 715.199 39.7733 8 3 0 10 752.710 72.2500 4 3 0 10 714.709 102.279 11 3 0 10 741.467 68.5570 6 4 0 10 123.944 44.6627 4 -4 0 -10 172.284 29.0405 8 4 0 10 121.103 45.1460 6 4 0 10 68.4553 70.5831 9 -4 0 -10 144.558 25.7977 1 4 0 10 57.7623 64.4828 11 -4 0 -10 128.495 115.195 18 5 0 10 32.5911 69.1301 9 5 0 10 93.1826 45.0406 4 5 0 10 35.5879 63.5696 11 -5 0 -10 60.5067 17.1035 1 -5 0 -10 26.5438 217.082 18 5 0 10 14.9749 43.2174 6 -5 0 -10 35.1181 18.7027 8 6 0 10 321.322 60.2313 6 -6 0 -10 283.698 26.9913 8 6 0 10 162.444 46.9584 4 7 0 10 1121.71 73.7582 6 7 0 10 1067.56 79.3333 4 8 0 10 431.038 108.782 4 12 -1 -10 121.210 24.2618 1 -12 -1 10 112.798 30.5588 1 -12 1 10 103.364 45.6738 2 -12 1 10 52.2818 34.0514 1 11 -1 -10 87.5422 33.5495 5 -11 -1 10 97.1575 37.4494 1 11 -1 -10 96.1798 26.3333 1 -11 1 10 61.2296 38.9815 1 -11 1 10 49.2856 54.1056 2 10 -1 -10 231.660 36.2938 5 10 -1 -10 238.928 33.6292 1 -10 -1 10 238.405 42.0142 1 10 1 -10 199.086 39.9095 6 -10 1 10 109.119 65.2096 5 -10 1 10 112.557 58.5663 2 9 -1 -10 237.677 38.2054 5 9 -1 -10 156.123 34.9236 1 -9 -1 10 256.194 40.7827 1 -9 -1 10 198.900 49.5312 5 9 -1 -10 247.025 35.7657 8 -9 1 10 226.725 59.2352 2 -9 1 10 276.255 66.8455 5 9 1 -10 216.198 42.5141 6 -8 -1 10 198.979 34.1875 1 8 -1 -10 175.253 34.9151 5 8 -1 -10 204.035 33.4071 8 8 -1 -10 175.340 29.1714 1 -8 -1 10 154.799 47.3353 12 -8 -1 10 134.435 47.5006 5 -8 1 10 190.506 55.3489 2 8 1 -10 131.159 35.5513 6 -8 1 10 -66.166 114.459 6 7 -1 -10 63.8951 25.6117 5 -7 -1 10 24.8188 44.3200 12 7 -1 -10 101.437 21.4596 1 -7 -1 10 55.4640 40.3595 5 -7 -1 10 38.3137 28.1222 1 7 -1 -10 89.1459 24.7520 8 -7 -1 10 81.3270 38.7429 2 -7 1 10 123.235 103.531 6 -7 1 10 80.5137 45.2897 2 7 1 -10 66.0885 38.4537 6 -6 -1 10 47.3410 42.7759 12 6 -1 -10 52.6007 118.430 18 -6 -1 10 75.4902 25.8244 8 6 -1 -10 73.7937 21.4399 1 6 -1 -10 71.9241 23.6358 8 -6 -1 10 66.7586 27.7722 1 6 -1 -10 38.9108 22.9946 5 -6 -1 10 86.0556 36.1919 2 -6 -1 10 28.9532 36.8761 5 6 1 -10 -9.1922 33.8033 6 6 1 -10 67.4299 36.0705 5 -6 1 10 86.8789 100.004 6 -6 1 10 15.4341 40.1451 2 -6 1 10 -111.48 119.221 9 -5 -1 10 93.7688 23.6747 1 5 -1 -10 138.920 29.4703 8 5 -1 -10 -15.530 126.807 18 -5 -1 10 96.9286 34.0924 2 -5 -1 10 124.658 33.9324 5 5 -1 -10 112.683 19.0364 1 -5 -1 10 130.516 26.7642 8 5 -1 -10 101.554 21.2486 5 -5 1 10 143.812 89.6604 4 5 1 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50.5236 2 -2 1 10 249.635 110.748 9 -2 1 10 363.688 89.5329 4 2 1 -10 441.371 46.0680 5 1 -1 -10 273.500 107.807 18 -1 -1 10 189.624 36.0120 2 1 -1 -10 215.345 25.7649 8 -1 -1 10 222.142 34.9187 5 -1 1 10 238.435 85.3494 11 1 1 -10 152.718 34.5386 5 -1 1 10 35.3717 95.6898 9 -1 1 10 205.466 59.2839 6 -1 1 10 256.620 76.9694 4 1 1 -10 197.903 41.5952 2 0 -1 10 72.4807 56.0817 6 0 -1 10 21.1738 25.1124 2 0 -1 10 62.4752 25.9306 5 0 -1 -10 20.9094 16.0749 8 0 -1 -10 -47.100 100.327 18 0 1 10 80.3252 73.6485 11 0 1 -10 4.08646 21.4026 8 0 1 -10 43.9393 29.2198 2 0 1 -10 31.7229 17.3167 1 0 1 -10 52.9196 32.2216 5 0 1 10 5.46339 90.3223 9 0 1 10 -38.658 46.9655 6 0 1 10 27.2759 43.4136 4 -1 -1 -10 83.4067 15.5717 8 1 -1 10 92.6879 25.7665 2 1 -1 10 68.3855 50.1803 6 -1 -1 -10 152.744 101.973 18 -1 1 -10 112.178 20.4851 1 1 1 10 64.7895 46.3920 6 -1 1 -10 77.2195 25.9965 8 1 1 10 98.3525 83.7840 9 1 1 10 56.8355 67.1469 11 1 1 10 121.144 42.5854 4 -1 1 -10 104.880 30.6426 2 -1 1 -10 74.6080 33.2695 5 -2 -1 -10 -82.643 83.9714 18 2 -1 10 44.3628 24.9414 2 2 -1 10 53.9204 53.4910 6 -2 1 -10 45.7503 28.1659 8 2 1 10 55.6938 42.4910 6 -2 1 -10 16.5376 36.0448 5 -2 1 -10 51.2482 17.5098 1 2 1 10 84.8998 39.4739 4 2 1 10 -4.8848 63.8294 11 -2 1 -10 45.5324 29.2465 2 2 1 10 104.513 81.7204 9 -3 -1 -10 -38.730 103.366 18 3 -1 10 20.6497 26.9526 2 3 -1 10 28.2693 55.2158 6 3 1 10 28.2807 62.1642 11 3 1 10 67.7552 38.8851 4 3 1 10 66.8923 46.1503 6 3 1 10 83.2821 78.0712 9 -3 1 -10 30.6759 17.1963 1 -3 1 -10 138.590 36.2929 5 -3 1 -10 -4.3351 26.5607 8 4 -1 10 695.201 46.2958 2 4 -1 10 672.515 68.8482 6 -4 1 -10 674.478 52.7228 5 4 1 10 518.366 89.8226 11 4 1 10 728.251 66.3230 4 4 1 10 761.333 94.2496 9 -4 1 -10 756.095 47.6613 8 -4 1 -10 714.046 37.7519 1 4 1 10 706.060 65.1112 6 5 -1 10 573.070 65.8134 6 5 -1 10 474.648 44.3078 2 5 1 10 537.638 91.9022 9 5 1 10 436.200 86.3089 11 -5 1 -10 549.637 31.9255 1 -5 1 -10 439.897 49.4778 5 -5 1 -10 448.498 43.9559 8 5 1 10 475.518 59.1753 6 5 1 10 512.863 63.6473 4 6 -1 10 336.237 47.2333 2 6 -1 10 291.716 68.7855 6 6 1 10 345.884 61.0533 4 6 1 10 269.370 58.4858 6 -6 1 -10 422.241 41.6060 8 -6 1 -10 317.831 30.8681 1 7 -1 10 56.8404 28.9794 2 -7 1 -10 13.1384 18.2155 1 7 1 10 55.9291 39.0122 4 8 -1 10 91.3706 28.6511 2 -8 1 -10 116.679 26.1084 1 -10 -2 10 3.23147 30.7751 1 10 -2 -10 -7.8638 21.1648 1 -10 2 10 95.1211 64.2599 2 9 -2 -10 363.326 32.4067 1 -9 -2 10 326.113 49.6263 1 9 2 -10 386.812 52.7889 6 -9 2 10 189.823 60.8616 2 -9 2 10 190.149 103.820 6 8 -2 -10 58.1093 22.5186 1 -8 -2 10 91.5614 32.5921 1 8 -2 -10 52.1018 20.1213 8 8 2 -10 70.1508 42.8281 6 -8 2 10 90.9090 110.878 6 -8 2 10 29.4121 59.4760 2 7 -2 -10 153.267 29.3993 1 7 -2 -10 171.316 26.2890 8 -7 -2 10 203.846 44.8436 1 -7 2 10 75.6385 108.153 6 7 2 -10 237.672 52.5202 6 7 2 -10 158.660 65.7087 9 -7 2 10 -10.854 126.205 9 -6 -2 10 66.1251 162.120 18 -6 -2 10 178.203 37.6910 3 6 -2 -10 107.295 129.508 18 6 -2 -10 250.461 25.7736 8 -6 -2 10 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44.5476 6 4 2 -10 106.516 73.7891 9 -3 -2 10 108.440 28.1706 3 3 -2 -10 41.2316 104.782 18 3 -2 -10 134.166 30.8924 10 -3 -2 10 174.091 29.8576 8 -3 -2 10 174.097 33.0452 1 -3 -2 10 179.452 38.2560 5 -3 2 10 187.195 76.7480 4 3 2 -10 274.859 58.6280 2 -3 2 10 131.593 116.237 9 3 2 -10 182.149 46.0305 6 -3 2 10 232.230 86.3317 6 -3 2 10 121.015 105.917 11 -2 -2 10 137.485 22.6387 8 -2 -2 10 106.939 21.8950 1 -2 -2 10 184.145 43.4211 2 -2 -2 10 169.470 37.3938 3 -2 -2 10 186.516 38.6484 5 2 -2 -10 121.660 25.1778 10 2 -2 -10 35.8207 108.209 18 2 2 -10 118.303 46.4690 6 -2 2 10 157.724 69.0319 4 -2 2 10 184.208 104.625 11 -2 2 10 47.6746 113.902 9 2 2 -10 252.244 54.9631 2 -2 2 10 143.615 73.4249 6 -1 -2 10 151.700 36.6829 5 1 -2 -10 109.360 24.5784 10 -1 -2 10 75.7773 22.9513 8 -1 -2 10 81.3922 21.3839 1 -1 -2 10 72.7815 27.8693 2 -1 -2 10 50.5871 28.3604 3 1 -2 -10 -8.4471 101.321 18 1 2 -10 35.6960 46.5008 6 -1 2 10 55.7434 56.2855 4 1 2 -10 77.2813 41.5527 5 1 2 -10 104.012 36.0459 2 1 2 -10 120.336 91.4032 7 -1 2 10 -9.2332 89.2259 11 -1 2 10 172.910 110.813 9 -1 2 10 87.8539 64.4700 6 0 -2 -10 406.057 122.355 18 0 -2 10 287.455 29.9691 8 0 -2 10 324.062 40.9753 3 0 -2 10 290.031 31.3485 1 0 -2 10 283.814 35.5820 5 0 -2 -10 213.757 28.2059 10 0 -2 10 277.034 41.2342 2 0 2 -10 337.240 97.0804 7 0 2 10 308.733 106.834 9 0 2 10 208.818 61.0324 6 0 2 -10 218.600 54.3888 2 0 2 -10 326.608 50.3253 5 0 2 10 323.289 73.6296 4 0 2 10 224.746 85.1046 11 1 -2 10 146.026 24.0049 1 1 -2 10 172.610 37.6363 5 -1 -2 -10 158.579 23.6134 10 1 -2 10 113.529 31.1325 3 -1 -2 -10 13.0267 92.3491 18 1 -2 10 121.519 26.3433 2 1 2 10 65.1261 43.9941 4 1 2 10 151.364 74.1694 11 -1 2 -10 239.594 85.2363 7 1 2 10 123.415 93.4440 9 -1 2 -10 136.619 35.4558 2 -1 2 -10 166.089 40.1376 5 2 -2 10 378.554 36.7067 5 2 -2 10 341.160 31.9856 1 -2 -2 -10 63.8429 74.5763 18 2 -2 10 386.424 42.2881 2 -2 2 -10 363.269 56.9222 5 -2 2 -10 460.050 58.3946 2 -2 2 -10 359.728 34.4030 1 2 2 10 342.316 62.1301 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81.3731 6 1 0 -14 54.8177 21.6134 1 -1 0 14 51.7654 37.2851 2 0 0 14 41.8506 35.5260 2 0 0 14 73.2622 79.3271 6 0 0 -14 32.9880 20.5646 1 1 0 14 12.0456 74.7445 6 -1 0 -14 4.60056 19.1984 1 -2 0 -14 31.3110 17.4441 1 -8 -1 14 63.3612 37.2371 1 8 -1 -14 27.4255 21.8405 1 -8 1 14 63.7514 52.7653 2 7 -1 -14 236.638 34.2622 1 -7 -1 14 108.038 34.9410 1 7 1 -14 190.399 37.9619 1 -7 1 14 160.856 55.2269 2 -6 -1 14 297.252 56.1014 5 -6 -1 14 115.206 41.6646 2 -6 -1 14 171.033 33.6251 1 6 -1 -14 251.418 34.4690 1 -6 1 14 321.439 84.7541 2 6 1 -14 219.447 37.9978 1 6 1 -14 227.526 42.8566 5 -6 1 14 247.297 116.484 6 -5 -1 14 84.7160 41.5501 2 5 -1 -14 128.336 28.8397 1 -5 -1 14 42.7008 39.0680 5 -5 -1 14 75.1198 29.5041 1 -5 1 14 94.2615 107.594 6 5 1 -14 101.103 34.1717 5 -5 1 14 52.3347 46.9920 2 5 1 -14 189.421 31.3929 1 4 -1 -14 130.765 30.1745 1 -4 -1 14 221.432 51.5914 5 -4 -1 14 55.5945 33.6723 1 -4 -1 14 141.869 42.2223 2 4 1 -14 125.215 35.7398 5 4 1 -14 103.493 23.3765 1 -4 1 14 189.711 106.430 6 3 -1 -14 128.778 21.5647 1 -3 -1 14 86.1780 36.8356 5 -3 -1 14 100.796 38.6484 2 -3 1 14 185.617 105.208 4 -3 1 14 98.6466 96.1934 6 3 1 -14 197.419 32.0100 1 3 1 -14 191.683 45.0620 5 -2 -1 14 234.880 42.7659 2 -2 -1 14 263.391 51.3426 5 -2 1 14 104.365 86.7255 6 2 1 -14 296.628 36.1631 1 2 1 -14 262.751 44.8054 5 -2 1 14 221.399 88.8282 4 -1 -1 14 -0.3671 36.6909 2 -1 -1 14 -12.107 34.6234 5 -1 1 14 -6.8006 84.1237 6 1 1 -14 49.5397 29.5939 5 1 1 -14 -5.2831 23.0037 1 -1 1 14 112.670 80.9767 4 0 -1 14 216.295 46.2250 3 0 -1 14 197.682 40.2469 2 0 -1 14 231.462 54.5006 5 0 1 -14 157.866 35.8211 5 0 1 14 132.186 80.5002 4 0 1 14 187.128 82.0988 6 0 1 -14 191.014 26.3556 1 1 -1 14 36.4219 33.2941 2 1 -1 14 23.5450 30.1168 3 -1 1 -14 12.7115 21.7373 1 1 1 14 57.6901 71.2702 4 2 -1 14 48.4560 29.8104 2 2 1 14 30.6250 67.4427 4 -2 1 -14 -5.1023 20.4390 1 -6 -2 14 209.969 45.8541 1 -5 -2 14 336.618 43.9574 1 -4 2 14 260.839 114.464 4 -3 -2 14 -7.3190 23.1764 3 -3 -2 14 21.2369 27.4416 1 -3 2 14 112.721 97.2623 4 -2 -2 14 175.401 37.8731 1 -2 -2 14 165.360 42.6569 3 -2 2 14 133.376 86.9967 4 2 2 -14 192.928 37.2957 1 -1 -2 14 354.623 52.7721 2 -1 -2 14 284.064 41.0386 3 -1 2 14 169.911 97.9696 4 1 2 -14 330.990 33.0002 1 0 -2 14 -35.902 30.2725 3 0 -2 14 43.0679 24.6764 1 0 -2 14 14.8483 30.7813 2 0 2 -14 44.6600 22.1363 1 -7 0 15 23.9075 45.1241 2 7 0 -15 29.6034 23.9640 1 6 0 -15 140.885 27.8109 1 -6 0 15 248.787 50.4311 2 5 0 -15 321.704 39.1770 1 -5 0 15 396.988 76.5251 2 4 0 -15 -8.4502 24.5720 1 -4 0 15 -18.570 42.4338 2 3 0 -15 23.5274 23.5650 1 -3 0 15 36.3987 43.6669 2 -2 0 15 575.107 68.7613 2 1 0 -15 178.300 31.2619 1 -1 0 15 117.149 40.1663 2 0 0 -15 685.192 35.8788 1 0 0 15 633.070 62.1851 2 1 0 15 25.5519 38.6102 2 -1 0 -15 -5.9100 19.3123 1 -6 -1 15 -0.6801 38.4674 2 -6 -1 15 15.8486 32.0727 1 6 -1 -15 -3.9169 19.8308 1 -6 1 15 32.9300 49.6241 2 6 1 -15 30.1462 25.1710 1 5 -1 -15 105.245 21.5076 1 -5 -1 15 76.0092 27.2927 1 -5 -1 15 89.7372 40.5372 2 5 1 -15 116.884 25.4751 1 -5 1 15 92.0128 48.7833 2 -4 -1 15 140.356 40.7239 2 4 -1 -15 152.788 27.7154 1 4 1 -15 187.136 34.8999 1 -3 -1 15 595.782 68.7238 2 3 1 -15 637.198 40.6515 1 -2 -1 15 68.1937 39.5576 2 2 1 -15 45.2839 23.7200 1 -1 -1 15 -1.4853 36.2010 2 1 1 -15 45.4195 22.0640 1 0 -1 15 52.8508 34.7117 2 0 1 -15 16.5787 20.6305 1 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.9284 _exptl_absorpt_correction_T_min 0.7845 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54185 13.752 5.059 15.837 90.038 103.308 90.107 ) ; _shelx_hkl_checksum 45622